ML20138P014

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LOCA Amercoat D-6/Phenoline 305 Finish & Comanche Peak LOCA FSAR Curve, Final Rept
ML20138P014
Person / Time
Site: Comanche Peak, 05000000
Issue date: 04/11/1978
From: Ladage J, Montle J, Tellor M
CARBOLINE CO.
To:
Shared Package
ML20138M609 List: ... further results
References
FOIA-85-59 01684, 1684, NUDOCS 8511060295
Download: ML20138P014 (6)
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LAEORATORY TEST REPORT r

3 August 11, 1978 g

lO C Testing Project: 01684 T'NAI. REPORT l SUEJECT: LOCA; Amercoat D-6/Phenoline 305 Finish and the Coc:anche Peak i FSAR LOCA Curve

} RITERENCE: Cemanche Peak Nuclear Station; Mr. Don Sutton; Mr. Keith Falk; Mr. Dan W. McBride; Testing Project 01651 i PURPOSE: To determine tha performance of Ic Amercoat D-6/lc Phenoline.305 i Finish when exposed to the Comanche Peak Steam Electric Station, FSAR LOCA curve and evaluated according to ANSI N101.2-1972, Section 4.5 as interpreted by Carboline.

CONCLUSION: After the seven days of the Comanche Peak FSAR LOCA curve, the following exhibit an acceptable performance: ,

System Primer cure 1,2 le Amercoat D-6 17 days at 67-79'? (19-26*C) le Phenolice 305 Finish and 53-88% R.E.

3,4 le Amercoat D-6 17 days at 95-100*F '35-38'C)

Ic Phenoline 305 Finish and 100% R.R.

U PROCEDURE: A) Test Coupons Size: 2" x 4" x 1/4" Certified ASTM A36 Steel Surface Prep: Gritblasted to SSPC-SP5-63

. Abrasive Media: GTH #50 grit (Cleveland Metal Abrasives, Inc.)

3) Systems Tested Batch Numbers Drv Film Thickness 1,2 le Amercoat D-6 1503310 2.5 - 3.5 mils (cured in Cure Cabinet *) 1503210 le Phenolice 305 Finish 7B0427M 6.2 - 8.6 mils 6M39595 9.2 -11.1 mils 3,4 lc Amercoat D-6 1503310 2.4 - 3.3 mils (cured in High Humidity 1503210 Drum **)

Ic Phenoline 305 Finish 7B0427M 4.7 - 5.4 mils 6M3959M 7.3 - 8.0 mils

  • Cur Cabinet is at ambient temperature but, has hunidity controlled frem 50% to 90% R.H.
    • High Humidity Drum is at 100*F (38'C) and 100% R.H.

From the Carboline Research 8 Development Laboratory

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- . LA AORATORY TEST REPORT August 11, 1978/Page 2 Testing Project: 01684 FINAL REPORT PROCEDURE: (Continued)

C. Cure Schedule 1'

1,2 Amercoat D-6: 17 days et 67-79'F (19-26*C) and 53-88%

Relative Humidity.

Phenoline "105 Finish: 18 days at 71-80*F (22-27'C) and

55-70% Relative Humidity.

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- 3,4 Amercoat D-6: 17 days at 95-100*F (35-38'C) and 100%

Relative Humidity.

Phenoline 305 Finish: 18 days at 71-80*F (22-27'C) and 55-70% Relative Humidity. ,

}

l D. Exposure l ,

i i Texas Utilities Generating Company, Comman-he Peak Steam

! Electric Station, FSAR Figures 6.2.1-1 and 6.2.1-2.

. 1 l 1 1. Time / Temperature / Pressure Profile Time Temperature Pressure Spray Condition k

) Initial to 10 seconds 240*F (ll5'C) 44 psia Static 10 seconds to 15 mins. 270*F (132*C) 58 psia Dynamic 15 mins. to 1 hour1.157407e-5 days <br />2.777778e-4 hours <br />1.653439e-6 weeks <br />3.805e-7 months <br />

. 15 mins. 215'T (102*C) 34 psia Dynamic 1 hcur 15 mins. to

. 7 days 215'F-130*F 34-10 psia Dynamic (102*C-51'C) l (Note: This is the theoretical curve supplied by Comanche Peak. It was l followed as closely as possible with the LOCA apparatus available at I

Carboline Company. Please refer to the recorder chart (Lil5-129) for l

exact conditions of LOCA profile.)

~

2. Spray Solution H2 B03 (2000 ppm as Boron) in deioni:ed water.

pH = 8.5 - 10.0 (NaOH added to adjust pH).

i

CRADING PROCEDURI:

l i

j The test coupons were evaluated for performance in the following areas:

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1) Material flaking off l
2) Delamination between coats and/.or peeling

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,' 8 LABORATORY TEST REPORT

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( August 11, 1978/Page 3

-, Te. ting Project
01684

&gFINALREPORT GR.CING PROCIEUPI: (Continued)

. 3) Blistering of the topcoat

4) Chalking of the coating
5) Excessive cracking Grading procedu'res specified in Report N101.2 - 1972 of the American National Standards Institute-Protective coatingt for Light Water Nuclear Reactor Containment Facilities:

t 4.5 Methods of Ensining and Evaluating the Exeosed Test specimens The dynamic and/or static elevated temperature pressure and irradiation l test panels shall be evaluated within 2 hours2.314815e-5 days <br />5.555556e-4 hours <br />3.306878e-6 weeks <br />7.61e-7 months <br /> aad again after 2 weeks after j removal from the test chamber for the following surface defects; flaking, i delamination and/or peeling, blistering, and chalking. Defects listed.in Subsections 4.5.1 through 4.5.4 shall be dealt with as follows:

l 4^.5.1 Flaking. ASTM D772,. Evaluating Degree of Resistance to Tlaking I

(Scaling) of Exterior Paints, ? art 21, American Society for Testing and Materials, Philadelphia, Pa. 19103. Flaking shall not be permitted.

g 4.5.2 Delamination and/or Peeling. Delamination and/or peeling shall a .not be per:sitted.

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. 4.5.3 Blistering. Plistering shall be lir.ited to a few, intact blisters,

, Size No. 4, ASTM D714, Standard Method of ' Evaluating Degree of Blistering 2

of Paints, Part 21, American Society for Testing and Materials, Philadelphia, i i Pa.- 19103. The number and the size of blisters shall be recorded.

i i 4.5.4 Chalking. ASIM D6$9, Standard Method of Evaluating Degree of j  !

Resistance to Chalking of Exterior Paints, Part 21, American Sociecy for

- Testing and Materials, Philadelphia, Pa. 19103. Heavy chelking shall not be permitted.

5 Any other changes in coating properties which are not also associated with the separation, or the release, of coating from the substrate shall not be l a cause for rejection.

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LABORATORY TEST REPORT

( August 11, 1978/Page 4

.f" T: sting Project: 01684 FINAI. REPORT ANSI N101.2-1972 Criteria (As interpreted by Carboline)

Maximum Degree of Failure Allowable Flaking ASD D772 10 (None)

Delanination or Peeling None i ,

  • Blistering ASTM D714-56 Blister Size Blister Density'

. #2 None

  • NOTE: A blister is not #4 Few intact when it has resulted #6 Medium in coating being separated #8 Medium-Dense i frca the test coupon. .

Chalking ASTM D659 8 (Light)

. NOTE: Flaking, blistering and chalking are all. evaluated according to ASN Standards, with a rating of 10 ind1cating that no failure was observed in the specific grading area.

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Testingf^ icct: 01684 ,Q August 11 d'sfl/P.in ".

FINAL. R( R Panel Identification Dry Delamina- Other

  • and tion or Performance Pe r f o e m'.i ni .

Fi)= Chalking Characteristics F.va l u.it s on j Coating System Thickness Flaking Peeling Blistering i

IA* Ic Amercoat D-6 3.5 mils 10 None Nonc 10 ---- Acreptafsic (Primer cure 53-88% R.ll.

Ic Phenoline 305 Finish 6.5 mils 10.0 mils lil Ic Amercoat D-6 3.0 mils 10 None #4 Few Intact 10 ---- Accc, .htc j (Primer cure 53-88% R.II.)

, Ic Phenoline 305 Finish 6.2 mils I 9.2 mils

,' 2A* Ic Amercoat D-6 2.8 mils 10 None None 10 ---- Acceptable '.

(Primer cure 53-88% R ll.)

Ic Phenoline 305 Finish 7.7 mits "

10.5 mils 2ft Ic Incrcoat 11-6 2.5 mils 10 Mone #4 Few Intact 10 ---- Acceptable (Primer cure 53-88% R.ll.)

Ic Phenoline 305 Finish 8.6 mils 11.1 mils

! 10 None Nonc 10 ----

Accer'abic 3A* Ic Amercoat D-6 2.4 mils '

j (Primer cure 100% P.ll.) -

ic Phenoline 305 Finish 5.4 mils 7.8 mits ,

3.3 mils 10 None None 10 ----

Acceptahic

! 3 11 It Amercoat D-6 .

I (Primer cure 100% R.ll.)

Ic l'henoline 305 Finish 4.7 mils 8.0 mils

) . . _ . __ -

4A* Ic Amercoat D-6 2.6 mils 10 None None 10 ---- Acceptahlt (Primer cure 100% R.II.)

Ic Phenoline 305 Finish 4.7 mils ** '

7.3 mils 10 None Nonc 10 ---- Acccp alitr '

40 Ic Amercoat D-6 2.5 mits (Primer cure 10G% R.ll.)

Ic Phenotine 305 Finish 4.9 mils 7.4 mils __ _ _ _ _ _ _ _ . . . _ _ _ _

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August i U/ Pa ge . e.

Testings jject: 01684 .

f,1NAI. REPORT RESill.TS .

i Panel IdentificaLion. Irry Delanina- Other

! and Film , tion or . Performance Performanc Coating System Thickness Flaking Peeling Blistering Chalking Characteristics Evaluation deceptable Performance 10 None #4F to #8HI) #8 (Light)

As Interpreted by Carboline l s

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C John F. Hontle John J. J. adage, Jr. Michael D. Tellor ,

Developmental Chemist Supervisor Vice President

. Testing Department Research & Development Research & Development .

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LABORATORY TEST REPORT y;jN i

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[ Testi g Project: 901651 May 9, 1978

~~

FINAL REPCRT CChe ErNTIAL 1

i

SUBJECT:

LOCA test of systems topcoated with Phenoline 305 Fisish.

R_NCI:Commanche Peak Nuclear Power Station; Mr. Don Sutton, Mr. Keith Falk; 1 . Mr. Dan Mc3 ride; L-115-105 I PURPCSI: To test the perfor: nance of Phenoline 305 Finish over each of the 1 following primers:

,1) Ic Amercoat D-6 @ 2.0 - 3.0 mils

. 2) Ic Mobil Zinc 7 @ 2.0 - 3.0 mils -

3) Ic Carbo Zine 11 @ 11.0'- 12.0 mils i when exposed to the Co - anche Peak Steam Electric Station, FSAR LOCA Curve and evaluated according to the criteria of ANSI N101.2 - 1972, l

1 Section 4.5 as interpreted by Carbolise.

CCNCL"SICNS: After completion of the 7 day Co =2nche Peak ISAR 1CCA test, the systems tested exhibited the following perfor=ances when evaluated according to ANSI N101.2 - 1972, Sectie: 4.5 as interpreted by Carbo 11:e:

l ,

Coatist Svstem Perfor=ance

1) Amercoat D-6 @ 2-3 mils Vapor Phase Acceptable Phenoline 305 Finish
2) Amercoat D-6 @ 2-3 mils Liquid Phase Unace ptable Phenolise 305 Finish
3) Mobil Zinc 7 @ 2-3 mils vapor Phase Acceptable Phenolice 305 Finish
4) Mobil Zisc 7 @ 2-3 mils Liquid Phase Acceptable Phenoline 305 Finish i
5) Carbo Zine 11 @ 11-12 mils vapor Phase Unacceptable Phenoline 305 Finish
6) Carbo Zine 11 9 11-12 mils Liquid Phase Unacceptable j .Phenolise 305 Finish

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i LABORATORY TEST REPORT D

May 9, 1973/? age 2

$Na . f COiTIDEE IAL .

i, PRCCIDERE: A) Test Courons f

Size: 2" x 4" x 1/4" Certified ASTM A36 Steel.

