ML20138P298
| ML20138P298 | |
| Person / Time | |
|---|---|
| Site: | Comanche Peak, 05000000 |
| Issue date: | 08/25/1983 |
| From: | TEXAS UTILITIES ELECTRIC CO. (TU ELECTRIC) |
| To: | |
| Shared Package | |
| ML20138M609 | List:
|
| References | |
| FOIA-85-59 QI-QP-11.4-5, NUDOCS 8511070049 | |
| Download: ML20138P298 (24) | |
Text
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TEXAS UTILITIES GENERATING CO. , '
N SER . REVISION ! PAGE ,
CPSES QI-QP-11.4-5 21 I f 24 i
l08/25/83 i
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INSPECTION OF STEEL .
PREPARED SY:
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- I SUBSTRATE PRIMER I CATE '
I REPAIR AND SEAL AND APPROVED BY: [< n/ '
l FINISH C0AT APPLICATION -
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AND REPAIR
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APPROVED BY: , / j/ 6 J-j
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1.0 REFERENCES
1-A QI -Q P- 11. 4- 1, " Inspection of Steel Substrate Su rf ace Preparation and Primer Application and Repair" i
1-B t CCP-30, " Coating Steel Substrates Inside Reactor Buildings :
and Radiation Areas" '
1-C CCP-30A, " Coating Steel Substrates Inside Reactor Suildings and Radiation Areas" l r
1-0 CP-QP-18.0, " Inspection Reports" i
I 1-E QI-CP-il.4-22, "QC Verification of . Protective Coatings Unique Identification Number Verification" !
i 1-F CP-QP-15.0, " Tagging System" I.
2.0 2.1 GENERAL h
' PURPOSE AND SCOPE '
Tne purpose of this instruction is to cutline metneds j utilized by Quali ty Control personnel in of primer repair and seal ap gsg goat hgtpoepion pp dc repair, and i
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3.0 '
INSTRUCTION hu"N !
Visual inspection of painted surfaces as adcressed by this !
i instruction shall be made at approximately an arms length !
from the surface being inspected. The area of inspection i I
shall be adequately Adequate lighted during the inspection activity.
lighting is defined as the minimum light produced l j by a two (2) cell battery flashlight. I l
l 8511070049 852016 PDR FOIA !
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INSTRUCTION IS E NUMBER REVISION PAGE DATE TEXAS UTILITIES GENERATING CO.
( Ql-QP-11.4-5 2 of 24
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3.1 INSPECTION OF PRIMER
! 3.1.1 Primer Inspections prior to Application of Seal or Finish Coat I'
a) QC shall verify that construction has identified each piece with a unique number in accordance with References 1- A, 1-B and 1-C. The QC Inspector shall maintain a
! Protective Coating Unique Identification Numbe r Log, Attachment 1 for all protective coatings application on l all steel designated for use in the Reactor Sui!1ing.
Subsequent subaivision of coating steel in the field or shop shall be wi tnessed by QC in accordance wi th l Reference 1-E.
i j NOTE:
A. Unique number may be assigned to a lo t d i material to be prime coated at the same time.
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For example, six pieces steel to be coated i
at same time may all have same unique number, 1
- B. Liner plate is excluded from QP numbe rs , f l Equipment which is identi fied with permanent plant l
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identification numbe r need not be identified wi th a Protective Coatings unique identificatinn number.
NOTE: Condui t supports that the unique number is not readily visible will be documented and j
identified in the following manner on the IR:
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- 1) Beginning of the run in the area to be coated by Junction box numbe r, unique elevation, major equipment spin number.
- 2) The conduit identification numbe r.
- 3) The number of supports on the run in !
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the area as defined. The unique number of supports on which it is readily ,
visible.
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- 4) The tennination of the run or the ,
boundary of the area to be coated. I Implementation of this note shall be as directed by the QC Supervisor ano may be l unique fo r di fferent areas of inspection.
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f INSTRUCTION ISSUE V NUMBER REVISION - PAGE TEXAS UTILITIES GENERATING CO. DATE CPSES Ql-QP-11.4-5 21 3 f 24 08/25/83
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b) For all areas of liner plate which do not have adequate documentation, the Inspector shall perfom an Adhesion (patch) test. A calibrated E1cometer 106 Adhesion Tester shall be used to veri fy that the minimum acceptable tensile of adhesion to the steel substrate has been attained. Each test shall consist of three individual dollies tested to failure.
Cri teria : The minimum acceptable strength per dolly shall be 200 psi . If any one of the three dollies should test below the minimum i acceptable strength, tne prime coat shall be removed to the steel substrate over the entire item, c) Verify the primer has cured required amount of time per
- Reference 1-B or 1-C, as applicable.
d) Perfom a visual inspection of the primed surface in i
accordance with the following: ,
.' 1. Runs / sags - A 0FT measurement shall be cade wi th
( the Elcometer DFT gage. Runs / sags 7.0 mils or
! less thick (DFT) which show no evidence of !
mudcracking (See tiOTE) are acceptable. Refer to
! i References 1-B and 1-C for repair of runt / sags l l exceeding 7.0 mils. ;
, i il0TE: Mudcracking is defineo as irregula r ;
cracking as in a dried mud puddle. '
- 2. Dry Spray - Must be removed by screening or abrading before overcoating.
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- 3. Over Spray - Must be removed before overcoating. !
- 4. Contamination Oil and grease - unacceptable t
' Embeaded foreign materials - unacceptable Stains - rust (red) and zinc oxide (white) stains are acceptable provided loose particles are removed prior to application of finish coat.
- 5. Skips / damaged areas / gross discontinuities such as holioays or voids - unacceptable.
e) The inspector shall perfonn a 0FT inspection of the
( cured primer film. A calibrated 0-25 Elcometer
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INSTRUCTION REVISIOg' ISSUE PAGE TEXAS UTILITIES CENERATIN'O CO.
CPSES QI-QP-11.4-5 21 4 f 24 08/25/83 Inspector DFT gage Model III/1E, or equivalent, shall be used. A minimum of five separate spot measurements l (See Note 1) spaced evenly over the structure (See Note 2) shall be taken. Since the magnetic gage is sensitive to geometric discontinuities in the steel, measurements less than 1 inch from the edge or a hole shall be avoided where possible. (See Note 3)
Dry Film Thickness shall be as follows:
i l t1in.(mils) Max. (mils) l' CZ-II spot test 1.5 7.0 l
06 spot test 1.5 5.5 06 average DFT 2.0 5.0 CZ-Il average DFT 2.0 6.0 NOTE 1: A spot measurement is a series of three measurements in the same general area. The probe should be moved a short distance for each gage reading. Discard any unusually hign or low gage reading that cannot be repeated consistently. Take an average of these three gage readings as one spot measurerent.
NOTE 2: For small areas of. coating, 5 separate spot l measurements shall be taken. For larger i
areas, 5 spot measurements shall be taken for every 100 square feet of coating.
NOTE 3: Items with appreciable surface curvature and .
Other geometrical discontinuities, such as !
handrails, gratings, stairs, sway struts, etc., shall be exempt from dry film tnickness '
l measurement per Reference 1-B and 1-C.
