ML17324B209

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Forwards Application to State of Mi Dept of Natural Resources for Mod of NPDES Permit Mi 0005827 to Allow Discharge of Make Up Plant Prefilter Backwash Water Into Lake Michigan
ML17324B209
Person / Time
Site: Cook  American Electric Power icon.png
Issue date: 01/22/1987
From: Alexich M
INDIANA MICHIGAN POWER CO. (FORMERLY INDIANA & MICHIG
To:
NRC OFFICE OF INFORMATION RESOURCES MANAGEMENT (IRM)
References
AEP:NRC:0170C, AEP:NRC:170C, NUDOCS 8701290188
Download: ML17324B209 (46)


Text

't'EGULATORY p

FORMATION DISTRIBUTION -SY .M (R IDB) l.

ACCESSION, NBR: 8$01290188 DOC. DATE: 87/01/22 NOTARIZED: NO DOCKET FACIL: 50-'315 donald C. Cook Nuclear Power Planti Unit ii Ind iana 5 05000315 50-316'Donald C. Cook Nuclear Power Planti Unit 2. Ind iana 5 05000316 AUTH. NAME AUTHOR AFFILIATION ALEXICH> M. P. Indiana 8c Michigan Electric Co.

RECIP. NAME RECIPIENT AFFILIATION Document Control Branch (Document .Control Desk)

SUBJECT:

Forwards application to State of MI Dept of Natural Resources for mod of NPDES Permit MI 0005827 to allow discharge of make up plant prefilter backwash water into Lake Michigan.

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INDIANA 8 NICHIGAN ELECTRIC CONPANY P,O. BOX 16631 COLUMBUS, OHIO 43216 January 22, 1987 AEP:NRC:0170C 10 CFR 50.36 (b)

Donald C. Cook Nuclear Plant Unit Nos. 1 and 2 Docket Nos. 50-315 and 50-316 License Nos. DPR-58 and DPR-74 NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM (NPDES) PERMIT Nuclear Regulatory Commission Attn: Document Control Desk Washington, D AC. 20555

Dear Sirs:

In accordance with Section 3.2 of Appendix B (Environmental Protection Plan) of the Donald C. Cook Nuclear Plant Unit Nos. 1 and 2 Facility Operating License, attached is a copy of an application to the State of Michigan Department of Natural Resources for modification of the D. C. Cook NPDES Permit No. MI 0005827. This application is for your information only and has been submitted to the State of Michigan for approval of a facility change which would allow discharge of make-up plant prefilter backwash water to Lake Michigan.

This document has been prepared following Corporate procedures which incorporate a reasonable set of controls to insure its accuracy and completeness prior to signature by the undersigned.

Very truly yours, M. . Ale ich Vice preeidene cm Attachment cc: John E. Dolan W. G. Smith, Jr. - Bridgman R. C. Callen G. Bruchmann G. Charnoff NRC Resident Inspector - Bridgman J ~ G. Keppler - Region III 87012'70188 870122 PDR ADOCK 05000315 .

-P PDR pe%

ATTACHMENT TO AEP:NRC:0170C NPDES PERMIT APPLICATION LETTER FROM JACK A. DRUCKEMILLER (I&MECo)

TO PAUL D. ZUGGER (MICHIGAN DEPARTMENT OF NATURAL RESOURCES),

DATED DECEMBER 23, 1986

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. eattachmect tc REP:NRC70C

~ eeeeemmee INDIANA & NICHIGAIVEIECTRIC CONPANY ONE SUMMIT SQUARE, P.O. BOX 60. FORT WAVNE, IN, 46801 Telephone (219) 425 2111'ecember 23, 1986 Paul DE Zugger, Executive Secretary Water Resources Commission Department of Natural Resources P. 0. Box 30028 Lansing, Michigan 48909

Dear Mr. Zugger:

RE: Donald C. Cook Nuclear Plant NPDES Permit No. MI0005827 Enclosed is a revised Industrial and Commercial Wastewater Discharge Application for the Donald C. Cook Nuclear Plant. This application is submitted for approval of a facility change.

The facility change involves rerouting of Makeup Plant Prefilter back-wash water to Lake Michigan via outfalls 001 or 002 (Unit 1 and Unit 2 discharges). The filter backwash water is currently discharged to the Plant's Turbine Room Sump, which subsequently discharges to an onsite Absorption Pond. The ability to discharge this effluent to Lake Michigan would aid us in performing repairs to the sump and would allow us to reduce the volume of groundwater discharges. Screening data for this waste stream is provided in the enclosed application.

Note that the line diagram flowsheet for Section 1, Item 6 is as pro-posed, reflecting the planned rerouting of the filter backwash water.

Your timely consideration of the request for facility modification is appreciated since repairs of the Turbine Room Sump are scheduled for early 1987. Please call me if you require information or have any questions regarding the information provided. We would be happy to meet with the people responsible for drafting the permit modification.

"-- Very truly yours,

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'~.)d: C< Z~~a

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. Jack A. Druckemiller Manager of Environmental Affairs JAD/df Enclosure c: W. G. Smith, Jr.

p'c EPA I.D. NUMBER 98 647 SECTION I PERMIT NUMBER 3 M I 0 0 0 I APPLICATION FOR DISCHARGE PERMIT IS:

SEE INSThUCTIONS ON REVERSE SIDE NOD IF I CAT ICII EXISTING I'EW IICREASED USE RE ISSUANCE l2 Q CI Cl O A. PARENT CCtPANY/CEPT./earn lTEM B'l V'/BIIIEAU I C PIA'IT CR FACILITY E STAtZARD IhQJSTRIAL CIASSIF ICATION (REFER TO TABLE II)

PHYSICAL D, TYPE GF Fxxl I LOCATION Fs STREET IAlBc& G~ STREET IW'E ADDRESS N I I HI CITY NivE I. ZIP CODE AND INFORMATION J. TC54ISH I P 'e COITIIY (REFER TO TABLE I)

CO. IIAHE CO. IAPBER ELLE Lo HAvE OF AUIIL'RIMC"'lTACT PERSON I ~ I I NV AFFA He ~iE tPJ'oER OI ADDRESS (IF DIFFERENT FRCII ABOVE)

L2~S L4 x2.~I PI CITY ICE OI STATE Rs ZIP IE 5~ TYPE OF TREAI"E!IT FAC ILITY Te PROGRAM FOR EFFECTIVE RESIDLQLS HAIIsGEHENT (REFER TO Tr'~ II) DATE SIEVIITIED

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YES Id) EIN.A. DATE ItPLEHEHTED U. BACK~ POwER SIXRCE V. POILUTICII INC IDENI'REVENTIOII PLAN We IAPBER OF EPPLDVEES El 'VES Q ta N,A, H O.,

XI TYPE OF DISO5QGE Ye DO YOU HAVE A CERTIFIED OPERATOR7 Qg YES Q IIO Opbt'JIVE b HAHE BOTH Q . SIRFACE WATER FACILITY ¹ CERT IFICATIOII ¹ ITEM Ao tttHE NGE Bs tQ%

MAILING ADDRESS IN>IAN & MI HIGAN ELECTR IC CO OF CI STREET ADDRESS CR POST OFFICE BOX APPLICANT Do CITY N% Eo STATE FI ZIP CODE RE'rUIPXO SICuap&f "r I'o"atty ot Iau that I havo personally exoslnod and an tanlllar ulth the Infatuation subnl \ted In this appl Ication acean 5 4"4 I"at ~ bas 4 nn nY lnnulry at these Indlvlduals I~dlately ro5ponslble Ior obtalnlnG the Intomatlon. I believe that the

"" ac<<<<tn

~ anu coxjplote. I an a aro that thoro are slonltlcant penalties Ior subntttlfxt talse Infomatlon, Includlnq the pa55lbl llty ot tine and II prlsanxant.

SIGNATUPE OF APPLICANT SIGNATURE OF LOCAL GOVERIPITNTAL REPRESENTATIVE (SEE NOTE ON REVERSE SIDE)

r. IZ 29 ylt Vice Preside enge 15

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NSTRUCTIONS FOR COMPLETING SECTION I ITEMS I AIR 2 This fom requires Information about the facility address, discharge location, plant controls, type of disposal facility and name, address, and signature of the applicant and local goverrmental representative.

Enter Envlrcxvwental Protection Agency I .D ~ Number If ave I labia.

ENTER THE PERNIT NIS4)ER IN THE BOX AT THE TCP OF THIS FCRM. THE PERMIT'I4)MBER CAN BE FC()NO ON THE FRONT PAGE OF YOUR EXPIRING pERulT. If this is a ne<<or not previously permitted facility, then leave blank and a number wil I be assigned.

In the box titled "Request for Olscharge Is" check one of the five categories (modification, existing unpermitted, new, Increased use, or reissuance) <<hlch your permit application fall> Into (see page 14 for definitions).

PHYSICAL LOCATION ADORESS ANO ItlFCfLAATICN A.-C. Enter the naming Information In accordance with the fol lowing:

- For industrial facilities, provide the parent Company name (A.), the division name (8.), and the plant name (C.).

- For federal and state facilities provide the department name (A.), the division or the bureau name (B.), and the facility name (C.).

- For cormerclal facilities provide the owner'S namO. doing business as (d.b.a.) (A.) and the fpcl lity nome (C.).

O. Enter typo of foci llty. Examples of this are: foundry; high school; automatic car wash; dry cleaners; self-serve I aundroPlat, E. Refer to Table III (page 5) for the list of Standard Industrial Classification Code (SIC). Enter the code number that best describes the maJor product or service produced ~

F.-l. Enter the phySiCal IOCatlen Of the faCllity. 00 NOT uSe pOSt Of{ICe bOX number.

J.-K. Enter the township and county In which this facility Is located. The county code number can be found In Table I (page 5).

L.-R. Enter the n~, title, address and telephone number of the facility's authorized contact person. This person should be thoroughly familiar with the facts reported on these {ones ln the event that contact regarding the permit application must be made.

S. Refer to Table Il (page 4) for the list of Treatment Facility Types, enter up to five methods used by the facility to treat the waStewater.

T". Indicate whether this facility has a "Residuals Management Plan". If so, enter date plan was submitted and the date the plan was or is to be Implemented . Such a plan may be needed as deemed appropriate by the proper Division staff.

U. Indicate ~hether the waste treatment facilities have a back-up source of power or whether emergency procedures have been developed In case of a power outage to tho waste treatment facility. If the waste treatment facility Is not dependent on a source of power, check the "NA" box.

r V. Indicate whether this facility has submitted a Pollution Incident Prevention Plan as required under the Michigan ){ater ReSOurCeS CCnmISSIOn Part 5 RuleS fOr the "Spl liege Of Ol I and Palluting MaterlaISw.

W. If facility has sanitary wastewater (water used for domestic purposes; e.g., toilets, sinks, showers), enter the nuN)er of v

people using I

this feel I ity.

X. Check the typo of discharge(s) frcm this facility.

Y. Indicate ~bather your waste treatment or control foci lltles are under the supervision of a certified operator. If yos.

please provide the person'S name, social security number, and certificate number plus tho company's foci llty number.

ITEM 2 MAILING AOORESS FOR ALL CORRESPONOENCE A. Provide the nme of the applicant. For the purposes of this application tho applicant Is defined as the person signing below in accordance with tho directions provided on pago 14. Correspondenco regarding this application and future permit matters wll I be sent to the applicant.

8. Provide the name of the facility, company, or organization <<hlch the applicant In "A." above uses for receipt of sall.

C.-O. Provide the applicant's address to be used for future correspondence.

SIGNATURE OF LOCAL GOVERNuENTAL REPRESENTATIVE NOTE: If sanitary sewage Is to bo discharged {rom housing developments, apartment buildings, shopping centers, or other ccnmerclal developments. Into a system other than an approved municipal sanitary ~esto collection system, this application shall be co-signed by an authorized municipal official or township offlcor.

It ls the rule of the Ccrnisslon that applications Involving the disposal of sewaoe of human origin from any entity other thon local qover~nt should Include the local government as a co-signer of the statement, and that al I proceedings and hearings against said e"tity "111 Include the local unit of government as a party by appropriate notice, and all permits Issued as a result of such hearings and proceedinqs will be filed jointly aqainst the said unit and entity (Water Resources Ccnmission Part 5 Rules R SZS.IO+(SI and the Michigan Hater Resources ccnnlss ion Act 245 p.A. of 192g as amended section B(b)). This co-signature requirement ls oniY aopl enable << a<<taa se~age discharges and is not for any nonsanltary ~aste streams fraa this facility.

