ML19295G726

Revised Final Status Survey (FSS) Report - Phase 2, Auxiliary Building Basement Survey Unit 05100

ML19295G726
Person / Time
Site:	Zion  File:ZionSolutions icon.png
Issue date:	09/01/2019
From:	Massengill R ZionSolutions
To:	Office of Nuclear Material Safety and Safeguards
Shared Package
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References
ZS-2019-0090
Download: ML19295G726 (252)

Text

ZION STATION RESTORATION PROJECT FINAL STATUS SURVEY RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 PREPARED BY / DATE: 2019-09-01 R. Massengill, Radiological Engineer REVIEWED BY / DATE: 2019-09-01 R. Decker, Radiological Engineer APPROVED BY / DATE: 2019-09-01 D. Wojtkowiak, C/LT Manager

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 TABLE OF CONTENTS

1. EXECUTIVE

SUMMARY

................................................................................................ 7

2. SURVEY UNIT DESCRIPTION ...................................................................................... 8

3. CLASSIFICATION BASIS.............................................................................................. 13

4. DATA QUALITY OBJECTIVES (DQO) ...................................................................... 30

5. SURVEY DESIGN ............................................................................................................ 34

6. SURVEY IMPLEMENTATION ..................................................................................... 41

7. SURVEY RESULTS ......................................................................................................... 43

8. QUALITY CONTROL..................................................................................................... 61

9. INVESTIGATIONS AND RESULTS ............................................................................. 61

10. REMEDIATION AND RESULTS .................................................................................. 62

11. CHANGES FROM THE SURVEY PLAN ..................................................................... 63

12. FINAL STATUS SURVEY PLAN .................................................................................. 64

13. DATA QUALITY ASSESSMENT (DQA) ..................................................................... 65

14. ANOMALIES .................................................................................................................... 66

15. COMPLIANCE EQUATION .......................................................................................... 66

16. CONCLUSION ................................................................................................................. 68

17. REFERENCES .................................................................................................................. 70

18. ATTACHMENTS ............................................................................................................. 71 ATTACHMENT 1 .............................................................................................................. 72 ATTACHMENT 2 .............................................................................................................. 90 ATTACHMENT 3 ............................................................................................................ 108 ATTACHMENT 4 ............................................................................................................ 115 ATTACHMENT 5 ............................................................................................................ 146 ATTACHMENT 6 ............................................................................................................ 167 ATTACHMENT 7 ............................................................................................................ 173 ATTACHMENT 8 ............................................................................................................ 174

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 LIST OF TABLES Table 1 - Auxiliary Building 542 Foot Elevation Characterization Concrete Core Sample Analysis Summary (2012-2013) ...................................................................................................16 Table 2 - Auxiliary Building Characterization Concrete Core Samples (2012-2013) - Eberline Laboratory Analysis (1)...................................................................................................18 Table 3 - Summary of Auxiliary Building Continuing Characterization Concrete Core Samples (2017) - On-Site Analysis (1) ..........................................................................................21 Table 4 - Auxiliary Building Continuing Characterization Concrete Core Samples (2017) -

Eberline Laboratory Analysis (1) ....................................................................................29 Table 5 - Dose Significant Radionuclides and Mixture .................................................................31 Table 6 - Base Case DCGLs for Auxiliary Building Basement Survey Unit (BcDCGLB) LTP Chapter 5, Table 5-3 ......................................................................................................33 Table 7 - Operational DCGLs for Auxiliary Building Basement Survey Unit (OpDCGLB) LTP Chapter 5, Table 5-4 ......................................................................................................33 Table 8 - Surrogate Ratios .............................................................................................................35 Table 9 - Action Levels for Survey Unit 05100 ............................................................................36 Table 10 - Adjusted Minimum Number of ISOCS Measurements................................................37 Table 11 - Investigation Levels......................................................................................................39 Table 12 - Synopsis of Survey Design ...........................................................................................40 Table 13 - Auxilairy Building Surfaces - Statistical Quantities - Systematic Population ............44 Table 14 - Elevated Measurement ROC Concentrations and SOFs ..............................................46 Table 15 - Summary of ISOCS Replicate Measurements for QC .................................................50 Table 16 - Summary of Results for Judgmental/Investigational Measurements Taken in the Auxiliary Building........................................................................................................51 Table 17 - Summary of FSS Concrete Core Analysis by Eberline ................................................52 LIST OF FIGURES Figure 1 - Auxiliary Building 542 foot Elevation ............................................................................. 9 Figure 2 - Auxiliary Building 560 foot Elevation ........................................................................... 10 Figure 3 - Auxiliary Building 579 foot Elevation ........................................................................... 11 Figure 4 - Characterization Concrete Core Sample Locations ....................................................... 15 Figure 5 - Characterization Concrete Core Sample Locations (2017) ............................................ 20

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 LIST OF ACRONYMS AND ABBREVIATIONS ABEDCT Auxiliary Building Equipment Drain Collection Tank ALARA As Low As Reasonably Achievable AMCG Average Member of the Critical Group BAE Boric Acid Evaporator BcDCGL Base Case Derived Concentration Guideline Level BFM Basement Fill Model DQA Data Quality Assessment DQO Data Quality Objective DCGL Derived Concentration Guideline Level EMC Elevated Measurement Comparison FOV Field of View FSS Final Status Survey HTD Hard-to-Detect HUT Hold Up Tank IC Insignificant Contributor LTP License Termination Plan LBGR Lower Bound of the Gray Region MARSSIM Multi-Agency Radiation Survey and Site Investigation Manual MDC Minimum Detectable Concentration NaI Sodium Iodide NRC Nuclear Regulatory Commission OH Overhead OpDCGL Operational Derived Concentration Guideline Level QAPP Quality Assurance Project Plan QC Quality Control RE Radiological Engineer RHR Residual Heat Removal

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 ROC Radionuclides of Concern SOF Sum of Fractions TEDE Total Effective Dose Equivalent UBGR Upper Bound of the Gray Region UCL Upper Confidence Level ZNPS Zion Nuclear Power Station ZSRP Zion Station Restoration Project

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100

1. EXECUTIVE

SUMMARY

This Final Status Survey (FSS) Release Record for survey unit 05100, Auxiliary Building Basement, has been generated for the Zion Station Restoration Project (ZSRP) in accordance with ZionSolutions procedure ZS-LT-300-001-005, Final Status Survey Data Reporting (Reference 1) and satisfies the requirements of Section 5.11 of the Zion Station Restoration Project License Termination Plan (LTP) (Reference 2). The FSS package for basement survey unit 05100, Auxiliary Building Basement includes FSS design and FSS results for the Auxiliary Building basement floor surfaces, wall surfaces, sumps and elevator pit on the 542 foot elevation and ledges on the 560 foot and 579 foot elevations.

The Final Status Survey (FSS) sample plan for this survey unit was developed in accordance with ZionSolutions procedure ZS-LT-300-001-001, Final Status Survey Package Development (Reference 3), the ZSRP LTP, and guidance from NUREG-1575, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM)

(Reference 4).

In accordance with ZSRP LTP Chapter 5, section 5.5.2.1 and Table 5-19, the Auxiliary Building basement survey unit has a MARSSIM classification of 1. A survey plan was designed based upon use of the Sign Test as the nonparametric statistical test for compliance. Both the Type I () and Type II () decision error rates were set at 0.05. The Canberra In Situ Object Counting System (ISOCS) was selected as the primary instrument used to perform FSS of the Auxiliary Building basement survey unit. The surface area of the Auxiliary Building Basement survey unit was determined to be 7,226 m2. Based solely on the surface area covered by a single ISOCS measurement (a nominal Field of View [FOV] of 28 m2) the minimum number of measurements necessary to cover the surface area was 233 measurements (see LTP Chapter 5, Table 5-18). However, due to physical structural anomalies, building corners/edges, and, to ensure 100% coverage of all surfaces, 425 systematic ISOCS measurements were actually collected. Some of the measurements represented an FOV less than 28 m2. The additional measurements were added to conservatively ensure 100% coverage of every surface. When necessary, the grid dimensions or the field of view were modified to ensure 100% areal coverage was achieved.

LTP Chapter 6, section 6.4.5 states, The dose from penetrations is summed with the dose from the wall and floor surfaces of both basements that the penetration interfaces. The Containment penetrations interfaced with the Auxiliary Building and the Turbine Building (through the Unit 1/Unit 2 East and West Main Steam Valve Houses). Consequently, the FSS design employed the Derived Concentration Guideline Levels (DCGLs) for the

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Containment penetrations, which was the most limiting. The resultant dose was added to each Basement to ensure compliance with the LTP.

The results of ISOCS measurements taken in the Auxiliary Building basement survey unit indicate that 16 of the 425 systematic measurements had a Sum-of-Fraction (SOF) greater than 1.0 when considering the concentration of all applicable Radionuclides of Concern (ROC), and applying the respective Operational Derived Concentration Guideline Levels (OpDCGL) for the Auxiliary Building basement from ZionSolutions TSD 17-004, Operational Derived Concentration Guideline Levels for Final Status Survey (Reference 5). However, none of the ISOCS measurements were greater than Base Case Derived Concentration Guideline Levels (BcDCGL) from TSD 17-004 and the survey unit passed the Sign Test. Therefore the null hypothesis was rejected and the Auxiliary Building basement survey unit is acceptable for unrestricted release.

2. SURVEY UNIT DESCRIPTION The Auxiliary Building footprint contained numerous systems and components including the following: Hold Up Tank (HUT) system components, Boric Acid Evaporator (BAE) feed pumps, drain collection tanks and piping, Safety Injection System, Residual Heat Removal (RHR) system components, Containment Spray, Chemical Drain, Blowdown Heat Exchanger, Waste Gas, charging pumps, Refuel Water Storage Tanks and Letdown Heat Exchanger.

The Auxiliary Building basement survey unit is a Class 1 basement FSS unit. The Auxiliary Building basement survey unit is comprised of the combined interior perimeter walls and floor surfaces of each remaining building basement from the 542 foot, 560 foot and 579 foot elevations, following demolition. This survey unit consists of the Auxiliary Building basement floor at the 542 foot elevation, the two horizontal surfaces beneath the Unit 1 and Unit 2 primary piping penetrations at the 560 foot elevation, the two horizontal surfaces above the Auxiliary Building Equipment Drain Collection Tank (ABEDCT) areas at the 579 foot elevation, and all the associated walls below the 588 foot elevation.

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 1 - Auxiliary Building 542 Foot Elevation

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 2 - Auxiliary Building 560 Foot Elevation

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 3 - Auxiliary Building 579 Foot Elevation

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Prior to demolition, the Auxiliary Building was located between the Unit 1 and Unit 2 Containments and the Turbine Building. The structure was designed to house support systems for the operation of both reactors. Major support systems that were located in the Auxiliary Building include Containment Spray, Residual Heat Removal, Reactor Water Cleanup, Reactor Water Charging and Safety Injection systems. In addition, the Auxiliary Building also contained various filters and tanks designed to batch and/or process gaseous, liquid and solid wastes resulting from reactor operation. With the exceptions of the service water, primary de-ionized water, control air, fire protection, nitrogen gas and service air, all the systems within the Auxiliary Building contained radioactive material.

The structure itself was designed to contain and control leakage from these systems during normal operation as well as unusual events. System leakage and maintenance activities over the operating life of the facility had resulted in the radiological contamination of most of the interior surfaces of the Auxiliary Building. Most of the cubicles that contained major systems were posted as contaminated areas identifying removable radioactivity. Based on the building design-basis and the operating history, all internal survey units within the Auxiliary Building were considered to be Class 1 areas.

The basic decommissioning end-state for the Auxiliary Building consists of the concrete foundation, concrete walls below 588 foot elevation and the 542 foot elevation concrete floor. All systems and components contained within the Auxiliary Building were disassembled and/or demolished, packaged and properly dispositioned as either radioactive or non-radioactive waste.

After demolition was complete, structural surfaces of the Auxiliary Building above the 588 foot elevation were removed. Most of the 570 foot elevation and the 560 foot elevation were removed as well. The 542 foot elevation contained the floor (including sumps and pits) and the interior perimeter walls. No interior cubicle walls or commodities remained. The 560 foot elevation only contained each containment pipe tunnel floor and no walls or commodities. The 579 foot elevation only contained the floors above the ABEDCT areas southeast of Unit 2 Containment and northeast of Unit 1 Containment and no walls or commodities.

Engineering drawings indicated that the concrete walls of the remaining structure are 5 feet thick and the 542 foot elevation floor was up to 4 feet thick.

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100

3. CLASSIFICATION BASIS Based on the Zion Station Historical Site Assessment (HSA) (Reference 6), the 542 foot elevation of the Auxiliary Building was identified as Class 1 areas and contained the following survey units:

• 05100 - Auxiliary Building,

• 05101 - Unit 1A RHR Pump Room,

• 05102 - Unit 1B RHR Pump Room,

• 05103 - Unit 2A RHR Pump Room,

• 05102 - Unit 2B RHR Pump Room,

• 05105 - Unit 1 Pipe Chase,

• 05106 - Unit 2 Pipe Chase,

• 05107 - Hold Up Tanks,

• 05108 - Auxiliary Building Central,

• 05109 - Auxiliary Building South,

• 05110 - Auxiliary Building North,

• 05111 - Auxiliary Building West,

• 05112 - Gas Decay Tanks Area

• 05113 - Unit 1 Auxiliary Building Equipment Drain Collection Tank Room,

• 05114 - Unit 2 Auxiliary Building Equipment Drain Collection Tank Room,

• 05115 - HUT Recirculation and BAE Feed Pumps,

• 05116 - Auxiliary Building Equipment Drain Tank and Pumps,

• 05117 - Auxiliary Building Sump A, and

• 05118 - Auxiliary Building Sump B.

Based on the HSA, the 560 foot and 579 foot elevations of the Auxiliary Building were identified as Class 1 areas and contained the following survey units:

• 05217 - Unit 1 Vertical Pipe Chase,

• 05218 - Unit 2 Vertical Pipe Chase,

• 05313 - Unit 1 Horizontal Pipe Chase, and

• 05314 - Unit 2 Horizontal Pipe Chase.

The Basement Fill Model (BFM) applies to the steel and concrete walls and floor surfaces, below the 588 foot elevation of the Unit 1 Containment Building, Unit 2 Containment Building, Auxiliary Building, Turbine Building, WWTF, the lower portion of the SFP, Fuel Transfer Canals, Crib House and Forebay, Unit 1 and Unit 2 Steam Tunnels and the Circulating Water Intake Piping and Circulating Water Discharge Tunnels. The BFM source term also includes the end-state embedded piping and penetrations. The survey

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 units designated for structures below 588 foot elevation from the HSA that were presented in LTP Chapter 2, Table 2-2 were based on screening values and source term assumptions that are significantly different from the BFM and are therefore not applicable. The twenty-three (23) survey units identified in the HSA that remained in the end-state of the Auxiliary Building following demolition were combined into one FSS unit for basement structures.

In May and June of 2012, a characterization survey was performed of the Auxiliary Building 542 foot elevation and Auxiliary Building interior perimeter walls. The characterization survey consisted of surface scans and the acquisition of a series of concrete core samples taken in the 542 foot elevation concrete floor and lower interior perimeter walls. In March of 2013, two (2) additional concrete cores were taken in the Auxiliary Building elevator shaft and the HUT Cubicle floors as these areas became accessible. During the time that initial characterization was performed, all radioactive systems and components were still located inside the Auxiliary Building. Consequently, ambient radiation dose rates inside some of the cubicles on the 542 foot elevation prohibited the direct assessment of concrete surfaces by scanning or direct measurement.

During the initial characterization of the Auxiliary Building basement, extensive beta/gamma scan surveys were performed on the floors and lower walls of the 542 foot elevation in an effort to determine the locations representing the worst-case radiological condition for concrete in each survey unit. These scans were performed of accessible walls surfaces to the extent practicable while standing on the 542 foot elevation, to a nominal elevation of approximately six feet up the wall from the floor. The scan surveys indicated that, for a majority of the lower wall surfaces on the Auxiliary Building 542 foot elevation, the residual radioactivity was indistinguishable from ambient background. This was particularly true for all the outer wall surfaces in the east portion of the Auxiliary Building 542 foot elevation, including the Waste Gas Decay Tank area, the Lake Discharge Tank area, the Blowdown Monitor Tank area and the areas adjacent to the Cavity Fill Pump cubicles. Residual contamination at concentrations greater than the ambient background was only detected on the outer walls of the Unit 1 and Unit 2 Pipe Chases, the Unit 1 and Unit 2 ABEDCT cubicles and the outer walls of the HUT cubicles.

However, with the exception of the HUT cubicles, the contamination identified on the walls in the Pipe Chases and ABEDCT cubicles was not uniform. The contamination on the walls in these cubicles was primarily from valve leakage and gland seal spray from primary system pumps.

A total of 20 concrete core samples were collected. The locations selected were biased toward locations where physical or observed radiological measurements indicated the presence of fixed and/or volumetric contamination of the concrete media. When possible, locations were determined based upon elevated observed contact dose rates or count rates

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 from scans. In addition, visual observations of floor and wall surfaces, such as discoloration or standing water, were used to identify potential locations of surface contamination. The goal was to identify, to the extent possible, the locations that exhibited the highest potential of representing the worst-case radiological condition for concrete in each survey unit. This judgmental sampling approach also ensured that there was sufficient source term in the cores to achieve the sensitivities required to determine the radionuclide distributions of gamma emitters as well as Hard-to-Detect (HTD) radionuclides.

The locations where the core samples were taken are illustrated in Figure 4. The concrete cores, split into pucks, were analyzed on the on-site gamma spectroscopy system. A summary of the on-site gamma spectroscopy results for the analysis of the concrete cores taken from the 542 foot elevation of the Auxiliary Building is presented in Table 1.

Figure 4 - Characterization Concrete Core Sample Locations

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 1 - Auxiliary Building 542 Foot Elevation Characterization Concrete Core Sample Analysis Summary (2012-2013)

Co-60 Cs-137 Core Avg. Avg.

Surface Surface Location Sample ID# Depth Subsurface Subsurface Activity (1,3) Activity (1,3)

(inches) Activity (2,3) Activity (2,3)

(pC/g) (pC/g) (pC/g) (pC/g) 1A RHR Pump Room B105101-CJFCCV-001 5.5 6.11E+01 1.06E+01 3.74E+03 3.06E+02 2A RHR Pump Room B105103-CJFCCV-001 4.0 4.56E+02 2.04E+02 2.51E+04 4.92E+03 2B RHR Pump Room B105104-CJFCCV-001 1.0 4.08E-01 4.20E-01 9.44E+00 1.79E+00 Unit 1 Hot Pipe Chase B105105-CJFCCV-001 5.0 7.00E+00 8.89E-01 9.83E+03 2.65E+03 Unit 2 Hot Pipe Chase B105106-CJFCCV-001 4.5 3.86E+00 1.51E+00 2.77E+03 1.05E+03 Unit 2 Hot Pipe Chase B105106-CJFCCV-002 1.0 1.75E+01 3.60E+00 3.09E+03 4.14E+02 Hold-up Tank Cubicles B105107- CJFCCV-002 14.0 1.18E+01 3.71E-01 1.17E+02 2.26E+00 Central Common Area B105108-CJFCCV-001 4.5 4.32E-01 1.74E-01 1.92E+03 2.18E+02 Central Common Area B105108-CJFCCV-002 4.0 2.80E+00 1.28E+00 1.13E+02 1.53E+01 Central Common Area B105108-CJFCCV-003 3.0 3.03E+01 1.65E+00 1.67E+03 7.26E+01 Central Common Area Elevator Shaft B105108-CJFCCV-004 4.0 4.05E+00 2.71E-01 1.51E+02 4.92E+00 South Common Area B105109-CJFCCV-001 1.0 4.22E+00 8.22E-01 1.43E+03 2.13E+02 North Common Area B105110-CJFCCV-001 1.0 8.09E+00 1.81E+00 2.11E+03 3.50E+02 North Common Area B105110-CJFCCV-002 1.5 3.28E-01 7.85E-02 6.37E+01 5.17E+00 East Common Area B105111-CJFCCV-001 3.5 2.06E+00 7.66E-01 1.13E+03 1.99E+02 East Common Area Wall B101111-CJWCCV-002 0.5 1.94E-01 2.85E-01 9.52E-01 4.25E-01 Unit 1 ABEDCT Room B105113-CJFCCV-001 5.5 1.96E+02 1.33E+01 5.69E+03 1.54E+02 Unit 1 ABEDCT Room B105113-CJFCCV-002 5.5 3.76E+01 6.98E+00 1.79E+03 1.50E+02 Unit 1 ABEDCT Room Wall B105113-CJWCCV-003 1.0 6.71E+02 1.69E+02 1.66E+04 3.77E+03 (1) Represents surface activity of floor following removal of loose contamination (surface to depth of 0.5 inches)

(2) Represents average of activity over entire depth of core sample minus the surface activity (0.5 inches to depth of core)

(3) Bold values indicate concentration greater than MDC. Italicized values indicate MDC value.

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Co-60, Cs-134 and Cs-137 were the only plant-derived gamma-emitting radionuclides identified. ZionSolutions TSD 14-028, Radiological Characterization Report (Reference 7) presents additional detail on the concrete sampling methodology and results of the radiological analysis of each concrete core sample obtained from the Auxiliary Building basement.

Analyses of the concrete core samples taken from the Auxiliary Building 542 foot elevation indicate that there was extensive radiological contamination at depth. This is most likely due to the fact that the 542 foot elevation was routinely flooded with contaminated water during operations. In the first 1/2-inch of floor, Co-60 concentrations averaged 46 pCi/g with a maximum concentration of 456 pCi/g, and Cs-137 concentrations averaged 3,352 pCi/g with a maximum concentration of 25,100 pCi/g. In both Unit 1 and Unit 2 Pipe Tunnel rooms, Cs-137 concentrations of 530 pCi/g and 1,740 pCi/g were observed at depths of 4 and 5 inches, respectively. In addition, sample analysis indicated a Cs-137 concentration of 56.80 pCi/g at a depth of 2 inches in the central common area, a Cs-137 concentration of 31.10 pCi/g at a depth of 3.5 inches in the east floor area and a Cs-137 concentration of 63.10 pCi/g at a depth of 2.5 inches in the Unit 1 Equipment Drain Collection Tank room.

The top 1/2-inch puck from six (6) of the 20 cores from the Auxiliary Building were sent to Eberline Laboratory for gamma spectroscopy and HTD analyses for radionuclides such as H-3, C-14, Tc-99, Ni-63, Sr-90, and alpha emitters. The results of the analyses are presented in Table 2. The mixture percentages for the initial suite of radionuclides for the Auxiliary Building basement concrete were developed in TSD 14-019, Radionuclides of Concern for Soil and Basement Fill Model Source Terms (Reference 8) using the results of all core sample analyses, including the cores sent to Eberline. Significant HTD radionuclides identified by the analysis of the concrete core samples include Ni-63 and H-

3. The other radionuclides positively detected at concentrations greater than their respective Minimum Detectable Concentration (MDC) included C-14, Tc-99, Sr-90, Ag-108m, Pu-238, Pu-239/240, Am-241 and Am-243.

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 2 - Auxiliary Building Characterization Concrete Core Samples (2012-2013) - Eberline Laboratory Analysis (1)

B105101- B105103- B105105- B105106- B105108- B105113-Radionuclide CJFCCV-001 CJFCCV-001 CJFCCV-001 CJFCCV-002 CJFCCV-003 CJWCCV-003 (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)

H-3 1.12E+01 1.68E+01 6.98E+00 2.96E+01 5.61E+00 4.71E+00 C-14 9.56E-01 4.88E+00 9.98E-01 1.48E+00 1.19E+00 3.10E+00 Fe-55 1.20E+01 3.16E+01 1.81E+01 1.12E+01 8.17E+00 1.73E+01 Ni-59 1.59E+01 2.08E+01 1.81E+01 1.74E+01 1.67E+01 1.75E+01 Co-60 2.62E+01 2.28E+02 3.20E+00 1.01E+01 1.83E+01 2.03E+02 Ni-63 1.52E+02 3.38E+03 2.91E+02 9.18E+01 8.59E+01 1.65E+03 Sr-90 1.07E+00 5.44E+00 1.52E+00 4.04E-01 3.29E-01 8.82E+00 Nb-94 2.29E-01 8.17E-01 6.19E-01 2.13E-01 3.02E-01 6.57E-01 Tc-99 1.45E+00 9.61E-01 6.70E-01 4.73E-01 9.09E-01 5.81E-01 Ag-108m 2.06E-01 1.66E+00 8.06E-01 2.53E-01 1.82E-01 5.96E-01 Sb-125 2.27E+00 7.79E+00 4.39E+00 2.46E+00 1.99E+00 4.57E+00 Cs-134 4.53E-01 1.47E+00 8.63E-01 8.11E-01 2.90E-01 1.23E+00 Cs-137 1.35E+03 1.33E+04 5.29E+03 1.88E+03 1.05E+03 4.19E+03 Pm-147 1.43E+01 8.17E-01 9.63E-01 5.30E+00 9.57E+00 7.19E+00 Eu-152 7.57E-01 2.58E+00 1.05E+00 6.75E-01 7.10E-01 1.80E+00 Eu-154 4.00E-01 1.38E+00 1.19E+00 3.95E-01 3.21E-01 1.05E+00 Eu-155 5.76E-01 1.76E+00 1.16E+00 6.33E-01 4.84E-01 1.05E+00 Np-237 2.04E-02 2.13E-02 2.39E-02 2.10E-01 1.92E-02 3.20E-02 Pu-238 1.77E-02 3.43E-01 1.32E-02 1.37E-02 1.78E-02 1.39E-02 Pu-239/240 1.77E-02 2.74E-01 1.06E-02 1.37E-02 1.33E-02 1.35E-02 Pu-241 2.48E+00 2.46E+00 1.79E+00 2.36E+00 1.73E+00 1.72E+00 Am-241 3.03E-02 2.29E-01 4.38E-02 2.72E-02 4.29E-02 3.17E-02 Am-243 2.89E-02 1.09E-01 6.01E-02 3.62E-02 3.36E-02 3.18E-02 Cm-243/244 3.91E-02 4.41E-02 3.95E-02 3.89E-02 4.02E-02 4.29E-02 (1) Bold values indicate concentration greater than MDC. Italicized values indicate MDC value.

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Radiological operations turnover surveys, conducted in 2016, identified numerous areas within the remaining structure that had elevated radiation levels. The elevated areas on the 542 foot elevation are as follows:

• Unit 1 A RHR pump room - 20 mr/hr on pipe in overhead (OH), 2-8 mr/hr on wall above trough, 1-22 mr/hr on the floor/trough.

• Unit 1 B RHR pump room - 1 to 40 mr/hr on floor/trough, 17 mr/hr on flush cut pipe in wall, 2.5 on wall.

• Unit 2 A RHR pump room - 32 mr/hr on the sides of pedestal, 1 to 18 mr/hr floor/trough, 2 mr/hr on wall.

• Unit 2 B RHR pump room - 14 mr/hr open pipe, 2-6 mr/hr on sides of pedestal, 1 to 2.8 of floor/trough.

• Unit 1 pipe chase - 12 mr/hr on rubble pile, 7 mr/hr on pipe, 1.5 to 3 mr/hr on sloped walls, 1 to 3 mr/hr on SW wall, 50 and 66 mr/hr on open pipes in OH, 1 to10 mr/hr on floor/pedestal,

• Unit 2 pipe chase - 2 to 16 mr/hr on open pipes in OH, 2 to 6 mr/hr on sloped walls, 2.5 mr/hr on drain, 2 mr/hr on pedestal.

• South Area - 1 to 6 mr/hr on floor, 2 to 8 on capped pipe ends in OH.

• North Area - 1 to 2.3 mr/hr on floor, 2 to 4.1 taped pipe ends in OH.

• Central Area - 1.6 to 4.8 mr/hr on floor, 2.1 to 2.2 mr/hr on drain.

• Gas Decay Tanks - 1 to 12.2 mr/hr on floor, 1.1 to 2.7 mr/hr on holes in floor.

• Unit 1 Equipment Drain Collection Tank - 225 on contact and 26 at 30 cm on capped pipe elbow in OH, 63, 67 and 141 mr/hr on open pipes in OH, 7.3 to 12 mr/hr on quartet of capped pipes in OH, 1 to 5 mr/hr on floor, 3.5 mr/hr on drain.

• Unit 2 Equipment Drain Collection Tank - 2 to 3 mr/hr on floor, 2.7 to 10 mr/hr on pipe ends in OH.

• HUT Recirculation and BAE Feed Pumps - 1.3 to 7.6 mr/hr on drain and floor.

• Auxiliary Building Drain Tank and pumps - 1 to 95 mr/hr on floor, 2 to 3 mr/hr on open pipes in OH.

In December of 2017, as part of continuing characterization activities, four (4) survey packages (B1-05100, B1-05105, B1-05106, and B1-05107) were implemented to collect and analyze a total of thirty-two (32) additional concrete cores throughout the Auxiliary Building basement 542 foot elevation for the purpose of determining the concentration profiles at depth and to develop a conservative ISOCS efficiency calibration for the Auxiliary Building basement. The first three (3) survey packages (B1-05100, B1-05105, and B1-05106) were located in the North, South and West portions of the Auxiliary Building basement. The fourth survey package (#B1-05107) was focused on the HUT

[19]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 area, or the West end of the Auxiliary Building basement. A total of twenty-two (22) floor and ten (10) wall core locations were collected.

Figure 5 - Characterization Concrete Core Sample Locations (2017)

Cores were collected from the floor and lower walls to a depth of 6 inches, or refusal. The cores were cut into 1/2-inch thick pucks, and onsite gamma spectroscopic analysis was performed on both sides of each puck throughout the length of the core. Additionally, 1/2-inch pucks from eight (8) of the sample locations that exhibited the highest gamma activity were sent to an accredited off-site laboratory for HTD radionuclide analyses. A summary of the on-site gamma spectroscopy results for the analysis of the concrete cores taken from the Auxiliary Building basement floor and walls for continuing characterization is presented in Table 3. A summary of the analysis of continuing characterization concrete cores for the full suite of radionuclides by an off-site laboratory is presented in Table 4.

[20]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 3 - Summary of Auxiliary Building Continuing Characterization Concrete Core Samples (2017) - On-Site Analysis (1)

B1-05105C-JFC-001-CV B1-05105C-JFC -002-CV B1-05105C-JFC-003-CV B1-05105C-JFC-004-CV (542 foot U1 HPT) (542 foot U1 HPT) (542 foot U1 HPT) (542 foot U1 HPT)

Depth Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 (in) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) 0 2.44E+01 1.57E+00 5.58E+02 4.24E+00 0.00E+00 4.38E+01 1.85E-01 1.10E-02 6.95E-01 1.92E-01 0.00E+00 1.67E+00 0.5 2.34E+01 1.68E+00 4.70E+02 4.68E+00 3.58E+01 3.58E+01 5.10E-02 9.97E-02 3.33E-01 9.10E-02 1.44E-01 1.13E+00 0.5 1.06E+01 0.00E+00 1.06E+02 1.71E+00 9.87E-02 6.28E+00 0.00E+00 7.11E-02 2.11E-02 0.00E+00 1.52E-02 1.26E-01 1 9.40E+00 3.64E-01 9.04E+01 1.27E+00 1.28E-01 4.60E+00 6.60E-02 7.68E-02 1.03E-01 1.09E-01 1.14E-01 2.41E-02 1 2.43E+00 0.00E+00 8.03E+00 7.24E-01 0.00E+00 7.90E-01 8.08E-02 3.18E-02 7.84E-02 6.87E-03 6.75E-02 1.82E-01 1.5 2.31E+00 2.10E-02 6.68E+00 7.76E-01 0.00E+00 6.75E-01 6.19E-02 2.68E-02 0.00E+00 1.28E-01 1.92E-03 3.07E-02 1.5 6.12E-01 9.44E-02 6.28E-01 3.83E-01 5.82E-02 1.39E-01 8.84E-02 0.00E+00 1.49E-01 3.63E-02 4.06E-02 0.00E+00 2 3.93E-01 0.00E+00 4.05E-01 3.48E-01 3.06E-03 1.05E-01 1.13E-02 8.42E-02 0.00E+00 6.07E-02 0.00E+00 5.57E-02 2 1.27E-01 8.75E-02 2.38E-01 1.87E-01 0.00E+00 2.17E-01 8.72E-02 1.08E-01 1.21E-01 1.19E-01 0.00E+00 1.91E-01 2.5 1.86E-01 6.74E-02 1.23E-01 1.77E-01 9.27E-03 7.94E-02 1.69E-01 0.00E+00 5.24E-02 2.40E-01 3.64E-02 2.48E-01 2.5 6.32E-02 0.00E+00 1.81E-01 9.57E-02 6.95E-02 6.43E-02 1.45E-01 1.09E-01 6.77E-02 0.00E+00 1.43E-01 1.58E-01 3 1.38E-01 8.38E-02 1.52E-01 1.21E-02 1.69E-01 5.79E-02 1.06E-01 3.31E-02 0.00E+00 9.19E-02 0.00E+00 0.00E+00 3 6.63E-02 1.96E-03 9.58E-02 7.76E-02 1.10E-01 2.78E-03 7.20E-02 0.00E+00 4.35E-02 8.95E-02 0.00E+00 1.28E-01 3.5 0.00E+00 1.10E-01 1.41E-02 1.70E-02 3.40E-02 0.00E+00 6.59E-02 2.75E-03 0.00E+00 1.40E-02 2.54E-02 1.90E-01 3.5 5.94E-03 1.19E-01 9.02E-02 7.72E-02 0.00E+00 1.17E-01 2.92E-02 0.00E+00 4.11E-02 5.60E-02 5.55E-02 6.61E-02 4 0.00E+00 4.72E-02 0.00E+00 1.51E-01 3.28E-02 0.00E+00 7.63E-02 9.91E-02 1.08E-01 7.17E-02 0.00E+00 0.00E+00 4 6.76E-02 7.02E-02 7.84E-02 9.01E-02 3.80E-02 1.26E-01 1.22E-01 3.24E-02 1.43E-02 1.19E-01 1.52E-02 0.00E+00 4.5 4.50E-02 0.00E+00 1.25E-01 6.52E-02 5.35E-02 1.17E-01 1.73E-01 5.74E-02 1.78E-01 1.72E-01 1.44E-01 1.17E-01 4.5 1.74E-01 1.09E-01 1.96E-01 7.71E-02 4.24E-02 1.70E-01 9.93E-02 7.38E-02 3.63E-02 1.46E-01 0.00E+00 2.51E-01 5 1.38E-01 4.08E-02 1.73E-01 9.00E-02 8.03E-03 6.61E-02 8.64E-02 4.23E-02 6.46E-02 0.00E+00 2.05E-02 6.40E-02 5 1.08E-01 4.19E-02 1.64E-01 7.31E-03 0.00E+00 4.88E-02 0.00E+00 0.00E+00 6.71E-02 4.77E-02 4.81E-02 0.00E+00 5.5 1.85E-01 0.00E+00 3.92E-01 0.00E+00 0.00E+00 1.52E-01 7.82E-02 1.08E-01 1.14E-02 9.54E-02 0.00E+00 5.01E-02 5.5 5.26E-02 4.80E-02 1.27E-01 0.00E+00 0.00E+00 1.14E-01 4.49E-02 0.00E+00 0.00E+00 6 3.50E-02 3.75E-03 3.89E-01 0.00E+00 0.00E+00 1.10E-01 1.85E-02 3.21E-02 8.17E-02 6 1.39E-03 7.60E-02 1.44E-01 1.06E-01 3.91E-02 1.37E-01 6.5 1.25E-01 7.30E-02 0.00E+00 7.74E-02 1.01E-02 1.71E-01 6.5 0.00E+00 9.74E-02 0.00E+00 8.58E-02 0.00E+00 1.03E-01 7 0.00E+00 0.00E+00 2.25E-02 1.50E-01 5.89E-02 7.99E-02 (1) Bold values indicate concentration greater than MDC. Italicized values indicate MDC value.

[21]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 3 (continued) - Summary of Auxiliary Building Continuing Characterization Concrete Core Samples (2017) - On-Site Analysis (1)

B1-05105C-JFC-005-CV B1-05105C-JFC-006-CV B1-05105C-JWC-007-CV B1-05105C-JWC-008-CV (542 foot U1 HPT) (542 foot U1 HPT) (542 foot U1 HPT) (542 foot U1 HPT)

Depth Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 (in) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) 0 2.08E+00 1.48E+00 9.06E+02 1.48E+00 1.09E-02 4.82E+02 1.31E-01 4.46E-03 5.29E-02 9.99E-01 1.19E-01 4.31E+00 0.5 1.90E+00 4.45E-01 6.95E+02 8.65E-01 3.49E-01 4.54E+02 1.86E-02 6.64E-02 7.18E-02 7.40E-01 0.00E+00 3.07E+00 0.5 6.49E-02 0.00E+00 1.53E+01 6.11E-02 0.00E+00 3.63E+00 0.00E+00 2.96E-02 2.27E-02 1.12E-01 0.00E+00 1.73E-02 1 1.72E-01 1.99E-01 1.17E+01 6.95E-02 7.74E-02 3.14E+00 1.98E-02 8.62E-02 0.00E+00 2.09E-02 2.05E-02 0.00E+00 1 4.66E-03 0.00E+00 2.19E-01 8.42E-02 0.00E+00 1.41E+00 5.91E-02 1.25E-01 0.00E+00 2.51E-02 7.14E-02 0.00E+00 1.5 9.33E-02 0.00E+00 1.99E-01 3.29E-03 9.91E-02 1.18E+00 0.00E+00 9.32E-02 6.54E-02 6.09E-02 5.64E-02 5.39E-02 1.5 0.00E+00 1.25E-01 1.93E-01 5.52E-02 0.00E+00 4.33E-01 1.10E-01 8.07E-03 0.00E+00 4.22E-02 5.32E-02 0.00E+00 2 7.48E-02 0.00E+00 7.33E-02 4.26E-03 3.76E-02 4.91E-01 0.00E+00 8.40E-02 0.00E+00 7.93E-02 4.04E-02 4.34E-02 2 9.07E-02 0.00E+00 2.78E-02 1.43E-02 4.59E-02 1.55E-01 9.81E-02 4.74E-02 0.00E+00 3.71E-02 8.01E-02 1.72E-01 2.5 5.18E-02 1.24E-02 0.00E+00 1.37E-01 8.99E-02 2.34E-01 4.49E-02 4.29E-02 1.74E-01 4.02E-02 0.00E+00 5.20E-02 2.5 6.97E-02 4.07E-03 4.04E-02 2.26E-02 0.00E+00 3.93E-01 9.73E-02 9.38E-02 0.00E+00 4.82E-02 6.24E-02 0.00E+00 3 3.85E-02 3.99E-02 1.67E-02 2.43E-02 5.66E-02 3.81E-01 4.29E-02 1.09E-01 1.52E-01 1.13E-01 1.17E-02 2.85E-02 3 6.06E-02 6.02E-02 8.84E-02 4.30E-02 0.00E+00 3.20E-01 6.94E-02 3.97E-02 1.80E-01 0.00E+00 4.53E-02 0.00E+00 3.5 1.51E-01 1.52E-01 1.41E-01 1.28E-01 1.07E-01 1.59E-01 9.48E-02 4.57E-01 6.50E-02 3.13E-02 1.16E-01 1.10E-01 3.5 1.42E-01 0.00E+00 1.86E-02 7.42E-02 3.45E-02 1.53E-01 2.73E-03 0.00E+00 2.48E-01 8.54E-02 3.03E-02 6.71E-02 4 4.24E-02 0.00E+00 0.00E+00 4.10E-02 0.00E+00 1.47E-01 1.31E-01 1.59E-01 2.17E-01 7.74E-02 7.97E-02 6.29E-02 4 3.02E-02 0.00E+00 4.27E-02 6.72E-02 0.00E+00 2.36E-01 1.85E-02 0.00E+00 0.00E+00 7.06E-03 3.73E-02 9.60E-02 4.5 8.49E-03 0.00E+00 0.00E+00 8.98E-02 5.20E-02 2.10E-01 1.77E-01 4.73E-02 1.57E-01 6.41E-02 1.55E-01 5.29E-02 4.5 2.25E-02 0.00E+00 0.00E+00 1.77E-01 8.71E-02 2.19E-01 1.09E-01 1.34E-01 9.14E-02 0.00E+00 0.00E+00 3.72E-03 5 0.00E+00 4.47E-02 1.09E-02 6.32E-02 1.21E-01 1.76E-01 5.09E-02 8.05E-02 9.22E-03 2.25E-02 0.00E+00 1.67E-01 5 1.44E-02 0.00E+00 4.36E-02 4.54E-02 2.61E-02 2.85E-01 7.98E-02 5.81E-02 2.16E-01 6.81E-02 2.66E-02 6.17E-02 5.5 5.50E-02 0.00E+00 9.01E-03 3.44E-02 0.00E+00 2.83E-01 1.20E-01 4.99E-02 0.00E+00 0.00E+00 8.11E-02 0.00E+00 5.5 1.18E-02 0.00E+00 9.37E-01 0.00E+00 1.91E-02 2.27E-02 6 0.00E+00 0.00E+00 1.00E+00 6.28E-02 9.64E-02 0.00E+00 6 6.57E-02 6.72E-03 8.72E+01 8.39E-01 8.93E-02 1.91E+00 6.5 4.38E-02 0.00E+00 1.79E+02 1.52E+00 6.67E-02 5.29E-02 6.5 7

(1) Bold values indicate concentration greater than MDC. Italicized values indicate MDC value.

[22]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 3 (continued) - Summary of Auxiliary Building Continuing Characterization Concrete Core Samples (2017) - On-Site Analysis (1)

B1-05106C-JFC-001-CV B1-05106C-JFC-002-CV B1-05106C-JFC-003-CV B1-05106C-JFC-004-CV (542 foot U2 HPT) (542 foot U2 HPT) (542 foot U2 HPT) (542 foot U2 HPT)

Depth Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 (in) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) 0 5.03E-02 0.00E+00 6.92E-01 6.02E-01 9.53E-02 8.85E+00 2.84E+01 4.39E-01 1.25E+03 2.36E+01 2.13E-02 1.01E+03 0.5 1.22E-01 1.47E-01 5.17E-01 5.07E-01 1.90E-02 5.94E+00 1.61E+01 1.12E-01 6.09E+02 1.54E+01 1.64E-01 6.09E+02 0.5 1.31E-01 0.00E+00 1.69E-01 1.96E-01 7.38E-02 3.98E-01 2.76E-01 2.28E-02 4.70E-01 5.27E-01 0.00E+00 1.04E+01 1 0.00E+00 1.65E-01 3.33E-01 2.01E-01 7.56E-02 3.58E-01 1.73E-01 1.76E-02 5.90E-01 5.08E-01 0.00E+00 8.97E+00 1 7.98E-02 9.99E-02 4.27E-01 0.00E+00 1.68E-01 1.78E-01 1.37E-01 3.96E-02 3.60E-01 3.87E-01 3.18E-02 6.76E+00 1.5 2.85E-02 9.17E-02 4.39E-01 1.95E-01 0.00E+00 1.53E-01 5.61E-02 0.00E+00 3.22E-01 5.37E-01 9.47E-02 6.53E+00 1.5 3.07E-02 0.00E+00 1.83E-01 5.59E-02 0.00E+00 2.15E-01 7.79E-02 0.00E+00 6.35E-02 1.74E+00 0.00E+00 2.81E+00 2 4.62E-02 2.20E-01 2.65E-01 6.38E-02 0.00E+00 3.58E-01 1.32E-01 0.00E+00 4.63E-02 2.37E-01 0.00E+00 2.55E+00 2 7.98E-02 0.00E+00 1.66E-01 7.48E-02 1.55E-01 1.55E-01 9.73E-02 8.10E-02 2.73E-01 2.29E-01 0.00E+00 8.22E-01 2.5 1.92E-01 0.00E+00 1.07E-02 1.46E-01 0.00E+00 2.18E-01 3.45E-02 8.22E-02 1.00E-01 1.76E-01 9.11E-02 6.38E-01 2.5 7.23E-02 0.00E+00 3.42E-01 8.28E-02 5.62E-02 2.74E-01 1.98E-01 2.05E-02 9.23E-02 1.07E-01 6.80E-03 1.62E-01 3 4.71E-02 5.77E-02 2.98E-01 1.18E-01 8.63E-03 0.00E+00 5.62E-02 0.00E+00 2.30E-01 7.88E-02 0.00E+00 1.44E-01 3 3.85E-02 2.26E-02 1.15E-01 1.11E-01 0.00E+00 1.13E-01 6.79E-02 2.91E-02 0.00E+00 4.17E-02 5.81E-02 1.30E-01 3.5 1.60E-02 2.22E-02 2.26E-01 1.35E-01 0.00E+00 1.03E-01 0.00E+00 0.00E+00 2.41E-02 1.11E-01 0.00E+00 0.00E+00 3.5 7.91E-03 0.00E+00 1.76E-01 1.68E-01 0.00E+00 1.03E-01 5.01E-02 2.18E-01 1.48E-01 9.53E-02 0.00E+00 1.17E-01 4 1.09E-01 9.82E-02 2.18E-01 9.66E-02 1.93E-02 2.27E-01 0.00E+00 1.85E-01 9.40E-02 1.54E-01 0.00E+00 1.14E-01 4 1.46E-02 0.00E+00 4.44E-01 8.47E-02 4.75E-02 3.15E-02 2.75E-02 3.33E-04 1.05E-01 9.44E-03 7.48E-02 1.76E-01 4.5 6.96E-02 2.84E-02 3.69E-01 8.46E-03 4.86E-02 0.00E+00 2.19E-02 6.02E-02 1.56E-01 6.04E-03 5.36E-02 2.08E-02 4.5 6.01E-03 1.51E-01 1.23E-01 6.98E-02 0.00E+00 3.16E-02 4.59E-02 0.00E+00 5.06E-02 4.94E-02 0.00E+00 0.00E+00 5 1.65E-01 1.51E-01 1.63E-01 1.91E-01 0.00E+00 9.85E-02 5.82E-02 0.00E+00 7.03E-02 1.70E-02 0.00E+00 2.23E-02 5 9.35E-02 1.20E-02 9.71E-02 0.00E+00 1.70E-02 1.66E-01 6.11E-02 0.00E+00 6.87E-02 7.43E-02 0.00E+00 6.14E-03 5.5 6.68E-02 0.00E+00 9.56E-02 2.79E-02 0.00E+00 7.39E-02 3.67E-02 0.00E+00 2.92E-02 8.92E-02 1.18E-01 1.73E-01 5.5 2.06E-02 0.00E+00 2.60E-01 1.07E-01 2.73E-01 2.36E-01 5.50E-02 0.00E+00 1.71E-02 1.56E-02 0.00E+00 1.42E-01 6 1.63E-03 2.99E-02 1.84E-01 1.65E-02 1.52E-01 6.63E-02 0.00E+00 0.00E+00 1.26E-02 8.66E-02 1.11E-02 1.45E-01 6 8.79E-02 6.38E-02 2.07E-01 2.46E-02 0.00E+00 4.82E-02 6.5 1.06E-01 0.00E+00 1.27E-01 1.16E-01 0.00E+00 1.00E-01 6.5 2.40E-01 0.00E+00 1.52E+00 6.12E-02 5.78E-03 1.08E-01 7 2.00E-01 4.36E-02 1.20E+00 0.00E+00 8.26E-03 2.65E-01 (1) Bold values indicate concentration greater than MDC. Italicized values indicate MDC value.

[23]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 3 (continued) - Summary of Auxiliary Building Continuing Characterization Concrete Core Samples (2017) - On-Site Analysis (1)

B1-05106C-JWC-005-CV B1-05106C-JWC-006-CV B1-05106C-JWC-007-CV B1-05106C-JWC-008-CV (542 foot U2 HPT) (542 foot U2 HPT) (542 foot U2 HPT) (542 foot U2 HPT)

Depth Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 (in) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) 0 5.86E-01 0.00E+00 2.90E+00 3.25E-01 1.14E-01 9.83E-01 2.47E+01 3.67E-01 1.83E+02 2.28E+00 1.11E-01 1.52E+01 0.5 3.45E-01 0.00E+00 1.87E+00 1.60E-01 6.01E-02 6.94E-01 1.77E+01 2.10E-01 1.18E+02 1.51E+00 9.69E-02 8.15E+00 0.5 1.47E-01 2.21E-02 1.07E-01 1.15E-01 1.36E-01 8.83E-02 2.53E-01 1.71E-01 2.27E-01 1.07E-01 0.00E+00 1.15E-01 1 1.74E-01 0.00E+00 2.04E-03 1.63E-02 3.93E-02 4.38E-03 1.21E-01 1.41E-02 9.88E-02 1.58E-01 0.00E+00 1.18E-01 1 0.00E+00 5.70E-02 8.92E-02 8.27E-02 6.13E-02 0.00E+00 7.21E-02 4.61E-04 2.20E-01 4.51E-02 8.07E-02 1.12E-01 1.5 1.26E-01 8.64E-02 3.95E-02 6.22E-02 0.00E+00 2.60E-01 1.11E-01 0.00E+00 1.98E-01 1.45E-01 0.00E+00 9.95E-02 1.5 9.62E-02 1.14E-01 1.27E-01 4.63E-02 1.87E-01 1.52E-01 7.04E-02 0.00E+00 2.09E-01 3.03E-02 0.00E+00 9.35E-02 2 9.62E-02 7.57E-02 1.10E-01 1.16E-01 8.70E-02 1.06E-01 6.24E-02 1.75E-01 1.73E-01 7.41E-02 1.31E-02 6.67E-02 2 1.40E-01 1.13E-02 1.03E-01 1.48E-01 0.00E+00 1.35E-01 4.39E-02 0.00E+00 1.94E-01 6.43E-02 7.32E-02 8.46E-02 2.5 1.36E-01 0.00E+00 7.78E-02 1.31E-01 1.15E-03 1.72E-01 8.75E-02 3.75E-02 2.37E-01 0.00E+00 0.00E+00 1.03E-01 2.5 6.58E-02 3.04E-02 3.60E-02 1.03E-01 6.00E-02 1.17E-01 3.91E-02 6.80E-03 7.86E-03 1.32E-01 5.66E-02 2.34E-01 3 1.30E-02 3.98E-02 1.60E-01 1.72E-01 0.00E+00 1.90E-01 1.03E-01 5.16E-02 1.70E-01 1.14E-01 5.99E-03 1.30E-01 3 5.24E-02 0.00E+00 0.00E+00 5.03E-02 4.18E-02 1.94E-01 7.34E-02 9.22E-02 2.35E-01 1.56E-01 3.13E-02 1.59E-02 3.5 2.10E-02 2.65E-02 6.43E-02 8.56E-02 0.00E+00 1.94E-01 1.23E-01 4.61E-02 2.19E-01 3.72E-02 2.91E-02 2.19E-02 3.5 4.21E-02 5.84E-02 6.64E-02 9.82E-02 5.84E-02 0.00E+00 9.24E-02 1.68E-01 1.62E-01 1.39E-01 0.00E+00 1.41E-01 4 9.54E-02 0.00E+00 6.23E-02 3.25E-02 4.85E-02 1.53E-01 8.70E-02 2.03E-02 1.34E-01 8.55E-02 8.34E-02 0.00E+00 4 5.50E-02 2.12E-02 1.58E-01 0.00E+00 0.00E+00 0.00E+00 2.34E-02 1.64E-01 2.38E-01 0.00E+00 1.40E-01 1.57E-02 4.5 1.61E-01 0.00E+00 3.17E-02 2.11E-02 1.02E-01 8.96E-02 1.12E-01 1.04E-01 9.57E-02 5.47E-02 0.00E+00 7.45E-03 4.5 2.68E-02 0.00E+00 0.00E+00 6.72E-02 3.41E-02 2.33E-01 1.51E-01 8.68E-02 1.43E-01 0.00E+00 0.00E+00 3.48E-02 5 8.05E-03 7.66E-02 0.00E+00 2.03E-01 1.58E-01 1.55E-01 1.66E-01 1.22E-01 1.50E-01 1.78E-01 1.99E-01 0.00E+00 5 7.09E-02 5.49E-02 3.82E-02 1.96E-01 1.96E-01 1.58E-01 1.17E-01 0.00E+00 2.91E-01 1.02E-01 0.00E+00 9.94E-02 5.5 9.19E-02 4.68E-02 9.19E-02 1.81E-01 2.97E-03 2.47E-01 8.34E-02 9.92E-03 3.26E-01 1.02E-01 1.90E-01 1.23E-01 5.5 6

6 6.5 6.5 7

(1) Bold values indicate concentration greater than MDC. Italicized values indicate MDC value.

[24]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 3 (continued) - Summary of Auxiliary Building Continuing Characterization Concrete Core Samples (2017) - On-Site Analysis (1)

B1-05107C-JFC-001-CV B1-05107C-JFC-002-CV B1-05107C-JFC-003-CV B1-05107C-JFC-004-CV (542 foot HUT) (542 foot HUT) (542 foot HUT) (542 foot HUT)

Depth Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 (in) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) 0 2.22E+01 1.81E-01 1.18E+03 1.07E+00 2.60E-02 1.83E+01 2.61E+01 2.52E-01 2.02E+02 3.44E+00 0.00E+00 2.55E+02 0.5 2.43E+01 3.09E-01 1.41E+03 5.97E-01 7.20E-03 7.71E+00 1.86E+01 2.40E-01 1.26E+02 2.64E+00 1.44E-01 1.38E+02 0.5 1.16E+01 2.52E-01 5.82E+02 2.25E-03 1.16E-01 6.49E-02 0.00E+00 1.13E-01 2.63E-01 4.92E-01 1.01E-02 8.26E-01 1 1.00E+01 1.95E-01 5.19E+02 8.65E-02 2.76E-02 2.55E-03 5.31E-02 0.00E+00 1.70E-01 4.53E-01 6.91E-02 5.45E-01 1 4.56E+00 0.00E+00 8.27E+01 1.26E-01 0.00E+00 0.00E+00 9.93E-02 6.73E-02 2.04E-01 1.87E-01 1.62E-01 6.37E-02 1.5 4.04E+00 5.22E-02 6.84E+01 3.29E-02 0.00E+00 8.93E-02 0.00E+00 1.26E-01 1.20E-01 2.38E-01 1.59E-02 9.56E-02 1.5 2.95E+00 0.00E+00 3.13E+01 7.40E-02 0.00E+00 0.00E+00 4.46E-02 0.00E+00 1.61E-01 2.37E-02 6.44E-02 5.76E-02 2 2.51E+00 2.79E-01 2.47E+01 1.15E-01 1.08E-01 1.70E-01 3.88E-02 0.00E+00 1.67E-01 9.14E-02 4.13E-02 9.69E-02 2 1.58E+00 0.00E+00 1.09E+01 1.16E-01 5.75E-02 1.13E-01 3.01E-02 3.16E-02 2.31E-01 6.56E-02 1.63E-02 1.66E-01 2.5 1.49E+00 1.74E-01 1.14E+01 0.00E+00 0.00E+00 1.02E-01 1.59E-01 0.00E+00 1.90E-01 1.43E-01 6.84E-02 1.33E-01 2.5 1.32E+00 1.10E-01 9.13E+00 1.20E-01 0.00E+00 4.99E-02 9.55E-02 8.96E-02 1.34E-01 1.74E-01 1.64E-01 2.71E-01 3 1.24E+00 4.33E-02 9.85E+00 0.00E+00 1.30E-02 6.42E-02 1.16E-01 0.00E+00 1.18E-01 1.59E-01 6.27E-02 9.70E-02 3 7.37E-01 8.93E-03 7.42E+00 6.55E-02 0.00E+00 8.34E-02 1.71E-02 0.00E+00 4.40E-02 7.88E-02 7.90E-03 9.80E-02 3.5 8.46E-01 2.57E-02 6.43E+00 9.30E-03 9.36E-02 5.72E-02 7.25E-02 0.00E+00 1.69E-01 9.61E-02 9.91E-03 9.85E-03 3.5 4.50E-01 8.63E-02 5.60E+00 6.74E-02 7.92E-02 0.00E+00 6.57E-02 3.96E-02 1.92E-01 1.43E-02 6.16E-02 4.53E-02 4 5.24E-01 4.39E-02 6.08E+00 4.90E-02 1.56E-01 6.21E-02 5.76E-04 9.89E-02 1.32E-01 9.65E-02 0.00E+00 0.00E+00 4 7.40E-01 1.29E-02 6.27E+00 1.04E-01 2.26E-03 1.20E-01 1.07E-01 1.11E-03 2.66E-02 1.18E-01 1.35E-01 0.00E+00 4.5 8.25E-02 1.14E-02 1.13E-01 6.40E-02 1.39E-02 1.60E-01 7.99E-02 1.18E-01 2.14E-01 4.5 4.08E-03 1.30E-01 1.89E-01 1.67E-01 4.78E-02 1.32E-01 7.42E-02 0.00E+00 2.61E-02 5 6.04E-01 1.89E-02 5.30E+00 6.99E-02 1.40E-02 0.00E+00 4.15E-02 0.00E+00 1.45E-01 4.52E-02 0.00E+00 0.00E+00 5 2.51E-01 8.88E-02 2.12E+00 3.49E-02 8.78E-02 3.66E-02 8.07E-02 7.38E-02 1.41E-01 4.10E-02 2.96E-02 1.17E-01 5.5 3.72E-01 6.98E-02 2.04E+00 1.07E-01 1.20E-01 0.00E+00 6.72E-02 0.00E+00 2.11E-01 6.84E-02 2.32E-03 4.37E-02 5.5 2.03E-01 0.00E+00 9.12E-01 0.00E+00 1.10E-01 1.34E-01 2.98E-02 9.90E-02 3.27E-02 6 1.41E-02 4.42E-02 7.58E-01 4.27E-03 4.31E-03 1.20E-01 4.38E-02 1.46E-01 1.19E-01 6 2.35E-02 0.00E+00 1.23E-01 6.5 1.51E-02 5.20E-02 8.39E-02 6.5 7

(1) Bold values indicate concentration greater than MDC. Italicized values indicate MDC value.

[25]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 3 (continued) - Summary of Auxiliary Building Continuing Characterization Concrete Core Samples (2017) - On-Site Analysis (1)

B1-05107C-JWC-005-CV B1-05107C-JWC-006-CV B1-05107C-JWC-007-CV B1-05107C-JWC-008-CV (542 foot HUT) (542 foot HUT) (542 foot HUT) (542 foot HUT)

Depth Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 (in) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) 0 4.74E-01 4.52E-01 2.43E+03 2.86E+01 1.80E+00 1.36E+04 1.84E+01 4.48E-01 3.79E+02 2.56E+00 0.00E+00 1.14E+04 0.5 4.84E-01 5.05E-01 1.67E+03 2.11E+01 3.72E+00 1.24E+04 1.44E+01 6.94E-01 2.86E+02 1.46E+00 0.00E+00 7.97E+03 0.5 1.34E-01 3.77E-02 8.67E-01 3.69E-02 9.06E-02 1.64E+03 1.48E+00 8.30E-02 2.77E+01 3.17E-01 1.62E-01 2.02E+03 1 2.01E-01 1.23E-01 7.04E-01 7.93E-01 8.03E-02 6.11E+03 1.67E+00 2.37E-02 2.39E+01 2.89E-01 5.12E-01 1.79E+03 1 2.48E-02 6.59E-02 8.90E-01 1.37E-01 9.62E-02 3.06E+03 1.46E+00 1.57E-02 2.23E+01 2.51E-01 1.81E-01 7.60E+02 1.5 1.31E-01 5.84E-02 5.40E-01 1.87E-01 2.72E-02 8.03E+02 1.21E+00 0.00E+00 1.78E+01 5.68E-02 1.40E-01 8.87E+02 1.5 1.47E-03 1.24E-04 9.19E-01 1.28E-01 0.00E+00 2.60E+02 9.70E-01 0.00E+00 4.16E+00 4.19E-02 3.17E-03 3.01E+02 2 1.08E+00 6.99E-02 1.08E+00 1.12E-01 4.06E-01 1.79E+02 7.81E-01 2.73E-01 3.98E+00 1.15E-01 0.00E+00 3.42E+02 2 7.68E-02 2.40E-02 5.22E-01 2.39E-01 0.00E+00 2.82E+01 2.45E-01 3.16E-02 8.60E-01 1.17E-01 1.04E-02 9.89E+01 2.5 1.11E-01 5.70E-02 5.48E-01 2.05E-01 1.82E-02 2.52E+01 2.47E-01 1.78E-02 2.32E-01 4.06E-02 0.00E+00 7.46E+01 2.5 1.21E-01 1.40E-02 3.44E-01 1.74E-01 2.67E-01 1.12E+01 3.75E-01 1.66E-01 2.53E-01 2.08E-02 8.68E-02 6.84E-01 3 7.30E-02 2.38E-03 3.36E-01 1.17E-01 0.00E+00 8.30E+00 5.36E-01 2.35E-01 2.15E-01 1.04E-01 8.72E-02 7.15E-01 3 3.64E-02 3.67E-02 5.13E-01 4.04E-02 0.00E+00 1.59E+00 1.88E-01 7.32E-02 1.52E-01 9.61E-02 8.04E-02 1.23E+00 3.5 3.40E-02 0.00E+00 3.52E-01 4.96E-02 3.90E-02 1.80E-01 8.41E-02 1.10E-01 5.91E-01 3.5 1.31E-01 2.61E-02 6.51E-01 1.46E-01 0.00E+00 1.29E-01 1.25E-02 0.00E+00 2.59E-01 4 0.00E+00 1.23E-01 3.73E-01 3.26E-02 0.00E+00 7.20E-01 0.00E+00 0.00E+00 1.54E-01 2.39E-02 0.00E+00 1.93E-01 4 6.22E-02 1.79E-02 6.96E-01 4.85E-02 0.00E+00 4.91E-01 1.01E-01 4.39E-02 1.82E-01 1.84E-01 4.36E-02 5.69E-01 4.5 1.22E-01 0.00E+00 5.54E-01 7.02E-02 0.00E+00 5.90E-01 1.75E-01 1.22E-02 1.61E-01 5.81E-02 2.26E-02 7.31E-01 4.5 7.46E-02 2.87E-02 0.00E+00 8.33E-02 7.48E-03 2.73E-01 6.30E-02 5.15E-02 1.09E-01 1.24E-01 0.00E+00 4.15E-01 5 6.44E-03 4.25E-02 3.43E-02 1.20E-01 0.00E+00 2.13E-01 8.05E-02 3.75E-02 1.35E-01 5.53E-02 1.09E-01 4.31E-01 5 9.50E-02 0.00E+00 1.80E-01 1.34E-01 0.00E+00 1.95E-01 1.16E-01 0.00E+00 0.00E+00 3.38E-02 0.00E+00 2.32E-01 5.5 8.32E-02 0.00E+00 1.62E-01 1.63E-02 7.46E-02 2.21E-01 1.33E-01 0.00E+00 9.93E-02 0.00E+00 1.11E-01 2.04E-01 5.5 6.72E-02 7.53E-03 8.71E-02 4.95E-02 1.41E-02 5.29E-01 5.80E-02 0.00E+00 9.18E-02 8.11E-02 4.37E-02 1.61E-01 6 1.16E-02 2.26E-01 2.47E-02 9.01E-02 1.26E-02 5.07E-01 1.05E-01 5.10E-03 1.89E-01 7.71E-02 3.35E-02 1.69E-01 6 1.62E-01 4.54E-02 1.67E-01 1.24E-01 0.00E+00 1.61E-01 1.30E-02 5.39E-03 1.25E-01 2.19E-02 7.36E-03 1.77E-01 6.5 7.35E-03 0.00E+00 0.00E+00 4.40E-02 9.35E-02 2.00E-01 4.31E-02 2.98E-02 3.46E-02 4.23E-02 1.77E-02 3.41E-01 6.5 3.02E-03 1.16E-02 8.90E-02 8.71E-02 4.53E-02 8.62E-01 1.84E+01 4.48E-01 3.79E+02 1.09E-01 1.28E-01 2.45E-01 7 1.59E-01 4.33E-02 1.33E-01 5.05E-02 8.64E-03 8.66E-01 1.44E+01 6.94E-01 2.86E+02 6.56E-02 0.00E+00 1.75E-01 7 3.09E-02 3.24E-03 2.40E-01 1.18E-01 5.88E-02 2.43E-02 3.78E-02 4.04E-02 1.64E-01 7.5 1.08E-01 0.00E+00 6.32E-02 3.02E-02 9.40E-03 3.45E-01 8.01E-02 8.93E-02 1.70E-01 (1) Bold values indicate concentration greater than MDC. Italicized values indicate MDC value.

[26]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 3 (continued) - Summary of Auxiliary Building Continuing Characterization Concrete Core Samples (2017) - On-Site Analysis (1)

B1-05100C-JFC-001-CV B1-05100C-JFC-002-CV B1-05100C-JFC-003-CV B1-05100C-JFC-004-CV (542 foot Floor) (542 foot Floor) (542 foot Floor) (542 foot Floor)

Depth Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 (in) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) 0 6.88E+00 0.00E+00 1.02E+03 4.35E+00 1.89E-01 8.63E+01 2.33E+01 3.89E-01 2.12E+03 1.11E+01 0.00E+00 3.12E+01 0.5 8.17E+00 2.08E-01 1.10E+03 4.02E+00 1.99E-01 4.39E+01 2.81E+01 2.23E-01 2.52E+03 1.02E+01 1.31E-01 2.17E+01 0.5 7.87E+00 2.90E-01 5.31E+02 1.13E-01 0.00E+00 5.44E-01 9.65E+00 2.07E-01 3.64E+02 2.17E+00 1.16E-03 2.03E+00 1 7.04E+00 9.82E-02 4.41E+02 9.23E-03 1.41E-01 5.48E-01 1.11E+01 1.35E-01 4.45E+02 2.48E+00 1.70E-01 2.60E+00 1 3.21E+00 2.75E-01 1.38E+02 7.75E-02 0.00E+00 4.34E-01 4.59E+00 3.38E-01 2.67E+02 1.07E+00 3.73E-02 2.46E+00 1.5 3.07E+00 1.94E-01 1.57E+02 4.44E-01 0.00E+00 4.44E-01 9.35E+00 5.39E-02 5.42E+02 8.64E-01 0.00E+00 1.98E+00 1.5 2.82E-01 0.00E+00 1.24E+01 5.01E-02 1.42E-02 2.29E-01 5.30E-01 3.41E-01 2.50E+01 1.33E-01 0.00E+00 1.14E+00 2 3.60E-01 0.00E+00 1.89E+01 2.45E-02 1.83E-03 2.05E-01 8.24E-01 5.39E-02 3.25E+01 9.48E-02 0.00E+00 1.21E+00 2 8.52E-01 0.00E+00 4.91E+01 1.76E-01 0.00E+00 2.58E-01 1.65E+00 0.00E+00 6.81E+01 2.04E-01 2.04E-01 1.87E+00 2.5 6.40E-01 2.16E-02 3.64E+01 1.89E-01 2.54E-02 1.32E-01 1.43E+00 0.00E+00 5.56E+01 3.32E-01 0.00E+00 1.83E+00 2.5 1.68E-02 5.44E-02 3.76E-01 5.47E-02 5.78E-02 3.08E-01 6.81E+00 4.61E-01 1.57E+02 1.10E-01 5.04E-02 9.25E-01 3 1.62E-01 3.86E-03 2.63E-01 0.00E+00 1.55E-01 2.08E-01 9.14E+00 1.46E-02 2.00E+02 1.09E-01 2.60E-02 7.33E-01 3 2.49E-02 5.32E-02 5.97E-02 9.28E-02 0.00E+00 3.33E-01 1.12E+01 6.51E-02 1.48E+02 8.66E-02 0.00E+00 1.16E-01 3.5 6.85E-02 7.79E-03 1.50E-01 1.86E-02 0.00E+00 3.65E-01 1.00E+01 2.35E-01 1.36E+02 4.06E-02 0.00E+00 2.13E-01 3.5 0.00E+00 1.42E-02 5.74E-02 6.11E-02 1.51E-02 2.31E-01 5.93E+00 0.00E+00 9.51E+01 1.62E-02 5.08E-02 6.86E-02 4 3.89E-02 5.17E-02 1.21E-01 1.04E-01 6.89E-02 2.65E-01 5.23E+00 5.84E-01 7.06E+01 0.00E+00 0.00E+00 4.94E-02 4 1.47E-01 4.17E-02 2.45E-02 1.95E-02 0.00E+00 2.31E-01 2.03E+00 8.95E-03 2.27E+01 2.53E-01 0.00E+00 3.67E+00 4.5 8.77E-02 7.23E-02 1.25E-01 3.17E-02 1.18E-01 2.84E-01 1.44E+00 7.31E-02 1.97E+01 2.87E-01 2.72E-02 4.74E+00 4.5 1.02E-01 3.68E-02 1.18E-01 5.78E+01 0.00E+00 3.83E+02 1.14E-01 9.99E-03 4.00E+00 3.27E+00 2.04E-01 1.06E+01 5 6.99E-02 5.83E-02 1.19E-01 5.73E+01 7.50E-01 3.75E+02 4.88E-02 0.00E+00 6.27E+00 1.84E+00 0.00E+00 7.26E+00 5 4.36E-02 1.59E-01 2.78E-03 1.83E-01 0.00E+00 1.65E+01 1.14E-01 1.30E-01 2.45E+00 5.81E-02 1.02E-01 6.96E-01 5.5 0.00E+00 9.21E-03 5.84E-02 2.69E-01 1.08E-01 1.65E+01 5.68E-02 8.38E-03 3.21E+00 0.00E+00 3.10E-02 6.44E-01 5.5 4.72E-02 7.32E-02 6.04E-01 1.06E-01 1.85E-03 2.92E+00 1.86E-02 1.30E-01 1.04E-01 6 1.70E-02 1.07E-01 5.87E-01 1.05E-01 2.47E-02 3.29E+00 0.00E+00 1.08E-02 8.65E-02 6 1.01E-01 7.99E-02 6.15E-01 5.04E-01 5.03E-02 1.26E+01 6.5 0.00E+00 6.07E-02 5.34E-01 4.41E-01 1.62E-02 1.04E+01 6.5 1.46E-01 0.00E+00 5.13E-01 1.05E-01 4.91E-02 5.01E+00 7 1.60E-01 0.00E+00 5.12E-01 1.70E-01 1.56E-01 5.01E+00 7 5.79E+00 1.18E-01 3.35E+02 7.5 1.15E+01 4.35E-01 7.66E+02 (1) Bold values indicate concentration greater than MDC. Italicized values indicate MDC value.

[27]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 3 (continued) - Summary of Auxiliary Building Continuing Characterization Concrete Core Samples (2017) - On-Site Analysis (1)

B1-05100C-JFC-005-CV B1-05100C-JFC-006-CV B1-05100C-JFC-007-CV B1-05100C-JFC-008-CV (542 foot Floor) (542 foot Floor) (542 foot Floor) (542 foot Floor)

Depth Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 Co-60 Cs-134 Cs-137 (in) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) 0 3.50E+00 2.28E-02 1.50E+01 9.96E-02 3.20E-02 6.15E+00 2.34E+00 1.16E-02 2.62E+01 2.55E-01 1.64E-01 2.12E+00 0.5 2.20E+00 5.40E-02 8.90E+00 8.43E-02 0.00E+00 3.52E+00 2.21E+00 1.52E-01 1.48E+01 1.37E-01 1.07E-01 1.23E+00 0.5 2.14E-01 6.02E-02 4.14E-01 0.00E+00 3.95E-02 7.92E-02 5.56E-01 4.51E-02 2.18E-01 0.00E+00 0.00E+00 7.16E-03 1 2.59E-01 6.13E-02 4.60E-01 4.94E-03 0.00E+00 0.00E+00 5.38E-01 0.00E+00 1.67E-01 9.26E-02 6.77E-02 0.00E+00 1 7.95E-01 5.58E-02 1.16E+02 4.37E-02 1.05E-01 0.00E+00 1.89E-01 0.00E+00 0.00E+00 1.40E-01 7.61E-02 7.32E-02 1.5 8.81E-01 5.31E-02 1.13E+02 4.77E-02 7.75E-02 0.00E+00 2.47E-01 0.00E+00 0.00E+00 6.36E-02 0.00E+00 9.26E-02 1.5 8.11E+00 2.91E-01 2.82E+02 0.00E+00 0.00E+00 1.57E-01 0.00E+00 0.00E+00 0.00E+00 1.99E-02 3.55E-02 5.44E-02 2 8.08E+00 0.00E+00 3.02E+02 0.00E+00 0.00E+00 1.91E-03 2.62E-02 2.09E-02 0.00E+00 1.05E-01 0.00E+00 8.17E-02 2 6.13E+00 0.00E+00 2.67E+02 3.86E-02 0.00E+00 1.49E-01 2.65E-02 1.36E-01 1.05E-01 2.12E-01 3.95E-02 1.38E-01 2.5 5.16E+00 7.04E-02 2.03E+02 1.18E-01 0.00E+00 3.34E-02 0.00E+00 8.95E-02 0.00E+00 1.02E-01 8.90E-02 0.00E+00 2.5 5.78E-01 2.30E-01 1.56E+01 4.35E-02 1.69E-01 1.36E-01 8.85E-02 1.14E-01 0.00E+00 9.99E-02 0.00E+00 9.57E-01 3 6.36E-01 4.55E-04 1.52E+01 4.35E-02 4.03E-02 8.35E-02 1.33E-01 7.09E-02 7.68E-03 1.38E-01 0.00E+00 1.21E+00 3 1.21E+00 8.83E-02 3.24E+01 7.55E-02 1.39E-01 1.70E-01 6.01E-02 0.00E+00 1.39E-01 1.80E-01 0.00E+00 7.51E-01 3.5 1.58E+00 2.14E-01 4.04E+01 3.83E-02 0.00E+00 1.47E-01 0.00E+00 0.00E+00 1.17E-01 2.67E-01 0.00E+00 6.28E-01 3.5 2.16E+00 4.87E-02 1.67E+02 0.00E+00 0.00E+00 1.89E-01 1.22E-01 2.78E-03 9.85E-02 1.95E-01 0.00E+00 2.23E-01 4 1.97E+00 4.82E-02 1.47E+02 3.77E-02 0.00E+00 1.01E-01 4.75E-04 2.18E-01 0.00E+00 7.96E-02 4.62E-02 1.20E-01 4 3.59E+00 1.78E-01 4.60E+01 4.59E-02 1.61E-02 7.20E-02 2.65E-02 5.43E-02 0.00E+00 9.72E-02 4.21E-02 7.17E-02 4.5 3.17E+00 4.76E-02 3.74E+01 5.12E-02 2.53E-02 1.11E-01 0.00E+00 1.03E-01 1.19E-01 4.90E-02 1.19E-02 1.74E-01 4.5 4.79E+00 0.00E+00 4.20E+01 1.05E-01 6.60E-03 1.08E-01 1.12E-01 2.16E-01 7.20E-02 1.35E-01 3.11E-02 6.71E-04 5 4.40E+00 9.93E-02 3.84E+01 9.23E-02 7.71E-03 0.00E+00 1.54E-01 0.00E+00 5.23E-02 7.44E-02 0.00E+00 1.39E-01 5 5.59E+00 1.85E-01 1.38E+02 1.33E-01 2.40E-02 1.52E-01 5.47E-02 1.29E-01 1.45E-02 7.43E-02 0.00E+00 0.00E+00 5.5 4.50E+00 2.30E-01 1.21E+02 0.00E+00 7.56E-02 9.78E-02 4.10E-02 2.65E-02 8.72E-02 0.00E+00 0.00E+00 1.44E-02 5.5 7.44E-02 0.00E+00 1.46E-01 0.00E+00 4.91E-02 2.83E-02 0.00E+00 2.29E-02 0.00E+00 6 1.29E-01 8.00E-03 8.66E-02 9.71E-02 0.00E+00 0.00E+00 3.91E-02 1.15E-01 3.29E-02 6 4.24E-02 0.00E+00 1.12E+00 2.76E-01 1.77E-02 9.43E-02 0.00E+00 1.61E-02 5.89E-02 6.5 3.63E-02 0.00E+00 1.14E+00 8.67E-02 8.88E-02 2.56E-01 2.20E-02 2.45E-02 5.63E-02 6.5 7

7 7.5 (1) Bold values indicate concentration greater than MDC. Italicized values indicate MDC value.

[28]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 4 - Auxiliary Building Continuing Characterization Concrete Core Samples (2017) - Eberline Laboratory Analysis (1)

B1-05105C-JFC- B1-05105C-JFC- B1-05106C-JFC- B1-05106C-JFC- B1-05107C- B1-05107C- B1-05100C-JFC- B1-05100C-JFC-Radionuclide 005-CV 006-CV 003-CV 004-CV JWC-006-CV JWC-008-CV 003-CV 005-CV (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)

H-3 5.07E+00 2.23E+01 3.86E+01 2.35E+01 9.23E+00 -7.73E+00 4.70E+01 1.22E+01 C-14 2.30E+00 1.57E-01 8.52E-01 1.60E+00 1.11E+01 2.87E+01 8.06E-01 2.04E+00 Fe-55 -9.50E-02 1.18E+01 9.84E-01 -1.79E+00 -8.22E+00 -1.27E+01 -5.92E-01 -3.74E-01 Ni-59 -1.19E+00 8.73E+00 6.32E+00 9.28E+00 1.51E+01 -8.80E+00 8.60E-01 1.76E+00 Co-60 2.45E+00 1.20E+00 3.43E-01 2.67E+01 5.53E+01 3.37E+00 1.57E+00 4.63E+00 Ni-63 3.99E+01 8.15E+01 6.88E+02 7.58E+02 2.76E+03 3.14E+02 1.80E+01 1.38E+02 Sr-90 0.00E+00 4.72E-01 1.64E-01 5.42E-01 -1.34E-01 2.57E+00 4.05E-01 8.69E-01 Nb-94 -2.65E-02 -1.24E-01 1.87E-02 1.71E-01 2.32E+00 -6.22E-02 1.25E-01 -1.02E-01 Tc-99 9.74E-01 2.86E-01 8.47E-01 1.18E+00 6.15E+00 4.02E+00 9.09E-01 6.29E-01 Ag-108m -9.28E-02 -1.73E-02 -5.39E-02 -1.95E-01 1.65E+00 -1.85E-01 -5.35E-02 -2.03E-01 Sb-125 -1.00E+00 -1.44E-01 -1.79E-02 -5.25E+00 1.25E+01 -5.38E+00 -1.27E+00 4.76E-02 Cs-134 -5.11E-01 2.62E-02 0.00E+00 -1.14E+00 3.72E+00 2.72E+00 -6.34E-01 2.84E-02 Cs-137 1.15E+03 4.52E+01 2.05E+01 1.00E+03 3.32E+04 1.56E+04 2.78E+02 1.22E+01 Pm-147 8.20E-01 9.12E-01 1.03E+00 3.22E+00 1.24E+00 2.93E+01 5.47E-01 8.61E-01 Eu-152 3.20E+00 -8.61E-01 1.55E+00 2.71E-01 -1.42E+01 5.87E+00 -1.62E-01 -5.43E-01 Eu-154 -1.92E-01 8.13E-02 5.42E-02 4.35E-01 8.60E-01 8.03E-01 5.32E-02 3.43E-01 Eu-155 -1.66E-01 2.65E-01 -5.77E-04 2.41E-01 -3.93E+00 2.23E+00 -3.52E-01 5.81E-02 Np-237 1.27E-01 -3.08E-03 2.51E-03 -3.32E-02 4.47E-02 -1.17E-01 4.13E-02 2.11E-01 Pu-238 3.64E-02 -6.34E-03 7.45E-02 1.21E-02 0.00E+00 -9.63E-02 -2.08E-02 -4.46E-04 Pu-239/240 1.65E-02 8.27E-03 -2.38E-02 1.21E-02 -4.30E-02 3.23E-01 -1.25E-02 -1.55E-02 Pu-241 -1.69E+00 2.41E+00 -4.93E+00 1.50E+00 1.49E+01 -2.23E+01 -1.22E+00 -2.06E+00 Am-241 -2.49E-02 2.07E-02 -3.53E-04 3.25E-02 2.49E-02 5.94E-02 6.37E-02 6.78E-02 Am-243 7.16E-02 4.18E-03 7.37E-02 1.67E-01 3.85E-01 2.62E-01 6.50E-02 1.59E-01 Cm-243/244 -6.54E-03 2.45E-02 -1.21E-02 -1.93E-02 4.52E-02 9.06E-02 7.68E-02 1.09E-01 (1) Bold values indicate concentration greater than MDC. Italicized values indicate MDC value.

[29]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 The results of the on-site gamma spectroscopic analysis of the 1/2-inch pucks indicated that the activity concentrations correspond to an SOF of less than 0.1 for twenty-nine (29) of the thirty-two (32) sample locations below a depth of 2 inches, illustrating that the majority of the source term was surficial and not at depth.

The FSS unit for the Auxiliary Building 542 foot elevation floor and walls was designated as Class 1, and the FSS areal coverage was set at 100% which is consistent with MARSSIM, Table 5.9.

A Radiological Engineer (RE) performed a visual inspection and walk-down of the survey unit on December 4, 2017, prior to performing FSS. The purpose of the walk-down was to assess the physical condition of the survey unit, evaluate access points and travel paths and identify potentially hazardous conditions. A final classification assessment was performed in accordance with procedure ZS-LT-300-001-002, Survey Unit Classification (Reference 9) as part of the survey design for FSS.

Based upon completion of Survey Unit Classification Basis for final classification, which included a review of the historical information, the results of the Characterization Survey data and completion of a final Survey Unit Classification Worksheet, the correct final classification of survey unit 05100 was determined to be Class 1.

4. DATA QUALITY OBJECTIVES (DQO)

Final Status Survey planning and design hinges on coherence with the Data Quality Objective (DQO) process to ensure, through compliance with explicitly defined inputs and boundaries, that the primary objective of the survey is satisfied. The DQO process is described in the ZSRP LTP in accordance with MARSSIM. The appropriate design for a given survey was developed using the DQO process as outlined in Appendix D of MARSSIM.

The DQO process incorporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline condition is technically known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis, was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would indicate that residual activity within the survey unit does not exceed the release criteria. Therefore, the survey unit would satisfy the primary objective of the FSS sample plan.

The primary objective of the FSS sample plan is to demonstrate that the level of residual radioactivity in survey unit 05100 did not exceed the release criteria specified in the LTP

[30]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).

ZionSolutions TSD 11-001, Technical Support Document for Potential Radionuclides of Concern during the Decommissioning of the Zion Station (Reference 10) established the basis for an initial suite of potential ROC for the decommissioning of the Zion Nuclear Power Station (ZNPS). LTP Chapter 2 provides detailed characterization data that described contamination levels in the basements. The survey data for basements is based on core samples obtained at biased locations with elevated contact dose rates and/or evidence of leaks/spills and analyzed for the presence of plant-derived radionuclides.

ZionSolutions TSD 14-019 evaluates the results of the concrete core analysis data from the Containments and Auxiliary Building and refines the initial suite of potential ROC by evaluating the dose significance of each radionuclide.

LTP Chapter 6, section 6.5.2 discusses the process used to derive the ROC for the decommissioning of ZNPS, including the elimination of Insignificant Contributors (IC) from the initial suite. Based upon the analysis of the mixture, it was determined that Co-60, Ni-63, Sr-90, Cs-134 and Cs-137 accounted for 99.5% of all dose in the non-activated contaminated concrete mixes.

Table 5 presents the ROC for the decommissioning of Auxiliary Building structural surfaces and the normalized mixture fractions based on the radionuclide mixture.

Table 5 - Dose Significant Radionuclides and Mixture

% of Total Activity Radionuclide (normalized)(1)(2)

Co-60 0.92 Cs-134 0.01 Cs-137 75.32 Ni-63 23.71 Sr-90 0.05 (1) Based on maximum percent of total activity from Table 20 of TSD 14-019, normalized to one for the dose significant radionuclides.

(2) Does not include dose significant radionuclides for activated concrete (H-3, Eu-152, Eu-154).

[31]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity. This is done through the development of DCGLs.

The DCGLs represent average levels of radioactivity above background levels and are presented in terms of surface or mass activity concentrations. Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for structures.

The end-state basements will be comprised of steel and/or concrete structures that will be covered by at least three feet of clean soil and physically altered to a condition where it would not realistically allow the remaining structures, if excavated, to be occupied. The exposure pathways in the BFM are associated with residual radioactivity in floors and walls that is released through leaching into water contained in the interstitial spaces of the fill material. The BFM assumes that the inventory of residual radioactivity in a given building is released either instantly or over time by diffusion, depending on whether the activity is surficial or volumetric, respectively. The activity released into the fill water will adsorb onto the clean fill, as a function of the radionuclide-specific distribution coefficients, resulting in equilibrium concentrations between the fill and the water.

Consequently, the only potential exposure pathways after backfill, assuming the as-left geometry, are associated with the residual radioactivity in the water contained in the fill.

The final outputs of the BFM are the Basement DCGLs, which are calculated using the BFM Groundwater (GW) and BFM Drilling Spoils Dose Factors. DCGLs are calculated separately for the GW and Drilling Spoils scenarios and for the summation of both scenarios. The summation DCGL is designated as the Base Case DCGL (BcDCGL) and is used during FSS to demonstrate compliance (analogous to the DCGLW as defined in MARSSIM). The BcDCGLs are radionuclide-specific concentrations that represent the 10 CFR 20.1402 dose criterion of 25 mrem/year and are calculated for each ROC and each backfilled basement. Additional information pertaining to the calculation of DCGLs for basement surfaces is provided in LTP Chapter 6, section 6.6.8.

When applied to structures, the DCGLs are expressed in units of activity per unit of area (pCi/m2). The unity rule is applied when there is more than one ROC. The measurement results for each singular ROC present in the mixture are compared against their respective DCGL to derive a dose fraction.

The BcDCGLs for the unrestricted release of the Auxiliary Building basement survey unit are provided in Table 6. The IC dose percentage of 5% was used to adjust the Auxiliary Building basement DCGLs to account for the dose from the eliminated IC radionuclides.

[32]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 6 - Base Case DCGLs for Auxiliary Building Basement Survey Unit (BcDCGLB)

LTP Chapter 5, Table 5-3 Base Case DCGL Radionuclide (pCi/m2)

Co-60 3.04E+08 Cs-134 2.11E+08 Cs-137 1.11E+08 Ni-63 1.15E+10 Sr-90 9.98E+06 Each radionuclide-specific BcDCGL is equivalent to the level of residual radioactivity (above background levels) that could, when considered independently, result in a Total Effective Dose EquivalentTEDE of 25 mrem/year to an Average Member of the Critical Group (AMCG). To ensure that the summation of dose from each source term is 25 mrem/year or less after all FSS is completed, the BcDCGLs are reduced based on an expected, or a priori, fraction of the 25 mrem/year dose limit from each source term. The reduced DCGLs, or Operational DCGLs can be related to the BcDCGLs as an expected fraction of dose based on an a priori assessment of what the expected dose should be based on the results of site characterization, process knowledge and the extent of planned remediation. The OpDCGL is then used as the DCGL for the FSS design of the survey unit (calculation of surrogate DCGLs, investigations levels, etc.). Details of the OpDCGLs derived for each dose component and the basis for the applied a priori dose fractions are provided in TSD 17-004, Operational Derived Concentration Guideline Levels for Final Status Survey. The OpDCGLs for the unrestricted release of the Auxiliary Building basement survey unit are provided in Table 7.