3.2 PRIMER REPAIRS 3.2.1 Sags and Runs Over 7.0 flils DFT l Sags and runs over 7.0 mils DFT may be abraded by sanding i or aluminum screening. If surface is acceptable per Section '
3.1, document such on Attachment 3. If surface is unaccept-able refer to Section 3.2.2 or 3.2.3 as applicable.
3.2.2 Primer Touch-up Repair (Primer Damaged to Steel Surface)
The coating inspector shall conduct the fol lowing i l
inspections to document primer touch-up repair operations i when the damage is to the steel surface and spot p m me. i ""
%- y INSTRUCTION ISSUE REVISION PAGE TEXAS UTILITIES GENERATING CO. )
( CMES Ql-QP-11.4-5 ' 5 of 24 j 21 l08/25/83 l
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sandblasting or power tool abrading is required for surface preparation, a) Ambient Conditions The inspector shall detemine air temperature, surface temperature, relative humidity and dew point of substrate
, s tructu res. A calibrated non-mercury filled dry bulb ,
themometer or calibrated temperature recorder (Bristol !
4069TH or equivalent) shall be used for air temperature '
detemination. A calibrated non-mercury wet bulb ;
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! thermometer or a calibrated humidity recorder (Bristol l
! 4069TH or equivalent) shall be used to determine '
relative humidi ty. The dew point shall be determined by the difference in dry and wet bulb tempera tures using the U.S. Department of Commerce Weather Bureau !
Psychometric Tables, WB No. 235. When dry bulb readings i j are grea ter- than 100*F. the dew point should be '
i detemined using the 100'F dry bulb reading, and relative humidi ty shall be detemined by subtracting set bulb from the surface tempera ture or ambient ;
j tempe ratu re, whicheve r is greater. If the dry bulb ~
t themometer exceeds 100 F, the instrument shall be !
l retu rned to the calibration lab fo r recalibration. ,
The surface temperature snall be detemined by placing a calibrated surface tempe ra tu re thermome ter (0mega-Amprobe fast temp. range of 10 -250 F) in contact with the substrate surface until the temperatu re reading stabilizes.
', Final surface preparation shall not begin unless the tempera ture of the surface is a minimum of 5 above the dew point.
Nomal condi tions of ambient and surface temperature (
for application of primer shall be as follows:
Ambient Temp. ( F) Surface Temp. (*F) '
l Dimetcote 6 40-120 40-130 Carbozinc 11 40-95 40-110 In no case shall Carboline and Aceron limits be exceeded (0*-130*F ambient and 0*-200*F surface temperatures).
Coating ma terial (if thinned) shall be thinned in l accordance with Reference 1-B or 1-C. I Humidi t$haMlues may vary from 10% to 95%; however, primer !
not be applied to a wet or damp surface.
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i INSTRUCTION ISSUE REVISION PAGE TEXAS UTILITIES GENERATING CO.
j CPSES QI-QP-11.4-5 21 08/25/83 6 of 24 l A
I The surface temperature shall be a minimum of 5* above the dew point.
i b) Verify abrasive acceptablility (if used) by obtaining a sample of the abrasive to be used. The abrasive shall
, be verified to be dry by feel with no grease, oil or !
deleterious materials. Particle size must be sufficient l to achieve a minimum of 1 mil surface profile. '
c) Veri fy acceptabili ty of blast cleaning equipment (if used) prior to use by-1
- 1. Verifying that water separators are installed in j the air supply system and that separators have i
been drained of accumulated water and drains lef t i partially open. i
- 2. Air supply contamination shall be checked at the I nozzle prior to use by exposing a sheet of white 7-paper or cloth to the blast of air (no sand) for approximately 30 seconds. The paper or cloth shall be examined fo r evidence of contamination (oil, water, foreign matter, etc.). No evidence of contamination is acceptable.
j d) Verify that the blasted or power to' l ed surface has i been brushed or vacuumed to the extent requi red for j final surface inspection. The adjacent areas shall be
, cleaned to the extent necessary to avoid contamination l during subsequent coating applications. l e) Veri fy acceptabili ty of the blast cleaned or power tooled surfaces oy performing the following inspections:
- 1. Absence of Foreign Matter -- A visual inspection shall be performed to determine that all oil and grease, dirt, millscale, rust, corrosion products, l oxides, paint or other foreign matter have been .
I completely removed from the surface except for i light shadows, very slight streaks or slight !
discolorations caused by rust stains, mill scale, oxides, or slight, tight residues of paint or .
j coating that may remain.' At least 95 percent of !
each square inch of surface area shall be free of all residues, and the remainder shall be limited ,
to light discolorations as mentioned above. '
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NOTE: If coating removal is required from an area or item which has been coated in room u s mco oA
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t INSTRUCTION s REVISION ISSUE NUMEER PAGE l TEXAS UTILITIES GENERATING CO. DATE CPSES QI-QP-11.4-5 21 7 of 24 08/25/83
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accordance with this instruction, shadows or tight residues of primer wnich may remain in the profile of the previously prepared substrate is acceptable.
- 2. Removal of Sharp Projections -- A reinspection for sharp projections that were not Diended (rounded) during blast cleaning or power tooling shall be perfomed.
Weld splatter on structural steel shall be removed .
by either grinding or sand blasting. However, if i the weld splatter should remain after the above f
, operation, the weld splatter will be acceptable.
Sharp projections are not acceptable.
Protrusions and peaks shall be ground to a rounded contour.
I NOTE: Any mechanical surface preparation other i than sandblasting or hand or power ,
( tooling of sharp edges or weld spatter '
will require a visual welding inspector's acceptance of the work perfomed.
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- 3. Anchor Pattern Depth -- The anchor pattern depth i of the blasted surface shall be inspected at random i
locations using a Keane-Tatar Surface Profile Comparator (model 373) or equivalent.
The anchor pattern depth for a blasted surface shall be a minimum of 1.0 mils. !
Surfaces that have been power tooled with "3M l Clean-N-Strip", 80 grit or coarser " flapper wheels",
sanding discs, " roto peans" or equivalent provide acceptable surface profile.
No maximum profile will be specified, providing I
that correct millage and su rface uni formi ty requirements- can be obtained after primer l application.
f) Veri fy applicatar quali fications per Section 3.3.1.
g) Veri fy air supply acceptabili ty per Section 3.3.4.
( h) 1. Coating Materials Identification The inspector shall inspect the coating material containers prior to mixing contents for product
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INSTRUCTION '
(.O REVISION (' . ' ISSUE NUMBER -
DATE PAGE TEXAS UTILITIES GENERATING CO.
QI-QP-11.4-5 8 of 24 21 03/25/83 i
identification and verify that all materials are correct for coating application.
Approved materials are: !
I CZ-11 Dimetcote l Carbo Zinc base (gray or green) Dimetcote 6 base Carbo Zinc filler Dimetcote filler Carboline #21 or 33 Thinner Amercoat #65 or 101 !
Thinner !
I He shall also verify that each component container I is identified by batch number and that the shel f life has not expired. Carbo Zinc 11 base has a shelf life of 12 months. Carbo Zinc filler and Dimetcote 6 base and filler have a shelf life of 24 months.
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- 2. Mixing Operations i i
An inspector shall witness each mixing / thinning l opera tion. The inspector shall verify that mixing
( operations are perfomed in accordance wi th i Reference 1-A and 1-8.
