ML20138P014

From kanterella
Jump to navigation Jump to search
LOCA Amercoat D-6/Phenoline 305 Finish & Comanche Peak LOCA FSAR Curve, Final Rept
ML20138P014
Person / Time
Site: Comanche Peak, 05000000
Issue date: 04/11/1978
From: Ladage J, Montle J, Tellor M
CARBOLINE CO.
To:
Shared Package
ML20138M609 List: ... further results
References
FOIA-85-59 01684, 1684, NUDOCS 8511060295
Download: ML20138P014 (6)
v • d • e


Text

,

y..s..,.,:

-..p g.e. : _.,

.-5 e,c,.- gg.;;.p,.: :,.

LAEORATORY TEST REPORT r

3 August 11, 1978 glO Testing Project: 01684 C

T'NAI. REPORT l

SUEJECT:

LOCA; Amercoat D-6/Phenoline 305 Finish and the Coc:anche Peak i

FSAR LOCA Curve

}

RITERENCE:

Cemanche Peak Nuclear Station; Mr. Don Sutton; Mr. Keith Falk; Mr. Dan W. McBride; Testing Project 01651 PURPOSE:

To determine tha performance of Ic Amercoat D-6/lc Phenoline.305 i

i Finish when exposed to the Comanche Peak Steam Electric Station, FSAR LOCA curve and evaluated according to ANSI N101.2-1972, Section 4.5 as interpreted by Carboline.

CONCLUSION:

After the seven days of the Comanche Peak FSAR LOCA curve, the following exhibit an acceptable performance:

System Primer cure 1,2 le Amercoat D-6 17 days at 67-79'? (19-26*C) le Phenolice 305 Finish and 53-88% R.E.

3,4 le Amercoat D-6 17 days at 95-100*F '35-38'C)

Ic Phenoline 305 Finish and 100% R.R.

U PROCEDURE:

A)

Test Coupons Size:

2" x 4" x 1/4" Certified ASTM A36 Steel Surface Prep: Gritblasted to SSPC-SP5-63 Abrasive Media: GTH #50 grit (Cleveland Metal Abrasives, Inc.)

3)

Systems Tested Batch Numbers Drv Film Thickness 1,2 le Amercoat D-6 1503310 2.5 - 3.5 mils (cured in Cure Cabinet *)

1503210 le Phenolice 305 Finish 7B0427M 6.2 - 8.6 mils 6M39595 9.2 -11.1 mils 3,4 lc Amercoat D-6 1503310 2.4 - 3.3 mils (cured in High Humidity 1503210 Drum **)

Ic Phenoline 305 Finish 7B0427M 4.7 - 5.4 mils 6M3959M 7.3 - 8.0 mils

  • Cur Cabinet is at ambient temperature but, has hunidity controlled frem 50% to 90% R.H.
    • High Humidity Drum is at 100*F (38'C) and 100% R.H.

From the Carboline Research 8 Development Laboratory

..._A v.........o........4................,,k.6.......,6..r............

(c ar'b oIIr1e)

..,.........e....,.,y..

....a.,...i. 4.

. u. r r u.

8511060295 851016 PDR FogA CARDE85-59 POR

)

'S~

. y :-;:~ 1.p;..-:xV. ~, '

7,5. _ j?.e.

.,g., ' ~. ~.

2..:.

.p...

o LA AORATORY TEST REPORT August 11, 1978/Page 2 Testing Project: 01684 FINAL REPORT PROCEDURE: (Continued)

C.

Cure Schedule 1

1,2 Amercoat D-6: 17 days et 67-79'F (19-26*C) and 53-88%

Relative Humidity.

Phenoline "105 Finish: 18 days at 71-80*F (22-27'C) and 55-70% Relative Humidity.

t 3,4 Amercoat D-6: 17 days at 95-100*F (35-38'C) and 100%

Relative Humidity.

Phenoline 305 Finish: 18 days at 71-80*F (22-27'C) and

}

55-70% Relative Humidity.

l l

D.

Exposure i

i Texas Utilities Generating Company, Comman-he Peak Steam Electric Station, FSAR Figures 6.2.1-1 and 6.2.1-2.

1 l

1 1.

Time / Temperature / Pressure Profile Time Temperature Pressure Spray Condition k

)

Initial to 10 seconds 240*F (ll5'C) 44 psia Static 10 seconds to 15 mins.

270*F (132*C) 58 psia Dynamic 15 mins. to 1 hour1.157407e-5 days <br />2.777778e-4 hours <br />1.653439e-6 weeks <br />3.805e-7 months <br /> 15 mins.

215'T (102*C) 34 psia Dynamic 1 hcur 15 mins. to 7 days 215'F-130*F 34-10 psia Dynamic (102*C-51'C) l (Note: This is the theoretical curve supplied by Comanche Peak. It was l

followed as closely as possible with the LOCA apparatus available at I

Carboline Company. Please refer to the recorder chart (Lil5-129) for l

~

exact conditions of LOCA profile.)

2.

Spray Solution H B03 (2000 ppm as Boron) in deioni:ed water.

2 pH = 8.5 - 10.0 (NaOH added to adjust pH).

i CRADING PROCEDURI:

l i

j The test coupons were evaluated for performance in the following areas:

f 2)

Delamination between coats and/.or peeling I

1)

Material flaking off l

From the Carboline Research & Development Laboratory j

Th....ma... d... s,. i.h.4 i.,,...a 4....,...,*. 6..,.s.., 6.,. r.4,.. o....,

............s.......,6.......,...i.4.

pg I

v-

.s.

x _.;.,. ;. x.

8 LABORATORY TEST REPORT

~

(

August 11, 1978/Page 3 Te. ting Project: 01684

&gFINALREPORT GR.CING PROCIEUPI: (Continued) 3)

Blistering of the topcoat 4)

Chalking of the coating 5)

Excessive cracking Grading procedu'res specified in Report N101.2 - 1972 of the American National Standards Institute-Protective coatingt for Light Water Nuclear Reactor Containment Facilities:

t 4.5 Methods of Ensining and Evaluating the Exeosed Test specimens The dynamic and/or static elevated temperature pressure and irradiation l

test panels shall be evaluated within 2 hours2.314815e-5 days <br />5.555556e-4 hours <br />3.306878e-6 weeks <br />7.61e-7 months <br /> aad again after 2 weeks after j

removal from the test chamber for the following surface defects;

flaking, i

delamination and/or peeling, blistering, and chalking. Defects listed.in l

Subsections 4.5.1 through 4.5.4 shall be dealt with as follows:

I 4^.5.1 Flaking. ASTM D772,. Evaluating Degree of Resistance to Tlaking (Scaling) of Exterior Paints, ? art 21, American Society for Testing and Materials, Philadelphia, Pa.

19103. Flaking shall not be permitted.

4.5.2 Delamination and/or Peeling. Delamination and/or peeling shall g a

.not be per:sitted.

.; m 4.5.3 Blistering. Plistering shall be lir.ited to a few, intact blisters, Size No.

4, ASTM D714, Standard Method of ' Evaluating Degree of Blistering of Paints, Part 21, American Society for Testing and Materials, Philadelphia, 2

i i

Pa.- 19103. The number and the size of blisters shall be recorded.

i i

4.5.4 Chalking. ASIM D6$9, Standard Method of Evaluating Degree of j

Resistance to Chalking of Exterior Paints, Part 21, American Sociecy for Testing and Materials, Philadelphia, Pa. 19103. Heavy chelking shall not be permitted.

Any other changes in coating properties which are not also associated with 5

the separation, or the release, of coating from the substrate shall not be l

a cause for rejection.

i

+

1

(

5 i '{

From the Carboline Resea'ch & Development t.a5oratorv j

l G

r m....*... i 4... #..a 6. a.a ; e.....a d e e.,.... *. b.. 8.. a a. l. 4,.. a.....

(car 6oiIne)

a.,.........e.......,i.

...a.,...n...

s 4

3a amad e a4ha'h4 f',' enha ete.Au.

f

..m.

\\

LABORATORY TEST REPORT

(

August 11, 1978/Page 4

.f" T: sting Project: 01684 FINAI. REPORT ANSI N101.2-1972 Criteria (As interpreted by Carboline)

Maximum Degree of Failure Allowable Flaking ASD D772 10 (None)

Delanination or Peeling None

  • Blistering ASTM D714-56 Blister Size Blister Density' i
  1. 2 None
  • NOTE: A blister is not
  1. 4 Few intact when it has resulted
  1. 6 Medium in coating being separated
  1. 8 Medium-Dense i

frca the test coupon.

Chalking ASTM D659 8 (Light)

NOTE:

Flaking, blistering and chalking are all. evaluated according to ASN Standards, with a rating of 10 ind1cating that no failure was observed in the specific grading area.

?.

t, -

.e a

,.m From the Carboline Research & Development Laboratorf A

  • Q N T h.... ;..: 4... #.,. i. h.4 i.,,.... e........ ',*. n..,..., s.. i. 4,.. m.....,,

(c ar*b o11rie]

..........e......,4......,i..i.4.

t N.

Testingf^ icct: 01684

,Q August 11 d'sfl/P.in ".

FINAL. R(

R Panel Identification Dry Delamina-Other and Fi)=

tion or Performance Pe r f o e m'.i ni.

j Coating System Thickness Flaking Peeling Blistering Chalking Characteristics F.va l u.it s on i

Acreptafsic IA* Ic Amercoat D-6 3.5 mils 10 None Nonc 10 (Primer cure 53-88% R.ll.

Ic Phenoline 305 Finish 6.5 mils 10.0 mils Accc,.htc lil Ic Amercoat D-6 3.0 mils 10 None

  1. 4 Few Intact 10 j

(Primer cure 53-88% R.II.)

Ic Phenoline 305 Finish 6.2 mils I

9.2 mils Acceptable '.

2A* Ic Amercoat D-6 2.8 mils 10 None None 10 (Primer cure 53-88% R ll.)

Ic Phenoline 305 Finish 7.7 mits 10.5 mils Acceptable 2ft Ic Incrcoat 11-6 2.5 mils 10 Mone

  1. 4 Few Intact 10 (Primer cure 53-88% R.ll.)

Ic Phenoline 305 Finish 8.6 mils 11.1 mils Accer'abic 3A* Ic Amercoat D-6 2.4 mils 10 None Nonc 10 j

(Primer cure 100% P.ll.)

ic Phenoline 305 Finish 5.4 mils 7.8 mits 3 11 It Amercoat D-6 3.3 mils 10 None None 10 Acceptahic I

(Primer cure 100% R.ll.)

Ic l'henoline 305 Finish 4.7 mils

)

8.0 mils 4A* Ic Amercoat D-6 2.6 mils 10 None None 10 Acceptahlt (Primer cure 100% R.II.)

Ic Phenoline 305 Finish 4.7 mils 7.3 mils 40 Ic Amercoat D-6 2.5 mits 10 None Nonc 10 Acccp alitr '

(Primer cure 10G% R.ll.)

Ic Phenotine 305 Finish 4.9 mils 7.4 mils

q August i U/ Pa ge. e.

Testings jject: 01684 f,1NAI. REPORT RESill.TS i

Panel IdentificaLion.

Irry Delanina-Other and Film tion or Performance Performanc Coating System Thickness Flaking Peeling Blistering Chalking Characteristics Evaluation deceptable Performance 10 None

  1. 4F to #8HI)
  1. 8 (Light)
  • Panel suspended in the vapor ANSI N101.2-1972, Section 4.5, phase As Interpreted by Carboline l

s l

i ff6u f,

hf f) /6u b O

f x

C John J. J. adage, Jr.

Michael D. Tellor John F. Hontle Developmental Chemist Supervisor Vice President Testing Department Research & Development Research & Development 9

8

/bj XC: JFH/CJW/DWl/PDI./ilDT t

l

}

l

~

l y;jN i q" g LABORATORY TEST REPORT

[

May 9, 1978

{V_d

~~

Testi g Project: 901651 FINAL REPCRT CChe ErNTIAL 1

i

SUBJECT:

LOCA test of systems topcoated with Phenoline 305 Fisish.

