ML19295G791

Revised Final Status Survey (FSS) Report - Phase 2, RR 6100 Isocs Reports Part 1 of 2

ML19295G791
Person / Time
Site:	Zion  File:ZionSolutions icon.png
Issue date:	04/18/2016
From:	ZionSolutions
To:	Office of Nuclear Material Safety and Safeguards
Shared Package
ML19295G627	List: ML19295G587 ML19295G611 ML19295G612 ML19295G617 ML19295G621 ML19295G625 ML19295G670 ML19295G674 ML19295G699 ML19295G702 ML19295G705 ML19295G726 ML19295G728 ML19295G734 ML19295G738 ML19295G742 ML19295G747 ML19295G751 ML19295G758 ML19295G764 ML19295G768 ML19295G788 ML19295G791 ML19295G795 ML19295G816 ML19295G818 ML19295G820 ML19295G822 ML19295G826 ML19295G828 ML19295G831 ML19295G837 ML19295G841 ML19295G843 ML19295G846 ML19295G850 ML19295G853 ML19295G855 ML19295G857 ML19295G859 ML19295G863 ML19295G866 ML19295G870 ZS-2019-0090, Revised Final Status Survey (FSS) Report - Phase 2, Release Record - Waste Water Treatment Facility Survey Unit 09100
References
ZS-2019-0090
Download: ML19295G791 (249)

Text

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****         r:;AM~1A     :S ,..' E C T R U M         A N A L Y S __ S                        *****
************ ; - ~********************************************* ~ *~ *******

.lename: 545 2 iport Generated On 4/1 8/2 016 1:49:25 PM 1mple Title B306100AFRWC001GD tmple Description TB 560 1mple Identification 1mpl e Type 1mpl e Geometry iak Locate Threshold 3 .00 iak Locate Range (in channels ) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mpl e Size 1.000E+OOO SQM 1mple Taken On

quisition Started 4/ 1 8/ 2 016 1

39: 2 4 PM

.ve Time 600.0 seconds ial Time 600.6 seconds !ad Time 0.10 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBWALL Da.\~ \\o.\,~o.~~J 'OJ Q~~ 12- !5-1~ O{glO [84]

1ak Analysis Report 4 / 1 8/2 01 6 1: 4 9: 25 P} Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 545 2 Sample

Title:

B306 1 00AFRWC001GD Peak Analysis Performed on: 4/18/2016 1: 4 9: 25 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid {keV) {keV ) Area Uncert. Counts 1 307- 316 310.71 77.33 0 .61 6.09E+OOO 36. 2 9 1.37E+002 2 1400- 1 413 1407. 22 351.77 1. 13 5.15E+001 21. 83 2 .45E+001 3 2429- 2441 2434.79 608.88 1. 23 3.72E+001 19.19 2 .08E+001 4 58 2 7- 5850 5840.50 1460.39 0 .93 l.82E+00 2 2 8.71 6.00E+OOO

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted sing l et

rors quoted at 2 .000 sigma

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1terference Corrected Act i ty Report 4 / 1 8/2016 9: 2 5 PM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306l00AFRWC001GD Nuclide Library Used: C:\GENIE2K\CAMFILES\ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energj' Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K-40 1. 000 1460.82* 10.66 1. 2 4086E+006 2 . 2 3417E+005 Bi-211 0. 9 99 35 1. 07* 1 3.02 l.4 22 44E + 005 6.44957E+004

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold =             0. 3 0 Errors quoted at 2 .000 s igma

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1terference Corrected Act i ~y Report 4/ 1 8/ 2 01 6 1 9:25 PM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activit y Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 l.2 40 862E+006 2 . 2 34170E+005 Bi -2 11 0.999 1.4 22 436E+005 6.449567E+004

      ? = Nuclide i s part of an undetermined solution X  = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2. 00 0 sigma
 **********     U N I   D E N T I     F I  E D      P E A K S       **********

Peak Locate Performed on: 4/18/ 2 01 6 1:49:25 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second Z; Uncertainty Type Nu c li d e 1 77.33 1.0146E-00 2 596. 1 7 To l. Pb214-XR Pb2 14 -XR Eu-155 Pb212-XR Pb2 1 2 -XR 3 608.88 6.1932E- 00 2 5 1 .64 Tol. Zr-97 Sb-125 Sb-125 Cs- 1 34 Bi -2 14 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 s i gma [87]

4/18/ 2 01( 1: 49: 25 PM Page 5 tclide MDA Report N U C L I D E M D A R E P O R T ***** Detector Name: 545 2 Sample Geometry: Sample

Title:

B306l00AFRWC001GD Nuclide Library Used: C:\GENIE2K\CAMFILES\ Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( i: ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) K-40 1460. 82

• 10.66 1.284E+005 1. 2 8E+005 1 .241E+006 5.496E+004

+                                                                                   7. 2 90E+004 Cr-5 1       32 0.08     9.91   1.552E+005       1.55E+005 2 .129E+004 Mn-54        834.85    99.98    1.704E+004       1.70E+004 -4.993E+003       7.775E+00 3 Co-58        810.76    99.45    1.364E+004       1.36E+004 6.131E+003        6.080E+00 3 Co-:-6 0   117 3 . 23  99.85    1.883E+004       1.30E+004 8.559E+003        8.536E+003 1 332 .49   99.98    1. 2 98E+004                 -2 .016E+004    5.555E+003 Nb-94        702.65    99.81    1. 5 96E+004     1.46E+004 2 .502E+003       7.291E+003 871. 0 9  99.89    1.456E+004                   -5 .736E+00 3   6.5 2 3E+003 Sn-11 3      255.13      2. 1 1 7.532E+005       2 .18E+004 3 .544E+004      3.570E+005 391.7 0   64.97    2 .177E+004                    1.021E+004    1.009E+004 Cs- 134      475.36      1. 48  9.006E+005       l .60E+004 -5.671E+004      4.119E+005 563.25      8.34   1 .892E+005                    1. 163E +005  8.721E+004 569.33    1 5.37   9.359E + 004                 -8.553E+003     4. 27 6E+004 604.7 2   97.62    2 .157E+004                  -6.920E+003     1 .013E+004 795.86    85.46    1.603E+004                     3 .557E+003   7.166E+003 801.95      8.69   1.669E+005                   - 4.770E+00 4   7.503E+004 1038.6 1      0.99   l.544E+006                     1 .8 3 1E+005 6.883E+005 1167.97       1. 79  1.002E+006                   -3.810E+005     4.523E+005 1365.19       3.0 2  4.660E+005                   -3.078E+005     2 .017E+005 Cs-137       66 1. 66  85.10    1.585E+004       1.59E+004 -3 .221E+00 3     7.141E+00 3 Eu-1 52      12 1 .78  28.67    6.657E+004       5.42E+004 5.999E+00 4       3 . 2 16E+004 244.70      7.61   2 .036E+005                  -1.062E+005     9.649E+004 295.94      0.45   3.623E+006                     2 .528E+005   1.7 1 2E+006 344.28    26 .60   5.417E+004                   -4.163E+004     2 . 52 8E+004 367.79      0.86   1. 7 53E+00 6                -8.468E+005     8.189E+005 411.1 2     2 . 24 6.082E+005                   -1.607E+0 0 5   2 .806E+005 443.96      2 .83  4 . 699E+005                 - 3 .784E+005   2 .156E+005 488.68      0.42   3.322E+006                     1.663E+006    1 .524E+006 563.99      0.49   3.086E+006                     1.858E+005    l .417E+006 586. 2 6    0.46   3.887E+006                     5 .673E+005   1.807E+006 678.62      0.47   3.321E+006                     2 .166E+006   1.517E+006 688.67      0.86   1.650E+006                     1.249E+005    7.458E+005 7 1 9.35    0.28   5.559E+006                     1.326E+006    2 .531E+006 778.90    12 .96   1 .25 7E+005                 -6.620E+004     5.731E+004 81 0 .45    0.32   4. 22 4E+006                   1.899E+006    1 .883E+006 867.37      4.26   3 .408E+005                    2 . 29 7E+004 1 .52 6E+005 919.33      0.43   3 .301E+006                  - 3 . 63 3E+006 1.468E+006 964.08    1 4.65   1.471E+005                     9 . 62 1E+004 6.812E+004 1085.87     10 . 2 4 1 . 401E+005                 - 1. 2 1 6E+005 6.179E+004 1089.74       1. 73  8. 3 06E+005                 - 4.740E+005    3.664E+005 1112.07     13.69    1 . 3 1 9E+005                 8.597E+004    5.972E+004 1 2 12.95     1. 43  1.155E+006                   - 4.917E+004    5.150E+005

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4/18/ 2 01 1:49: 25 PM Page 6 1c.lide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) Eu-1 52 1249.94 0. 1 9 8.670E+006 5.42E+004 5.069E+006 3.857E+006 1299.14 1. 63 9.170E+005 4.324E+005 4.018E+005 1408.01 2 1. 07 6.125E+004 3.715E+004 2 .606E+004 1457.64 0.50 9.959E+006 2.650E+007 4.784E+006 1528.10 0.28 3.978E+006 -6.623E+004 1.631E+006 Eu-154 123.07 40.40 4.706E+004 4.71E+004 3.273E+004 2 .273E+004 247.93 6.89 2 .082E+005 -2.230E+005 9.819E+004 591.76 4.95 3 . 1 69E+005 1.769E+005 l.457E+005 692.42 1. 78 7.875E+005 3 .519E+005 3.554E+005 723.30 20.06 8.871E+004 -5.714E+003 4.089E+004 756.80 4.52 3.017E+005 1.016E+005 1. 351E+005 873.18 12.08 1. 2 89E+005 7.940E+004 5.816E+004 996.29 10.48 1.401E+005 -6.595E+004 6. 2 33E+004 1004.76 18.01 9.550E+004 2.530E+004 4.323E+004 1274.43 34.80 5. 2 09E+004 1.321E+004 2 .342E+004 1596.48 1. 80 6.021E+005 2 .562E+005 2 .433E+005 Eu-155 45.30 1. 31 9.038E+005 7.44E+004 6.551E+005 4. 2 76E+005 60.01 1. 22 1.338E+006 -1.087E+006 6.431E+005 86.55 30.70 7.436E+004 5.630E+004 3 .614E+004 105.31 2 1.10 9.810E+004 7.190E+004 4.754E+004 Tl -2 08 583.19 85.00 2.031E+004 2 .03E+004 -1.240E+004 9.417E+003

+      Bi-21 1     351. 07*  13.02    8.220E+004     8.22E+004    1 .422E+005     3.736E+004 Pb-- 2 11    404.85     3.78   3.606E+005     3.61E+005  -4.305E+005       1 .665E+005 42 7.09    1. 76  7. 32 9E+005              - 2 .544E+004     3.359E+005 8 32 .01   3.52   5.120E+005                  3 .759E+005     2.349E+005 Bi-212         39.86    1. 06  9.709E+005     2 .67E+005 -1.977E+005       4.555E+005 727.33     6.67   2.675E+005                  2 .296E+005     1. 233E+005 785.37     1.10   1. 539E+006                 8.4 2 9E+005    7.041E+005 1620.50      1. 4 7 7.909E+005                  2 . 82.'.2E+004 3.242E+005 Pb-212       115.18     0.60   3.124E+006     4.53E+004    5.516E+005      1.508E+006 23 8.63  43.60    4.535E+004                  3.382E+004      2.176E+004 300.09     3.30   4.046E+005                -9.180E+005       1.887E+005 Pb212-XR       74.8 2 10.28    2 .387E+005    l. 35E+005   2.740E+005      1. 1 63E+005 77.11  17.10    1.351E+005                  1.190E+005      6.567E+004 87.35    3.97   5.702E+005                  2 .789E+005     2 .771E+005 89.78    1. 46  1.521E+006                -1. 2 77E+006     7.389E+005 Bi-2 14      609.32   45.49    4.778E+004     4.78E+004    7.894E+004      2 . 2 48E+004 768.36     4.89   2 .999E+005               -5.132E+004       1.354E+005 806.18     1. 2 6 1.111E+006                  5.072E+005      4.974E+005 934.06     3.11   5.4 22 E+005                3.689E+005      2.458E+005 1120. 2 9  14.92    1. 2 32E+005                1.997E+004      5.587E+004 1155.21      1. 63  9.257E+005                -4.4 2 9E+003     4.096E+005 1 238.1 2    5.83   3.164E+005                  9.707E+004      1.428E+005 1280.98      1. 43  1. 2 67E+006                9.743E+005      5 .699E+005 1377.67      3.99   4.322E+005                  1 . 2 93E+005   1.922E+005 1385.31      0.79   1. 732E+006               - 1.810E+006      7.456E+005 1401.52      1. 33  9.295E+005                -2.2 68E+005      3.925E+005 1407.99      2.39   5.391E+005                  3 . 2 69E+005   2.293E+005 1509. 2 1    2.13   6.064E+005                -1.218E+004       2.561E+005 1661. 2 7    1. 05  9.842E+005                  3.754E+005      3.905E+005

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1c}ide MDA Report 4/18/ 2 0H 1:49:25 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Bi-214 1 729.59 2.88 4. 2 03E+005 4.78E+004 1.959E+005 1.723E+005 1 764.49 15.30 1.384E+005 1.332E+005 6.199E+004 1847.43 2.03 6.538E+005 -9.916E+004 2 .712E+005

 >                 2 118.51      1.16   O.OOOE+OOO                     O.OOOE+OOO O.OOOE+OOO Pb-214        2 41.99     7.25   2 .611E+005   5 . 3 8E+004     1.717E+005 1. 2 50E+005 295.22    1 8.42  8.924E+004                    - 2 . 2 64E+004 4. 22 0E+004 351. 93   35.60   5.380E+004                      7.185E+004 2 .553E+004 7 85.96     1. 06 1 .582E+006                     8.642E+005 7.228E+005 Pb2 14 -XR      74.82     5.80  4. 2 31E+005   2 . 3 8E+0 05    4.857E+005 2.061E+005 77.11     9.70  2 . 3 81E+005                   2 .098E+005 1.158E+005 87.35     2.24  1.011E+006                      4.943E+005 4.911E+005 89.78     0.82  2 .709E+006                   -2 . 2 73E+006 1.316E+006 Ra-226        186. 2 1    3.64  4.684E+005     4.68E+005        2.591E+005 2 .244E+005 Ac-228        129.07     2.42   7.566E+005     7.84E+004        1.881E+005 3 .649E+005 2 09. 2 5  3.89   4.009E+005                   -3.793E+005 1.908E+005 2 70. 2 4  3.46   4.647E+005                   -1.605E+004 2 . 2 01E+005 328.00     2 .95  5. 3 07E+005                 -6.239E+0 0 3 2 .494E+005 338.32    11. 2 7 1.403E+005                      9.472E+00 3 6.591E+004 409.46     1. 92  6.578E+005                   -5.423E+005 3.015E+005 463.00     4.40   3. 406E+005                     7.939E+004 1.576E+005 794.95     4.25   3.036E+005                   - 4.771E+005 1.347E+005 91 1. 20  25.80   7.840E+004                      3.440E+004 3.619E+004 964.77     4.99   4.283E+005                     2 .666E+005 1 .982E+005 968.97    15.80   1.331E+005                     1.035E+005 6. 1 50E+004 1 588. 2 0    3.22   3.350E+005                   -7 .027E+004 1.353E+005 Pa -23 1       27.36    10.30   7.074E+004    7.07E+004        4.196E+004 3 . 22 8E+004 283.69      1. 70  9.735E+005                     4.887E+005 4.611E+005 30 0.0 7    2 .47  5.405E+005                   -1. 22 6E+006 2 .521E+005 302.65      2.2 0  6.182E+005                     4.055E+005 2 .886E+005 330. 0 6    1. 40  1.049E+006                   - 6.997E+005 4.911E+005 Th- 23 4       92.38     2 .13  1.009E+006    1 .01E+006       4.910E+005 4.898E+005 92.8 0    2 .10  1.020E+006                     5.649E+005 4.948E+005 112.8 1     0.2 1  9.036E+00 6                    4.136E+006 4.366E+006 U-235        143.76     10.96   1.555E+005    2 .99E+004     -1.295E+004 7.472E+004 1 63.33     5.08   3. 2 70E+005                 -7.552E+004 1.568E+005 1 85.7 1   57.20   2.993E+004                     1.991E+004 1.434E+004 2 02. 11    1. 08  1.499E+006                   -7.465E+005 7.155E+005 2 05.31     5.01   3.370E+005                     1.344E+005 l.611E+005 Am-24 1        59.54    35.90   4.516E+004    4.52E+004      -3 .589E+00 4 2 .170E+004
     + = Nucl ide identified during the nuclide identification

• Energy line found in the spectrum

     >     Calculated MDA is z ero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @     Half-life too short to be able to perform the decay correction

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' ***        GAMM A       S P E C T R U M         A N A L Y S 1- S                *****

.l ename: 54 52 iport Generated On 5/2/2 01 6 2 :47: 3 4 PM tmple Title B3 0 6100AFRWC002GD tmple Description TB #2 PEDESTAL WALL tmple Identification tmple Type tmple Geometry iak Locate Thr e shold 3 . 00 iak Locate Range (in channels) 85 - 81 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10.000 keV tmple Si ze 1.000E+OOO SQM tmple Taken On

quisition Started 5/ 2 /2016 2:37:32 PM

.ve Time 600. 0 seconds ial Time 6 00 .7 seconds iad Time 0.1 1 % Energy Calibration Used Done On 1/13/2 01 5 Efficiency Calibration Used Done On 4/14/2 01 6 Efficiency ID TBWALL p* P 1)"\o. \l"\1<\o.\eJ '°J

                                                                      ~JJ,5"- /8' t)/,I~

[91]

iak Analysis Report 5 / 2 / 2 0 16 2 :4 7 :34 PM Page 2 '*** P E A K A N A L Y S I S R E P O R T ***** Detector Name: 5452 Sample

Title:

B306100AFRWC002GD Peak Analysis Performed on: 5/2/2016 2 : 4 7: 33 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) ( keV ) Area Uncert. Counts 1 113- 1 2 3 117.45 28.95 0 .9 0 5.26E+001 32 . 0 7 6.84E+001 2 152- 159 155.04 38.37 0 .6 4 1 .32E+OOO 22 .87 6.37E+001 3 296- 305 301.19 74.95 0 .6 1 4.53E+001 43.94 1 .94E+002 4 2428- 2 441 2 435.37 609.02 1.11 5.83E+001 2 1. 70 2.07E+00 1 5 5827- 5848 5837.78 1 459.71 2. 0 2 1.87E+002 2 8.71 5.28E+OOO First peak in a multiplet region

=   Other peak in a multiplet region
=   Fitted singlet

rors quoted at 2 .000 sigma

[92]

1terference Corrected Activ -Y Report 5/ 2 / 2 01 6 2:  : 34 PM Page 3 "*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample

Title:

B306100AFRWC002GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTI FIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM ) Uncertainty K-40 0.998 1460. 82

• 10.66 1. 272 69E+006 2. 24767E+005 Th-231 0.875 25.64* 14.10 8.75985E+004 5.73474E+004 84.21* 6.60 1.61142E+005 1.60908E+005 89.95 1. 00

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuc l ide confidence index threshold=            0.30 Errors quoted at 2 .000 sigma

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1terference Corrected Activ -Y Report 5/2/2016 2; . : 3 4 PM Pag e 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 0.998 1.272689E+006 2.247668E+005 X Pa- 23 1 0.377 Th-231 0.875 9.588715E+004 5.401920E+004

     ?    Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2. 000 sigma
 **********      U N I D E N T I F I E D          P E A K S       **********

Peak Locate Performed on: 5/2/2016 2 :47:33 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 2 38.37 2 .1923E-00 3 1738.61 Tol. Eu-155 Bi-21 2 4 609.0 2 9.7131E-00 2 37.24 Tol. Zr-97 Sb-125 Sb-125 Cs-134 Bi -2 14 M First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [94]

iclide MDA Report 5/2 / 2 0 1 6 2 :47:34 PM Page 5

• • • • N U C L I D E MD A R E P O R T *****

Detector Name: 545 2 Sample Geometry: Sample

Title:

B306100AFRWC00 2GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM)

+      K-40       1460.82*    10.66 1.172E+005        1.17E+00 5 1. 2 73E+00 6      4.940E+004 Cr-5 1       320.08      9.9 1 1.497E+005      1 .50E+005 6.485E+004         7.019E+004 Mn-54        834.85    99.98 1. 52 5E+004      1.53E+004 -4.121E+00 2        6.883E+00 3 Co-58        810.76    99.45 1.604E+004        1.60E+004 1.825E+00 3         7.283E+003 Co-60      1173. 23    99.85 1.685E+004        1.34E+004 1.296E+004          7.545E+003 1 332 .49   99.98 1.343E+004                        3 .765E+003   5.782E+003 Nb-94        702.65    99.81 1.576E+004        1.51E+004 - 8.004E+002        7.194E+003 871.09    99.89 1. 5 07E+004                      8.551E+003    6.778E+00 3 Sn- 1 13     255. 1 3   2. 1 1 7. 3 71E+005    2 . 2 1E+004 1.151E+005       3.489E+005 391. 70   64.97 2 . 2 13E+004                     4.809E+00 3   1.028E+004 Cs- 134       475.36     1. 48   9.418E+005     1.97E+004 5.638E+004          4. 32 5E+005 563.25     8.34 1.911E+005                        1.167E+005    8.813E+004 569.33    15.37 9.690E+004                      -5 .773E+004    4.442E+004 604.72    97.62 2 .576E+004                     - 2 .513E+003   1. 22 3E+004 795.86    85.46 1.974E+004                      - 7.860E+001    9.017E+003 801. 95    8.69 1.583E+005                      -1.056E+005     7.074E+004 1038.61      0.99 1 .765E+006                     - 4.876E+00 4  7.991E+005 1167.97      1. 79 8.300E+005                     -2 .684E+005   3.661E+005 1365.19      3.0 2 4.938E+005                    -2 .664E+005    2 .156E+005 Cs-137        661.66    85.10 1.799E+004        1.80E+004 -4.641E+00 3       8.208E+003 Eu -152       121.78    28.67    6.9 1 7E+004   5.75E+004 -5.025E+00 3       3.346E+004 2 44.70    7 .61 2 .243E+005                      8.713E+003   l.068E+005 2 95.94     0.45 3 .790E+006                       1.332E+006   1.795E+006 344. 2 8  26.60 5.751E+004                      - 1 .266E+00 4  2 .694E+004 367.79      0.86 1.692E+006                     -2 .971E+005    7.882E+005 411. 1 2   2 . 2 4 7.150E+005                  -2 . 2 91E+005  3 . 3 39E+005 443.96     2 .83 5.454E+005                       1. 3 55E+005 2 .534E+005 488.68     0.42 4.007E+006                        1 .711E+006  1.867E+006 563.99      0.49 3.119E+006                     -l.635E+006     1.434E+006 586. 2 6    0.46 4.037E+006                        2 .326E+006  1.882E+006 678.62      0.47 3.240E+006                       2 .069E+006   1. 4 77E+006 688. 67     0.86 1.746E+006                       1.024E+006    7.940E+005 719.35      0. 2 8 6.042E+006                      4.804E+005   2 .772E+006 778.90    12.96 l.122E+005                         6.877E+004   5.054E+004 810.45      0.32 4.969E+006                        6.075E+005   2.256E+006 867.37      4.26 3.809E+005                     - 4.614E+004    1.727E+005 919.33      0.43 3.431E+006                       3 .2 2 9E+006 l.534E+006 964.08    14.65 1.350E+005                        6.774E+004    6.207E+004 1085.87     10.2 4 1.665E+005                     -2.242E+004     7.502E+004 1089.74       1. 73 9.550E+005                    -4.246E+005     4. 2 86E+005 1112.07     13.69 1. 33 8E+00 5                   -1.560E+005     6.068E+004 1212.95       1. 43 1. 35 9E+00 6                   5.760E+005    6. 1 69E+005

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iclide MDA Report 5/2/ 2 016 2 :47:34 PM Page 6 Nucli de Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( i) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) Eu- 1 52 1249.94 0.19 7.326E+006 5.75E+004 6.185E+005 3 .185E+006 1299.14 1. 63 7. 2 97E+005 - 5.069E+005 3 .082E+005 1408.01 21.07 6.579E+004 4.390E+004 2 .833E+004 1457.64 0.50 9.911E+006 2.360E+007 4 . 760E+006 1 528 .10 0. 2 8 3 .736E+006 -3.444E+006 1.510E+006 Eu-154 12 3 .07 40.40 5 .001E+004 4.94E +004 1.323E+004 2 .421E+004 247.93 6.89 2 .283E+005 -3 .283E+003 1.082E+005 591. 76 4.95 2 .927E+005 -4.529E+004 1.336E+005 692.4 2 1. 78 7.875E+005 - 5.301E+005 3.554E+00 5 723.30 2 0.06 8.695E+004 - 4.348E+004 4.001E+004 756.80 4.5 2 3 . 5 57E+005 -4.832E+004 l .622E+005 873.18 12.08 1. 2 06E+005 4. 2 80E+004 5.400E+004 996.29 10 .48 1.457E+005 -4.082E+004 6.511E+004 1 004.76 18.01 8.020E+004 4. 7 60E+004 3.558E+004 1274.43 34.80 4.941E+004 3 .177E+004 2.209E+004 1596.48 1. 80 6.411E+005 -3.263E+005 2 .628E+005 Eu-155 45.30 1. 3 1 1. 2 38E+006 7.69E+004 4. 27 9E+005 5.946E+005 60.01 1.2 2 1.463E+006 - 2 .971E+003 7.057E+005 86.55 30.70 7.686E+004 5.3 75E+004 3.739E+004 1 05.31 21.10 1.017E+005 -2 .838E+004 4.936E+004 Tl-208 583.19 85.00 2 . 2 88E+004 2 . 2 9E+004 2 .657E+004 1.070E+004 Bi-211 351. 07 13.02 1 .487E+005 1. 4 9E+005 1.176E+005 7 . 061E+004 Pb-211 404.85 3.78 4.111E+005 4.11E+005 - 1 .329E+005 1.917E+005 42 7.09 1. 76 8.532E+005 1.861E+005 3.961E+005 8 32. 0 1 3.52 4.326E+005 4.030E+003 1.952E+005 Bi-212 39.86 1. 06 1.537E+006 2.48E+005 - 1.200E+006 7. 3 84E+005 727.33 6.67 2 .484E+005 -7.590E+004 1.137E+005 785.37 1.10 1.427E+006 -1.325E+006 6.477E+005 1 620.50 1. 4 7 6 .3 2 6E+005 2 .107E+005 2 .451E+005 Pb-2 1 2 115.18 0.60 3.587E+006 4.86E+004 1.562E+006 1 .740E+006 238.63 43 . 60 4.855E+004 7.407E+004 2.336E+004 300.09 3.30 4.737E+005 -2 .487E+005 2.233E+005 Pb212-XR 74.82 10. 2 8 2 .464E+005 1 .42E+005 3 .581E+005 1 . 201E+005 77.11 17.10 1 .417E+005 -1.481E+004 6.901E+004 87.35 3 . 97 5 .983E+005 6.802E+005 2 .911E+005 89.78 1. 4 6 1.552E+006 -3 .458E+005 7.540E+005 Bi-21 4 609.32 45.49 5.549E+004 5.55E+ 004 8.024E+00 4 2 . 633E+004 768.36 4.89 3.511E+005 1.574E+005 1.609E+005 806. 1 8 1. 26 1.169E+006 2 .932E+005 5.264E+005 934. 0 6 3.11 5.792E+00 5 2.363E+0 0 5 2 .643E+005 11 2 0. 2 9 14.92 1. 2 67E+005 5.213E+0 0 3 5.759E+004 11 55.21 1. 63 1.058E+006 2 .960E+005 4.759E+005 1238.12 5.83 2 .430E+005 -4.6 1 2E+004 1 .061E+005 128 0 .98 1. 43 1 .133E+006 -9.373E+004 5.026E+005 1 377.67 3.99 4.143E+005 2 .484E+005 1.833E+005 1385.31 0.79 1.410E+006 -2.367E+006 5.849E+005 14 01.52 1. 33 1.004E+006 -9.338E+004 4.300E+005 1407.99 2.39 5.790E+005 3.864E+005 2 .493E+005 1509.21 2 .13 6.553E+005 1 .770E+005 2. 805E+005 1661. 2 7 1.05 9.842E+005 3.754E+005 3.905E+005 [96]

5/2/2016 2:47:34 PM Page 7 iclide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM) Bi-2 1 4 1729.59 2 .88 3.013E+005 5.55E+004 8.397E+004 l. 1 2 8E+005 1764.49 1 5.30 8.881E+004 - 6.676E+004 3 .7 1 9E+004 1847.43 2 .03 5.402E+005 -1.319E+005 2 .144E+005 211 8.51 1.16 O.OOOE+OOO O.OOOE+OOO O.OOOE+OOO

  >                                                                            1.368E+005 Pb-214       241.99      7.25   2 .848E+005   5.51E+004    4.066E+005 295.22    18.42    8.965E+004               -3.434E+004     4. 2 41E+004 35 1. 93  35.60    5.508E+004                 6.433E+004    2 .6 1 7E+004 785.96      1. 06  1.544E+006                 6.301E+005    7.036E+005 Pb214-XR       74.82     5.80   4.367E+005    2 .50E+005   6.347E+005    2 .1 2 9E+005

77. 11 9.70 2 .499E+005 - 2 .611E+004 1.217E+005 87.35 2.24 1.060E+006 1. 2 06E+006 5.160E+005 89.78 0. 82 2 .763E+006 -6.157E+005 1.342E+006 Ra-226 186. 2 1 3.64 4.659E+005 4.66E+005 -1.480E+004 2 .232E+005 Ac-228 129.07 2.4 2 8.431E+005 7.30E+004 -2.163E+005 4.082E+005 209.25 3.89 4.288E+005 -1. 2 03E+005 2 .047E+005 270. 2 4 3. 4 6 4.196E+005 -1.233E+005 1.975E+005 328.00 2.95 5.060E+005 1.618E+005 2.371E+005 338.32 11. 27 1.591E+005 4.180E+004 7.529E+004 409.46 1. 92 8.427E+005 2.963E+005 3.940E+005 463.00 4.40 3.583E+005 4.090E+005 1.664E+005 794.95 4 . 25 4.107E+005 3.552E+004 l.882E+005 91 1. 2 0 25.80 7.303E+0 04 4 . 0 96E+004 3.351E+004 964. 77 4.99 3.966E+005 3.125E+005 1 .823E+005 968.97 15.80 1. 2 68E+005 1.033E+005 5.834E+004 1 588.20 3.22 3.567E+005 -3.902E+004 1.462E+005 Pa-23 1 27.36* 10.30 1. 1 35E+005 l.14E+005 l.199E+005 5.368E+004 283.69 1. 70 8.463E+005 - 1.926E+005 3.975E+005 300.07 2 .47 6.329E+005 - 3.323E+005 2 .983E+005 302.65 2 . 20 6.834E+005 2.310E+004 3.212E+005 330.06 1. 40 1.043E+006 -7.515E+005 4.876E+005 Th-234 92.38 2.13 1.048E+006 1.05E+006 3.489E+005 5.089E+005 92.80 2 .10 1.063E+006 6.193E+005 5.163E+005 1 12.81 0.21 1.053E+007 -6.587E+005 5.113E+006 U- 235 143.76 10.96 1.659E+005 2 .91E+004 -7.878E+004 7.993E+004 163.33 5.08 3 .395E+005 -2.558E+004 1.630E+005 185.71 57.20 2 .912E+004 -7.005E+003 1.394E+004 202.11 1. 08 1.533E+006 3.503E+004 7.323E+005 2 05.31 5.0 1 3.128E+005 -1.340E+005 1.490E+005 Am-241 59.54 35.90 4.905E+004 4.91E+004 -2 .960E+00 2 2 .364E+004

     + = Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
     > == Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ = Half-life too short to be abl e to perform the decay correction

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************************** *************************'                                              * ~: **** ** * * ** * ***
****        G A M MA           S I:- E C T R U M                       A N A L Y S I S                                *****
.lename: 5452

!port Generated On 4/14/ 2 016 3:08:08 PM tmple Title B306100AFRFC003GD tmple Description U-1 STS TB FLOOR 56 3 tmple Identification tmple Type tmple Geometry !ak Locate Threshold 3 .00 !ak Locate Range (in channels ) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Si ze 1 .000E+OOO SQM tmple Taken On

quisition Started 4/14/ 2 016 2 :58:05 PM

.ve Time 600.0 seconds !al Time 601.0 seconds 1 C: ,. iad Time 0 * ..L V 0 Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TB FLOOR lM

                ~~ r   ~~'-'      \t.,.~   s~-..e     "'fb    Arc.l,..~'ll\lt  '3 -"-e.-rc.,e- ' ~ cl~
               ~.O     "'>-Sc:c.s AS     \1:k)' C:..0\\'11-..~ C!L \              -L         ~         I
                     \                                                         """'-~ 1ZI'\. c..,.\\'1!.t::.T 1)0.~tt. '~ o.\\da\eJ b/

0~ J,,/ /8' t) e,;a [98]

iak Analysis Report 4/14/ 2 0 16 3 : 08: 08 H. Page 2

****              P E A K      A N A L Y S I S           R E P O R T                 *****
**************************************************************** ~'********

Detector Name: 545 2 Sample

Title:

B306100AFRFC003GD Peak Analysis Performed on: 4/14/2016 3:08: 07 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 284 - 306 300.47 74.77 0.84 2 .25E+002 89.18 4.55E+002 2 947 - 96 1 954.64 2 38.51 1. 35 6.69E+001 41. 2 8 1. 2 4E+002 3 1401- 1412 1406.8 1 351. 67 0.55 7.53E+001 2 7. 22 4. 3 7E+001 4 2325- 2335 233 0.6 1 58 2 .81 0.30 4.17E+00 1 2 0.7 3 2.73E+001 5 24 25- 2444 2 435.38 609.02 1.14 1.09E+00 2 2 9.19 2 .96E+001 6 3634- 3648 3 640.4 2 910.4 2 0.86 4.35E+001 16.87 9.49E+OOO 7 5828- 585 2 5840.01 1 460. 2 7 2 . 17 3.79E+00 2 41. 41 1. 22 E+001 8 7049- 7062 7055.8 2 1764. 0 3 0.78 3.70E+001 12.17 O.OOE+OOO

= First peak in a multiplet region
= Other peak i n a multiplet region Fitted singlet

rors quoted at 2. 000 sigma

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1terference Corrected Acti ty Report 4/14/ 2 01 6 8 :0 8 PM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFRFC003GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K-40 1. 000 1460.82* 10 .66 7.00378E+005 9.77803E+004 Tl-2 08 1. 000 58 3 .19* 85.00 5.96712E+003 3.05316E+003 Pb-212 0.873 11 5.18 0 .60 23 8.63* 43.60 1 . 11 080E+004 7.08997E+003 30 0 . 0 9 3.3 0 Bi- 2 14 0. 32 9 609.32* 45.49 2 .99515E+004 8.76409E+003 768.36 4.89 8 0 6. 1 8 1. 26 934. 0 6 3. 11 1 120. 2 9 14.92 1 155.21 1. 63 1238.12 5.83 128 0. 98 1. 43 1377.67 3.99 1385. 3 1 0 .79 1401.52 1. 33 1407.99 2 .39 1509.21 2 .13 1661.27 1. 05 17 2 9.59 2 .88 1764.49* 15.3 0 5.36646E+004 1.81608E+004 1847.43 2 .03 2 118.5 1 1. 16 Pb- 2 1 4 0 . 491 2 41.99* 7. 25 6.67917E+004 4. 2 6052E+004 2 95. 22 1 8. 42 351.93* 35.60 1. 92 583E+004 7.61612E+0 0 3 785.96 1. 06

       * = Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :           10.0 0 0 keV Nuclide confidence index threshold                     0.30 Errors quoted at 2 . 000 s i gma

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1t erference Corrected Acti cy Report 4/14/2016 8:08 PM Page 4

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • ***********************i*******************
      • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 7.003775E+005 9.778033E+004 Tl-208 1. 000 5.967122E+003 3.053155E+003 X Bi-211 0.999 Pb-2 1 2 0.873 7.905 1 51E+003 7. 1 97705E+003 Bi-2 1 4 0.329 3.443078E+004 7.893060E+003 Pb-2 1 4 0.491 l. 92 5832E+004 7.615745E+003

      ?    Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2.000 sigma
 **********       U N I D E N T I F I E D          P E A K S      * *** , .*****

Peak Locate Performed on: 4/14/ 2 016 3: 0 8: 07 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. ( keV) Counts per Second ~ Uncertainty Type Nuclide 1 74.77 3.7479E-001 39.66 Tol. Pb214-ZR Ba-133 Pb212-XR Pb212-XR Pb2 14 -XR 6 910. 42 7.25 2 4E -00 2 38.77 Tol. Eu-1 52 Ac-228 M First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 s i gma [101]

1clide MDA Report 4/14/ 2 01( 3 :08:08 PM Page 5

• • • • N U C L I D E M D A R E P O R T *****

Detector Name: 54 52 Sample Geometry: Sample

Title:

B306100AFRFC003GD Nuclide Library Used: C:\GENI E2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) K-40 1460.8 2

• 10.66 4.796E+004 4.80E+004 7.004E+005 2 .148E+004

+                                                                                   2 .385E+004 Cr-51        320.08       9.91   5.005E+004      5.00E+004 1. 790E+004 Mn-54        834.85     99.98    5.459E+003      5.46E+00 3 -2 . 27 4E+00 3  2 .531E+003 Co-58        810.76     99.45    5.406E+003      5.41E+00 3 2 .782E+00 3     2 .507E+003 Co-60      1173. 23     99.85    6.415E+003      4.49E+00 3 1.398E+003       2 .970E+003 133 2 .49    99.98    4.487E+00 3                 -2 .539E+003    l .991E+003 Nb-94        702.65     99.81    5. 32 9E+00 3   4.71E+00 3 1.040E+002       2 .483E+003 871. 09    99.89    4.711E+00 3                   4.678E+003    2 .152E+003 Sn-113       255.13       2 . 11 2 .568E+005     7.84E+ 00 3 -5.842E+004     1. 2 35E+005 391. 7 0   64.97    7.8 3 7E+003                  2 .403E+003   3.716E+003 Cs- 1 34     475.36       1. 48  3. 2 16E+005    6.34E+003 1. 2 15E+005      l. 5 08E+005 563 . 25     8 . 34 5.631E+004                  - 7.076E+003    2.622E+004 569.33     15.37    3. 2 74E+004                -5.858E+002     1.531E+004 604.72     97.6 2   7.730E+00 3                 -2 . 2 67E+003  3.693E+003 795.86     85.46    6.335E+00 3                 -5 .156E+002    2.941E+003 8 01. 95     8.69   5.888E+004                  -3.370E+004     2.720E+004 1038.61        0 .99  5.158E+005                  -2 .32 9E+005   2.354E+005 1167.97        1. 79  3.539E+005                  - 1.707E+005    1.637E+005 1 3 65. 1 9    3.0 2  1.182E+005                  - 4.565E+004    5.060E+004 Cs-137       661.66     85.10    4.913E+003      4.9 1E+00 3 -1.940E+00 3    2.Z50E+003 Eu-152       1 2 1. 78  2 8.67   2.016E+004      1 .93E+004 -2 .038E+004     9.809E+003 2 44.70      7.61   7.169E+004                  -2 .741E+004    3.454E+004 2 95.94      0.45   1. 2 64E+006                  1.697E+006    6.071E+005 3 44. 2 8  26.60    1.926E+004                  - 3 .033E+002   9.173E+003 3 67. 7 9    0.86   5.615E+005                    2 .055E+005   2 .661E+005 411.12       2 .24  2.167E+005                  -1. 2 02E+005   1.0 2 3E+005 443.96       2 .83  1.806E+005                    6.236E+004    8.534E+004 488.68       0.42   1.149E+006                    5.696E+005    5.388E+005 563.99       0.49   9.713E+005                  -2 .890E+005    4.527E+005 586.26       0.46   1 .463E+006                   1.094E+006    6.957E+005 678.62       0.47   9.944E+005                  - 1. 746E+005   4.594E+005 688.67       0.86   6.480E+005                    3.092E+005    3.031E+005 719.35       0. 2 8 1.915E+00 6                 -2.584E+005     8.919E+005 778.90     12.96    4.132E+004                  -8.377E+00 3    1 .918E+004 810.45       0.32   1. 67 5E+00 6                 3. 2 95E+005  7.764E+005 867.37       4.26   1.154E+005                  -1.163E+005     5. 2 94E+004 919.33       0.43   1.310E+00 6                   7.8 2 1E+005  6.059E+005 964.08     14.65    4.564E+004                    3 . 2 16E+003 2 .136E+004 1085.87      10.24    5.579E+004                    2 .442E+004   2 .567E+004 1089.74        1. 73  2 .790E+00 5                -2 .629E+005    1. 2 63E+005 11 1 2 .07   13.69    3 .955E+004                 -4.856E+004     1.809E+004 1 2 12.95      1. 43  4.103E+00 5                 -3 .800E+005    1.883E+00 5

[102]

1clide MDA Report 4/14/ 2 011 3 :08:08 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( %) {pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Eu- 1 52 1249.94 0.19 3.038E+006 1 . 93E+004 -7.456E+005 1. 390£+00 6 1 2 99.14 1. 63 3.561£+005 2 .570E+005 1.627£+00 5 1408.01 2 1. 07 2 . 2 00E+004 -5.483E+00 3 9.761E+00 3 1457.64 0 . 50 3 .776E+006 1.589E+007 1.835E+00 6 1 52 8.10 0.28 1.141E+006 -5.394E+004 4.732E+005 Eu- 1 54 1 23 .07 40.40 1.472E+004 1 . 47E+004 6.010E+002 7.168E+003 2 47.93 6.89 7.646E+004 -3 .578E+004 3 .678E+004 591.76 4.95 9.894E+004 - 1.008E+005 4.612E+004 692.42 1. 78 2 .971E+00 5 - 1.934E+005 1 .384E+005 723.30 20.06 2 .731E+004 -1.972E+004 1.274E+004 756.8 0 4.5 2 1.223E+005 1.888E+004 5.696E+004 873. 1 8 12 .08 3.993E+004 -2 .126E+004 1.8 2 8E+004 996. 2 9 10.48 4.830E+004 1. 25 2E+004 2 . 2 07E+004 1004.76 18.01 2 .535E+004 - 8.574£+003 1.146£+004 1 27 4.43 3 4.80 l.523E+004 -1.556E+004 6.904E+00 3 1 59 6 .48 1. 80 2 .404E+00 5 8.700£+00 3 1.045E+00 5 Eu-15 5 45.30 1. 31 2 .872E+005 2 . 2 3E+004 1.585E+005 1.377E+00 5 60.01 1.22 4.131E+005 1.560E+005 2 .002E+00 5 86.55 3 0.70 2. 232E+004 2 .894E+004 1.091E+004 10 5.31 21.10 3. 003E+004 6.708E+003 1.465E+004

+     Tl-2 0 8     583 , 19* 85.00    4.206E+00 3    4. 2 1E+00 3   5.967E+003    l.9 1 0E+003 Bi-2 11      351.07*   13.02    2 .603E+004    2.60E +004 5 . 2 66E+004     1. 207E+004 Pb-211       4 0 4.85    3.78   1.384E+005     1. 38E+005 9.934E+004        6.565E +004 427. 0 9    1. 76  2 .630E+005                   1.479E+005    1. 2 37E+005 832. 0 1    3.52   1 .508E+005                   5.260E+003    6.978E+004 Bi- 212        39.86     1. 06  3.494£+005     8.58E+004      1.002E+005    1.674E+005 727.33      6.67   8.584£+004                    6.509E+004    4.015£+004 785.37      1.10   4.799£+005                    9.339£+004    2.2 2 5E+005 1 62 0 .50    1. 47  2 .879E+005                   8.920E+004    1. 2 46E+005
+     Pb- 2 12     115.18      0 . 60 1.023E+006     l.08E+004 1.010E+006         4.988E+005 2 38.63*  43 . 60  1.081E+004                    1 .111E+004   5.180E+003 300.09      3.30   1 .52 4E+005                -2 .716E+005    7.280E+004 Pb21 2 -XR     74.82   10 . 28  7.179E+004     4.05E+004 1.411E+004         3 .515E+004 77.11   17. 10   4.047E+004                  -2 . 3 31E+002  1.978E+004 87.35     3.97   1.714£+005                    1. 775E+005   8. 3 77E+004 89.78     1.46   4.488E+005                  -2.621E+003     2.191E+005
+     Bi- 21 4     609.32*   45.49    9.907E+003     3.92E+003 2.995E+004         4.583E+003 768.36      4.89   1. 2 04E+005                -3.804E+004     5. 62 9E+004 8 0 6.18    1. 2 6 4.169E+005                    4.946E+003    1.930E+005 934.06      3.11   1.770E+005                    1. 2 31E+00 5 8. 1 71E+004 1120. 2 9   14.92    5.082E+004                    3.763E+004    2 . 3 86E+004 1155.21       1. 63  3.753E+005                  - 5.617E+005    1. 73 3E+00 5 1238.12       5.83   1 . 2 13E+005                 8.838E+004    5.649E+004 1280.98       1. 43  3.808E+005                    2 .564E+005   1.731E+005 1377.67       3.99   1.098E+005                    1. 2 94E+004  4.842E+004 1385.31       0. 79  5.136E+005                  -8. 2 82E+004   2 . 2 42E+005 1 401.52      1.33   3 .476E+005                 -1.472E+005     1.542E+005 1407.99       2 .39  1.936E+005                  -4.8 2 5E+004   8.591E+004 1509. 2 1     2.13   1.841E+005                    1. 22 8E+00 5 7.924E+004 1 661. 2 7    1. 05  3.065E+005                    1.4 2 9E+00 5 1. 2 56E+00 5

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lClide MDA Report 4/14 /2 01 3 :08:08 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM)

+     Bi-2 14     1729.59       2.88   1.623E+005     3 .92E+003      1.219E+005    7.087E+004 1764.49*     15.30   3 .925E+003                    5.366E+004    O.OOOE+OOO 1847.43       2.0 3  1 .583E+005                  -8.416E+00 3    6. 3 95E+004
  >               2118.51       1.16   O.OOOE+OOO                     O.OOOE+OOO    O.OOOE+OOO
+     Pb- 2 14      2 41.99*    7.25   6.500E+004     9.52E+00 3      6.679E+004    3.115E+004 2 95. 22   18.42   3.113E+004                     3.495E+004    1.496E+004 351.93*    35.60   9. 52 0E+003                   1. 926E+004   4.414E+003 785.96      1. 06  5.033E+005                     l.207E+005    2 . 33 5E+005 Pb214-XR        74.82     5.80   1. 272E+005    7.13E+004       2 .501E+004   6. 22 9E+004 77.11     9.70   7.134E+004                   -4.109E+002     3.488E+004 87.35     2 . 24 3.038E+005                     3 .145E+005   1 .485E+005 89.78     0 .8 2 7.991E+005                   - 4.667E+003    3.902E+005 Ra-226        186. 2 1    3.64   1. 4 61E+005   1. 4 6E+005   -7.441E+003     7.068E+004 Ac-228        1 2 9.07    2.42   2 .598E+005    2 . 72 E+004    1.8 2 8E+005  1. 2 67E+00 5 2 09. 2 5   3.89   1 . 422E+005                   4.464E+004    6 .877E+004 2 70. 2 4   3.46   1.588E+005                     6.189E+004    7.633E+004 328.00      2.95   l.640E+005                     2 . 940E+003  7.798E+004 338. 32    11. 27  5.034E+004                     7.360E+003    2 .410E+004 409.46      1. 92  2.651E+00 5                    l.051E+005    1. 2 55E+005 463.00      4.40   1.155E+005                     l.612E+003    5.447E+004 794.95      4. 2 5 l.273E+005                     l.554E+004    5.911E+004 911. 2 0   25.80   2 .720E+004                    2 .511E+004   1. 279E+004 964.77      4.99   1 .375£+005                    l .636E+005   6.445E+004 968.97     15.80   4. 2 98E+004                   3 .616E+004   2 .013E+004 1588.20       3.22   l .645E+005                    l.027E+005    7 .3 54E+004 Pa- 23 1        27.36    10.30   2 .155E+004    2 .16E+004      l.198E+004    1.003E+004 283.69      1. 70  2 .888E+005                  - 8.146E+004    1. 38 0E+00 5 300.07      2. 47  2 .036E+005                  - 3.629E+005    9.7 2 5E+004 302.65      2 . 20 2 . 2 69E+005                  2.463E+00 4   l.083E+005 330.06      1. 40  3.545E+005                     3.673E+004    l.688E+005 Th - 2 3 4      92.38     2 .13  3.022E+005     3 .02E+ 00 5  - 8.686E+004    l.475E+00 5 92.80     2 . 10 3.047E+005                   - 9.958E+004    l.487 E+00 5 112.81      0. 2 1 2 .854E+006                  -l.752E+006     1.390E+00 6 U-235         143.76     10.96   5. 2 00E+004   9 . 24 E+00 3 -l.086E+004     2 .528E+004 163.33      5.08   l.153E+005                   -3 .421E+004    5.601E+004 1 85.7 1   57. 2 0 9. 238 E+003                   l. 33 5E+003  4.469E+003 2 0 2 . 11  1. 08  5. 25 0E+005                   3. 2 52E+005  2 .542E+005 2 05.31     5.0 1  l.1 2 0E+00 5                  4. 3 29E+004  5.4 2 1E+004 Am- 2 41        59.54    35.90   l.373E+004     l.37E+004     -3 . 9 60E+00 3 6 .653E+003
     + = Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ = Half-life too short to be able to perform the decay correction

[104]

******~'******************~     *************************' w****************
****         G A MMA      S 1-' E C T R U M       A N A L Y S I S                    *****
********************~***************************************************

.lename: 545 2 iport Generated On 4/18/2016 3:12:11 PM 1mple Title B306100AFRWC004GD 1mple Description TB 560 tmple Identification 1mple Type 1mple Geometry !ak Locate Threshold 3 .00 iak Locate Range (in channels) 85 - 8192 !ak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmpl e Si ze 1.000E+OOO SQM tmple Taken On

quisition Started 4/18/2016 3 :0 2 :09 PM

.ve Time 600.0 seconds !al Time 600.6 seconds iad Time 0. 09 s;; Energy Calibration Used Don e On 1/13 /2 015 Efficiency Calibration Used Done On 4/14 /2 016 Efficiency ID TBWALL 1)C\il\ \\o.\,c'\akJ by Q~~ I c)- 5J 18

                                                                    ~ ~ /0

[105]

iak Ana~ysis Report 4/18/2016 3:12:11 PM Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 545 2 Sample

Title:

B306100AFRWC004GD Peak Analysis Performed on: 4/18/2016 3:1 2 : 1 0 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8 1 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV ) Area Uncert. Counts 1 297- 3 08 301.83 75.11 0.51 5.80E+001 45.00 1 .78E+002 2 368- 376 371. 4 7 9 2 .54 0. 3 8 2 . 2 0E+001 2 5.94 6.70E+001 3 5828 - 5851 5839.98 1460. 26 2 .01 1 .53E+00 2 2 4.74 O.OOE+OOO First peak in a multiplet region Other peak in a multiplet region Fitted singlet

rors quoted at 2 . 000 s igma

[106]

1terference Corrected Acti ty Report 4 /18/ 2 016 ~ . :2: 11 PM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFRWC004GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence ( keV) ( 'o ) (pCi/SQM ) Uncertainty K-40 0.999 1 460.82* 10.66 1.04309E+006 l .91441E+005 Cd-109 0.968 88.03* 3.70 1.40078E+005 l .67541E+005 Th227-XR 0.375 85.43 1. 34 88.47* 2 .18 2.37747E+005 2 .84603E+005 Ac228-XR 0.391 89.96 1. 90 93.35* 3.10 1.67190E+005 2 .04370E+005

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuclide confidence index threshold =               0.30 Errors quoted at 2 .000 sigma

[107]

1terference Corrected Acti ty Report 4/ 1 8/2016 L2: 11 PM Page 4 "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 0.999 l.043087E+006 l.914407E+005

  ?   Cd-109       0.968        l.400778E+005        l.675406E+005
  ?   Th227-XR     0.375        2.377467E+005        2 .8460 2 7E+005
  ?   Ac228-XR     0.391        l.671896E+005        2 .043697E+00 5
      ?    Nuclide i s part of an undetermined solution X    Nuclide rejected by the interference analysis
      @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .000 sigma
 **********     U N I D E N T I F I E D         p E A K      s   **********

Peak Locate Performed on: 4/ 1 8/2 0 1 6 3:1 2 :10 PM Peak Locate from Channel: 85 Peak Locate To Channel: 81 92 Peak Energy Peak Si ze in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 75.11 9.66 1 7E-002 77.62 Tol. Pb2 1 4-XR Ba- 1 33 Pb212-XR Pb212-XR Pb2 1 4-XR M = First peak in a multiplet region rn = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000 s i gma [108]

tclide MDA Report 4/18/ 2 011., 3: 12 :11 PM Page 5

• • • • N U C L I D E MD A R E P O R T *****

Detector Name: 545 2 Sample Geometry : Sample

Title:

B306100AFRWC004GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL . NLB Nucli de Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV ) ( ~) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM )

+      K-40       1460.8 2

• 1 0 .66 1.845E+004 1.84E+004 1.043E+006 O.OOOE+OOO Cr-51 320.08 9.91 1.351E+00 5 1.35E+005 5.795E+004 6. 2 88E+004 Mn-54 834.85 99.98 1.427E+004 1.43E+004 1.049E+003 6. 3 91E+003 Co-58 810.76 99.45 1.513E+004 1.51E+004 -5.638E+002 6.828E+003 Co-60 1173.23 99.85 1.559E+004 1.43E+004 8.186E+002 6.915E+00 3 133 2 .49 99.98 1.429E+004 8.616E+002 6.211E+00 3 Nb - 94 70 2 .65 99.81 1.476E+004 1.38E+004 1.006E+004 6.691E+00 3 87 1. 09 99.89 1.375E+004 2 .077E+003 6. 11 9E+00 3 Sn- 11 3 255.13 2 .11 7.564E+005 2 .50E+004 l.791E+005 3.586E+00 5 391.70 64.97 2.500E+004 1.543E+004 l.171E+004 Cs - 13 4 475.36 1. 48 9. 006E +005 1. 66E+004 5.731E+005 4.119E+005 563.25 8 .34 1.565E+005 -9.693E+004 7.083E+ 0 04 569.33 15.37 8.531E+004 7.454E+002 3.862E+004 604.72 97.6 2 2 .132E+004 7.168E+003 l.OOOE+004 795.86 85.46 1 .662E+004 9.916E+003 7.459E+00 3 801. 95 8.69 1. 35 9E+005 -l.551E+005 5.954E+004 1 038.61 0 .99 1.418E+006 3 .856E+005 6. 2 56E+005 1 167.97 1. 79 7.697E+005 1 .015E+005 3 . 3 60E+005 1 365.19 3.02 3.676E+005 -1. 3 32E+005 l.524E+005 Cs- 1 37 661. 66 85.10 l.885E+004 1.89E+004 5. 3 41E+002 8.641E+003 Eu-1 52 1 2 1. 78 2 8.67 5.897E+004 5.7 1E+004 2.128E+004 2 .837E+004 244.70 7.6 1 2.121E+005 6.868E+004 l .007E+005 295.94 0.45 3.657E+006 2 .858E+006 l.729E+00 6 344. 2 8 2 6.60 5.715E+004 - l.732E+004 2 .676E+004 367.79 0.86 1.602E+006 2 .134E+004 7.4 3 1E+005 411 . 1 2 2.24 6.586E+005 1.908E+005 3 .057E+005 443.96 2.83 4.750E+005 4.0 3 6E+005 2 .182E+005 488.68 0.42 3.429E+006 -l. 2 13E+005 l.578E+006 563.99 0. 4 9 2.735E+006 -8.553E+005 1. 2 42E+006 586. 2 6 0.46 3.634E+006 l.711E+006 l.680E+006 678.62 0.47 2.797E+006 -l.730E+004 1.255E+006 688.67 0.86 1.723E+006 6.461E+005 7.822E+005 719.35 0. 2 8 5.771E+006 -l. 25 8E+005 2.637E+006 778.90 12.96 l.007E+005 - 3.518E+004 4.480E+004 8 1 0.45 0.32 4.830E+006 1.246E+0 0 6 2 . 1 87E+00 6 867.37 4.26 3.346E+005 -l.517E+005 l.496E+005 919.33 0. 43 3.431E+006 9.630E+005 1. 5 34E+006 964. 0 8 14.65 l.081E+005 -l.378E+005 4.862E+004 1085.87 10.2 4 1.187E+005 3.363E+004 5.111E+004 1089.74 1. 73 7.702E+005 -3 .049E+005 3.362E+005 111 2 .07 13.69 1 . 1 76E+005 -6.570E+004 5.255E+004 121 2 .95 1. 43 l. 2 20E+006 -6.348E+005 5.476E+00 5

[109]

tclide MDA Report 4/18/201\., 3:12:11 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM) Eu-15 2 1 2 49.94 0.19 8.311E+006 5.71E+004 2 .386E+006 3 .677E+006 12 99. 1 4 1. 63 9.170E+005 -2 .464E+003 4.018E+005 1408.01 21.07 7.392E+004 3 . 7 50E+004 3. 2 39E+004 1457.64 0.50 8.912E+006 2 .324E+007 4. 2 60E+006 1 52 8.10 0. 2 8 3 .473E+006 -2 .517E+006 1. 378E+00 6 Eu-154 123.07 40.40 4.125E+004 4.13E+004 -3 .200E+004 1 . 983E+004 247.93 6.89 2 .283E+00 5 2 .803E+004 1.082E+005 591.76 4.95 2 .661E+005 1.825E+005 1. 2 03E+005 692.42 1. 78 7.875E+005 -2 .348E+004 3.554E+005 723.30 2 0.06 7.750E+004 -1.168E+004 3.528E+004 756.80 4.52 2 .850E+005 -1.910E+00 5 1. 2 68E+005 873.18 12 .08 1.042E+005 -7.543E+004 4.582E+004 996. 2 9 10.48 1.510E+005 5.713E+00 3 6.776E+004 1004.76 18.01 8.187E+004 1. 2 44E+004 3.642E+004 1274.43 34.80 4.454E+004 1.331E+004 1.965E+004 1596.48 1. 80 6.774E+005 -2 .668E+005 2 .809E+005 Eu-155 45.30 1. 3 1 8.915E+005 6.84E+004 5.961E+005 4.215E+005 60.01 1. 22 1.254E+006 4.484E+004 6.012E+005 86.55 30.70 6.841E+004 4.610E+004 3.317E+004 1 05.31 21.10 8.3 57 E+004 -2 .900E+004 4.027E+004 Tl-208 583.19 85.00 2.014E+004 2 .01E+004 2.388E+004 9. 3 31E+003 Bi-211 351. 07 1 3.02 1.463E+005 1.46E+005 7.141E+004 6.9 43E+004 Pb-211 404.85 3.78 3.961E+00 5 3 .82E+005 1.614E+005 1.842E+005 4 27 .09 1. 76 8. 2 49E+005 8.468E+004 3 .819E+005 8 32 .01 3.52 3.822E+005 4.745E+004 1.700E+005 Bi -2 1 2 39.86 1. 06 1.017E+006 2 .31E+005 9.572E+005 4.783E+005 727.33 6.67 2 .306E+00 5 5.99 1E+004 1.049E+005 785. 3 7 1.10 1.259E+00 6 5.515E+005 5 . 6 38E+005 1620.50 1. 4 7 9.553E+005 1.017E+005 4.064E+005 Pb-212 115.18 0.60 3.043E+006 4.36E+004 1.120E+006 1.468E+006 238.63 43.60 4.3 60E+004 2.692E+004 2 .088Et004 300.09 3.30 4.485E+005 -5.566E+005 2 .106E+005 Pb 212 - XR 74.8 2 10.28 2 .265E+005 1.30E+005 3 . 3 18E+005 1.101E+005 77.11 17.10 1.300E+005 4.743E+00 3 6.313E+004 87.35 3.97 5. 3 49E+005 7.639E+005 2 .594E+005 89.78 1. 46 1.326E+006 -1.388E+006 6.413E+005 Bi -2 14 609.3 2 45.49 4.778E+004 4.78E+004 5.200E+004 2.248E+004 768.36 4.89 3 .266E+005 1.983E+005 1.487E+005 806. 1 8 1. 26 l.130E+006 5.309E+005 5.073E+005 934.06 3.11 4.937E+005 -8. 2 62E+00 3 2.216E+005 1120.29 14.92 1.410E+005 l .011E+005 6.477E+004 1155.21 1. 63 8.618E+005 -3.346E+005 3.776E+005 1238.12 5.83 3.114E+005 -2.234E+005 1.403E+005 1280.98 1. 43 1.156E+006 1.037E+006 5.144E+005 1377.67 3.99 3.316E+005 - 3.083E+004 1.4 2 0E+005 1385.31 0.79 1.673E+006 - 6.130E+005 7.163E+005 1401. 52 1. 33 1. 2 27E+006 3.581E+005 5.411E+005 1407.99 2.39 6.506E+005 3.300E+005 2 .851E+005 1509. 2 1 2 .13 5.227E+005 -2.524E+005 2 .143E+005 1661. 2 7 1. 05 1.191E+006 - 7. 1 32E+005 4.940E+005 [110]

1cli.de MDA Report 4/18/ 2 0H, 3:12: 1 1 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) Bi -2 14 1729.59 2 .88 4.441E+005 4.78E+004 2 . 2 39E+005 1.842E+00 5 1764.49 15.30 1.409E+005 1.041E+005 6.321E+004 1847.43 2 .03 5.812E+005 2.473E+005 2 .348E+00 5

 >                  2118.51        1.16 O.OOOE+OOO                      O.OOOE+OOO     O.OOOE+OOO Pb-214        241.99       7.25 2.611E+005      5.38E+004       2.926E+005     1.250E+005 295.22     18.4 2 8.883E+004                      6.424E+004     4. 2 00E+004 351.93     35.60 5.380E+004                      2.985E+004      2 .553E+004 785.96       1. 06 1.332E+006                     6.010E+005     5.979E+005 Pb214-XR        74.82      5.80 4.014E+005      2 . 2 9E+005    5.882E+005     1.952E+005 77.11      9.70 2 .292E+005                    8.361E+003      1.113E+005 87.35      2.24 9.480E+005                     1.354E+006      4.598E+005 89.78      0 .82 2 .36 1E +006                -2 .471E+006     1.142E+006 Ra-226         1 86.2 1     3.64 4.263E+005      4. 2 6E+005    8.371E+004     2 .034E+005 Ac-2 2 8       1 2 9. 07    2 .42 7.610E+005     7.62E+004      2 . 2 05E+005  3.671E+005 209.25       3.89 4.023E+005                    -9.643E+004     1.915E+005 270.24       3. 46 3.914E+005                    2 .046E+005    1.834E+005 328.00       2.95 4.665E+005                   -3.573E+004      2 .173E+005 338.32     11. 27 1.419E+005                     6.370E+003     6.671E+004 409.46       1. 92 8.082E+005                    5.060E+005     3.767E+005 463.00       4.4 0 3.018E+005                    1. 27 9E+005   1.382E+005 794.95       4.25 3.340E+005                     9.770E+004     1. 4 99E+005 91 1. 20   25.8 0 7.6 1 5E+ 0 04               - 6.668E+003     3.507E+004 964.77       4.99 3.122E+005                   - 6.230E+005     1.401E+005 968.97     15.80 1.070E+005                      7.254E+004     4.843E+004 1 588.2 0      3.22 4.627E+005                     3.088E+005     1 .992E+005 Pa-23 1          27.36    10.30 6.807E+004      6 . 81E+004     3.555E+004     3.095E+004 2 83.69      1. 70 7.743E+005                    1.230E+005     3.615E+005 300.07       2 .47 5.992E+005                  - 7.436E+005     2.814E+005 302.65       2 . 2 0 6.637E+005                  5.887E+005     3 .114E+005 330.06      1. 40 9.787E+005                     4.319E+005     4.557E+005 Th-234           92 . 3 8  2 . 1 3 8.636E+005   8.6 4E+00 5   - 1 .234E+005    4.169E+005 92.80     2 . 1 0 8.713E+005                   2.653E+005     4. 2 05E+005 112.81        0. 2 1 8.432E+006                 -4.115E+006      4.064E+006 U-235         143.76      10.96 1.544E+005      2 .74E+004      2.513E+004     7.4 1 8E+004 1 63.33      5.08 3 .193E+005                     8.806E+003     1. 52 9E+005 1 85.71     57. 2 0 2 .735E+004                 -2 . 2 91E+00 3  1.306E+004 2 02.11      1. 08 1. 2 74E+006                 -1. 1 62E+006    6.027E+005 205.3 1      5.01 3 .039E+005                     5.902E+004     1.445E+005 Am-24 1         59.54     35.90 4.077E+004      4.08E+004     -2.446E+004      1.950E+004
     + = Nuclide identified during the nuclide identification
      * = Energy line found in the spectrum
     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @     Half-life too short to be able to perform the decay correction

[111]

**************************     *************************            I- ***************
****         G A MM A    S P E C T R U M          A N A L Y S 1. S                *****
.lename: C:\GENIE2K\CAMFILES\00001407.CNF iport Generated On                 5/ 3 /2016        6:53:0 2 AM tmple Title                        B306100AFRWC005GD tmple Description                  TB WALL tmple Identification tmple  Type tmple  Geometry iak Locate Threshold                 3.00 iak Locate Range (in channel s )        85 -     8 1 92

!ak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Size 1. OOOE+OOO SQM tmple Taken On

quisition Started 5/2/20 1 6 3:3 1 : 32 PM

.ve Time 600.0 seconds ial Time 600.5 seconds iad Time 0 . 09 % En ergy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBWALL DJa~o.\ida+ed Joy

                                                                        ~
                                                                        /~~o- It t1 /,I()

[112]

iak Analysis Report 5/3/2 01 6 6:53:02 AM Page 2

"***               P E A K        A N A L Y S I S          R E P O R T                 *****

Detector Name: 5452 Sample

Title:

B306100AFRWC005GD Peak Analysis Performed on: 5/3/2 01 6 6:53: 0 1 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV ) Area Uncert. Counts 1 296- 306 3 00. 2 0 74.70 0.34 3 . 5 5E+001 48.77 2 .34E+002 2 946- 959 953 . 33 238. 1 9 0.4 2 4. 3 9E+001 28.17 5.61E+001 3 1400- 1413 1406.67 351. 64 0.35 4.lOE+OOl 22.33 3.00E+OOl 4 2 42 6- 2 440 2 433.90 608.65 1. 46 7.llE+OOl 2 1. 88 1.69E+001 5 58 2 6- 5848 58 3 7.65 1459.68 1. 82 1.51E+002 26.92 8.05E+000

= First peak in a multiplet region Other peak in a multiplet region
= Fitted singlet

rors quoted at 2.000 s igma

[113]

1terference Corrected Acti* .y Report 5 / 3 / 2 01 6 6 3:02 AM Page 3 "*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample

Title:

B306100AFRWC005GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K-40 0.998 1460.8 2

• 10.66 1.02889E+006 2 .04078E+005 Pb-212 0.87 2 115.18 0.60 2 38.63* 43.60 2 .97822E+004 1.96939E+004 3 00.09 3.30 Pb-214 0. 4 92 2 41. 99* 7. 2 5 1 .79079E+005 1.18350E+005 2 95. 22 18.42 351.93* 35 .60 4.13939E+004 2 .35007E+004 785.96 1. 06

      * = Energy l ine found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuclide confidence index threshold=                0.30 Errors quoted at 2 . 000 sigma

[114]

tterference Corrected Acti * -Y Report 5/3/20 1 6 6 3:02 AM Page 4 "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0 .998 1 .0 2 8893E+006 2 .040784E+005 X Bi-21 1 0.999 Pb-212 0 .872 2.289805E+004 2 .006629E+004 Pb-214 0 . 4 92 4.139387E+004 2 .350013E+004

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysi s
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at          2 .000 sigma
 ******* **     U N I D E N T I F I E D             P E A K S     **********

Peak Locate Performed on: 5/3/2 01 6 6:53: 0 1 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . ( keV) Counts per Second *nty Type Nuclide 1 74.7 0 5.9190E- 0 02 Tol. Pb214-XR Ba-133 Pb212-XR Pb212-XR Pb214-XR 4 608.65 l . 1852E-001 Tol. Zr-97 Sb-125 Sb-125 M = Fir s t pea k in a multiplet region m = Other peak in a multiplet region

                                                                                 ~

F = Fitted singlet Errors quoted at 2 . 000 sigma [115]

1clide MDA Report 5/3/20 1 6 6:53:02 AM Page 5

• • • • N U C L I D E M D A R E P O R T **** '~

Detector Name: 545 2 Sample Geometry: Sample

Title:

B306100AFRWC005GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) (%) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM)

+      K-40       1460.82* 1 0 .66       1.417E+005     1.42E+005 1.029E+006        6.163E+004 Cr-51        320.08        9.91   1.552E+005     1 .55E+005 8.577E+004       7.290E+004 Mn- 54       834.85     99.98     1.595E+004     1 .59E+004 1.751E+003       7.231E+00 3 Co-58        810.76     99. 4 5   1.648E+004     1.65E+004 -8.591E+003       7.501E+00 3 Co-60      117 3 . 23   99.85     1.456E+004     1 .43E+004 - 1.351E+003     6.402E+00 3 1 332 .49    99.98     1.4 2 9E+004                 1.034E+004    6.211E+00 3 Nb-94        702.65     99.8 1    1 .411E+004    1. 40E+004 -2 .017E+004     6.369E+003 871.09     99.89     1.403E+004                 -3 .541E+003    6. 2 56E+003 Sn-113       2 55.13      2 .11   7.905E+00 5    2 .18E+004 -3 .900E+004     3.756E+005 3 91.70    64.97     2 .177E+004                -1.303E+004     1.009E+004 Cs-134       4 75.36      1. 48   8.792E+005     1.80E+004 -5.646E+005       4.012E+005 563.25       8.34    1.836E+OOS                   7. 2 08E+004  8.438E+004
                    .569. 33   15.37     9.581E+004                   4.458E+004    4.387E+004 6 0 4.72   97. 62   2.503E+004                  -1.926E+00 3   1 . 1 86E+004 795.86     85.46    1.799E+004                  - 5.796E+003    8.145E+003 801.95       8.69   1.852E+005                    1 .111E+005   8.420E+004 10 38.61       0 .99  1.631E+006                    8.175E+005   7.319E+005 11 67.97       1. 79  8.857E+005                    5.367E+00 5  3 .940E+005 1365.19        3.0 2  4.035E+OOS                 -8.572E+004     1. 704E+005 Cs-137        661. 66    85.10    1 .885E+004    1.89E+004 1 .379E+004       8.641E+00 3 Eu-15 2      121.78      2 8.67   6.668E+004     5.4 2E+004 6.749E+004       3 .222E+004 2 44.70       7.61   2.335E+00 5                   1.951E+004   1.114E+005 2 95.94       0.45   3.934E+00 6                   3.863E+005   1.867E+006 3 44. 2 8  26 .60    5.417E+004                 -5.582E+00 4    2 . 52 8E+004 3 67.79       0 .86  l.812E+006                    3.004E+005   8.485E+005 411.12        2 .2 4 6.848E+005                 - 1.080E+005    3.189E+005 443.96       2 .83   4.800E+005                 - 1 .961E+005   2 . 2 07E+005 488.68       0.42    3.249E+006                 -2 .127E+006    1.488E+00 6 563.99       0.49    3.184E+006                   2 . 3 44E+006 1.466E+006 586.26       0.46    3.948E+006                    9 .859E+005  1.837E+006 67 8. 62     0.47    3. 1 99E+006                 1.145E+006    1.456E+006 688.67       0.86    1.625E+006                    6.812E+004   7.333E+005 719.35       0. 2 8  5. 2 61E+006               -2 .536E+005    2 .382E+006 778.9 0    12.96     1.208E+005                 - 4.927E+004    5.487E+004 81 0 .45     0 .32   4.969E+006                 -6.109E+006     2.256E+00 6 867.37       4.26    3 .153E+005                -2 .611E+005    1.399E+005 919.33       0.43    3 .793E+006                  2 .388E+006   1.715E+006 964.08     14.65     1.307E+005                   1.156E+005    5.992E+004 1085.87      10.24     1.583E+005                   1. 2 05E+005  7.088E+004 1089.74        1. 73   9.040E+005                 -9.033E+004     4.031E+00 5 1 112.07     13.69     1.108E+005                 -2.319E+005     4.915E+004 1212.95        1. 43   1.085E+006                 -8.033E+005     4.803E+OOS