- 3. Thinning Operation l An inspector shall veri fy that primer thinning j i
complies with thinning requirements established i in References 1-A and 1-B. t
- 4. coating materials, are When mixed / thinned in locations other than the field, the ins pector verifying the mixing operation shall fill out the Paint Mixing Slip, Attachment 5. The inspector perfoming the pre-application inspection shall record the infomation from the Paint Mixing Slip on the Inspection Report, Attachment 3. The Paint Mixing Slip need not be retained.
f i) Verify that primer is applied and pot life is not exceeced in accordance with Reference 1-B and 1-C. If a brush technique is used, the inspector shall verify that a short bristle brush is used and rebrushing is I avoided.
j) Verify that hose length is less than 75 feet.
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\ g- INSTRUCTION ISSUE NUMBER RWISIO PACE TEXAS UTILITIES GENERATING CO. DATE QI-QP-11.4-5 21 08/25/83 l
3.2.3 Primer Touch-up Repair (Primer Damace Does Not Extend to Steel Surface The coating inspector shall conduct the following inspections for primer touch-up repair operations when the damage is wi thin the primer coat and sandblasting to the steel substrate is not required.
a) Verify surface is abraded lightly then wiped clean per Reference 1-B and 1-C.
g b) Perfom inspections (e) through (j) in paragraph 3.2.2.
i l '3.2.4 Repair of Primer by Recoating The coating inspector shall conduct tne fol lowing inspections for primer recoating repair. Only two (2) overcoats shall be applied.
a) Verify that the surface has been solvent cleaned or !
cleansed in accordance with Reference 1-B and 1-C. A l
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clean white cloth shall be used to check primed surface cleanliness. Contamination, otner than rust (red) and i l
zinc oxide (white) stains, is unacceptable and require
- l further cleaning. !
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b) Perfom inspections (e) througn (j) in Section 3.2.2. ,
! I c) Minor defects (mechanical damage such as construction l damage or exposing substrate during surface preparation operation!, etc.) perfom inspection (a) through (c) in Section 3.7.2.
I e d) Major defects (mechanical damage such as construction i
l damage or exposing substrate during surface preparation l operations, etc.) perfom inspection (a) through (c) in l Section 3.7.3.
3.2.5 Complete Primer Repair (Primer Damace to Steel Surface !
i t Extends Over Entire Item)
The coating inspector shall conduct the following inspections
' to document primer repair when the damage is to the steel surface and requires surface preparation to steel substrate over entire item:
I a) Verify ambient conditions per Section 3.2.2(a) prior to surface preparation.
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i INSTRUCTION I ISSUE NUMBER REVISION. PAGE
' TEXAS UTILITIES GENERATING CO. DATE CPSES ,
l QI-QP-11.4-5 21 08/25/83 10 of 24 I
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b) Perfom inspections (a) through (j) in Section 3.2.2. j 3.2.6 Documentation of Primer Repair Inspections I I
All inspections required by Section 3.2 shall be documented I on an IR, Attachment 3, in accordance with Reference 1-0.
The completed IR shall be forwarded to the PPRV for retention.
NOTE 1: If the repair is on an item which is fabricated out of several pieces of steel bearing different l
t QP numbers, all QP numbers will be recorded in
, the "Renarks" section of the IR.
l l NOTE 2: All items within the scope of each inspection which are detemined by the Ins pector to be satisfactory may be documented on a single IR.
i NOTE 3: A reject tag will be applied to any unsat area, with the inspection report, inspector's name and phone extension listed per Reference 1-F.
3.3 PRE-APPLICATION INSPECTIONS :
i The QC inspector shall verify the following items prior to ;
applying coatings:
l 3.3.1 Coatina Applicator Qualifications '
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I' The Inspector shall verify (by Qualification Record or list [
of quali fica tion records in QA File) that the coating I dpplicators on each shift are qualified for safety-related ,
l coating work.
- 3.3.2 Anbient Conditions The inspector shall detemine air tempe ratu re, su rface tempera ture, relative humidity and dew point of substrate structures. A calibrated non-me rcury filled dry tsul b thermometer or calibrated temperature recorder (Bristol 4069TH or equivalent) shal l be used for air temperature j i detemination. A calibrated non-mercury wet bulb thennometer or a calibrated humidi ty recorder (Bristol 4069TH or equivalent) shall be used to determine relative humidi ty. The dew point shall be detemined by the difference in dry and wet bulb temperatures using the U.S.
l Department of Commerce Weather Bureau Psychometric Tables, j WB No. 235. When dry bulb readings are greater than 100*F, j
( the dew point should be detemined using the 100*F dry bulb ;
reading, and relative humidi ty shall be determined by subtracting wet bulb from the surface temperature or ambient
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($ INSTRUCTION l REVISION ' ISSUE PAGE NUMBER DATE
, TEXAS UTILITIES GENERATING CO.
QI-QP-1;.4-5 11 of 24 l 21 08/25/83 temperatu re, whichever is greater. If the dry bulb thermometer exceeds 100 F, the instrument shall be returned to the calibration lab for recalibration. The surface tempera ture shall be determined by placing a calibrated surface temperature thermometer (0mega-Amprobe fast temp.
range of 10 -250*F) in contact with the substrate surface until the temperature reading stabilizes.
The pennissible range of surface and ambient temperature for application of finish coat shall be 50-120*F.
I Maximum values of relative humidity shall be 85%.
The surface temperature shall be a minimum of 5 F above the dew point.
3.3.3 Coated Surface Acceptabili ty i
The Inspector shall visually reinspect the previously coated I surface just prior to finish coat application for evidence of '
contamination (oil, grease, fo reign ma tter) and stains. '
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Contamination is unacceptable. All contamination must be j removed per Reference 1-B or 1-C prior to finish coating. i Rust (red) and zinc oxide (white) stains are acceptable i provided all loose particles have been removed (as evidenced
, by existence of no stain on cloth) from the coated surface :
! by approved cleaning operations. Phenoline Thinner or Xylol i are approved cleaners for seal coat. Thinner wiping is not !
j recommended for Dimetcoat primer. Use Carboline #33 cleaner :
for CZ11 Primer. '
3.3.4 Air Supply Acceotabili ty 1
The Inspector shall inspect the air supply system (pressure i pots and spray guns) for the existence of suitable filters /
traps / separators.
The effectiveness of these items shall be verified by placing a clean piece of cheesecloth (or white fabric) over the exit of the air lines and allowing air to flow for 30 seconds minimum. The cloth shall show no evidence of moisture, oil or foreign matter when examined.
3.3.5 Finish Coat Mixing Operations 3.3.5.1 Prior to mixing, the inspector shall verify that each component is identi fied by batch numbers and that the 24 month shelf life has not been exceeded.
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a INSTRUCTION ISSUE REVISION PAGE TEXAS UTILITIES GENERATING CO. l DATE CPSES i .
QI-QP-11.4-5 i i 12 of 24 l 21
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I' 3.3.5.2 The inspector shall veri fy that mixing / thinner operations are performed in accordance with References 1-B and 1-C.
Thinning may be done up to two quarts of Phenoline Thinner per gallon of Phenoline 305.