R_NCI:Commanche Peak Nuclear Power Station; Mr. Don Sutton, Mr. Keith Falk; 1

Mr. Dan Mc3 ride; L-115-105 I

PURPCSI: To test the perfor: nance of Phenoline 305 Finish over each of the 1

following primers:

,1)

Ic Amercoat D-6 @ 2.0 - 3.0 mils 2)

Ic Mobil Zinc 7 @ 2.0 - 3.0 mils 3)

Ic Carbo Zine 11 @ 11.0'- 12.0 mils i

when exposed to the Co - anche Peak Steam Electric Station, FSAR LOCA l

Curve and evaluated according to the criteria of ANSI N101.2 - 1972, 1

Section 4.5 as interpreted by Carbolise.

CCNCL"SICNS:

After completion of the 7 day Co =2nche Peak ISAR 1CCA test, the systems tested exhibited the following perfor=ances when evaluated according to ANSI N101.2 - 1972, Sectie: 4.5 as l

interpreted by Carbo 11:e:

Coatist Svstem Perfor=ance 1)

Amercoat D-6 @ 2-3 mils Vapor Phase Acceptable Phenoline 305 Finish 2)

Amercoat D-6 @ 2-3 mils Liquid Phase Unace ptable Phenolise 305 Finish 3)

Mobil Zinc 7 @ 2-3 mils vapor Phase Acceptable Phenolice 305 Finish 4)

Mobil Zisc 7 @ 2-3 mils Liquid Phase Acceptable Phenoline 305 Finish i

5)

Carbo Zine 11 @ 11-12 mils vapor Phase Unacceptable Phenoline 305 Finish 6)

Carbo Zine 11 9 11-12 mils Liquid Phase Unacceptable j

.Phenolise 305 Finish

)

a i

REk

[

From the Carboline Research & Development Laboratory y

rh.. w 4..: 4... #,a 4.h.d i. en,.

a...-- =.h. n..,.#

u i.4,.. H.

.#. a w.,.y i. i.

.,i,.,ii.4.

[ car 6oHnq) i f))~.[~ f~&~

.~

" ~ ~ ~ " ~ _ ~ ~

~ ~ '

ump

+-

i LABORATORY TEST REPORT D

$Na. f May 9, 1973/? age 2 COiTIDEE IAL i,

PRCCIDERE:

A)

Test Courons f

Size:

2" x 4" x 1/4" Certified ASTM A36 Steel.

Surface Prep: Gritblasted to SSPC-SPS-63 Abrasive Media: 6FH d50 grit (Cleveland Metal Abrasives, Incl

?

3)

Dry Film 3'

Systems Tested Batch Numbers Thickness

1) Ic Amerecat D-6 6-705416 2.5 - 3.0 mils 6-705420 le Phenoli=e 305 Timish 7I25285 4.8 - 6.2 mils __

7I25005 7.3 - 8.5 mils 1

2) Ic Mobil Zi=c 7 FT7I24 2.1 - 2.7 mils Ic Phenoline 305 Finish 7I252SM 5.3 - 6.9 mils I

7I2500M 8.0 - 9.0 m:.ls

)

't

3) Ic Carbo Zi=c 11 7I5106M 11.0 -13.0 mils 710966Z l

le Phenolise 305 Finish 7I252SM 4.0 - 5.5 mils i

/'- -

7I2500M 16.0 -17.0 mils C)

Cure Schedule Primers (all systems): 17 days at 65-76'? (lS-24*C) and 27-90*. R.H.

Topccat (all systems): 10 days at 72-77'T (22-26*C) and 31-45". R.3.

D)

Ersosure Texas Utilities Generating Company, Coimnanche Peak Steam Electric Station, FSAR Figures 6.2.1-1 and 6.2.1-2 4

l s

b From the Carboline Research 86 Develcpment Laboratcry j

f i

V n....h i.. i.... torn i.h.d i.,,. a.....,.,h. b..,.#

, u

.d,.. x...,,

n..

..i..

y i. si.

., i..n.4.

.~

,.4-

.c 'e.

.Y o ~ >

~

.~

e4 i

LABORATORY TEST REPORT O'e May 9, 1978/Page 3 CCNFIDENTIAL l.

Time / Temperature /?ressure Profile I

Time Temocrature Pressure Sorav Condition Initial sc 10 seconds 240*F (115'C) 44 psig Static 10 seconds to 15

  • s.

270*T (132*C) 58 ;sig

. W.e 15 mins. to 1 hour1.157407e-5 days <br />2.777778e-4 hours <br />1.653439e-6 weeks <br />3.805e-7 months <br /> 15 mins.

215'T (102*C) 34 psig Dy-mmic 1 hour1.157407e-5 days <br />2.777778e-4 hours <br />1.653439e-6 weeks <br />3.805e-7 months <br /> 15 mins. to 7 days 215-130*F 34-10 psig Dynamic (102-51*C) q t

Please refer to the recorder chart (L115-105) for exact conditions of 4j 1CCA profile.

2.

Spray Solution l

H,30 2000 ppa as Baron) in deieni:ed water.

p2 =3 (5.- 10.0 (NaOH added to adjust pH) 8.

i GRADING PRCCIDURI:

~:..

,.ff - '

The test coupons were evaluated for performance in the following areas:

1)

Material flaking off 2)

Del =*mtion between coats and/or peeling 3) 311stering of the topcoat 4)

^= m,g of the coating 5)

Excessive cracking Grading procedures specified in Report K101.2 - 1972 of the A=erican i

National Standards Institute-Protective Coa-dngs for light Water Nuclear j

Reactor Containment Facilities:

4.5 Methods of Er=s ing and Evaluatine the Exoosed Test Soecinens The dynamic rad /or static elevated temperature-pressure and irradiation test panels shall be evaluated within 2 hours2.314815e-5 days <br />5.555556e-4 hours <br />3.306878e-6 weeks <br />7.61e-7 months <br /> and again after 2 weeks after removal from the test chamber for the following surface defects: flaking, delanisation and/or peeling, blistering, and chalking. Defects listed in Subsections 4.5.1 through 4.5.4 shall be dealt with as follows:

1 l

t 4

I i

From the Carboline Research & Development Laboratory j

V Th....h. ;.. i 4.,. swoi.h.4 i.,,.. 4....m.

  • . b.~.,. #.., ka

.4,.. H. -..,

...,,...#....,i. i..a.,i..ii.d.

(car *6olir1e,)

i l

l l

l l

-O

_ _ >.. a :.1. :

a:.-

_z s'

l h LABORATORY TEST REPORT May 9,1978/Page 4 4.5.1 naking. ASTM D772, Evaluating Degree of Resistance to naki:

"~

(Scaling) of Exterior Paints, Part 21, American Society for Testing and Materials, Pniladelphia, Pa.

19103. nakiss shall not be per:sitted.

4.5.2 Delamination and/or Peeling. Delamination and/or peeling shall not be permittad.

4.5.3 Blisterina. Blistering shall be limited to a few, intact blisters, j

Size No. 4, ASS D714, Standard Method of Ivaluati 3 Degree of Blistering of Paints, Part 21, American Society for Testing and Materials, Philadelphia, Pa.

19103. The number and the size of blistars shall be recorded.

}

4.5.4 Chalking. ASS D659, Standard Method of Evaluating Degree of j

Resistance to Chalking of Exterior Paints, Part 21, American Society for 1

Testing and Materials, Philadelphia, Pa.

19103.- Heavy chalki g shall i

not be permitted.

Any other changes in coating properties which are not also associated with j

the separation, or the release, of coating from the substrate shall not be I

l a cause for rejection.

j ANSI N101.2 - 1972 Criteria l'l (As interpreted by Carboline)

Maximus Degree of Failure Allowable 1

L naking ASE D772 10 (None)

Delamination or Peeli=g None

  • Blisteri=g AS 2 D714-56 Blister Size Blister Densirv
  1. 2 None

~

  • NOTI: A blister is g f4 Few intact when it has resul ed
  1. 6 Mediom in coating being separated
  1. 8 Medium-Dense from the test coupon.

i Chalking ASS D659 8 (I.ight)

NOTI:

Haking, blistering and 4= Wag are' all evaluated accordi:g to ASS Standards, with a rating of 10 indicating that no failure was observed in the specific grading area.

a l

E

$ $4 From the Carboline Research & Development Laboratory j

t n.,.a.i I4.,. Maia.4t.erv.

4...

. = +.b.n.i,

...4,..w......

n.

4.w yi.sim -i.n.d.

(Car *b oIine,)

-W SYM&M ee 4,

t

,7

..P,,

Hay 9",. 978/Pai f;

. s CONFIDENTIAL i

li 1

j Panel Identification Dry Film Delanina-Other

+

and Thickness tion or Blister-Performance Performance

}

Coatina System (Hils)

Flakint Peeling ing Chalking Characteristics Evaluation l

Blistering at

.)

IA)4 Ic Ameron D-6 2.5/3.0

.10 None None 10 bottom edge, Acceptable both sides, Ic Phenoline 305 4.8 5.0 larger than Finish 7.3 8.0

  1. 2F-BT-intact Blistering at 18 I-Ic Ameron D-6 2.3/2.4 10 None
  1. 2F-BT on 10 bottom edge, Unaccepta.e side 1 -

both sides, Ic Phenoline 305 6.2/5.4

.i Finish I'5/D intact larger than

  1. 2F-BT-cracked L

Blistering at 2A)* ic Hobil Zinc 7 2.7/2.6 10 None None 10 bottom edge, Acceptable

~

Ic Phenoline 305 5.3/5.4 both sides.

Finish 8.0/8.0 larger than

  1. 2F-BT-intact j

t-Blistering at g

28)

,j Ic Hobil Zinc 7 2.4/2.1 10 None None 10 bottom edge, Acceptable both sides:

Jf6J 6

Ic Phenotine 305

  1. 2H-BT.One #2 I

Finish 9.0/9.0 at top edge, Side 1.

I, Acceptable Performance I

ANSI N101.2-1972, Section 4.5, 10 None

  1. 4F to
  1. 8 Light APanel suspended in the

[

  1. 8HD vapor phase As interpreted by Carholine LAH/T-127) k' V

l t

k; j

Hay 9, 1978/ Pas CONFIDENTIAT.

- ll Panel Identification Dry Film L'elseina-Other and Thickness Lion or Blister-Performance Performance Coating System (Hils)

Flaking Peeling ing Chalking Characteristics Evaluation p

1.arger than Blistering at 3A)*

Ic Carbo Zinc 11 11.0/11.5

.10 None

  1. 2F-BT, Side 10 bottom edge:

Unacceptable Ic Phenoline 305 5.0/ 5.5 1; #6F, 4F-One larger

/$'

?'

Finish 16.0/17.0 BT, Side 2 than #2-Bf-Intact. One larger than

-j

'l

  1. 2-B aL top edge, Side 2, Intact.

1,:,

A I.arger than Three hairline Ic Carbo Zinc 11 13.0/12.2 10 fee

  1. 2F-BT, near 10 cracks 1/4-1/2" Unacceptable

./r, 38) h Ic Phenoline 305 4.0/ 4.8 Blistering edges', Side 2 on upper edges-i' Finish 17.0/17.0 (peeled) coating intact.

(1) Because blistering is limited to few-moderate, in. tact slisters occuring at i

the edges only, panels IA, 2A and 28 are rated " Acceptable".

?

Acceptable Performance 10 None

  1. TF to #8HD
  1. 8 I.ight

As Interpreted by Carboline l.A D, 1277 l

I t

I.

l I

i h

j, i

.e, ~.,,.

-..s.

LABORATORY TEST REPORT

(

D Ofj May 9, 1978/Page 7 CONFICEE IAI.

DISCUSSICN OF RE M TS:

Although panels lA, 2A and 23 do not meet the strict standards of ANSI N101.2, Section 4.5, Carboline interprets the standard as pertaNag primarily to the plane areas of a test coupon, and places limited significance en the discontinuous surfaces such as edges, channels, veld spatter, ate. Therefore,. the performance of these panels (IA, 2A, 23) having intact edge blisters, with 3

1 no other effects to the coating system or substrate, is rated l

" Acceptable".