Table 7 - Operational DCGLs for Auxiliary Building Basement Survey Unit (OpDCGLB)

LTP Chapter 5, Table 5-4 Operational DCGL Radionuclide (pCi/m2)

Co-60 9.81E+07 Cs-134 6.81E+07 Cs-137 3.58E+07 Ni-63 3.71E+09 Sr-90 3.22E+06

[33]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Instrument DQOs included a verification of the ability of the survey instrument to detect the radiation(s) of interest relative to the OpDCGL. The Canberra ISOCS was selected as the primary instrument used to perform FSS of basement surfaces. Response checks were required prior to issuance and after use. Control and accountability of ISOCS units was required to assure data quality.

As part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results. The actual recorded value was used as the recorded FSS result for measurement and/or sample values that are less than MDC. Negative values were recorded as zero. For radionuclides less than MDC, the value representing the highest abundance was selected. Results were not reported as less than MDC. Sample report summaries included unique sample identification, analytical method, radionuclide, result, uncertainty, laboratory data qualifiers, units, and the observed MDC.

In accordance with the LTP, for laboratory analysis, MDCs less than 10% of the OpDCGL were preferable while MDCs up to 50% of the OpDCGL were acceptable. The maximum acceptable MDC for measurements obtained using field instruments was 50% of the applicable OpDCGL.

5. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey unit and nature of the hazards. Guidance for preparing FSS plans was provided in procedure ZS-LT-300-001-001 Final Status Survey Package Development. The FSS plan uses an integrated sample design that combines direct measurements (by ISOCS) and sampling (concrete cores).

The Canberra ISOCS was selected as the primary instrument for performing FSS of basement surfaces. The ISOCS was selected as the instrument of choice to perform FSS of basement surfaces due to the fact that an ISOCS measurement will provide results that can be used directly to determine total activity with depth in concrete and, the surface area covered by a single ISOCS measurement is large (a nominal FOV of 10-30 m2) which essentially eliminates the need for scan surveys. In addition, after an ISOCS measurement is collected, it can be tested against a variety of geometry assumptions to address uncertainty in the source term geometry if necessary.

The DQO process determined that Co-60, Ni-63, Sr-90, Cs-134 and Cs-137 would be the ROC in Survey Unit 05100. During FSS, concentrations for HTD ROC Ni-63 and Sr-90 were inferred using a surrogate approach. Cs-137 is the principle surrogate radionuclide for Sr-90 and Co-60 is the principle surrogate radionuclide for Ni-63. The mean, maximum and 95% Upper Confidence Level (UCL) of the surrogate ratios for concrete core samples taken in the Auxiliary Building were calculated in TSD 14-019 and are

[34]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 presented in LTP Table 5-15 and Table 8 below. The maximum ratios are used to infer HTD concentrations during FSS unless area specific ratios were determined.

Table 8 - Surrogate Ratios Auxiliary Building Ratios Mean Max 95%UCL Ni-63/Co-60 44.143 180.450 154.632 Sr-90/Cs-137 0.001 0.002 0.002 The equation for calculating a surrogate DCGL is as follows:

Equation 1 1

=

1 2 3

+ + +

2 3 Where: DCGLSur = Surrogate radionuclide DCGL DCGL2,3n = DCGL for radionuclides to be represented by the surrogate Rn = Ratio of concentration (or nuclide mixture fraction) of radionuclide n to surrogate radionuclide Using the OpDCGLs presented in Table 7 and the maximum ratios from Table 8, the following surrogate calculations were performed:

Equation 2 1

(137) = = 3.50 + 07 /2 1 0.002 3.58 + 07 + 3.22 + 06 (137) (90)

The surrogate OpDCGL that was used for Cs-137 in this survey unit for direct comparison of sample results to demonstrate compliance is 3.50E+07 Ci/m2.

Equation 3 1

(60) = = 1.70 + 07 /2 1 180.45 9.81 + 07 +

(60) 3.71 + 09(63)

The surrogate OpDCGL that was used for Co-60 in this survey unit for direct comparison of sample results to demonstrate compliance is 1.70E+07 Ci/m2.

The action level for investigation in a Class 1 basement structure survey unit is the OpDCGL. The surrogate DCGL for Co-60 while inferring Ni-63 is 1.70E+07 Ci/m2 and

[35]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 the surrogate DCGL for Cs-137 while inferring Sr-90 is 3.50E+07 Ci/m2. The action levels for survey unit 05100 are presented in Table 9.

Table 9 - Action Levels for Survey Unit 05100 DCGL ROC (pCi/m2)

Co-60 (1) 1.70E+07 Cs-134 (2) 6.81E+07 (3)

Cs-137 3.50E+07 (1) Based on the surrogate adjusted DCGL of 1.70E+07 Ci/m2 for Co-60 while inferring Ni-63 (2) Based on the Operational DCGL (3) Based on the surrogate adjusted DCGL of 3.50E+07 Ci/m2 for Cs-137 while inferring Sr-90 The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set.

The Elevated Measurement Comparison (EMC) does not apply to this survey unit. At ZSRP, EMC only applies to soils. All other media (structural surfaces, embedded pipe, buried pipe and penetrations) will be remediated to their applicable BcDCGL.

To ensure that the number of ISOCS measurements based on the necessary areal coverage in a basement surface FSS unit was sufficient to satisfy a statistically based sample design, a calculation was performed and documented in LTP section 5.5.2.2 to determine sample size using the standard method as presented in MARSSIM. If the sample size based on the statistical design required more ISOCS measurements than the number of ISOCS measurement required by the areal coverage, then the number of ISOCS measurements was adjusted to meet the larger sample size.

Following the guidance in MARSSIM, the Type I decision error that was used for this calculation was set at 0.05 and the Type II decision error was set at 0.05. The Upper Bound of the Gray Region (UBGR) was set at the OpDCGLB. The Lower Bound of the Gray Region (LBGR) was set at the 0.5 of the OpDCGLB.

The relative shift (/) was calculated as discussed in LTP Chapter 5, section 5.6.4.1.6.

The relative shift (/) for the survey unit data set is defined as shift (), which is the UBGR, or the OpDCGLB (SOF of 1) minus the LBGR (SOF of 0.5), divided by sigma (),

which is the observed standard deviation relative to the associated DCGL. The optimal value for / should range between 1 and 3. The largest value the / can have is 3. If the / exceeds 3, then the value of 3 will be used for /.

[36]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 For the Auxiliary Building basement, a Class 1 survey unit, the standard deviation of the concrete cores analyzed for the full initial suite was used for sigma (). The relative shift

(/) was calculated as discussed in LTP, section 5.6.4.1.6. The / calculations were confirmed and documented as part of the FSS design process, including the evaluation of any additional data from continuing characterization. The value of / exceeded 3, consequently a value of 3 was used as the adjusted relative shift (/) for the Auxiliary Building basement FSS survey unit. From Table 5-5 of MARSSIM, the required number of measurements (N) for use with the Sign Test, using a value of 0.05 for the Type I and Type II decision errors, is 14 measurements for a / value of 3.

The required areal coverage for a Class 1 basement survey unit is 100%. The LTP requires that sufficient measurements be taken in a Class 1 FSS unit to ensure that 100%

of the surface area was surveyed (ISOCS FOV overlapped to ensure that there were no un-surveyed corners and gaps). In cases where the physical configuration or measurement geometry makes the acquisition of a 28 m2 FOV difficult or prohibitive, then the FOV for the ISOCS measurement was reduced provided that the adjusted number of samples remained constant and the minimum areal coverage represented by the FSS unit classification was achieved. To ensure that were no un-surveyed corners and gaps, the number of measurements that were taken in the Auxiliary Building FSS unit was adjusted by overlaying the center-point of the ISOCS measurement on a 4 m x 4 m (16 m2) grid system.

Table 10, which is reproduced from LTP Table 5-19, presents the Auxiliary Building FSS unit and the adjusted number of ISOCS measurements that will be taken for FSS.

Table 10 - Adjusted Minimum Number of ISOCS Measurements Required Adjusted # of Adjusted Adjusted Areal ISOCS Areal Areal FSS Unit Classification Coverage Measurements Coverage Coverage (m2) (FOV-28 m2) (m2) (% of Area)

Aux Bldg. 542 foot Class 1 6,503 407(1) 6,503 100%

Floor & Walls (1) Adjusted to ensure number of measurements that will be taken in Class 1 FSS units will ensure 100% areal coverage, including overlap to ensure that there are no un-surveyed corners and gaps (FOV based on a 4 m x 4 m grid system).

When the survey grids were established on the walls and floor of the Auxiliary Building structural surfaces, obstacles and physical constraints were encountered that prompted further adjustments to the number of samples and the FOV. Some measurements were not feasible and other measurement locations were added.

Four hundred and seven (407) systematic ISOCS measurements were originally planned for the Auxiliary Building FSS unit (FSS unit 05100), based on a source to detector

[37]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 distance of 3 meters for the ISOCS detector. Additional measurements were required due to adjustments for obstacles and physical constraints, which increased the total number of ISOCS measurements necessary to achieve 100% areal coverage to four hundred and twenty five (425) systematic ISOCS measurements.

The areal coverage requirements for FSS of structures as specified in the LTP is commensurate with the probability that a small area of elevated activity could exist within a FSS unit in a concentration exceeding the BcDCGL and the likelihood that such an area would not be detected by the FSS ISOCS measurements. It is highly unlikely that the ISOCS, with a nominal FOV of approximately 28 m2 would not detect and account for elevated areas. The primary basis used to determine reasonable areal coverage for the ISOCS measurements is the potential for the OpDCGL to be exceeded. The criterion for selecting reasonable and risk-informed areal coverage is based on a graded approach similar to the guidance for scan surveys during FSS provided in MARSSIM, where the coverage is based on the expected fraction of the DCGL (in this case the OpDCGL). All ISOCS measurement locations collected for survey unit 05100, the Auxiliary Building basement floor and walls, are provided on maps in Attachment 1 of this document.

ZSRP LTP Chapter 5, section 5.1 states that concrete core samples will be collected during FSS at 10% of the locations where an ISOCS measurement was collected with the locations selected at random to confirm the HTD to surrogate radionuclide ratios. Only HTD radionuclides included as ROC (Ni-63, Sr-90, for the Auxiliary Building) were analyzed in the FSS confirmatory samples. The concrete core locations were selected from the floor and lower walls in the survey unit to alleviate safety concerns from working at heights and to focus on the areas expected to contain the majority of residual radioactivity. For FSS unit 05100, the initial survey design required a minimum of 407 ISOCS measurements and consequently, forty-two (42) additional concrete core samples were acquired for assessment of HTD ROC. Due to additional adjustment during implementation, the number of concrete core samples were increased to a total of forty-six (46) concrete core samples to accommodate the increased sample size in accordance with LTP section 5.1.

The coordinates for all of the ISOCS measurement locations were conspicuously marked to designate where to position the survey rig to the center-point of the instrument FOV.

The ISOCS detector was then positioned either vertically or horizontally and adjacent to the surface at the center-point of each designated floor or wall measurement location.

Each survey measurement location would then be reproducible utilizing permanent markings on the Auxiliary Building floor and walls and annotated on the survey map.

The implementation of quality control measures as referenced by LTP Chapter 5, section 5.9 and ZionSolutions ZS-LT-01, Quality Assurance Project Plan (for Characterization

[38]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 and FSS) (QAPP) (Reference 11) includes the collection of a replicate measurement at 5% of the measurements taken in a survey unit with the locations selected at random.

Twenty-three (23) ISOCS measurements were selected randomly for the replicate measurements for this survey unit.

To achieve 100% areal coverage for the 6,503 m2 of floor and wall surfaces that constitute this survey unit, along with the minimum of 10% replicate measurements, four hundred and fifty-three (453) ISOCS measurements (425 systematic, 23 replicate, and 5 investigational) were taken at 425 locations.

The source term geometry for ISOCS efficiency calibration, i.e., concentration depth profile and areal distribution of the residual radioactivity in structures, is required to generate efficiency curves (i.e., efficiency as a function of energy) for the ISOCS gamma spectroscopy measurements. The concrete cores obtained during characterization, continuing characterization and FSS provided the requisite information regarding the distribution of activity with depth for the Auxiliary Building basement concrete. The basis for the chosen ISOCS efficiency calibrations for the FSS of the Auxiliary Building basement concrete are documented in ZionSolutions TSD 14-022, Use of In-Situ Gamma Spectroscopy for Final Status Survey of End State Structures (Reference 12). A majority of the ISOCS measurements were collected using the circular plane geometry. The varied geometries were necessary due to the structural anomalies encountered within the survey unit. The elevator pit, located on the west side of the Auxiliary Building basement floor, is a poured concrete box (pit) that required a different geometry. The rectangular plane geometry was used for the elevator pit. The second location with a varied geometry is sump B. The sump is a metal lined (intact) space on the Auxiliary Building basement floor near the east wall (G wall). The Room geometry was used for the sump. ISOCS geometries specifically employed within this survey unit are provided in Attachment 2 of this report. Maps of the surface area scanned by the ISOCS FOV are provided in Attachment 1.

For this Class 1 basement structure survey unit, the Investigation Levels for ISOCS measurement results are those levels specified in LTP Chapter 5, Table 5-25 and are reproduced below in Table 11.

Table 11 - Investigation Levels Classification Direct Measurement Class 1 >Operational DCGL Table 12 provides a synopsis of the survey design for survey unit 05100.

[39]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 12 - Synopsis of Survey Design FEATURE DESIGN CRITERIA BASIS Survey Unit 7,226 m2 LTP Ch. 5, Table 5-23 Surface Area

• UBGR = SOF of 1

• LBGR = SOF of 0.5 Number of

• Type I error = 0.05 425 (systematic adjusted)

Measurements (N)

• Type II error = 0.05

• / = 3 (adjusted)

MARSSIM Table 5.5 L = Square Root (A/N), Square Root Grid Spacing (7,226 m2) = 16 m2 or 4 m by 4 m (LTP Chapter 5, section systematic grids 5.6.4.5.2)

• Co 9.81E+07 pCi/m2

• Cs-134 - 6.81E+07 pCi/m2 OpDCGLs for Auxiliary DCGLs

• Cs-137 - 3.58E+07 pCi/m2 Building Basement,

• Ni 3.71E+09 pCi/m2 (LTP Chapter 5, Table 5-4)

• Sr 3.22E+06 pCi/m2 Investigation Level >Operational DCGL (LTP Chapter 5, Table 5-25)

Scan Areal Class 1 100% areal coverage, 7,226 m2 or 100% areal coverage Coverage (LTP Chapter 5, Table 5-19) 21 measurements selected randomly for Quality Control replicate measurement analysis (23 (LTP Chapter 5, section 5.9)

(QC) measurements were collected)

Concrete Core Forty-six (46) concrete core samples (LTP Chapter 5, section 5.1)

Samples

[40]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100

6. SURVEY IMPLEMENTATION For survey unit 05100, compliance with the unrestricted release criteria was demonstrated through a combination of direct measurements using the ISOCS and the analysis of concrete core samples.

A walkdown and turnover survey was satisfactorily performed in the Auxiliary Building basement in accordance with the Isolation and Control requirements of procedure ZS-LT-300-001-003, Isolation and Control for Final Status Survey (Reference 13). The turnover surveys consisted of surveys for loose surface contamination as well as the acquisition of several ISOCS measurements. All smear results were less than 1,000 dpm/100 cm2 and all ISOCS measurements taken for turnover indicated a SOF of less than one for all ROC. The Auxiliary Building basement was deemed acceptable for turnover and FSS commenced on February 2, 2018, under FSS Sample Plan #B1-05100A-F, which included DQOs, survey design, detailed FSS instructions, job safety analysis, and related procedures for reference. A Field Log (ZS-LT-300-001-001 Attachment 14) was used to document field activities and other information pertaining to the performance of the FSS.

FSS field activities were projected to take eighteen (18) working days to complete. Daily briefings were conducted to discuss the expectations for job performance and to review safety aspects of the job. The survey required field activities were performed during normal working hours and concluded on March 22, 2018.

ZionSolutions TSD 17-003, Evaluation of Efficiency Calibration Geometries for In-Situ Gamma Spectrometry During Final Status Surveys (Reference 14) was generated to address the Request for Additional Information (RAI) (HP RAI 6) from the Nuclear Regulatory Commission (NRC) pertaining to discrepancies between the LTP and TSD 14-022 with regard to the acquisition of additional concrete core samples to validate that the proper geometries were applied to ISOCS measurements. In resolution, LTP section 5.3.4.4 details several commitments to acquire additional concrete core samples in the Auxiliary Building as continuing characterization. Thirty-two (32) additional core samples were collected throughout the Auxiliary Building basement. Addendum 1 to TSD 14-022 provides the justification for the selection of reasonably conservative geometries for efficiency calibrations for the ISOCS based on the physical conditions of the remediated surface and the anticipated depth and distribution of activity.

Prior to implementing the sample plan for the FSS of the Auxiliary Building basement structure, the physical condition of the concrete surfaces to be surveyed were assessed to ensure that the geometry was not significantly changed from that assumed in TSD 14-022.

ISOCS measurements were acquired using the geometry labeled as 3M90D_CP_2IN, or similar, which assumed a circular plane source with a contaminant depth of 2 inches.

[41]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 With the 90-degree collimation shield installed and a source to detector distance of 3 meters, this orientation corresponded to a nominal FOV of 28 m2. A guide attached to the detector assembly in the form of a plumb-bob or wooden stud was used to establish a consistent source to detector distance and center the detector over the selected measurement location.

The ISOCS measurement locations specified in FSS package #B1-05100A-F were marked based on the grid coordinates provided in the survey package. During the implementation of the survey unit requirements, it was observed that several locations, identified for ISOCS measurements, no longer existed. Additionally, to ensure 100% areal coverage, several ISOCS measurement locations were added. Finally, the geometries employed for several ISOCS measurements required slight modification due to obstructions that made the original source to detector distance impossible. A total of four hundred and twenty-five (425) ISOCS measurements were collected for survey package #B1-05100A-F. Two (2) additional locations, the elevator pit and the B Sump, had specific geometries established to better define the levels of contamination present. Twenty-three (23) replicate measurements were also acquired in the Auxiliary Building basement at the locations specified in FSS survey package #B1-05100A-F. The ISOCS detector face was oriented perpendicular to the surface of interest represented by the grid coordinate. See Photograph 1 for an example of an ISOCS measurement being conducted.

Photograph 1 - ISOCS Systematic Measurements of Auxiliary Building 542 Foot Elevation

[42]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100

7. SURVEY RESULTS The SOF or unity rule is applied to the data used for the survey planning, and data evaluation and statistical tests for basement surfaces since multiple radionuclide-specific measurements were performed and the concentrations inferred based on known relationships. The unity rule is the mathematical test used to evaluate compliance with radiological criteria for license termination when more than one radionuclide has been determined to be potentially present.

The equation for the unity rule is:

Equation 4 C1 C2 Cn

+ +............ 1 DCGL1 DCGL 2 DCGL n Where: Cn = concentration of radionuclide n DCGLn = DCGL of radionuclide n.

The application of the unity rule serves to normalize the data to allow for an accurate comparison of the various data measurements to the release criteria. When the unity rule is applied, the DCGLW (used for the nonparametric statistical test) becomes one (1). The BcDCGLB are directly analogous to the DCGLW as defined in MARSSIM. The use and application of the unity rule was performed in accordance with section 4.3.3 of MARSSIM.

As described in LTP Chapter 5, section 5.10.3.2, the Sign Test was used to evaluate the measured residual radioactivity against the dose criterion. The Operational SOF (OpSOF) for each measurement was used as the sum value for the Sign Test. The Sign Test then demonstrated that the mean activity for each ROC was less than the OpDCGLB at a Type 1 decision error of 0.05 (see Attachment 3).

For building surfaces, areas of elevated activity were defined as any area identified by measurement (systematic or judgmental) that exceeded the OpDCGL but was less than the BcDCGL. Any area that exceeded the BcDCGL would have required remediation. The OpSOF for a systematic or a judgmental measurement/sample(s) can exceed one without remediation as long as the survey unit passes the Sign Test and, the mean OpSOF for the survey unit does not exceed one. Once the survey data set passes the Sign Test (using OpDCGLs), then the mean radionuclide activity (pCi/m2) for each ROC from systematic measurements along with any identified elevated areas from systematic and judgmental samples can be used with the BcDCGLs to perform a mean Base Case SOF (BcSOF) calculation. The dose from residual radioactivity assigned to the FSS unit is the mean BcSOFB multiplied by 25 mrem/yr.

[43]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Direct measurement locations were denoted on the concrete walls and floor of the Auxiliary Building basement by marking a 4 meter by 4 meter grid pattern using a random start point that was overlaid over the exposed surface, providing sufficient overlap between locations to ensure 100% areal coverage. See Attachment 1, Figures 1 through 15 for a depiction of all measurement locations.

The systematic sample population consisted of four hundred and twenty-five (425) direct measurements that were acquired using the ISOCS. A summary of the results of the 425 ISOCS measurements taken for non-parametric statistical testing results when compared to the OpDCGLB is provided in Table 13. The complete ISOCS measurement and gamma spectroscopy reports are presented in Attachment 7. The concentrations for Ni-63 and Sr-90 are inferred based on the maximum ratios as specified in Table 8.

Table 13 - Auxilairy Building Surfaces - Statistical Quantities - Systematic Population Individual Measurement Metrics Total Number of Systematic Measurements = 425 Number of Quality Control Measurements = 23 Number of Judgmental/Investigational Measurements = 5 Total Number of Measurements = 453 Mean Systematic Measurement OpSOF = 0.143 Max Individual Systematic Measurement OpSOF = 2.189 Number of Systematic Measurements with OpSOF >1 = 16 Statistical Quantities - Systematic Measurement Population MEAN MEDIAN MAX MIN ST. DEV. BcDCGL Avg Avg Dose BcSOF ROC per ROC (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) per (mrem/yr)

ROC Co-60 8.88E+05 9.21E+04 2.46E+07 0.00E+00 3.17E+06 3.04E+08 0.003 0.073 Ni-63 1.60E+08 1.66E+07 4.44E+09 0.00E+00 5.72E+08 1.15E+10 0.014 0.348 Sr-90 6.28E+03 1.61E+03 1.49E+05 4.12E+00 1.37E+04 9.98E+06 0.001 0.016 Cs-134 5.22E+04 4.18E+04 7.29E+05 0.00E+00 5.69E+04 2.11E+08 0.000 0.006 Cs-137 3.15E+06 8.10E+05 7.46E+07 2.06E+03 6.86E+06 1.11E+08 0.028 0.708 ZionSolutions procedure ZS-LT-300-001-004, Final Status Survey Data Assessment, section 5.3.3 states that only samples, or measurements, taken as part of the systematic sample population for the survey unit are used to derive statistical data. Since the sixteen (16) measurements provided in Table 14 were evaluated independently, they were not included in the statistical data presented in Table 13. The total SOF for the Auxiliary Building basement structural FSS unit based on the mean concentration for each ROC as

[44]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 measured by the systematic sample population when compared against the BcDCGLs is 0.046.

During the FSS of the Auxiliary Building basement, sixteen (16) measurements were identified where the result exceeded the OpDCGLB but was less than the BcDCGLB. As previously stated, the OpSOF for a systematic or a judgmental measurement/sample(s) may exceed one without remediation as long as the survey unit passes the Sign Test and, the mean OpSOF for the survey unit does not exceed one. Once the survey data set passes the Sign Test (using OpDCGLB), the mean radionuclide activity (pCi/m2) for each ROC from systematic measurements along with any identified elevated areas from systematic and judgmental samples will be used with the BcDCGLB to perform a BcSOF calculation for each surface FSS unit in a basement in accordance with the following equation (from LTP Chapter 5, Section 5.5.4, Equation 5-5). The mean BcSOF for the survey unit will then be adjusted by adding the BcSOF from the elevated areas to the mean to account for the additional dose attributed to the elevated areas.

Equation 5

= +

=1 x where:

BcSOFB = SOF for structural surface survey unit within a basement using BcDCGLs Mean ConcB ROCi = Mean concentration for the systematic measurements taken during the FSS of structural surface in survey unit for each ROCi BcDCGLB ROCi = BcDCGL for structural surfaces (DCGLB) for each ROCi Elev ConcB ROCi = Concentration for ROCi in any identified elevated area (systematic or judgmental)

SAElev = surface area of the elevated area SASU = adjusted surface area of FSS unit for DCGL calculation

[45]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 The adjusted surface area of the Auxiliary Building FSS unit (SASU) is 7,226 m2. The surface area of each of the elevated areas is 28 m2, equating to the FOV of the individual ISOCS measurement. Table 14 presents the elevated concentration and the calculated BcSOF for each ROC in each of the sixteen (16) identified elevated areas. The individual elevated BcSOF for each elevated ROC were than summed to provide a total BcSOF adjustment to the mean BcSOF for the survey unit.

Table 14 - Elevated Measurement ROC Concentrations and SOFs Elevated Area #1 - B1-05100AF-SWC-204-GD Elev Conc 1 Co-60 = 1.22E+07 pCi/m2 SOF 1 Co-60 = 0.000 2

Elev Conc 1 Ni-63 = 2.20E+09 pCi/m SOF 1 Ni-63 = 0.001 2

Elev Conc 1 Sr-90 = 2.52E+04 pCi/m SOF 1 Sr-90 = 0.000 2

Elev Conc 1 Cs-134 = 2.84E+05 pCi/m SOF 1 Cs-134 = 0.000 2

Elev Conc 1 Cs-137 = 1.26E+07 pCi/m SOF 1 Cs-137 = 0.000 SOF 1 TOTAL = 0.001 Elevated Area #2 - B1-05100AF-SWC-205-GD Elev Conc 2 Co-60 = 1.46E+07 pCi/m2 SOF 2 Co-60 = 0.000 Elev Conc 2 Ni-63 = 2.63E+09 pCi/m2 SOF 2 Ni-63 = 0.001 Elev Conc 2 Sr-90 = 2.74E+04 pCi/m2 SOF 2 Sr-90 = 0.000 Elev Conc 2 Cs-134 = 0.00E+00 pCi/m2 SOF 2 Cs-134 = 0.000 Elev Conc 2 Cs-137 = 1.37E+07 pCi/m2 SOF 2 Cs-137 = 0.000 SOF 2 TOTAL = 0.001 Elevated Area #3 - B1-05100AF-SWC-206-GD Elev Conc 3 Co-60 = 1.30E+07 pCi/m2 SOF 3 Co-60 = 0.000 Elev Conc 3 Ni-63 = 2.35E+09 pCi/m2 SOF 3 Ni-63 = 0.001 Elev Conc 3 Sr-90 = 2.46E+04 pCi/m2 SOF 3 Sr-90 = 0.000 Elev Conc 3 Cs-134 = 8.72E+04 pCi/m2 SOF 3 Cs-134 = 0.000 Elev Conc 3 Cs-137 = 1.23E+07 pCi/m2 SOF 3 Cs-137 = 0.000 SOF 3 TOTAL = 0.001 Elevated Area #4 - B1-05100AF-SWC-212-GD Elev Conc 4 Co-60 = 1.29E+07 pCi/m2 SOF 4 Co-60 = 0.000 Elev Conc 4 Ni-63 = 2.33E+09 pCi/m2 SOF 4 Ni-63 = 0.001 Elev Conc 4 Sr-90 = 1.69E+04 pCi/m2 SOF 4 Sr-90 = 0.000 Elev Conc 4 Cs-134 = 2.27E+05 pCi/m2 SOF 4 Cs-134 = 0.000 Elev Conc 4 Cs-137 = 8.46E+06 pCi/m2 SOF 4 Cs-137 = 0.000 SOF 4 TOTAL = 0.001

[46]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 14 (continued) - Elevated Measurement ROC Concentrations and SOFs Elevated Area #5 - B1-05100AF-SFC-256-GD Elev Conc 5 Co-60 = 2.24E+07 pCi/m2 SOF 5 Co-60 = 0.000 2

Elev Conc 5 Ni-63 = 4.04E+09 pCi/m SOF 5 Ni-63 = 0.001 2

Elev Conc 5 Sr-90 = 3.20E+04 pCi/m SOF 5 Sr-90 = 0.000 2

Elev Conc 5 Cs-134 = 6.63E+04 pCi/m SOF 5 Cs-134 = 0.000 2

Elev Conc 5 Cs-137 = 1.60E+07 pCi/m SOF 5 Cs-137 = 0.000 SOF 5 TOTAL = 0.002 Elevated Area #6 - B1-05100AF-SFC-257-GD Elev Conc 6 Co-60 = 1.82E+07 pCi/m2 SOF 6 Co-60 = 0.000 Elev Conc 6 Ni-63 = 3.28E+09 pCi/m2 SOF 6 Ni-63 = 0.001 Elev Conc 6 Sr-90 = 3.50E+04 pCi/m2 SOF 6 Sr-90 = 0.000 Elev Conc 6 Cs-134 = 3.72E+05 pCi/m2 SOF 6 Cs-134 = 0.000 Elev Conc 6 Cs-137 = 1.75E+07 pCi/m2 SOF 6 Cs-137 = 0.001 SOF 6 TOTAL = 0.002 Elevated Area #7 - B1-05100AF-SFC-258-GD Elev Conc 7 Co-60 = 1.88E+07 pCi/m2 SOF 7 Co-60 = 0.000 Elev Conc 7 Ni-63 = 3.39E+09 pCi/m2 SOF 7 Ni-63 = 0.001 Elev Conc 7 Sr-90 = 3.24E+04 pCi/m2 SOF 7 Sr-90 = 0.000 Elev Conc 7 Cs-134 = 1.32E+05 pCi/m2 SOF 7 Cs-134 = 0.000 Elev Conc 7 Cs-137 = 1.62E+07 pCi/m2 SOF 7 Cs-137 = 0.000 SOF 7 TOTAL = 0.002 Elevated Area #8 - B1-05100AF-SFC-259-GD Elev Conc 8 Co-60 = 2.01E+07 pCi/m2 SOF 8 Co-60 = 0.000 Elev Conc 8 Ni-63 = 3.63E+09 pCi/m2 SOF 8 Ni-63 = 0.001 Elev Conc 8 Sr-90 = 5.94E+04 pCi/m2 SOF 8 Sr-90 = 0.000 Elev Conc 8 Cs-134 = 1.98E+05 pCi/m2 SOF 8 Cs-134 = 0.000 Elev Conc 8 Cs-137 = 2.97E+07 pCi/m2 SOF 8 Cs-137 = 0.001 SOF 8 TOTAL = 0.002 Elevated Area #9 - B1-05100AF-SFC-260-GD Elev Conc 9 Co-60 = 1.81E+07 pCi/m2 SOF 9 Co-60 = 0.000 Elev Conc 9 Ni-63 = 3.27E+09 pCi/m2 SOF 9 Ni-63 = 0.001 Elev Conc 9 Sr-90 = 5.90E+04 pCi/m2 SOF 9 Sr-90 = 0.000 Elev Conc 9 Cs-134 = 1.12E+05 pCi/m2 SOF 9 Cs-134 = 0.000 Elev Conc 9 Cs-137 = 2.95E+07 pCi/m2 SOF 9 Cs-137 = 0.001 SOF 9 TOTAL = 0.002

[47]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 14 (continued) - Elevated Measurement ROC Concentrations and SOFs Elevated Area #10 - B1-05100AF-SFC-273-GD Elev Conc 10 Co-60 = 2.29E+07 pCi/m2 SOF 10 Co-60 = 0.000 2

Elev Conc 10 Ni-63 = 4.13E+09 pCi/m SOF 10 Ni-63 = 0.001 2

Elev Conc 10 Sr-90 = 5.62E+04 pCi/m SOF 10 Sr-90 = 0.000 2

Elev Conc 10 Cs-134 = 7.29E+05 pCi/m SOF 10 Cs-134 = 0.000 2

Elev Conc 10 Cs-137 = 2.81E+07 pCi/m SOF 10 Cs-137 = 0.001 SOF 10 TOTAL = 0.003 Elevated Area #11 - B1-05100AF-SFC-274-GD Elev Conc 11 Co-60 = 2.46E+07 pCi/m2 SOF 11 Co-60 = 0.000 Elev Conc 11 Ni-63 = 4.44E+09 pCi/m2 SOF 11 Ni-63 = 0.001 Elev Conc 11 Sr-90 = 5.06E+04 pCi/m2 SOF 11 Sr-90 = 0.000 Elev Conc 11 Cs-134 = 1.93E+05 pCi/m2 SOF 11 Cs-134 = 0.000 Elev Conc 11 Cs-137 = 2.53E+07 pCi/m2 SOF 11 Cs-137 = 0.001 SOF 11 TOTAL = 0.003 Elevated Area #12 - B1-05100AF-SFC-295-GD Elev Conc 12 Co-60 = 4.31E+05 pCi/m2 SOF 12 Co-60 = 0.000 Elev Conc 12 Ni-63 = 7.78E+07 pCi/m2 SOF 12 Ni-63 = 0.000 Elev Conc 12 Sr-90 = 8.58E+04 pCi/m2 SOF 12 Sr-90 = 0.000 Elev Conc 12 Cs-134 = 4.70E+04 pCi/m2 SOF 12 Cs-134 = 0.000 Elev Conc 12 Cs-137 = 4.29E+07 pCi/m2 SOF 12 Cs-137 = 0.001 SOF 12 TOTAL = 0.001 Elevated Area #13 - B1-05100AF-SFC-350-GD Elev Conc 13 Co-60 = 7.50E+05 pCi/m2 SOF 13 Co-60 = 0.000 Elev Conc 13 Ni-63 = 1.35E+08 pCi/m2 SOF 13 Ni-63 = 0.000 Elev Conc 13 Sr-90 = 6.90E+04 pCi/m2 SOF 13 Sr-90 = 0.000 Elev Conc 13 Cs-134 = 8.58E+04 pCi/m2 SOF 13 Cs-134 = 0.000 Elev Conc 13 Cs-137 = 3.45E+07 pCi/m2 SOF 13 Cs-137 = 0.001 SOF 13 TOTAL = 0.001 Elevated Area #14 - B1-05100AF-SFC-351-GD Elev Conc 14 Co-60 = 9.66E+05 pCi/m2 SOF 14 Co-60 = 0.000 Elev Conc 14 Ni-63 = 1.74E+08 pCi/m2 SOF 14 Ni-63 = 0.000 Elev Conc 14 Sr-90 = 1.49E+05 pCi/m2 SOF 14 Sr-90 = 0.000 Elev Conc 14 Cs-134 = 1.49E+05 pCi/m2 SOF 14 Cs-134 = 0.000 Elev Conc 14 Cs-137 = 7.46E+07 pCi/m2 SOF 14 Cs-137 = 0.002 SOF 14 TOTAL = 0.003

[48]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 14 (continued) - Elevated Measurement ROC Concentrations and SOFs Elevated Area #15 - B1-05100AF-SFC-352-GD Elev Conc 15 Co-60 = 1.08E+06 pCi/m2 SOF 15 Co-60 = 0.000 2

Elev Conc 15 Ni-63 = 1.95E+08 pCi/m SOF 15 Ni-63 = 0.000 2

Elev Conc 15 Sr-90 = 9.98E+04 pCi/m SOF 15 Sr-90 = 0.000 2

Elev Conc 15 Cs-134 = 0.00E+00 pCi/m SOF 15 Cs-134 = 0.000 2

Elev Conc 15 Cs-137 = 4.99E+07 pCi/m SOF 15 Cs-137 = 0.002 SOF 15 TOTAL = 0.002 Elevated Area #16 - B1-05100AF-SFC-466-GD Elev Conc 16 Co-60 = 1.92E+07 pCi/m2 SOF 16 Co-60 = 0.000 Elev Conc 16 Ni-63 = 3.46E+09 pCi/m2 SOF 16 Ni-63 = 0.001 Elev Conc 16 Sr-90 = 3.36E+04 pCi/m2 SOF 16 Sr-90 = 0.000 Elev Conc 16 Cs-134 = 1.86E+05 pCi/m2 SOF 16 Cs-134 = 0.000 Elev Conc 16 Cs-137 = 1.68E+07 pCi/m2 SOF 16 Cs-137 = 0.000 SOF 16 TOTAL = 0.002 The sum of the BcSOFTOTAL for each of the sixteen (16) elevated measurements equals 0.029. This value is then added to the mean BcSOF for the Auxiliary Building basement structural FSS unit of 0.046 resulting in an adjusted total BcSOF for the Auxiliary Building basement of 0.075. This SOF equates to a dose of 1.868 mrem/yr. This value is the dose assigned to the survey unit based on the average of the systematic measurements adjusted for the dose contribution of elevated areas.

The implementation of required QC measures included the collection of twenty-three (23)

ISOCS measurements at locations throughout the Auxiliary Building for replicate measurement analysis. The replicate ISOCS measurement results are provided in Table

15. The concentrations for Ni-63 and Sr-90 are inferred based on the maximum ratios as specified in Table 8.

[49]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 15 - Summary of ISOCS Replicate Measurements for QC Co-60 Cs-134 Cs-137 Ni-63 Sr-90 MEASUREMENT ID 2 2 2 (pCi/m ) (pCi/m ) (pCi/m ) (pCi/m2) (pCi/m2)

B1-05100AF-QWC-006-GD 0.00E+00 0.00E+00 2.98E+02 5.39E+04 1.49E+05 B1-05100AF-QWC-024-GD 4.79E+04 8.64E+06 3.26E+02 1.08E+04 1.63E+05 B1-05100AF-QWC-074-GD 5.93E+03 1.07E+06 1.61E+02 2.33E+04 8.03E+04 B1-05100AF-QWC-102-GD 2.84E+04 5.12E+06 1.47E+03 3.94E+04 7.33E+05 B1-05100AF-QWC-116-GD 8.55E+04 1.54E+07 8.06E+02 4.22E+04 4.03E+05 B1-05100AF-QWC-131-GD 1.19E+05 2.15E+07 3.51E+05 0.00E+00 3.51E+05 B1-05100AF-QWC-132-GD 5.18E+05 9.35E+07 7.20E+03 0.00E+00 3.60E+06 B1-05100AF-QWC-156-GD 2.13E+05 3.84E+07 2.40E+04 1.44E+04 1.20E+07 B1-05100AF-QWC-167-GD 9.21E+04 1.66E+07 2.62E+03 3.32E+04 1.31E+06 B1-05100AF-QWC-208-GD 2.20E+06 3.97E+08 9.50E+03 7.03E+04 4.75E+06 B1-05100AF-QWC-218-GD 3.40E+04 6.14E+06 8.48E+02 7.85E+04 4.24E+05 B1-05100AF-QWC-230-GD 3.55E+04 6.41E+06 1.07E+02 3.79E+04 5.36E+04 B1-05100AF-QFC-243-GD 3.28E+04 5.92E+06 3.06E+01 0.00E+00 1.53E+04 B1-05100AF-QFC-272-GD 6.81E+06 1.23E+09 1.01E+04 7.14E+04 5.06E+06 B1-05100AF-QWC-292-GD 1.46E+06 2.63E+08 3.38E+04 4.56E+03 1.69E+07 B1-05100AF-QFC-331-GD 1.19E+05 2.15E+07 1.64E+03 5.51E+04 8.21E+05 B1-05100AF-QFC-333-GD 8.06E+04 1.45E+07 1.00E+03 1.30E+04 5.01E+05 B1-05100AF-QFC-334-GD 1.42E+06 2.56E+08 3.28E+03 1.07E+05 1.64E+06 B1-05100AF-QFC-341-GD 6.07E+05 1.10E+08 4.18E+04 1.48E+05 2.09E+07 B1-05100AF-QFC-373-GD 4.69E+05 8.46E+07 4.10E+03 2.60E+04 2.05E+06 B1-05100AF-QFC-395-GD 6.70E+04 1.21E+07 8.82E+02 8.11E+04 4.41E+05 B1-05100AF-QFC-405-GD 1.83E+05 3.30E+07 1.72E+03 8.26E+04 8.61E+05 B1-05100AF-QFC-409-GD 1.92E+05 3.46E+07 3.22E+03 1.69E+04 1.61E+06 The complete ISOCS gamma spectroscopy reports are presented in Attachment 7.

[50]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Investigational ISOCS measurements were taken when the surface being measured had irregular surfaces. Generally, locations with trenches or holes were resurveyed with the source to detector distance reduced to account for the uneven surface. Five (5) investigational measurements were taken within the Auxiliary Building basement and the results are provided in Table 16 with additional detail in Attachment 5. Each measurement represents the gamma result at that location in units of pCi/m2. The concentrations for Ni-63 and Sr-90 were inferred based on the maximum ratios as specified in Table 8. The SOF for each individual investigation measurement when compared against the OpDCGL was less that one.

Table 16 - Summary of Results for Judgmental/Investigational Measurements Taken in the Auxiliary Building Co-60 Ni-63 Sr-90 Cs-134 Cs-137 OpSOF MEASUREMENT ID (pCi/m ) (pCi/m ) (pCi/m ) (pCi/m ) (pCi/m2) 2 2 2 2 B1-05100A-FIFC-278-GD 4.88E+06 8.81E+08 7.02E+03 2.11E+05 3.51E+06 0.390 B1-05100A-FIWC-005-GD 3.69E+04 6.66E+06 2.74E+02 3.44E+04 1.37E+05 0.007 B1-05100A-FIFC-365-GD 9.16E+04 1.65E+07 2.70E+03 2.05E+04 1.35E+06 0.044 B1-05100A-FIFC-369-GD 1.66E+06 3.00E+08 7.48E+03 3.37E+02 3.74E+06 0.204 B1-05100A-FIFC-404-GD 3.19E+05 5.76E+07 2.46E+03 3.51E+04 1.23E+06 0.054 Forty-six (46) concrete core samples were acquired as part of the FSS of survey unit 05100. The concrete core samples were acquired at 10% of the locations where an ISOCS measurement was collected with the locations selected at random. Only HTD radionuclides included as ROC (Ni-63 and Sr-90) were analyzed in the FSS confirmatory samples. The top 1/2-inch puck from each of the FSS confirmatory concrete core samples, representing the concrete from the exposed surface to a depth of 1/2 inch, were sent to Eberline Laboratory for analysis of the ROC, including Ni-63 and Sr-90. The analysis results indicated detectable concentrations of Co-60 and Ni-63 in several samples at ratios less than the maximum ratio from Table 8. Cs-137 was positively detected in 29 of the 46 samples however, Sr-90 was detected in only one sample. The Sr-90 result, while greater than the MDC was within the range of uncertainty and believed to be a false-positive result. The sample was re-analyzed and the results indicated that Sr-90 was no longer positively identified. No further action or analysis was performed. The results are presented in Table 17 below.

[51]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 17 - Summary of FSS Concrete Core Analysis by Eberline B1-05100AF-SWC-017-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 -1.74E-02 5.47E-02 1.75E-01 Ni-63 -1.70E-01 1.25E+00 2.15E+00 Sr-90 1.23E-01 3.99E-01 7.01E-01 Cs-134 3.71E-01 1.92E-01 3.06E-01 Cs-137 1.97E-01 2.39E-01 3.94E-01 B1-05100AF-SWC-041-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 -1.63E-02 7.61E-02 1.18E-01 Ni-63 6.00E-01 9.97E-01 1.68E+00 Sr-90 1.77E-01 3.59E-01 6.21E-01 Cs-134 -4.05E-03 3.55E-02 1.19E-01 Cs-137 2.52E+00 3.75E-01 2.61E-01 B1-05100AF-SWC-057-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 -1.68E-02 6.83E-02 1.36E-01 Ni-63 5.74E-01 9.53E-01 1.61E+00 Sr-90 1.42E-01 2.99E-01 5.19E-01 Cs-134 -3.23E-02 7.61E-02 2.02E-01 Cs-137 2.19E-01 1.52E-01 2.37E-01 B1-05100AF-SWC-088-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 3.40E-02 1.04E-01 1.51E-01 Ni-63 1.91E+00 1.01E+00 1.66E+00 Sr-90 2.52E-01 3.22E-01 5.45E-01 Cs-134 -4.04E-01 2.18E-01 1.65E-01 Cs-137 1.95E-01 1.15E-01 2.24E-01 B1-05100AF-SWC-101-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 -3.10E-02 1.63E-01 2.16E-01 Ni-63 1.18E-01 8.69E-01 1.48E+00 Sr-90 2.42E-01 2.73E-01 4.59E-01 Cs-134 3.95E-02 1.28E-01 2.26E-01 Cs-137 5.87E-01 2.08E-01 2.59E-01

[52]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 18(continued) - Summary of FSS Concrete Core Analysis by Eberline B1-05100AF-SWC-115-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.71E-01 1.02E-01 1.85E-01 Ni-63 2.96E+00 9.73E-01 1.56E+00 Sr-90 1.59E-01 2.94E-01 5.08E-01 Cs-134 -3.63E-03 7.41E-02 1.88E-01 Cs-137 1.32E+00 4.61E-01 6.85E-01 B1-05100AF-SWC-116-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.37E-01 1.32E-01 2.33E-01 Ni-63 0.00E+00 1.22E+00 2.08E+00 Sr-90 6.89E-02 4.53E-01 8.04E-01 Cs-134 2.63E-02 7.32E-02 1.81E-01 Cs-137 5.50E-01 2.06E-01 2.77E-01 B1-05100AF-SWC-150-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 2.02E-01 1.19E-01 2.48E-01 Ni-63 1.14E+00 1.23E+00 2.06E+00 Sr-90 -2.66E-01 4.07E-01 7.67E-01 Cs-134 -1.71E-01 1.20E-01 1.58E-01 Cs-137 6.46E+00 7.81E-01 2.64E-01 B1-05100AF-SWC-151-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 2.92E+01 1.94E+00 8.73E-01 Ni-63 4.55E+02 4.43E+00 1.63E+00 Sr-90 2.22E-01 3.46E-01 5.92E-01 Cs-134 -3.81E-01 8.29E-01 1.05E+00 Cs-137 3.64E+02 3.74E+01 2.15E+00 B1-05100AF-SWC-156-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.26E+01 8.81E-01 5.12E-01 Ni-63 1.15E+02 2.38E+00 1.63E+00 Sr-90 1.52E-01 3.87E-01 6.73E-01 Cs-134 -1.80E-01 2.26E-01 4.28E-01 Cs-137 2.55E+02 2.67E+01 1.19E+00

[53]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 19(continued) - Summary of FSS Concrete Core Analysis by Eberline B1-05100AF-SWC-162-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 8.61E-02 1.74E-01 3.02E-01 Ni-63 3.15E+00 1.29E+00 2.09E+00 Sr-90 3.83E-01 3.96E-01 6.61E-01 Cs-134 4.38E-02 8.92E-02 1.87E-01 Cs-137 8.89E+00 1.04E+00 4.00E-01 B1-05100AF-SWC-163-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 -5.68E-02 1.73E-01 2.53E-01 Ni-63 1.30E-01 9.64E-01 1.65E+00 Sr-90 5.62E-01 3.84E-01 6.16E-01 Cs-134 2.99E-01 2.15E-01 2.77E-01 Cs-137 -1.07E-01 2.23E-01 3.13E-01 B1-05100AF-SWC-179-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 5.60E-01 1.60E-01 3.57E-01 Ni-63 7.13E+00 1.20E+00 1.80E+00 Sr-90 3.43E-01 4.61E-01 7.83E-01 Cs-134 8.61E-03 5.00E-02 2.11E-01 Cs-137 5.14E+00 6.88E-01 4.14E-01 B1-05100AF-SWC-190-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 -4.00E-02 1.09E-01 1.73E-01 Ni-63 2.61E-01 9.67E-01 1.65E+00 Sr-90 2.35E-01 3.21E-01 5.45E-01 Cs-134 1.65E-02 7.63E-02 1.73E-01 Cs-137 1.97E-01 1.33E-01 2.02E-01 B1-05100AF-SWC-201-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 2.65E-01 1.29E-01 2.48E-01 Ni-63 1.69E+00 1.22E+00 2.03E+00 Sr-90 3.38E-01 4.88E-01 8.31E-01 Cs-134 -7.75E-03 5.26E-02 1.60E-01 Cs-137 1.87E+00 3.42E-01 2.98E-01

[54]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 20(continued) - Summary of FSS Concrete Core Analysis by Eberline B1-05100AF-SWC-210-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 2.48E-01 1.04E-01 1.64E-01 Ni-63 1.29E+00 1.21E+00 2.03E+00 Sr-90 4.75E-01 4.47E-01 7.40E-01 Cs-134 4.51E-03 6.04E-02 3.04E-01 Cs-137 2.13E+00 4.17E-01 4.48E-01 B1-05100AF-SWC-231-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 6.04E-02 1.25E-01 2.14E-01 Ni-63 9.24E-01 1.16E+00 1.94E+00 Sr-90 5.23E-01 3.82E-01 6.17E-01 Cs-134 -3.49E-01 2.49E-01 2.17E-01 Cs-137 2.87E-01 2.47E-01 3.99E-01 B1-05100AF-SFC-239-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.68E-02 5.26E-02 7.33E-02 Ni-63 5.15E-01 1.28E+00 2.18E+00 Sr-90 -9.07E-02 3.77E-01 6.90E-01 Cs-134 -4.80E-04 3.10E-02 9.19E-02 Cs-137 2.04E-02 5.38E-02 9.06E-02 B1-05100AF-SFC-250-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.38E-01 1.21E-01 1.91E-01 Ni-63 3.06E-01 9.14E-01 1.55E+00 Sr-90 -1.90E-01 3.13E-01 5.83E-01 Cs-134 -4.33E-02 5.17E-02 1.15E-01 Cs-137 7.02E-01 1.63E-01 2.90E-01 B1-05100AF-SFC-255-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.17E-01 1.36E-01 1.56E-01 Ni-63 -6.42E-01 1.18E+00 2.04E+00 Sr-90 1.18E-01 3.68E-01 6.47E-01 Cs-134 -2.73E-02 7.96E-02 2.02E-01 Cs-137 3.13E-01 1.95E-01 3.03E-01

[55]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 21(continued) - Summary of FSS Concrete Core Analysis by Eberline B1-05100AF-SFC-263-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 9.66E-02 1.17E-01 1.95E-01 Ni-63 2.71E-01 8.11E-01 1.38E+00 Sr-90 1.29E-01 2.69E-01 4.66E-01 Cs-134 -2.35E-02 5.74E-02 1.32E-01 Cs-137 4.88E-01 2.04E-01 2.91E-01 B1-05100AF-SFC-276-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 -1.44E-02 1.48E-01 1.73E-01 Ni-63 -1.01E+00 1.05E+00 1.83E+00 Sr-90 4.44E-01 3.45E-01 5.60E-01 Cs-134 -2.86E-02 4.07E-02 2.72E-01 Cs-137 -1.74E-02 1.95E-01 2.88E-01 B1-05100AF-SFC-282-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.11E-01 1.50E-01 2.70E-01 Ni-63 6.00E-01 1.00E+00 1.69E+00 Sr-90 3.22E-01 3.22E-01 5.36E-01 Cs-134 9.71E-03 7.67E-02 2.64E-01 Cs-137 3.85E-01 2.72E-01 4.28E-01 B1-05100AF-SFC-289-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 2.56E-01 8.54E-02 1.44E-01 Ni-63 2.42E+00 1.25E+00 2.05E+00 Sr-90 2.74E-01 4.16E-01 7.11E-01 Cs-134 2.20E-03 5.64E-02 1.49E-01 Cs-137 1.08E+00 2.45E-01 2.76E-01 B1-05100AF-SFC-293-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 -4.19E-02 1.68E-01 2.25E-01 Ni-63 -1.51E-01 1.12E+00 1.92E+00 Sr-90 -1.22E-01 3.39E-01 6.25E-01 Cs-134 -6.79E-03 1.28E-01 2.28E-01 Cs-137 6.79E+01 8.26E+00 6.37E-01

[56]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 22(continued) - Summary of FSS Concrete Core Analysis by Eberline B1-05100AF-SFC-300-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 5.98E-02 1.52E-01 1.89E-01 Ni-63 2.11E+00 1.16E+00 1.92E+00 Sr-90 2.14E-01 3.34E-01 5.71E-01 Cs-134 6.93E-02 8.40E-02 2.14E-01 Cs-137 9.37E-01 2.45E-01 2.56E-01 B1-05100AF-SFC-316-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.78E-02 7.91E-02 2.89E-01 Ni-63 2.21E-01 1.10E+00 1.87E+00 Sr-90 2.90E-01 4.36E-01 7.45E-01 Cs-134 -1.30E-01 1.36E-01 2.79E-01 Cs-137 1.22E+00 3.07E-01 3.55E-01 B1-05100AF-SFC-321-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.59E-02 1.51E-01 2.20E-01 Ni-63 1.39E-01 1.04E+00 1.77E+00 Sr-90 2.76E-01 3.29E-01 5.55E-01 Cs-134 8.07E-03 1.06E-01 2.19E-01 Cs-137 1.49E-01 1.20E-01 1.85E-01 B1-05100AF-SFC-326-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 2.12E-02 1.41E-01 1.71E-01 Ni-63 4.04E-01 1.21E+00 2.05E+00 Sr-90 7.69E-01 4.72E-01 7.47E-01 Cs-134 -7.73E-03 4.68E-02 2.47E-01 Cs-137 6.98E-02 1.64E-01 2.60E-01 B1-05100AF-SFC-329-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.17E-01 1.35E-01 2.37E-01 Ni-63 1.09E+00 1.27E+00 2.13E+00 Sr-90 8.94E-01 5.55E-01 8.80E-01 Cs-134 1.38E-02 6.18E-02 1.55E-01 Cs-137 3.97E+00 5.20E-01 2.64E-01

[57]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 23(continued) - Summary of FSS Concrete Core Analysis by Eberline B1-05100AF-SFC-332-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 7.43E-02 8.48E-02 1.59E-01 Ni-63 2.62E-01 9.78E-01 1.66E+00 Sr-90 2.15E-01 3.26E-01 5.57E-01 Cs-134 2.55E-02 5.65E-02 1.52E-01 Cs-137 1.99E+00 2.98E-01 3.23E-01 B1-05100AF-SFC-345-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 2.70E-02 7.95E-02 1.23E-01 Ni-63 -2.04E-01 1.00E+00 1.72E+00 Sr-90 7.83E-02 3.83E-01 6.73E-01 Cs-134 -5.06E-01 2.41E-01 1.60E-01 Cs-137 1.02E-01 7.76E-02 2.35E-01 B1-05100AF-SFC-347-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 8.11E-02 8.80E-02 1.96E-01 Ni-63 3.03E+00 1.28E+00 2.08E+00 Sr-90 2.80E-01 3.97E-01 6.77E-01 Cs-134 -7.02E-02 1.20E-01 1.69E-01 Cs-137 2.95E+00 4.56E-01 3.15E-01 B1-05100AF-SFC-348-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 4.33E-02 2.46E-01 2.68E-01 Ni-63 -3.06E-01 1.13E+00 1.94E+00 Sr-90 5.41E-01 3.60E-01 5.75E-01 Cs-134 2.53E-01 2.20E-01 3.73E-01 Cs-137 2.16E-01 2.23E-01 3.66E-01 B1-05100AF-SFC-354-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 5.04E-02 9.01E-02 1.56E-01 Ni-63 6.35E-01 1.13E+00 1.91E+00 Sr-90 2.57E-01 3.96E-01 6.78E-01 Cs-134 -2.39E-02 5.44E-02 1.73E-01 Cs-137 1.31E-01 1.00E-01 1.93E-01

[58]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 24(continued) - Summary of FSS Concrete Core Analysis by Eberline B1-05100AF-SFC-363-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 4.27E-01 1.30E-01 1.95E-01 Ni-63 3.43E+00 1.12E+00 1.79E+00 Sr-90 4.53E-01 4.38E-01 7.29E-01 Cs-134 1.42E-01 1.55E-01 2.59E-01 Cs-137 9.38E+01 9.26E+00 7.20E-01 B1-05100AF-SFC-369-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 9.59E-03 1.12E-01 1.70E-01 Ni-63 4.12E-01 9.75E-01 1.65E+00 Sr-90 3.07E-01 4.03E-01 6.83E-01 Cs-134 -8.66E-04 4.38E-02 2.10E-01 Cs-137 -3.82E-02 1.50E-01 2.17E-01 B1-05100AF-SFC-375-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 2.21E-02 1.06E-01 1.32E-01 Ni-63 2.01E+00 1.13E+00 1.86E+00 Sr-90 8.41E-02 3.62E-01 6.40E-01 Cs-134 -3.48E-03 5.86E-02 1.33E-01 Cs-137 3.31E-01 1.32E-01 2.11E-01 B1-05100AF-SFC-379-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 8.73E-02 1.51E-01 2.49E-01 Ni-63 1.84E+00 1.08E+00 1.77E+00 Sr-90 -9.43E-02 3.63E-01 6.61E-01 Cs-134 2.96E-03 6.64E-02 2.46E-01 Cs-137 7.51E-01 2.80E-01 3.81E-01 B1-05100AF-SFC-383-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 2.48E-02 1.35E-01 2.11E-01 Ni-63 7.14E-01 9.28E-01 1.56E+00 Sr-90 7.80E-02 3.22E-01 5.70E-01 Cs-134 -3.64E-02 6.92E-02 2.34E-01 Cs-137 7.00E-01 2.07E-01 2.39E-01

[59]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 25(continued) - Summary of FSS Concrete Core Analysis by Eberline B1-05100AF-SFC-411-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 -1.26E-02 3.61E-02 2.06E-01 Ni-63 1.30E+00 1.04E+00 1.74E+00 Sr-90 3.61E-01 3.89E-01 6.51E-01 Cs-134 -6.83E-01 3.11E-01 1.93E-01 Cs-137 5.42E-01 2.10E-01 2.86E-01 B1-05100AF-SFC-433-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.43E+01 9.42E-01 4.16E-01 Ni-63 5.91E+02 5.52E+00 1.86E+00 Sr-90 4.24E-01 3.83E-01 6.31E-01 Cs-134 -2.75E-01 2.33E-01 3.04E-01 Cs-137 5.46E+01 5.78E+00 8.27E-01 B1-05100AF-SFC-434-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 1.24E+01 8.39E-01 3.44E-01 Ni-63 8.26E+01 2.17E+00 1.70E+00 Sr-90 9.17E-02 3.34E-01 5.88E-01 Cs-134 -1.17E-01 1.73E-01 2.68E-01 Cs-137 8.57E+01 8.41E+00 6.18E-01 B1-05100AF-SFC-435-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 3.68E-02 1.22E-01 1.63E-01 Ni-63 5.00E-01 1.01E+00 1.72E+00 Sr-90 3.87E-01 4.00E-01 6.68E-01 Cs-134 1.01E-03 4.22E-02 1.94E-01 Cs-137 1.37E-01 1.46E-01 2.45E-01 B1-05100AF-SFC-436-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 -5.21E-02 1.28E-01 2.44E-01 Ni-63 9.96E-01 1.19E+00 2.00E+00 Sr-90 -1.92E-01 3.97E-01 7.39E-01 Cs-134 -3.55E-01 2.55E-01 2.24E-01 Cs-137 7.93E-02 1.93E-01 2.96E-01

[60]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Table 26(continued) - Summary of FSS Concrete Core Analysis by Eberline B1-05100AF-SFC-438-CV Result Uncertainty MDC ROC (pCi/g) (pCi/g) (pCi/g)

Co-60 2.07E+00 2.22E-01 2.05E-01 Ni-63 3.82E+00 1.13E+00 1.80E+00 Sr-90 5.40E-02 3.45E-01 6.13E-01 Cs-134 -4.11E-01 3.12E-01 2.02E-01 Cs-137 1.95E+02 2.04E+01 8.88E-01

8. QUALITY CONTROL Twenty-three (23) replicate measurements were taken during the FSS of this basement structure. The measurement results were evaluated using NRC acceptance criteria specified in Inspection Procedure No. 84750, Radioactive Waste Treatment, and Effluent and Environmental Monitoring (Reference 15). Twenty-one (21) of the replicate measurements had an acceptable difference when compared to the original measurement at that location. Two (2) replicate measurements at wall locations 74 & 116 did not have acceptable difference for Cs-137 when compared to the original measurement.

ISOCS measurement location 74 (B1-05100AF-SWC-074-GD) identified Cs-137 activity at 1.72E+04 pCi/m2, which was less than the MDC (3.09E+04 pCi/m2) and only 0.048%

of the OpDCGL for Cs-137. However, when comparing K-40 results, there was an acceptable agreement between the standard and comparison samples.

ISOCS measurement location 116 (B1-05100AF-SWC-116-GD) identified Cs-137 activity at 4.57E+04 pCi/m2, which was greater than the MDC (5.32E+03 pCi/m2) but only 0.128% of the OpDCGL for Cs-137. There is not acceptable agreement between the standard and comparison measurements. K-40 was also used to determine whether the measurement was acceptable. However, K-40 in the aforementioned sample was also less than the MDC and also did not have an acceptable agreement between the standard measurement and the QC measurement. Pre and post use operational checks of the ISOCS did not indicate any issues with the instrument or the quality of the data. In addition, other replicate measurements taken at several other locations were in agreement. Consequently, it was decided that no further action was necessary. Refer to Attachment 4 for data and quality control analysis results.

9. INVESTIGATIONS AND RESULTS During FSS activities, five (5) investigation ISOCS measurements were taken within the Auxiliary Building, one (1) wall location and four (4) floor locations. These measurements were taken due to uneven surfaces (ruts, trenches, holes, etc.). The results

[61]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 of these measurements are summarized in Table 16 of this report. These five (5) investigative measurements employed the same ISOCS geometry but the detector to source distance was reduced by 1 foot to account for the uneven surface being measured while not accounting for this in the ISOCS efficiency model to ensure that the measurement results are conservative.

In each of the five (5) investigation ISOCS measurements taken, the reduced source to detector distance did not appreciably change the original measurement result. The OpSOF for each individual investigation measurement when compared against the OpDCGL was less that one. Refer to Attachment 5 for Investigation sample results. See Photograph 2 for an example of an investigative ISOCS measurement location.

Photograph 2 - Example of Auxiliary Building Investigative ISOCS Measurement Location

10. REMEDIATION AND RESULTS Chapter 4 of the ZSRP LTP states that remediation beyond that required to meet the release criteria is unnecessary and that the remaining residual radioactivity in structures was ALARA.

Once the area was turned over for FSS, no remedial activities were performed within the Auxiliary Building. However, during the FSS survey of the Unit 1 Containment penetrations numbers T123 & T124 in April of 2018, debris fell out of the penetrations and onto the Auxiliary Building basement floor. The floor and adjacent wall were surveyed and indicated 15,000 dpm/100 cm2 direct frisk and <1,000 dpm/100 cm2 removable. A direct reading on the adjacent wall indicated 1.4 mR/hr (fixed). The debris was removed and follow-up surveys indicated <1,000 dpm/100 cm2 (direct frisk) and

[62]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100

<1,000 dpm/100 cm2 (removable). This incident was captured and documented on April 9, 2018 through the generation of Condition Report ES-ZION-CR-2018-0510.

In May of 2018, remediation work was performed on the Spent Fuel Pool (SFP) pad, which was located adjacent to the west boundary of the Auxiliary Building. The potential for the remedial activities to radiologically impact the Auxiliary Building basement floor and walls existed. Therefore, Remedial Action Support Survey (RASS) B1-05100ZF was developed to verify that the events described in the CR and the SFP remediation did not change the radionuclide inventory identified in the Auxiliary Building basement FSS survey.

The results of the RASS indicated that neither the CR events nor the SFP remedial activities adversely affected the Auxiliary Building basement FSS.

Twenty-five (25) ISOCS measurement locations on the floor and walls were re-assessed using ISOCS direct measurements at the same locations that were analyzed previously.

The re-survey results were compared to the original (FSS) measurements. The comparison indicated the following:

• Five (5) locations exhibited Cs-134 levels >20% more than the original levels identified during FSS. However, all five (5) measurements were less than the OpSOF and therefore of minimal dose significance.

• Three (3) locations exhibited Cs-137 levels >20% more than the original levels identified during FSS, with the maximum being a 50.5% increase.

• Eight (8) locations exhibited Co-60 levels >20% more than the original levels identified during FSS, with the maximum being a 203% increase.

The ISOCS RASS results are summarized in Attachment 6 of this document. The average difference between the twenty-five (25) original ISOCS measurements and the corresponding RASS measurements for Co-60 was +12.3%. The average difference between the twenty-five (25) original ISOCS measurements and the corresponding RASS measurements for Cs-137 was -14.3%. Since Cs-137 has a much greater abundance in the isotopic mix identified in Table 5, the lower readings for Cs-137 had a much greater effect on the OpSOF than Co-60. The mean OpSOF for the 25 sample results for the RASS was 0.13, as compared to the OpSOF for the original FSS results which was 0.17.

Therefore, neither the event described in CR ES-ZION-ACT-2018-0510 nor the SFP remediation had any measurable effect on survey unit 05100 FSS data.

11. CHANGES FROM THE SURVEY PLAN Although the survey plan was not changed, the methodology for accepting control of the area and performing the FSS survey was modified due to weather considerations. Ice and

[63]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 snow removal as well as water management of the entire surface area that encompasses survey unit 05100 was not feasible. Therefore, a segmented approach was used to allow segments of the Auxiliary Building basement to be turned over to FSS. Prior to the onset of the inclement weather, a series of three comprehensive surveys were performed in the Auxiliary Building basement on December 20, 2017, and December 21, 2017, in support of the demolition contractors effort to prepare the basement for turnover to the C/LT group for FSS. During this time, several items were identified for remediation and any identified loose surface contamination was cleaned. A follow up survey was performed to determine the effectiveness of cleanup effort throughout the Auxiliary Building basement which included sixty-five (65) smear samples. All sixty-five (65) smears were less than 1,000 dpm/100 cm2. These surveys provided sufficient assurance that the source term in the Auxiliary Building was fixed and any movement of water or ice would not transport source term from its end state location. The Auxiliary Building basement surface area was separated into seven (7) segments. Each segment was prepared for FSS individually (segment 1, segment 2,). When a segment was ready for FSS, isolation and controls were established in accordance with ZionSolutions procedure ZS-LT-300-001-003. Once FSS was performed on a segment of the basement, the area was placed under isolation and control by FSS to ensure that preparatory functions within other areas of the Auxiliary Building basement would not impact previously completed segments of the Auxiliary Building.

Several minor changes were made to the FSS plan. The changes were as follows:

• The number of Hard to Detect (HTD) sample locations were increased from forty-two (42) to forty-six (46) to ensure the minimum number of 10% required by the LTP.

• The HTD core bore sample locations were changed from every 10th ISOCS location to random locations (totaling 10% of the total number of ISOCS measurements). The forty-six (46) locations were selected from floor and lower wall ISOCS locations, per the LTP, to allow for safe sample collection.

• Some sample locations were eliminated due to differences in the FSS survey package and the actual conditions observed in the field.

• Some measurement locations were added to ensure 100% areal coverage within the survey unit.

12. FINAL STATUS SURVEY PLAN There were no addendums to the FSS plan.

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100

13. DATA QUALITY ASSESSMENT (DQA)

The DQO sample design and data were reviewed in accordance with ZionSolutions procedure ZS-LT-300-001-004, Final Status Survey Data Assessment (Reference 16) for completeness and consistency. Documentation was complete and legible. Surveys and the collection of measurements were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 1. The survey design had adequate power as indicated by the Retrospective Power Curve (see Attachment 6).

The analytical results indicated four hundred and nine (409) out of four hundred and twenty-five (425) measurements were less than a SOF of one (1). Sixteen (16) locations were identified with a SOF > one (1). An analysis of each of the aforementioned measurements is provided in Attachment 6.

Forty-six (46) concrete core samples were analyzed off site for HTD radionuclides as part of the FSS of survey unit 05100. The results indicated that Cs-137 was positively detected in twenty-nine (29) of the forty six (46) samples, twenty (20) out of the forty six (46) samples had positive results for both Ni-63 and Co-60 and one (1) sample had positive results for both Sr-90 and Cs-137. The maximum Ni-63 to Co-60 ratio for the positive samples was for sample location B1-05100AF-SFC-433-CV which exhibited a Ni-63/Co-60 ratio of 41.46, which is less than the maximum ratio from LTP Chapter 5, Table 5-15.

The maximum Sr-90 to Cs-137 ratio was for sample location B1-05100AF-SFC-329-CV.

In that sample, a ratio of 0.2 was derived for Sr-90/Cs-137. The Sr-90 result, while greater than the MDC was within the range of uncertainty and believed to be a false-positive result. The sample was re-analyzed and the results indicated that Sr-90 was no longer positively identified.

The Sign Test (Attachment 3) was performed on the data and compared to the original assumptions of the DQOs. The evaluation of the Sign Test results clearly demonstrates that the survey unit passed the unrestricted release criteria, thus, the null hypothesis was rejected.

The preliminary data review consisted of calculating basic statistical quantities (e.g.,

mean, median, standard deviation). All data was considered valid including negative values, zeros, values reported below the MDC, and values with uncertainties that exceeded two standard deviations. The mean and median values for each ROC were well below the respective OpDCGLs. Also, the retrospective power curve showed that a sufficient number of samples were collected to achieve the desired power. Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs.

The data for Co-60 and Cs-137 is represented graphically through a frequency plot and a quantile plot. All graphical representations are provided in Attachment 6.

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100

14. ANOMALIES No anomalies were observed during the performance or analyses of the survey.

15. COMPLIANCE EQUATION There are four distinct source terms for the end-state at Zion: backfilled basements, soil, buried piping and groundwater. Demonstrating compliance with the dose criterion requires the summation of dose from the four source terms (see Equation 6-11 from LTP Chapter 6, section 6-17).

The final compliance dose will be calculated using LTP Equation 6-11 after FSS has been completed in all survey units. The results of the FSS performed for each FSS unit will be reviewed to determine the maximum dose from each of the four source terms (e.g.,

basement, soil, buried pipe and existing groundwater if applicable) using the mean BcSOF of FSS systematic results plus the dose from any identified elevated areas. The compliance dose must be less than 25 mrem/yr. The dose contribution from each ROC is accounted for using the BcSOF to ensure that the total dose from all ROC does not exceed the dose criterion.

The term for each basement includes the dose contributions from wall and floor surfaces within the basement, the dose contribution from embedded pipe within the basement, the dose contribution from penetrations within the basement and the dose contribution from concrete fill in the basement when clean concrete debris was used as fill. Each (structural surfaces, embedded pipe and penetrations) are surveyed separately during FSS. The dose from clean concrete fill is predetermined in accordance with LTP Chapter 5, Table 5-16, which is conservatively based on a maximum allowable MDC of 5,000 dpm/100cm2. The dose from fill assigned to the Auxiliary Building basement is 0.99 mrem/yr, which equates to a SOF of 0.0396.

LTP Chapter 6, section 6.4.5 requires that the dose from penetrations be added to each Basement that the penetrations interfaces with. The penetrations in the Auxiliary Building interface with both with the Unit 1 and Unit 2 Containment Buildings and with the Turbine Building. The dose from penetrations interfacing between the Auxiliary Building and both Unit 1 and Unit 2 Containments is derived in the Release Records for both Unit 1 Containment Penetrations and Unit 2 Containment penetrations. The dose from penetrations interfacing between the Auxiliary Building and the Turbine Building is derived in the Release Record for the Auxiliary Building Penetrations.

After the FSS of all dose components in a given basement is complete and all dose component survey units pass the Sign Test, the SOF for each dose component is calculated using Equations 5-5 or 5-6 as applicable from LTP Chapter 5, section 5.5.4. For the

[66]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building structural surfaces, sixteen (16) elevated areas were identified by the compliance survey (elevated areas are defined as areas exceeding the OpDCGL but less than the BcDCGL). The mean BcSOF for the Auxiliary Building structural surfaces, adjusted for the elevated measurements is 0.075, which equates to a dose of 1.868 mrem/yr.

Basement surface area adjustments (i.e., increases) were applied to the DCGL calculation for certain basements to ensure that the DCGLs accounted for the contribution of residual radioactivity from basements/structures that cannot, on their own, support a water supply well but, were hydraulically connected to a basement that could support a well. In accordance with LTP section 5.5.6.1, this adjustment must be made to the Auxiliary Building structural BcSOF due to its hydraulic conductivity with the SFP/Transfer Canal FSS unit. Area weighting using Equation 5-8 from LTP Chapter 5, section 5.5.6.1 was used to sum the residual activity in the Auxiliary Building structure and the SFP/Transfer Canal structure on an area-weighted basis. The BcSOF for the SFP/Transfer Canal is 0.039. The derivation of this value is documented in the Release Record for the SFP/Transfer Canal structure. LTP Chapter 5, section 5.5.6.1, Table 5-23 states that the total area for the Auxiliary Building plus the area of the SFP/Transfer Canal is 7,226 m2 and the stand-alone area of the SFP/Transfer Canal is 723 m2. The result is provided in Equation 7.

Equation 7 723 (0.039) = 0.004 7226 The SOF of 0.004 is added to the adjusted mean BcSOF of 0.075 for the Auxiliary Building to derive the adjusted BcSOF of 0.079 for the Auxiliary Building basement structure. This equates to a dose of 1.966 mrem/yr. The adjusted BcSOF for the Auxiliary Building structure is then used in the following equation to calculate BcSOFBASEMENT for the Auxiliary Building.

Equation 8 Bc = + + +

where:

BcSOFBASEMENT = BcSOF (mean of FSS systematic results plus the dose from any identified elevated areas) for backfilled basements BcSOFB = BcSOF for structural survey unit(s) within the basement (mean of FSS systematic results plus the dose from any identified elevated areas)

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 BcSOFEP = BcSOF for embedded pipe survey unit(s) within the basement (mean of FSS systematic results plus the dose from any identified elevated areas)

BcSOFPN = BcSOF for penetration survey unit(s) within the basement (mean of FSS systematic results plus the dose from any identified elevated areas) and connected basements SOFCF = SOF for clean concrete fill (if applicable) based on maximum MDC during URS The variable for BcSOFPN for the Auxiliary Building penetrations shared with the Turbine Building is 0.002. The derivation of this value is documented for the Auxiliary Building Penetrations Release Record (B1-05120A).

The adjusted mean BcSOFPN value for the Unit 1 Containment/Auxiliary Building shared penetrations is 0.059. The derivation of this value is documented in the Unit 1 Containment Penetration Release Record (B1-01112A).

The mean BcSOFPN value for the Unit 2 Containment/Auxiliary Building shared penetrations is 0.008. The derivation of this value is documented in the Unit 2 Containment Penetration Release Record (B1-02112A). The total BcSOFPN value, combining the shared penetrations from Unit 1 Containment, Unit 2 Containment and the Turbine Building is 0.069.

The value for embedded pipe in the Auxiliary Building is from the floor drain pipe embedded in the concrete floor of the 542 foot elevation. From the Release Record for the Auxiliary Building Embedded Floor Drain Pipe, the BcSOFEP value is 0.007.

The BcSOFBASEMENT value for the Unit 2 Containment is then derived as follows; Equation 9

= 0.079 + 0.069 + 0.007 + 0.040 = 0.195 The BcSOFBASEMENT for the Auxiliary Building basement is 0.195. This SOF equates to a dose of 4.865 mrem/yr TEDE to an AMCG from residual radioactivity in the Auxiliary Building basement.

16. CONCLUSION Survey unit 05100 has met the DQOs of the FSS plan. The ALARA criteria as specified in Chapter 4 of the LTP were achieved. The EMC is not applicable to structural surfaces.

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 All identified ROC were used for statistical testing to determine the adequacy of the survey unit for FSS. Evaluation of the data shows that sixteen (16) of the ROC concentration values exceeded the OpDCGL. However, none of the values exceeded the BcDCGLs for the ROC. Additionally, the sixteen (16) elevated locations were evaluated, (see Table 14) and the dose was included in the total dose for the survey unit.

The total mean BcSOF for the Auxiliary Building basement structure is 0.079, which is the sum of mean BcSOF from the Auxiliary Building adjusted to account for elevated measurements and residual radioactivity in the SFP/Transfer Canal on an area-weighted basis. The total dose contribution from the Auxiliary Building basement structure, including dose from penetrations, embedded pipe and fill is 4.865 mrem/yr TEDE (BcSOFBASEMENT = 0.195).

The sample data passed the Sign Test. The null hypothesis was rejected. The Retrospective Power Curve showed that adequate power was achieved. The survey unit is properly classified as Class 1. Therefore, in accordance with the LTP Section 5.10, the survey unit meets the release criterion. Survey unit 05100 is acceptable for unrestricted release. See Photograph 3 for aerial view of Auxiliary Building.

Photograph 3 - Aerial View of the Auxiliary Building

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100

17. REFERENCES

1. ZionSolutions procedure ZS-LT-300-001-005, Final Status Survey Data Reporting

2. Zion Station Restoration Project License Termination Plan

3. ZionSolutions procedure ZS-LT-300-001-001, Final Status Survey Package Development

4. NUREG-1575, Multi-Agency Radiation Survey and Site Investigation Manual

5. ZionSolutions TSD 17-004, Operational Derived Concentration Guideline Levels for Final Status Survey

6. Zion Station Historical Site Assessment

7. ZionSolutions TSD 14-028, Radiological Characterization Report

8. ZionSolutions TSD 14-019, Radionuclides of Concern for Soil and Basement Fill Model Source Terms

9. ZionSolutions procedure ZS-LT-300-001-002, Survey Unit Classification

10. ZionSolutions TSD 11-001, Technical Support Document for Potential Radionuclides of Concern During the Decommissioning of the Zion Station

11. ZionSolutions ZS-LT-01, Quality Assurance Project Plan (for Characterization and FSS)

12. ZionSolutions TSD 14-022, Use of In-Situ Gamma Spectroscopy for Final Status Survey of End State Structures

13. ZionSolutions procedure ZS-LT-300-001-003, Isolation and Control for Final Status Survey

14. ZionSolutions TSD 17-003, Evaluation of Efficiency Calibration Geometries for In-Situ Gamma Spectrometry During Final Status Surveys

15. U.S. NRC Inspection Procedure No. 84750, Radioactive Waste Treatment, and Effluent and Environmental Monitoring

16. ZionSolutions procedure ZS-LT-300-001-004, Final Status Survey Data Assessment

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100

18. ATTACHMENTS Attachment 1 - Figures and Maps Attachment 2 - ISOCS Geometries Attachment 3 - Sign Test Attachment 4 - QA Information and Charts/QC Replicate Measurement Assessments Attachment 5 - Auxiliary Building ISOCS Measurements Attachment 6 - Graphical Presentations and Supplemental Information Attachment 7 - ISOCS Reports Attachment 8 - Eberline Reports

[71]

ATTACHMENT 1 FIGURES AND MAPS

[72]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 1 - Auxiliary Building Basement ISOCS Measurement Locations

[73]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 2 - Auxiliary Building Basement Floor ISOCS Measurement Locations

[74]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 3 - Auxiliary Building Basement FSS ISOCS Measurement Locations - Wall A

[75]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 4 - Auxiliary Building Basement FSS Measurement Locations -Wall B

[76]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 5 - Auxiliary Building Basement FSS Measurement Locations - Wall C

[77]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 6 - Auxiliary Building Basement FSS Measurement Locations - Walls D & E

[78]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 7 - Auxiliary Building Basement FSS Measurement Locations - Walls F & G

[79]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 8 - Auxiliary Building Basement FSS Measurement Locations - Walls H & I

[80]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 9 - Auxiliary Building Basement FSS Measurement Locations - Walls J & K

[81]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 10 - Auxiliary Building Basement FSS Measurement Locations - Wall L

[82]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 11 - Auxiliary Building Basement FSS Measurement Locations - Walls M & N

[83]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 11 - Auxiliary Building Basement FSS Measurement Locations - Walls O & P

[84]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 12 - Auxiliary Building Basement FSS Measurement Locations - Walls Q & R

[85]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 13 - Auxiliary Building Basement FSS Measurement Locations - Walls S & T

[86]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 14 - Auxiliary Building Basement Measurement Locations - Wall U

[87]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 15 - Auxiliary Building Basement Measurement Locations - Wall V

[88]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Figure 16 - Concrete Core Sample Locations for FSS

[89]

ATTACHMENT 2 ISOCS Geometries

[90]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 AUXILIARY BUILDING ISOCS GEOMETRIES The CP template applies to surface volumes which contain levels of contamination that are subject to variations in activity over depth. This source term geometry can be conservatively modeled by single or multiple contaminated source term layers from the surface to a given depth (in this case, 2.0 inches that correspond to the observed contamination depth from the characterization data).

Additional Geometries Two locations within the Auxiliary Building Basement footprint were identified based on their unique physical characteristics. The first location was the Elevator Pit, which is a poured concrete box in the floor of the 542 foot elevation of the Auxiliary Building. The pit is approximately 9 feet long by 9 feet wide by 5 feet 8 inches deep. The second location identified was Sump B, which is also on the Auxiliary Building floor on the 542 foot elevation adjacent to the G wall. Sump B is a steel lined pit (liner is intact) that is approximately 9 feet long by 8 feet wide by 6 feet deep. Note that there was a second sump in the Auxiliary Building Basement denoted as Sump A. This sump was previously filled to the floor elevation with grout.

Auxiliary Building Geometries The results of the gamma spectroscopic analysis of the 1/2 inch pucks indicated that twenty-nine (29) of the thirty-two (32) sample locations did not exhibit activity greater than 0.1 SOF below a depth of 2 inches (see Tables 1 through 4).

As a result of this analysis, the geometries selected for the floor and lower walls were as follows:

• 4M 90D_CP_2in - Which corresponds to a 4 meter source to detector distance, 90 circular plane, 2.0 inch concrete depth

• 3M 90D_CP_2in - Which corresponds to a 3 meter source to detector distance, 90 circular plane, 2.0 inch concrete depth

• 2.5M 90D_CP_2in wall - Which corresponds to a 2.5 meter source to detector distance, 90 circular plane, 2.0 inch concrete depth The varied source to detector distance was necessary to ensure 100% areal coverage in some areas.

Two (2) additional geometries were utilized within the Auxiliary Building basement. These geometries were used because they would provide a more accurate representation of the activity present in those areas based on the physical geometry and/or construction. These special geometries were as follows:

• Elevator Pit - Based on the configuration and construction of the pit, a Rectangular Plane geometry template was used to determine the activity present from the concrete floor and walls of the Elevator Pit.

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100

• Sump B - Based on the configuration and construction of the sump, a Room/Box geometry template was used to determine the activity present on the floor and wall surfaces of Sump B.

The sump floor was modeled to contain 60% of the activity and each of the four (4) walls modeled to contain 10% of the activity present within the sump.

Sump A was previously grouted to floor level. Therefore, a special geometry was not necessary for this sump.