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Il ~ CTiON i PERMIT I

NUMBER MI0005827

...SEE INSTRUCTIONS ON REVERSE SIDE NWICIPAL ITEM Ae 3 Be QNFACE HATER IIITAxE e

eLtrrt RA% OF WATK+lAY SOURCE OF CUAIITITY (ttAX.)

WATER Ce PRIVATE HELL SUPPLY OUAtrtrv (ttAX.)

De C

OeJAMTITY (yAX.) ~DAV Ae FRDCEss HATER (Irtcuolra ctxtlAOT ITEM Be COCLIIG HATER) ttXtCOtrTACT COG.ItlG teATKR otAYrtrv (t Ax. OAuDNS/DAY

~DAV OUAltrITY (PAx.)

Ce SlVIITARV HATER FACILITY mwrtrv (we.) OALLONS/DAY WATER De OTHER SPF FY USAGE rAwlrtrv (ttAx.)

tgivk OF SUBSPACE ITEM Ce IU dER 5 UJ e I

PARA"KTER WITS

~/YEAR CRITICAL eYre'lE OF SUBSTA'AE MATERIALS 'e Ce: PARA'BTKR tAt BER

, le tet I

PRIORITY WITS ONITITY POLLUTANTS W/YEAR USED'TORED t4V% OF SUBSTAICE PARAtKTER tAt BER WITS PRODUCED OUUITIIY LJ/YEAR REFER tlat% OF SISSTA'rCE TO TABLES Ikl et I

PARADER tAPBER eIVBe V, OFUtrllv WITS LJ/YEAR tv'F sUBsTArtcE 1 POUNDS 2 GALLONS llJ Ih PARNETKR tltBER et:

3 CUBIC WITS YARDS ll OUI! I IY LJ/YEAR 4 TONS tlA% OF SUBSTAtKE CL PARAtBTKR tktBDI I

WITS QNITITY LJ/YEAR IF'F StllSTAetCE 4J te PARA'KTKR tlt'BER

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Illl TS

/YEAR No change from information previously provided.

INSTRUCTIONS FOR CCNPLETING SECTION I ITEMS 3, 4, ANO 5 This form requires inforr)ation about thc water supply-to the facility, the facility's water usage, and critical materials and pr(or ity pollutants used, stored, cr produced at this facility.

ENTFR HE PERMIT a'GMSER IN THE SC( AT THE TCP CF THIS FORM ~ THE PERMIT hlNSER CAN SE FOUNO CN THE FRONT PAGE OF YOUR EXPIRING pE(bllT. If this Is 4 new or not previously pemltted facility, then leave blank and a number>>ill be asslf'ned.

J ITEM 3 SOURCE CF 'dfATER SUPPLY List all ~ater supplies used. The volume may be estimated frcm ~ater supply meter readings or from billing statements from a>>ater supply If water utility. River, is not metered, est(rate frcm pump capacity. Where a narc Is required, enter name of ~ate~ supply; e.g.,

Mud Lake, Huron or the City of Millpond.

ITEM 4 FACIL>TY WATER USAGE List myounts of water to bc uSed for various purposes as:

Process Water - see Glossary for definition (page 48).

Noncontact Cooling Water - see Glossary for defln(tlon (paga 48I.

Sanitary Water - Water used for domestic purposes; e.g., toilets, sinks, showers.

If water Is first used for one purpose and the same water Is subsequently used for one or more other purposes, Indicate the volume per day of the last deslcnated use before treatment and/or discharge. For exar)pie, If ~ater ls Initially used as noncontact cooling water and then as process water, the quantity of ~ater given should be Indicated as process water.

The total of Item 4 should equal the total of Item 3. Any difference In these totals should be explained In an attached sheet of this application.

ITEN 5 CRITICAL MATERIALS ANO PRICRITY POLLUTANTS USEO. STCPEO, PPCOUCED L(St all Chem(Cal SubStanCeS wh(Ch are ln MIChlgan'S Crit(Cal MaterialS Rag(Ster Table IV (page 6) and/Or U.S. EPA'S Pr(Ority a II t t List T hl y th s 7) that a .ly d, t d. 0 M day this f )lily.

18

Vc RECTION I PERMIT MI0005827

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NUMBER SEE IN Sl'RUCTION S ON REVERSE SIDE

'IO LINE OIIGRW SHOttlta IHE waTER FLOW TIIIWROH YOIN FACILITY F~

CAPiRIEUTItG WAS&iWATERi IIICLUOING FROCESS AVD PROOUCTIOtl AREAS. SAIIITARY FLOWSi COOLINS WATER> AIIO STORtWATER RIltOFFa YOU HAY GROUP SIHIIAR OPERATIC:tS INTO A SI;ISLE LIIIT, T% WATER BAV:tCE QePJ) QCW avERAGE FLCWS. SHM aLL SIGIIIFICAtIT LOSSES CF WATER TO PRODUCTS, ATii)SPHERES A:8 DISCHARGEe YOU QOQP USE ACTUAI. HEASURtmTS WHEttEVER AVAIIA3LEI OTHERWISE USE YOR REST ESTIHATEe DESCRIPTION AND DIAGRAM See line diagram on following page.

INSTRUCTIONS FCR CCMPLETING SECTIQI I ITEM 5 This farm recuires infor. ation about the water flaw throuah your feel llty frcm Intake to discharge.

ENTER,H F54<IT N4i'BER IN THE OX AT TlrE TCP OF THIS" FORM. ~ HE PERMIT NINER CAN BE FOINO ON THE FRONT PAGE OF YOLR EXISTING pE~iiT. If this ls a rew or not previously permitted facility, then leave blank and a n~ber will be assigned.

ITEM 6 oEScRipTIc'0 Auo LINE DIAG+i'I OP FACI LITY '5 pRocESSES ANO TREATMENT SCHEME A. Briefly describe the route taken by water in your feel I ity fram the Intake ta the discharge and also provide a line drawing, Exama le Cesar l ation and 0 I a r am liarratlve: The rinse water fram the various plating operations is collected In ane of the two 35,000 gallon ranks. calcium cnlor ldo and alum are added to assist In fluoride removal and aid In coagulation. The. water 4s adjusted to a DH of about 5.5 using dilute sulfuric acid. The pH Is!hen raised to a pN of about 10.3 with lime to precipitate the metals ns hydroxide. Polymer Is added to flocculate the metal hydroxides. The

<<esto stream flows through a clarifier, the metal hydroxide settles to the bottom as "sludge". The treated water flaws fram the clarifier to a manhole where it ccmmlngles with ccntact cooling water fram the strip line. This ccrrmingled water ls discharged to the Buck River. The sludge fram the clarifier goes to a vacuum filter where it Is dewarared. The sludge Is later taken to a landfill.

Calcium Chloride Alum Sul furic Acfd Lime Polymer Plating 70,000 Wastewater Gallon Acidification tfeutra1 Izat fan Flo ccul ation Tank Batch Bumps Bump Sludge Clarifier Hon-contact Tank Thickener Cooling Water Calcium Chloride Vacuum Mater Filter Alum Sulfuric Acid Sludge Hanhole Lime Gondola Landfill Buck Rive John Ooe, Inc., Oeertown, manufactures sleeve bearings for automotive and truck engines. Production Is divided into 3 phases. Metal powder Is produced In tho first phase. This Is acccmpanled by melting copper, tin and load Into Ingots In an electric furnace and applying a Jet of water to quench and solidify the molting metal Into powder form. The second phase consists of adhering tho fine metal powder to a coll ot steel by passing the two slowly through furnaces. Water used to cool the strip constltutos the contact cooling water. Bearings are then formed and machined from tho coated steel. In the third phase, most bearings receive a nickel strike and lead, tin copper olectroplate. The remaining bearings are aluminum or babbitt and receive a tin or lead plate. Rinse water before and after the various plating operations constitutes the process water.

Hunfci pa I Sanitary Hunf c i pa 1 Water Facility Treatment Supply 30,000 gpd Stormwater Stripe Lfne Cooling Mater 295.000 gpd 250,000 gpd Maste Treatment Buck Rfve Plant 45,000 gpd Powder Hfg. Plating Process 4,000 gpd 40,000 gpd 20

150,000 lb/hr Mell No. I Visitor's Hain Ht. Boiler Potable and Center Sanitar Mater 57,000 GPD Outfall OOE (Hl 341)

Fron Unit I or 2 Extended Dual Seepage Lagoons Hake-up Mater Plan Aeration STP Operated Alternately Well No. 2 Plant hr Sanitary 0.015 HGD Avg Back-Up Ht. 0.031 HGD Hax 8 I r Internal Outfall OOC (HI 396) 0 014 HGD Avg Internal Outfall OOA (HI 397) orxwa ter 0.112 HGD Av ., 0.266 HGD Hax North Catch Basin 501 Essentia I Service Mater Homal Start-Up 28.8 VGD Flash Flash T n Outfall 001 (HI 393) n Circulating Mater Discharge Unit I Stean 1200'ffshore schg Bay Unit I Ste. Gen.

1118 HGO Avg., 1277 HGO Hax Unit I Hake-Up Outfall 0 Mater Plant Regeneration Turbine Outfall 3 intake Cribs Intake Nn- n Roon (Hl 374) 003'HI 0' fshore Forebay Unit 1.817 x OnHI te 395) 2 2 Hake-Up Sunp Absorption Mater Plant Pond In-Plant Sueps isc Floor Drat Outfall 002 (Hl 394) Unit 2 Unit 2 Stm. Gen.

Circulating Water Discharge Unit 7 Stean 1200'ffshore schg Ba! Condenser 1425 HGO Avg. ~ 1718 HGO Hax Boreal Start-Up Essential Flash Tank lash Tank Service Mater 28.8 HGO Internal Outfall 008 (Hl 398 0.109 HGO Avg., 0.282 HGO Hax ~ v Lake Hichigan Stonawa ter South Catch Basin Mastewa:er Flow Diagran, 1984 502 Outfall OOF Donald t. Cook Nuclear Plant Pre-filter Backwash to Unit I C. E. Ihwk - 2/20/85 or Unit 2 Discharge Bay Revised - 11/18/86 0.0972 HGD avg.

'utfall 003 De-icing Dschg was used 42 days 0.5832 NÃl sax.

In 1984 -- 224 HGO Avg., 839 HGO Hax

Section I, Item 6, cont'd.

Outfall Descriptions Outfall OOF - Pre-Filter Backwash Make-up water of ultra-high purity is required for the steam generators. The first step in treating intake lake water is solids removal using multi -media filters. The filters are called pre-filters since they are the initial step in the treatment process.

Alum (aluminum sulfate) is injected into the water supply upstream of the pre-filters to act as a coagulant on the filter media.

When the pre-filters are saturated with solids removed from the lake water, the pre-filters are backwashed with additional lake water, and the solids are flushed to the turbine room sump then discharged to an on-site absorption pond.

The proposed plant modification would reroute the pre-filter backwash to Lake Michigan. There would be a small net increase in the amount of solids returned to Lake MIchigan as a result of the alum added during treatment. The design maximum amount of alum which could be used is 624 lb alum per day which would cause a net increase of 0.05 ppm solids when discharged through Outfall 001 or 0.04 ppm solids when discharged through Outfall 002. The attached screening data show that the typical pre-filter backwash contains only 1.7 pg/1 aluminum and 25 pg/1 sulfate.

SECTION I PERMIT MI0005827 NUMBER

,bEE INSVRUCTIONS QN REV.ERSE SIDE

  • PAP OF THE IREATtEIIT FA"ILITY LOCATION, SHCHIIIG THE LOCATION OF Tte DISCHARGE POItlT(S) AID OTHER IIIFCQQTION RBXKSTED ITEM As PROVIDE ON REVERSE Sl "E OF PAGE.

7 LOCATION MAP See topo IDap on following page.

21

INSTPUCTICNS FFFI CCt!PI.ETIIK'ECT(Oil I ITCM 7 This tern reculres a location nap of the treat@ant feei lity showing discharge point(s).

FIITER T."E P ~ -IIT '.L".:BER IN THE BOX AT THE TOP CF THIS FORM. THE PERIIT '.:IIMBEn CAN BE FO(j;(0 CW TIIE FPO'IT PABE CF YOIJR EXPIRlls PE%.'IT. If this is a nrw cr rot previcusly permitted feel li ty, then leave blank and a nurber will be assigned.

ITEM 7

'.C ATICN MAP A. Provide s detailed lccatlon nz of the treatr!ent,facility, shcwing the Iccatlon of the discharge point(s) for all surface

<<ater and groundwater discharges, and all 'known sucply and drinking <<ater wells of ad acent properties to the facility.

For cotn surface and r<<rouncwater d lscnarge applicants, indicate ,he location and Identification nun'ber of any groundwater nonitorinc wells relative to .he facility <<hlch are currently belno used by the applicant to .onitor the groundwater. Also, Include t..e receiving stree<<, lake, or stom sewer and the streets and roads in the area.