^

f/

B

'Q0 i

Alicia 5. Boldt Michael D. Tellor J

Mentle l

Acting Group Leader Supervisor Vice President Testi=g Department Research & Development Research & Development i

Aj f

C: C.~W / ::WM / POL / 3CT t

6 l

l E

I t

i.

1 i

n r-=

C

From the Cartoline Research & Development Laboratory

}

Q s

Th....ho s.. I 4.

to,n i.h.a r.,,.. 4....,...

,h. 6....i.., so..r.4,.. H.w..

n......

4...

..y i. vi.

.,i

.n.4.

pgg

~

l

- - - - - =

. p.m s. ~...-v.

.....y.;.

c...,. ~

.. ~. -

~

e vi 9 wm y

w c mN M C$ E

,1 c:

w g> ra i

e E o-g C."'.

4

'j w >= >= 1 b..

n.

5

@C E El

<t2 2 5 g gm 2 Ed c v "<

t ED-l C u 'JU b9 Z

w 1

t id o

=

C l

i C

~

ce 1

u-1 o

a i

W e-8

[

1 i

3_

1 i

y C

l 4

=

e a.

=

o n

A d

e e

e 9

5-Q I

3 i

a tu 5

I.

4 S

'o 5

a.

a 0

g9 i

-= S 5

i

=

1

.)

1 l

l l

l' I

o_

M7 cc bt C70gg co pis code co'ott CC Cbt CC'011 CC'Cil

\\ -

(s Me) =antv224Wil l

l Emm O O

      • GpW&4Mme*9(=.*

y 6MM p-Wsw Nwy eese e y

a m.

4

4gg, y

m.--w-i

w

,.,e e

em%,

[ -

3 9

v' 0

O 9

M 0

4 g

u DE-P$ t., Ot4(.- IO O */o SP RAT. tiA%. 51, l

h Fitoill g

o

)

l!

h O.

c

,4 3

b o

lis 3 s

i (t

.i 3 4 L ':

i oe o

IIs 0

0 nc (L.

{

Q i

n 1,

$1 4

3 s.,

,3 t.

d'l.11l11_j l_(1.1111_l_Llllill l_l lllli 1 1 111111 llilllli 111111-

'l n

8 to' 105 106 go e go.

go' io 10 1

TIME (sec)

COMANCilE PEAK S.E.S.

FNAL SAFETY ANALYSIS f1EPOrlT UNITS J pnd 2 cot 4TAltittI247 PRESSURE I

TRANSIEt4T - DEPSG FGilE 6.2.1-1 1

1

- 3. - :-. t.

g.7,,.,g 2

.{

1 e

4.'S

.y

.v O

OAK RIDGE NATIONAL LABORATORY

~

UNicN CARBIDE CcRPcRATicN NUCWR DIVis101 O

POST QPPICE 803 X CAK RIDGE. TEMNE$$EE $7CO September 28, 1978 f

Mr. Charles Wiegers Pcwer Industry Manager Car $ cline 350 Hanley Incustrial Ccur St. Louis, MO 63144 Cear Mr. Wiegers:

As ycu requested, enclosed is me revised forma copy of

/?

Carocline rescr: dated August li,1978.

Please call on us if we can be of additional help.

Sincerely yours, b.'v

/

/,

e L. T. Corbin, Secticn Head Analytical Chemistry Divisien LTC:c w i

Encicsures I

i l

~

        • -N9ee8"**g
  • l
  • 'usP

=M,.

, - u. :. -.

,, 3.....y,,,

-2..-

i f ~

dbr.

1 OAK RIDGE N ATIONAL LABORATORY Orgmafgo av UNicN CAR 8tol CcR9cRATtcN NUCLUM CmsiCM east arries sox x p

82, i ou moca. rannassa srisa i

August 17, 1973 i

Mr. Dan W. McBride Nuclear Market Specialis:

Cartoline 350 Hanley Industrial Court St. Louis, MO 63144 Cear Mr. McBride:

Enclosed are One results of the irradiation, decantamination, and CBA tests you requested. The conditiens of the twc OSA tests were identical and are listed in Table 2.

If we can be of furtner assistance, please feel free to call on us.

1 Sincerely yours.

b.

l-L. T. Corbin, Section Head Analytical Chemistry Divisien LIC:cnw 1

Enclosures f

d

^r g

,u o'

- - - - -+ -,. -..

'W

~

.W W****b6-w w

r 7--y

,e

-ww y

,p.%

2q.-

.n g

, t ai a

I

. Manufacturer:

Carboline Analytical Chemistry Divisicn Cak Ridge National Laboratcry St. Louis, M0 Date:

-uc. 16, 1978 v

i Report of Irradiation, Decentamination,'and OSA Testing The irradiation, decentamination, and design basis accident (CSA) tests are conducted, respectively, in accordance with Sechtel Corp. Standard i

Specification Ccatings for Nuclear Pcwer Plants, spec. Nos. CP-951, CP-952, and CP-956 (or with modifications as noted in Table 2 CSA test conditions).

The tests are designed also to meet tne specifications set in botn A.N.S.I.

i l

Prctective Coatings (Paints) for Lient Water Nuclear 1

re;crt N 101.2-1972, Reacter Centainment Facilities, and N 5.12-1974, Protective Ceatines (Paints)

The DBA test spray solutten and the test ecnditions for tae-Nuclear Industry.

1 are listed in Tables 1 and 2.

After both the DSA and the irradiation tests, the ccatings are examined for signs of chalking, blistering, cracking, peeling, All delsmination, and flaking, accceding to ASTM standards wnere acclicable.

l except tha decontamination test panels are returned to the coating manufac-1 turer.

The irradiation tests are run using a s;ent uel assemoly, receved fran the Hign Flux Isotcpe Reacter (HFIR) at ORML, as.ne scurce of radiatien.

l The l

These fuel asseelies are stored under 20 feet of demineraliced water.

fuel is 935 enriched U235 as U30s ccmbined with aluminum. The spent fuel assemclies are removed after each 23-megawatt day ceriod. Irradiation is done using the garza energy from the accumulated mixed fission products.

This scre readily simulates conditions arounc a reactor tnan dcas a cobalt Also, the higher gamma activity affords shcrter irradiation time source.

i to achieve accumulated deses. The dose rate (nur days after removal of a fuel assecly frem the reacter is 1 x 10a rads /heur.

l 4

i 1

The fuel asseoly is 20 inches high. A 20-foot long, 3-1/2-inch i

f i

diarcter pi;e, with one end capped, is used for the air irradiation tests.

The capped end is icwered into the four-inch opening of the center of the fuel ass eoly. The open end, ateve the water level, is ccvered witn an "0" l

ring sealed flange to which is attached a steel cable and an air outlet j

i The air inlet is located at the bottem of tne pice. The test spect-hose.

mens are connected to tne bettem of the cable and icwered into the 0

. l@b3 C.

Evaluated s

y'7 6 ~

t A; proved D,/- (

r I

4

~

~

-y.- -

- x g. -rm.

,,gg,

m.

.....,.,q, j

i Manufacturer:

Carboline Analytical Chemistry Division

}

Cak Ridge National Laboratory St. Louis, M0 Date:

Auc. 16, 1978 i

l i

radiation field. Also at the center of the fuel assembly is a stainless j

steel clad cadmium tube used as a neutron abscrber. This prevents contami-nation of the test specimens by induced radiation.

7

}

The decontamination procedure is as follcws: a mixture of fission product nuclides (aged greater than 90 days and less than three years) is neutralized to pH 4 and innediately applied to the test specimens. The specimens are previcusly degreased in alcohol. Af ter the contaminated spc is air dried, the activities of four of the nuclides are measured by ccunting j

dith a Tae(Li) detector and a multichannel pulse heignt analy:er. The speci-a 1

mens are tnen suspended in a beaker of water at 25'C and washed by stirring 4

I l

for 10 minutes. The specimens are removed, the backs rinsed in water, air i

dried, and ccunted as abcve. The ratics of the activities before, to tacse after the decentamination are repor,ed as decontaminatien facters for water.

I The decentamination and counting steps in 25*C and 80*C acids are repeated, t

i 1

and the respective decontamination factors calculated. The " total overall f

M l

0.F." is calculated as tne ratio of the total activity at the beinning of the test to the total activity at the completion of the three washing steps.

i 4

All activities are corrected for decay between counts. A computer has been programed to de all the calculations.

i e

1 I

i i

f i

i l.

l I

t i

I O-M i

Evaluated X4\\W.4tG l

Approved,/... 4D. ' // /.. Q l

e t' -

m

.~.r~.-.o--

[..

. $[.__

=_ - -

p :;.:.,.;;-

- ~ - ~ - -

=

}

t' Manufacturer:

Carecline Analytical Chemistry Division I $

Cak Ridge National Laboratory

's-St. Louis, M0 Date:

Auc. 16. 1978 Cecentamination Test Results:

l I

These tests perfer-ced according to ORNL Master Analytical Manual Metned No. 2 0920 and Bechtel Corp. Spec. CP-952.

CRNL Leg Scek No. A 7562; A7-17 T Decentamination Facter (CF)

E'{C8"f0 g,

i Sa=cle Water Acid Acid Activit{

Numcer Centaminant 325'C 925'C 380*C Overall Removed i

i 53-200 Ce-144 50 2.1 6.9 710 i

(193LF/191HS)

Ru-106 16 1.7 1.5 40 Ir-95

->2300

>1.5

>l.2

>4100 Cs-137

~

17 7.8 7.1 34 TOTAL 40 1.9 2.4 180 99.4 1

1 55-203

-Ce-144 82 3.8 4.2 1300 t

(CZ11/ES3hS)

Ru-106 31 1.9 1.8 110

?

Cs-137 4200

>1.0

>1.5

>6400 Zr-95 14 2.7 7.4 51 4

TOTAL 57 2.7 2.0 300 99.7 j

! 204 Ce-144 660 1.9 1.0 1300 i

(CZil/305HS)

Ru-106 18 3.3 3.6 210' Cs-137

>2000

>1.6

>l.0

>4800 Zr-95 7.1 2.3 7.4

~ 23

~

TOTAL 61 2.7 1.7 230 99.6 i

Ce-144 l

Ru-lC6 Cs-137

~

Ir-95 i

TOTAL f

Ce-144 Ru-106 Cs-137 I

Zr-95 l

TOTAL IPercent of total activity removed = (1 - h) x 100.

I

/

t i

Approved A,/,

ce-D3 C g

g i

I i

4e g

  • 4"

-B#

N -. _

' ~'-

7_

- app s y., _...;,

9

. Manufacturer:

Cartoline Analytical Chemistry Oivisicn Oak Ricge National La cratory t

St. Louis..M0 Cata:

Auc. IS, 1973

~

i 1

Table 1.

OCA solution composition, distilled water 0.23 M toric acid (3,C00 ppm bcron) 0.064 M, sodium tnicsulfate Adjusted to pH 9.5 with sodium hydroxide i

1 i

1 Table 2.

08A test conditions

  • Time Temcerature (*F1 Pressure (csic)

Comments i

f Sta rt 10 seconds 307 60 Steam injection.

f 2 hrs 47 min 307 60 a.:

J(

5 minutes 307-280 60-30 Injected cold spray.

20 minutes 280-250 30 Adjusted pressure.

t 4 days 250 30 l

3 minutes 250-230 10 Crained; injected cold i

spray.

i l

15 minutes 230-200 10 Adjusted cressure.