[92]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: 4M90D CP_2in

[93]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: 4M90D CP_2in (continued)

[94]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: 4M90D CP_2in (continued)

[95]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: 3M90D CP_2in

[96]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: 3M90D CP_2in (continued)

[97]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: 3M90D CP_2in (continued)

[98]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: 2.5M90D CP_2in

[99]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: 2.5M90D CP_2in (continued)

[100]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: 2.5M90D CP_2in (continued)

[101]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: Elevator Pit

[102]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: Elevator Pit (continued)

[103]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: Elevator Pit (continued)

[104]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: Sump B

[105]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: Sump B (continued)

[106]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Geometries: Sump B (continued)

[107]

ATTACHMENT 3 SIGN TEST

[108]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 SIGN TEST Survey Area 05100 Description Auxiliary Building Survey Unit B1-05100A-F Description Auxiliary Building Classification 1 Type I Error 0.05 Number of Measurements 425

1. SOF 1-WS Sign # SOF 1-WS Sign (WS) (WS) 1 0.0095 0.99 +1 33 0.0134 0.99 +1 2 0.0066 0.99 +1 34 0.0313 0.97 +1 3 0.0090 0.99 +1 35 0.0536 0.95 +1 4 0.0042 1.00 +1 36 0.2406 0.76 +1 5 0.0059 0.99 +1 37 0.1381 0.86 +1 6 0.0067 0.99 +1 38 0.0644 0.94 +1 7 0.0035 1.00 +1 39 0.0194 0.98 +1 8 0.0033 1.00 +1 40 0.0109 0.99 +1 9 0.0027 1.00 +1 41 0.0078 0.99 +1 10 0.0028 1.00 +1 42 0.0089 0.99 +1 11 0.0032 1.00 +1 43 0.1134 0.89 +1 12 0.0091 0.99 +1 44 0.1593 0.84 +1 13 0.0038 1.00 +1 45 0.0608 0.94 +1 14 0.0026 1.00 +1 46 0.0168 0.98 +1 15 0.0014 1.00 +1 47 0.0114 0.99 +1 16 0.0025 1.00 +1 48 0.0107 0.99 +1 17 0.0055 0.99 +1 49 0.0758 0.92 +1 18 0.0018 1.00 +1 50 0.1306 0.87 +1 19 0.0044 1.00 +1 51 0.1255 0.87 +1 20 0.0042 1.00 +1 52 0.2405 0.76 +1 21 0.0059 0.99 +1 53 0.0549 0.95 +1 22 0.0065 0.99 +1 54 0.0383 0.96 +1 23 0.0028 1.00 +1 55 0.0759 0.92 +1 24 0.0075 0.99 +1 56 0.0582 0.94 +1 25 0.0052 0.99 +1 57 0.0069 0.99 +1 26 0.0023 1.00 +1 58 0.0197 0.98 +1 27 0.0040 1.00 +1 59 0.0179 0.98 +1 28 0.0046 1.00 +1 60 0.0332 0.97 +1 29 0.0078 0.99 +1 61 0.0022 1.00 +1 30 0.0183 0.98 +1 62 0.0038 1.00 +1 31 0.0087 0.99 +1 63 0.0016 1.00 +1 32 0.0052 0.99 +1 64 0.0047 1.00 +1

[109]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 SIGN TEST (Continued)

1. SOF 1-WS Sign # SOF 1-WS Sign (WS) (WS) 65 0.0061 0.99 +1 104 0.0070 0.99 +1 66 0.0024 1.00 +1 105 0.0707 0.93 +1 67 0.0023 1.00 +1 106 0.0721 0.93 +1 68 0.0035 1.00 +1 107 0.0858 0.91 +1 69 0.0041 1.00 +1 108 0.0044 1.00 +1 70 0.0047 1.00 +1 109 0.0049 1.00 +1 71 0.0037 1.00 +1 110 0.0102 0.99 +1 72 0.0072 0.99 +1 111 0.0020 1.00 +1 73 0.0067 0.99 +1 112 0.0157 0.98 +1 74 0.0026 1.00 +1 113 0.0079 0.99 +1 75 0.0033 1.00 +1 114 0.0240 0.98 +1 76 0.0033 1.00 +1 115 0.0020 1.00 +1 77 0.0035 1.00 +1 116 0.0108 0.99 +1 78 0.0030 1.00 +1 117 0.0005 1.00 +1 79 0.0020 1.00 +1 118 0.0006 1.00 +1 80 0.0011 1.00 +1 119 0.0036 1.00 +1 81 0.0285 0.97 +1 120 0.0037 1.00 +1 82 0.0612 0.94 +1 121 0.0026 1.00 +1 83 0.0473 0.95 +1 122 0.0041 1.00 +1 84 0.0240 0.98 +1 123 0.0030 1.00 +1 85 0.0229 0.98 +1 124 0.0307 0.97 +1 86 0.0275 0.97 +1 125 0.0014 1.00 +1 87 0.0209 0.98 +1 126 0.0195 0.98 +1 88 0.0370 0.96 +1 127 0.1336 0.87 +1 89 0.0311 0.97 +1 128 0.0253 0.97 +1 90 0.0112 0.99 +1 129 0.0040 1.00 +1 91 0.0058 0.99 +1 130 0.0561 0.94 +1 92 0.0304 0.97 +1 131 0.0230 0.98 +1 93 0.0239 0.98 +1 132 0.0083 0.99 +1 94 0.0029 1.00 +1 133 0.0762 0.92 +1 95 0.0047 1.00 +1 134 0.1212 0.88 +1 96 0.0720 0.93 +1 135 0.0923 0.91 +1 97 0.0256 0.97 +1 136 0.0871 0.91 +1 98 0.0748 0.93 +1 137 0.0492 0.95 +1 99 0.0100 0.99 +1 138 0.0316 0.97 +1 100 0.0038 1.00 +1 139 0.1277 0.87 +1 101 0.2739 0.73 +1 140 0.2253 0.77 +1 102 0.0257 0.97 +1 141 0.5791 0.42 +1 103 0.0043 1.00 +1 142 0.1876 0.81 +1

[110]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 SIGN TEST (Continued)

1. SOF 1-WS Sign # SOF 1-WS Sign (WS) (WS) 143 0.0703 0.93 +1 182 0.0058 0.99 +1 144 0.0581 0.94 +1 183 0.1817 0.82 +1 145 0.1732 0.83 +1 184 0.0664 0.93 +1 146 0.3478 0.65 +1 185 0.0308 0.97 +1 147 0.0259 0.97 +1 186 0.1802 0.82 +1 148 0.0160 0.98 +1 187 0.0265 0.97 +1 149 0.0083 0.99 +1 188 0.0253 0.97 +1 150 0.0167 0.98 +1 189 1.0817 (0.08) -1 151 0.0110 0.99 +1 190 1.2501 (0.25) -1 152 0.0729 0.93 +1 191 1.1173 (0.12) -1 153 0.1386 0.86 +1 192 0.0236 0.98 +1 154 0.0180 0.98 +1 193 0.2413 0.76 +1 155 0.0913 0.91 +1 194 0.2084 0.79 +1 156 0.0983 0.90 +1 195 0.1163 0.88 +1 157 0.0399 0.96 +1 196 0.0132 0.99 +1 158 0.0341 0.97 +1 197 1.0038 (0.00) -1 159 0.0667 0.93 +1 198 0.0754 0.92 +1 160 0.0835 0.92 +1 199 0.0309 0.97 +1 161 0.0363 0.96 +1 200 0.0284 0.97 +1 162 0.0390 0.96 +1 201 0.0110 0.99 +1 163 0.0677 0.93 +1 202 0.0169 0.98 +1 164 0.1836 0.82 +1 203 0.0151 0.98 +1 165 0.0561 0.94 +1 204 0.0334 0.97 +1 166 0.0253 0.97 +1 205 0.0326 0.97 +1 167 0.0089 0.99 +1 206 0.0047 1.00 +1 168 0.0089 0.99 +1 207 0.0054 0.99 +1 169 0.0389 0.96 +1 208 0.0073 0.99 +1 170 0.0662 0.93 +1 209 0.0081 0.99 +1 171 0.0087 0.99 +1 210 0.0042 1.00 +1 172 0.0076 0.99 +1 211 0.0042 1.00 +1 173 0.0056 0.99 +1 212 0.0062 0.99 +1 174 0.0026 1.00 +1 213 0.0127 0.99 +1 175 0.0035 1.00 +1 214 0.0113 0.99 +1 176 0.0057 0.99 +1 215 0.0060 0.99 +1 177 0.0059 0.99 +1 216 0.0108 0.99 +1 178 0.0061 0.99 +1 217 0.0084 0.99 +1 179 0.2598 0.74 +1 218 0.0061 0.99 +1 180 0.0042 1.00 +1 219 0.0085 0.99 +1 181 0.0047 1.00 +1 220 0.0155 0.98 +1

[111]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 SIGN TEST (Continued)

1. SOF 1-WS Sign # SOF 1-WS Sign (WS) (WS) 221 0.0079 0.99 +1 260 0.0919 0.91 +1 222 0.0092 0.99 +1 261 0.0275 0.97 +1 223 0.0070 0.99 +1 262 0.0128 0.99 +1 224 0.0063 0.99 +1 263 0.0114 0.99 +1 225 0.0074 0.99 +1 264 0.0079 0.99 +1 226 0.0116 0.99 +1 265 0.0132 0.99 +1 227 0.0127 0.99 +1 266 0.1212 0.88 +1 228 0.0065 0.99 +1 267 0.2014 0.80 +1 229 0.0070 0.99 +1 268 0.1638 0.84 +1 230 0.0087 0.99 +1 269 0.2443 0.76 +1 231 0.0040 1.00 +1 270 0.4853 0.51 +1 232 0.0075 0.99 +1 271 0.3870 0.61 +1 233 0.0113 0.99 +1 272 0.5651 0.43 +1 234 0.0115 0.99 +1 273 0.4060 0.59 +1 235 0.0159 0.98 +1 274 0.0501 0.95 +1 236 1.7757 (0.78) -1 275 1.2510 (0.25) -1 237 1.5759 (0.58) -1 276 0.5873 0.41 +1 238 1.5706 (0.57) -1 277 0.5921 0.41 +1 239 2.0335 (1.03) -1 278 0.9200 0.08 +1 240 1.9089 (0.91) -1 279 0.0737 0.93 +1 241 0.1171 0.88 +1 280 0.0596 0.94 +1 242 0.0880 0.91 +1 281 0.0499 0.95 +1 243 0.0126 0.99 +1 282 0.0826 0.92 +1 244 0.0099 0.99 +1 283 0.0883 0.91 +1 245 0.0106 0.99 +1 284 0.1885 0.81 +1 246 0.0137 0.99 +1 285 0.2399 0.76 +1 247 0.0118 0.99 +1 286 0.1711 0.83 +1 248 0.0243 0.98 +1 287 0.2845 0.72 +1 249 0.1801 0.82 +1 288 0.3423 0.66 +1 250 0.2015 0.80 +1 289 0.2425 0.76 +1 251 0.3483 0.65 +1 290 0.0079 0.99 +1 252 0.5965 0.40 +1 291 0.0103 0.99 +1 253 2.1603 (1.16) -1 292 0.0128 0.99 +1 254 2.1725 (1.17) -1 293 0.0121 0.99 +1 255 0.7498 0.25 +1 294 0.0223 0.98 +1 256 0.2408 0.76 +1 295 0.0503 0.95 +1 257 0.2753 0.72 +1 296 0.0240 0.98 +1 258 0.3562 0.64 +1 297 0.0176 0.98 +1 259 0.1176 0.88 +1 298 0.0393 0.96 +1

[112]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 SIGN TEST (Continued)

1. SOF 1-WS Sign # SOF 1-WS Sign (WS) (WS) 299 0.1286 0.87 +1 338 0.5505 0.45 +1 300 0.1504 0.85 +1 339 0.2373 0.76 +1 301 0.3841 0.62 +1 340 0.0601 0.94 +1 302 0.0396 0.96 +1 341 0.0608 0.94 +1 303 0.0244 0.98 +1 342 0.0470 0.95 +1 304 0.0822 0.92 +1 343 0.0662 0.93 +1 305 0.0844 0.92 +1 344 0.0538 0.95 +1 306 0.5466 0.45 +1 345 0.0510 0.95 +1 307 0.1222 0.88 +1 346 0.0441 0.96 +1 308 0.0376 0.96 +1 347 0.1360 0.86 +1 309 0.0478 0.95 +1 348 0.0899 0.91 +1 310 0.0180 0.98 +1 349 0.1900 0.81 +1 311 0.0288 0.97 +1 350 0.1122 0.89 +1 312 0.0708 0.93 +1 351 0.0999 0.90 +1 313 0.0195 0.98 +1 352 0.3299 0.67 +1 314 0.1289 0.87 +1 353 0.0836 0.92 +1 315 0.0627 0.94 +1 354 0.0917 0.91 +1 316 0.0609 0.94 +1 355 0.0509 0.95 +1 317 0.0665 0.93 +1 356 0.0510 0.95 +1 318 0.0656 0.93 +1 357 0.1436 0.86 +1 319 0.0761 0.92 +1 358 0.1757 0.82 +1 320 0.5054 0.49 +1 359 0.0391 0.96 +1 321 0.6064 0.39 +1 360 0.0421 0.96 +1 322 0.4017 0.60 +1 361 0.0366 0.96 +1 323 0.1830 0.82 +1 362 0.0152 0.98 +1 324 0.0891 0.91 +1 363 0.0194 0.98 +1 325 0.2089 0.79 +1 364 0.0252 0.97 +1 326 0.0708 0.93 +1 365 0.1992 0.80 +1 327 0.1754 0.82 +1 366 0.1576 0.84 +1 328 0.1245 0.88 +1 367 0.1253 0.87 +1 329 0.7068 0.29 +1 368 0.1266 0.87 +1 330 1.0305 (0.03) -1 369 0.1055 0.89 +1 331 2.1892 (1.19) -1 370 0.1377 0.86 +1 332 1.4884 (0.49) -1 371 0.4458 0.55 +1 333 0.0535 0.95 +1 372 0.0164 0.98 +1 334 0.1972 0.80 +1 373 0.0284 0.97 +1 335 0.1405 0.86 +1 374 0.0116 0.99 +1 336 0.3454 0.65 +1 375 0.0156 0.98 +1 337 0.6169 0.38 +1 376 0.0123 0.99 +1

[113]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 SIGN TEST (Continued)

1. SOF 1-WS Sign # SOF 1-WS Sign (WS) (WS) 377 0.0181 0.98 +1 402 0.0553 0.94 +1 378 0.0198 0.98 +1 403 0.0295 0.97 +1 379 0.0269 0.97 +1 404 0.0544 0.95 +1 380 0.0324 0.97 +1 405 0.0952 0.90 +1 381 0.0217 0.98 +1 406 0.3149 0.69 +1 382 0.0386 0.96 +1 407 0.1078 0.89 +1 383 0.0541 0.95 +1 408 0.1983 0.80 +1 384 0.0593 0.94 +1 409 0.1470 0.85 +1 385 0.0390 0.96 +1 410 0.0772 0.92 +1 386 0.0353 0.96 +1 411 0.0718 0.93 +1 387 0.0623 0.94 +1 412 0.0342 0.97 +1 388 0.0920 0.91 +1 413 0.0203 0.98 +1 389 0.0665 0.93 +1 414 0.0112 0.99 +1 390 0.0777 0.92 +1 415 0.0157 0.98 +1 391 0.0434 0.96 +1 416 0.4187 0.58 +1 392 0.1231 0.88 +1 417 0.5157 0.48 +1 393 0.1093 0.89 +1 418 0.5508 0.45 +1 394 0.2839 0.72 +1 419 0.0524 0.95 +1 395 0.1625 0.84 +1 420 0.0186 0.98 +1 396 0.0513 0.95 +1 421 0.0295 0.97 +1 397 0.1623 0.84 +1 422 0.5810 0.42 +1 398 0.0178 0.98 +1 423 0.1514 0.85 +1 399 0.0082 0.99 +1 424 0.0519 0.95 +1 400 0.0163 0.98 +1 425 1.6120 (0.61) -1 401 0.0370 0.96 +1 Number of positive differences (S+) 409 Critical Value 229 Survey Unit MEETS the Acceptance Criteria

[114]

ATTACHMENT 4 QA INFORMATION AND CHARTS/QC REPLICATE MEASUREMENT ASSESSMENTS

[115]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 ISOCS QA Letter to File Dates 02/02/2018 to 03/22/2018 Location Auxiliary Building ISOCS Detector 6279 This letter documents the Quality Control of ISOCS 6279 during the Auxiliary Building FSS.

The attached files are the Full QA reports/graphs for the referenced ISOCS unit. The control limits and parameters are located in Procedure ZS-RP-108-006-004, Rev. 4, Section 4.3.5.

The reports will show the date and times collected for the Peak Position (Energy channel),

Peak resolution or Full Width at Half Maximum (FWHM), and Peak activity (after correction for radioactive decay).

Measurements rejected will be signified with an R preceding the date. These were rejected for various reasons, i.e. (run time did not meet the 300 seconds, wrong dates that were used for the assay of source, days the ISOCS was not used for FSS/turnover surveys, or multiple runs made during adjusting gains during the pre-check). Measurements with flags will be listed below with comments.

Peak energy-1274.53 kev Value Flags Measurement Time Sample ID Analyst (keV) LU:SD:UD:BS 2/2/18 10:09:37 AM 1.2713E+03 Be:

No historical QA data to compare. Moved from Truck Monitor to Aux Bldg. Basement, unit not completely settled. Spectrum evaluated and deemed acceptable to continue. All data collected during FSS are inspected to verify peaks are in proper channels and FWHM are acceptable.

Peak energy-86.54 kev Value Flags Measurement Time Sample ID Analyst (keV) LU:SD:UD:BS 2/23/18 3:45:57 AM PM Post 1.2761E+03 Ab:

Drifting occurred from initial QC. Spectrum evaluated and deemed acceptable to continue, all other parameters were within limits. All data collected during FSS are inspected to verify peaks are in proper channels and FWHM are acceptable.

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 FWHM-86.54 kev Value Flags Measurement Time Sample ID Analyst (keV) LU:SD:UD:BS 2/3/18 2:22:16 PM 3.6291E+00 Ac:

2/15/18 2:20:20 PM Post 3.8897E+00 Ac:

2/24/18 10:03:34 AM Post 4.0707E+00 Ac:

2/24/18 4:08:02 PM Post 3.7642E+00 Ac:

3/2/18 8:11:33 AM Pre 3.1328E+00 In:

3/2/18 12:32:28 PM Pre 3.2411E+00 In:

3/2/18 3:40:55 PM Post 2.9409E+00 In:

3/3/18 7:19:21 AM Pre 3.6120E+00 Ac:

3/3/18 3:41:53 PM Post 3.5435E+00 Ac:

3/5/18 8:38:31 AM Pre 3.4333E+00 Ac:

3/5/18 10:30:17 AM Post 3.4950E+00 Ac:

3/5/18 3:40:58 PM Post 3.7141E+00 Ac:

3/6/18 7:27:28 AM Pre 3.6852E+00 Ac:

These measurements are grouped together for the same reason; the environmental conditions were the majority of the flags, snow moving into the area, rising humidity, all causing issues with the MCA/Pre amp/detector. Spectrums were evaluated because of the higher than normal FWHM, all others parameters were within limits. All data collected during FSS are inspected to verify peaks are in proper channels and FWHM are acceptable.

FWHM-1274.53 kev Value Flags Measurement Time Sample ID Analyst (keV) LU:SD:UD:BS 2/3/18 2:22:16 PM 3.6223E+00 Ac:

2/15/18 2:20:20 PM Post 4.0730E+00 Ac:

2/24/18 10:03:34 AM Post 4.3218E+00 Ac:

2/24/18 4:08:02 PM Post 3.5368E+00 Ac:

2/28/18 8:32:14 AM Pre 3.1417E+00 In:

2/28/18 3:49:56 PM Post 3.0854E+00 In:

3/2/18 8:11:33AM Pre 3.2623E+00 In:

3/2/18 12:32:28 PM Pre 3.3938E+00 In:

3/2/18 3:40:55 PM Post 3.6057E+00 Ac:

3/3/18 7:19:21AM Pre 3.9100E+00 Ac:

3/3/18 3:41:53 PM Post 3.3874E+00 In:

3/5/18 8:38:31 AM Pre 3.7302E+00 Ac:

3/5/18 10:30:17 AM Post 3.5300E+00 Ac:

3/5/18 3:40:58 PM Post 3.8723E+00 Ac:

3/6/18 7:27:28AM Pre 3.7929E+00 Ac:

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 These measurements (same as 86.5 keV FWMH) are grouped together for the same reason; the environmental conditions were the majority of the flags, snow moving into the area, rising humidity, causing issues with the MCS/Pre-amp/detector. Spectrums were evaluated because of the higher than normal FWHM, all other parameters were within limits. All data collected during FSS was inspected to verify peaks were in proper channels and FWHM were acceptable.

Decay Corrected - 86.54 kev Value Flags Measurement Time Sample ID Analyst (keV) LU:SD:UD:BS 2/7/18 10:15:30 AM Pre 7.2217E-01 In:

2/7/18 4:01:41 PM Post 6.9156E-01 In:

Spectrum evaluated and deemed acceptable to continue, all other parameters were within limits. All data collected during FSS are inspected to verify peaks are in proper channels and FWHM are acceptable.

Decay Corrected - 86.54 kev Value Flags Measurement Time Sample ID Analyst (keV) LU:SD:UD:BS 2/15/18 7:45:40 AM Pre 7.0404E-01 In:

Environmental conditions contributed to the other flags on this date, causing issues with the MCA/Pre amp/detector. Spectrums were evaluated because of the higher than normal FWHM, all others parameters were within limits. The activity was deemed acceptable. All data collected during FSS are inspected to verify peaks are in proper channels and FWHM are acceptable.

Decay Corrected - 86.54 kev Value Flags Measurement Time Sample ID Analyst (keV) LU:SD:UD:BS 2/22/18 3:48:24 PM Post 6.3727E-01 Ac:

3/8/18 3:40:40 PM Post 6.3967E-01 Ac:

Decay Corrected - 1274.53 kev Value Flags Measurement Time Sample ID Analyst (keV) LU:SD:UD:BS 2/22/18 3:48:24 PM Post 6.9423E-01 Ac:

3/8/18 3:40:40 PM Post 6.5819E-01 Ac:

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 These measurements are grouped together for the same reason; a different ISOCS source was used. The sources are identical in all aspects except assay date. The correct assay date for the 6279 unit was 6/13/2011. The source that best fits the activity here is assay date 6/03/2009 used for 6278. All other parameters were within limits. All data collected during FSS was inspected to verify peaks were in proper channels and FWHM was acceptable.

No other flags were identified.

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Replicate Measurement Assessment Survey Unit # 05100 Survey Unit Name Auxiliary Building Basement Sample Plan # B1-05100A-F Sample

Description:

Comparison of systematic and QC ISOCS measurements of concrete wall at GRID #6, #24, #74, #102, #116, #131, #132, #156, #167, #208, #218, #230, #243, #272, #292,

1. 331, #333, #334, #341, #373, #395, #405, and #409 STANDARD COMPARISON ROC Activity Standard Resolution Agreement Activity Standard Comparison Acceptable Value Error Range Value Error Ratio (Y/N)

B1-05100AF-SWC-006-GD B1-05100AF-QWC-006-GD Cs-137 1.61E+05 3.62E+04 4 0.5-2.0 1.49E+05 3.60E+04 1.1 Y B1-05100AF-SWC-024-GD B1-05100AF-QWC-024-GD Cs-137 1.70E+05 4.03E+04 4 0.5-2.0 1.63E+05 4.19E+04 1.0 Y B1-05100AF-SWC-074-GD B1-05100AF-QWC-074-GD Cs-137 1.72E+04 1.92E+04 1 0.1-2.5 8.03E+04 1.30E+04 0.2 Y B1-05100AF-SWC-102-GD B1-05100AF-QWC-102-GD Cs-137 7.39E+05 1.08E+05 7 0.5-2.0 7.33E+05 1.08E+05 1.0 Y B1-05100AF-SWC-116-GD B1-05100AF-QWC-116-GD Cs-137 4.57E+04 7.54E+03 6 0.5-2.0 4.03E+05 6.96E+04 0.1 N K-40 4.05E+04 3.07E+04 1 0.4-2.5 7.90E+05 2.38E+05 0.05 N B1-05100AF-SWC-131-GD B1-05100AF-QWC-131-GD Cs-137 3.87E+05 6.45E+04 6 0.5-2.0 3.51E+05 5.93E+04 1.1 Y B1-05100AF-SWC-132-GD B1-05100AF-QWC-132-GD Cs-137 3.58E+06 4.51E+05 8 0.6-1.66 3.60E+06 5.54E+05 1.0 Y B1-05100AF-SWC-156-GD B1-05100AF-QWC-156-GD Cs-137 1.17E+07 1.43E+06 8 0.6-1.66 1.20E+07 1.46E+06 1.0 Y B1-05100AF-SWC-167-GD B1-05100AF-QWC-167-GD Cs-137 1.18E+06 1.65E+05 7 0.5-2.0 1.31E+06 1.79E+05 0.9 Y B1-05100AF-SWC-208-GD B1-05100AF-QWC-208-GD Cs-137 4.76E+06 5.95E+05 8 0.6-1.66 4.75E+06 5.95E+05 1.0 Y B1-05100AF-SWC-218-GD B1-05100AF-QWC-218-GD Cs-137 4.80E+05 7.85E+04 6 0.5-2.0 4.24E+05 7.27E+04 1.1 Y B1-05100AF-SWC-230-GD B1-05100AF-QWC-230-GD Cs-137 5.36E+04 3.15E+04 2 0.4-2.5 5.36E+04 3.16E+04 1.0 Y B1-05100AF-SWC-243-GD B1-05100AF-QWC-243-GD Cs-137 1.28E+05 3.90E+04 3 0.5-2.0 1.53E+05 2.05E+06 0.8 Y B1-05100AF-SWC-272-GD B1-05100AF-QWC-272-GD Cs-137 4.84E+06 6.15E+05 8 0.6-1.66 5.06E+06 6.44E+05 1.0 Y B1-05100AF-SWC-292-GD B1-05100AF-QWC-292-GD Cs-137 1.69E+07 2.05E+06 8 0.6-1.66 1.69E+07 2.05E+06 1.0 Y B1-05100AF-SWC-331-GD B1-05100AF-QWC-331-GD Cs-137 8.07E+05 1.19E+05 7 0.5-2.0 8.21E+05 1.21E+05 1.0 Y B1-05100AF-SWC-333-GD B1-05100AF-QWC-333-GD Cs-137 4.57E+05 8.13E+04 6 0.5-2.0 5.01E+05 8.57E+04 0.9 Y B1-05100AF-SWC-334-GD B1-05100AF-QWC-334-GD Cs-137 1.62E+06 2.26E+05 7 0.5-2.0 1.64E+06 2.29E+05 1.0 Y B1-05100AF-SWC-341-GD B1-05100AF-QWC-341-GD Cs-137 1.99E+07 2.42E+06 8 0.6-1.66 2.09E+07 2.53E+06 1.0 Y B1-05100AF-SWC-373-GD B1-05100AF-QWC-373-GD Cs-137 1.93E+06 2.54E+05 8 0.6-1.66 2.05E+06 2.68E+05 0.9 Y B1-05100AF-SWC-395-GD B1-05100AF-QWC-395-GD Cs-137 3.89E+05 6.99E+04 6 0.5-2.0 4.41E+05 7.40E+04 0.9 Y B1-05100AF-SWC-405-GD B1-05100AF-QWC-405-GD Cs-137 9.12E+05 1.33E+05 7 0.5-2.0 8.61E+05 1.29E+05 1.1 Y B1-05100AF-SWC-409-GD B1-05100AF-QWC-409-GD Cs-137 1.76E+06 2.35E+05 7 0.5-2.0 1.61E+06 2.15E+05 1.1 Y

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Replicate Measurement Assessment (continued)

Survey Unit # 05100 Survey Unit Name Auxiliary Building Basement Sample Plan # B1-05100A-F Comments/Corrective Actions: With the exception Table is provided to show acceptance criteria of the replicate measurement at grid #116, there was used to assess split samples.

acceptable agreement between the standard measurement and the replicate measurement.

ISOCS measurement location 116 (B1-05100AF-SWC-116-GD) identified Cs-137 activity at 4.57E+04 pCi/m2, which was greater than the MDC (5.32E+03 pCi/m2) but only 0.128% of the OpDCGL for Cs-137. There is not acceptable agreement between the standard and comparison measurements. K-40 was also used to determine whether the measurement was acceptable. However, K-40 in the aforementioned sample was also less than the MDC and also did not have an acceptable agreement between the standard measurement and the QC measurement. Pre and post use operational checks of the ISOCS did not indicate any issues with the instrument or the quality of the data. In addition, other replicate measurements taken at several other locations were in agreement. Consequently, it was decided that no further action was necessary.

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ATTACHMENT 5 AUXILIARY BUILDING ISOCS MEASUREMENTS

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SWC-001-GD 2.04E+04 3.68E+06 5.28E+02 5.44E+04 2.64E+05 0.0095 B1-05100AF-SWC-002-GD 3.41E+04 6.15E+06 2.68E+02 4.89E+04 1.34E+05 0.0066 B1-05100AF-SWC-003-GD 4.12E+04 7.43E+06 3.84E+02 7.23E+04 1.92E+05 0.0090 B1-05100AF-SWC-004-GD 2.56E+04 4.62E+06 1.77E+02 9.27E+03 8.87E+04 0.0042 B1-05100AF-SWC-005-GD 2.83E+04 5.11E+06 2.40E+02 5.71E+04 1.20E+05 0.0059 B1-05100AF-SWC-006-GD 1.98E+04 3.57E+06 3.22E+02 6.34E+04 1.61E+05 0.0067 B1-05100AF-SWC-007-GD 2.62E+04 4.73E+06 1.09E+02 3.02E+04 5.46E+04 0.0035 B1-05100AF-SWC-008-GD 1.98E+04 3.57E+06 7.08E+01 7.74E+04 3.54E+04 0.0033 B1-05100AF-SWC-009-GD 7.39E+03 1.33E+06 1.02E+02 5.58E+04 5.10E+04 0.0027 B1-05100AF-SWC-010-GD 3.33E+04 6.01E+06 2.04E+01 3.59E+04 1.02E+04 0.0028 B1-05100AF-SWC-011-GD 9.06E+03 1.63E+06 1.63E+02 2.60E+04 8.13E+04 0.0032 B1-05100AF-SWC-012-GD 6.83E+04 1.23E+07 3.30E+02 2.40E+04 1.65E+05 0.0091 B1-05100AF-SWC-013-GD 2.37E+04 4.28E+06 1.50E+02 2.08E+04 7.49E+04 0.0038 B1-05100AF-SWC-014-GD 1.01E+04 1.82E+06 1.07E+02 3.21E+04 5.37E+04 0.0026 B1-05100AF-SWC-015-GD 0.00E+00 0.00E+00 4.78E+01 4.56E+04 2.39E+04 0.0014 B1-05100AF-SWC-016-GD 9.59E+03 1.73E+06 1.06E+02 2.98E+04 5.31E+04 0.0025 B1-05100AF-SWC-017-GD 3.23E+04 5.83E+06 1.70E+02 7.76E+04 8.49E+04 0.0055 B1-05100AF-SWC-018-GD 2.49E+03 4.49E+05 6.22E+01 5.41E+04 3.11E+04 0.0018 B1-05100AF-SWC-019-GD 3.10E+04 5.59E+06 1.22E+02 5.92E+04 6.11E+04 0.0044 B1-05100AF-SWC-020-GD 3.88E+04 7.00E+06 1.11E+02 2.53E+04 5.54E+04 0.0042 B1-05100AF-SWC-021-GD 2.90E+04 5.23E+06 2.32E+02 6.28E+04 1.16E+05 0.0059 B1-05100AF-SWC-022-GD 4.40E+04 7.94E+06 2.14E+02 5.93E+04 1.07E+05 0.0065 B1-05100AF-SWC-023-GD 3.04E+04 5.49E+06 5.18E+01 2.05E+04 2.59E+04 0.0028 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SWC-024-GD 4.51E+04 8.14E+06 3.40E+02 0.00E+00 1.70E+05 0.0075 B1-05100AF-SWC-025-GD 3.38E+04 6.10E+06 1.89E+02 3.59E+04 9.44E+04 0.0052 B1-05100AF-SWC-026-GD 2.49E+03 4.49E+05 1.12E+02 3.64E+04 5.60E+04 0.0023 B1-05100AF-SWC-027-GD 4.73E+03 8.54E+05 1.81E+02 7.69E+04 9.07E+04 0.0040 B1-05100AF-SWC-028-GD 1.06E+04 1.91E+06 2.82E+02 0.00E+00 1.41E+05 0.0046 B1-05100AF-SWC-029-GD 3.00E+04 5.41E+06 4.16E+02 6.82E+03 2.08E+05 0.0078 B1-05100AF-SWC-030-GD 1.10E+04 1.98E+06 1.20E+03 3.28E+04 6.01E+05 0.0183 B1-05100AF-SWC-031-GD 4.12E+04 7.43E+06 3.86E+02 5.51E+04 1.93E+05 0.0087 B1-05100AF-SWC-032-GD 1.10E+04 1.98E+06 3.00E+02 1.58E+04 1.50E+05 0.0052 B1-05100AF-SWC-033-GD 7.30E+03 1.32E+06 8.54E+02 5.28E+04 4.27E+05 0.0134 B1-05100AF-SWC-034-GD 1.73E+04 3.12E+06 2.10E+03 1.98E+04 1.05E+06 0.0313 B1-05100AF-SWC-035-GD 3.85E+04 6.95E+06 3.54E+03 5.18E+04 1.77E+06 0.0536 B1-05100AF-SWC-036-GD 3.40E+04 6.14E+06 1.67E+04 2.84E+04 8.34E+06 0.2406 B1-05100AF-SWC-037-GD 8.17E+03 1.47E+06 9.62E+03 1.99E+04 4.81E+06 0.1381 B1-05100AF-SWC-038-GD 3.13E+04 5.65E+06 4.36E+03 2.27E+04 2.18E+06 0.0644 B1-05100AF-SWC-039-GD 4.03E+04 7.27E+06 1.11E+03 8.05E+04 5.54E+05 0.0194 B1-05100AF-SWC-040-GD 3.11E+04 5.61E+06 6.34E+02 0.00E+00 3.17E+05 0.0109 B1-05100AF-SWC-041-GD 2.20E+04 3.97E+06 4.08E+02 4.37E+04 2.04E+05 0.0078 B1-05100AF-SWC-042-GD 5.40E+04 9.74E+06 3.80E+02 1.90E+04 1.90E+05 0.0089 B1-05100AF-SWC-043-GD 3.49E+04 6.30E+06 7.72E+03 7.58E+04 3.86E+06 0.1134 B1-05100AF-SWC-044-GD 1.61E+03 2.91E+05 1.11E+04 2.89E+04 5.56E+06 0.1593 B1-05100AF-SWC-045-GD 2.54E+04 4.58E+06 4.12E+03 3.19E+04 2.06E+06 0.0608 B1-05100AF-SWC-046-GD 2.54E+04 4.58E+06 1.07E+03 3.69E+03 5.34E+05 0.0168 B1-05100AF-SWC-047-GD 4.26E+04 7.69E+06 5.94E+02 2.73E+04 2.97E+05 0.0114 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

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FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SWC-048-GD 6.25E+04 1.13E+07 4.30E+02 5.71E+04 2.15E+05 0.0107 B1-05100AF-SWC-049-GD 2.13E+03 3.84E+05 5.26E+03 4.18E+04 2.63E+06 0.0758 B1-05100AF-SWC-050-GD 4.40E+04 7.94E+06 8.80E+03 1.65E+05 4.40E+06 0.1306 B1-05100AF-SWC-051-GD 3.44E+04 6.21E+06 8.58E+03 6.82E+04 4.29E+06 0.1255 B1-05100AF-SWC-052-GD 5.82E+04 1.05E+07 1.66E+04 2.50E+04 8.29E+06 0.2405 B1-05100AF-SWC-053-GD 2.85E+05 5.14E+07 2.66E+03 1.27E+04 1.33E+06 0.0549 B1-05100AF-SWC-054-GD 4.26E+05 7.69E+07 9.28E+02 1.23E+03 4.64E+05 0.0383 B1-05100AF-SWC-055-GD 6.70E+05 1.21E+08 2.48E+03 7.34E+04 1.24E+06 0.0759 B1-05100AF-SWC-056-GD 4.72E+05 8.52E+07 2.10E+03 3.06E+04 1.05E+06 0.0582 B1-05100AF-SWC-057-GD 5.68E+04 1.02E+07 1.98E+02 5.32E+04 9.89E+04 0.0069 B1-05100AF-SWC-058-GD 2.58E+05 4.66E+07 2.86E+02 2.72E+04 1.43E+05 0.0197 B1-05100AF-SWC-059-GD 1.94E+05 3.50E+07 4.04E+02 5.04E+04 2.02E+05 0.0179 B1-05100AF-SWC-060-GD 1.24E+05 2.24E+07 1.81E+03 3.39E+03 9.04E+05 0.0332 B1-05100AF-SWC-061-GD 3.00E+04 5.41E+06 1.11E+01 1.85E+04 5.54E+03 0.0022 B1-05100AF-SWC-062-GD 3.83E+04 6.91E+06 3.66E+01 6.71E+04 1.83E+04 0.0038 B1-05100AF-SWC-063-GD 0.00E+00 0.00E+00 6.46E+01 4.40E+04 3.23E+04 0.0016 B1-05100AF-SWC-064-GD 2.28E+04 4.11E+06 1.81E+02 5.52E+04 9.07E+04 0.0047 B1-05100AF-SWC-065-GD 6.11E+04 1.10E+07 1.71E+02 6.35E+03 8.53E+04 0.0061 B1-05100AF-SWC-066-GD 2.48E+04 4.48E+06 4.12E+00 5.87E+04 2.06E+03 0.0024 B1-05100AF-SWC-067-GD 1.98E+04 3.57E+06 4.16E+01 4.00E+04 2.08E+04 0.0023 B1-05100AF-SWC-068-GD 1.88E+04 3.39E+06 1.51E+02 1.90E+04 7.54E+04 0.0035 B1-05100AF-SWC-069-GD 3.84E+04 6.93E+06 4.94E+01 7.84E+04 2.47E+04 0.0041 B1-05100AF-SWC-070-GD 5.62E+04 1.01E+07 6.14E+01 3.77E+04 3.07E+04 0.0047 B1-05100AF-SWC-071-GD 3.10E+04 5.59E+06 6.48E+01 6.44E+04 3.24E+04 0.0037 B1-05100AF-SWC-072-GD 5.31E+04 9.58E+06 2.44E+02 4.26E+04 1.22E+05 0.0072 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[149]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SWC-073-GD 4.12E+04 7.43E+06 2.98E+02 4.83E+03 1.49E+05 0.0067 B1-05100AF-SWC-074-GD 3.27E+04 5.90E+06 3.44E+01 1.04E+04 1.72E+04 0.0026 B1-05100AF-SWC-075-GD 3.13E+04 5.65E+06 3.68E+01 6.60E+04 1.84E+04 0.0033 B1-05100AF-SWC-076-GD 3.55E+04 6.41E+06 4.02E+01 4.38E+04 2.01E+04 0.0033 B1-05100AF-SWC-077-GD 3.34E+04 6.03E+06 9.00E+01 1.56E+04 4.50E+04 0.0035 B1-05100AF-SWC-078-GD 3.19E+04 5.76E+06 2.80E+01 4.59E+04 1.40E+04 0.0030 B1-05100AF-SWC-079-GD 2.39E+04 4.31E+06 1.05E+01 2.82E+04 5.26E+03 0.0020 B1-05100AF-SWC-080-GD 7.62E+03 1.38E+06 4.12E+01 4.20E+03 2.06E+04 0.0011 B1-05100AF-SWC-081-GD 2.55E+05 4.60E+07 9.30E+02 1.38E+04 4.65E+05 0.0285 B1-05100AF-SWC-082-GD 3.06E+05 5.52E+07 2.98E+03 4.23E+04 1.49E+06 0.0612 B1-05100AF-SWC-083-GD 1.83E+05 3.30E+07 2.56E+03 0.00E+00 1.28E+06 0.0473 B1-05100AF-SWC-086-GD 1.47E+05 2.65E+07 1.06E+03 1.25E+04 5.30E+05 0.0240 B1-05100AF-SWC-087-GD 1.05E+05 1.89E+07 1.14E+03 3.02E+04 5.69E+05 0.0229 B1-05100AF-SWC-088-GD 2.10E+05 3.79E+07 9.92E+02 6.41E+04 4.96E+05 0.0275 B1-05100AF-SWC-089-GD 9.91E+04 1.79E+07 1.05E+03 5.55E+02 5.27E+05 0.0209 B1-05100AF-SWC-090-GD 6.04E+04 1.09E+07 2.32E+03 1.94E+04 1.16E+06 0.0370 B1-05100AF-SWC-091-GD 1.14E+05 2.06E+07 1.65E+03 5.91E+04 8.25E+05 0.0311 B1-05100AF-SWC-094-GD 9.88E+04 1.78E+07 3.16E+02 5.84E+04 1.58E+05 0.0112 B1-05100AF-SWC-095-GD 4.07E+04 7.34E+06 2.06E+02 2.86E+04 1.03E+05 0.0058 B1-05100AF-SWC-096-GD 2.47E+05 4.46E+07 1.07E+03 4.25E+04 5.35E+05 0.0304 B1-05100AF-SWC-097-GD 1.14E+05 2.06E+07 1.20E+03 4.41E+03 6.01E+05 0.0239 B1-05100AF-SWC-098-GD 1.06E+04 1.91E+06 1.05E+02 5.55E+04 5.24E+04 0.0029 B1-05100AF-SWC-099-GD 3.68E+04 6.64E+06 1.10E+02 6.40E+04 5.51E+04 0.0047 B1-05100AF-SWC-101-GD 1.46E+05 2.63E+07 4.40E+03 4.12E+04 2.20E+06 0.0720 B1-05100AF-SWC-102-GD 5.36E+04 9.67E+06 1.48E+03 9.06E+04 7.39E+05 0.0256 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[150]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SWC-103-GD 7.45E+04 1.34E+07 4.86E+03 6.69E+04 2.43E+06 0.0748 B1-05100AF-SWC-104-GD 6.83E+04 1.23E+07 4.08E+02 1.31E+04 2.04E+05 0.0100 B1-05100AF-SWC-105-GD 3.25E+04 5.86E+06 1.20E+02 1.20E+04 6.01E+04 0.0038 B1-05100AF-SWC-106-GD 3.59E+06 6.48E+08 4.32E+03 7.12E+04 2.16E+06 0.2739 B1-05100AF-SWC-107-GD 1.45E+05 2.62E+07 1.20E+03 5.39E+03 6.00E+05 0.0257 B1-05100AF-SWC-108-GD 2.30E+04 4.15E+06 1.22E+02 8.46E+04 6.08E+04 0.0043 B1-05100AF-SWC-109-GD 6.30E+04 1.14E+07 1.97E+02 3.07E+04 9.83E+04 0.0070 B1-05100AF-SWC-110-GD 3.53E+05 6.37E+07 3.42E+03 7.41E+04 1.71E+06 0.0707 B1-05100AF-SWC-111-GD 6.96E+05 1.26E+08 2.14E+03 3.94E+04 1.07E+06 0.0721 B1-05100AF-SWC-112-GD 9.59E+05 1.73E+08 2.06E+03 0.00E+00 1.03E+06 0.0858 B1-05100AF-SWC-113-GD 4.05E+04 7.31E+06 1.14E+02 2.79E+04 5.69E+04 0.0044 B1-05100AF-SWC-114-GD 4.70E+04 8.48E+06 1.18E+02 2.90E+04 5.92E+04 0.0049 B1-05100AF-SWC-115-GD 4.68E+04 8.45E+06 4.46E+02 7.66E+04 2.23E+05 0.0102 B1-05100AF-SWC-116-GD 1.09E+04 1.97E+06 9.14E+01 3.08E+03 4.57E+04 0.0020 B1-05100AF-SWC-117-GD 6.23E+04 1.12E+07 8.28E+02 1.41E+04 4.14E+05 0.0157 B1-05100AF-SWC-118-GD 4.50E+04 8.12E+06 3.56E+02 1.33E+04 1.78E+05 0.0079 B1-05100AF-SWC-119-GD 1.86E+05 3.36E+07 8.54E+02 5.64E+04 4.27E+05 0.0240 B1-05100AF-SWC-120-GD 1.18E+03 2.13E+05 7.28E+01 6.00E+04 3.64E+04 0.0020 B1-05100AF-SWC-121-GD 2.48E+04 4.48E+06 6.22E+02 2.84E+04 3.11E+05 0.0108 B1-05100AF-SWC-122-GD 3.52E+03 6.35E+05 1.95E+01 3.42E+03 9.74E+03 0.0005 B1-05100AF-SWC-123-GD 5.47E+03 9.87E+05 2.04E+01 5.78E+02 1.02E+04 0.0006 B1-05100AF-SWC-124-GD 1.39E+04 2.51E+06 1.57E+02 4.00E+04 7.83E+04 0.0036 B1-05100AF-SWC-125-GD 3.32E+04 5.99E+06 6.70E+01 5.64E+04 3.35E+04 0.0037 B1-05100AF-SWC-126-GD 1.24E+04 2.24E+06 7.46E+01 5.24E+04 3.73E+04 0.0026 B1-05100AF-SWC-127-GD 3.64E+04 6.57E+06 1.18E+02 1.93E+04 5.89E+04 0.0041 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[151]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SWC-128-GD 3.09E+04 5.58E+06 1.62E+01 6.40E+04 8.11E+03 0.0030 B1-05100AF-SWC-129-GD 3.18E+05 5.74E+07 7.80E+02 5.88E+04 3.90E+05 0.0307 B1-05100AF-SWC-130-GD 9.24E+03 1.67E+06 5.60E+01 4.55E+03 2.80E+04 0.0014 B1-05100AF-SWC-131-GD 1.43E+05 2.58E+07 7.74E+02 1.59E+03 3.87E+05 0.0195 B1-05100AF-SWC-132-GD 5.33E+05 9.62E+07 7.16E+03 0.00E+00 3.58E+06 0.1336 B1-05100AF-SWC-133-GD 9.14E+04 1.65E+07 1.39E+03 6.36E+03 6.94E+05 0.0253 B1-05100AF-SWC-134-GD 5.18E+04 9.35E+06 6.12E+01 5.76E+03 3.06E+04 0.0040 B1-05100AF-SWC-135-GD 3.19E+05 5.76E+07 2.56E+03 5.41E+04 1.28E+06 0.0561 B1-05100AF-SWC-136-GD 5.55E+04 1.00E+07 1.36E+03 1.58E+04 6.82E+05 0.0230 B1-05100AF-SWC-137-GD 3.88E+04 7.00E+06 4.08E+02 1.30E+04 2.04E+05 0.0083 B1-05100AF-SWC-141-GD 8.66E+04 1.56E+07 4.96E+03 2.32E+04 2.48E+06 0.0762 B1-05100AF-SWC-142-GD 1.92E+05 3.46E+07 7.66E+03 3.59E+04 3.83E+06 0.1212 B1-05100AF-SWC-143-GD 1.06E+05 1.91E+07 6.00E+03 2.51E+04 3.00E+06 0.0923 B1-05100AF-SWC-144-GD 1.25E+05 2.26E+07 5.50E+03 8.11E+04 2.75E+06 0.0871 B1-05100AF-SWC-147-GD 4.40E+04 7.94E+06 3.22E+03 4.51E+04 1.61E+06 0.0492 B1-05100AF-SWC-148-GD 1.80E+04 3.25E+06 2.10E+03 3.89E+04 1.05E+06 0.0316 B1-05100AF-SWC-149-GD 8.91E+04 1.61E+07 8.56E+03 1.38E+04 4.28E+06 0.1277 B1-05100AF-SWC-150-GD 6.33E+04 1.14E+07 1.55E+04 5.53E+04 7.73E+06 0.2253 B1-05100AF-SWC-151-GD 2.03E+05 3.66E+07 3.96E+04 1.19E+05 1.98E+07 0.5791 B1-05100AF-SWC-152-GD 1.10E+05 1.98E+07 1.26E+04 6.67E+04 6.31E+06 0.1876 B1-05100AF-SWC-153-GD 2.56E+05 4.62E+07 3.86E+03 1.09E+04 1.93E+06 0.0703 B1-05100AF-SWC-154-GD 8.42E+04 1.52E+07 3.68E+03 4.32E+04 1.84E+06 0.0581 B1-05100AF-SWC-155-GD 8.16E+04 1.47E+07 1.17E+04 7.21E+04 5.86E+06 0.1732 B1-05100AF-SWC-156-GD 2.22E+05 4.01E+07 2.34E+04 4.52E+04 1.17E+07 0.3478 B1-05100AF-SWC-157-GD 7.91E+04 1.43E+07 1.47E+03 1.76E+04 7.36E+05 0.0259 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[152]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SWC-158-GD 7.59E+04 1.37E+07 7.58E+02 4.86E+04 3.79E+05 0.0160 B1-05100AF-SWC-159-GD 5.45E+04 9.83E+06 3.46E+02 9.50E+03 1.73E+05 0.0083 B1-05100AF-SWC-160-GD 2.34E+05 4.22E+07 1.99E+02 6.18E+03 9.93E+04 0.0167 B1-05100AF-SWC-161-GD 5.43E+04 9.80E+06 5.04E+02 3.93E+04 2.52E+05 0.0110 B1-05100AF-SWC-162-GD 7.34E+04 1.32E+07 4.76E+03 4.48E+04 2.38E+06 0.0729 B1-05100AF-SWC-163-GD 6.84E+04 1.23E+07 9.40E+03 2.81E+04 4.70E+06 0.1386 B1-05100AF-SWC-164-GD 7.13E+04 1.29E+07 8.88E+02 7.63E+04 4.44E+05 0.0180 B1-05100AF-SWC-165-GD 1.26E+06 2.27E+08 1.14E+03 5.75E+04 5.71E+05 0.0913 B1-05100AF-SWC-166-GD 1.83E+04 3.30E+06 6.70E+03 1.09E+05 3.35E+06 0.0983 B1-05100AF-SWC-167-GD 9.80E+04 1.77E+07 2.36E+03 3.08E+04 1.18E+06 0.0399 B1-05100AF-SWC-168-GD 1.01E+05 1.82E+07 1.95E+03 2.51E+04 9.73E+05 0.0341 B1-05100AF-SWC-169-GD 5.94E+04 1.07E+07 2.14E+02 3.78E+04 2.20E+06 0.0667 B1-05100AF-SWC-172-GD 1.07E+05 1.93E+07 5.40E+03 8.41E+03 2.70E+06 0.0835 B1-05100AF-SWC-173-GD 3.11E+05 5.61E+07 1.19E+03 7.57E+04 5.93E+05 0.0363 B1-05100AF-SWC-174-GD 3.07E+05 5.54E+07 1.38E+03 8.23E+04 6.91E+05 0.0390 B1-05100AF-SWC-175-GD 7.88E+05 1.42E+08 1.42E+03 7.22E+04 7.10E+05 0.0677 B1-05100AF-SWC-179-GD 1.30E+06 2.35E+08 7.30E+03 1.96E+05 3.65E+06 0.1836 B1-05100AF-SWC-180-GD 4.57E+05 8.25E+07 1.92E+03 1.20E+05 9.60E+05 0.0561 B1-05100AF-SWC-181-GD 2.64E+05 4.76E+07 6.54E+02 2.76E+04 3.27E+05 0.0253 B1-05100AF-SWC-182-GD 5.71E+04 1.03E+07 3.52E+02 3.70E+04 1.76E+05 0.0089 B1-05100AF-SWC-183-GD 4.97E+04 8.97E+06 3.42E+02 7.61E+04 1.71E+05 0.0089 B1-05100AF-SWC-184-GD 5.26E+04 9.49E+06 2.46E+03 4.91E+04 1.23E+06 0.0389 B1-05100AF-SWC-185-GD 6.48E+04 1.17E+07 4.36E+03 1.20E+04 2.18E+06 0.0662 B1-05100AF-SWC-186-GD 2.17E+04 3.92E+06 5.10E+02 8.54E+03 2.55E+05 0.0087 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[153]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SWC-187-GD 2.28E+04 4.11E+06 3.70E+02 6.84E+04 1.85E+05 0.0076 B1-05100AF-SWC-188-GD 0.00E+00 0.00E+00 3.72E+02 2.05E+04 1.86E+05 0.0056 B1-05100AF-SWC-189-GD 8.29E+03 1.50E+06 9.48E+01 5.25E+04 4.74E+04 0.0026 B1-05100AF-SWC-190-GD 1.53E+04 2.76E+06 1.63E+02 2.05E+04 8.13E+04 0.0035 B1-05100AF-SWC-191-GD 2.04E+04 3.68E+06 2.96E+02 2.18E+04 1.48E+05 0.0057 B1-05100AF-SWC-192-GD 4.69E+04 8.46E+06 2.02E+02 1.67E+04 1.01E+05 0.0059 B1-05100AF-SWC-193-GD 4.81E+04 8.68E+06 2.16E+02 1.08E+04 1.08E+05 0.0061 B1-05100AF-SWC-194-GD 3.27E+06 5.90E+08 4.72E+03 0.00E+00 2.36E+06 0.2598 B1-05100AF-SWC-195-GD 4.24E+04 7.65E+06 9.60E+01 2.61E+04 4.80E+04 0.0042 B1-05100AF-SWC-196-GD 4.85E+04 8.75E+06 1.17E+02 1.23E+04 5.84E+04 0.0047 B1-05100AF-SWC-197-GD 5.20E+04 9.38E+06 1.69E+02 2.31E+04 8.46E+04 0.0058 B1-05100AF-SWC-198-GD 2.23E+06 4.02E+08 3.48E+03 5.91E+04 1.74E+06 0.1817 B1-05100AF-SWC-199-GD 6.76E+05 1.22E+08 1.84E+03 2.76E+04 9.20E+05 0.0664 B1-05100AF-SWC-200-GD 2.67E+05 4.82E+07 1.06E+03 0.00E+00 5.28E+05 0.0308 B1-05100AF-SWC-201-GD 2.47E+06 4.46E+08 2.44E+03 0.00E+00 1.22E+06 0.1802 B1-05100AF-SWC-202-GD 2.75E+05 4.96E+07 7.10E+02 1.31E+04 3.55E+05 0.0265 B1-05100AF-SWC-203-GD 2.70E+05 4.87E+07 6.06E+02 5.24E+04 3.03E+05 0.0253 B1-05100AF-SWC-204-GD 1.22E+07 2.20E+09 2.52E+04 2.84E+05 1.26E+07 1.0817 B1-05100AF-SWC-205-GD 1.46E+07 2.63E+09 2.74E+04 0.00E+00 1.37E+07 1.2501 B1-05100AF-SWC-206-GD 1.30E+07 2.35E+09 2.46E+04 8.72E+04 1.23E+07 1.1173 B1-05100AF-SWC-207-GD 2.71E+05 4.89E+07 4.96E+02 3.74E+04 2.48E+05 0.0236 B1-05100AF-SWC-208-GD 1.78E+06 3.21E+08 9.52E+03 4.70E+04 4.76E+06 0.2413 B1-05100AF-SWC-209-GD 1.19E+06 2.15E+08 9.66E+03 3.11E+04 4.83E+06 0.2084 B1-05100AF-SWC-210-GD 1.50E+06 2.71E+08 1.94E+03 3.02E+04 9.68E+05 0.1163 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[154]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SWC-211-GD 1.51E+05 2.72E+07 2.82E+02 2.21E+04 1.41E+05 0.0132 B1-05100AF-SWC-212-GD 1.29E+07 2.33E+09 1.69E+04 2.27E+05 8.46E+06 1.0038 B1-05100AF-SWC-213-GD 2.29E+05 4.13E+07 4.32E+03 1.85E+04 2.16E+06 0.0754 B1-05100AF-SWC-214-GD 1.94E+05 3.50E+07 1.34E+03 1.70E+04 6.72E+05 0.0309 B1-05100AF-SWC-215-GD 9.76E+04 1.76E+07 1.51E+03 7.35E+04 7.54E+05 0.0284 B1-05100AF-SWC-216-GD 4.22E+04 7.61E+06 5.14E+02 8.29E+04 2.57E+05 0.0110 B1-05100AF-SWC-217-GD 3.12E+04 5.63E+06 1.02E+03 2.80E+04 5.12E+05 0.0169 B1-05100AF-SWC-218-GD 1.46E+04 2.63E+06 9.60E+02 3.82E+04 4.80E+05 0.0151 B1-05100AF-SWC-221-GD 4.89E+04 8.82E+06 2.10E+03 3.77E+04 1.05E+06 0.0334 B1-05100AF-SWC-222-GD 4.15E+04 7.49E+06 2.06E+03 5.10E+04 1.03E+06 0.0326 B1-05100AF-SWC-223-GD 2.51E+04 4.53E+06 1.66E+02 5.47E+04 8.31E+04 0.0047 B1-05100AF-SWC-224-GD 1.30E+04 2.35E+06 2.82E+02 4.48E+04 1.41E+05 0.0054 B1-05100AF-SWC-225-GD 1.17E+04 2.11E+06 4.32E+02 2.75E+04 2.16E+05 0.0073 B1-05100AF-SWC-226-GD 2.51E+04 4.53E+06 4.24E+02 4.09E+04 2.12E+05 0.0081 B1-05100AF-SWC-229-GD 2.19E+04 3.95E+06 1.79E+02 2.14E+04 8.94E+04 0.0042 B1-05100AF-SWC-230-GD 3.55E+04 6.41E+06 1.07E+02 3.79E+04 5.36E+04 0.0042 B1-05100AF-SWC-231-GD 3.98E+04 7.18E+06 2.10E+02 5.83E+04 1.05E+05 0.0062 B1-05100AF-SWC-232-GD 6.71E+04 1.21E+07 6.10E+02 0.00E+00 3.05E+05 0.0127 B1-05100AF-SWC-233-GD 5.76E+04 1.04E+07 5.14E+02 4.23E+04 2.57E+05 0.0113 B1-05100AF-SWC-234-GD 3.41E+04 6.15E+06 2.56E+02 2.48E+04 1.28E+05 0.0060 B1-05100AF-SFC-236-GD 1.05E+04 1.89E+06 6.86E+02 2.82E+04 3.43E+05 0.0108 B1-05100AF-SFC-237-GD 4.55E+04 8.21E+06 3.34E+02 6.42E+04 1.67E+05 0.0084 B1-05100AF-SFC-238-GD 3.84E+04 6.93E+06 2.18E+02 4.95E+04 1.09E+05 0.0061 B1-05100AF-SFC-239-GD 4.83E+04 8.72E+06 3.48E+02 4.73E+04 1.74E+05 0.0085 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[155]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SFC-240-GD 8.22E+04 1.48E+07 7.36E+02 9.60E+03 3.68E+05 0.0155 B1-05100AF-SFC-241-GD 5.48E+04 9.89E+06 2.96E+02 2.80E+04 1.48E+05 0.0079 B1-05100AF-SFC-242-GD 4.71E+04 8.50E+06 3.48E+02 1.02E+05 1.74E+05 0.0092 B1-05100AF-SFC-243-GD 4.04E+04 7.29E+06 2.56E+02 6.28E+04 1.28E+05 0.0070 B1-05100AF-SFC-244-GD 1.85E+04 3.34E+06 3.02E+02 6.09E+04 1.51E+05 0.0063 B1-05100AF-SFC-245-GD 2.63E+04 4.75E+06 3.42E+02 6.91E+04 1.71E+05 0.0074 B1-05100AF-SFC-246-GD 9.35E+04 1.69E+07 4.00E+02 2.90E+04 2.00E+05 0.0116 B1-05100AF-SFC-247-GD 8.43E+04 1.52E+07 4.98E+02 4.15E+04 2.49E+05 0.0127 B1-05100AF-SFC-248-GD 1.61E+04 2.91E+06 3.50E+02 3.49E+04 1.75E+05 0.0065 B1-05100AF-SFC-249-GD 3.80E+04 6.86E+06 3.34E+02 0.00E+00 1.67E+05 0.0070 B1-05100AF-SFC-250-GD 4.75E+04 8.57E+06 3.90E+02 2.29E+04 1.95E+05 0.0087 B1-05100AF-SFC-251-GD 3.88E+04 7.00E+06 1.15E+02 5.59E+03 5.75E+04 0.0040 B1-05100AF-SFC-252-GD 3.98E+04 7.18E+06 2.84E+02 7.54E+04 1.42E+05 0.0075 B1-05100AF-SFC-253-GD 6.97E+04 1.26E+07 4.82E+02 2.35E+04 2.41E+05 0.0113 B1-05100AF-SFC-254-GD 7.55E+04 1.36E+07 4.52E+02 3.89E+04 2.26E+05 0.0115 B1-05100AF-SFC-255-GD 1.42E+05 2.56E+07 5.12E+02 1.93E+04 2.56E+05 0.0159 B1-05100AF-SFC-256-GD 2.24E+07 4.04E+09 3.20E+04 6.63E+04 1.60E+07 1.7757 B1-05100AF-SFC-257-GD 1.82E+07 3.28E+09 3.50E+04 3.72E+05 1.75E+07 1.5759 B1-05100AF-SFC-258-GD 1.88E+07 3.39E+09 3.24E+04 1.32E+05 1.62E+07 1.5706 B1-05100AF-SFC-259-GD 2.01E+07 3.63E+09 5.94E+04 1.98E+05 2.97E+07 2.0335 B1-05100AF-SFC-260-GD 1.81E+07 3.27E+09 5.90E+04 1.12E+05 2.95E+07 1.9089 B1-05100AF-SFC-261-GD 6.10E+05 1.10E+08 5.62E+03 6.34E+04 2.81E+06 0.1171 B1-05100AF-SFC-262-GD 1.60E+05 2.89E+07 5.46E+03 4.42E+04 2.73E+06 0.0880 B1-05100AF-SFC-263-GD 6.78E+04 1.22E+07 5.78E+02 2.64E+04 2.89E+05 0.0126 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[156]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SFC-264-GD 7.39E+04 1.33E+07 3.76E+02 1.10E+04 1.88E+05 0.0099 B1-05100AF-SFC-265-GD 7.78E+04 1.40E+07 3.60E+02 5.91E+04 1.80E+05 0.0106 B1-05100AF-SFC-266-GD 7.76E+04 1.40E+07 5.80E+02 5.49E+04 2.90E+05 0.0137 B1-05100AF-SFC-267-GD 9.40E+04 1.70E+07 3.80E+02 5.81E+04 1.90E+05 0.0118 B1-05100AF-SFC-268-GD 9.80E+04 1.77E+07 1.22E+03 7.68E+04 6.11E+05 0.0243 B1-05100AF-SFC-269-GD 3.41E+05 6.15E+07 1.12E+04 4.91E+04 5.58E+06 0.1801 B1-05100AF-SFC-270-GD 1.28E+06 2.31E+08 8.76E+03 7.44E+04 4.38E+06 0.2015 B1-05100AF-SFC-271-GD 4.62E+06 8.34E+08 5.28E+03 7.55E+04 2.64E+06 0.3483 B1-05100AF-SFC-272-GD 7.77E+06 1.40E+09 9.68E+03 8.26E+04 4.84E+06 0.5965 B1-05100AF-SFC-273-GD 2.29E+07 4.13E+09 5.62E+04 7.29E+05 2.81E+07 2.1603 B1-05100AF-SFC-274-GD 2.46E+07 4.44E+09 5.06E+04 1.93E+05 2.53E+07 2.1725 B1-05100AF-SFC-275-GD 8.35E+06 1.51E+09 1.79E+04 1.81E+05 8.96E+06 0.7498 B1-05100AF-SFC-276-GD 2.22E+06 4.01E+08 7.62E+03 9.81E+04 3.81E+06 0.2408 B1-05100AF-SFC-277-GD 2.86E+06 5.16E+08 7.46E+03 3.50E+04 3.73E+06 0.2753 B1-05100AF-SFC-278-GD 4.38E+06 7.90E+08 6.86E+03 4.24E+04 3.43E+06 0.3562 B1-05100AF-SFC-279-GD 8.22E+05 1.48E+08 4.78E+03 6.89E+04 2.39E+06 0.1176 B1-05100AF-SFC-280-GD 4.39E+05 7.92E+07 4.50E+03 1.22E+05 2.25E+06 0.0919 B1-05100AF-SFC-281-GD 1.38E+05 2.49E+07 1.34E+03 1.88E+04 6.69E+05 0.0275 B1-05100AF-SFC-282-GD 1.01E+05 1.82E+07 4.32E+02 4.62E+04 2.16E+05 0.0128 B1-05100AF-SFC-283-GD 7.53E+04 1.36E+07 3.88E+02 9.78E+04 1.94E+05 0.0114 B1-05100AF-SFC-284-GD 5.08E+04 9.17E+06 3.10E+02 3.04E+04 1.55E+05 0.0079 B1-05100AF-SFC-285-GD 9.62E+04 1.74E+07 4.16E+02 1.12E+05 2.08E+05 0.0132 B1-05100AF-SFC-286-GD 3.92E+05 7.07E+07 6.70E+03 1.66E+05 3.35E+06 0.1212 B1-05100AF-SFC-287-GD 1.11E+06 2.00E+08 9.44E+03 9.19E+04 4.72E+06 0.2014 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[157]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SFC-288-GD 5.92E+05 1.07E+08 8.96E+03 6.87E+04 4.48E+06 0.1638 B1-05100AF-SFC-289-GD 1.37E+06 2.47E+08 1.14E+04 4.18E+04 5.71E+06 0.2443 B1-05100AF-SFC-290-GD 5.87E+06 1.06E+09 9.58E+03 2.14E+05 4.79E+06 0.4853 B1-05100AF-SFC-291-GD 3.20E+06 5.77E+08 1.39E+04 5.97E+04 6.93E+06 0.3870 B1-05100AF-SFC-292-GD 1.40E+06 2.53E+08 3.38E+04 1.40E+04 1.69E+07 0.5651 B1-05100AF-SFC-293-GD 1.54E+05 2.78E+07 2.78E+04 0.00E+00 1.39E+07 0.4060 B1-05100AF-SFC-294-GD 1.00E+05 1.80E+07 3.10E+03 0.00E+00 1.55E+06 0.0501 B1-05100AF-SFC-295-GD 4.31E+05 7.78E+07 8.58E+04 4.70E+04 4.29E+07 1.2510 B1-05100AF-SFC-296-GD 8.21E+04 1.48E+07 4.08E+04 0.00E+00 2.04E+07 0.5873 B1-05100AF-SFC-297-GD 2.30E+05 4.15E+07 4.04E+04 1.23E+05 2.02E+07 0.5921 B1-05100AF-SFC-298-GD 9.28E+05 1.67E+08 6.04E+04 2.12E+05 3.02E+07 0.9200 B1-05100AF-SFC-299-GD 1.01E+05 1.82E+07 4.72E+03 2.73E+04 2.36E+06 0.0737 B1-05100AF-SFC-300-GD 1.28E+05 2.31E+07 3.60E+03 4.83E+04 1.80E+06 0.0596 B1-05100AF-SFC-301-GD 8.62E+04 1.56E+07 3.12E+03 1.91E+04 1.56E+06 0.0499 B1-05100AF-SFC-302-GD 1.17E+05 2.11E+07 5.28E+03 2.24E+04 2.64E+06 0.0826 B1-05100AF-SFC-303-GD 3.28E+05 5.92E+07 4.80E+03 3.29E+04 2.40E+06 0.0883 B1-05100AF-SFC-304-GD 1.17E+06 2.11E+08 8.38E+03 0.00E+00 4.19E+06 0.1885 B1-05100AF-SFC-305-GD 2.02E+06 3.65E+08 8.48E+03 0.00E+00 4.24E+06 0.2399 B1-05100AF-SFC-306-GD 5.73E+05 1.03E+08 9.52E+03 1.00E+05 4.76E+06 0.1711 B1-05100AF-SFC-307-GD 3.10E+05 5.59E+07 1.86E+04 8.72E+04 9.28E+06 0.2845 B1-05100AF-SFC-308-GD 7.85E+04 1.42E+07 2.36E+04 4.78E+04 1.18E+07 0.3423 B1-05100AF-SFC-309-GD 8.64E+04 1.56E+07 1.65E+04 8.67E+04 8.27E+06 0.2425 B1-05100AF-SFC-310-GD 2.89E+04 5.22E+06 3.70E+02 6.49E+04 1.85E+05 0.0079 B1-05100AF-SFC-311-GD 6.25E+04 1.13E+07 4.48E+02 1.68E+04 2.24E+05 0.0103 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[158]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SFC-312-GD 6.76E+04 1.22E+07 5.68E+02 5.10E+04 2.84E+05 0.0128 B1-05100AF-SFC-313-GD 9.52E+04 1.72E+07 3.72E+02 7.81E+04 1.86E+05 0.0121 B1-05100AF-SFC-314-GD 7.00E+04 1.26E+07 1.17E+03 1.00E+05 5.86E+05 0.0223 B1-05100AF-SFC-315-GD 3.13E+05 5.65E+07 2.14E+03 9.06E+04 1.07E+06 0.0503 B1-05100AF-SFC-316-GD 1.31E+05 2.36E+07 1.10E+03 4.21E+04 5.49E+05 0.0240 B1-05100AF-SFC-317-GD 8.90E+04 1.61E+07 8.18E+02 4.52E+04 4.09E+05 0.0176 B1-05100AF-SFC-318-GD 1.32E+05 2.38E+07 2.16E+03 5.07E+04 1.08E+06 0.0393 B1-05100AF-SFC-319-GD 6.01E+05 1.08E+08 6.44E+03 8.54E+04 3.22E+06 0.1286 B1-05100AF-SFC-320-GD 5.90E+05 1.06E+08 8.10E+03 0.00E+00 4.05E+06 0.1504 B1-05100AF-SFC-321-GD 2.51E+05 4.53E+07 2.58E+04 6.62E+04 1.29E+07 0.3841 B1-05100AF-SFC-322-GD 7.63E+04 1.38E+07 2.42E+03 4.12E+04 1.21E+06 0.0396 B1-05100AF-SFC-323-GD 1.02E+05 1.84E+07 1.26E+03 2.18E+04 6.32E+05 0.0244 B1-05100AF-SFC-324-GD 6.07E+04 1.10E+07 5.46E+03 4.38E+04 2.73E+06 0.0822 B1-05100AF-SFC-325-GD 1.35E+05 2.44E+07 5.32E+03 3.43E+04 2.66E+06 0.0844 B1-05100AF-SFC-326-GD 3.10E+05 5.59E+07 3.68E+04 2.02E+05 1.84E+07 0.5466 B1-05100AF-SFC-327-GD 2.30E+05 4.15E+07 7.60E+03 1.15E+04 3.80E+06 0.1222 B1-05100AF-SFC-328-GD 1.11E+05 2.00E+07 2.14E+03 3.69E+04 1.07E+06 0.0376 B1-05100AF-SFC-329-GD 9.91E+04 1.79E+07 2.84E+03 9.98E+04 1.42E+06 0.0478 B1-05100AF-SFC-330-GD 3.71E+04 6.69E+06 1.07E+03 3.98E+04 5.35E+05 0.0180 B1-05100AF-SFC-331-GD 9.21E+04 1.66E+07 1.61E+03 2.43E+04 8.07E+05 0.0288 B1-05100AF-SFC-332-GD 8.10E+05 1.46E+08 1.62E+03 0.00E+00 8.10E+05 0.0708 B1-05100AF-SFC-333-GD 8.56E+04 1.54E+07 9.14E+02 9.78E+04 4.57E+05 0.0195 B1-05100AF-SFC-334-GD 1.37E+06 2.47E+08 3.24E+03 1.38E+05 1.62E+06 0.1289 B1-05100AF-SFC-335-GD 1.82E+00 3.28E+02 4.38E+03 1.40E+04 2.19E+06 0.0627 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[159]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SFC-336-GD 3.61E+05 6.51E+07 2.70E+03 7.54E+04 1.35E+06 0.0609 B1-05100AF-SFC-337-GD 6.15E+05 1.11E+08 2.04E+03 8.36E+04 1.02E+06 0.0665 B1-05100AF-SFC-338-GD 1.23E+05 2.22E+07 4.02E+03 6.28E+04 2.01E+06 0.0656 B1-05100AF-SFC-339-GD 7.21E+04 1.30E+07 4.96E+03 7.12E+04 2.48E+06 0.0761 B1-05100AF-SFC-340-GD 5.16E+05 9.31E+07 3.32E+04 7.16E+04 1.66E+07 0.5054 B1-05100AF-SFC-341-GD 6.10E+05 1.10E+08 3.98E+04 1.56E+05 1.99E+07 0.6064 B1-05100AF-SFC-342-GD 5.13E+04 9.26E+06 2.78E+04 1.18E+05 1.39E+07 0.4017 B1-05100AF-SFC-343-GD 4.05E+05 7.31E+07 1.11E+04 1.20E+04 5.57E+06 0.1830 B1-05100AF-SFC-344-GD 1.18E+05 2.13E+07 5.68E+03 7.55E+04 2.84E+06 0.0891 B1-05100AF-SFC-345-GD 1.02E+05 1.84E+07 1.42E+04 1.09E+04 7.10E+06 0.2089 B1-05100AF-SFC-346-GD 8.89E+04 1.60E+07 4.58E+03 1.02E+04 2.29E+06 0.0708 B1-05100AF-SFC-347-GD 2.10E+05 3.79E+07 1.14E+04 6.09E+04 5.68E+06 0.1754 B1-05100AF-SFC-348-GD 2.06E+05 3.72E+07 7.84E+03 2.94E+04 3.92E+06 0.1245 B1-05100AF-SFC-349-GD 1.42E+06 2.56E+08 4.36E+04 5.51E+04 2.18E+07 0.7068 B1-05100AF-SFC-350-GD 7.50E+05 1.35E+08 6.90E+04 8.58E+04 3.45E+07 1.0305 B1-05100AF-SFC-351-GD 9.66E+05 1.74E+08 1.49E+05 1.49E+05 7.46E+07 2.1892 B1-05100AF-SFC-352-GD 1.08E+06 1.95E+08 9.98E+04 0.00E+00 4.99E+07 1.4884 B1-05100AF-SFC-353-GD 9.94E+04 1.79E+07 3.28E+03 5.82E+04 1.64E+06 0.0535 B1-05100AF-SFC-354-GD 1.09E+05 1.97E+07 1.33E+04 2.19E+04 6.67E+06 0.1972 B1-05100AF-SFC-355-GD 2.51E+05 4.53E+07 8.72E+03 8.57E+04 4.36E+06 0.1405 B1-05100AF-SFC-356-GD 9.16E+05 1.65E+08 2.04E+04 1.92E+04 1.02E+07 0.3454 B1-05100AF-SFC-357-GD 8.66E+05 1.56E+08 3.96E+04 4.04E+04 1.98E+07 0.6169 B1-05100AF-SFC-358-GD 1.11E+06 2.00E+08 3.38E+04 1.81E+05 1.69E+07 0.5505 B1-05100AF-SFC-359-GD 2.44E+05 4.40E+07 1.55E+04 1.31E+05 7.74E+06 0.2373 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[160]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SFC-360-GD 4.43E+04 7.99E+06 3.98E+03 4.70E+04 1.99E+06 0.0601 B1-05100AF-SFC-361-GD 7.21E+04 1.30E+07 3.92E+03 3.92E+04 1.96E+06 0.0608 B1-05100AF-SFC-362-GD 1.15E+05 2.08E+07 2.80E+03 1.79E+04 1.40E+06 0.0470 B1-05100AF-SFC-363-GD 7.68E+04 1.39E+07 4.28E+03 4.06E+04 2.14E+06 0.0662 B1-05100AF-SFC-364-GD 1.12E+05 2.02E+07 3.30E+03 6.30E+03 1.65E+06 0.0538 B1-05100AF-SFC-365-GD 1.69E+05 3.05E+07 2.84E+03 3.65E+04 1.42E+06 0.0510 B1-05100AF-SFC-366-GD 6.05E+04 1.09E+07 2.74E+03 9.43E+04 1.37E+06 0.0441 B1-05100AF-SFC-367-GD 1.01E+05 1.82E+07 9.08E+03 3.13E+04 4.54E+06 0.1360 B1-05100AF-SFC-368-GD 3.56E+05 6.42E+07 4.82E+03 9.16E+03 2.41E+06 0.0899 B1-05100AF-SFC-369-GD 1.41E+06 2.54E+08 7.50E+03 0.00E+00 3.75E+06 0.1900 B1-05100AF-SFC-370-GD 8.74E+05 1.58E+08 4.22E+03 3.70E+04 2.11E+06 0.1122 B1-05100AF-SFC-371-GD 8.90E+05 1.61E+08 3.32E+03 1.26E+04 1.66E+06 0.0999 B1-05100AF-SFC-372-GD 5.11E+05 9.22E+07 2.10E+04 0.00E+00 1.05E+07 0.3299 B1-05100AF-SFC-373-GD 4.53E+05 8.17E+07 3.86E+03 1.24E+05 1.93E+06 0.0836 B1-05100AF-SFC-374-GD 6.58E+05 1.19E+08 3.70E+03 7.88E+03 1.85E+06 0.0917 B1-05100AF-SFC-375-GD 4.07E+05 7.34E+07 1.80E+03 9.00E+04 8.99E+05 0.0509 B1-05100AF-SFC-376-GD 3.85E+05 6.95E+07 1.89E+03 9.35E+04 9.45E+05 0.0510 B1-05100AF-SFC-377-GD 3.81E+05 6.88E+07 8.46E+03 2.91E+04 4.23E+06 0.1436 B1-05100AF-SFC-378-GD 1.61E+05 2.91E+07 1.16E+04 3.96E+04 5.80E+06 0.1757 B1-05100AF-SFC-379-GD 9.56E+04 1.73E+07 2.24E+03 1.01E+05 1.12E+06 0.0391 B1-05100AF-SFC-380-GD 1.78E+05 3.21E+07 2.18E+03 3.68E+04 1.09E+06 0.0421 B1-05100AF-SFC-381-GD 8.78E+04 1.58E+07 2.16E+03 3.79E+04 1.08E+06 0.0366 B1-05100AF-SFC-382-GD 8.81E+04 1.59E+07 6.54E+02 4.55E+04 3.27E+05 0.0152 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[161]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SFC-383-GD 1.04E+05 1.88E+07 9.04E+02 2.33E+04 4.52E+05 0.0194 B1-05100AF-SFC-384-GD 6.99E+04 1.26E+07 1.38E+03 9.14E+04 6.92E+05 0.0252 B1-05100AF-SFC-385-GD 1.76E+05 3.18E+07 1.31E+04 1.07E+05 6.56E+06 0.1992 B1-05100AF-SFC-386-GD 2.08E+05 3.75E+07 1.02E+04 0.00E+00 5.09E+06 0.1576 B1-05100AF-SFC-387-GD 6.95E+05 1.25E+08 5.84E+03 7.15E+04 2.92E+06 0.1253 B1-05100AF-SFC-388-GD 1.05E+06 1.89E+08 4.54E+03 0.00E+00 2.27E+06 0.1266 B1-05100AF-SFC-389-GD 9.54E+05 1.72E+08 3.44E+03 1.52E+04 1.72E+06 0.1055 B1-05100AF-SFC-390-GD 1.53E+06 2.76E+08 3.24E+03 9.69E+04 1.62E+06 0.1377 B1-05100AF-SFC-391-GD 5.89E+06 1.06E+09 6.90E+03 5.33E+04 3.45E+06 0.4458 B1-05100AF-SFC-392-GD 5.63E+04 1.02E+07 8.86E+02 3.11E+04 4.43E+05 0.0164 B1-05100AF-SFC-393-GD 1.65E+05 2.98E+07 1.28E+03 2.79E+04 6.41E+05 0.0284 B1-05100AF-SFC-394-GD 2.10E+04 3.79E+06 6.18E+02 1.07E+05 3.09E+05 0.0116 B1-05100AF-SFC-395-GD 7.57E+04 1.37E+07 7.78E+02 3.76E+03 3.89E+05 0.0156 B1-05100AF-SFC-396-GD 4.27E+04 7.71E+06 6.58E+02 2.57E+04 3.29E+05 0.0123 B1-05100AF-SFC-397-GD 9.62E+04 1.74E+07 8.06E+02 6.40E+04 4.03E+05 0.0181 B1-05100AF-SFC-398-GD 7.93E+04 1.43E+07 1.04E+03 1.27E+04 5.22E+05 0.0198 B1-05100AF-SFC-399-GD 1.38E+05 2.49E+07 1.18E+03 1.30E+05 5.91E+05 0.0269 B1-05100AF-SFC-400-GD 2.60E+05 4.69E+07 1.12E+03 7.91E+04 5.58E+05 0.0324 B1-05100AF-SFC-401-GD 1.14E+05 2.06E+07 9.94E+02 5.50E+04 4.97E+05 0.0217 B1-05100AF-SFC-402-GD 2.30E+05 4.15E+07 1.68E+03 7.56E+04 8.40E+05 0.0386 B1-05100AF-SFC-403-GD 3.08E+05 5.56E+07 2.44E+03 7.91E+04 1.22E+06 0.0541 B1-05100AF-SFC-404-GD 3.47E+05 6.26E+07 2.64E+03 8.24E+04 1.32E+06 0.0593 B1-05100AF-SFC-405-GD 1.91E+05 3.45E+07 1.82E+03 1.20E+05 9.12E+05 0.0390 B1-05100AF-SFC-406-GD 1.06E+05 1.91E+07 1.94E+03 9.61E+04 9.69E+05 0.0353 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[162]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SFC-407-GD 1.47E+05 2.65E+07 3.70E+03 5.88E+04 1.85E+06 0.0623 B1-05100AF-SFC-408-GD 4.61E+05 8.32E+07 4.54E+03 4.71E+03 2.27E+06 0.0920 B1-05100AF-SFC-409-GD 2.48E+05 4.48E+07 3.52E+03 1.12E+05 1.76E+06 0.0665 B1-05100AF-SFC-410-GD 2.65E+05 4.78E+07 4.26E+03 8.80E+04 2.13E+06 0.0777 B1-05100AF-SFC-411-GD 2.58E+05 4.66E+07 1.94E+03 3.10E+04 9.71E+05 0.0434 B1-05100AF-SFC-433-GD 1.27E+05 2.29E+07 8.10E+03 7.49E+02 4.05E+06 0.1231 B1-05100AF-SFC-434-GD 1.97E+05 3.55E+07 6.84E+03 5.39E+03 3.42E+06 0.1093 B1-05100AF-SFC-435-GD 2.19E+05 3.95E+07 1.89E+04 9.92E+04 9.44E+06 0.2839 B1-05100AF-SFC-436-GD 2.02E+05 3.65E+07 1.05E+04 4.89E+04 5.25E+06 0.1625 B1-05100AF-SFC-437-GD 1.15E+05 2.08E+07 3.12E+03 0.00E+00 1.56E+06 0.0513 B1-05100AF-SFC-438-GD 1.64E+05 2.96E+07 1.07E+04 3.26E+04 5.33E+06 0.1623 B1-05100AF-SWC-439-GD 2.11E+05 3.81E+07 3.28E+02 4.55E+04 1.64E+05 0.0178 B1-05100AF-SWC-440-GD 6.32E+04 1.14E+07 3.14E+02 0.00E+00 1.57E+05 0.0082 B1-05100AF-SFC-441-GD 7.48E+04 1.35E+07 7.82E+02 4.98E+04 3.91E+05 0.0163 B1-05100AF-SFC-442-GD 8.55E+04 1.54E+07 2.18E+03 5.95E+04 1.09E+06 0.0370 B1-05100AF-SWC-443-GD 9.47E+04 1.71E+07 3.48E+03 1.25E+03 1.74E+06 0.0553 B1-05100AF-SWC-444-GD 8.95E+04 1.62E+07 1.68E+03 1.28E+04 8.42E+05 0.0295 B1-05100AF-SWC-445-GD 7.33E+04 1.32E+07 3.44E+03 6.33E+04 1.72E+06 0.0544 B1-05100AF-SWC-446-GD 6.37E+04 1.15E+07 6.30E+03 1.03E+05 3.15E+06 0.0952 B1-05100AF-SWC-447-GD 4.33E+05 7.81E+07 2.02E+04 6.71E+04 1.01E+07 0.3149 B1-05100AF-SWC-448-GD 1.33E+05 2.40E+07 7.00E+03 0.00E+00 3.50E+06 0.1078 B1-05100AF-SWC-449-GD 7.51E+04 1.36E+07 1.36E+04 2.00E+04 6.78E+06 0.1983 B1-05100AF-SWC-450-GD 1.31E+05 2.36E+07 9.64E+03 1.12E+05 4.82E+06 0.1470 B1-05100AF-SWC-451-GD 8.91E+04 1.61E+07 4.94E+03 9.78E+04 2.47E+06 0.0772 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[163]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Systematic FSS ISOCS Measurements (continued)

Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-SWC-452-GD 4.31E+05 7.78E+07 3.20E+03 4.94E+04 1.60E+06 0.0718 B1-05100AF-SWC-453-GD 2.72E+05 4.91E+07 1.23E+03 4.02E+04 6.15E+05 0.0342 B1-05100AF-SWC-454-GD 2.74E+05 4.94E+07 2.22E+02 6.71E+04 1.11E+05 0.0203 B1-05100AF-SWC-455-GD 1.42E+05 2.56E+07 1.51E+02 4.76E+04 7.54E+04 0.0112 B1-05100AF-SWC-456-GD 9.81E+04 1.77E+07 6.76E+02 2.12E+04 3.38E+05 0.0157 B1-05100AF-SFC-457-GD 4.98E+06 8.99E+08 8.76E+03 4.59E+04 4.38E+06 0.4187 B1-05100AF-SFC-458-GD 7.32E+06 1.32E+09 5.96E+03 0.00E+00 2.98E+06 0.5157 B1-05100AF-SFC-459-GD 2.81E+06 5.07E+08 2.70E+04 0.00E+00 1.35E+07 0.5508 B1-05100AF-SFC-460-GD 2.60E+05 4.69E+07 2.32E+03 2.69E+05 1.16E+06 0.0524 B1-05100AF-SFC-461-GD 7.14E+04 1.29E+07 9.80E+02 2.83E+04 4.90E+05 0.0186 B1-05100AF-SFC-462-GD 2.05E+05 3.70E+07 1.21E+03 1.59E+04 6.03E+05 0.0295 B1-05100AF-SFC-463-GD 6.36E+06 1.15E+09 1.43E+04 1.83E+05 7.15E+06 0.5810 B1-05100AF-SFC-464-GD 3.49E+05 6.30E+07 9.10E+03 6.62E+04 4.55E+06 0.1514 B1-05100AF-SFC-465-GD (2) 6.30E+04 1.14E+07 3.34E+03 3.49E+04 1.67E+06 0.0519 B1-05100AF-SFC-466-GD (3) 1.92E+07 3.46E+09 3.36E+04 1.86E+05 1.68E+07 1.6120 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15 (2) Measurement taken in Elevator Pit (3) Measurement taken in Sump B

[164]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - Measured Concentrations for Judgmental/Investigation ISOCS Measurements Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-IFC-278-GD (2) 4.88E+06 8.81E+08 7.02E+03 2.11E+05 3.51E+06 0.3904 B1-05100AF-IWC-005-GD (2) 3.69E+04 6.66E+06 2.74E+02 3.44E+04 1.37E+05 0.0066 B1-05100AF-IFC-365-GD (2) 9.16E+04 1.65E+07 2.70E+03 2.05E+04 1.35E+06 0.0442 B1-05100AF-IFC-369-GD (2) 1.66E+06 3.00E+08 7.48E+03 3.37E+02 3.74E+06 0.2045 B1-05100AF-IFC-404-GD (2) 3.19E+05 5.76E+07 2.46E+03 3.51E+04 1.23E+06 0.0544 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15 (2) Investigation measurement due to uneven surfaces. Offset reduced by 1 foot.

[165]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Auxiliary Building Basement - QC Replicate ISOCS Measurements Co-60 Ni-63 (1) Sr-90 (1) Cs-134 Cs-137 MEASUREMENT ID OpSOF (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2) (pCi/m2)

B1-05100AF-QWC-006-GD 0.00E+00 0.00E+00 2.98E+02 5.39E+04 1.49E+05 0.0050 B1-05100AF-QWC-024-GD 4.79E+04 8.64E+06 3.26E+02 1.08E+04 1.63E+05 0.0076 B1-05100AF-QWC-074-GD 5.93E+03 1.07E+06 1.61E+02 2.33E+04 8.03E+04 0.0030 B1-05100AF-QWC-102-GD 2.84E+04 5.12E+06 1.47E+03 3.94E+04 7.33E+05 0.0232 B1-05100AF-QWC-116-GD 8.55E+04 1.54E+07 8.06E+02 4.22E+04 4.03E+05 0.0172 B1-05100AF-QWC-131-GD 1.19E+05 2.15E+07 7.02E+02 0.00E+00 3.51E+05 0.0170 B1-05100AF-QWC-132-GD 5.18E+05 9.35E+07 7.20E+03 0.00E+00 3.60E+06 0.1333 B1-05100AF-QWC-156-GD 2.13E+05 3.84E+07 2.40E+04 1.44E+04 1.20E+07 0.3554 B1-05100AF-QWC-167-GD 9.21E+04 1.66E+07 2.62E+03 3.32E+04 1.31E+06 0.0433 B1-05100AF-QWC-208-GD 2.20E+06 3.97E+08 9.50E+03 7.03E+04 4.75E+06 0.2661 B1-05100AF-QWC-218-GD 3.40E+04 6.14E+06 8.48E+02 7.85E+04 4.24E+05 0.0153 B1-05100AF-QWC-230-GD 3.55E+04 6.41E+06 1.07E+02 3.79E+04 5.36E+04 0.0042 B1-05100AF-QFC-243-GD 3.28E+04 5.92E+06 3.06E+01 0.00E+00 1.53E+04 0.0024 B1-05100AF-QFC-272-GD 6.81E+06 1.23E+09 1.01E+04 7.14E+04 5.06E+06 0.5462 B1-05100AF-QWC-292-GD 1.46E+06 2.63E+08 3.38E+04 4.56E+03 1.69E+07 0.5685 B1-05100AF-QFC-331-GD 1.19E+05 2.15E+07 1.64E+03 5.51E+04 8.21E+05 0.0313 B1-05100AF-QFC-333-GD 8.06E+04 1.45E+07 1.00E+03 1.30E+04 5.01E+05 0.0192 B1-05100AF-QFC-334-GD 1.42E+06 2.56E+08 3.28E+03 1.07E+05 1.64E+06 0.1319 B1-05100AF-QFC-341-GD 6.07E+05 1.10E+08 4.18E+04 1.48E+05 2.09E+07 0.6347 B1-05100AF-QFC-373-GD 4.69E+05 8.46E+07 4.10E+03 2.60E+04 2.05E+06 0.0865 B1-05100AF-QFC-395-GD 6.70E+04 1.21E+07 8.82E+02 8.11E+04 4.41E+05 0.0177 B1-05100AF-QFC-405-GD 1.83E+05 3.30E+07 1.72E+03 8.26E+04 8.61E+05 0.0366 B1-05100AF-QFC-409-GD 1.92E+05 3.46E+07 3.22E+03 1.69E+04 1.61E+06 0.0575 (1) Concentrations inferred based on maximum ratios from LTP Chapter 5, Table 5-15

[166]

ATTACHMENT 6 GRAPHICAL PRESENTATIONS AND SUPPLEMENTAL INFORMATION

[167]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Quantile Plot for Co-60 Survey Unit: 05100

Description:

Auxiliary Building Basement Mean: 3.85E+05 pCi/m2 3.00E+07 2.50E+07 Concentration (pCi/m2) 2.00E+07 1.50E+07 1.00E+07 5.00E+06 0.00E+00 0% 20% 40% 60% 80% 100%

Percentage

[168]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Histogram for Co-60 Survey Unit: 05100

Description:

Auxiliary Building Basement Mean: 3.85E+05 pCi/m2 Median: 8.78E+04 pCi/m2 ST Dev.: 1.01E+06 Skew: 5.37 100%

90%

80%

70%

Frequency 60%

50%

40%

30%

20%

10%

0%

4.92E+06 7.38E+06 1.23E+07 1.72E+07 2.21E+07 Upper End Value (pCi/m2)

Upper Value Observation Observation %

Frequency 4.92E+06 398 93%

4.92E+06 8 4%

7.38E+06 5 2%

9.84E+06 3 0%

1.23E+07 1 0%

1.48E+07 3 1%

1.72E+07 0 0%

1.97E+07 4 0%

2.21E+07 1 0%

2.46E+07 3 1%

TOTAL 426 100%

[169]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Quantile Plot for Cs-137 Survey Unit: 05100

Description:

Auxiliary Building Basement Mean: 2.22E+06 pCi/m2 8.00E+07 7.00E+07 6.00E+07 Concentration (pCi\m2) 5.00E+07 4.00E+07 3.00E+07 2.00E+07 1.00E+07 0.00E+00 0% 20% 40% 60% 80% 100%

Percentage

[170]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Histogram for Cs-137 Survey Unit: B1-05100A-F

Description:

Auxiliary Building Basement Mean: 2.22E+06 pCi/m2 Median: 6.91E+05pCi/m2 ST Dev.: 3.89E+06 Skew: 5.16 70 60 50 Frequency 40 30 20 10 0

Upper End Value (pCi/m2)

Upper Value Observation Observation %

Frequency 7.46E+06 382 76%

1.49E+07 21 14%

2.24E+07 14 3%

2.98E+07 3 4%

3.73E+07 3 1%

4.48E+07 1 0%

5.22E+07 1 1%

5.97E+07 0 0%

6.71E+07 0 0%

7.46E+07 1 1%

TOTAL 426 100%

[171]

FSS RELEASE RECORD AUXILIARY BUILDING BASEMENT SURVEY UNIT 05100 Retrospective Power Curve for Survey Unit 05100

[172]

ATTACHMENT 7 ISOCS REPORTS (SEE SEPARATE FILES FOR ISOCS)

[173]

ATTACHMENT 8 EBERLINE REPORTS

[174]

EBERLINE ANAL YT!CAL CORPORATION 601 ScAFmORO F<OAD OM RIDGE. TENNESSEE 37[)30 PHONE ([l6Ci) L,[ll-*0Ul3 FAX ([)65) L,[)3*-4621 EBS-OR-43652 April 30, 2018 Patricia Giza Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099 CASE NARRATIVE Work Order# 18-04022-0R SAMPLE RECEIPT This work order contains seventeen solid samples received 04/05/2018. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.