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Unit Steam Generator Blowdnwn BRIDGMAN. MICH.

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C Il

S CTION I PERMIT

'e s NUMBER MI0005827

, 'EE INSTRUCTICNS QN REVERSE SIDE A, DO YCU OPERATE A CC!KENIRATED Nfle"AI, FEEDItIG FACILITY. (IF tQ CIYattRE TO ITE{ JU)

ITEM Be tltSER OF ACRES NB) FCR mtfFItsTYDA'EDI'? esses CO!IF It'O'Eras HAS A RIPOFF DIVRSICtt tUO CONCEN C.

':rex.

IF TtsERE IS CFEN srsTEM Bmt cc:silftdED? (IF to, colattAIE To ITEII 9) YES tfO TRATED ANIMAL Ds WAT IS TI{E EESIGN BASIS FOR iteE mtfIPOL SYSTEI{? CPECII Ct{E OF THE FOLLCNltti AIQ Et{TER tllSER OF IIIOYES OP RAIN?

0 10 YEAR, 2II HOUI STORM INCIG

~~

25 YEARi 2II HOUI STORM ItfCHES FEEDING OPERATION TYPE I s Q OTTER (SPECIFY) INCHES E H{AT IS T'riE IAtSER CF ACRES CF CCtiTRIBUTItIG CRAINAGE ~

esses WAT IS THE CESIGif SYFEIY FACTOR FOR THIS mlfIRC4 SYSTEM?

Fe LJ LJ

~

Ae LIST iYFE OF AtfltW. ~

lTEM Be GIVE THE CO!IF I!~~%lac tAIBBI CF THIS 1YPE OF AtfIMAL Itf OPB{

9 C. Greets TIE IAt~ CF THIS TYPE OF A!IIMAL tN ICUSED CCS I!>> eE! sT.

As LIST TYPE OF Aeflt'AL>>

TYPE IL Be GIVE TITS tklBER OF THIS lYPE OF ANIYAL Itl OPEtt co:F I!~L aa.

NUMBER OF Ce GIVE 1HE Qi~~ OF THIS TYPE OF AIIIYAL IN HOUSED CC!Ff!:E ~IT.

ANIMALS A~ LIST TYPE OF AtatsALe IN UI GIVE THE!Ar'BER OF THIS 1YPE OF Atilt'AL ltt CPEN OPEN 4n Be mtiF I tiEY~'6 e AND I Cs GIVE THE hUSER OF THIS TYPE OF ANli{ALIN HOUSED HOUSED CO'IF I tiger VT ~

CONFINEMENT LIST TYPE OF A!IlteALe t~

Ae Be GIVE TH~ OF THIS TYPE OF ANIIW. IN OPEN Col t&'Eras Ce GIVE THE USER OF THIS 1YPE OF ANIMAL IN HOUSED CO'< t.! ~s:IT A>> LIST TYPE OF ANIYAL>>

B. GIVE IIeE rfftSER OF THIS lYPE OF ANIt'AL IN OPEN mlF I re Era ~

C. GIVE Te{E IAtSER OF 1HIS lYPE OF At(tl%. IN HOUSED co.'F II:F,'~E!IT.

Ae LIST 1YPE OF AIIIYAL, B~ GIVE THE IAIBER OF THIS lYPE OF ANIMAL IN OPEN mriFI!usta, C>> GIV'E IHE Ifft+ER OF 1HIS TYPE OF ANIMAL IN HOUSED CCriF I t IEYEta e Ae LIST TYPE OF AftlYALe Be GIVE THE IAFSER OF 1HIS 1YPE OF ANltW. Itf OPEN mr& I!F !IT C~ GIVE THE tAJZER OF 1HIS TYPE OF WIMAL IN IIXISED mrfF IIKMEtae As LIST 1YPE OF ANIYALs Bs GIVE THE raJ~MR OF DNS TYPE OF ANIYAL It( OPEN CO!Fire+a.

Cs GIVE THE!AtBER OF IHIS TYPE OF AtfttW. IN HOUSED 0YFI!ax!a.

23

INSTRUCTICNS FOR CCMPLETING SECTION I ITEMS 8 AND 9 This form requ(ros Into~orion about tho design, slzo, and type and numbers of animals in a concentrated an(mal feedlot.

ENTER THE PERvII T NUvBER IN THE BOX AT THE TCP OF THIS FORM. THE PERMIT NUMBER CAN BE FOU!4) ON THE FRONT PAGE OF YOUR EXPIRING pE~~HT. If this Is a ne>> or not provlously petmitted facl,lity, then leave b lank and a nusber <<III be assigned.

GENERAL INFCRMATICN Not all animal feeding coerat(ons are required to obtain NPOES permits. Exclusions are based on size and occurrence of discharge.

In particular, for animal feed(ng operations, the size. cutoffs depend on whether or not pollutants are discharged through a man,ade device or y direct ccntact with the facility or animals. A facility for laying hens or brollers is not required to have a permit unless It has a liquid manure handllnq system or continuous overflow watering . Also, facilities which d(scharge only In the case of a 25 year, 24 hour2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> storm event are not required to have a permit.

ITEM 9-8 Give only the area used for the animal confinement or feeding facility. Oo not Include any area used forr growingw ng or opera operatl ng feed.

ITEM 9-C Check "yes" if any system for collection of runoff has been constructed. Supply the Information undern e 0, E, an d F to th e b est of your knowledge.

ITEM IO-8 ANO C Give the maximum number of each type of animal in opon ccnflnermnt or housed under roof (either pari lolly or totally) <<hlch are held at your facility !or a total of 45 days or more In any l2 month period.

Use the following categories for type of animals:

- Slaughter Cattlo - Lambs

- Feeder Cattle -

- Mature Oairy Cattle (ml (ked or dry) - Turkeys Laying Hens I

- Swine (oacn weighing over 55 pounds) - Brollersl

- Horses - Oucks

- Sheep A permit Is not required unless the facility has a liquid manure handling system or continuous overflow watering.

ANIMAL FEEDING CPEPATICN reanS a lot or factllty (other than on aquatic animal production facility) where the following conditions are cet;

, (A) Animals (other than aquatic animals) have been, are, or <<III be stabled or confined and fed or maintained for a total of 45 days or rore In any l2 month period; and II (8) Crreps, vegotatlon, forage growth, or post-harvest residues are not sustained In the normal growing season over any portion of the lot or facility.

Two or more animal feeding opertlons under ccnmon ownership are a single animal feeding operation It they adJoin each other or If they uso a cormon area or system for the disposal of ~astes.

ANIFIAL UNIT means a unit of measurement for any animal feeding operation calculated by adding the following numbers: The nuaber of slaughter and feeder cattle multiplied by I.O; plus the number of mature dairy cattle multiplied by I.4; plus the number of swino weighing over 25 klloqrams (approxlmatoly 55 pounds) multiplied by 0.4; plus the number of sheep multiplied by O.l; plus the neer of horses multiplied by 2.0.

CC:ICENTPATEO ANIMAL FEEOING CPERATION means an animal foedlng operation which meets the criteria set forth In either (A) or (8) belOW Or whlCh the OlreCtOr 'deS(gnatOS aS SuCh On a CaSe-by-CaSO baSIS.

A. More than the numbers of animals speci!led In any of the following catogorlos are confined (REGAROLESS OF wHETHER A SURFACE WATER OISCHARCE EXISTSI:

4 I. I,OOO slaughter or feeder cattle.

2. 700 mature dairy cattle (whether milked or dry cows).
3. 2,500 swine each weighing over 25 k(ioqrams (approximately 55 pounds).

4, 500 horsos,

5. I0,000 sheep or lambs.

6~ 55,000 turkeys.

IOO,COO lay(ng hens or bOllers (lf the facility has a continuous overflow watorln9) ~

30,000 laying hans or brollers (If the facility has a liquid manure handling system) ~

5,000 ducks.

IO. I,OCO animal units.

B. Moro than the following numberS and types of animals are confined (WITH SURFACE WATER OISCHARGE AS OESCRIBEO BELOw ):

I. 300 slaughter or feeder cattle.

24

SECTION I PERMIT

~ SEElSSTRUCTIONS QLjMB0tII3 M20005827 ON REVERSE SIDE A. CO YOU CPERATE AN AOit2TIC ANlteAL PROCUCTICN FACILI7P.

(IF:a, axtrt:a2E To trDI L?)

ITESI 10 B>> ItEIICATE TI!E TOTAL M'BER OF POhDSs RACEWAYS F28 SIHILAR STsRsUCTUIES AT YON FACILIT(~

escsesee AQUATIC

'PECIFY, ANIMAL PRODUTION IIDICATE I>t WHICH ~SR.Vt email VT)NTH PAXIVut FEEDIlCi OCCURSe FACILITY De BfttR TWa TOTAL esuBER OF POCDS OF FOOD FED IXRIIIG THIS t 2.':itW?

Ae IS sHIS SPECIL' CR COLD WATER SPEC!E?

ITEM O~

ct B. GPec IHE t~V'E OF DIIS SPECIEe qj CL Vt Ce De BlTER Tike TOTAL HARVESTABLE WEIGHT OF THIS SPECIE PRCCXED BY THIS FACILITY PER YEAR IN FIXES.

Be'fER DK PAXIVut WKiGHT PRESBtf FOR THtS SPECIE WIICH I XLD REPRESBff YOUR teAL OPEPATIONe SPECIES Ae IS stilS SPECIE A &vest OR COLO WATER SPECIE.

OF AQUATIC GIVE rtsE tvV'E OF THIS SPECIEe ANIMALS PRODUCED C~ EtffER ~c TOTAeL YARVESTABLE 'hEIGHT OF THIS SPECIE AT THIS PRODUCED i'IIIS FACILITY PER YEAR IN PIXfeDS ~

FACILITY o. BtrER a;E t'LYi"ul WEIGHT PRESBIT FCR IHIS SPECIE WHICH WCD RFFRESEs'tT YOtsR tOR'tAL OPERATIONe IS TsilS SPECIE A 'es?RN CR COLD WATER SPECIE?

Be GIVE THE sVV1E OF DIIS SPECIEe C. BticR THE TOT" HARssESTABLE WEIGHT OF THIS SPECIE Fke?f0)CED BY THIS FACI lY PER Y AR IN PtXVBS.

D. BtfER THE NAXI;ue WEIGHT PRESENT FOR THIS SPECIE hHICH VCtAD F EPRESEt<T YCLst tCFteAL CPERATIOtt ~

Ae IS THIS SPECIE A WAILst OR CAD WATER SPECIE?

Be GIVF '>>N IFeE OF THIS SPECIEe C. ENiER THE TOTAL HARVESTABLK WEIGttf OF THIS SPECIE PR<FUCED BY THIS FACILIIY PER YB8 Itt PCQIDSe D. BtfER THE vtAxllut hEIGHT pREsBIT F0R THls spEclE hHlcH WOAD REPRESBIT YOUI tJORNAL OPEPATIOtle As IS THIS SPECIE A WA/UI CR CtXD WATER SPECIE?

B. GIVE. THE IIA'E OF THIS SPECIEe Ce BITER TltE TOTAL HtJWESTABLE h'EIGHT OF THIS SPECIE PRODUCED BY DIIS FACILITY PER YEAR IN PIXtDSe De BffKR TIE PAXIYll< hEIGHT PRESENT FOR THIS SPECIE HIICH VtXAD REPRESBtr YIXR ttORNAL OPERATICtl ~

Ae IS THIS SPECIE A WARst OR 0XD WA'fER SPECIE?

e B. GIVE IIIE t0VK OF THIS SPECtEe Ce BITER TIE TOTAL NRVESTABLK h'EIGtff CF THIS SPECIE PPOIXJCED RY THIS FACILITY PER YGQ Itt PCtflOS.

D, BITER TIE ttAXlt%l4 WEIGHT PRESENT FCR THIS SPECIE hHICH VOILD PCVESBtf YOUR tORNs< OPVRATIOtfe 27

cr INSTRUCTIONS FOR CcrPLETING SECTION I ITEMS 10 ANO I I This !orm requires Information about the design, size, and type and numbers of animals In an aquatic anlnal production facility EIITER Tl'E P ~ (IT rUUBER IN TH BOX AT TH+ TCP OF THIS FQR4 ~ THE P~~IT NlPIBER CAN BE FCUNO ON THE FRGI(T PAGE OF YOUR EXPIRING FERMI T. Ir this is 4 new cr not previously pemitted facility, then leave blank and a neer wll I be assigned.

