Text

Revised Final Status Survey (FSS) Report - Phase 2, RR 05100, Part 8 of 9
	ML19295G764
Person / Time
Site:	Zion File:ZionSolutions icon.png
Issue date:	02/28/2018
From:	; ZionSolutions
To:	; Office of Nuclear Material Safety and Safeguards
Shared Package
ML19295G627	List: ML19295G587; ML19295G611; ML19295G612; ML19295G617; ML19295G621; ML19295G625; ML19295G670; ML19295G674; ML19295G699; ML19295G702; ML19295G705; ML19295G726; ML19295G728; ML19295G734; ML19295G738; ML19295G742; ML19295G747; ML19295G751; ML19295G758; ML19295G764; ML19295G768; ML19295G788; ML19295G791; ML19295G795; ML19295G816; ML19295G818; ML19295G820; ML19295G822; ML19295G826; ML19295G828; ML19295G831; ML19295G837; ML19295G841; ML19295G843; ML19295G846; ML19295G850; ML19295G853; ML19295G855; ML19295G857; ML19295G859; ML19295G863; ML19295G866; ML19295G870; ZS-2019-0090, Revised Final Status Survey (FSS) Report - Phase 2, Release Record - Waste Water Treatment Facility Survey Unit 09100;
References
	ZS-2019-0090
	Download: ML19295G764 (385)
	v • d • e

3/13/2018 12:34:44AM Page I of6 Analysis Report for 12-Mar-18-10026 B105100A-FSWC-101CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Mar-18-10026 Sample Description : B105100A-FSWC-101CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.461 E+02 grams Facility : Default Sample Taken On : 3/9/2018 9:35:00AM Acquisition Started : 3/13/2018 12:14:36AM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.6 seconds Dead Time : 0.13 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24263 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 12:34:40AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

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3/13/2018 12:34:44AM Page 2 of6 Analysis Report for 12-Mar-18-10026 B105100A-FSWC-101CV 0.0" - 0.5" o.o*

Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 609.55 1 213 - 122 1 1218.67 2 .67E+Ol 15.41 3.06E+Ol 1. 02 2 661.88 1 317 - 1329 1323.30 5.80E+Ol 17. 78 1 . OE+Ol 1. 33 3 1460.93 2916 - 2928 2921.92 6.47E+Ol 17.16 6.57E+OO 1. 82 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Libr::iry\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460.82

10.66 5.41E+OO 1. 51E+OO Cs-137 0.99 661.66

85. 10 3.48E-Ol 1.15E-01 Bi-214 0.99 609. 32

45.49 2 .83E-01 1. 67E-01 768.36 4.89 806.18 1.26 934.06 3 .11 11 2 0.29 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377 . 67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2 .13 1661. 27 1. 05

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3/13/2018 12:34:44AM Page3 of6 Analysis Report for 12-Mar-18-10026 8105100A-FSWC-101CV 0.0" - 0.5" 0.0" Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1729.59 2 .88 1764.49 15.30 1847.43 2 .03 2 118. 51 1.16

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.998 5.41E+OO 1.51E+OO Cs-137 0.992 3.48E-01 1.15E-01 Bi-214 0.997 2.83E-01 1.67E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

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3/13/2018 12:34:44AM Page4 of6 Analysis Report for 12-Mar-18-10026 8105100A-FSWC-101CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 12:34:40AM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (ke V) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCi!grams) (pCi/grams)

(keV)

An Pk 511. 00 100.00 2 .41E-0 1 2 .07E-01 2 .07E-01 BE-7 477.60 10.44 3.62E-01 1.18E+OO 1.18E+OO

+ K-40 1460.8 2

10.6 6 5.41E+OO 1. 08E+OO 1.08E+OO Co-6 0 1173.23 99.85 9.33E-02 1.61E-01 1.88E-01 1332.49 99.98 9.91E-02 1. 61E-01 Nb-94 702.65 99.81 2 .40E-03 1.16E-01 1.30E-01 871.09 99.89 -2 .0lE-02 1.16E-01 Ag-108m 79 .13 6.60 1 .27E-01 1 .30E - 01 2 .17E+OO 433.94 90.50 5.25E-02 1.30E-01 614. 2 8 89.80 - 1.91E-01 1.93E-01 722 . 94 90.80 -2 .62E-02 1.58E-01 Sb- 12 5 176.31 6.84 5.24E-01 3 . 1 9E-0 1 1. 60E+OO 380.45 1. 52 9.31E-01 7.63E+00 427.87 2 9.60 -1. OlE-01 3 .19E-01 463.36 10.49 3 .22E-01 1.15E+OO 600.60 17.65 -3 . 59E-01 6.89E-01 606.71 4.98 1.94E+OO 3.73E+OO 635.95 11. 22 -2.35E-01 1. llE+OO 671.44 1. 79 6.96E-01 6.87E+OO

[2514]

3/13/2018 12:34:44AM Page 5 of6 Analysis Report for 12-Mar-18-10026 B1051OOA-FSWC-101 CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCUgrams) (pCUgrams) (pCilgrams)

(keV)

Ba-133 79.61 2.65 -7.71E-01 2. 15E-01 5.05E+OO

81. 00 32 .90 1.24E-02 3 .79E-01 276.40 7.16 1. 26E-01 1. 34E+OO 302.85 18.34 -2 .25E-01 5 . 02E-01 356.01 62.05 1.14E-01 2 .15E-01 383.85 8.94 -3 .38E-01 1. 2 6E+OO Cs-1 34 475.36 1. 48 1.66E+OO 1.55E-01 8.19E+OO 563. 2 5 8.34 8.70E-02 1.42E+OO 569.33 15.37 1. 2 0E-01 7.45E-01 604. 72 97.6 2 -2 .78E-02 1.64E-01 795.86 85.46 -2 .79E-0 2 1.55E-01 801.95 8.69 1.94E-01 1.45E+00 1038.61 0.99 -4.14E+OO 1. 22E+Ol 1167.97 1. 79 -1 . 03E+Ol 8. 2 3E+OO 1365.19 3.0 2 -3. 71E+OO 2 .15E+OO

+ Cs- 137 661.66

85.10 3. 48E-01 1. llE-01 1. llE-01 Eu-15 2 121.78 2 8.67 2 .07E-01 3.46E-01 3.46E-01 244.70 7.61 1.52E-01 1.45E+OO 295.94 0.45 3 .93E+OO 2 .47E+Ol 344.28 2 6.60 -2 .15E-01 3 .80E-01 367.79 0.86 -6.15E+OO 1.09E+Ol 411.12 2 . 2 4 -7.66E-01 4.63E+OO 443. 96 2 .83 -5.58E-01 3.63E+OO 488 . 68 0 . 42 -1 . 14E+Ol 2 .76E+Ol 563.99 0.49 -3 .84E-01 2 .41E+Ol 586.26 0.46 1.88E+Ol 3.15E+Ol 678.62 0.47 -9.46E+OO 2 .56E+Ol 688.67 0.86 -4.73E+OO 1.39E+Ol 719.35 0. 2 8 l.67E+Ol 4 . 83E+Ol 778.90 12. 96 4 . 92E-01 9.49E-01 810.45 0.32 -3.05E+OO 3 .82E+Ol 867.37 4.26 1.20E+OO 3. llE+OO 919.33 0.43 -4.93E+OO 2 .83E+Ol 964. 08 14.65 3.46E-02 1. 08E+OO 1085.87 10. 2 4 -7.65E-02 1. 32E+OO 1089.74 1. 73 - 5.57E+OO 6.84E+00 1112. 07 13.69 -3.02E-01 7.79E-01 1 212.95 1. 43 -5.12E+OO 7. 3 7E+OO 1 2 49.94 0.19 2 .09E+OO 6.87E+Ol 1 2 99.14 1. 63 2 .79E+OO l.04E+Ol 1408.01 21.07 -1.54E-01 7.08E-01 1457.64 0 . 50 3.43E+OO 7.71E+Ol 1528.10 0. 2 8 -1.07E+Ol 3.67E+Ol Eu-154 123 .07 40.40 1. 2 6E-01 2 .40E-01 2 .40E-01 247.93 6.89 - 9.58E-Ol l.47E+OO 591.76 4.95 9.90E-01 2 . 3 8E+OO 692.42 1. 78 7.51E-01 6.73E+OO 723. 30 20.06 6.27E-01 7.91E-01 756.80 4.52 -$.26E-02 2 .51E+OO 87 3 .18 12. 08 -l.37E-01 1 . 00E+OO 996.29 10 . 48 -9.09E-01 1.17E+OO

[2515]

3/13/2018 12:34:44AM Page 6 of6 Analysis Report for 12-Mar-18-10026 B 1051OOA-FSWC-101 CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) , Activity NuclideMDA LineMDA Name (pCilgrams) (pCl/grams) (pCi!grams)

(keV)

Eu-154 1004.76 18.01 - 2 .74E-01 2 .40E-01 6.55E-01 1274.43 34.80 1.57E-01 5.07E-01 1596.48 1. 80 -8.93E+OO 5.15E+OO Eu-155 45.30 1. 3 1 6.32E+OO 3.30E-01 2 .14E+Ol 60.01 1. 22 5.36E+OO 2 . 2 7E+Ol 86.55 30.70 -8.79E-0 2 3.30E-01 105.31 2 1.10 2.0lE-0 2 4.34E-Ol Ra-226 186.21 3.6 4 2.29E+OO 2.98E+OO 2.98E+OO Pa-231 2 7.36 10 .3 0 1. 02E+OO 2 .36E+OO 2 .36E+OO 2 83.69 1. 70 -1.93E-01 4.90E+OO 300.07 2 .47 - 2 .40E+OO 3 .96E+OO 302.65 2 . 20 -1.87E+OO 4.18E+OO 330.06 1. 40 2. 46E+OO 8. llE+OO U- 235 143.76 10. 96 1. 2 4E-01 1.91E-Ol 8.17E-01 163. 33 5.08 - 2 .13E-01 2 .02E+OO 185.71 57.20 1.76E-01 1. 91E-01 2 02 .11 1. OB 1.70E+OO 1.00E+Ol 2 05.31 5 .01 9.81E-01 2 .27E+OO Am-241 59.54 35 .90 1.94E-01 8.02E-01 8 . 02E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

'? = CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level

[2516]

0000024263.CNF Live Time :1200.000 sec Real Time :1201.550 sec 60 start: 1: O.l(kev)

Stop : 4096: 2047. l(kev)

Acq. start :rue Mar 13 00:14 :36 2018 55 50 45 40 35

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500 1000 1500 2000 2500 3000 3500 4000 Channel

~

ROI Type: 1

3/13/2018 1:20:17AM Page 1 of6

~~Apex-Gamma Analysis Report for 12-Mar-18-10027 B105100A-FSWC-101CV 0.0" - 0.5" 0.5

GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Mar-18-10027 Sample Description : 8105100A-FSWC-101CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.461 E+02 grams Facility : Default Sample Taken On : 3/9/2018 9:35:00AM Acquisition Started : 3/13/2018 1:00:10AM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.5 seconds Dead Time : 0.12 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 -4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24265 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 1 :20:13AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

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3/13/2018 1:20:17AM Page 2 of6 Analysis Report for 12-Mar-18-10027 B 1051OOA-FSWC-101 CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.82 473 - 482 477.81 4.SOE+Ol 28.17 1. 34E+02 0.89 2 1460.90 2915 - 2929 2921.86 5.64E+Ol 16.32 7.12E+OO 1.27 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.8 2

10.66 4. 71E+OO 1. 42E+OO Pb-212 0.99 115 . 1 8 0.60 2 38.6 3 *k 43 .60 2. 49E-01 1. 61E-0 1 3 00.0 9 3 .30

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2519]

3/13/2018 1:20:17AM Page 3 of6 Analysis Report for 12-Mar-18-10027 B105100A-FSWC-101CV 0.0" -0.5" 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.999 4.71E+OO 1.42E+OO Pb-212 0.995 2.49E-01 1.61E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2520]

3/13/2018 1:20:17AM Page 4 of6 Analysis Report for 12-Mar-18-10027 B105100A-FSWC-101CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 1:20:13AM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCl/grams) (pCi/grams)

(keV)

An Pk 5 11. 00 100.00 2 .98E-01 2 .08E-01 2.08E-01 BE-7 477.60 10.44 1.16E-02 1.13E+OO 1.13E+OO

+ K-40 1460.82

10.66 4 . 71E+OO 1.14E+OO 1.14E+00 Co-60 1173.23 99.85 l.79E-03 1.49E- 01 1.76E-01 1332.49 99.98 -1.61E-0 2 l.49E-01 Nb-94 702.65 99.81 3 .48E-0 2 1.16E-01 l.18E-01 871.09 99.89 -2 .03E-0 2 1.16E-01 Ag-108m 79.13 6.60 3.56E-01 1.13E-01 2 .35E+OO 433.94 90.50 -2 .33E-02 l.13E-01 614.28 89.80 -9 .35E-02 1.69E-01 722. 94 90.80 -1.05E-02 1.39E-01 Sb-125 176.31 6.84 -2 .75E-01 3 .7'.2E-01 1. 32E+00 380.45 1. 52 -2 .18E+OO 6.45E+OO 427.87 2 9.60 1.18E-01 3 . 72E-01 463.36 10.49 1.04E-0 1 9.75E-01 600.60 17.65 -7.46E-02 6 . 75E-01 606.71 4.98 2 .37E+OO 3.56E+OO 635.95 11. 22 -3 .16E-01 1.15E+OO 671. 44 1. 79 -3 .89E+OO 6.73E+OO