3 days 200 10 End of tes:

i

  • These da*a are taken from recorder charts on permanent file at CENL.

i ORNL Log Ecct ac. A7562; A7-17-8 i

I Evaluated iC C

Approved [

v

..,3.g.p

, 7, 4y - -

,.y c.-..~

f d

Oy2 Manufacturse:

Cartoline Analytical Chemistry Division Cak Ridge National Laboratory St. Lcuis. 0 Date:

Auc. 16, 1978 v

s i

1 System Identification:

x Steel Panel Concreta S1cck CZil/191HB Radiatien Tclerance Test Results:

1 CRNL Master Analytical Manual Method No. 2 0921; 7

Bechtel Cor;:. Scec. No. CP-951; ORNL Log Ecck No. A 7562; A7 8 i

Initial Ocse Rate:

1.5 x 107 rads /hr

)

Test Concucted In:

x air water 1

1 Cumulative Ocse Rate: Cen ents samele Nc.

1 X 10' rads 1 x 10' rads Coatincs intact, no defects.

S1-1 sides A, B.

Ceatines intact, no defects, 51-2 sides A, B.

j l

t i

1 1

l Additienal Cc : ents:

I t

l e',

i Evaluated sd

/m/ /b

./

ACQroved l

TX l.901 4/78

.,9 - ~ ' -:,

4.q,. yye.:

._ " -[F

'_~

j e

i

't i

@'3.

' Manufacturer:

Cartoline Analytical Chemistry Division Cak Ridge National Lateratory St. Leufs. M0 Cate:

A.c. 15. 1978 i

l System Identification:

x Steel Panni concrete Stock 4

SP81/191HS Radiation Tolerance Test Results:

4 l

CRNL Master Analytical Manual Methec No. 2 0921; Bechtel Cer;). Spec. No. CP-951; j

CR.m. Leg Book No. A 7552; A7-17-8 i

Initial Cose Rate:

1.5 x 107 rads /hr I

Test C:nducted In:

x air water

\\

t t

f Cumulative Ocse Rate: Cements

}

Samole No.

1 % 10' radi 1 x 10' reds

$2-23 Coatings intact, no defects, sides A, B.

$2-24 Ccatings intact, no defects, i

sides A, B.

'I i

Additicnal Cements:

I i

k j

r Evaluated AC W 4 4

,. Q Apcreved I

/,/ f,d A A

TX 4901 4/78 l

.~-~...v e-n q -

-,--.,r

-a~~

,,m-o m

m,-

~ -- ww

-,a, e-

.-~

.a

- q...,,,.

a..:.

. 3.-.- -

.,,. c

.9 ;

am. -

win.

J '

g.

Manufacturer:

Carboline Analytical Chemistry Division i

Cak Ridge National Lateratory St. Lcuis. YO Cate:

Auc. 16, 1973 4

v 4

4 Svstem Identification:

x Steel Panel Concrete Block 3

193LF/191HB

" I Radiatien Tolerance Test Results:

._l CRNL Master Analytical Manual Method No. 2 0921; i

Bechtel Corp. Scec. No. CF-951; i

CRNL Leg Ecok No. A 7562; A7-17-8 1

Initial Ocse Rate:

1.5 x 107 rads /hr Test Conducted In:

x air water i

I Cur ulative Oose Rate: Cements p-Samole No.

1 X 10' rads 1 x 10' rads I

j

.c

~,

t 53-43 Ccatines intact, no defects, N

2<

sides A, S.

s r

53-1/1 Coatines intact, no defects, sides A B.

t 1

i j

i Additional Ccrrents:

s a

t

'l 1

Evaluated

- Mba 1

L w/. ~.n..p

e.8P

  • T

+M M

un*

9 s

--m

,,-,---m---

-s c-e-mw

--g

,-r

,-m

,--,,wr

-,,--p-

,,,------g.ww-,,,y ev,m-,,wg---

pm,<,4-e rew,--,,,_,y v,,

'1

., _ e y.,

-.s I

i i

l l

teollne w

DBA AND RADIL* ION TOLIRANCZ TEST PANEI, PREPARATION DATA 1.

PRODUCT TO BE TISTED Carboline 193 LP PM:ner/ Carboline 191 EE 2.

TTPE STBSTRATI Car:1fied ASTM A36 Steel SIZE 2" x 4" x 1/4" f

j 3.

SURPACE PRZPARATION (describe) SSPC-SP3-63 Pever Tool CIsan with N I

" Scrip n Clean" j

^

7%

4 PRCDCCT DATA:

SAMPLZ NO.(s) 'S3-160; S3-163 DATE AND TIME CORING CCMPCUND C1 PRIMER APPI.IID ~ /

J

'1 3.

PRODUCT APPI.ICATION CONDI!!ONS THICKNESS M & OATI CCAT PRODCC CODES 3ATCH d METHOD R/M('P MR.H.

(ins.)

APPLIED r ' ' ;-

Carbcline 193 IJ 7E1949M Spray.

74*P/42*.53-160).0026/.0026 3-10-78 Primer 7I.2868M S3-163).0026/.002 Carboline 191 EB 7E1151M Spray 80*T/ S: 53-160).0043/.0035 3-16-79 7J2147M S3-163).0038/.0035 i

Primer 68-80*T Primer 24 J.

  • 5.

CTRI%. CONDI!!CNS: AMBIENT TEMP 73-7a

'P KII,. HUMIDIIT

4. _ u.

Primer 6

MINIMUM CORE 53 DAYS v + d ve. ? ^c "

wnm, = 1 6.

TEST PROCEDCRE ORNL Master h=Weni e

7.

TESTING PERPCRMED BY Analvtical Chm 4etrv DATE STEMI*"ID t.g.?n Diviston l

Cak Ridge National I.aboratory du/

T h Sbl9

! RIP

, S- 06376-3 T

j i

r e

w9

" ' ~ "

I

.-,-w--

..m.

1

.,c;,.

DEA TEST RESUL*S l

t t

i f

4 0

l i,

s 4

+

~

9.

\\

\\'

i e

\\

w 1

4 e

Test Report No.

I I

?

e t

e 4

(

k A

e

  • O@*De-m J eAM q

a p,

==

-g em g,,e, I

4 4-M-9p w.

\\

- -.... - ~

=

1 1

Anal 'ical Chemistry Division Manufacturer:

Carb< 'ne Oak...dge National Laboratory Date:

Auc. 16. 1973 St. Louis, M0 Table 1.

OSA solution composition, distilled water I

0.23 M boric acid (3,000' ppm boren) l 0.064 M sodium thiosulfate 3

}

Adjusted to pH 9.5 with sodium hydroxide f

1 4l 1

i Table 2.

DBA test conditiens*

2 l

Time Tercerature (*F)

Pressure (esic)

Coments i

4 Star

}

10 seconds 307 60 Staam injection.

j I

2 hrs 47 min 207 60 i

5 minutes 307-230 60-30 Injected cold spray.

20 minutes 280-250 30 Adjusted pressure.

l 4 days 250 30 3 minutes 250-230 10 Orained; injected cold spray.

l 15 minutes 230-200 10 Adjusted pressure.

3 days 200 10 End of test

  • These data are taken fran reco-der charts on pennanent file at CPML.

i CTdL Log Sock No.' A7562; A7-17 8

}

@iO Evaluated A.,roee/ t 22 /-r l ()

l

"*WOtOO

-pyy yy

i

.-..... ~

~~*-o-..i.,.-.-

aa.

I 1

\\

1 Analythal Chemistry Division Manufacturer:

Carboiine Oak Ridge National Laboratory St. Lcuis, M0 Cate:

Aug. 16, 1978 x Steel Concrete 31ock System Identification:

193LF/191HB - Power tool clean CBA Test Results:

ORNL Master Analytical Manual Method No. 2 0922; A7-17-8 CRNL Log Book No. A 7562; I

4 Comments **

Samole No.

CSA Phase l

Ceatines intact, no defects, sides A, S.

S3-160 soray Coatings intact, no defects, sides A, 3.53-163 scray a

?

I 1

1 l

i

    • (SA) = sand blast; (SH) = shot biast; (GR) = grit clast.

' Irradiated.

s i

(.

Evaluated Approved I

e

1----'-

t a

11 1

DECONTAlfINATION TES'"

TEST PANEI. PREPARATION DATA

~'

l 1

j i

u

.i 1

l l

1 k

- v. :.,.

1 i

i Test Report No.

1 4

1

?

't

~ -- E

~~-

}

-_____.m_

, ;~.

c-

.1.

.e

_.s.

^

.?

?

ubT.NU.

Waoe 3 carbollrie 1

~

DECONTAMINATION TIST j

~

SECHTEL CP-952 AND A.N.S.I. N-5.12

/

TEST PANEL PREPARATICN DATA J

1 1;

pgdDUCT TO BE TESTED _

Carboline 193 U Primer / Carboline 191 E3 2;

nti SUBSTRA;E Cartified ASTM A36 Steel SIZE 2" x 4" x 1/4" Sandblasud to SS7C-5710-63 with a 1-3 mil blast 3.

SURFACE IEEPARATION (dese:1be) profile

' 4.'

PRODUCT DATA:

SAMPLE NO. (s)53-200 PRCDUCT APPLICATICN CONDITICNS THICXNESS DATE COAT PRODUC"-

CODES -

3ATCH i ME* HOD R/M(*Pl!R.H.

( in s. )

APPLIC le Carbo 11==

193 2 7E1949M Spray 74*/427.53-200) 3-10-78

.0032/.0033 Primer 71.2868H

.-g 7d181M Spray 80*/23:

33-200) 3-16-79 1c Carbo 11=e 1?! E3

.0043/.0046 7J2147M A

Primer 74-80 Primer 23-42 5.

C; KING CONDITICNS: AM31LYr TEMP. 73-73

'T REL. EMIDITY 33-56 Primer 6

N CURE 53 days DAYS f

s 6.

TEST PROCEOURE ORNL Master Aastyrical Manual Method No. 2 0920 DATE SU3MIA.a 5-M 3 1

7.

TES ING PERFORM BT i=alvtical Ch==# e rv Div.

Cak Ridge National Laboraccry

s. HJ
  • 0

/i

/) y TE.C REPCRT NO./SR-119 t

4 TS- 06376-1 i

~

e -.

    • H' e

e,., n me,, _,

,m

- - ! s,-. 3*..".

+..4,

- -.. -. ~..

~a.--...

s~

~.- -- - - -..-

0 l

I]

O e

UEMANON *TST REsta,73 es 1

4 i

g gb' 9

e n

t b

I l

0 Tes: Report No.

1 0

l v

I O

e w&.tm.a

>.aee

-M=e

.*M,a%6.G

+-

h.,.

3..

. :;p.7:

,5

. - ~ - ~ -

i Analytical Chemistry Divisten Manufactursr:

Carbeline Oak Ridge Natienal Laborator~v j

i St. L.

s. MO Date Auc.16,1978
0 Decentaminatien Test Resu1*J:

These tasts performed according to ORNL Master Analytical Manual Method No. 2 0920 and Sechtel Corp. Spec. CP-952.

ORNL Log Book No. A 7562; A7-17-8-I Pe Decontamination Factor (CF)

Water Acid Acid Activity l

Simple

.t

' Nu=ber

' Contaniinant 925'c 925'C 980*C Overall Rernevedl S3-200 Ce-144 50 2.1 6.9 710 (193Lc/1911G)

Ru-106 16 1.7 1.5 40 Cs-137

>2200

>1.5

>1.2

>4100 Ir-95 17 7.8 7.1

~ 34 TOTAL

' 40 1.9 2.4 180 99.4..

i I.

I 1

e 1 ercent of tith 1 activity removed = (1 - h) x 100.

P Approved A

~

AO

'4 g.

4 t

?

..-.._.4..

- - * ~ '

t..

-l I

l 9

j

  1. 9 5 #/f 4l NO l

1 d

a PHYSICAL PRCPER*II3 g

d a

I i

1 4

4

.1 I

I i

I t

t i

Tes Repor !!c. C i G ^

J 1

a h

=*

F 9 empp

-"*W.'4=m @$-4

.,gg

1 I

[ - * ~.. s _ -;.- c.*f

",. z _.-y.,5.;...:;:.

1 l

f j

i i

di t.ar*D 5!!n o~.

PHYSICAL PRG?!RT:E5 SECNTEL CP-9 54.C3 A. 't. i. I. N-3.1 Carboline 193 LF/Carbolise 191 F.3 J

1.