Surface Prep: Gritblasted to SSPC-SPS-63 Abrasive Media: 6FH d50 grit (Cleveland Metal Abrasives, Incl Dry Film

? 3) Thickness 3' Systems Tested Batch Numbers ,

1) Ic Amerecat D-6 6-705416 2.5 - 3.0 mils
  • 6-705420 le Phenoli=e 305 Timish 7I25285 4.8 - 6.2 mils __

7I25005 7.3 - 8.5 mils 1

! 2) Ic Mobil Zi=c 7 FT7I24 2.1 - 2.7 mils Ic Phenoline 305 Finish 7I252SM 5.3 - 6.9 mils I

7I2500M 8.0 - 9.0 m:.ls

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! 3) Ic Carbo Zi=c 11 7I5106M 11.0 -13.0 mils 710966Z l

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/'- - - le Phenolise 305 Finish 7I252SM 4.0 - 5.5 mils 7I2500M 16.0 -17.0 mils C) Cure Schedule Primers (all systems): 17 days at 65-76'? (lS-24*C) and 27-90*. R.H.

Topccat (all systems): 10 days at 72-77'T (22-26*C) and 31-45". R.3.

D) Ersosure Texas Utilities Generating Company, Coimnanche Peak Steam Electric Station, FSAR Figures 6.2.1-1 and 6.2.1-2 4

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  • i LABORATORY TEST REPORT O'e "

May 9, 1978/Page 3 CCNFIDENTIAL

< l. Time / Temperature /?ressure Profile I

Time Temocrature Pressure Sorav Condition Initial sc 10 seconds 240*F (115'C) 44 psig Static 10 seconds to 15

  • s. 270*T (132*C) 58 ;sig . W.e 15 mins. to 1 hour1.157407e-5 days <br />2.777778e-4 hours <br />1.653439e-6 weeks <br />3.805e-7 months <br /> Dy-mmic 15 mins. 215'T (102*C) 34 psig 1 hour1.157407e-5 days <br />2.777778e-4 hours <br />1.653439e-6 weeks <br />3.805e-7 months <br /> 15 mins. to Dynamic 7 days 215-130*F 34-10 psig q ,

(102-51*C) t 4 Please refer to the recorder chart (L115-105) for exact conditions of j 1CCA profile. .

2. Spray Solution l

H,30 2000 ppa as Baron) in deieni:ed water.

p2 =38.(5.- 10.0 (NaOH added to adjust pH) i GRADING PRCCIDURI:

~:. . .

,.ff - ' The test coupons were evaluated for performance in the following areas:

1) Material flaking off
2) Del =*mtion between coats and/or peeling
3) 311stering of the topcoat
4) ^= m ,g of the coating
5) Excessive cracking i Grading procedures specified in Report K101.2 - 1972 of the A=erican j

National Standards Institute-Protective Coa-dngs for light Water Nuclear Reactor Containment Facilities:

4.5 Methods of Er=s ing and Evaluatine the Exoosed Test Soecinens The dynamic rad /or static elevated temperature-pressure and irradiation test panels shall be evaluated within 2 hours2.314815e-5 days <br />5.555556e-4 hours <br />3.306878e-6 weeks <br />7.61e-7 months <br /> and again after 2 weeks after removal from the test chamber for the following surface defects: flaking, delanisation and/or peeling, blistering, and chalking. Defects listed in

' Subsections 4.5.1 through 4.5.4 shall be dealt with as follows:

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"~ 4.5.1 naking. ASTM D772, Evaluating Degree of Resistance to naki:

(Scaling) of Exterior Paints, Part 21, American Society for Testing and Materials, Pniladelphia, Pa. 19103. nakiss shall not be per:sitted.

4.5.2 Delamination and/or Peeling. Delamination and/or peeling shall not be permittad.

4.5.3 Blisterina. Blistering shall be limited to a few, intact blisters, j Size No. 4, ASS D714, Standard Method of Ivaluati 3 Degree of Blistering <

- of Paints, Part 21, American Society for Testing and Materials, Philadelphia, Pa. 19103. The number and the size of blistars shall be recorded.

} 4.5.4 Chalking. ASS D659, Standard Method of Evaluating Degree of j Resistance to Chalking of Exterior Paints, Part 21, American Society for 1

Testing and Materials, Philadelphia, Pa. 19103.- Heavy chalki g shall i not be permitted.

j Any other changes in coating properties which are not also associated with I the separation, or the release, of coating from the substrate shall not be a cause for rejection.

l -

j ANSI N101.2 - 1972 Criteria l

'l (As interpreted by Carboline)

Maximus Degree of Failure Allowable 1 L

naking ASE D772 10 (None)

Delamination or Peeli=g None

  • Blisteri=g AS 2 D714-56 Blister Size Blister Densirv
  1. 2 None

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  • NOTI: A blister is g f4 Few intact when it has resul ed #6 Mediom in coating being separated #8 Medium-Dense from the test coupon.

i Chalking ASS D659 8 (I.ight)

NOTI: Haking, blistering and 4= Wag are' all evaluated accordi:g to ASS Standards, with a rating of 10 indicating that no failure was observed in the specific grading area.

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CONFIDENTIAL i li 1 Other -

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j Panel Identification Dry Film Delanina- ,,

tion or Blister- Performance Performance .

.: and Thickness .

Evaluation l Peeling ing Chalking Characteristics

} Coatina System (Hils) Flakint Blistering at .)

IA)4 None 10 bottom edge, Acceptable ,.,

Ic Ameron D-6 2.5/3.0 .10 None

  • both sides, Ic Phenoline 305 4.8 5.0 larger than '

Finish 7.3 8.0 #2F-BT-intact

! Blistering at 18 10 bottom edge, Unaccepta .e I- Ic Ameron D-6 2.3/2.4 10 None #2F-BT on ,

side 1 - both sides,

.i Ic Phenoline 305 6.2/5.4 intact larger than

  • Finish I'5/D #2F-BT-cracked L

Blistering at 2A)*

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' None None 10 bottom edge, Acceptable ic Hobil Zinc 7 2.7/2.6 10 both sides.  :

Ic Phenoline 305 5.3/5.4 larger than Finish 8.0/8.0 #2F-BT-intact j ,

t-Blistering at g

28) None 10 bottom edge, Acceptable

,j Ic Hobil Zinc 7 2.4/2.1 10 None  !,

both sides:

! Ic Phenotine 305 Jf6J 6

  1. 2H-BT.One #2 I Finish 9.0/9.0 at top edge, Side 1.

I, Acceptable Performance ANSI N101.2-1972, Section 4.5, 10 None #4F to #8 Light APanel suspended in the [

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  1. 8HD vapor phase

! As interpreted by Carholine LAH/T-127) k' V

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  • Hay 9, 1978/ Pas

- CONFIDENTIAT. .

L'elseina- Other

- ll Panel Identification Dry Film Blister- Performance Performance ,,,

' and Thickness Lion or .

Peeling ing Chalking Characteristics Evaluation Coating System (Hils) Flaking p

1.arger than Blistering at , ',

3A)* #2F-BT, Side 10 bottom edge: Unacceptable Ic Carbo Zinc 11 11.0/11.5 .10 None .

1; #6F, 4F- One larger /$' ,

Ic Phenoline 305 5.0/ 5.5 BT, Side 2 than #2-Bf-

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Finish

  • 16.0/17.0 Intact. One larger than -j*

'l #2-B aL top

  • edge, Side 2, Intact. 1,:,

A I.arger than Three hairline

38) #2F-BT, near 10 cracks 1/4-1/2" Unacceptable ./r, Ic Carbo Zinc 11 13.0/12.2 10 fee Blistering edges', Side 2 on upper edges- i'h Ic Phenoline 305 4.0/ 4.8 (peeled) coating intact.

Finish 17.0/17.0 -

- (1) Because blistering is limited to few-moderate, in. tact slisters occuring at '

i the edges only, panels IA, 2A and 28 are rated " Acceptable".

?

10 None #TF to #8HD #8 I.ight

  • Panel suspended in the  !.

Acceptable Performance vapor phase  ; j ANSI N101.2-1972, Section 4.5, .

As Interpreted by Carboline l.A D, 1277 l

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LABORATORY TEST REPORT

.. ( D May 9, 1978/Page 7 Ofj -

CONFICEE IAI.

DISCUSSICN OF RE M TS: Although panels lA, 2A and 23 do not meet the strict standards of ANSI N101.2, Section 4.5, Carboline interprets the standard as pertaNag primarily to the plane areas of a test coupon, and places limited significance en the discontinuous surfaces such as edges, channels, veld spatter, ate. Therefore,. the performance of these panels (IA, 2A, 23) having intact edge blisters, with 1

3 no other effects to the coating system or substrate, is rated

" Acceptable".

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f/ B 'Q0 i Alicia 5. Boldt Michael D. Tellor J Mentle l Acting Group Leader Supervisor Vice President

! Testi=g Department Research & Development Research & Development i

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l h Fitoill g __

)

o . ..

l! ,4 h .

O.

c 3

b o ..

s lis 3 i (t .i -

3 4 L ':

i o e o '

IIs 0 '

0 nc . - ':;

(L. ** ,

{- Q

. i n ,-

4 1, $1

- s.,

.  : 3

,3 ___

t.

! d'l.11l11_j l_(1.1111_l_Llllill l_l lllli 1 1 111111 llilllli 111111-

'l go e go. go' io n 10 8 to' 105 106 1

COMANCilE PEAK S.E.S.

TIME (sec)

FNAL SAFETY ANALYSIS f1EPOrlT UNITS J pnd 2 cot 4TAltittI247 PRESSURE I

' TRANSIEt4T - DEPSG FGilE 6.2.1-1 1 -

1 -

- 3 . - :- . t . .

g.7,,.,g 2 .,

.{ ..

1 .

e

' 4.'S

.y

.v O OAK RIDGE NATIONAL LABORATORY

~ & .....,.. .,

UNicN CARBIDE CcRPcRATicN NUCWR DIVis101 O

POST QPPICE 803 X

  1. CAK RIDGE. TEMNE$$EE $7CO September 28, 1978 f < Mr. Charles Wiegers Pcwer Industry Manager Car $ cline 350 Hanley Incustrial Ccur St. Louis, MO 63144 Cear Mr. Wiegers: -

As ycu requested, enclosed is me revised forma copy of

/? Carocline rescr: dated August li,1978.

Please call on us if we can be of additional help.

Sincerely yours,

/

b .'v

/, e L. T. Corbin, Secticn Head Analytical Chemistry Divisien LTC:c w i

Encicsures I

i .

l, . . .

~

        • -N9ee8"**g
  • l ** *'usP =M,.

, - u. :. - . --

,, 3. . ...y,,, ,

-2..-

if~

dbr.

1 OAK RIDGE N ATIONAL LABORATORY Orgmafgo av UNicN CAR 8tol CcR9cRATtcN NUCLUM CmsiCM 82, i p east arries sox x ou moca. rannassa srisa i

August 17, 1973 i

Mr. Dan W. McBride Nuclear Market Specialis:

Cartoline

' 350 Hanley Industrial Court St. Louis, MO 63144 Cear Mr. McBride:

Enclosed are One results of the irradiation, decantamination, and CBA tests you requested. The conditiens of the twc OSA

% tests were identical and are listed in Table 2.

If we can be of furtner assistance, please feel free to call on us.

Sincerely yours.

1

b. l-L. T. Corbin, Section Head Analytical Chemistry Divisien LIC:cnw 1

Enclosures f

d

^r g

'W o' - - - - -+ -, . - . . ...,

~

.W '

W****b6- ,u -

- - , - - - r 7--y , . - .- - ,e -ww y

- -  :,p.% 2q .- _. ,

- ,,.n , g

, t: ai -

a I

Carboline Analytical Chemistry Divisicn

. Manufacturer: Cak Ridge National Laboratcry St. Louis, M0 Date: -uc. 16, 1978 v

i Report of Irradiation, Decentamination,'and OSA Testing The irradiation, decentamination, and design basis accident (CSA) tests are conducted, respectively, in accordance with Sechtel Corp. Standard i

Specification Ccatings for Nuclear Pcwer Plants, spec. Nos. CP-951, CP-952, and CP-956 (or with modifications as noted in Table 2 CSA test conditions). .

The tests are designed also to meet tne specifications set in botn A.N.S.I. i re;crt N 101.2-1972, Prctective Coatings (Paints) for Lient Water Nuclear l

1 Reacter Centainment Facilities, and N 5.12-1974, Protective Ceatines (Paints) for tae-Nuclear Industry. The DBA test spray solutten and the test ecnditions 1

are listed in Tables 1 and 2. After both the DSA and the irradiation tests, the ccatings are examined for signs of chalking, blistering, cracking, peeling, delsmination, and flaking, accceding to ASTM standards wnere acclicable. All l

except tha decontamination test panels are returned to the coating manufac-1 turer.