[2521]

3/13/2018 1:20:17AM Page 5 of6 Analysis Report for 12-Mar-18-10027 8105100A-FSWC-101CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCUgrams) (pCi/grams) (pCi/grams)

(keV)

Ba-133 79.61 2 .65 5 .15E-01 2 .lOE-01 5.63E+OO

81. 00 32 .90 -2 .17E-01 3.86E-01 276.40 7.16 4.93E-01 1. 53E+OO 302.85 18.34 1. 96E-01 5.97E-01 356.01 62.05 -5.58E-02 2.lOE-01 383.85 8.94 - 4.47E-01 1.08E+OO Cs- 134 475.36 1. 48 - 1.82E+OO l.59E-01 7.46E+OO 563.25 8.34 -2 . 3 3E-01 1. 30E+OO 569.33 15.37 2 .06E-01 7.61E-01 604.72 97.6 2 9.25E-04 l.64E-01 795.86 85.46 2 .09E-02 1.59E-01 801.95 8.69 -3 .03E-01 1.53E+OO 10 3 8.61 0.99 3 .53E-01 1.38E+Ol 1167. 97 1. 79 -3 .13E+OO 1.00E+Ol 1365.19 3.0 2 -3 .73E-01 3 .13E+OO Cs-137 661.66 85.10 l.83E-01 2 . llE-01 2 . llE-01 Eu-1 52 121.78 28.67 7.31E-03 2 .93E-01 2 .93E-01 244.70 7.6 1 5.55E-01 1.48E+OO 295.94 0.45 2.95E+OO 2 .40E+Ol 344. 2 8 2 6.60 -l.08E-01 4.28E-Ol 367.79 0.86 -6. 2 3E+OO 1.17E+Ol 411.12 2 .24 9. 2 7E-01 4.98E+OO 443. 96 2 .83 9.79E-01 3 .69E+OO 488.68 0.42 -3.47E+OO 2 . 3 8E+Ol 563.99 0 . 49 -2.97E+OO 2 .16E+Ol 586. 2 6 0.46 1.95E+Ol 3 .31E+Ol 678. 62 0.47 5.53E-01 2 .69E+Ol 688.67 0.86 - 9.12E+OO 1. 24E+Ol 719. 35 0. 2 8 -7.79E+OO 4.18E+Ol 778.90 12.96 -4.43E-01 8.32E-01 810.45 0.32 2.97E+00 3. 71E+Ol 867.37 4.26 9.07E-01 2 .73E+OO 919.33 0.43 -9.53E-01 3 .23E+Ol 964.08 14.65 -6.46E-01 8.84E-01 1085.87 10. 2 4 - 5.0lE-01 1 .32E+OO 1089.74 1. 73 -1.50E+OO 8.39E+OO 111 2 . 07 13. 69 l.30E-0 1 1.00E+OO 1212 .95 1. 43 -2.89E+OO l.06E+Ol 1249.94 0.19 -7.31E+Ol 6. llE+Ol 1 299.14 1. 63 -5 .47E+OO 7.30E+OO 1 408.01 2 1. 07 -3 .0lE-01 5.58E-01 1 457.64 0.50 -6 .85E+OO 7.24E+Ol 1528.10 0. 2 8 -2 . 2 5E+OO 4.09E+Ol Eu-154 123.07 40 . 40 3.79E-03 2 .12E-01 2. 12E-01 247.93 6.89 -6.39E-01 1. 3 9E+OO 591.76 4.95 -4.17E-01 2 .16E+OO 692.42 1. 78 -2 . 08E+OO 6. 3 9E+OO 723. 30 20.06 3.47E-02 6.47E-01 756.80 4 . 52 4.29E-01 2 .25E+OO 873.18 1 2 .08 -2.95E-01 1. 04E+OO 996. 2 9 10.48 -7.65E-01 1.17E+OO

[2522]

3/13/2018 1:20:17AM Page6 of6 Analysis Report for 12-Mar-18-10027 8105100A-FSWC-101CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCl/grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 1.14E-01 2. 12E-01 6.84E-01 1274.4 3 3 4.80 9.lOE-02 4.48E-01 1596.48 1. 80 -1.73E+OO 5. 96E+OO Eu-155 45.30 1. 3 1 1.33E+Ol 3 .73E-01 2 .37E+Ol 60.01 1. 22 4.73E+OO 2 . 2 4E+O l 86 . 55 30.70 1. 2 9E-01 3 .73E-01 105.31 2 1.10 2 .92E-01 4.86E-01 Ra-226 186.21 3. 64 1.98E+OO 3.12E+OO 3.12E+OO Pa-231 2 7.36 10.30 2 . 72E-01 1. 85E+OO l.85E+OO 2 83.69 1. 70 1.08E+OO 5.70E+OO 300.07 2 .47 -3 .09E+OO 3.92E+OO 302.65 2 .20 l.63E+OO 4.97E+OO 330.06 1. 40 -l.45E+OO 7.73E+OO U-2 35 143.76 10. 96 5 . 96E-02 1.99E-01 8 . 41E-01 163.33 5.08 - 1 .41E-01 1 . 98E+OO 185.71 57. 2 0 1.59E-01 1 . 99E-01 2 02 .11 1. 08 3.86E+OO 9.80E+OO 2 05.31 5 . 01 -7.79E-01 2 .00E+OO Am- 2 41 59. 54 35.90 1.12E-01 7.78E-01 7.78E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2523]

0000024265.CNF Live Time :1200.000 sec Real Time :1201.500 sec Start: 1: O.l(kev) stop : 4096:2047.l(kev)

Acq. Start :Tue Mar 13 01:00:10 2018

[2524]

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/13/2018 1:22:49AM Page 1 of6

~§jff~pex-Gamma Analysis Report for 12-Mar-18-10029 8105100A-FSWC-101CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Mar-18-10029 Sample Description : 8105100A-FSWC-101CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 9.429E+01 grams Facility : Default Sample Taken On : 3/9/2018 12:40:00PM Acquisition Started : 3/13/2018 1:02:42AM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24267 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 1:22:45AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2525]

3/13/2018 1:22:49AM Page 2 of6 Analysis Report for 12-Mar-18-10029 B 105100A-FSWC-101 CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (keV) 1 2 38.76 951 - 960 954.62 3.55E+Ol 18. 2 5 4.09E+Ol 0.59 2 3 51.97 1402 - 1412 1 406.91 3.65E+Ol 15.07 1. 50E+Ol 0.34 3 1460.69 5834 - 5848 5840.71 5.lOE+Ol 16.15 1. OlE+Ol 0.42 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canbarra\Apex\Root\Default\Library\ZION UB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460. 82

10.66 7.45E+OO 2 .45E+OO Bi-211 0.87 351.07

13. 02 1.51E+OO 6.69E-01 Pb-212 0.99 11 5 .18 0.60 23 8.63

43.60 3 .28E-01 1.77E-01 300.09 3.30 Pb-214 1. 00 241. 99 7.25 2 95. 22 18.42 351.93

35.60 5 . 52E- 01 2 .45E-01 785. 96 1. 06

[2526]

3/13/2018 1:22:49AM Page 3 of6 Analysis Report for 12-Mar-18-10029 8105100A-FSWC-101CV 0.0" - 0.5" 0.5"

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.997 7.45E+OO 2 .45E+OO

? Bi-211 0.877 1. 51E+OO 6.69E-01 Pb-21 2 0.998 3.28E-01 1.77E-01

? Pb-214 1. 000 5.52E-01 2 .45E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2527]

3/13/2018 1:22:49AM Page 4 of6 Analysis Report for 12-Mar-18-10029 B105100A-FSWC-101CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 1:22:45AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a m!,Jltiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCi!grams) (pCl!grams)

(keV)

An Pk 511. 00 100.00 1. 36E-0 1 2.2 0E-01 : . 2 0E-01 BE-7 477.60 10.44 -3.56E-01 1 .51E+OO 1. 51E+OO

+ K-40 1460.82

10.66 7.45E+OO 2 . 2 9E+OO 2.2 9E+OO Co-60 11 73.23 99.85 2 .18E-02 2.17E-01 2.17E-01 1332.49 99.98 -6.30E-02 2.37E-01 Nb-94 70 2 .65 99.8 1 5.25E-0~ 1.93E-0 1 2.03E-01 871. 09 99.89 1. 07E-01 1.93E-01 Ag-108m 79.13 6.60 1.18E+OO 1.67E-01 3.lOE+OO 433.94 90.50 7.83E-02 l .67E-01 614. 2 8 89.80 -2.79E-01 2.25E-01

22 .94 90.80 5.17E-02 2 .56E-01 Sb-125 176.31 6.84 -7.66E-0 1 5.71E-01 1.25E+OO 380.45 1. 52 -1.15E+OO 8.58E+OO 427.87 2 9.60 -4.25E-02 5.71E-01 463.36 10.49 7.70E-Ol 1. 45E+OO 600.60 17.65 6.02E-01 9. 3 5E-0 1 606.71 4.98 4.83E-02 4. 3 7E+00 635.95 11. 22 -2 .59E-01 1.04E+OO 671.44 1. 79 6.79E+OO 1.13E+01

[2528]

3/13/2018 1:22:49AM Page 5 of6 Analysis Report for 12-Mar-18-10029 B1051 OOA-FSWC-1 01 CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCVgrams)

(keV)

Ba-133 79.61 2 .65 3 .15E+OO 2 .74E-01 7.67E+OO

81. 00 3 2 .90 -3 .37E-01 5.05E-01 2 76.40 7.16 -1.02E+OO 1.66E+OO 302.85 18.34 1. llE-01 6.66E-01 356.01 62.05 -2 . 2 1E-01 2 .74E-01 383.85 8.94 1. 6 0E-01 1. 35E+OO Cs-134 475.36 1. 48 4.74E+OO 2 .00E-01 1.lOE+Ol 563.25 8.34 7.0lE-02 1 .69E+OO 569.33 15.37 -6.39E-04 1. 2 4E+OO 604. 72 97.6 2 3 .40E-02 2 .00E-01 795.86 85.46 -1.13E-01 2. 03E-01 801.95 8.69 -1.46E-01 2. 0lE+OO 1038.61 0.99 1.35E+Ol 2 . 31E+O l 1167.97 1. 79 1.43E+OO 1.27E+Ol 1365.19 3.0 2 2.44E+OO 6.64E+OO Cs-137 661.66 85.10 2.45E-02 2 .82E-01 2 .82E-Ol Eu-152 1 21.78 2 8.67 4.52E-02 3.06E-01 3.06E-01 2 44.70 7.61 2.16E-01 l . 64E+OO 2 95.94 0.45 -1.85E+OO 3. 51E+Ol 3 44.28 2 6.60 -2 .64E-01 3. 60E-01 3 67.79 0.86 6.44E+OO 1.54E+Ol 411. 12 2.24 3.12E+OO 6.77E+OO 443.96 2.83 3. 72E+OO 5.56E+OO 488.68 0.42 3.09E+OO 3.34E+Ol 563.99 0.49 l.74E+Ol 2 .98E+Ol 586. 2 6 0.46 3.31E+Ol 4.14E+Ol 678. 62 0.47 4.82E+OO 2 .77E+Ol 688.67 0.86 -1.69E+OO 2 .38E+01 719.35 0.28 4.49E+OO 7.38E+01 778. 90 12. 96 3.87E-01 1. 38E+OO 810.45 0.32 -2.66E+01 4.93E+Ol 867.37 4.26 -2. 1 9E+OO 3 .90E+OO 919.33 0.43 1.39E+01 4.70E+01 964.08 14.65 -2. 72E-01 1.53E+OO 1085 . 87 10.24 7.62E-01 2 .83E+OO 1089 . 74 1. 73 -5.51E+OO l . 80E+01 1112. 07 13.69 -3.71E-Ol l.04E+OO 1212.95 1. 43 8.56E-01 1. 55E+01 1249.94 0.19 -5.18E+Ol 7.03E+01 1299.14 1. 63 -5.44E+OO 9.73E+OO 1408.01 21.07 -3.85E-01 6.92E-01 1457.64 0.50 1.81E+02 1. 2 6E+02 1528.10 0.28 -4.74E+Ol 7.82E+Ol Eu-154 123.07 40.40 -l.15E-01 2 . 2 1E-01 2 .21E-01 247.93 6.89 -5.85E-01 1. 53E+OO 591.76 4.95 - 1.71E+00 2 .82E+OO 692.42 1. 78 -3.29E-01 1 . 22E+Ol 723. 30 2 0.06 7.62E-01 l.19E+OO 756.80 4.52 l.71E+OO 3 .52E+OO 873.18 12.08 -7.13E-01 1.67E+OO 996.29 10.48 1. 35E+OO 2 .19E+OO

[2529]