GENERAL INFrA"ATI Col E Not all flsnf4...sere required to obtain NPOES permits. Exclusions are based on size and occurrence of discharge. For aquatic anit.,a'I production facilities, the si o cutofts are based on whether the species are warm water or cold water, on the production

>>eight per year in harvcstaale pounds, and on the amount of feeding In pounds of food (tor cold ~ater species). ~ AI sor ' f ac llltl. es whiCh dl sc h a rr~e less than 30 days per year, or only during periods ot excess runoff (tor warm water tish) a r e not require to have a permit.

cG!IGENTPATEG ACUATIc ANUAAL PRGQUGTIGN FAGILITY means a hatchery, fish farm, or other er facility ac c contal which w s grows or holds con a ns, aquatic anim It. r ni 4 I s iin e her ot the following cateoorles, or>>hlch the Director designates as such on a case-by-case baSls.

A. Cold. water tish species or other cold ~afar aqua. ic animals Including, but not limited to the Salnonldae ae f am IIy 0 I fls h

.g., rout and salmon) In ponds, raceways or other similar structures>>hlch discharge at least 30 da s per year b u t d oes not include:

I. Facilities ~hlch procuce less than 9,090 harvest weight kllograms (approxlnately 20,000 pounds) of aquatic animals per year.

2. Facilities which feed less than 2,272 kllograms (approximately 5,000 pounds) of food during the calendar month of naxlnum feeding.
8. Ham ~afar fish species or other wana water aquatic aninals Including, but not limited to, the Amelurldae, Cetrachldae, and Cyprlnidae families of tish (e.g., respectively, cattish, sunfish, and minnows) In ponds, raceways, or other similar structures wnlch discharge at least 30 days per year, but does not Include:

I. Closed ponds which discharge only during periods of excess runoff.

2. Facilities >>nlch produce less than 45,454 harvest >>eight kllograms (approximately 100,000 pounds) of aquatic animals year ~

ITEM II-B Give the total number ot discrete ponds or raceways ln your facility. Under "other" give a descriptive name of any structure which Is not a pond or a race~ay but which results In discharge to waters of the United States.

ITEM II-O The value given for maximus monthly pounds of food should be representative of your normal operation.

ITEM 12-8 The name of fish species should be proper, connon, or sclentltlc names.

ITEM 12% AI4) 0 The values given for total weight produced by your facility per year and the maximum weight present at any one time should be representative of your normal operation.

NOTE: Tha permittee shall continue with Section II and address Items I, 2, 4, and 5 on pages 31, 33, and 35.

28

SECTlON l PERMlT NI0005827 NUMBER D LIST NA"E AttD NAILI'5 ADDRESS OF ALL PROPERTY OwNERS ADJACEIIT TO TIE TREAIt+Ãf FACILITY At Ol DISCIELKNDISFOSAL AREA.

ITEM 12 MAILING LIST OF ADJACENT No change from information previously provided.

PROPERTY OWNERS

l , ~ at SECTION II SEE 'INSTRUCTIONS NUMgfR~~ M20005827 ON. REVERSE SIDE ITEM Ae mIFAll ITKR Be UKATIC>>M OF DISQTARGE Inc HAT NI CP RECEIVINGi t>>ATER 'LIE>> GROLIEtIATER CR NA% OF StjIFACE

'k,

~ 4 SECTIN i(LLJII,

~OF T04'I ~~, I2AIGE ~1 C DO YCU DISQUQGE Sc~KC,IALLY (IF tio, c" ai:aa To E) YES X ro DISCHARGE LOCATION D. IF YES LIST DISQLIRGE PERIODS tQ>> / DAY MO ~ / DAY MRS SCHEDULE FLOW

~ ~ ~"~

RATE WASTEWATER Iti HI

~ ~ /OAY ZXH~DI~ Ee LJIID APPLI CAT ICI RATE N ~ LJ ~

1 CONTACT COOLING Fe TYPE OF HASTEnATER DISCHURGE L3j M w HASTBIATER TYPE COBE LJ 2 NONCONTACT c (YEARLY AVERAGE)

G~ DISCHARGE SCHGXIT DAY/YEAR LeiL6.M COOLING He DISCHA'2GE FLOII PATE UNIT CODE 3 PROCESS TOTAL YEARI.Y 4 SANITARY 5 STORMWATER DAILY MINIIUI 0 ~ 0972 ~2

/NIT C~D DAILY tILXWM 0 le LltlT CCOE 1 MGY I. THE v/NIHLM DISCHARGE FUITI RATE TO BE AUIHCR IZED IN PEP<IIT>>

AUTHOR I ZED 2 MGD 3 GPD J, I'AXItUIOESIG'I DISCHARGE FLOTI RATE.

DESIGN 0 . 58 Ai DO YCU USE HATER TREAT.SAT (IF IIO. CCal:AIE TO ITm 3)

AINITIVES TO TREAT YOLII DISCHARGE~

0 YES B NAME F>>J.'2CT ICOSI, A'c2 Q&IICAL Gd&5ITICN OF THESE ACOI TIVcS>>

2 WATER TREATMENT ADDITIVES C>> tA"E M) ADCRESS OF t>>A'AIFACTURERS OF THESE ADDITIVES>>

UNITS CUUE 1 MQ/I 2 UQ/I De EXPECTED DISCHARGE CQICEtIIRATICN OF AIX)ITIVES>>

M INIMLM UMI TS AVERAGE INITS MAXIPLII UNITS CODE CODE CCCE ACOII'IVE tQ%

ADDITIVE IIA%

ADDITIVE N/4%

Ee DO YOU TREAT THE DISCHARGE TO REtOVE ADDITIVES? YES Qx,<

Fe NH8T IS THE RDOVAL EFFICIENCY AMD DISCHARGE FREOUENCY?

X REteVAL HRS./DAY DAYS/W.

ADDITIVE N/W LJ ADDITIVE HNI E rmi TIVE IIAHE G>> AS AI ATTAQIEta IO THIS APPLICAT(OII f%OVIDE SPECIFIC PAYALIAMCR AOUATIC TOXICOUXiICAL DATA OR REFDIEIICE I>>>IQI ARE AVAILABLE/VID IITFOR"ATIOM QI THE RATE CF DEGRADATION OF TIE PRODUCTS FCR EACH AIXIITIVE>>

INSTRUCTIONS FOR CO!cPLETI JIG SECTICN I I ITENS I A40 2 This torri requires Infcrriat(on on tha facility 's dlscharqe location, discharge schedule, volvcce flow rate and water treatment addit(ves.

ENTER THE P RWIT MJNBER IJI THE BOX AT THE TOP CF THIS FOPJ4. THE PER!!IT NU'!BER CAN 8E FGUJ'0 ON THE FRONT PAGE OF YOUR EX~IR)IJG PERMIT. I! this is a ice or not previously permitted facility, t!:en leave blank and a number will be assigned.

Enter the out!'all number In space provided for each page of Section II. Fcr wach Individual dlscharqe point a separate set of Sectlcn II forms i.ust be filled out.

ITEu I OISCcCAmSE LMATIOJJ SCHEOULE AliO FJOW RATES A. Enter the IOCatlcn Ot dlSCharge, thlS Shbuld inCluce quarter-quarter SeCtlan, quarter SeCtian, tO>>n, and ranqe.

8. List name of receiving>>ater (If surface ~ater discharge).

C. Indicate whethei tact I lty discharges cn a seasonal basis.

O. If yes, list discharge periods.

Provide the land application rates used or expected to be used In terms of Inches per hour, hours per day, and Inches per week.

F. Indicate the type of wastewater to be discharged from this outfall. Refer to the waste>>ater type code given in the lett margin. vore than one code may be appl )cable.

G. Provide the avera e number of hours per day In>>hlch the facility dlscharqes treated wastewater and the total ncmiber of days per year in whlCh the dlSCharge OCCurS.

<<H. Provide current'from the last l2 months) or expected flow rates as requested. Refer to unit code qtven In the left margin for the appropriate flo>> units. MGY - million gallons per year; tCO - million gallons per day; GPO - gallons per day.

t I. Provide the maximum dlscnarge flow rate which you want to have authorized within the perm)t. NOTE: For NPOES permits only, the use of such a flow rate will not place an actual limit restriction on the flow but will be the flow rate used to develop effluent limits. Also, >>hen the monthly Operating Reports are reviewed by ccmpilance staff It will help than to determine if any ne>> or Increased uses might have occurred at the facility.

Provide the deslqn flow for this specific outfall discharge (e.g. batch treatment system flow, packaged treatment system flow, or soce other finite treatrent system flew).

ITE)4 2 WATER TREATMENT ADDITIVES A. Indicate whether discharge Is treated with conditioners, Inhibitors, or mlcrobloclde. If not, continue to Item S.

8, Give name, function, and chemical composition of additives used.

C. Give name and address of the manufacturer(s) of the additives used.

0. Indicate expected minimum, average and maximum discharge concentrations of the additive(s) for this discharge.

. E. Indicate,~bather you treat the discharge,to rocove the additive(s) before'discharge of wastewater.

F. Indicate the removal efficiency of each additive from the wastewater and the discharge frequency of each additive to the

'uc'face water or groundwater.

G. NOTE: It Is the responsibility of the applicant to supply the product Information as requested In this Item 4. Information requested but not supplied may result In the application being returned to the applicant for ccmpiet)on.

32

' SECTION II PERMIT D

NUMBE MC0005827 SEE.".N STRUCTIONS ON REVERSE SIDE r

~00 F lTEV As IF% CF PROCESS COICTRIBUTlt4 TO THE DISDIARGE THROUCIH THIS OUTFAU. IGNI SIC CODE 3 Be PROCESS SDCEDLLE (YEARLY AVERAGE)

IOWS/WV v v C/l Vl Ce PROCESS SYOLLPE FUTW RATE WIT COc/E PROCESS UJ TOTAl. YE/CRLY STREAMS CONTRIBUTING Cle 0

Ck DAILY Hlttit%A 0.072~6 TO DAILY AQXIPLPI OUTFALL De PROCESS PRODUCTI0'I PATE DISCHARGE N

~

Ae t~"6 CF PROCESS COtFERIBUTIICG TO THE DISCHARGE THROUCH 1HIS OUTFALL,AD SIC COD Be PRCYmSS SC'rMJLE (YEARLY AVERAGE)

SONS/DAY SAYS/YE/II Vl C/l Ce PROCESS 'hX.U'E Fltr/C RATE TOTAL YEARLY Ll 0 CAC Q DAILY Mltt I HIM

~NITS COD 1 POUNDS DAILY PAXIlLH 2 GALLONS WITS r/'TIME D. PROCESS PRORCTICXt RATE 3 CUBIC

~

A. tt/VE OF PRKESS CO:IIRIBUTIN TO THE DISCHCRGE YARDS

' TONS THIOUGtt TEC IS OUIFALL AINI SIC CODE B. PROCcSS SCHECULZ 'YEARLY AVERAGE) 5 MGY NSRS/DAY DAYS/YEAR Vl 6 MGD Vl Ce PROCESS WOLLPE FLOW RATE UJ 7 GPD 1DTAL YEARLY 0

Q. DAILY MINIPEM DAILY MAX De PROCESS PRODUCTION RATE WITS STIPE TIME

~

1 HOUR Ae IIA"E OF PROCESS CONTR IBUTIttG TO THE DISCHARGE TNROCCAH IH Ols ASSI SIC CODE 2 DAY IF'DEAS/DAY Be PROCESS SCHEDCLE (YEARLY AVERAGE) 3 WEEK DAYS/YEAR 4 MONTH Vl WIT CODE C/l 'SOLVE FLOW RATE 5 YEAR Ce PROCESS TOTAL YEARLY LJ Q. DAILY MINING DAILY PAXINFC De PROCESS PRODUCTIOtt RATE WITS ~IHE Ae IIA'E OF PROCESS CONIRIBUTltlG TO TISE DISCHARGE TIRCXI/AH THIS OUTFALL AND SIC CCXE Be PROCESS SCHEDULE (YEARLY AVERAGE)

DAYS/YEAR Vl WIT ONCE Vl Ce PROCESS MXltrE FUTIC RATE Llcl TOTAL YEARLY 0CL DAILY MIN INN DAILY HCXINH Ds PROCESS PRODUCTION RATE WITS P TIME 33

1.s INSTRUCTIONS FOR COMPLETING SECTION I I ITEM 3 ThlS fern rcqulreS infcmatlcn On the prOCeSS Streaee vhfoh COntribute tO thlS diSCharge.

EIITER THE PERMIT NL'uBER I:I THE BOX AT THE TCP OF THIS FORM ~ THE PEfbILT NLt<BER CAN BE FOUNO ON THE FRONT PAGE OF YOUR EXPIRIIQ pER'IIT. If this is a nev or not previously pemitted.facility, then leave blank and a nueber vill be assigned.