[116]

tclide MDA Report 5/3/2016 6:53:02 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity De c . Leve l Name (keV) (% ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) Eu- 1 52 1249.94 0.19 9.658E+006 5.42E+004 2 .663E+006 4.351E+006 1299.14 1. 63 8.161E+005 -2 .771E+005 3.514E+005 1408.01 21. 07 7.941E+004 2 .288E+004 3.5 1 4E+004 1457.64 0.50 9.095E+006 2 .300E+007 4.352E+006 1528.10 0.28 3.978E+006 -1.921E+006 1.631E+006 Eu-154 123.07 40.40 4. 5 55E+004 4.56E+004 -3.389E+004 2 .198E+004 247.93 6.89 2 .404E+005 -4. 22 9E+004 1.143E+005 591.76 4.95 2 . 6 61E+005 1 . 8 64E+005 1. 2 03E+005 692.42 1. 78 8.576E+005 -1. 1 67E+005 3 . 9 04E+005 723.30 2 0.06 8.143E+004 7.114E+004 3 . 72 5E+004 756.80 4. 52 3 .123E+005 1.181E+005 1 .404E+00 5 873. 1 8 12.08 1 .115E+005 - 1. 2 07E+005 4.949E+004 996. 2 9 10.48 1.536E+005 8.569E+003 6.905E+004 1004.76 18.01 9.121E+004 9.346E+004 4.109E+004 1274.43 34.80 4.941E+004 2 . 23 7E+004 2 .209E+004 1 596.48 1. 80 6.411E+005 -4.727E+005 2.628E+005 Eu-155 45.30 1. 31 9.119E+005 7.05E+004 1.943E+005 4.317E+005 60.01 1. 22 1.271E+006 -5.124E+005 6.095E+005 86.55 30.7 0 7.048E+004 3.330E+004 3 .421E+004 10 5.31 2 1. 1 0 9.160E+004 - 9.047E+002 4.428E+004 Tl-208 583.19 85.0 0 2.272E+004 2 . 2 7E+004 2 .076E+004 1.062E+004 Bi-21 1 351.07* 1 3.0 2 9.055E+004 9.06E+004 1 .132E+005 4.154E+004 Pb-2 1 1 404.85 3.78 4.199E+005 4. 2 0E+005 -5.025E+004 1.961E+005 427.09 1. 76 8.738E+005 - 4.198E+005 4.064E+005 832.01 3.5 2 4.586E+005 - 4.462E+004 2 .082E+005 Bi-212 39.86 1. 06 1 . 0 39E+006 2.37E+005 -1.854E+005 4.893E+005 727.33 6.67 2 . 3 67E+005 -1. 2 53E+005 l.079E+005 785.37 1.10 1.446E+006 -3 .902E+005 6.574E+005 1620.50 1. 47 6.326E+005 2 .107E+005 2 .451E+005

+     Pb-2 1 2     115.18       0.60   3.191E+006     2.96E+004      1. 3 90E+006  1. 542E+006 238.63*    43.60    2 .955E+004                   2.978E+004    1. 3 86E+004 30 0 . 0 9   3.30   5.0 2 3E+005                -6.990E+005     2 .375E+005 Pb212-XR       74.8 2   10. 2 8  2 .565E+005    1 .4 1E+005    6.383E+005    1 .252E+005

77. 11 17. 1 0 l.414E+005 -4.580E+003 6.886E+004 87.35 3.97 5.472E+005 5.712E+005 2 .656E+005 89.78 1. 46 1.463E+006 9.906E+00 5 7.099E+005 Bi -2 14 60 9. 32 45.49 5.436E+004 5.44E+004 8.750E+00 4 2 .577E+004 768.36 4.89 3.882E+005 4. 3 79E+005 1 .795E+005 8 0 6.18 1. 2 6 1. 25 9E+006 -6.191E+005 5.715E+005 934. 0 6 3.1 1 5.021E+005 l.524E+005 2 . 25 8E+005 1120.29 14 . 92 1 . 484E+005 6.762E+004 6.843E+004 1155. 21 1. 63 9.459E+005 - 1.064E+006 4.197E+005 1 23 8.12 5.83 3.662E+005 -1.482E+005 1.677E+005 1280.98 1. 43 1.180E+006 -1.640E+005 5. 2 60E+005 1377.67 3.99 4.891E+005 3 .941E+005 2 . 2 07E+005 1385. 3 1 0.79 1.842E+006 -4.133E+005 8.009E+005 1401.52 1. 33 1. 2 55E+006 4.789E+005 5.551E+005 1407.99 2 .39 6.989E+005 2 .014E+005 3.092E+005 1509.21 2 .13 6. 3 14E+005 1.044E+005 2 .686E+005 1661.27 1. 05 1.059E+006 4.504E+005 4.278E+005

[117]

1clide MDA Report 5/3/2016 6: 53 :0 2 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi -2 1 4 1729.59 2 .88 4.875E+005 5 .44E+004 2 .799E+005 2 .059E+005 1764.49 15.30 1 .632E+005 1.918E+005 7.438E+004 1847.43 2 .03 6.538E+005 - 2 .988E+005 2 .712E+005

 >                2 118.51      1. 16 O.OOOE+OOO                      O.OOOE+OOO     O.OOOE+OOO

+ Pb-214 2 41.99* 7.25 1.777E+005 3 . 3 1E+004 1 .791E+005 8.333E+004 2 95. 22 18.4 2 9.556E+004 3.366E+004 4.536E+004 351.93* 35.60 3.312E+004 4.139E+004 1. 519E+004 785.96 1. 06 1 .544E+006 8.740E+005 7.036E+005 Pb214-XR 74.82 5.80 4.547E+005 2 .49E+005 1.131E+006 2 . 2 18E+005 77.11 9.70 2 .494E+005 -8.073E+003 1. 2 14E+005 87.35 2 .24 9.698E+005 l.012E+006 4.707E+005 89.78 0.82 2 .605E+006 1.764E+006 1. 2 64E+006 Ra-226 186.21 3.64 4. 62 1E+005 4.62E+005 - 2.524E+004 2 .213E+005 Ac- 22 8 129.07 2.42 7.300E+005 8.41E+004 7.312E+004 3 .516E+005 209.25 3. 89 4.192E+005 2 .959E+005 2 .000E+005 270.24 3. 46 4.586E+005 5.450E+004 2 .170E+005 328.00 2.95 5.185E+005 3.415E+004 2 .433E+005 338.32 11.27 1.435E+005 4.588E+004 6.750E+004 409.46 1. 92 7.963E+005 -3.239E+005 3.708E+005 463.00 4.40 3.988E+005 3. 1 94E+005 1.867E+005 794.95 4.25 3.562E+005 -1.4 50E+005 1.610E+005 911. 20 25.80 8.409E+004 5.130E+004 3.904E+004 964.77 4.99 3.839E+00 5 3.988E+005 1.760E+005 968.97 1 5.80 1.159E+005 1. 2 1 3E+005 5. 2 91E+004 1588. 2 0 3.22 4.923E+005 1 .793E+005 2 .14 0E+005 Pa- 23 1 27.36 10.30 7.331E+004 7.33E+004 5.811E+004 3.357E+004 283.69 1. 70 9.302E+005 3.036E+005 4.394E+005 300.07 2 .47 6.710E+005 -9.339E+005 3.173E+005 302.65 2 . 2 0 7. 2 10E+005 -3.129E+005 3.400E+005 330.06 1. 40 1.063E+006 5.917E+005 4.978E+005 Th-234 92.38 2 .13 9.496E+005 9.50E+005 - 5.964E+005 4.598E+005 92.80 2 .10 9.763E+005 - 4.611E+005 4.730E+005 112.81 0.21 9.005E+006 -3.971E+006 4.350E+006 U- 235 143.76 10.96 1.645E+005 2 .93E+0 0 4 6.716E+004 7.926E+004 163.33 5.08 3.499E+005 -1.350E+005 1.683E+005 185.71 57. 2 0 2.929E+004 -5.067E+003 1.402E+004 2 02.11 1. 08 1.607E+006 -7.958E+005 7.691E+005 2 05.31 5.01 3.460E+005 1.676E+005 1.656E+005 Am-241 59.54 35 .90 4.308E+004 4.31E+004 4.159E+00 3 2 .066E+004

    +  = Nuclide identified during the nuclide identification
    *  = Energy line found in the spectrum
    >  = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @  = Half-life too short to be abl e to perform the decay correction

[118]

"***        G A MMA      S P E C T R U M          A N A L Y S I S               *****
"********************~**************************************************

.lename: 5452 iport Generated On 4/18 /2 01 6 2 :50:44 PM tmple Title B306100AFRWC006GD tmple Description TB 560 tmple Identification tmple Type tmple Geometry iak Locate Threshold 3 .00 iak Locate Range (in channel s ) 85 - 81 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10.000 keV tmple Si ze 1.000E+OOO SQM tmpl e Taken On

quisition Started 4/ 1 8/2016 2 :40:4 3 PM

.ve Time 600.0 seconds ial Time 600.5 seconds iad Time 0.07 % Energy Calibration Used Done On 1 /13/2015 Efficiency CalibLa t ion Used Done On 4/14/2016 Efficiency ID TBWALL L)c1.\o. \\~\, c\0-\eJ k, G'~ 7

                                                                     /J ..5-IS
                                                                      ~"

[119]

iak Analysis Report 4/18/ 2 01 6 2 : 50: 4 4 Pl\ Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 545 2 Sample

Title:

B306100AFRWC006GD Peak Analysis Performed on: 4/18/2016 2:5 0 :44 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV ) Area Uncert. Counts 1 945 - 959 954.9 7 238.60 0.76 4.17E+001 28.75 5.63E+001 2 1401- 1414 1407.0 2 351. 73 0.85 4.75E+001 2 1. 2 0 2 .35E+001 3 1584 - 1593 1588.35 397.10 0.76 8.03E-001 13.07 1.82E+001 4 2430 - 2441 2 435. 2 1 608.98 0.96 4.56E+001 18.09 1.44E+001 5 5831 - 5851 5840.09 1460. 2 9 1. 64 1.50E+00 2 2 7.37 1 .llE+OO l First peak in a multiplet region Other peak in a multiplet region

= Fitted singlet

rors quoted at 2 .000 sigma

[120]

1terf erence Corrected Act. ~ ty Report 4/ 1 8/ 2 016 50: 4 4 PM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFRWC006GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activit y Name Confidence (keV) ( %) (pCi/SQM ) Uncertainty K-40 1. 000 1460.8 2

• 10.66 1 .02 1 84E+006 2 .06614E+005 Sn-11 3 0. 900 2 55.1 3 2 .11 391.7 0
• 64.97 4. 72 794E+002 7.69958E+003 Pb-212 0.87 2 115.18 0.60 23 8.63* 43.60 2 .83124E+004 2 .00315E+004 300.09 3.3 0 Pb-214 0. 4 92 2 41. 99* 7. 2 5 1 .7024~E+005 1. 2 0388E+005 2 95. 22 18.42 351.93* 35.60 4.795 03E+ 00 4 2 . 2 7426E+004 785.96 1. 06

      * = Energy line found in the spectrum.
      @=Energy line not used for Weighted Mean Activit?

Energy Tolerance : 1 0.000 keV Nuclide confidence index threshold = 0.3 0 Errors quoted at 2 .000 sigma [121]

tterference Corrected Act: ty Report 4/18/ 2 01 6 >0: 4 4 PM Page 4 "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nucl ide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 1 .0 2 1842E+006 2 . 0 66142E+005 Sn-11 3 0.900 4.7 2 7943E+002 7.699580E+003 X Bi- 2 1 1 0.999 Pb- 212 0.872 2 .033793E+004 2 .037507E+004 Pb- 2 14 0. 492 4.795032E+004 2 . 2 74184E+004

     ? = Nuclide is part of an undetermined solution V

L\. Nuclide rejected b y the interference analysi s

     @      Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at        2 . 000 sigma
 **********       U N I D E N T I F I E D           P E A K S         **********

Peak Locate PPrfnrmerl on: 4/18/ 2 01 6 2 :50:44 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV) Counts per Second 9-; Uncertainty Type Nuclide 4 608.98 7.5944E-00 2 39.7 0 Tol. Zr-97 Sb-125 Sb-125 Cs - 134 Bi -2 14 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [122]

1clide MDA Report 4/18 /2 01l 2 :50:44 PM Page 5

• • • • N U C L I D E M DA R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B306100AFRWC006GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Acti1.7ity Dec. Level Name ( keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) (pCi/SQM)

+      K-40       1460.82*     10.66 l.556E+005       1.56E+005 1.022E+006        6.857E+004 Cr-51         320.08      9.91 1.402E+005      1.40E+005 1.848E+004        6.541E+004 Mn-54         834.85    99.98 1.617E+004       1.62E+004 8. 3 00E+003      7. 3 43E+00 3 Co-58        810.76     99.45 1.337E+004       1.34E+004 -4.954E+00 2      5.947E+00 3 Co-60      11 73. 2 3   99.85 1.383E+004       1.15E+004 -2 . 2 10E+003    6.0 3 6E+00 3 1332.49      99.98 1.149E+004                   -3 . 2 74E+003  4.811E+00 3 Nb-94        702.65     99.81 1.576E+004       1. 23E+004    4. 3 49E+003  7.194E+003 871. 09    99.89 1. 2 27E+004                 - 7.479E+003    5.379E+003

+ Sn-11 3 255.13 2 .11 6. 2 74E+005 1.41E+004 - 7.358E+005 2 .941E+005 391.70* 64. 97 1.414E+004 4.728E+002 6.273E+003 Cs-134 475.36 1. 48 1.073E+006 1.57E+004 1 .813E+005 4.980E+005 563.25 8.34 l.911E+005 9.444E+004 8.813E+004 569.33 15.37 9.690E+004 -4.969E+004 4.442E+004 604.72 97. 62 2 . 27 8E+004 -1.114E+004 1.074E+004 795.86 85.46 1.573E+004 -1.572E+002 7.015E+003 801. 95 8.69 1.523E+005 -8. 22 4E+004 6.773E+004 1038.61 0.99 1.315E+006 6.555E+004 5.741E+005 1167.97 1. 79 7.697E+005 -3.4 3 0E+005 3.360E+005 1365.19 3.02 5.071E+005 - 3.0 5 6E+005 2 . 22 2E+005 Cs-137 661.66 85.10 2 .065E+004 2 .07E+004 1. 2 47E+004 9.542E+00 3 Eu-1 52 1 2 1.78 2 8.67 6. 2 03E+004 5 .22E+004 3. 2 85E+004 2 .989E+004 2 44.70 7.6 1 2 .121E+005 -6.661E+004 1. 0 07E+005 2 95.94 0.45 3 .871E+006 2 .974E+006 1.836E+006 3 44. 2 8 2 6.60 5.222E+004 -2 .432E+004 2.430E+004 3 67.79 0.86 1.812E+006 7.514E+005 8.485E+005 411.1 2 2.24 6.745E+005 - 1.451E+002 3.137E+005 443.96 2.83 4.997E+005 3 .116E+005 2 .305E+005 488.68 0.42 3 .633E+006 1.990E+006 1 .680E+006 563.99 0.49 3 .247E+006 2 .111E+006 1.498E+006 586. 2 6 0.46 3 .948E+006 3 .194E+006 1.837E+00 6 678. 62 0.47 3 .157E+006 -1.173E+006 1.435E+00 6 688.67 0.86 1.770E+006 -5 . 55 6E+005 8.056E+005 7 1 9.35 0.28 5.630E+006 -2 .743E+006 2 . 5 66E+006 778.90 12.96 1. 2 08E+005 4.081E+004 5 .487E+004 810.45 0.32 4. 2 24E+006 1.020E+006 l.883E+006 867.37 4.26 3.017E+005 -5 .905E+004 1. 33 1E+005 919.33 0.43 3.020E+006 1.757E+005 l. 32 8E+006 964.08 14.65 1.432E+005 5.330E+004 6 .617E+004 1085.87 10. 2 4 1.638E+005 9.141E+00 3 7. 3 66E+004 1 089.74 1. 73 8.496E+00 5 -5.908E+005 3 .759E+005 1112.07 1 3 .69 1 .357E+00 5 1. 22 6E+004 6 .162E+004 1212.95 1. 43 1. 22 0E+00 6 -2 .308E+004 5 .476E+00 5 [123]

1clide MDA Report 4/18/201L 2 :50:44 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM) Eu-152 1249.94 0. 1 9 9.013E+006 5 . 2 2E+004 4.757E+006 4.028E+006 1299.14 1. 63 9.170E+005 2.464E+003 4.018E+005 1408.01 2 1. 07 7.941E+004 6.754E+004 3.514E+004 1457.64 0.50 9.121E+006 2 .439E+007 4.365E+006 1528. 1 0 0. 2 8 3 .978E+006 1.854E+006 1.631E+006 Eu-154 123. 07 40.40 4.292E+004 3.90E+004 1.932E+004 2.066E+004 247.93 6.89 2 .082E+005 - 7.224E+004 9.819E+004 59 1. 76 4.95 3 . 3 61E+005 1.287E+005 1.553E+005 692.42 1. 78 8.686E+005 6.382E+004 3.959E+005 7 23 .30 2 0.06 8.606E+004 - 5.286E+004 3.956E+004 756.80 4.52 3.419E+005 8.097E+003 1.552E+005 873. 1 8 12.08 1.161E+005 2 .992E+004 5. 1 79E+004 996.29 10.48 1 .4 2 9E+005 3 .098E+004 6.373E+004 1 004.76 18.01 7.115E+004 5.340E+004 3.106E+004 1274.43 34.80 3.898E+004 4.845E+002 l.687E+004 1 596.48 1. 80 5.597E+005 - 1. 494E+005 2 .221E+005 Eu- 1 55 45.30 1. 31 9.038E+005 7.41E+004 7.767E+005 4.276E+005 6 0 .0 1 1. 22 1.341E+006 -3 .052E+005 6.447E+005 86.55 30.70 7.410E+004 4.022E+004 3.601E+004 10 5.3 1 2 1. 10 8.474E+004 8.534E+001 4.086E+004 Tl-2 0 8 583.19 85 . 00 2 . 1 15E+004 2 .11E+004 1 . 603E+003 9.836E+003 Bi- 2 11 351. 07* 13.02 8. 0 64E+004 8.06E+004 1 .311E+005 3.658E+0 04 Pb-211 40 4.85 3.78 4.052E+005 4.05E+005 3.450E+005 1.888E+005 427.09 1. 76 8. 3 92E+005 -1.603E+005 3.891E+005 832.01 3.52 4.392E+005 7.401E+003 1.985E+005 Bi-212 39. 86 1. 06 8.916E+005 2.65E+005 1.880E+005 4.158E+005 727.33 6.67 2 .648E+005 l.874E+005 1. 22 0E+005 785.37 1.10 l.303E+006 1.041E+006 5.859E+005 1620.5 0 1. 47 7.909E+005 7.900E+004 3.242E+005

+     Pb-2 1 2     115.18       0.60   3.095E+006     3.05E+004      9.978E+005    1.494E+006 238.63*    43.60    3.049E+004                    2.831E+004    1.433E+004 300.09       3.30   4.834E+005                  -4.858E+005     2 . 2 81E+005 Pb2 12-XR      74.8 2   10. 2 8  2 .382E+005    l.38E+ 00 5    4.447E+005    1 . 160E+005 77.11    17.10    1.375E+005                    8.827E+004    6.691E+004 87.35      3 . 97 5.702E+005                    1 .603E+005   2 .771E+005 89.78      1. 46  1.465E+006                    2 . 25 0E+005 7. 1 09E+005 Bi -2 14     609.3 2    45.49    4.830E+004     4.83E+004      4 .314E+004   2 . 2 74E+004 768.36       4.89   3.350E+005                    9.468E+004    l.5 2 9E+005 806.18       1. 26  l . 1 50E+006                 9.155E+00 5   5 . 170E+005 934.06       3.1 1  5.498E+005                    2.860E+005    2 .496E+005 1120. 2 9    1 4.92   1.333E+005                    4.737E+004    6.089E+004 1155.21        1. 63  1.058E+006                    3 .620E+005   4.759E+005 1238.12        5.83   3.446E+005                    2.479E+005    1.569E+005 1280.98        1. 43  1.005E+006                    4.147E+005    4 . 387E+005 1377.67        3.99   4. 2 33E+005                  7.089E+004    1.878E+005 1385.3 1       0.79   1.732E+006                  - 9.214E+005    7.456E+005 1401.52        1. 33  1 . 137E+006                  2 . 23 4E+005 4.965E+005 1407.99        2.39   6.989E+005                    5.944E+005    3.092E+005 1 509.21       2 .13  5.523E+005                    2 .785E+005   2.291E+005 1661.27        1. 05  1.127E+006                    5.094E+004    4.621E+005

[124]

1clide MDA Report 4/18/20ll 2 :50:44 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi- 2 1 4 1 729.59 2 .88 3.947E+005 4.83E+004 1.679E+005 1.595E+005 1764.49 15.30 1.136E+005 5. 1 96E+004 4.959E+004 1847.43 2 .0 3 5.812E+005 2 .473E+005 2 .348E+005

 >                 2 118.5 1      1.16    O.OOOE+OOO                  O.OOOE+OOO O.OOOE+OOO

+ Pb- 2 14 2 41.99* 7.25 1 .834E+005 2 .95E+004 l.702E+005 8.616E+004 2 95. 22 18.4 2 9. 2 46E+004 1.949E+004 4.381E+004 3 51.93* 35.60 2 .949E+004 4.795E+004 1.338E+004 785.96 1. 06 1. 3 09E+006 4.360E+005 5.863E+005 Pb2 1 4-XR 74.82 5.80 4.222E+005 2 .42E+005 7.882E+005 2 .056E+005 77.11 9.70 2 .425E+005 1.556E+005 1 .179E+005 87.35 2.24 1.011E+006 2 .841E+005 4.911E+005 89.78 0 .8 2 2 .609E+006 4.006E+005 1. 2 66E+006 Ra- 226 186. 2 1 3.64 4.478E+005 4.48E+005 1. 4 71E+005 2.142E+005 Ac- 22 8 1 2 9.07 2 .42 6.991E+005 8.13E+004 2.400E+005 3.362E+005 2 09. 2 5 3 .89 3.965E+005 2 .438E+005 1.886E+005 2 70. 2 4 3 .46 4.502E+005 -3.550E+005 2 .128E+00 5 328. 00 2 .95 4.932E+005 3.746E+005 2.307E+005 338.32 11. 27 1.427E+005 5.900E+004 6.711E+004 409.46 1. 92 7.404E+005 -8.949E+005 3.428E+005 463. 00 4.40 3.375E+005 -6.939E+004 1.561E+005 794.95 4.25 3.100E+005 -2.546E+005 1.379E+005 91 1. 20 25.80 8.130E+004 6.334E+004 3.764E+004 964.77 4.99 4. 2 45E+005 1 .386E+005 1.963E+005 968.97 15.80 1. 2 94E+005 5.771E+004 5.963E+004 1588.20 3. 22 4.308E+005 -7.719E+004 1.833E+005 Pa -23 1 27.36 10.30 6.334E+004 6.33E+004 1.676E+004 2 .858E+004 283.69 1. 70 8.060E+005 2.913E+005 3.773E+005 3 00 . 0 7 2 .47 6.459E+005 -6.490E+005 3.047E+005 302.65 2 . 20 6.911E+005 9.472E+004 3.250E+005 330.06 1. 40 1.043E+006 -3.557E+005 4 .876E+005 Th-234 92.38 2. 1 3 9.807E+005 9.81E+005 -7.644E+004 4.754E+005 92.80 2 .10 1.000E+006 4.544E+005 4.850E+005 112.8 1 0. 2 1 8.764E+006 6.833E+006 4. 2 30E+006 U-235 1 43.76 1 0.96 1 .548E+005 2.92E+004 5.645E+004 7.436E+004 163.33 5.08 3 .132E+005 -1.028E+005 1 .499E+005 185.71 57.20 2 . 92 0E+004 3.288E+004 1 .398E+004 202. 1 1 1. 08 1.389E+006 - 8.197E+004 6.602E+005 2 05.3 1 5.0 1 2 .912E+005 -1.935E+005 1.382E+005 Am-24 1 59.54 35.90 4.548E+004 4.55E+004 -1.158E+004 2 .186E+004

    + = Nuclide identified during the nuclide identification

• Energy line found in the spectrum

    >     Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @     Half-li fe too short to be able to perform the decay correction

[125]

*************************~ **************************                 ****************
****        G A MMA      S .I:' E C T R U M         A N A L Y S I S                *****

.lename: C:\GENIE2K\CAMFILES\00001336.CNF iport Generated On 4/14/2016 4:01:07 PM 1mple Title B306100AFRWC07GD 1mple Description U-1 STS TB PEDESTAL WALL 1mple Identification 1mpl e Type 1mpl e Geometry iak Locate Threshold 3. 00 iak Locate Range (in channels) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 1. 000 FWHM 1mple Size l.OOOE+OOO SQM 1mple Taken On

quisition Started 4/14/ 2 016 1: 4 8: 4 9 PM

.ve Time 600.0 seconds ial Time 600.4 seconds iad Time 0. 07 5ci Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBWALL l)~dt 'to.\,~ce\ed ky

                                                                     ~

IJ.-6'-J'l

                                                                        ~ /,Id

[126]

iak Analysis Report 4/14 /2 016 4: 01: 07 PI Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B306100AFRWC07GD Peak Analysis Performed on: 4/14 /2 01 6 4:01:06 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV) Area Uncert. Counts 1 296- 308 3 00 .79 74.85 0.33 4.73E+001 46.88 1 .90E+00 2 2 5825- 5850 5838. 2 7 1459.84 1. 54 1.58E+00 2 31. 05 1.94E+001 = First peak in a multiplet region = Other peak in a multiplet region = Fitted sing l et ~rors quoted at 2 .000 sigma [127]

1terference Corrected Act: ty Report 4/14 /2 01 6 ) 1:07 PM Page 3 "*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample Ti t le: B306100AFRWC07GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K- 40 0. 950 1460.82* 10.66 1.07 3 97E+006 2 .31293E+005

       * = Energy line found in the spectrum.
       @=Energy line not used for Weighted Mean Activity Energy Tolerance :      1.000 FWHM Nuclide confidence index threshold          0.30 Errors quoted at 2.000 sigma

[128]

1terference Corrected Act: ty Report 4/ 1 4/ 2 016 )1:07 PM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0.950 1.073970E+006 2.312934E+005

     ? = Nuclide is part of an undetermined solution X  = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Error s quoted at       2 .000 s i gma
 **********        U N I D E N T I F I E D         P E A K       s  **** ,: ** ***

Peak Locate Performed on: 4/14/2016 4:01:06 PM Peak Locat e From Channel: 85 Pea k Locate To Channel: 8192 Peak En ergy Peak Si ze in Peak CPS Peak Tol. No . ( keV) Counts per Second  % Uncertainty Type Nuclide 1 74.8 5 7 .887 1E-00 2 99. 0 7 Tol. Pb212-XR Pb214-XR M = First peak in a multiplet region m Other peak in a multiplet region F Fitted singlet Errors quot ed at 2 . 000 s igma [129]

1cl ide MDA Report 4/14/ 2 01 4:01:07 PM Page 5

• • • • N U C L I D E M D A R E P O R T *****

Detector Name: 545 2 Sample Geometry: Sample

Title:

B306100AFRWC07GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) K-40 1460.8 2

• 10 .66 2. 2 34E+005 2 . 2 3E+005 1.074E+00 6 1.025E+005

+                                                                                     6.184E+004 Cr-5 1       32 0.08       9.91   l.330E+005      l. 3 3E+005 - l.280E+005 Mn-54        83 4.85     99.98    l.375E+004      l .3 7E+004 9.914E+00 3      6.130E+00 3 Co- 5 8      810.76      99.45    l.130E+004      1 . 13E+004 -8.048E+00 3     4.910E+00 3 Co-60      1173. 23      99.85    l.744E+004      l . 15E+004 1. 2 91E+004     7.841E+00 3 1332.49       99.98    l. 1 49E+004                   6. 2 04E+003  4.811E+00 3 Nb-94        70 2 .65    99.81    l.455E+004      l .35E+004 l.0 1 3E+003      6.585E+00 3 871. 09     99.89    l.347E+004                     2 .403E+003   5.978E+00 3 Sn-1 1 3     255.13        2 .11  7.468E+005      2 .06E+004 -1.919E+005       3.538E+005 39 1 .70    64 . 97  2 .064E+004                  -8.483E+003     9.5 2 7E+003 Cs-13 4      475.36        1. 48  9.812E+005      1.93E+004 -4.111E+005        4.522E+005 563.25        8.3 4  l. 609E+005                  -l.251E+005     7.308E+004 569.33      15.37    9.015E+004                     4.324E+004    4.104E+004 604.72      97. 62   l.932E+004                     4.090E+003    9.004E+003 795.86      85.46    l.974E+004                     2 .042E+004   9.017E+003 801. 95       8.69   l.696E+005                     6.822E+004    7.641E+004 10 3 8.61       0 .99  l .385E+006                    4.370E+005    6.089E+005 1 167.97        1. 79  9.706E+005                     3 .079E+005   4. 3 65E+005 1365.19         3 .0 2 3 . 2 67E+005                  l.390E+005    l. 32 0E+005 Cs- 1 37     661.66      85. 1 0  l . 3 33E+004   l.33E+004 -3. 54 1E+003      5.882E+003 Eu-152       121.78      28.67    6. 2 40E+004    4.98E+004 -5.553E+003        3.008E+004 244.70        7.61   2 .121E+005                    l.578E+00 3   l.007E+005 295.94        0 .45  3 .465E+006                  -9.608E+005     l.633E+006 344. 2 8    2 6.60   4.977E+004                   -7. 2 03E+004   2 .307E+004 367.79        0 .86  1 .641E+006                    l. 33 4E+006  7.628E+005 41 1. 12      2.24   6 .141E+005                  - 4.0 6 0E+005  2.835E+005 443.96        2.83   4.900E+005                     9 .1 7 1E+004 2.256E+005 488.68        0.42   2 .935E+006                  - 3 . 3 73E+005 1.330E+006 563.99        0.49   2 .735E+006                  -7 . 3 91E+005  l . 2 42E+006 586. 26       0 . 46 3.794E+006                   -1. 2 1 0E+005  1 .760E+006 678. 62       0.47   2 .937E+006                    7.115E+004    l.326E+006 688. 67       0.86   1.493E+006                   - 8.122E+005    6 .671E+005 719.35        0. 2 8 4.688E+006                     2 .758E+005   2 .095E+006 778.90      12.96    l.157E+005                     2 .771E+004   5. 23 1E+004 810.45        0. 32  3 .789E+006                  -l.172E+004     l.666E+006 867.37        4.26   3 . 2 83E+005                -1. 732E+005    l.464E+005 919.33        0.43   2 .946E+006                  - 1.009E+006    1. 2 91E+006 96 4 . 0 8  14.65    l. 2 78E+005                 -2 .542E+004    5.844E+004 1085.87       10.24    l.105E+005                   -9. 099E+004    4.702E+004 1089.74         1. 73  6.553E+005                   -4 . 927E+004   2 .788E+005 11 1 2 .07    13.69    l.131E+005                   -l.823E+004     5.031E+004 12 1 2 .95      1. 43  l.132E+00 6                  -2 .948E+005    5.037E+005

[130]

1clide MDA Report 4/14/ 2 01 4:01:07 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) {pCi/SQM ) (pCi/SQM ) Eu-15 2 1249.94 0.1 9 9.812E+006 4.98E+004 1.025E+007 4.428E+006 1 2 99.14 1. 63 8.682E+005 -1.920E+005 3.774E+005 1408.01 2 1 .07 7.392E+004 3.308E+004 3.239E+004 1457.64 0.50 9.623E+006 2 .446E+007 4.616E+006 1 528.10 0. 2 8 3.978E+006 1.854E+006 l .631E+006 Eu-154 123.07 40.40 4.373E+004 4 .3 7E+004 5 . 2 59E+00 3 2 .107E+004 2 47.93 6.89 2 .185E+005 -1.049E+005 1.033E+005 591.76 4.95 2 .779E+005 3.862E+003 1. 262E+005 692.42 1. 78 7.875E+005 5. 0 35E+005 3.554E+005 723.30 2 0.06 6.537E+004 - 1 . 1 56E+004 2 . 922 E+004 756.80 4.52 3.174E+005 9.750E+003 1 .430E+005 873.18 12.08 1.067E+005 -1.420E+005 4.707E+004 996. 2 9 10.48 1.250E+005 -1. 32 1E+005 5.479E+004 1004.76 18.01 8.973E+004 4.756E+004 4.035E+004 1274.43 34.80 4.848E+004 3. 107E+004 2. 162E+004 1 596.48 1. 80 4.596E+005 - 2 .348E+00 5 1.720E+005 Eu-155 45.30 1. 31 8.956E+005 6.97E+004 9.506E+005 4. 2 35E+005 60.0 1 1. 22 1.345E+006 4.582E+005 6.462E+005 86.55 3 0.70 6.974E+004 8.919E+004 3 . 3 83E+004 105.31 2 1.10 8.752E+004 5.847E+004 4. 22 5E+004 Tl-2 0 8 583.19 85.00 2 .082E+004 2.08E+004 2 .313E+004 9.670E+003 Bi-2 11 351.07 13.02 1.384E+005 l.38E+005 1.486E+005 6.546E+004 Pb-2 11 404.85 3.78 3.772E+005 3.77E+005 -1.898E.+005 1 .7 48E+005 427.09 1. 76 8.805E+005 2.763E+005 4. 0 98E+005 832.01 3.52 4.118E+005 5 .873E+004 1.848E+005 Bi-21 2 39.86 1. 06 1.011E+006 2 . 2 1E+005 4.357E+005 4.755E+005 727.33 6.67 2. 2 12E+005 6.570E+004 l.001E+005 785.37 1.10 1.346E+006 - 2 .047E+004 6.072E+005 1620.50 1. 4 7 6.905E+005 -5.425E+005 2 .740E+005 Pb-212 115.18 0.60 3.038E+006 4.40E+004 7.272E+005 1.465E+006 23 8.63 43.60 4 .3 95E+004 3.788E+004 2 .106E+004 300.09 3.30 4.432E+005 1. 2 86E+005 2 .080E+005 Pb212-XR 74.82 10. 2 8 2 . 23 6E+005 l. 2 4E+005 4.196E+005 1.087E+005 77.1 1 17. 1 0 1.242E+005 -2 .622E+004 6.023E+004 87.35 3.97 5.386E+005 3 .483E+005 2 .613E+005 89.78 1. 46 1.390E+006 7.544E+004 6.733E+005 Bi -2 1 4 609. 32 45.49 4.310E+004 4.3 1E+004 4.563E+004 2 .014E+004 768.36 4.89 3.350E+005 3.3 00E+004 1.529E+005 806.18 1. 2 6 9.599E+005 2 . 72 6E+005 4. 22 1E+005 934. 0 6 3.11 4.392E+005 -1.410E+005 l.943E+005 1 120.29 14.92 1 . 1 79E+005 3.964E+004 5.319E+004 1155.21 1. 63 1.058E+006 - 2 .340E+005 4.759E+005 1 238.12 5.83 3.401E+005 1.617E+005 1.546E+005 1 280.98 1. 43 1.133E+006 -1.179E+004 5.026E+005 1 377.67 3.99 4.408E+005 2 .758E+005 1.966E+005 1 385.3 1 0.79 1.788E+006 -4.651E+005 7.737E+005 1 401.5 2 1. 33 1 .039E+006 6.936E+005 4.4 7 6E+005 1407.99 2.39 6.506E+005 2 .911E+005 2.851E+005 1509.21 2.13 5.523E+005 -2 . 3 93E+004 2 . 2 91E+005 1661.27 1. 05 8.081E+005 -2 . 62 8E+005 3.0 2 5E+005 [131]

iclide MDA Report 4/14/201 4:01:07 PM Page 7 Nuclide Energy Yi eld Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) (pCi/SQM) Bi-214 1729.59 2 .88 3.013E+005 4.31E+004 - 3.265E+005 l. 1 2 8E+005 1764.49 15.30 1.590E+00 5 1.355E+005 7. 22 9E+004 1847.43 2 .03 4.950E+005 1.648E+005 l.917E+005 2118.51 1.16 O.OOOE+OOO O.OOOE+OOO O.OOOE+OOO Pb-2 14 241.99 7. 2 5 2 .537E+005 5.04E+004 9.848E+004 l.213E+005 2 95. 22 18.42 8.675E+004 1.833E+004 4.096E+004 351.93 35.60 5.044E+004 5 .208E+004 2 .386E+004 785.96 1. 06 1.463E+006 1 . 3 35E+005 6.633E+005 Pb2 1 4-XR 74.82 5.80 3.964E+005 2 .19E+0 0 5 7.437E+005 1. 927E+005 77.11 9.70 2 .189E+005 -4. 62 1E+004 1.062E+005 87.35 2.24 9.545E+005 6.172E+005 4.631E+005 89.78 0.82 2 .475E+006 1 .343E+005 l .199E+006 Ra-226 186.21 3.64 4.304E+005 4.30E+005 -3.134E+004 2.054E+005 Ac- 22 8 129.07 2.42 6.783E+005 7.14E+004 -1.485E+005 3. 2 57E+005 209. 2 5 3.89 4.137E+005 - 2 .168E+004 l .972E+005 27 0. 2 4 3 . 46 4.439E+005 2.419E+004 2.096E+005 32 8.00 2.95 4.489E+005 5.113E+004 2 .085E+005 338.32 11. 27 1 .311E+005 3.424E+004 6.133E+004 409.46 1. 92 7.404E+005 1.888E+005 3 .428E+005 463.00 4.40 3.313E+005 2 .348E+003 1 .530E+005 794.95 4 . 25 3.870E+005 1.574E+005 1.764E+005 911. 2 0 25.80 7. 1 42E+004 2 . 0 57E+004 3.270E+004 964.77 4.99 3.924E+005 1.900E+005 1.802E+005 968.97 15.80 1.255E+005 3.250E+004 5.769E+004 1588. 2 0 3. 22 3.114E+005 1.188E+005 l. 23 6E+005 Pa-2 31 27.36 10. 3 0 7.497E+004 7.50E+004 2 .257E+004 3.440E+004 283.69 1. 70 7.904E+005 - 7.363E+005 3.695E+005 300.07 2 .47 5.922E+005 1.718E+005 2 .779E+005 302.65 2 . 20 5 .872E+005 8.562E+004 2 .731E+005 330. 0 6 1. 40 9.099E+005 - 3.141E+005 4. 2 13E+005 Th-23 4 92.38 2.13 9.129E+005 9.13E+005 -5.630E+005 4.415E+005 92.8 0 2 . 10 9.246E+005 -2 .597E+005 4.471E+005 112.81 0 .2 1 8. 2 27E+006 -1.680E+006 3.961E+006 U-235 1 43.76 10 .96 1.395E+005 2.76E+004 2 .315E+004 6.676E+004 1 63.33 5. 0 8 3.069E+005 1.721E+005 l .467E+005 185.7 1 57. 2 0 2 .761E+004 - 8.020E+003 1.319E+004 202. 11 1. 08 1.394E+006 -2 .548E+004 6.628E+005 205.3 1 5.0 1 3.172E+005 4. 3 95E+004 1.512E+005 Am- 2 41 59.5 4 35.90 4.527E+004 4 . 53E+004 8.849E+003 2 .175E+004

     +  =  Nuclide identified during the nuclide identification
     *  =  Energy line found in the spectrum
     >  =  Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ =   Half-life too short to be able to perform the decay correction

[132]

****        GAMM A        S P E C T R U M         A N A L Y S I S              *****

.l ename: E:\4 -2 6-17\TB 56 0 SP08.CNF iport Generat ed On 4/27/2 01 7 11:34:35 AM tmpl e Title B306100AFRFC008GD tmpl e Description TURBINE BUILDING tmple Identification SP08 tmple Type tmple Geometry TB FLOOR iak Locate Threshold 3. 00 iak Locate Range (in channels ) 85 - 8 1 92 iak Area Range (in channels) 85 - 8 1 92 lentification Energy Tolerance 10.000 keV tmple Size 1.000E+OOO SQ M tmple Taken On 2/4/2 0 16 8:47:00 AM

quisition Started 2/4/2 01 6 8:47:19 AM

.ve Time 600.0 seconds ial Time 600. 3 s e conds iad Time 0 .05 % Energy Calibration Used Done On 1/27/2015 Efficiency Calibration Used Done On 4/24/2017 Efficiency ID TBFLOOR

1) o.\ ~ 1o.\\do.\ed O\f 0~'4- I

                                                              /,2-5-J'o
                                                               ~ (p/O

[133]

iak Analysis Report 4 /2 7/ 2 017 11:34:35 A Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5456 Sample

Title:

B306100AFRFC008GD Peak Analysis Performed on: 4/ 27/2 017 11:34: 3 5 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroi d ( keV) (keV ) Area Uncert. Counts 1 5826- 5851 5840.56 1 459 .4 5 1.8 1 1.69E+002 2 8.01 6.50E+OOO

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 .000 sigma

[134]

1terf erence Corrected Act. ... ty Report 4/27/2017 1 34:35 AM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFRFC008GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL . NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQ M) Uncertainty K-40 0.997 1460.82* 10 .66 1 .14839E+006 2 .1538 1E+0 05

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold=             0.30 Errors quoted at 2 .000 sigma

[135]

1terference Corrected Act _ i ty Report 4/ 2 7 /2 017 1 3 4 :35 AM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 0.997 1.148392£+0 0 6 2.153807£+005

     ? = Nuclide i s part of an undetermined solution X = Nuclide rejected by the interference analysi s
     @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2 . 000 s igma
 **********     U N I D E N T I F I E D          P E A K S        **********

Peak Locate Performed on: 4/ 27/2017 11:34:35 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV) Counts per Second  % Uncertainty Type Nuclide Al l peaks were identified. [136]

1clide MDA Report 4/27/ 2 01 1 1:34:35 AM Page 5

• • • • N U C L I D E M D A R E P O R T *****

Detector Name: 5456 Sample Geometry: TB FLOOR Sample

Title:

B306100AFRFC008GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV} ( %} (pCi/SQ M) (pCi/SQ M} (pCi/SQ M} (pCi/SQ M)

+      K-40       1460.82*     10.66     1.364E+005     1.36E+005 1.148E+006          5.895E+004 Cr-51        32 0.08      9.91    1.460E+005     1.46E+005 - 6.017E+004        6.832E+004 Mn-54        834.85     99.98     1.348E+004     1.35E+004 - 2.541E+003        5.995E+00 3 Co-58        810.76     99.45     1.390E+004     1.39E+004 4.876E+003          6. 2 11E+003 Co-60      117 3 . 23   99.85     1.491E+004     1.30E+004 1.135E+003          6.578E+003 1 332 .49    99.98     1. 2 98E+004                - 1. 2 97E+004   5.555E+003 Nb-94        702.65     99.81     1. 4 96E+004   1. 2 9E+004 -5.392E+002       6.794E+003 871. 09    99.89    1.289E+004                     4.907E+003     5.686E+003 Sn-113       255.13       2.11    6.721E+005     2 .06E+004 -4.634E+005        3. 1 64E+005 391. 70    64.97    2 .064E+004                  -8.611E+003      9.527E+003 Cs-134       475.36       1. 48   9.518E+005     1.69E+004 6.112E+005          4.375E+005 563 . 2 5    8 . 34  l . 737E+005                -5 . 069E+004    7.944E+004 569.33     15.37     9.904E+004                    2 .774E+003    4.549E+004 604.72     97. 62   2 .513E+004                    2 .1 1 1E+004 1.191E+004 7 95. 8 6  85.46    1.690E+004                     1 . 3 46E+004 7.601E+00 3 801.95       8.69   1.427E+005                   -1.042E+005      6. 2 94E+004 1038.61        0.99   1.631E+006                     1. 2 86E+006  7. 3 19E+005 1167.97        1. 79  8.104E+005                   -6.008E+005     3.564E+005 1365.19        3.0 2  4.660E+005                     4.054E+004    2.017E+005 Cs-137        661.66     85.10    1.906E+004      l.91E+004 l.305E+004         8.746E+00 3 Eu- 1 52      121.78     2 8.67   6. 3 14E+004    5.07E+004 - 8.558E+003       3.045E+004 244.70       7.61   2 .138E+005                    8.094E+004    1.016E+005 295.94       0.45   3.839E+006                     1.672E+006    1.8 2 0E+006 344. 2 8   2 6.60   5.261E+004                  -1.083E+004      2.450E+004 367.79       0.86   1 .615E+006                 -2 .048E+005     7.497E+005 411.12       2 . 24 6.255E+005                  -4.631E+005      2.892E+005 443.96      2 .83   4.850E+005                  -2 .081E+005     2.232E+005 488.68       0.42   3.358E+006                    2 .840E+006    1 .542E+006 563.99       0.49   3.053E+006                     6 . 1 95E+005 1.401E+006 586.26        0.46   3.978E+006                    1.441E+006     1.852E+006 678.62       0.47   3.199E+006                    1.164E+006     1.456E+006 688.67      0.86    1.815E+006                    6.8 3 4E+005   8.283E+005 719.35       0. 2 8  5.024E+006                  - 1 .167E+006    2 .263E+006 778.90      12.96    1.192E+005                    4.7 2 1E+004   5.403E+004 810.45       0.32    4.305E+006                    6. 1 54E+005   1 .924E+006 867.37       4.26    3.086E+005                  -7 . 3 82E+004   1.365E+005 919.33       0.43    3.020E+006                    1.170E+006     l.328E+006 964.08     14.65     1.307E+005                    9.558E+004     5.992E+004 1085.87      10.24     1.464E+005                    2 .873E+004    6.497E+004 1089.74        1. 73   7.909E+005                  - l.987E+005     3.466E+005 1112.07      13.69     1.197E+005                  - 1.939E+005     5.363E+004 1212.95        1. 43   1 . 1 32E+006                 1.527E+005     5.037E+005

[137]

1clide MDA Report 4 /27/ 201 11:34:35 AM Page 6 Nuclide Energy Yield Line MDA Nuc l ide MDA Activity Dec. Level Name (keV ) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Eu-15 2 1249.94 0.19 7.933E+006 5.07E+004 2 .700E+005 3 .489E+00 6 1299.14 1. 63 6.981E+005 -1. 36 1E+005 2.924E+005 1408.01 21. 07 5.071E+004 -6 . 2 48E+004 2.079E+004 1457.64 0.50 9.375E+006 2 .584E+007 4.492E+006 1528.10 0.28 4.415E+006 -2 .605E+006 l.849E+006 Eu-154 123.07 40.40 4.478E+004 3.65E+004 l.882E+004 2 .159E+004 247.93 6.89 2 .145E+005 -4 .181E+004 l .013E+005 591. 76 4.95 2 .927E+005 4.025E+004 1.336E+005 692.42 1. 78 8.116E+005 1.841E+005 3.674E+005 723.30 2 0.06 7.005E+004 -1.419E+003 3.156E+004 756.80 4.52 2.608E+005 - l.1 2 9E+004 1 . 147E+005 873. 1 8 1 2 .08 1.067E+005 2 .107E+004 4.707E+004 996. 2 9 10.48 1.484E+005 1. 2 85E+004 6 .645E+004 1004.76 18.01 7.306E+004 -7.196E+004 3 . 2 02E+004 1274.43 34.80 3.648E+004 -3 .020E+004 1.562E+004 1596.48 1. 80 6.021E+005 -5.728E+005 2 .433E+00 5 Eu-155 45.3 0 1. 31 8.123E+005 6.68E+004 7.423E+004 3.816E+005 60.01 1. 2 2 1.260E+006 1.031E+005 6 . 038E+005 86.55 3 0 .70 6.683E+004 4.912E+004 3. 23 7E+004 105.31 21.10 8.919E+004 2 . 67 4E+004 4.308E+004

      'l'l-2 0 8   583.19   85.00    2.2 42E+004   2.24E+004    1 .82 0E+004   l ,047E+004 Bi-211       351. 07  13.02    1.621E+005    1.62E+005    1 . 770 E+00 5 7.7 3 0E+004 Pb-211       404.85     3. 7 8 3.868E+005    3.87E+005  -8.703E+004      1 .796E+005 427 .09    1. 76  7.649E+005               -1.691E+005      3 .5 1 9E+005 832 .01    3.52   3.898E+005               -1.131E+005      1.738E+0 0 5 Bi-2 12       39.86     1. 06  9.806E+005    2 .11E+005 -1.084E+005      4.600E+005 727.33     6.67   2 .112E+005                3 .396E+004    9.516E+004 785.37     1.10   1. 303E+006                1 .441E+005    5.859E+005 1 620.50     1. 47  7.428E+005               -4.389E+004      3 .001E+005 Pb-212       11 5.18    0.60   3 .002E+006   4.59E+004    3.638E+005     1. 447E+006 23 8.63  43.60    4.592E+004                 l.167E+004     2 . 2 04E+004 300.09     3.30   4.536E+005               -5.0 3 8E+005    2 .132E+005 Pb212-XR      74.82   10.28    2 .519E+005   l.40E+005    5. 2 01E+005   1 . 2 28E+005 77.11   17.10    1.404E+005                 9.702E+00 4    6.834E+004 87.35     3.97   5.122E+005                 1. 205E+005    2 .480E+005 89.78     1. 4 6 1.365E+006               -9.318E+005      6.604E+005 Bi-2 14      609.3 2  45.49    5.789E+004    5.79E+004    8.308E+004     2 .753E+004 768.36     4.89   3.091E+005               -2 . 2 97E+005   1.399E+005 806.18     1. 2 6 1.006E+006                 1 .924E+005    4.449E+005 934.06     3.11   5.573E+005                 3 .063E+005    2 .534E+00 5 1120. 2 9  14.92    1. 455E+005                1. 27 1E+005   6.699E+004 1155. 2 1    1. 63  9.657E+005               -5.905E+004      4. 2 96E+005 1 23 8.12    5.83   3.446E+005                 3.483E+005     1 .569E+005 1 28 0.98    1. 43  1.005E+006                 4.980E+005     4.387E+005 1377.67      3.99   4.736E+005                 4. 2 58E+004   2 .130E+00 5 1385.31      0.79   1.788E+006                 6.476E+005     7.737E+005 1401.52      1. 33  1.106E+006                 1.868E+005     4.808E+005 1 407.99     2.39   4.463E+005               - 5.499E+005     1.829E+005 1509. 2 1    2. 1 3 5.801E+005                 1. 21 8E+005   2.429E+005 1661. 2 7    1. 0 5 1 .127E+006              -4.504E+005      4.621E+005

[138]

1clide MDA Report 4/27/20~ 11 :34:35 AM Page 7 Nuclide Energy Yield Line MDA Nucl ide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Bi -2 14 1729.59 2.88 5.966E+005 5.79E+004 2 . 2 78E+005 2 .604E+005 1764.49 1 5.30 1.732E+00 5 2 .185E+005 7.938E+004 1847.43 2 . 0 3 5 .812E+005 2 .473E+005 2.348E+005

  >                2118.51        1. 1 6 0.000E+OOO                  O.OOOE+OOO     O.OOOE+OOO Pb-2 1 4       2 41. 99     7.25 2 .596E+005     6.05E+004     8.691E+004     1. 2 43E+005 295. 22    18.42 9.441E+004                     9.020E+004     4.479E+004 351. 93   35.60 6.050E+004                      8.422E+004     2 .888E+004 785.96      1. 06 1.285E+006                  -1.911E+005      5.745E+005 Pb214-XR         7 4 .82   5.80 4.465E+005       2 .48E+005    9.218E+005     2 .177E+005 77.11      9.70 2 .476E+005                   1.710E+005     1.205E+005 87.35     2 . 2 4 9.077E+005                  2 .135E+005    4.395E+005 89.78     0.82 2.430E+006                   -1.659E+006      1.176E+006 Ra-226         186.21      3.64 4 . 122E+005     4.12E+005     3.069E+005     1.963E+005 Ac-228         1 2 9.07    2.42 7.116E+005       6.72E+004     4.048E+004     3 .424E+00 5 2 09. 2 5   3.89 3.906E+00 5                    1.160E+005     1 . 857E+005 270. 2 4    3. 46 4.668E+005                    4.463E+005     2 .211E+005 328.00      2.95 5.060E+005                     2.011E+005     2 .371E+005 338.32    1 1. 27 1.387E+005                  -7.431E+003      6.511E+004 409.46      1. 92 7.595E+005                    3 .773E+005   3.524E+005 463.00      4.40 3.583E+005                     1 .506E+004   1.664E+005 794.95      4.25 3. 2 82E+005                   1 .835E+005   1. 4 70E +005 911.2 0   25.80 6.719E+004                      4 . 979E+004  3.059E+004 964.77      4.99 3.796E+005                     2.067E+005    1 .738E+005 968.97    15 . 80 1.100E+005                    3.433E+004    4.996E+004 1588.20       3. 22 4.308E+005                    O.OOOE+O OO   1.833E+005 Pa-231          2 7.36   10.30 9.399E+004        9.40E+004  -2.375E+004      4.388E+004 283.69       1. 70 8.705E+005                    6.506E+005    4.095E+005 300.07       2 .47 6.061E+005                 -6.731E+005      2 .848E+005 302.65       2 . 2 0 6.756E+005                 1 .159E+005    3 . 1 73E+005 330.06       1. 40 1 .056E+006                -1.802E+00 5     4.945E+005 Th- 23 4         92.38      2 .1 3 9.341E+005    9.34E+005     3.192E+005     4.520E+005 92.80      2 .10 9.505E+005                   4.746E+005     4.600E+005 112.81       0. 2 1 8.141E+006                  2 .972E+006    3 .918E+006 U-235          143.76     1 0 .96 1.656E+005     2 .60E+004    2 .089E+004    7.976E+004 163.33       5.08 3.193E+005                    3.280E+004     1.529E+005 185.71     57.20 2 .601E+004                    8.106E+003     1. 2 39E+004 2 02 .11    1. 08     1.420E+006              - 4.872E+005     6.757E+005 2 05.31     5.01 2.994E+005                   - 8.933E+004     1.423E+005 Am-24 1          59.54    35.90 4. 2 71E+004     4. 2 7E+004   1 .845E+004    2 .046E+004
    + = Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @    Hal f- life too short to be able to perform the decay correction

[139]

****          G A M MA       S P E C T R U M        A N A L Y S I S                  *****
.lename: 5452

!port Generated On 4/18/2016 2 :10:58 PM tmple Title B306100AFRWC009GD tmple Description TB 560 tmple Identification tmple Type tmple Geometry !ak Locate Threshold 3 .00 !ak Locate Range (in channels ) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Size 1.000E+OOO SQM tmple Taken On

qui s ition Started 4/18/2016 2 :00:56 PM

.ve Time 600.0 seconds ial Time 600.5 seconds iad Time 0 . 08 % Energy Calibration Used Done On 1 /13/2015 Efficiency Calibration Used Done On 4/14/2016 Ef f icienc: ID 1 TBWALL 1)<<\~ ~o.\;do...\ t'd 'Dy 0~ I ~-5--lB' 06'/D [140]

iak Analysis Report 4/18/ 2 016 2: 10: 58 P' Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B306l00AFRWC009GD Peak Analysis Performed on: 4/18 /2 016 2:10:57 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 442 - 450 446.08 111. 22 0.61 -3.76E+OOO 24.69 7.18E+001 2 951- 961 955.48 238.72 0. 2 8 l.96E+001 22.35 4.34E+001 3 5829- 5850 5840. 2 9 1460. 3 4 1. 46 1.16E+002 23.29 5.35E+OOO

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2.000 sigma

[141]

1terference Corrected Act_ ty Report 4/18/ 2 016 10 :58 PM Page 3

• • • • • • • • • • • • • • • ~*********************************************************
      • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFRWC009GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQM ) Uncertainty K-40 1. 000 1460.82* 10.66 7.88496E+005 1 .72907E+005 Pb-212 0.894 115.18* 0.60 -1.49195E+005 9.80 92 1E+005 238.63* 43.60 l.33002E+004 1.5 32 15E+004 300.09 3.30

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold =        0. 3 0 Errors quoted at 2 .000 sigma

[142]

1terference Corrected Act~ .ty Report 4/18 /2 01 6 1 0:58 PM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 7.884957E+005 1.729071E+005 Pb-212 0.894 1. 33 0024E+004 1.532148E+004

     ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .000 sigma
 **********    U N I D E N T I F I E D          P E A K S     **********

Peak Locate Performed on: 4/18/2016 2 :10:57 PM Peak Locate From Channel: 85 Peak Locate To rhann~l

• 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second  % Uncertaint 1, Type Nuclide All peaks were identified. [143]

tclide MDA Report 4/ 1 8/20h 2 :10:58 PM Page 5

• • • • N U C L I D E MD A R E P O R T *****

Detector Name: 545 2 Sample Geometry: Sample

Title:

B306100AFRWC009GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (t) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM )

+      K-40       1 460.8 2

• 10.66 1.186E+D05 1.19E+005 7.885E+005 5.007E+004 Cr-51 320.08 9.91 1.469E+005 l.47E+005 6.987E+004 6.879E+004 Mn-54 834.85 99.98 1.572E+004 1.57E+004 1.314E+004 7.117E+003 Co-58 810.76 99.45 1.559E+D04 l.56E+004 1.022E+004 7.059E+003 Co-60 1173.~3 99.85 1.559E+004 1. 2 0E+004 -4.317E+00 3 6.9 1 5E+00 3 1332.49 99.98 1. 2 01E+D04 2 .774E+003 5.071E+003 Nb-94 70 2 .65 99.81 1.32DE+004 1.32E+004 - 4.871E+00 3 5.914E+003 871. 09 99.89 l.375E+D04 -1.183E+004 6.119E+003 Sn-11 3 255.13 2.11 7. 27 2E+005 2 . 2 8E+004 3.911E+004 3.440E+005 391. 70 64.97 2 .284E+004 -1.469E+004 1.063E+004 Cs-13 4 475.36 1. 48 9.617E+005 1.66E+004 -4.059E+005 4.425E+005 563 . 25 8 . 34 1.653E+005 1.722E+004 7.526E+004 569.33 1 5.37 8.777E+D04 -3.382E+004 3 .985E+004 604.72 97.62 2 .054E+D04 l.245E+004 9.616E+003 795.86 85.46 1. 662E+004 - 8.785E+003 7.459E+00 3 801.95 8.69 1.669E+005 1.347E+005 7.503E+004 1038.61 0 .99 1 .9 1 3E+006 l.496E+006 8.730E+00 5 1167.97 1. 79 7.904E+D05 -8.761E+004 3 .463E+005 1 365.19 3.0 2 4. 2 02E+005 8.793E+004 1.787E+005 Cs-137 661.66 85.10 1.821E+004 l.82E+004 l .315E+004 8.319E+003 Eu-1 52 121.78 2 8.67 5.845E+004 5.49E+004 -2 .476E+004 2 .810E+004 2 44.70 7.61 2 .001E+005 8. 1 9 0E+004 9 . 473E+004 2 95.94 0.45 3 .606E+006 1.335E+006 1.703E+006 3 44. 2 8 26.60 5.493E+004 3.737E +00 3 2.566E+004 3 67.79 0.86 1.602E+006 l.386E+006 7.4 3 1E+005 41 1.1 2 2.24 6.198E+005 1 .915E+005 2 .8 6 4E+005 443.96 2.83 4.800E+005 2 .610E+005 2 . 2 07E+005 488.68 0.42 3.173E+006 9.498E+005 1.450E+006 563.99 0.49 2 .809E+D06 - 6.378E+005 1. 2 79E+006 586.26 0.46 4.037E+00 6 4.132E+006 1.882E+006 678.62 0.47 2 .891E+00 6 l.855E+006 1. 3 03E+006 688.67 0.86 1. 54 7E+006 -4.694E+005 6.943E+005 719.35 0.28 5.486E+006 -1.866E+006 2 .494E+006 778.90 1 2 .96 1.085E+005 1.437E+004 4.870E+004 810.45 0.32 4.900E+D06 4.360E+006 2 . 222E+006 867. 3 7 4.26 3 . 3 46E+005 9.637E+004 1 . 496E+005 919. 33 0.43 3 .093E+006 -3.538E+006 1.365E+006 964.08 14.65 1. 322E+D05 l.197E+005 6.064E+004 1085.87 10. 2 4 1. 2 99E+005 -5.789E+004 5.671E+004 1089.74 1. 73 8.306E+005 -4.350E+005 3.664E+005 111 2. 07 1 3 .69 1.154E+005 -4. 3 65E+004 5. 1 44E+004 1212.95 1. 43 1.1 77 E+00 6 7.968E+005 5. 26 1E+00 5

[144]

1clide MDA Report 4/18 /2 01 l 2 :10:58 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM) Eu-1 52 1249.94 0.19 7.534E+00 6 5 .49E+004 2 .375E+005 3 . 2 89E+006 1299.14 1. 63 6. 2 90E+005 7.0 3 1E+004 2 .578E+005 1408.01 2 1. 07 7.580E+004 6.079E+004 3.333E+004 1457.64 0.50 8.077E+006 1.891E+007 3.843E+006 1528.10 0. 2 8 5.161E+006 -3.312E+005 2.222E+006 Eu-1 5 4 123.07 40.40 4.172E+004 4.17E+004 2.211E+004 2.007E+004 247.93 6.89 2 .134E+005 -1.123E+005 1.008E+005 591.76 4.95 3 .102E+005 1.004E+005 1.423E+005 69 2 .42 1. 78 7.996E+005 5.125E+005 3.614E+005 723.30 2 0.06 7.750E+004 - 7.799E+004 3.528E+004 756.80 4.5 2 2 .850E+005 -9.373E+004 1.268E+005 873.18 12 .08 1.139E+005 -7.638E+004 5 .065E+004 996.29 10.48 1.343E+005 1.143E+005 5 .943E+004 1004.76 18.01 7.848E+004 -4.055E+004 3 .473E+004 1274.4 3 3 4.80 4.350E+004 -2 .035E+004 1.913E+004 1596.48 1. 80 6.021E+005 -1.050E+005 2 .433E+005 Eu- 1 55 45.30 1. 31 9.965E+005 6.55E+004 7.444E+005 4.740E+005 60.01 1. 22 1 .182E+006 - 8.113E+005 5.650E+005 86.55 30.70 6.548E+004 5.333E+004 3.170E+004 105.31 21.10 8. 2 04E+004 2 .632E+004 3.951E+004 Tl- 2 0 8 583.19 85.00 2 .147E+004 2 .15E+004 9.081E+00 3 9.998E+003 Bi-211 35 1. 07 13.0 2 l .487E+005 1.49E+005 2. 053 E+005 7.061E+004 Pb- 2 11 404.85 3.78 3.538E+005 3.54E+00 5 2.659E+004 1. 63 0E+005 427.09 1. 76 8.601E+005 -2 .069E+005 3 . 99 6E+005 832.01 3.5 2 4.890E+005 4.151E+005 2 .234E+005 Bi -2 12 39.. 86 1. 06 1. 2 22E+006 2.34E+005 5.113E+005 5.812E+005 727.33 6.67 2 .337E+005 9.662E+003 1.064E+005 785.37 1.10 1.346E+006 - 2.908E+005 6.072E+005 1 620.50 1. 4 7 6.905E+005 2.633E+005 2 .740E+005

+     Pb-2 1 2     115.18*     0.60   1.740E+006     2 .47E+004  -l.492E+005    8.163E+005 238.63*   43.60    2 .475E+004                  l.330E+00 4  l.146E+004 300. 0 9    3.30   4.688E+005                 - 2 .230E+005  2 . 2 08E+005 Pb212 - XR    74.8 2   10.28    2 .170E+005    1. 2 0E+005   3 .653E+005  1 .0 5 4E+005

77. 1 1 17.10 1.202E+005 5.460E+004 5.8 2 5E+004 87.35 3.97 4.962E+005 - 5.870E+004 2.401E+00 5 89.78 1. 46 1 . 2 88E+006 - 4.496E+005 6. 22 4E+00 5 Bi -2 1 4 609.32 45.49 4.592E+004 4.59E+004 5.0 2 8E+004 2 .155E+004 768.36 4.89 3.308E+005 2 .674E+005 1.508E+005 806.18 1. 26 1.169E+006 -2 .558E+004 5. 2 64E+005 934.06 3.11 4.673E+005 2 .991E+005 2 .084E+005 11 2 0. 2 9 14.92 1.410E+005 1.239E+005 6.477E+004 11 55. 2 1 1. 63 9. 2 57E+005 - 2 .165E+005 4.096E+005 1238.1 2 5.83 3.114E+005 l.883E+005 1.403E+005 1280 . 98 1. 43 1.309E+006 l.120E+006 5.906E+005 1 377.67 3.99 3.544E+005 -2 .416E+005 1. 5 3 4E+005 1385.31 0.79 1.673E+006 1 .067E+006 7.163E+005 1401. 52 1. 33 9.678E+005 -8.064E+005 4.117E+005 1407.99 2.39 6.671E+005 5.350E+005 2 .934E+005 1509. 2 1 2 .13 5.801E+005 -1.828E+005 2 . 42 9E+005 1 661. 2 7 1. 05 1 .127E+006 -l.078E+006 4. 62 1E+005

[145]

tclide MDA Report 4/ 1 8/ 2 0 1 E 2: 1 0:58 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( \, ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) Bi-214 1729.59 2 .88 5.630E+005 4.59E+004 1.579E+005 2 .436E+00 5 1764.49 1 5.3 0 1.611E+005 1.503E+005 7.334E+004 1847.43 2 .03 4.950E+005 -2 .550E+005 1.917E+005

  >              2118.51        1.16   O.OOOE+OOO                      O.OOOE+OOO    O.OOOE+OOO Pb-214      241.99       7.25   2.349E+005     5. 2 9E+004      2 . 2 19E+004 1.119E+005 295.22     18.42    8.590E+004                    -2 .574E+004    4.053E+004 351. 93    35.60    5. 2 93E+004                    2 .1 72 E+004 2.510E+004 785.96       1. 06  1.355E+006                    -4.158E+005     6.093E+005 Pb214-XR      74.82      5.80   3 .847E+005    2 .12E+005       6.474E+005    1.869E+005 77.11      9.70   2. 119E+005                     9.625E+004    1.027E+005 87.35      2.24   8.794E+005                    -1.040E+005     4.255E+005 89.78      0.82   2.294E+006                    -8.005E+005     1.108E+006 Ra-226      1 86.2 1     3.64   4.492E+005     4.49E+005        1.731E+005    2 . 1 48E+005 Ac-228      129.07       2.42   6.815E+005     8.41E+004      - 2 .393E+005   3.274E+ 0 05 209. 2 5     3.89   4.023E+005                    - 2 .646E+004   1 .915E+005 270. 2 4     3.46   4.439E+005                      5.749E+004    2 .096E+005 328.00       2. 95  4.997E+005                    -5. 2 96E+004   2 .339E+005 338. 32    11. 27   1.311E+005                    -3.761E+004     6.133E+004 409.46       1. 92  7.273E+005                      4.653E+004    3.363E+005 463.00       4.40   3.345E+005                      2.459E+005    1.545E+005 794.95       4. 2 5 3.508E+005                      5.556E+003    1.583E+005 911.20     2 5 . 80 8.409E+004                      9.946E+004    3.904E+004 964.77       4.99   3.796E+005                      2.499E+005    1.738E+005 968.97     15.80    1.115E+005                      5.361E+003    5.071E+004 1588.20        3.22   3.567E+005                      1.103E+004    1.462E+005 Pa-2 31       27.36    10.30    8.771E+004     8.77E+004        7.830E+004    4.077E+004 283.69       1. 70  8.414E+005                    -3 .924E+005    3 .950E+005 300.07       2.47   6. 2 63E+005                  -2 .980E+0 0 5  2 .950E+005 302.65       2.20   6.637E+005                      3.640E+005    3 .114E+005 330.06       1. 40  1.049E+006                    -1.679E+005     4.911E+005 Th-234        92.38      2 .13  8.476E+005     8. 4 8E+005      5.562E+005    4.089E+005 92.8 0     2 .10  8.533E+005                      7 . 914E+004  4.115E+005 112.81       0 . 21 8.015E+006                      2 .187E+005   3 .855E+006 U-235       143.76     10 .96   1.451E+005     2 .85E+004     -4.014E+004     6.951E+004 163.33       5.08   3. 1 05E+005                    l.889E+005    1 .485E+00 5 1 85.71    57.2 0   2 .846E+004                     l.058E+00 4   1.361E+004 2 02.11      1. 08  1. 509E+006                   - 2 .684E+005   7. 2 03E+005 2 0 5.31     5.0 1  3 . 2 15E+005                 -1. 3 33E+005   1.533E+005 Am-241        59.54    35.90    4.029E+004     4.03E+004      -8.673E+003     1.9 2 6E+004
     + = Nuclide identified during the nuclide identification

• Energy line found in the spectrum

     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ =  Half-life    too short to be able to perform the decay correction

[146]

' *******~****************    '*************************        *****************
' ***        GAMM A       S P E C T R U M         A N A L Y S I S                     *****

.lename: 54 52 iport Generated On 4/18 /2 01 6 1:24:07 PM tmple Title B306100AFRWC010GD tmple Description TB 560 tmple Identification 1mple Type tmple Geometry iak Locate Threshold 3. 00 iak Locate Range (in channels) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mple Size 1.000E+OOO SQM tmple Taken On

quisition Started 4/18/2016 1:14:06 PM

.ve Time 600.0 seconds ial Time 600.6 seconds !ad Time 0.11 % Energy Calibration Used Done On 1 / 13 / 2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBWALL

1) o.\.tA. ~o_\i. c\a. \eJ by Ci)~

                                                                    /)-5-)i cJ/i,50

[147]

iak Analysis Report 4/ 1 8 / 201 6 1:2 4 :07 P1- Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B306100AFRWC0l0GD Peak Analysis Performed on: 4/18/2016 1: 2 4:0 7 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start en d centroid (keV) (keV ) Area Uncert. Counts 1 285 - 3 07 301.39 75.00 0.65 1.70E+002 73.72 3 .06E+002 2 948 - 960 955.85 238.82 0.68 5.32E+001 2 6.15 4.48E+001 3 1127- 11 3 6 113 1 .30 282.73 0.77 8.03E+OOO 15.01 2 .lOE+OOl 4 1176- 1187 118 1. 17 295.21 0.69 2 .74E+001 17.54 1.96E+001 5 2430- 2 44 2 2 434.81 608.88 0. 32 4. 1 4E+001 17.57 1. 3 6E+001 6 5829- 5851 5839.80 1460. 22 1.18 1 .86E+002 31. 66 1.68E+001 First peak in a multiplet region

= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 . 000 sigma

[148]

1terference Corrected Act:,. ~ ty Report 4/ 1 8/ 2 01 6 .... 24: 08 PM Page 3 ' *** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample Titl e : B306100AFRWC0l0GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQM ) Uncertainty K-40 0.999 1460.82* 10.66 1 .26935E+00 6 2.42341E+005 ...f ,., l'-