3/13/2018 1:22:49AM Page 6 of6 Analysis Report for 12-Mar-18-10029 B 1051OOA-FSWC-101 CV 0.0" - 0.5" 0.5" Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCi!grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 6.58E-01 2 .21E-01 1.19E+OO 1274.4 3 34.80 -1.50E-01 5.00E-01 1596.48 1. 80 -1.17E+OO 9.05E+OO Eu-155 45. 3 0 1. 31 -4 . 17E+OO 5.58E-01 2. 93E+Ol 60.01 1. 22 1 . lOE+Ol 3.04E+Ol 86.55 3 0.70 2 .36E-01 5.83E-01 105.31 2 1.10 9.65E-02 5.58E-01 Ra- 22 6 186.21 3.64 3.00E+OO 3.13E+OO 3.13E+00 Pa-231 2 7. 36 10. 3 0 1. 5 4E+OO 3.49E+OO 3 .49E+OO 283 . 69 1. 70 7.09E-01 6.98E+OO 300.07 2 .47 -5.34E+OO 4.91E+OO 302.65 2 .20 1. 04E-01 5.55E+OO 330.06 1. 40 -8.40E-01 1 .08E+Ol U-235 143.76 10. 96 5.31E-01 1. 92E-01 1. OlE+OO 163.33 5.08 -7.49E-01 2 .21E+OO 185.71 57. 2 0 7.38E-02 1.92E-01 20 2 .11 1. 08 - 3 .50E+OO 8.83E+OO 205.31 5.01 - 1.66E+OO 1. 96E+00 Am-241 59.54 35.90 -1.87E-01 9.97E-01 9.97E-01

+ ;:;;

Nuclide identified during the nuclide identification

"' Energy line found in the spectrum MDA value not calculated Half-life too short to be able to perform the decay correction

? ::, CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2530]

0000024267 .CNF Live Time :1200.000 sec Real Tire :1200.260 sec 60 start: 1: -0.0(kev) stop : 8192: 2047. 8(kev)