CLIENT ID LAB ID CLIENT ID LAB ID B 1051 OOAFSWCO l 7CV 18-04022-04 B 1051 OOAFSWCl 56CV 18-04022-13 B 1051 OOAFSWC04 l CV 18-04022-05 B 1051 OOAFSWC l 62CV 18-04022-14 B 1051 OOAFSWC057CV 18-04022-06 Bl05100AFSWC163CV 18-04022-15 B 1051 OOAFSWC088CV 18-04022-07 Bl05100AFSWC179CV 18-04022-16 B 105 lOOAFSWClOlCV 18-04022-08 Bl05100AFSWC190CV 18-04022-1 7 B 1051 OOAFSWC 115CV 18-04022-09 B 1051OOAFSWC201 CV 18-04022-18 Bl05100AFSWC116CV 18-04022-10 B 1051 OOAFSWC2 l OCV 18-04022-19 B 1051 OOAFSWC 150CV 18-04022-11 B 1051 OOAFSWC23 l CV 18-04022-20 B 105100AFSWC151CV 18-04022-12 ANALYTICAL METHODS Total Strontium was analyzed using EIChroM Method SRWOl Modified. Tritium was perfonned using Method LANL ER-210 Modified. Nickel-63 was perfonned using Method ASTM 3500-Ni Modified.

Gamma Spectroscopy was performed using EPA Method 901.1 Modified.

Laboratory qualifiers are as follows:

U - Result is less than the MDA.

ANALYTICAL RESULTS Combined Standard Unce1tainty is repo1ted at I-sigma value.

Minimum Detectable Activity (MDA) values for data represented in this rep01t are sample-specific.

MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.

Page 1 of 3

[175]

ANALYTICAL RESULTS CONTINUED TOT AL STRONTIUM Samples were prepared by acid digestion as appropriate for the matrix. Digested samples were acidified and were selectively extracted and precipitated. Precipitates were then mounted on 47mm filters. Filter was reweighed to determine aliquot size. Sample activities were determined by gas flow proportional counting.

Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are reported from Total Strontium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.

TRITIUM A representative aliquot of each sample was equilibrated with tritium free water. Equilibrates were transferred into a round-bottomed distillation flask and attached to a single stage still. A portion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were then counted by beta liquid scintillation.

Samples demonstrated acceptable results for all Tritium analyses. All results demonstrated slightly high method detection limits. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated an acceptable relative percent difference and normalized difference.

Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.

NICKEL-63 A representative aliquot of each sample was placed into an appropriately sized beaker. Stable elemental Nickel carrier was added to each sample prior to digestion. Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was dete1mined by beta liquid scintillation.

Samples demonstrated acceptable results for all Nickel-63 analyses. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.

GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass/aliquot of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.

Page 2 of 3

[176]

ANALYTICAL RES UL TS CONTINUED GAMMA SPECTROSCOPY CONTINUED Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. Most Cobalt-60 and Cesium-137 results demonstrated slightly high method detection limits. Some samples demonstrated results that are greater than the method detection limit. These results are reported from the Canberra Gamma Apex "Nuclide MDA Report" and are not positive. These results are qualified as non-detect (U). The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Bismuth-214 and Cesium-13 7 replicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-13 7 laboratory control sample demonstrated an acceptable percent recovery.

CERTIFICATION OF ACCURACY I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her designee to be accurate as verified by the following signature.

/ \ ~ - , ~ ~ ~ <<= J M.R. McDougall-- ) (

Laboratory Manager Date: 4/30/2018 Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please visit http://eberlincanalytical.com/ to provide us with feedback on our services.

Page 3 of 3

[177]

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Eberline Analytical ,----ZionSoluUons,-LLC ___ Patricia Giza SDG.

Purchase Order:

18-04022 677118 . -...-------,.--------*-.--**--*-*--*------------ ------

Final Report of Analysis 101 Shiloh Blvd ---------- ---------

ENVIRONMENTAL

_.... ___Analysis_ Category: L -~--------- -------- *--**. *- ... -----------~------ --** -------------

Zion, IL 60099 Sample Matrix: so Sample j Analysis Batch ' Report Lab ID I Sample '

Type  :

Client ID Date Receipt Date Date a1_.;nnrn ! 4/11/2018 I ID 18 04022 i Analyte Tritium Method LANL ER-210 Modified i Result 2.22E+02 cu 8.00E+OO CSU I MDA  ; Qualifier Units or_;,o 18-04022-01 LCS KNOWN 04/05/18 00:00 18-04022-01 LCS  : SPIKE 04/05/18 00:00 4/5/2018 , 4/11/2018 18-04022 Tritium LANL ER-210 Modified 2.24E+02 5.58E+OO 1.37E+01 3.64E+OO : i ora,o

• • ----*-<-** i ora,o 18-04022-02 MBL BLANK 04/05/18 00:00 4/512018 "! 4/11/2018 18-04022 Tritium LANL ER-210 Modified 4.88E+OO 2.27E+OO 2-28E+OO 3.67E+OO 18-04022-03 DUP B105100AFSWC017CV 03/07/i8 09:35 4/5/2018 4/11/2018 18--04022 Tritium LANL ER-210 MnrlifiF>rl fi SSF+OO 1.28E+01 1.28E+01 2.17E+01 u ' "°""

18-04022-04 DO 8105100AFSWC017CV 03/07/18 nq-'.'\_'i 4/5/2018 i 4/11/2018 18-04022 Tritium LANL ER-210 Modified 6.70E+OO 1.29E+01 1.29E+01 , 2:19E+01 '

u orno

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• 9.93E-01 1.66E+OO u oCl/o TRG TRG j B105100AFSWC101CV

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' 3.22E+OO ' u i cC.Uo 18-04022-10 TRG - B105100AFSWC116CV 03/07/18 08:40 4/5/2018 I 4111/2018 rn -="" Tritium lANL ER 210 MnrlrhPrl -6.66E-01 1 SOC+OO 1_50E+OO 2.61E+OO - u i oCilo 18-04022-11 TRG B105100AFSWC150CV 02/21/18 rn=t*an 4/5/2018 4/11/2018 rn -="" Tritium LANL ER-210 Modified 6.72E-01 7.83E-01 7.84E 01 1.32E+OO u  :

oC:,o

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+o

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'" TRG 8105100AFSWC156CV 'V:\n

-- " TRG  : 8105100AFSWC162CV 02/15/18 15:50 4/.s/?018 4/11/2018 18 04022 Tritium LANL ER-210 Modified 2.44E-01 1.39E+OO 1.39E+OO 2.39E+OO u pCi/g TRC B105100AFSWC163CV 02/15/1813:50 4/fit:mrn I ,111-1'"'118 10 " ' " " ' Tritium LANL ER-210 Modified 6.94E 01 1.30E+OO 1.30E+OO _ 2.26E+OO u oC:,o 18-04022-16 i TRG B105100AFSWC179CV 03/07/18 n7*1n 4/5/2018 J 4/12/2018 I 1f!-!1"-1l',.I Tritium LANL ER-210 Modffied -8.43E-01 1_89E+OO 1.90E+OO - 3.30E+OO u ~;;,,;

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+o ,o ' TRG B105100AFSWC201CV 03/06/1815:13 4/5/2018 4/12/2018 : 1R...04022 Tritium LANL ER-210 Modified -1.01E+OO 1.25E+OO 1.25E+OO *r 2.19E+OO  : u i orno I LANL ER-210 Modified 0 OOF+OO 1 OOF+OO 1.09E+OO  : 1.88E+OO u oCi/o TRG ' B105100AFSWC210CV 03/06/1814:40 4/5/2018 I 4/12/2018 : 18 04022 Tritium 1 4'F+OO  : i 2.48E+OO u ' pCi/g TRG i B105100AFSWC231CV 03/06/18 14:30 4/5/2018 4/12/2018 18 04022 Tritium LANL ER-210 Modified 2.53E 01 1.43E+OO CU=Counting Uncert.ainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621

[178]

Printed: 4/30/2018 3:20 PM Page 2 of 22 Report To: Work Order Details:

Patricia Giza 18-04022 Eberline Analytical -' -Pu~fl~;~* OrrlAr SDG:

677118

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Zion Solutions, LLC_ -.>------.. *-**

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101 Shiloh Blvd ------------- ---------- -

Ana/vs/s ENVIRONMENTAL Zion, IL 60099 Sample Matrix: * >::()

Lab  ! Sample I Client Sample Receipt Analysis ' Batch I Analyte Method Result cu CSU MDA Qualifier ,

Report ID  ! Type ID Date Date I Date I ID Units 18-04022-01 LCS KNOWN 04/05/18 00:00

• 4/5/2018 4/9/2018 I 18-04022 Nickel-63 ASTM 3500-Ni Modified 1.50E+03 4.50E+01 erne 18-04022-01 LCS SPIKE 04/05/18 00:00 . 4/5/2018 4/9/2018 18-04022 Nickel-63 ASTM 3500-Ni Modified 1.48E+03 8.98E+OO 8.75E+01 **: 2.11E+OO orno 18-04022-02 MRI BLANK 04/05/18 00:00 4/5/2018 ' 4/9/2018 rn.o.oo, Nickel-63 ASTM 3500-Ni Modified O.OOE+OO 1.21E+OO 1.21E +00

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1B-04022-11 TRG  ! B1051DOAFSWC150CV 02/21/18 08:40 4/5/2018 4/9/2018 18-04022 Nickel-63 ASTM 3500-Ni Modrfied 1.14E+OO 1.23E+OO 1.23E+OO 2.06E+OO u orno 18-04022-1' 8105100AFSWC151CV 02/21/18 09:20 4/5/2018 4/9/2018 18-04022 Nlckel-63 ASTM 3500--Ni MnrlifiP.rl 4.55E+02 4.43E+OO 2.71E+01 1.63E+OO oC,,o 18-04022-13  :;~}; 8105100AFSWC156CV 02/21/18 n-~n 4/5/2018 4/9/2018 18-04022 Nickel-63 ASTM 3500--Ni MnrlrriArl , 1.15E+02 <.38E+OO 7.14E+OO 1.63E+OO  ; or.""

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---

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EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[179]

865/481--0683 FAX 865/483--4621

Printed: 4/30/2018 3:20 PM Page 3 of 22 Report To: Work Order Details*

Patricia Giza 18-04022 Eberline Analytical **-* Zion_Solutions, LLC.

Purchase Order:

SDG:

677118

"*----~-- .

Final Report of Analysis 101 Shiloh Blvd ------Analysis_ Cat~gory-__: ENVIRONMENTAL -. ----

Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample I Receipt Analysis Batch Report I j i

Analyte Method Result cu CSU MDA Qualifier Units ID Type , ID Date I Date I Date ID i 18-04022-01  :

04/05/18 00:00 4/5/2018 . 4111/2018 : 18 04022 Strontium 90 EIChroM SRW01 Modified 1 5.00E+D1 ,.8QE.Q1  : orno LCS KNOWN

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[180]

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Patricia Giza SOG:i 18-04022 Eberline Analytical .. .. Zion Solutions, LLC -*** . .............- ....- .........

, Order 677118 Final Report of Analysis 101 Shiloh Blvd __A_nalysis Category: I

---

ENVIRONMENTAL Zion, IL 60099 Sample Matrix: i so Client Sample Receipt ! Analysis Batch '  : Report

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' u nCi/n 18-04022-02 MBL BLANK 04/05/18 00:00 4/5/2018 , Al<:1'>')18 ,o "'"°' EPA901.1 Modified S fi3F-03 8.06E 02 8.06E-02 'i 3.97E-02 ' u ' ""*""

nC.,r 18-04022-02 MRI RI ANK 04/05/18 00:00 4/5/2018 1 1i:i_n,1n*,*; "" EPA901.1 Modified 8.19E-03 2.01E 02 2.01E-02 3.09E 02 . u 18-04022-02 MBL ' BLANK - 04105/18 nn~~ .t1<;nn15 - 4/5/2018 rn_n,nn Potassium-40 EPA901.1 Modified 1_95E-01 2.91E 01 2.91E-01  : 6.68E-01 u rC"r

'" r , rr MBL BLANK 04/05/18 nn*nn A.Sn018 4/5/2018 J 18-04022 - EPA901.1 Modtfied 8.56E 03 2.35E-02 2.35E 02 ' 8.51E-02 '

u """"

,r n , rr MBL BLANK nam1 s nn,nn " EPA901.1 Modtfied -1.31E-02 3.87E 02 3.87E-02  : 5.19E-02 T u """"

'" "" MRI BLANK 04/05/18 00:00 4/S/?018 4/fil'.)018 .. , 18 04022 lead-210 EPA901.1 Modffied 3.59E-01 3.18E-01 ' 3.18E-01 5.37E-01 u rCi/r 04/05/18 nn*on 4/5/2018 i 18-04022 Lead-212 EPA901.1 Modified 2.07E 02 4.49E-02 4.49E-02 7.20E 02 u pCi/g 18-04022-02 MBl BLANK 04/05/18 nn-nn

""'°'"

,,s,,nrn 4/5/2018 ,a_c,nn Lead 214 EPA 901.1 Modified 4.80E 02 6.67E-02 6.67E 02 1.15E-01 u

- ;;_~;;,-*-

18-04022-02 MBL BLANK 18-04022-02 MBL BLANK 04/05/18 00:00 415001' 4/5/2018 '18-04022 EPA901.1 Modified 1.35E-v, "

-02 3.50E-02  : 5.07E 02 u rCi/o 18-04022-02 : MBL ' BLANK 04/05/18 (l[):00 AIS/0018 4/5/2018 , 18-04022 Radium-226 EPA 901.1 Modified -1.09E-01 1.16E-01 1.16E-D1 1.27E-01 u rC.i/r 18-04022 EPA 901.1 Modified 1.13E-02 '""-°' 1.71E 01 u pCi/g 18 04022 02 ; MBL BLANK 04/05/18 00:00

,s,,nrn 4/5/2018 "'"-"' I

' u 18-04022-02 ° MBL BLANK 04/05/18 nn-nn 4/5/2018 "-04022 "

EPA901.1 Modified 6.43E-01 HOC.M "'1E-01  ! 6.57E 01 18-04022-02 i MBL BLANK 04/05/18 00:00 4/5/2018 4/5/2018 18-04022 Thallium 208 EPA 901.1 Modified 5.43E 03 1.51E-01 1<i11=_1J1

' 2.08E-01 u """"

04/05/18 00:00 4/5/2018 4/5/2018 18-04022 i Uranium-235 EPA901.1 Modified 1.95E 01 3.89E-01 , 404.Q1  ! 2.39E-01  : u pCl/9 18 04022-02 MBL BLANK CU=Counting Uncertainty;CSU=Comblned Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect

( EBERLINE

~ ***-"*" . . --- Af'1ALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[181]

865/481-0683 FAX 865/ 483-4621

Printed: 4/30/2018 3:20 PM Page 5 of 22 Report To: Work Order Details:

022 Eberline Analytical Final Report of Analysis Patricia Giza

- *

• Zion Solutions, LLC **-*--********

101 Shiloh Blvd

• • • ' P.~rc.h.;;;t!*.

....... Analysis

~+*i7t~!

Categoryt-ENVIRONMENT

• I 4L .. .. *------*****--***

Zion, IL 60099 **""" Sample Matrix.~ SO Receipt Batch Report lab

!O Sample Type Client ID Sample Date Date Analysis ;

Date j ID Analyte Method Result  ! cu CSU MDA Qualifier ;

Units

,__1s_._o,_0_2_2._0_3*+-D_U*P*-i-**B**1**05***1**o**O*A*F*S**W*C*0*1*7*C**v**-*---+-03_1_07..l.18.. 0.9..,3.5*****i .4./5/2018 4/5/2018

• 18-04022 Actinium-22.s". :E,:P.A,:..':0,.1*. ,..1*..*M::'c:'::","::.':****+*~'*:':'E:*.D,:1.*+-':*':O~E:*0:1.-+..:: 6 ..2::

1 E,*:O 1..*_1:.:*~13,.E:+:o:o.i.-*:":.....:..... p:i~g -----

18-04022-03 DUP , 8105100AFSWC017CV 03/07/1809:35 4/5/2018 : 4/5/2018 18-04022 Silver-108m EPA901.1 Modified 1.33E-01 1.54E-D1 1.54E-01 1 2.76E-01 U  : m,1m 18--04022-03 DUP : B105100AFSWCD17CV 03/07/18 09:35 4/5/2018 4/5/2018 ; 18-04022 Americium-2;41: +******:E:P,:A::9c0*1* .***1 :M*::o::d:;ifi:,d:**..f-.~3.c4:0;::Ec.~01;*'-~11'= .36;::E*0::.1+*1:l.:::::37E~*0*1***.. C4;.2f4:~E~.Q~1;-'- *:u***+********=,c;;c:',*****.J 1-18':*.:o,:o:.:,=,.*'o*:, *+ *o=:u:=e ....., =s**1::o,=*1:0+0A::,=s~w*:c=o=*11*c':v.:************ + *0=3"10=,=*1'1B'o'9:3~s:**t-,'1,:1:::'201':.*-'*1::s'12'0"1Bt-.+1:s.-04.::0~2~2't*"sca:,,:,m,c:*.1::3:3,*-,f** *=e~P'A:9::0:1.'1: cM,:,,,c:ifi:,,:. ..,.....:3.:86,:e=*.o:,:* '*1*'.1 'o"e.'0*1: -i*****1:*.1'oe.0=*1 * +** ***,*:.4~5::e'.*0~1=*****::u':-*+-**',*c=;;::,'* ***** 1 18-04022-03 DUP B105100AFSWC017CV 03/07/1809:35 4/5/2018 , 4/5/2018 04022 Bismuth-214 EPA90U Modified 8.29E-01 ) 4.60E-01 4.62E-01 I 8.75E-01 U oCi/a 18-04022-03 DUP , 8105100AFS~~?_1_~~-':'.'.... -- 03/07/1809:35 41'>1"Jll1tl 4/5/2018 1 18-04022 Cobalt-60 EPA901.1 Modified -1.74E-02  !'i47F-O? 5.47E-02 - 1.75E-01 U n(;i/n 18-04022-03 DUP , B105100AFSWC017CV 03/07/1809:35 4/5/2018 4/5/2018 18-04022 , ,..,., EPA901.1 Modified 3.71E01 1.92E-01 1.93E-01 3.06E-01 , U nrnn 1

18 04022--03 DUP B105100AFSWC017CV 03/07/18 09:35 4/5/2018 4/5/2018 18 04022 Cesium-137 EPA 901.1 Modified 1.97E-01 L<l8t:-U1 2.40E-01 3.94E-01 U n(;i/n 1..1,.s:.Q:c40:22:c*.0::3.. : ....:o.u..e.. ****+****"..1..0..'.1..o..0AFSWC017CV 03/07/18 09:35 4/5/2018 4/5/2018 18-04022 EPA 901.1 Modified 1.30E+OO 9.09E-01 9.11E-01 6.98E 01 ' U pCt/a 18-04022--03 DUP 8105100AFSWC017CV 03/07/1809:35 4/5/2018 4/5/2018 : 18-04022 Europium-154 EPA901.1 Modified 2.90E-01 4.01E-01 4.02E-01 I 3.57E-01 U oCi/a

.. DUP , B105100AFSWC017CV 03/07/1809:35 4/5/2018 4/5/2018 18-04022 EPA901.1 Modified ( -5.52E-02 8.62E-02 8.62E-02  : 5.21E-01 U oCi/a

_ -~~~-~~~.1 Modified

,o I DUP 8105100AFSWC017CV 03/07/1809:35 4/5/2018 4/5/2018 : 18-04022 Holmium-166m -  !'i.30E-02  ?.80E-01 2.80E-01 i 2.61E-01 U nl,J/n,, .....

18-04022-03 DUP , 8105100AFSWC017CV 03/07/1809:35 4/5/2018 4/5/2018  ! 18-04022 lodine-129 EPA901.1 Modified -1.96E+OO 1.61E+OO 1.62E+OO ' 1.95E+OO U nl,l/n 18-04022--03 DUP 8105100AFSWC017CV . '"()J/07/1809:35 4/5/2018 4/5/2018 18-04022 Potassium-40 EPA901.1 Modified 7.31E+OO 2.46E+OO 2.49E+OO i 2.68E+OO  ; PCIIQ 18-04022-03 DUP , 8105100AFSWC017CV 03/07/1809:35 4/5/2018 4/5/2018 1804022 ... EPA901.1 Modified -9.97E-02 1.58E-01 1.59E-01 _ 2.21E01  : U  : PCi/Q 18-04022-03 DUP 8105100AFSWC017CV 03/07/1809:35 4/5/2018 4/5/2018 18-04022 Niobium-94 EPA901.1 Modlfied 8.88E-02 1.41E-01 1.41E-01 I 2.29E-01 U oCi/a IIP  : 8105100AFSWC017CV 03/07/1809:35 4/5/2018 ' 4/5/2018 18--04022 Lead-210 EPA901.1 Modified -7.90F+OO 3.87E+OO 3.89E+OO I 5.32E+OO U oCl/o

,. DUP 8105100AFSWC017CV 03/07/18 09:35 4/!Jl:lUHl 4/5/2018 18 04022 Lead 212 EPA 901.1 Modified -?.:.lflF-0? fi.27E-02 fi.27E-02  ; 5.77E 01 U oCi/o 18--04022 03 DUP B105100AFSWCD17CV 03/07/18 09:35 4/5/2018 4/5/2018 18 04022 Lead 214 EPA 901.1 Modrt1eo -R ~1.:-0? 7.86E--02 7.87E-02  ; 7.02E-01 U  : nCi/o

,o 00 DUP 8105100AFSWC017CV 03/07/18 09:35 4/5/2018 ' 4/5/2018 Promethium=*1:~4:5j ....:E,:P:'.A:9,:0:1:*.1~MC:"'='"~d*-f-':':1.38=E+::'00-+**7+'*.4::;ce:=::.*"":...;..~ 7.4C::9E=:*01: ******;:1.1:2CEC'.+.,OCO.-t******"c*+'--'o'.;:.°":,">c..*.

• 18-04022-03 DUP 8105100AFSWC017CV 03/07/18 09:35 4/5/2018 : 4/5/2018 18-04022 Radlum-226 EPA 901.1 Modified 8.29E-01 4.60E-01 4.62E-01 ' 8.75E-01 : U  ! 0G1/a 1

18--04022 03 DUP B105100AFSWC017CV 03/07/18 09:35 4/5/2018 4/5/2018 ; 18--04022 EPA 901.1 Modified -:I !'i7F-O? 5.58E-01 5.58E-01  ! 8.51E 01 U i oCi/o 18-0402 B105100AFSWC017CV 03/07/18 09:35 4/5/2018 ' 4/5/2018 18--04022 Thorium 234 EPA 901.1 Modified 5.44E+OO 2.14E+OO 2.16E+OO 5.71E+OO , U  : n(;i/o

_1_**.04 . 02_2_.0_3

. **,. . .o..u.P_*+***"**1_o_s1.o...o.A...F..s..w ...c..o..1.1..c..v.....*..........+*****0***310111809:35 4/5/2018 4/5/2018 , 18--04022 Thallium-208 EPA901.1 Modified -1.32E-02 1.75E-01 1.75E-01 8.05E-01 1 u . "'"....

..)

18-04022-03 [ DUP B105100AFSWC017CV 03/07/1809:35 4/5/2018 4/5/2018 , 18-04022 , Uranlum-235 EPA901.1 Modified -2.74E-01 2.60E+OO 2.60E+OO I 1.44E+OO U  : pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE EBERLINE ANALYTICAL CORPORATION MY-------------------------* -"-A'"N -;_-L_*y-+*;-c-A*L 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[182]

Printed: 4/30/2018 3:20 PM Page 6 of 22 Report To Work Order Details:

Patricia Giza SDG: 18-04022 Eberline Analytical ' ---

Zion Solutions, LLC - ',,,, ---- Purchase Order:

• 677118

~------*---*-*--*** '""""""'--*--*------ - - - - - " " ' ...... ..... ... ...-------..*---------------.... ---- --- "----..---..--------- *---*--..-------

Final Report of Analysis 101 Shiloh Blvd.......... - .... ---------*---- .. .Analysis Category: _ ---..ENVIRONMENTAL so Zion, IL 60099 Sample Matrix:

Lab Sample Client Sample Receipt Analysis I Batch Report Analyte Method Result cu CSU MDA i Qualifier _

Unlts ID Type ID Date Date i Date ID

• i 18-04022-04 DO B 1051 OOAFSWC017CV 03/07/18 09:35 4/5/2018 4/5/2018 18-04022 Actinium-228 EPA901.1 Modified 3.27E-01  ! 6.99E-01 6.99E-01 U8E+OO u orno 18----04022-04 DO B105100AFSWC017CV 03/07/18 09:35 4/5/2018 4/5/2018 18-04022 Silver 108m EPA 901.1 Modified 2.06E 02 3.71E 02 3.71E-02 2.42E-01 u orno 18-04022-04 DO

"'1'"""'

I B105100AFSWC017CV

~----- 03/07/18 09:35 4/5/2018 ; 415/2018 18-04022 Americium-241 EPA 901.1 Modified -1.17E-01 9.61E-02 9.63E-02 4.49E-01 u ' -r""

18-04022-04 DO B105100AFSWC017CV 03/07/18 09:35 4/5/2018 ; 4/5/2018 ,18-040?7 Barium-133 EPA 901.1 Modified 3.63E-01 3.04E-01 3.05E-01 4 67F-01 u ,c,,,- -

,- '-* ' DO ' B105100AFSWC017CV 03/07/18 09:35 4/5/2018 : 4/5/2018 : 18---04022 Bismuth-214 EPA901.1 Modified 6.20E 01 3.69E-01 3.71E-01 5.47E-01 ' """"

18-04022-04 I DO B105100AFSWC017CV 03/07/18 09:35 4/5/2018 : 4/5/2018 18-04022 Cobalt-60 EPA901.1 Modified 8.30E-02 1.81E-01 '1,1,:01 2.84E 01 ' u -r"-

,o

"' I DO 8105100AFSWC017CV 03/07/18 09:35 4/5/2018 4/5/2018 e 18-04022 Cesium 134 EPA901.1 Modtfied -1.09E-01 1.14E 01 1.15E 01 2_93E-01 I u icu,

'" '"' DO B105100AFSWC017CV 03/07/18 09:35 4/5/2018 i 4/5/2018 ; 18 04022 Cesium-137 EPA901.1 Modified 2.76E-01 2.00E-01 2.00E 01 3.58E 01 : u PC'O

o 4/5/2018 EPA901.1 Modified -9.64E-03 3.30E-01

3.30E 01 6_69E-01 : u

'"' uu ' B105100AFSWC017CV 03/07/18 09:35 I 4/5/2018 18-04022 or,,o

'" '"' uu B1051 OOAFSWC017CV 03/07/18 09:35 4/5/2018 4/5/2018 18-04022 Ecrnpicm-1 S4 EPA901.1 Modtfied 2.05E 01 3.67E-01 ' 3.67E-01 3.39E-01 i u

,, ',, 00 B105100AFSWC017CV 03/07/18 09:35 4/5/2018 : 4/5/2018 18-04022 EPA 901.1 Modified ' 2.35E-01 o_34E-01 ' 2.34E 01 5.10E 01

' u oC,>o

-- 00 B105100AFSWC017CV 03/07/18 09:35 4/5/2018

• 4/5/2018

• 18-04022 Holmium 166m 1-<-_.. ___ EPA901_1 Modified 3.78E 02 nos 01

-, 2.68E-01 2.64E-01 i u -r""

18-04022-04 DO B105100AFSWC017CV 03/07/18 09,35 4/5/2018 ) 4/5/2018 18-04022 lodlne-129 EPA 901.1 Modified -1.85E+OO 1.53E+OO 1.54E+OO 1.87E+OO u or>>r

"' DO B105100AFSWC017CV 03/07/18003S 4/5/2018 i 4/5/2018

• 1fW40?? Potassium-40 EPA901.1 Modified 7.47E+OO 2.13E+OO 2.16E+OO 1.20E+OO -r""

18-04022-04 18 04022 04 DO DO 8105100AFSWC017CV B105100AFSWC017CV 03/07/18 OP-3S 03/07/18

,, nQ*S'i 4/5/2018

""""J18 415/2018 415/2018

,~Mon 10,MMO

- EPA901.1 Modified EPA901.1 Modified ~=t]~'

-5.66E-O 1.75E 01 5.22E 02 1.75E-01

_ 2.78E-01 2.65E-01 u

u u

pCi/p 18-04022-04 DO B105100AFSWC017CV 03/07/18 09:35 4/5/2018 4/5/2018 18-04022 Lead-210 EPA901.1 Modified -2.16E+OO 3.18E+OO 3.19E+OO 5.26E+OO ""-""

18-04022-04 DO B105100AFSWC017CV 03/07/18 09:35 8 ' 4/5/2018 18 04022 Lead 212 EPA901.1 Modified SCOC,O, 5.28E-01 5.29E 01 8.56E 01 u ,cu, 18 04022 04 DO B105100AFSWC017CV

-03/0 8 18-04022 Lead-214 EPA901.1 Modified 0 '""-"' 7.63E 01 7.64E-01 1.22E+OO u ,cu, 18-04022-04 DO B105100AFSWC017CV 03/07/18 09:35 4/5/2018 415/2018 18-04022 "" EPA901.1 Modified 7.47E 02 4.95E 01 4.96E-01 : 1.07E+OO u T

,cu, 18-04022-04 DO B105100AFSWC017CV 03/07/18 09:35 4/5/2018 - 4/5/2018 : 18-04022 Radium-226 EPA901.1 Modified 6,20E-01 3.69E-01 3.71E-01 1 5.47E 01 -r""

,oo 5.53E 01 8.47E 01 u '

18 04022-04 18-04022 04 DO DO B105100AFSWC017CV 8105100AFSWC017CV 03/07/18 09:35 03/07/18 09:35 4/5/2018 4/5/2018 C

a 4/5/2018 4/5/2018 18-04022 18-04022

~

Thorium-234 EPA 901.1 Modified EPA 5.43E~~rt

.25E+O . 0 2.80E+OO I 4.57E+OO u

,cu, 18-04022 04 DO 8105100AFSWC017CV 03/07/18 09:35 4/5/2018 i 4/5/2018 rn,04on Thalllum 208 EPA 901.1 Modified 5.39E-01 5.48E-01 ' 5.49E-01 9.60E 01 u -r""

18-04022-04 DO B105100AFSWC017CV 03/07/18 09:35 41512018 I 415/2018 18-04022 Uranium 235 EPA 901-1 Modified 3.00E+OO 2.67E+OO

' 2.67E+OO 1.43E+OO u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect

( ~

EBERLINE "AN.ALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[183]

865/481-0683' FAX 865/483-4621

Printed: 4/30/2018 3:20 PM Page 7 of 22 Report To.- Work Order Details*

Patricia Giza SDG. 18-04022 Eberline Analytical I ---- ... ----- -*-*

677118

---

~*---- Zion.Solutions, LLC . ------

Purchase Order:

Final Report of Analysis 101 Shiloh Blvd ENVIRONMENTAL .* **********

Zion, IL 60099 Sample Matrix: - so -;

!  ! Report Lab ID I Sample Type Client ID Sample Date Receipt Date Analysis Date Batch ID Analyte Method Result

. cu CSU MDA Qualifier  ! Units 18-04022--05 TRG B105100AFSWC041CV 03/07/18 09:25 4/5/2018 4/5/2018 18.04022 Actinium-228 EPA901.1 Modified 4.02E-01 4.03E-01 7.44E-01 u ' ,cu, 6.44E-01------\*

18-04022-05 TRG B105100AFSWC041CV 03/07/18 09:25 4/5/2018 4/5/2018 18-04022 Silver-108m EPA901.1 Modified 5.03E-02

-2.67E-02 7.08E-02 1.89E-01 7.08E-02 1.89E-01

' 1.27E-01 2.43E-01 '

u u

. *'~~'******

18-04022-05 TRG 8105100AFSWC041CV 03/07/18 09:25 4/5/2018 4/5/2018 18-04022 Americium-241 EPA 901.1 Modified 18-04022--05 TRG B105100AFSWC041CV 0310711809'25 4/5/2018 4/5/2018 18 04022 Barium 133 EPA 901.1 Modified

°*°'

1 5.93E-02 2.91E-01 5.93E-02 2.93E-01

! 1.85E 01 5.12E 01 u

PCl/c TRG B105100AFSWC041CV 03107118 09,25 41512018 4/5/2018 I 18 04022 , Bismu!h-214 EPA 901.1 Modified I

. CSIC7118m?S 4151?018 4/5/2018 18 04022 Cobalt-60 EPA901.1 Modified *163E*02 7.61E 02 7.61E 02 1.18E-01 u oCilo

.. . .. TRG B105100AFSWC041CV

.4 osc.ns u or;,o

' TRG B105100AFSWC041CV 03/07/18 OQ*?<;

""° """ 18-04022 Cesium 134 EPA 901.1 Modified 3.55E-02

"*"*°' 1.19E-01

' .. TRG B105100AFSWC041CV 03/07118 09:25 .,s,,orn ' 4/5/2018  : 18-04022 Cesium 137 EPA901.1 Modffied 2.52E+OO 3_75E-01 3.97E-01 2.61E 01 . pCi/g

' 2-27E-01 2.27E-01 3.49E 01 u orno

• 18 04022-05 TRG

. B105100AFSWC041CV 03/07/18 09:25 4/5/2018 4/5/2018

"*"'°" 152 EPA901.1 Modified 1.53E 02 154 3.03E-02 2.49E 01 2.49E 01 1.83E-01 u cC!lc i'

18-04022-05 TRG 8105100AFSWC041CV 03/07/18 0 8 4/5/2018 , 18-04022 EPA901.1 Modified 18-04022 05 TRG . B105100AFSWC041CV 03/07/18 09:25 4/5/2018 I 18--040?? Europium-155 EPA901.1 Modified 7.92E-02 0 07C o, ,me o, 2.84E-01 u .rn.

rn.0400, 6.33E-03 <COCO*

1.59E-01 . 1.43E 01 u *; pCi/g 18-04022-05 TRG I B105100AFSWC041CV 03/07/18 09:25 4/5/2018 4/5/2018 EPA901.1 Modified

~

1'.C,00, ,oo;oo.1'C EPA901.1 Modified -8.81E-02 1.19E-01 1.20E-01  : 1.48E-01 u oC;/c ....

18-04022-05 TRG 8105100AFSWC041CV 03/07/18 09:25 4/5/2018 4/5/2018

-.--~------

EPA901.1 Mo 1.82E+OO 1_84E+OO  : 2.24E+OO ornc 18--04022 05 TRG

' B105100AFSWC041CV

""""'" 4/5/2018 18-04022 Potassium 40 4/5/2018 ' 18-04022 EPA901.1 Modified 3. 6.03E-02 6.04E-02 i 1.67E-01 u ornc 18--04022 05 TRG B105100AFSWC041CV 18-04022-05 TRG ' B105100AFSWC041CV 03/07/18 09:25 4151201' 41512018 18 04022 , Nloblum-94 EPA901.1 Modified 3.55E-02 S.81E*02 8.81E 02 1.55E-01 u '

oCUc

, ,,c.oo u  ;

> oc

'"" B1051 OOAFSWC041 CV 03/07/18 09:25 4/5/2018 4/5/2018 18 04022

• Lead-210 EPA901.1 Modified 1.67E+OO 1.11E+OO 2.02E+OO *"""

,. > oc 1KG  :' B105100AFSWC041CV 03/07/18 09:25 4/5/2018 4/5/2018 rn.o,oo, Lead212 EPA901.1 Modified 1.66E 01 1.99E-01 1.99E-01  : 2.87E 01 u *"""

.. ... TRG B105100AFSWC041CV 03107/18 09:25 4/5/2018 4/5/2018 18-04022 Lead 214 EPA 901.1 Modified 8 1 2.89E-01 I 4.62E 01

.. ' .. TRG ' B105100AFSWC041CV 03/07/18 09:25 4/5/2018 4/5/2018 ,~o;o, ...

EPA901.1 Modified 9.38E 01 1.37E 01 2.27E-01 u ' orno

' 2_91E-01 cC!lo 18-04022 05 TRG

' B105100AFSWC041CV 03/07/18 09:25 4/5/2018 4/5/2018 18*04022 Radium 226 EPA 901.1 Modified 6.87E 01 2.93E-01 I 5.12E--01 18-04022 05 18-04022 05 TRG TRG

' 8105100AFSWC041CV B105100AFSWC041CV 03/07/18 09:25 03/07/18 09:25 4/5/2018 41512018 4/5/2018 '

4/5/2018 18-04022 18-04022 Thorium 234 125 EPA901.1 Modified EPA 901.1 Modified 9.63E 02 1.22E+OO 1.86E+OO 2.is.01 1.86E+OO

, 4.33E 01

i,.;;;;

u u

cCilo 18-04022 05 TRG B105100AFSWCD41CV 41512018 ; 4/5/2018 18-04022 Thallium 208 EPA901.1 Modified 4.91E-01 2.87E-01 2.88E*01 ' 5.33E 01 u om, 18--04022 05 TRG B105100AFSWC041CV >> 41512018 , 4/5/2018 18-04022 Uranium-235 EPA901.1 Modified ' 3.99E-02 1.30E+OO , 7PC,OO  : 7.07E-01 u i pCi/g CU=Counting Uncertainty;CS U=Combined Standard Uncertainty (1-sigma); M DA=Minimal Detected Activity; LCS=Laboratory Control Sample;M BL=Blan k;DU P=Duplicate; TRG=Nonnal Sample;DO=Duplicate Original; U=Non-detect EBERLINE EBERLINE ANALYTICAL CORPORATION

~ ANALYTICAL 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621

[184]

Printed: 4/30/2018 3:20 PM Page 8 of 22 Report To: Work Order Details:

Patricia Giza 18-04022 Eberline Analytical ' .

Zion LLC Purchase Order.

SDG:

677118 . --------- ------*-------------

Final Report of Analysis 101 Shiloh Blvd- .

.. . .. - ... ......... *- - .. ___...._.._..___ ,__.Analysis Category: i *- ENVIRONMENTAL.... ... ----* ..* - --------

Zion, IL 60099 Sample Matrix: so L*b Sample Client Sample Receipt i Analysis i Batch

! cu i Report ID i

Type ID Date Date Date i ID Analyte Method Result i

! CSU MDA Qualifier Units 18-04022-06 TRG B105100AFSWC057CV 03/07/18 09:1( 4/5/2018 : 4/512018 I 18 04022 Actinium 228 EPA 901.1 Modified 6.57E-01 3.46E-01 3.48E-01  : 7.74E-01 u oC""

18-04022-06 TRG B105100AFSWC057CV 03/07118 09:1( 4/5/2018 415/2018 18.040,; Silver-108m EPA901.1 Modified -5.25E-02 1.29E--01 1.29E-01 1.45E--01 u ..rn..

18--04022-06 TRG 8105100AFSWC057CV 03/07/18 ml*1( 4/5/2018 : 4/S/?01' ,S.040>0

'""" EPA 901.1 Modified i -4.65E-01 2.69E-01 2.70E 01 2.65E 01 u "°""

18-04022-06 TRG 8105100AFSWC057CV 03107/18 09:10 4/512018 4/5/2018 18-04022 Barium-133 EPA901.1 Modified 1.07E 02 7 '"*°' 7.32E 02  ; 2.61E--01 u "°""

18-04022-06 TRG B105100AFSWC057CV 03/07/1809:10 4/51201" 4/5/2018  ! 18 04022 Bismuth 214 EPA901.1 Modified 6.49E 01 ,iie:61 2.75E-01 6.14E-01 "°""

18-04022-06 TRG B105100AFSWC057CV 03/07/1809:10 415/2018 4/5/2018

• 18-04022 Cobalt-60 EPA901.1 Modified i .1,3e.02 6 RSF.07  : 6.83E-02 i 1.36E-01 u oColo 18-04022-06 TRG B105100AFSWC057CV 03/07/18 09:10 415/2018 4/5/2018 c 18-04n?? Cesium-134 EPA 901.1 Modified ' .3 nF.07 7.61E-02  ; 7.61E-02  ! 2.02E-01 u ..c,,..

18-04022-06 TRG  ; B105100AFSWC057CV 03/07/18 09:10 4/5/2018 4/5/2018 : 18-040?? Cesium-137 EPA901.1 Modified 2.19E*01 1.52E*01 1.52E-01 2.37E-01  :

u  ; orno 18-04022-06 TRG  : B105100AFSWC057CV 03/07118 mm 4/5/2018 4/5/2018 18 04022

• EPA 901.1 Modified .'3,F.C, 4.49E*01 4.49E-01  ! 3.53E-01 u "°""

1" 8105100AFSWC057CV 03/07118091C 4/5/2018 ! 4/5/2018 18-04022 EPA901.1 Modified S.07E*02 ;53e.61 2.58E-01 1.78E-01 u "°""

-~--- -~**-*** ---- . .

18-04022-06 TRG B 1051 OOAFSWC057CV 03107/18 09:1C 4/5/2018 4/5/2018 j 18 04022 EPA901.1 Modlfied *4.12E*02 7 OfiF.01 2.06E-01 I 3.31E-01 u """"

18-04022-06 TRG ' B105100AFSWC057CV 03/07/18 09:10 4/5/2018 : 4/5/2018  ! 18-04022 Holmium-166m EPA901.1 Modlfied

.. 2.36E*02 1.82E*01 1.82E-01 1.74E-01 u "'oC.:>o 18-04022-06 TRG  ; B105100AFSWC057CV 03/07/18 09:10 4/5/2018 : 4/5/2018  ! 18-04022 lodine--129 EPA901.1 Modffied 1.08E-01 1.50E-01 1.50E-01 I 2.13E-01 u 18-04022-06 TRG  : B105100AFSWC057CV 03/07/18 09:10 4/5/2018 4/5/2018 18-04022 Potassium-40 EPA901.1 Modified 6.82E+OO 2.30E+OO 2.33E+OO 2.90E+OO

• pCi/g 18---04022 06 TRG 8105100AFSWC057CV 03/07/18 09:10 4/5/2018 4/5/2018 18-04022 § EPA901.1 Modified '4.78E*02 1.01E-01  ; 1-01E-01 ' 1.40E-01 u . oC""

18-04022-06 TRG B105100AFSWC057CV 03/07/18 flQ*1[1 MSO>J18 4/5/2018 18 04022 *: Niobium-94 EPA901.1 Modified 7.58E*02 8.70E 02 8.70E 02 . 1 1.51E 01 u . oC:>o 2.79E+OO .....  ;

18--04022 06 TRG 8105100AFSWC057CV 03/07/18 09:10 4/5/2018 4/5/2018 I 18 04022 Lead 210 EPA901.1 Modified , "C+OC 2.01E+OO 2.01E+OO *1 u pCi/g

"" . "" TRG 6105100AFSWC057CV 03/07/18 09:10 4/5/2018 4/5/2018 I 18 04022 Lead 212 EPA 901.1 Modified 4.53E*01 2.38E 01 2.40E 01 *1 3.61E 01 ' oC""

18-04022-06 TRG 8105100AFSWC057CV 03/07/18 09:10 4/5/2018 4/512018 18.04077 Lead-214 EPA901.1 Modified S.06E*01 2.65E-01 2.67E-01  :

4_85E-01 oC,lo 18---04022 06 TRG 8105100AFSWC057CV 03/07/18 09:10 4/5/2018 4/512018 i rn.om, EPA 901.1 Modified 4.38E-02 1.89E*01 1.89E-01 . 2.61E 01 u "°""

• 18*04022

• S.49E*01 * ;iie:,; 2.75E-01 6.14E-01 oCi>o 18---04022-06 TRG *-* 03/07/18 09:10 4/5/2018 4/5/2018 Radium-226 EPA 901.1 Modified

.o ,oc.M , o,c 01 18---04022-06 TRG B105100AFSWC057CV 03/07/18 09:iO 4/5/2018 4/5/2018 : 18 04022 EPA 901.1 Modified 2.95E 01 4.38E-01 u oC:>o 18--04022 06 TRG B105100AFSWC057CV 03/07/1809:10 4/5/2018 4/5/2018 i 18 04022 Thorium 234 EPA901.1 Modified  ! 2.66E+OO  :  ?.75F+OO 2.75E+OO - ' 4.58E+OO u  ; oC:>o 18---04022-06 TRG i B105100AFSWC057CV 03/07/1809:10 4/5/2018 4/5/2018 j 1R-04'1?? Thallium-208 EPA 901.1 Modified . S.57E*01  ; 4.02E*01 4 03E*01 i 7.18E--01 u i """"

18-04022-06 TRG B105100AFSWC057CV 03/07/18 09:10 4/5/2018 41512018 I 18-04022 \ Uranium-235 EPA901.1 Modified 1.80E 01 j 1.Hti::+nn 1 rnc+oo  : 8.26E-01

u pCl/g CU==Countlng Uncertainty;CSU=Combined Standard Uncertainty (1-sigma); MDA=Minimal Detected Activity; LCS=Laboratory Control Sample; M BL=Blank; DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect

( ~,E_l::11;:RLI NE

~ ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[185]

865/481-0683 FAX 865/483-4621

Printed: 4/30/2018 3:20 PM Page 9 of 22 Report To* Work Order Details:

Patricia Giza 18-04022 Eberline Analytical I .

Z.ionS.olutio.ns,LLC ... ------- ---------- -------

SDG:

, nmor 677118 ...

---

----.\- --*--:** ------

Final Report of Analysis 101 Shiloh Blvd

~. ENVIRONMENTAL . .......

Zion, ll 60099 Sample Matrix: so Lab I Sample I

Client ID Sample Date I Receipt Date

! Analysis Date Batch ID Ana!yte Method Result I cu CSU I

MDA ( Qualifier Report Units ID Type 18-04022-07 TRG B105100AFSWC088CV 03/07/18 08:55 4/5/2018 4/5/2018 18-04022 Actinium-228 EPA 901.1 Modified 3.54E-01 3.45E-01 3.45E-01 6.55E-01 . u rr;;r 18-04022-07 TRG . B105100AFSWC088CV 03/07/18 08:5~ 4/5/2018 4/5/2018 rn.04on SiTae,.108m EPA 901.1 Modified -3.87E-03 1.06E-01 1.06E-01 1.49E-01 u pC;tg

. .. .4 4'C.01 u ornr 18 04022 07 TRG B105100AFSWC088CV 03/07/18 08:55 415/2018 ' 415/2018

'"*"'°" _..

Barlum-133

, ,. I EPA901.1 Modified EPA901.1 Modified 7 <CC.OS 2.42E-01 8.96E 02 i

2.43E-01 8.97E-02 2.37E 01 2.32E-01 u oCi/o 18-04022-07 TRG  ! B105100AFSWC088CV 03/07/18 08:55 . 4/5/2018 4/5/2018 18--04022

• ... TRG B105100AFSWC088CV 03/07/18 08:55 4/5/2018 4/5/2018 1R.040?? Bismuth-214 EPA 901.1 Modified  ! 7.03E 01 3.23E 01  : 3.25E-01 .

4.34E-01 ,r;;*

,. .. TRC B105100AFSWC088CV 03/07/18 08:55 4/5/2018 4/5/2018 1804022 i Cobalt-60 EPA 901.1 ModTfiP.d 34oc.02 1.04E*01  ! 1.04E 01  ; 1.51E-01 ' u  ;;.

18 04022-07 TRG B1051 OOAFSWC088CV 4/5/2018 4/5/2018 18-04022 - Cesium 134 EPA 901.1 Modified -4.04E-01 218E*01 2.19E-01 . 1.65E-01 u Tr.;,r 18 04022 07 TRG B105100AFSWC088CV 03/07/18 nP.-i;t:; 4/5/2018 4/5/2018 C 18-04022 Cesium 137 EPA 901.1 Modffied 1.95E-01 1.15E-01 1.16E 01 2.24E 01 u rrnr 18 04022 07 V 03/07/18 08:55 4/5/2018 4/5/2018 : 18-04022 EPA 901.1 Modified -3.19E-01 4.14E-01 4.15E 01

. "'"*°' u """" ...

.,, "" B105100AFSWC088CV 03/07/18 08:55 4/5/2018 4/5/2018 18*04022 EPA901.1 Modffied 1.10E*01 "76F.01 2.76E 01 1.70E-01 . u ,,r;;,

TRG

.. -* TRG B105100AFSWC088CV 03/07/18 08:55 4/5/2018 4/5/2018 I 1R-040?? EPA901.1 Modified .152E,01 1 esc.01 . 1.87E-01 2.85E 01 u """"

18-04022-07 TRG B105100AFSWC088CV 03/07/18 08:55 4/5/2018 4/5/2018 : 18-04022 Holmium-166m EPA 901.1 Modified *1.21E*02 1.67E-01 1.68E-01 1.39E-01 u °' ° 18 04022-07 TRG 03/07/18 08:55 [ 4/5/2018 4/5/2018 i 18-04022 Iodine 129 EPA901.1 Modified 414E*02 1.43E-01 1.43E01 1.81E01 u pCitg_

18-04022-07 TRG TRG 81051 OOAFSWC088CV 8105100AFSWC088CV 03/07/18 08:55 03/07-/18 08:55

'. 4/5/2018

! 4/5/2018 41512018 . 18-04022 41512018

• 18-04022 Potassium-40 EPA 901.1 Modified EPA 901.1 Modified 3.03E-02 1.98E+OO  ;

9.55E-02 -"]

2.02E+OO 9.55E 02 _

1.90E+OO 1.62E 01 - ' u

,,r;;,,

18 04022 07 TRG 81051 OOAFSWC088CV 03/07/18 08:55 j 4/5/2018 _ 4/5/2018 18.04022 -* EPA 901.1 Modified *1.00E*01 112e.01  ! 1.12E-01 1.15E 01  ! u rrnr 03/07/18 08:55 4/5/2018 4/512018 18-040" Lead.210 EPA901.1 Modified 1.81E+OO 1.86E+OO 1.86E+OO *:* 2.64E+OO ii pCi/g 18-04022-07 TRG B105100AFSWC088CV 18-04022-07 18 04022 07 18-04022-07 18-04022-07 TRG THC TRG TRG B105100AFSWC088CV

- -*-~.,.--- ., **----------

B105100AFSWC088CV B105100AFSWC088CV 03/07/18 08:55 03107/18 08:55 03/07118 08:55 03107118 08;55 4/5/2018 4/5/2018 4/5/2018 41512018 4/5/2018 4/5/2018 41512018 I

18-04022 18-04022 4/5/2018 ' 18-04022 18-04022 Lead-212 Lead*214 Promethium 145 Radium 226 EPA901.1 Modlfied EPA 901.1 Modlfied EPA901.1 Modffied EPA901.1 Modified

~t~=

5.00E-01 1.80E-01 1.82E-01

'40E,01 2.07E-01 3.25E-01 6.54E-01 3.60E-01 2.53E-01 4.34E-01 u

u pCilg pCi/g rr;;r TRG B105100AFSWC088CV 03107118 osss 4151?018 , 4/5/2018 18-04022

"""'" EPA901.1 Modified -3.02E-02 2.76E 01 2.76E-01

' ,,oc:01 lJ """"

TRG THC B105100AFSWC088CV B105100AFSWC088CV 03/07/18 08:55 03/07/18 08:55 4/5/2018 4/5/2018 * ,1sne1, 4/5/2018 18*04022 ,

18,04022 Thorium-234 EPA901.1 Modified EPA901.1 Modified 2.09E+OO 4.12E-01 2.31E+OO 3.61E 01 2.32E+OO 3.62E-01

_ 3.87E+OO

' 6.33E-01 u

u

,cu,

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18-04022-07 TRG B105100AFSWC088CV 03/07/18 08:55 4/5/2018 4/5/2018 18-04022 Uranium-235 EPA 901.1 Modified 1.68E-01 1.06E+OO 1.06E+OO 7.58E-01 u . pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Ouplicate Original;U=Non-detect

( EBERLINE ----~*-*--------ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[186]

865/481-0683 FAX 865/483-4621

Printed: 4/30/2018 3:20 PM Page 10 of22 Report To* Work Order Details:

Patricia Giza 18-04022 Eberline Analytical ' Zion Solutions, LLC

' Purchase Order.: :

SDG:

677118------- ..... --------- ---------

~ ---------------*-****-***-*-*-***----------- *--- ......... -*** - - ... -- ---****----- ---------*--****

Final Report of Analysis 101 Shiloh Blvd

--- -----------*---- _______ ._,_ -: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so L,b Sample Client Sample Receipt ' Analysis ' Batch Analyte Method i Result cu CSU MDA

Quahfier

'i Report ID 18-04022-08 Type TRG ID B105100AFSWC101CV Date 03/07/18 07:25 Date 4/5/2018 Date 4/5/2018

! ID 18-04022 . Actinium-228 EPA901.1 Modified I 3.17E--01 5.17E-01 5.17E-01

': 9.31E-01 : u  :

Units or.Uo 18-04022-08 TRG B105100AFSWC101CV 03/07/18 07:25 4/5/2018 : 4/5/2018 18-04022 Si1ver-108m EPA901.1 Modified 5.57E-02 1.29E-01 1.29E-01 ' 1.64E-01 u pCi/o 18-04022-08 TRG 8105100AFSWC101CV 03107/18 07:25 4/5/2018 4/5/2018 18-04022 Americium-241 EPA 901.1 Modified -2.56E-01 1.69E-01 1.70E-01 2.11E-01 u PCi/o 18-04022-08 TRG B105100AFSWC101CV 03107/18 07:25 4/5/2018 4/5/2018 18-04022 Barium-133 EPA901.1 Modified -2.76E-02 6.89E-02  : 6.89E-02 2.36E-01 u oCi/o

• o 00 TRG B105100AFSWC101CV 03/07/18 07:25 4/5/2018 i 4/5/2018 ; 18-04022 Bismuth 214 EPA901.1 Modified 1.72E-02 1.14E 01 1.14E-01 5.46E 01 u orno 1----

• o Oo TRG 8105100AFSWC101CV 03/07/18 07:25 4/5/2018 4/5/2018 , 18-04022 Cob,lt-60 EPA 901.1 Modified -3.10E-02 1.63E-01 1.63E-01 I 2.16E-01  ; u I ,mo

,_ 00 TRG '

B105100AFSWC101CV 03/07/18 07:25 4/5/2018 4/5/2018 , 18-04022 *- EPA901.1 Modified 3.95E-02 1.28E-01 1.28E-01  ! 2.26E-01 I u oCi/o 18-04022-08 TRG 8105100AFSWC101CV 03/07/18 07:25  : 4/5/2018 4/5/2018 18-04022 Cesium-137 EPA 901.1 Modified 5.87E-01 2.08E-01 2_10E-01 2_59E-01 ' oCi/o 18-04022-08 TRG B105100AFSWC101CV 03/07/18 07:25 4/5/2018 4/5/2018 18-04022 EPA901.1 Modified -7.28E-02 3.53E-01 3.53E-01 3.25E-01 u oC.ilo 18-04022-08 , TRG B105100AFSWC101CV 03/07/18 07:25 4/5/2018 4/5/2018 18-04022 t::1-'A~(Jl.1 MorllTIPrl -0 SAF-0? ><.23E-01 3.23E 01 1.69E 01 u oC.ilo 18-04022-08  ! TRG

...L B105100AFSWC101CV 03/07/18 07:25 ,, 4/5/2018 4/5/2018 C

18-04022 EPA901.1 Modified 1.69E 02 1.82E-01 1.82E-01  :

2.57E 01 u

' pCi/q 18-04022-08 TRG  : B105100AFSWC101CV 03/07/18 07:25 4/512018 4/5/2018 18-04022 Holmium-166m EPA901.1 Modified 8.76E-02 2.28E-01 2.28E-01 1.35E-01 : u I ,cv, 18-04022--08 TRG I B105100AFSWC101CV 03/07/1807:25 4/5/2018 4/5/2018 04022 lodlne-129 EPA901.1 Modified 3.82E-02 6.36E-02 6.37E-02  : 9.92E-02 ' u ' ,cv, 18-04022-08 TRG B105100AFSWC101CV 03/07/1807:25 4/5/2018 4/5/2018 1R-040"

~

-- EPA901.1 Modified 7.71E+OO 2.44E+OO 247E+OO 2.57E+OO ' I oCi/o 18-04022-08 TRG 8105100AFSWC101CV 03/07/18 07:25 4/5/2018 4/5/2018 18-04022 - EPA901.1 Modified -356F-O? 143E-01 1.43E-01 . 2.01E 01 I u  : oCi/o 18-04022-08 TRG 8105100AFSWC101CV 03/07/18 07:25 4/5/2018 ! 4/5/2018 18-04022 Niobium-94 EPA901.1 Modified -8.56E-03 1.31E-01 1.31E-01 I 1.92E-01 ' u  : pCi/g

• o , 00 4/5/2018 4/!l/LUlti j 1ti-U4U£L Lead 210 EPA901.1 Modified 1 44F+OO 118E+OO 1.19E+OO 1.91E+OO

• u --- oCi/o -

!KU B105100AFSWC 101 CV 03/07/18 07:25 i

,o 00 TRG B105100AFSWC101CV 03/07/1807:25 4/5/2018 4/5/2018  ! 18 04022 Lead-212 EPA901.1 Modified 3 <'E-01 1.84E-01 1.85E 01

3.09E 01 I u --***' or.ilo Lead-214 4.70E-01 3.11E-01 3.12E-01 4.?SE-01 u PCi/Q 18-04022-08 M

TRC TRG 8105100AFSWC101CV B105100AFSWC101CV 03107/18 07:25 03/07118 07:25 4/5/2018 4/5/2018 4/5/2018 ; 18-04022 4/5/2018 I 18-04022 Promethium 145 EPA 901.1 Modified EPA901.1 Modified -1.16E-01 U5E-01 1.15E-01 I 1.56E-01

u

' oCi/o

• o 00 TRG  :' B105100AFSWC101CV 03/07/18 U/:L!J 4/5/2018 4/5/2018  ! 18 04022 Radium-226 EPA 901.1 Morlififirl 1 72F-02 1.14E-01 1.14E 01  : 5.46E 01 . u oCi/o

,o oo TRG  : B105100AFSWC101CV 03107/18 U/:£0 4/5/2018 4/5/2018 I 18-04022 EPA 901.1 Modified -SOOF-0? 3.74E-01 3.74E-01 5.25E-01 u oCi/o

-- 00 TRG I B105100AFSWC101CV 03/07/18 07:25 4/5/2018 4/5/2018 - 18 04022 Tl EPA901.1 Modified 1.95E+OO 146E+OO 1.46E+OO 2.35E+OO u pCi/o 18-04022-08 TRG i B105100AFSWC101CV 03/07/18 07:25 4/5/2018 4/5/2018 18 04022 EPA 901.1 Modified 2.79E-01 4.88E-01 4.68E 01 7.13E 01 . u PCi/q 18-04022-08 TRG  : B105100AFSWC101CV 03/07/18 07:25

'i 4/5/2018 4/5/2018 18-04022 Uranium-235 EPA 901.1 Modified 4.10E-01 1.23E+OO 1.23E+OO 6.96E-01 u  :' pCi/g CU=Counting Uncertainty;CS~ombined Standard Uncertainty (1-sigma);MOA=M inimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Du plicate;TRG=Normal Sample; DO=Ouplicate Original; U=Non-detect

( r.;;J

~

EBERLINE ------------- ANALYTICAL

-- EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[187]

865/481-0683 FAX 865/483-4621

Printed: 4/30/2018 3:20 PM Page 11 of 22 Report To: Work Order Details:

Patricia Giza SDG: 18-04022 Eberline Analytical ,_

Zion Solutions, LLC_

, nmor, 677118 Final Report of Analysis 101 Shiloh Blvd -**- Analysis Category:) __ ENVIRONMENTAL Zion, IL 60099 Sample Matrix: ' so i I 'i Report I

Lab Client Sample Receipt ; Analysis Batch I Sample Analyte Method Result cu CSU MDA Qualifier i Units ID Type ID Date Date , Date ID 1 '

18-04022-09 TRG B105100AFSWC115CV 03/07/1815:30 4/5/2018 4/5/2018 18-04022 Actinium-228 EPA901.1 Modtfied 9.95E-01 3.30E-01 I 3.34E-01 '

4.96E-01  ; oCT/o 18-04022-09 TRG '

- B105100AFSWC115CV 03/07/1815:30 41512018 4/5/2018 18-04022 Silver-108m EPA 901.1 Modified -6.95E-02 1.24E-01 ' 1.24E-01 1.47E-01 - u """"

' 4/5/2018° I -1.<Ln,ln?? Americium-241 EPA 901.1 Modified -3.69E-01 2.67E 01 1 2.68E-01 2.82E-01 u or;;"

'"" TRG B105100AFSWC115CV 03107/18 1,;-~n 41512018 '

2.82E 01 i u

'"" "" TRG B105100AFSWC115CV 03107/18 15:30 4/5/2018 : 4/512018 18-04022 Barium 133 EPA901.1 Modified -1.83E-01 1.51E-01

' 1.51E 01 '

erne 18 04022 09 TRG 8105100AFSWC115CV (l'>./(17/18 1'i-'>.(l

"'"" ' 4/5/2018  ! 18-04022 Bismuth-214 EPA901.1 Modified 6.40E-01 2.66E 01  ; 2.68E-01 4.95E--01 er;,"

' 03/0711815,30 41512018 ! 4/5/2018 18-04022 Cobalt 60 EPA 901.1 Modified 1.71E-01 1.02E-01 I 1.02E 01 1_85E-01 u or.,/o TRG B105100AFSWC115CV

-S fiSF-OS 7.41F-07  ; 7.41E-02

' 1.88E 01 u oC_;/o TRC

' B105100AFSWC115CV 03/07/181.S-SO 03/07118 1,-,0

""'°  !

4/5/2018 . 18 04022 4/5/2018 I 18-04022 Cesium-134 EPA901.1 Modlfied EPA901.1 Modified 1 '7F+OO 4.61E-01 4.65E 01 __ 6.85E-01 - orno 18-04022-09 TRG

' B105100AFSWC115CV Cesium 137 1 3.93E-01 i u or;,"

18-04022-09 TRG B105100AFSWC115CV 03107/18 "" ""'"18 - 4/5/2018 C 18-04022 152 EPA901.1 Modffied -1.00E+OO 5.60E-01 S.62E-01

'" "" TRC B105100AFSWC115CV 03107/18 15:30 4/5/2018 '. 4/5/2018 ,;";";; - 154 EPA901.1 Modffied -1.69E-01 3.33E 01 3.33E-01 i

1.90E-01

'i u erUe 4/5/2018 _ 41512018 : 18-04022 Europium 155 EPA 901.1 Modified 9.41E-02 1.72E-01 1.72E 01 3.34E-01 u pCi/g

" TRG B105100AFSWC115CV 03/07/1815:30

,o TRG B105100AFSWC115CV 03/07/18 1!'i"'.'s0 ,1/'i/?01R : 4/5/2018 04022 ' Holmium 166m EPA901.1 Modified 5.21E-02 2.06E-01 2.06E 01

' 1.68E-01 i

u or;;"

1.64E-01 2.41E 01 u orno 18-04022--09 TRG B105100AFSWC115CV 03/07/18 1'i*'>.n

"'"" ' 4/5/2018 I 18 04022 1R~ri;;n;;

lodine-129 EPA901.1 Modified 2.07E-01 1.63E 01

, ,oc+oo 2.55E+OO "T 2.71E+OO orno 18-04022-09 TRG B105100AFSWC115CV 03/07/18 1'i*'>.(l

""'" ' 41s12018 , Potassium-40 EPA901.1 Modified 9_81E+OO 18 04022 09 TRG B105100AFSWC115CV 03/07118 ""

,;";; I 4/5/2018

• 18-04022 Manganese 54 EPA901.1 Modified 1.52E-01 1_26E-01 1.26E 01 1.19E-01

' 1_36E-01 1.58E-01 u

u "r;;"

erUe 18-04022-09 TRG B105100AFSWC115CV 03/07/181530 41517018 I 4/5/2018 i 18-04022 Niobium-94 EPA901.1 Modified -7.96E-02 l 1.19E-01 -

.~-- u

" TRG 8105100AFSWC115CV 03/07/1815,30 ,</,c/*)(HQ \

4/5/2018 C 18 04022 Lead-210 EPA901.1 Modtfied 1.71E+OO 2.19E+OO 2.19E+OO '

3.06E+OO '"""

" TRG ' 8105100AFSWC115CV 03/07/1815:30  : 4/'i/?018 : 4/5/2018 1R-O,C7? Lead-212 EPA901.1 Modifif!d 3 92F-01 1 '7F-01 1.93E 01 5.66E-01 u oC1'o

- q 70F-01 S O.F-01 3.08E-01 4.70E 01 oC1'o

'" M TRG B105100AFSWC115CV 03107/1815:30 4/5/201P. ' ,1/'i/2018 "-"'"" Lead-214 EPA 901.1 Modified i 18-04022-09 TRG B105100AFSWC115CV 03/07/1815:30 -*-4/5i2018 I 4/5/2018 18-04022 Promethium-145 EPA901.1 Modified 1_,,c_n, 2.43E 01 2.43E-01  ! 3.19E 01 u oCUo

--*~-- --,,

'" "" TRG ' B105100AFSWC115CV 03/07/1815:30 41512018 i 41512018 I 1_~ 04022 " EPA 901.1 Modified 6.40E 01 2.66E-01 2.68E 01 4.95E-01 or;,"

" '" TRG B105100AFSWC115CV 03/07/1815:30 A/,C/'J(\1fl : 4/5/2018 l 1" "'"°" EPA 901.1 Modified 2.38E 01 3.16E-01 3.16E 01 5_37E-01 u ,r;,"

18 04022--09 TRG B105100AFSWC115CV 03/07/18 15:30 415/2018 4/5/2018 i 18.~'°" "

"", EPA901.1 Modified 1.38E+OO ,.35E+OO 2.35E+OO ', s 1'F+OO u oCi/o 18 04022-09 1KG B105100AFSWC115CV 03/07/18 15:30 4/5/2018 4/5/2018 18-04022 Thallium-206 EPA901.1 Modified 3.0BE-01 HSF-01 2.35E-01 ' 5.0SE-01 u oCi/o 18 04022 09 TRG B105100AFSWC115CV """" 1,-,0 4/5/2018 C 4/5/2018 : 18-04022 Uranium-235 EPA901.1 Modtfied 5.57E-01 , 7'F+M 1.23E+OO

• 1 9.07E 01 u pCl/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Ouplicate Original;U=Non-detect

( ~

EBERLINE ANALYT1CA"L EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[188]

865/481-0683 FAX 865/ 483-4621

Printed: 4/30/2018 3:20 PM Page 12 of 22 Reporl To: Work Order Details:

Patricia Giza SDG: 18-04022 Eberline Analytical **- Zion.Solutions, LLC .. . ------------

Purchase Order: 677118

. ------------*. '"--------*** - ------~ --- --- -------------------- ---*--*-------

Final Report of Analysis 101 Shiloh i.----.--------------

Blvd Analysis Category:' __ ENVIRONMENTAL

---

~ ---- ------ ----------- ,, ...... *....

Zion, IL 60099 Sample Matrix: so Lab Sample i Client Sample I Receipt '. Analysis Batch Analyte Method i Result cu CSU MDA j Qualifier ! Report ID Type ID Date I Date Date  : ID I Units

... TRG 8105100AFSWC116CV 03/07/18 08:40 4/5/2018 e 4/5/2018 ; 18-04022 Actinium 228 EPA901.1 Modified 5.97E-01 4.37E-01 4.38E 01 9.24E--01 u  : oh:o

.," TRG 8105100AFSWC116CV 03/07/18 08:40 4/5/2018 4/5/2018 18-04022 Silver 108m EPA901.1 Modified 6.19E-02 1.38E-01 1.38E 01 1.45E-01 u orHo

.. "" 03/07/18 08:40 4/5/2018 : 4/5/2018  : 18 04022 Americium-241 EPA901.1 Modified .J,SE.01 2.23E 01 2.23E-01 i 2.75E-01 I u oC;Jo 18*04022,10

'" TRG TRG 8105100AFSWC116CV 8105100AFSWC116CV 03/07/18 08:40 4/5/2018 4/5/2018  ! 18-04022 Barium-133 EPA901.1 Modified 2.89E-02 7.16E-02 7.16E-02  : 2.00E-01 u

' "°""

,o 3.97E-01 3.98E-01 6.75E*01

u orHo 1KG B105100AFSWC116CV 03/07/1808:40 4/5/2018 4/5/2018 04022 Bismuth 214 EPA 901.1 Modified 6.73E 01 I

" ,o:o,on I .rn.

'" '" TRG B105100AFSWC116CV 03/07/18 08:40 4/5/2018 4/5/2018 Cobalt-60 EPA 901.1 Modified 1.37E-01 1.32E 01 ' 1.32E 01 2.33E-01  : u '

.rn.

18-04022-10 TRG  : 8105100AFSWC116CV 03/07/18 mi-,m 03/07/18 08:40 4/5/2018 : 4/5/2018 4/5/2018 4/5/2018 18-04022 Cesium 134 Cesium 137 EPA 901.1 Modified EPA 901.1 Modlfied 2.63E-02 5.50E--01 7.32E-02 2.06E-01

' 7.32E 02 2.08E-01 I 1.81E-01 2.77E 01 u

.r,,.

18-04022-10 TRG i B105100AFSWC116CV 4.33E-01 4.33E-01 3.87E 01 u oC.;Je 18-04022-10 r -------------,, ..,_ TRG B105100AFSWC116CV 03/07/18 08:40 4/5/2018 T 4/5/2018 18-04022 "r. EPA901.1 Modified 2.07E 03 i u or;:o 18-04022-10 TRG 8105100AFSWC116CV 03/07/18 08:40 4/5/2018 4/5/2018 ;

4/5/2018 4/5/2018

'~""""

, 18-04022 r.

EPA901.1 Modified EPA901.1 Modified

-4.79E-02 1.70E-01 3.24E 01 1.73E01 3.24E-01 1.73E 01

1.96E-01 4.13E-01 u or""

18-04022-10 TRG B105100AFSWC116CV 03/07/18 08:40 '

18-04022-10 TRG 8105100AFSWC116CV 03/07/18 08:40 ' 4/5/2018 4/5/2018 18-04022 Holmiom* 16'm EPA 901.1 Modified -6.13E-03 1.98E 01 1.98E 01 I 1.63E-01 u .r::o 18-04022-10 TRG 8105100AFSWC116CV 03/07/18 08:40 41512018 4/5/2018

-;; ;,;;; lodine-129 EPA901.1 Modified 7.98E-02 1.07E*01 1.07E 01 I 179F.01 u .r,,.

EPA 901.1 Modified 1.15E+01 ,.63E+OO 2.70E+OO 2.07E+OO 18-04022-10

---"**~---

TRG 8105100AFSWC116CV 03/07/18 08:40 415"018 4/5/2018 18-04022 , Potassium-40 u

18-04022-10 TRG B105100AFSWC116CV B105100AFSWC116CV 03/07/18 08:40 03/07/18 08:40 41512018 4/5/2018 4/5/2018 4/5/2018 18-04022 I 18 04022 EPA901.1 Modified EPA901.1 Modified 6.90E-02

-8.42E 02 9.28E 02 1.30E 01 9.28E 02 1.30E-01 1.68E-01 1.76E 01 u orno 18-04022-10 TRG ' '

03/07/18 n1<-,1n 4/5/2018 4/5/2018 ,~r,rn Lead-210 EPA901.1 Modified 2.18E+OO 2.45E+OO 2.46E+OO  : 4.09E+OO u orHo 18-04022-10 TRG 0

" ' oC::o EffJ~@ TRG 0 V 03/07/18 08:40 4/5/2018 4/5/2018 i 18-04022 Lead-212 EPA901.1 Modtfied 7.03E 01 2.10E-01 2.13E-01 '

3.55E 01 100AFSWC116CV 03/07/18"" 4/5/~?18 4/5/2018 18-04022 Lead 214 EPA 901.1 Modified 5.59E-01 2.84E-01 2.86E 01  : 5.27E-01 pCi/g 18 04022-10 TRG B105100AFSWC116CV 03/07/18 e,.,o moo,o 4/5/2018 18 04022 j Promethium-145 EPA901.1 Modified 4.46E 02 1.56E*01 1.56E-01 2.54E 01 u .r,,.

~. .

18-04022-10 TRC, 16CV 03/07/18 08:40 415"018 ' 4/5/2018 18 04022 EPA901.1 Modified 6.73E 01 S97E.01 3.98E 01 I 6.75E-01 u oc;fo

--*- -1.35E-01 2.35E--01 2.35E-01  : 3.74E-01 u orno 03/07/18 01<*40 18-04022 EPA 901.1 Modified 18-04022 10 TRG

. B105100AFSWC116CV rrr B105100AFSWC116CV r

--- - -- r 03/07/18 01<*40

""'"18 4/5/2018 4/5/2018

-*;;:;,;;; EPA901.1 Modlfied 2.19E+OO 2.28E+OO 2.28E+OO . i. 3.24E+OO  ; u ' oCi/o 18----04022 10 TRG T""""'

18 04022-10 TRG B105100AFSWC116CV 03/07/18 08:40 4/5/2018 4/5/2018 11'04022 EPA901.1 Modified 5.93E 01 2.93E*01 2.94E*O* 1 ,ioe:01 . u .r::.

18 04022-10 TRG 8105100AFSWC116CV 03/07/18 08:40 4/5/2018 4/5/2018 18--04022 Uranium-235 EPA901.1 Modtfied '4.01E*02 1 4RF+nn 1 ,<Q,:: ...nn I n A<>!:: ')1 '. u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

( ~

EBERLINE

....... ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[189]

865/481-0683 FAX 865/483-4621

• , '  ;, _',aa.~.>a*,;,*.

Printed: 4/30/2018 3:20 PM Page 13 of 22 Report To: Work Order Details*

Patricia Giza 18-04022 Eberline Analytical ,_

Zion ... LLC

---

1*------"*"""-******* --

SDG:

Order: 677118 Final Report of Analysis I 101 Shiloh Blvd Analysis Category: !_ ENVIRONMENTAL -----

Zion IL 60099 Sample Matrix: - so i  :

Lab I Sample Client Sample I Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID  : -

Units 18-04022-11 TRG 8105100AFSWC150CV . ,,,_ 02/21 /18 08:40 4/5/2018 : 4/5/2018 18-04022

• Actinium-228 EPA901.1 Modified 2.87E-01 4.91E-01 - 4.91E-01 8.56E-01 u ' pCilc 18 04022-11 TRG 8105100AFSWC150CV 02/21/18 08:40 4/5/2018 ' 4/5/2018 18-04022 Si1ver-108m EPA901.1 Modified 4.81E--02 7.34E-02 7.34E-02 I 1.84E-01 u ,cu,

-- TRC i 8105100AFSWC150CV 02/21/18 08:4C 4/5/2018 415/201' 18-0402' EPA901.1 Modified 2.42E-01 2.13E 01 I

2.14E 01 3.19E-01 u  :

,Ci/c

.ra,,

1'-040?? TRG B105100AFSWC150CV 02/21/18 08:40 4/5/2018 4/5/2018 1'-040?; Rari"m-133 EPA901.1 Modified -1.89E-02 1.09E-01 1.09E-01 2.21E 01 u 4/5/2018 : 4/S/?01R rn.O,O?? - 7.59E-01 2.72E 01 2.74E 01 :

4.82E 01 pCiio

<e

'1, IKC B105100AFSWC150CV 02/21/18 08:40 EPA 901.1 Modified  :

-- TRG B105100AFSWC150CV 02/21/18 08:40 4/5/2018 4/5/2018 "-°'° Cobalt 60 EPA 901.1 Modified 2.02E 01 1.19E-01  : 1.19E-01 2.48E-01 u  : :r:::

-- TRG  : B105100AFSWC150CV 02/21/18 08:40 4/5/2018 4/5/2018 18 04022 Cesium 134 EPA901.1 Modified 1.71E 01 *1 1.20E-01 1.20E-01 1.58E-01 u  : -r"-

-- TRG - B105100AFSWC150CV 02/21/18 08:40 4/5/2018 4/5/20"18 18-04022 Cesium 137 EPA 901.1 Modified 6.46E+OO 7.81E 01 8.49E-01 2.64E-01

- .r.,,

TRG  : B105100AFSWC150CV 02/21/18 08:40 4022 - EPA901.1 Modified 1.33E-01 5.34E-01 5.34E 01 4.81E 01 u -

pCi/g

<e

'1, TRG  : B105100AFSWC150CV 02/21/18 08:40 4/5/2018 4/5/2018 18-04022 C.

- '" EPA901.1 Modified -1.34E-01 3.66E 01 3.66E 01 2.52E-01 u i pCi/g

• • ---'"*-~*-***

I 18-04022-11 TRG I B105100AFSWC150CV 4/5/2018 4/5/2018 '"~'°" C. EPA901.1 Modified 2.63E 01 2.60E 01 2.60E-01 3.72E-01 u -r::-

4/5/2018 : EPA901.1 Modified -6.54E-02 2_36E-01 2.36E 01 1.79E 01 u 18---04022 11 18-04022-11 TRG TRG

B105100AFSWC150CV B105100AFSWC150CV 02/21/18 08:40 4/5/2018 4/5/2018 4/5/2018 1RJ\dn??

'"-'""" lodine--129 EPA901.1 Modified -3.00E-01 2.31E 01 2.31E 01 2.23E-01 u '.~['.

18-04022-11 TRG 'I B105100AFSWC150CV 02/21/1808:40 4/5/2018 415/2018  ! 18-04022 Potasslum-40 EPA901.1 Modified 5.59E+OO 2.13E+OO 2.15E+OO 2.65E+OO  :

I

-r"-

18 0402211 TRG  : B105100AFSWC150CV 02/21/18 08:40 4/5/2018 4/5/2018 18-040?? -- EPA901.1 Modified 5.43E-03 1.37E 01 1.37E-01 2,;c_c, I u '

ca,,

18-04022-11 TRG 8105100AFSWC150CV 02/21/18 nFbin 4/5/2018 4/5/2018 '"-°'° Niobium-94 EPA 901.1 Modified -6.63E-02 1_54E-01 1.54E 01 , OOF-01 u *'"-

18-04022-11 IKC  : B105100AFSWC150CV 02/21/18 08:40 4/5/2018 . 4/5/2018 ,s_040,? Lead-210 EPA 901-1 Modified 2.97E+OO 1.53E+OO 1.54E+OO I 2_83E+OO u rn '"'

18-04022-11 TRC B105100AFSWC150CV 02/21/18 08:40 41512018 4/5/2018

• HU1Ml?? Lead 212 EPA901_1 Modified I 5.44E 01 2.37E-01 2.39E-01 4_36E-01 i

,c,1, ------

18-D4022-11 TRG i 8105100AFSWC150CV 02/21/18 08:40 4/5/2018 4/5/2018 18-04022 Lead-214 EPA 901.1 Modtfied 4.70E-01 3.27E 01 I 3.28E-01 5.99E-01 I u -

,c,1, 18-04022-11

- --1---

TRG  : B105100AFSWC150CV 02/21/18 08:40 4/5/2018 4/5/2018 18-04022

-- EPA901.1 Modified -4.33E 02  :;o,e.01 2.09E-01 3_06E--01 u i -r::-

18-040?? EPA901.1 Modtfied 7.59E-01 . 2.72E 01 2.74E 01 4.82E-01 .ra,,

18-04022-11 TRG 8105100AFSWC150CV 02/21/18 08:40 4/5/2018 4/5/2018 18-04022-11 TRG i - 02/21/18 f\R*,ln 4/5/2018 4/5/2018 Hc040,? EPA901.1 Modified 2.48E-02 i 2_36E-01 2.36E 01  :

5.83E 01 -

u :Clio 18 04022 11

-- TRG 8105100AFSWC150CV 02/21/18 mi-.1! 4/5/2018 4/5/2018 , HW,1f\?? I T EPA901.1 Modified 2.36E+OO , 2.25E+OO 2_25E+OO 3.29E+OO u -

18-04022-11 TRG B105100AFSWC150CV 02/21/18 08:40 4/5/2018 415/2018 : 18-04022 Thallium-208 EPA901.1 Modified 3.65E-01  ! 3.27E 01 3.27E-01  ! 6.42E-01 u :r::o 18-04022 11 TRG 8105100AFSWC150CV 02/21/18 08:40  ! 4/5/2018 4/5/2018 18-04022  ! Uranium-235 EPA901.1 Modified -8.91E-01 1.93E+OO 1.93E+OO 9.58E-01 u pCi/g CU=Counting U ncertainty;CSU=Combined Standard Uncertainty ( 1-sigma ); MDA=Minimal Detected Activity; LCS=Laboratory Control Sample;M BL=Blank; DU P=Duplicate;TRG=Normal Sample;DO=Duplicate Orig in al; U=Non-detect

( ~

EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[190]

865/481-0683 FAX 865/ 483-4621

Printed: 4/30/2018 3:20 PM Page 14 of 22 Reporl To: Work Order Details:

Patricia Giza SDG: 18-04022 Eberline Analytical ' -*----

Zion.Solutions, LLC n

Order:'. 677118 Final Report of Analysis 101 Shiloh Blvd ENVIRONMENTAL

___ Ana_lysis _Category:_'. ---------- - -- - . -- *------------..------ ... ... --- ---*--*--"

Zion, IL 60099 Sample Matrix: . so Lab Sample i Client Sample 'i Receipt Analysis-*: Batch Analyte Method

! Result

! cu I CSU i

MDA

Qualifier i Report ID . Type ID Date  : Date Date ID Units 18-04022-12 '

18-04022-12 j TRG TRG B105100AFSWC151CV B105100AFSWC151CV 02/21/18 09:20 02/21/18 09:20 4/5/2018 4/5/2018 --,

4/5/2018 4/5/2018 18-04022 18--04022 Actiniurn-228 Si1ver-108m EPA 901.1 Modified EPA901.1 Modffied 9.59E 01

-4.81E-01 I 2.38E+OO 5.51E-01 2.38E+OO 5.52E-01 3.61E+OO 7.88E-01 u

u

"°""

orno 18-04022-12 ;

.*........... TRG B105100AFSWC151CV 0?1?1118 0920

.... "morn 4/5/2018 04022 Americium-241 EPA901.1 Modffied 1.89E+OO  ! 1.09E+OO 1.09E+OO 1.80E+OO .

~--- '-~;.::;*,~ '"--

pCi/g 18-04022-12 TRG B105100AFSWC151CV 02/21118 OS*?O M.S/?O,S 4/5/2018 04022 Barlum-133 EPA901.1 Modified -5.51E-01 1.86E+OO 1.86E+OO 1.62E+OO u 18-04022-12 TRG B105100AFSWC151CV ' 02121118 00?0 ,11i:;1?n1s : 4/5/2018 i 18--04022 "" EPA901.1 Modified 1.50E-01 1.67E+OO 1.67E+OO 1.96E+OO f u oCilo 8.73E-01 -

18--04022-12 i TRG B105100AFSWC151CV 02/21/18 MOO ""'"18 4/5/2018 e 18 04022 Cobalt-60 _____ ,, EPA 901.1 Modified 2.92E+01 1.94E+OO

' 2.45E+OO or.ilo 18-04022-12 TRG B105100AFSWC151CV 02/21/18 09:20 4/5/2018 4/5/2018 **:* 18-04022 Cesium-134 EPA 901.1 Modified -3.81E-01 8.29E-01 8.29E-01 1.05E+OO u """"

18-04022-12 TRG 8105100AFSWC151CV 02/21/18 09:20 4/5/2018 4/5/2018 -04022 Cesium-137 EPA 901.1 Modified 3.64E+02 . 3.74E+01 . 4.18E+01 2.15E+OO .

4.43E+OO 5.66E+OO 5.66E+OO 1.95E+OO u or>!o 18-04022 12 , TRG 8105100AFSWC151CV 02/21/18 M*?n

""'"" 4/5/2018 I 1R.11Afl??