Enter outfal I nosher in soace provided for each page of Section II'. For each individual dlscharce point a separate set of Section II oms nust be I i lied out.

ITEM 3 PROCESS STREw'IS CO NRI UTING 0 Ol SCHARGE:

~ FOR EACH SEPARATE PROCESS PROVIOE THE FOLLONIIG INFORMATION A. Enter the naae of the process vhich contributes to this discharge. Also provide the proper SIC code ~

8. Indicate the yearly average process schedule In hours per day and days-per'-year.

C. Provide the I lou rate Inforr ation as requested based on your last l2 months of operations. Refer to unit code given in the left r>>rgin for the pproprlate flo~ units.

0. Process oroduct Ion Rate - Certain pemlt limitations a'ay be based on production rates. The production rates used to detemine per+It limits shel I be represented by a reasonable neasure of actual production of the production durir g the hich anth of the previous year, or the eonthly average for the highest of the facility, such as the previous five years, or other reasonable assure as stated in applicable U.S E,P.A. categorical rules and regulations.

~

For new sources or nev dlschargers, actual production shall be est!anted using projected production.

Record your production rates in the temS and units used In the applicable U.S.E.P.A. categorical rules and regulations for your type of facility.

P sECTiON II PER IVIIT SEE INST,RUCTIONS NUMBER~~ MZ0005827 ON REVERSE SIDE (IIIF7'Q. MJKII ITEM 'S IIEE DISCH/WE FR'W THIS OUTFALL DIREC1ED GRQh'0 OR Ae G"OL"WATHS7 (IF:SOP CQITlthK TO ITEAH5)

TO THE

~ CI YES Be HAS A HP~EOLrsIC/4. STLLDY OR ITS EOUIVALEIIT BEEN PERFORMED CR ts THEE SLFFICIBIT 0<<REIIT HY"RCGEQ PuICAL ItSON ATICI AVAILAUILEAS REEXJRED ILY CQHISSIQl PART LF ONCXB2TER RULE/ CF AUGUST ltt, 194

~ 5EATER RESOURCES R.h3.tZ07 (PAGE 4+ FCR

'Ee QS GROUNDWATER THtS EXIST:4G CR PRO?OS DISCHARGE! IF VES ATTACH A CCPV CF THE REPORT.

DISCHARGE C ARE YCU RgtFSTINS ~l EXES Tlc4 FRCM SUB'IITTtt4 A HYDROGEOLOGICAL REPCRT UteER INFORMATION E R 3 2 2 i L7 f) (P cE ~8)

~ c R FROM G R0 Ih &4 ' <<E 0 4 IAAR E MFA4 Is 7 @ I 1 Tc R I txi R YES IXCER IEF 0 R 725.2'MO (5) (PAGE 47) OF 1IAE PART /Ml RULES ~ IF YES ATTACH CODA'.E.'iTS e'Me Eit?~'~'IATIQP TO CEIXISTRATE THAl'Qht DISCHARGE HQAD OUALIFY FOR Ec(f uo T IQH 9 APE YCU R GUEST ~ ~ P1 A VARIANCE F~u RN E 323.2205 (PAGE 4p (thXeEGRADATIQI) OF YES NO THE H'TER?ESCURCES Ce 'TIISSIC4 PART D GRIXheHATER RULES. IF YESP ATTACH SUCH QXIjEeiTS eeS ACECESSA'LR( TO ++YEA'~STRATE THE NEED FCR A VARIANCE IN TERMS OF THE CRITERIA S?ECtFIED Hl RU 0 )2h ~70 (?AGE II27) OF 1HE PART ~ RULES ~

E~ L ST:'4L Cn=',ICAL SIDST",X S UHICH ARE IN MICHIGAN S CRITICAL MATERIALS REGISTER TABLE IV (PAGE t7) A,AD/CR U S ~ EPA S PRIVITY POLLUTANT LIST TABLE V (PAGE 7) OR ANY OTHER SUBSTAe4CES teT APPLICABLE/BELIEVED ABSENT 5HICH ARE OR e'AY BECOf<<E INJURICUS TO THE CESIGtl2TED USES OF T% GRIXhe54LTER OR TO THE PUBLIC HM.TH M'T ARE DISCHARGED OR EXPECTED TO BE DISCH2RGED TO THE GRIXheHATERJIY THIS FACILITYP Es> D'ATE TIAE FttlAL EFFLLENT CQXBITRATIQI Ae RECCRD AIL DATA IN ITEM 7 OF SECTIQl II I:I THIS ECOLE.ET.

THE A?FLIC'M'iT HAY BE R OUIRED TO CO PRESENTS DATA PROVIDED IN ITEM 7 ADDITIQIALHASTE ANALYSES~

Ae DISCHWGE CNAIL>CTERISTICS CQXEIITRATICtt WitS CODE 0 AIIALVSES SAMPLE TY CO%

ITEM (FIVE 5 BCD5

'COD (ae;ICV.

DAY BIOLOGIC'AL OXYGEN DBIAVED)

OXYGEN D We)

EXPECTED WASTE WATER CHARAC-,

TERISTICS TCC (TOTAL CRGANIC Ce'ARBQI)

A IONIA NI Inn Eti (As i4)

IOTA SUSPEiXED SOLIDS u1 ~ LJ UNITS CODE TOTAt. PHOSPHCRUS (As P) 1 Mg/I LJ1 2 Ug/I TOTAt. RESICUAL C7e'ZINE 3 COUNTS/

DISSO'ED 07LYGEN L1J 100 ml MIN 4 S.U.

5 F

.'PH ~ LJ 6 LBS/OAV FECAL COLIFCR'I BACTERIA ~3 TG5'EPATthAE (Sttt ER) ~5 TmERATURE (HNiTER) ~5 Be OTHER HASTEHATER CHARACTERISTICS SAMPLE 2205.

1 GRAB 0 I t. P, G R E A' E LJ LJ LJ

~

I

~

LJ LJ LJ LJ

~

2 24 HOUR LJ COMPOSITE LJ LJ See attached sheets for data.

35

INSTRUCTIONS FCR COMPLETlt)G SECTIOtl I I ITEMS 4 ANO 5 This iona requires Information on a specific outfall discharging to either !he groundwaters or the surface waters.

E)ITER THE PETIT )~MB R IN TH BOX AT THE TCP OF THIS ifCph1. THE PERztf NUMBER CAN BE FCUNO Ol THE FRCtlT PAGE OF YOUR EXPIRING pEPMIT. If this Is a new or not previously permitted foci llty, then leave blank and a number <<II I be assigned.

Enter The outfall number in The space provided for each page of Section I I. For each Individual dlschar e colnt a se arete set o'.Section II fotns (Items 4 and 5) nust be filled out.

ITE)I 4 GRQ'NOWATEQ OISC'ttARGE It:ENATION (00 tlOT INCLUDE OEEP WELL INUECTIC.'1 INFORMATI(XI lN THIS IT&4)

A.-O. The applicant shall address each of these parts It the discharge frcm this outfal I ls to the groundwater.

ITB4 5 EXISTltiGw OR EXPFCiEO (FCR A NEW OISCHARGE) WASTEWATER CHAQACTERISTICS OF GROUtCWATER CR SURFACE WATER DISCHARGE (00 NOT INCLUOE W=l.L IN) i I l lxFOPVAT 8 ltl Hl 0 .4 A. The applicant shall report available discharge data (real data for existing discharge or expected data for a proposed discharge) for the pora.etors as listed. These parameters shall be addressed for either a surface water discharge or as appropriate for a groundwater dlsct:ar ge. fcr assistance in determining aopropriate parameters a groundwater discharge applicant may contact the Ground<<ater Quoilty Division, Pernlts Section or the appropriate Groundwater Quality Division's District office.

The applicant shel I rcport the sample type code best describing each reported place of data. See coding on the left margin of this forn.

If this outfall Is a surface abater discharna. tho applicant nust report quantitative data for each parameter Identified by an asterisx. ino appl cant t:.Yy, ho<<ever, request That The report ng o oara tor one or more o these required parameters be

<<alved.. Such request nust be supported by adoquato rationale. Make such a request an attachment to this application.

8. If data Is available for other parameters not listed above In A. or other parts of this application the applicant should report that data ln the blank spaces provided ln this part.

NOTES: I. Unit codes for paramotors reported in parts A and 8 can be tound on the left hand side of this form.

2. Grab sample shall be used to analyzo for pH, temperature, total phenols, reslduol chlorine, oil and grease. and fecal collforn in a surface water discharge unless other frequency-sample type analyses aro available. See Glossary (pago 46) for definition of grab sample.
5. 24-hOur compOSIte samples shall be used to analyze for Total 8005, CCO, TrA, Ammonia Nitrogen, and Total Suspended Solids in a surface water discharge unless other frequency-sample type analyses at'e available. See Glossary (page 46) for definition of composite ststiple.
4. You are not required to report unless you wish to dononstrate your for a "net" effluent limitation for one or nore pollutants, that Is, an effluent limitation adJusted eligibility REPORTI:)G OF INTAKE CATA.

by subtracting the average lovel of the pollutant(s) present In your Intake water. )(POES regulations allow net limitations only In certain circunstancos. To demonstrate your eligibility, report the average of tho results of analyses on water (lf your woter Is treated before use, test the water after it is treated), and attach a separote yout'ntake sheet containing the following for each pollutant:

(a) A statement thot the intake woter Is drawn from the body of water Into which the discharge Is made.

(Otherwise. you are not eligible for net limitations.)

(b) A statement of the extent to which the level of the pollutant Is reduced by treatment of your wastewater, (Your limitations >>ill be adJusted only to the extent that the pollutant is not removed.)

(c) When applicable (for example, whon the pollutant represents a class of ccmpounds), a demonstration of the oxtent to which the pollutants In the Intake very physically, chemically, or biologically from the pollutants contained In your discharge. (Your limitations will be adJusted only to the extent that the intake pollutants do not vary from the discharged pollutants.)

5. It you have twO Or nOre Substantially Indontlcal outfalls, you may request permission frcm your permitting authority to sample and analyze only one outfall and submit the results of the onalysls tor other substantially identical outfalls. If your request Is granted by the permlttlno authority, on a separate sheet attached to the application form identify which outfall you did test, and describe why the outfalls which you did not test are substantially identical to the outfall which you did test.

36

cECTION II PERMIT MI0005827 Shh INSTRUCTIONS NUMBER ON REVERSE SIDE LITEM (UIBLL!r EB n>> Faugrtrr, REQUESTED IlFcrPATIQN ~~i'~'<

taTF! f FW 4:E Dt SOUR'RS ".~' PROVIDE EXPECTED'VAL[ES ADDRESSED ~ SQ?FACE WATER DISCHARGERS ~

FOR THE QUANTITATIVE AND 6 '. [XI[TAT[YE NFcr~ATIQ[ RECUESIED BELOW A. Is TH[s'.Ac[LIIY A PRIVACY I[~TRY2 'REFER To TABLE IA PAGE U~t Q YES

([F I/) (4 TQ E) ([F YES CO TO B)

PRIORITY INDIC;TE 1/PE CF PRIHARY lrlcUSIRY AS LISTED Itt TABLE IA PNiE UQ.

POLLUTANTS /C";;Tt.'."S'tlW C.)

AND ADDITIONAL

c. DCES iH[s cU[FALL DtsciURGE cQffA[rr A;[Y PRQCEsswABTEHATER2

[IF '<<o "o TQ E) (IF '/Esi c4 To D) Q YES t/O INFORMATION D . It@[CATE 'Htot GcJ <<FRACTIQ[s EST BE TESTED FQR.