                                                                                      ~

Hg 203 Pb-2 1 2 0.900 0.975 279.20* 115.18

01. 56 0.60 3.17303E+003 5.95007E1003 f ""'",,

2 38. 63

• 43.60 3.61328E+004 1.86845E+004 3 00.09* 3.30 2.73152E+005 1.80456E+005

       * = Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :        10.000 keV Nuclide confidence index threshold=                0.3 0 Errors quoted at 2 .000 s igma

[149]

1t~rfer~nce Corrected Act~ Lty Report 4/18/ 2 016 .1.. . 24: 08 PM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 0.999 1.269355E+006 2.423413E+005 II~ 203 QI ggg 3.1730341!:+003 5. 950870E:4tltl~' ,,1,/a Pb-212 0.975 3.864686E+004 1.858511E+004

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at          2 .000 sigma
 **********        U N I D E N T I F I E D            P E A K S       **********

Peak Locate Performed on: 4/18/2016 1: 2 4:07 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. g_ No . (keV) Counts per Second a Uncertainty Type Nucl ide 1 75. 00 2 .8324E-00 1 @ Tol. Pb214- XR Ba-133 Pb2 1 2-XR Pb21 2 -XR Pb214-XR 5 6 0 8.88 6.9053E- 00 2 Tol. Zr-97 Sb-125 Sb-125

                                                                                        ~

M = First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [150]

1clide MDA Report 4/18/2 0 h , 1:24:08 PM Page 5

• • • • N U C L I D E MD A R E P O R T *****

Detector Name: 545 2 Sample Geometry: Sample

Title:

B306100AFRWC010GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM )

+      K-40       1460.82*     10.66 1.984E+005       1.98E+005 1.269E+00 6         8.997E+004 Cr-51        32 0 .08      9.91 1 .552E+005    1.55E+005 1. 2 05E+004        7. 2 90E+004 Mn-54        834.85      99.98   1.661E+004    1.66E+004 9 . 53 7E+003       7.562E+003 Co-58        810.76      99.45 1. 3 09E+004    1. 31E+004 -1.163E+004        5.8 1 0E+003 Co-60      1173.23      99.85 1.744E+004       1. 4 7E+004 3 .652E+003       7.841E+00 3 1 332 . 4 9  99.98 1.469E+004                    -4.383E+003      6.414E+00 3 Nb-94        702.65     99.81 1.652E+004       1.46E+004 -2 .034E+003        7.573E+00 3 871. 09    99.89 1.456E+004                      7.430E+003     6.523E+00 3 Sn-113       255.13       2 .11 7.404E+00 5    2 .39E+004 2 .169E+005        3.506E+005 391. 70    64.97 2 .386E+004                     1.350E+004     1.114E+004 Cs-134       475.36       1. 48 1.055E+006     1.57E+004 - 1.922E+005        4.892E+005 563.25       8.34 1.797E+005                   -5. 2 08£+004    8. 2 44E+004 569.33     15.37 1.001E+005                    -1.120E+004      4.601E+004 604.72     97.62 2.106E+004                    -1.976E+004      9.876E+003 795.86     85.46 1.573E+004                    -7.703E+003     7.015E+003 8 01. 95     8.69 1.641E+005                     5.467E+004    7. 3 63E+004 1 0 38.61      0 .99 l.573E+006                  - 5.771E+005    7. 0 31E+005 1167.97        1. 79 8.300E+005                  -4.4 28 E+005   3.661E+005 1365.19        3.0 2 4. 3 61E+005               -1. 4 62 E+005   1. 8 67E+005 Cs-137        661 . 66   85.10 1 .754E+004      1.75E+004 1.0 52 E+003       7.984E+003 Eu-15 2       12 1. 7 8  28 .67  6.610E+004     5.71E+004 1.981E+004         3 .193E+004 2 44.7 0     7.61 2.342E+005                     1.763E+004    1.118E+00 5 2 95.94      0.45 3.588E+006                     1.420E+006    1.695E+00 6 344. 2 8    2 6.60 5.7 1 5E+004                -5 .498E+004     2 .676E+004 367.79        0 .86 1.667E+006                    4. 2 67E+005  7.756E+005 4 11 .12     2.24  6.024E+005                 -1.57 1 E+005    2.776E+005 443.96       2.83 5. 32 1E+005                   2 . 2 88E+005 2.467E+005 488.68       0.42 2 .976E+006                 -2 .824E+006     1.351E+006 563.99        0.49 3 . 0 53E+006               -2 .861E+006     1.401E+006 586. 2 6      0.46 4. 3 48E+006                   5.470E+006    2 .037E+006 678.62        0.47 3.439E+006                     1 . 3 08E+006 1.576E+006 688.67       0.86 1.815E+006                   -8.199E+005      8. 2 83E+005 7 1 9. 3 5   0.28 5. 33 7E+006                 -5.362E+006      2 .420E+006 778.9 0    1 2 .96 1. 475E+005                    9.803E+004    6.821E+004 810.45       0.32 4.056E+006                   - 3.332E+006     1.800E+006 867.37       4. 2 6 3.468E+005                 -5.678E+004      1. 55 7E+005 919.33       0.43 3.020E+006                   -8.784E+004      1. 32 8E+006 964.08     14.65 1.392E+005                      3.1 5 8E+004   6.415E+004 1085.87      10. 2 4 1. 4 64E+005                  1. 93 0E+004   6.497E+004 1089.74        1. 73 7.909E+005                  -1.716E+005      3.466E+005 1112.07      13.69 1. 239E+005                   -1.111E+005      5.574E+004 1 212.95       1. 43 1.359E+006                    5.470E+005     6.169E+005

[151]

4/18/ 2 0ll 1: 2 4:08 PM Page 6 1cli,de J.v!DA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Eu-1 52 1249.94 0.19 9.013E+006 5.71E+00 4 l. 465E+006 4.0 2 8E+006 1 2 99.14 1. 63 9.629E+005 - 3 .792E+005 4. 2 48E+005 1 4 0 8.01 2 1. 07 7.392E+004 1.083E+004 3 . 2 39E+004 1 457.64 0.50 1.033E+007 3 .161E+007 4.969E+006 1528.10 0. 2 8 4.987E+006 4.415E+004 2.135E+006 Eu-1 5 4 1 23 .07 40.40 4.656E+004 4.66E +004 1.848E+004 2.249E+004 2 47.93 6.89 2 .422E+005 1.911E+004 l.152E+005 591.76 4.95 2 .854E+005 -1.961E+005 l. 2 99E+005 692.42 1. 78 9.115E+005 -8. 1 94E+005 4.174E+005 723.30 20. 0 6 8. 1 43E+004 2 .848E+004 3 .725E+004 756.80 4.5 2 3.419E+005 6.248E+004 l.552E+005 873.18 1 2 .08 1. 2 48E+ 0 05 1.706E+004 5.611E+004 996.29 10.48 1.658E+005 4.999E+004 7.5 1 8E+004 1004.76 18.01 1.060E+005 -1.855E+004 4.849E+004 1274.4 3 34.80 4.753E+004 1 .828E+0 0 3 2 .114E+004 1596.48 1. 80 7.115E+005 -2 .241E+005 2 .980E+005 Eu-155 45.30 1. 3 1 8.359E+005 7.58E+004 2 .511E+005 3.937E+005 60.01 1. 22 1. 3 38E+006 -5.472E+005 6.431E+005 86.55 30.70 7.584E+004 5.334E+004 3.688E+004 10 5.31 2 1.10 9.506E+004 3.489E+004 4.601E+004 Tl-208 583.19 85.00 2 . 4 0 5 E-1. 0 0 4 '"> A"P * "f\A L... .'":tUD i~ VU":t 1. 9 58E+004 1.129E+004 Bi-211 351.07 1 3.02 l .538E+005 1 .54E+005 2.572E+005 7.319E+004 Pb-2 11 404 .85 3.78 3.772E+005 3.77E+005 - 2.847E+005 1.748E+005 4 27. 0 9 1. 76 7.955E+005 3.4 5 1E+002 3.673E+005 8 32 . 0 1 3.52 4.392E+005 - 4.513E+005 1.985E+005 Bi -2 1 2 39.86 1. 0 6 9.825E+005 2.37E+005 -6 .554E+005 4.6 1 3E+005 727.33 6 . 67 2 .367E+005 1.542E+005 1.079E+005 785.37 1. 10 1 .427E+006 5.930E+005 6.477E+005 1 620.50 1. 4 7 6.905E+005 2 .633E+005 2 .740E+005

+       Pb- 2 12       115.18       0.60   3.197E+006            2 . 61E+004             6.315E+00 4   1.545E+006 2 38.63*   43.60    2.606E+004                                    3.613E+004    1. 2 11E+004 300. 09 ~-   3.30   2.579E+00 5                                   2 .73~E+005   1.155E+005 Pb212-XR          74.82    10. 2 8  2.478E+00 5           1 .40E+005              2 .802E+00 4  1. 2 08E+005

77. 11 17.10 1.398E+005 -1.699E+004 6.8 0 4E+004 87.35 3.97 5.844E+005 4.659E+005 2 .842E+005 89.78 1.4 6 1.498E+006 -1.611E+005 7. 2 75E+005 Bi- 2 1 4 609. 32 45.49 4.646E+004 4. 65 E+004 5.786E+004 2 . 1 82E+004 768.36 4.89 3.627E+005 - 3.333E+004 1.667E+005 806.18 1. 2 6 1.091E+006 2 .138E+004 4.874E+005 934.06 3.1 1 5.0 2 1E+005 -7.887E+004 2 . 25 8E+00 5 1120. 2 9 14.92 1. 3 00E+005 4.458E+004 5 . 92 6E+004 1155. 2 1 1. 63 1.022E+006 -5 . 2 16E+005 4.579E+005 1 23 8.12 5.83 2 .960E+005 2 .045E+005 1 . 32 6E+005 1280.98 1. 43 1.133E+006 -3 .064E+005 5 .026E+005 1377.67 3.99 3.857E+005 - 2 .788E+005 l.690E+005 1385.31 0.79 2 .3 08E+006 -2 .222E+005 1.034E+006 1401.52 1. 33 1.198E+006 6.603E+005 5.266E+005 1407.99 2.39 6.5 0 6E+005 9.529E+004 2 .851E+005 1509. 2 1 2.13 7.421E+005 3.699E+005 3 . 23 9E+005 1661. 2 7 1. 05 9.842E+005 3.754E+005 3.905E+005

[152]

tclide MDA Report 4/18 /2 0 lt, 1:24:08 PM Page 7 Nucl ide Energ~' Yield Line MDA Nuc l ide MDA Activity Dec. Level Name (keV ) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi-2 14 1729.59 2 .88 4.664E+005 4.65E+004 - 9. 32 9E+00 3 1 .953E+005 1764.49 15.30 1. 2 80E+005 7.784E+004 5.681E+004 1 847.43 2.03 4.436E+005 l .23 6E+005 1.660E+00 5

  >              2 11 8.51      1.16   O.OOOE+OOO                    O.OOOE+OOO    O.OOOE+OOO Pb- 2 1 4    2 41. 99    7. 2 5  2 .718E+005   5 .61E+004 -2 .602E+005       1.304E+005 295.22    1 8.42    8.504E+004                   3 . 3 48E+004  4.010E+004 351. 93   3 5.6 0   5.613E+004                    6 .927E+004   2 .670E+004 785.96      1. 06   1.463E+006                   1.103E+005     6 .633E+00 5 Pb214-XR       74 . 82   5.80    4. 3 92E+005  2 .46E+005 4.967E+004         2 .141E+00 5 77.11     9.70    2 .465E+005                 -2 .995E+004    1. 2 00E+005 87.35     2 . 24 1 .036E+006                   8. 2 57E+005   5.037E+005 89.78     0.8 2  2 .668E+006                  -2 .868E+005    1. 2 95E+006 Ra-226       186.21      3.64    4.916E+00 5   4.92E+005 3.301E+005          2 . 3 60E+005 Ac-228       129.07      2 .42  7.419E+005     7. 2 2E+004 -1.685E+004      3. 576E+005 209. 2 5    3.89   4.459E+005                    2 .979E+00 5   2 .133E+005 270. 2 4    3.46   4.565E+005                    l.503E+005     2 .159E+005 328.00      2 .95  5. 2 16E+005                  1.452E+005    2 .449E+005 338.32    11.27    1.458E+005                    3 .077E+004    6.867E+004 4 0 9.46    1. 92  7.140E+005                  - 1.8 2 9E+005  3 . 2 96E+005 4 63.00     4.40   3.583E+005                    2 .159E+005   1 . 664E+005 794.95      4. 2 5 3.222E+005                    8.069E+004    1.440E+005 911. 20   25.80    7.223E+004                    6.402E+004    3.311E+004 964.77      4.99   4.007E+005                  -1.122E+004     l.844E+005 968.97    15.80    1 .306E+005                   6.704E+004    6.0 2 6E+004 1 588.2 0      3. 22  3.958E+005                    2 .138E+005   1.658E+005 Pa-23 1       27.36    10.30    6.897E+004     6.90E+004 5.042E+004         3.140E+004 283.69       1. 70  8.846E+005                    3.178E+005    4.166E+005 300.07       2 .47  6.459E+005                    4.380E+004    3.047E+005 302.65       2 . 20 7.355E+005                    3.406E+005    3.472E+005 330.06       1. 40  1.015E+006                  -5.645E+005     4.737E+005 Th- 23 4      92.38      2 .13  9.807E+005    9.81E+005 -4.141E+005         4.754E+005 92.8 0    2 .10   9.849E+005                  -2 .790E+005    4.773E+005 112.81       0. 2 1 9. 2 39E+006                  5. 2 48E+006  4.467E+006 U-235       1 43.76    10.9 6   1.573E+005    3.09E+004 -5.522E+004         7.562E+004 1 63.33     5.08    3.436E+005                  -6.713E+004     1.651E+005 185.7 1    57.20    3.086E+004                    4.621E+003    1.481E+004 2 02 . 11   1. 08   1.552E+006                    4.789E+005    7.416E+005 2 05.3 1    5.01    3 .401E+005                 -l.390E+005     1. 62 6E+005 Am- 2 41       59.54    35.90    4. 3 97E+004  4.40E+004 -5.351E+004         2 . 1 10E+004
    +    Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    >    Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Half-life too short to be able to perform the decay correction

[153]

"************************* ~************************* * *****************

• • • • G A MMA S P E C T R U M A N A L Y S I S *****

.lename: 54 5 2 iport Generated On 4/19/2016 8:27:53 AM 1mple Title B306100AFRFC011GD tmple Description TB 580 1mpl e Identification tmple Type tmple Geometry !ak Locate Threshold 3 .00 !ak Locate Range (in channels ) 85 - 8 1 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10.000 keV 1mple Size 1.000E+OOO SQMl ,,, , tmple Taken On

quisition Started 4/19/2016 8:17:50 AM

.ve Time 600.0 seconds !al Time 601.3 seconds iad Time 0. 2 1 9_; Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/20 1 6 Efficiency ID TBFLOOR

                                                                \)o.+~ ~o.\\q~~ec\ 'by
                                                                 ~4
                                                                  /p-6,-/~

01/~ [154]

ia k Analysi s Report 4/19/2016 8 : 2 7 : 5 3 AJ.v1 Page 2

"***               P E A K       A N A L Y S I S          R E P O R T                       *****

Detector Name: 5452 Sample

Title:

B306100AFRFC011GD Peak Analysis Performed on: 4/19/2016 8:27:52 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 12 2 115.79 28.54 0.69 5.22E+001 2 0.93 2.18E+001 2 296- 306 301. 23 74.96 0.97 6.96E+001 40.08 1.38E+002 3 455- 462 458.83 114.41 0. 2 5 -1.46E+OOO 21. 39 5.75E+0 01 4 949- 959 954.66 238.52 0.88 3 .02E+001 2 1 .74 3 .68E+001 5 1 402- 1413 1407.44 351. 8 3 1. 25 3 .36E+001 18.13 1 .94E+001 6 2430- 2440 2435.90 609. 1 5 1. 24 3 .79E+001 15.13 8. 1 3E+OOO 7 5829- 5850 5839.7 2 1460. 2 0 1. 84 l.40E+002 2 4.47 2 .57E+OOO First peak in a multiplet region

= Other peak in a multiplet region Fitted sing l et

rors quoted at 2 .000 sigma

[155]

1terference Corrected Act_ ity Report 4/19/2016 0; 2 7:53 AM Page 3 '*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample

Title:

B306100AFRFC011GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB

 . . . ... . . . .. . . . . . . . . . IDENTIFIED NUCLIDES            . . ............... .. .

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQMl) Uncertainty K-40 0.999 1460.8 2

• 10.66 9.57354E+005 l.86380E+005 Pb-21 2 0.895 115.18* 0.60 - 5.83073E+004 8.51950E+005 2 38.63* 43.60 2 .05117E+004 l.51118E+004 300.09 3.30 Pb-214 0. 4 92 2 41.99* 7.25 1 . 2333 6E+005 9.08241E+004 2 95. 22 18.42 351.93* 35.60 3.39524E+004 1.91003E+004 785.96 1. 06 Th-231 0.877 25.64* 14.10 8.79164E+004 4.094 2 1E+004 84.21* 6.60 2 .50334E+005 1 .55563E+005 89.95 1. 00

        * = Energy line found in the spectrum.
        @=Energy line not used for Weighted Mean Activity Energy Tolerance :                   10.000 keV Nuclide confidence index threshold =                       0.30 Errors quoted at 2 .000 s igma

[156]

1terference Corrected Act~ _ty Report 4/ 1 9/2 01 6 c... 27: 53 AM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQMl ) Uncertainty K-40 0.999 9.573543E+005 1.863797E+ 0 05 X Co-57 0.744 X Bi-211 0.999 Pb-21 2 0.895 1 .48651 4E+004 1 .543482E+004 Pb-214 0. 4 92 3.395236E+004 1.909983E+004 X Pa-231 0.376 Th-231 0.877 9.843777E+004 3.959380E+004

     ?     Nuclide is part of an undetermined solution X     Nuclide rejected by the interference analysis
     @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2 . 000 s igma
 **********     U N I D E N T I F I E D            p E A K     s  **********

Peak Locate Performed on: 4/19/2016 8: 27 :52 AM Peak. Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV) Counts per Second  % Uncertainty Type Nuclide 6 609.15 6.3116E- 00 2 39.95 Tol. Zr-97 Sb-125 Sb-125 Cs-134 Bi-214 M = First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [157]

1clide MDA Report 4 / 1 9/ 2 01 1 8: 2 7:53 AM Page 5

• • • • N U C L I D E M D A R E P O R T *****

Detector Name: 545 2 Sample Geometry: Sample

Title:

B306l00AFRFC0 l 1GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQMl) (pCi/SQMl) (pCi/SQMl) (pCi/SQMl)

+      K-40       1 460.8 2

• 10.66 8.666E+004 8.67E+004 9.574E+005 3.411E+004 Cr-51 320.08 9.91 1.450E+005 1.45E+00 5 l.082E+005 6.784E+004 Mn-54 834.85 99.98 l.477E+004 1.48E+004 7.733E+00 2 6.642E+00 3 Co-58 810.76 99.45 l .337E+004 l.34E+004 -1 . 089E+004 5.947E+00 3 Co-60 1173.23 99.85 l.654E+004 l.43E+004 -9.2 44E+00 3 7.393E+00 3 1332. 4 9 99.98 1.429E+004 1.034E+004 6. 2 11E+003 Nb-94 70 2 .65 99.81 l.517E+004 1.38E+004 -7.996E+00 3 6.897E+003 871. 09 99.89 1.375E+004 8.035E+00 3 6.119E+00 3 Sn-113 255. 1 3 2 .11 6.793E+00 5 2 . 1 6E+004 4 .2 48E+005 3.200E+005 391.70 64.97 2 .159E+004 6 .037E+003 l.OOOE+004 Cs- 1 3 4 475.36 1. 48 9. 2 15E+005 1.75E+004 -2 . 72 8E+005 4.224E +005 563.25 8.3 4 l.874E+005 5.379E+0 0 3 8.628E+004 569.33 15.3 7 8.655E+004 4. 2 12E+004 3.924E+004 604.72 97. 62 2 .041E+004 - 1 .501E+00 3 9.550E+003 795.86 85. 4 6 1.746E+004 - 1.122E+003 7.877E+00 3 80 1 .95 8.69 1.523E+00 5 9.423E+004 6.773E+004 1038.61 0.99 1.385E+00 6 - 2 .365E+005 6.089E+005 1167.97 1. 79 1.018E+006 l .083E+006 4.601E+005 1365. 1 9 3 . 02 4. 3 61E+00 5 1. 2 89E+005 1.867E+005 Cs -137 661.66 85. 1 0 1.927E+004 1 .93E+004 1.1 2 7E+004 8.849E+003 Eu-1 5 2 121.78 28.67 5.463E+004 5.46E+004 - 1.843E+004 2 .619E+004 244.70 7 . 61 2 .146E+005 1 . 2 18E+005 1.020E+005 295.94 0.45 3.657E+006 2 . 3 93E+006 1.729E+006 344.28 26.60 5.715E+004 4.185E+00 4 2 .676E+004 367.79 0.86 1.654E+006 3.682E+005 7.692E+005 411.12 2.24 6. 1 41E+005 8.988E+004 2 .835E+005 443.96 2.83 4.997E+005 -1.502E+005 2 . 3 05E+005 488.68 0.42 2 .763E+006 -2 .421E+006 1. 2 45E+006 563.99 0.49 3 . 11 9E+006 9.635E+005 l.434E+006 586. 2 6 0.46 3.634E+006 1.3 3 4E+006 1.680E+006 678.62 0.47 2 .542E+006 - 3.4 2 6E+005 1.128E+006 688.67 0.86 1.599E+006 6.162E+005 7. 2 05E+005 719.35 0. 2 8 5.183E+006 2 . 2 65E+006 2 .343E+006 778.90 12.96 9.437E+004 -3 .344E+0 0 4 4.163E+004 810.45 0.32 4. 22 4E+006 -8.440E+004 1 .883E+006 867.37 4.26 3.283E+005 7.032E+004 1.464E+005 919.33 0.43 3.677E+006 7.401E+005 1.656E+006 964.08 14.65 1. 2 92E+005 1 . 007E+005 5.918E+004 1 085.87 10. 2 4 1.611E+005 - 3 .844E+004 7. 22 9E+004 1 089.74 1. 7 3 9.873E+005 -1. 3 16E+005 4.448E+00 5 1 112.07 13.69 1.154E+005 -4.430E+004 5.144E+004 1212.95 1. 43 1.282E+006 1.154E+005 5.783E+005

[158]

1clide MDA Report 4/19/ 2 0 1L 8: 2 7:53 AM Page 6 Nuclide Energy Yiel d Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQMl) (pCi/SQMl ) (pCi/SQMl ) (pCi/SQMl) Eu- 1 52 1249.94 0.19 8.125E+006 5.46E+004 -1.488E+006 3.584E+006 1299.14 1. 63 8.930E+005 -4.817E+005 3.898E+005 1408.01 2 1. 07 6.579E+004 2 .702E+004 2 .833E+004 1457.64 0.50 8.615E+006 2 .093E+007 4. 1 12E+00 6 1528.10 0. 2 8 2.460E+006 5. 2 98E+005 8.716E+005 Eu-154 123.07 40.40 3.952E+004 3 .95E+0 0 4 -1. 32 5E+002 1.896E+004 247.93 6.89 2.145E+005 -1.940E+005 l.013E+005 591. 76 4.95 2 .580E+005 7.080E+004 1.162E+005 692.4 2 1. 78 7.996E+005 -2 .737E+005 3 .614E+005 723.30 2 0.06 6.892E+004 -9.186E+003 3.099E+004 756.80 4. 52 3.225E+005 2 .832E+005 1.455E+005 873. 1 8 12.08 1.067E+005 5 .864E+003 4.707E+004 996. 2 9 10 .48 1 . 5 36E+005 4.760E+004 6.905E+004 100 4.76 18.01 7.848E+004 4.831E+004 3.473E+004 1 274.43 34.80 4. 2 42E+004 9. 632 E+003 1.859E+004 1596.48 1. 80 7.744E+005 2 . 2 71E+005 3.294E+005 Eu-155 45.30 1. 31 1.006E+006 6.63E+004 8.612E+005 4.787E+005 60.01 1. 22 1. 201E+006 8.428E+003 5.742E+005 86.55 3 0.70 6.633E+004 6.989E+004 3. 2 12E+004 105.31 2 1.10 8.137E+004 -3 .682E+00 3 3.916E+004 Tl-208 583.19 85.00 2.014E +004 2.01E+004 1 .517E+004 9.331E +003 Bi-211 351.07* 13.0 2 7.078E+004 7.08E+004 9.283E+004 3.165E+004 Pb-211 404.85 3.78 3.503E+005 3.50E+005 -1.818E+005 1.613E+005 42 7.09 1. 76 8.532E+005 2 .8 3 4E+005 3 .961E+005 832 .01 3.5 2 4. 1 89E+005 -2 .227E+005 1.883E+005 Bi -2 12 39.86 1. 06 1.138E+006 1.90E+005 - 5.566E+005 5.388E+005 727.33 6.67 1.896E+005 - 1 .774E+004 8.435E+004 785.37 1.10 1.346E+006 - 2 . 26 5E+005 6 .072E+005 1 620.50 1. 47 8.777E+005 4.740E+005 3.676E+005 + Pb-2 1 2 11 5.18* 0.60 1.518E+006 2.28E+004 -5 .831E+004 7.051E+005 23 8.63* 43.60 2 . 2 75E+004 2 .0 5 1E+004 1.046E+004 30 0 . 0 9 3.30 4.511E+005 -1.685E+005 2 .119E+005 Pb2 1 2-XR 74.8 2 10. 2 8 2 .162E+005 1. 2 3E+005 4.125E+005 1.050E+005

77. 11 17.10 1. 22 8E+005 - 1.374E+004 5.953E+004 87.35 3.97 5.161E+005 5.415E+005 2 .499E+005 89.78 1. 46 1.365E+006 - 1.877E+004 6.604E+005 Bi-2 14 609. 32 45.49 4.453E+004 4.45E+004 3.928E+004 2 . 085E+004 768.36 4.89 3 . 1 36E+005 2 . 2 42E+005 1.422E+005 806.18 1. 2 6 1 .070E+006 -5. 1 78E+005 4.771E+005 934.06 3.1 1 4.673E+005 -2 .802E+004 2 .084E+005 1 120. 2 9 14.92 1. 316E+005 -5. 3 07E+00 3 6.008E+004 11 55. 2 1 1. 63 8.618E+005 - 3.699E+005 3.776E+005 1238.12 5.83 3.213E+00 5 1.248E+005 1.452E+005 128 0 .98 1. 43 1.005E+006 4.412E+005 4.387E+005 1377.67 3.99 3. 316E+005 - 3 .083E+004 1 .420E+005 1385.31 0.79 1. 2 54E+006 -1. 3 85E+006 5 .065E+005 1401.52 1. 33 1.137E+006 1. 2 01E+005 4.965E+005 1407.99 2 .39 5.790E+005 2 . 37 8E+005 2 .493E+005 1509. 2 1 2 .13 6.782E+005 4. 52 5E+005 2 .920E+005 1661. 2 7 1. 05 9.0 1 7E+005 3.003E+005 3 .493E+005

[159]

1clide MDA Report 4/19/201L 8:27:53 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQMl ) (pCi/SQMl) (pCi/SQMl) (pCi/SQMl) Bi -2 14 1729.59 2 .88 4.875E+005 4.45E+004 7. 27 7E+004 2 .059E+00 5 1764.49 15.30 1. 2 25E+005 1.013E+005 5.404E+004 1847.43 2 . 03 6.188E+00 5 2 .885E+005 2 .536E+00 5 2 118.51 1. 16 O.OOOE+OOO O.OOOE+OOO O.OOOE+OOO

  >                                                                              6.289E+004

+ Pb-2 14 241.99* 7.25 1 . 3 68E+005 2 .59E+004 1. 2 33E+00 5 295. 22 18.4 2 8.759E+004 2.016E+004 4.138E+004 351.93* 35.60 2.589E+004 3.395E+004 1.158E+004 785.96 1. 06 1.442E+006 -4.171E+005 6.529E+005 Pb214-XR 74.82 5.80 3.832E+005 2 .17E+005 7.310E+005 l .860E+005 77.11 9.70 2.165E+005 -2 .422E+004 1.050E+005 87.35 2 .24 9.146E+005 9.597E+005 4.430E+005 89.78 0 .82 2.430E+006 -3.343E+004 1.176E+006 Ra-226 186.21 3.64 4.035E+005 4.04E+005 -9.467E+003 1.920E+005 Ac-22 8 129.07 2.42 6.750E+005 7.69E+004 2 .618E+005 3.241E+005 209. 2 5 3.89 3 .876E+005 2. 103E+005 1.842E+005 270.24 3. 4 6 4 .264E+005 2 .115E+005 2 .009E+005 328.00 2.95 5.154E+005 1.856E+005 2 .418E+005 338.32 11.27 1. 23 1E+005 -7 .416E+004 5 .731E+004 40 9.46 1. 92 7.072E+005 l .845E+005 3 . 2 62E+005 463. 00 4. 4 0 3.313E+005 2 .437E+005 1.530E+005 794.95 4.25 3.616E+005 5.452E+004 1.637E+005 911.20 25.80 7.691E+004 3.612E+004 3 .545E+004 964.77 4.99 3 .796E+005 4. 72 5E+005 1.738E+005 968.97 15.80 l.229E+005 3 .716E+004 5.637E+004 1588.20 3 . 22 4.471E+005 8. 26 4E+004 1.914E+005 Pa- 23 1 2 7.36

• 10.30 6.361E+004 6.36E+004 1. 2 04E+005 2 .869E+004 283.69 1. 70 8.657E+005 2 .095E+005 4.072E+005 300. 0 7 2 .47 6.026E+005 -2 . 2 51E+005 2 .831E+005 302.65 2 . 20 6.516E+005 -5 .683E+00 4 3 .053E+005 330. 0 6 1. 40 l.036E+006 2 .177E+005 4.842E+005 Th-234 92.38 2 .1 3 9.070E+005 9.0 7E+005 9.787E+005 4. 3 84E+005 92.80 2 .10 9.105E+005 9.450E+005 4.400E+005 112.8 1 0.21 7.999E+006 2 .930E+006 3.846E+006 U- 235 1 43.76 10.96 l. 383E+005 2.57E+004 2.660E+004 6.615E+004 1 63.33 5.08 3 .158E+005 - 4.898E+003 1 .512E+005 1 85.71 57. 2 0 2 .574E+004 -6.782E+003 l .225E+004 2 02.11 1. 08 l . 3 62E+006 - 5.843E+005 6.470E+005 205.31 5.0 1 3. 073E+005 8.551E+004 1.462E+005 Am- 2 41 59.54 35.90 4.094E+004 4.09E+004 4. 2 96E+003 1.957E+004

     +     Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @  = Half-life too short to be able to perform the deca~1 correction

[160]

• • • • • • • • • • • • • • • • • • • • • • • • • ************************* ~****************
      • G A MMA S r E C T R U M A N A L Y S I S *****

.lename: 54 52 iport Generated On 4/ 1 4/ 2 016 2 :26:37 PM 1mple Title B306100AFRFC0l 2G D 1mple Description U-1 STS TB FLOOR 560 1mpl e Identification 1mpl e T~ pe 1 1mple Geometry iak Locate Threshold 3.00 iak Locate Range (in channels ) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 1. 000 FWHM 1mple Si ze 1. OOOE+OOO SQM 1mple Taken On

quisition Started 4/14/ 2 016 2 : 1 6: 35 PM

.ve Time 600.0 seconds ial Time 600.4 seconds iad Time 0 . 07 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBFLOOR D o.h,. \to.\1de1teJ loy

                                                                   ~4
                                                                    ,.,_,_,~

0110 [161]

!ak Analysis Report 4/14/2016 2 :26:37 P Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 545 2 Sample

Title:

B3061 0 0AFRFC012GD Peak Analysis Performed on: 4/14/2016 2:26:36 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid ( keV) (keV) Area Uncert. Counts 1 1400- 1414 1406.51 351.60 1. 26 5.46E+001 23.96 3.04E+001 2 5825- 5850 5839.53 1460. 1 5 1. 62 1.40E+00 2 3 0 .63 2 . 2 4E+001

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 . 000 sigma

[162]

1terference Corrected Act j_ :y Report 4/14/ 2 016 <. 6:37 PM Pag e 3

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • r***************
      • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Ti tle: B306l00AFRFC0l2GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zi o n Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yie ld Activity Activity Name Confidence (keV) ( t, ) (pCi/SQM) Uncertainty K-40 0. 976 1460.82* 1 0.66 9.51387E+005 2 . 2 4590E+005 Bi -2 11 0. 985 351.07* 13.02 l.50792E+005 7.04854E+004

       * = Energy line found in the spectrum.
       @ = Ene rg y line not used for Weighted Mean Activity Energy Tolerance :        1.000 FWHM Nuclide confidence index threshold =             0.3 0 Errors quoted at 2 .000 sigma

[163]

1terference Corrected Acti ty Report 4/14/2016 '. 6: 37 PM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nucl ide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0 .976 9.513867E+005 2.245902E+005 Bi-211 0 .985 1 .507923E+005 7.048536E+004

     ?  =  Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysi s
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2 .000 sigma
 **********     U N I D E N T I F I E D         P E A K S     **********

Peak Locate Performed on: 4/14/20 1 6 2:26:36 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Si z e in Peak CPS Peak Tol. No . (keV) Counts per Second ~ Uncertainty Type Nuclide Al l peaks were i dentified. [164]

1clide MDA Report 4/14/ 2 01 2 : 2 6:37 PM Page 5

• • • • N U C L I D E M D A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B306 1 00AFRFC0l2GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zi o n Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM) 1460.8 2

• 10.66 2 .371E+005 2 .37E+005 9.514E+005 1.093E+005

+      K-40

7. 2 90E+004 Cr-51 32 0.08 9.91 1.552E+005 1.55E+005 -8.048E+004 Mn-54 834.85 99.98 1.452E+004 1.45E+004 - 4.892E+003 6.518E+00 3 Co-58 810.76 99 . 45 1.489E+004 1.49E+004 -3 .951E+003 6.709E+00 3 Co-60 1 173. 23 99.85 1.8 2 9E+004 1.39E+004 1.525E+004 8. 2 65E+003 1332.49 99.98 1 .387E+004 -5.120E+003 6.000E+003 Nb-94 702.65 99.81 1.652E+004 1 .58E+0 0 4 5.695E+003 7.573E+00 3 87 1. 09 99.89 1.581E+004 -9 . 7 2 0E+003 7.145E+003 Sn-113 255.13 2 .11 7.532E+005 2 .45E+004 5. 2 63E+005 3.570E+005 391. 70 64. 97 2 .452E+004 1.302E+004 1.147E+004 Cs-134 475.36 1. 4 8 9.812E+005 1. 97E+004 2 .193E+005 4.522E+0 0 5 563.25 8.34 1 .816E+005 1.122E+004 8. 3 42E+004 569.33 15.37 1 .042E+005 7.518E+004 4.806E+004 604.7 2 97. 62 2 . 2 31E+004 9.440E+003 1.050E+004 795.86 85.46 1.974E+004 8.489E+003 9.017E+003 801. 95 8.69 1.8 2 7E+005 -8.690E+004 8. 2 95E+004 1 038.61 0.99 1.451E+006 1 .234E+006 6.419E+005 11 67.97 1. 79 1.063E+006 4.981E+005 4.8 2 5E+005 1365.19 3 . 02 4.035E+005 2.317E+005 1 .704E+005 Cs-137 661. 66 85.10 1. 947E+004 1. 95E+004 1.4 2 9E+004 8.951E+003 Eu-152 121.78 2 8.67 6.313E+004 6.03E+004 4.082E+00 4 3 .045E+004 244.7 0 7.61 2.171E+005 -1.999E+005 1.032E+005 295.94 0.45 4.012E+006 2 .632E+006 1.906E+006 344. 2 8 26.6 0 6.031E+004 -4.006E+00 4 2 .834E+004 367.79 0.86 1. 5 75E+006 5.095E+005 7 . 2 97E+005 411. 12 2.24 6.141E+005 - 7.522E+005 2 .835E+005 443.96 2.83 5.366E+005 3.825E+005 2 .490E+005 488.68 0.42 3.4 2 9E+006 2 .373E+006 1.578E+006 563.99 0.49 3.086E+006 -8.822E+005 1.417E+006 586.26 0.46 3 .666E+006 5.007E+004 1.696E+006 678.62 0.47 2 .891E+006 1.772E+006 1.303E+006 688.67 0.86 1.985E+006 1. 696E+006 9 . 135E+005 719.35 0.28 5.486E+006 -5.137E+004 2 .494E+006 778.90 12.96 1.225E+005 -4.468E+004 5.5 6 9E+004 810.45 0.32 4.830E+006 -1.694E+006 2 .1 8 7E+006 867. 3 7 4.26 3.586E+005 -4.844E+005 1.615E+005 919. 33 0.43 3.557E+006 -6.845E+005 1.596E+006 964.08 14.65 1.278E+005 5.832E+004 5.844E+004 1085.87 10.24 1.147E+005 -2.052E+005 4.911E+004 1089.74 1. 73 8.682E+005 3.114E+005 3.852E+005 1112.07 1 3 .69 1.430E+005 -2.076E+005 6.525E+004 121 2 .95 1. 43 1.132E+006 - 2.161E+005 5.037E+005

[165]

1clide MDA Report 4/14/ 2 01 2 : 2 6:37 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) Eu-1 52 1249.94 0.19 7.110E+006 6.03E+004 -2 .903E+005 3 .077E+006 1299.14 1. 63 7.885E+005 -4.590E+005 3 . 3 76E+005 1408.01 21. 07 7.392E+004 -l.187E+004 3 . 2 39E+004 1457.64 0.50 9. 2 74E+006 2 .382E+007 4.442E+006 1528. 10 0. 2 8 4.415E+006 3.385E+00 5 1.849E+006 Eu-154 123.07 40.40 4.443E+004 4.44E+004 -3.409E+00 3 2 .142E+004 247.93 6.89 2 . 3 12E+005 4.656E+004 1.097E+005 591. 76 4.95 3.033E+005 9.782E+004 1. 389E+005 692.42 1. 78 9.522E+005 6.079E+005 4.377E+005 723.30 2 0.06 9.043E+004 7.895E+004 4.175E+004 756.80 4.52 3.017E+005 - 2 . 99 9E+005 l .351E+005 873.18 12 .08 1.403E+005 -2 . 2 55E+004 6.389E+004 996. 2 9 10.48 1. 343E+005 5.498E+004 5.943E+004 1004.76 18.01 8.0 2 0E+004 2 .754E+004 3.558E+004 1 274.4 3 3 4.80 5.1 22 E+004 2 . 3 74E+004 2 . 2 99E+004 1 596. 4 8 1. 80 8.318E+005 5.550E+005 3 . 5 81E+005 Eu-155 45.30 1. 31 9.357E+00 5 7 . 3 9E +00 4 5.519E+005 4.436E+005 60.01 1. 22 1. 2 97E+00 6 -7.924E+004 6. 22 5E+005 86.55 30.70 7.392E+004 3.211E+004 3 .592E+004 10 5.31 21.10 9.129E+004 - 4.458E+003 4.413E+004 Tl- 2 08 583.19 85.00 1.979E+004 l.98E+004 5.038E+002 9. 1 57E+003

+     Bi-211       351.07*  13 . 02  9.315E+004      9.32E+004 1.508E+005           4. 2 84E+004 Pb- 211      40 4.85    3 .78  3.836E+005      3.84E+005 -1.075E+005          1 .7808+005 427. 0 9   1. 76  7.955E+005                       l.949E+005    3 .673E+005 832. 0 1   3.52   3 .898E+005                    - 6.148E+004    1.738E+005 Bi-212        39.86     1. 06  l.028E+006      2 .65E+0 0 5 -2.368E+005       4.838E+005 727.33     6.67   2 .648E+005                      1.817E+005    1. 22 0E+005 785.37     1.10   l.503E+006                       6.543E+005    6.858E+005 1 620.50     1. 4 7 7.428E+005                       5.047E+004    3.001E+005 Pb-21 2      115. 1 8   0.60   3 .014E+006     4 . 41E+004 - 1.313E+006       l.453E+006 238.63   43.60    4.407E+004                       4.999E+004    2 .112E+004 30 0 .09   3.30   4.953E+005                     - l .489E+005   2 .340E+005 Pb212-XR      74.82   10. 2 8  2 .414E+005     l .3 4E+00 5 4. 5 05E+005      l.176E+005

77. 11 1 7.10 l.340E+005 7.889E+004 6.5 1 3E+004 87.35 3.97 5.784E+005 4.680E+005 2 .8 1 2E+005 89.78 1. 46 1. 4 97E+006 -4.473E+005 7. 2 65E+005 Bi -2 14 609.32 45.49 5. 1 06E+004 5.1 1E+004 6.093E+004 2 .412E+004 768.36 4.89 3 . 1 3 6E+005 -l.891E+004 l.422E+005 806.18 1.26 l. 2 06E+006 7.805E+005 5 .449E+005 934.06 3.1 1 5.720E+005 3 .159E+005 2 .607E+005 1120. 2 9 14.92 l.645E+005 6 . 32 3E+004 7.651E+004 1155. 2 1 1. 63 l.143E+006 3 . 1 62E+005 5.181E+005 1238.12 5.83 3.164E+005 l.041E+005 1.428E+005 1 280.98 1. 43 1 .156E+006 -7. 2 16E+005 5. 144E+005 1377.67 3.99 3.544E+005 -l .007E+004 l.534E+005 1385.31 0.79 1.673E+006 -9 .778E+005 7.163E+00 5 1401.52 1. 33 l.168E+006 -2 .456E+005 5.118E+005 1407.99 2 .39 6.. 506E+005 -l.045E+005 2.851E+005 1509.2 1 2 .13 5.523E+005 2 .785E+005 2.291E+005 166 1. 27 1. 05 l. 2 51E+006 1. 689E+005 5.239E+005

[166]

1clide MDA Report 4/14/201 2 : 2 6:37 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( !;,) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Bi-2 1 4 1729.59 2 .88 4.44 1E+005 5.11E+004 2 . 23 9E+005 l.842E+005 1 764.49 15.30 1.732E+005 2 .185E+005 7.938E+004 1847.43 2 .03 5.812E+005 -5.495E+004 2 .348E+005

 >                2118.51       1. 16    O.OOOE+OOO                     O.OOOE+OOO     O.OOOE+OOO Pb-214       241.99      7.25     2.604E+005     5.42E+004      1. 5 14E+005    1.246E+005 2 95.22   18.4 2     9.707E+004                     6. 2 90E+004   4.612E+004 351. 93   35.6 0     5.423E+004                    2 .349E+004     2 .575E+004 785.96      1. 06    1.582E+006                    l.043E+006      7.228E+005 Pb214-XR       74.82     5.80     4. 2 78E+005   2.3 6E+005     7.985E+005      2 . 084E+005

77. 11 9.70 2 . 3 62E+005 1.391E+005 1.148E+005 87.35 2 .24 1. 025E+006 8. 2 94E+005 4.984E+005 89.78 0.82 2 .665E+006 - 7.965E+005 l. 2 94E+006 Ra-226 186. 2 1 3 .64 4.734E+005 4.73E+005 2 .310E+005 2.269E+005 Ac-228 12 9.07 2 .4 2 7 . 639E+005 8. 2 0E+004 1.658E+005 3.685E+005 2 0 9.25 3 .89 4.165E+005 1.963E+005 l.986E+005 270.24 3 . 46 5 .167E+005 1.858E+005 2 .460E+005 328.00 2 .95 5.060E+005 l.582E+005 2.371E+005 338.32 11. 27 1.489E+005 l.923E+004 7.0 2 0E+004 409.46 1. 92 7 . 468E+005 -6.792E+005 3.460E+005 463.00 4.40 3.611E+005 1 .407E+005 l .678E+005 794.95 4. 2 5 3.919E+005 8.505E+004 1 .788E+005 911.20 25.80 8.201E+004 2 .858E+004 3.800E+004 964.77 4.99 3.796E+005 2 .586E+005 l.738E+005 968.97 15.80 l.145E+005 - 2 . 804E+003 5 . 2 1 9E+004 1 588. 2 0 3.2 2 5.063E+005 3 .800E+005 2.2 1 0E+005 Pa-231 27.36 10.3 0 6.133E+004 6.13E+004 l.787E+004 2.758E+004 2 83.69 1. 70 9.032E+005 -3 .093E+005 4.2 5 9E+005 3 00 . 0 7 2.47 6.617E+005 - 1 .989E+005 3. 1 2 7E+005 30::2. 65 2.20 6.516E+005 - 5.734E+005 3. 053E+005 330.06 1. 40 9.933E+005 -6.269E+005 4.630E+005 Th-234 92.38 2.13 9.779E+005 9.78E+0 05 8. 2 87E+003 4.740E+005 92.8 0 2.10 9 . 877E+005 1.649E+005 4.787E+005 112.81 0.2 1 9.177E+006 8.146E+006 4.4 3 6E+006 U-235 143.76 10.96 l . 604E+005 3.02E+004 3 .348E+004 7.720E+004 163.33 5.08 3.193E+005 8.785E+004 l.529E+005 1 85.71 57. 2 0 3 .024E+004 2 .085E+004 l.450E+004 2 02 .11 1. 08 l.460E+006 -1.558E+005 6.959E+005 205.31 5.01 3. 1 3 9E+005 -8.633E+004 1.495E+005 Am-241 59.54 35.90 4.240E+004 4. 24 E+004 -1.855E+004 2.032E+004

    +     Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ Half-l ife too short to be able to perform the decay correction

[167]

*************************1    *************************         ' ****************
****         G A MMA      S P E C T R U M       A N A L Y S I S                *****
.lename: 54 52 iport Generated On                 4/18/2016      1:0 2 :59 PM tmple  Title                        B306100AFRFC013GD tmple  Description                  TB 560 tmple  Identification tmple  Type tmple  Geometry iak Locate Threshold                 3 .00

!ak Locate Range (in channels) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Si ze 1.000E+OOO SQM tmpl e Taken On

quisition Started 4/18/2016 12:5 2 :57 PM

.ve Time 600.0 seconds !al Time 601.l seconds iad Time 0.18 % Energy Calibration Used Done On 1/1 3/ 2015 Efficiency Calibration Used Done On 4/14 /2 016 Efficiency ID TBFLOOR Ua.ttA. 'Jo.li'da1eo/ by G)~~ IJ-C.~li 0'110 [168]

iak Analysis Report 4/18/ 2 016 1: 0 2 :59 P1 Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B306 10 0AFRFC 0 13GD Peak Analysis Performed on: 4/18/2016 1 :0 2 :59 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV) Area Uncert. Counts 1 1 13- 119 115.84 28.55 0.47 1.83E+001 1 7.49 2.27E+001 2 2 93- 306 301.51 75.03 0.7 1 1.39E+00 2 53.83 2.12E+00 2 3 1129- 11 39 1134.01 2 83.40 0.41 1.22E+001 18.24 2.88E+001 4 1 401- 14 1 3 1406.83 3 51.68 0. 99 4.43E+001 2 2.28 2.97E+00 1 5 232 6- 2336 2 331. 1 9 58 2 .96 1. 0 6 1.93E+001 14.44 1.38E+001 6 2 42 9- 2444 2 435.84 609.14 1. 22 6.62E+001 19.53 9.76E+OOO 7 5830- 585 1 5841.30 1460.59 0.65 1.68E+002 2 8.17 8.19E+OOO

=  First peak in a mul tiplet region
=  Other peak in a mul tiplet region
=  Fitted singlet

rors quoted at 2. 000 sigma

[169]

1terference Corrected Acti ty Report 4/18/ 2 01 6 l , 2: 59 PM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFRFC013GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( i;;) (pCi/SQM ) Uncertainty K-40 1. 000 1460.82* 10.66 1.14418E+006 2.16272E+005 31.83 fva II~ 203 0.972 279.20* 81. 56 4.8:20801!:+003 7. 25476E t GOY. t.F ,1.0 s~t/- Tl-208 1. 000 583. 1 9* 85.00 1.05050E+004 7.97879E+00 3 Bi-211 0.999 351. 0 7* 1 3.02 1 .22277E+00 5 6.45974E+004 ~,i.,f../1# Th- 23 1 0.878 25.64* 1 4.10 3 .07689E+004 3.03250E+004

84. 2 1

• 6.60 4.99454E+005 2 . 2 6070E+005 89.95 1. 00

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :        10.000 keV Nuclide confidence index threshold=                 0.3 0 Errors quoted at 2 .000 sigma

[170]

1terference Corrected Act i ty Report 4/ 1 8/20 1 6 1 .,2 : 59 PM Page 4 ' *** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 1.144184E+006 2.162718E+005 II~ 203 0.972 4.820804E1003 7.254764E1003 Tl-208 1. 000 1.050497E+004 7.978790E+00 3 Bi-211 0.999 1 .222770E+005 6.459741E+004 X Pa-231 0.515 Th-231 0.878 3.9 0 5311E+004 3 .005580E+004

       ? = Nuclide i s part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at         2 . 000 sigma
  ********'**       U N I D E N T I F I E D          P E A K S      *********

• Peak Loca t e Performed on: 4/18/2016 1:02:59 PM Peak Locate From Channel: 85 Peak Locate To Channel: 81 92 Peak Energy Peak Size in Peak CPS Peak Tol.

No . ( keV) Counts per Second ~~ Uncertainty Type Nu clide 6 609.14 1.1041E-001 2 9.49 Sum M = First peak in a multiplet region m Other peak in a multiplet region F Fitted singlet Errors quoted at 2 .000 s igma [171]

iclide MDA Report 4/18/20ll 1 :0 2 :59 PM Page 5 "*** N U C L I D E M D A R E P O R T *****

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • ~************************

Detector Name: 5452 Sample Geometry: Sample

Title:

B306100AFRFC013GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Leve l Name ( keV) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM )

+      K-40       1460.82*    10 .66    1 .426E+00 5    1.43E+005 l.144E+006           6.207E+004 Cr-51        32 0.08      9.91   1.638E+00 5     1.64E+005 1. 2 03E+005         7.722E+004 Mn-54        834.85    99.98     1.805E+004      1.81E+004 2 .976E+003          8.284E+00 3 Co-58        810.76    99.45     1.536E+004      1 .54E+004 -1.912E+004         6.944E+00 3 Co-60      1173. 2 3   99.85     1.654E+004      1. 2 0E+004 -7.433E+00 2       7. 393 E+00 3 1332.49     99.98     1.201E+004                   - 7.841E+00 3     5.071E+00 3 Nb- 94       702.65    99.81     1.496E+004      1.50E+004 -6 .240E+002         6.794E+00 3 871. 0 9  99.89     1 .532E+004                  -3 .755E+002      6.903E+003 Sn- 1 13     255.13      2 .11   7.105E+005      2 .35E+004 -2 .526E+004        3.356E+005 391. 70   64.97     2 . 3 53E+004                  4.151E+003      1.097E+004 Cs- 1 34     475 . 36    1. 48   1.055E+006      1.97E+004 -6. 2 57E+005        4.892E+005 563.25      8. 3 4  1.836E+005                   -1.103E+004       8.438E+004 569.33    15.37     9.798E+004                     6.162E+004      4.496E+004 604.72    97.62     2 .302E+004                  - 5.436E+00 3    1 .085E+004 795.86    85.46    1.974E+004                      9.490E+003      9.017E+003 801. 95     8.69   1.776E+005                    -6.4 8 7E+004    8.040E+004 1038.61       0 .99  1.315E+006                      3.046E+005     5.741E+005 1167.97       1. 79  1.077E+006                      5.591E+005     4.898E+005 1365. 1 9     3.02   4.361E+005                      l.207E+005     l.867E+005 Cs-137        661. 66   85. 1 0  2.282E+004       2.28E+004 2 .643E+004         1.063E+004 Eu-1 52       121.78    2 8.67   6.458E+004       5.82E+004 -1.311E+004         3 .117E+004 244.7 0     7.61   2.250E+005                   -1.919E+005       1.072E+005 295.94      0 .45  4.221E+006                      3 .130E+006    2 .011E+006 344.28    2 6.60   5.822E+004                   - 1.152E+004      2 .730E+004 367.79      0 .86  1.801E+006                      7.114E+00 3    8 . 426E+005 411.1 2     2.24   7.296E+005                      5.566E+004     3 .412E+005 443.96      2 .83  5.044E+005                      3.575E+003     2 . 32 9E+005 488.68      0.42   3 .464E+006                  -1.011E+006       1.595E+006 563.99       0.49   3 .086E+006                    2 .842E+005     1.417E+006 586. 2 6     0.46   3 .887E+006                    1.585E+004      1.807E+006 678. 62    0.47    3.071E+006                     1.687E+006      1.392E+006 688.67     0.86    1. 62 5E+006                   7.1 1 5E+004    7.333E+005 719.35      0.28    5.701E+006                   - 3.404E+005      2 .602E+006 778.90    12.96     l .289E+005                    3.309E+004      5.888E+004 8 10 .45    0.32    4.830E+006                   - 5.610E+006      2 .187E+006 867.37      4.26    3.468E+005                     4.744E+0 0 4    1.557E+005 919.33      0.43    3.906E+006                   -5.656E+0 0 5     1.771E+006 964.08    14.65     1. 2 16E+00 5                -5.660E+0 0 4     5.536E+004 1085.87     10.24     1.495E+005                   -2.992E+004       6.649E+004 1089.74       1. 73   8.496E+005                   -2.891E+005       3.759E+005 1 112.07    13.69     1. 3 00E+005                 -1.092E+005       5.875E+004 1212.95       1. 43   1.155E+006                     5.650E+00 5     5.150E+005

[172]

tclide MDA Report 4/18/ 2 01 t 1:02:59 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (% ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM) Eu- 1 52 1249.94 0.19 9.658E+00 6 5 .82E+004 - 2 .405E+006 4.351E+006 1299.14 1.6 3 7.885E+00 5 -7 . 33 1E+004 3.376E+005 1408.01 21. 07 7.392E+004 1.098E+004 3.239E+004 1457.64 0.50 9.696E+006 2 .771E+007 4.653E+006 1528.10 0.28 4.615E+006 2 .649E+006 1. 94 9E+006 Eu-154 1 23 .07 40.40 4.530E+004 4.53E+004 - 2 .778E+004 2 .185E+004 2 47.93 6.89 2 .386E+005 1.859E+005 l.134E+005 591.76 4.95 3 . 23 4E+005 -1.847E+004 l.489E+005 692.42 1. 78 8. 2 33E+005 7.382E+005 3 .733E+005 723.30 20.06 8. 2 38E+004 4.486E+004 3 .772E+004 756.80 4.52 3 . 3 72E+005 -2 .033E+004 1.529E+005 873. 1 8 1 2 .08 1.403E+005 1.349E+005 6.389E+004 996.29 10.48 1.6 1 0E+005 5.584E+004 7. 2 79E+004 1 004.76 18.01 9.688E+004 1 .794E+004 4. 3 92E+004 1274.43 3 4.80 4.848E+004 -8.720E+003 2 .162E+004 1 596.48 1. 80 6.774E+005 -2. 668E+005 2 .809E+00 5 Eu- 1 55 45.30 1. 31 9.608E+00 5 7.55E+004 -3.582E+005 4.559E+005 60.01 1. 22 l.469E+00 6 2 .636E+005 7 .083E+005 86.55 30.70 7.554E+004 5.070E+004 3 .672E+004 1 05.31 2 1. 10 9. 1 85E+004 -3.979E+004 4.441E+004

+     Tl-208       583.19*    85.00    1.177E+004     l.18E+004 1.050E+004          5.145E+003
+-    Bi-21 1      351.07*    13. 0 2  8.863E+004     8.86E+004 1. 22 3E+005        4.058E+004 Pb- 211      404.85       3 .78  4. 2 56E+005   4. 2 6E+005 1.117E+004        1.990E+005 427.09       1. 76  9.070E+005                     4.610E+005    4. 23 0E+005 83 2 . 0 1   3 . 52 4.771E+005                   - 1.058E+005    2 .175E+005 Bi -2 12       3 9.86     1. 06  1.128E+006     2 .43E+0 0 5 3 .583E+005      5. 33 7E+005 727.33       6.67   2 .426E+005                    7.704E+004    l.109E+005 785.37       1.10   l. 52 1E+006                   4. 2 60E+005  6.950E+005 1620.50        1. 4 7 7.909E+005                     1. 3 7 )E+005 3. 2 42E+005 Pb-212       1 15.18      0.60   3 . 2 95E+006  4.47E+004 1.8 2 9E+006        l .594E+006 238.63     43.60    4.466E+004                     5.109E+004    2 .141E+004 300.09       3.30   4.906E+005                   - l.063E+006    2 .317E+005 Pb212-XR       74.82    10. 2 8  2.512E+005     1. 3 9E+005 6.416E+005        l. 2 25E+005

77. 11 17.10 1.386E+005 -1.677E+0 0 4 6.742E+004 87.35 3 .97 5.835E+005 5.922E+005 2 .836E+00 5 89.78 1. 46 1.526E+006 -9.377E+005 7.410E+005 Bi-214 609.32 45.49 5 .008E+004 5 . 01 E+00 4 6.196E+004 2 . 3 63E+004 768.36 4.89 3 . 2 66E+005 -3.511E+005 l.487E+005 806.18 1. 2 6 l. 2 76E+006 4. 1 82E+005 5.801E+005 934.06 3 . 11 5.498E+005 2.843E+005 2 .496E+00 5 1 12 0 . 2 9 1 4.92 l.333E+005 4.760E+004 6.089E+004 1 155. 2 1 1. 63 1.143E+006 4.921E+003 5 .181E+005 12 3 8. 1 2 5.83 3 . 62 0E+005 1.425E+005 1.656E+005 1280.98 1. 43 1.1 5 6E+006 - 9.075E+005 5.144E+005 1377.67 3.99 4.322E+005 2 .615E+005 1 . 922 E+005 1385.31 0.79 1.895E+006 - 2. 5 97E+005 8. 2 72E+005 1 40 1. 52 1. 33 1. 1 37E+006 8.537E+005 4.965E+005 1407.99 2 .39 6.506E+005 9.660E+004 2 .851E+005 1509.21 2 .13 4.181E+005 1 . 3 92E+005 1 .620E+005 1661.27 1. 05 9.017E+005 -8.446E+005 3 .493E+005

[173]

tclide MDA Report 4/18/ 2 01- 1:0 2 :59 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM) Bi-2 14 1729.59 2 .88 4. 2 03E+005 5.01E+004 1.959E+005 1.723E+005 1764.49 15.30 1. 4 79E+005 1.545E+005 6.676E+004 1847.43 2 .0 3 6.867E+005 - 3.892E+005 2 .876E+005

  >              2 118.51       1.1 6   O.OOOE+OOO                   O.OOOE+OOO   O.OOOE+OOO Pb- 2 1 4    2 41.99      7.25    2 .669E+005   5.61E+004      1.436E+005 1. 2 79E+005 2 95. 22   1 8.42    1.022E+005                   4.243E+004 4.867E+004 351. 93   35.60      5.613E+004                   8.361E+004 2 .670E+004 78 5 .96     1. 06   1 .601E+006                  1.052E+006 7.323E+005 Pb214-XR       74.8 2     5.80    4.452E+005    2 .44E+005     1.137E+006 2 .171E+005

77. 1 1 9.70 2 .443E+005 -2 .956E+004 1.188E+005 87.35 2 . 24 1.034E+006 1 .050E+006 5.027E+005 89.78 0.82 2 .717E+006 -l.670E+006 l. 319E+006 Ra-2 2 6 1 86.21 3.64 4.928E+005 4.93E+005 2 .187E+005 2.3 66E+005 Ac-228 129.07 2 .4 2 7.739E+005 7.22 E+004 4.161E+005 3 .7 3 5E+005 209.25 3 .89 4.485E+005 1.666E+005 2 .146E+005 270.24 3. 46 4.728E+005 -2 .549E+005 2 . 2 41E+005 328.00 2 .95 4.965E+005 9.934E+004 2.323E+005 338. 32 11.27 1.481E+005 9.977E+004 6.982E+004 409.46 1. 92 8.483E+00 5 6.635E+004 3.968E+005 463.00 4.40 3.375E+005 - 1.586E+005 1.561E+005 794 . 95 4.25 4.014E+005 1 .959E+005 1.836E+005 91 1. 2 0 25.80 7.223E+004 - 7.226E+004 3.311E+004 964.77 4.99 3.663E+005 -4.861E+004 1.672E+005 968.97 15.80 1.306E+005 1.337E+005 6.026E+004 1 588.20 3 . 22 4. 62 7E+005 1.265E+005 1.992E+005 Pa-231 27.36* 10.3 0 6.405E+004 6.41E+004 4. 2 12E+004 2.891E+004 283.69* 1. 70 5.773E+005 2.313E+005 2.630E+005 300.07 2 .47 6.554E+005 -1.421E+006 3.095E+005 302.65 2 . 20 6.987E+005 -4.054E+005 3.288E+005 330. 0 6 1. 40 9.860E+005 -8.271E+005 4.593E+005 Th-234 92.38 2 .13 1.014E+006 1.01E+006 -1.701E+005 4.9 1 9E+005 92 . 80 2 .10 1.028E+006 3.538E+005 4.989E+005 112.81 0.2 1 9.277E+006 3.115E+006 4.485E+006 U-235 1 43.76 10.96 1.632E+005 3.12E+004 6.748E+004 7.858E+004 1 63.33 5.08 3.236E+005 -2.563E+005 1.551E+005 185.71 57. 2 0 3.117E+004 9.474E+00 3 1.496E+004 202. 11 1. 08 1.629E+006 7.746E+005 7.803E+005 2 05.31 5.0 1 3 .460E+005 - 2 .987E+005 1.656E+005 Am-241 59.54 35.90 4.964E+004 4.96E+004 2 .438E+004 2 .392E+004

    + = Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    >= Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been c alculated
    @ = Half-life too short to be able to perfo rm the decay correction

[174]

****        G A MMA      S P E C T R U M          A N A L Y S I S                 *****

.lename: 5452 !port Generated On 4/19/2016 9:17:53 AM tmple Title B306100AFRFC014GD tmple Description TB 580 tmple Identification tmple Type tmple Geometry !ak Locate Threshold 3.00 !ak Locate Range (in channels ) 85 - 8 1 92 iak Area Range (in channels) 85 - 8 1 92 lentification Energy Tolerance 10.000 keV tmple Size 1 .000E+OOO SQM tmple Taken On

quisition Started 4/19/2016 9: 0 7:51 AM

.ve Time 60 0 . 0 seconds ial Time 60 0 .7 seconds iad Time 0. 12 ~ Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBFLOOR l) cA\~ io.\\da}eJ by

                                                                   ~c4
                                                                   /J - tl, - /t 0 '{,JO

[175]

iak Analysis Report 4/19/ 2 01 6 9:17:53 A. Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B3061 00AFRFC014GD Peak Analysis Performed on: 4/19/2016 9: 1 7:5 3 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV) Area Uncert. Counts 1 297- 309 301. 4 6 75.02 0.61 7.50E+001 3 8.48 1.11E+002 2 14 01- 1414 1407. 2 7 351.79 0.69 5.05E+001 2 0.96 2 .15E+001 3 2429- 2 441 2 435. 2 3 6 0 8.99 1.14 4.43E+001 16.75 9.75E+OOO 4 5831- 5 849 5839.99 1 460.26 0.87 9.98E+001 2 4.84 1.62E+001

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 . 000 sigma

[176]

1terference Corrected Acti Lt y Report 4/ 1 9/20 1 6 :; 1 7:53 AM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFRFC014GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K-40 1. 000 1460.82* 10 .66 6.80229E+005 1. 7 934 7E+005 Bi -2 11 0. 999 351. 07* 1 3.02 1.39532E+005 6.2 0 892E+004

       *=Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold             0.3 0 Errors quoted at 2.000 sigma

[177]

1terference Corrected Acti _ty Report 4/19/2016 S .L7: 53 AM Page 4 "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 6.802293E+005 1. 793470E+005 Bi-211 0.999 1.395324E+005 6.208922E+004

     ?     Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2.000 sigma
 **********      U N I D E N T I F I E D         P E A K S      **********

Peak Locate Performed on: 4/19/2016 9:17:53 AM Peak Locate From Channel: 85 Peak Locate To rh~nnPl

• 8192 Pea k Energy Peak Si z e in Peak CPS Peak Tol.