'" EPA901.1 Modlfied

--i 18 04022-12 , TRG B105100AFSWC151CV 02/21/18 no-?n

""""" 4/5/2018 : **13:04022 EPA901.1 Modffied 4.03E 02 8.28E-01 8.28E 01 1.24E+OO u oCa!a 18-04022-12 :

---

TRG . B105100AFSWC151CV 02/21/18 no-?r

'"""" 4/5/2018 18-04022 - EPA901.1 Modffied 5.20E-02

-1 07E-01 8.47E-01 6.69E-01 8.47E 01 6.69E-01 i 1.76E+OO 1 SSF+OO u

u oCilo orno 18-04022-12 TRG B105100AFSWC151CV 02ri'1. t18 09:20 4/S/?018 4/5/2018 18-04022 : Holmium-166m EPA901.1 Modified 18-04022-12 TRG 81051OOAFSWC151 CV 02/21/18 09:20 4/5/2018 : 4/5/2018 , 18-04022 i lodine-129 EPA901.1 Modified -S.52E-01 1.35E+OO 1 SSF+OO 0 4.SF+OO u orno

?SOF+OC

• 7 14E+OO 18-04022-12 TRG B105100AFSWC151CV 02/21/18 09:20 18 04022

---

Potasslum-40 EPA 901.1 Modified 9.90E+OO 2.63E+OO 18-04022-12 TRG B105100AFSWC151CV 02/21/18 09:20 4/5/2018 4/5/2018 18-0 54 EPA 901.1 Modified 1.94E--01 6.15E-01 6.15E-01 ' 9.41E 01 u oCl/o 18-04022-12 TRG . 8105100AFSWC151CV 02/21/18 09:20 4/5/2018

""""" 18-04022 Niobium-94 EPA901.1 Modified -1.01,-01 1.79E 01 1.79E-01 8.11E 01 u oCilo 10:;,;:;; EPA901.1 Modlfied 3.34E+01 7.70E+OO . 7.89E+OO 2.15E+01 u i 18 04022 12 18-04022-12 TRG TRG 8105100AFSWC151CV B105100AFSWC151CV 02/21/18 09:20 02/21/18 09:20 4/5/2018 4/5/2018 4/5/2018 4/5/2018 =; Lead 210 Lead-212 EPA901.1 Modlfied I 1.66E+OO 1.32E+OO 1.32E+OO . 2.78E+OO u oCi/o 18-04022-12 TRG B105100AFSWC151CV 02/21/18 09:2fl l 4/5/2018 4/5/2018 18-04022 Lead-214 EPA901.1 Modffied 2.32E+OO 2.97E+OO 2.97E+OO 4.28E+OO u . """"

4/5/2018 4/5/2018 18-04022 Promethium 145 EPA901.1 Modffied -s. 1.07E+OO 1.08E+OO  ; O,F+OO u or>!o 18-04022-12 TRG B105100AFSWC151CV 02/21/18 09:20 18-04022-12 TRG 8105100AFSWC151CV 02/21/18 09:20 4/512018 4/5/2018 18-04022 " EPA 901.1 Modified 1.50E 01 1.67E+OO 1.67E+OO 1.96E+OO . u or>!a 4/5/2018 ; --1;;o1A;:;.:;.:; u oCila 18--04022-12 TRG B105100AFSWC151CV 02/21/18 09:20 02/21/18 09:20 4/5/2018 4/S/?018 4/5/2018 18-04022 Antimony 125 Thorium 234 EPA 901.1 Modified EPA901.1 Modified 2.97E+OO 3.04E-01 ,

5.04E+OO 2.58E+OO 5.05E+OO 2.58E+OO 6.73E+OO 1.50E+01 u

. oCila 18-04022 12 TRC B10510DAFSWC151CV 18-04022-12 TRG B105100AFSWC151CV 02/21/18 fl<:i-?fl 41512018 4/5/2018 1 1P.....nAfl?? Thallium-208 EPA 901.1 Modified 2.41E+OO , ?SOF+OO 2.61E+OO 1.20E+OO u . oCiio 18 04022-12 TRG B105100AFSWC151CV 02/21/18 no-?n 4/512018 : 415/2018 18-04022 Uranium-235 EPA901.1 Modified -1.21E+01 /  ; '1F+M 1 '7F+O; 7.20E+OO u  ! pCl/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=DupHcate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

( EBERLINE

~ '"............-.. ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE. TN 37830

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Printed: 4/30/2018 3:20 PM Page 15 of 22 Report To: Work Order Details:

Patricia Giza 18-04022 Eberline Analytical __ ,__

.. *-* Zion Solutions, LLC -----------*-*

SDG:i

, n,rle, 677118 Final Report of Analysis ------------ 101 Shiloh Blvd Onolv,i< ENVIRONMENTAL Zion, IL 60099 Sample Matrix: >:;()

Lab Sample Client Sample Receipt : Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 18-04022-13 TRG B105100AFSWC156CV 02/21/18 13:30 4/5/2018 4/5/2018 18-04022 Actlnium-228 EPA 901.1 Modified 7.06E-01 1.03E+OO 1.03E+OO 1.61E+OO

• u ,ma

., S,O.M u 18-04022-13 TRG B105100AFSWC156CV 02121/18 13:30 . 4/5/2018 4/5/2018 . 18-04022 Silver 108m EPA 901.1 Modffied 2.38E-01 2.38E 0~ 3.48E 01 18-04022-13 TRG B105100AFSWC156CV 02/21/18 13:30 4/512018 , 4/5/2018 18-04022 Arnericium-241 EPA 901.1 Modified 8.91E-01 5.19E 01 5.21E 01 8.50E 01 ""'-

18-04022-13 TRG i 8105100AFSWC156CV 0212111a 1::i*:1r 4/5/2018 4/5/2018 18-04022 Barium-133 EPA901.1 Modified 1.98E-01 7.31E-01 7.31E-01 7.91E-01 u or.;,o 18-04022-13 TRG ' 8105100AFSWC156CV 02/21/1813:30 4/5/2018 4/5/2018 18-04022 Bismuth 214 EPA 901.1 Modified i 4.13E-01 7.13E-01 7.13E-01 1.07E+OO u pl'""

1.09E+OO ---

'° * ,'° o TRG B105100AFSWC156CV 02/21/1813:30 4/5/2018 4/5/2018 I 18 04022 Cobalt-60 EPA 901.1 Modified , 1.26E+01 8.81E-01 5.12E-01

.,c TRG '

B1D5100AFSWC156CV 02/21/1813:30 4/5/2018 41512018 18-04022 Cesium 134 EPA 901.1 Modified i -1 ROF-01 ,,,0.01 2.26E 01 4.28E 01 , u 2.55E+02 ,.67E+01 2.98E+01 1.19E+OO 18--04022 13 TRG 8105100AFSWC156CV 02/21/1813:30 4/5/2018 41512018 ' 18--04022 Cesium-137 EPA901.1 Modified

,o - .s oso.o, 2.26E+OO ,.26E+OO 1.12E+OO u

' TRG 8105100AFSWC156CV 02/21/1813:30 4/5/2018 4/5/2018 18--04022 EPA901.1 Modified

'° '° TRG B105100AFSWC156CV 02/21/1813:30 4/5/2018 4/5/2018 I 18-04022 EPA901.1 Modified ,,,o.m 3.72E 01 3.72E-01 6.26E 01 u or""

18-04022-13 TRG

• B10510DAFSWC156CV 02/21/18 13:3C 41512018 41512018 18-04022 EPA901.1 Modified 1.38E-01 5.32E-01 5.32E-01 8.53E-01 u ""'"

02/21/18 13:3C 4/5/2018 ,S.0,077 Holmium-166m EPA 901.1 Modified 7.53E-02 3.50E-01 SSOF-01 4.98E-01 u 18-04022-13 TRG B105100AFSWC156CV I 4/5/2018 18-04022-13 TRG ' B1051DOAFSWC156CV 02/21/18 13:30 41512018 4/5/2018 rn.0,077 lodlne-129 EPA 901.1 Modftied -9.04E-01 9.89E-01 9.90E-01 1.22E+OO u ' pCi/g

'" *- TRG B1051DOAFSWC156CV 02/21/18 13:30  :

4/512018 4/5/2018 4/5/2018 18-04022 18-04022 Potassium-40 EPA901.1 Modrfied EPA 901.1 Modftied 5.71E+OO

-1.89E-02 2.29E+OO 2.52E 01 2.31E+OO 2.52E 01 3.10E+OO 3.77E 01 u

'" '° TRG i B105100AFSWC156CV 02/21/1813:30 4/5/2018 '"'"

• - '" TRG ' B105100AFSWC156CV 02/21/18 13:30  ; 4/5/2018 4/512018

• 18 04022 Niobium-94 EPA901.1 Modified 6.SOE 03 2.87E-01 2.87E-01 3.88E-01 u

,ma

-- " TRG .

B 1051 OOAFSWC 156CV 02/21/1813:30 41512018 4/5/2018 18-04022 lead 210 EPA 901.1 Modified 4.66E+OO o '1F+OO 5.42E+OO --T S.06E+OO u '"'"

<O TRG B105100AFSWC156CV 02/21/1813:30 41512018 , 4/5/2018 18-04022 Lead-212 EPA901.1 Modified * -1.83E-01 S R3F-01 5.83E-01

• 9.20E 01

• u '"'"

'° 13 TRG 8105100AFSWC156CV 02/21/1813:30 4/5/2018 4/5/2018 18.0,077 Lead-214 EPA901.1 Modified 1 06F+OO 1.17E+OO 1.17E+OO I 1.72E+OO u pCi/g

,o

"' !KC  ! 8105100AFSWC156CV 02121118 n,o 4/5/2018 4/5/2018 1$-04022 ,. .,, EPA901.1 Modified i 8.16E+OO 1.11E+OO 1.19E+OO J 1.35E+OO u prno 18--04022-13 TRG B105100AFSWC156CV fl'.11<!1/18 n*:*m 4/5/2018 4/5/2018 18-04022 Radium 226 EPA 901.1 Modified 4.13E-01 7.13E-01 7.13E 01  : 1.07E+OO - u or""

18-04022 13 TRG . B105100AFSWC156CV 021211181330 4/5/2018 4/5/2018

'"*"'°" EPA901.1 Modified -3.61E-01 7 MO+OO 2.01E+OO 2.90E+OO u "'"'"

18-04022-13 TRG

• B105100AFSWC156CV 021211181330 4/5/2018 4/5/2018 18-04022 T EPA901.1 Modified  ; 000+00

""";"" 5.01E+OO 7.72E+OO [ u ""'"

18-04022-13 TRG 8105100AFSWC156CV 02121/18 "'° 4/5/2018 4/5/2018 18-04022 Thallium-208 EPA 901.1 Modified ---6.98E-01 1.18E+OO 1.18E+OO 1.19E+OO u pCi/Q 18 04022-13 TRG B105100AFSWC156CV 02/21/18 13:30 4/512018 4/5/2018 18-04022 ' EPA901.1 Modffied -3.50E-01 5.11E+OO 5.11E+OO 2.67E+OO ; u pCl/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Origlnal;U=Non-detect

( ~

EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[192]

865/481-0683 FAX 865/483-4621

Printed: 4/30/2018 3:20 PM Page 16 of 22 Report To: Work Order Details:

Patricia Giza SOG:! 18-04022 Eberline Analytical 1-Zion Solutions, LLC

' Purchase nrrlPr 677118 Final Report of Analysis 101 Shiloh Blvd--- -------------*--"*-*-------**" ------------ ____'::.f!_f!!tsis ....

• ENVIRONMENTAL Zion, IL 60099 Sample MatnX

  '. so Lab ID I Sample Type i Client ID Sample Date Receipt ---: Analysis Date Date Batch ID i; Analyte Method i Result cu CSU MDA Qualifier I Report Units 18-04022-14 18 04022-14 TRG TRG  ;

B105100AFSV1/C162CV 8105100AFSV1/C162CV 02/15/18 15:50 02/15/18 1,;-,;n 4/5/2018 : 4/5/2018 , 18-04022 4/5/2018 , 4/5/2018 18-04022 Actinium-228 Silver 108m EPA901.1 Modified EPA901.1 Modified 8.03E-01

-3.07E-02 4.36E-01 1.43E-01  ;

4.38E-01 1.43E 01 '

9.41 E-01 2.10E-01 u

u *

.::ii-18-04022-14 TRG . 81051 OOAFSVVC162CV 02/15/18 1,;-,;n 4/512018 4/5/2018 I 18-04022 Americium 241 EPA901.1 Modified 4.83E-D2 1_59E-01 1.59E-01 3.25E-01 u '

pCt/g 18-04022-14 TRG  ; 81051 OOAFSVVC162CV 02/15/18 15:50 4/5/2018 4/5/2018 r -*;;;*;:;-;;:;~.; Barium-133 EPA901.1 Modified 6.17E-02 1.42E 01 1.42E-01 2.93E-01 i u

• rr_;,r 18-04022-14 TRG  : 8105100AFSV1/C162CV 02/15/181!'i*fi(l 4/5/2018 4/5/2018 '"-04on OH EPA 901.1 Modified 4.04E-01 3.70E 01 3.70E-01 6.00E 01 i u rr::r 18-04022-14 TRG  ; 8105100AFSV1/C162CV 02/15118 ,sso 4/5/2018 4/5/2018 18 04022 Cobalt-60 EPA 901.1 Modified 8.61E-02 1.74E 01 1.74E-01 3.02E 01 u ' """"

u 18-04022-14 TRG  ; B105100AFSV1/C162CV 02/15/1815,50 4/5/2018 . 415/2018

.,..  ;, "'""" Cesium-134 EPA901.1 Modified 4.38E O? 8.92E 02 8.92E-02 1.87E-01  ;

--- - 415/2018 18-04022 Cesium--137 EPA901.1 Modified 8.89E+OO 1.04E+OO 1.14E+OO I 4.00E-01 rr_:,o 18 04022 14 TRC TRG '

B105100AFSVVC 162CV 81051 OOAFS\11/C 162CV 02/151181S*SO 02/15118 ,.,so 4/5/2018 4/5/2018 4/5/2018 18-04022 ... 152 EPA901.1 Modlfied 1.90E 01 6_53E-01 6.53E 01 4.73E-01 I u

rC:,o

,o" ' fRG . 81051 OOAFSV1/C162CV 02/15118 ,s-so

""'° ' 4/5/2018 I 11LMnn 154 EPA 901.1 Modi~~-? ___ ,_ 4.28E 02 2.48E 01 2.48E-01 2.44E 01

' u ' pCUg

,o 0

' TRG  ; 8105100AFSV1/C162CV 02115/18 ,s-so  ;,;,;;," 4/5/2018 ; 18-04022 155 EPA901.1 Modified 4.94E 02 2.88E-01 2.88E 01 3.84E-01 I u i oCf/o

,o . TRG  ; 8105100AFSV1/C162CV 02/15/1815:50 4/512018 41512018 : **1,,-n::;;:;-;:; EPA 901.1 Modified 2.30E-02 2.28E 01 2.28E-01 i 1.97E--01 u or:,o

-;;;:;;:;;;,, 2.26E-01 2.27E-01 2.27E-01 . u 18-04022-14 TRC ' 8105100AFSVVC 162CV 02115/1815:50 4/5/2018 : 4/5/2018 lodine-129 EPA901.1 Modified -3.16E-01 I rr:,r 1R.n4(J")_2-14

'"" ' B105100AFSV1/C162CV 02115/18 15:50 18-04022 Potassium-40 EPA901.1 Modified fi MF+OO 1.91E+OO 1.94E+OO 1.81E+OO I '

B105100AFSV1/C162CV .,.,.02/15/1815:50 4/5/2018 I 4/5/2018 18 04022 EPA901.1 Modified _s,,c_o,

'""-°' 1.51E-01 '.20E-01 i u """"

'" ' TRG 8105100AFSVVC162CV 02/15/1815:50 4/5/2018 - 4/5/2018 ; 18-04022 Niobium-94 EPA901.1 Modified 3A5E 02 1.06E-01 1.06E 01 ' 1.60E-01  ; u rC:,o

,o TRG B105100AFSWC162CV 02/15/18 *;,;.;;;;*-  ;;;,;;;; T 4/5/2018 18-04022 Lead-210 2.83E+OO 2.84E+OO  : 4.74E+OO I u  : or:,o 18-04022 14 TRG 81051 OOPJCSV1/C162CV 02/15/1815:50 WOMO 4/5/2018 18-04022 Lead 212 Er EPA901.1 ~ ;i~tii~rOO Modified .44E-01 3.45E 01 I 5.63E-01 ' u "°""

18-04022-14 TRC B105100AFSV1/C162CV 02/15/1815:50 4/5/2018 _ 4/5/2018 <O " ' " " " ,_,ad-214 EPA901.1 Modified :l.?8F-01 3.87E 01 3_87E-01 . 6.42E 01  ; u I rr.;,r

,o 02/15/1815:50 4/5/2018 ,,_,,,,,,, EPA901.1 Modified < SSF-M 1.95E--01 1.95E-01 i 3.24E 01  : u rr_;,o

,o TRG '

B105100AFSV1/C162CV 02115/18 1_,;-_,;n

""""" 4/5/2018 ,,_,,,,,,-, EPA 901.1 Modified 4.04E-01 3.70E 01 3.70E-01 , s ooc_o, i u  ; ,co, TRG B105100AFSV1/C162CV

""'"" 4.23E-01 4.23E 01 7 o,c_o, u ,c,1,

'" TRG i 8105100AFSVVC162CV 02115/18 1,;.,;n 4/512018 415/2018 -"'"" EPA901.1 Modified 4.98E 02 I

-* ..'"' TRG i B105100AFSV1/C162CV 02/15118 15:50 4/5/2018 4/5/2018 1804022 . EPA901.1 Modified 7.34E-01 2.52E+OO 2.52E+OO 'T 3.36E+OO u rCilo

.. 4/5/2018 .,--~~-;:;;;:;:;::; 4.15E-01 4.15E 01  : 7.38E-01  : u oCilr

...--- TRC i 81051 OOAFSVVC162CV 02/15/18 15:50 4/5/2018 T EPA 901.1 Modified 2.09E 01

,o TRC B105100AFSV1/C162CV 02/15/18 15:50 4/5/2018 4/5/2018 1,,~,,,, EPA901.1 Modified 1.03E+OO 1.97E+OO 1.97E+OO  : 1.08E+OO i u pCi/g CU=Coonting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);M DA=M inimal Detected Activity; LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate;TRG=Normal Sample; DO=Duplicate Original; U=Non-detect

( ~

EBERLINE ANALYTICA.L EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[193]

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Printed: 4/30/2018 3:20 PM Page 17 of 22 Report To: Work Order Details*

Patricia Giza SDG i 18-04022 Eberline Analytical ', __ Zion Solutions, LLC ----- _

Purchase Order:

-- 677118

.... ------------- - - - - - - - - - - - - * * . **I*

Final Report of Analysis 101 Shiloh Blvd -- Analysis Category:

ENVIRONMENTAL Zion,* 11 ,:.nnQQ Sample Matrix: so Lab i Sample : Client Sample Receipt ! Analysis Batch Analyte Method Result cu 'i CSU MDA Qualifier Report Units ID i Type ID Date Date Date ID i I -

18-04022-15 : TRG B105100AFSWC163CV 02/15/18 13:50 i 4/5/2018 4/512018 18 04022 -- EPA 901.1 Modified  ! 7.71E-D1 5.65E 01 5.66E 01 - 8.98E-D1 u i """"

18 04022 15 ; TRG B105100AFSWC163CV 02/15/1813:50 415/2018 4/5/2018 18-04022 Silver 108m EPA 901.1 Modified 1.34E 02 1.86E-D1 1.86E-01 2.54E-01 u i "' ""

u 18-04022 15 TRG B105100AFSWC163CV 02/15/1813:50  ! 4/5/2018 4/5/2018 18-04022 1R-C"077 1

EPA901.1 Modified -1.65E 01 9.23E 02

'""-" 4.10E-01 u

18 04022 15 TRG B105100AFSWC163CV 02/15/18 1'.'\*"iO 4/512018 4/5/2018 EPA,_,_,,

901.1

__ ., Modified

~

6.64E--02 1.19E 01 1.19E-01 4.61E-01 18-04022-15 TRG B105100AFSWC163CV 02/15/18 13:50 4/5/2018 4/5/2018 18-04022 Bismuth 214 EPA 901.1 Modffied 4.84E-01 4.29E 01 4.29E 01 7.51E-01

' u """"

18-04022-15 18-04022-15 TRG TRG 8105100AFSWC163CV B105100AFSWC163CV 02/15/18 13:50 02/15/18 13:50 4/5/2018 4/5/2018 4/5/2018

• 1* 4/5/2018 18-04022 18-04022 Cobalt-60 Cesium-134 EPA901.1 Modffied EPA901.1 Modified

-5.68E 02 2.99E-01 1.73E-01 2.15E--01 1.73E-01 2.16E-01 2.53E 01 2.77E-01

'i u u '

or_.,o

• o

'" TRG B105100AFSWC163CV 02/15/18 13:50 4/5/2018 ! 4/512018 18-04022 EPA901.1 Modified 1.07E 01 2-23E-01 2.23E-01 3.13E-01 - u orno

• o ..

.,., TRG B105100AFSWC163CV 02/15/18 13:50 4/5/2018  ! 4/5/2018 18-04022 ,oo EPA901.1 Modified 2.07E+OO 1.01E+OO 1.02E+OO 6.64E-01 u arno

-0 15 i TRG B105100AFSWC163CV 02/15/18 13:50 4/5/2018 ' ,11,;1?nrn "-°'"' -154 EPA901.1 Modified 6-42E-02 7 07F_01 2.82E 01 3.39E-01 u ' """"

18-04022 15 j TRG 8105100AFSWC163CV 02/15/1813:50 4/5/2018 4/5/2018

,;;; EPA 901.1 Modified 8.37E 01 3.27E-01 3.30E-01 5.30E-01 u """"

' 02/15/18 13:50 4/5/2018 4/5/2018 18-04022 Holmium-166m EPA 901-1 Modified -1.19E-01 3.46E-01 34SF-01 2.56E-01 u or.""

18-04022-15 TRG TRG '

B105100AFSWC163CV B105100AFSWC163CV 02/15/1813:50 4/512018 4/5/2018 18-04022 Iodine 129 EPA901.1 Modlfied 2.54E+OO

' 1.74E+OO 1.74E+OO 1.91E+OO u orno MS,,01' 71SF+OO 2.HF+OO 18-04022-15 TRG 8105100AFSWC163CV 02/15/18 13:50 4/5/2018 , 1R...Mfl"/' EPA901.1 Modified 7.31E+OO 1-24E+OO

,o .,., TRG B105100AFSWC163CV 02/15/18 13:50 4/5/2018 4/5/2018 1'~077 0 EPA901.1 Modffied -1.33E-02 '.81E-01 1 ,OF_01 2.91E-01 u - """

18-04022-15 TRG 8105100AFSWC163CV 02/15/18 13:50  ; 4/5/2018 : 4/5/2018 18-04022 Niobium 94 EPA 901.1 Modffied 9.35E 02 1.69E-01 1.70E-01 2.46E 01 u - """"

18-04022-15 I TRG - B105100AFSWC163CV 02/15/18 13:50 4/5/2018 4/512018 '

18 04022 Lead-210 EPA901.1 Modffied -5.82E-01 3.18E+OO 3.18E+OO ' 5.17E+OO u -""*

18 04022 15 ; TRG B105100AFSWC163CV 02/15/18 13:50

,;;;;;,-, 4/5/2018 rn_o,on Lead-212 EPA 901.1 Modified 5-28E-01 3.29E-01 3.30E 01 5.38E-01 u ' '"""

B105100AFSWC163CV 02/15/1813:50 4/o/?018 4/5/2018 ,s_o,on Lead-214 EPA 901.1 Modified 8.77E-01 4 <RF-01 4.80E-01 1.21E+OO u or_.,o 18-04022-15 TRG TRG B105100AFSWC163CV 02/15/1813:50 4/5/2018 4/5/2018

,s_,,.,,.,-, EPA901.1 Modified - 1.52E+OO  ; SSF-01 7'0F-O, 1 10F+OO u  ; arno

,o iR-04077 4.84E 01 4 7QF.01 4.29E-01 7 COF_o, u "r""

'" TRG B105100AFSWC163CV 02/15/1813:50 ""'°" 415/2018 EPA901.1 Modified 18-04022-15 TRG 8105100AFSWC163CV 02/15/1813:50 4/5/2018 4/5/2018 1R-~M7 EPA 901.1 Modified 6.46E 02 5.33E-01 5.33E-01 8.29E 01 u """"

18-04022 15 TRG 8105100AFSWC163CV 02/15/18 13:50 4/5/2018 4/5/2018 18-04022 Thorium 234 EPA901.1 Modified -2.93E+OO 2.66E+OO 2.67E+OO 3.85E+OO u """"

18-04022-15 TRG 8105100AFSWC163CV 02/15/18 13:50 41512018 , 415/2018 18-04022 Thallium-208 EPA901.1 Modffied 1.44E-01 , 4.99E-01 4.99E-01 S SSF-01 u or""

18 04022-15 TRG B105100AFSWC163CV 02/15/18 13:50 415/2018 4/5/2018 18-04022 Uranium 235 EPA901.1 Modified 1.64E+OO 2.75E+OO 2.75E+OO  : 1.44E+OO i u pCi/g CU=Counting Uncertainty;CSU=Combined Standard uncertainty ( 1-sigma); MDA=Minimal Detected Activity; LCS=laboratory Control Sample; M Bl=Blan k;DU P=Duplicate; TRG=Normal Sample; DO=Duplicate Original;U=Non-detect

(. EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[194]

865/481-0683 FAX 865/483-4621

Printed: 4/30/2018 3:20 PM Page 18 of 22 Report To: Work Order Details:

Patricia Giza 18-04022 Eberline Analytical Zion, Solutions, LLC _________ ---- .. ------ ---. Purchase OrrlP.r SDG:

677118 Final Report of Analysis '

101 Shiloh Blvd

~ .. - ,. *- ,.

ENVIRONMENTAL ' -

so Zion, IL 60099 Sample Matrix:

Lab Sample Client Sample I Receipt '

Analysis Batch l Analyte Method Result  :: cu I! CSU MDA Qualifier Report ID Type ID Date Date ' Date i ID ' I Units 1&-04022-16 TRG B105100AFSWC179CV 03/07/18 07:10 4/5/2018 4/5/2018 i 18-04022 Actlnium-228 EPA901.1 Modified 6.33E-01 4.18E-01 4.20E-01 7.74E 01 '* u '""'

4/5/2018 ( 4/5/2018 : 1&-04022 Silver-108m EPA901.1 Modified 7.16E 02 9.32E-02 i Q T~F-02 1.65E-01 : u  ! ,C,,,

-," !KC B105100AfCSWC179CV 03/07/18 07:10 i

u ,C,,,

" ' " TRG 8105100Af0SWC179CV 03/07/18 07:10 4/5/2018 : 415/2018 c 1/U\l[n?? Americium 241 EPA901.1 Modified i -5.39E-01 2.91E 01 2.93E-01  : 2.76E 01 i

-," TRG  : 8105100AFSWC179CV 03/07/18 07:10 41512018 I 4/5/2018 : 18-04022 Barium-133 EPA901.1 Modified 5.30E-02 7.36E-02 7.36E 02  :

2.89E 01 u '

03/07/18 07:10 4/5/2018 4/512018 ' 1&-04022 Bismuth-214 EPA901.1 Modified  : 8.38E 01 2.92E 01 2.95E-01 4.62E-01 eC."e

'" '-16 !KC ' B105100AFSWC179CV  :

03/07/18 07:10 4/5/2018 ' 1&-04022

• Cobalt-60 EPA 901.1 Modffied 5.60E 01 1.60E 01 1.63E-01 3.57E-01 u 18 04022 16 TRG B105100AFSWC179CV

""'"'" ,,_o,cn ,me 18-04022-16 TRG  : 8105100AFSWC179CV 03/07/18 07:10 4/5/2018 4/5/2018 Cesium 134 EPA901.1 Modified 8.61E 03 5.00E 02 5.00E-02 2.11E-01 u

,e ..

-," TRG I B105100AFSWC179CV 03/07/1807:10 4/5/2018 _ 4/5/2018 18-04022 Cesium-137 EPA901.1 Modrfied 5.14E+OO 6.88E-01 7.37E-01 ' 4.14E 01 *

,c;;e 18-04022-16 TRG ' B105100AFSWC179CV 03/07/18 04022 EPA901.1 Modrfied 3.16E-01 *: 4.06E 01 4.06E-01 3.95E 01 u ' -c"e

! -5.18E 03 2.20E-01 2.20E-01 1.93E-01 u 18 04022 16

, .. TRG B105100AFSWC179CV 03/07/18 07:10 4/5/2018 4/5/2018 18 04022 EPA901.1 Modrfied

,cu,

,e

!KG B105100AFSWC179CV 03/07/18 07:10 4/5/2018 4/5/2018 , 18-04022 EPA901.1 Modified

., 6.64E-02 1.47E-01 1.47E-01 3.38E 01 u

,e 03/07/18 07:10 4/5/2018 4/5/2018 18-04022 Holmiurn-166m EPA901.1 Modified 1.05E 02 1.97E 01 1-74E-01 u eme

' " TRG 8105100Af0SWC179CV 1 "'-"'

18-04022-16 TRG 8105100AFSWC179CV 03/07/18 2018 : 4/5/2018 i 18 04022 Iodine 129 EPA901.1 Modified 2.22E-01 ,,;,c ;;  ; ;,c;, 2.57E-01  : u eC;;,

, 4'F+OO 2_03E+OO ,c;;_

18 04022 16 TRG 8105100AFSWC179CV 03/07/18 07:10 4/5/2018 , 4/5/2018 18 04022 Potassium-40 EPA901.1 Modified 1.03E+01 2.38E+OO 18-04022-16 18-04022-16 TRG TRG B105100AFSWC179CV 8105100AFSWC179CV 03/07118 07:10 03/07/18 07:10 4/5/2018 4/5/2018 ;

4/5/2018 4/5/2018 1'-040" 18-04022 Nioblurn-94 ____ EP EPA901.1 Modified -2.30E-02

-02 1.32E 01 9.46E-02 1 S?F-01 9.46E 02 1_89E-01 1.32E-01 u

u cc;,:

03/07/18 07:10 4/5/2018 4/5/2018 1&-04022 Lead-210 EPA901.1 Modified 2.14E+OO 0 OOF+CO ,O,C+OC 2.92E+OO u em:

18 04022 16 TRG B105100AFSWC179CV j ---  ;,,:;;;;;;

18 04022 16 TRG 8105100AFSWC179CV '" " " ' )1' 4/5/2018 Lead-212 EPA901.1 Modified 8.42E-01 ""-"' ""-"' 4.57E 01  : . oCiJc TRG '

B105100AFSWC179CV 03107/18 07:10 4151201' 4/5/2018 18--04022 Lead-214 EPA901.1 Modified ' 4.99E 01 ,OCF,01 3.21E 01 S,SF-01

, ,,,_01 u  :

em,

,me

" TRG 03/07/18 07:10 4)5)2018 , 4/5/2018 18 04022 Prornethium-145 EPA901.1 Modified 3.51E 01 2_32E-01

'""'-"' ' u TRG B105100AFSWC179CV 03/07/18 07:10 4/5/2018 4/5/2018 18-04022 Radium 226 EPA901.1 Modlfied 8.38E 01 ,:,,e:o,  ; ;,c_;:  ; soc_;; ,me

,,. TRG B105100AFSWC179CV 03/07/18 07:10 4/512018 4J.S1'01' 18-04022 EPA901.1 Modrfied 2.78E 01 3.72E-01 3.73E-O' 6.11E-01 , u pCi/g 18-04022-16 TRG I B105100AFSWC179CV 10 4/5/2018 ,,,,.,,,,, 18 04022 Thorium 234 EPA901.1 Modlfied 3.84E+OO 0 OOF+CC O&CF+CC 0 40F+CO u eme 18-04022-16 TRG 8105100AFSWC179CV ,,, 0710 415/2018 , 4/5/2018 1804022, Thallium-208 EPA901.1 Modrfied 6.14E-01 5.19E-01 5,20E-01 8.41E 01 ' u ,me 18 04022 16 TRG B105100Af0SWC179CV 03/07/18 07:10 4/5/2018 4/5/2018 18-04022 Uranium 235 EPA901.1 Modrfied -1.21E+OO ' '1E+OO 1.51E+OO 8.14E-01 u pCi/g CU=Countlng Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sarnple;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[195]

Printed: 4/30/2018 3:20 PM Page 19 of 22 Report To* Work Order Details:

Patricia Giza 18-04022 Eberline Analytical ,. . .

Zion Solutions, LLC. -------- .. .

.*.J .. _. .. . --~:_"'.'.

SDG:

Order: 677118

~ .

Final Report of Analysis 101 Shiloh Blvd  : ENVIRONMENTAL ...

Zion, IL 60099 Sample Matrix: so  :

Lab  ! Sample Client Sample  ! Receipt Analysis Batch  : I Report Ana!yte Method Result  : cu CSU MDA Qualifier

• Units ID Type ID Date Date Date ID EPA901.1 Modified 3 56E*01 4.07E-01 4.08E-01 7.59E 01 u oC::o 18 04022 17 TRG 8105100AFSWC190CV 03/06/1813:00 4/5/2018 4/5/2018 18 04022 18-04022-17 1KG B105100AFSWC190CV 03/06/18 13:00 4/5/2018 4/5/2018 rn_n.tn??  %,o,.108m EPA 901.1 Modified ,.84E*De 6.SSE 02 6.55E-02 1.34E-01 u or.::o

. .1 scc.c 1.40E-01 1.40E-01 1.83E 01 u

-*~;;.,~--- ""

18 04022 17 TRG B105100AFSWC190CV 03106/18 13:0C 41512018 4/5/2018 13.04022 EPA 901.1 Modified  :

347E.O, SS4F.n? 6.34E-02 -- 2.18E 01 u oC::o 18-04022-17 TRG B105100AFSWC190CV 03106118 " or 41512018 4/512018 18-04022 Barium-133 EPA 901.1 Modified  :

18-04022-17 TRG B105100AFSWC190CV 03106/18 nee 41512018

• 415/2018 ! 18-04022 Bismuth 214 EPA 901.1 Modified 4.77E*01 2.74E 01 2.75E-01  : 4.02E-01 or.::o 18-04022-17 TRG B105100AFSWC190CV 03106118 13:00 4/512018 4/512018 : rn.~on CoS,,.~C EPA901.1 Modified ~CCF.C, 1.09E*01 1.09E-01 I 1.73E-01 u oC::o 18 04022-17 TRG I 8105100AFSWC190CV 03/06118 13:0C 41512018 4/512018

• rn.~on EPA901.1 Modified 1 SSC.C,  ; s;c.n; 7.63E 02  : 1.73E-01 u  :

"°""

18-04022-17 TRG  :

B105100AFSWC190CV 03106/18 13:0C 4/5/2018 41512018 18-04022 Cesium-137 EPA 901.1 Modified 1.97E 01 1.33E 01  :

1.33E-01 2.02E-01 u  ! or::o

• -*** .. TRG  : B105100AFSWC190CV 03/06/18 13:00 4/5/2018 4/5/2018 1R.040" EPA901.1 Modified 352E*02 3.38E-01 3.38E 01 2.61E 01 u oC::o

,o

'1, 1KG B105100AFSWC190CV 03/06/18 13:00 4/5/2018 4/5/2018 ' "18-04022 *::: EPA901.1 Modified -1.14E 01 1.68E 01 1.68E 01 1.28E-01 u ,,r;,,,

18-04022-17 1KG . B105100AFSWC190CV 03/06/18 1::t*nn 41512018 4/5/2018 \ 1R_n.tn??

EPA901.1 Modified .s SCF.CS 1.00E*01 1.00E-01 2.25E-01 u or::o B ! rn_n.tn?? EPA901.1 Modified 1.86E-01 1.74E-01 1.74E-01 1.12E--01 u orno 03/06/18 13:00 18-04022 17 TRG B105100AFSWC190CV """'l18 41'i/")fJ1  :

18-04022-17 TRG B105100AFSWC190CV 03/06118 13:00 41512018 4/5/2018 04022 lodine-129 EPA901.1 Modified -2.22E-02 5.14E-02 5.14E*02 7.33E 02  : u . orno 18-04022-17 TRG B105100AFSWC190CV 03/06/18 13 00 415/2018 4/5/2018 a 18-04022 *" EPA901.1 Modified . 4.82E+OO , ,sc;nn 1 1.58E+OO . 1 o-F,CC .

"°""

03/06/181300 41512018 41512018 ! 1R.0407' -. EPA901.1 Modified 4.96E-03 6.01E 02 , 6.01E 02  : 1.86E-01 u pCi/g 18-04022 17 TRG 8105100AFSWC190CV 1.00E 01  ! 1.20E-01 u

...' *-'" nf';/~

18-04022 17 1KG 8105100AFSWC190CV 03/06/18 nnn 4/5/2018 4/5/2018 : 1R.n.tn?? Niobium 94 EPA 901.1 Modified -5.97E-02 1.00E 01 i 18-04022-17 TRG B105100AFSWC190CV 03/06/18 1'.a\*flfl 41512018 . 4/5/2018 '. 18-04022 Lead-210 EPA901.1 Modified ' -4.45E--03 1.03E+OO 1.03E+OO i 1.54E+OO  : u orno 18-04022 17 TRG  : 8105100AFSWC190CV 03/06/18 13:UU """)1'

• 4/5/2018 18*04022 Lead212 EPA 901.1 Modified 3.42E-01 1.50E 01 1.51E-01  : 2.58E-01 u ';c::o 18-04022-17 TRG B105100AFSWC190CV 03/06/18 13:00 41512018 4/5/2018 18-04022 Lead-214 EPA901.1 Modified_-*- 4.85E 01 2.23E 01 2.25E-01 - 2.95E 01 . orno

• - TRG 8105100AFSWC190CV 03/06/18 13:00 41512018 4/5/2018 C 18-04022 Promethium 145 EPA 901.1 Modified 6.51E 02 9.68E-02 9.68E-02 . i 1.35E 01 u

• or::o 1 TRG B105100AFSWC190CV 03/06/181'.HlO 415/2018 41512018 I -226 ,_,EPA901.1

___ ,,, ___ , Modified 4.77E-01 2.74E-01 2.75E 01 **: 4.02E-01  : "r""

• --* 4.17E-01 u . "r""

18-04022-17 TRG . B105100AFSWC190CV 03/06/18 13:00 4/5/2018 4/5/2018 18 04022 EPA901.1 Modified 6.72E-03 2.91E 01 2.91E-01 '

18 04022 17 TRG

. B105100AFSWC190CV 03106/18 13:00 4/5/2018 , 4/5/2018 : 18-04022 EPA 901.1 Modified 1.32E+OO 1.21E+OO 1.21 E+OO 1.92E+OO u * "°""

18 04022 17 TRG B105100AFSWC190CV 03/06/1813:00 4151201a , 41512018 I 18-04022 Thallium 208 EPA 901.1 Modified 4.40E--01  ; 2.63E-01 I 2.64E-01 I 6.35E--01 u i or::o 18-04022-17 TRG B105100AFSWC190CV 03/06/181:'l*OO 4/5/2018 4/5/2018 ; 18 04022 Uranium-235 EPA901.1 Modified * -1 ':l~i::-/J1 i 9.01E 01 i 9.01E-01 5.78E-01 I u i pCi/g CU=Counting Uncertairrty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Dupllcate Original;U=Non-detect EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[196]

Printed: 4130/2018 3:20 PM Page 20 of 22 Reporl To* Work Order Details:

Patricia Giza 18-04022 Eberline Analytical Zion*,:._~;_*:;,_~~-~~:.: LLC

.. L.. ..

SDG:

Purch~se--O~d~;~-! 677118 Final Report of Analysis 101 Shiloh Blvd .... Analvsi, ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so i

Lab ID Sample Client ID Sample i Receipt Analysis Date Batch Analyte Method Result cu

! CSU MDA Qualifier Report Units Type Date

' Date ' ID i 18-04022-18 TRG B105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 18-04022 Actinium-228 EPA 901.1 Modified 3.90E-01 5.31E-01 5.32E-01 9.08E-01 u pC(/g 18--04022-18 TRG . B105100AFSWC201CV 03/06/1815:13 4/5/2018 : 4/5/2018 18-04022 Silver-108m EPA901.1 Mnrlifif'~ -8.41E-O, 1.44E-01 1.44E-01 1.66E-01 u cC;,o 18-04022-18 TRG . B105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 18 04022 Americium 241 EPA901.1 MnrlifiPr -1.21E-OC 1.87E-01 1.87E-01 2.90E-01 u crno

,c IHC JHG

B1051 OOAFSWC201 CV B105100AFSWC201CV 03/06118 15:13 03/06/18 15:13 4/5/2018 4/5/2018 4/512018

• 4/5/2018 18 04022 18-04022 Barium 133 us EPA 901.1 ~~nrlm.,,,

EPA901.1 Mnrlifi<>rl

'°'"-°'

5.51E 01 7.95E-02 3.90E-01

3.91E-01 2.27E-01 6.14E-01

, u u .

orno

"°""

-,o TRG B105100AFSWC201CV 03/06/18 15:13 4/5/2018 4/5/2018 18-040?? Cobalt-60 EPA901.1 Modified . 2.65E-01 1.29E-01 1.29E-01 2.48E-01 . oc;/o 18-04022-18 TRG . B105100AFSWC201CV 03/06/18 15:13 4/5/2018 4/5/2018 18-040" Cesium-134 EPA 901.1 Modified i -7.75E-03 5.26E-02 5.26E-02 1.60E-01 u cr.;,o 18--04022-18  : 8105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 1'-040,, Cesium-137 EPA901.1 Mnrlffii>rl 1.87E+OO 3.42E 01 3.55E 01 2.98E 01 . crnn TRG

' 18-04022 Europium-152 EPA901.1 Modrfied ' 1.88E 02 4.72E 01 4.72E--01 4.55E-01 u eCO,c 18--04022-18

-,o TRG TRG .

B105100AFSWC201CV 8105100AFSWC201CV 03/06/1815:13 03/06/18 15:13 1~~~18 18 18-04022 Europium-154 EPA901.1 Modrfied EPA901.1 Modrfied 1.35E--01 3.56E-01 1

2.24E--01 2.34E--01 2.24E-01 2.35E 01 2.11E-01 3.58E 01 u

u oc;/n crnc 18-04022-18 TRG . B105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 18-04022

,. ***- I

-,o TRG B105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 rn.n,nn Holmium 166m EPA 901.1 Modified 1.44E-01  ; 1.85E-01 1.85E-01 1.70E-01

' u cC;,o

,o -,o TRG B105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 ,~n,nn lodine-129 EPA 901.1 Modrfied 2.53E--03 1.47E-01 1.47E-01 2.10E-01 ' u crno o ,oF,nn 2.39E+OO 1.98E+OO  ; pCi/g 18--04022-18 i TRG B105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 18-04022 PotassiL:m-40 EPA901.1 Modified

'"'"'°" .

-,o TRG B105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 18-04022 : "' EPA901.1 Modified 7 03E-03 1 SSF-01 1.35E-01 1.98E-01 j u I ii:,; "

-,o TRC B1 D5100AFSWC201 CV 03/06/1815:13 4/5/2018 4/5/2018 18-04022 i Niobium-94 EPA901.1 Modified 1.21E 01 9.86E 02 1 9.88E 02 2.03E 01 u pCi/g 18-04022-18 TRC ' B105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 18-04022 Lead-210 EPA901.1 Modified 2.93E+OO 1.37E+OO 1.38E>OO 2.62E+OO u nCl/o

,o -,o TRG  : B1D5100AFSWC201CV 03/06/1815:13 4/5/2018 I 4/5/2018 18 04022 Lead 212 EPA901.1 Modified 2.55E-01 1.98E 01 1.98E 01 3.18E 01 u cr;,c

'" "" IHC B105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 rn_n,rnn lead-214 EPA 901.1 Modified 7.64E-01 3.05E-01 3.0BE-01 5.57E-01 I crnc

'" "" '" 1KG B 1051 OOAFSWC201 CV 03/06/18 15:13 4/S/2018 4/5/2018

• 18 04022 Promethium-145 EPA 901.1 Modified 7.65E-02 1.69E 01 1.69E 01 ' 2.76E 01  : u cCO,c

-,o TRG B105100AFSWC201CV 03/06/18 15:13 4/5/2018 4/5/2018 18 04022 Radium 226 EPA901.1 Modified 5.51E-01 3.90E-01 3 91F-01 6.14E 01 ] u cCO,c

-,o TRG 8105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 18-04022 EPA901.1 Modified 3.00E-02 2.91E-01 2.91E-01 ' 4.93E-01 ' u

'" -,o TRG B105100AFSWC201CV 03/06/1815:13 4/5/2018 4/5/2018 18-040'7 Thorium-234 EPA 901.1 Modified 8.99E-01 2.32E+OO 2.32E+OO 3.18E+OO  ; u '

oC.1/o

-,o TRG B105100AFSWC201CV 03/06/1815:13 4/St,018 4/5/2018 1'-040" Thallium 208 EPA 901.1 Modified 3.38E-01 2.78E-01  ! 2.79E 01 6.28E 01 u "' ""

'" "" TRG B105100AFSWC201CV 03/06/1815:13 4/5/2018 C 4/5/2018 , 1.<Ln,1n?? ' EPA 901.1 Modified 1.29E+OO 1.60E+OO ] 1.60E+OO 8.92E-01  ; u pCllg CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[197]

Printed: 4/3012018 3:20 PM Page 21 of 22 Report To: Work Order Details; Patricia Giza 18-04022 Eberline Analytical ' _Zion Solutions, LLC ...*...... *-*--*-*----*---*--*-*--- -*- ---------------.,

SDG:

Purchase Order.: 677118 Final Report of Analysis 101 Shiloh 1,....----------- ---------- Blvd

___ Analysis_ Category: : ENVIRONMENTAL **-**--- . ---

Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample I Receipt Analysis I' Batch ro Analyte Method I Result  ! cu CSU I MDA Qualifier i

' Report fD 18-04022-19 Type TRG B105100AFSWC210CV ID Date 03/06/1814:40 Date 415/2018 Date 4/5/2018 18-04022 Actinium-228 EPA 901.1 Modified 5.78E 01 =-, sosc.o* 9.67E-01 u Units pCi/g

~;;;; ---**

18-04022-19 TRG B105100AFSWC210CV 03/06/1814:40 4/5/2018 4/5/2018 18-04022 Silver-108m EPA901.1 Modffied 6.13E-02 141F.01 141F.0' 2.41E-01 ' u

,o ' ,o TRG B105100AFSWC210CV 03/06/18 14:40 4/5/2018 4/5/2018 ' 18 04022 Americium-241 EPA901.1 Modlfied -2.22E-01 1.08E-01 1.08E-01 3.83E-01 ' u ornc

• -*-*-- ----- -  ; ioe:a co co TRG  : 8105100AFSWC210CV 03/06/18 14:40 4/51201' , 4/5/2018 18 04022

• Barium-133 EPA 901.1 Modlfied -1.28E 03 1.20E 01 4.16E-01 u oO:

co 18-04022 , EPA901.1 Modified HOCM 358F*O* 2.36E 01 TRG  : 8105100AFSWC210CV 03/06/18 14:40 4/5/2018 4/5/2018 Bismuth-214 t ... 8.38E-01 I '

18-04022-19 TRG  : B105100AFSWC210CV 03/06/18 14:40 4/5/2018 I 4/5/2018 18-04022 I Cobalt-60 EPA901.1 Modffied 2.48E-01 1 04F,01 1 05F-01 1.64E 01 --*

18-04022-19 TRG B105100AFSWC210CV 03/06/18 14:40

' 4/5/2018 4/5/2018 18-04022 ,

18-04022 Cesium-137 EPA 901.1 Modified EPA901.1 Modified 2.13E+OO

,c 4,1-°'

6.04E-02 4.31E 01 3.04E 01 4.48E-01

' u  :

°' '"

,c,1, 18-04022-19 TRG ' 8105100AFSWC210CV 03/06/18 14:40 4/5/2018 4/5/2018 18-04022-19 TRG B105100AFSWC210CV 03/06/18 14:40 4/5/2018 4/5/2018 18-04022 ' Europium-152 EPA 901.1 Modified 1.96E+OO 9.71E-01 9.76E 01 6.24E 01 u ' ,o:,,

18-04022-19  ! TRG  : B105100AFSWC210CV 03/06/18 14:40 4/5/2018 4/5/2018 18-04022 EPA 901.1 Modified 5.31E,02 3.76E 01 3.76E 01 3.21E-01 u '°"'

180402219 i 8105100AFSWC210CV 03/06/1814:40 4/5/2018 4/5/2018 18 04022 C EPA 901.1 Modified 3 18F-01 2.27E-01 2.27E-01 4.61E 01 u 18 04022-19 TRG TRG

8105100AFSWC210CV 03/06/1814:40 4/5/2018 I 4/5/2018 I 18 04022 Holmium-166m EPA901.1 Modified 1.56E 01 2.48E-01 2.48E-01  : 2.34E-01 u ' '.~(~-

18-04022-19 TRG 8105100AFSWC210CV 03/06/1814:40 415/2018 4/5/2018 18-04022 lodine-129 EPA 901.1 Modified -8.98E 01 1 OAC+M 1 OAC+M 1.71E+OO , u ,r:,,

18-04022-19 TRG 8105100AFSWC210CV 031 18 18 04022 Potassium-40 EPA 901.1 Modlfied 7.64E+OO 2,,c;a, ,,6c;,6 1.96E+OO  ! ' --"-

18-04022-19 TRG B105100AFSWC210CV 03/06 2018 1 4/5/2018 1R-040?, -- EPA901.1 Modrfied -6.69E-02 1.52F-01 1.52E-01 2.27E-01 **c u ,o:,,

18-04022-19 TRG  : 8105100AFSWC210CV 03/06/18 14:40 4/5/2018 4/5/2018 18-04022 Niobium-94 EPA901.1 Modified -8.72E 02 1.45E--01 14CF-01 1.97E-01 u -""-

---

**-----*--*  : 8105100AFSWC210CV 03/06118 14:40 4/5/2018 4/5/2018 18-04022 Lead-210 EPA901.1 Modified

' --3.62E+OO 3.18E+OO 3.18E+OO 4.77E+OO i u oC:,o 18 04022 19 TRG 03/06/18 14:40 4/5/2018 4/5/2018 18-04022 Lead-212 EPA901.1 Modrfied 9.90E-01 4.77E-01 4.79E-01 7.21E-01 ' or.:,o

' -G B105100AFSWC210CV

-- ' 19 TRG  : B105100AFSWC210CV 03/06/18 14:40 4/5/2018 4/5/2018 18-04022 Lead-214 EPA901.1 Modified 6.81E-01 5.31E-01 5.32E-01 1.17E+OO j u or.:,o

-- 19 TRG '

B105100AFSWC210CV 03/06/18 14:40 4/5/2018 4/5/2018 18-04022 Promethlum-145 EPA 901.1 Modified 1 OOC+OO 6.57E-01 6.60E-01 9.80E-01  : u or:,o

,o:,,

,0 19 TRG B105100AFSWC210CV 03/06/18 14:40 4/5/2018 4/5/2018 1'-"40" Radium 226 EPA 901.1 Modified 838F-01 '5BF,Q1 3.58E-01 2.36E 01 j

,o 19 TRG B105100AFSWC210CV 03/06/18 14:40 41512018 4/512018 1',"40" EPA901.1 Modified 4.69E-02 5.4TE-01 5 47F,01 8.25E-01 I u --"-

-- 19 TRG 8105100AFSWC210CV 03/06/1814:40 03/06/1814:40 4/5/2018 4/512018 18 04022 Thorium-234 Thallium-208 EPA 901.1 Modified EPA901.1 Modlfied 4.87E+OO 7.57E-01 2.04E+OO S.21E-01 2.06E+OO S.22E-01  :

5.34E+OO 8.32E 01  :

i u u

or,,o orno 18-04022-19 TRG B105100AFSWC210CV 4/5/2018 : 4/5/2018 18 04022 18-04022 19 TRG 8105100AFSWC210CV 03/06/1814:40 4/5/2018 4/5/2018 i 18-04022 Uranium 235 EPA901.1 Modified I 7 '"'-"' °'"";"" 7 40C+M 1.35E+OO i u ' pCi/g CU=Counting Uocertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;OO=Duplicate Original;U=Non-detect

(

0 EBERLINE EBERLINE ANALYTICAL CORPORATION

~--~--*- ANALYTICAL 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[198]

---...*:c-***,*,,.*.-

Printed: 4/30/2018 3:20 PM Page 22 of 22 Report To: Work Order Details*

Patricia Giza 18-04022 Eberline Analytical . --- ----.------------- -

_______ Zion Solutions, LLC SDG:

...,..,.....,....... nrrlF:;:*i*-

677118 Final Report of Analysis 101 Shiloh Blvd Analvsis ENVIRONMENTAL Zion. IL 60099 Sample Matrix:

• so I

I' Lab Sample Client Sample Receipt Analysis i Batch  : I Report Analyte Method Result cu CSU I MDA Qualifier ID

' Type ID Date Date Date ID ' ' l ' Units 18--04022-20 f TRG B105100AFSWC231CV 03/06/1814:30 4/5/2018 4/5/2018 18~:6*ii---!--- . AcUnium-228_ ...

EPA 901.1 Modified 1.93E-01 4.77E-01 i 4.77E-01 ' 8.51E-01 u  : pCilo 41512018 i 4/5/2018 j 18-04022 Silver-108m EPA 901.1 Modified 1.27E-01 1.16E-01 1-16E-01 1-79E-01 u 18--04022-20 18--04022-20 TRG TRG B105100AFSWC231CV B105100AFSWC231CV 03/06/1814:30 03/06/1814:30 4/5/2018 4/5/2018 : 18-04022 ; Americium-241 EPA 901.1 Modified -1.28E-02 1.61E-01 ' 1.61E-01 2.35E-01 u

oCi/o pCi/o 18-04022-20 TRG  : B105100AFSWC231CV 03106118 14:30 41512018 415/2018 18-04022 i Barium-133 EPA901:1 Modified 2.97E-01 1,94E-01 '

1.95E-01 2.54E-01 u

u  :

oCilo 18-04022-20 TRG  : B105100AFSWC231CV 03106118 14:30 41512018 41512018 i 1S-04022 : Bismuth-214 EPA901.1 Modified 1.52E-01  : 3.55E-01 i 3-55E-01 5.39E-01 oCilo 18-04022-20 03/06/181430 41512018 41512018 18-04022 Cobalt-60 EPA901.1 Modified 6.04E-02 1.25E-01 1.25E-01 2.14E-01 u oCilo

-- -----~----- ----*--***

TRG B105100AFSWC231CV ' '

18--04022-20 TRG  : B105100AFSWC231CV 03/06/18 14SO 41512018 41512018 ' 18-04022 ; Cesium-134 EPA901.1 Modified -3.49E-01 '

2.49E-01 2.49E-01  : 2.17E-01 ' u '

oCi/o i  :

00 TRG B105100AFSWC231CV

- u:1111hlH:J 14*:111 41512018 ' 4/512018 18-04022 Cesium-137 EPA901.1 Modified 2.87E-01  :

2.47E-01

' 2.47E-01

' 3.99E-01 i u u

oCi/o oG;/o 18-04022-20 '

18--04022-20 TRG TRG B105100AFSWC231CV B105100AFSWC231CV US/Ub/18 14 SU U3/U6/18 14:SU 4/'1,018 4/5/201' 4/5/2018 4/b/,018 18-04022 ]

' 18 04022 EPA901.1 Modified EPA901.1 Modified

-1.72E-01

-3.64E-02 4.88E 01 3.84E-01

• 4.88E 01 3.84E-01

': 3.51E 01 1.81E-01  : u pCiig_

B105100AFSWC231CV 03/06/1814:30 4/5/2018 , 4/5/2018 I 18 04022 :cc EPA901.1 Modified -1.83E-02 1.03E-01 1.03E-01 2.80E-01 u oCilo 18--04022 20 18---04022-20 TRG TRG B105100AFSWC231CV 03/06/1814:30 41512018 4/5/2018 18-04022 Holmium-166m EPA901.1 Modified ' -1.53E-01 2.55E-01 2.56E-01 i' 1.42E-01 i' u

. oCilo 18-04022-20 TRG B105100AFSWC231CV 11:1/llhl]tl 14*:1!1 41.'11:.l!lltl : 4/5/2018 18-04022 lodine-129 EPA 901-1 Modified 'i 1.09E-02 6.88E-02 6.88E-02 1.04E-01 u oCi/o 18-04022-20 TRG B105100AFSVVC231CV 03/06/1' 14:SU 41,i,u18 EPA901.1 Modified ' 7.06E+OO 2.52E+OO i 2.54E+OO 2.89E+OO ' '

oCi/o

""'°" 18-016}~- **j***-~:tassium-40 i 18-04022 * '" 1.62E-01 1.62E-01 2.54E--01 u 18-04022-20 18-04022-20 TRG TRG B105100AFSWC231CV 8105100AFSWC231CV 03/06/1814:30 03/06/1814:30 4/5/2018 4/5/2018 4/5/2018 4/5/2018 18-04022 Niobium-94 EPA901.1 Modified EPA901,1 Modified 3.20E 02 1.33E-02 1 A2E-01 'j 1 A2E-D1 2,17E-01 u

,-*- __P._~~g -***-*-

pCilo 18---04022-20 TRG B105100AFSWC231CV 03/06118 14:30 41512018 41512018 1S-04022 Lead-210 EPA 901.1 Modified 1.12E+OO 1.24E+OO a 1.25E+OO  ; 1.97E+OO u i oci/o 18--04022-20 TRG B105100AFSWC231CV 03/06/1814;30 4/5/2018 4/5/2018 18-04022 Lead-212 EPA 901.1 Modified 2.20E-01 1.92E-01 i 1.93E-01 3.13E-01 u oCilo 18--04022 20 TRG B105100AFSWC231CV 03/06/18 14:30 4/5/2018 4/5/2018 18-04022 Lead-214 EPA 901.1 Modlfied 3.52E-01 2.23E-01 2.23E-01  : 6.63E-01 u ' ,cu, 18---04022 20 TRG B105100AFSWC231CV 03/06/18 14:30 415/2018 4/5/2018 18-04022 - EPA 901.1 Modtfied 3.77E-02 1.20E-01 1.20E 01 1.84E 01

' u oCi/o 18--04022-20 TRG B105100AFSWC231CV 03/06/18 14:30 415/2018 4/5/2018 . 18-04022 Radium-226 EPA901.1 Modtfied 1.52E-01 3.55E-01 3.55E-01 5.39E-01 u PCi/0 18--04022-20 TRG B105100AFSWC231CV 03/06/18 14:30 4/5/2018 4/5/2018 ; 18-04022 EPA 901-1 Modified 1.24E-01 3.99E-01 3.99E 01 5.94E-01 u  : oCi/o 18-04022-20 TRG B105100AFSWC231CV 03/06/18 14:30 4/5/2018 I 4/5/2018 I 18-04022 Thorium-234 EPA901.1 Modified 4.11E+OO 1.88E+OO 1.90E+OO I 2.96E+OO I oCilo 18---04022-20 TRG B105100AFSWC231CV 03/06/18 14:30 4/5/2018 4/5/2018 18-04022 Thallium-208 EPA 901.1 Modified 4.13E-01 3.70E-01 3.70E-01 5.82E-01 u ,cu, 18-04022-20 TRG ' B105100AFS\1VC231CV 03/06/18 14:30 4/5/2018 ( 4/5/2018 : 18-04022 C Uranium-235 EPA901.1 Modified -1.14E+OO 1.47E+OO 1-47E+OO 7.70E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sarnple;MBL=Blank;DUP=Ouplicate;TRG=Norrnal Sample;DO=Duplicate Original;U=Non-detect

( ~

EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830

[199]

865/481-0683 FAX 865/483-4621

ZS-WM-131 Revision 0 ZIONSOLUTIONSrrc Information Use An EnergySo/urions Company RECD APR O5 2018 Attachment I - Chain-of-Custody Form 1 8 - 0 4 0 22 Sample ID Sampl Matrix Sample Type Sample Container Sample Date Sample Time Analysis Type Preservative Remaiks eLog Vol Unit Type Qty Bl05100AFSWCOl 7CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310712018 0935 5ROCIHTD NIA 0.0-0S' 1 101.6:ig Bl05100AFSWC041CV NIA CONCRETE CONCRETE 57.94 cm' Puck l 0310712018 0925 5ROCIHTD NIA 0.0-0. i"

' Bl05100AFSWC057CV NIA CONCRETE CONCRETE 57.94 cm-' Puck l 0310712018 0910 5ROCIHTD NIA

]23.3"g 0.0-03' 6 101.9'Jg Bl05100AFSWC088CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310712018 0855 5ROCIHTD NIA 0.0-0.5" 7 105.9,,g Bl05100AFSWCIOICV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310712018 0725 5ROCIHTD NIA 0.0-0.5" r 146.06g B105100AFSWC1 !5CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 03107/2018 1530 5ROCIHTD NIA 0.0-0.i"

'f 94.29g Bl05100AFSWCI 16CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310712018 0840 5ROCIHTD NIA 0.0-0 ..i" Cl 98.62g Bl05100AFSWC150CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 02121/2018 0840 5ROCIHTD NIA 0.0-0.:i" 1 97.99g Bl05100AFSWC151CV NIA CONCRETE CONCRETE 57.94 cm' Puck I 02121/2018 0920 5ROCIHTD NIA 0.0-0 ..i" 1,- 102.6 g Bl05100AFSWC156CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0212112018 1330 5ROCIHTD NIA 0.0-0.i" lj 96.47g Bl05!00AFSWC162CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0211512018 1550 5ROCIHTD NIA 0.0-0.5"

~ 90.81g B105100AFSWC163CV NIA CONCRETE CONCRETE 57.94 cm' Puck 1 02/1512018 1350 5ROCIHTD NIA 0.0-03' IS 97.73g Bl05100AFSWC179CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310712018 0710 5ROCIHTD NIA 0.0-0.:i" 17 Bl05100AFSWC190CV NIA CONCRETE CONCRETE 57.94 cm' Puck I 0310612018 1300 5ROCIHTD NIA 100.50g 0.0-1.0" 180.0(Jg Bl05100AFSWC201CV NIA CONCRETE CONCRETE 57.94 cm* Puck I 0310612018 1513 5ROCIHTD NIA 0.0-0.:i

\S 96.68g Bl05100AFSWC210CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310612018 1440 5ROCIHTD NIA 0.0-03' 120.4,.g Bl05100AFSWC231CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310612018 1430 5ROCIHTD NIA 0.0-03' 132.7:ig Bl05100AFSFC239CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310612018 0955 5ROCIHTD NIA 0.0-1.tl" 209.9'.:g BI 051 OOAFSFC250CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310612018 0940 5ROCIHTD NIA 0.0-0.:i" 130.0:ig

[200]

ZS-WM-131 18-04022 Revision 0 ZIONSOLUTIONSric An EnergySo/u/ions Company RtCiJ APR O~ lOlS [nformation Use Bl05100AFSFC255CV NIA CONCRETE CONCRETE 57.94 cm' Puck 1 0310612018 1246 5ROCIHTD NIA 0.0-05" 134.31g B 105100AFSFC263CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0930 5ROCIHTD NIA 0.0-0S' 110.4,g B 1051 OOAFSFC276CV NIA CONCRETE CONCRETE 57.94 cm' Puck 1 0310512018 1342 5ROCIHTD NIA 0.0-0S' 122.7: g B 1051 OOAFSFC282CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0852 5ROCIHTD NIA 0.0-03' 116.6Eg B 1051 OOAFSFC289CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1352 5ROCIHTD NIA 0.0-0.::

119.0: g B 1051 OOAFSFC293CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0210712018 1345 5ROCIHTD NIA 0.0-0S' 132.5: g B 105100AFSFC300CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 02/1312018 1250 5ROCIHTD NIA 0.0-0S' 85.562g Bl05100AFSFC316CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1358 5ROCIHTD NIA 0.0-0.::

108.I:g Bl05100AFSFC321CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 02/1312018 1410 5ROCIHTD NIA 0.0-0S' 148.8( g Bl05100AFSFC326CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 02/1412018 0815 5ROCIHTD NIA 0.0-0S' 134.3:g Bl05100AFSFC329CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1418 5ROCIHTD NIA o.o-o.::"

115.0f g Bl05100AFSFC332CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1405 5ROCIHTD NIA 0.0-0.:"

123.51g B 1051 OOAFSFC345CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0210712018 1045 5ROCIHTD NIA 0.0-0.:"

115.2~ g Bl05100AFSFC347CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0211212018 1310 5ROCIHTD NIA 0.0-0.:"

91.09; B 105100AFSFC348CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0211212018 1515 5ROCIHTD NIA 0.0-0.:"

88.01; Bl05100AFSFC354CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0210812018 1307 5ROCIHTD NIA 0.0-0.:"

110.07g B 105100AFSFC363CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0740 5ROCIHTD NIA 0.0-0.:"

85.52; Bl05100AFSFC369CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1453 5ROCIHTD NIA 0.0-0.:"

150.58g Bl05100AFSFC375CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1431 5ROCIHTD NIA 0.0-0.:"

119.51g B105100AFSFC379CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310612018 0746 5ROCIHTD NIA 0.0-0.:"

135.25g B 1051 OOAFSFC383CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0740 5ROCIHTD NIA 0.0-0.:"

118.83g Bl05100AFSFC411CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0805 5ROCIHTD NIA 0.0-0.~ 5 168.23 {'

[201]

ZS-WM-131 ZIONSOLUTIONSiic 1s-04022 Revision 0

[nformation Use An Enei-yySo/ulions Company

, A~~ os 201a B 1051 OOAFSFC433CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0210812018 1512 5ROCIHTD NIA 0.0-0S' 130.9:g Bl05100AFSFC434CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0210812018 0930 5ROCIHTD NIA 0.0-0S' 133.5c g Bl05100AFSFC435CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0210712018 1422 5ROCIHTD NIA 0.0-0S' 152.3c g B 105100AFSFC436CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0211412018 1030 5ROCIHTD NIA 0.0-0S' 133.5: g B 105100AFSFC438CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0210812018 1025 5ROCIHTD NIA 0.0-0S' 130.9: g Laborato1y: Date Submitted To Lab: Ship Container No.: Cooler Temperature: trill Number: f e;r/ f~

. r r~f (JVfN7 t .~ )lt Eberline Labs NIA NIA 810'7 ()/.)./5 bhgR Relinquished by: Date Time: Received by: Date: (mmldd/yyyy): Time:

(0410412018)

Reed R. Smith l3~b !Z1c)q rel f)fic/<£r ! {)!.f /01 /zo1g 13t;6 Relinquished by: Date Time: Received by: Date: (rrunlddlyyyy): Time:

ff7Jarr,\

Relinquished by:

f_f{,-~f t;;1;zm,s Date Time:

1650 A*Atx (;~ f O\J trn ,i>>J" t. 6t.{ ~"Jtf/101 R Date: (1mn/dcllyyyy): Time:

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(1mn/dd/yyyy): -v Co1mnents PO# 677118 7 day turnaround 5-ROC I HTD / H-3

[202]

EBERLINE ANAL.YTICAL COPPOFU\TIOf\l 601 SCMBORO F~OAD Ot,t, RIDGE. TENNESSEE Yi830 E!~VIC:E:'.3 F'HO~IE (865) L+81 0685 FAX (865) 485--l,621 EBS-OR-43651 April 30, 2018 Patricia Giza Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099 CASE NARRATIVE Work Order# 18-04023-0R SAMPLE RECEIPT This work order contains seventeen solid samples received 04/05/2018. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.

CLIENT ID LAB ID CLIENT ID LAB ID B 1051 OOAFSFC239CV 18-04023-04 B 1051 OOAFSFC3 l 6CV 18-04023-13 B 1051 OOAFSFC250CV 18-04023-05 B 1051 OOAFSFC32 l CV 18-04023-14 B 1051 OOAFSFC255CV 18-04023-06 B 1051 OOAFSFC326CV 18-04023-15 B 1051 OOAFSFC263CV 18-04023-07 B 1051 OOAFSFC329CV 18-04023-16 B 1051 OOAFSFC276CV 18-04023-08 B 1051 OOAFSFC332CV 18-04023-17 B 1051 OOAFSFC282CV 18-04023-09 B 1051 OOAFSFC345CV 18-04023-18 B 1051 OOAFSFC289CV 18-04023-10 B 1051 OOAFSFC347CV 18-04023-19 B 1051 OOAFSFC293CV 18-04023-1 1 B 1051 OOAFSFC348CV 18-04023-20 B 1051 OOAFSFC300CV 18-04023-12 ANALYTICAL METHODS Total Strontium was analyzed using EIChroM Method SRWOl Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.

Gamma Spectroscopy was performed using EPA Method 901.1 Modified.

Laboratory qualifiers are as follows:

U - Result is less than the MDA.

ANALYTICAL RES UL TS Combined Standard Unce11ainty is rep011ed at I-sigma value.

Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific.

MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.

Page 1 of 3

[203]

ANALYTICAL RES UL TS CONTINUED TOT AL STRONTIUM Samples were prepared by acid digestion as appropriate for the matrix. Digested samples were acidified and were selectively extracted and precipitated. Precipitates were then mounted on 47mm filters. Filter was reweighed to determine aliquot size. Sample activities were determined by gas flow proportional counting.

Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are rep01ied from Total Strontium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.

TRITIUM A representative aliquot of each sample was equilibrated with tntmm free water. Equilibrates were transfe1Ted into a round-bottomed distillation flask and attached to a single stage still. A portion of each middle distillation fraction was transfe1Ted to a liquid scintillation vial and cocktail was added. Samples were then counted by beta liquid scintillation.

Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique.

Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.

NICKEL-63 A representative aliquot of each sample was placed into an appropriately sized beaker. Stable elemental Nickel ca!Tier was added to each sample prior to digestion. Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.

Samples demonstrated acceptable results for all Nickel-63 analyses. Results for the method blank and laboratory fractions -03, -04, -06, -I 0, -15, -16 and -19 (Client ID: B 1051 OOAFSFC239CV DUP & DO, B 105100AFSFC255CV, B1051 OOAFSFC289CV, B1051 OOAFSFC326CV, Bl05100AFSFC329CV and B 1051OOAFSFC347CV) demonstrated slightly high method detection limits. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.

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[204]

ANALYTICAL RESULTS CONTINUED GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass/aliquot of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.

Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. Cobalt-60 and Cesium-13 7 results demonstrated slightly high method detection limits. Some samples demonstrated results that are greater than the method detection limit. These results are reported from the Canberra Gamma Apex "Nuclide MDA Report" and are not positive. These results are qualified as non-detect (U).

The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Bismuth-214 replicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Thorium-234 and Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.

CERTIFICATION OF ACCURACY I ce11ify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her C~designee to be accurate a ~ verified s by the following signature.

" **------ ~---

M.R Mc;;;;~,_,

Laboratory Manager Date: 4/30/2018 Eberline Analytical wants an \ cnc<)liragcs your l'cedback regarding our performance providing radioanalytical services. Please visit htlp://eberlineanalytical.corhfio provide us with feedback on our services.

Page 3 of 3

[205]

Printed: 4/30/2018 3:19 PM Page 1 of 22 Report To* Work Order Details:

Patricia Giza 18-04023 Eberline Analytical ., Zion.Solutions,LLC Purchase Order:

SDG:

f-i I /118 Final Report of Analysis '

101 Shiloh Blvd Analvsis r 1...1~'v11"',\,,flIIVICN -AL Zion, IL 60099 Sample Matrix: so I

Lab ID Sample Type i Client ID Sample Date Receipt Date .

Analysis Date .

Batch ID i Analyte Method Result cu i CSU i MDA  ! Qualifier '. Report Units 18-04023-01 18-04023-01 LCS LCS KNOWN SPIKE 04/05/18 00:00 04/05/18 00:00 4/5/2018 , 4111/2018 18-04023 4/5/2018 ; 4/1112018 \ 18-04023 Tritium Tritium LANL ER-210 Modified LANL ER-210 Modified 2.43E+02 2.17E+02 8.76E+OO 5.63E+OO

' 1.34E+01

.i 3.79E+OO .' '

om oc;fo 18-04023-02 MBL BLANK 04/05/18 00:00 4/fiJ:.>fl1R ; 411112018 ' 18-04023 Tritium LANL ER-210 Modified -7.60E-01 2.15E+OO 2.15E+OO i 3.74E+OO i u ' oCilo 18--04023-03 DUP B105100AFSFC239CV 03/06/18 09:55 4/5/2018 ' 4111/2018 18-04023 Tritium LANL ER-210 Modified -2.76E-01 1.04E+OO  : 1.04E+OO 1.81E+OO u oCilo

-*~--****-****--***

18--04023 04 DO B105100AFSFC239CV 03/06/18 09:55 41512018 I 411112018 18-04023 Tritium LANL ER-210 Modified -5.52E-01 1.04E+OO 1.04E+OO  !

1.81E+OO I u ' oC,to 18-04023-05 TRG B105100AFSFC250CV 03/06/18 09:40 4/5/2018 ' 4/1112018 18 04023 Tritium

._,.. LANL ER 210 0 1.06E+OO ' 1.86E+OO . u pCi/g 18-04023-06 TRG 8105100AFSFC255CV 03/06/1812:46 4/5/2018 ' 4/11/2018

• 18-04023 Tritlum LANL ER-210 Modified  : 9 67P.02 1.11E*OO 1.11E+OO  : 1.90E+OO u  : oCilo 18--04023-07 TRG B105100AFSFC263CV 03/06/18 09:30 41512018 , 411112018 I 18-04023 Tritium LANL ER-210 Modified 1 RSF.01 1.06F>OO 1.06E+OO I 1.82E+OO  : u ' oCilo 18--04023 08 TRG 8105100AFSFC276CV 03/05/1813:42 4/5/2018 4/11/2018 18-04023 Tritium LANL ER-210 Modified 1.33E-01 7.62E-01 7.62E-01 . 1.30E+OO u oCilo 18-04023-09 TRG B105100AFSFC282CV 03/06/18 08:52 41512018 : 411112018 I 18-04023 Tritium LANL ER-210 Modified 2.72E*01 1.56E+OO 1.56E+OO I 2.68E+OO i u oc,10 ...*.

"'"'"*-* "'"'-"* ****~*-*~-***

• - *- TRG B105100AFSFC289CV 03/05/18 13:52 41512018 , 411112018 I 18-04023 Tritium LANL ER-210 Modified *177E*01 1.01E>OO 1.01E+OO i 1.74E+OO i u oCilo

• - 11 TRG B105100AFSFC293CV 02/07/1813:45 4/5/2018 ' 4/11/2018 : 18-04023 Tritium LANL ER-210 Modified 3.12E-01 1.79E+OO 1.79E+OO i 3.07E+OO i u . oCilo

<O TRG B105100AFSFC300CV 02/13/18 12:50 4/5/2018 : 4111/2018 I 1R-04nn Tritiom LANL ER-210 MoctifiP.ct 2.26E+OO 1.91E+OO 1.91E+OO I 3.18E+OO I u  : oCilo

,o <O TRG B105100AFSFC316CV 03/05/1813:58 4/512018 I 411112018 : 18-04023 Tritium LANL ER-210 Modified -6.66E-01 1 SSF;OO , SSF;OO I 3.27E+OO i u oCilo

<O

" TRG B105100AFSFC321CV 02/13/1814:10 ~  : 4/11/2018 18-04023 Tritium LANL ER-210 Modified -5.64E-01 2.13E+OO 2.13E+OO i 3.70E+OO  : u m °

'" TRG B105100AFSFC326CV 02/14/1808:15 j 4/11/2018 18-04023 Tritium LANL ER 210 Modified j 8.3~~-~1 1.93E+OO 1.93E+OO . 3.28E+OO  :

u pCi/g

,o

• - TRG B105100AFSFC329CV 03/05/18 14:18 4/5/2018_,_j -~/12/2018 18*04023 Trttium LANL ER 210 -2.75E 01 l 1. E+OO 2.71E+OO i u  : PCilo

• - *- TRG  : B105100AFSFC332CV 03/05118 14:05 4/5/2018 i 4/12/2018 18-04023 Tritium LANL ER-210 Modified

-4.85E-01 1.84E+OO 1.84E+OO ' 3.18E>OO i u oCilo

<O 1KG 8105100AFSFC345CV 02/07/1810:45 4/5/2018 ' 4/12/2018 _ 1R-n4nn Tritiom LANL ER-210 Modified 1.74E*01 1 99F>OO 1.99E+OO I 3.42E+OO  : u oCi/o

,o

",, TRG B105100AFSFC347CV 02/12/1813:10 4/5/2018 : 4/12/2018 : 1!:l-lJ4l),!;;! Tritium LANL ER-210 Modified 4'3E>OO

'"H"" 2.23E+OO I 3.61E+OO i oCilo

,o oo TRG  : 8105100AFSFC348CV 02/12/1815:15 4/5/2018 i 4/12/2018 18-04023 Trttium LANL ER 210 Modified 3.67E+OO 1.71E+OO 1.m+<"' : 2.78E+OO i pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE EBERUNE l~NAL YTtCAl CORPrn"{A liON

~~ SERV1CES 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[206]

Printed: 4/30/2018 3:19 PM Page 2 of 22 Report To: Work Order Details:

Patricia Giza 18-04023 Eberline Analytical -- -- - --- --- ------"

---

ZionSolutions, LLC***--~-------

n SDG:

, nmor'.- 677118 Final Report of Analysis , __ 101 Shiloh Blvd Analysis Category.:_. ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch  : Report i'  :

Date ID Analyte Method Result cu CSU MDA  ; Qualifier

• Units ID Type ID Date Date 18-04023-01 LCS r

KNOWN 04/05/18 00:00 4/5/2018 4/10/2018 18-04023 Nickel-63 ASTM 3500-Ni Modtfied 1.50E+03 4.51E+01 -r pCUg SPIKF 4/10/?01' 18-04023 Nickel-63 ASTM 3500-Ni Modified 1.52E+03 '. 8.94E+OO

-****--***~***-**-- 2.05E+OO 8.97E+01

• ornr 18-04023-01 LCS 04/05/18 00:00 4/512018 MRI BLANK 04/05/18 00:00 4/5/2018 4/10/2018 18-04023 Nickel-63 ASTM 3500-Ni Modified 4.95E 01  : 1.23E+OO 1.23E+OO , 2.09E+OO , u  : orne

- DUP B105100AFSFC239CV 03/06/18 fl<l*'i"i *;smm 4/1fl/"Jfl1H

"-"'""" Nickel 63 ASTM 3500-Ni Modified 8.54E-02

• 1 1.27E+OO 1.27E+OO 2.17E+OO i u  : ,cv, 18-04023-04 18 04023 05 DO TRG

! B105100AFSFC239CV B105100AFSFC250CV 03/06/18 09:55 03/06/18 09:40 41512018 415/2018 411012018 411012018 18-0402' 18-04023 Nickel-63 Nickel 63 ASTM 3500-Ni Modified ASTM 3500 Ni Modified 515E-o-3_08E-01 1.28E+OO 9.14E-01 1.28E+OO **;

9.15E-01 2.18E+OO 1.55E+OO I u

u

-,' oCT/c 1" -- TRG  :

" 03/06/18 12:46 4/512018 4110/2018 18--04023 Nickel 63 ASTM 3500-Ni Modified -642E-01 1.18E+OO , rnF+OC 2.04E+OO i u i or.;,o 1" -- TRC B105100AFSFC263CV 03/06/18 09:30 4/5/2018 4/10/2018 18--04023 Nickel 63 ASTM 3500-Ni Modified 2.71E-01 8.11E-01 8.11E-01 1.38E+OO u or_;,o 10

'"° 8105100AFSFC276CV 03/05/1813:42 41512018 '~"'" Nickel 63 1.05E+OO 1.05E+OO ' ,oc.oo ' u '

rr""

4/1111")1118 ASTM 3500 Ni Modifiedj**-l----:~tE+~~*-*

18-04023-09 TRG  ! - -- 03/06/18 08:52 41512018 ' 411012018 18-04023 Nickel-63 ASTM 3500-Ni Modified 6.00E 01 'ooc.oc 1.00E+OO 1.69E+OO  : u  ; -r""

1" *- TRG  :

" :v 03/05/18 13:52 41512018 i 4110/2018 18--04023 Nickel-63 ASTM 3500-Ni Modified 2.42E+OO , ?SF+OC 1.26E+OO 2.05E+OO oCT;o

. TRC -1.51E-01 1.12E+OO 1.12E+OO 1.92E+OO , u or_;,o u

" 02/07/1813:45 4/5/2018 : 4/10/2018 18--04023 Nickel 63 ASTM 3500 Ni Modified  :

1" 18-04023-13

• - IHC TRG  :

B105100AFSFC316CV

" 02/13/1812:50 03/05/1813:58 4/5/2018 i 4/10/2018 4/5/2018 . 4/10/2018 18 04023 18--04023 Nickel 63 Nickel-63 ASTM 3500-Ni Mnrlifi<><'

ASTM 3500-Ni u,,nm ..n 2.11E+OO 2.21E 01 1.16E+OO 1.10E+OO 1.17E+OO 1.10E+OO 1.92E+OO 1.87E+OO **:

u  ;

18 04023-14 TRG  : 8105100AFSFC321CV 02/13/1814:10 4/5/2018  ! 4/10/2018 18--04023 ! Nickel 63 ASTM 3500-Ni Modified 1 OOF_01 ' o,c.oc ' o,c.oo ' 1.77E+OO

• u -

18 04023 15 TRG B105100AFSFC326CV 02/14/18 08:15 41512018 4/11/2018 : 18-04023 Nickel 63 ASTM 3500 Ni Modified 4.04E-01 1 ,,c.oc 121F*M

• 2.0SE+OO u """"

18 04023 16 TRG  : u :v 03/05/1814:18 4/5/2018 4/1112018 1R-040?S Nickel-63 ASTM 3500-Nl Modtfied 1.09E+OO 1.27E+OC 1-27E+OO  : 2.13E+OO I u  : """"

18-04023-17 TRG B105100AFSFC332CV 03/05/1814:05 4/5/2018 4/1112018 18-04023 Nickel-63 ASTM 3500-Ni Modtfied 2.62E-01 8_78E-01 9.78E-01 1.66E+OO u oC:,o 18-04023-18 TRG  :

' B105100AFSFC345CV 02/07/1810:45 4/5/2018 4/11/2018 I 18 04023 Nickel 63 ASTM 3500-Ni Modtfied -2.04E-01 ' 1.00E+OO 1.00E+OO a 1.72E+OO i u oC:,r 18-04023-20

• - TRG TRG  :'

B105100AFSFC347CV B105100AFSFC348CV 02/12/1813:10 02/12/18 15:15 4/5/2018 4/5/2018 4/11/2018 4/11/2018 18-04023 18-04023 Nickel 63 Nickel-63 ASTM 3500-Ni Modified ASTM 3500-Ni Modified 3.03E+OO

-3.06E-01

',,c.oo 1.13E+OO 1 OOF*M 1.13E+OO

'o,c.oc 1.94E+OO

--J u

': -r"-

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma ); M DA=Minimal Detected Activity;LCS=Laboratory Control Sam pie; MBL=Blank; DUP=Duplicate;TRG=Nonnal Sample; DO=Duplicate Original; U=Non-detect

-~EBERLINE I EBERLiNE CAL

~ SER 1CE5- ' 601 SCARBORO ROAD OAK RIDG~-TN-37830 865/481-0683 FAX 865/483-4621

[207]

Printed: 413012018 3:19 PM Page 3 of 22 Report To: Worl< Order Details:

Patricia Giza 18-04023 Eberline Analytical I -- -- -~--------------

SDG:

... Zion Solutions,. LLC ------- -- .. --- ----- Purchase Order: 677118 Final Report of Analysis 101 Shiloh Blvd

--- --, ---- ------------------------------ ------- Analysis Category: .

ENVIRONMENTAL Zion, IL 60099 Sample MatnX: 1 so Lab Sample i Client Sample Receipt Analysis i Batch  :

Analyte Method I Result i: cu CSU MDA  : Qualifier:

Report ID i Type ID Date Date Date ID Units 18-04023-01 18 04023 01 LCS LCS '

KNOWN SPIKE 04/05/18 00:00 04/05/18 00:00 4/5/2018 4/5/2018 4/11/2018 4111/2018 18-04023 18 04023 Strontium-90 Strontium 90 EIChroM SRW01 Modified EIChroM SRW01 Modified :

I 5.03E+O~-.

3.93E+01

) __ ::::~~: 1.38E+01 7.85E 01 '

oC,<o

"°""

18-04023-02 MBL BLANK 04/05/18 00:00 4/5/2018 4/11/2018 18-04023 Strontium-90 EIChroM SRW01 MorlifiP.'1 I 2.75E-01 4.97E-01 5.0GE-01 8.56E-01 u o, ""

18-04023-03 DUP ' B105100AFSFC239CV  ;,sncrn 41"""" 18-04023 Strontiurn-90 EIChroM .c::Rwn1 Mnrlifi,:,~ 5.52E 01 4.74E-01 5.11E-01 7.BOE-01 u arno

.,,,,, "s u arna 18-04023-04 DO  : B105100AFSFC239CV 4/1"-'" '~"'" Strootium-90 EIChroM SRW01 Modified 9.07E 02 3.77E 01 3.79E-01 6.90E-01 18 04023 05 TRG B105100AFSFC250CV 4/5/2018 4/11/2018 18.04023 Strontium-90 EIChroM SRW01 Modified ,1.90E*01 i1,F'.01 3.19E-01 5.83E-01 u """"

18-04023-06 TRG B105100AFSFC255CV 03/06/181NS 4/5/2018 4/11/2018 rn.c,cn Strontium-90 EIChroM SRW01 MorlifiP.rl 1.18E,01 SSSF.C, 3.71E-01 6.47E-01 u oc.,o 18-04023-07 TRG B105100AFSFC263CV 03/06/18 <N<~n 4/5/2018 4/11/2018 18-04023 Strontium-90 EIChroM SRW01 Modified 1.29E-01 * ,SOF.M 2.73E-01 4.66E-01 u oC.;,o 18 04023--08 TRG B105100AFSFC276CV 03/05/18 1'bl.? 4/5/2018 4/11/2018 18 04023 Strontium-90 EIChroM SRW01 Mmirfi,,.rl 4.44E 01 3.45E 01 3.78E*01 5.60E-01 u oC,<o 1 TRG B105100AFSFC282CV 03/06/18 08:52 4/5/2018 4/11/2018 18-04023 Slrontium-90 EIChroM SRW01 Modified 3.22E-01 3.22E-01 3.41E-01 5.36E-01 u """"

-***--* u 18-04023 10 TRG B105100AFSFC289CV 03/05/1813:52 4023 Strontium 90 EIChroM SRW01 Modified 2.74E-01 4.16E 01 4.27E 01 7.11E 01 * """"

'. 18--04023-11

,.. ______________ TRG i 8105100AFSFC293CV 02/07/1813:45 4/5/2018 4/11/2018 rn.c,cn Strontium-90 EIChroM SRW01 Morlifierl -1.22E-01 3.39E-01 3.42E-01 6.25E-01 u . oc.,o 18-04023-12 TRG B105100AFSFC300CV 02/13/1812:50 4/5/2018 4/11/2018 18-04023 Strontium-90 EIChroM SRW01 Mnrlifi,:,rl 2.14E*01 3.34E-01 3.42E-01 5.71E-01 u ac,a 18-04023-13 TRG B105100AFSFC316CV 03/05/18 13:58 4/5/2018 4/11/2018 ; 18-04023 Strontium 90 EIChroM SRW01 Modified '.90E,01 4.36E-01 4.48E 01 7.45E-01 u u

18-04023-14 TRG B105100AFSFC321CV 02/13/1814:10 4/5/2018 4/11/2018 18-04023 Strontium 90 EIChroM SRW01 Modified 2.76E-01 3.29E 01 3.43E 01 5.55E 01 """"

" " TRG B105100AFSFC326CV 02/14/18 08:15 4/5/2018 4/11/2018 18-04023 Strontium 90 EIChroM SRW01 Modifieri 7.69E-01 4.72E,01 5.43E 01 7.47E 01 "'°

" " TRG B105100AFSFC329CV 03/05/1814:18 4/5/2018 4/11/2018 18 04023 Strontium-90 EIChroM SRW01 Modified 8.94E 01 5.55E 01 6.36E-01 8.BOE-01 03/05/1814:05 4/5/2018 4/11/2018 Strontium-90 EIChroM SRW01 ModifiP.C 2.15E*01 3.26E*01 3.34E-01 i 5.57E-01 . u  ! "'° 18-04023 17 18-04023-18 TRG B105100AFSFC345CV 02/07/18 10:45 4/5/2018 4/11/2018 18--04023 . Strontium-90 EIChroM SRW01 MnrlifieC 7'SF.n? 3.83E-01 3.84E-01 6.73E-01 u TRG .