PRODUCT TESTED 4"x4"xl/32" s' teel Taber Abrasar ?anel 2.

TYPE SU35TnTE SURFACE PREPARATION (describe). Surface roughanad with sandpaper.

3.

~

15A, 16A, 17A 4

PRODUC"' CATA:

SAMPLE NCS.

RODUCT APPLICATION CCNDITICSS THICKNESS CA;E 4

CCAT P RODUC'"

CCDES BATCH i METHOD t h1(

  • F) *R. H.

( i.:s. )

APPLIED _

J Ic Carboli=a 193 1.F 8E163221 Spray 73*F/26 15A).CO33/.0035 12/16/7 1

1 8K240611 16A).003'./.0033 12/16/7 l

17A).0036/.0033 12/16/*

1 I

ic Carboline 191 E3 8K22S6:1 Spray 73*F/272 13A).0040/.0011 12/26/7 SJ182811 16A).0041/.0041 12/26/7 17A).0041/.0040 12/06/7 I

-\\_

C'JRINO OATA:e 5.

AP.3IENT TE!P. cs _7e e

  • ? REL. HCf. 9 7.s c e Crag TI,3g 4; j,y, s

6.

TEST P=.0CEDURE:

Bec ht el St andard CP 0 5!. and A.':. S. I. N-5.12 j

7.

TEST RESULTS:

7.1 ABRASICN

Federal Test :14thod Standard 111 Test Metnod 6192.

1000 cycles with it CS-17 vneel at:d. ICCO gram load.

l MICH -

38.3 =g.

AVERACE -

3 7.1. =g.

tE$ ~

36.6 =g.

i determined by une'of the ELCMETER ACHISION TISTIR j

T.2 A0llESICN:

AVERACE OF 5 TISTS psi 1

f DESCRISL FAILCRE 8

7.3

! REC *-Df?aCT RESISTANCE:

  • Curing Da:a - First Coa::

72-61*?

2 -6C: R.H.

la d:ys

(-

A:;fJVed:

b2 ;i

(

y 5-CG6-i p

~

J

+

i i

[

I O

  • OO-*MM F9 T @ M g.e-e, ge m gs..,g g y y g p 9*'*a= ham.

e _g 9

l l

l

7.

-a..

- ~. ~,, -

rm
.>.z.

7- _ - 5 3.g.. ;.-- -

o.

i l

,, 3 3 PHYSICAL PROPr.RTIES RECHTEL CP-954 AND A.N.S.I. N-5.12 1.

PRCOUCT TES E3 C'arboline 193 LF/Carbolina 191 H3 1

Cartif tad ASTM A36 - 2"x4"x1/4" steel panel 2.

77?I.SU3sT3 ATE 3.

SURFACE I' REPARATION (describe).

Crichlasted to S$7C-SP10-63 with a 1.0-2.0 =11 blast prof J.e.

i 4

PRCCUCT OATA:

SAMPLE ':05, 133, 163, 173, ISS, 193 e

k'RODUCT APPLICATION CONDITIONS THICKNESS OATE COAT P RCDUCT CODES BATCH !

M m.0D R/M(*FMR.H.

fins.)

APPLIED ic Carco11:a 193 LF SH165:21 -

Spray Iri/264 133/.V0J9/.0VJo A /16.

SK2406M 163).0038/.0039 12/16.

173).0038/.0039 12/16.

133).0038/.0038 12/16, i

19 3).0038/.0039 12/16; i

ic carboline 191 H3 SK2236M Spray 73*F/27:ll 133).0048/.0047 12/26.

SJ182SM 163).0040/.0040 12/26.

173).0051/.0043 12/26.

I e

183).0048/.0049 12/26, 193).0035/.0048 12/26.

1 t

l 1

5.

CURING DATA:*

ctaI ;t3E 52 days AM3IC;T TE:7. 61-79'T

  • F REL. act.

22-60*.

~

I Bechtel Standard CP-954 and A.N.S.I. % 5.12 6.

TEST PRCCIOURE:

7.

TEST RESULTS:

t.

i 7.1 A37.AS IcN:

Feders! Test :techod Standard 141 Test Method 6192, i

1000 cycles with a. C5-17 wheel and a 1000 gram load, s

i i

LCb -

H1CH -

AVERACE -

i l

f

  • 7.2 A0f tESIC'::

Deter =ined by une of the E1COMETER A0HESION TESTER I

630 p.g AVERACE OF 5 TESTS I

Cohesien of Carbo 11:a 193 LF i

i DESCRIZE FAIJJag 7.3

~;1 REC-;" PAC REs!STA!:CC:

  • Taria("Taca - frs f"Coac:

2 64-81*T 56 10 days i

l

^m/.\\

/

I G

Approved:

t_

t j

l V

.TS-C6376-4 j

)

m l

+--

4

~

LU s. < :f 4. '.L~ D

.?. ". _':. ;~;. :...

i.

J PHYSICAL PROPF.RTIES q

I 3ECHTEL CP-954 AND A.N.S.I. N-5.12 I

1.

PROCCCT TESTED Carbolice 193 LF/ Carboline 191 E3 1

2.

TYPE.SU3 STRATE Car-ified AS'IM A36 - 2"x4"x1/4" steel panel 3.

SURTACE PREPARATICN (describe) Sandblasted to SSPC-SPIC-63 wi h a 1.0-2.0 mil blas:

profile, y

4 PRCOUC DATA:

SA*.PLE NcS.

15P, ISP, 17P, ISP, 19P q

)RCCUCT APPLICATION CONDITICNS THICKNESS CATE CCAT PRODUCT COOES 3ATCH #

M E*HCD R/M(*F):2.H.

fins.)

APPLIED 1

1c carne 1A=a 193 tr Sa16aza spray 73 r/267.

15P).c02s/.c037 12/16/7 i

8E2406M 16P).0039/.0036 12/16/7 17P).0039/.0038 12/16/7 ISP).0037/.0038 12/16/7 19P).0037/.0038 12/16/7 q

ic Carboline 191 E3 SK2236M Spray 73*F/27 15P).0040/.0042 12/26/"

8J132EH 16P).0043/.0043 12/26/7 17?).C044/.0041 12/26/7 187).0041/.0042 12/26/7 197).0041/.0C42 12/26/7

~.

7c.,'

5.

C*.72tNC cATA:,

A '.3IENT TE:'.P.

61-79'?

  • 7 REL. HUM. 12-60 CURE !!ME 52 davs 6.

TEST PRCCIOURE:

Sechtel Standard CP-954 and A.N.S.I. N-5.12 9

7.

TEST RESULTS:

4 1

l 7.1 A 3 RAS ION:

Federal Test Method Standard 141 Tes: Method 6192, 1000 cycles with a CS-17 wheel and a 1000 gram load.

I HTCH -

AVERACE -

g-

  • 7.2 A0HE51CN:

Deter 3!ned by use of the ELCCHETIR A HESIO 4 TESTER AVERACC 0F 5 7ESTS 665 pst DESCRISE TA* *_7RE Cohesien of Csrboline 193 LT

,3 OIREC -I'*? C ?IsISTA!:CE:

l

  • Caring Oz:a - Firs: Coat:

64-81*7

$6-77: R.E.

10 days e

Approved:

uMr

.I3-C63764 l

t i

O

.4

_~

':.g.:.

,; &,._._ p' :

.O;, 7.. :..:..,

' 9 i';:_ ;..

t PHYSICAL PRCP".RTIES O

BEch7ET. CP-954 A:.*D A.M. S. I. N-5.12 1.

P'.00CCT TISTC Carboline 193 LF/ Carboline 191 H3 Cart.ified ASTM A36 - 2"x4"x1/4" s:eci panel 1

2.

TYPE SU3 STRATI Shochlasted to SS?C-S?10-63 wi:h a 1.0-2.0 11 3.

SURfACI PRI?ARATICN (describe).

blast pro:u e.

4 PRCCUC"' CATA:

SA.MPLE NCS.

15Q, 16Q, 17Q, ISQ, 19Q hRCDUCT APPLICATICN CCNDIT!0NS THICKNISS OATI COAT PRCOUCT CODES BATCH #

METECD R ht (

  • F ):R. W.

(ins.)

APPLID is Carboline 193 LF shlosz.'s spray W ii.h 15w.wa,,.002

..,.6/7 sc406M 160).0039/.0034 12/16/7 17Q).0035/.0036 12/16/7 13Q).0036/.0035 12/:.6 /7 ISQ).0038/.0033 12/16/

4 73*F[27%

15Q).0046/.0041 12/26/7 le Carboline 191 E3 8C236M Spray SJ182SM 16Q).0041/.0042 12/26/7 17Q).0042/.0040. 12/26/7 18Q).0044/.0041 12/26/7 1

19Q).0047/.0044 12/26/7 3

t 5.

CURING DATA:

AMBIENT TI:iP. 61-79*7

  • F REL. HL?i.

22-60%

CURE TIMI

$2 days 6.

TEST PRCCDURE:

Bechtel Standard CP-954 and A.':.S.I. % 5.12 t

l 7.

TT.ST RESUL*S :

I 4

7.1 A ER.AS ICN:

Federal Test :4ethod Scandard 141 Teve Me: hod 6192, 1000 cycles with a CS-17 wheel and a 1000 gram load.

LC' * -

HICH -

AVERACI -

  • 7.2 ACMESICN:

Determined by use of. the ELCCttETER AOHESION TISTIR AVI.UCC i1F 5 TESTS 670 psi DESCRISE TAILURE Cohesien of Carbcline 193 LT O!RIcT-!MPAC RESTSTANCEh 7.3

= Caring Oa:a - Firs: Coac:

64-81*F

$6-772 K.E.

10 days Ih/ y\\

i A; proved:

u,6

/

.TS- 06376-4 p

~

e m

l

~-

~

l 1

1 J

=_

^ ~. -?~L.

~ '

, g,- #

_,. a..

-e i

~

1 1

s i

PHYSICAL PROF UTIES d',"-

4 j

6-

)

SECMTEL CP-954 A::D A.N.S.I. N-5.12 I

Carbo 11na 193 II/Carbolise 191 E3 I

1.

PRCOUC; TESTED 2.

TTPE SUBSTRATE Schedula' 40 pipe,16" lens, 2.375" 0.D.

Critblasted to SSPC-SP10-63 with a 1.0-2.0 mil 3.

SURTACE PREPARATICN (describe).

oAas: pro:ne.

4.

PRCDUC* OA*A:

SAMPLE **05.

15C,16C.17C. ISC,19C, 20C. 21C I

l RCDUCT APPLICATION CCNDITIONS THICKNESS DATI i

CCAT PRCDUCT CODES 3ATCH #

METHOD R/M(*F):R.H.

(ins.)

APPLIED

'c Carboline 193 LI 831682x Spray W F/ W

C).004 0/.00D 22/16/7 i

sx2406x 16C).c040/.0038 12/16/7 17C).0039/.0036 12/16/7 i

i 18C).c040/.0035 12/16/7 j

j 19C).0036/.0032 12/16/7 l

2CC).0040/.0034 12/16/7 1

210).0039/.0036 12/16/7 l

ic Carbo 11=a 191 H3 8K2286M Spray 73*T/272 15C).0055/.00$0 12/26/7

~~

16C).0050/.0045 12/26/7 SJ182SM 17C).0046/.0056 12/26/7 1sc).c042/.c045 12/26/-

c',

19C).0052/.0058 12/26/~

5.-

CURINC DATA:,

q *c8E,, Q"'F~if*

883 u

. CugI" L,g '

~

24-602 AM3ICIT TEMP.

61-79'T

'T REL., HUM.

D Coat 81*F 28-492 36 days

  • ^i"t*NOC1 a - Firs:Beencel Scandard CP-954 Tf.

3GRE:

and A..f.S.I. N-3.12 4

6.

1 i

7.

  • IST RESUt.TS:

j i

7.1 ASRASICN

Federal Test Method Standard 141 Test Method 6192, j

1000 cycles with a CS-17 wheel and a 1000 gram load.