No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 75.02 1. 2502E- 001 51. 3 0 Tol. Pb214-XR Ba-133 Pb212-XR Pb212-XR Pb214-XR 3 608.99 7 .3 750E-00 2 3 7.84 Tol. Zr-97 Sb-125 Sb-125 Cs-134 Bi -2 14 M = First peak in a multiplet region m Other peak in a multiplet region F Fitted singlet Errors quoted at 2 .000 sigma [178]

1clide MDA Report 4/19/20lt, 9:17:53 AM Page 5 "*** N U C L I D E M D A R E P O R T ***** Detector Name: 545 2 Sample Geometry: Sample

Title:

B306100AFRFC014GD Nuclide Librar 11 Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( ~) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM)

+      K-40       1460.8 2

• 10.66 1.840E+005 1.84E+005 6.802E+005 8. 2 77E+004 Cr-51 320.08 9.91 1.232E+005 1. 2 3E+005 -6.845E+004 5.693E+004 Mn-54 834.85 99.98 1.171E+004 1.17E+004 -4.121E+003 5. 11 3E+003 Co-58 810.76 99.45 1. 28 1E+004 1. 28E+004 -9.537E+001 5.670E+003 Co-60 117 3 . 23 99.85 1.130E+004 1.13E+004 1.687E+003 4.772E+003 1 33 2 .49 99.98 1.343E+004 8.961E+003 5.782E+003 Nb-94 70 2 .65 99.8 1 1.195E+004 1. 2 0E+004 - 1.385E+003 5.289E+003 871. 09 99.89 1. 2 59E+004 2.181E+003 5.535E+003 Sn-11 3 255.13 2.11 6.539E+005 1.90E+004 -8.600E+004 3 .073E+005 391.70 64.97 1.901E+004 - 2 .055E+003 8.715E+003 Cs- 1 3 4 475.36 1. 48 9.111E+005 l.69E+004 3.991E+005 4.172E+005 563. 2 5 8.34 1.394E+005 l .276E+004 6. 2 32E+004 569.33 1 5.37 8.655E+004 -1.510E+004 3.924E+004 604.72 97.62 2 .041E+004 -1.671E+004 9.550E+00 3 795.86 85.46 1.690E+004 3.022E+003 7.601E+00 3 801. 95 8.69 1.359E+005 - 1.751E+005 5.954E+004 1038.61 0.99 1.161E+006 - 4.627E+004 4.972E+005 1167.97 1. 79 6.549E+005 - 1. 2 05E+006 2 .786E+005 1365.19 3.02 4.5 1 3E+005 -3 . 3 59E+005 l .943E+005 Cs - 1 37 661. 66 85.10 1.731E+004 1.73E+004 -9.836E+00 3 7.869E+00 3 Eu - 1 52 121.78 28.67 4.830E+004 4.7 2 E+004 -9.812E+00 3 2 .303E+004 244.70 7.6 1 1 .815E+005 -6 .003E+004 8.542E+004 295.94 0.45 3. 2 61E+00 6 8.462E+005 1.531E+006 344.28 2 6.60 4.718E+004 -3.343E+004 2 .178E+004 367.79 0.86 1.403E+006 4.322E+005 6 . 43 6E+005 411.12 2.24 6.255E+005 -1. 2 60E+005 2 .892E+005 443.96 2.83 4.595E+005 1 .537E+005 2 .104E+005 488.68 0.42 3.429E+006 2.556E+006 1 .578E+006 563.99 0.49 2.369E+006 1.278E+006 1 .059E+006 586. 2 6 0.46 3.567E+006 l.027E+006 1.647E+006 678. 62 0.47 2 .375E+006 1. 2 49E+005 1.044E+006 688.67 0.86 1 .574E+006 9. 2 19E+005 7.076E+005 719.35 0. 2 8 5. 2 61E+006 2.194E+005 2 .382E+006 778.90 12 .96 1. 04 7E+005 -3.182E+004 4.679E+004 810.45 0. 32 3.969E+006 -1.561E+005 1.756E+006 867.37 4. 2 6 3. 2 83E+005 3.018E+005 1.464E+005 919.33 0.43 3.617E+006 3.633E+006 1. 62 7E+006 964.08 1 4.65 1 .117E+005 9.903E+004 5.039E+004 1085.87 10.24 1.263E+005 - 5.566E+004 5.491E+004 1089.74 1. 73 8.682E+005 2 .981E+005 3 .8 52 E+005 1112.07 13.69 9.556E+004 -2 . 2 32E+005 4.154E+004 1212.95 1. 43 1.109E+006 -2 .803E+004 4.921E+005

[179]

4/19/20 h 9:17:5 3 AM Page 6 1clide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activit y Dec. Level Name ( keV} ( %} (pCi/SQM} (pCi/SQM ) (pCi/SQM ) (pCi/SQM) Eu-152 1 249.94 0.19 6.886E+006 4.72E+004 - 8.836E+004 2 .965E+006 1299.14 1. 6 3 7.598E+005 1.361E+00 5 3. 2 32E+005 14 0 8.01 21. 07 6.579E+004 1.240E+004 2 .833E+004 1457.64 0.50 7.959E+006 1.765E+007 3 .784E+006 1528.10 0. 2 8 2 .852E+006 -2. 164E+006 l.067E+006 Eu - 1 54 123.07 40.40 3 .432E+004 3.43E+004 -1.440E+004 1.636E+004 247.93 6.89 2 .029E+005 -7.441E+004 9.552E+004 591.76 4.95 2 .495E+005 5.664E+004 l. 1 2 0E+005 692.42 1. 78 7.751E+005 -1.844E+005 3 .492E+005 723.30 2 0.06 7. 2 27E+004 -2.692E+003 3. 2 67E+004 756.80 4.5 2 2 .850E+005 -6.970E+004 1. 2 68E+005 873.18 12 .08 1 . 1 15E+005 4.598E+004 4.949E+004 996. 2 9 10.48 1.250E+005 -1.915E+004 5.479E+004 1 004.76 18 . 01 8.351E+004 -5.155E+004 3.724E+004 1274.4 3 3 4.80 3 .775E+004 -1.453E+003 1.625E+004 1 596.48 1. 80 6.02 1E+005 2 .562E+005 2 .433E+005 Eu-155 45.30 1. 31 6.965E+005 5.36E+004 -2 .016E+005 3 . 2 37E+005 60.01 1. 22 9.394E+005 2 .432E+003 4.434E+005 86.55 30.70 5.359E+004 4.486E+004 2 .575E+004 105.31 21.10 6.841E+004 -1.065E+004 3. 2 68E+004 Tl -2 08 583.19 85.00 1 .925E+004 1 .93E+004 9.961E+003 8.888E+003

+     Bi-2 11      351.07*   13 . 02  7 . 743E+004   7 , 74E+004 1 . 395E+005    3 . 498E+004 Pb-211       404.85      3.78   3 .432E+005    3. 2 3E+005 - 4.856E +004   1.578E+005 427.09      1. 76  7.491E+005                 - 5.844E+005    3.440E+005 832.01      3.5 2  3.229E+005                 - 5.843E+004    1.404E+0 05 Bi -2 1 2      39.86     1. 06  7.357E+005     1.90E+005 -3.134E+005       3.376E+005 727.33      6.67   1 .896E+005                -1.809E+005     8.435E+004 785.37      1.10   1.427E+006                   4.604E+005    6.477E+005 1620.5 0      1. 4 7 4.891E+005                 -7.900E+004     1.733E+005 Pb- 212      115.18      0.60   2 .516E+006    3.67E+004 1.676E+006        1.204E+006 238.63    43.60    3 . 670E+004                 1.689E+004    1.743E+004 3 00.09     3.30   3.928E+005                 - 5.902E+005    1 .828E+005 Pb212-XR       74.82   10. 2 8  1 .957E+005    1.06E+005 4.4 3 8E+0 0 5    9.471E+004 77.11   17.10    1 .059E+005                -4.391E+0 0 4   5.105E+004 87.35     3.97   4. 2 40E+005                 4.673E+0 0 5  2 .039E+00 5 89.78     1. 46  1.156E+006                   4.328E+0 0 5  5.558E+005 Bi-214       609.32    45.49    4.161E+004     4.16E+004 4.644E+0 0 4      1.939E+004 7 68.36     4 . 89 2 .755E+005                  1.587E+005    l. 2 31E+005 806. 1 8    1. 2 6 9.361E+005                   4.446E+005    4. 1 02E+005 934. 0 6    3 .11  5.0 2 1E+005                 3.917E+005    2 . 25 8E+005 112 0 . 2 9 14.92    1. 2 84E+005                 6.262E+004    5.843E+004 1155. 2 1     1. 63  9.459E+005                 -7.696E+0 0 5   4.197E+005 1238.1 2      5.83   2 .558E+005                -7.788E+0 0 4   1 . 1 2 5E+005 1280.98       1. 43  9.771E+005                   5.893E+004    4. 2 48E+005 1377.67       3.99   3.756E+005                   3 .964E+004   1.6 3 9E+005 1385.31       0 .79  1.732E+006                   6.154E+005    7.456E+005 1401. 52      1. 33  1.106E+006                   6.670E+004    4.808E+005 1407.99       2.39   5.790E+005                   1.092E+005    2 .493E+005 1509. 2 1     2 . 13 6.314E+005                   3 .8 2 9E+005 2 .686E+005 1661. 2 7     1. 0 5 1.059E+00 6                -1.314E+005     4. 2 78E+005

[180]

1clide MDA Report 4/19/ 2 011_ 9:17:53 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) (pCi/SQM) Bi -2 14 1729.59 2 .88 3 .013E+005 4.16E+004 8. 3 97E+004 1.128E+005 1764.49 15.3 0 1.359E+005 8.427E+004 6.073E+004 1847.43 2 .03 5.40 2E +005 -8.654E+004 2 .144E+005

 >                 2118.51      1.16   O.OOOE+OOO                    O.OOOE+OOO     O.OOOE+OOO Pb- 2 14     241.99      7.25   2.223E+005     5. 02E+004     1.4 1 8E+00 5  1.056E+00 5 295.22    18.42    8.106E+004                    4.858E+004     3.811E+004 351.93    35.60    5.021E+004                    5 .777E+004    2.374E+004 785.96      1. 06  1.463E+006                    1.488E+005     6.633E+005 Pb2 1 4-XR      74.82    5.80    3 .468E+005    1.87E+005      7.866E+005     1.679E+005 77.11     9.70  1.866E+005                   -7.741E+004      9.000E+004

87. 3 5 2 . 24 7.515E+005 8.282E+005 3 .614E+005 89.78 0.82 2 .057E+006 7.706E+005 9.895E+00 5 Ra-226 1 86. 2 1 3. 64 3.533E+005 3 .53E+005 9.915E+004 1.669E+005 Ac-228 129.07 2 .4 2 5.853E+005 7.99E+004 -1.359E+005 2 .793E+005 209.25 3.89 3.547E+005 - 6.923E+004 1.677E+005 27 0 .24 3.46 3.840E+005 - 3.822E+005 1. 7 97E+00 5 328. 00 2.95 4.489E+005 2 .778E+005 2 .085E+005 338.32 11. 2 7 1. 2 85E+005 4.668E+004 6.002E+ 0 04 409.46 1. 92 6.795E+005 -3 .983E+005 3.123E+005 463. 00 4.40 3.053E+005 6.673E+004 1.399E+005 794.95 4.25 3.453E+005 -7.357E+004 1.556E+005 911. 2 0 25.80 7 . 986E+004 1.134E+005 3 .693E+0 0 4 964.77 4.99 3. 2 80E + 005 1.979E+005 1.480E+005 968.97 15.80 1.054E+005 6.387E+004 4.764E+004 1588.2 0 3 . 22 3.567E+005 - 5.768E+00 4 1.462E+005 Pa- 23 1 2 7.36 10.30 7.318E+004 7. 32E+004 5.195E+004 3 . 3 47E+004 28 3 .69 1. 70 8.008E+005 3.681E+005 3 .747E+005 300. 07 2 .47 5.248E+005 -7.884E+005 2 .442E+005 302.65 2 . 20 5.687E+005 -5.458E+005 2. 638E+005 330. 0 6 1. 40 9.019E+005 -5.836E+004 4 . 1 73E+005 Th-2 34 92.38 2 .13 7. 2 19E+005 7. 2 2E+005 -7.783E+004 3.459E+005 92.8 0 2 .10 7.302E+005 7.974E+004 3.498E+005 112.8 1 0 .21 6.937E+006 -8.164E+00 5 3.315E+006 U-235 1 43.76 10 .96 1 .295E+005 2 . 22 E+004 3 . 3 73E+004 6. 17 4E+004 1 63.33 5.08 2 .628E+005 -3 . 3 41E+004 1. 2 47E+005 1 85.71 57. 2 0 2 . 2 24E+004 7. 2 47E+00 3 l.050E+004 20 2 .11 1. 08 1.184E+006 3 .034E+005 5.580E+005 205.31 5.01 2 . 5 99E+005 -8 .288E+004 1. 2 25E+005 Am- 2 41 59.54 35.90 3 .129E+004 3. 1 3E+004 6 .503E+00 3 1. 4 7 5E+004

    +      Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    >= Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Hal f- life too short to be abl e to perform the decay correction

[181]

****        G A MMA      S P E C T R U M        A N A L Y S I S                   *****

.l ename: 5452 iport Generated On 4/18 /2 016 2 : 22 :3 5 PM tmple Title B306100AFQWC009GD tmple Description TB 560 ' 1mple Identification 1mple Type tmple Geometry iak Locate Thre shold 3. 00 iak Locate Range (in channels) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mple Si ze 1.000E+OOO SQM 1mple Taken On

quisition Started 4/18/ 2 016 2 :1 2 : 33 PM

.ve Time 600.0 seconds ial Time 600.5 seconds iad Time 0.08 % Energy Calibration Used Done On 1/1 3 /2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBWALL

                                                                      -P~t6. \Ja\,c\o.\cJ. by o~~

1:,-6,-IYi 0 '116 [182]

iak Analysis Report 4/ 1 8 /2 016 2 : 22 : 35 Pi. Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B306100AFQWC009GD Peak Analysis Performed on: 4/18/2016 2 : 22 :3 4 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV) Area Uncert. Counts 1 1 1 74- 1183 1178.69 294.58 0.49 1.97E+001 17.82 2 .63E+001 2 1401- 1412 1407.05 351.73 0.67 4.05E+001 2 0 .47 2.5 5E+001 3 2 428- 2 443 2436.61 609.33 1. 29 6.89E+001 19.97 1.0lE+OOl 4 5828- 5851 5841.46 1460.63 1. 31 1 .24E+00 2 2 4.45 6.19E+OOO First peak in a multiplet region Other peak in a multiplet region Fitted singlet

rors quoted at 2 .000 sigma

[183]

iterference Corrected Act1 _ty Report 4/18/ 2 016 22:35 PM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFQWC009GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( gc:) (pCi/SQM ) Uncertaint~, K-40 1. 000 1460.82* 10.66 8.44191E+ 005 l.82121E+005 Bi-21 1 0.999 351.07* 13. 0 2 1.11729E+005 5.93298E+004 Pb-21 4 0.778 2 41. 99 7. 2 5 2 95. 22

• 18.42 3.51481E+004 3.23072E+004 351. 93* 35.60 4. 0 86 2 8E+004 2 . 1 6862E+004 785.96 1. 06

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuclide confidence index threshold=               0. 3 0 Errors quoted at 2. 000 sigma

[184]

1terference Corrected Acti ty Report 4/ 1 8/ 2 01 6 :2: 35 PM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 8.441911E+005 1.821208E+005 Bi-211 0.999 l .562543E+004 l.063903E+005 Pb-214 0.778 3.514812E+004 3.230688E+004

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2 . 000 sigma
 **********     U N I D E N T I      F I  E D    P E A K s        **********

Peak Locate Performed on: 4/18/ 2 01 6 2: 22 :34 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Si ze in Peak CPS Peak Tol. No. ( keV) Counts per Second  % Uncertainty Type Nuclide 3 609.33 1.1478E-001 29.0 0 Tol. Zr-97 Sb-125 Sb- 1 25 Cs - 1 34 Bi - 21 4 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted s i nglet Errors quoted at 2 .000 s i gma [185]

~elide MDA Report 4/ 1 8/ 2 0 1 2:22:35 PM Page 5 "*** N U C L I D E MD A R E P O R T ***** Detector Name: 545 2 Sample Geometry: Sample

Title:

B306l00AFQWC009GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) 1460.8 2

• 10 .66 1.321E+005 l.32E+005 8.442E+005 5.680E+004

+      K-40 6.879E+004 Cr-51        32 0. 0 8    9.9 1  1.469E+005     1. 4 7E+005 8.623E+004 Mn-54        83 4.85    99.98    1.375E+004     1.37E+004 8.779E+003          6.130E+003 Co-58        810.76     99.45    1. 2 23E+004   1. 2 2E+004 2.331E+003        5.379E+003 Co-60      117 3 . 23   99.85    1.525E+004     1.53E+004 - 1.250E+004        6.749E+003 1 33 2 .49   99.98    1.584E+004                    8.145E+003     6.990E+003 Nb-94        702.65     99.81    1.296E+004     9.77E+00 3 8.685E+002         5.794E+003 871. 0 9   99.89    9.768E+003                  -1.416E+004      4.125E+003 Sn-113       2 55. 1 3    2 .11  6.576E+005     1.94E+004 2.188E+004          3.092E+005 391. 7 0   64.97    1.943E+004                    5.4 22 E+003   8. 92 5E+003 Cs- 1 34     475.36       1. 48  8.683E+005     1.80E+004 4.261E+005          3.958E+0 0 5 563.25       8.34   l.757E+005                  -3.346E+004      8.045E+004 569.33     15.37    8.777E+004                  -3.382E+0 0 4    3.985E+004 604.72     97. 62   2.33 6E+004                 -1.140E+004      1.103E+004 795.86     85.46    1.799E+004                    1.949E+004     8.145E+003 801. 95      8.69   1. 4 91E+005                -7.153E+004      6.617E+004 1038.61        0 .99  1.451E+006                    9. 1 00E+004   6.4 1 9E+005 1167.97        1. 79  1.002E+006                    2 . 2 1 9E+005 4.523E+005 1 365.19       3.0 2  4.035E+005                  -8.919E+004      1.704E+005 Cs-137       661. 66    85.10    1 .585E+004    1.59E+004 - 1. 746E+004       7.141E+003 Eu - 152     121.78     2 8 . 67 6.001E+004     5.34E+004 1.502E+004          2 .888E+004 244.7 0      7.61   1.938E+005                  -2.609E+005      9.158E+004 295.94       0.45   3 .790E+006                 -3.198E+005      l .795E+006 344.28     2 6.60   5.340E+004                    2 . 3 74E+004  2 .489E+004 367.79       0.86   1 .628E+006                 -1.999E+006      7.563E+005 411 .12      2.24   6.478E+005                  - 1.508E+005     3.003E+005 443.96       2.83   4.900E+005                  - 6.679E+005     2 . 2 56E+005 488.68       0.42   3.096E+006                    5.912E+005     1.411E+006 563.99       0.49   2.951E+006                  -2 .466E+005     1.350E+006 586.26       0 . 46 3. 2 49E+006                  9.354E+005     1.488E+006 678.62       0.47   2 .937E+006                 - 1.075E+006     1 .326E+006 688.67       0 . 86 1 .650E+006                   1.098E+006     7.458E+005 719.35       0.28   5.771E+006                    3 .111E+006    2 .637E+006 778.90     12.96    1.085E+005                  -5 . 2 98E+004   4.870E+004 81 0 .45     0. 32  3.598E+006                    l.899E+005     1.571E+006 867.37       4. 2 6 2. 2 86E+005                - 2. 618E+005    9.654E+004 919.33       0.43   3.850E+006                    1.0 2 1E+006   1.743E+006 964. 0 8   1 4.65   1.117E+005                    6.262E+004     5.039E+004 1085.87      10. 2 4  1. 52 5E+005                -1.523E+004      6.799E+004 1089.74        1. 73  9.040E+005                    6.209E+005     4.03 1E+00 5 1 112.07     13.69    1.108E+005                  -6.076E+004      4.915E+004 1212.95        1. 43  1 .155E+006                   4.501E+005     5.150E+005

[186]

4/18/ 2 01l 2 : 22 :35 PM Page 6 1clide MDA Report Nuclid e Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Eu- 1 52 1249.94 0.19 7.110E+006 5 . 3 4E+004 -2.468E+006 3.077E+006 1299.14 1. 63 7.885E+005 -1.843E+006 3.376E+005 1408.01 21. 07 7.941E+004 4.120E+004 3 .514E+004 1457.64 0.50 8.336E+006 1.885E+00 7 3 .973E+006 1528.10 0.28 4.203E+006 - 1.954E+00 6 1 .743E+006 Eu-154 123.07 40.40 4.200E+004 4. 2 0E+004 1. 3 80E+004 2 .021E+004 247.93 6.89 2 .155E+005 -1. 2 08E+005 1.018E+005 591. 76 4.95 2 .362E+005 -2.134E+005 1.053E+00 5 692.42 1. 78 7.875E+005 2.878E+005 3 .554E+00 5 723.30 20.06 8.695E+004 7.101E+004 4.001E+004 756.80 4.52 3.324E+005 2.479E+005 1.505E+005 873.18 1 2 .08 9.621E+004 1. 509E+004 4.183E+004 996. 2 9 10.48 1.250E+005 -9.081E+004 5.479E+004 1004.76 18.01 8.668E+004 6.088E+004 3 .882E+004 1274.43 34.80 4.557E+004 -2 .907E+00 3 2 .016E+004 1596.48 1. 80 5.597E+005 - 3.949E+005 2 . 22 1E+005 Eu-155 45.30 1. 31 8.491E+005 6.35E+004 5.432E+005 4.003E+005 60.01 1. 22 1.082E+006 2 .568E+004 5 . 1 48E+005 86.55 3 0.70 6.355E+004 4.934E+004 3 .074E+004 105.31 2 1. 10 8.031E+004 -1.760E+004 3 .864E+004 Tl-208 583.19 85.00 1 .813E+004 1.81E+004 1. 22 2E+004 8. 32 7E+003

+     Bi-211       351.07*    13.02    8. 0 34E+004   8.03E+004 1.117E+005         3.643E+004 Pb-211       404.85       3.78   3 .707E+005    3.66E+005 -2 .187E+005       1.715E+005 427.09       1. 76  7.804E+005                    5.194E+005    3.597E+005 83 2 .01     3.5 2  3 .664E+005                 -4. 2 07E+005   1.621E+005 Bi-21 2       3 9.86      1. 06  8.589E+005     2.43E+00 5 -3 .940E+005      3.995E+005 727.33       6.67   2 .4 2 6E+005               -5 .055E+004    1.109E+005 785.37       1.10   1 . 2 59E+006               - 1. 1 55E+006  5.638E+005 1620.50        1. 4 7 8. 3 56E+005                  3 . 2 92E+004 3.466E+005 Pb- 2 1 2    115.18       0.60   2 .781E+006    4.05E+004 8.822E+005         1 . 3 37E+006 238.63     43 .60   4.050E+004                    5.729E+00 4   1 .933E+004 30 0 . 0 9   3.30   4.713E+005                  -1. 22 1E+005   2 . 22 0E+005 Pb21 2 -XR    74.8 2    10. 2 8  2 .132E+005    1 . 1 6E+005 3 .613E+005     1. 0 35E+005

77. 11 17. 1 0 1. 1 65E+005 2. 1 88E+004 5.638E+004 87.35 3.97 4.850E+00 5 2. 2 08E+005 2.345E+005 89.78 1. 4 6 1.238E+00 6 -3.745E+005 5.971E+005 Bi -2 14 609.32 45.49 5.155E+004 5.15E+004 9.010E+004 2 .436E+004 768.36 4.89 3 .266E+005 l .935E+005 1.487E+005 806.18 1. 2 6 9. 11 6E+005 1 .818E+005 3.980E+005 934.06 3.11 5.186E+005 -1.448E+005 2 .340E+005 1120.29 14 .92 1. 2 67E+005 3.609E+004 5.759E+004 1 155.21 1. 63 8.837E+005 - 2 .953E+005 3.886E+005 1238.12 5.83 3.064E+005 9.456E+004 1.378E+005 1280.98 1. 43 1.133E+006 -8.340E+005 5.0 2 6E+005 1 377.67 3.99 3.652E+005 -2.290E+004 1.587E+005 1385.31 0.79 1.612E+006 -1.525E+006 6.858E+005 140 1 .5 2 1. 33 1.335E+006 - 2.337E+005 5.953E+005 1 407.99 2 .39 6.989E+005 3.626E+005 3 .092E+005 1 509. 21 2 .1 3 5.227E+005 2.437E+005 2 .143E+005 1661. 27 1. 05 1 .251E+006 6.757E+005 5. 23 9E+005

[187]

!Slide MDA Report 4/18/201 l 2 : 22 : 35 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi -2 14 1729.59 2 .88 4. 2 03E+005 5.15E+004 - l.100E+005 l.723E+00 5 1764.49 15.30 1. 3 84E+005 4.338E+004 6.199E+004 1847.43 2 .03 6.188E+005 2 .885E+005 2 .536E+OOS 2118.51 1.16 O.OOOE+OOO O. OOOE+OOO O.OOOE+OOO

+      Pb- 2 14      241.99     7. 2 5 2 .421E+005    2.94E+004 2 .064E+005       1.155E+00 5 295. 22

• 18.42 5.021E+004 3 .515E+004 2 . 2 69E+004 351.93* 35 .60 2 .938E+004 4.086E+004 1.332E+004 785.96 1. 06 l.399E+006 5.818E+OOS 6.315E+005 Pb214-XR 74.82 5.80 3 .779E+005 2 .05E+00 5 6.403E+OOS l.835E+005 77.11 9.70 2 .053E+005 3.857E+004 9.939E+004 87.35 2 . 24 8.596E+005 3.914E+005 4.156E+OOS 89.78 0.82 2 . 2 04E+006 -6.669E+005 l.063E+006 Ra- 2 26 186.21 3.64 4.331E+005 4. 3 3E+005 9.412E+004 2 .068E+005 Ac-228 129.07 2.42 6.684E+005 7 .8 4E+004 2 .082E+005 3.208E+005 209. 2 5 3.89 4.0 23 E+005 4. 2 06E+00 5 l.915E+005 270. 2 4 3.46 4. 2 42E+005 1.424E+004 l.998E+005 328.00 2 .95 4.867E+005 9.419E+004 2.274E+005 338.32 11. 27 1. 2 76E+005 2 . 12 0E+004 5.958E+004 409.46 1. 92 7.532E+005 4.050E+005 3.492E+005 463.00 4.40 3.120E+005 -5.942E+004 l.433E+005 794.95 4. 2 5 3.562E+005 3.042E+005 l.610E+005 911. 2 0 25.80 7.840E+004 l. 2 51E+004 3.619E+004 964.77 4.99 3.176E+005 9.505E+004 1.4 2 8E+00 5 968.97 15.80 1.054E+005 2 .031E+004 4.764E+004 1588.20 3. 22 3.768E+005 -2 .360E+005 1.563E+005 Pa- 23 1 27.36 10.30 6 . 133E+004 6.13E+004 3.971E+003 2 .758E+004 2 83.69 1. 70 8.008E+00 5 -2 .972E+005 3 .747E+005 300.07 2 .47 6. 2 96E+00 5 -1.632E+005 2 .966E+005 30 2 .65 2 . 20 6.597E+005 -2 .079E+005 3.094E+005 330.06 1. 40 1.015E+006 3.607E+005 4.737E+005 Th- 23 4 92.38 2 .13 8. 2 64E+005 8. 2 6E+005 -5.060E+005 3.982E+005 92.80 2 .10 8.332E+005 -5 .925E+005 4.014E+005 112.81 0. 2 1 7.907E+006 1.077E+005 3.801E+006 U- 2 35 143.76 10.96 l.447E+005 2 .78E+004 -2 .409E+004 6.932E+004 163.33 5.08 3 .078E+005 6.074E+004 l.472E+005 185.71 57.20 2 .779E+004 8. 63 1E+003 l.327E+004 2 02.11 1. 08 l.420E+006 -7.821E+005 6.757E+005 205.31 5.0 1 3.117E+005 -5.512E+004 l.484E+005 Am-241 59.54 35.90 3.596E+004 3 .60E+004 -1.974E+004 l.709E+004

     +      Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
     > = Calculated MDA is zero due to z ero counts in the region, or the r egion is outside the spectrum, or MDA has not been calculated
     @ =    Half-life   too short to be able to perform the decay correction

[188]

"**** * *******************    ~********************** *

• i *****************

"***          GAMM A      S .I! E C T R U M         A N A L Y ~ I S               *****
.lename : E:\Zion Nuclear\Inspector Shots\B306100ASJWC15GD.CNF iport Generated On                   1/31/2 01 7       1:35: 2 9 PM tmple  Title                         B3061008SJWC15GD tmple  Description                   Clean/Dirty Oil Tank Room tmple   Identification                East Wall 1mpl e  Type tmpl e  Geometry                      3 meter iak Locate Threshold                    3. 00 iak Locate Range (in channels )             85 -   8 1 92 iak Area Range (in channels )               85 -   8 1 92 lentification Energy Tolerance            10.000 keV tmple Size                              1.000E+OOO SQ MET tmple Taken On

quisition Started 1 2 / 22/2 015 2 :34:58 PM

.ve Time 600.0 seconds ial Time 600.5 seconds iad Time 0 .09 % Energy Calibration Used Done On 1/27/2015 Efficiency Calibration Used Done On 1/31/2017 Efficiency ID CRIBHOUSE 3M u~,o. ~ohAa\.e~ lov Q~ ( tz-eo~1y; O'bOO [189]

iak Analysis Report 1 /3 1 /20 1 7 1 :35: 2 9 f Page 2

"***             P E A K        A N A L Y S I S               R E P O R T                *****

Detector Name: 5456 Sample

Title:

B306 100 8S JWC 15GD Peak Analysis Performed on: 1 /31/2017 1:35: 2 9 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV ) Area Uncert. Counts 1 2 97 - 308 301.80 75.18 0.69 8.39E+001 60.43 3.26E+002 2 5 27- 533 5 2 9.95 13 2 . 2 6 0. 33 4. 2 3E+OOO 24.87 7.78E+001 3 1404- 1415 14 0 9.38 352 . 22 0.7 3 5. 3 0E+001 23.92 3.60E+001 4 2433- 2448 2439.06 609.67 0.41 5.68E+001 21. 42 1.92E+001 5 5838- 5859 5847.73 1461. 2 4 1. 56 1.59E+00 2 25.22 O.OOE+OOO First peak in a multiplet region Other peak in a multiplet region

=  Fitted singlet

rors quoted at 2 . 000 sigma

[190]

1terference Corrected Act . ~ty Report 1/31/2017 35 : 29 PM Page 3 "*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sampl e

Title:

B306l008SJWC15GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQ M) Uncertainty K-40 1. 000 1 460.82* 10.66 l.07 62 7E+006 1. 94616E+005 Tc-99m 0.897 1 40.51* 89.00 l.15 52 2E+003 6.79272E+003 Bi- 2 1 1 0.998 3 51.07* 13.02 1. 46183E+005 7.00631E+004

       * = Energy line found in the spectrum .
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :         10.000 keV Nuclide confidence index thre shold =         0. 3 0 Errors quoted at 2 .000 sigma

[191]

1terference Corrected Act . ~ty Report 1/3 1 /2017 35: 2 9 PM Page 4 "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 1. 000 1. 076268E+006 1 .946164E+005 Tc-99m 0.897 l . 1 55223E+003 6.792718E+003 Bi-211 0.998 1.461826E+005 7.006305E+004

        ? = Nuclide is part of an undetermined solution X     Nuclide rejected by the interference analysis
       @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2 .000 sigma
 ** * *******      U N I D E N T I F I E D           P E A K S       **********

Peak Locate Performed on: 1/31/2 017 1:35: 2 9 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nucl ide 1 75.18 1 .3985E- 001 72 . 02 Tol. Pb214-XR Ba- 1 33 Pb2 1 2-XR Pb212-XR Pb21 4 -XR 4 6 09.67 9.4594E-00 2 37.7 4 To l . Zr-97 Sb-125 Sb-125 Cs-134 Bi- 2 14 M = First peak in a multiplet region m = Other peak in a multiplet region F Fitted singlet Errors quoted at 2 . 000 sigma [192]

1clide MDA Report 1 /3 1/ 2 01 1:35: 29 PM Page 5 "*** N U C L I D E MD A R E P O R T ***** Detector Name: 5456 Sample Geometry: 3 meter Sample

Title:

B3061008SJWC15GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name {keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) + K-40 1460.82* 10.66 1.832E+004 1.83E+004 1.076E+006 O.OOOE+OOO Cr-51 32 0.08 9.91 1.712E+005 1.71E+005 1.384E+004 8.092E+004 Mn-54 834.85 99.98 l. 3 97E+004 1.40E+004 -3 .572E+003 6.243E+003 Co-58 810.76 99.45 1.531E+004 1. 53E+004 -1. 41 2E+003 6.919E+003 Co-60 1173. 2 3 99.85 1.649E+004 1.46E+004 4.863E+003 7.370E+003 1332.49 99.98 1.461E+004 7.1 3 4E+003 6.379E+003 Nb-94 702.65 99.81 1.358E+004 1. 3 6E+004 -3.550E+003 6.107E+003 871. 09 99.89 l.601E+004 - 2 .631E+003 7. 2 47E+003 Sn-113 255.13 2 .11 8.505E+005 2.31E+004 1. 209E+005 4.055E+00 5 391. 7 0 64.97 2 . 3 13E+004 -8.282E+003 1.077E+004 Cs-134 475.36 1. 48 1.077E+006 1.79E+004 1.604E+005 5 .001E+005 563.25 8.34 1.917E+005 1.4 6 0E+005 8.852E+004 569.33 15.37 1.139E+005 5.2 3 6E+004 5. 2 96E+004 604.72 97.6 2 1.788E+004 -1.813E+004 8. 2 92E+003 795.86 85.46 2.058E+004 9.618E+003 9.443E+003 801. 95 8.69 1.717E+005 -3.468E+005 7.746E+004 1038.61 0.99 l.348E+006 3.540E+005 5.906E+005 1 167.97 1. 79 9.006E+005 6.252E+005 4.016E+005 1365 .1 9 3.02 3.837E+005 -2.405E+005 1.607E+005 Cs-137 661. 6 6 85.10 1.695E+004 1.69E+004 1.132E+004 7.694E+003 Eu-152 121. 78 28.67 7.323E+004 5.84E+004 4.239E+004 3 .550E+004 244.70 7.61 2 .614E+005 7.329E+004 1.253E+005 295.94 0.45 4.429E+006 2 .860E+006 2 .115E+006 344.28 2 6.60 6.574E+004 - 8.012E+003 3.106E+004 367.79 0.86 2 .097E+006 -2 .139E+005 9.908E+005 411.12 2 . 24 7.462E+005 8.393E+004 3 .496E+005 443.96 2 .8 3 6.010E+005 3.577E+005 2 .812E+005 488.68 0.4 2 3.583E+006 -8.1 1 6E+005 1.655E+006 563.99 0.49 3.227E+006 3 . 92 6E+005 1 .489E+006 586. 2 6 0.46 3.770E+006 1.909E+006 1.749E+006 678. 62 0.47 3.050E+006 2 .889E+005 1.383E+006 688.67 0.86 1.931E+006 -3 . 1 44E+004 8.869E+005 719.35 0. 2 8 5. 2 30E+006 -5 .454E+004 2.368E+006 778.90 12.96 1. 2 36E+005 -5 .708E+004 5. 626E+004 810.45 0. 32 4.742E+006 1.256E+006 2 .143E+006 867.37 4. 26 3.520E+005 1.615E+005 1.583E+005 919.33 0.43 3.843E+006 2 .058E+006 1.740E+006 964.08 14.65 1.362E+005 - 2 .588E+004 6.266E+004 1085.87 10. 2 4 1.429E+005 5 . 2 43E+004 6.324E+004 1089.74 1. 73 8.090E+005 4.540E+005 3 .557E+00 5 1112.07 1 3 .69 1.057E+005 -2.989E+004 4.663E+004 1 212 .95 1. 43 1 .007E+006 -4.944E+005 4.412E+005 [193]

1 /31/2 0 1 1:35:29 PM Page 6 1clide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Eu- 1 52 1249.94 0.19 7. 2 94E+006 5.84E+004 1.455E+006 3 .171E+006 1299. 1 4 1. 63 8.885E+005 4.702E+005 3 .879E+005 1408. 0 1 21. 0 7 5.843E+004 -3.061E+004 2 . 4 68E+004 1457.64 0.50 8.845E+006 -6. 2 32E+006 4. 22 9E+006 1528.10 0. 2 8 2 .440E+006 5.254E+005 8 .643E+005 Eu-15 4 123.07 40.40 4.969E+004 4.22E+004 -1.404E+004 2 .405E+004 247.93 6.89 2 .852E+005 2.136E+005 1. 3 67E+005 591. 76 4.95 2 .301E+005 -2 .734E+005 1.023E+005 692.42 1. 78 9.557E+005 1.636E+00 5 4.397E+005 723.30 20.06 7.805E+004 4.358E+004 3 .558E+004 756.80 4.52 3 . 2 09E+005 -2 .023E+004 1 .448E+005 873. 1 8 1 2 .08 1. 2 45E+005 -1.471E+004 5.599E+004 996. 2 9 10.48 1.454E+005 1. 568E+004 6.499E+004 1004.76 18.01 9.392E+004 4.442E+003 4. 2 45E+004 1274.43 34 . 80 4.222E+004 6.354E+003 1.850E+004 1596.48 1. 8 0 8.768E+005 6.345E+005 3 .812E+005 Eu-155 45. 3 0 1. 31 2 .081E+006 8. 2 1E+004 -3 . 2 79E+004 1.011E+00 6 60.01 1. 22 2 . 3 64E+006 1. 3 67E+006 l .151E+00 6 86.55 30.70 8. 2 08E+004 5.982E+004 4.000E+004 105.31 2 1.10 9.696E+004 -4.521E+004 4.697E+004 Tl -2 08 583. 1 9 85.00 2 .228E+004 2 . 2 3E+004 2 .461E+004 1.041E+004 + Bi -2 11 351. 0 7* 13.0 2 9.360E+004 9. 3 6E+004 1.462E+005 4. 3 07E+004 Pb-2 11 404.85 3 .78 4.946E+005 3.65E+005 -9.720E+003 2 . 33 5E+005 427.09 1. 76 9.542E+005 2 .578E+005 4.467E+005 832.01 3.52 3.652E+005 -2 .815E+005 1.616E+005 Bi- 212 39.86 1. 06 2 .800E+006 2.32E+005 1. 3 96E+006 1. 3 64E+006 727.33 6.67 2 .324E+005 1.338E+005 1 .058E+00 5 785.37 1.10 1.497E+006 1.022E+006 6.830E+005 1 620.5 0 1. 4 7 7.834E+005 3.652E+005 3 . 2 11E+005 Pb-21 2 115. 1 8 0.60 3.229E+006 4.70E+004 -2 .445E+006 1.561E+006 238.63 43.60 4.702E+004 1 .427E+004 2 .259E+004 300.09 3.30 5 .859E+005 -3 . 444E+005 2 .793E+005 Pb2 1 2-XR 74.8 2 10.28 3 .170E+005 1.78E+005 4.707E+005 1.552E+005 77.11 17.10 1.780E+005 -2 .718E+004 8.704E+004 87.35 3.97 6.217E+005 1 .682E+005 3 .028E+005 89.78 1. 46 1. 598E+006 -9.644E+005 7.774E+005 Bi-214 609. 32 45.49 5.096E+004 5.10E+004 7.4 3 7E+004 2 .408E+004 768. 3 6 4.89 3 .4 1 6E+00 5 -7.052E+004 1 . 562E+005 8 0 6.18 1. 2 6 1. 219E+006 -2 .886E+004 5.519E+005 934. 0 6 3.11 4.754E+005 1.476E+004 2 .125E+005 1 1 2 0. 2 9 14.92 1.436E+005 1.905E+005 6.608E+004 1 155. 2 1 1. 63 1 .171E+006 6.641E+005 5.324E+005 1238. 1 2 5.83 3 .051E+005 1.050E+005 1. 3 72E+005 1 2 80.98 1. 43 1 .103E+006 6.598E+005 4.8 82E+005 1377.67 3.99 3 .629E+005 3.940E+004 1.578E+005 1385.31 0.79 1.831E+006 -1.466E+006 7.958E+005 140 1. 52 1. 33 1.190E+006 9.541E+005 5.232E+00 5 1407.99 2 .39 5.143E+005 -2.694E+005 2 .172E+00 5 1509.21 2 .13 6.727E+005 -1.892E+005 2 .896E+00 5 1661.27 1. 05 1 .179E+006 -3 .902E+005 4.891E+005 [194]

1clide MDA Report 1 /31/ 2 01 1: 35 : 2 9 PM Page 7 Nucl ide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Bi -2 14 1729.59 2 .88 3.905E+005 5.10E+004 1.661E+005 1.578E+00 5 1764.49 15.3 0 1.463E+005 1.528E+005 6.602E+004 1847.43 2 .03 6.460E+005 3 . 25 7E+005 2 .679E+005

 >                2118.51       1.16 O.OOOE+OOO                     O.OOOE+OOO       O.OOOE+OOO Pb- 2 14     24 1. 99    7.25 2.927E+005 5.94E+004           2 . 62 8E+005    1.407E+005 295.22    1 8.42 1 .066E+005                    8.006E+004       5. 0 86E+004 351.93    35.60 5.942E+004                      7.615E+004       2 .834E+004 785.96      1. 06 1.477E+006                  -6.464E+005        6.708E+005 Pb214-XR       74.8 2    5.80 5.618E+005 3 .14E+005          8. 3 43E+005    2 .750E+005 77.11     9.70 3 .138E+005                  -4.791E+004       1.534E+005 87.35     2.24 1. 1 02E+006                   2 .982E+005     5.367E+005 89.78     0.82 2 .846E+006                  -1.717E+006       1.384E+006 Ra-2 2 6      186.2 1    3 .64 4.884E+005 4.88E+005         - 1.487E+005      2.344E+005 Ac-228        129.07     2 .4 2 8.153E+005 7.45E+004       -1.692E+005        3.943E+005 2 09.25    3 .89 4.684E+005                     1.115E+004      2.245E+005 2 70.24    3 . 46 5.437E+005                    2 .720E+005     2.595E+005 328.00     2 .95 6.162E+005                     1.031E+005      2.922E+005 338.32   11. 2 7 1. 691E+00 5                   7.820E+004      8.031E+004 409.46     1. 92 8.677E+005                  -9 .840E+005       4.065E+005 463.00     4. 40 3 .762E+005                    3 .360E+004     1.754E+005 794.95      4.25 4.091E+005                   - 6.8 2 3E+004     1. 87 5E+005 911.20   25.80 7.447E+004                       3.000E+004      3.424E+004 964.77     4.99 4.080E+005                      1 . 562E+005    1.881E+005 968.97    15.8 0 1.157E+00 5                  - 1.783E+004       5.281E+004 1588.2 0     3.22 4.100E+005                   - 6.472E+004       1.731E+005 Pa- 23 1       27.36   10 .3 0 3.375E+005 3 . 3 8E+005     -1. 3 84E+00 5     1.651E+005 283.69      1. 7 0 1.042E+006                 -9.329E+00 5       4.952E+005 300.07      2 .47 7.828E+005                  -4.601E+005        3.732E+005 302 . 65    2 . 20 8 . 523E+ 0 05                8 . 7 1 7E+004  4.056E+005 330.06      1. 40 l.361E+006                    1 .033E+006      6.467E+005 Th-234         92.38     2 .13 l.071E+006 1. 0 7E+006         4.423E+005      5. 2 08E+005 92.80     2 .10 1.088E+006                    7. 2 99E+005     5. 2 89E+005 11 2.81     0.21 9.0 2 0E+006                 -1.691E+006        4.357E+006 U-2 35       1 43.76   10.96 1.823E+005 3 .13E+004           1.806E+005       8.813E+004 163.33      5.08 3 .526E+005                    1.435E+005       1.695E+005 185.71    57. 2 0 3 .127E+004                 -1.822E+004        1.501E+004 202.11      1. 08 1.633E+006                  -9.212E+005        7.819E+005 205.31      5.01 3.680E+005                   -1. 62 5E+005      1.765E+005 Am-24 1        59.54   35.90 8.079E+004 8. 0 8E+004          6.940E+004       3.933E+004
    +     Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @     Half-life too short to be able to perform the decay correction

[195]

****          GAMM A       S t' E C T R U M         A N A L Y ::, I S                  *****
.lename: E: \ Zion Nuclear \ Inspector Shots\B306100ASJWC16GD.CNF
!port Generated On                    1/31 /2 017     2 :05:44 PM tmple  Title                          B3061008SJWC16GD tmple  Description                    Clean/Dirty 5"ii Tank Room tmple  Identification                 North Wall tmple  Type tmpl e Geometry                       3 meter iak Locate Threshold                    3 . 00

!ak Locate Range (in channels) 85 - 81 92 !ak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10 . 000 keV tmpl e Size 1.000E+OOO SQ MET tmple Taken On

quisition Started 12/ 22 /2015 2:52:47 PM

.ve Time 600.0 seconds !al Time 600.3 seconds !ad Time 0 . 05 % Energy Calibration Used Done On 1/27/2015 Efficiency Calibration Used Done On 1/31/2017 Efficiency ID CRIBHOUSE 3M

                                                                  \ ) o:\C\ \lo.\ ic\o..\ec\ 'oy Q~4
                                                                    ,~-{,,~/'l 6150

[196]

iak Analysis Report 1 /31/2017 2 :05:44 f Page 2

****             P E A K      A N A L Y S I S           R E P O R T              *****

Detector Name: 5456 Sample

Title:

B30610 0 8SJWC16GD Peak Analysis Performed on: 1 /31 /2 017 2:05:4 3 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area Uncert. Counts 1 2 431- 2447 2440.63 610 .06 1. 48 6.05E+001 21.19 1.65E+001 2 3875 - 3884 3879.34 969.6 2 0.37 1. 2 0E+001 9.73 5.00E+OOO 3 5839- 5859 5849.31 1461.64 1. 31 1.44E+00 2 27.19 1.08E+001

=  First peak in a mul tiplet region
=  Other peak in a mul tiplet region
= Fitted singlet

rors quoted at 2 .000 sigma

[197]

1terference Corrected Act ity Report 1/31/2017 05:44 PM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B3061008SJWC16GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQ M) Uncertainty K-40 0.999 1460.8 2

• 10.66 9.76374E+005 2 .0 2 688E+00 5

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold =       0.30 Errors quoted at 2 .000 sigma

[198]

1terference Corrected Act ity Report 1 / 3 1 /2017 05: 44 PM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 0.999 9.763741E+005 2 .026880E+005

      ?  = Nuclide is part of an undetermined solution X   = Nuclide rejected by the interference analysis
      @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at        2. 000 sigma
 **********       U N I D E N T I F I E D        P E A K S          **********

Peak Locate Performed on: 1 /31/2017 2:05:43 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak To l. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 61 0 .06 1.00 83E- 001 3 5. 0 3 Tol. Zr-97 Sb- 125 Sb- 1 25 Cs- 1 34 Bi-2 14 2 969.62 2 .0000E-00 2 8 1.1 2 To l . Eu-152 Ac-228 Ac-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 s igma [199]

1cl i de MDA Report 1/31/ 2 0 ] 2 :05 : 44 PM Page 5

• • • • N U C L I D E MD A R E P O R T *****

Detector Name: 5456 Sample Geometry: 3 meter Sample

Title:

B3061008SJWC16GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) (%) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M)

+       K-40       1460. 82

• 10.66 1.603E+005 1.60E+005 9.764E+005 7.101E+004 Cr-5 1 32 0.08 9.91 1.479E+005 1.48E+005 -4.877E+004 6.927E+004 Mn-54 834.85 99.98 1.448E+004 1.45E+004 5.936E+003 6.498E+003 Co-58 810.76 99.45 1.531E+004 1. 53E+004 1 .072E+004 6.919E+003 Co-60 1173. 2 3 99.85 1.486E+004 1. 34E+004 -2 .910E+00 3 6.557E+003 13 32 .49 99.98 1.336E+004 4.443E+003 5.750E+003 Nb-94 70 2 .65 99.81 1.264E+004 1. 2 6E+004 -9. 1 92E+003 5.636E+003 871. 09 99.89 1.504E+004 4.870E+002 6.763E+003 Sn-113 255.13 2 .11 6.611E+005 2 . 1 9E+004 -1. 93 4E+005 3.108E+005 391. 70 64.97 2.189E+004 -3.910E+003 l.0 1 6E+004 Cs- 134 475.36 1. 48 9 . 2 76E+005 1.68E+004 6.145E+005 4. 25 6E+005 563. 2 5 8. 3 4 l.578E+005 - 1.010E+005 7.153E+004 569.33 15. 3 7 8.603E+004 -l. 3 71E+004 3 .900E+004 604.72 97. 62 l.833E+004 -8.061E+003 8.515E+00 3 795.86 85.46 l.684E+004 -9.569E+002 7.571E+003 801. 95 8.69 1.517E+005 2 .600E+004 6.747E+004 1038.61 0.99 l.510E+006 1 .016E+006 6.718E+005 1167.97 1. 79 8. 27 4E+005 -l.710E+005 3.650E+005 1365.19 3.02 4.632E+005 3.224E+005 2.004E+005 Cs-137 661.66 85.10 l.871E+004 l .87E+004 4.669E+003 8.5 7 6E+00 3 Eu- 15 2 121. 78 2 8.67 6.037E+004 5. 0 1E+004 -2 .464E+004 2 .907E+004 244.70 7.61 l. 932E +005 -7.276E+002 9.123E+004 2 95.94 0.45 3.508E+006 1.156E+006 1.654E+006 344. 2 8 2 6.60 5.011E+004 -l.610E+004 2 . 32 5E+004 367.79 0.86 l .502E+006 -3.942E+005 6.935E+005 411.12 2 . 24 6.064E+005 1 . 1 71E+005 2 .797E+005 443.96 2 .8 3 4.881E+005 -1.093E+005 2 . 2 48E+005 488.68 0.4 2 3.042E+006 1. 3 66E+005 l .385E+006 563.99 0.49 2.604E+006 -l. 62 7E+006 l.177E+006 586. 2 6 0.46 4. 23 9E+006 3. 517E+006 l.984E+006 678. 62 0.47 2.629E+006 -l.376E+006 l.172E+006 688.67 0.86 l. 2 39E+006 -2 . 2 39E+006 5.410E+005 719.35 0. 2 8 4.298E+006 9.550E+005 l.902E+006 778.90 1 2 .96 l.062E+005 6.029E+004 4.755E+004 810.45 0.32 4.670E+006 l.430E+006 2 .107E+006 867.37 4.26 3.746E+005 -4.751E+004 1. 696E+005 919. 33 0.43 3.899E+006 1.545E+006 1 .768E+006 964.08 14.65 1. 2 90E+005 4. 2 71E+004 5.908E+004 1085.87 10.24 1.429E+005 5. 3 19E+004 6.324E+004 1089.74 1. 73 7.683E+005 l.577E+004 3 . 3 54E+005 111 2 .07 13.69 l.032E+005 -4.024E+004 4. 5 39E+004 1 212 .95 1. 43 1. 2 57E+0 0 6 7.572E+005 5 . 6 62E+005

[200]

lClide MDA Report 1 /31/201 2 :05:44 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Eu-15 2 1 249.94 0.19 8.275E+006 5.01E+004 4.984E+006 3.661E+006 1299.14 1. 63 7.846E+005 -2 .614E+005 3.359E+005 1408.01 21. 07 8. 22 8E +004 7.380E+004 3.660E+004 1 457.64 0.50 8.819E+006 -3.784E+006 4.2 1 6E+006 1528.10 0. 2 8 3 .156E+006 -1.363E+006 1.222E+006 Eu-154 123.07 40.40 4. 21 8E+004 4 . 11E+004 -3.678E+004 2.029E+004 247.93 6.89 1 .905E+005 -1. 752E+005 8.930E+004 59 1. 76 4.95 2 .604E+005 1.7 5 0E+005 1. 17 5E+005 692.42 1. 78 7.448E+005 2 . 2 00E+005 3.343E+00 5 723.30 2 0.06 5 .993E+004 -7.0 2 8E+004 2.652E+004 756.8 0 4. 52 2 .595E+005 - 2 .890E+004 1.141E+005 873.18 12 .08 1 . 22 4E+005 -9.130E+004 5.495E+004 996. 2 9 10.48 1.632E+005 4.732E+004 7.386E+004 1004.76 18.01 8.336E+004 9.488E+00 3 3 .717E+004 1274.4 3 34.80 4.112E+004 - 6.142E+004 1.795E+004 1596.48 1. 80 6.712E+005 6.742E+004 2 .784E+005 Eu-155 45.3 0 1. 3 1 9.704E+005 7.18E+004 6.4 3 7E+004 4. 5 61E+005

60. 0 1 1. 22 1.603E+006 2 .0 5 1E+005 7.704E+005 86.55 3 0.70 7.185E+004 l.014E+005 3 .488E+004 1 05.3 1 2 1.10 8. 32 5E+004 -3 . 1 2 0E+004 4.011E+004 Tl-208 58 3 . 1 9 85.00 2 .376E+004 2 . 3 8E+004 3.7 3 9E+004 1.114E+004 Bi-211 351. 0 7 13.0 2 1.387E+005 1. 3 9E+005 1. 3 10E+005 6.564E+004 Pb-211 404.85 3.78 3.595E+005 3 .60E+005 -7.613E+004 1. 660E+005 427. 0 9 1. 76 8.572E+005 -2 .161E+00 5 3 .982E+005 832. 01 3.52 4. 0 34E+005 6.990E+004 1.807E+005 Bi -2 1 2 39.86 1. 06 1. 1 44E+006 2 .07E+005 -l.550E+005 5.358E+005 727. 33 6.67 2. 0 66E+005 -8.127E+004 9.291E+004 785.37 1.10 1 .231E+ 0 06 4.042E+005 5.500E+005 1 620.50 1. 47 6.266E+ 0 05 2 .087E+005 2 .427E+005 Pb- 212 115.18 0.60 3.095E+006 4.09E+004 8.455E+005 1. 494E+006 2 38.63 43.60 4.091E+004 2 .911E+004 1.953E+004 300.09 3.30 4.492E+005 -8. 2 17E+005 2 .110E+005 Pb2 12-XR 74.82 10. 2 8 2 .618E+005 1. 4 7E+005 4.479E+005 1. 2 76E+005 77.11 17.10 1.469E+005 8.826E+004 7.150E+004 87.35 3.97 5.427E+005 4.952E+005 2 .633E+005 89.78 1. 46 1. 374E+006 -1.132E+006 6 .653E+005 Bi-21 4 609.32 45.49 5.096E+004 5. 1 0E+004 6.028E+004 2 .408E+004 768.36 4.89 3 .077E+005 5.091E+004 1.393E+005 806.18 1. 2 6 l.107E+006 -2.301E+005 4.956E+005 934.06 3.11 5.256E+005 2.5 92 E+005 2 .376E+005 1120.29 14.92 1.376E+005 3.070E+004 6.307E+004 1155.2 1 1. 63 1.171E+006 4.797E+005 5. 32 4E+005 1238.12 5.83 3. 2 95E+005 1. 041E+005 1.494E+005 1280.98 1. 43 1 . 1 27E+006 4.022E+005 5.002E+005 1377.67 3.99 4. 2 95E+005 1.703E+005 1. 911E+005 1385.31 0.79 1. 4 72E+006 -1.028E+006 6.164E+00 5 1401.52 1. 33 1.246E+006 3 .843E+005 5.5 1 5E+005 1 407.99 2.39 7. 2 42E+005 6.495E+005 3. 22 1E+005 1 509. 2 1 2.13 6.262E+005 1.852E+005 2.664E+005 1 661. 2 7 1. 05 1 .048E+006 4.460E+005 4.236E+005

[201]

1clide MDA Report 1/31/ 2 0~ 2 :05:44 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (% ) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Bi -21 4 1729.59 2 .88 4.8 2 3E+005 5.10E+004 2 .769E+005 2 . 0 37E+005 1764.49 15.30 1. 1 83E+005 4.831E+004 5 . 2 02E+004 1 84 7.43 2 . 03 5.742E+0 0 5 2 .443E+005 2 . 32 0E+005

 >                2 11 8.51          1. 1 6 O.OOOE+OOO                    O.OOOE+OOO   O.OOOE+OOO Pb-2 1 4     2 41. 99         7.25   2 .468E+005     5 .17E+004    1.876E+005   1 .178E+005 2 95. 22        18.42   8.607E+004                    6.642E+004   4.061E+004 351. 93         35.60   5.171E+004                    7. 1 07E+004 2 .449E+004 785.96           1. 06  1. 32 7E+006                - 6.515E+004   5.954E+005 Pb214-XR         74.8 2       5.80   4.640E+005      2.59E+00 5    7.939E+005   2 . 2 62E+005 77.11         9.70   2 .590E+005                   1.556E+005   l. 2 60E+005 87.35        2 . 24 9.619E+005                    8.776E+005   4.667E+005 89.78         0 .82  2 .447E+006                 -2 .016E+006   1.185E+006 Ra-22 6      186. 2 1         3.64   4. 25 6E+005    4. 2 6E+005   2 .850E+005  2 .030E+005 Ac-22 8      129. 07          2.42   7.345E+005      6.96E+004     5.714E+004   3.538E+005 209. 2 5         3.89   4.111E+005                    2 .799E+005  1.958E+005 2 70. 2 4        3.46   4.074E+005                  -8.436E+004    1.913E+005 328.00           2.95   4.832E+005                  -1.555E+005    2 .257E+005 338.32          11.2 7  1.417E+005                    3.903E+004   6.664E+004 409.46           1. 92  7.185E+005                    2 .513E+005  3 .319E+005 463. 00          4.40   3.596E+005                    3.063E+005   1.671E+005 794.95           4.25   3.384E+005                    1.388E+005   l .522E+005 911. 2 0        25 .80  6.963E+004                    2 .855E+004  3 .182E+004 964.77           4.99   4.040E+005                    7. 2 13E+004 1.861E+00 5 968.97          15.80   1.157E+005                    6.455E+004   5 . 2 81E+004 1588.20            3.22   3.734E+005                  -1.103E+004    1.549E+005 Pa- 2 3 1       27.36        10.30   1.162E+005      1.16E+005     1.084E+004   5.440E+004 283.69           1 . 70 8.031E+005                  -1.475E+005    3.758E+005 300.07           2.47   6.001E +005                 -l.098E+006    2 .818E+005 302.65           2. 2 0 6.921E+005                    2 .849E+005  3. 2 55E+005
                    '°\""'lf"I
                    .:>.:>U. UO f"lr

1. 4 0 l.042E+006 1 .161E+005 4.874E+005 Th- 234 92.38 2.13 9. 2 08E+005 9 .2 1E+005 -2 .028E+004 4.455E+005 92 .80 2 .10 9.416E+005 5.174E+005 4.556E+005 112.81 0. 2 1 8.398E+006 l.303E+006 4.046E+006 U- 235 143.76 10 . 96 1.559E+005 2 .78E+004 3 .943E+004 7.494E+004 163.33 5.08 3.119E+005 1.0 9 4E+005 1.492E+005 185.7 1 57. 2 0 2.776E+004 2.411E+004 1 .3 25E+004 2 02.11 1. 08 1.441E+006 -1.874E+005 6.862E+005 2 05. 3 1 5.01 3.163E+005 -4.865E+004 1.507E+005 Am-241 59.54 35.90 5.466E+004 5.47E+004 2 .000E+00 3 2 . 62 7E+004

     +     Nuclide identified during the nuclide identification

• Energy line found in the spectrum

     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ = Half-l ife too short to b e able to perform the decay correction

[202]

*** * ******************** j     *************************            ~*****************
****          G A M MA      S l:? E C T R U M        A N A L Y S I S                              *****
.lename: E: \ Zion Nucl ear \Turbine Building\B306100AFJWC017GD.CNF iport Generated On                     1/31/2017       11: 40 : 12 AM -    '{'e - '('I:>.\(\ V'CfN"'!' 1 ""~,:.*,*~"

1mple Title B306100AFJWC017GD tmple Description VALVE PIT ---. tmple Identification tmple Type tmple Geometry SQ M !ak Locate Threshold 3 . 00 !ak Locate Range (in channels ) 85 - 81 92 iak Area Range (in channels ) 85 - 81 92 lentification Energy Tolerance 10.000 keV tmple Size 1. OOOE+OOO 1 tmpl e Taken On

quisition Started 3/3/2 01 6 1 : 32 :14 PM

.ve Time 600.0 seconds ial Time 600.4 seconds !ad Time 0 . 06 % Energy Calibration Used Done On 1 /2 7 /2 015 Efficiency Calibration Used Done On 4/11 /2 016 Efficiency ID TB VALVE PIT

1) 0.. \ " ~o.\ \d a.~~ 'Q1 9~~~

1=2-, - ,i

                                                                       , , 10

[203]

ia k Analysis Report 1 /3 1 / 2 017 11:40:12 Page 2

****             P E A K        A N A L Y S I S             R E P O R T                *****

Detector Name: 5456 Sample

Title:

B306 1 00AFJWC017GD Peak Analysis Performed on: 1/31/2017 11:4 0 :12 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI RO I Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV ) Area Uncert. Counts 1 5830- 5853 5842.83 1 460.02 1.08 1. 3 9E+00 2 2 6. 32 8.57E+O OO

= First peak in a multiplet region Other peak in a multiplet region Fitted singlet

rors quoted at 2 .000 sigma

[204]

1terference Corrected Act ity Report 1/3 1 / 2 017  : 40:1 2 AM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Titl e : B306100AFJWC017GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/1 ) Uncertainty K-40 0.999 1460.82* 10.66 3.82069E+006 7.93761E+005

• Energy line found in the spectrum.

      @=Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold =       0. 3 0 Errors quoted at 2 .000 s igma

[205]

1terference Corrected Act ity Report 1/31/ 2 017 ;40:1 2 AM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/1 ) Uncertainty K-40 0.999 3.820690E+006 7.9376 1 0E+005

      ?    Nuclide is part of an undetermined solution X  = Nuclide rejected by the interference analysis
      @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at    2 .000 sigma
  **********    U N I D E N T I F I E D        P E A K S        **********

Peak Locate Performed on: 1 / 3 1/2017 11:40:12 AM Peak Locate From Channel: 85 Peak Locate To Channel: 81 92 Peak Energy Peak Size in Peak CPS Peak To1 . No. (keV) Counts per Second  % Uncertainty Type Nuclide All peaks were identified. [206]

lClide MDA Report 1/31/ 2 0 11:40:1 2 AM Page 5 "*** N U C L I D E MD A R E P O R T ***** Detector Name: 5456 Sample Geometry: SQM Sample

Title:

B306100AFJWC0l7GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/1 ) (pCi/1 ) (pCi/1 ) (pCi/1 )

+      K-40       1460.8 2

• 1 0 .66 5.975E+005 5.97E+005 3 .821E+006 2.617E+005 Cr-51 32 0.08 9.91 9.699E+005 9.70E+005 2 .937E+005 4.518E+005 Mn-54 834.85 99.98 6.833E+004 6.83E+004 -5.058E+004 3.054E+004 Co-58 810.76 99.45 7.460E+004 7.46E+004 2 . 2 84E+004 3.366E+004 Co-60 11 73 . 2 3 99.85 6.451E+004 5.57E+004 -l.798E+004 2.846E+004 13 32 .49 99.98 5.568E+004 -5.057E+003 2.397E+004 Nb-94 7 0 2 .65 99.8 1 8.592E+004 6.86E+004 3 .106E+004 3.938E+004 871. 09 99.89 6.864E+004 -6 .141E+003 3.068E+004 Sn-113 255.1 3 2 .11 4.909E+006 1 .28E+005 -1.071E+006 2.303E+006 391.7 0 64.97 1. 2 83E+005 -2 .067E+004 5.896E+004 Cs-134 475.36 1. 48 5. 3 85E+006 8 .2 5E+004 -3 .590E+005 2.461E+006 563.25 8.34 7.744E+005 -3 .532E+004 3.453E+005 569.33 15.37 3 .863E+005 -1.513E+005 1.704E+005 604.72 97.62 9.743E+004 -1. 36 4E+004 4.511E+004 795.86 85.46 8. 2 51E+004 4.917E+004 3.703E+004 8 01. 95 8.69 7.537E+005 - 1.044E+005 3.353E+005 10 38.6 1 0.99 4.417E+006 - 3 . 3 93E+006 1.832E+006 11 67 . 97 1. 79 3 .838E+006 5.973E+005 1.707E+006 1 36.5. 19 3.02 l.660E+006 -2 .144E+005 7.009E+005 Cs- 1 37 66 1. 66 85.10 l.108E+005 l.11E+005 8.058E+004 5.125E+004 Eu- 1 52 1 21. 78 28.67 5.994E+005 2 .68E+005 -1.385E+005 2 .880E+005 2 44.7 0 7.61 1. 508E+006 5.524E+004 7.124E+005 2 95.94 0.45 2.460E+007 1.079E+007 1.158E+007 344. 2 8 2 6.6 0 3.390E+005 l.401E+005 1.571E+005 367.79 0.86 1.008E+007 3.039E+006 4.654E+006 411.12 2.24 3.705E+006 -2.568E+005 1.702E+006 443.96 2.83 3.223E+006 -5.488E+005 1. 4 91E+006 488.68 0.4 2 1.806E+007 8.917E+006 8. 2 09E+006 563.99 0.49 l. 2 08E+007 -3 . 2 37E+006 5.330E+006 586. 2 6 0 . 46 l.950E+007 2 . 2 75E+006 8.986E+006 678.62 0.47 1.281E+007 l.877E+006 5.652E+006 688.67 0.86 7.368E+006 2 .179E+006 3.269E+006 7 1 9.35 0.28 2 .325E+007 5.385E+006 1.034E+007 778.90 12.96 6. 2 92E+005 -2.999E+0 0 5 2. 868E+005 810.45 0. 32 2 . 3 47E+007 4.377E+006 1 . 061E+007 867.37 4. 2 6 1 .548E+006 -l.599E+005 6.885E+005 919.33 0.43 l .456E+ 0 07 2 .067E+006 6.423E+006 964.08 14.65 6.120E+ 0 05 4.883E+005 2 .808E+005 1 085.87 10 . 2 4 5.613E+005 -5.077E+005 2 .440E+005 1089.74 1. 73 3 .686E+006 1.243E+006 1 .62 6E+006 1 11 2 .07 13.69 3.959E+00 5 -3.583£+005 1.704E+005 121 2 .95 1. 43 4.433E+006 2 .669E+006 1.949E+006

[207]

1clide MDA Report 1 /31 /2 0 . 11:40:12 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/1 ) (pCi/1 ) (pCi/1 ) (pCi/1 ) Eu-15 2 1249.94 0.19 2 .917E+007 2.68E+005 -1.572E+007 1.2 5 6E+007 1299.14 1. 63 3 . 63 0E+006 4.817E+005 1.578E+006 1408.01 2 1. 07 2 .677E+005 8.457E+004 1.153E+005 1457.64 0.50 3.509E+007 7.989E+007 1.676E+007 1528.10 0.28 1. 2 60E+007 - 9.181E+006 4.882E+006 Eu-154 123.07 40.40 4. 2 94E+005 1.79E+005 2 .006E+005 2 .064E+005 247.93 6.89 1.443E+006 -7.487E+005 6.754E+005 591.76 4.9 5 1.455E+006 8.042E+005 6.566E+005 692.42 1. 78 3.987E+006 1.112E+006 1.793E+006 7 23 . 3 0 2 0.06 3.828E+005 1.688E+005 1.736E+005 756.80 4.52 1. 4 70E+006 -9.606E+005 6.556E+005 873.18 12.08 5.678E+005 2 .043E+005 2 .538E+005 996. 2 9 10.48 5.421E+005 -4.385E+005 2 .356E+005 1004.76 18.01 2 .654E+005 7.009E+004 1.121E+005 1274.43 34.80 1.785E+005 -1.602E+005 7.822E+004 1596.48 1. 80 3.353E+006 -4.049E+005 1.451E+006 Eu- 1 55 45.30 1. 31 8.367E+006 7.11E+005 -4. 2 00E+006 3. 92 8E+006 60.01 1. 22 1. 32 0E+007 3.780E+006 6. 32 7E+006 86.55 30.70 7.109E+005 5.411E+005 3.445E+005 105.31 21.10 8.443E+005 -5.002E+005 4.063E+005 Tl- 2 08 583.19 85.00 1.172E+005 1.17E+005 7.605E+004 5 .445E+004 Bi-211 351. 07 13.0 2 9.564E+005 9.56E+005 1.215E+006 4.527E+005 Pb-211 404.85 3.78 2 .368E+006 1 .90E+006 4. 2 00E+005 1.095E+006 42 7.09 1. 76 4.626E+006 - 1.186E+006 2 .120E+006 832.01 3.52 1.904E+006 1.902E+005 8.489E+005 Bi -212 39.86 1. 06 1. 2 62E+007 1.12E+006 2 .881E+006 5.995E+006 727.33 6.67 1.119E+006 4. 27 9E+005 5.056E+005 785.37 1. 1 0 7.590E+006 5.797E+006 3.468E+006 1 620.50 1. 4 7 3.247E+006 1 .637E+006 1.347E+006 Pb-212 1 15.18 0.60 2.976E+007 3.22E+005 - 1. 2 45E+007 1 .432E+007 2 38.63 43.60 3. 2 24E+005 1 .886E+005 1.539E+005 3 00.09 3.30 3.157E+006 -1.322E+006 1.480E+006 Pb212-XR 74.82 10.28 2.426E+006 1.35E+006 3.934E+006 1.181E+006

77. 11 17.10 1.351E+006 -1.033E+005 6.559E+005 87.35 3.97 5.410E+006 1.101E+006 2 .621E+006 89.78 1. 46 l.386E+007 - 1 .804E+005 6.699E+006 Bi-2 1 4 609. 32 45.49 2.490E+005 2 .49E+005 2 .819E+005 1.168E+005 768.36 4.89 1.461E+006 -2 .001E+006 6.569E+005 806.18 1. 2 6 5.774E+006 -l.509E+004 2 .601E+006 934.06 3.11 2 .502E+006 1. 25 4E+006 l.133E+006 1120. 2 9 14.9 2 6.133E+005 6.778E+005 2 .814E+005 1155. 2 1 1. 63 4.114E+006 5.422E+005 1.825E+006 1238. 1 2 5.83 l.113E+006 6.098E+005 4.911E+005 1280.98 1.43 4.956E+006 3.223E+006 2 .210E+006 1377.67 3.99 l .497E+006 1.228E+005 6.508E+005 1385.31 0.79 6.597E+006 - 9.259E+005 2 .806E+006 1 401. 52 1. 33 4. 2 37E+006 5.437E+004 1.824E+006 1 407.99 2.39 2 . 3 56E+006 7.443E+005 1.015E+006 1509.21 2.13 2 .411E+006 2 .561E+005 l.018E+006 1661.27 1.05 3.115E+006 -6.511E+005 l.166E+006

[208]

1clide MDA Report 1/31 /2 0 _ 11:40:12 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/1 ) (pCi/ 1 ) (pCi/1 ) (pCi /1 ) Bi- 214 1729.59 2 .88 l. 2 79E+006 2 .49E+00 5 -2 .861E+005 4.954E+005 1 764.49 15.30 5 .039E+005 1.863E+005 2.247E+005 1847.43 2 .03 1.848E+006 6.154E+005 7.159E+005

 >               2 118.5 1      1.16    O.OOOE+OOO                      O.OOOE+OOO      O.OOOE+OOO Pb- 2 14     241.99       7. 2 5  1.8 2 1E+006   3 .50E+005       1.114E+005      8.667E+005 295.22      18.4 2   6.144E+005                      4.941E+005      2 .895E+00 5 351.93      35.60    3.499E+005                      4.455E+005      1.656E+00 5 785.96       1. 06   7.501E+006                      3.825E+006      3 .410E+006 Pb214-XR       74.8 2     5.80    4.300E+006     2 . 3 8E+006     6.972E+006      2 .093E+006 77.11      9.70    2.381E+006                    - 1.822E+005      1.156E+006 87.35      2 . 24  9.588E+006                      1. 951E+006     4.645E+006 89.78      0 .8 2  2 .467E+007                   -3. 2 12E+005     1.193E+007 Ra-226       186. 2 1     3 .64   3.597E+006     3.60E+006        1.792E+006      1.713E+006 Ac-228       12 9.07      2 .42   7.438E+006     3.63E+005        3.976E+006      3 .583E+006 2 0 9. 2 5   3.89    3.411E+006                      3.085E+006      l.625E+006 270. 2 4     3.46    2 .976E+006                   -1.286E+006      1. 3 95E+006 328. 00      2 .95  3 .193E+006                    -1.197E+006      1.485E+006 338. 32     11.27     9 .072E+005                     2.271E+004      4. 2 43E+005 409.46       1. 92  4 . 2 68E+006                  -2.422E+006      1.958E+006 463. 00      4.40   2 .026E+006                      7.789E+005      9.353E+005 794.95        4. 25  1.659E+006                       9.886E+005     7.445E+005 911.20      2 5.80   3.631E+005                       2.245E+005     1.674E+005 964.77        4.99   1.855E+006                      1.777E+006      8.534E+005 968.97      15.8 0   5.553E+005                      1.402E+005      2 .543E+005 1588.20        3. 22  1.685E+006                    - 1.459E+006      7.168E+005 Pa-2 31       27.36     10. 3 0  1. 4 78E+006   1.48E+006      - 6.282E+005      7.066E+005 283.69        1. 70  5.411E+006                    -1. 22 6E+006     2. 515E+006 300.07        2.47   4.217E+006                    -1. 766E+0 0 6    1.977E+006 302.65        2.20   4. 2 77E+006                  - 3 .647E+0 0 6   1.990E+006 330.06        1.40   7.039E+006                      5.366E+006      3 . 2 84E+006 Th-234         92.38       2.1 3  9.059E+006     9.06E+006      -2 .177E+006      4. 3 73E+006 92.80       2.10   9. 2 39E+006                    3 . 92 2E+004   4.460E+006 112.81        0. 2 1 8.165E+007                    -l.034E+007       3.923E+007 U- 235       1 43.76     10.96    1.414E+006     2 . 2 6E+005   -1.096E+006       6.778E+005 163.33       5.08    2 .482E+006                     2 .522E+005     1.179E+006 185.71      57.20    2.264E+00 5                     l.039E+005      1.078E+005 202.11       1. 08   1.094E+007                    -7.844E+006       5.181E+006 205.31       5.01    2 .579E+006                     6.925E+005      1. 22 7E+006 Am-24 1        59.54     35.90    4.414E+005     4.41E+005      -5.514E+004       2 .114E+005
    + = Nuclid e identified during the nuclide identification
    * = Energy line found in the spectrum
    >= Calculated MDA is z ero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Half-life too short to be able to perform the decay correction

[209]

***************************    ************************* ~**************
****        GAMM A         SP~ CTR UM          AN ALYS ~ S                            *****
.lename: E:\0000 1 678.CNF
!port Generated On                4 /26/2017       5:55:44 PM 1mple  Title                       U2B306100AFJWC018GD tmple Description                 U 2 TB SUMP PIT tmple Identification tmple Type 1mple  Geometry iak Locate Threshold                3. 00 iak Locate Range (in channels )        85 -   8192

!ak Area Range ( in channels ) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mpl e Si ze 1.000E+OOO SQ METER tmple Taken On 2/29/2016 1 2 :00:00 PM

quisition Started 3/7/2016 10:09:34 AM

.ve Time 600.0 seconds !al Time 600.9 seconds !ad Time 0.16 % Energy Calibration Used Done On 1/27/2015 Efficiency Calibration Used Done On 4/11/2016 Efficiency ID TB VALVE PI T 1).,.\~ \la.\,do..\cc\ l..o~

                                                         ~~

12-lo - 11 I\IC) [210]

iak Analysis Report 4/ 2 6/ 2 0 17 5 : 55 :4 5 PM Page 2

****                P E A K        A N A L Y S I S               R E P O R T                 *****

Detector Name: 5456 Sample

Title:

U2B306 1 00AFJWC018GD Peak Analysis Performed on: 4/26/2017 5:55:44 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 2 95- 306 300.58 74.88 1.13 1.08E+00 2 78.87 5.76E+002 2 440- 447 44 2 .96 110.5 0 0.57 2 .72E+OOO 46.4 1 2 .64E+002 3 1396- 1414 1405.28 3 51. 2 0 1. 96 2 .40E+002 50.95 1. 2 1E+002 4 2322- 23 40 232 9.88 58 2 .38 1. 33 9. 2 7E+001 3 0 .44 4.13E+001 5 2 424- 2445 2 434. 62 608.56 1. 75 2 .43E+002 44.35 6.60E+001 6 2 633 - 2 654 2 643.68 66 0 .8 2 1. 46 4.45E+002 53.78 7.41E+001 7 4943 - 4 954 4948.90 1236.8 0 0.42 2 .80E+001 16.25 1.50E+001 8 58 23- 5850 5837.11 1458.59 0.95 3.61E+00 2 43.51 2 .46E+001 9 704 2- 7062 7052.7 2 1762. 0 3 1. 0 2 7.70E+001 19.47 4.96E+000

= First peak in a mul tiplet region
= Other peak in a mul tiplet region
= Fitted singlet

rors quoted at 2 .000 sigma

[211]

1terference Corrected Activ / Report 4/ 2 6/ 2 017 5 -, : 45 PM Page 3 N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample

Title:

U2B306100AFJWC018GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQ M) Uncertainty K-40 0.992 1460.82* 10.66 9.90112E+006 1. 46963E+006 Cs-1 3 7 0.999 661.66* 85.10 1 .37278E+006 2 .33907E+005 Tl -2 08 0.999 583.19* 85.00 2 .82532E+005 9.878 2 8E+004 Bi -2 11 1. 000 3 51.07* 13.0 2 4.51247E+006 1.20299E+006 Bi-214 0.377 609. 32

• 45.49 1.38991E+006 3 .03750E+005 768.36 4.89 806.18 1. 2 6 934.06 3 .11 11 2 0. 2 9 14.9 2 1155. 2 1 1. 63 1238.12* 5.83 l _35582E+006 7.94171E+005 1280.98 1. 43 1377.67 3 .99 1385.31 0.79 14 01. 52 1. 33 1407.99 2 .39 1509. 2 1 2 .13 1661.27 1. 05 1729.59 2 .88 1764.49* 15.30 1.55102E+006 4.11126E+005 1847.43 2 .03 2 118.51 1.16 Pb-214 0. 3 09 2 41. 99 7. 2 5 2 95. 22 18.4 2 3 51.93* 35.60 1.650 3 6E+006 4.38970E+005 785.96 1. 06

      * = Energy line found in the spectrum.
      @=Energy line not used for Weighted Mean Activity Energy Tolerance :         10.000 keV Nuclide confidence index threshold =             0. 3 0 Errors quoted at 2 .000 sigma

[212]

1terference Corrected Activ J Report 4 / 2 6/2017 5 *. : 45 PM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 0.992 9.901119E+006 l.469630E+006 Cs-137 0.999 1.372778E+006 2.339068E+005 Tl -2 08 0.999 2.825 3 17E+005 9.878276E+004