Acq . Start :Tue Mar 13 01:02:42 2018 55 50 45 40 35

[2531]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/13/2018 12:58:28AM Page I of7

~~~pex-Gamma Analysis Report for 12-Mar-18-10028 B105100A-FSWC-115CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Mar-18-10028 Sample Description : B105100A-FSWC-115CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 9.429E+01 grams Facility : Default Sample Taken On : 3/9/2018 12:40:00PM Acquisition Started : 3/13/2018 12:14:42AM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 2400.0 seconds Real Time : 2400.5 seconds Dead Time *; 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24264 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 12:58:24AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2532]

3/13/2018 12:58:28AM Page 2 of7 Analysis Report for 12-Mar-18-10028 B 1051 OOA-FSWC-11 SCV 0.0" - OS 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 77.41 306 - 314 310.16 3.30E+Ol 20.39 6.40E+Ol 0.77 2 238.75 947 - 959 954.59 6.91E+Ol 22 .98 4.78E+Ol 0.50 3 295.42 1175 - 1186 1180. 96 4.03E+Ol 21. 2 6 5.74E+Ol 0 . 84 4 351.:2 1401 - 1415 1405.89 7.36E+Ol 25.16 5.88E+Ol 1. 2 3 5 511.34 2037 - 2049 2043.70 3 .48E+Ol 20.62 5.43E+Ol 0 . 31 6 609.41 2429 - 2443 2435.70 4.55E+Ol 16.42 l .50E+Ol 0.34 7 661.59 2636 - 2652 2644. 2 7 2 .73E+02 35.39 2.55E+Ol 1. 33 8 1172.89 4 682 - 4697 4688.99 4.44E+Ol 17 .13 1.92E+Ol 0.51 9 1332. 39 5322 - 5333 5327. 2 0 2 .61E+Ol 14.28 l.98E+Ol 0.61 10 1460.4 2 5832 - 5847 5839.61 6.18E+Ol 19.33 2 .04E+Ol 0.27 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDE$

Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty An Pk 0.98 511. 00

100.00 1. 3 2E-01 7.99E-02 K-40 0.97 1460.82

10.66 4 . 52E+OO 1. 4 7E+00 Co-60 0.99 1173.23

99.85 2 .93E-01 1.15E-01 1332.49

99.98 1.88E-01 l.04E-01 Cs-137 0.99 661.66

85.10 1. 41E+00 2 .49E-01 Pb-212 0.99 115 .18 0.60 238.63

43.60 3 .19E-01 1.18E-01 300.09 3.30 Pb212-XR 0.99 74.82 10. 2 8

[2533]

3/13/2018 12:58:28AM Page 3 of7 Analysis Report for 12-Mar-18-10028 81051 OOA-FSWC-115CV 0.0" - 0.5" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb212-XR 0 .99 77 .11 *k 17.10 5.31E-01 3 .46E-01 87.35 3.97 89.78 1. 46 Bi-214 0.99 609.3 2

45.49 4.13E-0 1 1.57E-01 768.36 4.89 806.18 1. 26 934.06 3 .11 1120.29 1 4.92 1155.21 1. 63 1238.12 5.83 128 0 .98 1. 43 1377. 67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 1661.27 1. 05 1729.59 2 .88 1764.49 15.30 1847.43 2 . 03 2118. 51 1.16 Pb-214 0. 99 241. 99 7.25 2 95. 22

18.42 5.12E-01 2 .82E-01 351.93

35.60 5 . 56E-01 2. l OE-01 785.96 1. 06 Pb214-XR 0.99 74.82 5.80 77 .11

9.70 9.36E-01 6.16£-01 87.35 2.24 89.78 0.82

=Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

[2534]

3/13/2018 12:58:28AM Page 4 of7 Analysis Report for 12-Mar-18-10028 B105100A-FSWC-115CV 0.0" - 0.5" 0.0" Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

An Pk 0.982 1. 32E-01 7.99E-02 K-40 0.974 4.52E+OO 1.47E+OO Co-GO 0.990 2 .35E-01 7.73E-02 Cs-137 0.999 1. 41E+OO 2 .49E-01 X Bi-211 0.935 Pb-21 2 0.998 3 .19E-01 1.18E-01

? Pb212-XR 0.992 5 . 3 1E-Ol 3 .46E-0 1 Bi-214 0.999 4 .13 E- Ol 1.57E-01 Pb-214 0.994 5.41E-01 1.69E-01

? Pb214-XR 0.992 9.36E-01 6.16E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2535]

3/13/2018 12:58:28AM Page 5 of7 Analysis Report for 12-Mar-18-10028 B105100A-FSWC-115CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 12:58:24AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL. NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCUgrams) (pCi/grams) (pCi/grams)

(keV)

+ An Pk 511.00

100.00 1.32E-01 1.19E-01 1.19E-01 BE-7 477.60 10.44 1.57E+OO 1.33E+OO 1. 3 3E+OO

+ K-40 1460.8 2

10.6 6 4.52E+OO 1. 60E+OO 1.60E+OO

+ Co-60 1173. 23

99.85 2 .93E-01 1.39E-01 1. 3 9E-01 13 32 .49

99.98 1.88E-01 1 .43E-01 Nb-94 702.65 99.8 1 2 .34E-02 1 .23E-01 1 .23E-01 871.09 99.89 4.31E-02 1.44E-01 Ag-108m 79.13 6 . 60 -6.41E-01 1.31E-01 2 .06E+OO 43 3 .94 90.50 4.lOE-02 1.36E-0 1 614.28 89.80 5.34E-02 1.75E-01 722 . 94 90.80 -4. 51E-02 1. 3 1E-01 Sb-1 2 5 176.31 6.84 3.33E-01 3.33E- 01 1.08E+OO 380.45 1. 52 -2.15E+OO 6.43E+OO 427.87 2 9.60 -2 . 2 2E-01 3.33E- 01 463.36 10.49 -4.64E-01 1. 09E+00 600.60 17.65 2 .92E-01 7.78E-01 606.71 4.98 -8.33E-01 3.74E+OO 635.95 11. 22 -1.70E-02 1.08E+OO 671.44 1. 79 2.36E+OO 7.13E+OO

[2536]

3/13/2018 12:58:28AM Page 6 of7 Analysis Report for 12-Mar-18-10028 B105100A-FSWC- 115CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity Nuc/ideMDA LlneMDA Name (pCi/grams) (pCi/grams) (pCl/grams)

(keV)

Ba-133 7 9.61 2 .65 -1 . 69E+OO 1 .95E- 01 4.95E+OO

81. 00 32 .90 -3 .34E-01 2 . 96E-01 276.40 7. 1 6 5.28E-01 1.21E+OO 302.85 18 . 34 -1.0lE-01 4.52E-01 356. 01 62 . 0 5 -7.09E-0 2 1. 95E-01 383.85 8.94 - 2.77E-01 1.04E+OO Cs- 134 475.36 1. 48 6.94E+00 1 .62E-01 8.68E+OO 563. 25 8.34 -2 .69E+00 1.32E+OO 569. 33 15.37 6.30E-02 7.99E-01 604. 72 97. 62 -4.08E-02 1. 62E-01 795.86 85.46 7.32E-02 1.66E-01 8 01. 95 8.69 6.83E-02 1.59E+OO 1 038.61 0.99 6.60E+OO 1. 56E+Ol 1167. 97 1. 79 -1.32E+Ol 1. 55E+Ol 1365.19 3.0 2 1.0lE+OO 4.41E+OO

+ Cs-137 66 1 .66

85.10 1.41E+OO l .25E-0 1 1 .25E-01 Eu - 152 121.78 2 8.67 1. 32E-01 2.SOE-0 1 2 .50E-01 244.7 0 7.6 1 9.75E-01 1. 2 5E+OO 295.94 0.45 9.42E+OO 2 . 72E+Ol 344.28 2 6.60 -4.55E-0 2 3.38E-01 367.79 0.86 -3.20E+00 9. 72E+OO 411.12 2 .24 9.54E-03 5.0lE+OO 443. 96 2 .83 -1.19E+00 3 .66E+OO 488.68 0.42 -l.03E+Ol 2. 56E+Ol 563 . 99 0.49 -1.50E+Ol 2 .24E+Ol 586.26 0.46 2.05E+Ol 2 . 96E+Ol 678.62 0.47 2.0lE+Ol 2 .59E+O l 688.67 0.86 -1.16E+Ol 1.46E+01 719.35 0. 2 8 3.51E+Ol 4. 1 6E+01 778.90 12.96 -5. 72E-02 9.07E-01 810.45 0.32 1.39E+Ol 3 .77E+Ol 867.37 4.25 1.27E+OO 3 .43E+OO 919.33 0.43 -1.51E+OO 3 .50E+Ol 964.08 14.65 4.91E-02 1. 2 3E+OO 1 085.87 10.24 -2. 1 4E-:01 1.42E+OO 1089.74 1. 73 7.97E+OO 9.19E+OO 1112. 07 13.69 -9.50E-01 1. 27E+OO 1212.95 1. 43 9.16E+OO 1. 27E+01 1 2 49.94 0 .19 2.73E+OO 7.34E+Ol 1 2 99.14 1. 63 6.09E+OO 9.06E+OO 1408.01 2 1. 07 2.62E-01 6.98E-01 1457.64 0.50 1. 2 7E+0 2 7.17E+Ol 1 528.10 0.28 -3.57E+Ol 4.20E+Ol Eu - 154 1 23 .07 40.40 9.86E-02 l.76E-01 1. 76E-01 2 47.93 6.89 2 .46E- 01 1. 2 0E+OO 591. 76 4.95 -2 . 93E- Ol 2 .30E+OO 692.42 1. 78 3 . 31E+OO 7.67E+OO 723. 30 2 0.06 -2 .31E-01 6.04E-01 756.80 4.5 2 3.60E-0 2 2. 93E+OO 873.18 12.08 -4.47E-01 1. 2 4E+OO 996. 2 9 10.48 1.0lE+OO 1. 3 1E+00

[2537]

3/13/2018 12:58:28AM Page 7 of7 Analysis Report for 12-Mar-18-10028 8105100A-FSWC-115CV 0.0" -0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCi/grams) (pCilgrams)

(keV)

Eu-154 1004.76 18.01 1.23E-01 1. 76E-01 8.18E-01 1274.43 34.80 -6.65E-02 3.77E-01 1596.48 1. 80 7.52E-01 7. 2 9E+OO Eu-155 45.30 1. 31 -4.89E+OO 3.36E-01 2 .19E+Ol 60.01 1. 2 2 2.09E+OO 2 .27E+Ol 86.55 30.70 2.54E-02 3.36E-01 105. 3 1 21.10 9.03E-0 2 3.58E-01 Ra- 226 186. 2 1 3.64 7. 2 4E-01 2.32E+OO 2.32E+OO Pa-23 1 2 7. 3 6 10.30 2 .32E+OO 2 .57E+OO 2.57E+00 283.69 1. 70 1. 92E+OO 4.64E+OO 300.07 2 .47 1.92E-01 3.69E+OO 302.65 2 . 20 9.82E-01 3.84E+OO 330.06 1. 40 -3.64E+OO 7.43E+OO U-235 143.76 10. 96 -1. 27E-01 1.48E-01 6.09E-01 1 63.33 5.08 -3 .68E-01 1.40E+OO 185.71 57. 2 0 9.14E-02 1.48E-01 20 2 .11 1. 08 3.09E+OO 7.0lE+OO 205.31 5.01 - 2 .31E-01 1.52E+OO Am-241 59.54 35.90 2 .74E-01 7.95E-01 7.95E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2538]

0000024264.CNF Live Time :2400.000 sec 60 Real Time :2400.510 sec start: 1: -0.0(kev)

Stop : 8192: 2047. S(kev)

Acq. Start :Tue Mar 13 00:14:42 2018 55 50 45

[2539]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/13/2018 6:43:03PM Page 1 of7

-~ pex-Gamma Analysis Report for 13-Mar-18-10010 8105100A-FSWC-115CV o.o* - 0.5" 0.0" GAMMA SPECTRUM ANAL YS/S Sample Identification : 13-Mar-18-10010 Sample Description : 81051 OOA-FSWC-115CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 9.429E+01 grams Facility : Default Sample Taken On : 3/9/2018 12:40:00PM Acquisition Sta*rted : 3/13/2018 5:30:50PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 3600.0 seconds Real Time : 3604.6 seconds Dead Time : 0.13 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24299 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 6:42:59PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2540]

3/13/2018 6:43:03PM Page 2 of7 Analysis Report for 13-Mar-18-10010 B1051 OOA-FSWC-115CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid. Area Uncertainty Counts (keV) 1 2 38.65 473 - 481 477.49 8.42E+Ol 43.42 3 .56E+02 1. 07 2 35 2 .02 700 - 708 703.99 9.83E+Ol 31. 81 1. 45E+02 0 .80 3 583.28 1160 - 1169 1166.17 4.26E+Ol 22 .59 7.49E+Ol 1. 02 4 609.35 1214 - 1223 1 2 18. 2 8 6.44E+Ol 24.65 7. 72E+Ol 1. 30 5 661.79 1317 - 1328 1323 .12 4.51E+0 2 46.23 6.63E+Ol 1. 53 6 1173.73 2340 - 2353 2 347.07 7.82E+Ol 22.09 3.17E+Ol 1.12 7 1332.77 2660 - 2671 2 665.35 6.23E+Ol 19. 72 2 .74E+01 1. 25 8 1461.18 2917 - 2929 2 922.41 1. 23E+02 25.34 2 .88E+Ol 1. 31 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.98 1460.82

10.66 5. 2 9E+OO 1.19E+OO Co-60 0.97 1173.23

99.85 3.06E-01 9.00E-02 1332.49

99.98 2 .66E-01 8.68E-02 Cs-137 0.99 661.66

85.10 1.40E+OO 2 . 2 1E-01 Tl-208 0.99 583.19

85.00 1. 21E-01 6.58E-0 2 Bi-211 0.86 351.07

1 3.02 1. 2 5E+OO 4.51E-01 Pb-212 1. 00 11 5 .18 0.60 23 8.63

43.60 2 .41E-01 1.30E-01 300.09 3 .30 Bi-214 1. 00 609.32

45.49 3.53E-Ol 1 . 42 E- 01 768.36 4.89

[2541]

3/13/2018 6:43 :03PM Page 3 of7 Analysis Report for 13-Mar-18-10010 B105100A-FSWC-115CV 0.0" - 0.5" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi - 214 1. 00 806.18 1. 26 934.06 3.11 1120. 2 9 14.92 11 55. 2 1 1. 63 1238.12 5.83 1 2 80.98 1. 43 1377.67 3.99 1385. 31 0.79 140 1. 52 1. 33 1407.99 2 .39 1509 .2 1 2 .13 166 1 . 2 7 1. 05 1729.59 2 .88 1 764.49 15.30 1847.43 2 .03 2 118.51 1.16 Pb-214 0.99 241. 99 7.25 295. 22 1 8.42 351.93

35.60 4.57E-01 1.65E-01 785. 96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Toierance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.980 5.29E+OO l. 1 9E+00 Co-60 0.974 2 .85E-01 6.25E-02 Cs-137 0.997 1.40E+OO 2.21E-01 Tl-208 0.998 l .21E-01 6.58E-02

? Bi-211 0.865 1. 2 5E+OO 4.51E-01 Pb-21 2 1.000 2 .41E-01 1 .30E-01 Bi-214 1.000 3.53E-01 1.42E-01

[2542]

3/13/2018 6:43:03PM Page 4 of7 Analysis Report for 13-Mar-18-10010 B 105100A-FSWC-115CV 0.0" - 0.5" 0.0" Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

? Pb-214 0.999 4.57E-01 1.65E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2543]

3/13/2018 6:43:03PM Page 5 of7 Analysis Report for 13-Mar-18-10010 B105100A-FSWC-115CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 6:42:59PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCi!grams) (pCl!grams)

(keV)

An Pk 511 . 00 100.00 4. 2 6E-01 1.83E-01 1.83E-01 BE-7 477.60 10.44 2 .58E-0 1 1. llE+OO 1. llE+OO

+ K-40 1460.82

10.66 5. 2 9E+OO 1.03E+OO 1. 03E+OO

+ Co-60 1173.23

99.85 3.06E-01 9.78E- 02 9.94E-02 1332.49

99.98 2 .66E-01 9.78E-02 Nb-94 702.65 99.81 -6.96E-03 l.15E-01 1.15E-01 871.09 99.89 8.08E-02 1.17E-01 Ag-108m 79.13 6.60 9.71E-Ol 1.15E-01 2 . llE+OO 433.94 90.50 -1.76E-0 2 1.15E-01 614.28 89.80 -8. l OE-02 1.34E-01 722 .94 90.80 2 .41E-02 1.21E-01 Sb-1 2 5 176.31 6.84 - 2 .69E-01 3 .64E - 01 1.26E+OO 3 80.45 1. 52 3 . 2 8E+OO 6.59E+00 427.87 2 9.60 5.79E-03 3 .64E-01 463. 3 6 10.49 1. 53E-01 l . llE+OO 600.60 17.65 -6.83E-0 2 5.99E-01 606.71 4.98 - 9.76E-01 2 .94E+OO 635.95 11. 22 -4.62E-02 9. 2 0E-01 671. 44 1. 79 l.25E-02 5.56E+00

[2544]

3/13/2018 6:43:03PM Page 6 of7 Analysis Report for 13-Mar-18-10010 81051 OOA-FSWC-115CV o.o* -0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCUgrams) (pCilgrams)

(keV)

Ba-133 79.61 2.65 2 .52E+00 1 .87E-0 1 5.lOE+OO 8 1. 00 32.90 -1.75E-01 3.64E-01 276.40 7.16 -8.36E-02 1. 2 5E+OO 302.85 18.34 1 .60E-01 5.22E-01 356. 01 62.05 -8.34E-02 1.87E-0 1 3 83.85 8.94 -5. llE-01 1.00E+OO Cs-134 475. 3 6 1. 48 - 1. 2 0E+OO l.17E-O l 7.37E+OO 563.25 8.34 -7.37E-02 1 .21E+00 569.33 15.37 1. 2 9E-01 6.39E-01 604. 72 97.6 2 -5.40E-02 1.33E-01 795.86 85.46 -5.33E-02 1.1 7E-0 1 801.95 8.69 4.36E-02 1. 3 0E+00 1038.61 0.99 -1.38E-01 1.17E+Ol 1167.97 1. 79 - 1 . 92E+OO 8.93E+OO 1365.19 3.0 2 -5.40E-01 3.28E+OO

+ Cs- 137 661.66

85.10 1.40E+OO 1. 05E-01 1.05E-01 Eu-152 121.78 28.67 3 .46E-02 2 .63E- 01 2.63E-01 2 44.70 7.61 -2 .91E-01 1.25E+OO 2 95.94 0.45 1.81E+Ol 2 .40E+Ol 344. 2 8 2 6.60 9.93E-02 3.89E-01 367.79 0.86 -2 .45E+OO 1. llE+Ol 411.12 2 . 24 4 .3 9E-01 4.54E+OO 443. 96 2 .83 -1.59E+OO 3.53E+OO 488.68 0.42 l.08E+Ol 2.68E+Ol 563.99 0.49 4.41E+OO 2.08E+Ol 586. 2 6 0.46 -2.41E+Ol 2.90E+Ol 678.62 0.47 -5.18E+OO 2.23E+Ol 688.67 0.86 5.79E+OO 1. 30E+Ol 71 9. 35 0.28 -1. 29E+Ol 3.41E+Ol 778.90 12.96 2.55E-01 8.33E-0 1 81 0 .45 0.32 2.38E+O l 3.74E+Ol 867.37 4. 2 6 -7.81E-01 2 .60E+OO 919.33 0.43 -7 . 85E+OO 2.75E+Ol 964.08 14.65 5.86E-03 9.23E-01 10 85.87 10.24 -4.58E-01 1. 15E+OO 1 0 89.74 1. 73 5 . 34E-01 6.72E+00 1 11 2 . 07 13.69 -5 . 84E-0 2 8.60E-0 1 1212 .95 1. 43 1.12E+OO 7.80E+OO 1249.94 0.19 -2 .48E+Ol 5.59E+Ol 1299.14 1. 63 -2 .25E+00 8.05E+OO 1408.01 2 1.07 l.38E-01 5.69E-01 1 457.64 0.50 -1.80E+Ol 5.52E+Ol 1 528.10 0.28 2 .13E+Ol 3.93E+Ol Eu-154 123.07 40 . 40 -2 .35E-0 2 1. 84E-0 1 1.84E-01 247.93 6.89 -3 .04E-01 l.31E+OO 591. 76 4.95 -4.79E-01 2 . 27E+OO 692.4 2 1. 78 -7.66E-01 5.55E+OO 723 . 3 0 20. 0 6 1.43E-01 5.57E-01 756.80 4. 52 -5.43E-02 2 .53E+OO 873. 1 8 1 2 .08 2 .88E- 01 9.31E-01 996.29 1 0.48 -2 .34E-01 l.05E+OO