  • The irradiation tests are run using a s;ent uel assemoly, receved fran the Hign Flux Isotcpe Reacter (HFIR) at ORML, as .ne scurce of radiatien.

l The l These fuel asseelies are stored under 20 feet of demineraliced water.

fuel is 935 enriched U235 as U30s ccmbined with aluminum. The spent fuel assemclies are removed after each 23-megawatt day ceriod. Irradiation is done using the garza energy from the accumulated mixed fission products.

' This scre readily simulates conditions arounc a reactor tnan dcas a cobalt source. Also, the higher gamma activity affords shcrter irradiation time i

to achieve accumulated deses. The dose rate (nur days after removal of a 4

fuel assecly frem the reacter is 1 x 10a rads /heur.

l i

i 1

The fuel asseoly is 20 inches high. A 20-foot long, 3-1/2-inch f

i diarcter pi;e, with one end capped, is used for the air irradiation tests.

The capped end is icwered into the four-inch opening of the center of the  !

! fuel ass eoly. The open end, ateve the water level, is ccvered witn an "0" l

i j ring sealed flange to which is attached a steel cable and an air outlet

  • hose. The air inlet is located at the bottem of tne pice. The test spect-mens are connected to tne bettem of the cable and icwered into the Evaluated

. 0l@b3 ,.

C.s t

A; proved D,/- ( y'7 r 6~

I 4

~ '"" ~

-y .- -

- x g. -rm.

, ,gg , m.

.....,.,q, .

l

j ._ . . .

! i I

}

. Manufacturer: Carboline Analytical Chemistry Division Cak Ridge National Laboratory St. Louis, M0 Auc. 16, 1978 Date:

i l i

radiation field. Also at the center of the fuel assembly is a stainless

j steel clad cadmium tube used as a neutron abscrber. This prevents contami-nation of the test specimens by induced radiation.

7 The decontamination procedure is as follcws: a mixture of fission

}

product nuclides (aged greater than 90 days and less than three years) is neutralized to pH 4 and innediately applied to the test specimens. The specimens are previcusly degreased in alcohol. Af ter the contaminated spc

! is air dried, the activities of four of the nuclides are measured by ccunting j dith a Tae(Li) detector and a multichannel pulse heignt analy:er. The speci-a 1

4 mens are tnen suspended in a beaker of water at 25'C and washed by stirring I '

for 10 minutes. The specimens are removed, the backs rinsed in water, air l

i ,

dried, and ccunted as abcve. The ratics of the activities before, to tacse after the decentamination are repor,ed as decontaminatien facters for water.

t I The decentamination and counting steps in 25*C and 80*C acids are repeated, i 1 .

f M and the respective decontamination factors calculated. The " total overall 0.F." is calculated as tne ratio of the total activity at the beinning of l

!  ! the test to the total activity at the completion of the three washing steps.

i 4 All activities are corrected for decay between counts. A computer has been programed to de all the calculations.

i e 1

I i i

f i i

l. l I

! t ,

i I

! O-M X4\W.4tG i  ; Evaluated .

l Approved ,/... 4D. -

e t //

- /. . Q ,

l m

'-- .~.r~.-.o-- . [. . . $[.__ _

=_ - - .-. . - -. . _

p :;.:. ,.;;- . ..

- ~ - ~ - - = . . . . . _

}

t' .

Manufacturer: Carecline Analytical Chemistry Division ,

I $ Cak Ridge National Laboratory l Auc. 16. 1978

's- St. Louis, M0 Date:

Cecentamination Test Results:

l I These tests perfer-ced according to ORNL Master Analytical Manual Metned No. 2 0920 and Bechtel Corp. Spec. CP-952.

CRNL Leg Scek No. A 7562; A7-17 T

' Decentamination Facter (CF) E'{C8"f0 g, ,

Sa=cle Water Acid Acid Activit{

, i Overall Removed Numcer Centaminant 325'C 925'C 380*C i

53-200 Ce-144 50 2.1 6.9 710 i 1.5 40 i (193LF/191HS) Ru-106 16 1.7 Cs-137 ->2300 >1.5 >l.2 >4100

~

Ir-95 17 7.8 7 .1 34 TOTAL 40 1.9 2.4 180 99.4 1

1

! 55-203 -Ce-144 82 3.8 4.2 1300 (CZ11/ES3hS) Ru-106 31 1.9 1.8 110 t ,.

? .

Cs-137 4200 >1.0 >1.5 >6400 4

Zr-95 14 2.7 7.4 51 TOTAL 57 2.7 2.0 300 99.7 j

! 204 Ce-144 660 1.9 1.0 1300 ,

i (CZil/305HS) Ru-106 18 3.3 3.6 210' Cs-137 >2000 >1.6 >l.0 >4800 Zr-95

~

7.1 2.3 7.4 ~ 23 TOTAL 61 2.7 1.7 230 99.6 i Ce-144 l Ru-lC6

, Cs-137 Ir-95

~

, i TOTAL f Ce-144

' Ru-106

- Cs-137 -

I Zr-95 '

l TOTAL -

IPercent of total activity removed = (1 - h) x 100.

I

-- t .

/

i Approved A,/, ce-D3 C g . g i

I i

g 4e .

  • *4" -B# N -. _ . ,

' ~'-

- app s y., _ . ..;, .

7_

9

. Manufacturer: Cartoline Analytical Chemistry Oivisicn

' t Oak Ricge National La cratory St. Louis. .M0 Cata
Auc. IS, 1973

~

i 1

Table 1. OCA solution composition, distilled water 0.23 M toric acid (3,C00 ppm bcron) 0.064 M, sodium tnicsulfate Adjusted to pH 9.5 with sodium hydroxide i

1 i

1 . .

Table 2. 08A test conditions

  • Time Temcerature (*F1 Pressure (csic) Comments i

f Sta rt 10 seconds 307 60 Steam injection.

f 2 hrs 47 min 307 60

! a.:

5 minutes 307-280 60-30 Injected cold spray.

J(

20 minutes 280-250 30 Adjusted pressure.

t 4 days 250 30 3 minutes 250-230 10 Crained; injected cold l

i spray.

i 15 minutes 230-200 10 Adjusted cressure.

l 3 days 200 10 End of tes:

i

  • These da*a are taken from recorder charts on permanent file at CENL.

i ORNL Log Ecct ac. A7562; A7-17-8 i

I Evaluated iC C Approved [

v

,.y c.-..~ .. . . _ _ .

..,3.g.p , 7, _

4y - - . , . ,

f d

Manufacturse: Cartoline Analytical Chemistry Division Oy2

  • St. Lcuis. v0 Cak Ridge National Laboratory Auc. 16, 1978 s Date:

i 1

System Identification: x Steel Panel Concreta S1cck CZil/191HB 1 Radiatien Tclerance Test Results:

' CRNL Master Analytical Manual Method No. 2 0921; Bechtel Cor;:. Scec. No. CP-951; 7

ORNL Log Ecck No. A 7562; A7 8 i

Initial Ocse Rate: 1.5 x 107 rads /hr

)

Test Concucted In: x air water 1 -

1 Cumulative Ocse Rate: Cen ents samele Nc. 1 X 10' rads 1 x 10' rads S1-1 Coatincs intact, no defects.

- sides A, B.

51-2 Ceatines intact, no defects,

' sides A, B.

j l  !- .

t i

1 1 l

' Additienal Cc : ents:

I  !

t .

l e',

, i Evaluated sd ACQroved

./ /m/ /b l TX l.901

. 4/78

4.q,. yye .:

'_~ -- .. , ;; . , .  ; .

._ " -[F _

. ,9 - ~ ' -:,

j .. . .. . . . . . . .

e i

't i

' Manufacturer:

Cartoline Analytical Chemistry Division

@'3 . ,

St. Leufs. M0 Cak Ridge National Lateratory Cate: A.c. 15. 1978 i

l System Identification: x Steel Panni concrete Stock 4

SP81/191HS Radiation Tolerance Test Results:

4 CRNL Master Analytical Manual Methec No. 2 0921; l

- Bechtel Cer;). Spec. No. CP-951; j CR.m. Leg Book No. A 7552; A7-17-8 i

Initial Cose Rate: 1.5 x 107 rads /hr I Test C:nducted In: x air water

\

t .

t

' Cumulative Ocse Rate: Cements f 1 x 10' reds

} Samole No. 1 % 10' radi

$2-23 Coatings intact, no defects,

- sides A, B.

$2-24 Ccatings intact, no defects, i sides A, B.

'I  %

i Additicnal Cements:

I i

k j r Evaluated AC W4 4 ,. Q Apcreved I /,/ Af,d A TX 4901 4/78 l

.~-~...v -.-. ..

e- --

n , q - , -

-,--.,r -a~~ ,,m-o m m,- ~ -- ww -,a, - e- .-~ .a

.9 ; .- - - q.. . , , , . a. .:. . . .. . . -

. 3 .- .- - . , ,. c am. - -

win. J ' _

< g. Manufacturer: Carboline Analytical Chemistry Division i

Cak Ridge National Lateratory 4

v St. Lcuis. YO Cate: Auc. 16, 1973 4

4 Svstem Identification: x Steel Panel Concrete Block 3

193LF/191HB I

Radiatien Tolerance Test Results:

._l CRNL Master Analytical Manual Method No. 2 0921; i Bechtel Corp. Scec. No. CF-951; i CRNL Leg Ecok No. A 7562; A7-17-8 1

Initial Ocse Rate: 1.5 x 107 rads /hr Test Conducted In: x air water i

I

  • Cur ulative Oose Rate: Cements I

p- Samole No. 1 X 10' rads 1 x 10' rads j .c ~,

t 53-43 Ccatines intact, no defects,

, N ,

r 2<

- sides A, S.

s

! 53-1/1 Coatines intact, no defects, sides A B.

! t 1

i j i

; Additional Ccrrents

s a t

'l 1

Evaluated -

Mba 1 a.ro,ed L w/. ~.n..p _., . -.. ,.f g--- .,,,ey_p.-,m9_

,  % - ,,p-.,,g.__7 -

.- -w - - .. -, y=..i ,, ,,.-- , -* .- - - . . . .

. .-. - - . ,~ ,.._- . . . . - _ _ _ -.

c m .- -- ,

.n - .7 . ,. e . , 3 . ., ..y..-

= -

i

}

i .

ct- Manufacturer: Carboline Analytical Cheraistry Division

~

St. Louis, M0 Oak Ridge National Lateratory s Cate: Aug. 16, 1972 System Identification: x Steel Panel Concrete Block CZ11/305HB i 'I l Radiation Tolerance Test Results:

g CRNL Master Analytical Manual Method No. 2 0921; l

  • 4 Bechtel Corp. S;ec. No. CP-951; CRNL Lcq Scek No. A 7562; A7-17-8
j

.i Initial Ocse Rate: 1.5 x 107 rads /hr i Test Conducted In: x air water i

i

}

Cumulative Cose Rate: Ccf=ents Samcle No. 1 X 10e rads 1x 10' rads57-122 Coatines intact, no defects, I

  • sides A, B.

4 t

4 57 123 Coatings intact, no defects.

l Sides A, B.

i 1

l

] Additienal Corrents:

I o

a Y N e a. b i Accrevec [ . / .

e TX 4901 l l 4/78 i

l ,,

.. .-. . . ._. . _ - - - . . . . . --. ..- - = _ _ . --

,o*- , , , ..g p., ,,

,,3 33 , .; . .. .. ,

+ -- -c._ ~ u. u 1

Manufacturer: Carboline Analytical Chemistry Division Oak Ridge National t,aboratory St. l.cu4 s. g Auc. 16. 1978

< Date:

System Identification: x Steel Concrete Stock CZ11/191HB

. 08A Test Results: -

ORNL Master Analytical Manual Method No. 2 0922; i CRNL Log Sock No. A 7562; A7-17-8 7

i Samole No! OBA Phase Cemen ts" S10-180A serav (GR) Coatinos intact, no defects, sides A. 9.

! S10-182A /sorav IGR) Coatines intact, no defects, sides A 9.

Y #

i i  :

i i

i i

  • teradiated. "(SA) = sand blast; (SH) = snot blast; (GR) = grit blast.

I 1

& ua e .

A Croved , [ # -

- . ~

.4'=.. . D-. g

  • *W -
  1. es v-- , ,,, ,

. - . . - - , , . , - , - . . - . , e ., , . - 7 , - -- . , - - - , - - , . . - - - - , - - - ,,, . _ , -

{' ' " _ '-  ;. y . .

.L : ; C; v. ,

A - ..-

' I Cartoline Analytical Chemistry Division Manufacturer: Cak Ridge National Lateratory St. Louis. v0 Date: Auc. 16, 19,s I

x Steel Concrete Block Svstem Identificatien:

4 C211/191HB

' CBA Test Results:

  • 5 CRNL Master Analytical Manual Method No. 2 0922; g

ORNL Log Sock No. A 75c2; A7-17-8 CSA Phase Cearents-* .