  ?  Bi -2 11   1. 000      4.512468E+006        l .202994E+006 Bi-214     0.377       l.438936E+006        2.335058E+005
  ?  Pb-214     0.309       l.650360E+006        4.389701E+005
     ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2. 000 sigma

[213]

1terference Corrected Activ J Report 4/ 2 6/ 2 017 5  ; : 45 PM Page 5

 **********     U N I D E N T I F I E D       P E A K S        **********

Peak Locate Performed on: 4/26/2 017 5:55:44 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 74.88 1.8038E-001 72.87 Tol. Pb214-XR Ba-133 Pb212-XR Pb2 1 2-XR Pb2 1 4-XR 2 110.50 4.53 1 9E - 00 3 1 7 0 6 . 65 Tol. Eu-155 Pb-212 Th-234 U235-XR M = First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [214]

1clide MDA Report 4/ 2 6/ 2 017 5:55:45 PM Page 6

• • • • N U C L I D E M DA R E P O R T *****

Detector Name: 5 456 Sample Geometry: Sample

Title:

U2B306100AFJWC018GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) 1460.8 2

• 10.66 1.027E+006 l.03E+006 9.901E+006 4.765E+005

+      K-40 1 .085E+00 6 Cr-5 1       32 0.08      9.91   2 .249E+006      2 .25E+006 3 .7 5 8E+005 Mn-54        834.85     99.98    1.110E+005       l.11E+005 1. 2 65E+005       5.182E+004 Co-58        810.76     99.45    l.123E+005       1.12E+005 -4. 3 87E+004      5 . 22 4E+004 Co-60      1173. 2 3    99.85    1.480E+005       l.31E+005 l.160E+005         7.018E+004 1 33 2 .49   99.98    1.307E+005                      l.155E+005    6.145E+004 Nb-94        702.65     99.81    1.151E+005       1.15E+005 4.421E+004         5.397E+004 871. 09    99.89    1.150E+005                      3.354E+004    5.387E+004 Sn- 113      255.13       2 . 11 l . 1 04E+007    2 .52E+005 8.971E+006        5.362E+006 391. 70    64. 97   2 .517E+005                     4.675E+004    1. 2 05E+005 Cs-1 34      475.36       1. 48  l.011E+007       1.43E+005 -6.821E+006        4.820E+006 563.25       8. 3 4 1.576E+006                      1.657E+005    7.460E+005 569.33     15. 37   8 . 32 7E+005                 -5.099E+004     3 .935E+005 604.7 2    97. 62   2.33 1E+005                   - 9.038E+003    l. 12 9E+005 795.86     85.46    1.433E+005                    - 5. 2 64E+004  6.738E+004 801. 95      8.69   1. 2 87E+006                  -5. 3 19E+005   6.019E+005 1 038.61       0.99   9.003E+006                      3 .818E+005   4.123E+006 1167.97        1. 79  7.932E+006                      5.863E+006    3 .753E+006 1 365.19       3.02   2.445E+006                      1.779E+006    1 .093E+006
+      Cs-137       661. 66*   85. 10   1.776E+005       l.78E+005 1. 373E+006        8.464E+004 Eu -152      121. 78    2 8.67   l.201E+006       3.88E+00 5 -5.662E+005       5.887E+005 244.70       7.61   3.085E+006                    -1. 33 3E+006   1.501E+006 295.94       0.45   5.093E+007                      6.171E+007    2 .474E+007 344. 2 8   2 6.60   6.568E+005                      3.014E+005    3 .159E+005 367. 7 9     0 .86  l.893E+007                    - 9.000E+006    9.076E+00 6 411.12       2.24   7.291E+006                      3 .430E+005   3.494E+00 6 443.96       2 .83  5.655E+006                      2 . 3 42E+004 2.707E+00 6 488.68       0.42   3.133E+007                    -1.666E+006     l.485E+007 563.99       0.49   2.566E+007                    -l.750E+007     l.212E+007 586. 2 6     0.46   3.440E+007                    -1.772E+007     1.644E+007 678.62       0.47   2.260E+007                      1. 25 6E+007  1 .054E+007 688.67       0.86   1. 286E+007                   -5 .782E+00 5   6 .017E+006 719.35       0.28   4.155E+007                    -4.147E+007     l.949E+007 778.90     1 2 .96  8.843E+005                      3 .780E+005   4.143E+005 810.45       0.32   3.253E+007                      4.439E+006    1.514E+007 867.37       4.26   2.466E+006                      2 . 92 5E+004 l.148E+OO 6 919.33       0.43   2.215E+007                    - 1.201E+007    1.022E+007 964.08     14.65    9.435E+005                      1.019E+006    4 . 465E+00 5 1085.87      10. 2 4  1 .026E+006                   - 4.939E+005    4.761E+00 5 1089.74        1. 73  6.268E+006                      5.353E+006    2 .917E+00 6 1112.07      13.69    8.062E+005                    -2 .935E+006    3 .756E+00 5 1212.95        1. 43  7.601E+006                      4.606E+006    3 .533E+00 6

[215]

tclide MDA Report 4/26/2017 5:55:45 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Eu-15 2 1249.94 0.19 5.134E+007 3.88 E+00 5 4. 3 06E+007 2 . 3 64E+007 1299.14 1. 63 5.089E+00 6 -8. 3 28E+005 2 . 3 07E+006 1408.01 2 1. 07 3 .878E+00 5 3 . 2 45E+005 l.753E+005 1457.64 0.50 5.591E+007 2 . 2 40E+008 2 .717E+007 1528.10 0. 2 8 2 .524E+007 8. 6 65E+006 l.1 2 0E+007 Eu-154 123.07 40.40 8.356E+005 2 .74E+005 -5.92 6E+004 4.0 95E+005 247.93 6.89 3.205E+006 5. 22 4E+005 l. 55 6E+006 591. 7 6 4.95 2 .380E+006 -4.893E+005 l.119E+006 692.42 1. 78 6.266E+006 2 .760E+006 2.932E+006 723.30 2 0.06 6.284E+005 3 .804E+005 2.963E+005 756.80 4.52 2 .434E+006 -l.610E+006 l.137E+006 873.18 12.08 9.589E+005 2 .952E+005 4.493E+005 996. 2 9 10.48 l.053E+006 -1.008E+005 4.913E+005 1004.76 18.01 6.093E+005 3.197E+005 2 .840E+005 1 274.43 34.80 2 .742E+005 -l.594E+005 1. 26 0E+005 1596.48 1. 80 3 .143E+006 -9.078E+005 l. 3 46E+006 Eu-155 45.30 1. 31 1.577E+007 1.16E+006 -9.661E+006 7. 62 8E+006 60.01 1. 22 2 . 22 0E+007 -3.438E+006 l.082E+007 86.55 30.70 l.156E+006 - 3.774E+004 5 .67 2E +005 105.31 21.10 l.561E+006 7.540E+005 7.646E+005

+     Tl-208       583.19*  85.00    l. 2 64E+005    1. 2 6E+005    2 .825E+005   5.907E+004
+     Bi-211       351.07*  13.0 2   l. 3 03E+006    l. 3 0E+006    4.512E+006    6. 2 61E+005 Pb-211       404.85     3.78   4.223E+006      3 .10E+006   -4.768E+005     2.022E+006 427.09     1. 76  8.789E+006                     3.036E+006    4. 2 02E+006 832.01     3.52   3.104E+006                     l.059E+006    l.449E+006 Bi -212       39.86     1.06   l.850E+007      l.88E+006    -2.502E+006     8. 9 35E+006 727.33     6.67   l.878E+006                     7.700E+005    8.855E+005 785.37     1.10   l.115E+007                     l.154E+006    5.247E+006 1620.50      1. 4 7 4.594E+006                   -3.155E+005     2 .0 2 0E+006 Pb-212       115.18     0.60   5.797E+007      6.15E+00.5   -2.889E+007     2 .842E+007 238.63   43.60    6.153E+005                     9. 3 33E+005  3 .004E+005 300.09     3.30   6.067E+006                   -l.407E+007     2 .935E+006 Pb21 2-XR     74.82   10.28    3.938E+006      2 . 2 9E+006   7.969E+006    l.936E+006 77.11   17.10    2 .291E+006                  -1.077E+005     1.126E+006 87.35     3.97   8.931E+006                   -2 .498E+006    4.381E+006 89.78     1. 46  2 .414E+007                  -1.092E+006     l.184E+007
+     Bi- 2 14     609.32*  45.49    3.123E+005      3 .12E+005     l.390E+006    l.484E+005 768.36     4.89   2.713E+006                     l.085E+006    1. 28 3E+00 6 806.18     1. 2 6 8.619E+006                   - 8.476E+005    4.024E+00 6 934.06     3.11   3.736E+006                     3 .912E+006   l.750E+00 6 1120.29    14.92    l.010E+006                     l.227E+006    4.7 9 6E+00 5 1155.21      1. 63  7.081E+006                     1.176E+006    3.309E+00 6 1238.12*     5.83   l.113E+006                     1.356E+006    4.909E+00 5 1280.98      1. 43  6.437E+006                     2 .534E+006   2 .950E+00 6 1377.67      3.99   2.499E+006                     l.943E+006    1.152E+00 6 1385.31      0.79   9.939E+006                     4.806E+005    4.478E+00 6 1401.52      1. 33  6.401E+006                     3 .064E+006   2 . 906E+OO 6 1407.99      2 .39  3.410E+006                     2 .854E+006   1. 541E+00 6 1509.21      2 .13  3.463E+006                   -2 .689E+006    l.544E+00 6 1661.27      1. 05  4.591E+006                   - 2 .007E+006   l.904E+00 6

[216]

lClide MDA Report 4 /26/2 017 5:55:45 PM Page 8 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M)

+     Bi-2 14    1 729.59      2 .88  2 .447E+006      3 .1 2E+005   2 .023E+006 1.080E+006 1 764.49*    15. 3 0 3 .331E+005                    1.551E+006  1.393E+005 1 847.43      2 .03  3 .095E+006                    8.792E+004  1.339E+006 2 118.51      1.16   O.OOOE+OOO                     O.OOOE+OOO  O.OOOE+OOO
+     Pb-214       2 41.99     7. 25  3.525E+006       4.77E+00 5    1.514E+006  1.718E+006 2 95. 22   18.42   1.240E+006                     1.781E+006  6 . 025E+005 351.93*    35.60   4.766E+005                     1.650E+006  2 . 2 90E+005 785.96      1.06   1.165E+007                     5.371E+006  5.487E+006 Pb214-XR       74. 82    5.80   6.979E+006       4.04E+006     1.413E+007  3.432E+006

77. 11 9.70 4.039E+006 -1.898E+005 1.985E+006

87. 35 2 . 24 1.583E+007 -4.428E+006 7.765E+006 89.78 0. 82 4. 2 98E+007 -1.944E+006 2 .108E+007 Ra-226 186. 21 3.64 7.222E+006 7.22E+006 8.433E+005 3 .525E+006 Ac-228 129.07 2 .42 1.363E+007 5.83E+005 9.740E+006 6 .678E+006 209. 2 5 3.89 6.444E+006 3.366E+006 3 . 1 41E+006 27 0 . 2 4 3.46 6.367E+006 9.498E+005 3 .090E+006 328.00 2 .95 6.089E+006 -1. 22 8E+006 2 .933E+006 338.32 11.27 1 .695E+006 1.651E+006 8.182E+005 409.46 1. 92 8.392E+006 - 4.859E+006 4.020E+006 463. 00 4.40 3 .514E+006 - 8.793E+005 1.679E+006 794.95 4. 2 5 2 .956E+006 5.133E+005 1.393E+006 911. 20 25.80 5.830E+005 7.963E+005 2 .773E+005 964.77 4.99 2 .755E+006 2.332E+006 1. 3 04E+006 968.97 15.80 8.180E+005 5.471E+004 3 .856E+005 1588.20 3 . 22 2 . 32 4E+006 9.522E+005 1.036E+006 Pa-2 31 27.36 10.30 2 .182E+006 2 .18E+006 - 6.332E+005 1.058E+006 283.69 1. 70 1.178E+007 3.257E+006 5 .700E+006 3 00 . 0 7 2 . 47 8 . 106E+006 -1.879E+007 3 .921E+006 3 02.65 2 . 20 8.975E+006 - 4.120E+006 4.340E+006 330. 0 6 l. 40 l .230E+007 -1 . 511E+007 5 . 914E+006 Th-2 3 4 92.38 2 . 13 1 .999E+007 2 .00E+007 1.580E+007 9.801E+006 92.80 2 . 10 2 .003E+007 -2 .446E+005 9.823E+006 112.81 0 . 21 1 . 954E+008 8.889E+007 9.575E+007 U-235 1 43.76 10 .96 2.743E+006 4.64E+005 -9.571E+005 1. 3 42E+006 163.33 5.08 5.402E+006 3 .100E+005 2 .639E+006 185.71 57. 2 0 4.637E+005 1.507E+005 2 .264E+005 2 02. 11 1. 08 2 .349E+007 -8.765E+006 1.146E+007 2 0 5 .31 5.01 4.967E+006 -2 .351E+005 2 .421E+006 Arn-24 1 59.54 35.90 7.482E+005 7.48E+ 0 05 1.379E+00 5 3 .648E+005

     + = Nuclide identified during the nuclide identification
     * = Energy l ine found in the spectrum
     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @    Half-life    too short to be able to perform the decay correction

[217]

****         G A MMA     S P E C T R U M         A N A L Y S I S          *****
.lename: C:\GENIE2K\CAMFILES\B306100AFJFC019GD.CNF iport Generated On                4/11/2016        8:56:35 AM tmple Title                       B306100AFJC019GD tmple Description                 TB ELEVATOR--stmP 1mpl e Identification tmple  Type 1mple  Geometry

!ak Locate Threshold 3.00 iak Locate Range (in channels ) 85 - 8192 !ak Area Range (in channels ) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mple Siz e 1.000E+OOO SQ METER tmple Taken On

quisition Started 3/3 0/ 2 016 1:08:28 PM

.ve Time 600.0 seconds !al Time 600.4 seconds !ad Time 0.06 'i:i Energy Calibration Used Done On 1/27/2015 Efficiency Calibration Used Done On 4/11/2016 Efficiency ID TB VALVE PIT [218]

iak Analysis Report 4/11/ 2 016 8:56:36 AI Page 2

****              P E A K        A N A L Y S I S            R E P O R T               *****

Detector Name: 5456 Sample

Title:

B306100AFJC019GD Peak Analysis Performed on: 4/11 /2 016 8:56:35 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 819 2 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV ) (keV) Area Uncert. Count s 1 2 431- 2 449 2 44 1. 57 610 . 3 0 0.60 6.79E+001 23 . 0 7 1.91E+001 2 5843- 5864 5853.48 14 62 .68 2 . 11 1.41E+00 2 2 5.53 5.62E+OOO

= First peak in a multipl et region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 . 000 sigma

[219]

1terference Corrected Acti ty Report 4/11/ 2 01 6 i6: 3 6 AM Page 3

• *** N UCLIDE I D E N T I F I C A T I O N R E P O R T *****

Sample Titl e : B306100AFJC019GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQ M) Uncertainty K-40 0.994 1460. 82

• 10.66 3 .87614E+006 7.76756E+005

       * = Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold =       0.30 Errors quoted at 2 .00 0 sigma

[220]

1terference Corrected Act: ty Report 4/11 /2 01 6 j6:36 AM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 0.994 3.876141E+006 7.767560E+005

      ?    Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2 .000 s igma
 **********      U N I D E N T I F I E D       P E A K s     **********

Peak Locate Performed on: 4/11/2016 8:56:35 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 610. 3 0 1.1310E-001 34. 00 Tol. M First peak in a multiplet region m Other peak in a multiplet region F Fitted singlet Errors quoted at 2 .000 sigma [221]

1clide MDA Report 4/11/ 2 01 1 8:56:36 AM Page 5

• • • • N U C L I D E M D A R E P O R T *****

Detector Name: 5456 Sample Geometry: Sample

Title:

B306100AFJC0 1 9GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M)

+      K-40       1 46 0 .82* 10.66     4. 93 6E+005     4.94E+005 3 .876E+006         2 .097E +0 05 Cr - 51      32 0 .08     9.91   9.770E+005       9.77E+005 -5.123E+004         4.554E+005 Mn-54        834.85     99.98    7.083E+004       7.08E+004 3.123E+004          3.179E+004 Co-58        810.76     99.45    7.460E+004       7.46E+004 7.783E+00 3         3.366E+004 Co-6 0     1 17 3 . 23  99.85    7.288E+004       5.92E+004 -6 .861E+004        3. 2 64E+004 1332.49      99.98    5.924E+004                     - 1.8 2 9E+004  2 .575E+004 Nb-94        702.65     99.81    7.340E+004       7. 2 4E+004 8.980E+003        3.312E+004 871. 09    99.89    7. 2 37E+004                     1.750E+004    3.254E+004 Sn-113        255.13       2.11   5. 3 59E+006     1. 32E+005 -2 .618E+006       2 .528E+006 391.70     64.97    1. 32 2E+005                     4.215E+004    6 .094E+004 Cs-1 3 4      475.36       1. 48  5.879E+006       8.67E+004 9.847E+005          2 .707E+006 563. 2 5     8.34   8.180E+005                     - 2 .541E+005   3 .671E+005 569. 33    15.37    5.081E+005                       3.458E+005    2 . 3 13E+005 604. 72    97.62    9.571E+004                       3.504E+004    4. 42 5E+004 795.86     85.46    8.667E+004                       4.136E+004   3.911E+004 801 .95      8.69   7.537E+005                     -4.4 2 1E+005  3.353E+005 10 38.61        0.99   6.966E+006                       4.506E+006   3.106E+006 11 67.97        1. 79 4.275E+006                        1.045E+006   1 .926E+006 1 365 . 19      3.02  1.512E+006                     - 4.049E+005    6. 2 69E+005 Cs-137        661.66     85 . 10 9 . 2 03E+004     9 . 2 0E+004 -3.2 03E+004    4 o184E+004 Eu-152       121.78      2 8.67  5 .867E+005      2 .49E+005 -3.809E+005        2 .817E+005 2 44.70       7.61  1.501E+006                     -9.351E+005     7.087E+005 295.94        0.45  2.447E+007                     -1. 7 2 0E+006  1 .151E+007 344.28     2 6.60   3.085E+005                     -5.042E+005     1.418E+005 367.79        0.86  8.751E+006                     -6.585E+006     3 .989E+006 411.1 2      2 . 24 3.744E+006                     - 1 .385E+006   1. 72 1E+006 443.96       2 .8 3 2.889E+006                       4.830E+005    1. 32 4E+006 488.68       0.4 2  2.010E+007                       2 .255E+006   9. 232 E+006 563.99       0.49   1.459E+007                     -4.939E+005     6.585E+006 586. 2 6     0.46   2.166E+007                       2.370E+007    1.007E+007 678.62       0.47   1 .618E+007                    -1. 407E+007    7.335E+006 688.67       0.86   9. 2 71E+006                     4.052E+005    4. 2 21E+006 719.35       0. 2 8 2 .548E+007                      1.164E+007    1.146E+007 778.9 0    12 .96   4.003E+00 5                      5.650E+004    1. 72 3E+005 8 10 .45     0.32   2 .311E+007                      5.863E+006    1.043E+007 867.37       4.26   1.548E+006                       4.446E+005    6.885E+005 919.33       0.43   l.522E+007                     -1.154E+007     6.753E+006 964.08     14.65    4.749E+005                     -1.0 3 8E+005   2 .123E+005 1085.87       10. 2 4  7.033E+005                       5. 2 43E+00 5 3 .150E+005 1089.74         1. 73  3 .771E+006                    -2 .842E+006    1. 668E+OO 6 1 112.07      1 3.69   5.277E+005                       5.080E+004    2.364E+005 1212.95         1. 43  4.746E+006                       8.041E+005    2.106E+006

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4/11/201

• 8:56: 3 6 AM Page 6 1clide MDA Report Nucli de Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( 9s) (pCi/SQ M) (pCi/SQ M ) (pCi/SQ M) (pCi/SQ M)

Eu-152 1249.94 0.19 3.520E+007 2 .49E+005 -2 .152E+006 1.558E+007 1299.14 1. 63 3.630E+006 -3 . 29 9E+005 1.578E+006 1408.01 2 1.07 2 .493E+005 1.512E+005 1.060E+005 1457.64 0.50 3.318E+007 -8.417E+006 1.581E+007 1528.10 0. 2 8 9.743E+006 -3 .410E+006 3.452E+006 Eu-154 123.07 40.40 4.195E+005 1 .96E+005 2 .548E+004 2 .015E+005 247.93 6.89 1 .611E+006 -7. 32 1E+005 7.593E+005 591.76 4.95 1.477E+006 -1.760E+006 6.678E+005 692.42 1. 78 3.987E+006 -2 .225E+006 1.793E+006 723.30 2 0.06 3.661E+005 - 2 .806E+005 1.652E+005 756.80 4.5 2 1. 681E+006 3 .649E+005 7.611E+005 873.18 12.08 6.084E+005 2 .767E+005 2 .741E+005 996. 29 10.48 7.147E+005 3 .101E+005 3 . 22 0E+005 1004.76 18.01 4.027E+005 -2 .983E+005 1.807E+005 1274.43 3 4.80 1.959E+005 7.068E+004 8.694E+004 1596.48 1. 80 3 . 2 48E+006 1.068E+006 1.398E+006 Eu-15 5 45.30 1. 31 9.072E+006 7.45E+005 4.4 3 1E+006 4. 2 81E+006 60.01 1. 22 1.338E+007 1.641E+006 6.414E+006 86.55 30.70 7.447E+005 8.563E+005 3.615E+005 105.31 21.10 8.313E+005 - 5.157E+005 3.998E+005 Tl-2 08 583.19 85.00 1.181E+005 1.18E+005 8. 33 6E+004 5.491E+004 Bi-211 351. 07 13.0 2 9.690E+005 9.69E+005 1.178E+006 4.590E+005 Pb-211 404.85 3 .78 2 .432E+006 l.79E+006 l.915E+006 1.127E+006 427.09 1. 76 4.926E+006 2 .458E+006 2.270E+006 832.01 3.52 l.789E+006 -3.576E+005 7.916E+005 Bi -2 12 39.86 1. 06 9.316E+006 1.18E+006 -1.167E+006 4.342E+006 727. 33 6.67 1.184E+006 3 .531E+005 5.383E+005 785. 3 7 1.10 5.931E+006 2 .641E+006 2 .639E+006 1 620.50 1. 4 7 3.247E+006 - 7 .674E+005 l.347E+006 Pb-212 11 5.18 0 .60 3.320E+007 3.33E+005 1. 075E+007 l.604E+007 23 8.63 43.6 0 3.334E+005 3 .924E+005 1 .594E+005 300.09 3.30 3.157E+006 -1. 766E+006 1 .480E+006 Pb212-XR 74.82 10.28 2.487E+006 1. 3 6E+006 4.378E+006 1.211E+006

77. 11 17.10 1.363E+006 -2 .432E+005 6.619E+005 87.35 3.97 5.637E+006 1. 29 5E+006 2 .7 3 4E+006 89.78 1. 46 l.406E+007 - 4.417E+006 6.803E+006 Bi -2 14 609.32 45.49 2 .908E+005 2.91E+005 4.776E+005 1.377E+005 768.36 4.89 l.706E+006 - 3 .718E+004 7.793E+005 806.18 1. 26 5.585E+006 ~ . 2 78E+006 2 .507E+ 0 06 934.06 3.11 2 .574E+006 3 .855E+005 1.169E+006 1120.29 14.92 5.928E+005 6.951E+004 2 .712E+005 1155. 2 1 1. 63 4.447E+006 2 . 2 91E+006 1.992E+006 1 238.12 5.83 1 .302E+006 4.722E+00 5 5.854E+005 1 280.98 1. 43 4. 2 22E+006 1.003E+006 1.843E+006 1 377.67 3.99 1.540E+006 2.3 47E+005 6.721E+005 1385.31 0.79 8.553E+006 2 .637E+006 3.784E+006 1401.52 1. 33 3 .788E+006 4.567E+005 1.600E+006 1407.99 2 . 39 2 .194E+006 1.331E+006 9. 3 33E+005 1509.21 2 .1 3 2 .4 1 1E+006 -3 .807E+005 1.018E +0 06 1661.27 1. 05 3 .115E+006 8 . 68 1E+005 1.166E+006

[223]

1clide MDA Report 4/11/ 2 01 8:56:36 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M ) (pCi/SQ M) Bi-2 14 1729.59 2.88 1 . 2 79E+006 2 .91E+00 5 - 6.854E+005 4. 95 4E+005 1764.49 15.30 4.941E+005 4.431E+005 2 .198E+005 1847.43 2 .03 2 .564E+006 3.633E+005 l.074E+006

 >               2 118.51       1.16   O.OOOE+OOO                   O.OOOE+OOO O.OOOE+OOO Pb- 2 14      2 41.99     7.25   2 .002E+006 3 .47E+005 2 .1 3 0E+006 9.571E+005 2 95.22   1 8.42   6.144E+005                   3.828E+005 2 .895E+005 351.93    35.60    3.468E+005                   2 .958E+005 1.641E+005 785.96      1. 0 6  6. 2 90E+006                 3 .634E+006 2 .805E+006 Pb214-XR       74.82      5.8 0  4.407E+006 2 .40E+006 7.759E+006 2 .146E+006 77.11     9.7 0  2.403E+006                 -4.287E+005 1.167E+006 87.35    2.24    9.991E+006                  2 . 2 96E+006 4.846E+006 89.78      0 .82  2 .504E+007                -7.864E+006 1. 2 11E+007 Ra-226       186. 2 1    3.64    3.508E+006 3.51E+006 5.870E+005 1.668E+006 Ac-228       129. 0 7    2.42    7.028E+006 3 . 33E+00 5 6.415E+005 3.378E+006 209.25      3.89    3.190E+006                 -1.119E+006 1.514E+006 2 7 0 .24   3.46    3.137E+006                 -9.065E+005 1.475E+006 32 8.00     2.95   3.522E+006                   1. 92 7E+006 1.649E+006 33 8. 32  11.27     8.322E+005                 -6.045E+004 3 .868E +005 409.46      1. 92   4.451E+006                -2 .470E+006 2 .050E+006 463. 00     4.40   1.824E+006                 - l.780E+006 8.344E+005 794.95      4.25   1. 743E+006                  1.499E+006 7.863E+005 911. 2 0  25 .80   3.333E+005                   1. 3 4 7E+005 1.525E+005 964.77      4.99   1 .395E+006                -1. 37 8E+006 6. 2 33E+005 968.97    15.80    4.407E+005                 -7. 12 9E+004 1.970E+005 1 5 88. 2 0   3. 22  1. 749E+006                -6.967E+004 7.486E+005 Pa-2 31        27.36   10. 3 0  l.095E+006 1.09E+006 2.515E+00 5 5.150E+005 283.69      1. 70  6.418E+006                 -1. 7 2 4E+006 3 .019E+006 300.07      2 .47  4. 2 17E+006               -2 . 3 59E+006 1.977E+006 3 02 .65    2 .20  4.374E+006                   6.140E+005 2 .039E+006 33 0 .06    1. 40  7.331E+006                   1.069E+006 3. 430E+006 Th- 23 4        92.38     2 .13  9.322E+006 9.32E+0 0 6 -1.617E+006 4.504E+006 92.80     2 .10  9.472E+006                   2 .767E+005 4.577E+006 112.81       0. 2 1 8.843E+007                   7.361E+006 4. 262 E+007 U-235        143.76     10.96    l.407E+006 2 . 2 6E+ 0 05 -7.299E+005 6.740E+005 163.33       5.08   2.658E+006                   5.777E+004 1. 2 67E+006 185.71     57.20    2.264E+005                   1. 32 6E+005 1.078E+005 2 02 .11    1. 08   1. 2 38E+007                 6.980E+005 5.899E+006 205.31      5.01    2 .551E+006                -4.973E+005 1. 2 13E+006 Am-24 1        59 . 54  35.90    4.451E+005 4.45E+ 00 5 - 7.960E+004 2 .13 2E+005
    + = Nuclid e identified during the nuclide identification
    * = Energy line found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Half-life too short to b e abl e to perform the decay correction

[224]

**************************~ ************************* ****************
"***         GAMM A       S P ~ C T R U M          ANALYS.1S                           *****
.lename: C:\GENIE2K\CAMFILES\00001309.CNF
!port Generated On                 4/ 27/2 017        8:54: 0 8 AM Lmple  Title                       B306100AFJFC0,2.0GD   --

Lmple Description Lmpl e Identification 1mpl e Type tmple Geometry iak Locate Threshold 3.0 0 !ak Locate Range (in channels ) 85 - 8 1 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10.000 keV 1mple Si ze 1. 00 OE+O OO SQM 1mple Taken On 1 /7 /2 013 12:00:00 PM

quisition Started 4/7 /2 016 1:15:23 PM

.ve Time 660.0 seconds !al Time 660.6 seconds iad Time 0.09 % Energy Calibration Used Done On 1/13/20 1 5 Efficiency Calibration Used Done On 4/27/20 1 7 Efficiency ID UlEQDRN SUMP NEW l) at A \{ O. \ l dO. .\cJ 'o y' vJ4~ IJ~t ~lf I 110 [225]

ia k Analysis Report 4/27/2017 8:54:08 AM Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B306l00AFJFC0 2 0GD Peak Analysis Performed on: 4/27/2 017 8:54:08 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV ) Area Uncert. Counts 1 2 636- 2654 2 645.06 661.48 0.89 1. 3 9E+00 2 2 9.93 2 .54E+001 2 5829- 585 1 584 2 .06 1 460.78 1. 73 1.36E+00 2 2 6.14 8.79E+OOO

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2. 000 s igma

[226]

1terference Corrected Acti, y Report 4/27 /2 017 8 4:08 AM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B3 06100AFJFC020GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQM) Uncertainty K-40 1. 000 1460.8 2* 10.66 5.00151E+006 1.05362E+006 Cs-137 1.000 661.66* 85.10 4. 2 0594E+005 1.03947E+005

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold          0. 3 0 Errors quoted at 2 .000 sigma

[227]

1terference Corrected Activ y Report 4 /27/2 017 8 1:08 AM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 5.001512E+006 1 .053624£+006 Cs-137 1. 000 4. 2 05941E+005 1.039465£+005

     ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .000 sigma
 **********    U N I D E N T I F I E D         P E A K S      **********

Peak Locate Performed on: 4/27/201 7 8:54:08 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide All peaks were identified. [228]

iclide MDA Report 4/27/ 2 017 8: 5 4:08 AM Page 5

• • • • N U C L I D E MD A R E P O R T *****

Detector Name: 54 52 Sample Geometry: Sample

Title:

B306100AFJFC020GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) + K-40 1460.8 2

• 10.66 8.105E+005 8.11E+005 5.002E+006 3 .556E+005 Cr-51 32 0.08 9.91 4.747E+018 4.75E+018 -5.902E+017 2 . 2 14E+018 Mn-54 834.85 99.98 9.935E+005 9.93E+005 2 .643E+005 4.450E+005 Co-58 810.76 99.45 8.359E+009 8. 3 6E+009 3.697E+009 3 .778E+009 Co-60 1173.23 99.85 1.332E+005 l. 2 0E+005 5.812E+004 5.954E+004 133 2 .49 99.98 1. 2 01E+005 -9.651E+004 5.244E+004 Nb-94 70 2 .65 99.81 7.421E+004 6.62E +004 -4.035E+004 3.374E+004 871.09 99.89 6. 62 2E+004 3.827E+004 2.930E+004 Sn-11 3 255.13 2.11 4. 21 5E+009 1.46E+008 - 3.251E+008 1.999E+009 391.70 64.97 1.460E+008 1.336E+007 6.847E+007 Cs- 1 3 4 475.36 1. 48 1.565E+007 2 . 92 E+00 5 - 1.139E+006 7. 2 93E+006 563. 25 8.34 2 .396E+006 -l.101E+006 1.094E+006 569. 33 15.37 1.190E+006 - 6.534E+005 5.377E+005 604.7 2 97. 62 3 .234E+005 2.665E+005 1.523E+005 795.86 85.46 2 .915E+005 2 .065E+005 l.332E+005 8 01. 95 8.69 2 . 2 96E+006 -4.588E+004 1.024E+006 1038.6 1 0.99 2 .460E+007 2 .368E+007 l.102E+007 1167.97 1. 79 1.490E+007 -3.470E+005 6.689E+006 1365.19 3.02 7.854E+006 3.650E+006 3 . 429E+006

+ Cs-13 7 661.66* 85.10 1.005E+005 l.01E+005 4.206E+005 4.614E+004 Eu-152 121. 7 8 2 8.67 3.555E+005 3 .03E+005 -1.790E+005 l.713E+005 244.70 7.61 1.190E+006 -6.343E+005 5.677E+005 295.94 0.45 2 .006E+007 1.130E+007 9.510E+006 344.28 2 6.60 3.033E+005 7.972E+004 1 .421E+005 367.79 0.86 9.746E+006 2 .139E+006 4 . 566E+006 411.12 2 . 24 3 .659E+006 -2. 593E+005 1.703E+006 443.96 2 .8 3 3 .083E+006 1 .1 3 8E+006 1.436E+006 488.68 0.4 2 2 .019E+007 3.598E+006 9. 3 42E+006 563.99 0.49 1.617E+007 6.872E+005 7. 3 80E+006 586. 2 6 0. 46 2 . 3 27E+007 2.469E+007 1.086E+007 678.6 2 0.47 1.864E+007 -7.151E+006 8.495E+006 688.67 0.86 1.084E+007 -1. 2 44E+005 4.963E+006 719.35 0.28 2 .957E+007 -2 .922E+007 l. 3 34E+007 778.90 1 2 .96 5. 3 91E+005 -1. 3 12E+006 2 . 3 70E+005 810.45 0.32 2 .755E+007 1.133E+007 1. 2 43E+007 867.37 4.26 1.869E+006 -2 .713E+005 8.292E+005 919.33 0.43 1.714E+007 -1.621E+006 7.483E+006 964.08 14.65 8.629E+005 1. 2 67E+005 3 .987E+00 5 1085.87 10.24 9.355E+005 -3 .491E+005 4.172E+005 1089.74 1.73 5.761E+006 -1.131E+005 2 .580E+006 1 112.07 1 3 .69 6.8 2 1E+005 2 .501E+005 3 .027E+005 1212.95 1. 43 6.455E+006 8. 3 08E+005 2 .8 3 8E+006 [229]

4/27/2 0 17 8:54:08 AM Page 6 tclide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM } (pCi/SQM) (pCi/SQM ) (pCi/SQM) Eu-152 1249.94 0.19 5.420E+007 3.03E+005 3 .772E+007 2 .411E+007 1 299.14 1.63 5.292E+006 -l.743E+006 2 . 29 0E+006 1408.01 2 1.07 4.303E+005 -9.704E+004 1.862E+005 1 457.64 0.50 5 .598E+007 1.351E+008 2 .675E+007 1528.10 0.28 2 .032E+007 -5.393E+006 7.873E+006 Eu-154 123.07 40.40 2 .779E+005 2 .60E+005 8.360E+004 1.339E+005 247.93 6.89 1.357E+006 - 1.536E+005 6.449E+005 591.76 4.95 1.678E+006 -1.452E+005 7.599E+005 692.42 1. 78 5.848E+006 2 .441E+006 2 .680E+006 723.30 2 0.06 5.313E+005 1.762E+005 2 .435E+005 756.80 4. 52 2 .162E+006 -1. 3 04E+005 9.804E+005 87 3 .18 12.08 7.123E +005 1.136E+004 3 .152E+005 996.29 10.48 9.710E+005 - 2 .582E+005 4.340E+00 5 1004.76 18.01 5. 23 9E+005 5.041E+004 2 .318E+00 5 1 274.43 34.80 2 .603E+005 -3.152E+005 1 .121E.+ 005 1 596.48 1. 80 5.464E+006 -1. 3 08E+006 2 . 32 5E+006 Eu-155 45.30 1. 31 1.734E+007 6.67E+005 -6.107E+006 8. 23 1E+006 60.01 1. 22 2 .237E+007 3 .742E+006 1.072E+007 86.55 30.70 6.666E+005 4.542E+005 3.230E+005 105.31 21.10 7. 3 49E+005 -5 .894E+004 3.544E+005 Tl - 2 0 8 583. 1 9 85.00 1.092E+005 1. 0 9E+005 9.195E+004 5.108E+004 Bi -2 11 351. 07 1 3 .02 6.328E+005 6.33E+005 8.342E+005 2 .997E+005 Pb-21 1 404.85 3 .78 1.830E+006 1.83E+006 1.842E+005 8.521E+005 427.09 1. 76 4.302E+006 2.177E+006 2 .011E+006 832.01 3.52 1.870E+006 -6.651E+005 8. 2 95E+005 Bi-212 39.86 1. 06 1.246E+007 1. 2 6E+006 1.117E+006 5.890E+006 727.33 6.67 1. 2 61E+006 9.760E+005 5.793E+005 785.37 1.10 6. 2 41E+006 -1.524E+006 2.795E+006 1 620.5 0 1. 47 5.196E+006 4.623E+005 2.2 1 0E+006 Pb-212 115. 1 8 0.60 1.599E+007 1.91E+005 l.148E+007 7.723E+006 238.63 43.6 0 1.915E+005 2 .134E+005 9.172E+004 300.09 3.30 2 .076E+006 -1.725E+006 9.780E+0 0 5 Pb212-XR 74.82 10 . 28 1.704E+006 9.35E+005 2 . 1 36E+006 8.280E+005 77.11 17.1 0 9.345E+005 2 .757E+005 4.536E+005 87.35 3 .97 3.143E+006 1.841E+006 1.523E+006 89.78 1. 46 7.811E+006 -5 .594E+006 3.776E+006 Bi-214 609.32 45.49 2 .603E+005 2 .60E+00 5 3 .272E+005 1. 2 34E+005 768.36 4.89 1.699E+006 1.150E+006 7.773E+005 8 0 6.18 1. 2 6 5.533E+006 -8 .777E+005 2 .478E+006 934.06 3 .11 2 .420E+006 -1. 803E+006 1.082E+006 1120.29 14.92 7.049E+005 1. 639E+005 3 . 2 2 4E+005 1155.21 1. 63 5.738E+006 5.898E+005 2 .589E+006 1 238.12 5.83 1.649E+006 5.103E+005 7.430E+005 1 280.98 1. 43 5.762E+006 9.499E+005 2 .542E+006 1377.67 3 .99 2.013E+006 6.980E+005 8.788E+005 1385.31 0.79 8.647E+006 1.614E+006 3 .678E+006 1401.52 1. 33 3.756E+006 - 6.446E+006 1.490E+006 1407.99 2 .39 3.212E+006 - 7. 2 42E+005 1.390E+006 1509.21 2 .13 2 .828E+006 1. 3 18E+006 1.159E+006 1661 .27 1. 05 4.413E+006 -4.851E+006 1.652E+006 [230]

1clide MDA Report 4 /27/2017 8:54:08 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (% ) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Bi- 2 14 1729.59 2 .88 2 .557E+006 2 .60E+005 1. 3 81E+006 l.071E+006 1764.49 1 5 .30 7.464E+005 7.025E+005 3 . 33 6E+005 1847.43 2 .03 3 .789E+006 2 . 0 46E+006 1.587E+006

 >               2118.51       1.16 O.OOOE+OOO                    O.OOOE+OOO     O.OOOE+OOO Pb-214      241.99       7. 2 5 l.175E+006 2 .32E+005 l.125E+006           5.629E+005 295. 22   1 8.4 2 4.115E+005                    1.902E+005     1.950E+005 35 1. 93   35.60 2 . 32 1E+005                  2 .854E+005    1 . 099E+005 785.96       1. 06 6.501E+006                   1.687E+006     2 .912E+006 Pb214-XR      74.82     5.80 3.024E+006 1.65E+006 3 .791E+006              1.470E+006 77.11      9.70 1 .650E+006                   4.867E+005     8.007E+005 87.35     2.24 5.578E+006                     3 . 2 68E+006  2 .702E+006 89.78     0 .82 1.393E+007                  -9.974E+006      6.732E+006 Ra-226      186. 2 1    3.64 2.132E+006 2 .13E+006 4.004E+005             1 .023E+006 Ac-228      1 2 9.07    2.42 3.522E+006 3.57E+005 -2 . 2 68E+006          1.697E+006 2 09. 2 5   3.89 1.985E+006                    1.169E+006      9.499E+005 2 7 0.24    3.46 2 .036E+006                   1.056E+006     9.640E+005 328. 00     2.95 2 .077E+006                 - 1.979E+006     9.678E+005 338.32    11. 27 6. 2 96E+005                - 3 .443E+005    2 .959E+005 409.46      1. 92 3 .629E+006                  8.126E+005     1.690E+006 463.00      4. 40 1.724E+006                 - 6.990E+005     8.033E+005 794.95      4.25 2 .039E+00 6                  1.843E+006     9.348E+005 911.20    2 5.80 3 .567E+005                   1. 2 09E+004   1.632E+005 964.77      4.99 2 .146E+006                   1.077E+006     9.916E+005 968.97    15.80 6.735E+005                     7.016E+005     3.109E+005 1588.20       3 . 22 2 .512E+006               -1.612E+005      1.082E+006 Pa-23 1      2 7.36   10. 3 0 1.007E+006 1.01E+006 8.709E+005             4.688E+005 283.69      1. 70 3 .757E+006                -7.785E+005      1 .765E+006 300.07      2 .47 2 .774E+006                -2 . 3 05E+006   1 . 3 07E+006 302.65      2 . 2 0 3.080E+006                 1.075E+006     l.449E+006 330. 0 6    1. 40 4.766E+006                   l , 387E+006   2 . 23 3E+006 Th-234        92.38      2 .13 3 .405E+021 3 . 41E+02 1 1.763E+0 2 1       l.646E+0 2 1 92.8 0     2 .10 3 .456E+0 2 1                3.367E+0 2 1   1.670E+0 2 1 112.81       0.21 2 .866E+0 22                -1.200E+0 22     1.382E+022 U- 235      143.76     10.96 7.096E+005 1.37E+005 -l.150E+005              3.409E+005 163.33       5.08 1.434E+006                    9.760E+004     6.869E+005 185.7 1    57.20 1.374E+005                     5. 3 02E+003   6 . 595E+004 202. 1 1    1. 08 6.372E+006                  -4.778E+006      3.035E+006 205.31      5.01 1.383E+006                     1. 373E+005    6.587E+005 Am-2 41       59.54    35.90 4.708E+005 4.71E+005 -3 .201E+005             2 . 2 54E+005
    + = Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calcul a ted
    @ = Half-li fe too short to be able to perform the deca'l correction

[231]

****         GAMM A        SP t CTR UM           AN ALYS IS                    *****
.lename: C:\GENIE2K\CAMFILES\00001 3 17.CNF iport Generated On                4 /2 7/2017       8:56:01 AM tmple Title                       B306100AFJWC21GD tmple Description                 UNIT 2 EQ DR1TsuMP tmple Identification Lmple Type tmple Geometry iak Locate Threshold                3 .00 iak Locate Range (in channels)         85 -     8 1 92 iak Area Range (in channels)           85 -     8 1 92 lentification Energy Tolerance        10.000 keV tmple Size                          1.000E+OOO SQ METER tmple Taken On

quisition Started 4/11/ 2 016 1:4 2 :0 2 PM

.ve Time 660. 0 seconds ial Time 660.9 seconds iad Time 0. 1 4 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/27/2017 Eff i ciency ID UlEQDRNSUMP NEW Do.+tt Va/idaJ~j b

                                                               ~~r l~-t ... /';' .

II JO [232]

iak Analysis Report 4/ 2 7/ 2 017 8 : 56: 01 AM Page 2

****                P E A K        A N A L Y S I S              R E P O R T                  *****

Detector Name: 54 5 2 Sample

Title:

B306100AFJWC21GD Peak Analysis Performed on: 4/27 /2 01 7 8:56 :00 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. s tart end centroid (keV ) (keV) Area Uncert. Counts 1 2 92- 305 300.61 74.81 0.39 1.34E+002 4 9. 4 6 1.70E+00 2 2 843 - 851 846.98 2 11.57 0.61 2 .41E+001 18.56 2 .89E+001 3 2 430 - 2443 2436. 2 1 609.23 1. 01 5. 1 4E+001 17.94 1.06E+001 4 2 637- 2 65 2 2644.65 66 1. 37 1.29 1.15E+00 2 27.15 2 .33E+001 5 3636- 3647 3641.49 910 .69 0.53 2 . 3 0E+001 13.91 1.00E+OOl 6 5829- 5850 5840.51 1460.39 1.17 l. 1 1E+00 2 29. 11 2 .67E+001 First peak in a multiplet region Other pea k in a multiplet region

= Fitted singlet

rors quoted at 2 . 000 s igma

[233]

1terference Corrected Activ: Report 4/27/20 17 8: ' '. 01 AM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Titl e : B306100AFJWC21GD Nuclide Libr ary Used: C:\GENIE2K\CAMFILES\ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQ M) Uncertainty K-40 1. 000 1460.82* 1 0.66 4.08539E+0 0 6 1.12601E+006 Cs-137 1. 000 661.66* 8 5 .1 0 3. 2 2903E+0 0 5 8.57254E+004

      * = Energy line found in the spectrum.
      @=Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold =        0.30 Errors quoted at 2.000 sigma

[234]

1terference Corrected Activi Report 4/ 2 7 /2 01 7 8: ' 01 AM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 1. 000 4.085 39 1E+006 l.126014E+006 Cs-137 1. 000 3 . 229 0 27E+005 8.572540E+004

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .00 0 sigma
 **********     U N I D E N T I F I E D             P E A K S        **********

Peak Locate Performed on: 4/27/2 01 7 8:56: 00 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 74. 81 2 .0 25 4E- 001 37. 00 To l . Pb214-XR Ba-133 Pb212-XR Pb212-XR Pb214-XR 2 2 11.57 3. 656 4E-00 2 76.92 Tol. Th-227 Ac-228 U-235 U-235 3 609. 23 7.7823E- 00 2 3 4 . 93 Tol. Zr-97 Sb-125 Sb-125 Cs-134 Bi-214 5 910 .69 3 . 4780E- 0 02 6 0. 62 Tol. Eu-152 Ac-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [235]

1clide MDA Report 4/27/ 2 017 3:5 6 :01 AM Page 5

• • • • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B306100AFJWC21GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M)

+      K-40       1460.8 2

• 10 .66 1. 3 11E+006 1. 3 1E+006 4.085E+006 6.056E+005 Cr-5 1 320.08 9.91 6.618E+005 6.62E+005 -6.987E+004 3.101E+005 Mn-54 834.85 99.98 7.854E+004 7.85E+004 2.681E+004 3.555E+004 Co-58 810.76 99.45 7.648E+004 7.65E+004 -8.139E+00 2 3.457E+004 Co-60 117 3 . 23 99.85 9.893E+004 9.89E+004 2 .216E+004 4.486E+004 1 332 .49 99.98 l.005E+005 -8.963E+00 3 4.527E+004 Nb-94 70 2 .65 99.81 7.616E+004 7.62E+004 4.502E+004 3.471E+004 871. 09 99.89 8.174E+004 5.588E+00 3 3.706E+004 Sn- 1 13 255.13 2 .11 3.131E+006 9.86E+004 -8.610E+005 l.479E+006 391.70 64.97 9.863E+004 1.657E+004 4.573E+004 Cs-134 475.36 1. 48 5.375E+006 9.19E+004 3 . 3 14E+006 2 .509E+006 563.25 8.34 8 .814E+005 1. 4 68E+005 4.055E+005 569.33 15.37 4. 2 90E+005 -2 .673E+005 1.953E+005 604.72 97.62 1.041E+005 -7.520E+004 4.889E+004 795.86 85.46 9.192E+004 4.680E+004 4.174E+004 80 1 .95 8.69 9.568E+005 4.084E+005 4. 36 6E+005 1038.61 0.99 7.653E+006 1 .016E+006 3 . 39 6E+006 1167.97 1. 79 5.345E+006 3 . 33 1E+006 2 .416E+006 1 365.19 3.02 2 .158E+006 - l.031E+006 9.114E+005

+ Cs-137 661.66* 85.10 8 .492E+004 8.49E+ 0 04 3. 22 9E+005 3.865E+004 Eu-1 52 12 1. 7 8 28.67 3. 023E+005 2 .49E+005 -1.661E+005 l.457E+005 2 44.70 7.61 8.438E+005 -1.041E+006 3 .986E+005 2 95.94 0.45 l.769E+007 l.132E+007 8.402E+006 344. 2 8 26.60 2 .487E+005 -2 .618E+005 1.163E+005 3 67.79 0 .86 7.829E+006 l.582E+006 3 .655E+006 411.1 2 2.24 3 .075E+006 -9.564E+005 1.430E+006 44 3 .96 2.83 2 .323E+006 -3 .797E+004 1.073E+006 488.68 0.42 l.799E+007 -3 .805E+006 8.355E+006 563.99 0.49 1.451E+007 3 . 2 89E+006 6.659E+006 586. 2 6 0.46 1.813E+007 -1.080E+006 8.410E+006 678.62 0.47 l.578E+007 - 2 .831E+006 7.194E+006 688.67 0.86 8.052E+006 - 5.420E+006 3 .639E+006 719.35 0. 2 8 2 .898E+007 5.637E+006 1.327E+007 778.90 12.96 5 .903E+005 -2 .644E+005 2 .676E+005 810.45 0.32 2 . 3 69E+007 -4.411E+006 1.071E+007 867.37 4.26 1.885E+00 6 -1.930E+006 8.532E+005 919.33 0.43 1.861E+007 2 .383E+006 8.383E+006 964.08 14.65 6.889E+005 8 .032E+005 3 .167E+00 5 1085.87 10.24 7.445E+005 -5 .510E+005 3. 29 4E+005 1089.74 1. 73 4.513E+006 2 .762E+006 2 .003E+006 111 2 .07 13.69 5 .653E+005 -6.936E+005 2 .501E+005 1 21 2 .95 1. 43 5 .852E+006 1.887E+006 2 .596E+006 [236]

1clide MDA Report 4/27/2017 8:56:01 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Eu-15 2 1249.94 0.19 4.682E+007 2 .49E+005 - 1.709E+007 2 .088E+007 1299.14 1. 63 5.001E+006 - 5.941E+005 2 .199E+006 1408.0 1 21. 07 3.862E+005 1. 509E+005 1.686E+005 1457.64 0.50 4.682E+007 1.151E+008 2.236E+007 1 52 8.10 0. 2 8 1.878E+007 7.164E+006 7.454E+006 Eu-154 123.07 40.40 2 . 1 43E+005 2 .14E+005 1.305E+005 1.033E+005 247.93 6.89 8.929E+005 3.641E+005 4. 2 05E+005 591. 76 4.95 1.434E+006 9.063E+005 6.560E+005 692.42 1. 78 3.963E+006 4.591E+005 1.794E+006 723.30 20.06 3.902E+005 1.302E+005 1.781E+005 756.80 4.52 1.711E +006 6.038E+005 7.779E+005 873.18 12.08 6.863E+005 4.955E+005 3.116E+005 996. 2 9 10.48 7.190E+005 2 .711E+005 3. 198E+005 1004.76 18.01 4.907E+005 -2 .404E+005 2 .221E+005 1274.43 34.80 2 .418E+005 6.427E+004 1.070E+005 1596.48 1. 80 4.365E+006 1.498E+006 l.869E+006 Eu-155 45.30 1. 31 9.453E+006 4. 2 8E+005 -6.699E+006 4.452E+006 60.01 1. 22 1.336E+007 -2 .714E+006 6.392E+006 86.55 30.70 4.277E+005 3.687E+005 2 .074E+005 105.31 21.10 4.852E+005 -1.052E+004 2 .345E+005 Tl -2 08 583.19 85.00 1.040E+005 1.04E+005 3.953E+004 4.850E+004 Bi-2 11 351. 07 13.02 7.054E+005 7.05E+005 1.172E+006 3.360E+005 Pb-211 404.85 3.78 1.760E+006 1.76E+006 1.077E+006 8.170E+005 427.09 1. 76 4. 52 6E+006 3.023E+006 2 .123E+006 8 32 .01 3.5 2 1.909E+006 -2 .713E+006 8.490E+005 Bi-212 39.86 1. 06 1.246E+007 1. 1 0E+006 -2.606E+006 5.890E+006 727.33 6.67 1.102E+006 -6.645E+004 4.997E+005 785.37 1.10 7.170E+006 1.066E+006 3. 2 60E+006 1620.50 1. 47 5.393E+006 1.492E+006 2.309E+006 Pb-212 115.18 0.60 1 .633E+007 2 .06E+005 6.512E+006 7.892E+006 2 38.63 43.60 2 .059E+005 2 .630E+005 9.895E+004 3 00.09 3.3 0 2 .173E+006 -2 .340E+006 1.026E+006 Pb212-XR 74.82 10. 2 8 1.781E+006 9.59E+005 3 .652E+006 8.667E+005 77.11 17.10 9.587E+005 7.539E+004 4.656E+005 87.35 3.97 3.235E+006 3 . 1 45E+006 1. 568E+006 89.78 1. 46 7.955E+006 -2.168E+006 3.848E+006 Bi-2 14 609. 32 45.49 2 .269E+005 2 . 2 7E+005 3 .154E+005 1.067E+005 768.36 4.89 1.971E+006 1.970E+006 9.134E+005 806.18 1. 26 6.677E+006 4.370E+006 3.051E+006 934.06 3.11 2.505E+006 1.378E+006 1.124E+006 1120. 2 9 14.92 7.891E+005 5.401E+005 3.645E+005 1155. 2 1 1. 63 5.063E+006 5.418E+005 2 .252E+006 1238.12 5.8 3 1 .749E+006 -8.655E+005 7.932E+005 1 280.98 1. 43 5.754E+006 2.961E+006 2 .538E+006 1377.67 3.99 2.168E+006 4.740E+005 9.563E+005 1385.31 0.79 9.867E+006 4.761E+005 4. 2 89E+006 1401. 52 1. 33 5.755E+006 2 .452E+006 2 .490E+006 1407.99 2.39 3.399E+006 1. 32 8E+006 1 .484E+006 1509.21 2.13 3.663E+006 1. 2 69E+006 l.577E+006 1661.27 1. 05 5. 367E+006 - 4.196E+006 2 .129E+006 [237]

1clide MDA Report 4 /2 7/ 2 017 8:56:01 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) {%) (pCi/SQ M) {pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Bi -2 14 17 29 . 5 9 2 .88 2 .161E+006 2 . 2 7E+005 9.193E+005 8.7 3 1E+005 1764.49 15.3 0 7.170E+005 4. 12 2E+005 3 .189E+005 1847.4 3 2 .03 3 .409E+006 1.589E+006 1. 3 97E+006

 >                21 18.51      1.16    O.OOOE+OOO                      O.OOOE+OOO O.OOOE+OOO Pb- 2 1 4    2 41.99     7.25    1.160E+006 2 .50E+005 9.453E+00 5 5.559E+005 2 95. 22   18.42    4.178E+005                   - 8.592E+004 1.982E+005 351.93     35.60    2 .501E+005                    2 . 2 60E+005 1.189E+005 785.96      1. 06   7.654E+006                     4. 3 27E+ 00 6 3 .489E+006 Pb214-XR       74.82     5.80    3 .157E+006 1.69E+006 6.473E+006 l .536E+006

77. 11 9.70 1.690E+006 1.329E+005 8.209E+005 87.35 2 . 24 5.733E+006 5.575E+006 2 .780E+006 89.78 0 .82 1.416E+007 -3 .861E+006 6.851E+006 Ra- 226 186. 2 1 3 .64 2 . 2 60E+006 2 . 2 6E+006 1. 52 0E+006 1.087E+006 Ac- 2 2 8 129. 0 7 2 .42 3 .420E+006 4. 3 8E+005 - 7.734E+005 1.646E+006 209.25 3 .89 1.839E+006 - 1.513E+005 8.768E+005 270.24 3 .46 2 .090E+006 8.430E+005 9.907E+005 328.00 2 .95 2 .544E+006 2 .748E+005 1. 2 01E+006 338.32 11.27 6. 938E+005 3.388E+005 3 . 28 0E+005 409.46 1. 92 3 .490E+006 -2 .427E+006 1. 620E+006 463.00 4.40 1.605E+006 -4.519E+005 7 .437E+005 794.95 4.25 1.847E+006 -5.872E+005 8.387E+005 911.20 25.80 4.385E+005 4.099E+005 2 .041E+005 964. 77 4 . 99 2.024E+006 2 .329E+006 9.302E+005 968.97 15.80 6.541E+005 6.443E+005 3.012E+005 1588.2 0 3 . 22 2.512E+006 9.621E+005 1.082E+006 Pa - 2 31 27.36 10.30 8.098E+005 8.10E+005 4.101E+005 3.700E+005 283.69 1. 70 3.800E+006 1 .906E+006 1.787E+006 300.07 2.47 2.903E+006 - 3.127E+006 1. 3 71E+006 302.65 2.20 3.163E+006 - 1.315E+006 1. 490E+006 330.06 1. 40 5.326E+006 2 .192E+006 2 .513E+006 Th-234 92.38 2. 1 3 5.331E+006 5.33E+006 4.963E+005 2 .578E+006

92. 80 2.10 5.401E+006 1 . 762E+006 2 .612E+006 112.8 1 0. 2 1 4.766E+007 2 .891E+007 2 .305E+007 U-235 143.76 10.96 6.994E+005 1.44E+005 -2 .863E+00 5 3 . 35 8E+005 163.33 5. 0 8 1 .565E+006 1.584E+006 7.525E+005 185.71 57. 2 0 1.437E+005 1.422E+005 6.909E+004 202.11 1. 08 6.984E+006 5 .192E+006 3.341E+006 2 05.31 5.01 1.449E+006 -2 .960E+005 6.915E+005 Am- 2 41 59.54 35.90 4.604E+005 4.60E+005 7.031E+003 2 . 2 02E+005

    + = Nuc lide identified during the nuclide identification

• Energy line found in the spectrum

    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Half-life too short to be abl e to perform the decay correction

[238]

*************************~ *************************~ k****************
****         GAMM A       S P E C T R U M         A N A L Y S I S             *****
.lename: 54 52

!port Generated On 4/ 1 9/2016 12:44:43 PM

                                                        ~~

tmpl e Title B306100AFJFC02ZGD tmple Description TB 560 ~ tmple Identification tmple Type tmple Geometry !ak Locate Threshold 3 .00 !ak Locate Range (in channels ) 85 - 8192 !ak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Size 1.000E+OOO SQM tmple Taken On

quisition Started 4/19/2016 1 2

34:42 PM

.ve Time 600.0 seconds !al Time 600.3 seconds iad Time 0.04 ~~ Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/20 1 6 Efficiency ID TBFLOOR

                                                                ~Qtd VaJ,*cfa.~,J kJ
                                                                 ~                 lY I,_ t. ~IF
                                                                 /Ila

[239]

iak Analysis Report 4/19/2 0 16 12 :44:4 3 Ph Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 54 52 Sample

Title:

B306100AFJFC0 2 3GD Peak Anal y sis Performed on: 4/19/ 2 0 1 6 12:44:42 PM Peak Analysi s From Channel: 85 Peak Analysi s To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid ( keV) (keV ) Area Uncert. Counts 1 297- 306 300.61 74.81 0.7 2 4.24E+001 32 .75 9.76E+001 2 332- 346 340.14 84.7 0 0.40 2 .18E+001 36.50 1.07E+00 2 3 1400- 1414 1407.57 351. 86 0. 72 2 .96E+001 19.99 2 .44E+001 4 1958 - 1967 1962.49 490.72 0.46 8.77E+OOO 7.56 2 .23E+OOO 5 2 430 - 2 441 2 435.15 608.97 1. 06 3 .23E+001 15. 05 9.70E+OOO 6 2 635- 2 651 2 645. 29 66 1. 53 1. 32 9 .52E+001 22 . 22 8.76E+000 7 5323- 5334 5328.14 13 32 . 3 5 0.47 1.14E+001 10.15 5.62E+OOO 8 5830- 5848 5839.16 1460.06 0.86 8.88E+001 19.60 2 . 2 3E+OOO First peak in a multipl et region

=  Other peak in a multiplet region

= Fitted singlet -rors quoted at 2.000 sigma [240]

1terference Corrected Acti .ty Report 4/ 1 9 /2 016 l L 44:4 3 PM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFJFC023GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB

 . . . . . .. . .. . . . . . . . . . . IDENTIFIED NUCLIDES             ............... . ....

Nucl ide Id Energy Yield Activity Acti vi t: 1 Name Confidence (keV) (%) (pCi/SQM ) Uncertainty K-40 0 .999 1460.82* 10.66 6.05122E+00 5 1. 43591E+005 Ba-13 3 0 .579 79.61* 2 . 65 3 .79592E+00 5 3 .03 32 8E+005 81.00* 32.90 1.57523E+004 2 .65196E+004 276.40 7.16 30 2 .85 18.34 356. 01

• 62.05 1. 71608E+004 1.19050E+004 383.85 8.94 Cs - 137 1. 000 661.66* 85.10 5. 523 83E+004 1.44948E+004

        * = Energy l ine found in th e spectrum.
        @ = Energy line not used for Weighted Mean Activi t r Energy Tolerance :                   10.000 keV Nuclide confidence index threshold=                        0. 3 0 Errors quoted at 2 . 000 sigma

[241]

1terference Corrected Acti .ty Report 4/ 1 9/ 2 01 6 1~ 44:43 PM Page 4 "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0.999 6.051 2 23E+005 1.435909E+005 X Cd-109 0.982 Ba-133 0.579 1. 7 3 8888E+004 1.085385E+004 Cs-137 1. 000 5.52 3 8 2 7E+004 1.449484E+004 X Eu-155 0.301 X Bi-211 0.999

      ? = Nuclid e is part of an undetermined solution X = Nuclide rejected by the interference analysi s
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at         2 . 000 sigma
 **********       U N I D E N T I F I E D             P E A K S          **********

Peak Locate Performed on: 4/19/20 1 6 1 2 :44:42 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV ) Counts per Second ~ Uncertaint~/ Type Nuclide 4 4 90 . 7 2 1 . 46 21 E- 00 2 8 6. 2 3 Tol. Eu-15 2 5 608.97 5.3839E- 00 2 46.58 Tol. Zr-97 Sb-125 Sb-125 Cs - 134 Bi - 2 14 7 1332.35 1 .8971E-00 2 89. 2 0 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [242]

1clide MDA Report 4 / 1 9/2 0lb 12:44:4 3 PM Page 5

• • • • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B306100AFJFC023GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB Nuclide Energy Line MDA Nuclide MDA Activity Dec. Level Name (keV ) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) (pCi/SQM)

+      K-40       1460. 82

• 1 0 .66 7.904E+004 7.90E+004 6.051E+005 3.0 3 0E+004 Cr-51 320.08 9.91 1.255E+005 1. 2 5E+005 - 1.438E+004 5.806E+004 Mn-54 834.85 99.98 1.525E+004 1.53E+004 6. 3 47E+00 3 6.883E+00 3 Co-58 810.76 99.45 1.648E+004 1.65E+004 1. 22 6E+004 7.501E+00 3 Co-60 1 173. 2 3 99.85 1.685E+004 1. 68E+004 1. 21 5E+004 7.545E+00 3 1332.49 99.98 2 .001E+004 1. 26 0E+004 9.071E+00 3 Nb-94 7 02 .65 99.81 1. 32 0E+004 1. 2 6E+004 -4.377E+00 3 5.914E+003 871. 09 99.89 1.259E+004 - 9.673E+00 3 5.535E+003 Sn-1 1 3 255.13 2 .11 6.539E + 005 .2 .02E+004 -1. 3 71E+00 5 3 .073E+005 391.70 64.97 2 .024E+004 - 1.156E+004 9. 3 31E+003 Cs- 134 475.36 1. 48 9.418E+005 1.69E+004 5.984E+004 4.325E+00 5 563.25 8.34 1.518E+005 1.358E+004 6.850E+004 569.33 15.37 9.015E+004 5.953E+004 4.104E+004 604.72 97.62 1 .918E+004 -9.100E+00 3 8.933E+003 795.86 85.46 1 .690E+004 2 .300E+00 3 7.601E+003 8 01. 95 8.69 1.696E+005 2 .649E+004 7.641E+004 1 038.61 0 .99 1.202E+006 4.307E+005 5.175E+005 1 167.97 1. 79 8.857E+005 - 4.636E+004 3 .940E+005 1 365.19 3. 02 3.861E+005 6 . 0 49E+004 1.617E+005

+ Cs- 137 661.66* 85 .10 l. 1 70E+004 1.17E+004 5.524E+004 5.066E+00 3 Eu-152 1 21. 7 8 28.67 5.065E+004 5.07E+004 -5.477E+004 2 .421E+004 2 44.7 0 7.61 2.028E+005 9.138E+004 9.605E+004 2 95.94 0.45 3.429E+006 4. 27 0E+005 1.615E+006 344.28 26.60 5.222E+004 1.265E+004 2 .430E+004 367.79 0.86 1 .628E+006 - 2 .020E+005 7.563E+005 411.12 2 . 24 6.367E+005 1.618E+005 2 .948E+005 443.96 2 .8 3 5.626E+005 5. 3 49E+00 5 2 .620E+005 488.68 0.4 2 3.056E+006 9.186E+00 5 1. 3 91E+006 563.99 0.49 2.580E+006 -7. 2 09E+004 1 . 1 64E+006 586. 2 6 0.46 3.763E+006 1.671E+006 1.745E+006 678.62 0.47 2 .797E+006 2 .098E+006 1. 25 5E+006 688.67 0.86 1.406E+006 -1.116E+006 6. 2 40E+005 7 1 9.35 0.28 4.860E+006 1 .7 3 4E+006 2.1 8 1E+006 778.90 12.96 9 .654E+004 - 7.185E+003 4. 2 71E+004 81 0 .45 0.32 5 .037E+006 2 .612E+006 2 . 2 90E+006 867. 3 7 4. 2 6 3 . 2 83E+005 -4.194E+004 1. 4 64E+005 919. 33 0.43 3 .367E+006 -4. 2 71E+00 5 1.501E+006 964.08 14.65 1.307E+005 1. 3 83E+005 5.992E+004 1085.87 10. 2 4 1.334E+005 -8.003E+004 5.845E+004 1089.74 1. 73 8.496E+005 -1.807E+003 3.759E+005 111 2 .07 1 3 .69 1.084E+005 -7. 25 0E+004 4.797E+004 1212.95 1. 4 3 1. 2 41E+006 8.698E+00 5 5 .580E+005 [243]

4/ 1 9 / 2 01 6 12:44:43 PM Page 6 iclide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) Eu-15 2 1 249.94 0.19 6.886E+006 5.07E+004 3 . 12 0E+006 2 .965E+006 1299.14 1. 63 9.403E+005 1.780E+005 4.135E+005 1408.01 21. 07 5.883E+004 -3 . 37 7E+003 2 .484E+004 1457.64 0.50 7.005E+006 1.194E+007 3 . 3 07E+006 1528.10 0. 2 8 3 . 736E+006 1.590E+006 1.510E+006 Eu-154 123.07 40.40 3.632E+004 3. 63E+004 -3.077E+004 1.736E+004 247.93 6.89 2 . 072E+005 8.057E+004 9.766E+004 591. 7 6 4.95 2 .661E+005 3.438E+004 1. 2 03E+005 692.4 2 1. 78 7.497E+005 -4.069E+005 3 . 3 65E+005 723.30 20.06 6 . 892E+004 - 1.139E+003 3 .099E+004 756 . 80 4 . 52 2 .850E+005 5.280E+004 l. 2 68E+005 873.18 12.08 l.042E+005 -8.008E+004 4.582E+004 996. 2 9 10.48 l . 658E+005 1.964E+003 7.518E+004 1004.76 18.01 8.351E+004 8.889E+003 3 . 72 4E+004 1274.43 3 4.80 4.016E+004 -3 . 2 68E+004 1.746E+004 1596.48 1. 80 5.128E+005 - 7. 2 58E+005 1. 987E+005 Eu-155 45.30 1. 3 1 7.492E+005 4.70E+004 l.758E+005 3.501E+005 60.01 1. 22 9.889E+005 -5.646E+005 4.681E+005 86.55* 30.70 4.696E+004 1. 688E+004 2 . 2 43E+004 10 5.31 21.10 7. 2 27E+004 2 .540E+004 3.461E+004 Tl -2 08 583.19 85.00 2 . 098E+004 2 .10E+004 2 .373E+004 9.753E+00 3 Bi -2 11 351.07* 13.02 8. 3 65E+004 8. 3 6E+004 8.178E+004 3.809E+00 4 Pb- 2 11 404.85 3.78 3.467E+005 3 .47E+005 6. 23 0E+004 1.595E+005 427. 0 9 1. 76 7.955E+005 -5.626E+004 3 .673E+005 832. 0 1 3.5 2 4.189E+005 -3.4 1 9E+004 l.883E+005 Bi-212 39 . 86 1. 06 9.004E+005 2 . 1 8E+005 -8. 39 6E+004 4.199E+005 727.33 6.67 2.179E+005 8.812E+004 9.849E+004 785.37 1.10 1.189E+006 2 .071E+005 5. 2 88E+005 1 62 0 .50 1. 47 4.891E+005 -5 . 333E+005 1.733E+005 Pb-2 1 2 11 5.18 0.60 2.437E+006 3.92E+ 00 4 -2 .664E+006 1.164E+006 23 8.63 43.60 3.919E+004 4.470E+004 l.868E+004 30 0 . 0 9 3.30 4. 32 6E+005 -5.7 2 9E+00 5 2 .027E+005 Pb212-XR 74.8 2 10. 2 8 1.876E+005 l.05E+005 2 .712E+005 9.067E+004 77.11 17.10 1.050E+005 - 4.425E+00 3 5.064E+004 87.35 3.97 4.462E+005 5. 2 25E+004 2 .150E+005 89.78 1. 4 6 l.158E+006 7.493E+005 5.571E+005 Bi -2 14 609.32 45. 4 9 4.161E+004 4.16E+004 3 .735E+004 l.939E+004 768.36 4.89 2 . 5 96E+00 5 9.569E+004 l.152E+005 8 0 6. 1 8 1. 26 1 . 187E+006 4.398E+005 5.358E+005 934. 0 6 3.11 4.089E+005 3 .175E+005 l.792E+005 1120. 2 9 14.92 l .122E+005 l.104E+005 5.036E+004 1 155. 2 1 1. 63 9.257E+005 3 .691E+004 4.096E+005 1 238.1 2 5.83 2.680E+005 - 7.408E+004 l.186E+005 1 280.98 1. 43 l .084E+006 8.957E+005 4.781E+005 1377.67 3.99 3.652E+005 -1.1 2 8E+005 l.587E+005 1385.31 0.79 1.673E+006 l.067E+006 7.163E+005 14 01. 52 1. 33 l.198E+006 6.692E+005 5. 2 66E+005 1407.99 2.39 5.177E+005 -2 .972E+004 2 .187E+005 1509.21 2 .13 6.064E+005 -4. 2 99E+005 2 .561E+00 5 1661. 2 7 1. 05 l .25 1E+006 9. 3 84E+004 5. 23 9E+00 5 [244]

1clide MDA Report 4/19 /2 01t 12 : 44: 43 PM Page 7 Nuclide Energy Yield Line MDA Nucli de MDA Activity Dec. Level Name (keV ) Pl (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Bi-2 14 17 29 .59 2 .88 3 .947E+005 4.16E+004 1.679E+005 1.595E+005 1764.49 15. 3 0 1.072E+005 7.461E+004 4.639E+004 1847.43 2 .0 3 4.436E+005 -4.052E+005 1.660E+005