"°""

18-04023-19 TRG 8105100AFSFC347CV 02/1211813:10 4/5/2018 4/11/2018 , 18--04023 i Strontium 90 EIChroM SRW01 MnrlifiPr 2.BOE-01 3.97E-01 4.09E 01 6.77E-01 . u . ac.;,a 18 04023 20 TRG .' B105100AFSFC348CV 02/12/1815:15 """11' 4/11/2018 . 18-04023 i StronUum-90 EIChroM SRW01 Modified ; 5.41E-01 3.60E-01 4.06E-01 5.75E-01 ! u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-cletect

~

1 EBERLINE 601 SCARBORO YTIC/1,L ROAD OAK RIDGE, TN 37830 ON 865/481-0683 FAX 865/483-4621

[208]

Printed: 4/3012018 3:19 PM Page 4 of 22 Report To: Work Order Details:

Patricia Giza ,,, SOG: 18-04023 Eberline Analytical ---"

• • • • • • • - Zion_ Solutions, LLC ____

Purchase Order: 677118 ee Final Report of Analysis 101 Shiloh Blvd Onolvolo ENVIRONMENTAL Zion, IL 60099 Sample Matrix:* sn I Sample Client Sample Receipt Analysis Batch I . Report Lab ID I Type ID Date I Date I

Date ID l Analyte Method Result cu CSU MDA ( Qualifier Units 18-04023-01

' LCS KNOWN 04/05/18 00:00 4/5/2018 4/5/2018 18-04023 I Cobalt-60 EPA901.1 Modffied I 2.71E+02 1.06E+D1 I . om, 18-04023'01 LCS KNOWN 04/05/18 00:00 4/5/2018 4/5/2018 I 18-0402'.l Cesium-137 EPA901.1 Modffied 1.69E+02 eise;oo . rrv, ICS SPIKE 04/05/18 00:00 4/5/2018 4/5/2018 ; 18-04023 Cobalt-60 EP 1.54E+01 2.07E+01 2.31E+OO oClk e

18-04023--01 LCS SPIKE 04/05/18 00:00 4/5/2018 - 4/5/2018 : rn.ndn?'< EPA901.1 Modrfied 1.91E+02 2-29E+01

• 2.49E+01 2.52E+OO oCi/c e """*-*-*'"* I 18-04023-02 MBI BLANK 04/05/18 00:00 4/5/2018 4/5/2018 18 04023 Actinium-228 EPA901.1 Modrfied e eo0,00

• 14ie:01 1-48E-01 I 2.22E 01 IJ rrVr 4/5/2018 "18-04023 Silver-108m EPA901.1 Modified 1.19E-02 OOOC M 2.85E 02 I 4.55E 02 u rrVr 18 04023-02 MBL BLANK 04/05/18 00:00 4/5/2018 I

1S-04023-02 MBL BLANK 04/05/18 00:00 4/5/2018 4/5/2018 18-04023 Americium-241 EPA 901.1 MorlifiP.rl -4, 1BE-02 4.78E-02 4.79E-02 6.51E-02 u orno 18--04023-02 MBL BLANK 04/05/18 00:00 4/5/2018 4/5/2018 18-04023 Barium-133 EPA901.1 MnrlifiPrl 7 OR0,07 5.17E 02 5.17E 02 6.58E-02 u or.""

---

****-w* **---**--~*-* --- -- *-------- u 18-04023 02 MBL BLANK 04/05/18 00:00 4/5/2018 ! 4/5/2018 18-04023 Bismuth-214 EPA901.1 MnrlifiPrl  : 1.58E-02 9.20E-02 9.20E 02 1.39E-01 or.""

,r re 4/51201' . 4/5/2018 18-04023 Cobalt-60 EPA901.1 Modified 2.12E-02 3.SOE-02 3.50E 02 6.50E-02 u orno MBL BLANK 04/05/18 00:00

,r re 04/05/18 OO*OO ' O.OOE+OO 4.53E-02 4.53E-02 6.21E02 u rrVr MBL MBL BLANK BLANK 04/05/18 00:00 4/5/2018 4/5/2018 I

4/5/2018 4

18 04023 m 137

--EPA901.1 Modified EPA901.1 Modified e

2.03E 02 4.54E 02 4.54E-02 7 47F-07 u orno

• --* - EPA901.1 Modified -2.65E 02 1.34E 01 1.34E-01 1.05E-01 u -r"r o,

MBL MBL '

BLANK BLANK 04/05/18 00:00 04/05/18 00:00 4/5/2018 ; 4 4/0'701R , 4/5/2018 , 1',04C77 2

EPA901.1 Modified 7.96E 02 8.09E 02 8.10E-02 OSOC M u

' orno

' 04/05/18 nn-nn 4/5/2018 ' 1R.ndn?'l C, EPA901.1 Modified 7 .OSF-07 S C00.07 3.09E-02 6.36E-02 u or.""

18-04023-02 18-04023-02 MBL MBL BLANK BLANK 04/05/18 00:00

"""°

4/5/2018 ' at<-,/'Jll1R 1'-°'"" EPA901.1 MnrlifiPrl e4 S,F,07 9.72E-02 9.72E 02 3.95E-02 u or.""

18--04023-02 MBL BLANK 04/05/18 00:00 41512018 I 41512018 18-0402' lodloe-129 EPA 901.1 Modified 2.36E-03 1.95E-02 1.95E-02 '

2.93E-02 u  : rr,,r 18 04023 02 MBL BLANK 04/05/18 00:00 41512018 4/5/2018 1R-04077 Potassium-40 EPA 901.1 Modrfied 3,700.M '<00 01 3.18E 01 I

6.21E-01 u I rrl,r 18-04023--02 MBL BLANK 04/05/18 00:00 4/512018 4/5/2018 18 04023 Manganese-54 EPA901.1 Modified -8.37E-03 3.91E-02 7R1F-02 6.37E 02 u ' rCS,r

,mo

'" MBL BLANK 04/05/18 00:00 4/5/2018 4/5/2018 18 04023 Niobium-94 EPA901.1 MnrlifiPrl 1 04F,07 3.63E-02 3.63E 02 6.58E-02 u 18-04023-02 MBI BLANK 04/05/18 00:00 4/5/2018 4/5/2018 18-04023 '**"-'10 EPA901.1 Modified 4.50E 01 3.56E 01 3.56E-01 0 070,0, u rr,,,

4/5/2018 18-0407' Lead-212 EPA 901.1 Modified 6.26E~02 4.00E 02 , 4.01E-02 6.04E-02 rrna 18-04023-02 MBL BLANK 04/05/18 00:00 4/5/2018 18-04023-02 MBL BLANK 4/512018 4/5/2018 18-0407' Lead 214 EPA 901.1 Modified 9.67F-02 S SRF'"17 j 5.99E-02 1.15E-01 u oCi/o 18-04023-02 MBL BLANK 4/"il'if)1!j 4/5/2018 rn.M077 EPA901.1 Modified  : ,VOF-07 7 OFF-07 3.36E-02 5.04E-02 u orno e

1 SRF,07 0700,07 1 ORF,01

' u orno 18-04023 02 MBL .' BLANK 4/5/2018 i 4/5/2018 18 04023 Radium-226 EPA901.1 Mnrlifo*rl I 9.20E 02 18-04023-02 MBL i RIANK 41512018 ' 4/5/2018 : 18-04023 EPA901.1 Modified -,A3E-02 104E-01 1.04E 01 . ',oo.o, u orno 18-04023-02

,-- -- MBL BLANK 4/5/2018 I 4/5/2018 18--04023 EPA901.1 Modified I 5.84E-01 S '7F-01 5.33E 01 . ,a0e:o; u rrna M

MBL BLANK 04/05/18 00:00 4/5/2018 4/5/2018 18-04023

" EPA901.1 Modified -3.62E-02 1.42E 01 I 1.42E 01 m:Oi '

u rr;,a

'" rr MBL BLANK 04/05/18 00:00 4/5/2018 4/5/2018 1S-04023 Uranium-235 EPA901.1 Modrfied -2.HE-02 3.69E 01  ! 3.69E-01 2.26E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minirnal Detected Actlvity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect I ,

I CAL

! 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[209]

Printed: 4/30/2018 3:19 PM Page 5 of 22 Report To: Work Order Details*

Patricia Giza 18-04023 Eberline Analytical ****-* Zion Solutions, LLC -

SDG:

,nmer R77118 Final Report of Analysis

~--OMMoM****-**********----~*-"-******M*-MMM-MMMM * * -

• M - M - - - - - M - M M 101 Shiloh Blvd

. . ., ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so I i Lab Sample Client Sample I Receipt Analysis Batch

' cu

. i Report I Method Result I CSU MDA Quahfier:

I I Analyte fD Type fD Date i Date Date fD i Units 18"04023-03 DUP B105100AFSFC239CV 03/06/18 09:55 4/5/2018 4/5/2018 18-04023 Actinium-228 EPA 901-1 Modified 4.79E-01 1.S9E 01 1.91E 01 2.24E 01 oCilc

.. '"" DUP i

I B105100AFSFC239CV 031 4/5/2018 18--04023 Silver 108m EPA901.1 Modified -2.52E 02 - 6.75E 02 6.75E-02 7.03E-02 u *""* ..

. OlfP 8105100AFSFC239CV 03/06/18 09:55 4/512018 4/5/2018 18-04023 EPA901_1 Modified -2.66E-01 1.39E 01 1.39E 01 1.30E 01 u pCi/1

• -.. ... DUP B105100AFSFC239CV 03/06/18 09:55 i 4/512018  ;,sno,e 1R.O.OOS Barium-133 EPA 901.1 Modified 1.97E-02 3.65E-02  ; 3.65E-02 1.44E 01 u pCi/g

'"" DUP 8105100AFSFC239CV 03/06/18 o*iss**--; 4/5/2018 ""'"'18 1"-"'""' EPA 901.1 Modified 6.81E 01 1.56E---01 1.60E-01 1.96E-01 .

,rn, 18-04023-03 DUP B105100AFSFC239CV 03/06/18 09:55 4/5/2018 _ 4/5/2018 18-04023 Cobalt-60 EPA901.1 Modified 1.50E-02 3.28E-02 3.29E 02 "i,c_o, I u oCilo 18---04023-03 DUP B105100AFSFC239CV 03/06/18 09:55 4/5/2018 ; 41512018 1'-0407' Cesi.,m-134 EPA901.1 Modified 2.34E-02 3.79E-02 3.80E-02 o ooo no . u *""*

18---04023-03 DUP B105100AFSFC239CV 03/06/18 09:55 4/5/2018 I 4/fi/?018 1'-040,S I _,,, EPA901.1 Modified -1.16E-02 6.66E 02 6.66E 02 0 S1F-O? . u m "'° 18---04023 03 DUP B105100AFSFC239CV 03/06/18 09:55 _. 4/5/2018 i ,11,;1?n1a

• 1.ct_n,1n-:><l EPA901.1 Modified 7.94E 02 1.18E-01 1.18E-01 1.94E-01 u nrnc B10510DAFSFC239CV 03/06/18 09:55 415/2018 4151201' 18-0402' EPA901.1 Mnrliti<><' -1 ,sc_o, 1.38E 01 1.38E 01 I

9.51E-02 I u ,rn, 18-04023--03 DUP 18-04023--03 DUP 8105100AFSFC239CV 03/06/18 09:55 4/5/2018 4/5/2018 18-04023 EPA901.1 Mn,m, .. n 3.56E 02 1.06E-01 1.06E-01 1_74E-01 . u *""*

18-04023--03 DUP B105100AFSFC239CV 03/06/18 09:55 415/2018 4/5/2018 11\-040'3

' EPA 901.1 Modified . 2.56E-02 8.26E 02 8.26E 02 8.22E 02 u *""*

18-04023-03 DUP 8105100AFSFC239CV 03/06/18 09:55 4/5/2018 4/5/2018 ;18-040?::\ lodine-129 EPA 901-1 Modified 2.34E-02 7.14E-02 7.14E-02 9.83E-02 u nCilc 18-04023-03 DUP B105100AFSFC239CV 03/06/18 fl<l*'i',

""'"" 4/5/2018 18-04023 Potassium-40 EPA 901.1 Modified . 4.86E+OO 1.11E+OO 1.14E+OO ! 9.17E 01 nc.i,,

---

DUP B105100AFSFC239CV 03/06/18 09:55 .:1/'ir.lfl11' I .d/',/")ll1K ,R.0400, -

EPA 901.1 Modified ' 8.61E-03 5.98E-02 5.98E 02 8.67E 02 u u

oCl/o DUP I B105100AFSFC239CV 03/06/18 09:55 4/5/2018 4/5/2018 18 04023 Niobium-94 EPA 901. 1 Modified 1.02E-03 3.17E-02 3.17E-02 6.65E 02 18--04023-03 DUP i B105100AFSFC239CV 03106/18 09:55 4/5/2018 4/5/2018 18-04023 Lead-210 EPA 901.1 Modified 1.32E+OO 8.84E-01 8.87E-01 1.34E+OO u pCi/g 18-04023-03 DUP 8105100AFSFC239CV 03/06/18 09:55 4/5/2018 4/5/2018 18-04023 Lead 212 EPA901.1 Modified 3.39E 01 1.13E-01 1.15E-01 2.38E-01 *"""

18-04023-03 DUP 8105100AFSFC239CV 03/06/18 nfr!'i.701R 415/2018 '"-°'° *- EPA901.1 Modffied -3.19E-02 , OOF-01 1.00E 01 1.27E 01 u 4'S,701R 18-04023-03

---.- DUP B105100AFSFC239CV 03/06/18 09:55 41512018 "-°'° EPA901.1 Modified 6.81E 01 1.56E-01 1.60E-01 1.96E--01 18-04023-03 DUP B105100AFSFC239CV 03/06/18 09:55 41512018 4/5/2018  : HLMn?~ EPA901.1 MnrlifiPrl -4.70E-02 1.47E-01 1.47E-01 7.17E--01 ' u PCilo 18-04023-03 DUP B105100AFSFC239CV 03/06/18 09:55 4/5/2018 4/5/2018 , 18-04023 EPA901.1 Modified 2.68E+OO 1.07E+OO 1 osc,oe , 1.67E+OO  ; u oCilo

.. ,rn, 18-04023-03 DUP B105100AFSFC239CV 03/06/18 09:55 415/2018 4/5/2018 18-04023

" EPA901.1 Modified

"*--*---*--***"'~*-*

1.87E 01 1.33E-01 i 1.33E-01 2.52E 01 i u '

18 04023--03 I DUP B105100AFSFC239CV 03/06/18 09:55 415/2018 , 4/5/2018 18-04023 Uranium 235 EPA901.1 Modified -1.78E-01 5.87E 01 SR7F-01 . 3.99E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE

~ SERVICES FAX 865/483-4621

[210]

Printed: 4/30/2018 3:19 PM Page 6 of 22 Report To* Work Order Details:

,., .. Patricia Giza SDG: ,

18-04023 Eberline Analytical ' ---**"~*- "---

................Zion Solutions, LLC Purchase Order:

• 6i711s**

--**-***~"----*-***-*--*--*

Final Report of Analysis 101 Shiloh Blvd ---- Analysis Category. ,. ENVIRONMENTAL

---

~"**-**** - -* -**

Zion, IL 60099 Sample Matrix: so Sample Analysis Batch  ! Report i

Lab Client Sample Receipt ID Type I ID Date Date I Date I

I ID Analyte Method Result '

I cu CSU MDA I

Qualifier Units I *

" " DO 8105100AFSFC239CV 03/06/18 09:55 4/5/2018 4/5/2018 18-04023 Actlnlum-228 EPA901.1 Modified 3.57E-01 1.73E-01 1.74E-01 4.87E 01 u rr,:r 18 04023 04 DO

. 8105100AFSFC239CV

---

*03/06/18*--------*

09:55 4/5/2018 3 Silver-108m EPA901.1 Modified -5.47E-02 5.40E-02 5.41E-02 - 6.67E 02 u . rC"r DO . 03/06/18 4/5/2018 i 18 04023 EPA901.1 Modified 9.34E 02 1.26E 01 1.26E-01 1.43E-01 u  : rrnr 18-04023-04 B105100AFSFC239CV nQ*'iC

""'"" u

<O 0

' 0 DO B105100AFSFC239CV 03/06/18 nQ*<,~

" " " J1S 4/5/2018 18 04023 Barium-133 EPA 901-1 Modified 3.35E--D2 1.34E-01 1.34E-01 1.40E-01

' rC"r rC,:r

<O

' 0 DO l 0 03/06/18 09:55 41512018 4151201' 18 04023 Bismuth 214 EPA901.1 Modified 4.14E 01 1.47E01 1.49E-01 2.22E-01 18--04023 04 DO B105100AFSFC239CV 03/06/18 09:55 41512018 41512018 , 18-04023 Cobalt 60 EPA 901.1 Modified 1.68E-02 5.26E-02 5.26E 02 7.33E-02 u rC"r 18--04023 04 DO . B105100AFSFC239CV 03/06/18 09:55 4/5/2018 4/5/2018

• 1.1<.n,mn EPA901.1 Modified '

• 4.80E*04 3.10E-02 3.10E 02 9.19E 02 u """"

18----04023 04 DO 8105100AFSFC239CV 03/06/18 !Wl*">'i 4/5/2018 4/5/2018 18,04023 EPA 901.1 Modified 2.04E*02 5.38E-02 5.38E 02 9.06E 02 u "°""

DO  ; 4/5/2018 /0.MMO " EPA901.1 Modified 1.44E-02 1.33E-01 1.33E-01 , soc.a, i u rrnr 18-04023-04 B105100AFSFC239CV

<O r DO . 8105100AFSFC239CV 03/06/18 09:55 41512018 4151201 10.0,01, " EPA901.1 Modified 1.04E-01 1.05E-01 1.0SE 01 9.55E 02 . u ornr

<O r DO  ! B105100AFSFC239CV 03/06/18 09:5.!S 41512018 4/5/2018 1 11=1 n,1,vn " EPA901.1 Modified 9.32E-03 8.65E-02 -"i 8.65E 02 1.65E 01

• u  : rC"o

" r DO  : B105100AFSFC239CV 03/06/18 09:5.!S 4/512018 4/5/2018 18*04023 Holmlum-166m EPA901.1 Modtfied 6.01E 02 9.21E-02 9.22E-02 7.55E-02 u rr>:o

. - DO ' 8105100AFSFC239CV 03/06/18 og-c;_~ 41512018 4/5/2018 rn.o,cn lodine-129 EPA901.1 Modtfied 9.68E 03 6.39E 02 6.39E-02 8.69E-02 u """"

18 04023 04 DO 81051DOAFSFC239CV 03/06/18 nq*'iF 4/512018 , 4/5/2018 18-04023 Potassiurn-40 EPA901.1 Modified 4.31 E+OO 1.08E+OO 1.10E+OO 1.03E+OO *""-

18-04023-04 DO 8105100AFSFC239CV 03/06/18 l)Q*'i.~ 415/2018 4/5/2018 ,s.o,on * - EPA901.1 Modified 3.01E-02 S.94E*02 5.94E 02 , 9.69E 02 u  : or..lo

<O .r DO

' B105100AFSFC239CV 03/06/18 09:55 4/5/2018 4/5/2018 18,04023 EPA901.1 Modified 3.21E-03 2.36E-02 1 ,oc_o, 7.45E-02 u rC,:r

<O .r DO ' 0 /CV ' 03/06/18 09:55 4/5/2018 41512018 18-04023 lead 210 EPA901.1 Modified

• '2.39E

""*"" ;o;c;"" 1.01E+OO 1.64E+OO u rr,:r 18-04023--04 18 04023 04 no DO B105100AFSFC239CV 8105100AFSFC239CV 03/06/18 09:55 03/06/18 09:55 4/5/2018 1 4/5/2018 41512018 4/5/2018 18-04023

,s.o;o,s Lead 212 Lead-214 EPA901.1 Modified EPA 901.1 Modified '

01 5.15E-01 1 fi4F.01 9.48E-02 1.56E-01 2.25E-01 2.51E 01 rr"r 18-04023-04 DO B105100AFSFC239CV 03/06118 OO*SS 4/5/2018 4/5/2018 ,s.o.on Promethlum-145 EPA 901.1 Modified 6.97E-03 o e,c.o, 0 R?F.O, 1.19E-01 ; u oColo

~ - ' EPA901.1 Modified 4.14E-01 1.47E 01 1.49E*01 2.22E*01  ; rC"r 18-04023-04 DO 8105100AFSFC239CV 03106118 09>55 4/5/2018 41512018

'"*°'""

18-04023--04 DO B105100AFSFC239CV , 03106118 09*55 4/5/2018 4/5/2018 c 11'\.(l,1(1'?"'.l EPA901.1 Mnrlift<>rl 8.24E-02 1.30E 01 1.30E-01 1.19E*01 f u rC"r

• ">**~----~-- *-*-~ ,.. u 18 04023--04 DO B105100AFSFC239CV 03/06/18 09:55 41512018 41512018 18*04023 EPA901.1 Modified 2.90E+OO 1.08E+OO 1.09E+OO -

' "*""  ; rr"r rrnr 18-04023--04 DO B105100AFSFC239CV 03/06/18 09:55 41512018 4/512018 10.040,S EPA901.1 Modified 2.64E-01 1,0F.01 1.41E-01 . 2.52E 01 18-04023--04 DO  : B1D5100AF8FC239CV 03/06/18 09:55 4/5/2018 , 4/5/2018 18-04023 Uranium 235 EPA901.1 Modlfied 5.03E-02  : 0.20E*01 6.20E-01 3.96E-01 i u pCi/g CU::Counting Uncertainty;CSU::Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sam ple;MBL::Blank;DU P=Dupllcate; TRG=Nonnal Sample; DO=Duplicate Original; U=Non-detect NE LYT!CAL CORPORt\TlON 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[211]

Printed: 4/30/2018 3:19 PM Page 7 of 22 Report To* Work Order Details:

Patricia Giza 18-04023 Eberline Analytical ' ' "' *-"---**-"*

Zion Solutions, LLC

- - - - - - ------ Purchase SDG*

nrrl,:,r I

677118

---**'"- .. ,..--~-"-~

Final Report of Analysis 101 Shiloh Blvd Analysis Category: r----- ENVIRONMENTAL Zion, IL 60099 Sample Matrix: . so Lab I Sample Client Sample Receipt i Analysis Batch I Report

! Analyte Method Result I cu CSU MDA Qualifier; Units ID Type ID Date Date Date ID I 18-04023-05 TRG . B 105100AFSFC250CV 03/06/18 09:40 4/5/2018 4/5/2018 ' 18-04023 Aclinium-228 EPA901.1 Modffied

' 6.13E-01 3.67E-01 3.68E-01 6.68E 01 u .. "°""

18-04023-05 TRG B10510DAFSFC250CV 03106/18 09:40 4/S/?018 4/5/2018 18-04023 Silver-108m EPA 901.1 Modlfied 4.78E-02 8.36E-02 8.37E-02 1.15E-01 u oc,10

, "' TRG 81051 OOAFSFC250CV 03/06/18 09:40 4/5/2018 4/5/2018 18-04023 Americium 241 EPA 901.1 Modrfied 1.06E-01 1.73E-01 1.73E 01 2.45E 01 u orno 18-04023-05 TRG B105100AFSFC250CV 03106/18 09:40 4/5/2018 4/5/2018 '"-'"" EPA901.1 Modified 2.73E 02 , , "-"' 7.27E-02 1.58E-01 u erne a;o~o(h-214 2.4ie-61 o,7c_o, er""

18 04023 05 TRG 8105100AFSFC250CV 03/06/18 09:40 4/5/2018 4/5/2018 '"-'""" EPA 901-1 Modified 6.35E-01 4.02E-01 18-04023-05 TRG B105100AFSFC250CV 03/06/18 09:40 4/5/2018 41512018 18--04023 Cobalt-60 EPA 901.1 Modified 1.38E 01

• 1 1:i1"E~01  ; iie:01 1.91E-01 u i "r""

18 04023 05 TRG 8105100AFSFC250CV 4/5/2018 4/5/2018 18-04023 Cesium 134 EPA 901.1 Modified -4.33E-02 5.17E 02 5.17E 02 -,,,e:a, u er""

18-04023-05 TRG B105100AFSFC250CV 415/2018 4/5/2018 18-04023 Cesium-137 EPA 901.1 Modified 7.02E-01 1.63E-01 1.67E-01 ?SOF-01 I oc.,10

• - , eo TRG . B105100AFSFC250CV 03/06/18 09:40 4/5/2018 4/5/2018 18 04023 EPA901.1 Modified 1.50E 01 2.43E-01 2.43E-01 3.30E-01 ' u .

or;,o

• -

• eo TRG B105100AFSFC250CV 03/06/18 09140 4/5/2018 4/5/2018 18-04023 EPA901.1 Modified 3.79E-02 2.60E-01 2.60E 01 1.65E 01 u "r""

18 04023-05 TRG 8105100AFSFC250CV 03/06/18 09140 4/5/2018 ' 4/5/2018 18-04023 EPA901.1 Modified 2.38E-01 1.87E-01 1.88E-01 2.80E 01 u """"

' 18-04023 i Holmium-166m  ; iieioi  ; ,ieiai u

18-04023-05 TRG B105100AFSFC250CV 03/06/18 09 4C 4/5/2018 4/5/2018 EPA901.1 Modified 4.89E 03 1.35E 01 .

18-04023-05 TRG B105100AFSFC250CV 03/06/18 0914C 4/5/2018 415/2018 18--04023 lodine-129 EPA901.1 Modified 7.04E-02 1.08E-01 ' OOF 01 1.40E 01 u oC.;Jo 18-04023-05 TRG B105100AFSFC250CV 03/06/18 09*4C 415/2018 4/5/2018 18-04023 Potassium-40 EPA901.1 Modified 6.52E+OO 1.74E+OO 1.77E+OO 1.83E+OO oc,10 18-04023-05 TRG B105100AFSFC250CV 03/06/18 00*4C 4/512018 ; 4/5/2018 18-04023 EPA901.1 Modtfied -5.08E-03 8.16E 02 8.16E-02 1.32E-01 u oCl/o ss,c_o, 1.27E-01 u orno

, ec TRG B1D5100AFSFC250CV 03/06118 09:40 4/5/2018 ; 4/5/2018 '°-°'"°' Niobium-94 EPA901.1 Modified 6.12E 04 8.61E-02 u

'"

• ec TRG B105100AFSFC250CV 03/06/18 09:40 4/5/2018

• 4/5/2018 18-04023 Lead-210 EPA901.1 Modrfied 2.09E+OO 1.42E+OO 1.43E+OO 2.28E+OO

. -- TRG 8105100AFSFC250CV 03/06/18 09:40 4/5/2018 4/5/2018 18--04023 Lead 212 EPA901.1 Modified 5.63E 01 1.70E 01 1.72E-01 2.65E-01

"°""

, '3F-01 ,

18-04023-05 TRG 8105100AFSFC250CV 03/06/18 rnNO 4/5/2018 4/5/2018 1R-040?S Lead-214 EPA901.1 Modified 7.31E 01 2.19F-01 3.22E 01 """"

TRG 8105100AFSFC250CV 03/06/18 00*40 4/5/2018 4/5/2018 18-04023 Promethium 145 EPA901.1 Modified s,,c-o, 1.19E-01 1.19E-01

• 1.92E-01 u i oCl/o 18 04023-05

,s_n,no, 6.35E-01 245E-01 247E-01 4.02E-01 or.;,o 18-04023-05 TRG 03/06/18 09:40 """11' 4/5/2018 EPA 901.1 Modified

• -

• eo TRG B105100AFSFC250CV 03/06/18 09140 4/5/2018 4/5/2018 ' 18-04023 EPA901.1 Modified . 4.81E-02 2.05E 01 2.05E-01 3.63E-D1

• u oCi/c

• - TRG

. B105100AFSFC250CV 03/06/18 09:40 4/512018 4/5/2018 18-04023 Thorium 234 EPA 901.1 Modified 1.91E+OO ' ooc,oo 1.80E+OO 2.61E+OO *; u r """"

18--04023-05 TRG 8105100AFSFC250CV 03/06/18 09:40 4/512018 4/5/2018 18-04023 Thallium-208 EPA 901.1 Modified 5.98E-01 2.73E-01 2.75E-01 4.49E-01

• oCl/n 18--04023 05 TRG B105100AFSFC250CV 03/06118 09:40 41512018 4/5/2018 18-04023 Uranium 235 EPA901.1 Modified -5.53E-01 8.74E 01 8.75E-01 7.58E-01  ! u

• pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

( -~~

EBERLINE SER\/ICES

[212]

865/481-0683 FAX 865/483-4621

Printed: 4/30/2018 3:19 PM Page 8 of 22 Report To* Work Order Details:

Patricia ,..Giza SDG:* 18-04023 Eberline Analytical , ... ----

• • • - Zion Solutions, LLC *-***.

L.

Purchase Order: : 677118 -~--,.-* ----~--------*----*----------------

Final Report of Analysis 101 Shiloh Blvd Analv.sl.s -*--*-*******

ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab ID

Sample '

Type Client ID Sample Date Receipt Date i Analysis '

Date .

Batch ID  : Analyte Method Result l cu CSU MDA i Qualifier j Report Units 18-04023-06 TRG B105100AFSFC255CV 03/06/18 12'46 4/S/?01' 4/S/?018 ' 18-04023 Actinium-228 EPA901.1 Modrfied 5.58E-01 4.66E-01 4.67E-01 9.70E-01 ; u """'

1 18 04023 06 TRG B105100AFSFC255CV 03/06/1812 46 4/5/2018 4/5/2018 : 18--04023 i Sl1ver-108m EPA901.1 Modified 1.21E 02 1.22E-01 1.22E-01 1.99E-01 u """'

18-04023-06 TRG B105100AFSFC255CV 03/06/181246 4/5/2018 4/5/2018 18-04023 Americium-241 EPA901.1 Modified -8.27E-01 2.57E-01 2.60E 01 3.34E-01 u """'******

. ~-----

18-04023-06 TRG B105100AFSFC255CV 03/06/1812:46 4/5/2018 4/5/2018

• 18-04023 Barium-133 EPA 901.1 Modified 2.SBE-03 5.73E-02 5.73E-02 4.08E-01 u ' pCi/g 18 04023---06 TRG 8105100AFSFC255CV 03/06/1812:46 4/5/2018 4/5/2018 ,e.n,nn : Bismuth-214 E

. 8.37E-02 8.37E-02 6.72E-01 u 1.36E-01 1.56E-01 : u 18-04023-06 TRG B105100AFSFC255CV 03/06/18 12:46 03/06/18 12:46 4/5/2018 4/5/2018 4/5/2018 4/5/2018 18*04023 18*04023 C Cobalt-60 EPA 901.1 Modified EPA901.1 Modified 1.17E-01

-2.73E-02 1.36E-01 7.96E 02 ,.02e.01 : u TRG B105100AFSFC255CV 7 ""*"' """"

,o" 3 nc.n, 1 o,c.o, I TRG B105100AFSFC255CV 03/06/18 12:46 4/5/2018 4/5/2018 18*04023 EPA901.1 Modified 1.95E-01 3.03E 01

• pCi/g

-** ***-- *- iiie:o, ,me

'"" "' TRG B105100AFSFC255CV 03/06/18 12:46 4/5/2018 I 4/5/2018 18*04023 Europium-152 EPA901.1 Modified 6.97E 02 4.77E-01 5.36E-01 u 18-04023-06 TRG B105100AFSFC255CV 03/06/18 12:46 4/5/2018 i 4/5/2018 ,e.n4nn EPA901.1 Modified 1.05E*OC '8SF.OC 2.85E 01 2.77E-01 u oC:,o 18-04023-06 TRG B105100AFSFC255CV 03/06/1812:46 4/5/2018 '. 4/5/2018 e 18-04023 EPA 901.1 Modified 8.69E-01 2.79E 01 2.82E 01 4.39E-01 u "' ""

18-04023-06 TRG B105100AFSFC255CV 03/06/1812:46 4/5/2018 4/5/2018 18-04023 Holmium-166m EPA901.1 Modified -9.70E-03 , ,sc.c* , nc.n,

• 2.16E-01 u """"

18 04023-06 TRG B105100AFSFC255CV 03/06/1812:46 ""'°" ' .,,,,cm 18*04023 EPA 901.1 Modrfied .s 80E*01 1 csc.cn 1 CSC,nc 1.48E+OO , u oCi/c 18-04023--06 TRG B105100AFSFC255CV 03/06/18 12:46 4/5/2018 4/5/2018 1'.Mn" EPA901.1 Modffied se,c.cn 1 s,c.cn , m.nc 1.41E+OO """'

' ., nos.co 18 04023 06 TRG 81051 OOAFSFC255CV 03/06/18 12:46 4/5/2018 4/5/2018 18--04023 EPAS01.1 Modrfied ,,.e.02 8.64E 02 2.12E 01 u """'

18-04023-06 TRG B105100AFSFC255CV 1,cc,n,, - EPA901.1 Modified .4.5sE.02 1 ?RF.n1 1.28E-01 1.89E-01 u -"""

18-04023-06 18-04023-06 18 04023-06 TRG TRG TRG B105100AFSFC255CV B105100AFSFC255CV B105100AFSFC255CV ti~~~* 3 03/06/18 12:46 4/5/2018 4/5/2018 8

18-04023 18-04023 jO.CAC" Lead-210 Lead-212 Lead 214 EPA901.1 Modified EPA901.1 Modified EPA901.1 Modified

• 6.52E*00 7.31E-01 8.10E 01 7.40E-D1 7 "'°"""

4.34E-01 SQ1C.n1 7 ""'""'

4'.SF.n1 3.83E-01 5.61E-01 S81E*01 6.45E-01 8.43E 01 u L '"""

"c;;'

pCi/g 18-04023-06 TRG B105100AFSFC255CV 03/06/18 12:46 4/5/2018 4/5/2018 : 18-04023 Promethium-145 EPA901.1 Modified 18-04023-06 TRG B105100AFSFC255CV 03/06/18 12:46 4/5/2018 4/5/2018 rn.n,n,s Radium-226 EPA 901.1 Modified -2.73E-02 8.37E-02 8.37E-02

• 1 6.72E-D1 u oC:,o 18-04023-06 18-04023-06 TRG TRG B105100AFSFC255CV B"105100AFSFC255CV 03/06/18 12:46 03/06/18 12:46 4/5/2018 4/5/2018

.,,,,n1, 4/5/2018 18 04023 18-04023

-Thorium-234 EPA 901.1 Modified EPA 901.1 Modified 1.18E 02

-4.92E+OO 4.31E*01 1.95E+OO 4.31E-01 1.96E+OO 6.57E 01 snoc'°n u

u 18-04023-06 TRG B105100AFSFC255CV 03/06/18 12:46 4/5/201' 4/a/201' 18 04023 Thallium-208 EPA901.1 Modified 5.89E 01 H1C.n1 4.82E-01 ,o,c.n, u om"

. *---*~- ****--- -1.05E+OO i 11e~66 2.11E+OO 1.18E+OO u pCi/g 18 04023 06 TRG 8105100AFSFC255CV 03/06/1812:46 4/5/2018 4/5/2018 18-04023 Uranium 235 EPA901.1 Modified CU"'Counting Uncertainty;CSU"'Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Actlvity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Dupllcate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE NE CAL ON 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[213]

---~ SERVAC:E.5

Printed: 4/30/2018 3:19 PM Page 9 of 22 Report To: Worl< Order Details*

,. . . Patricia Giza 18-04023 Eberline Analytical .. .. _Zion Solutions, LLC SDG:

, Order: 677118 ____ ,,_

. ' "'~**- ...--- '" ---*- ..

Final Report of Analysis 101 Shiloh Blvd Analv.,I< ENVIRONMENTAL Zion, IL ~nnQQ Sample Matrix: ~n

Batch i Report Lab Sample 1 Client Sample Receipt Analysis ID Type ID Date I Date i

Date ID Analyte Method Result cu CSU MDA \ Qualifier Units 4/5/2018 I 4/5/2018 u 18 04023--07 TRG TRG

B105100AFSFC263CV B105100AFSFC263CV 03/06/18 09:30 03/06/18 09:30 rn.CAO,S 4/5/2018 I 4/5/2018 I 18-04023 Si1ver-108m EPA901.1 Modified EPA901.1 Modified 6.BOE-01 1.27E-02 4.72E-01 4.76E-02 ----_

4.73E 01 4.77E 02 9.54E 01 1.28E-01 u

,Ca,,

' -~--

18-04023-07 TRG  : 8105100AFSFC263CV 03/06/18 09:30 4/5/2018 415/2018 18-04023 Americium-241 EPA901.1 Modified 3.41E-01 , 1.82E-01 1.83E-01 __ 2.93E-01 u "' ""

u "'*"" ..

18-04023-07 TRG  : B105100AFSFC263CV 03/06/18 09:30 4/5/2018 4/5/2018 1/U'l.10?~ Barium 133 EPA901.1 Modified

""*"' i 6.89E 02 6.89E 02 1.82E 01 18-04023-07 TRG ' 8105100AFSFC263CV 03/06/18 09:30 4/5/2018 4/5/2018 18 04023 Bismuth-214 EPA901.1 Modified 7.47E 01* 2.67E-01 2.69E-01 3.92E-01 u

rm,

"*°'

"" '"' IRC 8105100AFSFC263CV 03/06/18 09:30 4/5/2018 4/5/2018 18--04023 Cobalt-60 EPA 901.1 Mnrlifi<>rl 1.17E-01 ' 1.17E-01 1.95E-01 i

"" '"' TRC 8105100AFSFC263CV 03/06/18 09:30 4/5/2018 4/5/2018 18--04023 EPA 901.1 Mnrlifi<>rl

• ""*"' 5.74E--02 5.74E-02  : 1.32E-01 u ""'"

" '" TRC B 105100AFSFC263CV 03/06/18 09:30 4/5/2018 4/5/2018 18-04023 EPA 901.1 Modified 4.88E 01 ,6.;,':01 2.06E-01 . 0 ,1s-01 ,r;,,

.. *- 18-040?3 EPA901.1 Modified 3.48E-02 '35'-01 2.35E 01 3.74E 01 u '"'"

TRG  : 8105100AFSFC263CV 4/5/2018 4/5/2018 .

• - TRG B105100AFSFC263CV 4/5/2018 , 4/5/2018 18-0407' EPA901.1 Modified 1.46E-01 ?05'-01 2.05E 01 1.75E 01 u

,o 0

'"' 1KG I B105100AFSFC263CV 03/06/18 09:30 4/5/2018 4/5/2018 '8.040,S EPA901.1 Modified 1.10E-01 2.17E-01 2.17E-01 . 3.02E-01 u  ;

EPA901.1 Modified . ., osc.o, 2.08E-01 2.08E 01 1.52E 01 u

'" '"' 1KG  : B105100AFSFC263CV ffilflfi/18 rl<l":ifl """18 4/5/2018

*°'""

18-04023 lodine-129 EPA 901.1 Modified 5.16E 02 1.25E-01 1.26E-01 1.66E-01 u  :

" '"' TRG i 8105100AFSFC263CV 03/06118 09 30 415/2018 4/5/2018 .

.. ." TRG  :

B105100AFSFC263CV 03/06118 09 3C 4/5/2018 4/5/2018 18 04023 Potassium-40 EPA901.1 Modified 4.55E+OO ,iie;66 168E+OO f 1.91E+OO \ ,r,,,

18-04023-07 TRC B105100AFSFC263CV 03/06/18 09,3C 4/5/2018 4/5/2018

• 1R-040:.i'.'I

.. EPA901.1 Modified 3.42E-02 1120-01 1.12E 01

- 1.90E 01 *-; u '"'"

i ...

u

'"" IRG i B105100AFSFC263CV 03/06/18 " ' " 4/5/2018 4/5/2018 4/5/2018 4/5/2018 1R.MO,S 18-04023 Niobium~94 Lead 210 EPA901.1 Modified EPA901.1 Modified 1.18E-02 2.03E+OO

'"'*°'

1.24E+OO 8.66E 02

, ,SC+OO

- 1.47E 01 2.29E+OO u

'" '"' TRG B105100AFSFC263CV [l:ilflfi/11::! fl'-J-:i!:

18-04023 07 TRG 8105100AFSFC263CV 03/06/18 09'30 415/2018 4/5/2018 18---04023 Lead-212 EPA901.1 Modified 3.46E 01 1.68E-01 1.69E-01 5.21E-01 u ,rnr

" . '" TRG B105100AFSFC263CV 03/06/18 09,30 4/5/2018 4/5/2018 18--04023 Lead-214 EPA 901.1 Modified 8.00E 01 2.75E-01 2.78E-01

.,! 5.77E-01 '"'"

18--04023-07 TRG ' B105100AFSFC263CV 03/06/18 09:30 4/5/2018 4/5/2018 ! 18-04023 Promethium-145 EPA 901.1 Modified 2.21E-02 1.50E-01 1.50E-01 2.35E-D1 u oCi/o 18-04023-07 TRG ' B105100AFSFC263CV rnm,;118 OQ*~n 4/5/2018 41512018 I 18-04023 Radium 226 EPA 901.1 Modified 7.47E-01 7E-01 , 2.69E 01 3.92E-01 ' i eC.Vo 18--04023-07 TRG  : B105100AFSFC263CV 03/06/180930 4/5'2018 4/5/2018 18 04023 EPA901.1 Modified 8.17E 02 ,A3E-01 I 2.43E-01  ;

4.01E-01  : u i rrnr

" *- TRG i B105100AFSFC263CV 03/06/1809,30 4/5/2018 4/5/2018 18-04023 Thorium-234 EPA901.1 Modified 1.45E+OO 2.21E+OO l 2.21E+OO ' 2.73E+OO , u  ! ""'"

... *- 2.92E 01 **;  ! u  !

TRG ' B10510DAFSFC263CV 03/06/18 09:30 4/5/2018 4/5/2018 18-04023 Thallium 208 EPA901.1 Modified 1.71E01 2.92E-01 5.33E-01 18-04023-07 B105100AFSFC263CV 03/06/18 mvm 4/5/2018 4/5/2018 18-04023 Uranium 235 EPA901.1 Modified -203E+0° 1.77E+OO  ! 1.77E+OO 7.95E-01 I u pCl/g TRG CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma); MDA=Minimal Detected Activity;LCS=laboratory Control Sample; MBL=Blank;DUP=Duplicate; TRG=Nonnal Sample; DO=Duplicate Original; U=Non-detect FAX 865/483-4621

[214]

Printed: 4/30/2018 3:19 PM Page 10 of 22 Report To* Work Order Details*

Patricia Giza SDG:' 18-04023 Eberline Analytical Zion .... ---.---.-.

LLC

__ Purchase Order:J--~ 677118

,.... ----~- . -------------------------- *--*---------*-*- .. - *-* **-- --- . --

Final Report of Analysis 101 Shiloh Blvd Analysis Category::_ ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so "'""'"""'""""

Lab Sample Client Sample Receipt  ! Analysis Batch Analyte Method Result cu CSU MDA Report ID I Type ID Date Date Date ID I  : Qualifier [ Units 18-04023-08 TRG  : B105100AFSFC276CV 03/05/18 13:42 4/5/2018 , 4/5/2018 : 18-04023 Actinium-228 EPA901.1 Modlfied 1.78E-01 I 6.11E 01 R.12E-01 9.86E 01 i u rr:,r 18-04023-08 TRG  : B105100AFSFC276CV 03/05/18 13:42 41512018 i 4/5/2018 C 18 04023 Silver-108m EPA901.1 Modtfied 4.12E-03 1.57E 01 1.57E-01 2.40E-01

' u -r"-

18-04023-08 TRG  : B105100AFSFC276CV 03/05/18 13:42 . 4/5/2018 4/5/2018 : --~;-;:,*.:;;:,;:; EPA901.1 Modified -5.15E-02  ! 6.10E-02 6.10E 02 3.89E-01  : u rrnr 18--04023--08 TRG  : B1051 OOAFSFC276CV 03/05/18 13:42 """'18 : 41512010 T~;-n-::;;:;::;:;; """ EPA901.1 Modified 1.17E+OO 3.84E 01 3.89E-01 4.63E 01 u rrnr 18-04023-08 TRG B105100AFSFC276CV 03/05/18 13:42 4/5/2018 4/5/2018 e

• 0 nM'l'l"> Bismuth-214 EPA901.1 Modified  : 1.13E+OO S.79E-01 3.83E-01

5.61E-01 ': rr:,r 1 -- TRG .' B105100AFSFC276CV 03/05/18 13:42 4/5/2018 4/5/2018 18-04023 Cobalt 60 EPA901.1 Modified  : 1.44E-02 1.48E-01 1.48E 01 i 1.73E-01 u -r""

o ,ro TRG B105100AFSFC276CV 03/05/18 13

42 4/5/2018 : 4/5/2018 i 18-04023 Cesium 134 EPA901.1 Modified 2.86E-02 4.07E-02 4.07E 02 i 2.72E-01 u pC;Jg u  : rr.:,r

'1~

'" , "" TRG 8105100AFSFC276CV 03/05/1813:42 4/5/2018 4/5/2018 . 18-04023 Cesium-137 EPA 901.1 Modified 1.95E-01 2.88E 01

,_ u

"" TRG B105100AFSFC276CV 03/05/18 13:42 4MC;R j 41512018 I 18-04023 152 EPA 901.1 Modlfied 1.31E+OO 1.38E-01 1.82E-01 9.23E 01 1.83E 01 '

6.02E-01 3.07E-01

' u rrnr rr.:,r 18 04023 08 TRG  : B105100AFSFC276CV 03/05/18 13:42 4MC18 l 4/5/2018 I 154 EPA901.1 Modlfied  :

'Q-""'"' EPA901.1 Modlfied 9.88E 01 3.22E-01 3.26E 01 5.05E 01 u rr.:,r 18-04023 08 18-04023-08 TRG TRG  :

B105100AFSFC276CV B105100AFSFC276CV 03/05/18 13:42 03/05/18 13:42 4/5/2018 4/5/2018 i 18-04023 Holmium-166m 155 EPA901.1 Modtfied 3.22E-01 2.23E 01 2.23E 01 . 2.48E-01 , u pCVg

'"""' i

,o ,or TRG B105100AFSFC276CV 03/05/18 13:42 ""'"" 4/5/2018 18-04023 lodice-129 EPA901.1 Modified -1.28E+OO 1.29E+OO 1.29E+OO 1.67E+OO u -r""

'" _, __,. TRG  : B105100AFSFC276CV 03/05/1813:42

"'""" ' 41512018 I *1*8~04023 '" EPA901.1 Modified 5.59E+OO 1.98E+OO 2.00E+OO 2.23E+OO -r""

18-04023 08 SFC276CV 03/05/18 13:42 4/5/2018 4/5/2018 : 18-04023 Manganese-54 EPA901.1 Modified -2.02E-03 6.74E-02 6.74E 02 2.38E-01 u rC:,r

--~*-- ---,-

04023-08 TRG i B105100AFSFC276CV 03/05/18 13:42 4MC18 . 4/5/2018 ; 18--04023 Niobium-94 EPA901.1 Modified 2.34E-02 1.30E-01 1.30E-01  : 2.16E-01 u rr:,r

4/5/2018 18--04023 Lead-210 EPA 901.1 Modified -3.13E-01 , snC+CC , SOC+OC 4.71E+OO u rr:,r 18-04023--08

---

18-04023-08 TRG B105100AFSFC276CV 03/05/18 13:42 1 me+rn>  ;,nc_n,

"'"-°' 6.05E 01 rr.>r TRG  : B105100AFSFC276CV 03/05/1813:42 ""'° : 4/512018 18-04023  : Lead-212 EPA 901.1 Modified er.>r 18-04023-08 TRG B105100AFSFC276CV 03/05/18 13:42  ; 4/512018 J 415/2018 18-04023 Lead-214 EPA901.1 Modified 2.34E+OO 7.22E-01 7.31E 01 1.20E+OO 18-04023-08 TRG i 8105100AFSFC276CV 03/05/18 13:42 4/5/2018 *; 4/512018 ' -iii r+roo EPA901.1 Modlfied 6.28E-01 9.46E 01 u

- --~cyp_ -

- 4/5/2018 ; EPA901.1 Modlfied 1.13E+OO 3.79E-01 3.83E 01 5.61E-01 rC.:,r 18-04023-08 TRG 8105100AFSFC276CV 03/05/18 13:42 4/5/2018 ' HJ, 18 04023 08 TRG  : B105100AFSFC276CV 031 5/2018 i 4/5/2018 j 1R-n4m:, EPA901.1 Modlfied -3.nCN

• QCC-01 4.90E-01 7.38E 01 u rr.:,r 03/05/18 13:42 4/5/2018 rium 234 EPA 901.1 Modified -' S,C+OC ,;qc+nn 2.83E+OO sc,c+nn u  : rC:,,

18--04023-08 TRG B105100AFSFC276CV  !

,o , ro 4/5/2018. I 4151201a I 7.27E-01 3.50E-01 3.52E 01 1.48E-01 -r",

TRG TRC B105100AFSFC276CV B105100AFSFC276CV

-- 03/05/18 13:42 03/05/18 13:42 4/5/2018 : 4/5/2018 18-04023 18 04023 Thallium 208 Uranium-235 EPA901.1 Modified EPA901.1 Modified 4.95E-01 2.41E+OO 2.41E+OO 1.33E+OO

' u pCl/g

i C U=Counting Uncertainty;CSU=Combined Standard Uncertainty { 1-sigma); MDA=Minimal Detected Activity; LCS=Laboratory Control Sample; MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample; DO=Duplicate Original; U=Non-detect 1-"=-'='='-=='-"===-'YTI CAL CO RPOfU, Tl ON I 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[215]

Printed: 4/30/2018 3:19 PM Page 11 of 22 Reporl To: Work Order Details:

Patricia Giza 18-04023-----*- *--*~---*-.

Eberline Analytical [ ___________________

Zion Solutions, LLC rv, SDG:

Order: 677118 I- ------*--*-----**-------,.---------------- --------------------

Final Report of Analysis 101 Shiloh Blvd Ono/.,<I< ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so  :

Lab Sample Client Sample i Receipt Analysis Batch  : cu Report ID Type ID Date i Date i Date I

ID Analyte Method Result CSU MDA  ; Qualffier j Units 18-04023-09 TRG i B105100AFSFC282CV 03/06/18 08:52 4/5/2018 ; 4/5/2018

• 18-04023 Actinium-228 EPA901.1 Modified 4-22E-01 6.29E-01 6.29E 01 1.15E+OO u rr,,r 18-04023-09 TRG i B105100AFSFC282CV 03/06/18 08:52 4/5/2018 4/5/2018 , 18-04023 Sl1ver-108m EPA 901-i Modified -9.15E-02 1.56E 01 1.56E 01 1.84E 01 u rra,r 18-04023-09 TRG i B1051 OOAFSFC282CV 03/06/18 08:52 4/5/2018 I 4/5/2018 18 04023 n EPA901.1 Modified 3.32E 01 ,_14E-01 2.15E-01 2.67E-01 u rrno 18-04023-09 TRG i B105100AFSFC282CV 03/06/18 08:52 4/5/2018 I 4/5/2018 18-04023 Barium-133 EPA901.1 Modified 8.35E-03 1.16E-01 1.16E-01 3.02E 01 u oC;fo 18-04023-09 18-04023-09 TRG TRG 8105100AFSFC282CV B105100AFSFC282CV 03/06/18 08:52 03106/18 08:52 4/5/2018 : 4/5/2018 , 18-04023 04023 Bismuth-214 Cobalt-60 EPA901.1 Modlfied EPA901.1 Modlfied 6.33E-01 1.11E-01

- 4_62E--01 1 soe:a,

,,e

,;

4_63E-01 7.21E-01 2.70E-01 u

u  :

rC"r rCa,r 18 04023 09 TRG 03/06/18 08:52 4/5/2018 4/5/2018 I 18-040?:! j Cesium-134 EPA901.1 Modified  ! 9.71E 03 7.67E-02 7.67E-02 2.64E-01 u rra,r TRG 8105100AFSFC282CV 03/06/18 08:52 4/5/2018 4/5/2018 rn.o,o,e I Cesium 137 EPA901.1 Modified 3.85E-01 2.72E 01 2_73E--01 4.28E 01 u '

TRG 8105100AFSFC282CV 03/06/18 08:52 4/5/2018 4/5/2018 I 1R-040?:! : EPA901.1 Modified 3.24E 01  ; 5.62E-01 S fiSF-01 3.94E-01  : u rn.o,o,e : - ,, 5.10E-01 5.10E-01 1.96E 01 u 18 04023 09 IKC 03/06/18 08:52 4/5/2018 4/5/2018 EPA901.1 Modified 2.84E 01 '

,r r , rr TRG B105100AFSFC282CV 03/06/18 m, ...,._, 4/5/2018 : 4/5/2018 18-04023 EPA 901.1 Modified 4.13E-02 1.50E 01 1.50E-01 2.93E-01 u rC_Ue 18-04023-09 TRG  :' B105100AFSFC282CV 03/06/18 08:52 4/5/2018 ; 4/5/2018 18 04023 Holmium 166m EPA 901.1 Modified 2.18E 02 2_82E-01 2_82E-01 1.71E 01 u rCUr 18-04023 EPA 901.1 Modified 3.11E 02  ; ooc.o, 1_14E-01 u rCa,r 18-04023-09 18-04023-09 TRG TRG i

B105100AFSFC282CV B105100AFSFC282CV 03/06/18 08:52 4/5/2018 ,

4/5/2018 4/5/2018 4/5/2018 1B-04023 Iodine 129 Potassium-40 EPA 901.1 Modified 5.42E+OO i '"" ;;

'.29E+OO 2.31E+OO 2.65E+OO pCi/g 18--04023 09 TRG  : B105100AFSFC282CV 03/06/18 OR*'i? 41512018 4/5/2018 : 18-04023 -- EPA901.1 Modified 7.36E 02 1.47E-01 1.47E-01 2.70E-01 u - oC!/o

- rr TRG ' 8105100AFSFC282CV 03/06/18 08:52 4/5/2018 4/5/2018 '"-""" EPA901.1 Modified

' 4.82E 02 1.44E-01 1.44E-01 2.23E 01 u '

rC_Ur

-- r*

TRG  : B105100AFSFC282CV 03/06/18 08:52 4/5/2018 41512018 18-04023 '000.,rn EPA901.1 Modlfied 2.07E+OO I OOF+OC I OOF+OO ' OOOF+OC u rCUr oii'i61 '°'e:01 , ,,.e:,1 rCa,r TRG B105100AFSFC282CV 03/06/18 08:52 4/5/2018 4/5/2018 18 04023 Lead-212 EPA901.1 Modtfied 5.06E-01 0 lo r , rr 1KG  : B105100AFSFC282CV 03/06/18 0/l*'i? 4/5/2018 41512018 +s.o,o,e Lead-214 EPA901.1 Modlfied 4.95E-01 3_05E-01 3.06E-01 ' 4.50E-01 pCi/g

,r , rr 1KG B105100AFSFC282CV 03/06/18 08:52 4/5/2018 4/5/2018 18 04023 Prome!hium-145 EPA901.1 Modified -3_97E-03 1.47E-01 1.47E--01 : 2.17E-01 u

,r , rr 1KG 8105100AFSFC282CV 03/06/18 08:52 4/5/2018 4/5/2018 18-04023 Radium 226 EPA901.1 Modified 6.33E 01 4.62E-01 4_63E-01 7.21E-01 u - "'rrur 18-04023 09 TRG ' 8105100AFSFC282CV 03/06/18 08:52 4/5/2018 4/5/2018 18-04023 EPA901.1 Modified 3.52E-01 3.65E 01 3.65E-01 6.02E-01 u i r r TRG  ! 8105100AFSFC282CV 03/06/18 08:52 415/2018 4/5/2018 18-04023 Thorium-234 EPA 901.1 Modified 2.84E+OO 1.75E+OO 1.76E+OO 2.89E+OO . u I rrnr 18--04023---09 TRG i B105100AFSFC282CV 03/06/18 08:52 4/5/2018 ; 4/5/2018 I 18--04023 EPA901.1 Modified 8.20E 01 5.27E-01 5.29E-01 9.39E-01  : u rrnn

,~r,n" , 1.57E+OO 1.57E+OO '>.03E-01 '. u  : pCi/g 18-04023-09 TRG B105100AFSFC282CV 03/06/18 08:52 4/5/2018 4/5/2018 EPA 901.1 Modified 1.30E 03 C U=Countlng Uncertainty;CSU=Combined Standard Uncertainty (1-sigma); MDA=Minimal Detected Activity; LCS=Laboratory Control Sam ple;M BL=Blank; DU P=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect I NE c111 ccr,PORAT10N 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[216]

I

Printed: 4/30/2018 3:19 PM Page 12 of 22 Report To: Work Order Details:

Patricia Giza SDG: 18-04023 Eberline Analytical 1- --- ----- . -------**--**---**----- .-------

_____.Zion Solutions, LLC ______ _ Purchase.. -Order: 677118 Final Report of Analysis 101 Shiloh Blvd

,_ ___ Analysis Category: ,- ENVIRONMENTAL Zion, IL 60099 Sample Matrix: ' so I Report Lab Sample Client Sample Receipt Analysis Batch I Method Result cu CSU MDA Qualifier :

ID Type I

I ID Date Date I Date ID Analyte II  ! I I Units 18-04023-10 TRG B105100AFSFC289CV 03/05/18 13:52 4/5/2018 4/6/2018 1'-11.im Actinium-228 EPA901.1 Modified 1.71E-01 4.00E 01 4.01E-01 6.64E-01 u oCllo 18-04023 , Silver 108m EPA901.1 Modified 3.05E--02 6.81E-02 6.81E-02 1.36E 01 u oCllo 18-04023-10 TRG B105100AFSFC289CV 03/05/1813:52

""'° 4/6/2018 4/6/2018 18 04023 Americium-241 EPA901.1 Modified -2.53E-01 2.17E 01 2.18E-01 2.42E-01 u oCllo 18 04023 10 TRG D

" 03/05/1813:52 03/05/1813:52 4/5/2018 4/5/2018 4/6/2018 18 04023 Barium-133 EPA901.1 Modified -5.61E-02 1.89E 01 1.89E-01 2.26E-01 u I rCllr 18--04023 10 TRG B105100AFSFC289CV e 1

EPA901.1 Modtfied 641E-01 2.76E-01 2.78E-01 4.25E-01  : Dll<IC 18-04023-10  ! TRG B105100AFSFC289CV 03105/18 13:52 ""'°'11R 4/6/2018 18 04023 Bismuth-214 2 SfiF-01 8.54E-02 8.64E-02 1.44E-01 oC.llo -

18-04023-10 '. TRG B1051 OOAFSFC289CV 03/05/18 13:52 4/5/2018 4/6/2018 18-04023 Cobalt-60 EPA901.1 Modrfied 18-04023-10 ' TRG 8105100AFSFC289CV 03/05/18 13:52 4/5/2018 , 4/6/2018 rn-11.iu1 Cesium-134 EPA901.1

__ ,_ Modtfied  ? ?OF-OS S MF-0> 5.64E-02 1.49E-01 u oCllo 18--04023 10 TRG D 03/05/18 1::;.,:;? 4/5/2018 4/6/2010 ,0 Cesium-137 EPA901.1 Modified I 1 08E+OO ,A5E-01 '"'-°' 2.76E 01 oCllo SD sr TRG  : B105100AFSFC289CV 03/05/18 1 '.".*'i? 4/5/2018 4/6/2018  ;;:;;,o,, EPA901.1 Modified -2_23E-02 , 1KM 2.17E-01 .' 3.27E-01 u .

,Clio SD EPA 901-1 Modified 1.22E--01 2.55E-01 2.55E--01  :  ;;,";;; u rr.lo Sr

'" TRG i 8105100AFSFC289CV 03/05/18 1'.".*<.? 41512018 416/2018 18--04023 '

,r ,r

,o TRC " "

03/05/1813:52 "°018 4/612018 100+0,, - EPA901.1 Modified

--3.15E-02 1.74E-01 1.74E 01 2.81E-01 u rCllr 18-04023--10 TRG . 8105100AFSFC289CV 03/05/18 13:52 4/5/2018 4/6/2018 18-04023 Holmium-166m EPA901.1 Modified 1.61E-02 1.67E-01 1.67E-01 1.46E-01 u orno 18-04023-10 TRG B1 ---

'" 03/05/18 13:52 4/5/2018 4/6/2018 18-04023 lodine-129 EPA901.1 Modified -9.79E-02 '.52E-01 , .S,F-M 1.84E 01 . u orno sr 1.63E+OO 1.67E+OO 1.21E+OO ac,,;

18 04023 10 TRG B105100AFSFC289CV 03/05/1813:52 4/5/2018 4/6/2018 , 18-04023 EPA901.1 Modified 6.64E+OO SD

' 03/05/18 13:52 4/5/2018 4/6/2018 18 04023 OS EPA901.1 Modified 741c-02 1.02E-01 1.03E-01 1.77E 01 u  : rCllo

TRG B105100AFSFC289CV 18--04023-10 TRG 'i B1051 OOAFSFC289CV 03/05/1813:52 . 41512018 416/2018 18-04023 Niobium 94 EPA901.1 Modrfied 2.90E-02 9.85E-02 9.85E-02 1.39E-01 u rCllo 18-04023-10 TRG B105100AFSFC289CV 03/05/1813:52 4/512018 41612018 18-04023 Lead-210 EPA901.1 Modified 1 RRF+OO 1 RnF+no 1.61E+OO ' '17E+OO u orno So SD TRG B105100AFSFC289CV 03/05/1813:52 4/5/2018 4/6/2018 18-04023 Lead 212 EPA901.1 Modified . 4.15E-01 '.20E-01 , "F-M

"-°' i oCllo 18-04023 10 TRG B105100AFSFC289CV 03/05118 1'*S, 41512018 4/6/2018  ;,_o+oo, Lead 214 EPA901.1 Modified . 7.500-01 2.80E-01 2.83E-01 5-18E-01  : or.lo T

18-04023 10 TRC B105100AFSFC289CV 03/05/18 13:52 +,s,0010 4/6/2018 l 18--04023 Promethium 145 EPA 901.1 Modified -9.74E-02 9.54E-02 9.56E 02 2.0SE-01 u rCllr 41s1,orn -;,- D+MO EPA 901.1 Modified 6.41E-01 2.76E-01 2.78E 01 4.25E-01 rCllr 1"

,r TRG B105100AFSFC289CV 03/05/1813:52 "018 ns, EPA901.1 Modified -1 07F-03 3.01E 01 301E-01 4.54E 01 u orno 18--04023-10 TRG TRG 8105100AFSFC289CV B105100AFSFC289CV 03105118 03105/18 nm 4MMS 4/6/2018 41612018 a 18-04023 18-04023 Thorium-234 EPA901.1 Modified 3.37E+OO , 1.86E+OO 1_87E+OO . 2.78E+OO u or.Ila 18-04023--10 TRG 8105100AFSFC289CV 03105/18 ns, ""'"" : 416/2018 18-04023 I Thallium-208 EPA901.1 Modtfied 4.45E-01 2.77E-01 2.78E-01 5.66E 01 u oCllo n'>.tnt;/18 1 '>.*t;?

,;;,;;;;-;-, 4/6/2018 18 04023 I Uranium-235 EPA901.1 Modified 2.00E 01 l 1.05E+OO 1 05E+OO -- 6.59E-01 u pCilg 18-04023--10 TRG i CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma); MDA=:M inimal Detected Activity; LCS=Laboratory Control Sample; M BL=B1ank; DU P=Duplicate; TRG=Nonnal Sample; DO=Duplicate Original; U=Non-detect 865/481-0683 FAX 865/483-4621

[217]

Printed: 4/30/2018 3:19 PM Page 13 of22 Report To: Work Order Details*

Patricia Giza SDG:i 18-04023 Eberline Analytical Final Report of Analysis

• • • -* Zion Solutions, LLC .----- ------**'"

101 Shiloh Blvd Purchase Order:

Analysis Category: -

677118 ENVIRONMENTAL

---~***-- *------,.*-- -------- ..

Zion, IL 6009Q Sample Matrix: i so Lab Sample Client Sample ' Receipt Date Analysis Date Batch ID Analyte Method Result cu  ! CSU MDA Qualifier :

Report Unlts ID Type ID Date

TRC 8105100AFSFC293CV 02/07/1813:45

' 4/5/2018 4/6/2018 18.040?1 EPA901.1 Modlfied 1.85E-01 ~ 5.52E 01 9.76E 01 u ,c;,,

,, EPA901.1 Modlfied -4.37E-02 1.51E*01 1.51E 01 2.39E*01 u "°""

' " B105100AFSFC293CV 02/07/18 13:45 41512018 416/2018 18-04023 Silver 108m TRG B105100AFSFC293CV 02/07/1813:45 41512018 4/6/2018 18.04023 EPA901.1 Modified *1.B2E*01 . i,1e.01 3.41E-01 4.78E-01 u ,r:,,

" TRG

' 81051 OOAFSFC293CV 02/07/1813:45 4/5/2018 : 4/6/2018 18-04023 EPA901.1 Modified *' '1E*03 1.12E.01 3.12E-01 5.08E-01 u ,r:,,

'" TRG B105100AFSFC293CV 02/07/1813:45 4/5/2018 4/6/2018 18.04023 Bism,th*214 EPA901.1 Modified 5.55E-01 6.54E-01 6.55E-01 9.67E-01 u ...

,C:,,

TRG B105100AFSFC293CV 02/07/1813:45 4/5/2018 4/6/2018 1'.040?1 Cch,,,.eo EPA901.1 Modified .4.19F.02 1.68E*01 1.68E-01 2.25E-01 u cCi/c 18-04023-11 TRG B105100AFSFC293CV 02/07/1813:45 4/512018 4/6/2018 1R.M0?1 EPA901.1 Modified *6.79E*03 1.28E*01 1.28E-01 2.28E-01 u ,me rn.c,m,

' ,mo

" " 1KG 8105100AFSFC293CV 02/0711813:45 4/5/2018 i 4/6/2018 Cesi,m*137 EPA 901.1 Modified 6.79E*01 S.26E*OO 8.96E+OO 6.37E-01 rn.c,m, .

i u ,mo

'" " 1KG B105100AFSFC293CV 02/07/18 13:45 4/5/2018 C 4/6/2018 EPA 901.1 Modified EPA 901.1 ~~"n;fi,,rl /

S.90E*01 R OOC.07 1.22E*OO 1.22E+OO I 8.46E-01 u  ;;;;; .

" TRG ' B105100AFSFC293CV 02/07/18 13:45 4/5/2018 4/6/2018 18-04023 378E*01 3.78E-01

• 1 4.33E 01

,,,e:,; ,r;,,

18-04023-11 TRG 8105100AFSFC293CV 02/07/18 13:45 4/5/2018 4/6/2018 1R.040?1 EPA901.1 Modified 1.13E*01 1.79F.01 3.79E 01 u 18-04023-11 TRG

' B105100AFSFC293CV 02/07/18 13:45 4/5/2018 , 4/6/2018 18-04023 Holmium 166m EPA901.1 Modlfied

• 110E*01 3.09E*01 3.09E-01  : 3.46E-01 u ,r;,,

18-04023-11 TRG B105100AFSFC293CV 02/07/18 13:45 4/5/2018 : 4/6/2018 1A.C.07' ,ooieo.170 EPA901.1 Modlfied 1.IOE*OO W3E*01 '.11E*01 i 3.27E-01 u """o 18-04023-11 TRG B105100AFSFC293CV 02/07/18 n*.:Jh 4/612018 1A.MC7' EPA 901.1 Modified 6.78E*OO ,.50E*OO , soc.co i ,.B6E*OO , orno u oc;;,

18-04023 11 TRG B105100AFSFC293CV 02/07/1813:45 415!201' 4/6/2018 18 04023 EPA901.1 Modified 's,c.o, 1.62E-01 1.62E-01  : 2.82E 01 , '

18-04023 11 TRG B105100AFSFC293CV 02/07/1813:45 41512018 416/2018 18 04023 Niobium-94 EPA901.1 Modified 1.60E-02 1.20E-01 1.20E-01 i 2.10E 01  ! u .

,r:,,

,r;,,

18-04023-11 TRG B105100AFSFC293CV 02/07/181:'l-4:"i 41512018 4/6/2018 1S.04 10 EPA901.1 Modified 1.59E*01 1.22E+OO 1.22E+OO 1 4.31E+OO u

,r,,, ...

,o 1' B105100AFSFC293CV 02/07/18 1?.*4'i 4/5/2018 4/6/2018 18-04023 Lead-212 EPA901.1 Modified 5.04E*01 4.58E 01 4.58E*01 e eee.01 u '

'"" 8105100AFSFC293CV 02/07/1813:45 41512018 4/6/2018 18-04023 Lead-214 EPA901.1 Modified 9.69E.01 9.01E*01 9.02E-01 1.47E+OO u i ocJ;o 18 04023--11 TRG /

'""'" u 11 7RC 8105100AFSFC293CV 02/07118 13:45 415/2018 4/6/2018 18-04023 Promethium 145 EPA901.1 Modified .poc.co 5.26E-01 .

5.22E-01

• oC:,,

,r:,,

18 04023--11 TRG 8105100AFSFC293CV 02/07/18 13:45 415!2018 4/6/2018 18-04023 Radium 226 EPA901.1 Modified 0 ooc.o, o o,c 01 6.55E 01 9.67E-01 , u 18-04023-11 TRG I 8105100AFSFC293CV 02/07/18 13:45 4/5/2018 4/6/2018 18-04023 Antimony-125 EPA901.1 Modified .375E.o, 1 eee.oo 1.68E+OO , 00,:,,:;.-on ! u ,r;,,

t-*--*-------**-- ! - - - - - - - - - - - - " -,--------* 4/6/2018 18*04023 Thorium 234 EPA901.1 Mor!ifiAti 2.13E*01 3.13E*OO 3.13E+OO 4.58E+OO  : u ,r,,,

18 04023 11 TRG 8105100AFSFC293CV 02/07/1813:45 4/5/2018 8105100AFSFC293CV 02/07/18 13:45 4/5/2018 : 4/6/2018 18*04023 Thallium 208 EPA 901.1 M,-,rllfiPrl R S7C.01 9.73E.()1 9.74E*01 u ,c.1,0 18 04023 . 1 ""*"" '

18 04023-11 I TRG  ! B105100AFSFC293CV 02/07/18 13:45 "'"018  : .d/ROf)18

'"*"'"" Uranium 235 EPA901.1 Modified 2.18E+OO 3.93E+OO 1.93E*OO i ' ssc.cc i u i pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect ON 601 SCARBORO ROAD OAK RIDGE, TN 37830 665/481-0683 FAX 865/483-4621

[218]

Printed: 4/30/2018 3:19 PM Page 14 of 22 Report To: Work Order Details:

Patricia Giza SDG:, 18-04023 Eberline Analytical Zion. Solutions,LLC -

, Order: 677118

- - **- ----* ---- .. ---1--------*:,,

Final Report of Analysis 101 Shiloh Blvd ~

', ENVIRONMENTAL ... ,, ... ' -*

Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch  ! Analyte Method Result  : cu '

CSU MDA  ; Qualifier i: Report Units ID Type ID Date  : Date Date ID  : ' -

• - TRE 02/13/1812:5( 4/5/2018 4/6/2018 18-04023 j Actinium 228 EPA901.1 Modified 1.09E+OO 5.35E 01 5.38E-01 9.28E-01 """"

8105100AFSFC300CV

' TRE B105100AFSFC300CV 02/13/181? .."if 4/5/2018 4/6/2018 18-04023 j Silver 108m EPA901.1 Modified -1.43E-01 1.75E 01 1.75E-01 1.72E-01 u '

oc;/o 18-04023-12 TRG B105100AFSFC300CV 02/13/18 12:50 4/5/2018 4/6/2018 18-04023 Americium-241 EPA901.1 Modified S.39E-02 2.38E-01 2.38E 01 3.23E 01 u oc;/o 18-04023-12 TRG . 8105100AFSFC300CV 02/13/18 12:50 4/5/2018 4/6/2018 18-04023 Barium 133 EPA901.1 Modified -1.01E-01 1.92E-01 1.92E-01 2.36E-01 u ,rn, TRG 02/13/18 12:50 41512018 41612018 18-04023 Bismuth-214 EPA901.1 Modified 5.93E-01 3.33E-01 . iise-01 6.57E 01 u oCl/o 04023-12

>,*e>***----

18-04023-12 l

TRG B1D5100AFSFC300CV 8105100AFSFC300CV 02/13/18 12:50 4/5/2018 : 4/6/2018 18-04023 Coball-60 EPA 901.1 Modified 5.98E 02 ,i,e:01 1,,e:01 1.89E 01 u """"

! u 18--04023-12 18-04023-12 TRG TRG

. B105100AFSFC300CV B105100AFSFC300CV 02/13/1812:50 02/13/181?*.';0 4/5/2018 4/5/2018 4/612018 4/6/2018 18-04023 1S-040?S Ces/om-134 Cesium-137 EPA901.1 Modified EPA901.1 Modified '

6.93E-02 9.37E 01 8.40E 02

? 4SF-01 8.41E-02 2.50E-01 2.14E-01 2.56E 01

,ra,,

- 4.46E-01 4.46E-01 4.37E-01 u rc;/o

<CS 18-04023-12 TRG B105100AFSFC300CV 02/13/181?-,:;n 4/5/2018 416/2018 18-04023 EPA901.1 Modified 4.36E 01 TRG 02/13/18 1?*'in 4/5/2018 '"-""" EPA901.1 Modified 1.01E-01 4.0SE-01 4.05E-01 2.27E 01 u or,,o 18--04023-12 B105100AFSFC300CV

,1/f-,l'J(JH! '

TRG 02/13/18 1')*'ifl 4/6/2018 "-"'""

EPA901.1 Modified 2.94E-01 2.40E--01 2.40E 01 3.66E-01 : u orno 18-04023-12 B105100AFSFC300CV 18-04023--12 TRG B105100AFSFC300CV 02/13/1812:50 41512018 4/6/2018 18-04023 Holmlum-166m EPA 901.1 Modified ' 3.02E-02 9_51E-02 9.51E 02 1.81E-01 ' u """"

-~*,----**-------

18-04023-12 TRG B105100AFSFC300CV 02/13/1812:50 4/5/2018 ; 4/6/2018 1a.04on lodine-129 EPA 901.1 Modified -8.29E-02 1.64E-01 1.64E-01 1.97E-01 ' u pC/lg 18-04023 12 TRG TRG B105100AFSFC300CV B105100AFSFC300CV 02/13/1812:50 02/13/18 1?*'il 4/5/2018 . 4/6/2018 ; 1R..n,1n,~

4/5/2018 _ ,l/fi/")1)1~ 18-04023 Potassium-40 EPA901.1 Modified EPA901.1 Modified 'A'!1FI

-1 2.24E+OO

,. -c 2.28E+OO 01 !

1.53E+OO 2.19E-01

u oC//o pCi/g

-"'"-°'

18-04023-12 TRG ' 8105100AFSFC300CV 02/13/18 12:50 4/5/2018 : 4/0/201/;l rn=oo, Niobium 94 EPA901.1 Modified 1.22E-01 1.22E-01 1.42E

' 18 18-04023 Lead 210 EPA 901.1 Modified 1 ;,c,oc 1.64E+OO 2.83E+OO u pCilg 18-04023-12 TRG 8105100AFSFC300CV 021

-- nf'a,~ _,,,_

• 18-04023-12 TRG 8105100AFSFC300CV 02/13/18 12:50 4/5/2018 41612018 1R-040?S , earl-?1? EPA 901.1 Modified 3 44E-01  ? 40F-01 2.41E 01 3.65E 01 u

---~*-~----*-----

18-04023-12 TRG B105100AFSFC300CV 02/13/18 12:50 4/5/2018 '""018 18-04023 Lead 214 EPA901.1 Modified se,F-01 ,AOE-01 2.41E-01 4.18E-01 u or.;;o TRG 8105100AFSFC300CV 02/13/18 12:50 4/5/2018 """'"18 18-04023 Promethium-145 EPA901.1 Modified 9.61E-02 1.60E-01 1.60E 01 ,.71E-01 u or.;;o TRG 8105100AFSFC300CV 02/13/1812:50 41512018 , 4/6/2018 18-04023 EPA901.1 Modified 5.93E-01

"-"' 3.35E-01 '57E-01 u pCl/g TRG 8105100AFSFC300CV 02/13/18 12:50 4/S/?018 41612018 1R-040n 1?S EPA901.1 Modified 1.05E-01 2.92E--01 2.92E 01 . ,i,e-01 u ' "°""

4/5/2018 I 4/6/2018 18 - EPA 901.1 Modified 1.22E+OO 2.65E+OO 2.65E+OO SO<C,00 u ,,,,,

B105100AFSFC300CV 02/13/1812:50 18-04023 12 TRG B105100AFSFC300CV 02/13/1812:50 4/5/2018 4/6/2018 18 04023 Thallium-208 EPA901.1 Modified 3.30E-01 3.09E--01 3.10E-01 7.1'F-01 u oC//o 18-04023-12 TRG ' B105100AFSFC300CV 02/13/1812:50 4/5/2018 4/6/2018 18-04023 Uranlum-235 EPA 901.1 Modified SOSF-01 1.76E+OO 1.76E+OO 1.04E+OO u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

( -~

EBERLINE SERV/CES

[219]

FAX 865/483-4621

Printed: 413012018 3:19 PM Page 15 of 22 Report To: Work Order Details:

Patricia Giza SDG:, 18-04023 Eberline Analytical Zion Solutions, LLC -- _____ ,__

L.

, nmor 1

677118

---

*--.. ****-~

Final Report of Analysis 101 Shiloh Blvd Analvs/s  : ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

• SC Lab ID i Sample Type i Client ID Sample Date Receipt Date Analysis :

Date I Batch ID Analyte Method Result cu  !

I CSU MDA i Qualifier

• Report Units 18-04023-13 18-04023-13 18-04023-13 TRG TRG TRG TRG TRG

' B105100AFSFC316CV B105100AFSFC316CV B105100AFSFC316CV B105100AFSFC316CV B105100AFSFC316CV 03/05/18 1'.'1-!'iR 03/05/18 13:58 03/05/18 13:58 03/05/18 13:58 03/05/18 13:58 4/S/?01' 4/5/2018 4/5/2018 4/5/2018 4/5/2018 4/6/2018 4/6/2018 4/6/2018 4/6/2018 4/6/2018 18-040~:--

18--04023 18--04023 18 04023 18-04023 Actlnlum-228 Si1ver-108m Americium-241 Barium-133 Bismuth-214 EPA901.1 Modified

____ ,. Modified EPA901.1 EPA901.1 Modified EPA901.1 Modified EPA901.1 Modified 6.59E-01 2.14E-01

-9.19E 03

-1_55E-01 5.23E-01 1.60E-01 1.15E 01

~: 1.15E-01 1.,ie-01 1.00E+OO 2.72E-01 4_01E-01 4.79E-01 7.15E 01 !

u u

u u

u om, om, or.;,,

om,

,r;,,

B105100AFSFC316CV 03/05/1813:58 _ 4/5/201' . 4/6/2018 18 04023 _ Cobalt-60 EPA901.1 Modified 1.78E 02 7.91E-02 7.91E-02 2.89E 01 u ,r,,,

18-04023-13 TRG  :

18,04023, 13 TRG B105100AFSFC316CV 03/05/1813:58 4/5/2018 I 4/6/2018 , 18 04023 EPA901.1 Modified ,,,,,

' 1.30E 01 1.36E-01 1.36E-01 2.79E 01 u "'""

• ' B105100AFSFC316CV 03/05/18 13:58, , 4/5/2018 4/6/2018 ; 18 04023 Cesium-137 EPA901.1 Modffied 3.07E-01 3.13E-01 3.55E 01 TRG "' ' "' 110

" "'~*-*--.-,- '

1.82E+OO 1 OOF+OO 1.01E+OO 6.57E-01 u orno

"'"° ' ""'° EPA 901.1 Modtfied C,

18--04023 13 1KG 8105100AFSFC316CV 03/05/18 13:58 18-04023 18--04023-13 TRC ': 8105100AFSFC316CV 18-04023 C EPA 901.1 Modified 1.22E-01 4 pF_M 4.12E-01 3.39E-01 u ,r,,,

18-04023-13 TRG  ! B105100AFSFC316CV 0 3 / 0 5 / ~ ~ ~/6/2018 03/05/1 r 8 , 18 04023 - EPA901.1 Modified 2.61E 01  ; iis!oi 1iie-01 4.60E-01 u orn,

-rn, 18-04023-13 TRC I 8105100AFSFC316CV 03/05/18 1 18 18-04023 \ Holmium-166m EPA901.1 Modified -4.08E-01 OSCCM 3.57E 01 2.73E 01 ' u

--*---*--- rn-nAnn i 3.43E+OO 1.99E+OO , nnF+nn 1.87E+OO u 18 04023 13 TRG B105100AFSFC316CV 03/05/18 13:58 4/5/2018 4/6/2018 lodine-129 EPA 901.1 Modified i

• - - '*- ,. TRG 8105100AFSFC316CV 03/05/18 13:58 4/5/2018 4/6/2018 18-04023 Potassium-40 EPA901.1 Modified 6.52E+OO 1 OCF+OO 1.93E+OO 1.11E+OO . oC"o

• -., - '*- ,. TRG ' 8105100AFSFC316CV 03/05/18 13:58 4/5/2018 4/6/2018 : 18-04023 )

EPA901.1 Modified ,1 S?F,C? 1 SSF-0, 1.68E*01 2.61E-01 : u orno

' TRG 8105100AFSFC316CV 03/05/18 13:58 4/5/2018 4/6/2018 18-04023 4/6/2018 ;18-040?'.'!

Niobium 94 EPA901.1 Mnrfifi<>.-i 1.44E-02 7.44E+OO 1 ,CF_M 3.82E+OO 1.40E-01 3.83E+OO 2.32E-01 5.15E+OO

! u u

orno

,r,,

18-04023-13 TRG i

8105100AFSFC316CV B105100AFSFC316CV 03/05/18 13:58 03/05/18 13:58 4/5/2018 4/5/2018 4/6/2018 rn.o.nn .

Lead-210 Lead-212 EPA901.1 Modified EPA901.1 Modrfied

': 8.80E-01 3.55E-01 3.57E-01 ' 4.96E-01 : O<!IIO

' " TRC B105100AFSFC316CV 03/05/181358 4/5/2018 4/6/2018 18 04023 Lead-214 EPA901.1 Mn.-iifi<>.-i -0 SSF-C? 7.75E-02 7.77E-02 7.60E 01 u oC;,o

" TRG  ! B105100AFSFC316CV 03/05/18 13:58 415/2018 MRl'H/18 18-04023 EPA 901.1 Mn.-iifi<>.-i I 1 ,OF+OO 7.16E 01 7.19E-01 ' 1.07E+OO

• u ,r;,o 18-04023-13 TRG  ! B105100AFSFC316CV 03105118 13;58 4/5/2018 416/2018 18-04023 Radlum-226 EPA901.1 Modified i _1 SSF.M 1.93E-01 1.93E-01 r 7.15E 01 u er""

-  ! 1'-0407' EPA901.1 Modified -4.10E-01 5.98E-01 5.98E 01 8.25E-01 u ,r,,,

" TRG B105100AFSFC316CV 03/05/18 13:58 4/512018 41612018 '

TRG I B105100AFSFC316CV 03/05/1813:58 4/5/2018 4/6/2018 18 04023 i Thorium-234 EPA 901.1 Modrfied -4.21E+OO 2.14E+OO 2.15E+OO 3.77E+OO u p~_ifE!___

., -"* . -----*----- *----.-' 1.1?F+nn u orno TRG B105100AFSFC316CV 03/05/18 13:58 4/5/2018 4/6/2018 , ,,+

18-04023!

Thalllum 208 EPA901.1 Mn.-iifi<>.-i 5.67E-01 5.70E-01 8.72E-01

" TRG B105100AFSFC316CV 03/05/18 13:58 4/5/2018 4/6/2018 I 18 04023 ' Uranium-235 EPA 901.1 Modrfied 5.50E 01 0 nF+OO 0 nF+OO 1.46E+OO : u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MOA=Min imal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=DupHcate; TRG=Normal Sample;DO=Dupllcate Original; U=Non-detect ON 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[220]

Printed: 4/30/2018 3:19 PM Page 16 of 22 Report To: Work Order Details:

Patricia Giza SDG.i 18-04023 Eberline Analytical ____

Zion Solution_s, LLC:. _ Purchase Order:  ! 677118 Final Report of Analysis 101 Shiloh Blvd - l'(Vli -1t'I.IMl=:NTAI Zion, IL 60099 Sample MatnX: so I' '

Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method j Result cu CSU MDA Qualifier i Units ID Type ID Date Date Date ' ID 18-04023-14 TRG B105100AFSFC321CV 02113118 14:10 I 4/5/2018 4/6/2018 18-04023 Actinium 228 EPA901.1 Modified 5.30E-02 5.39E-o* 5.39E-O" 8.77E-01 . u cC"c

' . u crnc

-- , __02/13/1 I 18-04023-14 TRG B105100AFSFC321CV 0211311s 14:10 4/5/2018 4/6/2018 18-04023 Silver 108m EPA 901-1 Modified 4.90E 02 1.20E-01 1.20E-01 1.66E-01

' 18-04023-14 TRG B105100AFSFC321CV 2018 18-04023 Americium 241 EPA901.1 Modified 1.53E 01 1.57E 01 1.57E-01 2.10E 01 u pCUg

- ' --- 1 R4F-O* <eac c* u 18 04023-14 TRG B105100AFSFC321CV 02/13/1814:10 4/5/2018 i 4/6/2018 18--04023 Barium 133 EPA 901.1 Modified 1.79E-01 2.32E 01 """"

u

,o"

.. TRG TRG B105100AFSFC321CV B105100AFSFC321CV 02/1311814:10 02/13/1814:10 4/S/?01'

""'°

4/6/2018 ' 1R-040?'.'l 4/e/?C1R : 1'-040,S Bismuth 214 Cobalt-60 EPA 901.1 Modified EPA901.1 Modified 2.84E~ 3.41E-01 1.51E-01 3.42E-01 1.51E-01 5.42E 01 2.20E-01 u  :

cC."c 18 04023-14 TRG 8105100AFSFC321CV 02/13/1814:10 "'""" '

18---04023 Cesium-134 EPA901.1 Modified 8.07E-03 1.06E-01 1.06E 01 I 2.19E-01 u --pCI/g ----

18-04023-14 TRG B105100AFSFC321CV 02/13/1814:10 4/5/2018 4/6/2018 18-04023 ' Cesium 137 EPA 901.1 Modified 1.49E-01 1.20E 01 1.ZOE-01  ! 1.85E-01 u ' or.""

18-04023-14 TRG B105100AFSFC321CV 02/13/1814:10 4/5/2018 : 41612018 18-04023 EPA901.1 Modified -4.68E 02 3.37E-01 3.37E-01

' 3.26E 01 u .rn.