[2545]

3/13/2018 6:43:03PM Page 7 of7 Analysis Report for 13-Mar-18-10010 B 1051 OOA-FSWC-115CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi!grams) (pCUgrams)

(keV)

Eu-154 1004.76 18.0 1 -1. 72E-01 1.84E-01 6.20E-01 1274.43 3 4.80 -1.75E-01 3.71E-01 1596.48 1. 80 -4.68E+OO 4.53E+00 Eu-155 45.30 1. 31 -2 .23E+OO 2 .98E-01 1. 82E+Ol 60.01 1. 22 -1. 35E+Ol 1.91E+Ol 86.55 30.70 -1.83E-01 2 .98E-01 105.31 2 1.10 -3 .44E-0 1 3.60E-01 Ra-226 186. 2 1 3.64 9.75E-0 1 2 .67E+OO 2 .G7E+OO Pa-231 27.36 10.30 2 .0BE+OO 2 .00E+OO 2 .00E+OO 283.69 1. 70 -1. 33E+OO 5.22E+OO 300.07 2 .47 -3 .79E+OO 3.85E+OO 302.65 2 .20 1.33E+OO 4. 3 4E+OO 330. 0 6 1.40 1.75E+OO 7.19E+OO U-235 143.76 10. 96 1.38E-01 l . 72E-01 6.90E-01 1 63.33 5.08 7 . 16E-01 1.73E+OO 185.71 57. 2 0 1.08E-01 1.72E-01 20 2 .11 1. 08 6.50E-01 8.55E+OO 205.31 5.01 -4.60E-01 1.79E+OO Am-241 59.54 35.90 -3 .64E-01 6.70E-01 6.70E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

...r = CAUTION: MDA value Is inconsistent with Currie MDA at 95% confidence level

[2546]

0000024299.CNF 250 Live Tine :3600.000 sec Real Tine :3604.620 sec start: l: O.l(kev) stop : 4096:2047.l(kev)

Acq. Start :Tue Mar 13 17:30:50 2018 200 150 =

7 t'.l V)

C

J 0

u

[2547]

100

~

50 c:,

"'t

....;:j "'

.~

~

I H c:,

~iJ~

co co

~

0 u 'f

....I I-8 0 *~lfr'l J , ~ . ~ ,.. *. \ v, 500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/13/2018 6:44:07PM Page 1 of6

~pex-Gamma Analysis Report for 13-Mar-18-10011 B105100A-FSWC-115CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10011 Sample Description : 81051 OOA-FSWC-115CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 9.429E+01 grams Facility : Default Sample Taken On : 3/9/2018 12:40:00PM Acquisition Started : 3/13/2018 6:24:00PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.2 seconds Dead Time : 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120- 8192 Peak Area Range (in channels) : 120-8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24301 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANAL YS/S REPORT Peak Analysis Performed on : 3/13/2018 6:44:03PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2548]

3/13/2018 6:44:07PM Page 2 of6 Analysis Report for 13-Mar-18-10011 B105100A-FSWC-115CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 661.59 2636 - 2653 2644.27 3.32E+02 37.11 8.13E+00 1.17 2 1460.46 5834 - 5845 5839.78 3.58E+Ol 14.70 1. 44E+Ol 0.36 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCUDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.97 1460.82

10.66 5.23E+00 2.20E+OO Cs-137 0.99 661.66

85.10 3.42E+OO 5.62E-01

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold == 0.30 Errors quoted at 2.000sigma

[2549]

3/13/2018 6:44:07PM Page 3 of6 Analysis Report for 13-Mar-18-10011 B105100A-FSWC-115CV 0.0" - 0.5" 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)

K-40 0.979 5.23E+OO 2.20E+OO Cs-137* 0.999 3.42E+OO 5.62E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2550]

3/13/2018 6:44:07PM Page 4 of6 Analysis Report for 13-Mar-18-10011 B105100A-FSWC-115CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 6:44:03PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCJ!grams) (pCi!grams) (pCilgrams)

(keV)

An Pk 5 11 . 00 100.00 3.15E-01 2 .93E-01 2. 93E-01 BE-7 477.60 10.44 9.60E-01 1.89E+OO 1. 89E+OO

+ K-40 1460.82

10.66 5.23E+OO 2 .53E+OO 2 .53E+00 Co-60 1173.23 99.85 6.59E-02 1. 7 9E-0 1 1. 79E-01 1332.49 99.98 -7 . 52E-02 2 .49E-01 Nb-94 702.65 99.81 -5.0lE-02 1.66E- 01 1. 66E-01 871. 0 9 99.89 -3 . 2 8E-0 2 1. 76E-01 Ag-108m 79 .13 6.60 1. 53E+OO 2 . 1 5E - 01 3 .22E+OO 433.94 90.50 -l.42E-01 2 .36E-01 614.28 89.80 -1.33E-02 2 .25E-01 722. 94 90.80 4 . 0lE-02 2 . 1 5E-01 Sb-125 176.31 6.84 4.0lE-01 6.82E-01 l.77E+OO 380.45 1. 52 2 .18E+O O 1.17E+Ol 427.87 2 9.60 2 . 2 9E-0 1 6.82E-01 463.36 10.49 4.84E-01 1.97E+OO 600.60 17.65 -6.84E-0 1 9.35E-01 606.71 4.98 9.60E-02 4.20E+OO 635.95 11. 22 1.55E-Ol 1 .68E+OO 671.44 1. 79 4.27E+ OO 1. OOE+Ol

[2551]

3/13/2018 6:44:07PM Page 5 of6 Analysis Report for 13-Mar-18-10011 B1051 OOA-FSWC-115CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi!grams) (pCi!grams)

(keV)

Ba-133 79.61 2 .65 4.99E+OO 3 . 04E-01 7. 96E+OO

81. 00 32 .90 -4.38E-01 4.91E-01 2 76.40 7.16 -6.31E-01 1.99E+OO 302.85 18.34 7.02E-02 8.52E-01 356.01 62 .05 -1.53E-01 3.04E-01 383.85 8.94 -2 .31E-01 1.99E+OO Cs-134 475.36 1. 48 -1. 2 9E+OO 1. 96E-01 1. 33E+Ol 563.25 8.34 1.llE-01 2 .0lE+OO 569.33 15.37 -l.81E-01 9.97E-01 604. 72 97. 62 -9.81E-02 1. 96E-0 1 795.86 85.46 - 5.69E-0 2 2 . 13E-01 801.95 8.69 - 2 .66E-0 1 2 .43E+OO 1 038.61 0.99 -7.67E+OO l.67E+Ol 1167. 97 1. 79 5.14E+OO l.14E+Ol 1365. 1 9 3.0 2 -l.19E+00 6.lOE+OO

+ Cs-137 661.66

85.10 3 .42E+OO 1.53E-01 1. 53E-01 Eu-1 52 121. 7 8 28.67 -2 .51E-02 3.83E-01 3.83E-01 244.70 7.61 -8.0lE-01 l.87E+OO 295.94 0.45 2 . 2 6E+Ol 4.26E+Ol 344.28 2 6.60 1.25E-01 6.07E-01 367.79 0.86 1.43E+Ol 2 .00E+Ol 411.12 2 .24 2 .18E+OO 9.15E+OO 443.96 2 .83 -3.15E+OO 7.14E+OO 488.68 0.4 2 -2.lOE+Ol 4.29E+Ol 563.99 0.49 -7.64E+OO 3.30E+Ol 586.26 0.46 4.17E+Ol 5.08E+Ol 678.6 2 0.47 2 .46E+Ol 3 .82E+Ol 688 . 67 0.86 l.32E+OO 1.98E+Ol 719.35 0.28 -3 .58E+Ol 6.97E+Ol 778.90 12. 96 3 .05E-01 9.51E-01 810.45 0.32 2 .18E+OO 3.95E+Ol 867.37 4.26 -l.57E+OO 3.13E+OO 919. 33 0.43 1.57E+Ol 5.08E+Ol 964.08 14.65 l.99E-01 1.22E+OO 1 085.87 10.24 6.lOE-01 l.66E+OO 1 089.74 1. 73 -6.51E+OO 9.84E+OO 111 2 . 07 13. 69 8.88E-02 1.36E+OO 1212.95 1. 43 2.44E+OO 1.63E+Ol 1 249.94 0. 1 9 7. 2 8E+OO 5.58E+Ol 1 2 99. 1 4 1. 63 -2 .34E+OO 1. 08E+Ol 1 408. 0 1 2 1.07 2 .15E-01 8.02E-01 1457.64 0.50 1.40E+02 l . 13E+0 2 1528.10 0.28 1.72E+Ol 6.43E+Ol Eu-154 123.07 40.40 -5.35E-02 2 .83E-01 2 .83E-01 2 47.93 6.89 5.87E-01 2 .13E+OO 591.76 4.95 -1.94E+OO 3.50E+OO 692.42 1. 78 3.70E+OO 9.96E+OO 723. 30 2 0.06 1.22E-Ol 9.42E-01 756.80 4.52 1.33E+OO 4.18E+OO 873. 1 8 12.08 1. 07E+OO 1.73E+OO 996. 2 9 10.48 1.69E-0 2 1.53E+OO

[2552]

3/13/2018 6:44:0?PM Page 6 of6 Analysis Report for 13-Mar-18-10011 B105100A-FSWC-115CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 -4. llE-01 2 .83 E- 01 8.95E-01 1~74.4 3 34.80 2 .40E-0 1 5.86E-01 1596.48 1. 80 5.62E+OO 1.37E+Ol Eu-155 45.30 1. 31 1.53E+Ol 5.59E-01 3.37E+Ol 60.01 1. 22 6.25E+OO 3.61E+Ol 86.55 30.70 4.35E-01 5.59E-01 105. 3 1 21.10 -6.91E-02 5.78E-01 Ra- 2 26 186. 2 1 3.64 3.23E+OO 3.BOE+OO 3.80E+OO Pa- 2 31 27.36 10.30 -9.44E-02 3.43E+OO 3.43E+OO 283.69 1. 70 -5.97E+OO 8.85E+OO 300.07 2 .47 -1.02E+Ol 6.43E+OO 302.65 2 . 20 1.44E+OO 7.18E+OO 330.06 1. 40 6.37E+OO 1.20E+Ol U-23 5 143.76 10. 96 1.92E-01 2 .30 E- 01 1.02E+OO 163.33 5.0 8 -1.49E-01 2 . llE+OO 185.71 57. 2 0 7.35E-02 2 .30E-01 202 .11 1. 08 3 .76E-01 l.lOE+Ol 205.31 5.01 -5 .09E-01 2 .31E+OO Am-241 59.54 35.90 2 .57E-01 1. 2 5E+OO 1.25E+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too shot1 to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2553]

0000024301.CNF Live Time 1200.000 sec Real Time 1200.230 sec 120 Start: 1 -0.0(kev)

Stop : 8192 2047. 8(kev)

Acq. start Tue Mar 13 18:24:00 2018 110 100 90 Vl C

=s 0

u

[2554]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/13/2018 5:06:08PM Page I of7

~pex-Gamma Analysis Report for 12-Mar-18-10030 B105100A-FSWC-116CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Mar-18-10030 Sample Description : B105100A-FSWC-116CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 9.862E+01 grams Facility : Default Sample Taken On : 3/9/2018 8:00:00AM Acquisition Started : 3/13/2018 1:33:15AM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 3600.0 seconds Real Time : 3604.6 seconds Dead Time : 0.13 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24268 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 5:06:04PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2555]

3/13/2018 5:06 :08PM Page 2 of7 Analysis Report for 12-Mar-18-10030 8105100A-FSWC-116CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.65 473 - 481 477 . 49 l.02E+02 43.65 3 .46E+02 1.13 2 351. 89 698 - 708 703.73 8.81E+Ol 35.95 l.98E+02 1. 38 3 583.30 1162 - 1171 1166.20 3 .09E+Ol 2 1. 22 7.22E+Ol 1.23 4 609.47 1212 - 1224 1 2 18.51 7.80E+Ol 2 7.86 8.80E+Ol 1. 49 5 661.90 1317 - 1327 1323.34 2 .70E+02 3 6.40 5.13E+Ol 1. 42 6 1173.64 23 41 - 2351 2346.88 3 .95E+Ol 17.74 3.30E+Ol 1. 32 7 1332.77 2662 - 2672 2665.37 4.89E+Ol 17.94 2.62E+Ol 2.16 8 1461. 2 6 2916 - 2930 2922.57 1. 4 6E+02 26.44 1.92E+Ol 2 .39 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.97 1460.82

10 .66 6.04E+OO 1. 21E+O O Co-60 0.98 1173. 23

99.85 l.48E-01 6.75E-0 2 1332.49

99.98 2 .00E-01 7 .50E-0 2 Cs-137 0.99 661.66

85. 1 0 8.02E-01 1. 45E-0 1 Tl-208 0.99 583.19

85.00 8.39E-0 2 5.85E- 02 Bi-211 0.89 351.07

13.0 2 1. 07E+00 4.69E-01 Pb-212 1. 00 115 . 18 0 .60 238.63

43.6 0 2 .79E-0 1 l. 2 8E-01 300.09 3.30 Bi-21 4 0.99 609.32

45.49 4.09E-01 l .54E-0 1 768.36 4.89

[2556]

3/13/2018 5:06:0BPM Page 3 of7 Analysis Report for 12-Mar-18-10030 B105100A-FSWC-116CV 0.0" - 0.5" o.o*

Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi-214 0.99 806.18 1.26 934.06 3.11 1120.29 14.92 1155. 21 1. 63 1238.12 5.83 1280.93 1. 43 1377.67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2 .39 1509.21 2 .13 1661. 2 7 1. 05 1729.59 2 .88 1 764.49 15.30 1 847.43 2 .03 2118.51 1.16 Pb-214 1. 00 241. 99 7.25 295. 22 18.42 351.93

35.60 3.91E-0 1 1.71E-01 785.96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.970 6.04E+OO 1.21E+OO Co-60 0.980 1.71E-01 5.02E-02 Cs-137 0.990 8.02E-01 1.45E-01 Tl-208 0.998 8.39E-02 5.85E-0 2

? Bi-211 0.897 1.07E+OO 4.69E-01 Pb-21 2 1. 000 2.79E-01 1.28E-01 Bi-214 0.999 4.09E-01 1.54E-01

[2557]

3/13/2018 5:06:08PM Page 5 of7 Analysis Report for 12-Mar-18-10030 B105100A-FSWC-116CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 5:06:04PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

An Pk 511 . 00 100.00 3 .82E-01 1.80E-01 1.80E-01 BE-7 477.60 10.44 l.13E-01 9.69E-01 9.69E-01

+ K-40 1460.8 2

10.66 6.04E+OO 8.65E - 01 8.65E-01

+ Co-60 1173 . 2 3

99.85 1.48E-01 8. 96E-02 9.03E-0 2 1 332 .49

99.98 2 .00E-01 8. 96E-02 Nb-94 702.65 99.8 1 -4.87E-02 1.02E-01 1.06E-01 871.09 99.89 -2 .95E-02 1. 02E-01 Ag-108m 79 .13 6.60 1.76E+OO 1.12E-01 1. 91E+OO 43 3 .94 90.50 9.92E-03 1.12E-01 614.28 89.80 -4.83E-02 1.34E-01 722.94 90 . 80 -5.16E-0 2 l.16E-01 Sb- 12 5 176.31 6.84 -2 .02E-01 3.33E- 01 1.26E+OO 380.45 1. 52 -1.96E+OO 5.64E+OO 427.87 2 9.60 4.35E-02 3.33E-01 463.36 10.49 -2 .17E-01 9.28E-01 600.60 17.65 -5.07E-02 5.80E-01 606.71 4.98 -5.08E-01 2 .83E+OO 635.95 11. 2 2 -4.91E-01 8.37E-01 671.44 1. 79 1. 04E+OO 5.58E+OO

[2558]

3/13/2018 5:06:0BPM Page 6 of7 Analysis Report for 12-Mar-18-10030 B105100A-FSWC-116CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCUgrams) (pCilgrams) (pCilgrams)

(keV)

Ba-133 79.61 2.65 2 . 0lE+OO 1. 7 5E-01 4.47E+OO

81. 00 32.9 0 -5.08E-01 2 .85E-01 276.40 7.16 -1.02E-01 1. 2 1E+OO 3 02.85 18.34 1. 32E-02 4. 61E-01 356.01 62.05 -6.63E-02 1. 7 5E-0 1 383.85 8.94 -3.47E-01 9.44E-01 Cs-134 475.36 1. 48 -2 .46E+OO 1.13E-01 6.35E+OO 563.25 8.34 3.27E-01 1.14E+OO 569.33 15.37 -4.85E-01 5.45E-01 604.72 97.62 -2 .86E-02 1.27E-01 795.86 85.46 2 .61E-0 2 1.13E-01 801. 95 8.69 -8.67E-0 1 1.08E+OO 1 038.61 0 .99 -1.23E+OO 1.22E+Ol 1 167.97 1. 79 1 .92E+OO 8.15E+OO 1365.19 3.0 2 -4.07E-01 2 .79E+OO

+ Cs-137 66 1. 66

85.10 8.02E-01 8.70E-02 8.70E-02 Eu-152 121. 78 2 8.67 -2 .15E-02 2 .48E-01 2 .48E-01 244.7 0 7 .6 1 -5.0lE-01 1.16E+OO 295.9 4 0.45 7.75E+OO 2 .13E+01 344.28 2 6.60 -8. 2 6E-0 2 3.37E-01 367.79 0 .86 -4.57E+OO 9.61E+OO 411.12 2 .24 6.43E-01 4. llE+OO 443. 96 2 .83 -2. 76E+OO 3. 2 4E+OO 488.68 0.42 8.35E-01 2.22E+01 563.99 0.49 9.50E+OO l.93E +Ol 586.26 0.46 2 .55E+OO 2.68E+Ol 678.62 0.47 3 . 2 9E+OO 2 .20E+Ol 688.67 0.86 2 . 2 6E+00 1.22E+Ol 71 9.35 0. 2 8 -7.73E+OO 3 .43E+Ol 778.90 12.96 -2 .78E-0 2 8.lOE-01 81 0 .45 0. 32 1.81E+Ol 3.60E+Ol 867.37 4.26 2 .67E-01 2 .59E+O O 919.33 0.43 -2 .52E+OO 2 .55E+O l 964. 0 8 14.65 -2 .03E-01 8.24E-01 1 085.87 10. 2 4 5.46E-01 1. 18E+OO 1 089.74 1. 73 4.23E-01 6.75E+00 1 112. 07 13. 69 - 1. 71E-01 7.43E-01 121 2 .95 1. 4 3 - 9.02E-01 7.33E+OO 1249.94 0.19 -3 . 71E+O l 5.83E+Ol 1299.14 1. 63 -2 .80E+OO 7.07E+OO 1408.01 21. 07 -5.87E-02 4.93E-01 1457.64 0.50 2 .58E-01 5.65E+Ol 1 528.10 0.28 5.06E-01 2 .66E+Ol Eu-154 123.07 40.40 7.38E-02 1.80E-0 1 1 .BOE-01 247.93 6.89 -3.41E-02 1. 2 0E+OO 591.76 4.95 3.33E-01 2.19E+OO 692.42 1. 78 -1.lOE-01 5.92E+OO 723.30 2 0.06 -5.86E-03 5.36E-01 756.80 4.52 -5.46E-01 2 .llE+OO 873. 1 8 12.08 3.83E-01 8. 71E-01 996. 2 9 10.48 -4.33E-01 9.47E-01