 >                21 1 8.51     1.16    O.OOOE+OOO                    O.OOOE+OOO O.OOOE+OOO Pb- 2 1 4     241.99      7.25    2 . 2 48E+005 4.58E+004       4. 62 2E+004 1 .069E+005 295. 22   18.42     8.374E+004                    6.776E+004 3 .945E+004 351. 93   35.60     4.582E+004                   2 .880E+004 2 .154E+004 785.96      1. 06   1. 2 36E+006                 2 .177E+005 5.500E+005 Pb21 4-XR       74.82     5.80    3 .325E+005 1.85E+00 5        4.806E+005 1.607E+005

77. 11 9.70 1.852E+005 -7.802E+00 3 8.927E+004 87.35 2.24 7.908E+005 9. 2 60E+004 3.810E+005 89.78 0.82 2.062E+006 1. 3 34E+006 9.918E+005 Ra- 22 6 186.21 3.64 3.916E+005 3 . 92E +005 -1.560E+005 1.860E+005 Ac- 22 8 129.07 2.42 6.766E+005 5 . 5 6E+004 3.786E+005 3 . 2 49E+005 209. 2 5 3.89 3.801E+005 1.058E+005 1.804E+005 270. 2 4 3.46 3.790E+005 O.OOOE+OOO 1.772E+005 328.00 2 .95 4.489E+005 7.081E+004 2 .085E+005 338. 3 2 11. 2 7 1.329E+005 8. 2 64E+004 6. 2 19E+004 40 9.46 1. 92 7.072E+005 3.812E+005 3. 2 62E+005 463.00 4.40 3.218E+005 1.054E+005 1.482E+005 794.95 4. 2 5 3.453E+005 2 .015E+005 1.556E+005 911. 2 0 25 .80 5.561E+004 -3 . 2 86E+004 2 .480E+004 964.77 4.99 3.752E+005 1.713E+005 1.716E+005 968.97 15.80 1.100E+005 1.054E+005 4.996E+004 1588.20 3 . 22 3.768E+005 1.900E+005 1.563E+005 Pa -2 31 27.36 10.30 6.194E+004 6.19E+004 2 .893E+004 2 .785E+004 283.69 1. 70 8.112E+005 6.524E+005 3 .799E+005 300.07 2.47 5.779E+005 -7.654E+005 2 .7 0 8E+005 302.65 2.20 6.309£+005 -5.166E+005 2.950E+005 330. 0 6 1. 40 9.787E+005 2 .363E+005 4.557E+005 Th- 23 4 92.38 2.13 7. 3 53E+005 7. 3 5E+ 00 5 -4.477E+004 3 .526E+005 92.8 0 2 .10 7.478E+005 3 .361E+005 3 .586E+005 11 2 .81 0. 2 1 6.895E+006 -4.732E+006 3 . 2 95E+006 U- 2 3 5 143.76 10.96 1.375E +005 2.5 1E+004 9. 62 4E+00 3 6.574E+004 163.33 5.08 2 .743E+005 -1.732E+00 5 l.304E+005 185.71 57. 2 0 2 .508E+004 -3 .648E+00 2 1.192E+004 202.11 1. 08 1. 2 91E+006 -1. 2 06E+00 6 6.112E+005 205.31 5.01 2 .853E+005 9.150E+004 1.352E+00 5 Am- 2 41 59.54 35.90 3 . 3 16E+004 3 . 3 2E+004 -7.423E+003 1.568E+004

    + = Nuclid e identified during the nuclide identification
    * = Energy line found in the spectrum
    >     Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calcul a ted
    @ = Half-l ife too short to be abl e to perform the decay correction

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• • • • • GAMM A S P E C T R U M A N A L Y S I S * ****

Filename: 5452 Report Generated On 4/1 3/2 016 1: 3 1:14 PM Sample Title B30 6 100AFJFSM023GD Sample Description Ul TB COL G2 7 Sample Identification Sample Type Sample Geometry Peak Locate Threshold 3 .00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 1. OOOE+OOO SQM Sample Taken On Acquisition Started 4/13/ 2 016 1: 2 0:1 2 PM Live Time 660.0 s econd s Real Time 660.9 second s Dead Time 0. 1 4 % Energy Calibration Used Done On 1/1 3 / 2 015 Efficiency Calibration Used Done On 4 / 1 3/ 2016 Efficiency ID DTMUD_FLOOR Ua+A Va}/dtt/c=J bf Q~~ IJ.-,-lr II I tJ [246]

Peak Analysis Report 4/13/2016 1:31:14 PM Page 2

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B306100AFJFSM0 23GD Peak Analysis Performed on: 4/13/2016 1: 3 1:14 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 123 116.5 1 28 . 72 1. 29 5.59E+002 96. 96 6.19E+002 2 232 6- 233 7 2 331.64 583. 0 7 0.83 2.53E+001 15.5 0 1.37E+001 3 2428- 2446 2 436.49 609.30 1. 51 9.99E+001 22 .8 0 9.06E+OOO 4 5829- 585 2 5842.73 1 460.95 0.89 1.32E+002 2 5.86 8.84E+OOO 5 7051- 7064 7057.62 1 764.48 0.39 3.54E+001 12.62 1 .64E+OOO M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2. 000 sigma [247]

Interference Corrected Activity Report 4/1 3/2 016 1: 3 1: 14 PM Page 3

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFJFSM023GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K-40 1. 000 1 460.8 2

• 10.66 8.14524E+005 1.74362E+005 Tl-208 1. 000 583. 1 9* 85. 0 0 1.24484E+004 7 .75903E+003 Bi-2 1 4 0. 32 6 609. 32
• 45.49 9.37674E+004 2.41767E+004 768.36 4.89 806. 1 8 1. 26 934. 0 6 3.1 1 11 20. 2 9 14.9 2 11 55. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377.6 7 3.99 1385.3 1 0.79 1401.52 1. 33 1407.99 2 .39 1509.21 2 .13 1661. 2 7 1. 05 1729.59 2 .88 1764.49* 15.30 l.70405E+005 6.23228E+004 1847.43 2 .03 2118.51 1.16 P a-23 1 0 .3 7 6 27.36
• 10.30 l .15 4 8 8E +0 06 3.43648E+0 05 2 83.69 1. 70 300.07 2 .47 302.65 2 . 20 330.06 1. 40 Th- 23 1 0 .43 0 25.64
• 14.10 8.43633E+005 2 .479 2 7E+005 84.21 6.60 89.95 1. 00

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy TolerRnce :         10.000 keV Nuclide confidence index threshold              0.30 Errors quoted at 2 . 000 sigma

[248]

Interference Corrected Activity Report 4/13/ 2 016 1:31:14 PM Page 4

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 8.145 2 38E+005 1.743619E+005 Tl- 2 08 1. 000 1. 2 44840E+004 7.7590 3 3E+003 Bi- 2 14 0.326 1.037919E+005 2 . 2 54013E+004

   ?  Pa-231        0.376        1.154877E+006      3 .436478E+005
   ?  Th-231        0.430        8.436334E+005      2 .479270E+005
      ?    Nuclide is part of an undetermined solution X    Nuclide rejected by the interference analysis
      @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2 .000 sigma
  **********     U N I D E N T I F I E D        P E A K S        **********

Peak Locate Performed on: 4/13/2016 1: 3 1:14 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertaint y Type Nu clide Al l peaks were identified. [249]

Nuclide MDA Report 4/13/ 2 016 1:31:14 PM Page 5 N U C L I D E MD A R E P O R T ***** Detector Name: 5452 Sample Geometry: Sample

Title:

B306100AFJFSM023GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM )

 +      K-40       1460.8 2

• 10.66 l.367E+005 1. 3 7E+005 8.145E+005 5.999E+004 Cr-51 320.08 9.9 1 l.463E+005 1 .46E+005 7.860E+004 6.897E+004 Mn-54 834.85 99.98 1.417E+004 1 .42E+004 8.830E+003 6.417E+003 Co-58 810.76 99.45 1.542E+004 1 .54E+004 - 1.700E+003 7.046E+003 Co-60 1173.23 99.85 1.601E+004 1.46E+004 1.281E+004 7. 2 11E+00 3 1332.49 99.98 1.464E+004 7.987E+003 6.479E+003 Nb-94 702.65 99.8 1 1.505E+004 1. 2 7E+004 1.132E+004 6.906E+003 871.09 99.89 1.265E+004 2.655E+003 5.642E+003 Sn-113 2 55.13 2.11 7.602E+005 2 .16E+004 6.112E+005 3.624E+005 391.70 64.97 2. 158E+004 - l.004E+004 1 .008E+004 Cs-134 475.36 1. 48 9.161E+005 1.80E+004 3.933E+005 4.236E+005 563.25 8.34 1.581E+005 9.369E+004 7. 2 41E+004 569.33 15.37 8.113E+004 9.393E+003 3.694E+004 604.72 97.62 2.282E+004 -2 .601E+002 1.082E+004 795.86 85.46 1.800E+004 -9.255E+003 8.235E+003 801. 95 8.69 1.756E+005 1.082E+004 8.024E+004 1038.61 0.99 1.748E+006 1. 093E+006 7.985E+005 1167.9 7 1. 79 8 . 617E+005 4.464E+005 3.867E+005 1365.19 3.02 4.462E+005 2.109E+005 1.948E+005 Cs - 137 661.66 85.10 1.679E+004 1.68E+004 3.265E+003 7.687E+003 Eu- 1 52 1 21.78 28.67 6.491E+004 5.45E+004 2.247E+004 3.145E+004 244.70 7.61 2.112E+005 -3.063E+004 1.0 0 8E+005 295.94 0 .45 3.856E+006 5.028E+OOG 1 .839E+006 344. 2 8 26.60 5.445E+004 -2 . 611E+004 2 .560E+004 367.79 0.86 1.617E+006 5.358E+005 7.566E+005 411.1 2 2 .24 6.555E+005 -1.429E+005 3.066E+005 443.96 2 .83 4.980E+005 1.549E+005 2.316E+005 488.68 0.42 3.630E+006 - 6.989E+005 1.692E+006 563.99 0.49 2.656E+OD6 5.623E+005 1. 21 5E+006 586.26 0.46 3.764E+006 -3 .067E+004 1.759E+006 678.62 0.47 2 .562E+006 -1.615E+005 1.152E+006 688.67 0.86 1.509E+006 1.041E+006 6.830E+005 719.35 0. 2 8 5.444E+006 1.718E+006 2 .498E+006 778.90 12.96 1.011E+005 2 .035E+004 4.555E+004 810.45 0.32 4.719E+006 - 1.651E+006 2.154E+006 867.37 4.26 2.720E+005 -5.326E+004 l .200E+005 919.33 0 . 43 3.095E+006 1.568E+005 1 .383E+006 964.08 14.65 1. 2 43E+005 4.509E+004 5.726E+004 1085.87 10.24 l.551E+005 -7.014E+004 7.009E+004 1089.74 1. 73 8.471E+005 -1.631E+004 3.794E+005 111 2 .07 13.69 1. 081E+005 - 1.538E+005 4.842E+004 121 2 .95 1. 43 1.121E+006 -2 .474E+005 5.040E+005

[250]

Nuclide MDA Report 4/13/2016 1 : 3 1 :14 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) Eu-15 2 1249.94 0.19 7.987E+006 5.45E+004 2 .790E+006 3.562E+006 1 29 9.14 1. 63 7.612E+005 -2 .088E+005 3.294E+005 1408.01 2 1.07 7.176E+004 -7.629E+001 3.175E+004 1457.64 0.50 7.811E+006 1 .854E+007 3.729E+006 1528.10 0.28 3 . 3 77E+006 - 5.288E+005 1.365E+006 Eu-1 5 4 123.07 40.40 4.572E+004 4.29E+004 -8.886E+003 2 . 2 15E+004 247.93 6.89 2 .128E+005 -2 . 2 47E+005 1.011E+005 591.76 4.95 2 .762E+005 -2 .479E+005 1.266E+005 692.4 2 1. 78 7.417E+005 -3 . 32 2E+00 5 3 .363E+005 723.30 2 0.06 7.994E+004 2 .858E+004 3 .684E+004 756.80 4. 52 3 . 2 86E+005 3 .899E+004 1.501E+005 873.18 1 2 .08 9 .164E+004 -8.644E+004 4.016E+004 996.29 10.48 1.558E+005 -4.183E+004 7.095E+004 1004.76 18.01 8.362E+ 0 04 -3 .534E+004 3 .773E+004 1274.43 3 4.80 4.294E+ 0 04 l.444E+004 1.910E+004 1596.48 1. 80 6. 1 2 4E+005 -2 .412E+005 2 .540E+OOS Eu-155 45.30 1. 3 1 2 .483E+006 7. 6 6E+004 2. 568E+005 1. 2 19E+006 60.01 1. 22 1.778E+006 -1.774E+006 8.653E+005 86.55 3 0.70 7.659E+004 8. 3 79E+004 3.736E+004 1 05.3 1 2 1.10 9.381E+004 3 .971E+003 4.554E+004 Tl-208 583.19* 85.00 1.085E+004 1.09E+004 1. 2 45E+004 4.761E+00 3

+

Bi- 2 11 351 . 07 13.02 1.340E+005 1.34E+005 1.418E+005 6.365E+004 Pb-211 404.85 3 .78 4.188E+005 3.90E+ 0 05 1.063E+005 1.970E+005 42 7.09 1. 76 7.542E+005 4.074E+005 3 .497E+005 8 32 . 01 3.52 3.900E+005 7 . 848E+004 1.760E+005 Bi -212 39.86 1. 06 3.730E+006 2 .24E+005 7.795E+005 1 .838E+006 727.33 6.67 2.238E+005 4.493E+004 1.025E+005 785.37 1. 10 1.420E+006 1.045E+006 6.508E+005 16 2 0 . 50 1. 4 7 5.720E+005 l.905E+005 2 . 2 1 6E+005 Pb-2 1 2 1 15 . 1 8 0 .60 3.002E+006 4.32E+004 -l.268E+006 1 .453E+006 238.G3 43.60 4.3 1 5E+004 6.646E+004 2 .075E+004 3 00 . 0 9 3. 3 0 4.532E+005 -4.528E+005 2 .144E+005 Pb2 1 2-XR 74.82 10.28 2 . .531E+005 1.43E+005 4.176E+005 1 .238E+005 77.11 17.10 1.426E+005 1.700E+005 6.964E+004 87.35 3.97 5.874E+005 2 .800E+005 2 .864E+005 89.78 1. 46 1.5 22E +006 1 .718E+005 7.411E+005

+      Bi-21 4      609.3 2

• 45.49 1. 9 44E+004 1 .94E+004 9 . 3 77E+004 8.451E+00 3 768.36 4.89 3 .0 2 0E+005 9 .172E+004 1.378E+00 5 806. 1 8 1. 2 6 1. 2 10E+006 - 1.806E+005 5. 52 9E+00 5 934.06 3 .1 1 5.657E+005 4.343E+005 2.600E+005 112 0 . 29 14.9 2 1.260E+005 8.684E+004 5.779E+004 1155. 2 1 1. 63 9.064E+005 -4.747E+005 4.051E+005 1 238.1 2 5.83 3.383E+005 2 .174E+005 1.552E+005 1 2 80.98 1. 43 1.086E+006 4. 3 65E+005 4.853E+00 5 1377.67 3.99 3.394E+005 1.433E+005 1.481E+005 1385.31 0.79 1.803E+006 - 1 .049E+006 7.927E+005 1401.52 1. 33 1.158E+006 -3.134E+005 5 .140E+005 1407.99 2 .39 6.315E+005 -6.714E+00 2 2 .794E+005 1509. 2 1 2 .13 6.130E+005 2 .4 2 0E+005 2 .639E+005 1661. 2 7 1. 05 8.899E+005 3 . 39 4E+005 3 .531E+005

[251]

Nuclide MDA Report 4/1 3 / 2 016 1:31:14 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM )

 +     Bi-214      1729.59       2.88    4. 2 18E+005 1.94E+004 2.278E+005 1.766E+005 1764.49* 15.30        4.647E+004                      1.704E+005 l.671E+004 1847.43       2.03    6.493E+005                      3 . 72 7E+005 2 .742E+OOS
   >               2118.51       1.16    O.OOOE+OOO                       O.OOOE+OOO O.OOOE+OOO P b - 21 4    241.99      7.25    2 .462E+005 4.89E+004 1.966E+005 l.181E+00 5 295. 22   18.42     9.178E+004                      3.812E+004 4. 3 72E+004 351.93    35.60     4.888E+004                      2 .540E+004 2 . 32 1E+004 785.96      1. 06   1.477E+006                      1. 064E+006   6.768E+005 Pb214-XR        74.8 2    5.80    4.487E+005 2 .51E+005 7.401E+005 2 .194E+005 77.11     9.70    2 . 5 15E+005                   2 .997E+005 1. 22 8E+005 87.35     2 . 24  1.041E+006                      4.962E+005 5 .077E+005 89.78     0.82    2 .709E+006                     3 .059E+005 1. 3 19E+006 Ra-226        186.21     3.64     4.661E+005 4.66E+005 4.625E+005 2 . 2 43E+005 Ac-228        129.07     2 .4 2   7.306E+005 7.27E+004 -5.128E+005 3 .533E+005 209.25     3 .89    4.301E+005                    -1.440E+005 2 .064E+005 270.24     3 .46    4. 2 30E+005                    7.746E+004 2 .004E+005 328.00      2 .95    4.515E+005                    - l.016E+005 2 .115E+005 338.32    11. 27     1.396E+005                      7.866E+004 6.600E+004 409.46      1. 9 2   7.965E+005                    - 4. 3 19E+004 3.736E+005 463.00      4.40    3 .035E+005                    - 7.522E+004 l.403E+005 794.95      4. 2 5  3 .661E+005                      l.272E+005 1.676E+005 911.20    2 5.80     7. 2 69E+004                    3 .129E+004 3.363E+004 964.77      4.99    3.760E+005                       2 .611E+005 1.736E+OOS 968.97    15.80     1.156E+00 5                      7.667E+004 5.322E+004 1588. 2 0    3.22    2.815E+005                       1.610E+004 l.117E+005
+      Pa- 2 31       2 7.36* 10.30     2 .932E+005 2 .93E+005 1.155E+006 l.438E+005 283.69      1. 70   9. 2 25E+005                     5.883E+005 4. 3 82E+005 300.07      2 .47   6.054E+005                    -6.049E+005 2 .864E+005 302.65      2 . 20  6.309E+005                    -6.969E+005 2 .970E+005 330.06              9 .361E+005                   - 6. 9 68E+004 4. 3 78E+00.5 Th- 2 34        9 2 .38   2 .1 3  1.012E+006 1.01E+006 3.466E+005 4.924E+005 9 2 .80   2 .10   1.014E+006                    -5 .550E+004 4.933E+005 11 2 .81    0. 2 1  8.493E+006                    -5.367E+006 4.109E+006 U- 23 5       143.76    10.96     1.536E+005 2 .94E+004 -6 . 2 02E+004 7.410E+004 163.33     5.08     3.391E+005                      1.168E+005 1.635E+005 185.71    57.20     2.943E+004                      9.309E+003 l.416E+004 2 0 2 .11  1. 08    1.538E+006                    -3 . 2 97E+005 7.382E+005 2 05. 3 1  5.01     3 .461E+005                     1.636E+005 1.664E+00 5 Am- 2 41        59.54   35.90     6 .131E+004 6.13E+004 -3 .899E+004 2 .985E+004
     + = Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ Half-life too short to be able to perform the decay correction

[252]

• • • • • GAMM A S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 4/13/2016 1:48:46 PM Sample Title B306100AFJFSM024GD Sample Description Ul TB COL G25 Sample Identification Sample Type Sample Geometry Peak Locate Threshold 3 .00 Peak Locate Range (in channel s ) 85 8192 Peak Area Range (in channels) 85 8192 Identification Energy Tolerance 10.000 keV Sample Si ze 1. OOOE+OOO SQM Sample Taken On Acquisition Started 4 /13/2016 1 :37:44 PM Live Time 660.0 seconds Real Time 661.0 seconds Dead Time 0 . 15 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/13/2016 Efficiency ID DTMUD_FLOOR T),,J 4 IJ,. J,'J aJecJ by

                                                               ~~

1:i-t-l'i'

                                                                /I It)

[253]

Peak Analysis Report 4/ 1 3/2 0 16 1:48:46 PM Page 2

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 545 2 Sample

Title:

B306100AFJFSM024GD Peak Analysis Performed on: 4/13/2016 1:48:46 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8 192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Ar e a Uncert. Counts 1 11 3- 124 116.97 2 8.83 1. 51 6.44E+002 99. 1 8 6.11E+00 2 2 5 0 7- 514 510.05 127.23 0.29 -4.36E+ OOO 25.42 8. 2 4E+001 3 5831- 5853 5840.04 1460.28 2.26 l.42E+ 00 2 2 7. 30 l.15E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [254]

Interference Corr ected Activity Report 4/13/2016 1:48:46 PM Page 3

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFJFSM024GD Nuclide Library Used: C: \ GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activit~, Activity Name Confidence (keV) (%) (pCi/SQM) Uncertainty K-40 1.000 1460.82* 10.66 8.71840E+005 1 .84443E+005 Co-57 0.787 1 22 .06* 85.60 - 1.0 9 075E+003 6.36534E+00 3 136.47 10.68 P a-23 1 0. 3 76 2 7.36* 10. 3 0 1. 32 949E+006 3 .8 12 04E+00 5 283.69 1. 70 300.07 2 .47 302.65 2 .20 330.06 1. 40 Th-23 1 0.4 2 9 25.64* 14.10 9 .71188E+005 2 . 74755E+005 84.21 6.60 89.95 1. 00

       * = Energy l ine found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuclide confidence index threshold             0 .3 0 Errors quoted at 2 .000 sigma

[255]

Interference Corrected Activity Report 4/13/ 2 016 1:48:46 PM Page 4

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1.000 8.718399E+005 1.844435E+OOS Co-57 0.787 - l.090751E+003 6.365338E+003

   ?  Pa-231       0. 376        l.329490E+006     3 .812038E+OOS
   ?  Th-231       0.429         9.711879E+005     2 .747548E+005
      ? = Nuclide is part of an undetermined s olution X = Nuclide rejected by the interference analysis
      @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .000 sigma
  **********    U N I D E N T I F I E D        P E A K S      **********

Peak Locate Performed on: 4/13/2016 1:48:46 PM Peak Locate From Channel: 85 Peak Locate To Channel: 819 2 Peak Energy Peak Size in Peak CPS Peak Tel. No. (keV) Counts per Second  % Uncertainty Type Nuclide All peaks were identified. [256]

Nuclide MDA Report 4/13/ 2 016 1 :48:46 PM Page 5

• • • • • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B306 1 00AFJFSM0 2 4GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM )

 +      K-40                1460.8 2

• 10.66 1.523E+005 1.52E+005 8.718E+005 6.783E+004 Cr-5 1 320.08 9.91 1. 3 85E+005 1. 39E+005 -2 .020E+004 6.507E+004 Mn-54 834.85 99.98 1.574E+004 1.57E+004 -6.647E+003 7.198E+00 3 Co-58 810.76 99.45 1.579E+004 1.58E+004 8.107E+003 7. 22 9E+003 Co-6 0 1173.23 99.85 1.575E+004 1. 3 6E+004 -1.734E+004 7.081E+003 1332.49 99.98 1.363E+004 - 2 .757E+003 5.973E+003 Nb-94 702.65 99.81 1.211E+004 1. 2 1E+004 -1.093E+004 5.434E+003 871.09 99.89 1.447E+004 - 8.895E+003 6.550E+00 3 Sn- 11 3 255.13 2 .11 7.076E+005 2 .00E+004 1.669E+005 3.361E+005 391.70 64.97 2 .004E+004 -3 .445E+00 3 9.311E+003 Cs- 134 475.36 1. 48 8.735E+005 1.57E+004 -1.654E+00 5 4.023E+005 563.25 8.34 1.669E+005 1 .416E+004 7.680E+004 569.33 15. 3 7 8.914E+004 -1.033E+004 4.094E+004 604.72 97.6 2 2 .008E+004 - 3.975E+003 9.451E+003 795.86 85.46 1.574E+004 4.711E+003 7.101E+003 801.95 8.69 1.6 2 4E+005 1.0 2 1E+005 7.364E+004 1038.61 0.99 1.639E+006 5.5 1 8E+005 7.441E+005 1 167.97 1. 79 9.191E+005 3.364E+005 4.154E+005 1 365. 1 9 3.02 4.338E+005 7.954E+004 1.886E+005 1? r; rt~

1...,::, - .L ..J / 661.66 85.10 1.754E+004 l.75E+004 -1.553E+004 8.062E+003 Eu-1 52 1 21.78 2 8.67 6.150E+004 5.68E+004 - 1.901E+004 2.975E+004 2 44.70 7.6 1 2 .171E+005 4.732E+004 1 .038E+005 2 95.94 0 .45 3.404E+006 1.857E+006 1.613E+006 344.28 2 6.60 5.683E+004 - 1.7 92 E+004 2.679E+004 367.79 0.86 1.585E+006 5.175E+005 7.407E+005 411.1 2 2.24 5.771E+005 -2 . 22 9E+005 2.674E+005 443.96 2.83 4.942E+005 -2 . 23 8E+005 2.297E+005 488.68 0.42 3 .177E+006 2 .023E+006 1.465E+006 563.99 0.49 2 .778E+006 - 1.127E+006 1.276E+006 586. 2 6 0.46 4.058E+006 3 .033E+006 1.9 0 6E+006 678.6 2 0.47 3 .132E+006 1.859E+006 1.437E+006 688.67 0.86 1.825E+006 -1.902E+005 8.410E+005 719.35 0.28 4.454E+006 -6.093E+006 2 .003E+006 778.90 1 2 .96 9.948E+004 1. 22 3E+OO':l 4.473E+004 810.45 0.32 4.946E+006 3 .472E+006 2.267E+006 867.3 7 4.26 3.4 3 5E+005 4.216E+004 1.557E+005 919.33 0.43 3.573E+006 -l.945E+006 l.6 2 2E+006 964.08 14.65 1. 2 68E+005 2 .994E+004 5.849E+004 1085.87 10. 2 4 1.479E+005 -6.632E+004 6.650E+004 1089.74 1. 73 9.055E+005 7.389E+005 4.086E+005 1112.07 13.69 1.137E+005 -1.488E+005 5.124E+004 1 2 12.95 1. 43 1.121E+006 -5.316E+005 5.040E+005 [257]

4/ 1 3 / 2 0 1 6 1:48:46 PM Page 6 Nuclide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Eu-1 52 1249.94 0.19 7.671E+006 5.68E+004 2 .474E+006 3 .403E+006 1299.14 1. 63 6.863E+005 -1 .170E+005 2 . 92 0E+005 1408.01 2 1. 07 7.015E+004 1.602E+004 3.095E+004 1457.64 0.50 8.101E+006 2. 12 6E+007 3.874E+006 1 52 8.10 0. 2 8 4. 3 43E+006 -7.783E+005 1.848E+006 Eu-154 1 23 .07 40.40 4.349E+004 4.35E+004 -8 .949E+003 2 .103E+004 2 47.93 6.8 9 2 .086E+005 -2 .415E+005 9.897E+004 591.76 4.95 2 .882E+005 -2 .569E+005 1. 32 6E+005 692.42 1. 78 8.488E+005 -1.796E+005 3.898E+005 723.30 2 0.06 7.591E+004 3.770E+004 3.483E+004 756.80 4.5 2 3 . 2 46E+005 9.600E+004 1.482E+005 873. 1 8 1 2 .08 1.215E+005 -l.361E+004 5.509E+004 996. 2 9 10.48 1. 2 90E+005 -9 .335E+004 5.751E+004 1004.76 18.01 8.362E+004 l.054E+004 3.773E+004 1274.43 3 4.80 4.463E+ 0 04 -3 .136E+004 1.995E+004 1596.48 1. 80 5.060E+005 -3.570E+005 2 .008E+005 Eu-155 45.30 1. 3 1 2 .080E+006 6.97E+004 4.384E+005 1.018E+006 60.01 1. 22 1.631E+006 -8.201E+005 7.918E+005 86.55 3 0.70 6.973E+004 2 .090E+004 3.393E+004 105. 3 1 2 1.10 8.859E+004 1.512E+003 4. 2 93E+004 Tl- 2 08 583.19 85.00 2 .165E+004 2 .16E+004 1.102E+004 1.016E+004 Bi-21 1 351.07 13.02 1.565E+005 1.57E+005 1.569E+005 7.492E+004 Pb-21 1 404.65 3 .78 3 .798E+00 5 3 .80E+005 6.888E+003 l.775E+005 427.09 1. 76 7.413E+005 -3 .091E+005 3.432E+005 832 .01 3.52 4.616E+005 -7 .024E+004 2 .118E+005 Bi -2 12 39.86 1. 06 3. 2 04E+006 2 .36E+005 -5 .754E+005 1.575E+006 727.33 6.67 2 . 362E+ 00 5 1 .952E+005 l.087E+00 5 785.37 1.10 1. 3 55E+006 8.428E+005 6.182E+0 0 5 16 2 0. 50 1. 4 7 6.715E+005 -1.135E+006 2 .713E+ 00 5 Pb-212 115.18 0.60 2.934E+006 4.39E+004 -4.163E+005 1.419E+006 23 8.6 3 43.60 4.392E+004 4.499E+004 2 .114E+004 3 00.09 3.30 4.342E+005 -3.338E+005 2 .049E+005 Pb21 2 -XR 74.8 2 10. 2 8 2 .355E+005 1 . 3 2E+005 3.850E+005 l .149E+005 77.11 17.10 1.319E+005 9.530E+004 6.426E+004 87.35 3.97 5. 2 97E+005 - 9.884E+004 2 .576E+00 5 89.78 1. 46 1.415E+006 4.896E+004 6.880E+005 Bi-214 609.32 45.49 5 .036E+004 5.04E+004 8.368E+004 2 . 3 91E+004 768.36 4.89 2 .703E+005 l.265E+005 1. 22 0E+005 806.18 1. 2 6 1.087E+006 - 4.453E+005 4 .913E+005 934.06 3.11 4.454E+005 3.383E+005 1.999E+005 1120. 2 9 14.92 l. 2 60E+005 8.948E+004 5.779E+004 1155. 2 1 1. 63 1.017E+006 1.147E+00 3 4.604E+005 1238.1 2 5.83 3.152E+005 2 .9 2 6E+005 1.437E+005 1 2 80.98 1. 43 1.145E+006 -9.306E+004 5.148E+005 1377.67 3.99 3 .485E+005 -1.672E+005 1.527E+005 1 3 85.31 0 .79 1.457E+006 -3 .503E+006 6.197E+005 1401.5 2 1. 33 1.055E+006 1.567E+005 4.625E+005 1407.99 2 .39 6.174E+005 1 .410E+005 2 .724E+005 1509. 2 1 2 .13 5.481E+005 3 .146E+005 2.315E+005 16 6 1. 2 7 1. 05 8.899E+005 -1.154E+005 3.531E+005 [258]

Nuclide MDA Report 4/13/ 2 016 1:48:46 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) Bi-2 14 17 2 9.59 2 .88 5. 2 46E+005 5.04E+004 3 .796E+005 2.280E+005 1764.49 15.30 l.4 3 8E+005 1. 26 0E+005 6.538E+004 1847.43 2 .03 5.914E+005 O.OOOE+OOO 2 .453E+005

   >                2118.51        1.16 O.OOOE+OOO                     O.OOOE+OOO O.OOOE+OOO Pb-214        2 41.99      7. 2 5 2. 601E+005 5.73E+004 1.650E+005 1. 25 1E+005 2 95. 22   1 8.42 8.375E+004                     2 .1 8 3E+004 3.970E+004 351.93     35.60 5.732E+004                      6.516E+004 2.743E+004 785.96       1. 06 l.391E+006                    2.975E+005 6.342E+005 Pb214-XR         74.82      5.80 4.173E+005 2 .32E+005 6.824E+005 2 .037E+005

77. 1 1 9.70 2 .325E+005 l.680E+005 l.1 33 E+005 87.35 2.24 9.388E+005 - l.752E+005 4.565E+005 89.78 0.82 2 .520E+006 8.718E+004 1. 22 5E+006 Ra-226 186. 2 1 3.64 4.1 26 E+005 4.13E+005 5.811E+004 1 .976E+005 Ac-228 12 9.07 2.42 7. 2 46E+005 7.07E+004 -5.371E+005 3 .503E+005 209. 2 5 3.89 3.941E+005 2 .038E+005 1.884E+005 2 70 . 24 3.46 4.441E+005 4. 33 4E+005 2 .110E+005 32 8.00 2.95 4.684E+005 1.566E+005 2 .199E+005 338.32 11. 27 1.350E+005 9.801E+004 6. 3 70E+004 409.46 1. 9 2 6.535E+005 -4.945E+005 3 .021E+005 463.00 4.40 3.062E+005 -4.969E+004 1.417E+005 794.95 4. 2 5 3.259E+005 2 .820E+004 1.476E+005 911. 2 0 2 5.80 7.072E+004 6.117E+004 3.265E+004 964.77 4.99 3.652E+005 - 1.9 2 4E+005 1.682E+005 968.97 15.80 1.179E+005 6.116E+004 5.437E+004 1588.20 3 . 22 4. 0 42E+005 2 .577E+005 1 .730E+005

+      Pa - 23 1       27.36*   10.30 2.951E+005 2 .95E+005 1 . 32 9E+006 1 .448E+005 283.69       1. 70 8.435E+005                  -2 .449E+005 3 .987E+005 300.07       2.47 5.801E+005                   - 4.460E+005 2 .737E+005 302.65       2.20 6 . 475E+005                   6.611E+004 3 .053E+005 330.06       1. 40 9.842E+005                    7.585E+004 4.619E+005 Th- 23 4        9 2 .38    2 .13 9.330E+005 9. 3 3E+005 -1.934E+005 4.530E+005 92.8 0     2 .10 9.451E+005                  -2 .430E+005 4.588E+005 112.81       0. 2 1 8.287E+OOG                 - 1.716E+006 4.007E+006 U-235         143.76     10.96 1.483E+005 2 .63E+004 1.979E+004 7 .143E+004 163.33       5.08 3 .1 2 6E+005                  7. 3 04E+003 l.503E+005 185.71     57. 2 0 2 .6 2 9E+004                 9. 3 95E+003 1.259E+004 202.11       1. 08 l.412E+006                  -2 . 22 7E+005 6.752E+005 205.31      5.01 2 .995E+005                     l.558E+004 1.431E+005 Am- 2 41        59.54    35.90 5.542E+004 5 . 54E+004 -3 .134E+004 2 .691E+004
     +     Nuclide identified during the nuclide identification

• Energy line found in the spectrum

     >     Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @     Half- life too short to be able to perform the decay correction

[259]

****         GAMM A       S P E C T R U M         ANALYSIS                         *****
.lename: 54 52 iport Generated On                 4/ 2 0/2016       1:34:36 PM tmple Title                        B306100AFIFC025GD tmple Description                  TB 560,Flooi Drain Sump tmple Identification tmple Type tmple  Geometry iak Locate Threshold                 3 .00

!ak Locate Range (in channels) 85 - 81 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 1 0.000 keV tmple Size 1.000E+OOO SQM tmple Taken On

quisition Started 4/20/2 01 6 1 :24:34 PM

.ve Time 6 00.0 seconds !al Time 6 00 .4 seconds iad Time 0. 07 !i5 Energy Calibration Us ed Don e On 1/13/ 2 015 Efficiency Calibration Used Done On 4/20 /2 016 Efficiency ID TBFLRDRNSUMP Dat "- Vo. ),do. t~J by

                                                                ~~
                                                                 /J- /,- /8
                                                                  //JO

[260]

~ak Analysis Report                       4/ 2 0/ 2 016     1: 3 4: 3 6 Pl               Page   2
****                P E A K        A N A L Y S I S           R E P O R T                   *****

Detector Name: 545 2 Sample

Title:

B306100AFIFC025GD Peak Analysi s Performed on: 4/20/2016 1:34:35 PM Pe a k Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 297- 3 05 301.51 75.03 0.97 7.14E+001 3 6.17 1 . 2 0E+002 2 794 - 801 7 97. 60 199.21 0.34 8.04E+OOO 17.21 3 . 3 0E+001 3 2 428- 2 445 2436. 3 2 609.26 0.4 2 6.lOE+OOl 2 1. 91 1.80E+001 4 2637- 2653 2644.91 661.44 1. 3 8 1.09E+00 2 23 .86 1.05E+001 5 3867- 3878 387 2 .89 968.55 0.59 1.40E+001 10.77 6.00E+OOO 6 5833- 5853 5841. 97 1460.76 1. 03 1.12E+00 2 25 .6 2 1.52E+001

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 .000 sigma

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1terference Corrected Acti _ty Report 4/ 2 0/ 2 016 34: 36 PM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFIFC025GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQM) Uncertainty K-40 1. 000 1460.82* 10.66 1.15653E+007 2 .83453E+006 Cs - 137 1. 000 661.66* 85.10 9.33912E+005 2 .32375E+005

       * = Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold =       0.30 Errors quoted at 2 .000 sigma

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 1.156525E+007 2 .834 52 9E+006 Cs-137 1. 000 9.339121E+005 2 . 323 750E+005

      ?   = Nuclide is part of an undetermined solution X     Nuclide rejected by the interference analysis
      @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2 .000 sigma
 **********      U N I D E N T I F I E D          P E A K S        **********

Peak Locate Performed on: 4/20/2016 1: 34:35 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Si ze in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncert ai nty Type Nuclide 1 75.03 l . 1 896E-0 01 50.68 Tol. Pb214-XR Ba-133 Pb212-XR Pb212-XR Pb214-XR 2 199. 21 1.3404E-00 2 2 13.93 Tol. Fe-59 3 609. 2 6 1.0167E-001 35 . 91 Tol.

                                                                                  ~Zr-97 Sb-125 Sb-125
                                                                                   ~       -
                                                                                  ~

5 968.55 2 .3333E-00 2 7 6 . 93 Tol. Eu-152

                                                                                  ~

Ac-228 M = First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000 sigma [263]

1clide MDA Report 4/20/ 2 01 1: 3 4: 36 PM Page 5

• • • • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B306100AFIFC025GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (% ) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM )

+      K-40       1460.8 2

• 10 .66 2 .742E+006 2 .74E+006 1.157E+007 1.231E+006 Cr-51 320.08 9.91 2 .187E+006 2. 1 9E+006 8.488E+005 1.026E+006 Mn-54 834.85 99.98 2 . 2 21E+005 2 . 2 2E+005 1.738E+005 1.001E+005 Co-58 810.76 99.45 2 .404E+005 2 .40E+005 1.343E+005 1.093E+005 Co-60 117 3 . 23 99.85 2 .672E+005 2 .67E+005 1.313E+005 1. 2 04E+005 1 332 .49 99.98 2 .699E+005 1.169E+005 l . 2 09E+005 Nb - 94 702.65 99.8 1 2 .407E+005 2 .41E+005 1. 3 4 6E+005 l .102E+005 871.09 99.89 2 .575E+005 6. 2 12E+004 1.175E+005 Sn-113 2 55.13 2 . 11 1.054E+007 3.17E+005 4. 32 8E+006 4.985E+006 3 91. 7 0 64. 97 3 .170E+005 -2 .082E+004 1. 4 71E+005 Cs-134 475.36 1. 48 1.481E+007 2 .58E+005 - 2 .376E+006 6.848E+006 563.25 8.34 2.220E+006 -4.971E+005 1.002E+006 569.33 15.37 1.2 8 4E+006 - 1.884E+004 5.830E+005 604.72 97.62 3 .459E+005 - 3 .046E+004 1.634E+005 795.86 85.46 2 .580E+005 4.726E+003 1.164E+005 801.95 8.69 2 .466E+006 6.651E+005 1.109E+006 1038.61 0.99 2.073E+007 -8.852E+005 9.116E+006 1 167.97 1. 79 1.413E+007 6.665E+006 6. 32 9E+006 1 365.19 3.02 6.095E+006 - 1 .073E+007 2.574E+006

+      Cs-13 7      661. 66*   85.10    1.838E+005       1 .84E+005     9.339E+005    8. 0 38E+004 Eu-15 2      121.78     2 8.67   9.732E+005       9.07E+005      1.031E+006    4.690E+005 244.70       7.61   3 .028E+006                   -2 . 2 72E+006  1.437E+006 295.94       0.45   5.476E+007                    -9.130E+006     2 .594E+007 344. 2 8   2 6.60   9.074E+005                      5.058E+ 0 05  4.276E+005 3 67.79      0.86   2 . 2 51E+007                 -1.813E+007     1.042E+007 411.12       2 . 24 1 .069E+007                   - 3.711E+006    5.005E+006 443.96       2 .8 3 8.098E+006                    -5.2 61E+005    3.768E+006 488.68       0.4 2  4.781E+007                    - 1 .383E+007   2 .192E+007 563.99       0.49   3.714E+007                    -2 . 2 81E+006  1 .673E+007 586. 2 6     0.46   5.782E+007                      1 .959E+007   2.691E+007 678.62       0.47   4. 2 56E+007                    8.566E+006    1.917E+007 688.67       0.86   2 .705E+007                     3.275E+007    1. 2 36E+007 719.35       0. 2 8 8.404E+007                      1.135E+007    3.835E+007 778.90     1 2 .96  1.735E+006                    -2 .049E+005    7.854E+005 81 0 .45     0. 32  7.346E+007                      2 .371E+007   3 . 3 35E+007 867.37       4.26   5.641E+006                    -1. 766E+006    2 .558E+006 919. 3 3     0.43   5.000E+007                    -1.144E+008     2 . 23 0E+007 964. 0 8   14.65    1.926E+006                      6.743E+00 3   8.819E+00 5 1085.87      10. 2 4  2 .198E+006                     7.545E+005    9.750E+005 1 089.74       1. 73  1 .409E+007                     6.107E+006    6.309E+006 111 2 .07    1 3 .69  1.893E+006                    -2.061E+006     8.530E+00 5 1 212 .95      1. 4 3 1.839E+007                      4.028E+006    8. 2 55E+00 6

[264]

tclide MDA Report 4/21/ 2 01 9: 2 5: 1 5 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( Z, ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Eu-1 52 1249.94 0.19 8.125E+006 5. 3 6E+004 2 .032E+006 3 .584E+006 1299. 1 4 1. 63 8.426E+005 -6 .074E+005 3 .646E+005 1408.01 21.07 5.358E+004 -1. 9 42E+004 2 . 2 22E+004 1457.64 0.50 8.964E+006 2 .082E+007 4. 2 87E+006 1528.10 0. 28 2 .460E+006 5. 2 98E+005 8.716E+005 Eu-154 123.07 40.40 4.408E+004 4.13E+004 -2.962E+004 2 .124E+004 247.93 6.89 2 .312E+005 -8.042E+004 l.097E+005 591.76 4.95 2.998E+005 1. 2 63E+005 1.371E+005 69 2 .4 2 1. 78 8.903E+005 -1.986E+005 4.068E+005 723.30 2 0.06 8.143E+004 6.836E+003 3 .725E+004 756.80 4. 52 3. 22 5E +005 -1.619E+005 1.455E+00 5 87 3 . 1 8 12 .08 1.385E+005 -3 . 33 5E+004 6.297E+004 996. 2 9 10.48 1.282E+005 - 5.792E+00 3 5.638E+004 1004.76 18.01 8.668E+004 3.858E+004 3.882E+004 1 27 4.43 34.80 4.131E+004 -3.040E+004 1.803E+004 1 596.48 1. 80 7.437E+005 -4.024E+005 3 .141E+00 5 Eu-155 45. 3 0 1. 31 1.470E+006 7.52E+004 7.215E+004 7.103E+00 5 60.01 1. 22 1.540E+006 -6. 53 8E+005 7.436E+005 86.55 30.70 7.519E+004 8.651E+004 3 .655E+004 105.31 21.10 8.856E+004 3 .015E+00 3 4. 276E+004

+     Tl -2 08     583.19*    85.00    1 .121E+004      1.12E+004       2 .117E+004    4.867E+003 Bi -2 11     351. 07    1 3 .02  1.390E+005       1.39E+005       1.086E+005     6.578E+004 Pb- 211      404.85       3 .78  4 .42 3E+005     4.12E+005       3.782E+005     2 .073E+00 5 427.09       1. 76  8.601E+005                     -4.413E+005      3.996E+005 83 2 .01     3.52   4.118E+005                     -4.465E+004      1.848E+005 Bi- 212       39.86       1. 06  1.907E+006       2 . 2 4E+00 5 -1. 35 6E+005    9. 2 30E+005 727. 33      6.67   2 . 2 44E+005                    8.455E+004     l.017E+005 785 . 37     1.10   1.346E+006                     - 6.083E+005     6.072E+005 1 620.5 0      1. 47  5 .670E+005                      1 .580E+005    2 .122E+005
+     Pb-21 2      115.18       0.60   3 .197E+006      2 .35E +00 4    5.851E+005     1. 545E+00 6 238.63*    43.60    2 .345E+004                      1.426E+004     1 .081E+004 300.09       3.30   4.999E+005                       2 .585E+005    2 .364E+005 Pb212-XR      74.82     10. 2 8  2 .411E+005      1. 3 7E+005     4.475E+005     1.174E+005 77.11     17.10    1. 3 73E+005                     6. 2 2 8E+004  6.680E+004 87.35       3 .97  5.752E+005                       3.852E+005     2 .795E+005 89.78       1. 4 6 1.501E+006                     - 6.326E+005     7.284E+005 Bi - 2 14    609. 32    45.49    4.619E+004       4.62E+004       3.970E+004     2 .168E+004 768. 3 6     4.89   3 .511E+005                      5.731E+00 3    1.609E+005 806.18       1. 2 6 1 . 2 93E+006                  -9.848E+00 5     5 .886E+005 934.06       3 . 11 4.582E+005                     - 1. 036E+005    2 .038E+005 112 0 . 2 9  14.9 2   1 .425E+005                    - 1 . 55 9E+00 5 6.552E+004 1155. 2 1      1. 6 3 1. 004E+006                    -5.610E+00 5     4.487E+005 1 238.1 2      5.83   3.164E+005                     - 1. 2 25E+005   1.428E+005 1280.98        1. 43  9.483E+005                     - 1.028E+006     4.104E+005 1 377.67       3.99   3.316E+005                     -4.111E+004      1.420E+005 1385.31        0 .79  1.788E+006                       6. 3 17E+005   7.737E+005 1401.52        1. 33  1.039E+006                       6.936E+005     4.476E+005 1407.99        2 .39  4.716E+005                     -1.709E+005      1.956E+005 1509.21        2.13   4. 5 64E+005                   - 1.114E+005     l.811E+005 1661. 2 7      1. 05  9 .017E+005                      3 .003E+005    3 .493E+005

[265]

1clide MDA Report 4 /21/2 0 1 l 9: 2 5:15 AM Page 7 Nuc l ide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) (% ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) Bi-2 14 1729.59 2 .88 2 .599E+005 4.62E+004 5.598E+004 9.208E+004 1764.49 15.30 1 . 2 80E+005 1.119E+005 5.681E+004 1847.43 2 .0 3 5 .812E+005 3. 2 62E+004 2 . 3 48E+005

 >                2 118.51      1.16 O.OOOE+OOO                      O.OOOE+OOO O.OOOE+OOO Pb- 2 1 4    241.99      7. 2 5 2.567E+005 4.90E+004        -2 .439E+005 1 .228E+005 295. 22   18.42 9.006E+004                     -2 .400E+003 4.261E+004 351.93   35.60 4.903E+004                        1.441E+004 2 .315E+004 785.96     1. 06 1 .442E+006                     3 .984E+004 6. 52 9E+005 Pb2 14 -XR    74.82     5.80 4. 27 3E+005 2 .42E+00 5         7.931E+005 2 .081E+005

77. 11 9.70 2 .421E+005 1.098E+005 1 . 178E+005 87.35 2. 2 4 1.019E+006 6.8 2 8E+005 4.954E+005 89.78 0.8 2 2 .672E+006 - 1.126E+006 l. 2 97E+00 6 Ra-226 186.2 1 3 .64 4.771E+005 4.77E+005 2 .334E+005 2 . 2 88E+005 Ac-228 129.07 2 .42 7.581E+005 6 .07E+004 -1.651E+005 3.656E+005 209.25 3. 89 4.354E+005 4.471E+004 2.081E+005 270.24 3. 4 6 5.112E+005 3 .305E+005 2.433E+005 328 .00 2.95 5.277E+005 - 8.410E+004 2 .479E+005 338.32 11. 2 7 1.489E+005 8.7 2 9E+004 7.020E+004 409.46 1. 92 8.971E+005 6. 3 25E+005 4. 2 12E+005 463. 00 4.40 3.639E+005 1.973E+005 1.693E+005 794.95 4.25 3.720E+005 1. 2 01E+005 1.689E+005 911. 2 0 25.80 6.073E+004 2 .687E+004 2 .7 3 6E+004 964.77 4.99 3.839E+005 1.892E+005 1.760E+005 968.97 15.80 1.319E+005 1.580E+005 6.088E+004 1588. 2 0 3. 22 4.778E+005 1. 4 93E+005 2 .067E+005

+ Pa - 23 1 2 7.36* 1 0 .30 8.951E+004 8.95E+004 9.875E+004 4.164E+004 283.69 1. 70 9.521E+005 9.097E+005 4.504E+005 300.07 2 .47 6.679E+005 3.454E+005 3.158E+005 302.65 2 . 2 0 6.756E+005 -4.397E+003 3.173E+005 330. 0 6 1. 40 1.043E+006 -1. 2 87E+005 4.876E+005 Th-234 92.38 2 .13 1 .000E+006 1.00E+006 1 .672E+005 4.850E+005 92.8 0 2 .10 1 .003E+006 2 .089E+005 4.863E+005 11 2 .8 1 0. 2 1 9.261E+006 6.535E+006 4.478E+006 U-235 143.76 10.96 1.548E+005 3 .02E+004 -3 .4 3 6E+004 7.436E+004 163.33 5.08 3.395E+005 3. 058E+004 1.630E+005 185.71 57. 2 0 3.024E+004 -4.583E+002 1 .450E+004 202.11 1. 08 1.638E+006 4. 2 75E+005 7.847E+00 5 2 05.31 5.01 3.557E+005 9.837E+004 1.704E+00 5 Am-241 59.54 35.9 0 5. 2 05E+004 5 . 2 0E+004 -9.292E+003 2 .513E+004

    + = Nuclide identified during the nuclide identification

• Energy line found in the spectrum

    >     Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Half-l ife too short to be able to perform the decay correction

[266]

****        GAMM A       S P E C T R U M            A N A L Y S I S                   *****
.lename: 5452 iport Generated On                  4/21/ 2 016       9:25:15 AM

r: ~..\'"'

tmple Title B306100AF7FC~26GD tmple Description TB 560,Fire Sump 1mple Identification tmple Type tmple Geometry iak Locate Threshold 3 .00 iak Locate Range (in channels) 85 - 81 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10.000 keV 1mple Size 1.000E+OOO SQM tmple Taken On

quisition Started 4/21/2 01 6 9:15:12 AM

.ve Time 600.0 seconds ial Time 601. 3 seconds iad Time 0.21 % Energy Calibration Us ed Done On 1/13/ 2 015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBFLOOR b a+a \J °' \\cL,.:(. ed b

                                                             ~~ 1
                                                              /J,-6,-/f
                                                               )/J.s

[267]

!ak Analys i s Report 4 / 2 1 / 2 0 16 9: 2 5:15 Al Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B306100AFJFC0 2 6GD Peak Analysis Performed on: 4/21/2016 9:25:14 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV ) ( keV ) Area Uncert. Counts 1 1 13 - 119 115.93 28.5 7 0.55 4. 2 9E+001 2 5.58 4.81E+001 2 950 - 958 954.75 2 3 8.54 0.69 2 .10E+001 2 1. 43 4.40E+00 1 3 2 0 39- 2 050 2044.49 51 1. 23 0.78 1.86E+001 15.44 1.64E+001 4 2 137- 2 146 2141.31 535.45 0.71 2.38E+OOO 10.51 1.06E+001 5 232 5- 2 337 2330.40 582.76 0.83 3.88E+001 16.5 2 1.12E+001 6 2 636- 2 654 2644.83 661. 42 1. 22 1. 28E+00 2 25.99 1.20E+001 7 5832- 5850 5841. 1 7 1 4 60.56 0.88 1.31E+00 2 27.75 1.83E+001 First peak in a multiplet region = Other peak in a multiplet region Fitted singlet -rors quoted at 2. 000 sigma [268]

1terference Corrected Acti ty Report 4/2 1 / 2 01 6 ~5: 15 AM Page 3

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Sampl e

Title:

B306100AFJFC026GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence ( keV) (%) (pCi/SQM) Uncertainty K-40 1. 000 1460.8 2

• 10.66 8.91296E+005 2 .04409E+005 Rb-83 0.638 520.40* 45.00 1.79735E+004 1.52925E+004 5 2 9.59* 2 9.30 3.61787E+003 1.59595E+004 552.55 16.00 Sr-85 0.988 514. 01
• 96.00 8.4 2 515E+00 3 7.07986E+003 Cs-137 1. 000 661. 66* 85.10 7.42368E+004 1.75142E+004 Tl-208 1. 000 583. 1 9* 85.00 2 .11700E+004 9.36499E+003 Pb-212 0.872 115.18 0.60 2 38.63* 43.60 1.4 2 638E+004 1.47211E+004 300.09 3.30 Pa-231 0.376 2 7.36* 10.30 9.87545E+004 6.35876E+004 283.69 1. 70 300.07 2 .47 302.65 2 .20 330. 0 6 1. 40 Th -23 1 0.431 25.64* 14.10 7.21 3 98E+004 4.63284E+004 84.2 1 6.60 89.95 1. 00

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :         10.000 keV Nuclide confidence index threshold =           0.30 Errors quoted at 2 .000 sigma

[269]

1terference Corrected Act i .ty Report 4/ 2 1 /2 016 ..25 :15 AM Page 4 "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertaint: 1 K-40 1. 000 8.91 2 959E+005 2 .044093E+005 Rb-83 0.638 3.617875E+00 3 1 .595112E+004 Sr-85 0.988 6.729 2 60E+003 1.029720E+004 Cs-137 1. 000 7.423683E+004 1. 751416E+004 Tl-2 0 8 1. 000 2 . 1 17003E+004 9.364992E+003 Pb-2 1 2 0.87 2 1.426375E+004 1.472113E+004

  ?  Pa-231        0.376            9.875450E+004        6.358764E+004
  ?  Th-231        0. 4 3 1        7.21 3 981E+004       4.632838E+004
     ?    Nuclid e is part of an undetermined solution X    Nuclide rejected by the interference analysis
     @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at        2 . 000 sigma
 ***** *****    U N I D E N T I F I E D             P E A K S       **********

Peak Locate Performed on: 4 /2 1/20 1 6 9:25 :1 4 AM Peak Locate From Channel: 85 Peak Locate To Channel: 81 92 Peak Energy Peak Size in Peak CPS Peak ToL No. (keV) Counts per Second  % Uncertainty Type Nuclide All peaks were identified. [270]

iclide MDA Report 4/21/201 9: 2 5:15 AM Page 5

• • • • N U C L I D E M D A R E P O R T *****
        • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • ~*****

Detector Name: 54 52 Sample Geometry: Sample

Title:

B306100AFJFC026GD Nuclide Library Us ed: C: \ GENIE2K\CAMFILES \ Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) (~ ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM )

+      K-40       1460. 82

• 10 .66 l. 94 7E+005 l .95E+005 8.913E+005 8.814E+004 Cr-51 320.08 9.91 l. 52 5E+005 l.52E+005 -5.503E+004 7.156E+004 Mn-54 834.85 99.98 l.572E+004 1. 57E+004 -2 .800E+003 7.117E+003 Co-58 810.76 99.45 l.751E+004 l.75E+004 -3.910E+003 8.018E+00 3 Co-60 1173. 23 99.85 1.744E+004 l.74E+004 5.496E+00 3 7.841E+00 3 133 2 . 4 9 99.98 1.822E+004 l. 3 01E+004 8.177E+00 3 Nb-94 702.65 99.81 l.496E+004 l.50E+004 -3 .074E+003 6.794E+00 3 871. 09 99.89 1.673E+004 9.013E+003 7.607E+003 Sn-113 255.13 2 .11 8. 2 89E+005 2 .55E+004 l.036E+006 3 .948E+005 391. 70 64.97 2 .547E+004 - 8.078E+00 3 l.194E+004 Cs-134 475.36 1. 48 1.000E+006 l.75E+004 -4.571E+004 4.617E+005 563.25 8.34 l.696E+005 l.181E+00 5 7.738E+004 569.33 15.37 9.1 3 1E+004 4.970E+003 4.162E+004 604.7 2 97. 62 2 .028E+004 5.864E+003 9.484E+003 795.86 85.46 1.746E+004 -l.860E+004 7.877E+003 8 01. 95 8.69 l.8 02E+005 l. 3 53E+004 8.168E+004 1038.61 0.99 1.631E+006 -2 .509E+006 7. 3 19E+005 1167.97 1. 79 9 .543E+005 2 . 62 5E+005 4. 2 83E+005 1365.19 3.02 4.035E+005 6.89 2E+004 l.704E+005 Cs - 137 661.66~ 85.10 l.377E+004 l . 38E+004 7.424E+004 6.102E+003

+                                                                                  2 .977E+004 Eu-152      121. 78     2 8.67  6.178E+004      5. 3 6E+004 -2 .610E+004 244.70        7.61  2.187E+005                  -7.980E+00 3    1.040E+005 295.94        0 .45 3.724E+006                  -8.900E+005     l.762E+006 344. 2 8    2 6.6 0 6 .298E+004                 - l.407E+004    2 .968E+004 367.79        0.86  1.692E+006                  - 1. 22 0E+006  7.882E+005 411 .12       2.24  7.438E+005                    3.964E+005    3 .484E+005 443.96        2.83  4. 3 79E+005                -1. 1 11E+005   1.996E+005 488.68        0.4 2 3.464E+006                  - 4. 25 3E+005  l.595E+006 563.99        0. 49 2.772E+006                    3 .006E+005   l. 2 60E+006 586. 26       0.46  4.375E+006                    2 .858E+006   2 .051E+006 678.62        0.47  2.844E+006                  -l. 3 11E+006   1.279E+006 688.67        0.86  l.837E+006                  -3 . 3 96E+005  8.394E+005 719.35        0.28  5.412E+006                    2 .826E+006   2 .457E+006 778.90      12.96   l.157E+005                    l.040E+004    5. 2 31E+004 81 0 .45      0.32  5.362E+006                  -l.350E+006     2 .452E+006 867.37        4.26  3.528E+005                  -2 .481E+005    1. 586E+005 919.33        0.43  2.946E+006                  -2 .658E+006    1. 2 91E+00 6 964. 0 8    14.65   1. 2 92E+005                  9.402E+004    5.918E+004 1085.87      1 0.24  l.187E+005                  -3 .258E+004    5.111E+004 1089.74        1. 73 8.496E+005                    5.194E+005    3 .759E+00 5 1112.07      13.69   l.482E+005                  - 7.446E+004    6.784E+004 1212.95        1. 43 l.061E+006                  -3 .772E+00 5   4.681E+005

[271]

4 /2 0 /2 01 1:34: 3 6 PM Page 6 1clide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQM) (pCi/SQM ) {pCi/SQM ) (pCi/SQM ) Eu-1 52 1 2 49.94 0 . 19 1. 333E+008 9.07E+005 -l.519E+008 5.945E+007 1299.14 1. 63 l.383E+007 3 .474E+006 6.058E+006 140 8.01 2 1. 07 l .202E+006 1.022E+006 5.318E+005 1457.64 0.50 l. 2 90E+008 3 .197E+008 6.155E+007 1528.10 0. 2 8 7.014E+007 l. 3 29E+007 2 .962E+007 Eu-154 12 3 .07 40.40 6.753E+005 6. 75E+005 3 .177E+005 3 . 2 52E+005 247.93 6.89 3.211E+006 l .661E+005 1.520E+006 591. 76 4.95 4.181E+006 -1.077E+005 1.903E+006 692.42 1. 78 1.195E+007 -7.738E+006 5.411E+006 723.30 2 0.06 1. 3 58E+006 1 .077E+006 6.279E+005 756.80 4 . 52 4.532E+006 -2 .105E+006 2 .034E+006 873.18 1 2 .08 2 .051E+006 1.929E+006 9. 32 7E+005 996. 2 9 10 . 48 2 .093E+006 -1.371E+006 9.310E+005 1004.76 18.01 1.173E+006 - 1.546E+006 5.189E+005 1 274.43 34.80 7. 3 10E+005 6.720E+005 3. 2 60E+005 1596.48 1. 80 1.179E+007 - 6.262E+006 5.014E+006 Eu-1 55 45. 3 0 1. 3 1 1. 3 46E+007 1.09E+006 1.394E+006 6.333E+006 60.01 1. 22 l.923E+007 -8.218E+006 9.188E+006 86.55 3 0.70 1.086E+006 5.689E+005 5. 2 61E+005 105.31 2 1.10 1.359E+006 2.873E+005 6.551E+005 Tl-208 583.19 85.00 3 .305E+005 3.31E+005 3.548E+005 1.544E+005 Bi-2 11 351.07 13.0 2 2 .011E+006 2.01E+006 1. 2 19E+006 9.519E+005 Pb-2 11 404.85 3.78 6.112E+006 6.11E+006 l.539E+006 2 .856E+006 427.09 1. 76 1. 2 15E+007 -l.419E+007 5.635E+006 832.01 3.52 6.196E+006 -l.925E+006 2 .786E+006 Bi-21 2 39.86 1. 06 1 .480E+007 3 .79E+006 -9.384E+006 6.908E+006 727. 33 6.67 3.786E+006 - 7.090E+005 l.7 3 9E+006 785.37 1.10 2 .049E+007 - 5.433E +006 9. 2 74E+006 1620.5 0 1. 4 7 l.052E+007 -2 .326E+006 4.173E+006 Pb- 212 115.18 0.60 4.783E+007 6.04E+005 -9.239E+00 6 2 . 3 07E+007 2 38.63 43.60 6 . 042E+005 2 .831E+005 2 .888E+005 300.09 3.30 7.676E+006 -5.150E+006 3.641E+006 Pb212-XR 74.82 1 0.28 3.634E+006 2 .10E+006 5.914E +006 l.766E+006 77.11 17.10 2.103E+006 - l.191E+006 l.021E+006 87.35 3 . 97 8. 2 10E+006 - 8.465E+005 3 .974E+006 89.78 1. 46 2 .1 2 1E+007 - 6. 2 76E+006 1. 025E+007 Bi- 2 14 609.3 2 45.49 7 . 489E+005 7.49E+005 9.764E+005 3 .538E+005 768.36 4.89 4.695E+006 2 .485E+006 2 .132E+006 8 0 6.18 1. 2 6 1.809E+007 l. 2 1 7E+007 8. 1 88E+006 934. 0 6 3 .11 8.505E+006 -2 . 28 0E+006 3 .877E+006 1120. 2 9 14.92 2 . 0 97E+006 2 . 32 8E+006 9. 62 4E+005 1155. 2 1 1. 63 1 .567E+007 7.195E+006 7.033E+006 1 238. 1 2 5.83 4.4 62 E+006 - 1.443E+006 1.999E+006 1280.98 1. 43 1.778E+007 1 . 816E+006 7.930E+006 1 377.67 3 .99 6. 3 98E+006 2 .5 9 9E+005 2 .839E+006 1385.31 0.79 2 .437E+007 -2 .935E+007 l.037E+007 1401.52 1. 33 1.856E+007 -8.828E+006 8. 1 87E+006 1407.99 2 .39 1.058E+007 8.997E+006 4.680E+006 1509.21 2 .13 8.390E+006 -3 . 3 05E+006 3 .480E+006 1 661. 2 7 1. 05 l.500E+007 - 5. 2 64E+006 5.953E+006 [272]

tclide MDA Report 4 /2 0/ 2 01 1:34: 3 6 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi-214 1729.59 2 .88 5 .601E+006 7.49E+005 2 .136E+006 2 . 22 2E+006 1764.49 15. 3 0 2 . 26 0E+006 2 .361E+006 1. 020E+006 1 847.43 2 .0 3 9.451E+006 4.406E+006 3.874E+006

  >               2 118.51      1.16    O.OOOE+OOO                    O.OOOE+OOO    O.OOOE+OOO Pb- 214      2 41.99     7. 2 5  3 . 6 68E+006   7. 3 3E+005   2 .033E+006   1.754E+006 2 95. 22  18. 42    1. 2 95E+006                  1.734E+005    6.128E+005 35 1. 93 35.60      7.332E+005                    8. 52 9E+005  3.469E+005 785.96     1. 06    2 .130E+007                 -4.023E+006     9.645E+006 Pb2 14 -XR     74.8 2   5.80     6.441E+006      3 .71E+006    1.048E+007    3.131E+006 77.11     9.70    3 .708E+006                 -2 .100E+006    1.800E+006 87.35    2 . 24   1. 455E+007                 - 1.500E+006    7.043E+006 89.78    0.82    3.776E+007                   - 1.117E+007    1.825E+007 Ra-226       186.21     3 .64    6.650E+006      6.65E+006   - 1.346E+006   3. 180E+006 Ac-228        129.07     2 .4 2  1.091E+007       1.16E+006   -4.839E+005    5 . 2 48E+006 2 0 9.25   3.89     6.147E+006                  -2 .933E+006   2 .931E+006 270.24     3. 46   6.041E+006                   -6 . 676E+006  2 .842E+006 328.00     2 .95   7. 2 52E+006                 -2.889E+006    3.396E+006 338.3 2  11. 2 7   2 . 2 20E+006                  1.002E+006   1 .049E+006 409.46     1. 92   1. 2 35E+007                 -2 .372E+006   5.778E+006 463. 00    4.40    4.947E+006                   -2.807E+00 5   2 . 2 89E+006 794.95     4.25    5.184E+006                     1. 518E+006  2 . 33 9E+006 911.20   25 .80    1.164E+006                     1.004E+006   5. 3 72E+005 964.77     4.99    5.657E+006                   -3 .180E+005   2 .590E+00 6 968.97   15.8 0    1. 770E+006                    7.034E+005   8.097E+00 5 1588. 2 0    3 . 22  6.556E+006                     1.561E+006   2 .789E+006 Pa -2 31       27.36   10.30     1. 2 13E+006     l. 2 1E+006   6.463E+005   5.561E+005 283.69      1. 70   1.306E+007                    1. 3 52E+007  6.159E+006 30 0 . 07   2 .47   1.025E+007                   -6.881E+006    4.865E+006 302.65      2 . 20  1.137E+007                    1. 3 11E+007  5.389E+006 330.06      1. 40   1.483E+007                   -5.492E+006    6.932E+006 Th-23 4        92.38     2 . 13  1.440E+007      1 .43E+007     6.088E+006   6.955E+006 92.8 0    2 .10   1.429E+007                   -6.310E+006    6.896E+006 11 2 .8 1   0. 2 1  1.397E+008                    1 . 285E+008  6.743E+007 U- 235       14 3.76   1 0.96    2 .240E+006     4.3 4E+005    5 .895E+005   1.074E+006 163.33      5.08    4.807E+006                    1.037E+006    2 .302E+006 185. 7 1  57. 2 0   4. 33 9E+005                  2.626E+005    2 .077E+005 2 02.11     1. 08   2 . 2 56E+007                 1.864E+006    1 .078E+007 2 05. 3 1  5.01     4.862E+006                    1.589E+006    2 .322E+006 Am- 2 41       59.54   35.90     6.494E+005      6 . 49E+005   3 .030E+004   3 .102E+005
    + = Nuclide identified during the nuclide identi f ication
     * = Energy l ine found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, o r the region is outside the spectrum, or MDA has not been calculated
     @ = Half-life too short to be abl e to perform the decay correction

[273]

"***         GAMM A        S E> E C T R U M        A N A L Y S .i S            *****
.lename: C:\GENIE2K\CAMFILES\00001387.CNF iport Generated On                   4/25/2016        9:09:00 AM 1mple Title                          B306100AFJWC027GD 1mple  Description                    TB 560,Fire Sump 1mpl e Identification 1mple  Type 1mple  Geometry iak Locate Threshold                   3.00 iak Locate Range (in channels)             85 -   8192 iak Area Range {in channels)               85 -   8 1 92 lentification Energy Tolerance           10.000 keV 1mple Size                             1.000E+OOO SQM 1mple Taken On

quisition Started 4/ 2 1/2016 9:45:04 AM

.ve Time 600.0 seconds ial Time 600.7 seconds

ad Time 0.11 %

Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/25/2016 Efficiency I D TBWALL2

                                                               /.:1- t. .. /<J
                                                                 /Its

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iak Analysis Report 4/ 2 5/20 1 6 9:09:00 AM Page 2

****               P E A K       A N A L Y S I S               REPORT                    *****

Detector Name: 545 2 Sample

Title:

B306100AFJWC0 2 7GD Peak Analysis Performed on: 4/25/ 2 0 16 9:09:00 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV ) Area Uncert. Counts 1 170- 176 172.93 42 .84 0. 33 1.llE+OOl 15.5 3 2.59E+001 2 296- 308 300.37 74.74 0.77 5 . 2 4E+001 60.65 3.26E+002 3 949- 96 0 953.76 238.29 0.48 4.46E+001 29 . 11 6.64E+001 4 1106- 1114 1110.36 277.48 0. 2 5 5.58E+OOO 15. 52 2 .44E+001 5 2 428- 2445 2436.46 609.29 1. 08 6.45E+001 20. 26 1.15E+001 6 2 633- 2 656 2 644.57 661. 35 1. 64 2 .41E+00 2 34.08 1. 22E+ 001 7 4473- 4485 4478.90 1 1 20.07 0. 35 2 .41E+001 12 .58 5.93E+OOO 8 5829- 585 2 5841.36 1460. 61 2 .05 1.80E+00 2 31. 83 1.82E+001 First peak in a mul tiplet region Other peak in a mul tiplet region

= Fitted singlet

• rors quoted at 2 . 000 sigma

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1terference Corrected Acti' .y Report 4/ 25 / 2 016 9 3:00 AM Page 3

• • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B306100AFJWC027GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQM) Uncertaint~/ K-40 1. 000 1460.8 2* 10.66 2 .19797E+006 4.3 32 89E+005 Cs-137 1. 000 661.66* 85.10 2 .55572E+005 4.74329E+004 Hg-203 0.995 2 79.20* 81. 56 4.30 23 0E+003 1.19785E+004 Pb-21 2 0.87 2 115.18 0.60 238.63* 43.60 6. 0 4919E+004 4.064 22 E+0 0 4 30 0 .09 3.30 Bi -2 1 4 0. 3 4 2 609. 32

• 45.49 1. 2388 1E+005 4.16334E+004 768.36 4.89 806.18 1.26 93 4.06 3.11 1120. 2 9* 14.92 1 .83743E+005 9.71985E+004 1155.2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.2 1 2.13 1661.27 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2 11 8.51 1.16 Th -22 7 0.367 5 0 .13* 8.40 8.11582E+004 l.1608 2E+005 79.69* 1. 95 1 .46688E+006 1. 74311E+006 94.97 0.0 3 210.62 1.25 235.96* 12.90 2.04453E+005 1.4 1 643E+0 05 256. 2 3 7.00 286. 0 9* 1. 74 2.01654E+005 5.63551E+005 299.98 2 .21 304 . 5 0 1.15 329.85 2 .90 334.37 1.14

[276]

1t e rference Corrected Acti* :y Report 4/25/2016 9 9:00 AM Page 4

       * = Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Ac tivity Energy Tolerance :    10.000 keV Nuclide confidence index threshold       0.30 Errors quoted at 2 .000 sigma

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1terference Corrected Acti :y Report 4/25/ 2 016 c 9:00 AM Page 5

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 2.197968E+006 4. 332 890E+005 Cs-137 1. 000 2.555724E+005 4.743287E+004 Hg-203 0.995 2.439392E+00 3 1. 22 2630E+004 Pb-21 2 0.87 2 3.465741E+004 5.294723E+004 Bi-214 0.34 2 1. 33 1609E+005 3 .8 2 7040E+004 X Rn-219 0.385 Th-227 0.367 8.731658E+004 1.147 92 6E+005