(REcER TO TABLE,A Pi E>>~) VOLATILE FOR

[Q[E! RR E'ot i'll..S FPAC'ftQr CHECKED, EACH SPECIFIC ORGANIC TOXIC POILUTA%'ITHIN SURFACE WATER DISCHARGE E/Ot FP/CT Q I DATA F R ~>>'w

~>

1~IX<le BF P~>>4,YKD FCR (SEE TABLE I IA WiE Iroas TRY ACFLIQ::fs W! TH <<PROCESS WASTS<ATER DtsoA?GE

?O UTA?iT I."I TABLE It lA PJvk II~)

~

gf, IN ADQITIQNi /LL PR[tVRY PROVIDE OUANTITATIVE BAsE/r?EU[f?AL ONLY RECORD ~ ~ "<<TA crr Fcv?s PRQYIDED (ITEN 7) IN THls BQQKLETi ACID (CQIT[lAlE Wl(W E-K BELOW)

Cl PESTICIDE Es IF ~v'v 9 .FACE hi[BR OISOQRGE APPLIC/@IT (FR[NARY OR SECQIDARY INDUSTRY)i REGARDLESS liic i rPE CF DISMvKiE. KICKS QR iAS REASQ[ TO BELIEVE THAT ANY POLLUTANT LISTED t?OT APPLICABLE/BELIEVED ABSENT QF Dt AEI - I t':D IVA PAGES ~>>I IS DISC}@AGED FRcrt ANY IX)TFALL THE QUANTITATIVE

[BE!X, EE PROV[Cue

'T'I (ITBI 7) IH[s REccRD ALL FQF/ss PRovlDED tN BQQKLET O PRESENT/DATA IS ATTACHED F. IF A:iY SLRFACE WATER DISCHrQGE APPLIC/i'iT (PRINRY OR SECQIDU?Y IN[XISTRY)t REGARDLESS OF TYPE CF D:SCQ'BGE, rTIQWS OR riAS R~>>>>QI TO BELIEVE 'Ar[Y POU.UTA//fs LIStED TABLE vA RAFF. 4> a".E DISQ~ED FR?Yc A/IY OUTFALL THE APPLICArff RE/CNS FCR THE PCLLUf'%EI!a PRESBIT /L4 PROv[DE Arf/ AVAILABLEQUANTITATIVE DATA.

~ DESCRIBE ltl X rKIT APPLICABuFJBa.[EYED ABSB[T REcx?D A" i 'TA crt FOE% PRov[DED (ITB[ 7) IN THls BQQKLETi 0 PRESENT/DATA Is ATTAOIED Gs A' Sl/?F~ hni'fER DISCHARGE APPLICUITS (PRII"ARY Ate) SECQZMY It?CUSTRIES) hrcn t?OT APPLICABLE/BELIEVED ABSENT vp I.R."A'AFACTURES 2. 4, 5 - TR[o?LQRQPIIE?K)xY AcET[c-ACID (2, 4, 5-T):

-[(, ". >-TRIOI~BroxY) PRQPA?K)[c AclD (s[LYEx, Z, 4, 5, TP)

('-'. 4. >TR[rpL. ?ex/) En?YL 2. 2-DICHLDRQPRQPIQIATE (ERBCNJ) 0, O'THYL 0 (Fi 4. MTRICHLQRQPHBIYL) ProsPHQRQTH[QATE (RQAEL))

zi 4> 5 Tntc4LQRQP?iEtKIL (TcP) 1 cR HEKAOAtx?QPt?BE (HcP)l (Au DATA F0R 1HE Aoo7/E LST BE GBIERATED US[tIG STANDAIQ ANALYTICALCALIBRATtON PROCED[RES) OR Icrchs CR H's REASQI TO BELIEVE 1WAT TCDD IS OR HAY BE PRESENT IN THEIR DISCHARGE' FEPCRT %ALITATIVE DATAi GBIERATED W!)Ict[ USED A SCREB[lta PROCBXRE [KIT PRESBlT/DATA IS ATTACHED CALIBRATED wl [H Ar?ALYTICAL sTAIEI/RDS, FQR Zi 3i 7 8i TETRACHLDRQDIBENzo P-D[ox[N (TC)D) ~ RECCRD ALL DATA Qr FORNS PROVIDED (ITEN ) Itt THIS BCOKLETe Je,[Fi THE SERFACE WA['ER DISQ{ARGE APPLICANT Krglrs OR HAS R TD BELIEVE 1HAT rK[1 APPLt CABLE BIQLQG[cA[ ToxlclTY TEsTs wcRE HADE Itl 1HE LAsT THREE (3) YEARs 0N Ar?Y 0F THE APPLIC "IT S Dtso?'V?GES OR Qr A RECEIV[ta WATER IN RE[ATION TO A DISCHARGE PROVIDE THIS Il'FORIiATIQI AS /N ATTAotElrT TO THIS APPLICATICNe APPLICABLE/SEE ATTACHED K~

L.

IF A CQ?fRACT [A<<<<ATQRY OR CQISULT[lG Ftf?rt PERFQRNED Ar[Y OF T[E Ar/LAYSES REQUIRED BY DO Trrts APPLICATIQI, PROv[DE nIE r?A?k Ar?D ADDRESS OF EAOI uBQRATCRY OR PI[VI AND n?E A'Ã4.YSES PERFCR?ED AS AN ATTAQFE?IT CF THIS APPLICATICNo

'/CU D[SOiACE Ai// 0[HER TOXIC OR IN/IS?I TABLES IV P/AE tr Ara t[A nt?QUy vA Pp:Es

. ~ ICAL SISSTAIICES t?QT LIS'fED IN

. IF YES, THAI IDBITI Y 'nF. X NQT APPLICABLE APPL[CABuJSEE rt)T APPLICABLE

~ BELOW CHB?ICAL S?SSTA/ICES //S ESTIYv'LTE THE Ftr?AL EFFLUBIT CQICEN[RATIQ6o Stsft[T THIS Ir/QfPATIQI AS Arr ATTAoriBIT TO THIS APPLICATIQ4 APPLICABLE/SEE ATTAOIED K. NUS Corporation Laboratory Services Division 5350 Campbells Run Road Pittsburgh, PA 15205 37

INSTRUCTIONS FCR COHPLETING SECTION I I ITEN 6 This form requires Information on a specific outfaLI discharginq to the surface ~aters.

ENTER HE P >I T '4'LeE I:I 'E BOX AT THE TOP OF THIS FCRH ~ THE PEIL4IIJ NV4IBER CAN BE FC'UNO ON THE FRONT PAGE OF YOUR EXPIRING pEFAIIT. It >>nis Is a new or not orevlously permitted facility, then leave blank and a number wll I be assloned.

Enter the outfall number In the space provided for each page of Section Il. For each Individual discharce point a separate set of Section I I, Item 6 for.. s must bo f1 lied out.

ITEN 6 eRIORITY >ALLO ANTS AXO AOOITICNAL INFO%".ATIC!I NOTE: 11 >cu lave two ol more substantial ly Indentical outfal ls. you may request pemlssion from your permitting authority to sa>>ole snd anulv-e only one outfal I and submit the rosults of the analysis for other substantially Identical outfalls.

If your . ecuest Is granted by the permitting authority, on a separate sheet attached to the application form Identify which ca+fbi I you dld test, and doser ILe why tho outfall Is which you did not tes>> are substantially identical to ihe outfall whion ypu Cid test, "OT- aO CFR part I22.21(g)(S), Friday, Aprl I I, 1983, provides for a Small Business Exemption from the reoorting of quantitative data for organic toxic pollutants and toxic pollutants as required by Part 122.21(q)(7)(ll)(A) or 122.21(g)(7)(ill)(A).

A.-C. Tnese parts are selt-explanatory and do not require further inStructionS. Simply go through each part and do as Indicated.

and E.-J.

Several industrial categories and subcategories have been exempted frcm submitting data on certain GC/MS Fractions

('0 CFR Part 122, Vol. 48, No. 64, Friday, April I, 1983, Notes I, 2, and 3).

Review the following list. to detemslne whether your facility qualifies to bo exempt from reporting GC/HS (Gas Chromatography/

Hass Spectroscopy) Fractions.

GCre Fraction Testing and Reporting Exemptions Textile !Allis Industry

- All four Gclms crganlc fractions In the Greige 'ullls subcategory.

- Pesticide fraction In all other subparts of this Industry.

Ore Slinin and Oresslnn Industry

- Volatile, bose/neutral, and pesticide fractions In the Base and Precious <x!tais Subcategory.

- All four Gc/.'As organic fractions In all other subcategories of this Industry.

Porcelain Enamelln Indust

.- All four GC/HS organic fractions.

Gum and Wood Chemicals Industr

- Pestlcido fraction In the Tall OII Rosin Subcategory and tho Rosin Based Derivatives Subcategory.

- Pesticide and base/neutral free.tons In all other subcategories of this Industry.

Leather Tanning and Flnlshln Indust

- Pesticide fraction ln all subparts.

Paint and Ink Formulation Indust

- Pesticide fracticn In all subparts.

Phot ra hlc Sup Iles Industr

- Pesticide fraction In all subparts.

Petrolevn Reflnln Industr

- Acid, base/neutral, and pesticide fractions.,

Pul and Pa or Indust

- Pesticide fraction In Papergrade Sulflt'e subcategories (pubparts J and U).

- Base/neutral and pesticide fractions In oeink subpart o, olssolvlng Kraft subpart F, and paperboard from waste Pape~

Subpart E.

- volatile. base/neutral, postlcldo fractions In the BOT Bleached Kraft subpart H, semi-chemical subparts 8 and C, and Nonlntegrated-Fine Papers Subpart R.

~

Acid, baso/neutral, and pesticide fractions In Fine Bleached Kraft subpart I, oissolvinq sulfite pulp subpart Ki <<oun Fine Papers Subpart 0, Market Bleached Papers Subpart S.

Kraft Subpart G, TISSue from Wastepaper Subpart T, and Nonlntegrated Tiss~~

Steam Electric Power Plant Indust

- Bose/neutral fraction In the once-Through cooling water, Fly Ash, and Bottom Ash Transport water process wastestre~s'8

SECTION NUilllBERIW II M20005827 SE.E 'INSTRUCTIONS GN,REVERSE SIDE OrrrmI. rom ITEM UsE THts D ra SHEET ro PECOS trscRJ artON as RECutRED ttl: (CIECX APPROPRIATE Box FCR WHtcH INFCRMartctl THts DATA SHEET REPRESBITS.)

7 O le SECTION I Ii ITEM +E e ROLNDIILTER Dl SCHARGE INFO&AT lotl (PAGE 55)

CRITICAL

2. SEcrtotl II, ITBL 6. PLIGRITY PGLUJTA'lfs IN sNFAGE wATER DtsctFULE (PAGE 37) See attached MATERIALS data sheets.

TOXIC O 3. B. BELow: cRITlcAL HATBLIALs (TABLE lv) IN sURFAcE HATER DtscHARGE (PAGE 39)

POLLUTANTS HAZARDOUS SUBSTANCES l.lsr IY Cqtrtcar yal "I l (rasLE IV PAGE 6),"IOT ADIRESSED IN SECTICtt It ITEM Fe . RIORITY NOT APPLICABLE ForuLUe JIITS WHIDI YGU JTGrr OR lAVE IIBSGII TI) BEI IEVF. To BE PRESENT IN THE DISCHARGE ~ SFE IN REVERSE Slo- G THIS PAE FOR FUI22IER DIRECT 105.

DISCHARGE APPLICABLE (SEE BEUJW)

Ae IA".E CF CRlftQIL t'ATERIAL CR PRIORITY POLLUTANT c-ICBII".->rtl;U svFLE UNIT CODE Saul TYPE rr GF ANAlYSES Iii~

I B. LVERAGE TYPE; 0 OF AIIALYSES LJ

~

WIT WIT c.,axt~ ctx2cBITFartc.l n.D rass CODE LJ CGDE A. IoeuE GF CRITICAL iealERIAL OR PRIORITY RXLUfatlr B. AVBIJME C io YTPATIIXIJ SA'PLE TYPEJ 9 OF AILALYSES

. LLLJ LltlfLJ I CCOE S %%X TYPE CF ANALYSES WIT CODE t'AXltltLree'rEtelrReLTIGlt Atg UNtT CODE Ce iuASS LJ UNITS CODE A, IA'E GF CRITICAL tATERIAL CR PRICRllY POLLUTAtff 1 Mg/I Util'COE SA"PLE TYPE F OF AtIALYSES 2 Ug/ I Be AVEIUeGE CclCBITPATIOIU SA"PLE TYPEJ r OF AIIALYSES LJ 3 UNI T GODS WIT CODE LOS/DAY FAXteLJ". Cot&'ITRATIOIIAND t ASS 4 KG/DAY Ce LJ A. ItauE CF CRITrCAL t>ATERIAL CR PRIORITY POLLUTANf WIT CODE SA'IPLE TYPE JJ OF ANALYSES 3, AvERA -E colcBITRATIc'I; satIPLE TYPE; rl 0F AJIALYBEs LJ Llt IT CODE WIT CODE HaxttUL co:CEIITRAT lett ate sass C.