I i

HICH -

AV! PACE -

I

_LCt

)

i

7.2 ADHESIC5

Determined by use of the II.CCMETER A2HISICN TESTER l

AVERACC CF 5 TESTS asi 4

DESCRISI TAILURE I

7.3 DIREC*-IMPACT RESTSTA?:CE:

if31/79 Fine Nu=ber Effec: of 100 usi i=:se:

15C No Effect 16C 3/S" dela=isa ion pa1=: sepa:a:ed fro = pipe 17C No Ef fec:

18C

.No Effec:

i 19C 1/4" dela=ina:Los pais: separa:ed f::= pipe 20C No Effec:

21C 1/4" dela=ina:1on pa1= sepa:a:ed f::= pipe i

b

'{ j)

RISULTS REVII*ED ST

,. as u.

0

' vf I,

t

+

i

gi i --- - _.. _

O

  • 4 g

,y eb g

g g

d.

S O

E PAYE!,PREPARATIO.V AND INDIVIDUAI, CHD11CAI, RESISTAVCE TEST RESI.T.*S 9

6 i

e S

e e

4 ee 4

4 e

l C

1 O

6 0

0 Tes Report No.

r 6

M "U

Pe'*Me d.i#we69,..

a.4W p g h#

    • .de FMe gapp

-- ~ _ _ _. _ -

, ~-

.w 2.,..

.;,...,,o

.,g g.g y.g,,,3

,-- r. e

  • A..

4

. ~.....

,?

3 TIST NO.

01720 i

l CHIh CAL RISISTA!!CI TIST RISULid SICHTIL CP-953 and A.N.S.I. N-5.12 l.

TYPI SUBSTRATI:

SI I 2"x4"xb'CONCRITI S'"IIL%$*M A36 CTHIR 1

1.

SURFACI PREPARATICN (describe) : Crichlasted to 55PC-5710-63 with a 1.0-2.0 i

mil blas: profile 3.

PRCDUCT TESTID:

Carbolihe 193 LT/

SAMPLI NO.:'

15E i

Carboline 191 H3 l

0 PRCDUCT APPLICATICN CCNDITICNS

  • HICKNISS DATI i

j CCAT PROCUCT CCDIS DATCH 4 MITHCD R/M ( *?) tR.H.

(ins.)

APPLII l

le Carboline 193 LF

$H168:M' Spray 73*T/26:

.0C38/.0037 12/16 '

8K2406M j

i i

t 4

le Carbcline 191 H3 3X:286M Spray 7 3* i/ 27'l;

.0043/.0041 12-26 '

d SJ1828M

]

J 3

s 4.

CURING CCMDITICMS:

AM3! INT TIMP. (*F)

% RIL. HUMIDITY I,INGTH OF CU'JI i

iST coa:

72'F-81* F 25-49:

10 dcys j

24-60:

6 wee'n 2ND coat 61*7,-79'T 1

5.

'"YPE Cr TIST r CHIMICAL IXPCSURI TIST PER SICHTIL CP-953 and A.N.S.I. N-5-12 I

I 5'

  • y O

5*

'T SCL"TICN 75' i

6.

TIST TIMPIRA*URI:

AME! INT 75' 7.

CHIMICAL SCLU*ICN (pH and Concentration)r 5* Ni:ric Acid (;h =0.25) 8.

  • IST CBSIRVATIONS:

DA*I STAR *ID 2-5-79 g

t T

ACCIPTANCI CHIMICAL EXPCSCRI P2SC2,TS s

CRI*IRIA 1 CAY l 2 CAYS l 3 OAYS l 4 OAYS l 5 :AYS 1

l l

' NI l

l 8.1TLAXING/PIILINGl NI NI NE NI l

l l

8.2 CIL;_MINATI6N l

NZ NZ NZ lZ

I l lhIN. [.*^.',J l l1f6EinLPl 8.3 3LISTERING l
C NC
E la l

8.4 CTHIR ITTICTS l

I l

NE NI NE NI 4 -

E*,*IU,**.I _'N '" "# * # U 3Y G.O.v; / j i

NI-No Iffe::

NC= No Change l

r -

LP= Liquid phasa

$= 311sters

/

p/

E=

rdge T=

Tew TIST FIPCF.T NO.

..' L..

c. c o;,,,,,,,

a

~--

~ ' ~ ' * ~ ~ *

..-...y 7-.

~ ** f a+

. e:

I

~

= _ _ - _ -,

Q* *

  • f7 y *i'i

, n..._.,gy z.

-c

=... -

t t

TE.fi

..o.

0177.

CHI

  • AL RISIST)lICI TEST RISUI BICHTIL CP-953 and A.N.S.I. N-5.12 4

E.

TYPE SU3 STRATE:

SIZE 2"xc%"CCNCRITI STIILASTM A36 CTHI"4

o SS?c-3710-63 with a 1.0-2.'0 2.

SURFACI PRIPARATION (describe) :

Cri:biss:

i mil blast profile 1

J

  • \\

Carboline 193 LF/

SAMP!I NC.**

3.

PRODUCT TESTID:

J Carboline 191 EB 1

PRODUCT APPLICATICN CCNOITICNS THICXMISS ::ATI 1

CCAT PRCDUCT CCDIS 2ATCH I METHCD R/M(*?)%R.H.

(ins.)

APPLII Ic carboline 193 L7 8H1682M Spray 73*T/26:

0033/.0033 12,

8K2406M i

1 1e Carboline 191 R3 SK2256M Spray 73*7/27:

0050/.0048 12.

l 8J132SM r

i

.i 4.'

CURING CCNDITICNS:

AM3IINT "!MP.

(*T)

% REL. HUMIDITY I.INGTM C** CU'AI i

IST coac 72*-81*F 25-49:

10 days 220 coac 61*-79*T 24-60:

6 weeles 1

5.

YPE Cr "IST:

t CE.".! CAL IXPOSURE TEST PER BICHTIL CP-9 5 3 and A.N.S. I. N-5-12 j

+

I5*

~

3 6.

TIST TriPI?JsTURI AF.BII T 75*

$*

  • F SCLU"'ICN 4

5: Selfuri Acid (ph= C.8)

I 7.

CMIMICAL SCLU"'ICN (;E and Concentra:icn):

i 2-5-79 l

8.

TEST CBSIRVATICNS:

DATI STARTID I

f ACCIPTANCI CHIM! CAL EXPCSURI RISU2.TS

~

CRITIRIA 1 CAY l 2 CAYS l 3 CAYS l4 ::AYS l 3 OAYS

~

j l

NE NI I

  • NE NE 8.1 T!. AXING /PIILING F-l f

NI l

U E

E E.2 CILAMINATICN 1

l I nf 3 cn I p ar.5 en i

y*

8. 3 3LIS~IRI'*G l

h.a 1

I t. LP Ifa:e in 1? l l_

l l

U U

E NE S.4 CTEIR ITTICTS NI= No E8 fee:

':C= N.: Chang

  • RESULTS F2VII4ID BY Nb[

= Few E=,r.dg e f) 7/ hY i

i i

LP= Liquid Phase B= 311s:er

37 7;pog; go, e

'*aAt,-

i 4

i

. y..

u

..,x..__.

r ir y-a erwr 4:

e

  • + - +

a-M-

esw g-ew**y-T--sr-w y

  • 1-

-e m

  • -w w

mus M

=-

. yy..,m. y,

..m..w - ~

,,*-s.,

",o

~

-~..-.. -

t 4

t 4

TIST NO.

01720 Ch*IMICAL RISISTANCI TIST RISULTS O

BICHTIL C?-9 5 3 and A.N. S. I. N-5.12 j

AS" SI: 2"xt."x1/4dCNCRITI STIIL us" CTHIR 1.

TYPE SUBSTRATI:

r.

~

[

2.

SURFACE PRIPARATICN (describe) : Cri: blasted to SSPC-SP10-63 vich a 1.0-2.0 4

1 aL.L DJ.ase proma.

13G Carbolina 193 LF/

SAMPLE NC. *

3. 'PRCDUC" TIS *ID:

Carboli=a 191 H3 i

P RODUC'"

APPLICATION CCNDITICNS THICICIISS OATI CCAT' PRCDUCT CCDES 3ATCH i METHCD R/M ( *?) %R.H.

(ins.)

APPLIII i

ic carboline 193 LF SE168 E Spray 73*i/25

.0038/.0039 12/15/

1 8K2406M

{

ic Carbo 11:a 191 H3 8K2286M Spray 73*T/27

.0043/.C041 12/25/*

8J1828M i

4.

CURING CCMDITICUS:

A.w3II'C TIMP.

(* T)

% RIL. HUMIDITY LINCTH Or CU2I 1st coat: 72*F-81*F 282-48:

10 days 2nd coat: 61*F-79'T 24 -60:

6 weeks 5.

"YPI Cr TIST:

N ICAL EXPCSURI TIST PIR 3ECH*IL CP-953 and A.N.S.I. N-5-12 9

6.

  • IST "I24PEPATURI:

AMBII C 75* + 5'

'T SCLUTICN 75*

5' ey 7.

CHIMIC.C,SCLOTICN (pH and Concentration) : 5: Eydra:1:a (;E = 10.75) 1 8.

TIST CESIRVATICNS:

DATE STAR"'ID 2/5/79 f

4 ACCIPTA!!CI CHI.v.:CA:. IXPCSORI ?.ISULTS CRITIRIA 1 hY' l 2 CAYS l 3 CAYS l 4 CAYS lSI OAYS j

i l

f l

h'E l

l l

NE NE NE 8.1 TIARING/PIILI:G NE l

l NE l

N7.

l l

S.2 CII.AJC::ATICN l

i NE NE NI f

l l

l i

l NE NE NI NE NE 8.3 ELIS IRING l

f _ NI -

l NE 8.4 CTHIR ITTICTS NI NE NI

\\_[a/./l/,.,

i i

,, S U..S r :.... a s,, 3y o

i l

NE = No Effect

()

G

')

t

  • TIST REPCST NC.

n......

I

_. -.. _.. _ _ _ _. _ _ _. - ~.. _ _ _, _.... -... ~ _..

- i."<+- -.

z,q,y,y.

-+

1rci.2 - -

i 4

4 b

TL.4r du.

v6*6w r

CHE CAL RESISTANCE TEST'FISUI BECHTEL CP-953 and A.N.S.I. N-5.12 U

l.

TYPI SUBSTRATI:

SIIII"::4"xh"CCNCRETI STIII/sSTM A36 CTHEM 2.

SURFACE PREPARATICN (describe) : Cri:blas: :o SS?C-S?lo-63 vi:n a 1.0-2.0 l

all blas: profile Carboline 193 LF/

SAMPLE NC.:*

15R 3.-

PRCDUCT TESTED:

Carboline 191 K5 PRCDUCT APPLICATICN CCNDITIONS THIC.<NES S DATE CCAT PRCOUCT CCDIS 3ATCH i ME'"HCD R/M ( * ?) 1h R. R.

(ins.)

APPLII le Carbo 11ne 193 LF 8H1682M Spray 73*T/26

.CO37/.0033 12-16 ~

8K2406M Ic Carholine 191 E3 8K2236M

' Spray 73*F/27*

.0C45/.0040 12-26-:

8J182SM 4.-

CURING CCUDITICMS :

.. L.

4 AMBIENT TEMP. (*F)

% RIL. HU M DITY LENGTH Cs' CTRE IST coat 71*-81*T 28-49I 10 days 2ND coa: 61*-79*7 24-60 6 weeks S.

TYPE CF TEST:

CHIMICAL EXPCSUP2 TIST PER SICHTEL CP-953 and A.N.S.I. N-5-12 6.

TEST *EMPERATCPI:

AMBIINT 75*

  • 5'
  • F

~

SCLU'"!CN 75*

  • 5'

'T 7.

CHEMICAL SCLU"ICN (pH and Concentra:icn): SI Sedi'= Hyd::xide (ph=11.75) 8.