[2559]

3/13/2018 5:06:08PM Page 7 of7 Analysis Report for 12-Mar-18-10030 B105100A-FSWC-116CV 0.0" -0.5" 0.0" Nuclide Energy Yield{%) Activity Nuc/ideMDA LineMDA Name (pCUgrams) {pCi/grams) {pCi/grams)

{keV)

Eu-154 10()4.76 18 . 01 -8.67E-02 1 .80E-01 5.46E-01 1274.43 34.80 -7.42E-03 3.36E-01 1596.48 1. 80 3.78E+OO 6 . 12E+OO Eu-155 45. 3 0 1. 31 8.36E-01 3.02E-01 1 . 81E+Ol 60.01 1. 22 -3 .09E+OO 1. 88E+Ol 86.55 30.70 1.22E-01 3.02E-01 105.31 21.10 2 .66E-01 3.93E-01 Ra-226 186.21 3.64 9.70E-01 2 .41E+OO 2.41E+00 Pa-23 1 2 7.36 10.30 1.44E+OO 1.8'7E+OO 1.87E+OO 2 83.69 1. 70 1.60E+OO 5.lOE+OO 300.07 2 .47 -3 .90E+OO 3.35E+OO 302.65 2 .20 1.lOE-01 3.84E+OO 330.06 1. 40 4.99E+OO 6.64E+OO U-235 143.76 10. 96 1.89E-02 l.53E-01 6.67E-01 16 3 . 33 5.08 2.2 0E-01 1.68E+OO 1 85.7 1 57. 2 0 4.54E-02 1.53E-01 202 . 11 1. 08 1.42E-01 7.89E+OO 205.31 5.0 1 -9 .49E-01 1.63E+OO Am-24 1 59.54 35.90 -1. 71E-Ol 6.51E-01 6.51E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA vaiue is inconsisient with Currie MDA at 95% r..onficience ievei

[2560]

0000024268.CNF Live Time :3600.000 sec Real Time :3604.570 sec start: 1: O.l(kev) stop : 4096: 2047. l(kev)

Acq. Start :Tue Mar 13 01:33:15 2018 V)

+-'

C:

J 0

u

[2561]

..,.=

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/13/2018 9:19:27PM Page I of6

~§~pex-Gamma Analysis Report for 12-Mar-18-10031 B105100A-FSWC-116CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Mar-18-10031 Sample Description : B105100A-FSWC-116CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 9.862E+01 grams Facility : Default Sample Taken On : 3/9/2018 8:00:00AM Acquisition Started : 3/13/2018 5:09:01PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.6 seconds Dead Time : 0.13 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24309 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 9:19:23PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2562]

3/13/2018 9:19:27PM Page 2 of6 Analysis Report for 12-Mar-18-10031 B105100A-FSWC-116CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 1461.26 2917 - 2927 ~922.58 5.22E+Ol 16.54 1.36E+Ol 1. 73 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.97 1460.82

10.66 6.46E+00 2.12E+OO

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2563]

3/13/2018 9:19:27PM Page 3 of6 Analysis Report for 12-Mar-18-10031 B105100A-FSWC-116CV 0.0" - 0.5" 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.970 6.46E+OO 2.12E+OO

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2564]

3/13/2018 9:19:27PM Page 4 of6 Analysis Report for 12-Mar-18-10031 B105100A-FSWC-116CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 9:19:23PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl/grams) (pCi/grams) (pCi/grams)

An Pk 511.00 100.00 3 .20E-01 2 .9'7E-01 2.97E-01 BE- 7 477.60 10.44 -3 .63E-01 1.60E+OO 1.60E+OO

+ K-40 1 460.82

10.66 6.46E+OO 2 .04E+00 2.04E+OO Co-60 1173. 2 3 99.85 -9.82E-03 2 .30E-01 2.73E-01 1332 .49 99.98 5.81E-0 2 2.30E-01 Nb-94 702.65 99.81 -7.47E-0 3 1.91E-01 2.0lE-01 87 1 .09 99.89 6.22E-02 1.91E-01 Ag-108rn 79.13 6.60 2.78E-01 1. 79E - 01 3.38E+OO 433.94 90.50 2 .53E-02 1.79E-01 614. 2 8 89.80 -3 .77E-02 2.44E-01 722 .94 90.80 1.89E-01 2.51E-01 Sb-125 176. 3 1 6.84 8.03E-01 4.83E-01 2.24E+OO 380.45 1. 5 2 2.40E+OO 9.26E+OO 427.87 2 9.60 1. 54E-02 4.83E-01 463.36 10.49 3 .14E-02 1.68E+OO 600.60 17.65 -3 .61E-01 1. 02E+OO 606.71 4.98 3 . 72E+OO 5.18E+OO 635.95 11. 22 - 1. 1 5E-01 1.64E+OO 671.44 1. 79 5.57E-01 9.47E+OO

[2565]

3/13/2018 9:19:27PM Page 5 of6 Analysis Report for 12-Mar-18-10031 B105100A-FSWC-116CV 0.0" -0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCi!grams) (pCl/grams)

(keV)

Ba-133 79.61 2.65 -2.84E+OO 2 .84E-01 -:'.48E+00

81. 00 32.90 -5.61E-01 5.37E-01 276.40 7.16 -4.17E-02 2 .24E+OO 302.85 18.34 -2 .03E-01 7.71E-01 356.01 62.05 -1.33E-01 2 .84E-01 38 3 .85 8.94 -3 .42E-01 1.55E+OO Cs-134 475.36 1. 48 6.03E-01 2 . llE-01 1. llE+Ol 563.25 8.34 -5.20E-01 1. 58E+OO 569.33 15.37 -3.38E-01 1. 08E+OO 604. 72 97.6 2 -6.57E-02 2 .23E-01 795.86 85.46 1.93E-02 2 . llE-01 801.95 8.69 -4.76E-01 1. 95E+OO 1038.61 0.99 7.59E+OO 2 . llE+Ol 1167.97 1. 79 3.08E+OO 1. 59E+Ol 1365. 1 9 3.0 2 -7.46E-01 5.64E+OO Cs-137 661.66 85.10 2 . 3 6E-01 2 .82E-01 2 .82E-01 Eu-1 52 121. 78 2 8.67 -7.53E-02 4.31E-01 4.31E-01 244.70 7.61 5.42E-01 2 .32E+OO 295.94 0.45 5. 72E+OO 3.59E+Ol 344.28 26.60 -6.89E-03 6.52E-01 367.79 0.86 -4.73E-01 1.53E+Ol 411.1"2 2 . 24 2 .82E+OO 8.03E+OO 443. 96 2 .83 2 . 72E+OO 5.18E+OO 488.68 0.42 -l.15E+Ol 4.15E+01 563.99 0.49 -6.12E+00 2.78E+O l 586.26 0.46 - 2 .52E+Ol 3.25E+01 678.62 0.47 -1.63E+Ol 3.08E+Ol 688.67 0.86 -3.28E+OO 2. llE+Ol 719.35 0.28 -2.07E+Ol 6.70E+Ol 778.90 12.96 -4.54E-01 1. 41E+OO 810.45 0.3 2 1. 2 5E+Ol 6.47E+Ol 867.37 4. 2 6 - 1. 72E+OO 4.04E+OO 919. 33 0.43 1.39E+Ol 5.66E+Ol 964.08 14.65 7.69E-02 1. 60E+OO 1085.87 10.24 1.32E+OO 2 .23E+OO 1089.74 1. 73 8.63E+OO 1.28E+Ol 1112. 07 13. 69 4.24E-01 1.74E+OO 1 212 .95 1. 43 5.02E+OO 1. 57E+Ol 1 249.94 0.19 5.00E+Ol 1.44E+02 1299.14 1. 63 -3.69E+OO l. 2 2E+Ol 1408.01 21. 07 9. llE-03 8. 2 6E-01 1457.64 0.50 -2 .62E+Ol 1.10E+0 2 1528.10 0. 2 8 2 .08E+OO 7.56E+Ol Eu-154 1 23 .07 40.40 5 . 34E-02 3 . 2 2E-01 3.22E-01 247.93 6.89 1.13E-01 2 .14E+OO 591.76 4.95 4.48E-01 3.29E+OO 692.42 1. 78 2 .02E+OO l.lOE+Ol 723. 30 2 0.06 5.71E-Ol l.lOE+OO 756.80 4.52 - 1.75E+OO 3.03E+OO 873.18 12.08 6.85E-01 1. 54E+OO 996. 2 9 10*. 48 8. 2 6E-01 2 .12E+OO

[2566]

3/13/2018 9:19:27PM Page 6 of6 Analysis Report for 12-Mar-18-10031 8105100A-FSWC-116CV 0.0" -0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCUgrams) (pC//grams)

(keV)

Eu-154 1004.76 18.01 5.46E-01 3. 2 2E-01 1.24E+OO 1274.4 3 3 4.80 -3.50E-01 5.88E-01 1596.48 1. 80 - 9.18E+OO 9.85E+0()

Eu-155 45.30 1. 31 - 1. 2 6E+Ol 5.32E-01 2 .83E+Ol 60 .01 1. 22 -8.47E+OO 3 . 3 GE+Ol 86.55 30.70 -3 .24E-02 5.32E-01 105.31 21.10 - 2 .38E-01 6.28E-01 Ra-226 186.21 3.64 1. 2 9E+OO 4.24E+OO 4.24E+OO Pa-231 2 7.36 10.30 2 .49E+OO 3.73E+OO 3.73E+00 283.69 1. 70 2 .73E-01 8.94E+OO 300.07 2 .47 -5.30E+OO 5.41E+OO 302.65 2 .20 -1.69E+OO 6 . 42E+OO 330. 0 6 1. 40 -5.21E-01 1.18E+Ol U- 235 143.76 10. 96 l.02E-0 2 2 . 72E-01 1.26E+OO 163.33 5.08 -5.08E-01 2 .84E+OO 185.71 57.20 1.09E-01 2 .72E-01 202 .11 1. 08 4.95E+OO 1. 44E+Ol 205.31 5.01 1.23E+DO 3 . 2 7E+OO Am-241 59.54 35.90 1. 79E-01 1 .22E+ OO 1. 2 2E+00

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2567]

0000024309.CNF Live Time :1200.000 sec Real Time :1201.610 sec Start: 1: O.l(kev)

Stop : 4096:2047.l(kev)

Acq. start :Tue Mar 13 17:09:01 2018

[2568]

500 1000 1500 2000 2500 3000 3500 4000 Channel

~

ROI Type: 1

3/13/2018 5:51 :03PM Page 1 of6 Analysis Report for 13-Mar-18-10012 B105100A-FSWC-150CV o.o* - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10012 Sample Description : B105100A-FSWC-150CV 0.0" -0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 9. 799E+01 grams Facility : Default Sample Taken On : 3/9/2018 3:30:00PM Acquisition Started : 3/13/2018 5:30:57PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.03 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24300 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 5:51 :OOPM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2569]

3/13/2018 5:51:03PM Page 2 of6 Analysis Report for 13-Mar-18-10012 B 1051 OOA-FSWC-150CV 0.0" -0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 351.98 1 403 - 1413 1406.92 1.70E+Ol 16 . 67 4.20E+Ol 1. 07 2 661.52 2 635 - 2653 2 643.97 4.24E+02 41.97 9.50E+OO 1. 33 3 1460.34 5834 - 5845 5839.30 1. 80E+Ol 11. 51 1. 20E+Ol 0.77 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA T/ON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 4 0 0. 96 1460.82

10 .66 2 .53E+OO 1.63E+00 Cs- 1 3 7 0.99 661.66

85.1 0 4. 2 1E+OO 6.55E-01 Bi-2 11 0.87 35 1 .07

13 . 02 6.77E-01 6.73E-01 Pb-2 14 1. 00 2 41.99 7 .25 2 95.22 1 8 .4 2 351.93

3 5.6 0 2 .48E-0 1 2. 46E-01 785.96 1. 06

= Energy line found in the spectrum .

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2570]

3/13/2018 5:51 :03PM Page 3 of6 Analysis Report for 13-Mar-18-10012 B105100A-FSWC-150CV 0.0" - 0.5" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.964 2.53E+OO 1.63E+OO Cs-137 0.997 4.21E+OO 6.55E-01

? Bi-211 0.876 6.77E-01 6.73E-Ol

? Pb-214 1. 000 2.48E-01 2 .46E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2571]

3/13/2018 5:51 :03PM Page 4 of6 Analysis Report for 13-Mar-18-10012 8 105100A-FSWC-150CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 5:51 :OOPM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCilgrams)

(keV)

An Pk 511. 00 100.00 2 .43E-01 2. 90E-01 2.90E-01 BE-7 477.60 10.44 7.15E-01 2 .33E+OO 2.33E+OO

+ K-40 1 460.82

10.66 2 .53E+OO 2 .26E+OO 2 .26E+OO Co-6 0 1173.23 99.85 1.27E-01 1.89E-01 2.29E-0 1 1332.49 99.98 -8.73E-0 2 1. 89E-0 1 Nb-94 70 2 .65 99.81 2 .38E-02 1. 2 9E-01 1 .78E-01 871. 09 99.89 -3 .03E-02 1.29E-Ol Ag-1 0 8m 79. 1 3 6.60 1.87E+OO 1. 71E-01 3 .lOE+OO 433.94 90.50 -7.09E-02 2 .29E-01 614. 2 8 89.80 -6.54E-02 2. 30E-01 722 .94 90.80 8.93E-02 1 . 71E-01 Sb-125 176.31 6.84 3.85E-03 6. 72E - 01 1 . 52E+OO 380.45 1. 52 -8.27E+OO 1.20E+Ol 427.87 2 9.60 -3.56E-01 6.72E-01 463.36 10.49 1. 54E-02 2 .13E+00 60 0 .60 17. 65 -l.12E-02 9.00E-01 606.71 4.98 3.90E+OO 4.71E+OO 635.95 11. 22 6.71E-01 1 . 48E+OO 671. 44 1. 79 -6.45E+OO 6.99E+OO

[2572]

3/13/2018 5:51:03PM Page 5 of6 Analysis Report for 13-Mar-18-10012 B1051 OOA-FSWC-150CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCilgrams) (pCilgrams)

(keV)

Ba-133 79.61 2 .65 l.30E+OO 2 .93E-01 7.31E+OO

81. 00 32 .90 -6.62E-01 4.86E-01 2 76.40 7.16 -9.39E-01 1.79E+OO 302.85 18.34 -8.03E-02 8.77E-01 356.01 62 .05 3.37E-02 2 .93E-01 383.85 8.94 -2 .51E-01 2 .02E+OO Cs-134 475.36 1. 48 2 . 2 8E+OO 2 .06E-01 1. 59E+Ol 563. 2 5 8.34 7.23E-01 2.04E+OO 569.33 15.37 8.07E-01 1. 37E+OO 604. 72 97.6 2 -1.06E-01 2 .06E-01 795.86 85.46 1. 25E-01 2.13E-01 801.95 8.69 - 2 . 2 2E+OO 1.64E+OO 1038.61 0.99 -3.84E+OO 1.94E+Ol 1167. 97 1. 79 5.09E+OO 1. 28E+Ol 1365.19 3 .02 2 .35E+OO 6.40E+OO

+ Cs- 137 661.66

85.10 4.21E+OO 1. 64E-0 1 l.64E-01 Eu-152 121. 7 8 2 8.67 l.66E-01 3.43E-01 3.43E-01 244.70 7.61 1. llE-01 1. 87E+OO 295.94 0.45 1. 25E+Ol 3 .84E+Ol 344. 2 8 2 6.60 - 2 .80E-01 5.42E-01 367.79 0.86 1.1 7E+OO 2 .09E+Ol 411.12 2 .24 -2 . 71E+OO 8.30E+OO 443. 96 2 .83 -8.15E-01 6. 96E+00 488.68 0.42 6.0lE+OO 4.72E+Ol 563.99 0.49 -9.58E+OO 3 .45E+Ol 586.26 0.4 6 3.69E+Ol 4. 2 6E+Ol 678.62 0.47 1.46E+Ol 3.00E+Ol 688.67 0.86 7.09E-Ol 1.83E+Ol 719.35 0. 2 8 1.93E+Ol 4.71E+Ol 778.90 1 2 .96 -6.24E-02 9.98E-01 810.45 0.32 -7.62E-01 5.50E+Ol 867.37 4. 2 6 -1. 2 7E+OO 3 . 2 8E+OO 919.33 0.43 2 .0lE+Ol 4.12E+Ol 964.08 14.65 -1.58E-01 1. 58E+OO 1085.87 10.2 4 1.17E+OO 2 .12E+00 1089.74 1. 73 6. 96E+OO 1.26E+Ol 111 2 .07 13. 69 8.92E-Ol 1.61E+OO 1212.95 1. 43 - 2 .73E+OO 1. 2 4E+Ol 1249.94 0.19 -9.89E+Ol 1. 02E+02 1 299.14 1. 63 4.18E+OO l.14E+Ol 1408.01 21.07 9.91E-02 1.13E+OO 1457.64 0.50 9.23E+Ol 8.81E+Ol 1528.10 0.28 2 .21E+Ol 6.90E+Ol Eu-154 123.07 40.40 2 .30E-02 2 . 3'7E-0 1 2.37E-01 247.93 6.89 -6.19E-01 1 . 86E+OO 591.76 4.95 2 .16E-01 3.06E+OO 692.42 1. 78 -8.80E+OO 7.65E+OO 723. 30 20.06 4.05E-01 7.76E-01 756.80 4.52 -1.49E+OO 3 .56E+OO 873.18 1 2 .08 3.42E-01 1.07E+OO 996. 2 9 10.48 -6.85E-01 1. 87E+OO

[2573]

3/13/2018 5:51:03PM Page 6 of6 Analysis Report for 13-Mar-18-10012 B1051 OOA-FSWC-150CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi!grams) (pCi!grams)

(keV)

Eu-154 1004.76 18.01 -4.04E-01 2.37E-01 9.26E-01 1274.43 34.80 7 . 71E-02 3.73E-01 1596.48 1. 80 -l.71E+OO 1. 2 3E+Ol Eu-155 45.30 1. 31 5.40E+OO 5.42E-01 3 .06E+Ol 60.01 1. 22 -1.53E+Ol 3. 2 1E+Ol 86.55 30.70 7.83E-0 2 5.42E-01 105.31 2 1.10 -1.20E-01 5.SOE-01 Ra-226 186. 2 1 3.64 1.95E+OO 3.52E+OO 3.52E+OO Pa-23 1 27.36 10.30 1.48E+OO 3.58E+OO 3.58E+OO 283.69 1. 70 2 .33E-01 8.32E+OO 300.07 2 .47 -5.21E+OO 6. 2 6E+OO 30 2 .65 2 .20 -3.02E+OO 7.07E+OO 330.06 1. 40 4.68E+OO 1.16E+Ol U-235 143.76 10.96 -3.22E-Ol 2 .22E-01 8.88E-01 163.33 5.08 -3.12E-01 1.88E+OO 185.71 57.20 2.84E-02 2.22E-01 202.11 1. 08 5.70E-01 1.09E+Ol 205.31 5.01 1.13E-01 2 .56E+OO Am-241 59.54 35 .90 -4.15E-01 l.lOE+OO l.lOE+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? -* C/\UT!ON: MDA value is inconsistent with Currie MDA at 95% confidence level

[2574]

0000024300.CNF Live Tille :1200.000 sec 120 Real Tille :1200.310 sec start: 1: -0.0(kev)

Stop : 8192: 2047. 8(kev)

Acq. start :Tue Mar 13 17: 30: 57 2018 110 100 90 II)

+-'

s:::::

0 u

[2575]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/13/2018 7:08:35PM Page I of6