Samole No"

! S10-180A. scrav (GR) Coatinos intact, no defects, sides A, 9.

i S10-18AA scrav (GR) Coatines intact, no defects, sides A. 9.

L 4 .

)

b t

t I

I I J l

' Irradiated. "(SA) = sand blast; (SH) = snot blast; (GR) = grit blast.

l l 3

I I i

.cL._r t Accroved - , [ / _

Evaluated v . a g e

e-a ,

  • " w- , , , , ,,

s. v.@ Mv h e

, y., , , - .4 .

_ . . , , ,_ . -- r- --

ya q _ m----y _

w,,,_ _ g -r v--c -- -.-.---- .e -- ---- - - - -

3.,m . , ., . ., , ,

ciertseline

- :s l

O -. .

CSA AND RADIATION TCLERANCE

< 1 4

i ,

TEST PANEL PREPARATION CATA i

1. PRCCCCT TO 3E TESTED Carbo Zine 11/ Carbo Zine 11 (renair)/ Carbeline 191 H3 i'

$ SC'*1 SI I 2" x 5" x 1/S" 1

2. TTPE SUISTRATE I

orofile I -

3. SURTACE PREPARA!!CN (describe) Crichlasted to SSPC-SP10-63 vich a 1-3 zil blast 4
Damaged area: 3M " Strip & Clean" fo11 cued by light needle gun i= ace =ent f g -- ,3 i S10-lSOA; 510-lS4A t 4. PRCDUCT CATA: SAMPLE No.(s)

' y s . -

l 5. ATE AND TOTE COROiG CCMPCUND CR PRD'.EK APPLIED APPLICATION CONDIT!CNS HICCiESS TIME & OATE PRODUCT PRCOUC- CODES 3ATC4 # METMCD R/M(*Fi!R.M. (ins.) APPLIED _

l . COAT Carbo Zinc 11 7M21:3M Spray 75'/45: 190A) .0021/.0023 4-15-75

. -,-.2 le W 7t0980Z 184A) .00:4/.00:2 ic Carbo Zine 11 7M3123M 3 rush 72*/45: 180A) .0017 4-21-76 j

' . 7LO980: 184A) .0013 le Carbo 11se 191 EI 7E11821 Spray 78'l36: 180A) .0041/.0044 5-1-73 e,

7J2147M 184A) .0039/.0040 j

7:imer 66-78'T Primer 40-87T 73-78*F 'T REI.. HOtIDITY 33-56:

5. CTRING CONDIT!CNS: A*.35ENT TET Primer lo 7 DAYS

' MINIMUM CURE CRNL Master Analytical Manual Method No. 2 092 1

6. TEST PRCCCURE I

i t TESTING PI2?CRMED BY Analytical Chemistry DivisionDATE SU5MITTED 5-3-78 7.

f vaA uc.ge amna. acora: cry

' i m y

\ * /} / d TI}TREPORTNQIO1k-[4 i

e l

! TS- 06376-3 l _

bd' >e.8P 9 *T +M M un*

-s e-mw

,, s --m ,,-,---m--- c- --g ,-r ,-m ,--,,wr -,,--p- ,,,------g.ww-,,,y ev,m-,,wg--- pm,<,4-e rew,--,,,_,y v,,

  • " '1 -

. , _ e y ., ,

-.s .

I i'

i l

l

. teollne w

DBA AND RADIL* ION TOLIRANCZ TEST PANEI, PREPARATION DATA

1. PRODUCT TO BE TISTED Carboline 193 LP PM:ner/ Carboline 191 EE SIZE 2" x 4" x 1/4"
2. TTPE STBSTRATI Car:1fied ASTM A36 Steel f

j 3. SURPACE PRZPARATION (describe) SSPC-SP3-63 Pever Tool CIsan with N I

" Scrip n Clean" j

  • . ^

SAMPLZ NO.(s) 'S3-160; S3-163 7%

4 PRCDCCT DATA:

J

'1

3. DATE AND TIME CORING CCMPCUND C1 PRIMER APPI.IID ~ / -

APPI.ICATION CONDI!!ONS THICKNESS M & OATI PRODUCT PRODCC CODES 3ATCH d METHOD R/M('P MR.H. (ins.) APPLIED CCAT r ' ' ;- Carbcline 193 IJ 7E1949M Spray. 74*P/42*.53-160) .0026/.0026 3-10-78

-* Primer 7I.2868M S3-163) .0026/.002 Carboline 191 EB 7E1151M Spray 80*T/ S: 53-160) .0043/.0035 3-16-79 7J2147M S3-163) .0038/.0035 i

Primer 68-80*T Primer 24 J.

  • 73-7a 'P KII,. HUMIDIIT 4. _ u .
5. CTRI%. CONDI!!CNS: AMBIENT TEMP Primer 6 MINIMUM CORE 53 DAYS ORNL Master h=Weni wnm, = 1 v e + d ve. ? ^c "
6. TEST PROCEDCRE DATE STEMI*"ID t.g.?n
7. TESTING PERPCRMED BY Analvtical Chm 4etrv Diviston l Cak Ridge National I.aboratory du/

! RIP T h Sbl9

, S- 06376-3 T

, j -

i

  • r

. e

" ' ~ " w9 I

. .-,-w-- ., ..m. . , - - - - - - - , ,

1

- - . ,c; , . _._ _ ,,, _ _,

DEA TEST RESUL*S l

, 1 t

t i

f 4

0 l

i, s

4

+ ,

~

9.

! \

\'

i e

\

w 1 4 e

Test Report No.

I I

?

e t .

e 4

(

. . A k e .

J eAM q a p,

  • O@*De- m
  • * * * "# == == -g em . g,,e, ,

I

  • w.

4 4-M- 9p .

\

- - . . . . - ~ _ __ = - . _ . . . _ _ ,,,

1 .

1 Anal 'ical Chemistry Division

- - * , Manufacturer: Carb< 'ne Oak ...dge National Laboratory St. Louis, M0 Date: Auc. 16. 1973 Table 1. OSA solution composition, distilled water I 0.23 M boric acid (3,000' ppm boren) l 0.064 M sodium thiosulfate 3

Adjusted to pH 9.5 with sodium hydroxide

}

f 1

4 l1 i

  • Table 2. DBA test conditiens*

2 Pressure (esic) Coments Time Tercerature (*F) l i

4 Star

} 60 Staam injection.

10 seconds 307 j .

i 60 2 hrs 47 min 207 I

307-230 60-30 Injected cold spray.

- 5 minutes 280-250 30 Adjusted pressure.

20 minutes l 30 4 days 250 10 Orained; injected cold 3 minutes 250-230 spray.

230-200 10 Adjusted pressure.

l 15 minutes 200 10 3 days End of test

  • These data are taken fran reco-der charts on pennanent file at CPML.

i CTdL Log Sock No.' A7562; A7-17 8

}

Evaluated

@iO A.,roee/ t 22 /-r l () .

l , .

_ -pyy yy

"*WOtOO - ,

i

. - - - . - - .-. . . . . ~ . _ . . _

~~*-o-..i.,.-.- aa. l I 1

\

. 1 Carboiine Analythal Chemistry Division

Manufacturer: Oak Ridge National Laboratory '

St. Lcuis, M0 Cate: Aug. 16, 1978 System Identification: x Steel Concrete 31ock 193LF/191HB - Power tool clean CBA Test Results:

ORNL Master Analytical Manual Method No. 2 0922; .

- CRNL Log Book No. A 7562; A7-17-8 -

I 4

Comments **

' - Samole No. CSA Phase l S3-160 soray Ceatines intact, no defects, sides A, S.53-163 scray Coatings intact, no defects, sides A, 3.

a

?

I 1 1

l '

i

    • (SA) = sand blast; (SH) = shot biast; (GR) = grit clast.

' Irradiated.

s i < , .

(.

& Approved ,

Evaluated - - -

I

- e __ .

-- 1----'- . _. . _ _ _ _ , , _ _ . , . , , .

t a

1 1

1 .

DECONTAlfINATION TES'"

~' TEST PANEI. PREPARATION DATA l

1 j

i u

.i 1

l l.

1 k

- v. : ., .

1 i

i

" Test Report No.

1 4

1

?

't

' ~~-

~ -- E - * --

} . ....._

"-- -_____.m_

, ;~.'

.. c- ,

_ . _ . . - . . . . , . . . . . . _., .1. .e _ .s.

^ - ..

.? Waoe 3

? ubT .NU.

carbollrie '

1

< ~

j DECONTAMINATION TIST

~

SECHTEL CP-952 AND A.N.S.I. N-5.12

' /

J TEST PANEL PREPARATICN DATA 1

1; pgdDUCT TO BE TESTED _ Carboline 193 U Primer / Carboline 191 E3 nti SUBSTRA;E Cartified ASTM A36 Steel SIZE 2" x 4" x 1/4" 2;

Sandblasud to SS7C-5710-63 with a 1-3 mil blast

3. SURFACE IEEPARATION (dese:1be) profile _ '

SAMPLE NO. (s)53-200

' 4 .' PRODUCT DATA

CONDITICNS THICXNESS DATE PRCDUCT

  • APPLICATICN ME* HOD R/M(*Pl!R.H. ( in s . ) APPLIC COAT PRODUC"- CODES - 3ATCH i 7E1949M Spray 74*/427.53-200) 3-10-78 le Carbo 11== 193 2 .0032/.0033 Primer 71.2868H

.-g 7d181M Spray 80*/23: 33-200) 3-16-79 1c Carbo 11=e 1?! E3 7J2147M .0043/.0046 A

Primer 74-80 Primer 23-42

'T REL. EMIDITY 33-56  :

5. C; KING CONDITICNS: AM31LYr TEMP. 73-73 Primer 6 N CURE 53 days DAYS . .

f -

s ORNL Master Aastyrical Manual Method No. 2 0920

6. TEST PROCEOURE DATE SU3MIA.a 5- M 3
7. TES ING PERFORM BT i=alvtical Ch==# e rv Div.

1

  • Cak Ridge National Laboraccry
s. HJ
  • 0
  • /i

/) y TE.C REPCRT NO./SR-119 t

4 TS- 06376-1 ,

i

~

e -.

" **H' e e,. , n me , , _ ,

-- - - ,m

- - ! s ,- . 3*..". '. ... +..4, _

- - . . - . ~ . . ~a.--... . .... .. ... - - - - s~ ~ .- -- - - - ..-

0 l -. -

. I]

O e

UEMANON *TST REsta,73 es 1

4 i

g gb' 9

e n

t b

I l0 Tes: Report No.

1 0

l v I -

- O e w& .tm.a

+- # h.,.

>.aee * -M=e @ .*M,a%6.G _

3.. . :;p.7: -

, 1 5 * . - ~ - ~ - - . . .. _

Manufactursr: Carbeline i Analytical Chemistry Divisten Oak Ridge Natienal Laborator~v j .

  • Date Auc .16,1978 i St. L. s. MO
0 Decentaminatien Test Resu1*J:

These tasts performed according to ORNL Master Analytical Manual Method No. 2 0920 and Sechtel Corp. Spec. CP-952. ,

ORNL Log Book No. A 7562; A7-17-8-I Pe #

Decontamination Factor (CF) .

Simple .... Water Acid Acid Activity l

' Nu=ber ' Contaniinant 925'c 925'C 980*C Overall Rernevedl

.t S3-200 Ce-144 50 2.1 6.9 710 Ru-106 16 1.7 1.5 40 (193Lc/1911G) -

Cs-137 >2200 >1.5 >1.2 >4100 Ir-95 17 7.8 7.1 ~ 34 TOTAL ' 40 1.9 2.4 180 99.4 ..

i I.

I 1

e 1P ercent of tith 1 activity removed = (1 - h) x 100.

Approved A

~

- AO

'4 -

g.

4 t

? . . . . , , . . . . . -

..-.._.4..- - * ~ '

,, : - t.. .

I

-l -

l 9 .

j .. --

l

. # 9 5 #/f 4l NO 1 .

d ,

a

. g PHYSICAL PRCPER*II3 d

a I

i 1

4 4

.1 I

I i

I t

t i

Tes Repor !!c . C i G ^

J 1

a h

=* '

F 9

  • empp
  • " ' -"*W.'4=m @$-4 .,gg ,,,,,

1 I

1

[ - * ~ . . s _ -;.- c .*f ", . z _.-y.,5.;. . .:;:. . "

l . . ..

f _

i i _._

j di t.ar*D 5!!n o~.