LJ SAMPLE TYPE Ae M% OF CRITICAL MATERIAL OR PRIGRITY POLUJTANT 1 GRAB IlIIT CODE SatPLE TYPE tt cF atIALYSES 2 24 HR.COMP. Be AVERariE CCIICBIIRATIotlt SA~ lYPEJ J. OF aiOLLYSES LJ C~ PAXL"LJI CCICBIIRATIotl atO PASS UNIT CODE UNIT CODE Ae IIAuE GF CRITICAL t'ATERIAL OR PRICRITY POLLUfattr Iilm B. I/ OF UNIT CODE SA'PLE TYPE 'F A'IALYSES I

AVERAGE CCtu~tfRATICII; SAMPLE TYPEe atIALYSES LJ C +AXI LlL CCICENTRAT ION AtiD Mass WIT CODE WIT CODE Ae ted% OF CRITICAL MATERtAL OR PRIORITY POLLUfattf Wtr CODE SaeIPLE lYPE JJ OF ANALYSES I

Be AVERAGE CCIICBITPAT[cttt SAMPLE 'fYPEJ Jr OF AJIALYSES LittT CODE Ltilf CODE C. MAXIELJL CCICEIITRATICN at8 MASS LJ A, tlat'IE GF CRITICAL IeaTERIAL OR PRIORITY POLLJJlatir SAeYeLE TYPE OF eV02LYSES

3. AYEPACE co'cBlrRATIotU saMPLE TYPE; Jl 0F Atw.YBEs r

C. MAXI,"EÃ Ccl2CBIIPATIOII atlt Wss Wlf CODE Wl T CODE acotrtctlaL PAGEs cF THIs ITBL 7 ARE ATTAcHED FGR TIE REsi GF lHE cRITIcaL CI YEs MATERIALS AND/GR PRICRITY PCLLUrattls RECIJIRED TO BE REPORTED ~ K:XJ 39

INSTRUCTIONS FOR CCMPLETING SECTION I I ITEM 7 This form Is to be used by both surface and groundwater applicants to record Intormatlon on any Michigan critical material, E,P.A.

priority pollutant, or hazardous substance In ~hlch this application requires data to be provided. This ~ould Include any chemical substance frcm the Mlchlqan Critical Materials Register (Table IV), the E.P.A. Priority Pollutant Listing (Table v), or Tables IIA-VA <<hlch lists Organic Toxic Pollutants, Other Toxic Pollutants, Conventional and Nonconventional Pollutants and Hazardous Substances ~

ITEM 7 CRITICAI. MATERIALS PRIORITY POLLUTANTS AND/OR HAZAROOUS SUBSTANCES IN THE OISCHARGE Material I 2 ~ 3 .. ~ 8 A. List the name of the chemical substance (critical material, priority pollutant, or hazardous substance) from Tables IV, V and I IA-vA as required In the bcx which you checked in A.1-3 . above. Enter each chemical substance's parameter number as listed in Tables IV, V and IIA-VA It provided.

B. Prbvlde the average concentration ot the chemical substance named In A. Indicate the sample type used and the number of analyses mace to provide the concentration data for the chemical substance named In A.

C. Provide the maximum concentration and determine the mass loading ot the chemical substance named In A NOTES: I. It only one analysis was made for a chemical substance then record that data as a maximum value.

analysis has been made for a chemical substance then provide an average value of those analyses andItthe more than one maximum va I ue,

2. This Section II, item 7, Data Sheet provides space tor recording data for 8 chemical substances Additional space for recording of data for more then 8 Materials can be made by making copies of (Materials).

this Item 7 Oats Sheet as needed. It Is also Important to use a separate set ot Data Sheets for each applicable reporting requirement as listed in A.l-3. and for each outtal(.

3. Refer to the left margin for the code number representing the sample type used and the appropriate unit codes.

40

ftaaarr Tg:

WAN ~boratopy $ aa Olvlaioh 53$ O Carnpba~un Road Pittmburgh, PA 1S2OS 412-788-f080 Park Waat y~

Ciiff Mine Road Pittabwgh, PA 182rS A 3B A Mnl 'rm XM WWF t3M ll CLIENT HNIE'HDIAHA l NICMIOAH ELECTRIC CO. HUS CLIENT HOf 010904 ADDRESSI P.O. BOX 312/D.C. COOK PLANT HUS SAMPLE Nf 16080400 BRIDGENNf NI 49106 VEHDOR HOf 05411000 REP(HT DATE f 08/29/86 MORK ORDER HOf 55830 ATlEHT ION( . D FITZSERALD/STENRT DATE RECEIVED! 08/08/86 SAMPLE IDEHTIFICATIO}lf NAKEUP PLAHT PREFILTB BACKNSM CO)P 08/06 0930 TEST BETE)KNATION UNITS e

~ N360 'i%'DES PART U-A REOUIRED-M032 Aaaonia as N (distillation) < 0.1 'S'1 MOSO mf 5<as (02) 2 Ml M116 Organic Carbon(nonwurseable) 3.8 aN/1 N120 COD (02) 1D as/1 M490 rM 7.9 M610 Solidsf susrended at 1D3 C 16 N361 HPDES PART V-B N010 Aluainua (Al> 1.7 Ml NO40 Bariua (Ba) < 0.1 afll N150 Cobalt (Co) < 0.01 rf/1 N190 Ironf total (Fe) 0.08 Nfl N230 Ma&esiua 08) 9.9' Nfl N240 Man@nese Ofn) 0.01 ~ 5'1 N260 Nolubdenua Ofo) ( 0.03 H/1 N340 Tin (Sn) <1 as/1 N350 Titaniua (Ti) < D.5 H/1 N055 Boron (B) < 0.2 aN/1 MO60 Broaide (Br) < 2.0 H/1 M225 Colorf True 5 Pt-Co N310 Fluoridef total (F) 2.7 H/1

)090 Hitrate (H) 0.3 as/1 M410 Nitf ite (N) ( 0.01 as/1 H435 Hitrosenf Kieldahl (H) 0.4 aN/1 N440 Nitrosenf Organic (H) 0,4 H/1 N540 Phosrhorusf total (P) 0.34 a&1 N730 Sulfatef turbidiaetf ic (SO4) 25 as/1 N740 Sulfide (S) < 0.1 <<l/1 M760 Sulfite (M3) (1 H/1 N770 Surfactants (NBAS) < 0,05 ~

as/1 N362 HPDES PART V< TOXIC NETALS N020 Antiaons (Sb) < 0.1 aC/1 PASE HOf 1 A Halllburton Campany CLIENT ORlGINAL

RKlllTTO:

mme Laboratory ces Olvisice 5350 Camp58b Run Road Pittsburgh, PA 15205 41 2-788-1080 Park West Two Cltt Mine Road Pittsburgh, PA t5275 LAB ANALYGXG REPQRT CLIENT @@t I)III(A4 NICHI6Q ELECTRIC CG. IfS CLIHfl Nt 414944 ADNESS! Pa O. BGX 312/D.C. CQGK PUNT )IS SNPLE I)t 16080440 BRIDGEMr i)I'910& VENOR )It 054ii400 REP(NT DATE t 08/29/86 NHX Gm NGt 55830 ATTENTII(t D FITZGERALD/STE)NT BATE RECEIVED t 08/08/86 SNYE IKITIFICATIGHt iNEUP PUOIT PREFILTER BACQiASH CORP 08/06 4930 TEST BETERKNTII( RFULTS UNITS N30 Arsenic (As) 0.042 H/1 N50 Berslliua ne) < 0,002 aN/1 N90 Cadaiua (Cd) ( 4,405 H/I Hi40 Chroaiua (Cr) C 0.01 Nfl

)l160 Correr (Cu) < 0.01 N/1

)i200 Lead (Pb) C 0.03 HR

%50 )fercars (HS) ( 0.4402 M1 iQ70 Hickel Oil) <003 H/1 i(290 Seleniua (Se) ( 0.044 Ml

)000 Silver (4) C 0.01 H/1

)030 Th> 11 iua (TI) ( 4.1 H/1 KBO Zinc (Zn) 0 07 Wl M270 Cuanider total (CS ( 0.405 ac)

N500 Phenolics C 0.02 af/I 0110 VOLATILES"PP IH RATER OVOi Acrolein < 100 u&l.

~

OV02 Acralonitr ile C 100 a5/1 OVO3 Benzene <5 Wl OV05 Broaofora (5 uS'1 OV06 Carbon Tetrachloride (5 a&i OVO7 Chiorobenzene <5 a&1 0V08 Chlorodibroaoaethane <5 uS3 OVO9 Chloroethane ( 10 uN/1 OV10 2Mloroethslvinsl Ether < 10 ul/3 OVli Chlorofora (5 u&l OV12 Dichlorobroaoaethsne <5 uN/1 OV14 iri-Bichloraethane (5 aN/1 OV15 ir2-Dichloroethsne'r <5 uN/1 OV16 1-Bichiar aethulene (5 aS'1 0V17 ir2-Bichlororrorsne <5 uS'1 OV18 fr3-Bichlororrarslene (5 aS/1 OV19 Ethslbenzene <5 oN/1 PA6E Nt 2 A Halilbunon Company CLlENT OR161NAL

REMIT TO:

Laboratory~loca Olviaion Partt Weat Two 5350 Camp~ Run Road Cllrf Mine Road Pittsburgh, PA 15205 Pittsburgh. PA 15275 412-788-1080 CLIE)(T %%1 1011(A 4 )fICHIEAN ELECTRIC CQ. IS CLIQfT )Ir 010904 A99RESSr P.O. MX 312/S.C. COOK PLANT NS %PLE Nl 16080400 SRISGE)tA)fr Ifi 49106 VE)IOR Nt 05411000 REPORT BATE t 0&/29/86 ')IOIN ORBER )Iz 55830 ATTHfTINl BATE RECEIVES t 08/08/86 SA)(PLE IBE)fTIFICATIO)fr NKHP PLANT PREFILTER SAC)OIAQI CO)fP 08/06 0930 TEST 9ETER)fINATIO)f RESULTS NITS OV20 )fethsl Sroaide ( 10 IVI OV21 )feths I Chlor ide OV22 OV23

)fethsi ene Chlor ide irir2r2-Tetrachloroethane

<5 10 ~/1 ns/1 skaeg M OV24 Tetrachlorcethslene(Perchloro) (5 u&l .

gg/7/ g Ecf~

OV25 Toluene (5 OV26 ir2-Trans-9ichloroethslene (5 ~4'cc fe5 I<+~

0V27 ir i)1-Tr ichloroethane <5 uf/I OV28 irir2-Trfchloroethane <5 OV29 Trichloroethslene (5 uf/I gfmfagje OV30 TrichforoFIaoroaethane (5 ee'(~id OV31 Vinsl chloride C 10 ~epic e 0120 ACIBS -.PP IN NATER OA01 2M)or orhenol C 10. u&l OA02 2r 4-Bichlor orhenol < 10 as/I OA03 2r 4-Binethslrhenol C 10 OA04 4r6-Binftr~cresoi < 50 u&1 OAOS 2r4-Oinitrorhenol < 50 trf/1 OA06 2-Nitrorhenol ( 10 o5/I OA07 4-Nitrorhenol C 50 OA08 rWIat 8-mresol C 10 us/I OA09 'entachl ororhenol < 50 trs/1 OA10 Phenol ( 10 us/I OA11 2>4r6-Trichlora henol < 10 OE30 Acid Extraction Hater 0130 BASE NEUTRALS - PP IN NATER DB01 Acenarhthene ( 10 os/I OB02 Acenarhthslene C 10 us/I DS03 Anthracene ( 10 us/)

0904 Benzidine C 50 a$ 1 OS05 Senzo(a)Anthtacene ( 10 us/I OB06 Senzo(a)Psrene C 10 us/I PAGE NOr 3 A Haliiburton Company CLIENT ORIGINAL

RtaltT TO:

wee ~ Laboratory 5350 Camp~

oea Div>s>on Run Road Pittsburgh, PA 15205 412-788-1080 Park Weat Two Cliff Mine Road Pittsburgh. PA 15275 LAB ANALYSXS REPORT CLIENT MEf INBMA 4 )IIC)IIMMETRIC CO. NS CLIENT )If 010904 AOMESS f P,O. BOX 312/B.C. CMK PUNT N)S SNAB )If id(je0400 BRIEGBANr HI 49106 KNNR Nf 05411000 REPORT BATE f 08'/8& RORK IIER )Nf 55830 ATTE1(TINf, D FITZGE)N.B/STHQRT BATE RECEIKSf 08/08/86 SANPLE IBENTIFICATIOHt QKEUP PLANT PREFILTER BACQASH Cm(P 08l06 0930 TEST BETER)GQTIN RESULTS OBD7 3r 4-Benzol iuoranthene ( 10 udl OB08 Senzo(shi)Parsi ene C 10 us/I OB09 Benzo(k) Fluaranthene ( 10 us/I OB10 Bis(ZWloraethoxs)Hethane ( 10 ud/I OB11 Bis(2-Chiaroethsl)Ether ( 10 us/I OB12 Bis(~loroisarronl)Ether C 10 uS'I OB13 Bis(2-Ettslhexsl)Phthaiate < 10 u5/I OB14 4-Bronc hensl Phensl Ether C 10 us'/I OB15 Batsl Benzsl Phthaiate ( 10 uS'I OB16 2-Chlaronarhthalene < 10 ua'I OB17 Phensl Ether