3.3.5.3 The inspector shall verify that the pot life has not expired j per References 1-B and 1-C.
3.3.5.4 When coating materials are mixed /tninnec in locations other j than the field, the inspector verifying the mixing operation shall fill out the Paint Mixing $ lip, Attachme nt 5. The !
inspector perfoming the pre-applicatian inspection shall
, record the infomation from the Paint Mixing Slip on the l
! Inspection Report, Attachment 1. The Paint Mixing Slip need l not be retained.
. 3.4 SURVEILLANCE OF SEAL OR FINISH C0AT APPLICATION The Inspector shall verify that hose length is less than 75 feet. If a brush technique is used, the inspector shall verify that a short bristle brush is used and rebrushing is avoided. :
- The inspector shall alsn ve ri fy that the seal coat (if i present) is solvent wiped with Phenoline 305 thinner or Xylol prior to finish coa *. application. ;
3.5 DOCUMENTATION OF PRI!1ER INSPECTION AND FINISH C0AT !
PRE-APPLICATION /APPLICATICN INSPECTIONS 1
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Results of inspections described in Sections 3.1, 3.3, and ;
3.4 shall be documented on an Inspection Report (IR), i Attachment 1, in accordance with Reference 1-D. The completed IR shall be forwarded to tne PPRV for retention, i NOTE 1: All items within the scope of each inspection I which are detemined by the Inspector to be satisfactory may be documented on a single ,
IR. :
l f 3.6 FINISH C0AT FINAL ACCEPTANCE INSPECTION l The inspector shall perfonn a final acceptance inspection of each finish coated item in accordance with Paragraphs .
3.6.1 through 3.6.5. For finish coated containment liner i plate su rfaces, the final acceptance inspection shall be '
performed at the completion of the curing period. For all i other finish coated items, the final acceptance inspection i
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g h ,,\ INSTRUCTION RESIONs .
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' ISSUE NUMBER DATE PA2E
' TEXAS UTILITIES GENERATING CO.
CPSES QI-QP-11.4-5 21
( 08/25/83 13 of 24 shall be perfomed immediately prior to turnover of each area within the containment building and should be coordinated with Area Management. In addi tion, finish coated containment liner surfaces shall be visually reinspected in accordance with Paragraph 3.6.2 immediately prior to turnover of each containment area.
3.6.1 Finish Coat Cure The QC Inspector may perfom a final acceptance inspection after a minimum topcoat cure of 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> or minimum cure for recoat as stated in Reference 1-B or 1-C, Section 4.4.21 Paragraph 4, which ever is greater. A calibrated non-mercury filled dry bulb thermometer, a calibrated temperature recorder, or local weather station may be used.
3.6.2 Visual Defects Inscettion The Inspector shall perfom a visual inspection of the cured finish coated substrate surface in accordance with the following:
k a) Runs / sags - Runs or sags in which the DFT of the total coating system is 15.0 mils or less thick, which show no evidence of mudcracking, are acceptable. Those i greater than 15.0 mils shall be repaired in accordance '
with Reference 1-B or 1-C.
b) Skips / damaged areas / dry spray / over spray / gross ~
discontinuities such as holidays, voids, and bubbles are not acceptable. ,
c) Pinholes -
acceptable to the extent allowed by Attachment 2.
d) Contamination - Embedded foreign materials unacceptable.
3.6.3 Dry Film Thickness (DFT)
The system.
Inspector shall perfom a DFT of the cured coating A calibrated 0-25 Elcometer Inspector DFT Gage Model III/1E, or equivalent, shall be used. A mir.imum of five separate spot measurements (See Note 1) spaced evenly over the structure (See Note 2) shall be taken. Since the magnetic gage is sensitive to geometric discontinuities in the steel, measurements less than 1 inch from an edge or a hole shall be avoided where possible, k
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bh TEXAS UTILITIES GENERATING CO.
IN R ON REVISIO i PAGE QI-QP-11.4-5 21 08/25/83 The average DFT of the total coating system shall be a minimum of 6.0 mils and a maximum of 13.0 mils. The spot test DFT of the total coating system shall be a minimum of 6.0 mils and a maximum of 15.0 mils.
The finish coated system shall exhibi t full " hiding" properties of the primecoat.
NOTE 1: A spot measurement is a series of three measure-ments in the same general area. The probe should '
be moved a short distance for each gage reading.
Discard any unusually high or low gage reading that cannot be repeated consistently. Take an average of these three gage readings as one spot measu rement.
NOTE 2: For small areas of coating , 5 separate spot measurements shall be taken. For larger areas, 5 spot measurements shall be taken for every 100 square feet of co ting.
( NOTE 3: Items with appreciable surface curvature and other geometrical discontinuities such as handrails, gratings, stairs, sway struts; etc. shall be exempt 1
from DFT measurement (See DCA 11421).
NOTE 4: PCR's from previous DFT inspections that are satisfactory per current requirements of DCA 12145 R.3, do not require additional DFT inspections
- provided no additional coatings have been applied to the area.
3.6.4 Continuity Inspection The Inspector shall test the continuity of the cured finish coat using a Tinker and Rasor Model M1 (67.5 volt) holiday detector. 100% of the finish coated surface area shall be tested.
The applied film should contain only a minor ntsnber of points of discontinui ty. No more than two points of discontinuity should occur within an area having a radius of 6 inches as measured from a point of discontinui ty (pinholes). No more than 40% of the total number _of i
allowable points of discontinuity should occur within any one area equal to 25% of the total area being coated. The total number of pinhole discontinuities allowed is defined
{ in Attachnent 2. No gross discontinuities are allowed.
3.6.5 Documentation of Finish Coat / Seal Coat Acceptance Inspections Results of inspections described in Sections 3.6 shall be documented on an Inspection Report (IR) Attachment 4. in
" m , 'l CsW INSTRUCTION . '-
1 NUMBER REVISIO ' 0 PACE
' TEXAS UTluTIES GENERATING CO.
. 21 08/25/83 15 of 24
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accordance with Reference 1-D. The completed IR shall be forwarded to the PPRV for retention.
NOTE 1: All items wi thin the scope of each inspection per Paragraph 3.6, which are determined by the Inspector to be satisfactory, may be documented on a single IR.
NOTE 2: A reject tag will be applied to any unsat area, with the inspection report, inspector's name and phone extension listed per Reference 1-F.
3.7 REPAIRS OF FINISH C0AT 3.7.1 Repairs of Runs and Sags The QC inspector shall verify that the area is abraded until the DFT of the total coating system is within 6.0 and 15.0 mils, and examined for mudcracking.
Tne presence or absence of mudcracking shall dictate the type of repair required per Reference 1-B or 1-C.
3.7.2 Repair of Minor Defects The QC inspector shall perfonn the following inspection when repairing minor defects (as defined by Reference 1-B or 1-C):
a) Verify ambient conditions per Section 3.2.2(a) prior to surface preparation, b) Verify that the damaged area'*is blasted or abraded and any exposed steel is ground per Reference 1-B or 1-C.
c) Verify damaged area is solvent wiped in accordance with Reference 1-B or 1-C.
d) Perfonn inspections described in 3.3.1, 3.3.2, 3.3.3, 3.3.4, 3.3.5, and 3.4 3.7.3 Repair of Major Defects The QC inspector shall perfonn the following inspection when repairing major defects (as defined by Reference 1-B or 1-C):
a) Verify ambient conditions per Section 3.2.2(a) prior to surface preparation.