     ?  = Nuclide is part of an undetermined solution X  = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .000 sigma
 **********    U N I D E N T I F I E D         P E A K S        *******~' **

Peak Locate Performed on: 4/ 25/2 0 1 6 9:09:00 AM Peak Locate From Channel: 85 Peak Locate To Channel: 81 92 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second t Uncertainty Type Nuclide All peaks were identified. [278]

tclide MDA Report 4/ 2 5/201 9:09:00 AM Page 6

• • • • N U C L I D E MD A R E P O R T *****

Detector Name: 54 52 Sampl e Geometry: Sample

Title:

B306100AFJWC027GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) (pCi/SQM)

+      K-40       1460.8 2

• 1 0 .66 3 .776E+005 3.78E+005 2 .198E+006 1.722E+005 Cr-51 32 0.08 9.91 3 .197E+005 3.20E+005 1. 250E+005 1.508E+005 Mn-54 834.85 99.98 3 .008E+004 3.01E+004 2 .313E+004 1. 3 69E+004 Co-58 810.76 99.45 2 .743E+004 2.74E+004 - 3 .577E+00 2 1.238E+004 Co-60 1173. 23 99.85 3 . 2 3 6E+004 2.85E+004 5.145E+003 1.460E+004 1332.49 99.98 2 .846E+004 - 2 .834E+003 1. 255E+004 Nb-94 7 02 .65 99.8 1 2 .877E+004 2 .16E+004 3 .185E+003 1.313E+004 871. 09 99.89 2 .160E+004 -1. 34 7E+004 9.430E+00 3 Sn-11 3 255.1 3 2 .11 1.599E+006 4.97E+004 -1.072E+006 7.606E+005 391.70 64.97 4.970E+004 2 .088E+003 2 .334E+004 Cs- 134 475.36 1. 48 1.947E+006 3.22E+004 -1. 2 61E+006 9.016E+005 563.25 8.34 3.507E+005 3.178E+005 1.616E+005 569.33 15. 3 7 1.733E+005 - 2 .144E+005 7.918E+004 604.72 97.6 2 4.155E+004 - 2 .833E+004 1.957E+004 795.86 85.46 3 . 2 16E+004 -1.797E+004 1.454E+004 801. 95 8.69 2 . 92 4E+005 -1.259E+005 1.310E+005 1 038.61 0.99 3.036E+006 2.475E+006 1. 3 68E+006 1 167.97 1. 79 1.655E+006 -4.413E+005 7.395E+005 1365.19 3.02 8.619E+005 5 .198E+004 3.747E+005

+ Cs - 137 661.66* 85.1 0 2 .743E+004 2.74E+004 2.556E+005 1.228E+004 Eu-15 2 121.78 28.67 l.554E+005 1.10E+005 -5.890E+004 7.530E+004 244.70 7.6 1 4.959E+005 -l.822E+005 2.373E+005 295.94 0 .45 7.999E+006 - 2 .357E+006 3 .805E+006 344.28 2 6.60 1.275E+005 -7.349E+004 6.029E+004 367.79 0 .86 3.473E+006 3 .2 2 7E+005 1.626E+006 411. 12 2.24 l.320E+006 -l. 2 55E+006 6.150E+005 443.96 2.83 1.153E+006 3.081E+005 5.401E+005 488.68 0.42 7.508E+006 l.241E+006 3.498E+006 563.99 0. 4 9 5.958E+006 3.583E+006 2.746E+006 586. 2 6 0.46 7.568E+006 7.678E+006 3.531E+006 678.62 0.47 5.770E+006 2 . 25 3E+006 2.623E+006 688.67 0.86 2 .968E+006 -1.246E+006 l.339E+006 719.35 0. 2 8 8.547E+006 -4.958E+006 3.820E+006 778.90 12.96 2 .134E+005 - 2 .304E+005 9.659E+004 810.45 0. 32 8. 62 8E+006 1. 785E+006 3.900E+006 867.37 4.26 5. 32 4E+005 -1 .364E+005 2.341E+005 919.33 0.43 7.146E+006 4.488E+005 3.245E+006 964.08 14.65 2 .304E+005 8.456E+004 l.054E+005 1085.87 10.24 2 .578E+005 7.950E+004 l.141E+005 1089.74 1. 73 1.595E+006 5.762E+005 7.094E+005 111 2 .07 13.69 1.950E+005 -2 .160E+005 8.628E+004 1 2 1 2 .95 1. 43 2 .475E+006 1.7 2 1E+006 1.125E+006 [279]

4/25/ 2 01( 9: 09:00 AM Page 7 1clide MDA Repo rt Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Eu-15 2 1249.94 0.19 1. 8 43E+007 1.10E+005 3.492E+006 8. 35 6E+006 1299.14 1. 63 1. 6 04E+006 -1.400E+006 7.002E+005 1408.01 21 .07 1.099E+005 6.664E+004 4.674E+004 1457.64 0.50 1.802E+007 5.100E+007 8.660E+006 1528.10 0. 2 8 9.550E+006 3.298E+006 4.133E+006 Eu-154 123.07 40.40 1.102E+005 8. 5 4E+004 2 .501E+004 5.338E+004 2 47.93 6.89 5. 2 18E+005 -4. 2 66E+005 2 .491E+005 591.76 4.95 5.664E+005 3 .580E+005 2 . 5 96E+005 692.42 1. 78 1.504E+006 9. 2 27E+005 6.817E+005 723.30 2 0.06 l.431E+005 6.853E+004 6.522E+004 756.80 4.52 5.183E+005 2 .497E+004 2 .305E+005 873. 1 8 12.08 1.738E+005 -7.130E+004 7.557E+004 996. 2 9 10.48 2 .902E+005 - 1 .591E+005 1.312E+005 1004.76 18.01 1.505E+005 -5.655E+004 6 .710E+004 1274.43 34.8 0 8.539E+004 -1.915E+004 3 .798E+004 1596.48 1. 80 1. 53 9E+006 - 8.183E+005 6.659E+005 Eu-155 45.30 1. 31 2 .7 2 5E+006 1. 79E+005 -3.997E+005 l. 2 99E+006 60.01 1. 22 4.104E+006 2 .518E+006 l.984E+006 86.55 3 0 .70 1.790E+005 2 .097E+005 8.725E+004 105.31 21.10 2 .164E+005 - 2 . 52 5E+004 1.050E+005 Tl-2 0 8 58 3 .19 85.00 4.058E+004 4.06E+004 3.469E+004 1 .892E+004 Bi-2 11 351. 07 13.0 2 3 .169E+005 3 .17E+005 4.078E+005 1.513E+005 Pb-211 404.85 3.78 8.561E+005 7. 3 3E+005 - 8.313E+004 4.018E+005 427.09 1. 76 1.801E+006 4.502E+005 8.427E+005 832 .01 3.5 2 7. 3 28E+005 -9.466E+005 3.282E+005 Bi-21 2 39.86 1. 06 3.119E+006 4.37E+005 -1.123E+006 1.48 1E+006 727. 33 6.67 4. 3 67E+005 2 . 52 8E+005 1.993E+005 785.37 1.10 2 .554E+006 2 .379E+005 1.1.58E+006 1 62 0 .50 1. 47 l.417E+006 5.392E+004 5.808E+005 + Pb- 2 12 115.18 0.60 7.833E+006 6.13E+004 5.338E+006 3.801E+006 238.63* 43.60 6.132E+004 6.049E+004 2 .883E+004 300.09 3.30 1.051E+006 -9.057E+005 4.989E+005 Pb212-XR 74.82 10. 2 8 6.499E+005 3.62E+005 1.555E+006 3.178E+005

77. 11 17.10 3.617E+005 -2 .503E+004 1.766E+005 87.35 3.97 1. 368E+006 1 .0 8 7E+006 6.666E+005 89.78 1. 46 3.429E+006 - 3 .4 3 5E+006 1 .668E+006

+ Bi -2 1 4 609.32* 45.49 4.414E+004 4.41E+004 1. 23 9E+005 1. 947E+004 768.36 4.89 6.163E+005 4.551E+005 2 .816E+005 806.18 1. 26 2.085E+006 - 6.384E+005 9.375E+005 934.06 3. 11 9.354E+005 -2.611E+005 4. 22 1E+005 112 0 . 2 9* 14.92 1.196E+005 1 .837E+005 4.948E+004 1155.21 1. 63 1 .770E+006 - 1. 769E+005 7.895E+00 5 1 23 8.12 5.83 5.023E+005 - 1. 92 9E+005 2 . 23 4E+005 1280.98 1. 43 2 . 314E+006 6.510E+005 l.042E+006 1377.67 3.99 6. 3 61E+005 - 1.468E+005 2.752E+005 1 385. 3 1 0 .79 2 .893E+006 5.547E+005 1. 2 31E+006 1 401. 52 1. 33 1. 92 6E+006 1. 3 40E+006 8. 3 33E+005 1 407.99 2.39 9.671E+005 5 . 8 65E+005 4.114E+005 1509. 21 2.13 1. 29 3E+006 3 .754E+00 5 5. 62 1E+005 1 661. 27 1. 05 1.616E+006 - 1.513E+006 6. 25 8E+005 [280]

1cl i d e MDA Report 4/25/ 2 01( 9:09:00 AM Page 8 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM)

+         Bi-2 1 4   1729.59        2 .88  7.070E+005 4.41E+004           3.008E+005 2 .857E+005 1764.49      15.3 0   2 .691E+005                    2 . 1 22E+005 1. 2 16E+005 1 847.43       2 .03  1.040E+006                     4.426E+005 4. 2 03E+005
  >                  2 11 8.51      1.16   O.OOOE+OOO                     O.OOOE+OOO O.OOOE+OOO Pb- 2 14     241.99       7.25   6.107E+005 1.13E+005           2 . 2 41E+004 2 .943E+005 295.22     18.42    1. 93 6E+005                   1.867E+004 9. 2 08E+004 351. 93    35.60    1.127E+005                     3.623E+004 5.370E+004 785.96       1. 06  2 .656E+006                    2 .359E+005 1.204E+006 Pb2 1 4-XR     74.82      5.80   1.152E+006 6. 3 8E+005         2 .757E+006 5 .632E+005 77.11      9.70   6.376E+005                   -4.413E+004 3 .113E+005 87.35     2 .24   2.424E+006                     1.926E+006 1.181E+006 89.78      0.82   6.106E+006                   -6.116E+006 2 .969E+006 Ra-226        186.21      3 .64   1.055E+006 1.06E+006         -1.005E+004 5.075E+00 5 Ac-228        12 9. 0 7   2 .4 2  1.731E+006 1. 3 5E+005        5. 2 43E+005 8.370E+00 5 209.25      3 .89   9.722E+005                   -4.795E+005 4.665E+005 2 70. 2 4   3 . 46 1.016E+006                     2 .890E+005 4. 83 9E+005 328. 00     2 .95  1.074E+006                    -3.192E+005 5.059E+005 338. 32    11. 27   2 .975E+005                    2 . 3 22E+004 1.406E+005 409.46      1. 92  1 .642E+006                    1.052E+006 7.692E+005 463.00      4.40    6.576E+005                  -1.4 1 2E+005 3 .049E+005 794.95       4. 2 5  6.750E+005                    3 . 32 0E+005 3 .065E+005 911. 2 0   2 5.80   1. 3 46E+005                   1.273E+005 6.189E+004 964.77       4.99   6.685E+005                   -2.343E+005 3 .054E+005 968.97     15.80    2.141E+005                     5.060E+004 9.793E+004 1588.20       3 . 22 1.001E+006                     5.911E+005 4.428E+005 Pa-23 1        2 7.36   10.30    2.110E+005 2 .11E+005          8.714E+004 9.739E+004 283.69       1. 70  1.986E+006                     8.081E+005 9.426E+005 300.07       2 .47  1.404E+006                   -1. 2 10E+006 6.665E+005 30 2 .65     2 . 20 l .!:>37E +0 06                6.2 7 6E+005 7 . 2 85E+005 33 0.0 6     1. 40  2.291E+006                     8.099E+005 l.080E+006 Th- 23 4       92 . 3 8   2 .13  2.319E+006 2 .32E+006          1 .786E+004 1 .127E+006 92 .80     2 .10  2.346E+006                   - 9.102E+005 1 .140E+006 112.81       0. 21  2.167E+007                     2. 841E+006 1.051E+007 U-235        143.76     10.96    3.685E+005 6.71E+004           3.3 20E+004 l.779E+005 163.33       5.08   7.610E+005                     2 .934E+005 3 .665E+005 185.71     57. 2 0  6.708E+004                     4.506E+003 3. 22 6E+004 2 02 .11     1. 08  3.517E+006                   -1.549E+006 1.689E+006 2 05. 3 1    5.01   7.625E+005                     9.909E+004 3 . 662 E+005 Am- 2 41       59.54    3 5.90   1 .353E+005 1. 3 5E+005        6.209E+003 6. 53 1E+004
       +     Nuclide identified during the nuclide identification
       * = Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @    Half-life too short to be able to perform the decay correction

[281]

GA MM A s p C T R U M A N A L Y S s *****

 "************* *************~ ~*************************** ****************

_lename: E:\4 17\00001521.CNF

!port Generated On                  5/1/2017        9:47:33 AM tmple  Title                        B306100AFJFC028GD 1mple   Description                  turbine BUILDING tmple  Identification tmple  Type tmple Geometry

?ak Locate Threshold 3. 00 1ak Locate Range (in channels) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mple Size 1.800E+001 sq meter tmple Taken On 1/28/2 01 3 1 2 : 00 : 00 PM

quisition Started 1/21/2 01 6 2 : 22 : 23 PM ve Time 152.3 seconds

al Time 153.6 seconds ad Time 0.86 %

Energy Calibration Used Done On 1/27/ 2 015 Efficiency Calibration Used Done On 4/18/2017 Efficiency ID TB 560 EVS 1)"\°' \JI\ \,c\c:\\eJ b, 9~~ V I'-* l,-f<r

                                                                   ///¢

[282]

                                         ....JI .J.. / L U.J.. /      ::J ; "+/- I ; .J .J fi..l.'J

'*** P E A K A N A L Y S I S R E P O R T ***** Detector Name: 5456 Sample

Title:

B306100AFJFC0 2 8GD Peak Analysis Performed on: 5/1/2017 9:47:33 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV ) Area Uncert. Counts 1 1 23- 134 129.19 32 .00 1. 03 2.36E+002 59.05 2 .53E+002 2 2 03 - 209 205.40 5 1. 06 0.25 -8.95E+000 3 9.30 2 .04E+002 3 2 96 - 306 300.46 74.85 0.68 1.48E+00 2 79.48 5.97E+00 2 4 333 - 346 340.0 2 84.74 0.45 1. 4 9E+002 91. 39 6.99E+00 2 5 2 430- 2443 2434.7 0 608.58 1. 2 8 4.96E+001 27. 41 4.64E+001 6 2 634- 2 654 2643.78 660.85 1. 28 6.78E+003 166.18 3.50E+001 7 4682- 4694 4688.04 1171. 64 0. 4 9 3.31E+001 13.58 4.90E+000 8 5829- 5847 5838.60 1458.97 1. 36 9:16E+00 1 19.97 2 . 3 6E+000 = First peak in a multiplet region = Other peak in a multiplet region = Fitted singlet rors quoted at 2 .000 sigma [283]

_, * ,

• _,....., .c-:l..1. "~

---

--------- .... --..-v----.'f 4'\._.t""....., -'- '-

'*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample

Title:

B3 0 6100AFJFC028GD Nuclide Library Used: C: \ GENIE2K\CAMFILES \ Zion Lib-BNL.NLB I DENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/sq m) Uncertainty K-40 0.995 1460.82* 10.66 2 .29264E+004 5 .377 3 4E+00 3 Cd- 1 09 0.956 88.03* 3.70 1.25209E+005 8.11237E+004 Cs-13 7 0.999 661. 66* 85.10 1.42180E+005 1.74 2 67E+004 Th - 23 1 0.884 2 5.64* 14.10 1.06380E+004 3.67117E+003

84. 2 1

• 6.60 1.36896E+004 8. 9922 5E+00 3 89.95 1. 00 Am- 2 41 0.891 59.54* 35.90 - 1.59462E+002 7.00872E+002

       * = Energy l ine found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance:            10.000 keV Nuclide confidence index threshold =                                 0.30 Errors quoted at 2 .0 00 sigma

[284]

                                                      ..J/ ~ / £..V ..L I

"*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/sq m) Uncertainty K-40 0.995 2 . 2 92 641E+004 5. 3 77341E+003 Cd-109 0.956 2 .791014E+004 8.664495E+004 Cs-137 0.999 1.42 1 801E+00 5 1. 742670E+004 X Eu-155 0.341 X Pa-231 0.379 Th-23 1 0.884 1.063805E+004 3 .410752E+003 Am-241 0.89 1 -1.594619E+002 7.008718E+00 2

      ?    Nuclide    is part of an undetermined solution X = Nuclid e    rejected by the interference analysis
      @ = Nuclide contains energy l ines not used in Weighted Mean Activity Errors quoted at        2. 000 sigma
 **********      U N I D E N T I F I E D             P E A K S            **********

Peak Locate Performed on: 5/1/2017 9: 47 :33 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. ( keV) Counts per Se cond  % Uncertainty Type Nuclide 3 74.85 9.7268E-001 53.65 Sum 5 608.58 3.2579E-001 55.24 Tol. Zr-97 Sb-125 Sb-125 Cs-134 Bi-214 7 11 71.64 2 .1730E- 001 41. 02 Tol. Co-60 Cs - 134 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [285]

......... ..L...l.. \,,A\,;;;;; ... -J.J.JJ..J,. 4\. 1-;;" ,t..l'\J..1- ' - ..J/.J../ L. U.J../  ::J ~ ~ I * ...J 'i ttL"l .l:'ct(:J e ;:J '*** N U C L I D E MD A R E P O R T ***** Detector Name: 5456 Sample Geometry: Sample

Title:

B306100AFJFC0 2 8GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nucli de MDA Activity Dec. Level Name (keV) (%) (pCi/sq m) (pCi/sq m) (pCi/sq m) (pCi/sq m)

+                              K-4 0                                       1 460. 82

• 10 .66 3.008E+003 3 .01E+003 2 .293E+004 1 . 1 66E+003 Cr-51 320.08 9.91 6.955E+015 6.95E+015 -l.501E+015 3 . 3 84E+015 Mn- 54 834.85 99.98 4.926E+003 4.93E+0 0 3 -1.974E+002 2 .173E+003 Co-58 810.76 99.45 l.543E+007 l.54E+007 -2 . 3 79E+007 6.642E+006 Co-60 1173. 2 3 99.85 l. 2 44E+00 3 l.24E+00 3 7.007E+002 5.750E+002 1 332 .49 99.98 1. 25 0E+003 1.462E+003 5.744E+002 Nb-94 7 02 .65 99.81 3.689E+002 3 .69E+00 2 -1. 414E+00 2 l.610E+002 871. 09 99.89 3.692E+002 l.381E+002 l.581E+002 Sn-113 255.1 3 2 .11 3.367E+007 1. 2 5E+006 2.482E+007 l.643E+007 391. 70 64.97 l.253E+006 - l.681E+004 6.090E+005 Cs-134 475.36 1. 48 2 .516E+005 l. 3 6E+003 5.355E+004 l. 22 4E+005 563.25 8.34 2 .789E+004 1.842E+00 3 l. 32 8E+004 569.33 15.37 1. 457E+004 4.704E+00 3 6.924E+003 604.72 97.62 2 .743E+00 3 -2 .665E+003 l.312E+003 795.86 85 . 46 1 .358E+00 3 5.171E+002 5.992E+00 2 801. 95 8.69 l.403E+004 6.200E+003 6.225E+003 1038.61 0.99 1. 275E+005 3 .532E+004 5.565E+004 1167.97 1. 79 1 .305E+005 1.368E+005 6.048E+004 1 365.19 3.02 3.456E+004 3. 2 88E+002 1.417E+004

+ Cs-137 661.66* 85.10 8. 22 0E+00 2 8.22E+002 l.422E+005 3.826E+00 2 Eu-15 2 121.78 2 8.67 3 .889E+00 3 2 .03E+003 - 1. 491E+003 1.910E+00 3 2 44.70 7.61 l.539E+004 -8.496E+003 7. 51 6E+003 295.94 0.45 2 .675E+005 1. 23 7E+005 1.303E+005 344. 2 8 26.60 4.784E+003 1.707E+00 3 2 . 32 8E+00 3 367.79 0.86 1.413E+005 - 3 .456E+004 6.856E+004 411.12 2.24 6.471E+004 3 .905E+004 3 .149E+004 44 3 .96 2.83 5.506E+004 -2 .069E+004 2 .681E+004 488.68 0 .42 3.257E+005 1. 784E+005 l.577E+005 563.99 0. 4 9 2. 0 31E+005 1. 305E+005 9.672E+004 586.26 0.46 2.323E+005 -2 .055E+004 1 . 1 09E+005 678.62 0.47 9.373E+004 5.162E+004 4.1 2 2E+004 688.67 0.86 4.032E+004 5.786E+002 1.703E+004 719.35 0.28 1.641E+005 2 .640E+004 7.215E+004 778.90 12.96 3.701E+003 -3 .580E+00 3 1.628E+00 3 810.45 0. 32 l.412E+005 -7.189E+004 6.140E+004 867.37 4. 26 1.041E+004 1. 4 69E+00 3 4.482E+003 919.33 0.43 1. 2 68E+005 7.739E+00 4 5.595E+004 964.08 14.65 4.458E+003 2 .612E+003 2 .005E+00 3 1085.87 10. 2 4 6.107E+003 5.338E+003 2 .7 1 0E+00 3 1089.74 1. 73 3. 2 14E+004 7.161E+00 3 1.403E+004 1112.07 13.69 3.628E+00 3 -1.023E+004 1.553E+00 3 1212.95 1. 43 3.086E+004 4.073E+00 3 1. 2 80E+004 [286]

. ___ ..... __ . . _.......... -~-- - ..J/ .J.../ £. V.J.. I J * "':t I * ..J &:t: .t'1.l"'1 raye u Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/sq m) (pCi/sq m) (pCi/ sq m) (pCi/sq m) Eu-1 52 1249.94 0 .19 2.602E+005 2 . 0 3E+003 -3.585E+005 1.099E+005 1299.14 1. 63 2.819E+004 -5.108E+004 1.169E+004 1408.01 21. 07 2.032E+00 3 -9.726E+00 2 8. 2 1 1E+002 1457.64 0 .50 2.981E+00 5 5.926E+005 1.407E+005 1528.10 0. 2 8 1.056E+005 2 . 2 74E+004 3 .740E+004 Eu- 1 54 123.07 40.4 0 3.036E+003 1.69E+00 3 -8.105E+001 1.491E+003 2 47.9 3 6.89 1.811E+004 -3 .531E+00 3 8.837E+003 591. 76 4.95 2.128E+004 -9.405E+00 3 1.010E+004 692.42 1. 78 2.134E+004 -4.931E+00 3 9.012E+00 3 723.30 2 0.06 2.675E+003 6.084E+002 1.187E+00 3 756.8 0 4.5 2 1.166E+004 -1.763E+003 5.145E+003 873.18 12.08 3.887E+00 3 -2 .895E+003 1.664E+003 996. 2 9 10.48 5.5 0 0E+00 3 2 . 62 0E+003 2 .401E+003 1004.76 18.01 2.840E+003 1.886E+001 1 . 2 16E+00 3 1274.43 34.80 1. 686E+003 1 .5 3 0E+002 7.216E+002 1596.48 1. 80 1.863E+004 -3.435E+004 6.600E+003 Eu-1 55 45. 3 0* 1. 3 1 5.109E+004 4.50E+003 -6.716E+003 2 .453E+004 60.01 1. 22 1.032E+005 1.109E+003 5 .052E+004 86.55* 30.70 4 .505E+003 4.544E+00 3 2 .211E+003 105.31 21.10 6.749E+003 -3.292E+00 3 3.314E+00 3 Tl - 2 08 583. 1 9 85.00 1.079E+003 1.08E+003 9.341E+002 5.151E+00 2 Bi -2 11 3 51. 07 13.02 8.650E+00 3 8.65E+003 2 .966E+003 4. 2 10E+003 Pb-2 11 4 0 4.85 3 .78 3 . 2 72E+004 1. 36E+004 1.893E+004 1.593E+004 427.09 1. 76 7.333E+004 -1.999E+004 3.570E+004 832.01 3 . 52 1.356E+004 -1.042E+00 3 6.045E+003 Bi-212 39. 86 1. 06 5.916E+004 5.93E+003 -6.658E+004 2 .877E+004 727.33 6 . 67 5.931E+00 3 -8 . 3 67E+002 2 .608E+003 785.37 1.10 3 .662E+004 3.026E+003 1.605E+004 1 620.50 1 . 47 1. 4 34E+004 1.949E+003 4.533E+00 3 Pb - 2 1 2 115.18 0.60 1.662E+005 2 .51E+ 00 3 7.849E+003 8.168E+004 2 38 . 63 43.60 2.509E+003 7 .491E+002 1. 22 8E+00 3 300.09 3.30 3.098E+004 2 . 3 43E+004 1.508E+004 Pb212-XR 74.82 10.28 1 .067E+004 6.11E+00 3 2 . 2 99E+004 5 . 2 53E+00 3 77.11 17.10 6.112E+003 7.609E+OOO 3 .007E+00 3 87.35 3.97 2.510E+004 1.315E+00 2 1. 23 5E+004 89.78 1. 46 6.494E+004 2 . 800E+004 3.191E+004 Bi -2 1 4 609. 32 45.49 2.166E+00 3 2 .17E+00 3 2 .311E+00 3 1.036E+00 3 768.36 4.89 9.317E+00 3 - 2 .886E+003 4.155E+00 3 806.18 1. 26 3.246E+004 1.064E+004 l.422E+004 93 4.06 3. 11 1.618E+004 -5.389E+00 3 7.197E+003 11 2 0 .2 9 14.92 4.849E+003 2.227E+00 3 2.218E+003 1155.2 1 1. 63 2 .942E+004 -2 . 2 71E+004 1. 279E+004 1 23 8.12 5.83 9.055E+00 3 -8.577E+002 3.968E+00 3 128 0 .98 1.43 2.723E+004 -6.437E+003 l.1 2 9E+004 1377.67 3.99 1 .124E+004 -5.695E+003 4.747E+003 1385.31 0 .79 4.890E+004 2 . 2 80E+004 2.005E+004 1401.5 2 1. 33 3 .260E+004 4.782E+003 1 . 3 65E+004 1407.99 2 .39 1 .537E+004 -7.359E+003 6.212E+00 3 1509. 2 1 2 .13 1 .926E+004 -2 .062E+003 7.896E+00 3 1661. 2 7 1. 05 2 .999E+004 - 2 .856E+004 1 .123E+004 [287]

           **-** **-t' - - -                                      -'/..J../L..V..L/     .J * ~ I * ...J "'% .C"l.J.*.1        J:" Q'::jC:

Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( %) (pCi/sq m) (pCi/sq m) (pCi/sq m) (pCi/sq m) Bi-2 14 1729.59 2 .88 1.121E+004 2 .17E+003 3 .125E+ 0 03 4.198E+003 1764.49 1 5.30 4.117E+00 3 1.900E+003 l.790E+00 3 1847.43 2 . 03 1.849E+004 6.158E+00 3 7.163E+00 3

   >                         2 118.51      1.16    O.OOOE+OOO                           O.OOOE+OOO                      O.OOOE+OOO Pb- 2 14            2 41.99     7. 2 5  1.456E+004 3 .17E+00 3 5.535E+003                                    7.120E+003 2 95. 22  18.42     5.600E+003                          1.026E+003                       2 . 72 8E+003 351. 93   35.60     3.169E+003                          2 .387E+003                      l.543E+00 3 785.96     1. 06    3.611E+004                        -1.919E+004                        1. 570E+004 Pb2 1 4-XR            74.8 2   5.80     1.893E+004 1.08E+004 4.081E+004                                      9. 3 23E+00 3 77.11     9.70    1.079E+004                          1. 3 43E+001                     5 . 3 08E+003 87.35     2.24     4.455E+004                          2 .334E+002                      2 .191E+004 89.78     0.82     1.1 5 8E+005                        4.992E+004                       5.689E+004 Ra-226              186.21     3.64     2 .801E+004 2 .80E+004 8. 2 69E+00 3                                 1.374E+004 Ac-228              129.07     2.42     4.007E+004 2 .03E+003 - 9.415E+00 3                                  1.968E+004 209.25      3.89     2.833E+004                          1.786E+004                      1. 3 89E+004 270. 2 4    3.46     2.911E+004                          8.236E+003                      1.420E+004 32 8.00     2.95     3.577E+004                        -1.581E+004                       1. 740E+004 338. 32   11.27      9.060E+00 3                       -6.772E+003                       4.401E+00 3 409.46      1. 92    6.300E+004                        - 5. 2 32E+004                    3 .064E+004 463.00      4.40    3.249E+004                           1. 3 59E+004                    1.584E+004 794.95      4.25     9.806E+003                          1. 2 92E+003                    4. 3 12E+00 3 91 1. 20  2 5.80    2 .0 3 0E+00 3                    -4.494E+002                        9.092E+00 2 964.77      4.99    1.086E+004                           1.045E+00 3                     4.864E+00 3 968.97    15.80     3.438E+00 3                          5.336E+00 2                     1.540E+00 3 1 588.20       3 . 22  l.237E+004                           5. 2 65E+00 3                   5.000E+00 3 Pa- 2 31              27.36*  1 0.30    5.295E+003 5 .30E+00 3 1.456E+004                                    2 .564E+003 283.69      1. 70   5.7 3 1E+004                         8.429E+00 3                     2 .790E+004 300.07      2.47    4.1 3 9E+004                         3.130E+004                      2 .015E+004 3 02.65     2.20    4.590E+004                        - 2 . 2 54E+004                    2 . 23 4E+004 330.06     1. 40    7.824E+004                          1.157E+005                       3 .810E+004 Th-234                92.38    2.13     1.738E+018 1.74E+0 1 8 1.180E+018                                    8.542E+017 92.8 0   2 .10    1. 771E+018                         1.252E+018                       8.703E+017 112.81      0.2 1    1. 783E+01 9                        3 .056E+018                      8.760E+018 U-235              143.76     10.96     8.795E+00 3 1.78E+003 1. 25 0E+003                                   4.317E+00 3 163. 33     5.08     1.850E+004                        -5 .5 9 6E+00 3                    9 .067E+00 3 185.71     57.20     1.779E+003                          1. 0 33E+00 3                    8.725E+002 202.11      1. 08    1 .019E+005                       -5.581E+004                        4.999E+004 2 05. 3 1   5.01     2.223E+004                        -8.245E+002                        1. 091E+004

+ Am-2 41 59.54* 35.90 1.213E+00 3 1. 2 1E+003 - l.595E+002 5 .825E+00 2

         + = Nuclide identified during the nuclide identification
         * = Energy line found in the spectrum
         > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
         @ = Half-life too short to be able to perform the decay correction

[288]

"*************************      ' *************************            k***************
"***        G A M M A     S P E C T R U M          A N A L Y S .L S               *****
.lename: C:\User s \Zion Solutions\Documents\5-3-16\B306100AFIWC030GD.CN iport Generated On                    5/3/2016       1 2 :58 :2 7 PM tmple Title                           B306100AFIWC030GD tmple Description                     UNIT- 2 tmple Identification tmple Type tmple Geometry iak Locate Threshold                    3 .00 iak Locate Range (in channels)             85 -    8192 iak Area Range (in channels)               85 -   8192 lentification Energy Tolerance           10.000 keV tmpl e Size                             1. OOOE+OOO SQM tmple Taken On

quisition Started 5/3/2016 10: 2 1:0 2 AM

.ve Time 600.0 seconds ial Time 600.7 seconds iad Time 0. 12 % Energy Calibration Used Done On 1/1 3/ 2 015 Efficiency Calibration Used Done On 5/3/2016 Efficiency ID STWALL

                                                                ~dly
                                                                 /,.'1-6-1&1
                                                                   //16

[289]

ia k Anal y sis Report 5/ 3/2 01 6 12 : 5 8:27 PM Page 2

• • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 545 2 Sample

Title:

B306100AFIWC0 3 0GD Peak Analysis Performed on: 5/3/2016 12:58: 2 7 PM Peak Analysis From Channel: 85 Pea k Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid ( keV) ( keV ) Area Uncert. Counts 1 947- 96 1 954. 00 23 8.35 0.59 4.55E+001 3 1. 3 8 6.95E+001 2 2429- 24 41 2433.85 608.64 0.86 4.40E+001 2 0.47 2 .30E+001 3 5828- 585 1 5839.46 1460.1 3 1. 32 1.56E+00 2 2 8.05 1.07E+001 First peak in a multiplet region = Other peak in a multiplet region = Fitted singlet ~rors quoted at 2 .000 sigma [290]

1t erference Corrected Acti * -Y Report 5/3/2 016 12 3:27 PM Page 3 "*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample

Title:

B306100AFIWC030GD Nucl ide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nucl ide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM ) Uncertainty K-40 0. 999 1460.82* 10.66 1. 0 5762E+006 2 .10842E+0 0 5 Pb-21 2 0 .87 2 115.18 0.60 238.63* 43.60 3.01270E+004 2 .13402E+004 300.09 3 .30

       * = Energy line found in the spect rum .
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold          0 .30 Errors quoted at 2 .000 sigma

[291]

1terference Corrected Act i * -Y Report 5/ 3/2 01 6 12 3:2 7 PM Pag e 4 "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0 .999 1 . 057617E+006 2 .1084 2 5E+005 Pb-2 1 2 0. 87 2 3 . 012696E+004 2 .134018E+004

      ?     Nuclide is part of an undetermined solution X   = Nuclid e rejected by the interference analysi s
      @     Nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at         2.000 sigma
 **********       U N I D E N T I F I E D           P E A K S         **********

Peak Locate Performed on: 5/3/2 01 6 1 2 :58: 2 7 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Size in Peak CPS Peak Tol . No . (keV) Counts per Second  %~ inty Type Nucl ide 2 608.64 7 .3327E- 00 2 Tol. Zr- 97 V Sb-125 Sb-125 Cs - 1 34 Bi -2 14 M = First peak in a multipl et region m Other peak in a multipl et region F Fitted singlet Errors quoted at 2 .000 sigma [292]

1clide MDA Report 5/3/2 0 16 ~2 : 58: 2 7 PM Page 5

• • • • N U C L I D E MD A R E P O R T *****

Detector Name: 54 52 Sample Geometry : Sample

Title:

B306100AFIWC030GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Lev e l Name (keV ) (%) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) K-40 1 460.82* 10 .66 l.598E+005 l.60E+00 5 l .058E+006 7.074E+004

+

Cr-5 1 320.08 9.91 l.361E+005 1. 3 6E+005 -1.076E+005 6.348E+004 Mn-54 834.85 99.98 l.327E+004 l. 33E+004 - 8.114E+002 5.903E+00 3 Co-58 810.76 99.45 l.534E+004 1. 53E+004 1.007E+004 6.947E+00 3 Co-60 11 73.23 99.85 l. 3 69E+004 1. 37E+004 6. 3 80E+003 5.974E+00 3 1 332 .49 99.98 1.498E+004 - 3 .855E+003 6.565E+00 3 Nb-94 702.65 99.81 l.249E+004 1 . 2 5E+004 -2 .756E+003 5.568E+003 871. 09 99.89 1.485E+004 1.213E+004 6.679E+003 Sn-113 2 55.13 2 . 11 6.773E+005 2 .11E+004 2 .739E+005 3.195E+00 5 391.70 64.97 2 .113E+004 -4.812E+003 9.790E+00 3 Cs -1 34 475.36 1. 48 8. 62 0E+005 1.89E+ 00 4 -5. 2 09E+005 3 .934E+00 5 563.25 8.34 l.558E+005 6.711E+ 0 03 7.066E+004 569.33 15.37 9.300E+004 7. 3 76E+003 4.254E+004 604.72 97. 62 2 .360E+004 -1.8 1 9E+004 1.116E+004 795.86 85.46 l.894E+004 4.639E+00 2 8.634E+003 801. 95 8.69 1 .642E+005 -l.252E+005 7.382E+004 1038.61 0.99 l .555E+006 -4.574E+004 6.951E+005 1167.97 1. 79 9.112E+005 -3.886E+005 4.072E+005 1 365.19 3 . 02 3 . 454E+005 4.928E+003 1.416E+005 Cs-137 661.66 85. 10 1 .890E+004 l.89E+004 5.262E+003 8.678E+00 3 Eu-152 12 1.78 2 8.67 6.030E+004 5. 3 4E+004 4. 22 4E+003 2 .906E+004 2 44.70 7 . 61 2.213E+005 1 . 21 5E+004 1.054E+005 2 95.94 0.45 3.967E+006 5.349E+006 1.886E+006 344. 2 8 26.60 5.337E+004 - 3.337E+004 2 .492E+004 367.79 0.86 l.528E+006 -2.873E+005 7.075E+005 411.12 2 . 24 6.502E+005 1.545E+005 3 .020E+005 443.96 2 .83 5.258E+00 5 5.115E+005 2 .440E+005 488.68 0.4 2 3.431E+006 2 .627E+006 l.581E+006 563.99 0.49 2.685E+006 -7.299E+005 l. 2 19E+006 586. 2 6 0.46 3.788E+006 3 .398E+006 l .7 5 9E+006 678.62 0.47 3.448E+006 -2 .076E+005 l.584E+006 688.67 0.86 1.737E+006 -4.895E+005 7.906E+005 719.35 0.28 4.934E+006 -7.094E+004 2 . 22 3E+006 778.90 1 2 .96 l.121E+005 2 .624E+004 5.058E+004 810.45 0. 32 4.753E+006 2 .224E+006 2 .152E+006 867.37 4. 2 6 3 .805E+005 2 .064E+005 1 . 72 8E+005 919.33 0.43 3 .513E+006 l.994E+005 l.577E+006 964. 0 8 14.65 1.362E+005 l.490E+005 6. 2 71E+004 1085.87 10.24 l.448E+005 - 6.421E+004 6.425E+004 1089.74 1. 73 8. 5 86E+005 5.194E+005 3.810E+005 1112.07 1 3 .69 l.184E+005 -8.939E+004 5. 3 05E+004 1212.95 1. 43 1.308E+006 -2 .755E+005 5 .9 2 3E+00 5 [293]

1cl i de MDA Report 5/3/ 2 016 ~2: 58: 27 PM Page 6 Nuclide Energy Yi eld Line MDA Nuclide MDA Activit y Dec. Level Name (keV) ( ~) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM) Eu- 1 52 1249.94 0.19 9. 2 60E+006 5.34E+004 1.866E+006 4. 1 56E+006 1299.14 1. 63 8.861E+005 3 .579E+005 3.868E+005 140 8. 01 21.07 7.525E+004 -2 .682E+004 3.309E+004 1457.64 0.50 9.305E+006 2 .564E+007 4.459E+006 1528 . 10 0. 2 8 3 .158E+006 -1.216E+006 l. 22 3E+006 Eu-154 123.07 40.40 4. 2 67E+004 4. 2 7E+004 7.275E+003 2 .056E+004 247.93 6.89 2 .095E+005 - 1.685E+005 9.895E+004 591.76 4.95 2 .691E+005 6.518E+00 3 l.220E+005 692.42 1. 78 8.081E+005 3.254E+00 5 3.664E+005 723.30 2 0.06 6.176E+004 -2 .083E+004 2 .748E+004 756.80 4. 52 2 .857E+005 -7. 2 85E+004 1. 27 4E+005 873.18 12. 08 1.166E+005 -8.862E+003 5.213E+004 996. 2 9 10.48 1. 4 92E+005 -3.713E+004 6.696E+004 1004.76 18.01 8.566E+004 - 8.579E+004 3.837E+004 1274.43 34.80 4.519E+004 -2.931E+003 2. 000E+004 1596.48 1. 80 5.090E+005 1.695E+005 1.972E+005 Eu -155 45.30 1. 31 1 . 052E+006 7.44E+004 1.075E+006 5.024E+005 60.0 1 1. 22 1 .362E+006 -7. 2 78E+005 6.556E+00 5 86.55 30.70 7.439E+004 4.891E+004 3 .6 1 8E+004 105. 3 1 21.10 8.699E+004 -7. 2 07E+004 4.202E+004 Tl-208 583.19 85.00 2 .125E+004 2 .12E+004 1.989E+004 9 . 899E+003 Bi-211 351. 07 13.02 1.432E+005 1.43E+005 2 .034E+005 6.794E+004 Pb-211 404.85 3.78 4.140E+005 4.14E+005 2 .481E+005 1 .934E+005 427.09 1. 76 8.560E+005 4. 3 83E+005 3 .981E+005 832.01 3.52 4.259E+005 -5.223E+004 1.922E+005 Bi-212 39.86 1. 06 1 . 2 15E+006 1 .82E+005 3.494E+005 5.784E+005 727.33 6.67 1.824E+005 -5.315E+004 8.095E+004 785.37 1.10 1 . 238E+006 3.261E+005 5.545E+005 1 620.50 1. 47 6 . 853E+005 -2.875E+004 2 .7 1 9E+005 + Pb-2 1 2 11 5.18 0.60 3.074E+006 3 .27E+004 -1.318E+006 1.485E+006 238.63

• 43.60 3.265E+004 3.013E+004 1.543E+004 30 0 . 0 9 3.30 4.910E+005 - 4.015E+005 2 .322E+005 Pb212-XR 74.8 2 10.28 2.4 1 9E+005 1. 3 5E+005 4.328E+005 l.179E+005

77. 11 17.10 1. 34 6E+005 1.137E+005 6.548E+004 87.35 3.97 5.804E+005 7. 22 1E+005 2 .824E+005 89.78 1. 46 1 .497E+006 3 .145E+005 7.273E+005 Bi -2 14 60 9.32 45.49 5 . 084E+004 5.08E+004 6.184E+004 2 .403E+004 768.36 4.89 2 .709E+005 -5.654E+004 1.211E+005 806.18 1. 2 6 1. 2 04E+006 5.559E+005 5.451E+005 934. 0 6 3 .1 1 4.142E+005 -2 .530E+005 1.8 2 1E+005 1120.29 14.9 2 1. 2 86E+00 5 1.870E+004 5.863E+004 1155.2 1 1. 63 9 . 934E+005 -6.006E+004 4.440E+005 1238.12 5.83 3.792E+005 2 .695E+005 1.743E+005 1 2 80.98 1. 43 9 . 968E+005 3 .770E+005 4.352E+005 1377.67 3.99 3 .518E+005 -1.337E+005 1. 52 2E+005 1385.31 0.79 1.775E+006 -1.116E+006 7.681E+005 1401. 52 1. 33 1.245E+006 3.893E+005 5.511E+005 1407.99 2 .39 6.623E+005 - 2 .360E+005 2 .912E+005 1509. 2 1 2 .13 7.563E+005 9.501E+004 3 . 3 14E+005 1661. 2 7 1. 05 8.951E+005 -l.425E+006 3 .467E+005

[294]

1clide MDA Report 5/3 / 2 016 ~2 : 58: 2 7 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi / SQM) (pCi/SQM ) (pCi/SQM) Bi -2 14 1729.59 2 .88 2 .991E+005 5 .08E+004 8.334E+004 1.119E+005 1764.49 15.30 1.535E+005 1.693E+005 6.961E+004 1 847.43 2 .0 3 7.127E+005 1.586E+005 3 .010E+005

 >                2 118.5 1       1.16    O.OOOE+OOO                    O.OOOE+OOO      O.OOOE+OOO Pb- 2 14     2 41.99       7. 2 5  2 .735E+005    5.18E+004      1. 3 01E+004    1. 3 13E+005 2 95.22     18.42     9.527E+004                    4.849E+004      4. 52 7E+004 351.93      35 .60    5.179E+004                    3 .893E+004     2 .456E+004 785.96        1. 06   1. 24 0E+006                -6 .073E+005      5.531E+005 Pb214-XR       74.8 2      5.80    4.287E+005     2 .37E+005     7.671E+005      2 .090E+005 77.11       9.70    2 .373E+005                   2 .004E+005     1.1 5 4E+005 87.35       2 . 24  1.029E+006                    1.280E+006      5.004E+005 89.78       0.82    2.666E+006                    5.600E+005      1. 2 95E+006 Ra-22 6       186. 2 1     3 .64    4.364E+005     4. 3 6E+005   2.132E+005      2.087E+005 Ac-22 8       129.07       2 .4 2   7. 33 3E+005   8.77E+004    -6.061E+004      3.537E+005 209.25       3 .89    4.069E+005                  -1.151E+005      1.941E+005 27 0 . 2 4   3 . 46   4.501E+005                  -3 .014E+004     2 .130E+005 328. 00      2 .95    4.950E+005                   5.180E+004      2 .319E+005 338.32     11. 2 7   1.549E+005                    1. 2 63E+005    7.332E+004 409. 4 6     1. 92   7.620E+005                    1.382E+005      3.542E+005 463. 00      4.40    3 .217E+005                 -8.647E+004       1.484E+00 5 794.95        4. 2 5  3 .807E+005                   9. 32 4E+00 3   1.735E+00 5 911.20      25 .80    8.766E+004                    1. 25 3E+005    4.086E+004 964.77        4.99    4.078E+005                    5.602E+005      1 .881E+005 968.97      15.80     1. 2 53E+005                  3.048E+004      5.765E+004 1588.2 0       3 . 22  2 .189E+005                 -9.135E+004       7 . 756E+004 Pa -2 31       27.36     10.30     7.659E+004     7.66E+004      4.685E+004      3.5 27E+004 283.69        1. 70   8.272E+005                  -7.582E+004       3 .885E+005 300.07        2 .47   6.560E+005                  -5.364E+005       3 .1 02E+005 302.65        2 . 20  6.941E+005                    l.952E+005      3.270E+005 330.06        1. 40   1.085E+006                    9.936E+004      5.095E+005 Th- 234        92.38       2 .1 3  9.635E+005     9.64E+005    -2 .332E+005      4.671E+005 92.80       2 .1 0  9 . 909E+005                  1.248E+006      4.8 0 6E+005 11 2.8 1      0. 2 1  9.104E+006                    3 .401E+006     4.4 0 4E+006 U- 235       14 3.76     10.96     1 .565E+005    2 .77E+004     2 .693E+003     7.534E+004 1 63.33      5.08     3 .117E+005                   1.688E+005      1. 4 94E+005 185.71      57. 2 0   2 .774E+004                 -4.710E+003       1. 32 7E+004 2 02.11      1. 08    1.496E+006                    8.509E+005      7.150E+005 2 05.31      5.01     3.067E+005                  -1. 649E+005      1.461E+005 Am-241         59.54     35.90     4. 630E+004    4.63E+004    -6.935E+0 0 3     2.228E+004
    +=Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    >     Calculated MDA is zero due to zero counts in the region, or the region i s outside the spectrum, or MDA has not been calculated
    @ = Half-l ife too short to be abl e to perform the decay correction

[295]

"***         G A M MA     S P E C T R U M         A N A L Y S .L S                  *****
.lename: 54 52 iport Generated On                 5/ 3 /20 1 6     10:50:50 AM tmple  Title                       B306100AFIWC031GD          " ~~     s T"Ct>---- -ht ~

tmple Description UNIT-1 tmple Identification tmple Type tmpl e Geometry iak Locate Threshold 3. 00 iak Locate Range (in channels ) 85 - 8 1 92 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmpl e Size 1.000E+OOO SQM tmple Taken On

quisition Started 5/3/2016 10:40:48 AM

.ve Time 600.0 seconds ial Time 600.6 seconds iad Time 0.09 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 5/3/2 01 6 Efficiency ID STWALL Po.to. \Jd),c\q_-\eJ k, 0~4 r

                                                                ;:i.- 1,--/'l
                                                                 /J/6-

[296]

!ak Analysis Report                         5/ 3/2 01 6     10:50:50 Afl.              Page   2
****                  P E A K        A N A L Y S I S            R E P O R T Detector Name:         5452 Sample

Title:

B306100AFIWC0 3 1GD Peak Analysis Performed on: 5/3/2016 10:50:49 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8 1 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV ) Area Uncert. Counts 1 2 97- 309 30 1. 4 0 75.00 0.64 7.57E+001 51. 55 2 .20E+00 2 2 947 - 959 954.86 238.57 1. 2 4 5.33E+001 28.46 5.67E+001 3 1174- 1 1 88 11 82. 00 295.42 0.90 4.39E+001 2 1. 82 2 .61E+001 4 2 428- 2442 2435 .0 5 608.94 1.11 5.90E+001 19.63 1.30E+001 5 2 63 1 - 2653 2643.66 661.13 1. 45 2 .99E+002 38. 2 5 1.73E+001 6 58 2 6 - 5848 5838.06 1459.78 1. 98 1.55E+00 2 27.46 8.57E+OOO

= First peak in a multiplet region Other peak in a multiplet region
= Fitted singlet

rors quoted at 2. 000 sigma

[297]

1terference Corrected Acti* ~y Report 5/ 3 / 2 016 10 J:50 AM Pa ge 3 "*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample Title : B306100AFIWC031GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM ) Uncertainty K-40 0.998 1460.82* 10 .66 1.05149E+006 2 .07020E+005 Cs-137 1. 000 661.66* 85.10 1 .69885E+005 2 .98 22 4E+004 Pb-212 0.975 115.18 0.60 2 38.63* 4 3 .60 3 .5 3 122E+004 1. 97001E+004 300.09* 3 . 30 4.28133E+005 2 . 23 900E+005

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tol erance :     10.000 keV Nuclide confidence index threshold             0 .3 0 Errors quoted at 2 .000 sigma

[298]

1terference Corrected Acti, -Y Report 5/3/2 01 6 10 ):5 0 AM Page 4

• • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0.998 1 .051488E+006 2.07 01 99E+005 Cs-137 1. 000 1.698852E+005 2.982237E+004 Pb-212 0.975 3.832991E+004 1.9624 2 6E+004

      ?    Nuclid e is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ = Nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at        2 .000 sigma
 **********       U N I D E N T I F I E D          P E A K S       **********

Peak Locate Performed on: 5/ 3 /2016 10:5 0 :49 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. ( keV ) Counts per Second  % Uncertainty Type Nuclide 1 75. 00 1 . 2 61 8E- 001 El Tol. Pb214-XR Ba-133 Pb212-XR Pb212-XR Pb214-XR 4 608.94 9.8345E-0 02 Tol. Zr-97 Sb-125 Sb- 125

                                                                                 & =?ii)

M = First peak in a multiple t region m Other peak in a multiple t region F Fitted singlet Errors quo t ed at 2 . 000 s igma [299]

1clide MDA Report 5/3/2 01 6 10:50:50 AM Page 5 "*** N U C L I D E MD A R E P O R T ***** Detector Name: 5 4 52 Sample Geometry: Sample

Title:

B306100AFIWC031GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) + K-40 1 46 0 .8 2

• 10.66 1.464E+005 1. 4 6E+005 1.051E+0 0 6 6 .406E+004 Cr-51 32 0 .08 9.91 1.4 2 8E+005 1.43E+005 -5. 2 46E+004 6.681E+004 Mn-54 834.85 99.98 1.478E+004 1.48E+004 1. 22 4E+004 6.659E+00 3 Co-58 8 1 0.76 99.45 1. 2 89E+004 1. 2 9E+004 -1.341E+003 5.717E+00 3 Co-60 117 3 . 23 99.85 1.575E+004 1.50E+004 -6.515E+003 7.005E+00 3 1 332 .49 99.98 1.498E+004 7.418E+00 3 6.565E+00 3 Nb-94 702.65 99.8 1 1 .407E+004 1 . 3 8E+004 - 1.166E+004 6.360E+00 3 8 7 1. 09 99.89 1. 3 82E+004 -2 .7 62 E+00 2 6.164E+003 Sn-113 2 55.13 2 .11 7. 2 64E+005 2 .48E+004 -3 .713E+005 3.440E+005 391.70 64.97 2 .478E+004 1.731E+004 1.161E+004 Cs-134 475.36 1. 48 1.069E+006 1.74E+004 -4.141E+005 4.968E+005 563.25 8.34 1.840E+005 -5 . 3 16E+004 8.471E+004 569.33 15.37 1.043E+005 -2 .036E+004 4.817E+004 604.72 97.62 2 . 32 7E+004 -1.061E+004 1.099E+004 795.86 85.46 1.744E+004 6.0 3 1E+00 2 7.882E+00 3 801.95 8.69 1.586E+005 5. 2 09E+004 7.103E+004 10 38.6 1 0. 99 1.667E+006 1 . 35 9E+006 7.508E+005 11 67.97 1. 79 8.940E+005 - 1.0 2 9E+005 3 .987E+005 1365.19 3 .0 2 3.833E+005 2 .070E+005 l.605E+005

+ Cs- 13 7 661.66* 85.1 0 1.686E+004 1.69E+004 l.699E+005 7.659E+00 3 Eu-152 121. 78 28.67 6.558E+004 5.97E+004 2.968E+004 3 .171E+004 244.70 7.61 2.243E+005 3.855E+004 1.070E+005 295.94 0.45 3.907E+006 2 .557E+006 1.856E+006 344. 2 8 2 6.60 5.967E+004 2 .167E+004 2 .806E+004 367.79 0 .86 1.785E+006 -2 . 2 79E+005 8.360E+005 411. 12 2. 2 4 6.905E+005 -9.105E+004 3 . 2 22E+005 44 3 .96 2 .8 3 6.100E+005 -1 .109E+005 2 .861E+005 488.68 0.4 2 3.149E+006 -2 .708E+006 l.440E+006 563.99 0.49 2.998E+006 -1. 3 14E+006 1. 3 76E+006 586.26 0. 4 6 3.848E+006 1.887E+006 1 . 790E+006 678. 62 0.47 3.013E+006 4.015E+005 1. 3 66E+006 688.67 0.86 1 .759E+006 1.486E+006 8.0 1 8E+00 5 719.35 0. 2 8 6.061E+006 3.427E+005 2 .786E+00 6 778.90 12.96 1 .085E+005 -1.080E+004 4.880E+004 8 10 .45 0. 32 3 .906E+006 -2 .965E+006 1.7 2 8E+006 867.37 4. 2 6 3 . 2 35E+005 -5.183E+005 1.442E+005 919.33 0.4 3 3.194E+006 8.799E+005 1.417E+006 964.08 14.65 1. 2 62E+005 1.350E+005 5.774E+004 1 085.87 10.24 1 . 3 85E+005 -1.586E+003 6.111E+004 1 089.74 1. 73 8.402E+005 -1.965E+005 3.718E+005 1 11 2 .07 13.69 1.072E+005 -1 .883E+005 4.745E+004 1 2 1 2 .95 1. 4 3 1. 32 7E+006 8.574E+005 6.018E+00 5 [300]

iclide MDA Report 5/3/2 01 6 10:50:50 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM) Eu-1 52 1249.94 0.19 8.934E+006 5.97E+004 -5. 2 55E+00 5 3 .993E+006 1299.14 1. 63 1.020E+006 -8.001E+00 5 4.536E+005 1408.01 2 1. 07 6.743E+004 -2 .401E+004 2 .918E+004 1457.64 0.50 9.154E+006 2 .401E+007 4.383E+006 1528.10 0. 2 8 3 .948E+006 1.841E+006 1.618E+006 Eu-154 12 3 .07 40.40 4.660E+004 4.52E+004 4.113E+004 2 . 2 53E+004 247.93 6.89 2 . 2 39E+005 - 2 .444E+005 1.062E+005 591.76 4.95 2 .910E+005 2 .555E+004 1.329E+005 692.42 1. 78 8.081E+005 2 .645E+005 3 .664E+005 723.30 2 0.06 7.711E+004 -3 .836E+004 3 .515E+004 756.80 4.52 3. 070E+005 -2 .055E+005 1.380E+00 5 873.18 12 .08 1.144E+005 2 .640E+004 5 .103E+004 996. 2 9 10.48 1.662E+005 -6 .723E+004 7.544E+004 1004.76 18.01 9.841E+004 -5 .607E+004 4.474E+004 1274.4 3 34.80 4.519E+004 -1.480E+004 2 .000E+004 1596.48 1. 80 7. 3 82E+005 1.483E+005 3. 118E+005 Eu-155 45.30 1. 31 8.775E+005 7.49E+004 -2 .506E+005 4.150E+005 60.01 1.22 1.348E+006 -6. 3 13E+005 6.482E+005 86.55 30.70 7.489E+004 7.476E+004 3 .643E+004 105. 3 1 2 1.10 9.001E+004 8. 23 4E+003 4.353E+004 Tl -2 08 583.19 85.00 2 .045E+004 2 .04E+004 1.179E+004 9.498E+00 3 Bi -2 11 351.07 13.02 1.403E+005 1.40E+005 8.471E+004 6.647E+004 Pb-2 11 404.85 3 .78 4.168E+005 4.05E+005 -2.395E+005 1.948E+005 427.09 1. 76 9. 32 0E+005 -1.510E+005 4.361E+005 832.01 3.52 4.054E+005 -5. 2 80E+004 1.820E+005 Bi-212 39.86 1. 06 1.124E+006 2.38E+005 -4.655E+005 5. 32 4E+005 727.33 6.67 2 .383E+005 1. 2 06E+005 l.089E+005 785.37 1.10 1.344E+006 2. 804E+005 6.074E+005 1620.50 1. 47 7.850E+005 3.659E+00.5 3. 2 18E+005

+     Pb-2 1 2    115.18     0.60   3.139E+006       2 .84E+004 -1.589E+006     1.517E+006 23 8.63* 43 .60   2.842E+004                    3 .531E+004   1.331E+004 300.09*    3.30   3.047E+005                    4.281E+005    1.391E+005 Pb2 12 -XR   74.8 2  10.28    2.455E+005       1.35E+005 4.967E+005       1.197E+005 77.11   17.10    1.349E+005                  -2 .128E+004    6.563E+004 87.35     3.97   5.824E+005                    9.402E+005    2.833E+005 89.78     1. 4 6 1.456E+006                  -1. 54 6E+006   7.066E+005 Bi - 2 14   609. 32  45.49    4.940E+004       4.94E+004 7.242E+004       2 . 3 32E+004 768. 36    4.89   3.127E+005                  -1.275E+005     1.420E+005 806.18     1. 2 6 1.093E+006                    8.374E+004    4.895E+00 5 934.06     3.11   5.356E+005                    3 .645E+005   2 .429E+005 1120.29   14.92    1 .334E+005                   7.738E+004    6.102E+004 1155.2 1    1. 63  9.747E+005                  - 9.739E+004    4.346E+005 1238.1 2    5.83   3 .415E+005                   2 . 3 85E+005 1 .555E+005 1280.98     1. 43  1.124E+006                    3 . 3 90E+005 4.985E+005 1377.67     3 .99  3 .926E+005                   2 .106E+005   1.726E+005 1385.31     0. 79  1.881E+006                    7.969E+005    8. 211E+005 1401. 52    1. 33  1.065E+006                    7.415E+005    4.611E+005 1407.99     2 .39  5.935E+005                  - 2 .113E+005   2.568E+005 1509.21     2 .13  5 .482E+005                   2 .764E+005   2 .273E+005 1661.27     1. 05  1.051E+006                    4.471E+005    4.246E+005

[301]

iclide MDA Report 5/ 3/2 01 6 ~0 :50:50 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activit y Dec. Level Name (keV ) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi -2 14 1729.59 2 .88 5 . 22 9E+005 4.94E+004 3 . 33 4E+005 2.239E+005 1764.49 15.30 1.349E+005 1. 2 70E+005 6.029E+004 1847.4 3 2 .03 6.144E+005 2 .864E+00 5 2 .518E+005

  >               2 118.51      1.16    O.OOOE+OOO                     O.OOOE+OOO     O.OOOE+OOO Pb- 2 14     241.99      7.25    2.807E+005      5 .18E+004 -6. 3 79E+004      1.349E+005 2 95. 22  18.42     9.490E+004                     2 . 3 88E+004  4.509E+004 351.93    35.60    5.179E+004                      4.016E+004     2 . 456E+004 785.96      1. 06  1.398E+006                      2 .809E+005    6.317E+005 Pb2 1 4-XR      74.8 2    5.80    4.352E+005      2 . 3 8E+005 8.803E+005       2 .122E+005 77.11     9.70   2 . 3 78E+005                 -3 .752E+004     1.157E+005 87.35     2 . 24 1.032E+006                      1 .666E+006    5.022E+005 89.78      0.82   2 .592E+006                   -2 .753E+006     1.258E+006 Ra- 2 26     186. 21      3.64   4.777E+005       4.78E+005 -7.882E+004         2.294E+005 Ac-228       1 2 9.07     2 .4 2 7.176E+005       7.60E+004 -3.727E+005         3.458E+005 2 0 9.25     3.89   4.343E+005                     2.263E+005      2.077E+005 270.24       3 .46  4.620E+005                     3.734E+004      2.190E+005 328.00       2 .95  4.563E+005                    -3 .806E+005    2.126E+00 5 338.3 2    11. 2 7  1.535E+005                      6. 2 16E+004  7.262E+004 409.46       1. 92  8. 2 52E+005                 -3 .088E+005     3.858E+005 463. 00      4.40   3.568E+005                   -3.426E+004      1.659E+005 794.95       4.25   3.505E+005                   -2.391E+005      1.584E+005 911. 2 0   2 5.80   7.597E+004                     1.913E+004     3.502E+004 964.77       4.99   3.664E+00 5                    3.006E+005     1.674E+005 968.97     15.80    1.187E+005                     7.432E+004     5.435E+004 1588.20        3 . 22 5. 2 92E+005                   2.511E+005     2 . 32 7E+005 Pa- 23 1       27.36    10.30    6.845E+004       6.85E+004 2.223E+004         3.120E+004 283.69      1. 70   9.760E+005                     7.085E+005     4. 62 9E+005 300. 0 7    2.47    6.590E+005                   -1.819E+005      3 .117E+005 3 02 .65    2.20    7. 2 95E+005                   7.724E+005     3 .447E+005 330.06      1. 40   9.716E+005                   - 1.001E+006     4. 52 9E+005 Th- 23 4       92.38     2.13    9.595E+005      9.59E+005 1.606E+005          4. 65 1E+005 92.80     2.10    9.704E+005                   - 1.293E+005     4.704E+005 112.81      0. 2 1  9.366E+006                     3.613E+006     4.535E+006 U-23 5       143.76     10.96    1.521E+005      3 .04E+004 -4.488E+004        7. 3 14E+004 163.33      5.08    3 . 3 20E+005                -1.586E+005      1.595E+005 185.71     57. 2 0  3 .043E+004                  -6.671E+003      1.461E+004 2 02 . 1 1  1. 08   1.581E+006                   -1.137E+006      7.572E+005 2 05. 3 1   5.01    3.388E+005                   - 1.617E+005     1 .622E+005 Am-241         59.54    35.90    4.436E+004      4.44E+004 -4.473E+ 00 4       2 . 1 3 1E+004
     +=Nuclide identified during the nuclide identification
     *=Energy line found in the spectrum
     >= Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ = Half-life too short to be able to perform the decay correction

[302]

' ***        GAMM A       S P E C T R U M         A N A L Y S I S          *****
'************** * ************************* * ******** ~******* * ***** ~****** ~

_lename: 54 52 iport Generated On 9/ 1 3/20 1 6 2:31:45 PM tmple Title B306100BFRFC007GD tmpl e Descriptio n Steam Tunnel Unit-1 tmple Identification 007 tmple Type tmple Geometry 1 meter iak Locate Threshold 3 .00 iak Locate Range (in channels ) 85 - 8192 ~ak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Size 1.000E+OOO S meters tmple Taken On

quisition Started 9/13/ 2 01 6 2:21:42 PM

.ve Time 6 00 . 0 second s ial Time 6 01 .5 seconds ,ad Time 0 .25 i Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 8/9/2016 Efficiency ID UNNELSTS 1 METER DATA VALIDATED DATE 1- B-t1 TIME osoo Q.?~' [303]

J /.J...J/ L V.J..U L ; .J .J.. ; <,+/- ..J r L'l

' ** * ** 1 * ********************************************* * **** * *********** * ** ' *** P E A K A N A L Y S I S R E P O R T ***** Detector Name: 545 2 Sample

Title:

B306 1 00BFRFC007GD Peak Analysis Performed on: 9/13/2 01 6 2 :31:44 PM Peak Anal y sis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 288- 307 300.37 74.75 0.74 2 .93E+002 115.05 8.59E+002 2 949- 960 955.4 2 23 8.71 1. 35 6.69E+001 42.78 1.56E+002 3 11 75 - 1190 1180.87 295.13 0.83 8.65E+001 39.58 1.00E+00 2 4 1348 - 1357 1352.88 338. 1 8 0.4 2 l .38E+001 2 1. 97 4.72E+001 5 1400 - 1416 1407.76 351. 91 0.74 l.54E+002 4 0 .64 8.16E+001 6 2037- 2047 2042.20 51 0 .66 1. 01 2 .62E+001 22 .68 4.28E+001 7 2327- 2339 2333.44 583.5 2 0.39 5.73E+001 21. 1 3 2 .07E+001 8 2428- 2446 2 436.54 609.31 1. 32 1 .97E+00 2 35.94 3 .75E+001 9 3635- 3650 3643.01 911. 07 0.41 5. 52 E+001 20.88 1 .78E+001 10 4472- 4487 4479.63 1120. 2 5 1.10 5.19E+001 2 1. 80 2 . 2 1E+001 11 4948- 4959 4953.66 1238.75 1. 03 2 .35E+001 15.11 1. 2 5E+001 12 5832- 5854 5843. 23 1461.07 1. 44 3 .09E+002 37.45 1.lOE+OOl 13 7052- 7067 7 0 60.19 1765.1 2 0.45 4.71E+001 16.16 5.89E+OOO = First peak in a mult iplet region = Other peak in a mult iplet region Fitted singlet rors quoted at 2 . 000 sigma [304]

ll...eriereuce I....ULL\:::C Leu l"iCL.L V .L LY r<.e_!JUL L  ::J / .L.:)/ L U .L O L;.:) .L ; 'f J .t"l'J .t'a.ye .:) ' ****************************1****************************************** '*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample

Title:

B306100BFRFC007GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL . NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( ~o ) (pCi/S me) Uncertainty K-40 1. 000 1460.8 2* 10.66 1.61 62 4E+007 ~ .40944E+006 Sr-85 0.98 2 5 14.01* 96.00 8.70872E+004 7.6337.2E+004 Ba-1 33 0. 322 79.61* 2 .65 1. 77645E+007 7.86081E+006

81. 00 32 .90 2 76.40 7.16 3 02.85* 18.34 1.09566E+006 5. 312 11E+005 3 56.01* 62.05 6.41027E+005 1. 974 3 3E+005 3 83.85 8.94 Tl -2 0 8 1.000 583. 1 9* 85.00 2 . 32 181E+005 8.99971E+004 Pb-212 0.975 115. 1 8 0.60 238.63* 43.60 3 .14441E+005 2 .07 3 81E+005 300.09* 3.30 6. 08 92 1E+006 2 .95467E+006 Bi-214 0. 612 609.32* 45.49 1. 52 158E+006 3.33025E+005 768.36 4 .89 806.18 1. 2 6 934.06 3.11 1120. 2 9* 1 4.92 1. 68162E+006 7.1 942 9E+00 5 1 155. 2 1 1. 63 1238.1 2* 5.83 2 .04731E+006 1. 32 822E+006 1280.98 1. 43 1377.67 3 . 99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 1661. 27 1. 05 17 2 9.59 2.88 1764.49* 15.30 1.9 327 9E+006 6.80799E+005 1847.43 2.03 2 118.51 1.16 Pb-2 14 0.977 241. 99* 7.25 1.8 9 072E+006 1. 24625E+006 2 95. 22* 18.42 1. 0 9 090E+006 5. 2 8699E+005 351.93* 3 5.60 1.117 3 0E+006 3.44150E+005 785.96 1. 06

       * = Energy l ine found in the spectrum.
       @ = Energy l ine not used for Weighted Mean Activity Energy Tolerance :                  10.000 keV Nuclide confidence index threshold                                  0.30 Errors quoted at 2.000 sigma

[305]

1 1...t::LLt::Lt::U\....t:: \....ULL C::\.... LC::U r:l.\....L..L.V..L.LY J:'\.t::]:--'ULI...  ::J / ..L..J/ L U..L.U L ; -J .l. * ":I: J r l"l ' ****************+************************************ * ***************** '*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/S me ) Uncertainty K-40 1. 000 1.6162 40E+007 2 .409441E+006 Sr-85 0.98 2 8.708724E+004 7.6337 2 5 E+004 Ba-133 0. 32 2 3.020642E+005 8.948579E+005 Tl-208 1. 000 2.321810E+005 8.999706E+004

     ~
     "-.... Bi-211                     0.999 Pb-212                    0.975                         2 .115146E+00 5                     3 . 22 6768E+005 Bi-214                     0.612                         1. 630877E+006                      2 .704369E+005 Pb-214                     0.977                         6.378 3 72E+005                     1. 40793 1E+00 6
             ?        Nuclide is part of an undetermined solution X    = Nuclide rejected by the interference analysis
            @ = Nuclide contains energy l ines not used in Weighted Mean Activity Errors quoted at                              2 . 000 sigma
  **********                      U N I D E N T I F I E D                                       P E A K S               **********

Peak Locate Performed on: 9/13/ 2 01 6 2:3 1:44 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Pea k Energy Peak Si ze in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 4 338.18 2 . 2 992E-0 02 159. 2 2 Tol. Eu-152 Th-227 Th-227 Ac-228 Pa-231 9 911. 07 9.1924E-002 37.86 Sum M First peak in a multiplet region m = Other peak in a multiple t region F = Fitted singlet Errors quo t ed at 2 .000 sigma [306]

tC.L.Lue 1*1ul"i rs..e1-1uL L  ::;, / .L..J/ L U.LU L. * ..J .1- * ':f ..J r 1*1 '** * *********** * ****************** ~************************ * *** * *************** '*** N U C L I D E MD A R E P O R T **** -r Detector Name: 5 4 52 Sample Geometry: 1 meter Sample Title : B306100BFRFC007GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( ';; ) (pCi/S me ) (pCi/S me ) (pCi/S me ) (pCi/S me)