~~~pex-Gamma Analysis Report for 13-Mar-18-10013 B105100A-FSWC-150CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10013 Sample Description : B105100A-FSWC-150CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 9. 799E+01 grams Facility : Default Sample Taken On : 3/9/2018 3:30:00PM Acquisition Started : 3/13/2018 6:48:29PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time ; 1200.0 seconds Real Time : 1200.3 seconds Dead Time ; 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24302 Certificate Name : Eu 155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 7:08:31PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2576]

3/13/2018 7:08 :35PM Page 2 of6 Analysis Report for 13-Mar-18-10013 B 1051 OOA-FSWC-150CV 0.0" - 0.5" 0.5~

Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 609.09 2 430 - 2 439 2434.41 1. 50E+Ol 11. 87 l.60E+01 0.69 2 661.47 2 636 - 2 651 2643.76 3 .01E+0 2 35.72 l.19E+Ol 1. 37 3 1460.24 5833 - 5844 5838.89 3.70E+Ol 14.42 1. 20E+Ol 0.48 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.94 1460.82

10 .66 5.20E+OO 2 .08E+OO Cs-137 0.99 661.66

85.10 2 .99E+OO 5.04E-01 Bi-2 14 0.99 609.32

45.49 2 .62E-01 2 .09E-01 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120. 2 9 14.92 1155. 2 1 1. 63 1 2 38.12 5.83 1 2 8 0 .98 1. 43 1 3 77.67 3.99 1 3 85.3 1 0.79 1401.52 1. 33 1407.99 2 .39 1509. 2 1 2 .13 1661. 2 7 1. 05

[2577]

3/13/2018 7:08:35PM Page 3 of6 Analysis Report for 13-Mar-18-10013 B 1051 OOA-FSWC-150CV O.O" - 0.5" 0.5" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi-214 0.99 1729.59 2.88 1 764.49 15.30 1 847.43 2 .03 2118.51 1.16

*= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.947 5.20E+OO 2 .08E+OO Cs-137 0.994 2 .99E+OO 5 . 04E-01 Bi-214 0.997 2 .62E-01 2 .09E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2578]

3/13/2018 7:08:35PM Page 4 of6 Analysis Report for 13-Mar-18-10013 B105100A-FSWC-150CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS

-Peak Locate Performed on : 3/13/2018 7:08:31PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LlneMDA Name (pCi!grams) (pCi/grams) (pCi/grams)

(keV)

An Pk 511 . 00 100.00 1.14E-01 2.59E-01 2.59E-01 BE-7 477.60 10.44 3.61E-01 2.05E+00 2 .05E+OO

+ K-40 1460.82

10.66 5. 2 0E+OO 2.25E+OO 2 . 2 5E+OO Co-60 1173. 2 3 99.85 -1.07E-01 2.16E-01 2 . 2 9E-01 1332 .49 99.98 9.70E-02 2 .16E-01 Nb-94 702.65 99.81 - 2 .50E-02 1.29E-01 1. 2 9E-01 871.09 99.89 -9.89E-0 3 1.51E-01 Ag-108m 79.13 6.60 2.45E+OO 2. 0'E-01 3 .15E+OO 433.94 90.50 -1.60E-02 2.2 9E-01 614.28 89.80 -1.61E-01 2 .30E-01 722 . 94 90.80 1.63E-02 2.07E-01 Sb-125 176.31 6.84 7.62E-01 6.88E-01 1.72E+00 380.45 1. 52 -1.54E+Ol 9.79E+OO 427.87 29.60 -1.44E-01 6.88E-01 463.36 10.49 -2 .40E-02 2 .02E+OO 600.60 17.65 1.12E-01 1. llE+OO 606.71 4.98 2 .15E+OO 5.29E+OO 635.95 11. 22 1.lOE-01 1.82E+OO 671. 44 1. 79 2 .62E+OO 8.63E+OO

[2579]

3/13/2018 7:08:35PM Page 5 of6 Analysis Report for 13-Mar-18-10013 B 105100A-FSWC-150CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCi/grams)

(keV)

Ba-133 79.61 2.65 6.58E+OO 2 .77E-01 7.66E+OO

81. 00 32.90 -5.75E-01 5.05E-01 276.40 7.16 9. 2 8E-01 1.86E+OO 302.85 18.34 -4.42E-01 6.91E-01 356.01 62.05 -5.44E-01 2 .77E-01 383.85 8.94 2 .63E-02 1. 78E+OO Cs-134 475.36 1. 48 -6 .37E+00 2 .13E-01 1.37E+Ol 563.25 8.34 l.12E+OO 2 .19E+OO 569.33 15.37 2 .04E-01 9.93E-01 604. 72 97.6 2 -2 .40E-01 2 .47E-01 795.86 85.46 2 .83E-02 2.13E-01 801. 95 8.69 -1.40E+OO 1 .84E+OO 10 3 8.61 0.99 -1.66E+Ol 2 .04E+Ol 1167. 97 1. 79 2 .91E+OO 1. 22E+Ol 1365.19 3.0 2 -4. 23E-01 6.40E+OO