('-
b) Verify area is abraded or spot blasted per Reference 1-B or 1-C.
penn me,t Tuoco oA
-- INSTRUCTION q[
NUMBER REVISIOf6id PAGE
. TEXAS UTILITIES GENERATIN CO.
CPSES QI-QP-11.4-5 16 of 24
, 21 08/25/83
(
c) Perfom inspections in Section 3.2.2.
d) Perfom inspections in Section 3.7.2(c).
3.7.4 Repair of Embedded Foreign Particles The QC inspector shall veri fy that embedded foreign particles are removed and the surface recoated per Section 3.7.5.
3.7.5 Repair of Pinholes and Discontinuities, Over Spray, Dry Spray ,
and/or Overcoating i a) Verify all loose particles are removed and area is solvent wiped.
b) Perfom inspections described in 3.7.2, except pinholes and small dicontinuities may be repaired at the time of final inspection wi thout a later i reinspection of the repair.
3.7.6 Documentation of Repairs l All repairs shall be documented on an Inspection Report, Attachment 1. Repairs involving application of primer will be documented on Attachment 3. l I
3.8 MAPPING OF LARGE AREAS For large areas (such as reactor containment liner plate) which have received coatings prior to 10/23/81 (Issuance date of Rev. 5 of this procedure), a unique number shall be assigned to the original inspection checklist. This number '
will be transferred to the area on a map drawing to provide traceabili ty to the original checklist. For any coatings applied af ter 10/23/81, the IR number shall be transferred to the area on the map drawing.
The map drawing shall be maintained by the QC Supervisor, or his designee, until the entire surface has been coated.
At this time, the completed map shall be transmitted to the Pemanent Plant Records Vault.
NOTE 1: Separate maps shall be maintained for the prime, seal and finish coats.
NOTE 2: If the coated area applicable to a given IR is irregular in shape, a sketch should be attached to penn no.1 Tuoco CA
(,Q.,^ INSTRUCTION REVISIOd : ISSUE BER DATE PAGE
- TEXAS UTILITIES GENERATING CO.
CPSES QI-QP-11.4-5 17 of 24
( 21 08/25/83 the IR to indicate the extent of the area inspected.
NOTE 3: Coating repairs requi ring recoating shall be mapped, but repairs only requiring touch-up need not be mapped.
NOTE 4: The following parameters (as necessary) should be considered for description of areas on the sketch:
a) Bottom and top elevations (vertical and diagonal surfaces) or elevation of su rfac'e (horizontal surfaces),
b) Dimersions in relationship to azimuths, column lines, reactor centerline or other corranents of known location.
c) Quadrant, compa rtment, cavi ty or room in which inspection is located.
d) Unit number.
( e) Relation of su rf ace to cardinal directions f (i .e. , North, Sou th, e tc.-) .
I r
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f;.
w no. s moco oA
l r
(.
% ~ M. . k.
INSTRUCTION REVISION ISSUE NUMBER DATE PAGE TEXAS UTIUTIES GENERATING CO.
I CPSES QI-QP-11.4-5 21 08/25/83 18 of 24 ATTACHMENT 1 1
01-CP-11.4 5 Rev. ,, ,
CI"awTto'n Dc4NM** OTUI$cy O F7ha, CPjeg, ,
l "
, .nsa. an. sui.rs q C inyec ion ecueutres , au. aseucasts artma sartsracrony gvft3 Qk,g l
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I O iasacerio= co atz us. uasariwacroav irine ustus sno k,T7 ~ ,
artm act W - ! ge
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2 . 5 ,3
, l 5EAL C0AT F INI5ti CGAi l 'l l l l ORIGINAL REPAIR I Ii 1 j 1. I RECORD ALL PROCIECIlvE COATINGS UNIQUE QP & 10 ND.'s: i ji l
, I (FCR wuLTIPLE ITEMS INDICATE IN " REMARKS WITH .
l' l l l 1 CORRESPONDING OFT READINGS rp0M ITEM 43 ABOVE.) Pro l ll i l
I lPADA. 3.1,1.3 IIl l
! t lyrstry cotuto ener ero DSDA 1 1 13 l l I I I 3. I PERFORM VISUAL INSPECTICN CF PR! PED SURFACE PER PARA. l l l l l3.1.1.d i li l 4_ l otoreow nrT or poturo cqAT pro pgoA 1 ! t . t re o l l l l l MULTIPLE ITEMS If4DICATE MIN. SPOT. MAX. SPOT AND AVER- t l l l ;
iAGE OFT FOR EACH ITEM IN 'PEMARK5") I l 1 l l
- 5. ! PERFORM VISUAL INSPECTIONS Cr paEv100 SLY COATED SURFACEI Ii i I PER PADA. 3.3.3 lI l !
4 yrgf rv enprArr pgnpac AoffmM Serrpvan' t Dro PrD19 me I I I I CCP30A l l l (
- 7. AM8!ENT CONDITIONS CHECKED PER PARA. 3.3.2 PO!CR TO i i i l lC0ATING ApptfCATICN I I I l l RECORD: l l l l lCATE: IINE: W.O. I i j i l 0.8 5.T. D.P. R.H. l l l 6 l l l l (CONT!!iUED nN SHEET 2 of 2) l l l assaans ones, specs, ettJ
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l[ggggg 8 L"l '
slGN4DJ,6 OC me M CrCA g
- 9) 8 l
Penn No.1
, L L u, s. 6.e.
INSTRUCTION ISSUE REVISION PAGE TEXAS UTILITIES GENERATING CO. DAM
(- CPSES i
, QI-QP-11.4-5 21 08/25/83 f19of24 ATTACHMENT 1 (CONTINUED)
COMANCHE PEAM STEAM ELECTRIC $TATtCN INSPECTION REPORT QI-QP-II.4-5,R.
(St.99 D8 ENTAL ) Eheet 2 0f 2 FCR FULL HEADING 5. SEE SbEET 1 .40 .
'"2 IN$r"ECTICN ATTRISuTES :
1 Th
. , .i m .e
- 8. IVErilf f OiJALIFICATION OF APPL!CATOR($) PEG DADA 3.3.1.
- I I I
! ILIST: I I I I i t i I l l l 6 I i
- 9. iAPPt[ CAT 10ri METHOD: ' ' ' I iSFRAY BRUSH i 6 8 6
- 11. IVERIFV HOSE LENGTH IS LESS THAN 75 FT. 8 I ' 4
- 12. IVERIFV MIXfNG OPERATIONS ARE PER CCP-30 CR CCP-30A AND I 8 i i IPARA. 3.3.5. I I I i l 13. ICCATING MATEDfA! DD9fc' IOrNTf Ff rATinal- I i i f *
/ l 'DECODS EATCW Y!"9FDE- ' ' 8 I
( I IPART 4: I ' I i 1 inar e i ' i i 6 THINNER: ' I i l f li!"E M11ED- I I I CATE: I I 14 IVERIFV POT LIFE AS STATED IN CCP-30 AND CCP-30A IS NOT EX-t 4 i i I
ICEECED PER PARA. 3.3.5 2. I I ' I I i 6 6 I i ! im% t I a@I 'h p _I i .#W &lMOM f MT F WYi i i ~l'A' I I i l 1
' l I I i 1 i I e i e 6 4 l l l t t l ROIARM38 (mset,SMC2,KTCJ j
NAN *C8 **
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4
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INSTRUCTION ISSUE NUMBER REVISION PAGE TEXAS UTILITIES GENERATING CO. DATE t
CPSES '
[ QI-QP-11.4-5 08/25/83 20 of 24 21 I
Attachment 2 '
l i
TOTAL NUMBER OF ALLOWABLE POINTS OF DISCONTINUITY
{
SURFACE AREA COND. "C" BEING C0ATED COMMERCIALLY (50. FT.) CONTINUOUS 10 5 10-50 10 (i 50-100 20-l 100-500 30 '
500-1000 50 1000-5000 75 l
. cross Oiscon:inut tes - rione 4110 .e, l I
4 c.m **** ^
(s 1
3 INSTRUCTION NUMBER l REVISION 0 PAGE g
c TEXAS UTIUTIES GENERATING CO.