18-04023-14 TRG B105100AFSFC321CV 02/13/18 14:10 4/5/2018 416/2018 i 18-04023 Europium 154 EPA901.1 Modified 9.66E 02 2.93E-01 2.93E-01 1.69E 01 u """"

• _* . ~--:-

18-04023-14 TRG B105100AFSFC321CV 02/13/18 14:10 4/5/2018 4/6/2018 18-04023 EPA901.1 Modified E-01 2.40E 01 u ornc

• ---18-04023-14 18 04023 14 TRG TRG S105100AFSFC321CV B105100AFSFC321CV 02/13/1814:10 02/1 4/5/2018 4/5/2018 4/6/2018 4/6/2018 i 18-04023 18 04023 Holmium-166m lodlne-129 EPA901.1 Modified EPA 901.1 Modified EPA 901.1

-1.40E-01 1.78E-02 ss,c+oc 2.97E-01 6.26E 02 1.85E+OO 2.97E-01 6.26E-02 1.88E+OO 1.15E-01 9.50E-02 7.81E-01 u

u

! -:~~

pCi/g 18-04023 14 TRG S105100AFSFC321CV 02/13/1814:10 4/5/2018 1 4/6/2018 18 04023 Potassium-40 Mnnm..n TRG B105100AFSFC321CV 02/13/1814:10 4/5/2018 I 4/6/2018 : 18 04023

. EPA 901.1 Modified 4.86E-02 1.15E-01 1.15E 01 2.11E-01 u n;..;/n ---

18-04023 14 TRG B105100AFSFC321CV 02/13/1814:10 ,1/",/'.}[)18 , 4/6/2018 ,~o,co, Niobium-94 EPA 901.1 Modified 5.54E-02 1.10E-01 1.10E-O* 2.03E-01 u crnc 18-04023 14 1 TRG B105100AFSFC321CV 02/13/1814,10 4/5/2018 4/6/2018 : 18-041"1'.J~ Lead-210 EPA901.1 Mnn,t;.,,-1 1 O,F+CO 1 oac+oo 1 oaF+OO , 1.73E+OO , u er.""

... TRG B105100AFSFC321CV 02/13/1814:10 4/5/2018 4/6/2018  ! 18-04023 Lead 212 EPA 901.1 Modified 3.52E-01 1_64E-01 1.65E 01 2.85E-01 u '

.r;,;**--

- '" ' TRG C 0?/13/18 14,10 4/5/2018 4/6/2018 '18-040,S Lead-214 EPA901.1 Modifled 5.15E01 2.64E-01 2.65E-01 4.29E 01 """*

.r,..

18-04023-14 TRG S105100AFSFC321CV 02/13/18 14:10 4/5/2018 41512018 I 18-04023 Promethium-145 EPA901.1 Modifled 3.87E-02 1.01E-01 1.01E 01 1.54E-01 u S105100AFSFC321CV 02/13/18 14:10 4/5/2018 4;512018 I 18 04023 Radium-226 EPA901.1 Modrfied i 2.84E-01 3.41E-01 s 4'F-01 5.42E-01 u cC.,,,

18--04023 14 18--04023 14 i TRG TRG 81 . 02/13/1814:10 4/S/2018 4/6/2018 "-°'""

-- EPA901.1 Modified

-2.29E 03 3.72E-01 , nF.o, 5.28E-01 u oC."c 18-04023-14 ; TRG 8105100AFSFC321CV 02/13/1814:10 4/5/2018 4/6/2018 , 18-04023 Thorium-234 EPA 901-1 Modified 2.20E+OO 1.30E+OO 1.31E+OO 2.17E+OO u ,c;;,

18--04023-14 TRG B105100AFSFC321CV 02/13/1814:10 4/5/2018 4/6/2018 ! 18-04023 Thallium-208 EPA 901.1 Modified 5.0BE-01 3.77E-01 3.78E 01 6.72E-01 u .r""

18-04023-14 TRG B105100AFSFC321CV 02/13/1814:10 4/5/2018 4/6/2018 i 18-04023 Uranium-235 EPA 901.1 Modified -7.23E-01 1.27E+OO 1.27E+OO 6.68E-01 u  ! pCi/g CU=Counting Uncertainty;CS U=Combined Standard Uncertainty ( 1-sigma);MDA=Min imal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Nonnal Sam ple;OO=Duplicate Original; U=Non-detect I

NE CAL. TION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[221]

I

Printed: 4/30/2018 3:19 PM Page 17 of 22 Report To: Work Order Details:

Patricia Giza SDG:1 18-04023 Eberline Analytical '___.. ____ Zion Solutions, LLC _ Pu;;:;hase Order: ! 677118 Final Report of Analysis 101 Shiloh Blvd

---

*---~--**** *----- ---- ------- ------------- ~-- ENVIRONMENTAL -- -

Zion, IL 60099 Sample Matrix: so

! . . Qualifier 1 Lab fD Sample i Type Client ID Sample Date i

I Receipt Date

' Analysis Date Batch ID Analyte Method i

Result I cu I CSU I MDA Report Units 18-04023-15 TRG 8105100AFSFC326CV 02/14/18 08:15 4/5/2018 4/6/2018 18-04023 Actinium 228 EPA901.1 Modified i 7.06E-01 4.77E-01 4.78E-01 8.98E 01 u orno 18-04023 15 TRG 8105100AFSFC326CV 02/14/18 08:15 4/5/2018 4/6/2018 1R-040?S Si1ver-108m EPA901.1 Modified 7.74E-02 1.20E-01

• 1.20E-01 2.02E 01 --! u "°""

18--04023 15 TRG -

8105100AFSFC326CV 02/14/1808:15 4/5/2018 4/6/2018 1S-C40?S EPA901.1 Modified . -5.34E-01 2.22E 01 2.24E-01 3.04E 01  : u

• orno 02/14/18 08:15 4/5/2018 4/6/2018 18-04023 EPA 901.1 Modified -1.48E-01 1.29E 01 1.29E 01 3_02E-01 u oC;,o 180402315 IKC 8105100AFSFC326CV 415/2018 416/2018  ! 18-04023 EPA 901.1 Modified 3.03E-01 3.16E-01 3.16E 01 5.45E 01 u

'I orno 18 04023--15 IKC 8105100AFSFC326CV 02/14/18 08:15 18-04023--15 IKC - 02114118 08:15 415/2018  ! 416/2018 : 18-04023 Cobalt-60 EPA901.1 Modified 2.12E-02 1.41E-01 1.41E-01 1.71E 01 u I or_;,o 18-04023--15 TRG B105100AFSFC326CV 02/14/18 08:15 4/5/2018 I 4/6/2018 18 04023 Cesium 134 EPA 901.1 Modified 7.73E 03 4.68E-02 4.68E-02 2.47E-01 u or""

18-04023--15 TRG B105100AFSFC326CV 02/14/18 08:15 4/5/2018 - 4/612018 18-04023 Cesium-137 EPA 901.1 Modified 6.98E-02 1.64E-01 1.64E-01 2.60E-01 u oCUo 18--04023-15 TRG B105100AFSFC326CV 02114118 0815 41512018 4/6/2018 : 18-04023

- -- EPA 901.1 Modified 3.53E-01 3.59E 01 3.60E 01 5.12E-01 u or;,o

• • ----18---04023-15 TRG B105100AFSFC326CV 02114118 08:15 4/5/2018 , 4/6/2018 18-04023 Europium 154 EPA 901.1 Modified -7 OSF-00 3.27E 01 , ne_o, 2.61E-01 u -r""

---

~-*, ""--"-------

18-04023-15 18-04023-15 TRG TRG B105100AFSFC326CV B105100AFSFC326CV 02114/18 08*15 02/14/18 08:15 4/5/2018 4/5/2018

! 4/6/2018 18 04023 18-04023 Europium-155 Holmium-166m EPA 901.1 Modified EPA901.1 Modified 6.17E-01 1.66E-01

- ,,ie-01

'?4F-01

- ;;;..i_o, 2.24E-01  ;,,i:a, -

• 3.90E 01 u u

or,,o

-r""

.r;,.

18 04023 15 TRG B105100AFSFC326CV 02/14/18 08:15 4/5/2018 ' 4/6/2018 : 18 04023 Iodine 129 EPA 901.1 Modified 7.21E 01 8.81F-01 8.82E-01 1.41E+OO lJ 18--04023 15 TRG B105100AFSFC326CV

---

* 02/14/18 08:15 4/5/2018 4/6/2018 18--04023 Potassium-40 EPA901.1 Modified 6. 2.07E+OO  ! 7 10F+OC 7'7F+OO . """"

B105100AFSFC326CV

~,-,_, ..,,_, ___-___ 02/14/18 08:15 4/5/2018 4/6/2018 18 04023 1R-04023 Manganese-54 EPA901.1 Modified EPA901.1 Modified 6.22E 02 1.19E---01 1_22E-01 1.44E-01

77F.O-1 ise

0-2.16E01

SQF_o;

• u u

orno or""

18-04023-15 TRG B105100AFSFC326CV 02/14/1808:15 4/5/2018 4/6/2018 Niobium 94 18-04023-15 TRG B105100AFSFC326CV 02/14/18 08:15  ; 4/5/2018 4/6/2018 1"-0407' Lead-210 EPA901.1 Modified 9.60E-01 2.38E+OO 7'RF+OO  ; S ROF+OO u orno

"--"-*-------* ,s_c,o,s 4 SSF-01 18-04023-15 TRG B105100AFSFC326CV 02/14/18 08:15 02/14/18 08:15 4/5/2018 4/5/2018 4/6/2018 4/6/2018 18--04023 Lead-212 Lead-214 EPA901.1 Modlfied EPA901.1 Modified 5.53E-01 3.44E-01 3.05E-01 3.57E-01 3.06E-01 3.57E-01 5.78E 01

' u orno 18 [~+c~l~51D0AFSFC326CV 18-04023--15 I . ~* 02114118 08:15 4/5/2018 4/612018 1'~'° EPA901.1 Modtfied -4.31E 02 2.97E 01 ,.97E-D1 ;oee_o, u -r""

18-04023-15 TRG 8105100AFSFC326CV 02114118 08*15 4/5/2018 4/6/2018 , 18-04023 EPA901.1 Modified 3.03E-01 iiee:01 3,ec_o, 5.45E-01 u or""

18-04023-15 TRG

'- 8105100AFSFC326CV 0 /2018 i 4/6/2018 I 18-04023 Antimony 125 EPA 901.1 Modified 2.97E 01 ,1iclo, 4.11E-01 6.65E-01 u or""

' - 02/14/18 08:15 4/5/2018 -234 EPA 901.1 Modified 4.61E+OO 1.62E+OO 1.64E+OO s c,F+M u .r;,.

1 '" TRG

• 8105100AFSFC326CV ,o

.r;,.

1"*"*023-15 8105100AFSFC326CV 02/14/18 08:15 4/Sl701R I 4/6/2018 1'-040,S T EPA901.1 Modified 4.13E-01 2.29E-01 2.30E-01 1.32E 01

'" 02/14/18 08:15 4/512018 4/6/2018 1R-040?S EPA901.1 Modified 5.24E-01 1.90E+OO 1.90E+OO 1.10E+OO u pCi/g 18-04023-15 TRG I B105100AFSFC326CV v, CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minirnal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBER~INE CAL CORPORAT!ON

~  :'.::--.JE:RV!CE.S 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[222]

Printed: 4/30/2018 3:19 PM Page 18 of 22 Report TO' Work Order Details*

Patricia Giza 18-04023 Eberline Analytical ----

___ Zi_on Solutions, LLC ____________

SDG:

677118

fll~~

Final Report of Analysis -- ,,.

101 Shiloh Blvd

--*- *** j .* , . . . . . . . . . .

ENVIRONMENTAL

--- ----..-----~-..---------..--------- ------- ------

Zion, IL 60099

. . . .!':.~.<!ff}!p7e Matrix: so Lab ID Sample Type Client iD Sample Dato Receipt Date Analysis j Date Batch ID Analyte Method Result l cu CSU MDA Qualifier Report Units B105100AFSFC329CV 03/05/18 14:18 4/5/2018 , 4/6/2018 18-04023 Actinium 228 EPA901.1 Modified 4.03E-01 3.11E-O 3.11E-01 6-21E-01 ' u or_;,.

,o ><O 1KG 8105100AFSFC329CV 03/05/1814:18 4/5/2018 4/6/2018 18-04023 Silver-108m,. ___ EPA901.1 Modified -2.69E 02 , o,c_c, 1.0BE-01 1.49E-01 u or,<c

,o

"" -- 1KG B105100AFSFC329CV 03/05/1814:18 415/2018 4/6/2018 18 04023 Americium-241 EPA901.1 Modified 6.27E 02 2.05E-01 2.05E-01 ,.61E-O' u or;,.

• - *--- TRG B105100AFSFC329CV 03/05/1814:18 4/5/2018 4/6/2018 18--04023 Barium 133 EPA 901.1 Modified 3.11E 02 1.69E-01 ,1,e:a: u .r;,.

18-04023-16

-,c TRC TRG B105100AFSFC329CV B105100AFSFC329CV 03/05/1814:18 03/05/1814:18 4/5/2018 4/5/2018 41612018 4/612018

~~=1~1Modified

.1 Modified 8.81E 01 1.17E-01 2.90E 01 1-35E-01

>e>F-n-1 SSF-01 4.51E-01 "7E-01 u orno

• ----------- 1 18-04023-16 TRG B105100AFSFC329CV 03/05/1814:18 4/5/2018 4/6/2018

• 1 Cesium-134 EPA901.1 Modified 1.38E-02 6_1SF-O, 6.18E-02 1.55E-01 u or,,o I

• --- ' TRG B105100AFSFC329CV 03/05/1814:18 4/5/2018 4/6/2018 I 18-04023 j Cesium 137 EPA901.1 Modified 3.97E+OO 5.20E-01 5.58E 01 2.64E 01 cC,<c

-,c TRG TRG B105100AFSFC329CV 03/05/18 14:18 03/05/1814:18 4/5/2018 ; 416/2018 , 18-04023 4/5/2018 415/2018 416/2018 , 18-04023 4/6/2018 18-04023

,_;,;;_;~~-~l~~J EPA901.1 Modified

-7.31E-O

~TI~-01 1.51E-01

-01 2.23E-01 4.50E-01 2.69E-01 2.23E-01 3.51E 01 1.80E 01 3.13E 01 u

u u

orno oC,,o

'" "" 1KG

" 03/05/18 14:18 i

-- -- "-°'° S SSF-00 u cC,<c

'" " TRG - 03/05/18 14:18 4/5/2018 I 4/6/2018 Holmium-166m EPA 901.1 Modified

'"""-°'

1.90E-01 1.49E-01

• - ,sc:o, TRG TRC

" -- CV 03/05/1814:18 03/05/1814:18 4/512018 4/6/2018 "-°'°

4/5/2018

• 416/2018 i 18-04023 Iodine 129 EPA 901.1 Modified EPA 901.1 Modified

-4 ""-°'

6.98E+OO

-,;~;;;,;,

2 1'F_O,

OOC+OC .

1.66E-01 0 OOC+OC u orno 18-04023-16 TRG -

" CV 03/05/18 14:18 4/5/2018

• 416/2018 "-°" - EPA 901.1 Modified 2.16E-02 , rnF-01 1.16E 01

• 1.89E 01 u

--';~;,;**--*

- 1 >OF-01 u

-,c

'"" C

" 03/05/1814:18 4/5/2018 4/6/2018 "-°'"" EPA 901.1 Modified -4.53E-02 1.20E-01 1.42E-01 18--04023-16 1KG TRG B105100AFSFC329CV 03/05/1814:18 03/05/18 14:18 4/5/2018 4/5/2018 4/612018 416/2018 18-04023 18 04023 Lead-210 Lead-212 EPA901.1 MnrlffiPrl EPA901.1 Modrfied 1 SOE+OO 2.60E--01

, SSF+OC 222e-01 1.33E+OO 2.23E-01 2.31E+OO 3.22E-01

, u u

oCl/c orO,c 389&01 er-,.

18-04023-16

- TRG TRG B105100AFSFC329CV 8105100AFSFC329CV 03/05/1814:18 03/05/1814:18 4/5/2018 4/5/2018 4/6/2018 , 18-04023 4/6/2018 1R-040" Lead-214 EPA901.1 Modified EPA901.1 Modified O ""-01 1.11E-01 1.42E-01 3.92E-01 1.43E-01 8.24E-01 2.40E-01 1 u ornc

, SoF-<V 4 S1F-O,

-,c 8105100AFSFC329CV 03/05/18 14:18 4/5/2018 4/6/2018

'"-'"'°" EPA901.1 Modified 8.81E-01 2.90E-01 o, ""

,o

'-16 TRG 8105100AFSFC329CV 03/05/1814:18 4/5/2018 4/6/2018 '"-°'"' EPA901.1 Modified 4.77E-02 3.16E-01 3.16E-01 5.29E-01 u oC,,c

- -- , 04F+OO u oC!/o 18 04023 16 SFC329CV 03/05/1814:18 4/5/2018 4/6/2018 '"-°" " EPA901.1 Modified 1.79E+OO 1.80E+OO 2.95E+OO '

18-04023 Thallium-208 EPA901.1 Modified 2.46E-01 2.75E-01 2.75E 01 5.20E-01 u orno 18-04023-16 TRG 8105100AFSFC329CV 03/05/18 14:18 4/5/2018 4/6/2018 EPA901.1 -'.38E-01 1.58E+OO 1.58E+OO **: 7.84E-01 u

' pCi/g 18--04023-16 j TRG B105100AFSFC329CV 03/05/1814:18 4/5/2018 4/6/2018 I 18-04023 Uranium 235 ~~,.,.,;t;,,,-1 CU=Counting U ncerta inty;CSU=Combined Standard Uncertainty ( 1-sigma); M DA=Min imal Detected Activity; LCS=Laboratory Control Sam ple;MBL=Blank: DUP=Duplicate; TRG=Nonnal Sam pie; DO=Duplicate Orig in al; U=Non-detect NE CAL ON 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[223]

Printed: 4/30/2018 3:19 PM Page 19 of 22 Report TO' Worn Order Details*

Eberline Analytical _____ __Giza Patricia ,.

SDG.* ' 18-04023

' _Zion Solutions,_ LLC 677118

---

--------- ---- -------- --- Purchase Order:

. i Final Report of Analysis 1--

101 Shiloh Blvd

' ENVIRONMENTAL Zion, IL 60099 Sample Matrix: , ~u I

L,b ID l Sample Type '

Client ID Sample Date Receipt Date Analysis Date Batch ID i'

Analyte Method I

Result cu ' CSU MDA , Qualifier i Report Units 18-04023-17 TRG

' 8105100AFSFC332CV 03/05/1814:05 4/5/2018 4/6/2018 18-04023 Actinium-228 EPA901.1 Modified 3.04E-01 3.61E-01 3.61E-01 ' 6.37E-01 ' u PC!IQ 18-04023-17 TRG B1D5100AFSFC332CV 03/05/1814:05 4/5/2018 4/6/2018 18-04023 Silver-108m EPA 901-1 Modified 2.13E-02 6.79E-02 6.80E-02  ! 1.39E-01 u ,c,,

--*-~--~-" "*-*"

18-04023--17 TRG B105100AFSFC332CV 03/05/1814;05 4/5/2018 ; 4/6/2018 18-04023 Americium-241 EPA901.1 Modified -5.26E-01 2.57E-01 2_59E-01 2.33E-01 u - oCilo 18-04023--17 TRG B105100AFSFC332CV 03/05/1814:05 41512018 4/6/2018 18-04023 Barium-133 EPA901.1 Modified 1.34E-02 6.84E-02 6.84E-02 2.27E-01 u - oCi/o 18-04023-17 TRG B105100AFSFC332CV 03/05/1814:05 4151'018 4/6/2018 18-04023 Bismuth-214 EPA 901.1 Modified 7.40E-01 ,AOE-01 2.43E-01 I 4.07E-01 '

' °' ,m 18-04023-17

---

TRG B105100AFSFC332CV 03/05/1814:05 4/5/2018 4/smrn , 18-04023 Cobalt-60 EPA901_1 MOdllled 7.43E-02 8.48E-02 8.49E 02 1.59E 01 u . pCi/o 18-04023--17 TRG B105100AFSFC332CV 18-04023 Cesium-134 u li?ii~t~:n:~~ii~

EPA 901.1 Moditiect 2.55E-02 5.65E-02 5.65E-02 I 1.52E-01 i pCl/g 18-04023--17 TRG 8105100AFSFC332CV I 1. E 01 3.15E 01 3.23E 01 i ---;;c1i; . __

18-04023-17 TRG B105100AFSFC332CV 18 04023 EPA901.1 Modified -3.25E-02 3.82E-01 3.82E-01 3_31E-01 , u oCilo 18--04023 17 TRG B105100AFSFC332CV 03/05/1614:05 4/5/2018 ; 4/6/2018

• 18-04023 EPA 901.1 Modified 4.88E-03 2.58E-01 2.58E-01 1.74E-01 u oCi/o

• • -<**'"*-W*-

18-04023--17

-- TRG B105100AFSFC332CV 03/05/18 14:05 4/5/2018 4/6/2018 18-04023 EPA901.1 Modified 2.03E-01 1.69E-01 1.69E-01 I

2.93E-01 u pCi/o 18 04023 17 TRG B105100AFSFC332CV

---

. 03/05/1614:05 41512018 4/6/2016 18-04023 EPA 901.1 Modified 2. 01 1.60E-01 i 1.38E-01 u _J pCl/g 18-04023-17 l TRG i B105100AFSFC332CV 03/05/1614:05 41512018 4/6/2018 18-04023 lodine-129 1 EPA901.1 Modified 4.53E-02 1.42E-01 1.42E-01 1.91E-01 u - ;i:;;;

18-04023-17 TRG

• B105100AFSFC332CV 03/05/1814:05 41512018 4/6/2018 18-04023 Potassium-40 EPA901.1 Modtfied 7.28F*OO 2.02E+OO 2.05E+OO 2.29E+OO oCi/o 18 04023 17 TRG B105100AFSFC332CV 03/05/1814:05 41512018 4/6/2018 18-040?3 - EPA 901.1 Modtfied -3.70F-o, 9.35E 02 9.35E 02 ' 1.37E 01 u '

oCi/o -

18-04023-17 TRG B105100AFSFC332CV 03/05/18 14:05 4/5/2018 4/6/2018

• 18-0.0,S Niobium-94 EPA901.1 Modtfied -2.26E-02 9.27E-02 9.27E-02 1.29E-01 u pCi/g 18-04023-17 TRG 8105100AFSFC332CV 03/05/1814:05 4/5/2018 ' 4/6/2018 18 04023 Lead 210 EPA901.1 Modtfied 5.73E-02 1.74 E+OO 2.25E+OO u PCl/o

,c,,

R~'fnt~

1'

.. TRG 8105100AFSFC332CV B105100AFSFC332CV V 03/05/18 14:05 03/05/18 14:05 03/05/18 14:05 4/5/2018 . 4/6/2018 4/5/2018 ( 4/6/2018 4/512018

• 41612018 18 04023 18-04023 18 04023 Lead 212 Lead-214 Promethium 145 EPA901.1 Modtfied EPA901.1 Modffied EPA901.1 Modified 3.06E-01 8.58E-01 5 36F-02 1.49E-01 2.53E-01 1.77E-01 1.49E-01 2.57E-01 1.77E-01 '

4.24E-01 4.69E-01 2.40E-01 u

u oCi/o pCi/g TRC 8105100AFSFC332CV 03/05/1814:05 4'S1'018 4/6/2018 18-04023 Radlum-226 EPA901.1 Modtfied 7.40E-01 2.40E-01 2.43E-01 4.07E-01 pCi/g 1 IKC - -- 03/05/18 14:05 4/b/2018 416,,01' 18-04023 EPA901.1 Modtfied -1.21E 02 3.09E-01 3.09E-01 i 4.69E-01 u i oCl/o 18 04023 17 IKC - -- 03/05/1614:05 41512018 4161201' , 18-04023

' EPA901.1 Modtfied 4.04E+OO 1.96E+OO 1.99E+OO 2.89E+OO u oCl/o 18-04023-17 TRG B105100AFSFC332CV 03/05/18 14:05 41512018 4/6/2018 : 18-04023 Thallium-208 EPA901.1 Modtfied 2.23E-01 2.95E-01 2.95E-01 5.03E-01 u '

oCl/o 18-04023-17 TRG B105100AFSFC332CV 03/05/18 14"05 415"018 4/6/2018 18-040'3 Uranium-235 EPA901.1 Modtfied i 4.74E-01 1.06E+OO

' 1.06E+OO i 7.00E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Samp1e;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE

~ SERVl*-,:c"', FAX 865/483-4621

[224]

Printed: 4/30/2018 3:19 PM Page 20 of 22 Report To: Work Order Details:

Patricia Giza 18-04023 Eberline Analytical -* ------ ..

_Zion Solutions, LLC ___

SDG:

Purchase Order: 677118 Final Report of Analysis 101 Shiloh

---

----------------- Blvd An_a/y~/s r -

ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample '. Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date  : ID 1

Analyte Method Result cu CSU MDA . Qualifier!

Units 18-04023-18 TRG 8105100AFSFC345CV 02/07/18 10:45 4/5/2018 4/6/2018  ! 18-04023 Actlnium-228 EPA 901.1 Modified 1.34E-O. 3.54E-01 3-54E-01 6.01E-01 u pCilo 18-04023-18 TRG 8105100AFSFC345CV 02/07/18 10:45 4/5/201 018 '. 18--04023 EPA 901.1 Modrfied -8.38E-02 1.13E--01 1.13E-01 -

1.0SE-01  ; u I oCilo 18-04023-18 TRG B105100AFSFC345CV 02107/18 10*45 4/5/2018 4/6/2018 ; 18-04023 Americium-241 EPA 901.1 Modified -3.21E-01 2.31E-01 2.31E-01 2.28E-01 u oCi/o 18-04023-18 TRG 8105100AFSFC345CV 02101118 rn-,s 4/5/2018 4/6/2018 ; 18--04023 Barium-133 EPA 901.1 Modified -0 RSF-OS SSSF-0? S OSF-C, 1.99E-01 u oCilo 18-04023--18 Bismuth-214 o eOE-01 2.37E-01 5.44E-01 18-04023-18 TRG TRG  :

B105100AFSFC345CV B105100AFSFC345CV 02/07/18 10:45 02/07/18 10:45 4/5/2018 4/5/2018

<1/h//llltl 4/6/2018 I

i 1H--ll<lll/:1 ;

18-04023  ! Cobalt-60 EPA901.1 Modified EPA901.1 Modified 2.70E-02 7_95E--02 7.95E-02 1.23E-01 u  !

°'"'"

oCilo 18-04023--18 TRG B105100AFSFC345CV 02/07/18 10:45 4/5/2018 4/6/2018  ! 18-04023 Cesium-134 EPA901.1 Modified -5.06E-01 2.41E-01 2.43E--01 1.60E-01

• u '

oCilo 18-04023-18 ; TRG 8105100AFSFC345CV 02/07/18 10:45 4/5/2018 4/6/2018  : 18-04023 Cesium-137 EPA901.1 Modified 1 02E-01 7.76E-02 7.78F-02 2.35E-01 u oCi/o

-SSRF-07 '70F-CO u oCUo 18 04023--18 18-04023-18 TRG

,au

' B105100AFSFC345CV 8105100AFSFC345CV 02/07/1810:45 02/07/18 10:4-b 4/5/2018 '

4/5/2018 4/6/2018 4/6/2018 I 1R-040?~

1'-U40,0 EPA 901.1 Modified EPA901.1 Modified 2 94E-02 S.29E-01 Usc-m 1.79E-01 3.23E 01 1.61E 01 u

pCilo TRG 4/6/2018 I 18 04023 u 18 04023--18 18-04023--18 TRG

' 8105100AFSFC345CV B105100AFSFC345CV 02/07/18 10:45 02107'18 1OAS 4/5/2018 4151201" 4/6/2018 18-04023 Holmium-166m EPA 901.1 Modified EPA 9" ~

1.09E 01 E-02 1.61E 01 1.64E-01 1.61E 01 1.64E-01 2.73E 01 1.32E-01 u pCl/g pCi/g

'° TRG i B105100AFSFC345CV 02107/18 10A5 4/512018 4/612018 I 18--04023 Iodine 129 EPA901.1 Modified 3.56E-02 1.29E---01 1.29E---01 1.73E-01 u i oCi/o 18-04023-18  ! TRG B105100AFSFC345CV 02/07/18 10-4,; 4/5/2018 4/6/2018 18-04023 J Potassium-40 EPA901.1 Modified 5.52E+OO 1 S6F+OO 1.59E+OO 1.38E+OO . orno 18-04023-18 j TRG B10510DAFSFC345CV 02/07/18 lU:4-b

""'"" 4/6/2018 ' 18-04023 j EPA901.1 Modified 205E-02 9.50E-02 9.50E-02 1.58E-01 u ' oCilo i u 18-04023--18 TRG B10510DAFSFC345CV 02/07/18 10:45 4/5/2018 41512019 I 18-04023 Niobium-94 EPA901.1 Modified 3AOE-03 3.71E--02 3.71E-02 1.24E-01  !  ! oCilo

., TRG B10510DAFSFC345CV 02/07/18 10:45 41512018 4/612018 18-04023 Lead 210 EPA901.1 Modified 1.37E+OO 1.69E+OO 1_69E+OO 2.40E+OO

• u oCilo 0 :

., ' TRG

' B 1 0510DAFS FC345CV 02/07/1810:45 41512018 4/6/2018 I 18-04023 lead 212 EPA901.1 Modified 4.22E--01 1.61E 01 1.63E 01 3.16E 01

' ,Cua 0

TRG B10510DAFSFC345CV 02/07/18 10-4,; 4/5/2018 4/6/2018 18-04023 Lead-214 EPA901.1 MnrlifiP.rf 8.27E-01 2.55E-01 2.59E-01 4.03E-01 -

! ocI,o

<O so 1KG

• 0

- 02/07/1810:45 4/5/2018 4/6/2018 18 04023 Promethium 145 EPA901.1 MOd1t1ea 6_53E-02 1.59E-01 1.59E 01 2.23E-01 u

• pCi/g 1KG

' - - 02/07/1810:45 4/5/2018 4/6/2018 j 18-04023 Radium-226 EPA901.1 Modified 6.80E-01 2.37E-01 2.39E-01 5.44E 01 u

pCi/g

'° TRG TRG

' B105100AFSFC345CV B105100AFSFC345CV 02/07/1810:45 02/07/1810:45 4/5/2018 41512018 41512018 I 18-04023 416'2018 I 18 04023 Thorium 234 EPA901.1 Modified EPA901.1 Modified 1.61E-01 3.30E+OO 203E-01 1.88E+OO 2.03E-01 1.89E+OO 3.63E-01 2_81E+OO u PCI/o oCilo 18-04023 18 TRG

v 02/07/18 10:45 02/07/18111"'1">

41512018 4/6/2018 a1noo1R I

i 18 04023 1R-fl4!1/:1 Thallium 208 Uranium-235 EPA901.1 Modified EPA901.1 Modified 5-12E-01

-S64E-01 3.06E-01 1 n1F+OO 3.07E-01 1.01E+OO 5.72E-01 fi.63E-01 .

u u

pCl/g pCl/g 1KG - 0 C U=Counting Uncertainty;CSU=Combined Standard Uncertainty ( 1-sigma); MDA=Minima I Detected Activity; LCS=Laboratory Control Sam pie; MBL=Blank;DU P=Duplicate; TRG=Normal Sample;DO=Duplicate Original; U=Non-detect EBERLINE EBERLINE ANALYTICAL CORPORATION

~ ANA.LYTICAL 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[225]

Printed: 4/30/2018 3:19 PM Page 21 of 22 Report To* Work Order Details:

Patricia Giza SDG:i 18-04023 Eberline Analytical -*-- _ Zion Solutions,LLC *---***** *-----*----

• 1- - **-*----*-**

. . J'LJrcha.se_Orde~:-- 677118 -------- - - ---- --- ------ *-

Final Report of Analysis 101 Shiloh Blvd Analysis Category: i ___ ENVIRCJNM.J=._NTAL,__________ *-*-** _________ __

Zion, IL 60099 Sample Matrix:: SO I

Lab Sample Client Sample Receipt : Analysis  ! Batch Report Analyte Method Result cu CSU MDA Qualifier  !

ID Type ID Date Date  ; Date ID Units 18-04023-19 TRG B105100AFSFC347CV 02/12/1813:10 4/5/2018 4/6/2018 18-04023 Actinium-228 EPA901.1 Modified 6.31E-01 4.44E-01 4.45E-01 9.06E-01 U _P~-~-!L 18-04023-19 TRG B105100AFSFC347CV 02/12/18 13:10 4/5/2018 4/6/2018 18-04023 S!1ver-108m EPA 901.1 Modi,:"'::':. ___ , __:4~.7c4c:Ec-0~2c._!-~ ' =""c:::*°'

. :....; _1::*':'*:sE,-0:1:_;' __1:0,9~1,:Ec,0~1!-!-,-":U'.,.,,,-+----,"ec:c:":"s___

1 18-04023-19 TRG B105100AFSFC347CV 02/12/1813:10 4/5/2018 4/6/2018 18-04023 Americium-241 EPA901.1 Modified 7.67E-02 2_30E-01 2.30E 01 : 2.82E-01 U ' nr;/n 18-04023-19 TRG B105100AFSFC347CV 02/12/1813:10 4/5/2018 j_Q4Q23l-~3-- --- EPA 901-1 Mnnrt ..,n -9.90E-03 7.13E-02 7.13E 02  : 2.17E-01 U nrnn 18-04023 19 TRG , B105100AFSFC347CV 02/12/1813:10 4/5/2018 4/6/2018 18~4Q2:i-r-~~-t~214- EPA901.1 Modtfied 5.20E-01 3.12E-01 3.14E-01  : 5.82E-01 U nrnn 18-04023-19 TRG '. 8105100AFSFC347CV 02/12/1813:10 **4/~/2[)1-8 , 4/6/2018 18-04023 Cobalt-60 EPA901.1 Modified 8.11E-02 RROF-0? 8.81F-02 1.96E-01 U **; nr:T/n TR(.; i B105100AFSFC347CV 02/12/18 13:10 4/fi/?018 4/6/2018 , 18--04023 Cesium-134 EPA 901.1 Modtfie,d ,-+-*,':;:;,.02,~E-Oc:--2+---10?,:;20E,-;;-01:---f- ,1:'.2:::':E ,o,1___ , _"1.06:9E~-:Oc:-1--"-.:'.u,__ ,;,,,,,, ,",:': "?"-- l TR(;

• B105100AFSFC347CV 02/12/18 13:10 4/5/2018 4/6/2018 18-04023 Cesium 137 EPA 901.1 Modified  ?.95E+OO 4.56E-01 4 AClF-!11 3.15E-01 I nr:,in

,o TRG  : 8105100AFSFC347CV 02/12/18 13:10 4/5/2018 4/6/2018 1A-04/1-r, * °" EPA 901.1 Modified -2.72E-02 <i.27E-01 5.27E-01 4.26E-01 U i nr;1n 18-04023-19 TRG  : 8105100AFSFC347CV 02/12/1813:10 --4/512018: 4/6/2018 --,-ij~Q4Q23 EPA901.1 Modified -2.48E-02 3.64E01 3_64E-01 2.21E01 U *; ,.,ru~

TRG B105100AFSFC347CV 02/12/1813:10 4/5/2018 : 4/6/2018 1A-040rl ,__ EPA901.1 Mnrlifo:,rl 1.88E-01 2.37E-01 2.37E-01 3.40E-01 U  : nt'.iln 18---04023--19 TRG - B105100AFSFC347CV 02/12/1813:10 4/5/2018 4/6/2018 111-u411z, EPA901.1 Mnrlifo*rl -1.60E-01  ?47E-01 2.48E01  : 1.86E01 § U

• nr.un 18 04023--19 TRG  ; B105100AFSFC347CV 02/12/18 13:10 ,11,;nnrn 4/6/2018 18-04023 lodine--129 EPA 901.1 Mo,Cdm:,":c'c.,..+*-:2~,6~2=E~0:;1:__f-:2c,1~1E=-:0~1 *t 0 0

02~,,1,2;;E~--0':1:-y--'2~,0~1~E.:-0~1 __,1 ___ '.u'., ,,--,*- _ ".'.rn'".".. 1 1---1~8~0~4~0::23~-~19~+~T~R=G:_~*,, --'~B1:'o,,,*.1,:o'o'.,AF~S~F~C*~34~7~c*v,, ________ ""' -l--'0~2,11~2,11::8-'1::3-'1~0+~.'.".:

"';:":":::'°:_J_'4~/~6/;20,1::...,..::1*'.,-0::'*,0~2::_3+,P,2o~ta~s::si~o~m~-4:;0'...J--~E'.:PA:".0:1.1 Modffied 5.91 E+OO 1.81 E+::_00:_--4 ___:1=::*E,+~o:,o:_,__1:,,:"~E~+:,0:0._,i_ --- ,___': __ _>"::::;rn",__ -~

18-04023--19 TRG B105100AFSFC347CV 02/12/1813:10 4/5/2018 , 4/6/2018 i 18--04023 Manganese-54 EPA901.1 Modified 3.83E-02 1.48E-01 1.48E-01 1 2.49E-01 U T nrll~

18-04023--19 TRG 8105100AFSFC347CV 02/12/1813:10 4/~1?01R ! 4/6/2018 18--040?:. EPA901.1 Modified -3.66E-02 1.19E-01 1.19E-01 1.76E 01  : U nCl/n

• -~-- -

18-04023-19 TRG , B105100AFSFC347CV 02/12/1813:10 4/fil?01R  ! 4/6/2018 111-1i4u:,:1 lead-210 EPA901.1 Modtfied 2.87E+OO 140F+rm 1.41E+OO 2.68E+OO ' U _ nr.11n

~~-~~::'3-:=c1*':--1,- ;T~R=G=---+~B:1;0:,':1:=00~A~F.,s:,,F,:C:34:7::C'.:V+-,-----l-o~2,11~2,11.,,,_1::3-',1::o:,.f.:'~;",~0*1",__l_',,,,1,,.1::20,1,,,=--,--::'°*"":~""'~'~',+--'=Le::ad~-,",:":.. ..J*----:::E~PA:.:':01:.,1:M:::o:di~fi:':,+--= ':'°:,:"c:=:*°'-'--:'=2*"E=::-o_'.___1+-"',,':,E,:o,1'...f--'.:3:,3~5~E=,-0:1:---,'----u=----1---,:_"c;,~'."._"_~

_1_B~?,~~~~::19~f--~7~R_'G;(--~~B:'.10~5'.1' :O;O~A~F~S'.:F:Cc34C7~C::V'.:-- -----j___:0::2:/i1'.'.2:l.1'. s'.1~3:t1;O -+':l,5;/2~0'.:1"8__:__

18--0402319 TRG 8105100AFSFC347CV 0

02/12/1813:10 14~1,61::20::_1~8: +---::'°*,~"'

M<;J?n-1R T 416/2018 1

"~+..---:

1i:t_nAn?-ct Promethium 145 L,a:,~d-:2':214:::+--- --::E~PA:9;,:01,_,,1:M"o:di,l~fi,e,cdc __ ,-,- __ ';,:':o".c:,,**;°':c: ,,+--"

3~.'°~"-:""_'.___-j--C3'.,2~0::ECOC1 --'.i _,:4,,7.~7~E2-0'.:1__ Cic---::-- ___"cc:"':'."~

EPA901.1 M"o:dl::";':c'+---4--:1;,3~1~E~0~2'__,'.__}':'.',sc.'.:=:'.'.'."'.j-1'."~"c=-"'1c--f---=i:;'.7:'=0E,,io'.'.'.1____:____ :UC---_+---':::"rn*,,'-"-_-~

1 18-04023-19 TRG B105100AFSFC347CV 02/12/1813:10 4/5/2018 -f 4/6/2018 18-04023 Radium 226 EPA901.1 Modified 5.20E-01 3.12E-01 3.14E-01 5.82E-01 U pCi/g 18-04023-19 TRG 8105100AFSFC347CV 02/12/1813:10 4/5/2018 i 4/6/2018 -04023 '""' EPA901.1 Modlfied 1.25E 01 2.83E-01 2.83E 01 5.09E-01 U nr;,"

TRG 8105100AFSFC347CV 02/12/1813:  ; 4/6/2018 , 1R-o.:i.,r;:, T EPA901.1 Modified 2.74E+OO 2.05E+OO 2.06E+OO

• 3.15E+OO  ! U nrnn

-w~*

TRG  : 8105100AFSFC34,1,c_v, ____-----+-- 0311~,1~_:3:.~~ ,nm ,1/f;/?01R 1A-f1,1nT! , EPA901.1 Modtfied 3.18E-01 3.17E-01 3.17E 01 - 1',,29E-01 I U nr.i/n 18-04023--19 TRG 8105100AFSFC347CV 02/12/1813:10 5/2018 i ,rn:.nn18 1R-04023 Uranium 235 EPA901.1 Modtfied -1.66E-01 1.78E+OO 1.78E+OO 8.30E-01 U pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

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Printed: 4/30/2018 3:19 PM Page 22 of 22 Report To: Work Order Details*

Patricia Giza 18-04023 Eberline Analytical Zion Solutions, LLC SDG:'

, Order 1

~----------------*------------ --------*---- ... - ......

Final Report of Analysis 101 Shiloh Blvd ,. --'* *-'- ,,. ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so SampJf) ' Sample l Analysis Batch l Report Lab ID I Type Client ID Date Receipt Date Date ID Analyte Method Result cu  ; CSU MDA *Qualifier; Units 1

~:i 18-04023-20 TRG 8105100AFSFC348CV 02/12/1815:15 4/5/2018 4/6/2018 C 18-04023 Actinium-228 EPA901.1 Modified 1.75E-01 6.39E-01 6.40E-01 1.09E+OO u 18-04023-20 TRG 8105100AFSFC348CV 02/12/1815:15 4/5/2018 4/6/2018

• 18-04023 Si1ver-108m EPA901.1 Modified 3.46E-01 '. 1.98E-01 1.98E-01 2.81E-01 '

u '

TRG B105100AFSFC348CV 02/12/1815:15 4/5/2018 4/6/2018 18 04023 Americium 241 EPA901.1 Modified -4.77E-01

.. ,....... ,; ..__ 3.31E 01 3.32E 01 4.76E 01 u l orno

,o , 00 1KG B105100AFSFC348CV 02/12/1815:15 ' 4/5/2018 4/6/2018 18 04023 Barium 133 EPA 901.1 Modified 4.78E..01 __ 3.15E 01 3.16E 01 4.94E..01 u ' pCUg

,o > 00 02/12/18 15:15 4/5/2018 4/6/2018 ,s,O,MO Bismuth-214 EPA901.1 Modified 2.80E-01 4.59E-01  : 4.59E-01 7.66E 01 u  : cCi/c IRG B105100AFSFC348CV ' '

,, '  : *; ,;;c*;, i u

' " TRG ' B1051 OOAFSFC348CV 02/12/1815:15 4/5/2018 ; 4/6/2018 ' 18-04023 , Cobalt.60 EPA901.1 Modified 4.33E..02 2.46E 01 2.68E-01 '""'

" TRG B105100AFSFC348CV 02/12/1815:15 4/512018 4/6/2018 I 18-0402::J - EPA 901.1 Modified 2.53E-01 2.20E-01 0 ooc o, 3.73E 01 u '""'

18-04023-20 TRG B105100AFSFC348CV 02/12/1815:15 4/5/2018 4/6/2018 18-04023 Cesium-137 EPA901.1 Modified 2.16E-01

' 2.23E-01 2.23E-01 3.66E-01  : u £.Ci~~--

TRC B105100AFSFC348CV 02/12/1815:15 4/5/2018 4/6/2018 18-04023 - EPA901.1 Modified 6.51E 01 5.88E 01 u pCi/g

- ~(';/n ,.,

1KG B105100AFSFC348CV 02/12/1815:15 4/5/2018 4/6/2018 18-04023 EPA 901.1 Modified 3.00E-01 4.23E-01 4.23E 01 3.85E 01  ! u

,o , 00 1KG 8105100AFSFC348CV 02/12/1815:15 4/5/2018 4/6/2018 18,04023 EPA901.1 Modified 7.73E-01 3.47E-01 3.50E 01 5.63E 01 u orno

'" '" TRG 8105100AFSFC348CV 02/12/1815:15 415/2018 , 4/6/2018 I 18 04023 EPA901.1 Modified 2.44E 01 3.32E 01 3.32E-01 3.04E-01  ! u oCi/c 1 SCC+OC  ; SCC+CC u oC:,o SO , 00 TRG B105100AFSFC348CV 02/12/1815:15 415/2018 4/6/2018 "*°'"' lodine-129 EPA901.1 Modified 8.73E 01 2.24E+OO i orno 4/6/2018 , 18-04023 Potassium-40 EPA 901.1 Modified 1.41E+01 3.49E+OO 3.56E+OO 2,98E+OO i 18--04023 20 TRG 8105100AFSFC348CV 02/12/1815:15 4/5/2018

-;;*;*;; ' ,ca,,

" "' TRG 8105100AFSFC348CV 02/12/1815:15 4/5/2018  ! 4/6/2018 18 04023 EPA901.1 Modified 4.15E 02 1.73E 01 2.97E-01 u i 18--04023 20 TRG 8105100AFSFC348CV 02/12/18 15:15 4/5/2018 4/6/2018 1R.04C?e ' EPA 901.1 Modified 6.31E 02 1.77E~01 1.77F,01 2.67E-01 *1 u  : cCi/c 18-04023-20 TRG 8105100AFSFC348CV 02/12/1815:15 4/5/2018 4/6/2018 rn.MMO Lead*210 EPA 901.1 Modified -9.30E+OO 4.63E+OO 4 SSC+OC 6.18E+OO ( u oCilo 0 S<C.CC 1 u or.:,o

, 00 TRG i B105100AFSFC348CV 02/12/1815:15 4/5/2018 ; 4/6/2018 "*°'"" Lead,212 EPA901.1 Modified 6.46E-01 3.49E-01 5.76E*01  :

18--04023-20 TRG B105100AFSFC348CV 02/12/1815:15 4/5/2018 4/6/2018 18-04023 Lead-214 EPA901.1 Modified 4.51E-01 4.57E-01 4.58E 01 7.60E 01 u i """"

~;;c;, i 1.27E+OO **

u

" '" TRG " /CV 0211211815,15 4/512018 4/6/2018 18-04023 Promethium 145 EPA901.1 Modified 1.30E+OO 8.46E 01 '""'

" " TRG B105100AFSFC348CV 0?11?/1R 1515 4/5/2018 4/6/2018 , 18-04023 Radium 226 EPA 901.1 Modified 2.80E 01 4.59E 01 4SOF,01 7.66E-01 j u "! oC.i/c 18-04023 20 '"" B105100AFSFC348CV 02/12/1815:15 4/5/2018 : 4/6/2018 18-04023 EPA901.1 Modified 1.00E-01 5.80E-01 5.80E-01 8.69E 01 , u ' or:,,

18--04023-20 TRG B105100AFSFC348CV 02/12/1815:15 4/5/2018 4/6/2018 , 18-04023 Thorium-234 EPA 901.1 Modified -2.05E+OO 2.49E+OO 2.50E+OO 4.25E+OO I u ,c,,

18-04023-20 i lRG B105100AFSFC348CV

-.-----**~-- '

02/12/1815:15 4/5/2018 4/6/2018 18-04023 Thallium-208 EPA901.1 Modified 3.44E 01 5.75E 01 5.75E-01 i 9.95E-01 ' u or""

18-04023--20 TRG B105100AFSFC348CV 02/12/18 1<.*15 4/5/2018 4/6/2018 C 18-04023 Uranium 235 EPA901.1 Modified i.25E+OO 2.98E+OO 2.98E+OO 1.62E+OO ( u i pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect EBERLINE EBERLINE ANALYTICAL CORPORATION

~ ANALYTICAL 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[227]

~=: ZS-WM-131 Revision 0 ZIONSOLl!TIONS LLC Information Use An EnergySofutions Company REC'D APR O5 2018 Attachment 1 - Chain-of-Custody Form 1 - O4 Q 2 1 Sample ID Sampl Matrix Sample Type Sample Container Sample Date Sample Time Analysis Type Preseivative Remarks eLog Vol Unit Type Qty Bl05IOOAFSWC017CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck 1 0310712018 0935 5ROC/HTD NIA 0.0-0.5" I 01.65g B105100AFSWC041CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 0310712018 0925 5ROCIHTD NIA 0.0-0.5" 123.37g Bl05l00AFSWC057CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 0310712018 0910 5ROCIHTD NIA 0.0-0.5" 101.99g Bl 051 OOAFSWC088CV NIA CONCRETE CONCRETE 57.94 cni3 Puck I 0310712018 0855 5ROCIHTD NIA 0.0-0.5

I 05.94g Bl05100AFSWCIOICV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 0310712018 0725 5ROCIHTD NIA 0.0-0.5" 146.06g B105IOOAFSWC115CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 0310712018 1530 5ROCIHTD NIA 0.0-0.5" 94.29g B105100AFSWCI 16CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310712018 0840 5ROCIHTD NIA 0.0-0.5" 98.62g BI 051 OOAFSWC I 50CV NIA CONCRETE CONCRETE 57.94 c1n' Puck I 02121/2018 0840 5ROCIHTD NIA 0.0-0.5" 97.99g Bl05100AFSWCl51CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 0212112018 0920 5ROCIHTD NIA 0.0-0.5" 102.61g B105!00AFSWCl56CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 02121/2018 1330 5ROC/HTD NIA 0.0-0.5" 96.47g B105100AFSWC162CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 0211512018 1550 5ROCIHTD NIA 0.0-0.5" 90.81g B105IOOAFSWC163CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 02/1512018 1350 5ROCIHTD NIA 0.0-0.5" 97.73g B105100AFSWC! 79CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 0310712018 0710 5ROCIHTD NIA 0.0-0.5" 100.50g B105100AFSWC190CV NIA CONCRETE CONCRETE 57.94 cm* Puck I 0310612018 1300 5ROCIHTD NIA 0.0-1.0" 180.00g Bl05100AFSWC201CV NIA CONCRETE CONCRETE 57.94 cm-' Puck I 0310612018 1513 5ROCIHTD NIA 0.0-0.5" 96.68g BI 051 OOAFSWC2 I OCV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 0310612018 1440 5ROCIHTD NIA 0.0-0.5" 120.44g B105IOOAFSWC231CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 1430 5ROCIHTD NIA 0.0-0.5" 132.73g B105100AFSFC239CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0955 5ROCIHTD NIA 0.0-1.0" 209.92g BI 051 OOAFSFC250CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 0310612018 0940 5ROCIHTD NIA 0.0-0.5" 130.05g

[228]

ZS-WM-131 Revision 0 ZIONSOL[TTIONSrrc An Eriei-gySo!ulions Company Information Use Bl05100AFSFC255CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck 1 0310612018 1246 5ROCIHTD NIA 0.0-0.5" l, 134.31g Bl 051 OOAFSFC263CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck 1 0310612018 0930 5ROCIHTD NIA 0.0-0.5" 7 110.42g B 105 IOOAFSFC276CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck 1 0310512018 1342 5ROCIHTD NIA 0.0-0.5"

~ 122.73g BI 051 OOAFSFC282CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0852 5ROCIHTD NIA 0.0-0.5"

't 116.66g B 1051 OOAFSFC289CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1352 5ROCIHTD NIA 0.0-0.5" li 119.03g B1051 OOAFSFC293CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0210712018 1345 5ROCIHTD NIA 0.0-0S' It 132.53g B 1051 OOAFSFC300CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0211312018 1250 5ROCIHTD NIA 0.0-0.5" tJ 85.562g e Bl05100AFSFC316CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1358 5ROCIHTD NIA 0.0-0.5" 108.12g

,, Bl05100AFSFC321CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 02/13/2018 1410 5ROCIHTD NIA 0.0-0.5" 148.80g Bl05100AFSFC326CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0211412018 0815 5ROCIHTD NIA 0.0-0.5"

~ 134.35g BI05IOOAFSFC329CV NIA CONCRETE CONCRETE 57.94 crn3 Puck 1 0310512018 1418 5ROCIHTD NIA 0.0-0.5" 11 Bl 051 OOAFSFC332CV Bl05100AFSFC345CV NIA NIA CONCRETE CONCRETE CONCRETE CONCRETE 57.94 57.94 cm3 cm3 Puck Puck 1

1 0310512018 0210712018 1405 1045 5ROCIHTD 5ROCIHTD NIA NIA 115.08g 0.0-0.5" 123.51g 0.0-0.5"

\<< 115.27g Bl05!00AFSFC347CV NIA CONCRETE CONCRETE 57.94 crn3 Puck 1 02/1212018 1310 5ROCIHTD NIA 0.0-0.5" l'i 91.09g B 1051 OOAFSFC348CV NIA CONCRETE CONCRETE 57.94 crn3 Puck 1 0211212018 1515 5ROCIHTD NIA 0.0-0.5" 88.0lg Bl05100AFSFC354CV NIA CONCRETE CONCRETE 57.94 crn3 Puck 1 0210812018 1307 5ROCIHTD NIA 0.0-0.5" 110.07g Bl05100AFSFC363CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0740 5ROCIHTD NIA 0.0-0S 85.52g B 1051 OOAFSFC369CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1453 5ROCIHTD NIA 0.0-0.5" 150.58g BJ05JOOAFSFC375CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1431 5ROCIHTD NIA 0.0-0.5" 119.51g Bl05100AFSFC379CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0746 5ROCIHTD NIA 0.0-0.5" 135.29g Bl05100AFSFC383CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0740 5ROCIHTD NIA 0.0-0.5" 118.83g Bl05JOOAFSFC411CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0805 5ROCIHTD NIA 0.0-0.75 168.23g"

[229]

ZS-WM-131 Revision 0 ZI()NSOLUTIONSrrc An Er:ergySolutions Company 18-04023 Information Use Bl05100AFSFC433CV N/A CONCRETE CONCRETE 57.94 cm3 Puck 1 02/08/2018 1512 5ROC/HTD N/A 0.0-0.5" 130.93g Bl05\00AFSFC434CV N/A CONCRETE CONCRETE 57.94 cm3 Puck 1 02/08/2018 0930 5ROC/HTD N/A 0.0-0.5" 133.53g BI 051 OOAFSFC435CV N/A CONCRETE CONCRETE 57.94 cm3 Puck I 02/07/2018 1422 5ROC/HTD N/A 0.0-0.5" 152.36g B105 l00AFSFC436CV N/A CONCRETE CONCRETE 57.94 cm3 Puck I 02/14/2018 1030 5ROC/HTD N/A 0.0-0.5" 133.53g B!05!00AFSFC438CV N/A CONCRETE CONCRETE 57.94 cm3 Puck I 02/08/2018 1025 5ROC/HTD N/A 0.0-0.5" 130.93g Laborato1y: Date Submitted To Lab: Ship Container No.: Cooler Temperature: ~;_bill Number: Fut£~

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Co1ru11ents PO# 677118 7 day turnaround 5-ROC I HTD / H-3

[230]

EBERL.INE /'..\NALYTICAL. COF,POF,ATION 601 SCAF<BOF/0 l~Ot1D OM RIDGE. TENNESSEE 378:SO VICES PHO~IE (86:::i) L,81 **06t13 FAX (865) /483**4621 EBS-OR-43653 April 30, 2018 Patricia Giza Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099 CASE NARRATIVE Work Order# 18-04024-0R SAMPLE RECEIPT This work order contains twelve solid samples received 04/05/2018. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.

CLIENT ID LAB ID ' CLIENT ID LAB ID B 1051 OOAFSFC354CV 18-04024-04 B 1051 OOAFSFC4 l l CV 18-04024-10 B 1051 OOAFSFC363CV 18-04024-05 B 1051 OOAFSFC433CV 18-04024-1 1 B 1051 OOAFSFC369CV 18-04024-06 B 1051 OOAFSFC434CV 18-04024-12 B 1051 OOAFSFC375CV 18-04024-07 B 1051OOAFSFC435CV 18-04024-13 B 1051 OOAFSFC379CV 18-04024-08 B 1051 OOAFSFC436CV 18-04024-14 B 1051OOAFSFC383CV 18-04024-09 B 1051OOAFSFC438CV 18-04024-15 ANALYTICAL METHODS Total Strontium was analyzed using EIChroM Method SRWOl Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.

Gamma Spectroscopy was performed using EPA Method 901.1 Modified.

Laboratory qualifiers are as follows:

U - Result is less than the MDA.

ANALYTICAL RESULTS Combined Standard Uncertainty is reported at I-sigma value.

Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific.

MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.

Page 1 of 3

[231]

ANALYTICAL RESULTS CONTINUED TOT AL STRONTIUM Samples were prepared by acid digestion as appropriate for the matrix. Digested samples were acidified and were selectively extracted and precipitated. Precipitates were then mounted on 47mm filters. Filter was reweighed to determine aliquot size. Sample activities were determined by gas flow propo1iional counting.

Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are repo1ied from Total Strontium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.

TRITIUM A representative aliquot of each sample was equilibrated with tritium free water. Equilibrates were transferred into a round-bottomed distillation flask and attached to a single stage still. A portion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were then counted by beta liquid scintillation.

Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique.

Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.

NICKEL-63 A representative aliquot of each sample was placed into an appropriately sized beaker. Stable elemental Nickel carrier was added to each sample prior to digestion. Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.

Samples demonstrated acceptable results for all Nickel-63 analyses. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.

GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass/aliquot of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.

Page 2 of 3

[232]

ANALYTICAL RESULTS CONTINUED GAMMA SPECTROSCOPY CONTINUED Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. Cobalt-60 and Cesium-137 results demonstrated slightly high method detection limits. Some samples demonstrated results that are greater than the method detection limit. These results are reported from the Canberra Gamma Apex "Nuclide MDA Report" and are not positive. These results are qualified as non-detect (U).

The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Actinium-228 and Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Bismuth-214 replicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique.

Results for the Cobalt-60 and Cesium-13 7 laboratory control sample demonstrated an acceptable percent recovery.

CERTIFICATION OF ACCURACY I ce11ify that this data rep011 is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her

~ accuratenrified by the following signature.

\'v- "'-,,,)' -\-,

i ---*----*

M.R. McDougall Laboratory Manager Date: 4/30/2018 Eberline /\nalytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please visit http://eberlineanalytical.eom/ to provide us with feedback on our services.

Page 3 of 3

[233]

Printed: 4/30/2018 3:19 PM Page 1 of 16 Report To.- Work Order Details:

Patricia Giza 18-04024 Eberline Analytical ,. '

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Units

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• 1.87E>OO 5.44E+OO 2.17E+OO 2.18E>OO 3.87E+OO 3.82E+OO u i '""'

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" " 00 i B105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/11/2018 1'-D.0?4 Tritium LANL ER 210 Modified 2.93E+OO 2.01E+OO 2.02E+OO 1 3.33E+OO u oCilo

" TRG B105100AFSFC363CV 03/06/18 07:40 4/5/2018 4/11/2018 18 04024 Tritium LANL ER 210 Modified 3.51E*01 2.09E+OO 209E>OO 3.58E>OO u 1KG I

8105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/11/2018 18,04024 Tritium LANL ER-210 Modified 4.16E,01 1.66E+OO 1.66c>UU ' 2.83E>OO u '"'"

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" B105100AFSFC375CV 03/05/18 14:31 4/5/2018 4/11/2018 18-04024 Tritium LANL ER-210 Modified *1.27c>OO 1.85E>OO 1.B5c>OU 3.25E>OO 1KG i

<O 18-04024-09 1KG TRG B105100AFSFC379CV B105100AFSFC383CV 03/06/18 07:46 03/06/18 07:40 4/5/2018 4/11/2018 18 04024 4/5/2018 , 4/11/2018 I 18-04024 Tritium Tritium LANL ER 210 Modified LANL ER-210 Modified

• 4.16E*01

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' pCilg oCi/o 18-04024-12 TRG 8105100AFSFC434CV 02/08/18 09:30 4/5/2018 4/12/2018 18-04024 Tritium LANL ER 210 Modified 3.13E-01 1.87E+OO 1.87E+OO - <\")(11-+(l!l

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18-04024-13 TRG 8105100AFSFC435CV 02/07/18 14:22 4/5/2018 4/12/2018 ; 18-04024 Tritium LANL ER 210 Mod1hed 6.72E-01 1.98E,OO 1.98E+OO '4<Hrn, u

,c,1, 18-04024-14 TRG B105100AFSFC436CV 02/14/18 10:30 4/5/2018 : 4/12/2018 ' 18-04024 Tritium LANL ER-210 Modified 1.51E-01 1.80E>OO 1.80E+OO ; 3.09E>OO u '

18--04024-15 TRG B105100AFSFC438CV 02/08/1810:25 4/5/2018 , 4/12/2018 180)4024 Tritium LANL ER-210 Modified 1.86E>OO 206E>OO 2.06E+OO 3.45E+OO u oCilo

--~------*-* '

18--04024-01 LCS KNOWN 04/05/18 00:00 4/5/2018 4/10/2018 :

' 1X--l14ll,'4 Nickel-63 ASTM 3500-Ni Modified 1 4SF,OS 4 '4F,01 ' pCi/g 18--04024-01 LCS SPIKE 04/05/18 00:00 4/o/2Ultl 4/1U/2U18 18-04024 Nickel-63 ASTM 3500-Ni Modit1ed 1.45E>03 8.67E+OO 8.56E+01 1.92E+OO oCilo 18-04024-02 MBL BLANK 04/05/18 00:00 41512018 4/10/2018 ; 18--04024 Nickel-63 ASTM 3500-Ni Modified 8.18E-01 1.17E>OO 1.17E+OO 1.97E>OO u  ! oCi/o 18--04024---03 DUP B105100AFSFC354CV 02/08/18 1;1*07 41512018 4110/2018 ' 1R,ll40?4 Nickel,S3 ASTM 3500-Nf Mnctififld 1.87E+OO 1.14E+OO 1.14E+OO 1.88E+OO  ; u ' oCilo 18-04024-04 DO B105100AFSFC354CV 02/08/1813:07 4/5/2018 4/10/2018 , 18--04024 Nickel 63 ASTM 3500 Ni Modified s.s,a-u, 1.13E+OO 1.13E+OO 1.91E+OO u oCi/o

---

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,c,1, 18--04024-05 TRG  ; B105100AFSFC363CV 03/06/18 07:40 4/5/2018 ; 4/10/2018 ; 18-04024 Nickel-63 ASTM 3500-Ni Modified 3.43E>OO 1.12E+OO 1.14E+OO 1./Sc>UO RG B105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/10/2018 ' 18--04024 Nickel 63 ASTM 3500 Ni Modified 4.12E-01 9.75E*01 9.75E,01 1.65E+OO u  ! oCilo 18-04024-07 TRG B105100AFSFC375CV 03/05/18 14:31 41512018 4/1012018 18-04024 Nickel-63 ASTM 3500-Ni Modified 201E>OO 1.13E,00 1.14E>OO 1.86E+OO oCilo 18-04024-08 TRG B105100AFSFC379CV 03/06/18 07:46 41512018 4110/2018 18-040?4 Nickel,63 ASTM 3500-Ni MnrlifiP.r! 1.84E+OO 1.08E+OO 1.08E+OO 1.77E+OO ' pCilg

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18-04024-09 TRG B105100AFSFC383CV 03/06/18 07:40 4WU1' 4/1U/2U1' 1'*U4U'4 Nickel,63 ASTM 3500-Ni Mn<11t1M 7.14E-01 9.28E-01 9.29E-01 1.56E+OO u ' £Cilg -

18-04024-10 TRG B105100AFSFC411CV 03/06/18 08:05 4/5/2018 : 4/10/2018 18,04024 Nickel-63 ASTM 3500-Ni Modified 1.30E*OO 1.04E*OO 1 05E>OO , 1.74E+OO u i pCi/9 18-04024-11 TRG B105100AFSFC433CV 02/08/1815:12 4/5/2018 4/10/2018 18-04024 Nicke1*63 ASTM 3500-Ni Modified 5.91E>02 5.52E>OO 3.52E+01 : 1.86E>OO ,c,1, i

18-04024-12 TRG B105100AFSFC434CV 02/08/18 09:30 41512018 ' 4111/2018 18-04024 Nickel,63 ASTM 3500*Ni Modified 8.26E>01 2.17E+OO 5.32E+OO 1/Uc>UO pCi/o 18-04024-13 TRG 8105100AFSFC435CV 02/07/1814:22 4/5/2018  ! 4/11/2018 18,04024 Nickel-63 ASTM 3500-Ni Modified 5.00E*01 1.01E+OO 1.01E+OO 1.72E>OO u oCi/o "18-04024-14 TRG B105100AFSFC436CV 02/14/18 10-:111 4/5/2018 I 4/11U!lltl 18-04024 Nickel-63 ASTM 3500-Ni Modified 9.96E,01 1.19F,OO 1.19E,OO 200E,OO u ' oCilo 1.13E+OO 1.16E+OO 1.80F,OO 18-04024-15 TRG B105100AFSFC438CV 02/08/1810:25

• """" 4/11/2018 18-04024 Nlckel-63 ASTM 3500-Ni Modified 3.82E+OO pCi/g CU=Counting Uncertainty; CSU=Combined Standard Uncertainty (1-sigma);M DA=Minimal Detected Activity; LCS=Laboratory Control Sample; MBL=Blank;DUP=Duplicate; TRG=Nonnal Sample; DO=Ouplicate Original; U=Non-detect EBERLINE I EBERLINE CAL CORPORATION

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[234]

Printed: 413012018 3:19 PM Page 2 of 16 Reporl To: Worl< Order Details:

Patricia Giza 18-04024 Eberline Analytical ____ Zion_Solutions, LLC SDG:

Purchase Order: ;

677118

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Type Client ID Sample Date i Receipt I Analysis Date I Date Batch ID Analyte Method Result 1 cu CSU MDA  :

Qualifier Report Units oC;>c 18 04024-01 LCS I KNOWN 04/05/18 00:00 415/2018 411112018 18-04024 EIChroM SRW01 Modified 5.04E+01 2.82E-01 18-04024-01 LCS SPIKE 04/05/18 00:00 4/5/2018 4/11/2018 18-04024 Strontium-90 -EIChroM SRW01. Modified 3.95E+01 1.68E+OO 139E+01 7.33E-01 oCilc 18-04024-02 MBL DUP BLANK S105100AFSFC354CV 04/05/18 00:00 02/08/18 13:07 02/08/18 n*n7 4/5/2018 4/5/2018 4/11/2018 4/11/2018 41512018 , 4111/2018 C

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18-04024-09 TRG B105100AFSFC383CV 03/06/18 07:40 4/5/2018 4/11/2018 18-04024 Strontium-90 EIChroM SRWD1 Modffied 7.80E-02 3.22E-01 3.23E-01 5.70E-01  ! u eCi/c

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18-04024-10 TRG  ! B105100AFSFC411CV 03/06/18 08:05 4/5/2018 4/11/2018 18 04024 Strontium 90 EIChroM SRW01 Modified , 3.61E 01 3.89E 01 u erne

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• 18-04024-13

"" TRG TRG i

J B105100AFSFC434CV B105100AFSFC435CV 02/08/18 09:30 02/07/18 14:22 4/5/2018 4/5/2018 4111rm11< ' 18 04024 4/11/2018 ' 18-04024 Strontium 90 EIChroM SRW01 Modified ,

EIChroM SRW01 Modified 9.17E 02 3.87E-01 siiE:01

- ,ooE:ai

- i22E:01 5.BBE-01 6.68E-01

- u u

ernc orno

• -*~*----*--

18 04024 14 TRG 8105100AFSFC436CV 02/14/18 10:30 4/512018 4111/2018  ! 18-04024 Strontium-90 EIChroM SRW01 Modified -1.92E-01 3.97E-01 4 OSF-01 7.39E-01 u -""*

18-04024-15 TRG i 8105100AFSFC438CV 02/08/18 10:25 4/5/2018 4/11/2018 I 1fW40?4 Stronlium-90 EIChroM SRW01 Modified SAOE,02 3.45E-01 3.46E-01 6.13E-01 , u oCile

---

**-*--*** I

, CSFoM ora,c 18-04024-01 LCS  ! KNOWN 04105118 00:00 4/5/2018 . 416/2018 18-04024 Cobalt-60 EPA901.1 Modffied 2.71E+D2 18-04024-01 LCS - KNOWN 04/05/18 00:00 /2018 18-04024 Cesium 137

.... ~-

EPA901.1 Modified 1.69E+02 6.75E+OO I oC:,o 18-04024-01 LCS  ! SPIKE 04/05/18 00:00 l <11,;nnrn 41612018 18-04024 Cobalt-60 EPA 901.1 Modified 2.69E+02 1-54E+01 2.07E+01 2.01E+OO  : oCilc

---

, OSFom  !

18--04024 01 LCS  ! SPIKE 04/05/18 00:00 4/5/2018 ; 4/6/2018 18-04024 Cesium-137 EPA901.1 Modified 1.91E+02 2.29E+01 2-49E+01  : pCl/g CU=Counting Uncertainty; CS U=Combined Standard Uncertainty ( 1-sigma); MDA=Minimal Detected Activity; LCS=La boratory Control Sample; MBL=Blank;DU P=Duplicate;TRG=Normal Sample; DO=Duplicate Original; U=Non-detect

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EBERLINE SERV,CES 601 SCARBORO ROAD OAK RIDGE, TN 37830

[235]

865/481-0683 FAX 865/483-4621

Printed: 4/30/2018 3:19 PM Page 3 of 16 Report To Work Order Details:

Patricia Giza 18-04024 Eberline Analytical --- . ,-~~*o*www** * * -

• Zion Solutions, LLC

• • w

• SDG:

Purchase Order.: 677118

---

-------------~-----* -

Final Report of Analysis 101 Shiloh Blvd ENVIRONMENTAL

--*--w,,-M,.WOw>.-WWW*WwWwW-ww,ww-***

---**"- ---*-*An_~lysis Category:

Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample I Receipt  ! Analysis Batch

' Report ID Type ID Date Date Date  !

i ID Analyte Method

Result I cu I CSU I

MDA

• Qualifier Units 18--04024-02 MBL BLANK 04/05/18 00:00 4/5/2018 ' 4/6/2018 : 18--04024 Actinium-228 EPA901.1 Modified ,__

7.63E-02 - 1.25E-01 1.25E-01 2.46E-01 - u I oCilo 18--04024-02 MBL BLANK 04/05/18 00:00 4/5/2018 4/6/2018 ' 1 R-040?4 Si1ver-108m EPA901.1 Modified 1.48E-02 3.77E-02 3.77E--02 '

6.16E-02 u i oCilo u orno 18-04024-02 MBL BLANK 04/05/18 00:00 4/5/2018 4/6/2018 18-04024 Americium-241 EPA 901.1 Modified 6.60E-03 2.67E-02 2.67E-02

' 6.65E-02 u

,c,10 18-04024-02 MBL BLANK 04/05/18 00:00 4/5/2018 4/6/2018 1B-04024 Barium-133 EPA901.1 Modified i -1.57E-02 6.09E-02 6.09E-02 6.26E-02 18-04024-02 MBL BLANK

• "'-M ___ ,_,_. _ _._M~**>

04/05/18 00:00 4/5/2018 4/6/2018 18-04024 Bismuth-214 EPA 901.1 Modified 6.57E-03 1_20E-01 1.20E-01 i 1.72E-01 u

'i oCilo

' u 18-04024-02 18-04024-02 MBL MBL BLANK BLANK 04/05/18 00:00 04/05/18 00:00 4/5/2018 4/5/2018 4/6/2018 4/6/2018 18-04024 18-04024 Cobalt-60 Cesium-134 EPA 901.1 Modified EPA901.1 Modified

-3.36E-02 2.90E-02 4.53E-02 5_31E-02 4.53E-02 5.31E-02 i' 6.05E-02 6.94E-02 u 'i oCilo oCilo 18-04024-02 MBL BLANK 04/05/18 00:00 4/5/2018 4/612018 18-04024 Cesium-137 EPA 901.1 Modified 5.08E-02 4?0F-02 4_21E-02 i 8.33E-02 ' u ,cu, 10

---

MBL BLANK 04/05/18 00:00 4/5/2018 4/6/2018 18 04024 EPA 901.1 Modified

1.17E-01  : 1_19E-01 i 1.19E-01 9.42E-02 ' u u

' pCUo 1- MBL BLANK 04/05/18 Ov.vv 1B 18-04024 EPA901.1 Modified 1.56E 02 f 1-11 E-01 i 1.11E-01 ' 4.55E-02 ' oCl/o

,o

-- MBL BLANK 04/05/18 00:00 4/5/2018 4/6/2018 . 18-04024 EPA901.1 Modified 1.17E 02 - 4.49E-02 4.49E-02 I 6.82E-02 u oCl/o

-- MBL BLANK 04/05/18 00:00 4/5/2018 4161201B 18 04024 Holmium 166m EPA 901.1 Modified 72E-02 7.86E-02 7.86E-02 3.97E 02 u

- oCi/o

• - MBL ' BLANK 4151201B 4/612018 18-04024 I Iodine 129 EPA901.1 Modified 1.90E-02 1.63E-02 1.63E-02 2.65E-02 u i orno

,o

---

MBL BLANK --- 4151201B 4/612018 18-04024 : Potassium--40 EPA901.1 Modified 9.47E 02 I

4-24E-O; 4.24E-01 I 7.11E-01 u i

""'°

,o MBL BLANK 04/05/18 00:00 4/5/2018 4/6/2018 18 04024 -* EPA901.1 Modffied -1.42E-02 i 4.69E-02 4.69E-02 I 6.37E-02 I u PCilO

-02 MBL BLANK 04/05/18 00:00 4151201B , 4/6/2018 18-04024 Niobium-94 EPA901.1 Modified 5.18E 03 i 4.04E-02 4.04E-02 I

6.98E-02 u __ J _ pCllg

' 3_24E-01 3_24E-01 u oCilo

)2 M

MBL MBL BLANK BLANK 04/05/18 00:00 04/05/18 00:00 4/5/2018 4/5/2018 : 4/6/2018

'j 18 04024 18-04024 Lead-210 lead-212 EPA901.1 Modffied EPA 901.1 Modffied 8.13E-02 2.52E 02 4 ?RF-0? 4 ?RF-0?

' 5.03E--01 7.03E-02 u r ;i:,io

~, -

,o MBL BLANK /2018 : 18-04024 Lead-214 EPA901.1 Modffied 1.19E 02 h 1s3F-O? 6.33E-02 1.03E-01 i u  ! orno

• - MBL BLANK 18 04024 Promethium-145 EPA901.1 Modified ,2.43E-03 3_24E-02 3.24E 02 4.86E 02 u 18 04024-02 **-* -

• 11 NK 04/05/18 00:00

---

4/5/2018 : 4te12018 I* 18-04024 Radium-226 EPA 901.1 Modffied 6.57E-03 UOE-01 1.20E-01 1.72E-01 u '

pCi/g u

18-04024-02 18 04024-02

~t-+1~

MBl 04/05/18 00:00 04/05/18 00:00 04/05/18 00:00 4/5/2018 4/5/2018 4/5/2018 4/6/2018 ; 18-04024 4t6t2018 I 1s...04024 4/6/2018 ' 18 04024 Antimony-125 Thorium-234 EPA901.1 Modffied EPA 901.1 Modffied EPA 9011 Modilied

-1.07E-01

-2.23E-02 2.53E-03 1.32E-01 4.28E-01 1.23E-01 1.32E-01 4.28E-01 1.23E-01 I 1.58E--01 6.42E-01 1.71E 01 u

u oCilo oCilo PCilQ BLANK " i

- -- MBL BLANK 04/05/18 00:00 4/512018 4/6/2018  ! 18-04024

' EPA901.1 Modified 1.54E 01 3.74E-01 3.74E-01 2.12E-01 u ' pCi/g CU=Countlng Uncertainty;CSU=Comblned Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[236]

Printed: 4/30/2018 3:19 PM Page 4 of 16 Report To: Work Order Details:

Patricia Giza 18-04024 Eberline Analytical -* *-*-**--- --********----****

.....*. Zion. Solutions, LLC. ---.-----------*------ --,------* -----*

SOG.*

Purchase Order:

677118

"--/,,_;_ - ---------------*--------* ---- -*-*----------~----------*------------------ ..*

Final Report of Analysis 101 Shiloh Blvd ' ' .

ENVIRONMENTAL Zion, IL 60099 Sample Matrix: ; so Lab Sample I

Client Sample Receipt Analysis i Batch 'i Analyte Method I Result I cu CSU MDA  : Qualifier:

Report ID

' Type ID Date Date Date I ID

! Units 18-04024-03 / DUP i B105100AFSFC354CV 02/08/18 13:07 4/5/2018 ; 4/6/2018 i 18-04024 ! Actinium-228 EPA901.1 Modified 5.94E-01 3.70E-01 3.72E-01 ' 7.19E-01 u i oCi/o 18-04024-03 ; DUP B105100AFSFC354CV 02/08/1813:07 4151,018 1 4/6/2018 . 18-04024 1 Silver-108m EPA901.1 Modified 6.09E-03 3.90E-02 3.90E-02 i 1.28E-01 u I oCi/o

.. - B105100AFSFC354CV 02/08/18 .,,,,,,, 4/6/2018 EPA901.1 Modified -401E-01 2.43E 01 2.44E 01 i 2.35E 01 u cCi/c I* """ i

=~*11

'"*'""" i uue B105100AFSFC354CV 02108/18 1:n)f 4/0,,U>S 4,SUO,S 18-04024 Barium-133 EPA901.1 Modified 2.93E-02 7.20E-02 7.20E-02 2.06E-01 u i 18-04024-03 DUP i B105100AFSFC354CV 02/08/1813:07 4/512018 41612018 18-04024 Bismuth-214 EPA901.1 Modified 5.12E-01 2.71E-01 2.72E-01 4.00E-01 i oc,10 e-*****

18--04024-03 DUP . B105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 18-04024 Cobalt-60 EPA901.1 Modified -2.13E-02 1.00E-01 1.00E-01 .

1.44E-01 u oCilo 18-04024-03 DUP ' B105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 18-04024 Ceslum-134 EPA901.1 Modified ' 3.26E-02 5.31E--02 5.32E-02 i 1.59E-01 u ' oCl/o 18-04024-03 DUP B105100AFSFC354CV 02/08/1813:07 4/5/2018 4/6/2018 18-040?4 Cesium-137 EPA901.1 Modified i 1.19E-01 1-12E-01 1.12E-01 ' 2.02E-01 u i oCi/o 18-04024 03 DUP B105100AFSFC354CV 02/08/18 13:07 4'0"° 4/6/2018 18-040?4 '"" EPA901.1 Modified i 1.0SE-01 1 RSF-01 1.89E-01 i 3.27E-01 u oCi/o 18-04024-03 DUP B105100AFSFC354CV 02/08/18 13:07

.. . 4/5/2018 4/6/2018 18 04024 ... 154 EPA901.1 Modified 1.64E-01 2.47E-01 2.47E-01 i 1.62E-01 u . pc,o 18-04024 03 DUP B105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 18 04024 '" EPA901.1 Modified i 1.15E-01 1.67E-01 1.68E-01 . 2.84E-01 u i pCi/p 18-04024-03 DUP B105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 18-04024 EPA901.1 Modified 9.96E-02 1.56E-01 1.57E-01 i 1.51E-01 u I

.. .. nllP 8105100AFSFC354CV 02/08/18 13:07 4151?018 4/6/2018 18-040?4 lodioo-1?9 EPA901.1 Modified ' 7.56E 02 1.38E--01 1.38E 01 ' 1.70E 01 u oCVo oCl/o 18-04024-03 DUP B105100AFSFC354CV 02/08/181::S:U/ 4/5/2018 4/6/2018 18-04024 Potasslum-40 EPA 901.1 Modified I 7.21E+OO 2.01E+OO 2.05E+OO  ! 2.14E+OO cCi/c 18-04024-03 DUP ' B105100AFSFC354CV 02/08/1813:07 4/5/2018 4/6/2018 18-04024 C EPA901.1 Modified ' 4.14E 02  ! 1.08E-01 1.08E-01 i 1.85E 01 u pCl/g 18 04024 03 DUP B105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 18-04024 Niobium--94 EPA901.1 Modified 4. 8.91E-02 I 1.52E-01 u oCl/o 18-04024-03 DUP B105100AFSFC354CV 02/08/1813:07 4/5/2018 4/6/2018 18-04024 Lead-210 EPA901.1 Modified ' 2.18E+OO 1.56E+OO 1.57E+OO I 2.38E+OO u oCVo 18-04024-03 18-04024-03 DUP DUP

' B105100AFSFC354CV B105100AFSFC354CV 02/08/1813:07 02/08/18 13:07 4/5/2018 4/5/2018 : 4/6/2018 4/6/2018 18-040?4 18-04024 Lead-212 Lead-214 EPA901.1 Modified EPA901.1 Modified 3.23E-01 6.22E-01 1.4SF-01 2.37E-01 1.46E-01 2.39E-01

. 3.43E-01 3.03E-01 u oCl/o cCi/c I

~ * .. M<*'

18 04024-03 i DUP B105100AFSFC354CV 02/08/18 13:07 4/5/2018 [ 4/6/2018 18-04024 . EPA 901.1 Modified ' 1.76E 01 1.63E-01 1.64E 01 . 2.46E 01 u OC"O 18-04024-03 DUP B105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 18-04024 EPA901.1 Modified

. 5.12 .71E-01 2.72E-01 '

4.00E-01 i oc,10 18--04024-03 DUP B105100AFSFC354CV 02/08/1813:07 415/2018 4/6/2018 18-04024 EPA901.1 Modified 7.11E-02 2.63E-01 2.63E-01 i 4.22E-01 u oCi/o 18-04024-03 DUP B105100AFSFC354CV 02/08/18 13:07 4151?018 4/6/2018 18-040?4 EPA 901.1 Modified 3.74E+OO 1.81E+OO 1 R?F+OO 2.81E+OO  : u oCi/o

.... I 1

,o

"" DUP B105100AFSFC354CV 02/08/1813:07 4/5/2018 [ 4/6/2018 18-04024 EPA901.1 Modified 4.82E-01 3.29E-01 3.30E-01 6.04E-01 u  ! pCl/o

'" "" DUP 8105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 1 18-04024 Uranium 235 EPA 901.1 Modified

' -1.04E+OO ' "0+00 1.17.-+nn 1 1.17i,.;_n1 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MOA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;OUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Orlginal;U=Non-detect

( -~

EBERLINE SEFIViCES

[237]

Printed: 4/30/2018 3:19 PM Page 5 of 16 Report To: Work Order Details*

Patricia Giza 18-04024 Eberline Analytical f,,,, ' ' "

Zion Solutions, LLC

"'C"""" """""

S/J/a

, Order.' 677118 Final Report of Analysis ~ 101 Shiloh Blvd

.. .,,,,,_,,"~ ... *~-***-----**-*-*--**-*----

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

• sn 1

Lab ( Sample CHent Sample Receipt i Analysis Batch '  ! Report ID I Type 10 Date Date Date ID Analyte Method Result CU CSU MDA  : Qualifier Units 18-04024-04 DO 8105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 18-04024 Actinium-228 EPA 901.1 Modifie,:d'.,,,j ..~6l.13:cc*::c:E*0::.1,.j.,:C3.::07~E~*:0~1-i-'3'.,.0:9'.:E~*0:1'....-~4~,8'.:00:E2,o~1.....j----*_:.,,.,",rn:,,."a ..

DO 8105100AFSFC354CV 02/08/1813:07 4/5/2018 i 4/6/2018 18-04024 Silver 108m EPA901.1 Modified fi.&1F-n~ 7.58E-02 7.59E-02 1.37E-01 U nr-;i,,

DO B105100AFSFC354CV 02/08/1813:07 4/5/2018 4/6/2018 18 04024 * . EPA901.1 Modtfied -4.14E-01 2.34E 01 2.35E 01 2.20E 01 U nr-,,,,

lJO B105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 18-04024 Barium-133 EPA 901.1 Modified -2.69E-02 "*ni:: n~ 5.23E 02 **2_~Q3E~Q1 U ~r;1~

DO 8105100AFSFC354CV 02/08/1813:07 214 EPA901.1 Modified 3.12E-01 '"':)f!F-01 2.29E-01 4.45E-01 U

'" DO B105100AFSFC354CV 02/ 18 04024 Cobalt-60 EPA 901.1 Modtfied 5.04E 02 9.01 E 02 ~ Cl1F-O? 1.56E-01 U '

18---04024-04 DO

• B105100AFSFC354CV 02/08/1813:07 4/5/2018 J 4/6/2018 18-04024 Cesium-134 EPA901.1 Modtfied 2.39E 02 5-44E 02 "'AA<="~ 1.73E-01 U tl~~

18-04024-04 DO S105100AFSFC354CV 02/08/1813:07 4/5/2018 4/6/2018 18-04024 Cesium-137 EPA901.1 Mmlifierl 1.31E-01 1.00E-01 1.01E-01 1.93E-01 U  :

18----04024 04 DO S105100AFSFC354CV 02/08/1813:07 4/5/2018 4/6/2018 18-04024 r. EPA901.1 Modified -1 "i?F.n1 2-47E-01 2-47E-01 3.60E-01 U

• nril.-.

18--04024-04 DO S105100AFSFC354CV 02/08/18 13:07 18-04024 r. EPA901.1 Modified -1.27E-01 ~:36E~Q1 2.36E-01 1.73E 01 U nr11 ...

Li:1s.~04~0J22~+co><4 18-04024-04 J =:Co,co,:

DO J isi11ooss1ico100AFAFCS~F<COi3~544C~V~*=====t~o~21".8,~'i'i~=

, 81D5100AFSFC354CV 02/08/1813:07

, ~..1,8.:*..o:*~0:02*: ..i*. E-~~~~~~~.~~~~-+-:E:P?A~s~o~1..1,: ,M*:::':"~:---f-"7 18-04024 Holmium-166m EPA901.1 Modified 2.12'.;;E;~.01:-f.~{

-1.27F-01

";;F.~011~+-1.:*;'8,:E~*~o.~1 - ,'.a',*'~'~E~.0~1-/--""uc-+ _ . ."""~?""'......

1.59E-01 1.59E-01 i 1.42E-01 U ' *:11n

• --1,,.*"0'*'0"2"w*'""*-"o"o--*--,,s*1-os*1-oo*A**,*s***,*c*,*,****c*v*.. '""'"""**0*"21"os"1*1,*,* ,..:,,01"* 41512018 , 4151201"8-~ .1"8".0"*"0"2*-: --,,-,-,,-,*. 1***2**s* ** ***I ;E,;P;'A,****s"o'1'1., :M*:,:,;ifi;a:,c, , .. , -.,,'.,;';1;:";

E,o:c2* +:, :' .44?~E*o""'1+""1~*'*:E-'0'1":cc.+1."8:1cE:*;;0;-1-+.. ,-cuc--* - ,:,,,,,!" *

• I

, UU B105100AFSFC354CV 02/08/1813:07 4/5/2018 4/6/2018 1R.n.&n?,1 Potassium-40 EPA901.1 Modified CJ.16E+OO ?Mi:+nn 2.48E+OO i 2.75E+OO .