TEST CBSIRVATICNS:

DATE STARTID 2-5-79 ACCIPTANCI CHE.CCAL EXPCSUF2 ?250L;S i

CRITIRIA 1 CAY l 2 CAYS l 3 CAYS l 4 ::AYS l 5 *:AYS l

l NE l

NI l

8.1 TLAXING/PEII,ING l NZ NE NE l

l I

l 8.2 DELAMINATION l

NI NE NE NE NE w

l vat 3 On &

k NO l

NO l

8.3 ELISTERING l

NE 1#2-6h :n E, l

l NI l

NI NE NI

8. 4 CTH::R ErrIC-S
I A/ (g NE= No Effec:

5= 311 ster 3

g.7 9...gzc *,y

~~

"a**

NC= No Change EA= 3ack

{},_'

f) ')

E= Edge T= Tev

,,S P2P C,...

.. ~.

C

  • ' - ~ ~.

- - ~ - - - - - - -

}

L_.-

.x. qwo,. z..;., ;;

...... 2.u a-

~

i J

TEST NO.

01720 i

CHIMACAL RISISTANCI TIST RISULTs BECHTIL CP-953 and A.M.S.I. N-5.12

-4.,

1.

WPI SU3 STRATI:

SI*I 2"x4"x1/dbsCRITI STEIL @

CTHI'4 l

2.

SUP. FACI PRIPARATION (describe)

Get: blasted to SS?C-SP10-63 wi:h a 1.0-2.0 f

a1.L blast profala.

3. ' PRODUCT TISTID:

Carbolins 193 LF/'

SAMPLI NC.:

13-1 i

Carbolina 191 EB i

e PRCDUCT APPLICATICN CCNDITICNS THICXNISS CATI i

j CCAT PRODUCT CCCES EATCH i MITHCD R/M (

  • F) )R. H.

(ins.)

APPLII:

a 1

e

~

Ic Carbolina 193 LF 8H168:M Spray 73*F/267.

.0033/.0035 12/16/

812406M i

k

}

ic carbo 11ne 191 HB 8K2236M Spray 73*F/27

.0042/.0041 12/26/7 1

8J1828K t

i.

l t

1 4.

' CURINO CCNDITIONS:

i AMBIINT TEMP. (*?)

% REL. !!UMIDITY LINGTH Of CU LI I

lac coat:

72*-81*F 28-49E 10 days I

l 2nd coat:

61*-79'T 24-60%

6 vaaks i

I.

5.

TY7I CF TEST:

i

}

CHIMICAL IXPCSURE TIST PER BECHTIL CP-953 and A.N.S.I. N-5-12 6.

TIST TEMPERATURI:

AliBIINT '

75*

  • 5'

'T SCLUTICN, 75* - 3'

  • F 7.

CHIMICAL SCLU'"ICN (pn and COncent-ation) :

5: A=meniu:n Evdr=xide (;E = 11.6) 8.

  • IST CBSIRVATICNS:

CATI STARTID 2/5/79 i

i i

l i

ACCIPTANCI C1!IMICAL EXPCS;RI RISULTS i

i CRITERIA 1 CAY l 2 CAYS l 3 DAYS l 4 CAYS l 5 OAYS l

l l

l l

l f

3.1 FIAXING/PIILI::G l NE NE NE NE NE l

l l

l 9.2 CILAMINATICN l

NE NE NE NE NE l

l l

l NE NE NE 8.3 ELISTERING NE NE f

f f

NE NE 8.4 CTHIA IFFECTS NE NI NE S

8 W

V yV i

, n T RIPo r NC.

l.

4

,e..

-.. ~,y

.v.

-_m

~3

,. - ~. -...

...--.....,.,,--e.,..._..--.,..,__.-w..m-y-,

--..,m,.-.,

q.py _

,,w..

J J

a

~

~

TIST No.

01/20

~

CH'. ICAL RISISTANCI TEST RISU..i BICHn L CP-9S3 and A.N.S.I. N-5.12 l.

TYPI SU3 STRATI:

SI*.II"x4"x5"CCNCRITI STIIIASTM A36 CTHIM i

2.

SURTACI P E?ARATICN (describe) : Cri:blas: :o SSPC-5710-63 vi:h a 1.0-2.0

. mil blast profile Carboline 193LF/

SAMPLI NC.**

15J 3.* PRODUCT TISTID:

Carbolina 19185 1

1 e

P RODUC"'

APPLICATICN CONDITICNS THICKNISS DATI e

CCAT PRCCUCT CCCES 2ATCH #

MITHCD R/M (

  • T) ) R. H.

(ins.)

AP P LI-j J'

ic Carboline 193 LF 8H1682M Spray 73*T/26:

.0037/.0038 12 -

8K2406M i

0 t

Ic Carboline 191 F.3 8K2286M 5 pray 73*F/27:

.0043/.0043 12 l' i

8J182SX t,

f I

1 4

4.- CURING CONDITIONS:

j

,j..

IW.BIINT TEMP. (*T)

% RIL. HUMIOITY LINGTH CF CU2I i

1ST coac 72*-81*7 28-49:

10 days 2ND coat 61"-79'T 24-40:

6 weeks 4

S.

"'t?I CT TISTs CHIMICAL IXPCSURI TIST PER SICHTIL CP-953 and A.N.S.I. N-5-12 I

5*

  • T i

6.

TEST TEMPIRATURI:

AMEIINT 75* I

'T SCLC"!CN 75*

I CH -.ICAL SCLC"'ICN (pH and Concentration) : $! Sodium scrate (ph= 9.7) 7.

J

}

2-5-79 8.

-IST C=SIRvATICNS:

DATI STARTsc ACCIPTANCI CHIMICAL EXPCSCRI RISULTS CRITIAIA 1 OAY l 2 CAYS l 3 CAYS l 4 CAYS l 5 OAyS l

  • NI l

l 8.1TLAXING/PIILINGl NI NI NI NI l

l l

i i

NI NI NE I

8.2 CILAMINATICN NI NI l

l

(

~

8.3 3LISTIRING l

NI NI I

XI NI f

8. 4 CTEIR ITTIC"'S l

NI NI NI NI NI RISUL"S PC'*IWID 3Y M,k gI. No gfgee:

/

TIST RIPC'.T No.

l

- ~ :.v.

~

. _3 p.p: ~. g,,4 A

TEST NO.

01720 4

CHEh.0L RESISTANCE TEST RESULL l

BECHTEL CP-953 and A.N.S.I. N-5.12 y

1.

TYPE SUBSTRATE:

SIOE

[CNCRETE STEEL M CTHE*4

.l 2.

SURFACE PREPARATION (de scribe) :-

Cri: blasted to SSPC-5710-63 vi:h a 1.0- 2.0 a u oAas; pro m e.

3. " PRODUCT TESTED:

Carbolina 193 LF/

SA.MPLE NC.*

15K Carbolina 191 HB

'4 PRCDUCT APPLICATICN CONDITICNS THICKNESS OATE CCAT PRCCUCT CCDES BATCH 4 METHCC R/M(*F)%R.H.

(ins.)

APP L!E:

Ic Carbolina 193 LF

.SE1682M Spray 73*F/26:

.0038/.0036 12/16 8K:406M i

1:

Carbo 11== 191 E3 8K2286M Spray 73*F/27:

.0042/.0043 12/26 SJ1328M 1

Ii s

l 4.

CURING CONDITICNS:

7..

Aw.3IENT TEMP. (*F)

% REL. HUMIDITY I.ENGTH C7 CU".tE L

l 1st coat:

72*-81*F 23-49:

10 days

~

2nd coa::

61*-79'T 24-60:

6 weeks i

5.

TYPE CF TEST:

s l

CHEMICAL IXPCSURE TEST PER BECMTEL CP-953 and A.N.S.I. N-5-12 S.

TEST TEMP!RATUFI; AMBIENT 75* + $*

  • T SC10 TION 75* * $*
  • ?

g 7.

CHEMICAL SCTUTICN (pH and Concentratien) :

0.5M sodium Fluoride (;H = 6.6) i 8.

TEST CBSERVATICNS:

DATE STARTED 2/5/79 I

~

ACCIPTANCE CXIMICAL EXPCSUP2 P250LTS CRITERIA 1 CAY l 2 CAYS l 3 OAYS l4 CAYS l5":AYS l

l l

l NE E

' NE 3

8.1 TI. AXING / PEELING E

NE l

f l

l f

8.2 CELAMINATICN l

NE NE NE NE NE l

l

\\

8.3 3LISTERING l

l NI NE NE HE NE l

l, NE.

l n

NE l

8.4 CTHEa ErrE TS 3E n

W #.U !)

~

t

=. 2 5 S = ev -,- s = v.

uz g, gig,,,

U yv TES: REPCRT No.

r

= -...

~

=-

.n.

- ~ '

?

-._...._.__n

j l

4 TIST NO.

01720 CRIM1 CAL RISISTANCE TIST RISULTd BICM"'IL CP-953 and A.N.S.I. N-5.12

-k a

S!:I"*'"*1/YCNCP2TI STIIL k3IM CTHER I

l 1.

TYPE SUBSTRATI:

1

2., SURFACI PRIPARATICN (describe) :

Cri: blasted to SSPC-SP10-63.

I i

l I

3.

PRCDUCT TISTID:

Carbolina 193 LF/

SAMPLI NO.:

15L 1

f I

Carbolina 191 E3 1

i APPLICATICN CCNDITICNS

  • HICKNISS CATI e

PRCDUCT CCAT PRCOUCT CCCES BATCH i MI*HCD R/M (

  • F) % R. H.

(ins.)

APPLII:

i J

)

is Carholina 193 LF 821682M 5 pray 73*T/26:

0037/.CCJ6 12/15/

t 812406M ic Carholina 191 E3 812286M Spray 73*T/27:

.0043/.0041 12/ $/*

i I

8J1828M I

d

)

i a

n

/

i 1

4.

' CURING CC:!DI*ICNS :

+

1 AMBIIN" TEMP. (*F)

% REL. HUMIDITY LINGTH Cr CU1:I i

ist c:at:

72*-81*F 28-49 10 days Ind coat:

61*-79*7 24-60 6 vuoks I

1 i

5.

YPE Cr TIST:

.I 1

)

CHIMICAL EXPCSURI IST PIR BICHTIL CP-953 and A.N.S.I. N-5-12 i

j 6.

IST TEMPIRA*UF2:

AMSIINT no<*

  • F SCLU"'ICN 75* - 5'
  • y 7.

CHIMICAL SOLO *ICN (pH and Cc=centracien) :

5 cit-1 Acid NH = 1.65) j 8.

  • IST CBSIRVATICNS:

OATI STARTID 2/5/79 4

i

+!

+

i nCCIPTANCI CHIM! CAL EXPCSCRI RISULTS i

i I

l l

CRITIRIA 1 CAY l 2 DAYS l 3 CAYS l4 CAYS l 5 CAYS l

NE NE

  • NE l

l 8.1TLAXINC/PIILI!1Gl NE NE l

f f.

NE NE l

8.2 CILAMINATICN NE NE NE f

NE NE NZ l.

NE l

l NE

[

8.3 3LIS IRING l _ NE.

l l

1

(

NE i

E.4 CTHER ITTICTS NE NI NE RISULTS FIVIIWID EY kb) a. N. E 1.e=

V i

0 I 1

, TIST FIPCRT NC.

5

..,.-.3,..,.....-

.. + - -

l I

t.

~

pya.

-g.

. 7 ;,4. g..,.,

,.7,,_,,

.g 4

i TIST NO.

01720 CHIMACAL RESISTANCI TEST RESULT 3 i

BECSTEL CP-953 and A.N.S.I. N-5.12 SI I "x4"x1/fCNCRITI STIEL @*

CTHIM 1

2 I

1.

TYPE SUESTRA"*I:

l 2.

SURFACI PREPA.'ULTICN (describe) :

Critblasted to SSPC-SP10-63 #.t!. a 1.0-2.0 i

mil blast prof 11a.

i j

3.
  • PRODUC" "ESTID:

Carbolina 193 LF/

SAMPLI NO.-

15M Carbolina 191 E3

-g' i

PRCDUCT APPLICATICN CONDITICNS THICKNISS DATI l

l CCAT PRCDUCT CCDES BATCH i METHOD R/M(*F)%R.H.