CPSES t QI-QP-11.4-5 l 21 08/25/83 21 M 24 ATTACHMErlT 3 ceutscsc nrx s Ew z.r:ra.: s .n:~
? e r* re IN37EC T:CN SEPCRT x
- c 4* = , :Eci; a .. .e n
- i *.: 44 .6 a ci
. I4P CTEM,IVE :COATIMS .. . .
vus n. ,4u . ::: a a s , s . ,4:. 2 .; e.4 . .. n.> .t. u i AS-31 d d 01-0P-11..:-5. Rev _ - ,
I- =c: ss du vs
- se v ca.g.ar;
- = F3ss.c := -w -pat ts-l .=ssit: := -
.:s ssss: := .sss- : ws: ei .
asoeu.cs q C aset: := ::ma.t t3, u asscasst artws $2rsra !:a* p K. Q C '8M ?:= :: watt *t:. .nsar srac?:ev ,'twe Ls t: s c.:. J t
- .ggir
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Ns;f:7.CN AT*918UTE3 gA ' ~
-l
- 2:
j , f :A?!I siciar.at ,
- 1. I For reeair of sacs and runs ever 5.5 mits ter, e,rer. I i ' : 4
- 0FT of Primer Coat in aress whicn nave been sanded or 1 6 i i screecea per Para. 3.2.1. (For mul tiple i ter's, inoicate l > '
I
[ Min. Scot. Max. Spot anc Average CFT witn arres:cedica l I
( l 1 GP & ID No's for each item in " Remarks.") I !
l l RECORD: Mini-.". Scot Test: ' ' l l i Maximum Scot Test: I I ! i l Average CFT: 1 i i f I 2. 8 Abrasive acceotable eer Para. 3.2.2.t,. 4 : i l i l
l 3. Secaraters installed. draieed, and drains lef t ! I l l i cartially ccen. '
i I f I l 4 Air succly free of conta tiratten. 8 i + t l
l 5. Blasted Or Doweratooled surface ard trefi?e- i l i i f
l l a. Surf ace and surrounding areas cleared per i ! l i 1 i ears. a.2.2.c. I t :
l b. Sur' ace free of foreign matter incl. Orease 4 oil '
l i I i c. Sharp (non-ro'unded) cro3ectiens removed i I !
I d. Ane%er :sttern deeth 1.0 mil. minimum. L?_?.e 1 I I
- I ;
'e. Sarf ace ligrtly abraced eer Para. 3.2.3 I f I i !
I i f. Surf ace wiced clean per Para. 3.2.3 er 1.2.4 I i i l I (Pecairs Only) I i ! ! !
- 6. 1 Unicue Nueer stanced er ciecets)- secord Unieue
- I 6 I Nueter(s) in "Reaarks' telow. I I ! l 6
- 7. 8 Ambient conditions checked eer Para. 3.3.2 orier to I i l I !
I primer acclication and record below: i i ' ! '
10 ATE: TIME: WET BULB ' IMP: 3 i 8 I I ORY EULB TEMo: PELATIVE HUMIO!TV: I l 6 i
- l DEW POINT: SURFACE TEMP: i i i i !
(, 8. I Substrate surface free of eestami%nts and less t*en Iil ! I j 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> elapsed since blasting. '
I l I 1 i (Continued on sent Sheet) i II f I I Ampus fes6 9 fuoco on
[
i
~ . - _ .. .. .,,,,_ . . * *
~. -
I INSTRUCTION ISSUE NUMBER SlON PAGE l TEXAS UTILITIES GENERATING CO. DATE '
' ' CPSES i 6
! QI-QP-11.4-5 21 '22 of 24
- 08/25/83 Attachment 3. Sheet 2 t
l CDMANCHE PCAN STEAM ELECTWic STATICN gg.gp.g,4 5, g,,,
INSPECTION REPORT Sheet of (RJp*LDeENTAL) - i l
I irtas - G-
=o. cart INSPECTION ATTRIBUTES = 3 smistug
.r 3 5 i,
b 9.
.n Tras. '91 tee er teamet*ar inttitied ==e em I.3.4 ' ' ' I
- 10. ! Air sucoly free of containatten. I I I I II.
8 Ouafficat*ca of treffettaa. ' List AeD1tcators:) 8 I I I 3
i e i e I i i e
- 12. '
verify Mining Coerstions ese cara. 3.2.2.h. ' ' ' '
- 13. t Coating Material Product identificatton: I I t I i a. Base tot No.- PAar A: i e i e 4 D. Filler Lot No. : i }
f c. Thinner Lot No. - ;
t i i i a. Tinie Mixed: i , i l
( ,
i , i ,
- 14. t dressure cet agitatec. i , i i 4
15 . 8 per tire act eres dee_ i e i i
- 16. i **ose fets tnan 7 5 * *a t . i e t t 8
a i e i i
' I aA5 t 6 i f m% fi laXD ee i Af Wa%%J' '
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l Poem No.1 TUGCO CA
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l INSTRUCTION ! REVISION ISSUE NUMBER -
DATE PAGE t
{ TEXAS UTILITIES GENERATING CO. '
CPSES ;
QI-QP-ll.4-5 ;
i 08/25/83 l 23 of 24 t' . .
21 i l
i Attachment 4 j CCM AN CHE #fAK STEAM ELECTRIC STATION ser :a INSPECTION REPORT =a
'rtu :sscasr.c=
PROTECTIy[ COA 7[NGs j.cuvcAr.c=
- istsrtw sT=ucront arw=4r.am 34 3l .
sys:.ac i m tw . car. *o.
jutAwarcm AS-31 ,le ,lauQ[.QP.11,4 ac. occ. e5,atv. a emanc.c =o Rev. , , j l
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] M7 a INSPECTICN ATTRIBUTES
- catt sio=a rung 4 FINISH CCAT FINAL ACCEPTANCE 2 a Ei is
- 1. 'l Verify curing is Ar CCP.30 or 30A and earn.1.6.1. I
- 2. I per'om visual fnseection of Ceated Sur'sce ce* eart II i 3.6.2. I l I
- 1. 1 Perfem CFT on coated sur'sce as ree cara. 3.6.3 'ree l I! I I *>1tiDie it ms indicate win. Scot. Max. Scot a ~f II I I Averaoe CF witri cor*escondino OP 1 tD Nc's <Sr ea'em II I I i item in *Demarks"). II I Coattmo System Spot Test Minimt;m! II! !