  • PHYSICAL PRG?!RT:E5

- SECNTEL CP-9 54 .C3 A . 't. i . I . N-3.1 J 1. PRODUCT TESTED Carboline 193 LF/Carbolise 191 F.3

2. TYPE SU35TnTE 4"x4"xl/32" s' teel Taber Abrasar ?anel
3. SURFACE PREPARATION (describe). Surface roughanad with sandpaper.

~

SAMPLE NCS.

15A, 16A, 17A 4 PRODUC"' CATA: ,

CCNDITICSS THICKNESS CA;E RODUCT APPLICATION CCDES BATCH i METHOD t h1(

  • F) *R . H . ( i.:s . ) APPLIED _

4 CCAT P RODUC'"

1 1

Carboli=a 193 1.F 8E163221 Spray 73*F/26 15A) .CO33/.0035 12/16/7 J Ic 16A) .003'./.0033 12/16/7 8K240611 l 17A) .0036/.0033 12/16/*

1 ic Carboline 191 E3 8K22S6:1 Spray 73*F/272 13A) .0040/.0011 12/26/7 I

SJ182811 16A) .0041/.0041 12/26/7

  • 17A) .0041/.0040 12/06/7 I -\_ 5. C'JRINO OATA:e
  • Crag TI,3g 4; j,y, AP.3IENT TE!P. cs _7es e *? REL. HCf. 9 7.s c e
6. TEST P=.0CEDURE: Bec ht el St andard CP 0 5!. and A.':. S . I . N-5.12 j
7. TEST RESULTS:

7.1 ABRASICN

Federal Test :14thod Standard 111 Test Metnod 6192. -

1000 cycles with it CS-17 vneel at:d . ICCO gram load.

l tE$ ~ 36.6 =g. MICH - 38.3 =g. AVERACE - 3 7.1. =g .

i T.2 A0llESICN: determined by une'of the ELCMETER ACHISION TISTIR j

1

' psi f

AVERACE OF 5 TISTS 8

. DESCRISL FAILCRE ,

7.3  ! REC *-Df?aCT RESISTANCE:

  • Curing Da:a - First Coa::

72-61*? 2 -6C: R.H. la d:ys

- , (-

A:;fJVed: ,

b2 ;i

( ~

5- CG6-i p , y

, J .

+

i i .-

[

I ,

F9 T @ M g .e-e, ge m gs. .,g g y y g p 9*'*a= ham. e _g O *OO-*MM 9

l l

l

o. -~.~,,-  ::rm  :.> .z. 7- _ - 5 3.g..
7. , _ ,

-a.. -

i l

,, 3 3 PHYSICAL PROPr.RTIES RECHTEL CP-954 AND A.N.S.I. N-5.12

1. PRCOUCT TES E3 C'arboline 193 LF/Carbolina 191 H3 1
2. Cartif tad ASTM A36 - 2"x4"x1/4" steel panel 77?I.SU3sT3 ATE
3. SURFACE I' REPARATION (describe). Crichlasted to S$7C-SP10-63 with a 1.0-2.0 =11

- blast prof J.e.

4 PRCCUCT OATA: SAMPLE ':05, 133, 163, 173, ISS, 193 i e APPLICATION CONDITIONS THICKNESS OATE k'RODUCT BATCH ! M m.0D R/M(*FMR.H. fins.) APPLIED COAT P RCDUCT CODES A /16.

Carco11:a 193 LF SH165:21 - Spray Iri/264 133/ .V0J9/.0VJo ic

- SK2406M 163) .0038/.0039 12/16.

173) .0038/.0039 12/16.

133) .0038/.0038 12/16, 19 3) .0038/.0039 12/16; i

i ic carboline 191 H3 SK2236M Spray 73*F/27:ll 133) .0048/.0047 12/26.

SJ182SM 163) .0040/.0040 12/26.

173) .0051/.0043 12/26.

I e 183) .0048/.0049 12/26, 193) .0035/.0048 12/26.

1 t ...,

l 1 5. CURING DATA:*

22-60*. - ctaI ;t3E 52 days AM3IC;T TE:7. 61-79'T *F REL. act.

> , ~

I'

6. TEST PRCCIOURE: Bechtel Standard CP-954 and A.N.S.I. % 5.12
7. TEST RESULTS: t.

7.1 A37.AS IcN: Feders! Test :techod Standard 141 Test Method 6192, i

i 1000 cycles with a. C5-17 wheel and a 1000 gram load, s

i .

H1CH - AVERACE -

, i LCb -

i l *7.2 A0f tESIC':: Deter =ined by une of the E1COMETER A0HESION TESTER I

f 630 p.g

! AVERACE OF 5 TESTS I ,

i DESCRIZE FAIJJag Cohesien of Carbo 11:a 193 LF i .

7.3 ~;1 REC-;" PAC REs!STA!:CC:

  • Taria("Taca - frs f"Coac:

' 2 64-81*T 56 10 days i

l

! ^

I

, t G

j Approved: ,_

j m/.\

/% t_

l V .TS- C6376-4 )

m l

- - - +-- 4 . _ , , _ _ . _ . _ _ _ _ . ,,

LU s . < :f 4 . ' .L~ D

~

.? . " . _': . ;~; . : . ..

J

i. .

PHYSICAL PROPF.RTIES q ,

I -

> 3ECHTEL CP-954 AND A.N.S.I. N-5.12 I

1. PROCCCT TESTED Carbolice 193 LF/ Carboline 191 E3 1
2. TYPE .SU3 STRATE Car-ified AS'IM A36 - 2"x4"x1/4" steel panel

. 3. SURTACE PREPARATICN (describe) Sandblasted to SSPC-SPIC-63 wi h a 1.0-2.0 mil blas:

profile, y 15P, ISP, 17P, ISP, 19P q 4 PRCOUC DATA: SA*.PLE NcS.

APPLICATION CONDITICNS THICKNESS CATE

)RCCUCT CCAT PRODUCT COOES 3ATCH # M E*HCD R/M(*F):2.H. fins.) APPLIED 1 1c carne 1A=a 193 tr Sa16aza spray 73 r/267. 15P) .c02s/.c037 12/16/7 i 8E2406M 16P) .0039/.0036 12/16/7 17P) .0039/.0038 12/16/7 ISP) .0037/.0038 12/16/7 19P) .0037/.0038 12/16/7 q .

ic Carboline 191 E3 SK2236M Spray 73*F/27 15P) .0040/.0042 12/26/"

. 8J132EH 16P) .0043/.0043 12/26/7 17?) .C044/.0041 12/26/7

    • 187) .0041/.0042 12/26/7 197) .0041/.0C42 12/26/7

~.

7c. ,' 5. C*.72tNC cATA:,

A '.3IENT TE:'.P . 61-79'? *7 REL. HUM. 12-60 CURE !!ME 52 davs

6. TEST PRCCIOURE: Sechtel Standard CP-954 and A.N.S.I. N-5.12 9
7. TEST RESULTS:

4 1

7.1 A 3 RAS ION: Federal Test Method Standard 141 Tes: Method 6192, l

1000 cycles with a CS-17 wheel and a 1000 gram load.

I' g- HTCH - AVERACE -

  • 7.2 A0HE51CN: Deter 3!ned by use of the ELCCHETIR A HESIO 4 TESTER 665 pst AVERACC 0F 5 7ESTS

. DESCRISE TA* *_7RE Cohesien of Csrboline 193 LT

,3 OIREC -I'*? C ?IsISTA!:CE:

l

  • Caring Oz:a - Firs: Coat:

64-81*7 $6-77: R.E. 10 days e

Approved: ,_ uMr

.I3- C63764 l t

i . O

.4 . - . . . . . _- . . . , _ _~ _ ,, _

. . ' - - -%.- ' 9 i';:_ ; .. ':.g.:. ; ,; & , ._._ p' :

.O; , 7. . :.. . .:. . , -

t PHYSICAL PRCP".RTIES O _.

BEch7ET. CP-954 A:.*D A.M. S . I . N-5.12

1. P'.00CCT TISTC Carboline 193 LF/ Carboline 191 H3 1
2. TYPE SU3 STRATI Cart.ified ASTM A36 - 2"x4"x1/4" s:eci panel
3. SURfACI PRI?ARATICN (describe). Shochlasted to SS?C-S?10-63 wi:h a 1.0-2.0 11

- blast pro:u e.

SA.MPLE NCS. 15Q , 16Q , 17Q , ISQ , 19Q 4 PRCCUC"' CATA: ,

APPLICATICN CCNDIT!0NS THICKNISS OATI hRCDUCT CODES BATCH # METECD R ht (

  • F ):R . W . (ins.) APPLID COAT PRCOUCT 15w .wa,,.002 ..,.6/7 is Carboline 193 LF shlosz.'s spray W ii .h

- sc406M 160) .0039/.0034 12/16/7

!' 17Q) .0035/.0036 12/16/7 13Q) .0036/.0035 12/:.6 /7 4 -

ISQ) .0038/.0033 12/16/

le Carboline 191 E3 8C236M Spray 73*F[27% 15Q) .0046/.0041 12/26/7 SJ182SM 16Q) .0041/.0042 12/26/7 17Q) .0042/.0040. 12/26/7

- 18Q) .0044/.0041 12/26/7 1

3 19Q) .0047/.0044 12/26/7 t .

5. CURING DATA:
  • F REL. HL?i. 22-60% CURE TIMI $2 days AMBIENT TI:iP. 61-79*7
6. TEST PRCCDURE: Bechtel Standard CP-954 and A.':.S.I. % 5.12 t

l 7. TT.ST RESUL*S :

I 4 7.1 A ER.AS ICN: Federal Test :4ethod Scandard 141 Teve Me: hod 6192, 1000 cycles with a CS-17 wheel and a 1000 gram load.

LC' * - HICH - AVERACI -

  • 7.2 ACMESICN: Determined by use of. the ELCCttETER AOHESION TISTIR AVI.UCC i1F 5 TESTS 670 psi

. DESCRISE TAILURE Cohesien of Carbcline 193 LT 7.3 O!RIcT-!MPAC RESTSTANCEh

= Caring Oa:a - Firs: Coac:

64-81*F $6-772 K.E. 10 days .

i> A; proved:  % Ih/ y\ u ,6

/ .TS- 06376-4 p 1

~

e l

- . . . . . m

" * * * " * ' * * - * , , , , _ , _ . , , ~- ~ - . - - . . . _ .

l 1

1 J

- _ _ _ . _. _. - - _ . . =_ _- -_-.- __ - . ..

~ '

, g ,- # .

_,. a..

^ ~ . -?~L.

_, -e .# .- - - - _ . -.-

~

i 1 1 . - . . - - . - -

s ,,

i 4

d' ,"- PHYSICAL PROF UTIES j  ; 6-I

) - SECMTEL CP-954 A::D A.N.S.I. N-5.12 I

1. PRCOUC; TESTED Carbo 11na 193 II/Carbolise 191 E3
2. TTPE SUBSTRATE Schedula' 40 pipe ,16" lens , 2.375" 0.D.
3. SURTACE PREPARATICN (describe). Critblasted to SSPC-SP10-63 with a 1.0-2.0 mil oAas: pro:ne. .
4. PRCDUC* OA*A: SAMPLE **05. 15C,16C.17C. ISC,19C, 20C. 21C l RCDUCT APPLICATION CCNDITIONS THICKNESS DATI I

3ATCH # METHOD R/M(*F):R.H. (ins.) APPLIED i CCAT PRCDUCT CODES

'c Carboline 193 LI 831682x Spray W F/ W C) .004 0/.00D 22/16/7 sx2406x 16C) .c040/.0038 12/16/7 i

17C) .0039/.0036 12/16/7 i i 18C) .c040/.0035 12/16/7 j

j 19C) .0036/.0032 12/16/7 l , -

2CC) .0040/.0034 12/16/7 1

210) .0039/.0036 12/16/7 l ,

< ic Carbo 11=a 191 H3 8K2286M Spray 73*T/272 15C) .0055/.00$0 12/26/7 SJ182SM

~~

16C) .0050/.0045 12/26/7 17C) .0046/.0056 12/26/7

c' , 1sc) .c042/.c045 12/26/-

5 .- CURINC DATA:, 19C) .0052/.0058 12/26/~

. CugI" :qL,g *c8E,, ' 883 Q"'F~if* u ~

AM3ICIT TEMP. 61-79'T 'T REL., HUM.24-602  :

4 D Coat 81*F 28-492 36 days and A..f.S.I. N-3.12

6. *^i"t*NOC1 Tf. a - Firs:Beencel Scandard CP-954 3GRE:

1 i

j 7. *IST RESUt.TS:

i  :

Federal Test Method Standard 141 Test Method 6192, ,

j 7.1 ASRASICN:

1000 cycles with a CS-17 wheel and a 1000 gram load.