(ins.)

APPLII:

ic Carbolina 193 LF 881682E Spray 73*T/26:

.0037/.0038 12/16/

l

)

i SE2406M 2

5 1

ic Carbolina 191 EB 8E2286E Spray 73*T/27:

.0042/.C042 12/26/~

i SJ1828M l

t 1

1 I

1

=

4.

" CURING CONDITICMS:

I I I j

W AMs!ENT r.v.P. (*r) t nEL. En !:ITY 1EnGTx cr cUnr l

ist coat:

72*-81*7 18-49%

10 days 4

t' 2nd coat:

61*-79'T 24-6C%

6 weeir.s 4

i

5. ' TYPE CF TEST:

j I

i CHEMICAL EXPCSURI TIST PER SECHTIL CP-953 and A.N.S.I. N-5-12 i

l i

1 6.

TEST TEMPERATUPE:

AMBIINT 75* t 5*

  • T SCLUTIIN 75*

5*

  • r 7.

CHIMICAL SOLC"'ICN (pH and Concentration) :

0.3M Eydrogen Peroxide (;E = a.5) t 8.

TIST CBSITJATICNS:

CATE STARTID 2/5/79 i

l ACCIPTANCI CMIMIIAL EXPCSURI RISULTS l

i I

CRI-IRIA 1 CAY l 2 CAYS l 3 CAYS l 4 IAYS l 5 CAYS j

)

f I

l Ng NI

'NE l

l 8.1TLAXING/PEILINGl NZ NE NI l

8.2 CILA.MINATION l

l l

l Nr Nr Ng NI l

l 4

l l

NI l

6.3 ELIS* IRING l

l l

NI Nr NI NI l

i l

Nr

_x i

s.4 CTxIR trrIC S N

Nt Nr 1

I 5ULIS RZv EwIU IY

- -)\\

f NE = No Effect V

02

. TEST RIreRT NC.

1 I

l 1

e-,-r

...y

.,-2--

---r. - -..

.e w

-mwm.,.

,,.#r e,-

.t-

.~-,-w--,-----.-c,-n7,n-m-+ew--w-e--r---~'-w--w----r-1.m e-w -r-w -

<:y.

'7y.>.

4: yg.t v -,

m :aq -

~_ ;

. w.'

y n

w--

- - - ~, >,.

t.

1 l

.t CHIP TAL RISISTANCE TEST RESUL**

.. ~.

BICHTIL CP-9 5 3 and A.N. S. I. N-5.12 J

.m 1.

TYPE SUBSTRATI:

SIZI "x4"xh" CONCRITI STII A$nt A36 CTHI4

/

2.

SURFACI PRI?ARATICN (describe) : Grieblast to SSPC-SP10-63 1.0-2.0 sil blast erofile 15 N

3.. PRCCUC"' TISTID: Carboline 193 LT/

SAMPLI NO.:

Carboline 191 HB PRCDUCT

. APPLICATICN CCNDITIONS TH*CXNISS CATI CCAT PROCUdT CCCES BATCH i MITHCD R/M (

  • T) %R.R.

(ins.)

APPLII i

Ic Carboline 193 LT 8H1682x Spray 73*T/26%

.0038/.0037 12 8K2406M 1

l l

Ic carboline,

191 HB 8K2286M Spray 73*T/27

.0041/.0041 12 '

EJ1828M 4.

CUR *NG CCNDITICNS:

O AMBIINT T.P.

(*F)

% REL. HUMIDITY LINCTH 07 CURI 15; coa: 72*T-81*T 28-49:

10 days 2ND. coat 61*-79'T 24-60:

6 wee *a

.i 5.

TY7I CF '*IST :

CHIMICAL IX7CSURE TEST PIR BICHTIL CP-953 and A.N.S.I. N-5-12 6.

'"IST TEMPERA'"URI AME INT 75* t

  • T SCLUT CN 75* O 5*

7 7.

CHIMICAL SCLUTICN (pH and Ccncentration) : 0.3M Potassium Per=anganate(ph= 5.0 8.

TIST CBSIRVATIONS:

CATE STARTID 2-3-79 ACCI?TANCI' CHIMICAL IX?CSURI.USULTS CRITIRIA 1 CAY l 2 CAYS l 3 DAYS l 4 CAYS l 5 CAYS j

l l

l l

l 8.1TLAXNG/PIILINGl

.E NE SI NE NE l

l l

l NE NE NE NE 8.2 DELAMINATICN NE l

l l

l 8.3 3LISTERING l

l NI NE NI NE NE 50 CD 6.4 CTHIR ITTICTS in LP NC NC NC NC 1

.NI

..o r.4:e::

SEV= Severe NC* No change C3= Cca:ing discolorat.?50UEIS EIYIINIU *"

' j [/y ?[

8 LP= Liquid phase

(}

GV g=**q-NP's4 se se e-e 69.'w.=

W W M 939eeepegyg M M_

p+N4$ Mg g

-g

4

i u.

~g e ; y; a-

... n.gg

. 3.t

r..,-

m_~

m w

-- u w..

.i 4

TEST NO.

01720 CHEM AL RISISTANCI TIST D.ISUL t

RECHTEL CP-953 and A.N.S.I. N-5.12 1.

TYPE SUBSTRATE:

SI:Z2"x4"z1/YCNCRITE STIIL @

CTHI4 2.

SURTACI PRIPARATION (describe) :

Cri:blasced to SSPC-SP10-63 with a 1.0-2.0 mil blast proff.14.

3. ' PRODUCT TESTED:

Carbolina 193 LF/

SAMPLE NO.:

15-C' 4

Carbolina 191 ER l

W 4

PRODUCT APPLICATICN CONDITICNS TH!CXNISS OATI CCAT P RCCCC"'

CCCES 3ATCH 3 MITHCD R/M(*F)4R.M.

(ins.)

APPLII:

le Carbolica 193 Lr sE1682M Spray 73*T/26:

.0039/.0037 12/16/'

8E2406M ic carbo 11aa 191 H3 SK:236M Spray 73

  • T/ 27*.

.0048/.004: 12/26/*

SJ1828M l

t 4

4.

'CURI'*G CCNDITICN? :

A!'3! INT TI:P. (*F)

% REL. HUMIDITY LINGTM C? CUnI ist coat: 7 *-81*T 28-49%

10 days 2nd coat:

61*-79'T 24-40:

6 week.s 5.

TYPE C7 TEST:

CHEMICAL EXPCSURE TIST PIR BECHTIL CP-953 and A.N.S.I. N-5-12 6.

TEST TI:GERA"'JRI:

AM3IINT 75* + 5'

'T SCLUT*CN 75* t 5'

'T 7.

CHEMICAL SCLUTION (pH and Cencantratien):

1.0 lb/1 gal. Trisodha Phosphate spa = u.as l

8.

TEST CSSIRVATICNSt DATI STAATED 2/3/79 i

t ACCIPTA*CI CHEM

  • CAL EXPC50P2 ?iSULTS Cn!"IRIA 1 CAY l 2 CAYS l 3 CAYS l4 CAYS l 5 :*AYS l

l l

l NE NE NE 8.1 TLAX**G/PIILING NE NE l

l l

8.2 OELA".*NATICN f

NE l

NE NE NE NE l

l l

NZ l

NE S.3 3* :S IRING l

NZ JE NZ l

NE, l

l S.4 C"XIR ET7ECTS l

NE NI NE NE l

r 3.,.S.

5 Rbv. a c.,.y %Al './ f /. Q w.

.c s.

NE = No E!Iec:

V gV 8

TEST REPCS.T NC.

I l

4

  • u***
  • * * * =
  • s hao

.w,g,,

,g-

,e,,.,

i 1

.. q.. ;,,

v.- m,

<m

._.u i

f 1

TEST NO.

017 0

" AL RISISTANCI TIST R.ISULO CMI.v.

O,*....

BICM'"!L CP-9 5 3 and A.N. S. I. N-5.12 2%N/{CNCRITE

$~IIL M CTHIR

~

1.

TYPI SUISTRAT_E: SI:1 l

2.

SURTACI PREPARATICN (describe) :

Critblasted to SSPC-SP10-63 wi.h a 1.0-2.0 au o.as: prozna.

Carbolina 193 LF/

SAypLI No.:

15 R

3. 'PRCCUC" "!STIo Carbolina 191 MB

(

P RCDUCT APPLICATICN CONDITICNS THICKNISS CATI i

CCAT P RCCUC'"

.CCIS 3ATCH i MI"'HC D R/M(*?)%R.H.

(ins.)

APPLII:

j ic Carboline 193 LF 8H1682M Spray 73*F/26:

.0339/.0038 12/16, I

8E2406M I

le Carbolina 191 E3 8K2256M Spray 73*F/07:

.0044/.0042 12/26.

8J181SM i

t i

e 4.

CURING CCNCITICMS:

AM3IIN':' TIMP. (*T)

% RIL. HU$4ICITY LI"CTH OF CUSI ist coat:

72*-81*T 28-49 10 days 2nd coat:

61*-79'T 24-60:

6 week.s i

5.

"YPI CF TIST:

i i

i CHIMICAL IX7CSURE TIST PER SICHTIL CP-953 and,A.N.S.I. N-5-12 e

6.

TEST TIM 7IRATUPIt AMBIINT 7s* + s*

  • T SCLUT CN 75*
  • 5'
  • ?

7.

CHIMICAL SCLU* CN (pH and Ccncentration) :

5 Oisodium Phosenate (-E = 3.5) t i.

8.

TIST CBSIRVATICNS DATI STARTID 2/5'/79 t

i ACCI7TA2:CI C:iIMICAL IXPCSURI ?.ISCLTS CR*TIRIA 1 OAY l 2 OAYS l 3 OAYS l 4 CAYS l 5 OAYS l

l 8.1TLAXINC/PIILINGl NE NZ NI XI

' NZ l

l l

8.2 OILAM:!!AT CN l

l NZ NE NE NE NE l

l l

l l

9.3 2*!STIRING l

NI NZ NE NE NI l, NE d

8.4 CTHIR ETTICTS NI NI NE NE RISCLTS 75VII*<TIO BY hk *[.b, k NE = No,,.,act 0

hl 5

TEST PIPOP.T No.

j a

.. y,

. - - ;., -c..

a.

,.c, r.

9, ti 3

.4

,. e t

J-SUMtfARY CT CE.MICAI, EXPCSLTI RESL'I.TS s

a

}.

1 l

Os.*.+6

  • !{

s f

Test Report No.

8 e

1 4

0 O

eme a

4

,g.

gg

,g

+

mm

P

}

J I

t C,C,."( O CIn C SICHTIL CP-951 AND A.N.S.I. N-5-12 CHIMICAL RESISTANCI TIST AISULTS Cuboline 193L7/ Carbo:,1=e 191 M3 CCATING SYSTEMS:

S t.

Sn St 51 0.30 M 51 CITRIC NITRIC SULTURIC HYORCGIN SCC:UM

'ROCUCT TISTID ACID ACID HYDRA :NI ACID PIRCXIII HY::RCXI t

pass fail pass fail pass pass O.5M Sn 51 0.30M 1.0t/ gal.

5%

PCTASIUM SCDIUM SCCIUM AMMONIUM P IPp.AN.

Tg:SCO gM c: Scc:gg TRCOCCT TISTID TLUCRI I BCRATI HYDRCXIOI CANATI PHCSPHATE PHCSPHATI j

I pass pass pass pass pass pass o,

d I

i i

t

,1 M i

725U:.TS AsPRCvI:

4'. s'(y,6 t

s 4

!\\

]

U TIST ?2?CRT NC.

\\017 0 i

I e

f. V
S-06376-6 89 espe.

- - - _ _ _ _ _ _ _ _ _ _ _ _ - - - - - - - - - - - - -.. - _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _

Retrieved from "https://kanterella.com/w/index.php?title=ML20138P014&oldid=4197079"