DO B105100AFSFC354CV 02/08/18 13:07 4/5/2018 , 4/6/2018 18-04024 EPA 901.1 Modified '5.92E-02 **1:*10E~61 1.10E-01 *: 1.91E-01 u

' " DO B105100AFSFC354CV 02/08/1813:07 4/5/2018 4/6/2018 18-04024 Niobium 94 EPA 901.1 Modified 2.37E-02 R 77F-m 8.77E-02 1-_32F=ci"1 , u 18-04024-04 DO B105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 18--04024 Lead-210 EPA 901.1 Modified  ? 81F+OO 1.52E+OO i 1.53E+OO 2.39E+OO ' u °' ""

18,04024-04 DO B105100AFSFC354CV 02/08/1813:07 4/5/2018 416/2018 18--04024 Lead 212 EPA901.1 Modified '.1..95E-01 1.82E-01 1.83E01 2.81E01  ;

,o 02/08/1813:07 4/5/2018 : 4/612018 1RJMn?A Lead-214 EPA901.1 Modified 4.78E-01 ~.78E-01 2.79E 01  : 4.24E-01  ;

DO 8105100AFSFC354CV

'" '" DO  : 8105100AFSFC354CV 02/08/18 13:07 4/5/2018 : 41612018 18-04024 EPA 901.1 Modified _P. ooi:_M **1*:*1sE~o*1 ,,ee.61 u 18-04024-04 DO B105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 1R-040?4 Radium-226 EPA 901.1 Modified 3.12E-01  ? ?RF-01 2.29E-01 4.45E-01 U DO I B105100AFSFC354CV 02/08/181?,07 4/5/2018 4/6/2018 18-04024 EPA901.1 Mnrlifieri 1.36E-01 2.46E-01 2.46E-01 4.03E 01 U

°' ""

18 04024-04 DO 8105100AFSFC354CV 02/08/1813:07 4/5/2018 4/6/2018 18-04024 EPA901.1 Modified 1.92E+OO 2.30E+OO 2.30E+OO 3.85E+OO U  ; nf'iin 18-04024-04 DO 8105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 : 18-04024 Thallium-208 EPA 901.1 ,M.'.' ."'d:ifi*:"*a:d:,.. +,,~Si':'.:..57::2E*0::...1+.,'::'*,'.c'.72E:::*01!_L

!~2,.7~3'.:E~,0~1'....;....~4.:*:0'.:E-20:1, --i----f**., 1":'.'.r;:'*",....,I 18-04024-04 DO B105100AFSFC354CV 02/08/18 13:07 4/5/2018 4/6/2018 j 18-04024 Uranium 235 EPA 901.1 Modified -5.96E-01 1.03E+OO . j *:; n:;i:;:,:(1(1 7 .39E 01 . : U pCi/g CU=Counting Uncertainty;CSU=Comblned Standard Uncertainty (i-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE T!ON - - - - - ---*--*--

-*~ S L , , , , I C c.. S 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[238]

Printed: 4/30/2018 3:19 PM Page 6 of 16 Report To: Work Order Details*

Patricia Giza 18-04024 Eberline Analytical Zion ... -*_:;:~- LLC SDG:

Purchase Order: : 677118

---

---- *-*--- *---*----~-----,------~--------------------- - ------*" '

Final Report of Analysis 101 Shiloh Blvd Analv.sl.s ENVIRONMENTAL

Zion, IL 60099 Sample Matrix: so Lab Sample ; Client Sample Receipt Analysis I

Batch Analyte Method I Result

cu CSU MDA ' Qualifier :

Report ID Type ID Date Date  ; Date ID '

Units 18--04024 05 18-04024-05 TRG TRG

' B105100AFSFC363CV B105100AFSFC363CV 03/06/18 07:40 03/06/18 07:40 4/5/2018 : 4/6/2018 4,s,,o,e i 4/6/2018 rn-0@4 18-04024 Silver 108m EPA 901.1 Modified EPA 901-1 Modified 5.64E-01

-1.18E-D1 5.82E 01 1.70E-D1 5.82E 01 1.7DE-01

- 1.06E+D0 2.3DE-01 u

u

' or.;,,

,cv, -

18 04024 05 TRG  ;

B105100AFSFC363CV 03/06118 07*,m .il'i/?111~  : 41612018 18 04024 Americium-24: _ EPA 901.1 Modified -4.77E-02 4.43E-01 4.43E-01 5.71E-01 u ,,r;,,

18-04024-05 TRG B105100AFSFC363CV 03/06118 07:40 415/201' 4/6/2018 '"-"'"" Barium 133 EPA 901.1 Modified 6.69E-02 2.24E 01 2.24E 01 5.78E-01 u rCi<,

"" . ' "" TRG  ; B105100AFSFC363CV 03/06118 07:40 4151201' 4/612018 18-04024 Bismuth-214 EPA901.1 Modified 9.44E-01 6.46E-01 6.48E-01 i 1.03E+OO u oCi/c

"" " "" TRG B105100AFSFC363CV 03/06/18 07:40 4/5/2018 4/6/2018 18 04024 Cobalt-60 EPA901.1 Modified ' 4.27E 01 1_30E-01 1.32E-01 i 1.95E 01 ' ' rCiio 18-04024-05 TRG 8105100AFSFC363CV 03/06/18 07:40 4/5/2018 ( 4/6/2018 18-04024 Cesiom-134 EPA901.1 Modffied 1.42E-01  ;-;;~~~; 1.SSE 01  ; 2.59E-01 i u i rCi<r 18-04024-05 TRG B1051 OOAFSFC363CV 03/06/18 07:40 4/5/201E 1 4/6/2018 18-040?4 - .,,, EPA901.1 Modified 9.38E+01 9.26E+OO 1.04E+01 , 7.20E-01 'i rCi<r 18-04024-05 TRG B105100AFSFC363CV 03/06/18 07:40 ,11_i;1?n1.1: 1 Mf>/?n18 18-04024 - EPA 901.1 Modified 2.51E 01 1.49E+OO 1.49E+OO § 9.44E 01 u ,,r;,,,

"" 152

' i  ;

u  ;~,;;

18-04024 05 TRG B105100AFSFC363CV 03/06/18 07:40 4151201' ' 4/6/2018 "-"""' 154 EPA901.1 Modified --3_80E-02 2.43E-01 2.43E 01 4.05E-01 18-04024-05 TRG 8105100AFSFC363CV 03/06/18 07:40 41512018 , 4/6/2018 18-04024 "" 155 EPA901.1 Modified --6.52E 02 ,,iiioi 4.82E-01 ' 6.15E 01 '

u "°""

18 04024 05 TRG 8105100AFSFC363CV 0310-*,- --.*-  ; rn-040?4 EPA901.1 Modified 3.38E-02 < OOC M 1.99E 01 3.27E-01 u rei>r

' ,r;,,,

18-04024-05 TRG B105100AFSFC363CV 03/06/18 07:40 4/5/2018 4/6/2018 1R-04C,4 Iodine 129 EPA901.1 Modified -3.86E+OO 7.94E 01 8.19E-01  ; 4.38E-01  ! u

'. 1KG B105100AFSFC363CV 03/06/18 07:40 4/512018 4/6/2018 ' 18-04024 Potassium 40 EPA901.1 Modified 1.03E+01 >SOC*OC 2.65E+OO 2.14E+OO I oCi/o 1"

1" re 1KG TRG

/CV B105100AFSFC363CV  :~~~I~~

03/ 18 : 1~04024 18-04024 Niobium-94 EPA901.1 Modified EPA 901.1 Modified

-4.65E 02 3.21E-02 1.56E-01 7.1SE-02 1.56E-01 7.15E 02 I 2.34E 01 1.48E-01 u

u oCiir rCi<r

,r,,,

18 04024-05 TRG B105100AFSFC363CV 03/0 18-04024 Lead-210 EPA 901.1 Modified 1.28E+OO 2.88E+OO 2.88E+OO '

4.54E+OO u 1" -- TRG u mm,1180740 4/5/2018 4/R/?018 18-040?4 Lead 212 EPA 901.1 Modified 6.28E 01 5.22E 01 5.23E-01  ! 8.59E 01 u ,r"-

1" TRG B105100AFSFC363CV 03/06/18 07:40 4/5/2018 4/6/2018 18 04024 Lead-214 EPA 901.1 Modified 1.03E+OO 9.05E-01 9.07E---01 , 1.48E+OO , u oC.iio ao TRG  ; B105100AFSFC363CV 03/06/18 07:40 4/5/2018 4/6/2018 1 1R_n,1n?,1 EPA 901.1 Modified 1 SSC*CC  ; SSC.M

"'"-" 7.66E 01 u ' rCiio 18-04024-05 18-04024-05 TRG TRG B105100AFSFC363CV B105100AFSFC363CV 03/06/18 07:40 03/06/18 07:40 4/5/2018 41512018 416/2018 4/6/2018 18-04024 18-04024 125 EPA901.1 Modified EPA901.1 Modffied OMC.M

-8.94E-01 1.09E+OO 6.48E 01 1.09E+OO --j 1.03E+OO 1_68E+OO i u

u rC"r oCi/o 18-04024-05 TRG TRG

• B1D5100AFSFC363CV B105100AFSFC363CV 03/06/18 07:40 03/06/18 07:40 41512018 r 4/6/2018 415120,18 4/6/2018 18 04024 rn.040,4 Thorium-234 Thallium 208 EPA901.1 Modified EPA901.1 Modified

' 9.60E 02 2.43E-01 4.27E+OO 6.98E 01 4.27E+OO 6.98E-01 5.57E+OO 1.17E+OO '

u u ' ~~:'.:'

03/06/18 07:40 41512018 4/6/2018 "-""' Uranlum-235 EPA901.1 Modffied 5.25E-02 4.42E+OO 4.42E+OO I' 1.93E+OO  ; u pCi/g 18-04024-05 TRG B105100AFSFC363CV CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Actlvity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Origlnal;U=Non-detect

=-c__:_c_.=_=-~='-"*===_'.____________

YT!CAl CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[239]

Printed: 4/30/2018 3:19 PM Page7of16 Report To: Work Order Details:

Eberline Analytical ' .

Patricia Giza Zion. Solutions, LLC ......

Purchase SD!+

Order:

18-04024 677118 Final Report of Analysis

- -------~-

101 Shiloh Blvd

___ Analysis Category i .

., .... --- ------'-- - **------*--------~--------*

ENVIRONMENTAL Zion, IL 60099 Sample Matrix: . Sf1 Lab ID

! Sample Type Client ID Sample Date I Receipt Date Analysis Date Batch ID  !

Analyte Method Result cu I CSU MDA Qualifier Report Units

' em, 18--04024-06 TRG 8105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/6/2018 18-0402' Actinium-228 EPA901.1 Modified 1.01E-01 4.02E 01 402E*O*

, ,cc.o*

6.77E-01

' u

,rn, TRG 8105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/6/2018 18 04024 Silver 108m CPa 0011 MeO,SoS -4.47E-02 1.36E 01 1.90E 01 u

,e

• e, ' I u TRG 8105100AFSFC369CV 03/05/18 14:53 '. 4/5/2018 4/6/2018 18-04024 Americium-241 EPA 901.1 Modified * -6.68E-02 4.89E-02 4.90E-02 3.18E-01 '""'

.. ... TRG B105100AFSFC369CV 03105118 14:53 I 41512018 4/6/2018 18-04024

• Barium 133 EPA901.1 Modified 1.30E-02 7.65E-02 7.65E-02 3.89E 01 u . ,rn, 18-04024-06 TRG . B105100AFSFC369CV 03/05/18 14:53  ; 4/5/2018 4/6/2018 a 18-04024 Bismuth 214 EPA901_1 Modified P 4'C.O* 4.31E-01 4.33E 01 6.28E 01 . ,rn, 18-04024-06 TRG B105100AFSFC369CV 03/05/1814:53 i 4/5/2018 4/6/2018 ' 18-04024 Cobalt 60 EPA 901-1 Modified PSPC.O, 1.12E-01 1.12E 01 1.70E 01 u ,rn, 18-04024-06 TRG 03/05/1814:53 i 4/5/2018 4/6/2018 § 18-04024 Cesium 134 EPA 901-1 Modified ., esc.04 4 ""*°' "'"*"' 2.10E 01 u .. P_Ci/g I

18-04024-06 TRG B105100AFSFC369CV 03/05/18 14:53 4/5/2018 : 41e12018 I 1i:t_n,1n?,1

. '"' EPA901.1 Modified 3.82E 02 1.SOE-01 'soc.o, 2.17E-01 u pCi/g

.. 'e, IRG B105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/6/2018 1 18 04024 EPA901.1 Modified -2.82E-01 4.90E 01  ; one;;, s1ss.01 '

u .,,,.

0 OAF e, 00,CM u ,Ca,,

18-04024-06 TRG ' B105100AFSFC369CV 03/05/1814:53 4/5/2018 , 4/6/2018 : 18 04024 EPA901.1 Modified 1.72E 01 3.20E-01

... ! TRG B105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/6/2018 18 04024 EPA 901.1 Modified 8.97E 01 2.71E 01 ?75F.O, ' 4.19E-01 u . ,a,c u .

' TRG  : B105100AFSFC369CV 03/05/18 1,1-"i'i 4/5/2018 4/6/2018 I 18-04024 Holmium 166m EPA901.1 Modified 2.15E-01

-1.99E+OO 2,CF.o,

OFC<OO 2.10E-01

' osc.oo 2.04E 01 1.30E+OO . : u er""

18-04024-06 TRG B105100AFSFC369CV 03/05/1814:53 '""018 ,1/F;/?1)18 I 1f1_n,ff\'),1 Iodine 129 EPA901.1 Modified pCl/g 18-04024-06 TRG B105100AFSFC369CV 03/05/1814:53 4/5/2018 4/6/2018 , 18--04024 Potassium-40 EPA 901.1 Modified 5.76E+OO 1.83E+OO  ; ssc.oo 2.03E+OO  : r *-*~;:.;~; ----

.. .... 4/6/2018

. EPA901.1 Modified 3.49E-02 1.18E-01 1.18E-O'. 1.99E 01 ' u .

18-04024-06 TRG TRG B105100AFSFC369CV 8105100AFSFC369CV 03/05/18 14:53 03/05/18 14:53 4/5/2018 4/5/2018 4'S,,018

'"'°'°

18-04024 Niobium-94 EPA901.1 Modified 6.55E 04 1.12E-01 ' 1.79E-01 u PC'P

-'------.. pCVg

• --* -------- **-*~- or,,,

18-04024-06 TRG B105100AFSFC369CV

.. 03/05/18 14:53 4/5/2018 4/6/2018 ,S.040'4 Lead-210 EPA901.1 Modified . 3.18E-01 2.09E+OO 2.09E+OO 3.86E+OO u 18-04024-06 IRG B105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/6/2018 ' 18-04024 Lead212 EPA901.1 M,.,nm,,.-1 6.77E-01 2.68E-01 2.70E 01 4.22E 01 u er,,

.. '" TRG B105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/6/2018 18-040?4 Lead 214 EPA901.1 Modified 9.48E-01  ;*";-.;-n, ,*i,e:,; a.ic:01

,r,,

.. '" TRG B105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/6/2018 18-040?4 Promethium 145 EPA901.1 Modified . 599E-01 .. F MF e, c 03E-01 7.57F-01

' u '""'

.. ... TRG 8105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/6/2018 jS.040'4 Radium-226 EPA901.1 Modified P 4?F-01 4.31E-01 4.33E-01 6.28E 01 pCi/c

,o 4,snorn ... 3.98E-01 3,98E-01 5.93E-01

u i er,,,

IRG B105100AFSFC369CV 03/05/18 14:53

_,~- **----*--

4/5/2018

*°'"" EPA901.1 Modified --8.81E 02 EPA901.1 Modified 8.29E+OO OOFC<OO S.91'*°"  ; pCVg

***~-;

.i,~'"* ..

18-04024-06 TRG B105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/6/2018 18-04024 Thorium 234 18 04024-06 TRG '

B105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/6/2018 18-04024 Thallium 208 EPA 901.1 Modified 3.58E 01 1,,s:,; 'iMe:01 * "snc.n, u 18-04024-06 TRG 8105100AFSFC369CV 03/05/18 14:53 4/5/2018 4/6/2018 18-04024 Uranium-235 EPA901.1 Modified 1.11E+OO j OFF*M , occ.ee 1.10E+OO u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect FAX 865/483- 621

[240]

Printed: 4/30/2018 3:19 PM Page 8 of 16 Report To: Work Order Details Patricia Giza 18-04024 Eberline Analytical Zion ... LLC SDG .

Purchase Order: ,

677118 Final Report of Analysis 101 Shiloh Blvd

. - ., ----- ""~"------------- -

ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab ID Sample Type Client ID Sample Date Receipt Date i Analysis '

Date i Batch ID Analyte Method Result II cu CSU MDA Qualifier!

Report Units 18-04024-07 TRG 8105100AFSFC375CV 03/05/18 14:31 4/5/2018 : 4t6t2018 I 18-04024 Actinlum-228 EPA901.1 Modffied 2.21E 01 3.99E-01 3.99E-01 6.97E-01 : u """"

18-04024-07 TRG S105100AFSFC375CV 03/05/18 14:31 4/5/2018 4/6/2018 : 18-04024  ! Si1ver-108m EPA901.1 Modffied 2.73E-02 6.26E-02 6.26E-02 1.16E-01 u . pCiic 18-04024-07 TRG B105100AFSFC375CV 03/05/18 14:31 415/2018 4/6/2018 § 18-0402~ .-;-,,Americium-241 EPA901.1 Modffied --4.66E-02 1.89E 01 1.89E-01 2.43E-01 u erne 03/05/18 14-'.'11 4/6/2018 I 18-04024 Barium-133 '40F.O, S ,SF.O, 1.59E-01 u ernc 18--04024-07 "18-04024-07 TRG TRG B105100AFSFC375CV B105100AFSFC375CV 03/05/18 14*'.'l1 41512018 4/5/2018 4/6/2018 , 18-04024 ) Blsmuth-214

---

*--EPA901.1 Modffied EPA901.1 Modified 8.65E-01 '.29E-01 6.27E 02 2.33E-01 4.06E 01 ernc 18--04024-07 TRG 8105100AFSFC375CV 03/05/18 14:31 4/5/2018 4/6/2018 18 04024 Cobalt-60 EPA901.1 Modified ,.21E-02 . 1ose:01 'o,c o, 1.32E-01 I u """"

18--04024-07 TRG B105100AFSFC375CV 03/05/1814:'.'11 41512018 41s12018 I 18--04024 : Cesium-134 EPA 901.1 Modified -S 4RF-OS 5.86E-02 5.86E-02  ; 1.33E-01  ; u pCi/c 18--04024-07 TRG B105100AFSFC375CV

,__ 03/05/1814:31 415/2018 , 4/S001S 18--04024 , Cesium-137 EPA901.1 Modified S.31E-01 1.32E-01 133E-01

• 2.11E-01 , er.""

18-04024-07 TRG 8105100AFSFC375CV 03/05/1814:31 41512018 18 04024 i - EPA901.1 Modified 1.58E-01 S.61E-01 se,F.0' 3.43E 01 '. u erno

"'"" I 18--04024 .SOOF-0, ,.49E-01 1.70E-01 u 18--04024-07 TRG B105100AFSFC375CV 03/05/18 14:31 41512018 4'W018  !

,S_MM4 i

l

- EPA901.1 Modified 2.49E 01

, MF.Oi 18 04024-07 TRG B105100AFSFC375CV 03/05/18 1,1*11 """'J1tl ""'"18 EPA 901.1 Modified.*---- 2.63E 01 ,.04E-01 3.02E-01 u *

• " '"' TRG 8105100AFSFC375CV 03105118 14:31 41512018 4/6/2018 I 18-04024 Holmium 166m EPA901.1 Modified 7.83E-02 1eie.01  ; ,;co* 1.50E-01 u oCi/o 1" 41512018

• 4/S/2018 [ 18-04024 ! lorlioe-1?9 EPA 901.1 Modified 2.28E-02 1.01E 01 1 01F-O* , 1.SOE-01 u ,cv,

' "' TRG B1D5100AFSFC375CV 03105118 14:31

-,-~ EPA 901_1 Modified erne 18-04024-07 TRG 8105100AFSFC375CV 03105118 14:31 4/512018 4/6/2018 I 18-04024 l Potassium--40 5.70E+OO 1.70E+OO 1.73E+OO 1.70E+OO 1 , 00

• TRG S1U'1 . ,. 03/05/181431 41512018 4/6/2018 : 18-04024 I EPA 901.1 Modified 6.67E-02 1.01E-01 , MF.O* 1.77E 01 u oCl/o i o arc eo u

'"' TRG B105100AFSFC375CV 03105118 14:31 41512018 4/6/2018 18-04024 Niobium 94 EPA901.1 Modified 2.13E-02 OQOC M 1.37E 01  : """"

18-04024-07 '. TRG . 8105100AFSFC375CV OS/05118 14:31 41512018 4/6/2018 c 18 04024 j Lead-210 EPA 901.1 Modified 255F+OO 112E+OO 1.12E+OO 2_15E+OO u *"""

18-04024-07 TRG B105100AFSFC375CV 03105118 14:31 41512018 , 41nnn1f! I 18-04024 ' lead-212 EPA901.1 Merlmerl 1.71F-01 1.33E-01 1.33E-01 3.40E-01 . u or11e 18-04024-07 41512018 , 4,snorn ' 18-04024 j lead 214 FPA901.1 Merlmorl 6.73E-01 2.50E 01 2.52E 01 3.90E 01 eClle

, .. TRG B105100AFSFC375CV 03/05118 14:31 18-04024-07 TRG ' B105100AFSFC375CV 03/05/18 14:31 4'SrHJ1tl d/f\r.1[11)1 ; ,,,_/1,1[1?,1 ; EPA 901.1 Mnrlffit>rl -5.64E-02 1.30E--01 1.30E 01

• 1.95E-01 u oCl/c 18--04024 07 TRG B105100AFSFC375CV 03/05/18 14:31 41512018 4/6/2018 I 18--04024 i Radium 226 EPA 901.1 Modffied 8_65E-01 2.29E 01 2.33E 01 4.06E-01 oCl/c 18--04024-07 TRG B105100AFSFC375CV 03/05/18 14:31 4/5/2018 4/6/2018 18--04024 EPA901.1 Modffied 5.42E 02 2.37E-01 2.37E-01 4.15E-01 u """"

18--04024 07 TRG B105100AFSFC375CV 03/05/18 14:31 41512018 4/6/2018 I 18--04024 1 Thorium-234 EPA901.1 Modified 7.63E 01 1.88E+OO 1.88E+OO 2_59E+OO u "°""

'" "" TRG

' B105100AFSFC375CV 03/05/18 14:31 4/S/701' 4/6/2018 18-04024  ! Thallium-208 EPA 901.1 Modified 4.32E 01 5.37E 01 5.37E-01 8.97E-01 u '

pCi/c

,o

"' TRG B105100AFSFC375CV 03/05/1814:31 4/5/2018 4/612018 I 18 04024  ! ' EPA 901.1 Modified -9.30E 02 , OOF+OO 1 OOF+OO 7.61E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect 865/481-0683 FAX 865/483-4621

[241]

Printed: 4/30/2018 3:19 PM Page 9 of 16 Report To- Work Order Details:

Patricia Giza 18-04024 Eberline Analytical .. *.** Zion Solutions, LLC SDG:

Purchase Order: 677118

---

r* ------------------- ----------***----**----*------------*

1 ....

Final Report of Analysis 101 Shiloh Blvd -- *---.--- ~nafysis_ Category: : ENVIRONMENTAL Zion, IL 60099 Sample Matrix: '. so

! Report Lab Sample Client Sample Receipt Analysis Batch

! Analyte Method Result cu . CSU MDA Qualifier Units ID I Type ID Date Date  :

Date ID 18-04024-08 18-04024--08 TRG TRG B105100AFSFC379CV 8105100AFSFC379CV 03/06/18 07:46 03/06/18 07:4 415/2018 415/2018 416/2018 4/6/2018 18-04024 18-04024 Actinium-228 Silver-108m EPA901.1 Modified EPA901.1 ~~,vt.r..,rl 3.65E-02 5.32E-02 6.65E-01 1.62E 01 i!

6.65E 01 1.62E 01 1.09E+OO 1.91E-01 u

u oCilo 18-04024 ... EPA 901.1 Modified 6.21 E 02 6.21E-02 2.35E-01 ----- u  ;,*;:.i;~*.

18-04024-08 TRG 8105100AFSFC379CV 03/06/18 07:4 415/2018 4/6/2018  ! 1.0'"*"'

18-04024-08 TRG 8105100AFSFC379CV " 415/2018 4/6/2018 18-04024 Barium-133 EPA901.1 Modified 1.74E-02 9.41E 02 --- 9.41E 02 -- ,,,e:o, u pCi/g 18-04024-08 TRG 8105100AFSFC379CV I 074 415/2018 4/6/2018 18-04024 Bismuth-214 EPA901.1 Modified 1.03E+OO 3.89E 01 3.93E 01 6.80E-01  :  : ~c,1,

'"" 8105100AFSFC379CV 03/06/18 07:46 4/5/2018 4/6/2018 1 18-04024 Cobalt 60 EPA901.1 Modified 8.73E-02 1.51E-01 1.51E-01 2.49E-01 . u orna

-,o ,oee.m 6.64E-02 6.64E 02 2.46E 01

u i oC.,a 18-04024-08 TRG 8105100AFSFC379CV 03/06/18 07:46 4/5/2018 4/6/2018 18-04024 EPA901.1 Modified

. oooco, '  :

18-04024-08 TRG 81051 OOAFSFC379CV 03/06/18 07:46 4/512018 4/6/2018 18 04024

. "' EPA901.1 Modified 7.51E-01  : 2.82E-01 3.81E-01

• '.31!

• EPA901.1 Modified -1.06E-O! 3.24E 01 ' 3.24E-01 3.56E-01 u 18-04024-08 18-04024-08 TRG TRG 81051 OOAFSFC379CV B105100AFSFC379CV 03/06/18 07:46 03106118 07:46 415/2018 4/6/2018 415/2018 , 4/6/2018

""°"

rn.o,o" . .,,, EPA901.1 Modified 7.11E-02 3.95E 01 ' 3.95E 01 1.SOE-01 u  : .,,,

. u  : 1 r.;,r 18 04024-08 TRG B105100AFSFC379CV 03/06/18 07:46 415/2018 ' 4/6/2018

"*°'"' EPA901.1 Modified 2.94E-02 2.17E-01 2.17E 01 3.12E 01 18 04024-08 TRG B105100AFSFC379CV 03/06/18 n7*.4R 415/2018 : 4/6/2018 1'.MO" Holmium-166m EPA 901.1 Modified 1.66E 01 2.89E-01 2.89E-01 1.47E 01 u """"

'" 0 00 TRG  : 0' ',, ,,,. 03/06118 07:46 4/5/2018 4/6/2018 18-04024 lodine-129 _. ___ EPA901.1 Modified , OOF.00 6.48E 02 6.48E 02 ! 1.01E 01 u  ;~""

,o. 00  : 18-04024 Polasslum-40 EPA901.1 Modified 5.93E+OO 1.84E+OO 1.87E+OO ***; 8.57E 01 or,,,

TRG B105100AFSFC379CV 03/06/18 07:46 4/5/2018 4/6/2018

.. TRG B105100AFSFC379CV 415/2018 416/2018 rn.MO" EPA901.1 Modified -2.45E-02 1.40E-01 1.40E 01 I 2.26E 01 u .pCVg

'"" B105100AFSFC379CV 415/2018 416/2018 18-04024 Niobium 94 EPA901.1 Modlfied 3.52E 02 1.06E-01 1.06E-01 1 C,F.01 u .P~~~ . ---

M 03/06/18 07:46 4/512018 : 4/6/2018 18-04024 Lead-210 EPA901.1 Modified + ,oe+oo 1.39E+OO 1.39E+OO 2.31E+OO u ,,c;,,,

1KG [ B105100AFSFC379CV '

,..-18-04024-08 TRG  : B105100AFSFC379CV 03/06/18 07:46 415/2018 4/6/2018 18-04024 Lead 212 EPA901.1 Modified S.OOE-01 0 1,e:01 2.21E-01 3.74E-01 . or""

, o,c 01  :

18-04024-08 TRG B105100AFSFC379CV 03/06/18 07:46 415/2018 416/2018 1R-040" Lead-214 EPA901.1 Modified 7.11E-01 S?1F-01 5.77E 01 '""*

.. TRG B105100AFSFC379CV 03/06/18 07:46 4/5/2018 4/6/2018 rn.o,o" EPA901.1 Modified -1.37E-02 1.24E 01 1.24E 01 1.83E 01 I u  : ,c,i;

"' ,,r;,,,

,e

'"" TRG 8105100AFSFC379CV 03/06/18 °'" 4/512018 416/2018 18-04024 Radium-226 EPA901.1 Modified 1.03E+OO 3.89E 01 3.93E 01 6.80E-01 '

e ,OF.01 u ,,c;,,,

18-04024-08 1KG . B105100AFSFC379CV 03/06/18 07:41: 4/5/2018 """J1S 18 04024 EPA901.1 Modified 1.86E-01 4.19E-01

OOC+OO 4.19E-01

,,r,,,,

18-04024 08 TRG  : B 1051 OOAFSFC379CV 03/06/18 07:46 415/2018 4/612018 18-04024 Thorium-234 EPA901.1 Modified 0 MF+OC 1.98E+OO 3.28E+OO u 18-04024 08 TRG  : 8105100AFSFC379CV 03/06/18 07:46 415/2018 : 416/2018 18-04024 EPA 901.1 Modified 9.74E-02 , 5.66E 01 5.66E 01 8.14E-01 u . pCl/g.

I*

18-04024-08 TRG ' 8105100AFSFC379CV 03/06/18 07:46 4/5/2018 4/6/2018 18-04024 Uranium 235 EPA901.1 Modified -1.D9E+OO l 1.42E+OO 1.42E+OO HOC M u pCi/g CU=Counting Uncertainty;CSU"'Combined Standard Uncertainty (1-sigma);MDA::Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE <::;: ~~ - ,-~~c-ON

... ~ _,c.RV,*,.,cc 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[242]

Printed: 4/30/2018 3:19 PM Page 10 of 16 Report To: Work Order Details Patricia Giza 18-04024 Eberline Analytical ----

Zion

• .::. **;"'*:*:* ...... --**"*-*-- .. *--~ ...

LLC Purchase Order:

SDG:

677118 Final Report of Analysis 101 Shiloh Blvd I\ -- *-'- - ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab ID  !

Sample Type Client ID Sample Date Receipt I Analysis Date ' Date Batch ID i Analyte Method Result i cu  : CSU MDA i

Qualifier i Report Units 18-04024-09 TRG B105100AFSFC383CV 03/06/18 07:40 4/5/2018 4/6/2018 1s-04024 I EPA901.1 Modtfied 2_61E-01 5.03E 01 5.03E 01 8.79E-01 u . ,cu,

--*"'-*----*- ...,. .03/06/18 u ,c,1, iS-04024-09 TRG 8105100AFSFC383CV 07:40 4/5/2018 ' 4/6/2018 18-04024 ' EPA901.1 Modtfied -5.29E-02 1.67E-01 1.67E-01 2.SOE 01 i

-- - TRG B105100AFSFC383CV 03/06/18 07:40 4/5/,018 i 4/6/2018 18-04024 EPA901.1 Modtfied --6.64E 01 2.75E 01 2.78E 01 3.61E 01 u

• pCi/g 1KG 8105100AFSFC383CV 03/06/18 07:40 4/5/2018 4/6/2018 I 18-04024 Barium-133 EPA901.1 Modtfied -1 .,,._," 8.15E-02 8.15E-02 4.16E 01 ! u ,,c;;,,

<o 18-04024-09 00 1KG TRG TRG I B105100AFSFC383CV B105100AFSFC383CV B105100AFSFC3S3CV 03/06/18 07:40 03/06/18 07:40 03/06/18 07:40 4/5/2018 4/5/2018 4/5/2018 4/6/2018 4/6/2018 4/6/2018 18 04024 18-04024 18-04024 Cobalt-60 Cesium 134 EPA901.1 Modtfied EPA 901.1 Modified EPA901.1 Modtfied 8.57E 01 2.48E-02

-3.64E-02 2.79E 01 1.35E-01 6.92E-02 2.82E-01 1.36E-01 6.92E-02 2.40E-01 2.11E-01 2.34E-01 i

i u

u i

zr~

,c11, 18-04024-09 TRG B105100AFSFC3S3CV 03/06/18 07:40 4/5/2018 4/6/2018 18-04024 Cesium-137 EPA901.1 Modified 7 OOE-01 2.07E-01 2.10E-01 2.39E-01 i i ,cv, 18 04024 09 TRG

' B105100AFSFC383CV 03/06/18 07:40 4/5/2018 4/6/2018 18-04024 EPA901.1 Modified 1 04E-01 4.08E-01 4.0SE 01 5.5SE 01 ' u oCl/o 18-04024 09 TRG B105100AFSFC383CV 03/06/18 07:40 4/5/2018 . 4/6/2018 18-040,4 . EPA901.1 Modified -3.03E-02 3.28E 01 3.28E 01 2.85E 01 ' u oCl/o 18-04024-09 TRG .

i B105100AFSFC383CV 03/06/18 07:40 4/5/2018 i 4/6/2018 ,,,_,,.,,,. EPA 901.1 Modified 5.23E-01 2.S2E-01 2.84E-01 4.47E-01 i u ,c11,

<0 >< 0 0 1KG B105100AFSFC383CV 03/06/18 07:40 4/5/2018 4/6/2018 18 04024 Holmium-166m EPA 901.1 Modified 1.99E-02 242E,01 2.42E-01 2.36E-01 . u pCi/g

• - ., -* TRG B105100AFSFC383CV 03/06/18 07:40 4/5/2018 '. 4/6/2018 18-04024 lodine-129 EPA901.1 Modified -240E+OO 1.54E+OO 1.54E+OO 1.60E+OO  : u ' ,cuo

- TRG . B105100AFSFC3B3CV 03/06/18 07:40 4/5/2018 4/6/2018 18-04024 EPA901.1 Modified 8.28E+OO 1.86E+OO 1.89E+OO i

1.44E+OO i oCl/o 1KG ' B105100AFSFC383CV 03/06/18 07:40 4/5/2018 4/6/2018 18 04024 - EPA Afl1.1 MnrlifiP.rl 7SOF-O? 14fiF-01 1.46E-01 2.51E-01 u

,c,1,

<O 18-04024 EPA 901-1 Modified 1.94E-02 '"'"-'" 9.07E-02 2.00E 01 u oCl/o

~

00 1KG i B105100AFSFC383CV 4/5/2018 4/C/2U1' 18 04024-09 TRG B105100AFSFC383CV ,. 18-04024 Lead-210 EPA901.1 Modified 6.13E+OO 3.35E+OO 3.36E+OO 4.55E+OO u pCl/o 18-04024--09 TRG B105100AFSFC383CV 03/06/18 07:40 4/5/2018 ; 4/6/2018 18-04024 Lead-212 .__ ,___ ,,_EPA901.1 Modified -1.64E-02 I 5.11 E-02 I 5.11E-02 4.71E-01 u ,c110

. 4/5/2018 , 4/6/2018

• • -*--**-* 1.04E+OO . 7.81E-01

' oCl/o TRG 8105100AFSFC383CV 03/06/18 07:40 18-04024 Lead-214 EPA901.1 Modified 4.89E 01 4.92E 01 B105100AFSFC383CV 03/06/18 07:40 4/5/2018 "'-""'" FPA S01.1 Mcrlifierl 1 18F+OO 6.21E-01 6.24E-01 9.32E-01 u i oCi/o 1KG 18--04024-09 TRG B105100AFSFC383CV 03/06/18 07:40 4/5/2018 4/C/2U1' 1'-U4'2' EPA 901.1 Modified 8.57E 01 2.79E 01 2.82E 01 2.40E-01 i oCl/c

-- -- TRG 8105100AFSFC383CV 03/06/18 07:40 4/5/2018 4/6/2018 18-04024 EPA901.1 Moditied -2.24E*01 5.19E-01 5.19E-01 7.55E-01 i u pCi/o

,c,1,

-- - TRG 8105100AFSFC383CV 03/06/18 07:40 4/5/2018 4/6/2018 18-04024 Thorium"234 EPA 901.1 Modified -5.53E+OO 2.50E+OO 2.51E+OO 3.40E+OO ! u i

TRG 8105100AFSFC383CV 03/06/18 07:40 4/5/2018  ! 4/6/2018 18-04024 Thallium-208 EPA 901.1 MortifiP.rt 7 60F-01 4.78E-01 4.79E-01 7.37E 01 i u oCl/o

<O 00 TRG 8105100AFSFC383CV 03/06/18 07:40 4/5/2018 i 4/6/2018 18-04024 Uranium-235 EPA 901.1 MnrHt11'!11

""-"' <aH""  ?:11F+/10 I 1.30E+OO i u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty j1-sigma);M DA=M inimal Detected Activity; LCS=Laboratory Control Sample; MBL=Blank;DUP=Duplicate; TRG=Nonnal Sam pie; DO=Duplicate Origlnal;U=Non-detect I EBERLINE CA.L CORPORATION i 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[243]

Printed: 4/30/2018 3:19 PM Page 11 of 16 Report To.- Work Order Details.-

---Patricia__________________

Giza 18-04024 Eberline Analytical ,--~-'""

. Zion Solutions, LLC ..

Purchase SDG:

677118

• • • • -- '*------------*-*"' ..,_,."--- . -*---- *------- *. Order: : - ---*-------.*.--- --------*---- ------------ ----*

Final Report of Analysis 101 Shiloh Blvd Analysis Category: i ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample i Client Sample i Receipt Analysis Batch I I Analyte Method Result cu CSU MDA  : Qualifier ( Report ID

.. Type ID Date Date  : Date I ID i  ! Units

• o TRG B105100AFSFC411CV 03/06/18 08:05 4/5/2018 4/6/2018 1 18-04024 Actinium 228 EPA901.1 Modified 7.10E 01 4.16E--01 4.18E 01 7.33E 01 u  : oCi/o

.. .. TRG  : B105100AFSFC411CV 03/06/18 08:05 4/5/2018 4/6/2018 I 18-04024 Silver-108m EPA901.1 Modified 9.37E 03 1.12E-01 1.12E-01 1.75E 01  : u oCi/o 18 04024-10 TRG  : B105100AFSFC411CV 03/06/18 08:05 4'"'"" 4/6/2018___ 1- 18-04024 EPA901.1 Modified U2E*01 1.53E 01 1.53E 01 2.89E 01 ' u  : oCi/o 18-04024-10 TRG  : B105100AFSFC411CV 03/06/16 08:05 4/5/2018 4/612018 1.ls-04074 Barium-133 EPA901.1 Modified 456E*01 2.'4F.01 2.,SF.01 2.51E--01 u  :

1.02E+OO 287E.Q1

• • 0 .. 1KG TRG i

8105100AFSFC411CV B105100AFSFC411CV 03/06/18 08:05 03/06/18 08:05 4/5/2018 4/5/2018 416/2018 1S.04024 4/6/2018 i 18-04024 Coba11*60 EPA901.1 Modified EPA901.1 Modified i -1.26E-02 2.82E*01 3.61E-02 3.61E-02  :

3.60E-01 2.06E-01 u

oCi/o 18-04024--10 TRG ' B105100AFSFC411CV 03/06/18 08:05 4/5/2018 416/2018 18--04024 Cesium-134 EPA901.1 Modified -6.83E-01 3.11E-01 3.12E-01 1.93E-01 u oCi/o 18-04024--10 TRG B105100AFSFC411CV 03/06/18 08:05 4/5/2018 i 4/6/2018 18-04024 Cesium-137 EPA901.1 Modified .S42E*01 2.10F.01 2.12E-01 2.86E-01 oCi/o 18 04024--10 TRG  : B105100AFSFC411CV 03/06/18 08:05 4/5/2018 4/6/2018 18--04024 EPA901.1 Modified S91E*03 2.22E 01 2.22E 01 3_02E-01 ' u oCi/o 18-04024--10 TRG i B105100AFSFC411CV 03/06/18 08:05 4/5/2018 4/6/2018 18-04024 Europium-154 EPA901.1 Modified 3.54E-02 3.00E-01 3.00E-01 1.54E-01 . u ' oCi/o 1 105100AFSFC411CV 0 5 EPA901.1 Modified 4.18E-02 1.12E-01 112E*01 2.59E-01

' u  !

,c,1, 18-04024--10 TRG i B105100AFSFC411CV 03/06/18 08:05 4/5/2018 4/6/2018 i 18-04024 Ho!mlum-166m EPA 901.1 Modified 1.86E-01 1.98E-01 1.99E-01  : 1.18E-01 u  : pCi/g 18-04024--10 TRG

' B105100AFSFC411CV 03/06/18 08:05 4/5/2018 I 4/6/2018 18--04024 lodine-129 EPA 901.1 Modified -1.78E-03 5.66E-02 566E.Q2 8.39E-02 u i cCi/c ...*

18---04024--10 TRG  ! B105100AFSFC411CV 03/06/18 08:05 4/5/2018 4/6/2018 C 18--04024 Potassium-40 EPA 901.1 Modified 6.14E+OO 1.78E+OO 181F+nn 1.31E+OO i 18-04024-10 TRG B105100AFSFC411CV 03/06/18 08:05 4/5/2018 4/6/2018 18--04024 C EPA 901.1 Modified --6.68E-02 1.29E 01 1.29E 01 1.92E-01 u pCi/g

.. .. Niobium-94

--*-.--EPA 901.1 Modified -2.47E-02 8.48E-02 8.48E-02 1.58E-01 u oCi/o TRG TRG

' B105100AFSFC411CV B105100AFSFC411CV 03/

03/06/18 08:05 4/5/2018

' 4/6/2018 18--04024 4/6/2018 ' 18--04024 Lead-210 EPA901.1 Modifi~d-

.. i 523E*01 1.10E+OO 1.10E+OO 1.67E+OO i

u oCi/o

____ _,,.._., ... ........ **--*- ****---~ i i

' ,,,,v 510F.01 18-04024-10 TRG TRG w

B105100AFSFC411CV 03/06/18 08:05 03/06/18 08:05 4/5/2018 , 4/6/2018 4/5/2018 18-04024 4/6/2018 : 18-04024 Lead-212 Lead-214 EPA 901.1 Modified

--~- EPA901.1 Mnrfifi,:,d O.OOE-01 1.76F.01

?fi7F.01 1.78E*01 2.71E*01  :

3.12E 01 7.19E-01

' oCi/o oCi/o 18-04024-10 TRG B105100AFSFC411CV 03/ 18 4/6/2018 18-04024 Promethium 145 EPA 901.1 Mod11led -895E*02 11QE.Q1 110E*01 1.53E-01  : u m ""

18--04024-10 TRG I B105100AFSFC411CV 03/ EPA 901.1 Modified 1.02c+UU 282E*01 2.87E*01 3.60E-01  !

,c,1,

.. .. i 4/5/2018 , 18./l4024

'"' EPA 901.1 Modified .1.81e.01 383E*01 3.84E-01 4.90E 01 i u '

oCi/o TRG TRG B105100AFSFC411CV B105100AFSFC411CV 03/06/18 08:05 03/06/18 08:05 4/5/2018 4/6/2018 4/6/2018 rn.o,n24 Thorium 234 EPA 901.1 Modified 2.48E+OO 1.37E+OO 1.37E+OO 2.22E+OO

. u pCi/g Thallium-208 EPA901.1 Modified 5.86E-01 S.86E*01 S 87F.n1 6.72E-01 u I cCi/o.

TRG TRG i

B105100AFSFC411CV B105100AFSFC411CV 03/06/18 08:05 03/06/18 08:05 4/5/2018 i 4/5/2018 4/6/2018 4/6/2018 18-04024 18-04024 Uranium 235 EPA 901.1 Modified 5.58E 01 1.18E+OO 1.18E+OO 6.22E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Samp1e;MBL=Blank;DUP=Dupllcate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect FAX 865/483-4621

[244]

~ - ~ - - *-*-*=- *-*--~--"

Printed: 4/30/2018 3:19 PM Page 12 of 16 Report To: Worn Order Details:

Patricia Giza 18-04024 Eberline Analytical ____ Zion Solutions, LLC SDG:

Purchase OrriP.r 677118

-- ----- ------- ---* *-----~ **><*-,,~---*--

Final Report of Analysis 101 Shiloh Blvd__ ,,

ENVIRONMENTAL -

so Zion, IL 60099 Sample Matrix:

Lab Sample I Client Sample I Receipt Analysis Batch Analyte Method Result I cu I CSU MDA *Qualifier!

Report ID Type ID Date Date Date I ID ' '

Units

rr::r 18-04024-11 TRG S105100AFSFC433CV 02/08/1815:12 4/5/2018 4/6/2018 18-04024 1 Actlnium-228 EPA 901. 1 Modified 6.90E-01 9.35E-01 9.35E-01 1.42E+OO - u rC:,r 18-04024-11 IKC B105100AFSFC433CV 02/08/1815:12 4/5/2018 4/6/2018 i 18-04024 Silver 108m EPA 901.1 Modified 2.53E-02 1.97E-01 ie~o1 1.97E01 2.91E 01 ' u '

18 04024 11 18-04024-11 TRG TRG r

• - 02/08/1815:12 02/08/1815:12 4/5/2018 4/5/2018 4/6/2018 4/6/2018 18-04024 1 Americium-241 18-04024 Barium-133 EPA 901.1 Modified EPA901.1 Modified

-4.85E 01 2.SOE-01

" 0 3 47F-O' 3.32E-01 3.47E-01 3.83E-01 3.97E 01 -- i u

u  :'

pCi/g 18 04024 11 TRG C 02/08/18 15:12 4/5/2018 4/6/2018  ! 18 04024 Bismuth-214 EPA901.1 Modified 9.44E-02 4.43E-O'. 4.43E-01 6.60E-01 ' u """"

-~"""

TRG 02/08/18 15:12 4/5/2018 4/6/2018 i 18--04024 ; Cobalt 60 EPA 901.1 Modified 1.43E>01 9.42E 01 1.19E+OO 4.16E-01 ' - ___ L pCi/g 18-04024-11 TRG C

B1D5100AFSFC433CV 02/08118 15:12 4/5/2018 : 4/6/2018 18-04024 Cesium 134 EPA901.1 Modified -" -* - -01 2.34E-01 3.04E 01  : u --~c,1, -

18-04024-11 TRG B1D5100AFSFC433CV 02/08/18 15:12 4/5/2018 4/6/2018 I 18 04024 i Cesium-137 EPA901.1 Modified 5.46E+01 5.78E+OO 6.42E+OO 8.27E-01 ' ' rrnr 18 04024 11 TRG 81051 OOAFSFC433CV 02/08/18 15:12 4/5/2018 , 4/6/2018 I 18-04024 *-- EPA901.1 Modified 13E-02 1.01E+OO 1.01E+OO 6.32E 01 u """"

18-04024-11 TRG 02/08/18 15:12 4/S"018 : 4/6/2018 18 04024 .- EPA901.1 MnrlifiP.rl -1.11E-02 3.24E 01 3.24E 01 3.25E-01  : u pCi/9 C

.L 18-04024-11 TRG B105100AFSFC433CV 02/08/18 15:12 4/5/2018 i 4/6/2018 ; 18 04024 - -- EPA901.1 Modified 2.04E 2.71E-01 4.43E-01 u rC.i/o 18--04024 11 1KG 0 02/08/1815:12 4/5/2018 , 416/2018 : 18-04024 Holmium 166m EPA901.1 Modffied 1.29E-01 3.17E-01 3.17E-01 2.50E-01 u rCi/r 18-04024-11 I TRG B105100AFSFC433CV 02/08/181512 4/5/2018  ! 4/6/2018 : HLn,ffl?,1 lodine-129 EPA 901.1 Modified _, '-" "-" 3.86E-01 4.87E-01 u rCi/r 18-04024-11 TRG B105100AFSFC433CV 02 8 .* 4/6/2018 i 18 04024 Potassium---40 EPA 901-1 Modified 8.73E+OO 1.91E+OO 1.96E+OO 1.56E+OO oCi/o 18-04024-11 TRG B105100AFSFC433CV 02/08/1815:12 4/5/2018 i 4/6/2018 i 18--04024 - EPA 901.1 Modffied 2.22E 01 2.43E 01 2.44E-01 3.80E-01 :.-T u rCiio 18--04024-11 TRG B105100AFSFC433CV 02/08/1815:12 4/5/2018 i 4/6/2018 I 18-04024 Nioblum-94 EPA901_1 M o d m , , - _ f { f ~ 0 1 I 2.86E-D1 u """"

18-04024-11 TRG B105100AFSFC433CV 02/08/1815:12 4M018 ' 4/6/2018 , 11s...Mn?,1 Lead-210 EPA901.1 Modified +00 3.71E+OO u rr.i/o 18-04024-11 TRG B105100AFSFC433CV 02/08/1815:12 ,:5,.;"18 i 4/6/2018 i 1RJ1,tn?,t Lead 212 EPA901.1 Modified 3.02E 01 3.16E 01 3.17E-01 5.23E-01 u rCi/r 18-04024-11

'"--,- ****m*~*

TRG B105100AFSFC433CV 02/08/1815:12 4/512018 i 4/6/2018 18-04024 Lead-214 EPA901.1 Modified 2.14E-01 5.33E-01 5.33E-01 7.85E 01 u oCi/o 18-04024-11 TRG :v 0?/08/1815:12 4151701 ethium-145 EPA901.1 Modified 1.23E+OO 4.15E-01 4.20E-01 5.72E-01 u -"""

-*---*-w**-**-*<.****

18-04024-11 TRG C

8105100AFSFC433CV 0,/0S/18 15:12 41.s/?018 ! 4/6/2018 ; 18-04024 Radium-226

---

* EPA901.1 Modified 4.43E-01 6.60E-01  :

u ,.r:,,.

18 04024-11 TRG B105100AFSFC433CV o,:os,rn 15112 4IS,,048 i 41612018 I 18-04024 '

"' EPA901.1 Modified 1.65E E 01 8.65E-01 1.27E+OO u rri/o 18-04024-11 TRG - r, 02/08118 15:12

""'""" 4/6/2018 , 18 04024 Thorium-234 EPA901.1 Modified 2.25E+OO 2.95E+OO 2.96E+OO 3.92E+OO u rrnr 1" ' TRG C

. -*. ICV 02/08/18 15:12 4/5/2018 ; 4/6/2018 I 18-04024 : Thallium-208 EPA901.1 Modified 4.64E-D1 3.35E-01 3.36E-01 5.91E 01 u oCi/o 1" TRG 0?/08/18 1512 41512018 4/612018 : 1R-04n?4 i EPA901.1 Modified 4.74E-D1 2.32E+OO 2.32E+OO 1.30E+OO u ' pCi/g C U=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sig ma); MDA=Minimal Detected Activity; LCS=Laboratory Control Sample; M BL=Blank; DU P=Duplicate;TRG=Normal Sample; DO=Duplicate Original; U=Non-detect I T!ON 160lscARB0RO ROAD OA~AR\DGE, TN 37830 865/481-0683 FAX 865/483-4621

[245]

Printed: 4/30/2018 3:19 PM Page 13 of 16 Report.To: Work Order Details:

Patricia Giza 18-04024 Eberline Analytical ---Zion ~-***"'.;.:;;-- LLC SDG:'

Purchase nrrlAr 6771 rn Final Report of Analysis 101 Shiloh Blvd ENVIR *-**

11~,

-~*M * * '

so Lab ID Sample :

Type  !

Client ID Zion, IL 60099 Sample Date Receipt Date Analysis Date Batch ID Analyte Sample Matrix:

Method Result

! cu I I

CSU I

MDA

- i Qualifier i Report Units TRG 81051 OOAFSFC434CV 02/08/18 09:30 4/5/2018 4/6/2018 I 18--04024 Actinium 228 EPA901.1 Modffied -1.03E-02  ; 9.58E 01 9.58E 01 1.42E+OO u or.;,,

I

" TRG

' '" -* 02/08/18 09:30 4/5/2018 4/612018 I 18--04024 Silver 108m 18-04024 , Americium-241 EPA901.1 Modified EPA901.1 Mnrlifi,ar 4.59E-02 -, . ,oii'.61 2.39E-01 T77E-01 2.07E 01 3.77E-01 3.18E-01 4.97E-01 u

u aCil,

,c;1, 18-04024-12 TRG 8105100AFSFC434CV 02/08/18 ClA*:\C 41512018 4/6/2018

-12 TRG i B105100AFSFC434CV 02/08/18 m:vv 41512018 4/6/2018 "*~"" Barium 133 EPA901.1 Mnrlffii>r .1 osc.o, 4.02E-01 4.02E 01 4.69E-01 u ' """'

18-04024-12 TRG B105100AFSFC434CV 02/08/18 4/612018 I 1RJ\.10?4 Bismuth-214 EPA901.1 Mnrlffi<>c 3.00E 01 4.79E-01 4.80E-01 7.35E-01 u pCi/g

' OQ*<\(

-~r-;*;~-*-

.,. 02/08/18 mi-:-u: 4/6/2018 ' 18-04024 EPA901.1 Mnrlffi"r S.39E-01 1 OSC+OC 3.44E 01 TRG TRG B105100AFSFC434CV B 1051 OOAFSF C434CV !l/l!IX/1!:I OQ*<\('

4/5/2018

.,s,,crn 4/6/2018 ; 18-04024 Cobalt-60 Cesium 134 EPA901.1 Mnrlifie,r ,

1 "C+W

.1 17E-01 1.73E-01 1.73E 01 2.68E 01 ' u

,rn,

'" TRG ' B105100AFSFC434CV 02108118 09'3C 41512018 4/6/2018 j 18-04024 Cesium-137 EPA 901.1 Modified , ss,c+M 8.41E+OO 9.49E+OO i 6.18E 01 i ,rn,

" TRG  ; B105100AFSFC434CV 02/08/18 09;30 4/5/2018 - 4/6/2018 : 18 04024 Europium 152 EPA901.1 Modified -129E-02 1 OOC+OO 1.20E+OO 7.53E 01 l u .,,.L pCi/g

" TRG ' B105100AFSFC434CV 02/08/18 09:30 4/5/2018 41612018 I 18-04024 EPA901.1 Modified 2.76E 01 4.11E-01 4.11E-01 3.80E 01 u .. '""'

.,. TRG  : B10510DAFSFC434CV 02/08/18 09:30 ""'01' ; 4/6/2018 : 18-04024 - -* EPA 901.1 Modified 1.35E-01 3.95E 01 3.95E 01 5.17E 01 i u or.;,,

'" !KG  : B10510DAFSFC434CV 02/08/18 09:30

""'"" ' 4/6/2018 ' 18 04024 Holmium 166m EPA901.1 Modified -191E-01 3.39E 01 3.40E 01 2.79E-01 ' u ,rn,

'" TRG ' B1051DOAFSFC434CV 02108118 09'30 41512018 41612018 18-04024 lodlne-129 EPA901.1 Modified ., 01E+OO 9.24E-01 9.74E-01 3.88E 01

• u ,rn,

.,. 2.06E+OO --!

" " TRG B105100AFSFC434CV 02108118 09,30 415/2018 _ 4/6/2018 18-04024 Potassium-40 EPA 901.1 Modified 7.10E+OO 1.92E+OO 1.96E+OO '"""

18-04024-12 TRG B1051DOAFSFC434CV 02/08118 OS*en 4/ci/?018 : 4/fl/?01R 18-04024 EPA 901.1 Modified ,.04E*02 2.36E-01 2.36E-01 3.59E-01 u m ""

.,. B105100AFSFC434CV 02/08118 CP*SC 4/<;l?01R : 4/hl?OiR 18-04024 Niobium 94 EPA901.1 Mnrlifi<>rl 1.75E-01 2.20E 01 2.20E 01 01 u ,cu, 1KG B1051DOAFSFC434CV 02108118 09,30 4/5/2018 ; 4/6/2018 I 18-04024 Lead 210 EPA901.1 Modified 2.90E+OO 2.42E+D0 2.42E+OO 3.85E+OO u *;;-;,,

" TRG B105100AFSFC434CV 02/08118 09,30 41512018 41612018 , 18 04024 Lead 212 EPA901.1 Mod;fted 1:: 771:-1)1 4.33E 01 4 35E 01

. I ..5.83E-01-*** i u

" TRG ' B105100AFSFC434CV 02/08/18 09:30 41512018 4/612018 18--04024 Lead-214 EPA901.1 Modlfied 5.04E 01 * ,oc r1 6.47E-01 8.58E 01 u '""'

18-04024-12 TRG

. B105100AFSFC434CV 02108118 OP*SO 4/S/?018 4/R/?01R 18-04024 Promethium-145 EPA901.1 Modified 2.47E+OO 4.20E-01 4.39E-01 6.63E-01  : u ornr

>>--.~-"---~-,--,"--

18---04024-12 TRG I 81051 OOAFSFC434CV 02/08/18 09:30 4/5/2018 4/6/2018 ' 1~0,0,; Radium-226 EPA901.1 Modffied 3.00E 01  ; ,OC.01 HCC.01 7.35E-01 I u ' rr;,,

18-04024-12 TRG 81051 OOAFSFC434CV 02/08/18 09:30 4/5/2018 416/2018

• 18-04024 EPA901.1 Mnn;r,.,,,; -902E-01 0 OSC.01 oo.c:o, ' 1.36E+OO 1 u oc;fo 18-04024-12 TRG B 1051 OOAFSF C434CV 02/08/18 09:30 4/5/2018 4/6/2018 1S.04024 Thorium 234 EPA 901.1 Modffied , mc+cr *;,;";;;;; ;a,.;;;;;; 4.67E+OO u ,r;,,

---

* 4/6/2018 : 18-04024 Thallium 208 EPA901.1 Modified 3.55E-01 5.73E 01 5.73E 01 9.62E-01 i u

,rn, 18-04024-12 TRG B105100AFSFC434CV 02/08/18 09:30 4/5/2018

• • -,-~- u 18--04024-12 TRG i B105100AFSFC434CV 02/08/18 09:30 41512018 I 4/6/2018 18--04024 Uranium-235 EPA901.1 Modified -3.24E+OO 3.79E+OO 3.79E+OO i 1.54E+OO  ! pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1*slgma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

( ~~

EBERLINE SERVJCES 601 SCARBORO ROAD OAK RIDGE, TN 37830

[246]

Ti ON __ - - -- - - - - -

=.:..:=..:.=..:.:...

865/481-0683 FAX 865/483-4621

Printed: 4/30/2018 3:19 PM Page 14 of 16 Report To: Work Order Details*

Patricia Giza - _,__ ---- 18-04024 Eberline Analytical Zion - - --- ----

LLC

... ,_ SDG:

, nme, 677118 Final Report of Analysis 101 Shiloh Blvd ._., '"*----- -

---

--------- ---**--*--- . ***---*-** .. ---- *.. ---------------------- ...... Analysis CategoryJ _____

ENVIRONMENTAL .*...... ------*------------------ -----

Zion, IL 60099 Sample Matrix: i so

. Report Batch Lab ID Sample Type I Client ID Sample Date Receipt j Analysis Date

• Date ID i Analyte Method I Result cu CSU MDA Qualifier Units 1S...04024-13 TRG B105100AFSFC435CV 02/07/1814:22 4/5/2018 4/6/2018 18-04024 Actinium-228 EPA901.1 Modified 5.75E-01 4.50E-01 4.51E-01 8.24E-01 u pCi/g 18-04024-13 TRG B105100AFSFC435CV 02/07/18 14:22 4/5/2018 4/6/2018 18-04024 Si1ver-108m EPA901.1 Modified 9.11E-02 9.73E-02  : 9.74E 02 1.81E-01 u ,r,,,----

18-04024-13 TRG B105100AFSFC435CV 02/07/18 /2018 18-04024 Americium-241 EPA901.1 Modified -5.60E-01 2.0SE-01 2.11E-01 2.82E 01 u '°"'

18-04024-13 TRG B105100AFSFC435CV 02/07/1814:22 4/5/2018

• 4/6/2018 18-04024 Barium-133 EPA901.1 Modified 3.99E-01 1.96E-01 1.97E-01 3.08E-01 u ,rn, 18-04024-13 TRG 8105100AFSFC435CV 02/07/1814:22 4/5/2018 4/6/2018 ,~n,oo, Bismuth 214 EPA901.1 Modified 1.99E-01 3.03E 01 3.03E-01 5.02E-01 u ,rn,

-,a TRG B105100AFSFC435CV 02/07/1814:22 4/5/2018 4/6/2018 18-04024 Cobalt 60 EPA 901.1 Modified seeF.n, 1.22E 01 1.22E01 1.63E-01 u ,,.,,

rn-,.,,._ ao TRG

' 8105100AFSFC435CV 02/07/1814:22

' 4/5/2018 4/6/2018 18 04024 Cesium 134 EPA901.1 Modified 1.0iE-03 4.22E 02 , "F-M 1.94E-01 u ,rn,

., .. u

':o TRG ' 8105100AFSFC435CV 02/07/18 14:22 4/5/2018 4/6/2018 18 04024 Cesium-137 EPA 901.1 Modified 1.37E 01 1.46E 01 1.46E-01 .

2.45E-01

,~.;;-- ....

-,, TRG B105100AFSFC435CV 02/07/18 14:22 4/5/2018 416/2018 18-04024 EPA901.1 Modified 4.55E-01 5.65E-01 5.66E 01 4.50E-01 u

-,o TRG 8105100AFSFC435CV 02107118 14*" 4/5/2018 i 4/6/2018 18 04024 EPA 901.1 Modified -6.66E-02 3.40E 01 i 3.40E-01 2.33E-01 u nrnn

-,o 'KG B105100AFSFC435CV 02/07/18 14:22 4/5/2018 4/6/2018 18-04024 EPA901.1 Modified 1.26E-01 1.01E-01  : 1.01E 01 3.61E-01 u ,,.;~*

0 IRG B105100AFSFC435CV 02/07/18 14:22 4/5/2018 4/6/2018 : !8-04024 Holmium 166m

- -,-w.-,*

EPA901.1 Mnrlifi<>rl -9.26E-02 1.13E-01 I 1.14E 01 1.79E 01 u ""

" TRG 02/07/18 1 2018 41512018 I 18-04024 , lodine-129 EPA901.1 Modrfied -1.12E+OO 9.91E-01 9.93E 01 1.25E+OO u ' '""' -

-,o TRG 'CC435CV 02/07/18 14:22 4/5/20!8 4/6/2018 C 18-04024  ! Potassium 40 EPA 901.1 Modtfied 6.48E+OO 1.67E+OO 1.70E+OO I 1.18E+OO .

18-04024-13 TRG 8105100AFSFC435CV 02/07/18 14:22 4/5/2018 4/6/2018 I 1i:i_nJ.n?a . Manganese-54 EPA901.1 Modified 5.08E-02 1.13E-01 1.13E-01 , 1.96E-01 u " '"

18-04024-13 TRG B105100AFSFC435CV 02/07/1814:2:c! """"118 4/6/20"18 18-04024 : Niobium 94 EPA901.1 Modified 8.65E-03 9.21E 02 9.21E-02 i 1.51E-01 u ' "'

18-04024 13 TRG 8105100AFSFC435CV 02/07/1814:22 41512018 4/6/2018 18-04024 Lead 210 EPA901.1 MnrlrtiArl ~"F+OO  ; ;;;";"" OSOE+nn  ! 3.59E+OO u '"

18-04024 13 TRG 8105100AFSFC435CV 02/07/1814:22 41512018 4/6/2018 18 04024 Lead-212 EPA901.1 M ... rlifi<>rl 4.zac-01 ,,,c:01 2.99E-01 4.74E 01 u '"'"

18-04024 13 TRG B105100AFSFC435CV 02/07/1814:22 41512018 4/6/2018 1R-04024 Lead-214 EPA901.1 ~~ ...rl;fi.,rl s s,c_c, 0 .99E-01 2.99E 01 4.60E-01 u pCUg 18-04024-13 TRG 02/07/18 14:22 4/5/2018 4J6J2or -145 EPA901.1 Modified 6.75E-01 4 S,E-01 4 83E-01 7.27E 01 u '""'

Radium-226 EPA901.1 Mnrlifo:,rl 1.09E-01 S 03E-01 3.03E-01 5.02E-01 u  !

18-04024-13 TRG B105100AFSFC435CV 02/07/18 14:22 4/5/2018 4/6/2018 I 18-04024 EPA 901.1 u 18-04024-13 TRG B105100AFSFC435CV 02/07/18 14:22 4/5/2018 4/6/2018 I 18 04024 Mnrlifii>rl 1.49E-01

_, SOF+nn S.81E-01 1 onF+nc 3.81E-01 6.02E 01 i u

TRG 8105100AFSFC435CV . 02/07/18 14:22 41512018 4/6/2018 18-04024 Thorium 234 EPA 901.1 M...rlifi<>rl 1.91E+OO 2.63E+OO TRG TRG B105100AFSFC435CV B105100AFSFC435CV 02/07/18 14:22 02/07/18 14:22 41512018 1 4/6/2018 4/5/2018 18 04024 Thallium-208 4/6/2018 : 18-04024 1 Uranium-235 EPA 901.1 Modified EPA901.1 Modified 1.91E 01

-5.06E-02 1.T1r;;,.""

3.92E-01 1pc+nn .

5.93E 01 . !

9.72E-01 '.

u u  :

pCilg pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma );M DA=Minimal Detected Activity; LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate;TRG=Normal Sample; DO=Duplicate Original; U=Non-detect I 'E,CRLINE ALYT:CAL CORPOR!\TION SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[247]

Printed: 4/30/2018 3:19 PM Page 15 of 16 Report To* Work Order Details:

Eberline Analytical Patricia Giza SDG: 18-04024 Zion ,u LLC . Order: 677118 Final Report of Analysis 101 Shiloh Blvd ENVIRONMENTAL Zion, IL 60099 Sample Matrix: : so Lab I Sample C!ir;nt Sample I Recr;ipt '. Analysis ' Batch I Analyte Method I Result cu CSU MDA  : Qualifier I Report ID Type ID Datr; Date Datr; I ID Units 180402414 TRG  : B105100AFSFC436CV 02/14/1810:30 4/5/2018 : 4/6/2018 e 18-04024 EPA901.1 Modified 6.73E 01  : 5.25E 01 5.26E 01 1.02E+OO . u i "Ci/"

18-04024-14 TRG  : B105100AFSFC436CV 02/14/1810:30 4/5/2018 4/6/2018 18-04024 Silsec-108m EPA901.1 Modified 8.09E-02 i 1.53E-01 1.53E-01 1.71E-01 ' u . pC;Jo 18-04024-14 TRG B1 02/14/18 10:30 41512018 : 4/6/2018 1"-"""" EPA901.1 Modified 2.40E-01 1.90E-01 1.91E-01 2.44E-01 i u ,c,;o 18-04024-14 TRG B105100AFSFC436CV 02/14/1810:30 4/6/2018 1'-U40'4 Barium-133 EPA901.1 Modified 1.71E-02 ' 7.17E-02 7.17E-02 ' 3.10E-01 u oCilo 18-04024-14 TRG

• • ,-------*-*-**-~*-w***-**

B1 -*

• • • • --*****--**-* 02/14/18 10:30 415/2018 , 4/6/2018 18-04024 Bismuth 214 EPA901.1 Modified 3.74E 01 i 3.60E 01 3.61E 01 i 5.83E-01 I

i u oCi/c 18-04024-14 TRG B105100AFSFC436CV 02/14/1810:30 415/2018 , 4/6/2018  ! 18-04024 Cobalt-60 EPA901.1 Modified -5.21E-02 i 1.28E-01 1.28E-01 i 2.44E-01 u oCi/c 18-04024-14 TRG B105100AFSFC436CV 02/14/1810:30 4/512018 4/6/2018 , 18-04024 Cesium-134 EPA901.1 Modified -3.SSE-01 i 2.SSE-01 2.56E-01

• 2.24E-01 I u "Cito 18-04024-14 : TRG I B105100AFSFC436CV 0?/1411810,0 41512018 4/6/2018 18-04024 Ceslum-137 EPA901.1 Modified 7.93E-O;--*-*j 1.93E-01 1.93E-01 2.96E-01 ' u ,c,,,

18-04024-14 ; TRG  ; 8105100AFSFC436CV !l//14/1H 11!":~II 41.,0llltl I 4/6/2018 1R-(J4!1:.i4 C, EPA901.1 Modified -4.36E-02 ' 4.33E-01 4.33E-01 3.17E-01 u pCi/0

,,_,~,,,. .

I 18-04024-14 i TRC. . B1 V om*na w-10

""""" 4/6/2018 C, EPA901.1 Modified -1.83E-01 4.11E-01 4.11E-01 i 1.72E-01 u ,c,;,

18--04024-14 TRG . B105100AFSFC436CV 02/14/1810:30 4/5/2018 4/6/2018 18--04024 Europium-155 EPA901.1 Modified 5.63E-02 2.00E-01 . 2.00E-01 3.02E-01 . u oCilc 18-04024 14 TRG 8105100AFSFC436CV 02/14/1810:30 4/5/2018 4/6/2018 18 EPA901.1 Modified 1.66E 01 2.51E-01 2.52E 01 1.42E-01 u oCilc 1" TRG B105100AFSFC436CV

• • • - 02/14/1810:30 4/5/2018 4/6/2018 18-04024 lodine-129 EPA 901.1 Modified 2.48E 02 i 6.86E-D2 6.86E-02 1.04E 01 u ,ci;,

18-04024-14 TRG B105100AFSFC436CV 02/14/18 10:30 4/512018 ' 4/6/2018 18-04024 Potassium-40 EPA901.1 Modified 7.0SE+OO  ? S?F,00 2.59E+OO 3.06E+OO '

I

,cu, 18 04024-14 TRG  ; 8105100AFSFC436CV 02/14/18 18-()4(1;,4 EPA901.1 Modified -2.54E-02 1.34E-01 1.34E-01 2.16E-01 u ,c,;,

111\111

""""" °'""'" '

i 18 04024-14 TRG ' 8105100AFSFC436CV 02/14/18 ,U:;jU 41512018 , 4/6/2018 I 18---04024 0 EPA901.1 Modified -2.18E-02 1.32E-01 1.32E-01 2.10E-01 i u oCi/q 18-04024-14 TRG B105100AFSFC436CV 02/14/18 10:30 4/5/2018 4/6/2018 18-04024 Lead-210 EPA901.1 Modified 1.SSE+OO 1.60F<OO 1.60E+OO 2.67E+OO I u "c""

C

v 18-04024 u

_"'_18.__.04024-14

---

TRG 02/14/1810:30 4/5/2018 , 4/6/2018 Lead-212 EPA901.1 ModFfiP.d 7.41E-01 2.27E-01 2.30E-01 3.90E-01 "Ci/"

18-04024-14 u 18-04024-14 TRG TRG B105100AFSFC436CV 8105100AFSFC436CV 02/14/18 10:30 02/14/1810:30 4/5/2018 !

4/5/2018 4/6/2018 4/S/2018 18-04024 18-04024 Lead-214

... EPA901.1 Modified cPAS01.1 Mod"ed 4.65E-01

-1.45E-03 3.71E-01 1.28E-01 3.72E-01 1.28E-01 5.89E-01 191E-01 .

I u

,c,1, oCi/q 18-04024-14 TRG B105100AFSFC436CV 02/14/18 10;30 4/5/2018 4/6/2018 18-04024 EPA901.1 Modified 3.74E-01 3.60E-01 3.61E-01 5.83E 01 u  : pCi/g 18--04024-14 TRG 8105100AFSFC436CV 02/14/1810:30 4/5/2018 4/6/2018 18-04024 Antimony-125 EPA901.1 Modified -4.18E-01 4.57E-01 4.57E-01 i 4.74E-01

• u PCi/c 18--04024-14 TRG B105100AFSFC436CV 021141181030 41512018 41612018 18-04024 Thorium-234 EPA901.1 Modified 2.60E+OO 1.68E+OO 1.68E+OO 2.70E*OO ! u "Ci/"

18--04024 14 TRG V 02/14/181030 41512018 4/6/2018 18--04024 Thallium-208 EPA 901.i Modified 9.66E-01 4.29E-01 4.32E-01 3.45E-01 : "Ci/"

18-04024-14 TRG B105100AFSFC436CV 02/14/1810:30 4/5/2018 4/6/2018 18-04024 Uranium-235 EPA901.1 Modlfied -2.14E+OO 1.54E*OO 1.54E+OO I 7.79E-01 i u pCi/g CU=Counting U ncertainty;CSU=Combined Standard Uncertainty (1-sig ma);MDA=M inimal Detected Activity; LCS=Laboratory Control Sample; M BL=Blank; DU P=Du plicate; TRG=Normal Sample;DO=Duplicate Orig in al ;U=Non-detect ON 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[248]

Printed: 4/30/2018 3:19 PM Page 16 of 16 Report To: Work Order Details i

Patricia Giza 18-04024 Eberline Analytical ,.

... .... Zion Solutions, LLC Purchase Order: .

SOG:

677118

• * - - * - - -..** ---***- . ---.********------- ; ----------------------~-----

Final Report of Analysis ________ 101________

., Shiloh,_' Blvd ENVIRONMENTAL Zion, IL 60099 Sample Matrix: 1 <:>n Lab Sample Client Sample Receipt ' Analysis Batch i I lI cu ' Report ID Type ID Date Date Date ID i

I Analyte Method i

Result CSU I MDA Qualifier '.

Units

" TRG 8105100AFSFC438CV 02/08/18 10:25 4/5/2018 4/6/2018 18-04024 EPA901.1 Modified 5.43E 01 4.13E 01 i

4.14E 01 7.3SE 01 u or.<<o 4/6/2018 , 18-04024 I -1.00E-01 1.14E-01 1.14E-01 , 1.53E-01 u I .r,,,

.. ..., 02/08/18 10:25 EPA901.1 Modified

<O

'iO TRG 8105100AFSFC438CV 4/5/2018 Silver 108m TRG 8105100AFSFC438CV 02/08/18 10:25 4/5/2018 4/6/2018 I 18 04024 Americium 241 EPA901.1 Modified -3.69E-01 4.92E-01 4.92E-01 6.02E-01 u '[ .r,,.

.. .." i Barium-133 EPA901.1 Modified 2.27E*01 3.64E*01 3.65E*01 . 6.20E 01 u i TRG TRG B105100AFSFC438CV B105100AFSFC438CV 02/08/18 10:25 02/08/18 10:25 41512018 4/5/2018 4/6/2018 1R-040?4 4/612018 ; 1R-fl40/4 Bismuth-214 EPA90i.1 Modified 8.80E-01 5.68E 01 5.70E 01 8.82E 01 u

. Oi ii,O

.,. TRG B1051DOAFSFC438CV 02/08/18 10:25 415/2018 4/6/2018 : rn.Mn?4 Cobalt-60 EPA 901.1 Modified 2.0TE+OO ,.22e.01 2-46E-01 - 2.0SE-01 i orno u i 18*0402.i.15 TRG 81051DOAFSFC438CV 02/08/18 10:25 4/5/2018 4/6/2018 18-04024 Cesium 134 EPA901.1 Modified A.11E*01 3.12E*01 3.12E-01  ; '02E*01 oCi>o 4/6/2018 -04024 EPA901.1 Modified 1 QSC+Cii 'e,c;o, 2.27E+01 8.88E 01 .

i oCi>o 18-04024-15

• iO i ""

TRG B105100AFSFC438CV B105100AFSFC438CV 02/08/18 10:25 02/08/18 10:2!:

41512018 4/6/2018 : 18-04024 Cesium-137 Europium-152 EPA901.1 Modffied ,.29E*01 i i1e~66 1.71E+OO 6.56E-01 u

.,. TRG B105100AFSFC438CV 02/08/18 10:25 4/5/2018 4/6/2018 18--04024 EPA901.1 Modtfied 0 7'F.m 2.00E-01 . 2.00E-01 3.35E 01 u "'orno

.,... TRG

• B105100AFSFC438CV 02/08/18 10:25 4/5/2018 4/6/2018 18-04024 EPA 901.1 Modtfied 1.BOE 01 4.33E 01 i -4.33E 01 6.81E-01 i u

.. TRG B105100AFSFC438CV 02/08/18 10:25 41512018 4/6/2018 18 04024 Holmium-166m EPA 901-1 Modtfied -3.09E-02 1.91E 01 i 1.91E-01 2.86E 01 i u orno 18-04024 lodine-129 EPA901.1 Modffied 7.92E 01 6.05E 01 6.06E 01 7.29E-01 I u orno 1 S.04024* 15 1KG 1KG B105100AFSFC438CV B1051DOAFSFC438CV 02/08/18 10:25 02/08/1810:25 4/5/2018 41512018 4/6/2018 4/6/2018 18-04024 Potassium-40 EPA901.1 Modtfied 7.96E+OO 1 QOCoM 1.92E+OO 1.74E+OO ,rna

-. u

=1 9.63E-02 1.08E-01 1.08E-01 1.9DE-01 aCi<a 18 04024-15 TRG B 1051 OOAFS FC438CV 02/08/18 10:25 41512018 4/6/2018  ! 18-04024 EPA901.1 Modtfied 18-04024-15 TRG i B105100AFSFC438CV 02/08/18 1O*?!'i 41512018 4/6/2018 ; 18-04024

.. EPA901.1 Modtfied 1.09E-01 1.59E-01 u er;,o 1M-04ll,'4-1t, TRG 8105100AFSFC438CV 02/08/18 1 O*?!'i 4/512018 4/6/2018 18*04024 lead-210 EPA 901.1 Modified 47~

4.45E+OO 5.84E+OO u i orno 1KG B105100AFSFC438CV 02/08/18 10:25 41512018 4/6/2018 18-04024 Le,d.212 EPA901.1 Modified 5.15 ., . 9.71E-01 u er;,o

• iO e

.,. TRG B105100AFSFC438CV 02/08/18 10:25 41512018 4/6/2018 18.040?4 lead*214 EPA901.1 Modified 9.12E-01 7.91E-01 7.93E-01 I 1.30E+OO u i "me

.. .. TRG B1051DOAFSFC438CV 02/08/18 10:?5 415/2018 4/6/2018 18 04024 EPA901.1 Modified 2.87E+OO 6.65E-01 6.81E 01 i 8.69E 01 u °' .. ,.

., TRG B105100AFSFC438CV 02/08/18 10:25 4/5/2018 4/6/2018 18 04024 Radium-226 EPA 90-U Modified ssoc.01 5.68E.01 5.70E-01 i 8.82E 01 I u i orno i 02/08/18 10:25 4/5/2018 rn.e,eo, EPA901.1 Modified .1,1e.01 1 SOC+M 1.56E+OO - : 2.11E+OO  : u i oCi>o 18--04024-15 1KG B1051DOAFSFC438CV

--~--- -- ' .. """"" rn.e,eo,  ;  ;;";""

18 04024-15 TRG B105100AFSFC438CV 02/08/1810:25 4/5/2018 I .4/Rl'.)fl18 Thorium-234 EPA901.1 Modified 4.71E+OO 4.51E+OO 5.93E+OO ) u ori<o 18--04024-15 18-04024-15 TRG TRG B1051DOAFSFC438CV B1051DOAFSFC438CV 02/08118 10:25 02/08118 10:25 4/5/2018 C 4/5/2018 '

4/6/2018 4/6/2018 18-04024 18-04024 Thallium-208 Uranium-235 EPA901.1 Modified EPA901.1 Modified 5.51E 01

-1.85E+OO ""'

4.01E+OO 3.46E-01 4.01E+OO 5.11E T 2.08E+OO  ! u

.ri<a pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect EBER~IN,,E: CAL CORPORATION

--*~ ~,_,rc-_RVls...~-E::::, 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

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ZS-WM-131 Revision 0 ZIC)NSOLl!TIONSric Information Use An EnergySo/u/ions Company REC'D APR O5 2018 Attachment 1 - Chain-of-Custody Form 1 8 ""' 0 4 0 2 4 Sample ID Sampl Matiix Sample Type Sample Container Sample Date Sample Time Analysis Type Preservative Remarks eLog Vol Unit Type Qty B105IOOAFSWCOl 7CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310712018 0935 5ROCIHTD NIA 0.0-0.5" 101.65g B105100AFSWC041CV NIA CONCRETE CONCRETE 57.94 cm' Puck I 0310712018 0925 5ROCIHTD NIA 0.0-0.5" 123.37g BI 051 OOAFS WC057CV NIA CONCRETE CONCRETE 57.94 cm' Puck I 0310712018 0910 5ROCIHTD NIA 0.0-0.5" 101.99g B105IOOAFSWC088CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310712018 0855 5ROCIHTD NIA 0.0-0.5" 105.94g B105IOOAFSWC101CV NIA CONCRETE CONCRETE 57.94 cmJ Puck I 0310712018 0725 5ROCIHTD NIA 0.0-0.5" 146.06g B105100AFSWCI 15CV NIA CONCRETE CONCRETE 57.94 cmJ Puck I 0310712018 1530 5ROCIHTD NIA 0.0-0.5" 94.29g B105100AFSWCI 16CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 0310712018 0840 5ROCIHTD NIA 0.0-0.5" 98.62g B105IOOAFSWCl50CV NIA CONCRETE CONCRETE 57.94 cnr Puck I 0212112018 0840 5ROC/HTD NIA 0.0-0.5" 97.99g B105100AFSWCl51CV NIA CONCRETE CONCRETE 57.94 Cl113 Puck I 0212112018 0920 5ROCIHTD NIA 0.0-0.5" 102.61g B105IOOAFSWCl56CV NIA CONCRETE CONCRETE 57.94 cm' Puck I 02121/2018 1330 5ROCIHTD NIA 0.0-0.5" 96.47g BI 051 OOAFSWC l 62CV NIA CONCRETE CONCRETE 57.94 cmJ Puck I 02/1512018 1550 5ROCIHTD NIA 0.0-0.5" 90.81g B105!00AFSWCl63CV NIA CONCRETE CONCRETE 57.94 cm' Puck I 0211512018 1350 5ROCIHTD NIA 0.0-0.5" 97.73g B105100AFSWCI 79CV NIA CONCRETE CONCRETE 57.94 cmJ Puck I 0310712018 0710 5ROCIHTD NIA 0.0-0.5" 100.50g B105IOOAFSWCl90CV NIA CONCRETE CONCRETE 57.94 cm' Puck I 0310612018 1300 5ROCIHTD NIA 0.0-1.0" 180.00g B 105100AFSWC201CV NIA CONCRETE CONCRETE 57.94 cm5 Puck I 0310612018 1513 5ROCIHTD NIA 0.0-0.5" 96.68g Bl05100AFSWC2!0CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310612018 1440 5ROCIHTD NIA 0.0-0.5" 120.44g B105!00AFSWC231CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck I 0310612018 1430 5ROCIHTD NIA 0.0-0.5" 132.73g B105IOOAFSFC239CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0310612018 0955 5ROCIHTD NIA 0.0-1.0" 209.92g BI 051 OOAFSFC250CV NIA CONCRETE CONCRETE 57.94 cm 5 Puck I 0310612018 0940 5ROCIHTD NIA 0.0-0.5"

[250] 130.05g

~~ ZS-WM-131 Revision 0 ZIONSOL[]TIONSLLC An EnergySofulions Col1l)any Information Use B105l00AFSFC255CV NIA CONCRETE CONCRETE 57.94 c1n' Puck 1 0310612018 1246 5ROCIHTD NIA 0.0-0.5" 134.3 lg B 105100AFSFC263CV NIA CONCRETE CONCRETE 57.94 cm Puck 1 0310612018 0930 5ROC/HTD NIA 0.0-0.5" 110.42g B105l00AFSFC276CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck 1 0310512018 1342 5ROCIHTD NIA 0.0-0.5" 122.73g B105l00AFSFC282CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0852 5ROCIHTD NIA 0.0-0.5" 116.66g B105100AFSFC289CV NIA CONCRETE CONCRETE 57.94 cm 3 Puck 1 0310512018 1352 5ROCIHTD NIA 0.0-0.5" 119.03g B105100AFSFC293CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0210712018 1345 5ROCIHTD NIA 0.0-0.5" 132.53g B105100AFSFC300CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 02/1312018 1250 5ROCIHTD NIA 0.0-0.5" 85.562g B105100AFSFC3 l6CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1358 5ROCIHTD NIA 0.0-0.5" 108.12g B105l00AFSFC321CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0211312018 1410 5ROCIHTD NIA 0.0-0.5" 148.80g B 1051 OOAFSFC326CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0211412018 0815 5ROCIHTD NIA 0.0-0.5" 134.35g B 1051 OOAFSFC329CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1418 5ROCIHTD NIA 0.0-0.5" 115.08g B105l00AFSFC332CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1405 5ROCIHTD NIA 0.0-0.5" 123.51g B105l00AFSFC345CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0210712018 1045 5ROCIHTD NIA 0.0-0.5

115.27g B 105100AFSFC347CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0211212018 1310 5ROCIHTD NIA 0.0-0.5" 91.09g B105l00AFSFC348CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0211212018 1515 5ROCIHTD NIA 0.0-0.5" 88.0lg B105!00AFSFC354CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0210812018 1307 5ROCIHTD NIA 0.0-0.5" 110.07g s B 1051 OOAFSFC363CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0740 5ROCIHTD NIA 0.0-0.5" 85.52g B105100AFSFC369CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1453 5ROCIHTD NIA 0.0-0.5" 150.58g 7 B105100AFSFC375CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310512018 1431 5ROCIHTD NIA 0.0-0.5" 119.51g B105100AFSFC379CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0746 5ROCIHTD NIA 0.0-0.5"

~ 135.29g 1 B 105100AFSFC383CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0740 5ROCIHTD NIA 0.0-0.5" 118.83g B105100AFSFC4l1CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0310612018 0805 5ROCIHTD NIA 0.0-0.75 to 168.23g

[251]

ZS-WM-131 18-04024 Revision 0

.ZIONSOL[TTIONSLLC Information Use An Ei;ergySofulions Company R[t,)  !\PRO 5 l018 B105l00AFSFC433CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0210812018 1512 5ROCIHTD NIA 0.0-0S' i\ 130.93g B105IOOAFSFC434CV NIA CONCRETE CONCRETE 57.94 cm3 Puck 1 0210812018 0930 5ROCIHTD NIA 0.0-0S 133.53g B105JOOAFSFC435CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0210712018 1422 5ROCIHTD NIA 0.0-0S' 152.36g Bl05JOOAFSFC436CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0211412018 1030 5ROCIHTD NIA 0.0-0.5" 133.53g Bl05!00AFSFC438CV NIA CONCRETE CONCRETE 57.94 cm3 Puck I 0210812018 1025 5ROCIHTD NIA 0.0-0.5" 130.93g Laboratmy: Date Submitted To L1b: Ship Container No.: Cooler Temperature: ?till Number: /t{f ft

. ,rr;f uvefn1~0h*"t Eberline Labs NIA NIA g10,7 ()///5 {:;/Jg)?

Relinquished by: Date Time: Received by: Date: (mrnlddlyyyy): Time:

Reed R. Smith (0410412018) l3 17l, K1cJq rtl f;.f((c/<ii r D4 /o4 /Jo1g I ' t/b, 1,>,

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Relinquished by: Date Time: Received by: Date: (mmldd/yyyy): Time:

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Relinquished by:

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Date: (mmldalyyyy): Time:

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(mmldd/yyyy):

Comments PO# 677118 7 day turnaround 5-ROC I HTD / H-3

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