I i

I - HICH - AV! PACE -

_LCt

) Determined by use of the II.CCMETER A2HISICN TESTER i , 7.2 ADHESIC5:

l asi 4

AVERACC CF 5 TESTS

. DESCRISI TAILURE I

7.3 DIREC*-IMPACT RESTSTA?:CE: if31/79 Fine Nu=ber Effec: of 100 usi i=:se:

15C No Effect 16C 3/S" dela=isa ion pa1=: sepa:a:ed fro = pipe 17C No Ef fec: .

18C .No Effec:

19C 1/4" dela=ina:Los pais: separa:ed f::= pipe i

20C No Effec:

i 21C 1/4" dela=ina:1on pa1= sepa:a:ed f::= pipe b

'

  • RISULTS REVII*ED ST ,. as u .

'{ j) vf I, t

. . 0

! .-- - . . . . . . . . - _ , , , , , + . .. _

i

gi i --- - _ . . _

g g , ,y eb g g O * *4 * @ $ .

d. . . . .;.

S O

E PAYE!,PREPARATIO.V AND INDIVIDUAI, CHD11CAI, RESISTAVCE TEST RESI.T.*S 9

6 i

e S

e e

  • 4 e

e 4

4

  • e l

C 1

O 6

0 0

Tes Report No.

r

' '"* 6 M *

"U Pe'*Me d.i#we69,.. a.4W p g h# **.de FMe gapp

- _. -- ~ _ _ _ . _ - _- - - .. . _ .. .

, ~- ... .; ,.. .,,o , ,, _. ,

.w

  1. 2.,.. -. . . .

. ,g g.g y.g,,,3

,-- r. e *A..

4

. ~ . . . . . . .. .,

,? .

3 TIST NO. 01720 i l ,

  • CHIh CAL RISISTA!!CI TIST RISULid

<- SICHTIL CP-953 and A.N.S.I. N-5.12 TYPI SUBSTRATI: SI I 2"x4"xb'CONCRITI S'"IIL%$*M A36 CTHIR l.

1 1. SURFACI PREPARATICN (describe) : Crichlasted to 55PC-5710-63 with a 1.0-2.0 i mil blas: profile SAMPLI NO.:' 15E

3. PRCDUCT TESTID: Carbolihe 193 LT/

Carboline 191 H3 i

  • HICKNISS DATI l 0 APPLICATICN CCNDITICNS i j ,

. PRCDUCT CCDIS DATCH 4 MITHCD R/M ( *?) tR.H. (ins.) APPLII CCAT PROCUCT l

$H168:M' Spray 73*T/26: .0C38/.0037 12/16 '

le Carboline 193 LF 8K2406M

! j i i d

t .

3X:286M Spray 7 3* i/ 27'l; .0043/.0041 12-26 '

4 le Carbcline 191 H3

  • SJ1828M J

] '

3 s

4. CURING CCMDITICMS:

% RIL. HUMIDITY I,INGTH OF CU'JI  ;

i

  • AM3! INT TIMP. (*F) 25-49: 10 dcys j iST coa: 72'F-81* F 24-60: 6 wee'n 2ND coat 61*7,-79'T 1 5. '"YPE Cr TIST r CHIMICAL IXPCSURI TIST PER SICHTIL CP-953 and A.N.S.I. N-5-12 I

I 5' *y i 6. TIST TIMPIRA*URI: AME! INT 75' O 5* 'T SCL"TICN 75' 5* Ni:ric Acid (;h =0.25)

- 7. CHIMICAL SCLU*ICN (pH and Concentration)r

  • IST CBSIRVATIONS: DA*I STAR *ID 2-5-79 g

8.

t T

ACCIPTANCI CHIMICAL EXPCSCRI P2SC2,TS s

1

,' CRI*IRIA 1 CAY l 2 CAYS l 3 OAYS l 4 OAYS l 5 :AYS

' NI l NI l NI

! 8.1TLAXING/PIILINGl NI l NE l NZ l NZ 8.2 CIL;_MINATI6N l lZ  ::I l NZ l

C 8.3 3LISTERING l :E l1f6EinLPl NC l lhIN. [.*^.',J l la ::I NI NE NI

! 8.4 CTHIR ITTICTS l NE l 4 -

l i '

NI- No Iffe:: NC= No Change E*,*IU,**.I

  • _'N..'" "# * # U 3Y G .O.v; r/ j-l $= 311sters

' . LP= Liquid phasa /

T= Tew p/

E= rdge a TIST FIPCF.T NO.

.. ..' L .. c . c o;,, , , , , ,

~ ' ~ ' * ~ ~ *

~--

..-...y 7-. . . . . , , , , ,

~ ** f a+ . e: ,.

I

, _ _ . ~ - _ . ___.. _ . - . _ __. _ . _ ., _ . _ _ . _ _ _ . _ . . . - . . . _ . - . . _ _ - . - _ , . _ _ . _ - , _ . . _ _ .

. . - . _ _ . -. = _ _ - _ - , . ,

' - - . , . , n . . ._.,gy z. _. , . ,, ,, _

Q* *

  • f7 y *i'i _  ; ::_ . -c .. - -

. = . . . - _ . . . .

t t

TE.fi ..o. 0177.

- - CHI *AL RISIST)lICI TEST RISUI 4

BICHTIL CP-953 and A.N.S.I. N-5.12 SIZE 2"xc%"CCNCRITI STIILASTM A36 CTHI"4 E. TYPE SU3 STRATE:

i Cri:biss: :o SS?c-3710-63 with a 1.0-2.'0

2. SURFACI PRIPARATION (describe) :

mil blast profile

  • \

J 1

PRODUCT TESTID: Carboline 193 LF/ SAMP!I NC.**

3.

J Carboline 191 EB 1

1 PRODUCT APPLICATICN CCNOITICNS THICXMISS ::ATI APPLII CCDIS 2ATCH I METHCD R/M(*?)%R.H. (ins.)

CCAT PRCDUCT

. 0033/.0033 12 ,

8H1682M Spray 73*T/26:

Ic carboline 193 L7

  • 8K2406M i

1 73*7/27: 0050/.0048 12 191 R3 SK2256M Spray .

1e Carboline l 8J132SM .

r i

.i 4.' CURING CCNDITICNS:

AM3IINT "!MP. (*T)  % REL. HUMIDITY I.INGTM C** CU'AI i

25-49: 10 days IST coac 72*-81*F 6 weeles 220 coac 61*-79*T 24-60:

1 t

5. YPE Cr "IST:

j CE.".! CAL IXPOSURE TEST PER BICHTIL +

CP-9 5 3 and A.N.S. I. N-5-12 -

~

SCLU"'ICN I5*

  • 3 *-

TIST TriPI?JsTURI AF.BII T 75* $*

  • F 6.

4 5: Selfuri Acid (ph= C.8)

I 7. CMIMICAL SCLU"'ICN (;E and Concentra:icn):

i 2-5-79

8. TEST CBSIRVATICNS: DATI STARTID l

I f '

ACCIPTANCI CHIM! CAL EXPCSURI RISU2.TS

~

~

j $ '

CRITIRIA 1 CAY l 2 CAYS l 3 CAYS l4 ::AYS l 3 OAYS

  • NE NE NE 8.1 T!. AXING /PIILING NI I l F- U NI E E l l f E.2 CILAMINATICN l ... I nf 3 cn I p ar.5 en i y*
8. 3 3LIS~IRI'*G 1

l h.a 1

  • I t . LP Ifa:e in 1? l U U l_

E NE l l . .

S.4 CTEIR ITTICTS NI= No E8 fee: ':C= N.: Chang

  • E= ,r.dg e RESULTS F2VII4ID BY Nb[

i = Few LP= Liquid Phase B= 311s:er  ;;37 7;pog; go, f)

- 7/ hY i i e

, "- '*aAt,- - . . . . . . . . .

i 4 * * . .

. y .. u

..,x..__. _-- ' - - . . . . . ,__ _

i r ir y- a erwr 4: e * + - + a- M- esw

  • g- ew**y-T--sr- w - y *1- -e m *-w w mus -- M =-

. yy . .,m. y ,

. ,,*-s., ",o , . ' , . , .

-~..-.. -

..m. .w - ~ ~

t . . . . - - . . . . . _

4 t 4 ...

TIST NO. 01720 Ch*IMICAL RISISTANCI TIST RISULTS O

j BICHTIL C?-9 5 3 and A.N. S . I . N-5.12

1. TYPE SUBSTRATI: SI: 2"xt."x1/4dCNCRITI
r. STIIL AS" us" CTHIR 4

SURFACE PRIPARATICN (describe)  : Cri: blastedproma. to SSPC-SP10-63 vich a 1.0-2.0 1

~

[ 2.

  • aL.L DJ.ase 13G Carbolina 193 LF/ SAMPLE NC . *
3. 'PRCDUC" TIS *ID: Carboli=a 191 H3 i '

P RODUC'" APPLICATION CCNDITICNS THICICIISS OATI

, i .

METHCD R/M ( *?) %R .H . (ins.) APPLIII CCAT' PRCDUCT CCDES 3ATCH i 1

SE168 E Spray 73*i/25 .0038/.0039 12/15/

ic carboline 193 LF

  • 8K2406M

{

8K2286M Spray 73*T/27 .0043/.C041 12/25/*

ic Carbo 11:a 191 H3

' 8J1828M i

4. CURING CCMDITICUS:

A.w3II'C TIMP . (* T)  % RIL. HUMIDITY LINCTH Or CU2I 282-48: 10 days 1st coat: 72*F-81*F 6 weeks 2nd coat: 61*F-79'T 24 -60:

5. "YPI Cr TIST:

9 N ICAL EXPCSURI TIST PIR 3ECH*IL CP-953 and A.N.S.I. N-5-12 AMBII C 75* + 5' 'T SCLUTICN 75* 5' ey

6. *IST "I24PEPATURI

1

,' 7. CHIMIC.C,SCLOTICN (pH and Concentration) : 5: Eydra:1:a (;E = 10.75)

DATE STAR"'ID 2/5/79

8. TIST CESIRVATICNS:

f 4

ACCIPTA!!CI CHI.v.:CA:. IXPCSORI ?.ISULTS i

l 4 CAYS lSI OAYS j CRITIRIA 1 hY' l 2 CAYS l 3 CAYS l h'E 8.1 TIARING/PIILI:G NE l NE l NE l l NE f i

l N7. l NE l S.2 CII.AJC::ATICN l NI l NE l NE NE 8.3 ELIS IRING l NE i NE l NI l NE l f l

NI NE NI l NE f _ NI -

8.4 CTHIR ITTICTS i i

,, S U. ..S r :. .. . ia s ,, 3y .

\_[a/ ./l/,., o l NE = No Effect () ' ')

' G t .

  • TIST REPCST NC. -

- -.. _ ,-.; _ ; . . - .. n . . . . ..

I

_ _ . . _ _ . . . _ _ . . . , . . - . . . . - .- . , . . . _ . _ . . _ . . . . . . _ , . _ _ _ . - . . _ . . _ _ _ _ . _ _ _ . - ~.. _ _ _ , _ . . . . - . . . ~ _ . . _.

- i."<+- - . z,q,y,y. ..,,,, _,

-+ *-. ,. . . , ,

--' 1rci.2 - - -

i - . .

4 4

b v6*6w TL.4r du.

r

  • CHE CAL RESISTANCE TEST'FISUI BECHTEL CP-953 and A.N.S.I. N-5.12 U SIIII"::4"xh"CCNCRETI STIII/sSTM A36 CTHEM
l. TYPI SUBSTRATI:
2. SURFACE PREPARATICN (describe) : Cri:blas: :o SS?C-S?lo-63 vi:n a 1.0-2.0 '

l all blas: profile SAMPLE NC.:* 15R 3.- PRCDUCT TESTED: Carboline 193 LF/

Carboline 191 K5

  • ' APPLICATICN CCNDITIONS THIC.<NES S DATE

. PRCDUCT APPLII 3ATCH i ME'"HCD R/M ( * ?) 1h R . R . (ins.)

CCAT PRCOUCT CCDIS Spray 73*T/26 .CO37/.0033 12-16 ~

le Carbo 11ne 193 LF 8H1682M 8K2406M 191 E3 8K2236M ' Spray 73*F/27* .0C45/.0040 12-26-:

Ic Carholine 8J182SM .

4.- CURING CCUDITICMS :

.. L .