'WIororhensI

< 10 uS'I OB18 Chfssene C 10 us/I OBO Bibenzo(arh)Anthracene ( 10 uI/I OB20 ir2-Bichlorobenzene C 10 u6'I OB21 }r3"Blchlorabenzene ( 10 us/I OB22 lr4-Bichlorobenzene C 10 u&

OB23 3r3'-Bichiarabenzidine ( 20 us/I 0924 Biethvi Phthalate C 10 u61 OB25 0 iaethsl Phtha late C 10 aN/1 OB26 BiMBatsI Phthalate C 10 u5/I OB27 2r 4-Bini trotoluene ( 10 u&I OB28 2rd-Binitrotoluene C 10 ukI NZ7 Bi-NWtsI Phthalata ( 10 us/I OB30 ir2-Oirhenslhsdrazine(Azobz) C 20 us/I OB31 Fluaranthene ( 10 us/I OB32 Fluor cue < 10 uN/I OB33 Hexachlarbeniene ( 10 OB34 Hexa chlor aha tadi ene C 10 us/I OB3S Hexachlarowscl orentidi ene C 10 us/I OB36 Hexachloroethane C 10 . u5ll OB37 Indeno(ir2r3 cd)Psrene ( 10 us/I

. OB38 Isorhorone C 10 uf/I PASE NOt ~4 A HaHlburton Company CLIENT ORIGINAL

RENT TO:

Laboratory S Ohision Park West Two 5350 Camp un Road Clitf Mine Road Pittsburgh, PA 15205 Pittsburgh, PA 15275 412-TM->OaO LAB ANALYSXB RFPQRT CUENT NAHEt IHBIANA 4 NICHISAN ELECTRIC CO. IJS CUENT NO t 010904 ABBRESSt P.O. BOX 312/S.C. COOK PUNT NS SIFFLE HOt 160e0400 BRISGB%lr NI 49106 tiENSOR Nt 05411000 NM ORDER NOt 55830 ATTENTIONt B FIT16ERALS/STEWART SATE RECEIKit 08/08/86 SNPLE ISENTIFICATIONt HAKEUP PLANT PREFILTER BAQOlASH CON'8/06 0930 TEST SETERNINATIGN RESULTS UNITS OB39 Ha> htha leuc ( 10 util OB40 Hi trobenzene < 10 uf/1 GB41 ~

N-Nitrosodiwthnlaaine C 10 uS'1 OB42 N-Nitrosodi~onlanine C 10 uf/1 GB43 lHlitrosodirhenuiaine C 10 All OB44 Phenanthrene < 10 a5'1 OB45 Parcae ( 10 H/1 OB46 1>2)4-Ttichlorobentene < 10 af/1 OE25 Base Neutral Extraction+ater 0142 PESTICIDES/PCB'S - PP IN NTER GE10 Pesticide/PCB ExtractionWter OPO1 Aldr in < 0.05 aS'1 OP02 alrha BHC ( 0.05 us/1 OP03 beta BHC- <005 aS'1 GP04 delta BHC ( 0.05 H/1

%05 Qwa NI: (Lindane) < 0.05 u&1 GPD6 Chl or dane < 0.50 ue/1 GP07 4-4'SDB < 0.10 uf/1 0P08 4-4'DDE ( 0.10 a&i GP09 4"4'DBT C 0.10 a&1 GP10 Dieldrin C 0.10 u&1 OPil Endosol fan I < 0.05 uS1 OP12 Endosul fan II ( 0.10 u&l OP13 Endosul fan Sulfate C Oe10 ad/1 0P14 Endr in ( 0.10 a5/1 OP15 Endrin Aldehsde C 0.10 anal OP16 Her tachl or ( 0.05 u&1

, OP17 Her tachlor Eroxide C 0.05 u5/1

'P18 Tox ar hene ( 1.0 a&i OP19 PCB-1016 C 0.5 Ml 0P20 PCB"1221 C 0.5 aN/1 OP21 PCB"1232 < 0.5 aQl PAGE NOt 5 A Halllburton Company CLl ENT ORlGINAL

REaafT To:

MAR ~ Laboratory S 53SO Camp un Road Pittsburgh, PA 15205 4 12.788 1080 Pa& West Two Clltt Mine Road P>ttaburgh, PA 15275 LAB ALAI YS X S REPORT CUENT MEt ISIQh i NCHISQ ELETRIC CO. NS CLIENT Nt 010904 ADDRESS t P.Oe M 312/D.Co COOK PLN(T iIS SANTE Nt 16080400 NI36EMr NI 49106 MSGR Nr 05411000 REPORT DATE 1 08/29/86 NNK ORDER Nt 55830 ATTENTINl 3 FITlOERALj/!iRMRT DATE RECHVB t 08/08/86 SSPLE IMCTIFICATINt SKEbP PLhNT PREFILTER MQNSH CII'8/06 0930 TEST DETERHIQTIN RESULTS NIITS OP22 PC3-1242 ( 0.5 u8/1 OP23 PCS"1248 C 0.5 uf/1 OP24 PCB"1254 C 1.0 ural OP25 PC3-1260 C loO ural R450 RADIN 226 NQ 228 R804 Radius-226 C 0,5 t Ci/1 NN5 Radiua-228 (3 rC1/1 R800 Gross A1]ha (4 eCi/1 R801 Gross Beta (6 rCi/1 8150 Chiorirter Totai Res DPD (CI2l C O.i '/1 CORKERS l Revicved arty Arrrovcd bet Jll A Haliibutton ComPan/ CLlK~EQQG)HA@

RalatT TOt Laboratory acesRun ONision Park West Two 5350 Camp~ Road Ctltt Mine Road Pittsburgh, PA 15205 Pittsburgh. PA 15275 412-788-1080 I AB ANALYGXR REPQRT CLIENT }NEt IIIMA4 IIICHISAN ELECTRIC CO, NUS CUENT Not OM04 ZiBRESSt P.a. Sm 31Z/b.C. CmX PUNT IIS SNflE No! INSH03 BRI 6ENQr IG 49106 KIN Not 0MIOOO REPORT jQTEt M/29/Q NRK ORBER Nt 55NO ATTENTIONt b FITICERAUI/STHSNT BQE RECEI~ t 08/08/Q SlIPLE DENTIFICATINt QKBP PUNt PREFIUER NQONSf-6RQ 111 08/Ob 0300 TEST BETERNnOTION RESULTS UNITS BQ4 Fecal Col ifora (N03 Q col/100al N82 OilrextrictiotMavileb'ic(3) < 3.0 af/1 COIltiEilTS t Rcvicuetl anti ~rrovcd bet JN A Halllburton CompanY CLIENT ORIGINAL

~ ~

RalktT TO:

NLjB ~ Laboratory 5350

~aces Camp~un Pittsburgh, Pa 15205 Division Road 412-788-1080 Pa& West Two Cliff Mine Road Pittsburgh, PA 15275 LAB ANALYBXB REPORT CLIEHT MEf IHDIAHA 4 HICHISIt ELECTRIC COo NS CLIEHT HOt 010904 ADDRESSl P.O. BOX 312/D.C. CGGK PUNT HUS SAHPLE NOf 16080404 BRIDOEHAHr HI 49146 N3DOR HOf 05411000 REPORT BATE t 08/29/86 NOR); ORDER NOf mm ATTEHTIOHt D FI DATE RECEIVBt 08/08/86 SIFLE IDEXTIFICATIOHf HAKEI'LANTPREFILTER BACKNASH-GRAB IU 08/06 0920 TEST DETERHIHATIOH RESllLTS IGTS BA35 Fecal Col ifori OPH)4 n col/14411 M683 Oil r extrsction&raviietr ic(h) < 3.0 85fl CQQSlTS l RevievQ anti Arrroved bet @ A Halliburton ComPany CllKNY ORlGlNA1.

RHatT TO:

~UB ~ Laboratory .~" lees Dbrision 5350 Cam Pittsburgh, Run Road 15205 412-788-1080 Park West Two Cliff Mine Road Pittsburgh, PA 15275 I AB ANALYS X S REPORT

%Et liaiIANA 6 NICHIEAN ELECTRIC CO. NS CLIENT NOt 010904 CLIENT A9$KSSf P.O. POX312/B.C. CON PLANT NI36EMr tQ 49106 II YHGN SANPLE NOt NO 1 16080402 05411000 REPORT SATED 08/29/86 NN 9CB NO! %830 ATTENTIONf 3 FITZERAL9/STENNT SATE RKEIlJBi 08/08/86 SAMPLE IEENTIFICATIONf NAKEUP PLANT PREFILTER EAClOQS .NQ II 08/05 1645 SPiiNINATION UNITS SA33 Fecal Califari OP$ 2 (3 cgl/100al 8681 Oilfextractiooaraviaetric(2) 3o4 All CHITS'af prrrovsd bs A Hailiburton Company CLIENT ORIGlNAL

REMIT TO:

Laboratory P "~lees Division Park West Two 5350 Camp Run Road Clltf Mine Road Pittsburgh, 15205 Pittsburgh, PA 15275 412-786-1080 I AB ANALYSXS REPORT CLIB}T SKI I}IIA}A4 NICHIM ELECTRIC CO, N}S CUENT NI 010904 ADDRESSI P,O. BOX 312/B,C, COCK PLAWT NJS SQPLE jm I 1g90401 BRIBGEMr NI 49106 KKN Nt 0MI000 REPORT NTE I 08/29/86 i}ON MER NI 55830 ATTENTINI B FITZGERAL/STEQRT BATE RECEIi/EBI 08/08/0 SNPLE IKlTIFICATII}I i}AKEUP PLNT PREFILTER BANNAS)HRAl I 08/05 1125 BETER}}IQTIO}} RESlJLTS N}ITS BA32 Fecal Colifora - M <3 col/l,00al R680 Oiir extractiot+raviaetric ,< 3.0

                                          'redye(}

CQ}ll}ENTSI Rpg I e'get} agQ +f hs i A Hsl }}burton Company CLl EHY ORlQINAL

'e'A fj <<3 ReaatT To: Laboratory &rvloae Olvialon Pa& Weat Two 5350 Camp Run Road Cliff Mine Road Pittsburgh. 15205 Pittsburgh, PA 15275 412-785-1050 I A39 A blAI V'~ ~X M R'.K'F'C) A' CLIENT ~l INSIANA 4 NIQGSAN ELECTRIC CO. Im CLIENT XOt DISS ASSRESS: . P.O. MX 3!2/S.C. COOK PLANT Im RIFLE N! 16101256 SRBGBSNi NI 49106 VENSGR NG! 05411000 REP6RT SATE l 11/07/86 IiRK GRSER Nt 55830 ATTENTINt SATE RECEIVES l 10/17/86 SAWLE ISaTIPICATIONt NAKEI'LANT ~LIER SAmiASH CGI'0/13-14 SETENINATION

                                                ~ ~

0110 VGLATILZSW IN RATER GV01 Acrolein < 100 u81 OV02 Acrslonitrile ( 100 as/1 Ott03 Senzene <5 us/1 OV05 Sroeofara (5 ue/I GV06 Carbon Tetrachloride (5 us/1 GV07 Chlarobenzene <5 u5/1 OV08 Chlorodibronoaethane (5 Wl GV09 Chloroethane ( 10 u&1 OVID 2-Chloroethslvinsl Ether ( 10 uSI GVII Chiorofora (5 ue/1 OV12 Sichlorobronooethane (5 u&l OVID irI-Sichlaraethane (5 us/1 OV15 Ir2-Sichloroethane < 5 u5/1 GVI6 ir I-S ichloraethsl ene (5 us/1 GVI7 irk-Sichlora rorane <5 H/1 OV18 ir3-Sichlorarrorslene (5 u5/1 OVI9 Ethslbenzene <5 uN/1 OV20 Nethsl Sroeide < 10 as/1 GV21 Nethsl Chloride < 10 u&l GV22 Ãethsl ene Chlor ide (5 uN/1 GV23 I ) ir2r 2-Tetr achl oroethane <5 u5/1 OV24 Tetrachloroeths iene<Perchlor a) (5 u01 OV25 Tttiuene <5 us/1 GV26 ir2-Trans-9ichioraethsl ene <5 us/1 CONSOLS GV27 Iiii i-Tr ichl oroethane (5 u5/1 OV28 irir2-Tr i chloroethane (5 as/1 OV29 Trichloroethslene <5 us/1 OV30 Trichiarofluaroeethane (5 us/l GV3I Vinsl chloride ( 10 uf/1 l Revieued and Arrroved bst AC A Halliburton Company CLIENT ORIGINAL}}