I Coating System sect Test Mastmum: '
l I I ,
i Average CFT Coating System: I I !
4 I 7ee<o m continuity insreetion eer curs- 1 4 4- I I l {
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(., * "8 "C8 "* i 8 'M isiemarups al1.A. CLOSED Q i s oc = m crom ,,
l
, TUGCO OA
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l INSTRUCTION i REVISION l ISSUE PAGE NUMBER f f DATE '
TEXAS UTILITIES GENERATING CO. ' ;
CPSES l QI-QP-11.4-5 ' 21 08/25/83 24 of 24 I
ATTACHMENT 5 ;
I I l
1 i I
' l 4
i I
I i
PAINT MIXING SLIP l
DATE: i i
! BLDG. ELEV. l i !
l COATING: COLOR. l I {
j TIME MIXED: TEMP.
t l
I BATCH # BASE (A) ,
- CAT./FLR (B) l THINNER (C)
GAL.
i l M&TE #'s INSP DATE: i l
i 1 l
i 1
l i
i 4
% ME $
O *se..e... e. . - o e. .*
e=:
?
O L'-
JM hr > \ d y LABORATORY TEST REPORT i N
r February 10, 1981
' '/
01931 Octs:
Testirg ? reject Nutter: ,
Tirne 7 days Dcte of G<cdirg: 2-3-81 Recorta Final Requested by: Mr. D. V. c3 ride Tofcl Design Test Durctn ? 7 davs
- LOCA' Testing, of Carbo Zinc 11/Phenoline 305 Finish repairability PURPCSE: To determine the performance o arboline 191 Pr /lc Phenoline 305 Finish as a repair system for Carbo Zine 11/ Pheno 11ae .3us unisT over a surface preparation of 3M " Clean 'n Strip" and 3M "Rotopeen" when exposed to the PWR 307*F.
LOCA Curve and evalusted according to ANSI N101.2-1972, Section 4.5, as interpreted by Carboline. This is a proposed repair procedure for the Waterford Nuclear Station Unit #3 which is being engineered by Ebasco Services, Inc.
CONCLUSICNS: After 7 days of the LOCA Carve, Carboline 191 Pr Ic Phenoline 305 Finish system over a surface preparation of 33 " clean 'n Strip" and 3M "Rotopeen" exhibits an acceptable performance when evaluated according to ANSI N101.2-1972, Section, 4.5, as interpreted by Carboline.
. j DISCUSSION: I r
gngb From the Cctoline Resecrch & Devercoment Lcboratory ,
(
the tecmecs ooio fumeed om nue crd occucie to rw e m or ou %
%.. no wee or ocmacy a e or answ.o. -carbolirie.J
February 10, . lya -
TESTING PROJECT: 01931 Paga 2 F ," Finni R'anet: 7 drya , .
PROCEDURE:
A. Test Couoans ,
Description:
2"x4"xl/4" steel certified Carboline STI (See Appendix 1)
Surface Preparation: Gritblasted to SSPC-SP5-63 with a 2.0- 'o mil blast profile. . ,
- ' Abrasive Medium: 50/50 mix of GEY d40 grit and S230 shot.
B. Systems Tested .
~
Batch Thinning DIT -
- System Number Color Thinner Ratio Range Ic C'arbo Zine 11 A) OE54775 Green #33 B) OE1981Z 0300 9L18183 12% . 3.0-3.5 mils Ic Phenoline 305 Finish A) OH1395M Gray Phenoline B) OH1491M C705 982285M 10% 4.0-4.5 mils Carbo Zine 11/Phenoline 305 Finish was removed by SSPC-SP3-63, power tool cleaning method. Detailed procedure is outlined in Section C; Repair' Procedurc.
Ic Carboline 191 Primer A) OC3362M Red #15 B) OC3361H 0500 9LO859M 15% 4.0-4.5 mils Ic Phenoline 305 Finish A) OH1395M Gray Phenoline B) OH1491M C705 9M2285M 10% 3.0-3.5 mils C. Recair Procedure
'- 1. Remove Carbo Zinc 11/Phenoline 305 Finish with 3M's " Clean 'n Strip" wheel
- a. A residual amount of Carbo Zine 11 is left on substrate.
- 2. Restore surface profile with 3M's "Rotopeen"
- a. Operate power tool in two directions over substrate.
- 3. Solvent wipe substrate to remove grease and oil which may be present from power tool cleaning.
D. Cure Schedule Carbo Zinc 11: Seven days at 100*F and 100% RH. Phenoline 305 Finish:
. - 48 hours5.555556e-4 days <br />0.0133 hours <br />7.936508e-5 weeks <br />1.8264e-5 months <br /> at'72-76*F and 27-32% RH. Carboline 191 Primer: 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> at 73-77'T and 29-32% RR. Phenoline 305 Finish: 72 hours8.333333e-4 days <br />0.02 hours <br />1.190476e-4 weeks <br />2.7396e-5 months <br /> at 72-78'T and 28-34% RH and a final cure at 150*F for 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br />.
I Fcbruary 10,.1981
.- . TESTING PROJECT: 01931 Pag 2 3 Final Repset: 7 d.ya f .
)
E. Exeosure PWR 307'F LOCA Curve 1
- 1. Time-Tesoerature-Pressure Curve Temperature ** Pressure **
Time 1
. Ambient Ambient-
, . Initial 60 psig
- Initial to 2 hours2.314815e-5 days <br />5.555556e-4 hours <br />3.306878e-6 weeks <br />7.61e-7 months <br />, 47 minutes 307'F (153*C) ?
--2 -hours,-47 minutes to 96 hours0.00111 days <br />0.0267 hours <br />1.587302e-4 weeks <br />3.6528e-5 months <br />
- 25a*F (121*C) ~30 psig
-..-1--- 10 psig -
~
l 200*F (93*C) 96 hours0.00111 days <br />0.0267 hours <br />1.587302e-4 weeks <br />3.6528e-5 months <br /> to 7 days l
. t Water Chemistry :
2..
0.28 Molar H 3303 (3000 ppm Boron) _
0.064 Molar Na22380 .
4 -
NaOH added to adjust to a pH of 9.5 at 77'F (25'C) in deionized water
- *After 2 hours2.314815e-5 days <br />5.555556e-4 hours <br />3.306878e-6 weeks <br />7.61e-7 months <br /> and 47 'sinutes of exposure, temperature of the test environw.n t;
- was reduced by spraying test solution at 200*F (93*C) into the test chamber which was at 307'T (153*C), giving a final temperature of 250*F (121*C). ,
- These are theoretical values. The next page contains graphs of-the theoretical and actual LOCA temperature and pressure curves. The data for the ictual IOCA curves are taken from the chart recording for this test, which is stored in lab book #230, page 57 .'
i Note: Test was interrupted to place spray nozzle in LOCA chamber. Time was added to test to make up for interruption.
GRADING PROCEDURE: The test coupons were evaluated for performance in the following' areas:
l
- 1) Material flaking off. 2) Delamination between coats and/or peeling. 3) Blistering of the topcoat. 4) Chalking of the topcott.
- 5) Excessive cracking.