4 AMBIENT TEMP. (*F)  % RIL. HU M DITY LENGTH Cs' CTRE 28-49I 10 days IST coat 71*-81*T 6 weeks 2ND coa: 61*-79*7 24-60 S. TYPE CF TEST:

CHIMICAL EXPCSUP2 TIST PER SICHTEL CP-953 and A.N.S.I. N-5-12

~

6. TEST *EMPERATCPI: AMBIINT 75*
  • 5' *F SCLU'"!CN 75*
  • 5' 'T
7. CHEMICAL SCLU"ICN (pH and Concentra:icn): SI Sedi'= Hyd::xide (ph=11.75)

TEST CBSIRVATICNS: DATE STARTID 2-5-79 8.

ACCIPTANCI CHE.CCAL EXPCSUF2 ?250L;S i CRITIRIA 1 CAY l 2 CAYS l 3 CAYS l 4 ::AYS l 5 *:AYS ,

8.1 TLAXING/PEII,ING l NE l NZ l NI l NE NE l I

NE l NE l NE l NI 8.2 DELAMINATION l NE w l

vat 3 On &

NO .%  !

8.3 ELISTERING l NE 1#2-6h :n E,k NO l l NE NI l NI l NI l

8. 4 CTH
:R ErrIC-S :I <

NE= No Effec: 5= 311 ster g.7 9...gzc *,y* A/ (g 3 * ~~ "a**

NC= No Change EA= 3ack E= Edge T= Tev ,,S

.- . P2P C ,. .... ~ .

{},_' f) ')

- - ~ - - - - - - - . - . - . . , . , . ,,.. : C *'-~~. -- ..,

.x. qwo,. z . .;. , ;;

} "_- - .

. L_.-

a-

. . . .. . 2.u

~ .--.

l i

J TEST NO. 01720 i

CHIMACAL RISISTANCI TIST RISULTs

-4

. BECHTIL CP-953 and A.M.S.I. N-5.12

1. WPI SU3 STRATI: SI*I 2"x4"x1/dbsCRITI STEIL @ CTHI'4 l 2. SUP. FACI PRIPARATION (describe) Get: blasted to SS?C-SP10-63 wi:h a 1.0-2.0 f a1.L blast profala.

SAMPLI NC.:

13-1

3. ' PRODUCT TISTID: Carbolins 193 LF/'

i Carbolina 191 EB i

e

. PRCDUCT APPLICATICN CCNDITICNS THICXNISS CATI i

CCCES EATCH i MITHCD R/M (

  • F) )R . H . (ins.) APPLII:

j a CCAT PRODUCT ~

e 1

8H168:M Spray 73*F/267. .0033/.0035 12/16/

! Ic Carbolina 193 LF 812406M i k 12/26/7 carbo 11ne 191 HB 8K2236M Spray 73*F/27 .0042/.0041 ic

! } -

8J1828K 1

t

i. ,,-

l t

1

4. ' CURINO CCNDITIONS:

i ..

AMBIINT TEMP. (*?)  % REL. !!UMIDITY LINGTH Of CU LI I

72*-81*F 28-49E 10 days I lac coat:

l 2nd coat: 61*-79'T 24-60% 6 vaaks i

I. 5. TY7I CF TEST:

i

} CHIMICAL IXPCSURE TIST PER BECHTIL CP-953 and A.N.S.I. N-5-12

- 6. TIST TEMPERATURI: AliBIINT ' 75*

  • 5' 'T SCLUTICN, 75* - 3' *F CHIMICAL SCLU'"ICN (pn and COncent-ation) : 5: A=meniu:n Evdr=xide (;E = 11.6)

! 7.

! 8. *IST CBSIRVATICNS: CATI STARTID 2/5/79 i

i i

l C1!IMICAL EXPCS;RI RISULTS i ACCIPTANCI i

i CRITERIA 1 CAY l 2 CAYS l 3 DAYS l 4 CAYS l 5 OAYS l 3.1 FIAXING/PIILI::G l NE l NE l NE l NE l NE l f ' NE 9.2 CILAMINATICN l NE l NE NE l NE l l NE

,  !, 8.3 ELISTERING l NE NE l NE l NE l NE NE 8.4 CTHIA IFFECTS NE NI NE f f f S 8 W . _

' yV

, n T RIPo r NC. V  :

i . .. .

l. ------ - . - . . . , . . - _ , _ _ _ _

4

, . , . , _ . - , . . ...--.....,.,,--e.,..._..--.,..,__.-w..m-y-, --..,m,.-., ,

,. ,e.. - . . ~ ,y .. .v. , -_m ~3 , . - ~ . - . . .

,,w ..

q.py _ ,,

J

. J -- . -. . . - . .

a

~

~

~

TIST No. 01/20 CH'. ICAL RISISTANCI TEST RISU. .i BICHn L CP-9S3 and A.N.S.I. N-5.12 SI*.II"x4"x5"CCNCRITI STIIIASTM A36 CTHIM

l. TYPI SU3 STRATI:

i 2. SURTACI P E?ARATICN (describe) : Cri:blas: :o SSPC-5710-63 vi:h a 1.0-2.0

. mil blast profile SAMPLI NC.** 15J 3 .* PRODUCT TISTID: Carboline 193LF/

1 . Carbolina 19185 1 DATI e

e APPLICATICN CONDITICNS THICKNISS

P RODUC"' AP P LI-j CCCES 2ATCH # MITHCD R/M (
  • T) ) R . H . (ins.)

. CCAT PRCCUCT J

' 193 LF 8H1682M Spray 73*T/26: .0037/.0038 12 ic Carboline -

  • 8K2406M i0 t

i 8K2286M 5 pray 73*F/27: .0043/.0043 12  ; l' Ic Carboline 191 F.3 t,

8J182SX .

f .

I 1 4 ,.

,j.. 4 .- CURING CONDITIONS:

j IW.BIINT TEMP. (*T)  % RIL. HUMIOITY LINGTH CF CU2I i

28-49: 10 days 1ST coac 72*-81*7 6 weeks

2ND coat 61"-79'T 24-40:

4

S. "'t?I CT TISTs CHIMICAL IXPCSURI TIST PER' SICHTIL CP-953 and A.N.S.I. N-5-12 i I 5* *T AMEIINT 75* I $* 'T SCLC"!CN 75*
6. TEST TEMPIRATURI:
7. CH" -.ICAL SCLC"'ICN (pH and Concentration) : $! Sodium scrate (ph= 9.7)

J } 2-5-79

8. -IST C=SIRvATICNS: DATI STARTsc CHIMICAL EXPCSCRI RISULTS ACCIPTANCI CRITIAIA 1 OAY l 2 CAYS l 3 CAYS l 4 CAYS l 5 OAyS NI NI 8.1TLAXING/PIILINGl NI NI l
  • NI l l i i NI NI NE l NI l NI I 8.2 CILAMINATICN l NI NI

(

~

8.3 3LISTIRING l XI NI I l l NI NI NI f NI NI

! 8. 4 CTEIR ITTIC"'S l ,

RISUL"S PC'*IWID 3Y M,k gI. No gfgee: ' /

TIST RIPC'.T No.

l

~ ., . .,

- ~:: .v.  : . . . . _3 p .p: ~ . g , ,4 A - - -

TEST NO. 01720

. 4 CHEh.0L RESISTANCE TEST RESULL l

y BECHTEL CP-953 and A.N.S.I. N-5.12

1. TYPE SUBSTRATE: SIOE

[CNCRETE STEEL M CTHE*4

2. SURFACE PREPARATION (de scribe) :- Cri: blasted to SSPC-5710-63 vi:h a 1.0- 2.0

.l ,

a u oAas; pro m e.

Carbolina 193 LF/ SA.MPLE NC.* 15K

3. " PRODUCT TESTED:

Carbolina 191 HB

'4

. PRCDUCT APPLICATICN CONDITICNS THICKNESS OATE CCAT PRCCUCT CCDES BATCH 4 METHCC R/M(*F)%R.H. (ins.) APP L!E:

Ic Carbolina 193 LF .SE1682M Spray 73*F/26: .0038/.0036 12/16 8K:406M i

1: Carbo 11== 191 E3 8K2286M Spray 73*F/27: .0042/.0043 12/26 SJ1328M 1

I i

s l 7..

4. CURING CONDITICNS:

Aw.3IENT TEMP. (*F)  % REL. HUMIDITY I.ENGTH C7 CU".tE L

1st coat: 72*-81*F 23-49: 10 days l

~

2nd coa:: 61*-79'T 24-60: 6 weeks i

s 5. TYPE CF TEST: .

l CHEMICAL IXPCSURE TEST PER BECMTEL CP-953 and A.N.S.I. N-5-12 S. TEST TEMP!RATUFI; AMBIENT 75* + $* *T SC10 TION 75* * $* *?

7. CHEMICAL SCTUTICN (pH and Concentratien) : 0.5M sodium Fluoride (;H = 6.6) g i 8. TEST CBSERVATICNS: DATE STARTED 2/5/79 I

~

! ACCIPTANCE CXIMICAL EXPCSUP2 P250LTS CRITERIA 1 CAY l 2 CAYS l 3 OAYS l4 CAYS l5":AYS l 3 8.1 TI. AXING / PEELING E NE l ' NE l E l NE l l NE f NE f 8.2 CELAMINATICN l NE l NE NE l HE NE l NE l NI l

\ 8.3 3LISTERING NE 8.4 CTHEa ErrE TS 3E n l NE l n l , NE .

l

. ~

t uz g, gig,,,

=. 2 5 S =- ev - - ,- s = -v. W .. #.U !)

' ' U yv

, TES: REPCRT No.

r

. = - . . . - . . .

. . _ . . ~ =- . _. .- _ - - - . . .

?

- ~ '

. . .n. . .. .  ; ; .; .

-._...._.__n j,

4 .

l _

01720 TIST NO.

- CRIM1 CAL RISISTANCE TIST RISULTd BICM"'IL CP-953 and A.N.S.I. N-5.12

-k a

1. TYPE SUBSTRATI: S!:I"*'"*1/YCNCP2TI I STIIL k3IM CTHER l .

1 I Cri: blasted to SSPC-SP10-63.

! 2. , SURFACI PRIPARATICN (describe) :

i .

l 1

SAMPLI NO.: 15L Carbolina 193 LF/

f I 3. PRCDUCT TISTID:

' I Carbolina 191 E3 1

e i *

. PRCDUCT APPLICATICN CCNDITICNS *HICKNISS CATI i

BATCH i MI*HCD R/M (

  • F)  % R . H. (ins.) APPLII:

. CCAT PRCOUCT CCCES J  :

5 pray 73*T/26: ;0037/.CCJ6 12/15/

Carholina 193 LF 821682M t

)* '

is

. 812406M 812286M Spray 73*T/27: .0043/.0041 12/ $/*

i

  • ic Carholina 191 E3 "

' I 8J1828M '

I d

) .

i n

a

/

i 1 -

+
4. ' CURING CC:!DI*ICNS :

i 1

AMBIIN" TEMP. (*F)  % REL. HUMIDITY LINGTH Cr CU1:I 28-49 10 days ist c:at: 72*-81*F Ind coat: 61*-79*7 24-60 6 vuoks I

1 i 5. YPE Cr TIST:

1

.I

) CHIMICAL EXPCSURI IST PIR BICHTIL CP-953 and A.N.S.I. N-5-12 i

  • F SCLU"'ICN 75* - 5' *y j 6. IST TEMPIRA*UF2: AMSIINT no<*

! 7. CHIMICAL SOLO *ICN (pH and Cc=centracien) : 5 cit-1 Acid NH = 1.65) j 8. *IST CBSIRVATICNS: OATI STARTID 2/5/79 4

i

+! +

i i .

nCCIPTANCI - CHIM! CAL EXPCSCRI RISULTS i I CRITIRIA 1 CAY l 2 DAYS l 3 CAYS l4 CAYS l 5 CAYS l l l 8.1TLAXINC/PIILI!1Gl NE NE

  • NE l NE NE l l 8.2 CILAMINATICN NE NE NE f. NE f NE l

[ 8.3 3LIS IRING l NE NE NZ l. NE f NE l 1 , ( E.4 CTHER ITTICTS NE NI NE l NE l _ NE . l i

RISULTS FIVIIWID EY kb) a . N. E 1.e= V i

0I 1

, TIST FIPCRT NC. -

  • * - . . + - -

5

  • * * ' -' -- ..,.-.3,..,.....-

l I

t.__._..____._..-.- - - . . . _ . _ , . - , . _ _ _ . - . _ _ . - . . . . _ _ _ _ . _ _ _ _ _ , . _ , . _ _ . - , . . _ , - . _ . - . _ _ _ . . _ - . . . . _ . . . . , , _ , . . _ _ , . _ . , - .

pya. -g .

~

. 7 ;,4 . g . . , . ,

,.7,,_,,

.g .:

4 i . .. . _. . . . . _ . . .

TIST NO. 01720

  • CHIMACAL RESISTANCI TEST RESULT 3 i .