+       K-40                 1460.8 2

• 10.66 1. 2 50E+006 1.25E+006 1.616E+007 5.545E+005 Cr-51 320. 0 8 9.91 1. 680E+006 1.68E+006 8. 23 3E+005 8 .068E+005 Mn-54 834.85 99.98 1.632E+005 1.63E+005 1.378E+005 7.599E+004 Co-58 810.76 99.45 1.664E+005 1.66E+005 - 5.667E+004 7.764E+004 Co-60 117 3 . 23 99.85 1. 93 6E+005 1.53E+005 - 8.697E+00 3 9.009E+004 1 332 .49 99.98 1 . 533 E+005 -3.597E+004 6.949E+004 Nb-94 702.65 99.81 1.540E+005 1.54E+0 0 5 -3 .193E+005 7.185E+004 871.09 99.89 1. 606E+005 6 .3 00E+004 7.453E+004 Sn-113 255.1 3 2 .11 8.547E+006 2 .48E+005 4.514E+006 4.137E+006 391. 70 64.97 2 .485E+005 -9.620E+003 1 .185E+005 Cs- 134 475.36 1. 4 8 1.096E+007 2 .05E+005 6.991E+006 5. 2 01E+006 563. 2 5 8.34 1.866E+006 -6.885E+005 8.782E+005 569.33 15.37 1.128E+006 - 1 .077E+005 5 . 3 39E+005 604.72 97.6 2 2 .671E+005 - 1.531E+005 1. 2 87E+005 795.86 85.46 2 .049E+005 2 .657E+004 9.602E+004 8 01. 95 8.69 2 .035E+006 2 .518E+005 9.545E+005 1038.61 0.99 1. 440E+007 -7.5 2 6E+006 6.565E+006 1167.97 1. 79 1.009E+007 -8.162E+006 4.674E+006 1 365.19 3.02 5.225E+006 -4.599E+005 2 .372E+006 Cs- 1 37 661. 66 85.10 2 .004E+005 2 .00E+005 1 .421E+005 9.434E+004 Eu-152 121. 78 2 8.67 7.646E+005 6.53E+005 -8.783E+004 3.747E+005 2 44.70 7.61 2 .578E+006 6.587E+005 1. 2 52E+006 2 95.94 0.45 4.311E+007 4.585E+007 2 .085E+007 3 44. 2 8 26.60 6.533E+005 3.575E+005 3 .1 3 7E+005 3 67.79 0.86 1.884E+007 -3.593E+006 9 .004E+006 411. 12 2.24 7.293E+006 1.085E+006 3 .476E+006 443.96 2.83 5.726E+006 1. 766E+005 2 .722E+006 488.68 0.42 3.581E+007 -1.617E+007 1.690E+007 56 3 .99 0.49 3.188E+007 7.388E+006 1.501E+007 586. 2 6 0.46 4.244E+007 4.062E+007 2 .020E+007 678.62 0.47 3.500E+007 2 .066E+007 1. 643E+007 688.67 0.86 2 .016E+007 8.630E+006 9.487E+006 719.35 0. 28 5.375E+007 -1.298E+005 2 .501E+007 778.90 12.96 1.268E+006 -8.927E+005 5.923E+005 810.45 0.32 5.226E+007 - 1. 4 71E+007 2 .441E+007 867.37 4.26 3 .877E+006 -2.296E+006 1. 804E+006 919.33 0.43 3 .768E+007 -1.963E+007 1.746E+007 964.08 14.65 1.492E+006 7.930E+005 7.045E+005 1085.87 10.24 1.477E+006 -1. 686E+006 6.756E+005 1089.74 1. 73 1.009E+007 7.513E+006 4.670E+006 1112.07 13.69 1. 2 76E+00 6 - 6.200E+005 5.906E+00 5 1212.95 1. 4 3 1. 430E+007 6.971E+006 6.673E+00 6

[307]

                                                             -:::J / .l.::>/L U.LO   L. ; ::> .l. ; ':I ~ t' 1v1      t' ctye 0 lC1-lUe lVJUJ-i Ke}JUL L Nuclide          Energy      Yield      Line MDA Nuclide MDA Activity                                     Dec. Level Name              (keV )       ( \;)   (pCi/S me) (pCi/S me)                   (pCi/S me)                  (pCi/S me)

Eu-1 52 1249.94 0.19 8.489E+007 6.53E+005 -2 .8 52 E+007 3.879E+007 1 2 99.14 1. 63 1.065E+007 4.972E+006 4.893E+006 1408.01 2 1. 07 7.826E+005 -1.065E+005 3.563E+005 1 457.64 0.50 9.725E+007 3.595E+008 4.713E+007 1528.10 0. 2 8 4.988E+007 -7.256E+006 2.219E+007 Eu-154 123.07 40.40 5.355E+00 5 4.60E+005 - 4. 92 1E+003 2.624E+005 247.93 6.89 2 .425E+006 - 2 .710E+006 l.171E+006 591. 76 4.95 3 .177E+006 1. 606E+006 1. 4 94E+OO 6 692.4 2 1. 78 9 .665E+006 -1.843E+006 4.546E+006 723.30 20.06 8.256E+005 9.031E+004 3 .868E+005 756.80 4. 52 4.043E+006 1. 242 E+006 1. 904E+006 873.18 12.08 1.2 8 5E+006 -9.778E+004 5.951E+005 996. 2 9 10.48 1.7 12 E+006 9.993E+005 7.970E+005 1004.76 18.01 9.462E+005 -1. 067E+005 4. 3 87E+005 1274.43 34.80 4.599E+005 1.409E+005 2 .099E+005 1596.48 1. 80 8.363E+006 -3. 2 11E+006 3.738E+006 Eu-155 45.30 1. 31 1. 1 48E+007 8.51E+005 1. 373E+006 5.573E+006 60.01 1. 22 l.614E+007 - 3.881E+006 7.894E+006 86.55 30.70 8.512E+005 1. 3 04E+006 4.185E+005 105.31 21.10 l.086E+006 4.588E+005 5. 3 27E+005

+      Tl-208             58 3 .19* 85.00    1.091E+005            l.09E+005 2.322E+005                          4.907E+004 Bi-211             351.07*   13.02    1.100E+006            1.10E+006 3 .055E+006                         5. 2 32E+005 Pb- 2 11           404.85      3.78   4. 22 0E+006          4. 2 2E+006 -4.878E+006                       2 .010E+006 4 2 7.09    1. 76  8.801E+006                            -1.145E+007                   4.179E+006 8 32 .01    3 . 52 4. 26 4E+006                            1.807E+006                  1.973E+006 Bi-212               39.86     1. 06  l. 23 9E+007          2 .64E+006 - 2 .740E+006                      5.988E+006 727.33      6.67   2.641E+006                              7. 22 2E+005                1.242E+006 785.37      1.10   l.607E+007                            - 8.345E+006                  7.540E+006 1620.50       1. 4 7 9.084E+006                              4.367E+006                  3 .994E+0 0 6
+      Pb-2 1 2           115.18      0.60   3.900E+007            3.18E+005         3.971E+007                  1.914E+0 0 7 23 8.63*  43.60    3.183E+005                              3.144E+005                  1. 52 8E+005 300.09*     3.30   4. 23 5E+006                            6.089E+006                  2 .022E+006 Pb212-XR             74.82   10. 2 8  2.741E+006            1.55E+00 6        5.897E+005                  1. 349E+006 77.11   17.10    1. 555E+006                             2 .604E+005                 7.646E+005 87.35     3.97   6.535E+006                              4.737E+006                  3. 2 13E+006 89.78     1. 46  1.748E+007                              7.775E+006                  8.592E+006
+      Bi-214             609. 32

• 45.49 3.074E+005 3 .07E+005 1. 52 2E+006 1.432E+005 768.36 4.89 3.513E+006 1.569E+006 1. 64 7E+006 806.18 1. 2 6 1. 445E+007 9.154E+006 6.788E+006 934.06 3.11 5.411E+006 - 3.828E+005 2 .513E+006 1120. 2 9* 14.9 2 9.603E+005 1. 682E+006 4.363E+005 1155. 2 1 1. 63 l.100E+007 4.143E+006 5.095E+006 1238.12* 5.8 3 1.900E+006 2 .047E+006 8.319E+005 1280.98 1. 4 3 l.199E+007 4. 3 22E+00 5 5.506E+006 1377.67 3 .99 4.082E+006 -3 .442E+006 1. 858E+006 1385.31 0.79 2.005E+007 -7.065E+006 9.104E+006 1401. 52 1. 33 1 . 2 04E+007 -l.435E+006 5.466E+006 1 407.99 2 .39 6.888E+006 -9.374E+005 3.136E+006 1 509. 2 1 2 .13 8.484E+006 4.644E+006 3.881E+006 1 661. 2 7 1. 05 1.124E+007 3.196E+006 4.841E+006

[308]

J /.l. ..J / L. V.l.U L. . J .l. . ":IJ r1*1 JCQ'jC::

!C.L.LUe l 'JU.t-i .Kef,JUL L. Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (~ ) (pCi/S me ) (pCi/S me) (pCi/S me ) (pCi/S me)

+         Bi -2 14               1729.59      2 .88   5.884E+006          3 .07E+005            l. 13 8E+006           2 .651£+006 1764 . 49*  15. 3 0  6.864E+005                                1. 93 3E+006           2 .877E+005 1847.43      ;2 . 03 6.181E+006                              -7 .1 3 9E+005           2 .661E+006 2118.51      1.16    O.OOOE+OOO                                O.OOOE+OOO             O.OOOE+OOO
   >                                                                                            1. 8 91E+006           9.188E+00 5
+          Pb-214                 24 1. 99*   7. 2 5  1.914E+006          4.02E+005 295. 22

• 18. 42 7.587E+005 1. 091E+006 3.623E+005 351. 93* 35.60 4.023E+005 1.117E+006 1.913E+005 785.96 1. 06 1.681E+007 - 5.405E+005 7.892E+006 Pb2 1 4-XR 74.8 2 5.80 4.857E+006 2 .74E+006 1.045E+006 2 .391E+006 77.11 9.70 2 .741E+006 4.590E+005 1.348E+006 87.35 2 . 24 1.158E+007 8.396E+006 5.694E+006 89.78 0.8 ~ 3 .113E+-007 1. 384E+007 1.530E+007 Ra- 2 26 186. 2 1 3.64 5.223E+006 5. 2 2E+006 1.343E+006 2 .545E+006 Ac-22 8 129.07 2 .4 2 8.761E+006 9.01E+005 - 1.859E+006 4.290E+006 209.25 3 .89 4.791E+006 1. 044E+006 2 .329E+006 27 0 .24 3 .46 5. 2 56E+006 2 .814E+006 2 .542E+006 32 8.00 2 .95 5.725E+006 9.021E+005 2 .749E+006 338.3 2 11. 2 7 1.570E+006 3.741E+005 7.547E+005 409.46 1. 92 8.677E+006 4.403E+006 4.140E+006 463.00 4.40 3 .786E+006 -1. 705E+006 1.800E+006 794.95 4.25 3 . 9 88E+006 -1. 632E+006 1. 865E+006 911. 20 25 .80 9.015E+005 6.821E+005 4.279E+005 964.77 4.99 4.527E+006 5.072E+006 2.142E+006 968.97 15.80 1.452E+006 1. 330E+006 6.876E+005 1588 . 2 0 3 . 22 5.862E+006 4.698E+006 2.684E+006 Pa - 23 1 2 7.36 10.30 7.538E+005 7.54E+005 9.043E+005 3.558E+005 28 3 .69 1. 70 9.960E+006 - 6.029E+006 4.800E+006 300.07 2.47 7.143E+006 8. 2 46E+005 3.443E+006 302.65 2 . 20 7.650E+006 2 .732E+006 3.6808+006 330. 0 6 1. 40 1. 217E+007 -4 . 800E+006 5.8448+006 Th-234 92.38 2 .13 1.164E+007 1.16E+007 -7.714E+00 5 5.717E+006 92.80 2 .10 1.173E+007 3 .951E+00 6 5.7618+006 112 . 81 0. 21 1.095E+008 -6 .141E+00 6 5.3708+007 U-2 35 1 43.76 10.96 1.887E+006 3 .34E+005 4. 29 0E+005 9.229E+005 1 63.33 5.08 3.884E+006 7.036E+005 1. 896E+006 185.71 57. 2 0 3 .342E+005 2 .588E+005 1. 629E+005 202. 11 1. 08 1.756E+007 -7.199E+006 8.5448+006 205.31 5.01 3 .695E+006 4.207E+005 1. 796E+00 6 Am- 2 41 59.54 35.90 5.454E+005 5 . 45E+005 l .652E+005 2 .666E+00 5

        + = Nuclide identified during the nuclide identification

• Energy line found in the spectrum

        >           Calculated         MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
        @ = Half-life too short to be able to perform the decay correction

[309]

'***         GA MM A      S P E C T R U M            A N A L Y S I S             **'~**
'******************* +* ****** * ********* * **' '~*****************************
.lename: 54 52 iport Generated On                   9/13/20 1 6        2 :45:03 PM tmple  Title                         B306100BFRFC008GD tmple  Description                   Steam Tunnel Unit-1 tmple  Identification                008 tmpl e Type tmple  Geometry                      1 meter iak Locate Threshold                   3. 00 iak Locate Range (in channels )            85 -      81 92 iak Area Range (in channels)               85 -      81 92 ientification Energy Tolerance           10 . 0 0 0 keV tmple Siz e                            1 . 000E +OOO S meters tmple Taken On

quisition Started 9/13/ 2 01 6 2: 35: 01 PM

.ve Time 6 00 . 0 seconds ial Time 60 1 .4 seconds iad Time 0 .24 % Energy Calibration Used Done On 1/13/2 01 5 Efficiency Calibration Used Done On 8/9/20 1 6 Efficiency ID UNNELSTS 1 METER DATA VALIDATED DATE L-6-!2 TIME osao o.,~4.: [310]

!d J\. l"l.!!ct.J..y;::,.J..;::, I'l.t::1-'V.L L                  J / .LJ/ L V.J..U     L * <,t .J

• V J r 1*1

' ********************* * **********************+***************************
'***                                    P E A K         A N A L Y S I S                   R E P O R T                      *****

Detector Name: 54 52 Sample

Title:

B306100BFRFC008GD Peak Analysis Performed on: 9/13/20 1 6 2 :45:03 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) ( keV) Area Uncert. Counts 1 297- 306 300.69 74.83 0.94 1.45E+002 69.89 4.72E+002 2 947- 962 954.73 23 8.54 0.8 3 9.70E+001 54.16 2 .12E+002 3 1173- 1190 1180.62 2 95.07 1. 22 1. 11E+00 2 44.49 1.18E+002 4 1 401- 1417 1407.64 351.88 1. 30 1. 4 7E+00 2 42.84 9.78E+001 5 232 6- 2338 23 31. 53 583.04 0.47 4.65E+001 26.23 4.75E+001 6 2428 - 2 446 2436.94 609.41 1. 62 2 .08E+002 35.81 3 .33E+001 7 2635- 2656 2 645.64 661.62 1. 56 3.92E+002 48.45 5.20E+001 8 3637- 365 1 3643.45 911. 18 0.49 3.03E+001 22.63 3.38E+001 9 4473- 4489 4480.45 11 2 0.45 0.87 6.54E+001 24.27 2 .56E+001 10 5829- 5854 5843.03 14 61. 0 2 1. 88 3.23E+00 2 35.94 O.OOE+OOO

= First peal: in a multiplet region Other peak in a multiplet region Fitted singlet

rors quoted at 2.000 sigma

[311]

rcerrerence 1....ULLC::CLt::U i"iCL.J.V.J.LY !'i.t::l,)UL L  ::J / L .:J / LV LU L ; 'f J ; V J r l"l raye J ' *********** * ****************** * ************************** +************* ' *** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample

Title:

B306100BFRFC008GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( *'ci ) (pCi/S me) Uncertainty K-40 1.000 1460.82* 10.66 1. 68 92 6E+007 2 .38446E+006 Ba-1 33 0. 32 1 79.61* 2.6 5 8.78755E+006 4.60204E+006

81. 00 32.90 276.40 7.16 302.85* 18.34 1. 40398E+006 6.06784E+00 5 356.01* 62.05 6.11293E+005 2 .02965E+005 383.85 8.94 Cs - 1 3 7 1. 000 661.66* 85.10 l.69440E+006 2 .92002E+005 Tl-208 1. 000 583.19* 85.00 1 .88 1 61E+005 1 .08552E+005 Pb-212 0.974 115.18 0.60 23 8.63* 43.60 4.55691E+005 2 .64883E+005 300.09* 3.30 7.80272E+006 3 .37574E+006 Bi-2 1 4 0. 3 50 609. 32* 45.49 1. 6 0 868E+006 3 .38048E+005 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120.29* 1 4.92 2 .12020E+006 8.04956E+0 0 5 11 55.21 1. 63 1238. 1 2 5.83 1 2 80.98 1. 43 1 377.67 3.99 1 385.31 0.79 1 401. 52 1. 33 1407.99 2 .39 1509.21 2 .13 1661.27 1. 05 1729.59 2 .88 1764.49 15.3 0 1847.43 2 .03 2 118.51 1.16 Pb-21 4 0.977 2 41. 99* 7.25 2 .74005E+006 1. 5 9154E+006 2 95. 2 Z* 18.42 1.39788E+006 6.03854E+005 351.93* 35.60 1.06547E+006 3 .53788E+005 785.96 1. 06

        *=Energy line found in the spectrum.
        @ = Energy line not used for Weighted Mean Activity Energy Tolerance :                 10. 000 keV Nuclide confidence index threshold =                                  0. 3 0 Errors quoted at 2 .000 s igma

[312]

l LCL.LCLCl!I...... C::: VV.L.LC::1......,l-C::U L"l.Vl-.LV .L l-Y l."\'C.t""'V..1...L.. J/ J.....J/ .£. VJ....U L.. * "":::t ....J

• V....J L l."l I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/S me ) Uncertainty K-40 1. 000 1. 68 92 61E+007 2 .384455E+006 Ba- 133 0.321 1.121905E+004 9.781 2 79E+005 Cs- 137 1. 000 1. 694396E+006 2 .920016E+005 Tl-2 08 1. 000 1 .88161 3E+005 1.0855 2 4E+005 X Bi-2 11 0.999 Pb-212 0.974 2 .771693E+005 3.844690E+005 Bi-214 0.350 1.685369E+ 00 6 3.116785E+005 Pb-~14 0.977 1.118649E+ 00 6 1.565014E+006

       ?         Nuclide is part of an undetermined solution X  = Nuclide rejected by the interference analysis
       @  = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at                             2 .000 sigma
  '~********'"               U N I D E N T I F I E D                                      P E A K S               **********

Peak Locate Performed on: 9/13/20 1 6 2 :45:03 PM Peak Locate From Channel: 85 Pea k Locate To Channel: 81 92 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV ) Counts per Second  % Uncertainty Type Nuclide 8 911.18 5.0417E-002 7 4.8 1 Sum M = First peak in a multiple t region m Other peak in a multiple t region F Fitted singlet Errors quoted at 2 . 000 sigma [313]

lC.L.LUe 1*1u.M. I',e]:.JUL L.  ::J / .L ..)/ L V.LU L , ":I ..J

• V ..J r t*J

'* +**** * *********************************************************************** ' *** N U C L I D E MD A R E P O R T ***** Detector Name: 5452 Sample Geometry: 1 meter Sample

Title:

B306100BFRFC008GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (t ) (pCi/S me ) (pCi/S me) (pCi/S me ) (pCi/S me )

+       K-40                 1460.8 2*    10.66    1.415E+005        1.42E+005 1. 689E+007                            O.OOOE+OOO Cr-51                  320.08       9.91   1.775E+006        1. 77E+006 - 6.834E+005                          8.540E+005 Mn-54                  834.85     99.98    1.692E+005        1. 69E+005 9.234E+004                            7.899E+004 Co-58                  810.76     99.45    1.616E+005        1.62E+005 6.327E+004                             7.525E+004 Co-6 0               117 3 . 23   99.85    1.682E+005        1.68E+005 - 1.498E+005                           7.738E+004 1332.49       99.98    l.697E+005                             l. 3 86E+00 5               7.769E+004 Nb-94                  702.65     99.81    1.714E+005        1 .33E+005 1 .021E+005                           8.057E+004 871. 09    99.89    1. 332 E+005                         -8.806E+004                   6.086E+004 Sn- 1 13               2 55. 1 3    2 .11  8.8 62 E+006      2 .85E+005 1.558E+006                            4. 2 94E+006 391. 7 0   64.97   2 .849E+005                           -9.019E+003                   1.367E+005 Cs-134                 475.36       1. 48 1 .170E+007        2 .14E+005 1.824E+006                            5.569E+006 563. 2 5     8.34  2 .093E+006                           - 1.501E+006                  9.920E+005 569.33     15.37   1.133E+006                            -4.106E+005                  5.364E+005 6 0 4.72   97. 62  2 .772E+005                             6.028E+004                 1.338E+005 795.86     85.46   2 .135E+005                             8.598E+004                 1.003E+005 801. 95      8.69  1.972E+006                              7.111E+004                  9. 2 30E+005 1 038.61        0.99  1.675E+007                              7.509E+006                 7.737E+006 1167.97         1. 79 9.360E+006                           -5.521E+006                   4.307E+006 1 365.19        3.02  4.081E+006                              1.841E+006                 1.800E+006

+ Cs- 1 37 661.66* 85.10 2 .102E+005 2 .10E+005 1.694E+006 9.925E+004 Eu-1 52 121. 78 2 8.67 7.940E+005 6.89E+005 -1.771E+004 3.894E+005 244.70 7.61 2 .578E+006 1.451E+006 1 .252E+006 295.94 0.45 4.743E+007 6.148E+007 2.301E+007 344.28 2 6.60 6.886E+005 - 6.599E+005 3.314E+005 367.79 0. 86 1.872E+007 - 1.005E+007 8.947E+006 411.12 2.24 8.202E+006 2 .160E+006 3.930E+006 443.96 2.83 6.359E+006 -4.233E+005 3 .038E+006 488.68 0.4 2 3.964E+007 8.365E+005 1.882E+007 563.99 0.49 3.573E+007 -3.898E+006 1.693E+007 586. 2 6 0.46 4.808E+007 6.555E+007 2 .302E+007 678.62 0.47 3.479E+007 - 4. 2 03E+006 1.633E+007 688.67 0.86 1.892E+007 -3 .8 2 5E+005 8.867E+006 719.35 0. 2 8 6. 2 78E+007 1.490E+006 2 .953E+007 778.90 12.96 1 . 2 51E+006 -2 .198E+005 5 .835E+005 810.45 0.32 5.043E+007 3 .5 3 1E+007 2 . 3 49E+007 867.37 4.26 3.695E+006 -1. 2 90E+006 1. 713E+006 919.33 0.43 4.500E+007 -2 . 5 86E+007 2 .112E+007 964.08 14.65 1. 418E+006 1.038E+006 6 .676E+005 1085.87 10.24 1.759E+006 3.059E+003 8.168E+005 1089.74 1. 73 1. 085E+007 4.788E+006 5.051E+006 1112.07 13.69 1. 2 30E+006 4.404E+005 5.674E+005 1212.95 1. 4 3 1 . 2 10E+007 -1.376E+007 5.571E+006 [314]

1*JLJ.l"1 !'I.C:]:JU L L :J / .l. .J/ L. U.l.V '-" * "":t .J

• V ...J r: 1*1 ra~ c: V IC.L.l.Ut::

Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( ~) (pCi/S me ) (pCi/S me) (pCi/S me ) (pCi/S me) Eu-1 52 1249.94 0.19 9.450E+007 6.89E+005 2 . 32 4E+007 4.359E+007 1299.14 1. 63 8.905E+006 4.811E+005 4.018E+006 1408.01 2 1 . 07 7.514E+005 - 6.753E+005 3.407E+005 1 457.64 0.50 9.669E+007 3.573E+008 4.685E+007 1 528.10 0 .2 8 3.828E+007 - 2 .114E+007 1.639E+007 Eu -15 4 123.07 40.40 5.633E+005 4.8 2 E+005 -1. 68 OE+OO 4 2 .762E+005 247.93 6.89 2 .606E+006 -1.688E+006 1.262E+006 591. 76 4.95 3 .417E+006 3 .514E+005 1 .614E+006 692.4 2 1. 78 8.998E+006 -4.645E+004 4. 2 1 2E+006 723.3 0 20.06 8.995E+005 7. 52 7E+005 4. 23 8E+005 756.80 4. 52 3 .632E+006 2 .1 8 1E+005 1. 698E+006 873.18 12.08 1. l 79E+006 8. 0 65E+004 5 . 422E+005 996.29 10.48 1. 591E+006 4. 3 47E+005 7.369E+005 1004.76 18.01 8.077E+005 - 1.174E+004 3 .694E+005 1274.43 34.80 4. 82 1E+005 -9.587E+004 2 . 2 10E+005 1596.48 1. 80 5.713E+006 -4.526E+006 2 .413E+006 Eu-1 5 5 45. 3 0 1. 3 1 1.174E+007 8.88E+005 6.074E+006 5.703E+006 60.01 1. 22 1.699E+007 -8.576E+006 8. 3 17E+006 86.55 30.70 8.876E+005 1. 355E+006 4. 3 67E+005 10 5.31 2 1.10 1.110E+006 -4.931E+005 5.449E+005

+          Tl-208                     58 3 .19* 85.00    1.601E+005        1.60E+ 005           1.882E+005                    7.459E+004 Bi-211                     3 51. 07* 1 3 .02  1. 2 02E+006      1. 2 0E+006          2 .913E+006                   5.745E+005 Pb-211                     404.85      3.78   5.038E+006        4.34E+006            3 .059E+006                   2 .419E+006 427.09      1. 76  1.074E+007                             1.078E+007                    5.146E+006 8 32 .01    3 . 52 4. 33 9E+006                         -5.717E+004                     2 .011E+006 Bi-212                       39.86     1. 06  1 .317E+007       2 .67E+006         -1. 164E+OO 6                   6.381E+006 727.33      6.67   2.670E+006                           -5 .873E+005                    1. 2 57E+006 785.37      1.10   1.548E+007                             3 .142E+006                   7. 2 48E+006 1 620.5 0     1. 4 7 8.627E+006                           -6.577E+006                     3.766E+006
+          Pb-2 1 2                   115.18      0.6 0  3.869E+007        4.03E+005            5.191E+006                    1 .898E+007 238.63*   43.6 0   4.026E+ 0 05                           4.557E+005                    1.949E+005 30 0 .09*   3.3 0  4.727E+006                             7.803E+006                    2 . 26 8E+006 Pb212-XR                     7 4.82  10.28    2 .733E+006       l.56E+00 6           7.569E+006                    1.345E+006 77.11   17.10    1.559E+006                           -1. 669E+005                    7.668E+005 87.35     3 .97  6.790E+006                             5.040E+006                    3 . 3 40E+006 89.78     1. 46  1.770E+007                             1.130E+007                    8.702E+006
+          Bi -2 14                   609.3 2

• 45.49 2 .915E+005 2 .92E+005 1. 609E+006 l.353E+005 768.36 4.89 3.620E+006 3 .850E+006 1. 700E+006 806. 1 8 1.26 1. 2 58E+007 -1. 322 E+007 5.855E+006 934.06 3.1 1 6.138E+006 6. 622 E+006 2 .877E+006 1120.29* 14.9 2 l.053E+006 2 .120E+006 4.8 2 5E+005 1155.21 1. 63 l .061E+007 -2 .540E+006 4.899E+006 1238.12 5.83 4.042E+006 4.903E+006 1. 903E+006 1280.98 1. 43 1. 249E+007 9.420E+006 5.756E+006 1377.67 3.99 4.339E+006 2 .803E+006 1. 987E+006 1385.31 0.79 l.920E+007 -1.899E+007 8.680E+006 1401.5 2 1. 33 l.220E+007 -5.476E+006 5.548E+006 1407.99 2.39 6.613E+006 -5.943E+006 2 .998E+006 1509. 2 1 2.13 8.076E+006 3.352E+006 3 .676E+006 1 661. 2 7 1. 05 l .086E+007 -3.715E+006 4.651E+006

[315]

lC.L.LUt::! 1*JLJh !'.t::!.f:JUL L. :J/.LJ/L. U.LO L. ; ':f;J; UJ r-1*1 J:'df::lt::! Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( \; ) (pCi/S me ) (pCi/S me ) (pCi/S me) (pCi/S me)

+           Bi-214                  1729.59       2 .88    5.388E+006 2.92 E+005           4.953E+006             2 .4 02E+006 1764.49     15.30      1 .589E+006                     1.528E+006             7. 3 91E+005 1847.43       2 .03    6.945E+006                      5.394E+006             3.043E+006
    >                               2 118.51      1.16     O.OOOE+OOO                      O.OOOE+OOO             O.OOOE+OOO
+           Pb- 2 14                  2 41.99*    7. 2 5   2 .421E+006 4.40E+005           2 .740E+006            1.172E+006 2 95. 22* 1 8.42     8.468E+005                      1.398E+006             4.064E+005 351.93*   3 5.60     4.398E+005                      1.065E+006             2 .101E+005 785.96      1. 06   1 .610E+007                    - 3.582E+006             7.538E+006 Pb2 14 -XR                  7 4.82    5.80     4.843E+006 2 .75E+006           1.341E+007             2 .384E+006 77 .11    9.70    2 .748E+006                    -2 .942E+005             1.352E+006 87.35     2 . 24  1. 2 03E+007                     8.933E+006             5. 92 0E+006 89.78     0.8 2   3.152E+007                       2 .013E+007            1. 54 9--E+007 Ra-2 2 6                   186.2 1     3.64    5.607E+006 5.61E+006             6.543E+006             2 .737E+006 Ac-228                     1 2 9.07    2 .42   9.117E+006 8.98E+005             1.113E+006             4.468E+006 209.25      3.89    5.089E+006                       3.409E+006             2 .478E+006 270.2 4     3.46    5.133E+006                     - 8.754E+005             2 .480E+006 328. 00     2 .95   5.982E+006                       1.403E+006             2 .878E+006 338.32    11. 27    1. 793E+006                      1.768E+006             8.663E+005 409.46      1. 92   9.379E+006                       1.667E+006             4.491E+006 463.00      4.40    4.098E+006                       1.888E+005            1. 956E+006 794.95      4.25    4. 2 42E+006                  -7.753E+004              1. 992E+006 911.20    2 5.80    8.979E+005                       3.007E+005            4. 2 61E+005 964.77      4.99    4.120E+006                       1 .805E+006           1. 938E+006 968.97     15.80     1.304E+006                       5.498E+005            6.136E+005 1588. 2 0       3. 22   4.565E+006                    - 4. 2 75E+006           2.035E+006 Pa- 2 3 1                   27.36    10.30     8.411E+005 8.4 1E+005            1.198E+006            3.994E+005 28 3 .69     1. 70   1.004E+007                    -3 .770E+006             4.840E+006 300.07      2 .47    7.675E+006                       1.856E+006            3.709E+006 302.65      2.20     7.866E+0 0 6                    1.156E+006             3.788E+006 330.06      1. 40    1. 222E+0 0 7                 -3.606E+006              5.873E+006 Th-234                      92.38     2 .13    1.156E+007 1.16E+007          -1.731E+006              5.677E+006 92.8 0    2 .10    1.163E+007                    - 2 .553E+006            5.711E+006 112.8 1     0.21     1.120E+008                      2 .359E+007            5.496E+007 U-235                     143.76     10.96     1. 871E+006 3.56E+005         -5.450E+005              9.149E+005 163.33      5.08     3 .945E+006                     1. 270E+006            1.927E+006 185.71     57. 2 0   3 .563E+005                     2 .789E+005            1. 739E+005 2 02.11     1. 08    1. 816E+007                     3 .123E+006            8.844E+006 2 05.3 1    5. 0 1   3 .911E+006                   -1.216E+006              1.905E+006 Am-24 1                     59.54    35.90     5.701E+005 5.70E+005          -6.719E+004              2 .790E+005
        +        Nucl ide identified during the nuclide identification

• Energy line found in the spectrum

        > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
        @ = Half-life too short to be able to perform the decay correction

[316]

'***           GA MM A       S P E C T R U M           A N ALYSIS                   *****
' *** * ***********~***** +* * ******************* * *************** * ***********

_lename: 5452

!port Generated On                     8/10/2016         4:01:17 PM tmple    Title                         B306100BFRWC009GD tmple    Description                   ST SE. WALL NUMB 9A SHOT tmple    Identification                9 tmple    Type tmple    Geometry

!ak Locate Threshold 3. 00 !ak Locate Range (in channels ) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Si ze 1. OOOE+OOO SQM tmple Taken On

quisition Started 8/ 10 /2 0 16 3:5 1 : 1 5 PM

_ve Time 600.0 seconds !al Time 601. 2 seconds iad Ti me 0.2 1 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 8/9/2016 Efficiency ID UNNELSTS 1 METER DATA VAUDA1l:D DATE/* 8-11 Tl ME_o 5:LO ar&/4" [317]

U/ .LV/ L...V..J..V -:I

• V .L * .J.. I .L J.".1 P E A K A N A L Y S I S R E P O R T **** *

' ****** +*****************************************************************

Detector Name: 5452 Sample

Title:

B306100BFRWC009GD Peak Analysis Performed on: 8/10/2016 4:01:17 PM Peak Analysi s From Channel: 85 Peak Analysi s To Channel: 8 1 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid ( keV) (keV) Area Uncert. Counts 1 11 3- 123 116.05 2 8 . 60 0.50 5. 3 9E+001 30.00 5.71E+001 2 259- 2 70 2 63.10 65.41 0. 42 9.92E+OOO 56.15 3 .10E+00 2 3 288- 306 300.40 74.75 1. 03 2 .16E+002 98. 2 0 6.50E+00 2 4 739- 749 743.08 185.56 0. 35 1.41E+001 41. 08 1 . 71E+00 2 5 950 - 959 954.99 2 38.60 0.50 9.13E+001 34.59 9.17E+001 6 1076 - 1086 1080.92 2 70.1 2 0. 2 5 1.15E+001 27.57 7.35E+001 7 1400- 1413 1407.59 3 51. 8 7 0.87 9.65E+001 32.26 5.95E+001 8 1847- 1 856 1851. 52 4 62. 95 0.55 1. 89E+00 1 16.32 2 .llE+OOl 9 2 326- 2 338 2 331 .93 583.14 0.42 2 .97E+001 20.04 2 .63E+001 10 2 425- 2 446 2435.86 6 0 9.14 0.89 1.52E+002 31. 92 2 .75E+001 11 4474- 4485 4479.38 1120.19 0.98 3 .22E+001 14.03 6.79E+000 12 4947 - 4958 4952.89 1238.56 0.32 1. 78E+OOO 14.94 2 .12E+001 13 5828 - 5853 5842.08 1 460.79 1. 86 2 .88E+002 36.35 9.84E+OOO First peak in a multiplet region

= Other peak in a multiplet region
= Fitted singlet

• rors quoted at 2 .000 sigma

[318]

lLt::L L t::Lt::lH;e l..,UL.L\::::l_;Lt::;:U hl_;L.l.V.l.LY J:\.t::.f:JU.LL U/ .l.V/ L V.l.U ':I

• V .L * .l. I r 1*1

'*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** Sample

Title:

B306100BFRWC009GD Nuclide Libr a ry Used: C:\GENIE2K\CAMFILE S \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( ~) (pCi/SQM) Uncertainty K-40 1. 000 1460.82* 10.66 1.50689E+007 2 .30775E+006 Hg-203 0.876 279.20* 81. 56 3 .11740E+004 7.46791E+004 Tl-208 1. 000 58 3 .19* 85.00 1. 2 0160E+005 8. 2392 5E+004 Pb-21 2 0.873 115.18 0.60 23 8.63* 43.60 4. 2 8843E+005 1. 76695E+005 300.09 3.3 0 Bi- 2 1 4 0.4 2 8 609.3 2

• 45.49 l . 1 72 84E+006 2 .84479E+00 5 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120. 2 9* 14.92 1.04430E+006 4. 62403E+005 1 155. 2 1 1. 63 1238.1:* 5.83 1. 55472E+005 1. 3034 9E+006 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1 401.5 2 1. 33 1407.99 2.39 1509. 2 1 2.13 1661. 2 7 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.491 2 41. 99* 7. 2 5 2 .57862E+006 l.06088E+006 2 95. 22 18.42 3 51. 93* 35.60 6 .98493E+005 2 .58780E+005 785.96 1. 06 Rn-219 0.43 5 271. 2 3* 10.80 2 . 3 5409E+005 5.64543E+005 401. 81 6 .60 Ra-226 0.999 186. 2 1* 3.64 6.95573E+005 2 .02363E+006 Th-231 0.875 2 5.64* 14.10 6.14949E+005 3 .71914E+005 84.21* 6 . 60 5 . 2 7017E+006 2 .69096E+006 89.95 1. 00 Th- 232 0.996 6 3 .81* 0.26 6. 0 6712E+006 3 .43516E+007 U-235 0.548 143.76 10.96 1 63.33 5.08 185.71* 57 .2 0 4.4 263 7E+00 4 1. 2 8779E+005 20 2 .11 1. 08 205.31 5.01 Arn-241 0.94 6 59.54* 35.90 4.44471E+00 4 2 .51 62 0£+005

[319]

lL.C::LLC::LC::!ll.,C:: l..,ULLC::l.,l..C:U rll..,l...LV.LL.Y I'I.C:_l:-IV.LL. U/ .l.V/ LV.l.U ""i

• V .1. * .L I r l"l Nuclide Id Energy Yield Activity Acti-vity Name Confidence (keV) ( %) (pCi/SQM ) Uncertaint y

          * = Energy line found in the spectrum.
          @ = Energy line not used for Weighted Mean Activity Energy Tolerance :                           10.000 keV Nuclide confidence index threshold                                          0 .3 0 Errors quoted at 2 .000 sigma

[320]

U/ J.U/ L UJ.U '"i

• u J.
• J. , r 1*i

' *** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nucl ide Wt mean Wt mean Nuclide Id Activi t 11 Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 l.506890E+007 2 . 3 07749E+006

   ?   Hg-203         0.876         3.117397E+004        7.467914E+004 Tl-208         1. 000        1. 2 01602E+005      8. 2392 47E+004 X   Bi-211         0.999 Pb-21 2        0.873         3.126785E+005        1. 815942E+005 Bi-214          0.428         1.104748E+006        2 .382165£+005 Pb-214         0.491         6.984931E+005        2.587653£+005
   ?  Rn-219          0.435         2 .354090£+005       5.645429£+005
   ?  Ra-2 2 6        0.999         6.955728£+005        2.023635£+006 X   Pa-231         0.384 Th-231          0.875         7.022051E+005        3.684124£+005
   ?  Th-232          0.996         6.067120E+006        3.435155E+007
   ?  U-235           0.548         4.426372E+004        l. 2 87790E+005
   ?  Arn-241         0.946         4.444715E+004        2.516198E+005
      ?   = Nuclide is part of an undetermined solution X   = Nuclide rejected by the interference analysis
      @   = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at        2 . 000 sigma
  **********       U N I D E N T I F I E D          P E A K S        **********

Peak Locate Performed on: 8/10/ 2 01 6 4: 01: 16 PM Peak Locate From Channel: 85 Peak Locat e To Channel: 81 92 Peak Energy Peak Size in Peak CPS Pea k Tol. No. (keV) Counts per Second i Uncertainty Type Nuclide 8 4 62 .95 3.1448E-00 2 86.48 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F Fitted singlet Errors quoted at 2 .000 sigma [321]

0/J.V/ L VJ.U ':t

• V J. * .L I r l"l lC..L..LUe 1*1u.H KefJUL L

' * * *** * ****~********************** * ******************************************** N U C L I D E M D A R E P O R T ***** '***************************************************************************'~** Detector Name: 5452 Sample Geometry: Sample

Title:

B306100BFRWC009GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( i5 ) (pCi/SQM ) (pCi/ SQM ) (pCi/SQM ) (pCi/SQM )

 +         K-40           1460.82*    10.66    1.259E+006       1 .26E+00 6 1.507E+007                  5.587E+00 5 Cr-51            320.08      9.91   1.618E+006       1. 62E+00 6 9.871E+005                  7.758E+00 5 Mn-54             834.85    99.98    1 . 582E+005     l.58E+00 5 -1.009E+005                  7.349E+004 Co-58             810.76    99.45    1.592E+005       1.59E+005 3.069E+004                    7.402E+004 Co-60           1173. 23    99.85    1.749E+005       1.47E+005 2 .553E+004                   8.075E+004 1 33 2 .49  99.98    1.466E+005                     -3.159E+004               6.615E+004 Nb-94            70 2 .65  99.81    l.496E+005       1. 5 0E+005 -6.530E+004                 6.964E+004 871. 09   99.89    1. 579E+005                      8.381E+004              7.321E+004 Sn-113           255.13      2 .11  7.477E+006       2 .38E+005 4. 22 3E+004                 3 .602E+006 391.70    64.97    2 . 3 84E+005                  -9.701E+003               1. 135E+005 Cs-134            475.36      1. 48  1.017E+007       1.98E+005 -2 .957E+006                  4.805E+006

• 563. 2 5 8.34 1.846E+006 5.363E+005 8.680E+005 569.33 15.37 1.051E+006 3. 651E+005 4.955E+005 604.72 97. 62 2 . 38 4E+005 - 4.077E+004 1.143E+005 795.86 85.46 1.984E+005 1.158E+005 9. 2 81E+004 801.95 8.69 1.894E+006 -2 .402E+005 8.837E+005 1038.61 0.99 1.422E+007 -1.529E+006 6.474E+006 1167.97 1. 79 1.061E+007 4.251E+006 4.931E+006 1365.19 3.02 4. 3 54E+006 -2 .243E+006 1. 937E+006 Cs-137 661.66 85.10 1. 949E+005 1 . 95E+0 0 5 8.861E+004 9. 1 62E+004 Eu-1 52 1 21. 78 2 8.67 7.050E+005 5.76E+005 - 5 .844E+005 3 .449E+005 2 44.7 0 7. 61 2 .348E+006 1.721E+006 1.137E+006 2 95.94 0.45 3.788E+007 2 .583E+007 1.824E+007 3 44.28 2 6.60 5.761E+005 -5.799E+005 2 .751E+005 3 67.79 0.86 1.634E+007 -2.176E+006 7.756E+006 411.12 2 . 24 6.750E+006 2.525E+005 3.204E+006 443.96 2 .8 3 4.959E+006 -4.018E+00 6 2 . 33 9E+006 488.68 0.42 3 .753E+007 -4.701E+00 6 1.776E+007 563.99 0.49 3 .137E+007 1.849E+007 1.475E+007 586.26 0.46 3 .963E+007 1. 562E+007 1. 880E+007 678.62 0.47 2 .963E+007 -1. 837E+007 1.375E+007 688.67 0.86 1.667E+007 3.145E+006 7.746E+006 719.35 0.28 4.947E+007 1.507E+007 2 . 2 87E+007 778.90 12.96 1.079E+006 -1.7 5 6E+005 4.977E+005 810.45 0 . 32 5.006E+007 3. 2 84E+007 2.331E+007 867.37 4. 26 3.535E+006 -2 .7 3 6E+006 1. 633E+006 919.33 0.43 3.895E+007 -4.154E+007 1.809E+007 964.08 14.65 1.148E+006 7.063E+005 5.326E+005 1085.87 10. 2 4 1.745E+006 2 .325E+005 8.096E+005 1089.74 1. 7 3 9.818E+006 -2 .758E+005 4.536E+006 1112.07 13.69 1. 2 06E+006 -5. 22 7E+005 5.555E+005 1212.95 1. 43 1. 2 69E+007 8.650E+006 5.866E+006

[322]

CJ/ .l.V/ L. V.l.U ":i

• U ..L *..LI r: l'J r: Cl ~ c:;

l(.;.L .L Ue 1*1u11. rs.e.!,JUL L Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) h) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Eu-15 2 1249.94 0.19 9. 2 67E+007 5.76E+005 5.274E+007 4.267E+007 1299.14 1. 63 9.697E+006 2 .025E+006 4 .415E+00 6 1 408.01 2 1.07 7.5 1 4E+005 -2 .124E+005 3 .407E+005 1457.64 0.50 9.337E+007 3 .032E+008 4.519E+007 1528.10 0. 2 8 3. 22 6E+007 -l.271E+006 l. 3 38E+007 Eu- 1 54 123.07 40.40 5.055E+005 3.9.=:E+005 8.010E+004 2. 474E+005 247.93 6.89 2.351E+006 -2 .637E+005 1.1 3 4E+006 591. 76 4.95 3.230E+006 -1.227E+006 1. 52 0E+006 692.42 1. 78 7.820E+006 7.594E+005 3 . 62 3E+006 723.30 20.06 7. 2 64E+005 1. 4 4 OE+004 3 .372E+005 756.8 0 4. 52 2 .928E+006 -5.506E+005 1.346E+006 873.18 12 .08 l.296E+006 8.808E+005 6.006E+005 996. 2 9 10.48 1.633E+006 2 .175E+005 7.574E+005 1004.76 18.01 9.054E+005 4.216E+005 4.183E+005 1274.43 34.80 3.921E+005 - 4.376E+005 1.760E+005 1596.48 1. 80 8.045E+006 4.607E+006 3 .579E+006 Eu-155 45. 3 0 1. 3 1 1.001E+007 7.80E+005 - 1.869E+006 4.837E+006 60.01 1. 22 1 .432E+007 -2 . 3 09E+006 6.984E+006 86.55 30.70 7.800E+005 1. 2 04E+006 3.829E+005 105.31 21.10 1.037E+006 -9.616E+004 5.082E+005

+           Tl-208                 583.19*   85.00    1.229E+005        1.23E+005          1. 2 02E+005             5.599E+004 Bi-211                 351. 07*  13.02    8.860E+005        8.86E+005          1. 910E+006              4.162E+005 Pb-2 11                404.85      3.78   4.160E+006        4. 1 6E+006        3.872E+004               1. 980E+006 427.09      1. 76  8.696E+006                           2.677E+005               4.126E+006 832.01      3.52   4.522E+006                           1. 325 E+006             2 .102E+006 Bi - 2 1 2               39. 86    1. 06  1.150E+007        2 . 2 4E+ 00 6   -4. 2 72E+006              5.545E+006 727.33      6.67   2 .244E+006                          5.526E+005               1. 044E+006 785.37      1.10   1.237E+007                         - 1.136E+007               5.691E+006 1 62 0.50     1. 4 7 9.303E+006                         -9.319E+005                4.104E+006
+           Pb-2 1 2               1 15. 1 8   0.60   3.603E+007        2 .36E+005         6.786E+006               1.765E+007 23 8.63*  43.60    2.356E+005                           4. 2 88E+005             1.114E+005 300.09      3.30   4.616E+006                         -9 .037£+006               2 . 212E+006 Pb2 12-XR                74.82   10.28    2 .437E+006       l.42E+006          2 .432E+004              1.197E+006 77.11   17.10    1. 42 3E+006                       -1.428E+005                6.989E+005 87.35     3 .97  5.951E+006                           5.863E+006               2 .921E+006 89.78     1. 46  1. 57 5E+007                       -7. 92 1E+006              7.728E+006
+           Bi- 214                609.32*   45.49    2 .797E+005       2 .80E+005         l.173E+006               1.294E+005 768.36      4.89   3 . 2 18E+006                        5.342E+005               1. 499E+006 806.18      1. 2 6 1. 2 49E+007                       - 1. 58 4E+005             5 .807E+006 934.06      3.11   5.051E+006                           9.172E+005               2 . 33 4E+006 1120. 2 9*  14.92    5 . 2 73E+005                        1. 044E+006              2 .198E+005 1155.21       1. 63  1.010E+007                         -2 .051E+004               4.642E+006 1238.12*      5.83   2 . 3 46E+006                        l.555E+005               1 .055E+006 128 0 .98     1. 43  1 .017E+007                          5.817E+006               4.599E+006 1377.67       3.99   4. 2 38E+006                         3 . 2 74E+006            1. 93 6E+006 1385.31       0.79   1.862E+007                         -1. 12 8E+007              8. 3 86E+006 1401. 5 2     1. 33  1.135E+007                           2 .094E+006              5.124E+006 1407.99       2.39   6.613E+006                         -l.869E+006                2.998E+006 1509. 2 1     2.13   6.812E+006                           4.349E+006               3.044E+006 1661. 2 7     1. 05  1 .047E+007                          1.403E+006               4.453E+006

[323]

lC.L.LUe t*JLJl"i I"\t:: .f:JU L L U/ .l.V/ L V.l.U ',I. VL * .l. I r 1*1 r a~c:: u Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve l Name (keV) ( ~:) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM )

+       Bi-2 14                    17 29 .59    2 .88   4. 33 1E+006    2 .80E+005         1.096E+006 1.874E+006 1764.49    15.30     1. 39 1E+006                       1. 22 0E+006 6.401E+005 1847.43      2 .03   6.382E+006                         4.442E+006 2 .762E+006
   >                               2118.51      1. 1 6  O.OOOE+OOO                         O.OOOE+OOO O.OOOE+OOO
+        Pb-214                      2 41.99*   7.25    1.417E+006      3.24E+005          2 .579E+006 6.701E+005 2 95. 22 18.42     9. 2 77E+005                      7 .12 9E+005 4.468E+005 351.93*  35.60     3. 2 40E+005                       6.985E+005 1. 522E+005 785.96     1. 06  1.246E+007                        -1. 748E+007 5.718E+006 Pb214-XR                       74.8 2   5.80    4.319E+006      2 .51E+006        4.311E+004 2 .122E+006 77.11    9.70   2 .509E+006                       -2 .517E+005 1 .232E+006 87.35    2 .24  1.055E+007                         1.039E+007 5.176E+006 89.78     0.82   2 .805E+007                      -1.410E+007 1.376E+007
+       Ra- 22 6                    186. 2 1*   3 .64  3.401E+006       3 .40E+006        6.956E+005 1.634E+006 Ac- 22 8                    129.07      2 .4 2 8.531E+006       7.82E+005         4.025E+006 4.175E+006 209.25      3.89   4.472E+006                       - l.110E+006 2 .169E+006 270.24      3.46   4.727E+006                         2 .050E+006 2 . 27 7E+006 328.00      2 .95  5.324E+006                         4.094E+006 2 .549E+006 338.32    11. 2 7  l.466E+006                         1.573E+006 7.028E+00 5 409.46      1. 92  7.971E+006                         3 .093E+006 3 .787E+006 463.00      4.40   3.596E+006                         1.164E+006 1.705E+006 794.95      4.25   3 .799E+006                      -3 .376E+006 1. 771E+006 911. 2 0  2 5.80   7.816E+005                         7.619E+005 3 .680E+005 964.77      4.99   3 . 3 99E+006                      2 .436E+006 1.578E+006 968.97    15.80    l.110E+006                         6.897E+005 5.167E+005 1 588.20      3. 22  4.384E+006                       -1. 614E+006 1. 945E+006 Pa -2 31                      2 7.36* 10. 3 0  7.140E+005       7 . 14E+005       8.418E+005 3 .359E+005 283.69      1. 70  1.010E+007                         2 .697E+006 4.869E+006 300.07      2.47   6.167E+006                       -1. 2 07E+007 2 .955E+006 302.65     2. 2 0  6.846E+006                       -1.904E+005 3 . 2 78E+006 330.06     1. 40   1.071E+007                         4.423E+006 5.115E+006 Th- 23 4                      92.38    2.13    1. 068E+007     1 .07E+007       -3 .455E+006 5.236E+006 92.8 0   2.10    1.079E+007                       -9. 32 6E+005 5.293E+006 112.81     0.21    1.047E+008                         8.135E+007 5.132E+007

+ U-23 5 143.76 10.96 1.715E+006 2 .16E+00 5 - 1.059E+006 8.369E+005 163.33 5.08 3 .653E+006 2 . 2 09E+006 1. 781E+006 185.71* 57. 2 0 2 .164E+005 4.426E+004 1.040E+005 202.11 1. 08 1.610E+007 1.598E+007 7.817E+006 2 05.31 5.01 3 .501E+00 6 -8.994E+005 1. 699E+006 + Arn-241 59.54* 35.90 4. 232E+ 00 5 4. 23 E+005 4.445E+004 2 .055E+005

      +        Nuclide identified during the nuclide identification
      * = Energy line found in the spectrum
      > = Calculated MDA is zero due to zero counts in the region, or the region is outside th e spectrum, or MDA has not been calculated
      @ = Half-life too short to b e able to perform the decay correction

[324]

'***         GA MM A       S P E C T R U M            A N A L Y S I S           *****
' **************~ * ********** * *******************************************~
.lename: 545 2 iport Generated On                    8/10/ 2 016        3:36:03 PM tmple  Title                          B306100BFRWC0l0GD tmple  Description                    STE. WALL NUMB 10 SHOT tmple  Identification                 10 1mple   Type tmple   Geometry iak Locate Threshold                    3. 00 iak Locate Range (in channels )             85 -     8192 iak Area Range (in channels)                85 -     8 1 92 ientification Energy Tolerance            10.000 keV tmple Siz e                             l.OOOE+OOO SQM tmple Taken On

quisition Started 8/10/ 2 016 3:26:01 PM

.ve Time 600.0 second s ial Time 601.4 seconds iad Time 0 . 23 9a Energy Calibration Used Done On 1 /13/ 2 015 Efficiency Calibration Used Done On 8/9/2016 Efficiency ID UNNELSTS 1 METER DATA-VALIDATED DATE/ .. i-1'1 TIME os*10

                                                           .a ,~4

[325]

                                           \.JI ..J.. v / ~ '\.J ..J.. \.J P E A K        A N A L Y S I S                            R E P O R T               *****

Detector Name: 5452 Sample

Title:

B306100BFRWC010GD Peak Analysis Performed on: 8/10/~016 3:36:03 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area Uncert. Counts 1 1 13- 121 116. 2 8 28.66 0.92 1.89E+002 54.52 2 .06E+002 2 2 84- 308 300.86 74.87 0.70 3.04E+002 126.41 8.94E+002 3 391- 399 395.08 98.45 0.38 -6.56E+000 48.17 2 .74E+002 4 945- 96 1 955.07 238.62 0.90 9.14E+001 54.01 2 . 0 3E+002 5 1175- 118 7 1180.53 2 95.05 0.57 7.36E+001 34.54 8.54E+001 6 1349- 1358 1 353 .09 338.23 0.91 2 .70E+001 22.31 4.30E+001 7 1401- 1417 1 407.50 351. 85 0.77 1.49E+002 39.57 7.65E+001 8 2 036- 2 051 2 042.90 510.8 3 1. 70 4.43E+001 26.50 4.37E+001 9 2 326- 2 34 0 2332 .1 3 583.19 1. 3 0 6.33E+001 25.39 3.38E+001 10 2 427- 2 44 2 2 435.7 3 609.11 1. 74 1.50E+002 31. 55 3.30E+001 11 2 638- 2 65 1 2 645.15 661. 50 1. 2 9 6.48E+001 2 1. 69 1. 92E+001 12 3635- 3649 3 64 2 .85 911.03 0.44 4.73E+001 2 0.70 2 .07E+001 13 3869- 388 0 3 874.19 968.88 1. 2 5 1.60E+001 13.61 1. 2 0E+001 14 447 3- 4486 4478.75 1120.03 0.43 3 .99E+001 15.86 8.13E+OOO 15 5830- 5852 5841. 72 1460.70 1. 66 3.40E+002 41. 86 2 .54E+001 16 7050- 70 64 7057.11 1764.35 0.50 3.80E+001 1 3.28 1.99E+OOO First peak in a multiplet region Other peak in a multiplet region

= Fitted singlet

• rors quoted at 2 .000 sigma

[326]

1~erierence ~orrecLeu ttcL~V~LY ~epuLL 0 / l. U / L Ul.U ..J ; ..J u . u J r 1*l '********** * *********** i ******************** * ************************* * * ' *** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** '***********************+*********************************************** Sample

Title:

B306100BFRWC010GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( ii ) (pCi/SQM ) Uncertainty K-40 1. 000 1460. 82

• 10.66 1. 77571E+007 2 .67754E+006 Sr- 85 0.984 514.01* 96.00 1.47 2 93E+005 9.03670E+004 Ba- 13 3 0. 32 1 79.61* 2 .65 1. 84460E+007 8.53845E+006

81. 00 32 .9 0 2 76.40 7.16 302.85* 18. 3 4 9.3 1 685E+005 4.62182E+005 356.01* 62 .05 6.16446E+005 l.91583E+005 383.85 8.94 Cs-137 1.000 661. 66* 85.10 2 .80004E+0 0 5 9 . 96089E+004 Tl-208 1. 000 58 3 .19* 85.00 2 .56094E+0 0 5 1. 07 32 3E+005 Pb-2 1 2 0.974 115.18 0.60 23 8.63* 43.60 4. 2 9497E+005 2 .63121E+005 30 0 .09* 3 . 30 5.17791E+006 2 .57063E+006 Bi -2 14 0.534 609. 32

• 45.49 l.16145E+006 2 .81336E+005 768.36 4.89 806.18 1. 2 6 934. 0 6 3 . 11 11 2 0. 2 9* 14.92 1. 2 9266E+ 0 06 5.24361E+0 0 5 1155. 2 1 1. 63 1238. 1 2 5.83 1280.98 1. 43 1 3 77.67 3.99 1 3 85.3 1 0.79 1401.52 1. 33 1407.99 2 .39 1 509.21 2 .13 1661.27 1. 05 17 2 9.59 2 .88 1764.49* 15. 3 0 1 .55877E+006 5.58771E+005 1847.43 2.03 2118.51 1.16 Pb-2 14 0 .977 2 4 1. 99* 7.25 2 . 5 8 2 55E+006 1.58107E+006 295. 2 2* 18.42 9. 2 7639E+005 4.60004E+005 351.93* 35.60 1. 0 7 445E+006 3.33952E+005 785.96 1. 06 Ac-228 0 . 3 51 129.07 2 .42 209. 2 5 3.89 270. 2 4 3.46 32 8.00 2.95 338.32* 1 1. 27 6.02499£+0 0 5 5.07809E+005 409.46 1. 92

[327]

re.er I erenc..:e ~ULLeC..:Leu 1-iC..: L .L '.' .L Ly J:\ei-)UL L 0/ .LV / L. V.L O ..J; ..JO; V..J r 1*i rayc:: '-f Nuclide Id Energy Yield Activity Activity Name Confidence ( ke\T) ( ~; ) (pCi/SQM ) Uncertainty Ac- 22 8 0.351 463.00 4.40 794.95 4. 2 5 91 1. 2 0* 25.80 7.97364E+005 3.55740E+005 964.77 4.99 968. 97 ,~ 15.80 4.55019E+005 3.89145E+005 1588. 2 0 3 . 22 Th - 23 1 0.944 2 5.64* 14.10 2 .15010E+006 8.04152E+005 84.2 1 1* 6.60 7.40635E+006 3.53287E+006 89.95* 1. 00 -1.05435E+006 7.74874E+006

        * = Energy line found in the spectrum.
        @ = Energy line not used for Weighted Mean Activity Energy Tolerance :                    10.000 keV Nuclide confidence index threshold =                              0.3 0 Errors quoted at 2 .000 sigma

[328]

L"-'-'..L. ..L.'-'..L.'-'J.J..._... _ _ _ _.__.__..._,.__,....... ..,..,_._..._ v ...._._ .J ..,.,.._..t""'_.._._ '**** +************************* * **********~***************************** ' *** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 1. 775713E+007 2.677545E+006 Sr-85 0.984 1. 47 29 29E+005 9.036700E+004 Ba-133 0. 32 1 3 .859891E+005 8.084119E+005 Cs-137 1. 000 2 .800035E+005 9.960890E+004 Tl-208 1. 000 2 .560940E+005 1.0732 2 7E+005 X Bi-211 0.999 Pb-212 0.974 3.613463E+005 3.499975E+005 Bi-214 0.534 1. 2 51300E+006 2.266063E+005 Pb-214 0.977 4. 2 77001E+005 l.248575E+006 Ac-228 0.351 6. 332 8 3 7E+005 2 . 3323 13E+005 X Ac228-XR 0.366 X Pa-231 0.674 Th-231 0.944 2 .388086E+006 7. 3 81714E+005

                ? = Nuclide                         is part of an undetermined solution X       =       Nuclide rejected by the interference analysi s
                @               Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at                                       2 .000 sigma
  **********                              U N I D E N T I F I E D                                                 P E A K S        **********

Peak Locate Performed on: 8/10/ 2 0 1 6 3:36:03 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide All peaks were identified. [329]

ic.1..1.ue 1v1uh !'l.ef_.)VL L 0 / .l.V/ L V.l.U rayc: u '*** N U C L I D E M DA R E P O R T ***** Detector Name : 545 2 Sample Geometry: Sample

Title:

B306100BFRWC010GD Nuclide Library Used: C:\GENIE2K\CAMFILES\ Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( s-, ) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM)

+         K-40                1460.8 2

• 10.66 1.849E+006 1. 85E+006 1. 776E+007 8.537E+005 Cr-51 32 0.08 9.91 1. 52 7E+006 1.53E+006 -1.680E+006 7.302E+005 Mn-54 834.85 99.98 1.692E+005 1. 69E+005 -6.292E+004 7.899E+004 Co-58 810.76 99.45 1. 579E+005 1.58E+005 3.243E+004 7. 3 40E+004 Co-60 117 3 . 23 99.85 1.537E+005 1.44E+005 1.202E+005 7.016E+004 1 332 .49 99.98 1.443E+005 3.710E+004 6.500E+004 Nb-94 702.65 99.81 1.724E+005 1. 4 7E+005 1. 670E+004 8.106E+004 871. 09 99.89 1.468E+005 -9.973E+004 6.768E+004 Sn-1 13 2 55.13 2 .11 8.426E+006 2 .53E+005 3 . 2 46E+005 4.077E+006 391. 70 64. 97 2 .533E+005 4.373E+004 1. 209E+005 Cs-134 475. 3 6 1. 48 1.119E+007 1. 97E+005 -6 .871E+006 5.312E+006 563. 2 5 8.34 1.794E+006 -4. 92 7E+005 8.421E+005 569.33 15.37 9.788E+005 -2 .091E+005 4.595E+005 604.72 97.62 2 .520E+005 -1.112E+005 1. 2 11E+005 795.86 85.46 1.971E+005 8. 2 03E+004 9. 2 15E+004 801.95 8.69 2 .048E+006 8.821E+005 9.606E+005 1038.61 0.99 1. 562E+007 -1 . 1 74E+007 7.175E+006 1 167.97 1. 79 8.451E+006 6.198E+006 3 .852E+006 1365. 1 9 3.0 2 4. 2 65E+006 1. 2 87E+006 1.892E+006

+ Cs-137 661.66* 85.1 0 1.151E+005 1.15E+005 2 .800E+005 5.169E+004 Eu-15 2 121. 7 8 28.67 7.396E+005 5.83E+005 5.561E+005 3 .622E+005 244.70 7.61 2 . 52 9E+006 5.640E+005 1. 2 28E+00 6 295.94 0.45 4. 2 89E+007 1.1 22 E+007 2 .074E+007 344.28 26.60 5.832E+005 - 3 .113E+005 2 .787E+005 367.79 0.86 1. 855E+007 1 . 1 02E+007 8.861E+006 411.12 2.24 7. 2 68E+006 1.478E+006 3.463E+006 443.96 2.83 5.748E+006 -2 .505E+006 2 .733E+006 488.68 0.42 3.819E+007 -2 .123E+007 1.809E+007 563.99 0.49 3.137E+007 2 .239E+007 1. 4 7 5E+007 586. 2 6 0.46 4.406E+007 2 .177E+007 2 .102E+007 678. 62 0.47 3 .266E+007 - 9.456E+006 1. 526E+007 688.67 0.86 1. 892E+007 -2 .071E+006 8.867E+006 719.35 0. 2 8 5.693E+007 - 5.671E+006 2 .660E+007 778.90 12 .96 1.159E+006 - 1.050E+006 5. 3 75E+005 810.45 0.32 4.968E+007 1.713E+007 2 . 3 12E+007 867.37 4.26 3 .535E+006 - 1.559E+006 1. 63 3E+006 919.33 0.43 3 .568E+007 -1. 987E+007 1. 646E+007 964.08 14.65 1. 2 91E+006 1 .251E+005 6 .039E+005 1085.87 10.24 1. 656E+006 -6.394E+005 7.650E+005 1089.74 1. 73 9.448E+006 -6.850E+006 4.351E+006 1112.07 13.69 1. 2 53E+006 -1.241E+006 5.791E+005 1 2 1 2 .95 1. 4 3 1. 31 4E+007 1. 794E+006 6.092E+006 [330]

lC.LlOe MLJH. .r1.epoL L 0/ 1.U/ L UJ.0 ..) : ..) 0 : U ':I .t't*1 rctye Nuclide Energy Yield Line MDA Nucli de MDA Activity Dec. Level Name (keV) (i ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) Eu-15 2 1249.94 0.19 9.173E+007 5.83E+005 5. 2 00E+007 4.221E+007 1299.14 1. 63 8.765E+006 -5.166E+006 3 .949E+006 1408.01 2 1. 07 6. 2 20E+00 5 3.957E+005 2. 760E+005 1457.64 0.5 0 1 .044E+008 3.930E+008 5.072E+007 1528.10 0.28 3.961E+007 2.643E+007 1. 706E+007 Eu - 154 123.07 40.40 5.182E+005 4.82E+005 - 1. 810E+005 2 .537E+005 247.93 6.89 2 .590E+006 - 1. 903E+006 1. 25 4E+006 591.76 4.95 3 .032E+006 1. 019E+006 1.421E+006 692 .4 2 1. 78 9.338E+006 7.691E+006 4.382E+006 723 . 3 0 2 0.06 8.609E+005 1. 462E+005 4.045E+005 756.80 4. 52 3 . 3 80E+006 -6.542E+005 1.572E+006 87 3 .18 12 .08 1. 2 28E+006 -9.662E+004 5.663E+005 996.29 10.48 1. 535E+006 -5.738E+005 7.085E+005 1004.76 18.01 9.542E+005 5.433E+005 4.427E+005 1274.4 3 3 4.80 4.821E+005 2 .003E+005 2 .210E+005 1596.48 1. 80 6.798E+006 -5.395E+006 2 .955E+006 Eu-155 45. 3 0 1. 31 l.330E+007 8.42E+005 3 .464E+006 6.485E+006 60.01 1. 22 l.659E+007 1 .493E+007 8.117E+006 86.55 30.70 8.4 2 3E+005 5.609E+005 4.140E+005 105.31 2 1.10 1. 0 33E+006 -2. 3 16E+005 5.060E+005

+      Tl-208             583.19*   85.00    1. 428E+005      1. 43E+005      2.561E+005                 6.592E+004 Bi-21 1            351. 07*  13.02    1. 068E+006      1.07E+006       2.938E+006                 5.072E+005 Pb-2 1 1           404.85      3 .78  4.408E+006       4.4 1E+006      l.598E+006                 2 .104E+006 427.09      1. 76  8.905E+006                     -7.010E+006                  4.231E+006 832.01      3.52   4.864E+006                     -3.584E+006                  2 .273E+006 Bi-212              39.86      1. 06  1.832E+007       2 .46E+006      l.022E+007                 8.954E+006 727.33      6.67   2 .459E+006                    -4.562E+004                  1 .151E+006 785.37      1.10   1.445E+007                       3 .791E+006                6.734E+006 1 62 0.5 0    1. 47  7.618E+006                     - 1.349E+006                 3.261E+006 115.18      0.60   3.625E+007       4.03E+005       6.890E+006                 1. 776E+007
+      Pb-212 1.952E+005 23 8.63*  43.60    4.032E+005                       4.295E+005 300.09*     3.30   3.660E+006                       5.178E+006                 1.735E+006 Pb212-XR            74.8 2   10.28    2 .572E+006      1.44E+006       2 .543E+005                1. 265E+006 77.11    17.10    l.442E+006                     -1. 569E+005                 7.081E+005 87.35      3.97   6. 5 44E+006                     9.848E+006                 3 .217E+006 89.78      1. 46  1.704E+007                       3.248E+005                 8.372E+006 Bi- 214            609.32*   45.49    2 .742E+005      2. 74E+005      l.161E+006                 1. 266E+005
+                                                                                                        1. 689E+006 768.36      4.89   3.599E+006                       3.290E+006 806.18      1. 2 6 1. 2 96E+007                   - 3.755E+006                 6 .044E+006 934.06      3. 11  5.323E+006                       1. 624E+006                2 .470E+006 1120.29*    14.92    5.990E+005                       1. 293E+006                2 .557E+005 1155.21       1. 63  l .010E+007                      3.622E+006                 4.642E+006 1238.12       5.83   3 .4 3 1E+006                  -2 .961E+005                 1.597E+006 1280.98       1. 43  l .077E+007                    -5 .408E+006                 4.896E+006 1 377.67      3.99   4.082E+006                       2 .112E+006                1. 858E+0 0 6 1385. 3 1     0.79   1. 5 66E+007                   -3 . 3 16E+007               6.908E+006 1401. 52      1. 33  1.062E+007                        4.601E+006                4.757E+006 1407.99       2 .39  5.474E+006                       3.483E+006                 2 .429E+006 1509. 2 1     2 .13  6.812E+006                       1. 82 0E+006               3.044E+006 1661.27       1. 05  l. 2 30E+007                      4. 32 9E+005              5.371E+006

[331]

Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( ":: ) (pCi/SQM ) (pCi /S QM ) (pCi/SQM ) (pCi/SQM ) + Bi-214 17 29 .59 2 .88 4.950E+006 2 .74E+00 5 8.075E+005 2 .184E+006 1764.49* 15. 3 0 4.437E+005 1.559E+006 1.664E+005 1847.43 2 . 03 6.945E+006 5 .553E+005 3 . 043E+006 2 118.51 1.16 O.OOOE+OOO O.OOOE+OOO O.OOOE+OOO

 >                                                                                 1.174E+006

+ Pb- 2 14 2 41. 99* 7. 2 5 2 .424E+006 3 .91E+005 2 . 5 83E+006 2 95. 22

• 18.42 6.557E+005 9 .2 7 6E+005 3 .108E+005 3 51. 93* 35.60 3.905E+005 1.074E+006 1.855E+005 785.96 1. 06 1.525E+007 9. 1 37E+006 7.113E+006 Pb21 4-XR 74.82 5.80 4.559E+006 2 .54E+00 6 4.507E+005 2 . 2 42E+006 77.11 9.70 2.541E+006 -2 .765E+005 1. 2 48E+006 87.35 2 . 24 1.160E+007 1.745E+007 5.702E+006 89.78 0. 82 3.034E+007 5.783E+005 1.491E+007 Ra-226 1 86. 2 1 3 . 64 5.244E+006 5.24E+006 2 .814E+006 2 .555E+006

+ Ac- 22 8 129.07 2 .42 8.755E+006 4.75E+005 9.376E+006 4. 2 87E+006 209.25 3 .89 4.779E+006 -1.666E+006 2 . 32 3E+006 2 70. 2 4 3 .46 5.026E+006 4.819E+006 2.427E+006 328.00 2 .95 5.835E+006 -3 .410E+004 2 .804E+006 338. 32 1* 11. 2 7 7.856E+005 6.025E+005 3 . 62 6E+005 4 0 9.46 1. 92 8.449E+006 1 . 854E+006 4.0 2 6E+006 463.00 4.40 3.596E+006 -1. 743E+006 1.705E+006 794.95 4. 2 5 4.040E+006 4.129E+006 1. 891E+006 911 . 2 0* 25.80 4.746E+005 7.974E+005 2 .145E+005 964.77 4.99 3.741E+006 5.140E+005 1. 749E+006 968.97* 15.80 5. 92 1E+005 4.550E+005 2 .575E+005 1 588.20 3 . 22 5.143E+006 - 9.411E+005 2 . 3 25E+006 Pa - 23 1 2 7.36* 10.30 1. 2 51E+006 1. 2 5E+006 2 .943E+006 6.0.46E+005 2 8 3 .69 1. 70 l.018E+007 6.420E+006 4.909E+006 3 00.07* 2 .47 4.890E+006 6.918E+006 2 .318E+006 3 02 .65 2 . 20 7. 392 E+006 1.2 1 0E+006 3 .551E+006 330.06* 1. 40 6.324E+006 4.850E+006 2.919E+006 Th- 23 4 92 . 38 2. 1 3 l.129E+007 1 . 13E+00 7 6.171E+006 5.545E+006 92.8 0 2 .10 1 .136E+007 4.575E+006 5.576E+006 112.8 1 0. 2 1 1. 051E+008 2 .689E+007 5.153E+007 U- 235 1 43.76 10.96 1. 845E+006 3 .34E+005 5. 23 5E+005 9.020E+005 163.33 5.08 3 .861E+006 l. 52 8E+006 1. 885E+006 185.71 57. 2 0 3 .342E+005 l. 2 62E+005 1. 629E+005 202.11 1. 08 l .797E+007 9.839E+005 8.752E+006 205.31 5.01 3 .821E+006 -7.178E+005 1. 860E+006 Am-241 59.54 35.90 5.559E+005 5.56E+005 l.964E+00 5 2 .719E+005

   + = Nucl ide identified during the nuclide identification

• Energy line found in the spectrum

   > =    Calculated    MDA is zero due to zero counts in the region, or the region i s outside the spectrum, or MDA has not been calculated
   @ = Half-life too short to be able to perform the decay correction

[332]}}