Grading procedures specified in Report N101.2-1972 of the American National Standards Institute - Protective Coatings for Light Water Nuclear Reactor Containment Facilities:
O aus 8
e 4
q )
. _ , . , . . - - - . , -w -.- - , . - - , , . - - . . ~ - < . _ - , - - . - - ,c.- -, , - - -
rnso:sc1cas
.~~ , . .
Act:31
. 400 - .-
.' . . Te: .pe rature 300 ~
< 1
/ -
~ ./ ,
k i -
o s-
/
f.,---_--_--_
f ,
a s .- .-
u ,' .
s s l '"*
aa 200 - /
/
u / .
() '
/ -
-(y - - .
g
. .10 0 --
~4 4 5 I 102 103 10 10 JO 10-1 100 101
~
Time (Seconds)
J 80 -
Pressure 60 ~ .;-----~~----------------- ---,
- l 0 / g M -
.o /
/ \
g
- w% /
/ I
/ g O
u - ,/
- 8 a
40 --
i
/ e I
- I O
V +/ t- .-------- .- ,
u ,i l f I
,/
' l 2 0. -
.. n
, , I l
e e -
/ .
~
1o2 10 3 10 4 10 5 10 10- 1 100 101 Time (Seconds) .
j ..
Icbruary 10,,1981
. TESTING TROJECT: 01931 Pago 6 Final Rep 7rt: 7 dnya , .
GRADING ,.
PROCEEURE: (coctinued) ,
~
4.5 Methods of Examinina and Evaluatina the Exuosed Test Specimens
~
- The dynamic and/or static elevated temperature-pressure and irradiation test ~
panels shall be evaluated within 2 hours2.314815e-5 days <br />5.555556e-4 hours <br />3.306878e-6 weeks <br />7.61e-7 months <br /> and again after two weeks after removal from the test chamber for the following surface defects: . flaking,
" delanNtion and/or peeling, blistering and chalking. Defects listed in :_.
- - Subsection 4 5.1 through,4.5.4 shall be dealt with as follows:
' 4.5.1 naking. ASTN D772, ' Evaluating Degree of Resistance to naking (Sealing) of Exterio'r Paints, Part 21, American Society for Testing and
Materials, Philadelphia, PA 19103. Flaking shall not be permi_tted.,-
- 4.5.2 Delamination and/or Peeling. Delanination and/or peeling shall not be permitted. ,
4.5.3 Blistering. Blistering shall be limited to a few, intact blisters, Size No. 4, ASTM D714, Standard Method of Evaluating Degree of Blistering of Paints, Part 21, American Society for Testing and Materials, Philadelphin ,
r ,
PA 19103. The number and the size of blisters shall be recorded. .
4.5.4 Chalking. ASTM D659, Standard Method of Evaluating Degree of Resistance to Chalking of Exterior Paints, Part 21, American Society for
- Testing and Materials, Philadelphia, PA 19103. Heavy chalking shall not be permitted.
Any oIher changes in coating properties which are not also associated with the separation, or the release, of coating from the substrate shall not be.
a cause for rejection.
ANSI N101.2-1972 Criteria (As interpreted by Carboline)
Maximum Degree of Failure Allowable F1'aking ASTM D772 ,
10 (None)
~
Delanination or Peeling None Blister Density
- Blistering ASTM D714 56 Blister Size .
- 2 None Few
- Notei~ A blister is not #4 Medium
- 6
' . intact in coating when beingit separated has resulted #8 Medium-Dense Chalking ASTM D659 6 (Moderate)
Note: Flaking, blistering and chalking are all evaluated according to ASTM Standards, with a rating.of,10 indicating that no failure was observed in the
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specific grading area. ,, ) .. .
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1 Fehman 10, 1981 .
TESTING PROJECT: 01931.
' i Page 5 : .
- Final Report _ 7 days j ,
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BESULTS: P14t 307'F IN'[ Curve '
, Other 1-Dry Delanina- Performance
.. Panel Identification Blister- Performance ,8 l )
and Film tion or Chalking Characteristics Evpluation.
Flaking Peeling ing ,I Coating System , Thickness i .
-- Acceptable .
1A)* None #4F-B None 4.5 mils 10 carboline 191 Primer Phenoline 305 Finish 3.5 mils 8.0 mils -
2A) None
-- Acceptable ,
4.5 mils 10 None #6N-5 Carboline 191 Primer ]
Phenoline 305 Finish 3.5 mits
~8.0 mils I
~-
+ , l
- /. , : j . *
. ' g' ,[t ', j 44F to . .
' Acceptable Performance None 46M to 16 (Hoderate)
- Panel suspended in the ANSI N101.2-1972, Section 4.5, 10 vapor phase. .
- 8HD As Interpreted By Carboline .
LAB /T-21878-1 e .
t .
- 9 a
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01931 Ecbru::ry 10, 1981 T7. STING PROJECT: ,
' Final Resort: 7 days ,j Pas 2 6 ,
f .
N
& . U fl ohn J. Ladage, Jr. J F. Moatie -
Robert M. Reals .
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Vice' President
,- Lab. Technician Group Leader Testing Department
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Research'and Development Testing Department
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Tjag/t.p. 01931 ,
cc: , S. Lopata/D. Porthouse/J. Montle/E. Skibs/S. Steinberg/P. Litzsinger/
M. Ditgan/ Group Leaders - .--- -
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- WP6eS 4 8
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- . c.arboline -
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1 . . .
Appendix 1 . ,
- Carboline Specification C31 .
Pracarationofdoncre'teSpecimens_:
- Concrete Com' position _ . .
Cement, ASM C150, Type II. Iow " 16 = M Gravel, ASM C33, size.'3/S inch Sand, ASM C33 NME{E ."
Water reducing admixture, ASM C494 Air entr=4a4a= admi ture, ASM C260. -
- Por.zolana ASM C618 , -
Water - Demineralired or distilled water Concrete Fronortions' , * .
Cement, 7 sacks per cubic yard
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Sand-cravel ratio, 55 sand, 45 graval by voluma .
Pozzolans, to 15 percent replacement of cemenc -
,- Air entraf,ing admixture, 4-7 percent . .
Water reducing admixture, as per manufacturer's instructions j * -
Water, to produce a 3 inch slump .
Preparation of Test Specisen: ,
.- Make and cure the specimen according to ASE C192, except that no form
' oils may be used. The face to be tested shall be composed to the form to Broom finish top simlata poured walla and the wood croweled surfacest surface to simlace floors. No test f ace shall be saw cut. When applicabit.,
concrete curing agents compatible with the coating system shall be used. "
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Panelst *
( - .
The sire for concreta panels shall be 2 by 4 inchas by 2.ir.ches. thick i 0.2 inches. .
Curinr Time 2
'.- 3afore concreta specimens are coated, they shall be cured a =f af ~= of. 28
' days in accordance with ACI 301, " Specifications for Structural Concrete for 3uildings." If a concreta curing primer is used, it _shall be applied j _ .
i l .
on the concrete within 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> after removal of the forms.
l - Carboline Specification ST1 Steal Test Sp'ecimana , an
. ..., .f;e:.
^" Panels _
The size for carbon steel panels shall be 2 by 4 inches by 1/4 inch thick 10.1 inchas with rounded edges and corners.
The steel for sach specimen shall meet the requirements of ASN A36, " Standard Specifi-j .
e cations for Structural Staal".
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