BECSTEL CP-953 and A.N.S.I. N-5.12 1

STIEL @*

2 CTHIM I 1. TYPE SUESTRA"*I: SI I "x4"x1/fCNCRITI  !

i

2. SURFACI PREPA.'ULTICN (describe) : Critblasted to SSPC-SP10-63 #.t!. a 1.0-2.0 i

l '

mil blast prof 11a.

Carbolina 193 LF/ SAMPLI NO.- 15M j 3.

  • PRODUC" "ESTID:

-g' Carbolina 191 E3 i  !

PRCDUCT APPLICATICN CONDITICNS THICKNISS DATI CCDES BATCH i METHOD R/M(*F)%R.H. (ins.) APPLII:

l CCAT PRCDUCT l;

l 881682E Spray 73*T/26: .0037/.0038 12/16/

) i ic Carbolina 193 LF 2 5

- SE2406M 1

i 8E2286E Spray 73*T/27: .0042/.C042 12/26/~

ic Carbolina 191 EB t

SJ1828M -

l .

1 1 I 1

=

4. " CURING CONDITICMS:

I I I j W AMs!ENT r.v.P. (*r) t nEL. En !:ITY 1EnGTx cr cUnr 4

l 72*-81*7 18-49% 10 days t

ist coat:

' 61*-79'T 24-6C% 6 weeir.s 2nd coat:

4 i .

j ,

5. ' TYPE CF TEST:

I i CHEMICAL EXPCSURI TIST PER SECHTIL CP-953 and A.N.S.I. N-5-12 i l SCLUTIIN 75* 5* *r  !

i 1 6. TEST TEMPERATUPE: AMBIINT 75* t 5* *T t

CHIMICAL SOLC"'ICN (pH and Concentration) : 0.3M Eydrogen Peroxide (;E = a.5)

,  ! 7.

TIST CBSITJATICNS: CATE STARTID 2/5/79 8.

i ACCIPTANCI CMIMIIAL EXPCSURI RISULTS l l  ;

j

)

i I CRI-IRIA 1 CAY l 2 CAYS l 3 CAYS l 4 IAYS l 5 CAYS I

! 8.1TLAXING/PEILINGl Ng NI 'NE l NE l NZ f l

l Nr Nr l Ng l NI l NI l 8.2 CILA.MINATION l 4 l l NI l NI l NI l l 6.3 ELIS* IRING l Nr NI l

i s.4 CTxIR trrIC S N Nt Nr l Nr _x _

i 1

I 5ULIS RZv EwIU IY - -)\

f

  • NE = No Effect '

. TEST RIreRT NC. V 02 -

1 I - . - - . - , . . . . __ ,, , ., ,,, , , _ _ _ ,

l 1

- . . . - - .e -- -mwm.,. -

e,- .~-,-w--,-----.-c,-n7,n-m-+ew--w-e--r---~'-w--w----r-1.m e- w -r- w -

. <
y. '7y.>. 4: yg.t v - , m :aq - ~_ ; . - n y w-- -

-. w.' - - - ~ , > , .

t. . ,

1 l . - . . . . . .

.t CHIP TAL RISISTANCE TEST RESUL**

.. ..~. _

BICHTIL CP-9 5 3 and A.N . S . I . N-5.12

.m

1. TYPE SUBSTRATI: SIZI "x4"xh" CONCRITI J

STII A$nt A36 CTHI4

/ .

2. SURFACI PRI?ARATICN (describe) : Grieblast to SSPC-SP10-63 1.0-2.0 sil blast erofile SAMPLI NO.: -

15 N

3. . PRCCUC"' TISTID: Carboline 193 LT/

Carboline 191 HB PRCDUCT . APPLICATICN CCNDITIONS TH*CXNISS CATI APPLII CCCES BATCH i MITHCD R/M (

  • T) %R .R . (ins.)

i CCAT PROCUdT 193 LT 8H1682x Spray 73*T/26% .0038/.0037 12 Ic Carboline 1

8K2406M ll 191 HB 8K2286M Spray 73*T/27 .0041/.0041 12  ! Ic carboline ,

' EJ1828M .

4. CUR *NG CCNDITICNS:

O AMBIINT T.P. (*F)  % REL. HUMIDITY LINCTH 07 CURI 15; coa: 72*T-81*T 28-49: 10 days 61*-79'T 24-60: 6 wee *a 2ND. coat

.i .

5. TY7I CF '*IST :

CHIMICAL IX7CSURE TEST PIR BICHTIL CP-953 and A.N.S.I. N-5-12 SCLUT CN 75* O 5*

6. '"IST TEMPERA'"URI AME INT 75* t $* *T 7
7. CHIMICAL SCLUTICN (pH and Ccncentration) : 0.3M Potassium Per=anganate(ph= 5.0
8. TIST CBSIRVATIONS: CATE STARTID 2-3-79 -

ACCI?TANCI' CHIMICAL IX?CSURI .USULTS

. CRITIRIA 1 CAY l 2 CAYS l 3 DAYS l 4 CAYS l 5 CAYS j SI l NE .E 8.1TLAXNG/PIILINGl NE l NE l l l NE NE NE 8.2 DELAMINATICN NE l NE l l l NI l NE l NI l 8.3 3LISTERING l NE l NE l 50 CD NC NC NC NC

. 6.4 CTHIR ITTICTS in LP ,

1 .NI ..o r.4:e:: SEV= Severe

! NC* No change C3= Cca:ing discolorat.?50UEIS EIYIINIU *" ' j [/y ?[

8 LP= Liquid phase (} GV g=**q-NP's4 se se e- e 69.'w.= -

W W M 939eeepegyg M M_ p+N4$ Mg g -g ;4

i

. . . n .gg ~g e ; y; a- ..

r. . ,-

m_~ ..

. 3.t

. ' w..

u . m

. w -- u l

.i 4

TEST NO. 01720 CHEM AL RISISTANCI TIST D.ISUL t

RECHTEL CP-953 and A.N.S.I. N-5.12

1. TYPE SUBSTRATE: SI:Z2"x4"z1/YCNCRITE STIIL @ CTHI4

' 2. SURTACI PRIPARATION (describe) : Cri:blasced to SSPC-SP10-63 with a 1.0-2.0 mil blast proff.14.

4 SAMPLE NO.: 15-C'

3. ' PRODUCT TESTED: Carbolina 193 LF/

W Carbolina 191 ER l

4
  • APPLICATICN CONDITICNS TH!CXNISS OATI PRODUCT CCCES 3ATCH 3 MITHCD R/M(*F)4R.M. (ins.) APPLII:

CCAT P RCCCC"'

sE1682M Spray 73*T/26: .0039/.0037 12/16/'

le Carbolica 193 Lr '

. 8E2406M SK:236M Spray 73

  • T/ 27*. .0048/.004: 12/26/*

ic carbo 11aa 191 H3 SJ1828M l

t 4 4. 'CURI'*G CCNDITICN? :

A!'3! INT TI:P. (*F)  % REL. HUMIDITY LINGTM C? CUnI 10 days ist coat: 7 *-81*T 28-49%

6 week.s  ;

2nd coat: 61*-79'T 24-40:

5. TYPE C7 TEST:

CHEMICAL EXPCSURE TIST PIR BECHTIL CP-953 and A.N.S.I. N-5-12

6. TEST TI:GERA"'JRI: AM3IINT 75* + 5' 'T SCLUT*CN 75* t 5' 'T .

CHEMICAL SCLUTION (pH and Cencantratien): 1.0 lb/1 gal. Trisodha Phosphate

7. spa = u.as li 8. TEST CSSIRVATICNSt DATI STAATED 2/3/79 ,

t ACCIPTA*CI CHEM

  • CAL EXPC50P2 ?iSULTS Cn!"IRIA 1 CAY l 2 CAYS l 3 CAYS l4 CAYS l 5 :*AYS l NE NE 8.1 TLAX**G/PIILING NE NE l NE l l NE NE l NE l 8.2 OELA".*NATICN f NE l NE l NE NZ S.3 3* :S IRING l JE NZ l NZ l l l NE S.4 C"XIR ET7ECTS l NI NE NE l l NE, l r l

3.,.S.w.

5 Rbv..ca c. , .y . s. %Al ' ./ % f/.Q ,

NE = No E!Iec: 8 gV

' V I

  • TEST REPCS.T NC. .. _.

l '

4

  • u*** * * * * =
  • s hao .w,g,, ,g- ,e,,.,

! i 1 -

. . q . . ;,, v .- m, .

. . <m

_ ._ ._.u -. .

i f

1

. TEST NO. 017 0

.. CMI.v. " AL RISISTANCI TIST R.ISULO O,*....

- BICM'"!L CP-9 5 3 and A.N . S . I . N-5.12

~

1. TYPI SUISTRAT_E: SI:12%N/{CNCRITE

$~IIL M CTHIR l 2. SURTACI PREPARATICN (describe) : Critblasted to SSPC-SP10-63 wi.h a 1.0-2.0 au o.as: prozna.

Carbolina 193 LF/ SAypLI No.:

15 R

3. 'PRCCUC" "!STIo Carbolina 191 MB APPLICATICN CONDITICNS THICKNISS CATI P RCDUCT

( '.

.CCIS 3ATCH i MI"'HC D R/M(*?)%R.H. (ins.) APPLII:

i CCAT P RCCUC'"

I Spray 73*F/26: .0339/.0038 12/16, ic Carboline 193 LF 8H1682M j '

8E2406M I

Carbolina 191 E3 8K2256M Spray 73*F/07: .0044/.0042 12/26.

le 8J181SM i -

t i

e*

4. CURING CCNCITICMS:

AM3IIN':' TIMP . (*T)  % RIL. HU$4ICITY LI"CTH OF CUSI 72*-81*T 28-49 10 days ist coat:

61*-79'T 24-60: 6 week.s 2nd coat:

i i

5. "YPI CF TIST:

i i

CHIMICAL IX7CSURE TIST PER SICHTIL CP-953 and,A.N.S.I. N-5-12 e

! 6. TEST TIM 7IRATUPIt AMBIINT 7s* + s* -

  • T SCLUT CN 75*
  • 5' *?.

! 7. CHIMICAL SCLU* CN (pH and Ccncentration) : 5 Oisodium Phosenate (-E = 3.5) t

8. TIST CBSIRVATICNS DATI STARTID 2/5'/79 i.

t i ACCI7TA2:CI C:iIMICAL IXPCSURI ?.ISCLTS CR*TIRIA 1 OAY l 2 OAYS l 3 OAYS l 4 CAYS l 5 OAYS XI ' NZ l NZ l NE 8.1TLAXINC/PIILINGl NI l l NE l NZ 8.2 OILAM:!!AT CN l NE l NE NE l l NZ l NI l 9.3 2*!STIRING l NI l NE NE d 8.4 CTHIR ETTICTS NI NI NE NE l , NE

' RISCLTS 75VII*<TIO BY hk *[.b , k NE = No ,,.,act '

5 TEST PIPOP.T No. 0 hl .

j a . _ .

. .., -. - ; ., -c.. -

a. , .c , r. ,

.. 9, .. .

. . y, , . .... ,

t i

3 .

, .4

,. e t

J-SUMtfARY CT CE.MICAI, EXPCSLTI RESL'I.TS s

a

}.

1 l

Os.*.+6

  • !{

s .

f Test Report No.

8 e

1 4

0 O eme

& - 4 ,g. .

gg ,g ,

+ * ... . , .

a mm

  • %. P }

- . J I

t C,C,."( O CIn C SICHTIL CP-951 AND A.N.S.I. N-5-12 CHIMICAL RESISTANCI TIST AISULTS Cuboline 193L7/ Carbo:,1=e 191 M3 CCATING SYSTEMS:

St 51 0.30 M 51 S t. Sn SULTURIC HYORCGIN SCC:UM CITRIC NITRIC HY::RCXI t

ACID HYDRA :NI ACID PIRCXIII

'ROCUCT TISTID ACID pass fail pass pass pass fail

' O.5M Sn 51 0.30M 1.0t/ gal. 5%

. PCTASIUM P IPp.AN. Tg:SCO gM c: Scc:gg SCDIUM SCCIUM AMMONIUM BCRATI HYDRCXIOI CANATI PHCSPHATE PHCSPHATI j TRCOCCT TISTID TLUCRI I I

o, pass pass pass pass pass pass d

I i '

i t

,1 M i

725U:.TS AsPRCvI:

t 4'. s'(y,6s 4  !\ ] '

U TIST ?2?CRT NC. \017 0 i

I e

f. V .
S-06376-6

-- .. 89 espe.

' - - - _ _ _ _ _ _ _ _ _ _ _ _ - - - - - - - - - - - - - . . - _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _

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