+ Cs- 137 661.66

85.10 2. 99E+OO 1. 71E-01 l.71E-01 Eu-152 12 1. 78 2 8 . 67 -1.58E-01 3.65E-01 3 .65E-01 244.70 7.61 3 . 3 6E-01 1 .76E+OO 295.94 0.45 l.56E+Ol 3.78E+Ol 344. 2 8 2 6.60 -3.76E-03 6.15E-01 367.79 0.86 -3.66E+OO 1.79E+Ol 411.12 2 .24 2.69E+OO 8.61E+OO 443. 96 2 .83 l.68E+OO 6. 96E+OO 488.68 0.42 3.56E+Ol 4.44E+Ol 563.99 0.49 -7.62E-01 3.54E+Ol 586. 2 6 0.4 6 l.52E+Ol 4.89E+Ol 678. 62 0.47 -6.98E+OO 3 . 2 9E+Ol 688.67 0.86 -9.73E+OO 1.75E+Ol 719.35 0. 2 8 2.41E+OO 6.05E+Ol 778.90 12. 96 1.78E-01 1.14E+OO 810.45 0.32 -3.81E+OO 5.26E+Ol 867.37 4. 2 6 l.93E+OO 3.97E+00 919.33 0.43 -3.64E+Ol 3.90E+Ol 964.08 14.65 7.30E-0 1 1. 71E+OO 1085.87 10.24 - 9. 2 4E-01 1. 93E+OO 1089.74 1. 7 3 3 .57E+OO 1.26E+Ol 1112 . 07 13. 69 8.92E-02 1.47E+OO 1 2 12.95 1. 43 -l.89E-01 1.33E+Ol 1249.94 0.19 5.60E+Ol 1.15E+0 2 1299.14 1. 63 2 .51E+OO 9.36E+OO 1408.01 21. 07 3 .45E-01 9.38E-01 1457.64 0.50 1 .52E+0 2 1.11E+02 1 528.10 0 . 28 2 . 21E+Ol 6.90E+Ol Eu-154 1 23 .07 40.40 6.32E-02 2 .89E-01 2. 89E-01 2 47.93 6.89 2 .07E-01 2 .07E+OO 591.76 4.95 l.45E+OO 3.65E+00 692.42 1. 78 1.98E+00 8.49E+OO 723. 30 20.06 9.63E-02 9.36E-01 756.80 4 .52 9.79E-01 4.42E+OO 873.18 12. 08 -5.35E-01 1.16E+OO 996. 2 9 10 . 48 7.06E-01 2 .03E+OO

[2580]

3/13/2018 7:08:35PM Page 6 of6 Analysis Report for 13-Mar-18-10013 B1051 OOA-FSWC-150CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCi/grams) (pCi!grams) (pCUgrams)

(keV)

Eu-1 5 4 1004 . 76 18.01 -8.64E-03 2 .89 E- 0 1 1. 19E+OO 1274.43 34.80 3.37E-02 5.64E-01 1596.48 1. 80 9.0lE-01 6.92E+OO Eu-155 45.30 1. 31 -2.44E+OO 4.99E-01 2.86E+Ol 60 . 01 1. 22 1. 2 0E+Ol 3.44E+Ol 86.55 30."70 -1. 2 7E-01 4.99E-01 1 05.3 1 21.10 -7.63E-02 5.82E-01 Ra-226 1 86. 2 1 3.64 -1.84E+OO 3. 2 1E+OO 3.21E+OO Pa-2 31 27. 3 6 10. 3 0 2 .93E +OO 4.43E+OO 4.4 3 E+OO 283.69 1. 70 -3.81E+OO 8.71E+00 300.07 2 .47 -2 . 72E+OO 5.43E+OO 302.65 2 . 20 -3.52E+OO 5.75E+OO 330.06 1. 40 -6.22E+OO 1 .0lE+O l U- 235 143.76 10. 96 -2.98E-01 2.06E-01 1.06E+OO 163.33 5.08 -1 . 34E-01 1.98E+OO 185.71 57.20 1. 63E-02 2 .06E-01 202 .11 1. 08 - 3. 09E+OO 1 . 03E+Ol 205.31 5.01 -1.33E+OO 2. 28E+OO Am-241 59.54 35.90 - 9 .22 E-02 1.17E+OO 1.17E+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2581]

0000024302.CNF Live Ti11e :1200.000 sec 60 Real Tille :1200.280 sec Start: 1: -0.0(kev)

Stop : 8192: 2047 . S(kev)

Acq. start :Tue Mar 13 18:48:29 2018 55 50 45

[2582]

1000 2000 3000 4000 5000 6000 7000 8000 Channel

~

ROI Type: 1

3/13/2018 7:30:30PM Page 1 of6 Analysis Report for 13-Mar-18-10014 B105100A-FSWC-151CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10014 Sample Description : B105100A-FSWC-151CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.026E+02 grams Facility : Default Sample Taken On : 3/9/2018 3:20:00PM Acquisition Started : 3/13/2018 7:10:21PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1203.4 seconds Dead Time : 0.28%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24303 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 7:30:26PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2583]

3/13/2018 7:30:30PM Page 2 of6 Analysis Report for 13-Mar-18-10014 B 1051 OOA-FSWC-151 CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 661.79 1317 - 1328 1323 .12 3.36E+0 4 370.15 4.82E+02 1. 48 2 871.16 1737 - 1748 1:41.78 7.63E+Ol 38.38 2 .33E+02 0.84 3 1173.55 2340 - 2353 2346.73 2 .25E+03 99.16 1.49E+02 1. 73 4 1332.84 2658 - 2672 2665.49 1.99E+03 91.68 7.84E+Ol 1.99 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Co-60 0.98 1173. 23

99.85 2 .43E+Ol 2 . 2 2E+OO 13 32 .49

99.98 2 .34E+Ol 2 .16E+OO Cs-137 0.99 661.66

85.10 2.88E+02 3.48E+Ol

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2584]

3/13/2018 7:30 :30PM Page 3 of6 Analysis Report for 13-Mar-18-10014 B105100A-FSWC-151CV 0.0" - 0.5" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

Co-60 0.982 2.39E+Ol 1. SSE+OO Cs-137 0.997 2.88E+02 3.48E+Ol

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2585]

3/13/2018 7:30:30PM Page 4 of6 Analysis Report for 13-Mar-18-10014 B105100A-FSWC-151CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 7:30:26PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide 2 871.16 6.36054E-02 25.14 Tol.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

An Pk 511. 00 1 00.00 2 .99E-01 1.03E+OO 1. 03E+OO BE-7 477.60 10.44 1 .42E+00 1.17E+Ol l.17E+Ol K-40 1 460.82 10.66 2. 46E+OO 4.57E+OO 4.57E+OO

+ Co-60 1 173. 23

99.85 2 .43E+Ol 4.57E-0 1 5.55E-01 1 332. 49

99 . 98 2.34E+Ol 4.57E-01 Nb-94 702.65 99.8 1 5.63E-01 5.86E - 01 5.86E-01 871.09 99.89 7.02E-01 7.20E-01 Ag-108m 79 .13 6.60 4.53E+OO 5.28E-01 l.16E+Ol 433.94 90.50 -3.20E-01 1 . 2 2E+OO 614.28 89.80 -3.26E-01 8. 3 7E-01 72 2 . 94 90.8 0 - 2 .88E-02 5. 2 8E-01 Sb-125 176.31 6 . 84 -2. 32E+OO 3 .7 1E+OO 8.14E+OO 380.45 1. 52 3.92E+Ol 6.21E+Ol 427.87 2 9.60 1.85E+OO 3 .71E+OO 463.36 10 . 49 2.28E+OO 1. 2 0E+Ol 600.60 17.65 -2. 98E+OO 4.15E+OO 606.71 4.98 - 2 .38E+OO 1.53E+O l

[2586]

3/13/2018 7:30:30PM Page 5 of6 Analysis Report for 13-Mar-18-10014 B 105100A-FSWC-151 CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA Line*MDA Name (pCilgrams) (pCl!grams) (pCi/grams)

(keV) f:b-12 5 635.95 11. 22 -4. 50E+OO 3.71E+OO 6.26E+OO 671. 4 4 1. 79 -1.64E+Ol 2 .69E+Ol Ba-13 3 79.61 2 .65 1.82E+Ol 1. 41E+OO 2 .86E+Ol

81. 00 32 .90 -8. 52E-01 2 .13E+OO 276.40 7.16 1.36E+OO 9. 83E+OO 302.85 18.34 6 . 03E-02 3. 96E+OO 356.01 62 .0 5 1.08E-01 1.41E+OO 38 3 .85 8.94 -1.85E+OO 1.04E+Ol Cs-134 475.36 1. 48 5.57E+Ol 6.34E-01 8.23E+Ol 563.25 8 . 34 4.52E+OO 8.94E+OO 569.33 15.37 - 5.99E-01 4.67E+OO 604.72 97. 62 1. llE-01 7.76E-01 795.86 85.46 2.91E-01 6.34E-01 801. 95 8.69 -1.14E+OO 6.0SE+OO 1038.61 0.99 2 .48E+Ol 7.25E+Ol 1167.97 1. 79 -4. 2 7E+Ol 9.80E+Ol 1365.19 3.0 2 4.42E+OO 1. 2 3E+Ol

+ Cs-137 661.66

85.10 2 .88E+02 7.41E-01 7.41E-Ol Eu-152 121.78 2 8.67 2 .38E-01 1. 59E+OO 1.59E+OO 2 44.70 7.6 1 -3 .41E+OO 8.93E+00 2 95.94 0.4 5 7.68E+O l 1.62E+02 3 44. 2 8 26.60 6.77E-0 1 3.17E+OO 3 67.79 0.86 4.74E+Ol 1.04E+0 2 411.12 2 .24 2.24E+Ol 4.60E+Ol 443.96 2 .83 -1 . 33E+O l 4.06E+O l 488.68 0.42 -5.31E+Ol 2 . 5 0E+02 563.99 0.49 5.68E+Ol 1. 51E+02 586. 2 6 0.46 -4.14E+Ol 1.62E+02 678.62 0.47 2 .17E+Ol 9.85E+Ol 688.67 0.86 5.52E+OO 5.45E+O l 719. 35 0.28 4.06E+OO 1. 72E+02 778.90 12. 96 1.32E+OO 4.33E+OO 810 . 45 0.32 -1.32E+02 1 .77E+02 867.37 4.26 -1.61E+OO 1.61E+Ol 919.33 0.43 1 .77E+Ol 1.75E+02 964.08 14.65 2 .21E+OO 5.49E+OO 1085.87 10.24 -l .13E+OO 7 .2 0E+OO 1089.74 1. 73 2 .07E+Ol 4 . 43E+Ol 1112. 0 7 1 3.69 -7.22E-Ol 5. llE+OO 1 212.95 1. 43 1.39E+Ol 3.54E+Ol 1249.94 0.19 5.48E+Ol 2 .06E+02 1299.14 1. 63 1.08E+OO 2. 33E+Ol 1408.01 21. 07 4.23E-0 1 1.60E+OO 1457.64 0.50 l. 1 9E+02 1.01E+0 2 15 2 8.10 0. 2 8 -3 .73E+Ol 1.06E+02 Eu-154 123. 0 7 40.40 3.50E-02 1. 02E+00 1 . 13E+OO 247.93 6.89 -2 .38E+OO 9.86E+OO 591.76 4.95 l.78E+OO 1. 51E+Ol 692.42 1. 78 -1.66E+OO 2 .57E+Ol 723.30 2 0.06 -2 .00E-01 2. 42E+OO 756.80 4.52 - 1.49E+OO l.18E+O l

[2587]

3/13/2018 7:30:30PM Page 6 of6 Analysis Report for 13-Mar-18-10014 81051 OOA-FSWC-151 CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCUgrams) (pCUgrams) (pCi!grams)

(keV)

Eu-154 873.18 1 2 .08 3 .59E+OO 1 . 02E+OO 5 .92E+OO 996.29 10.48 1.0lE+OO 6.77E+00 1004.76 18.01 9.42E-01 4.08E+00 1274.43 34.80 -5 .21E-01 l . 02E+OO 1596.48 1. 80 -3 .62E+OO 2 . ~5E+Ol Eu-155 45.30 1. 31 2 .46E+O l 1 . 9'";'E+00 1. 3 7E+02 60.01 1. 22 l.08E+02 1.44E+02 86.55 30.70 7.25E-01 1.97E+OO 105.31 21.10 - 1.17E-01 2 . 3 9E+OO Ra-22 6 186. 2 1 3.64 1.09E+Ol l.76E+Ol 1.76E+Ol Pa-231 2 7.36 10.30 3 .59E+O l 1.43E+Ol 1.43E+Ol 2 83.69 1. 70 -l.08E+Ol 4.14E+Ol 300.07 2 .47 6.88E-Ol 2 . 94E+Ol 302.65 2 . 20 5.02E-01 3 . 3 0E+Ol 330.06 1. 40 -1.30E+Ol 5.88E+Ol U-235 143.76 10. 96 -4.90E-01 1 . llE+OO 4.04E+OO 163.33 5.08 2 .25E+00 l.05E+Ol 185.71 57.20 1. 25E+OO l.llE+OO 202.11 1. 0 8 2 .37E+OO 6.20E+Ol 205.31 5.01 3 .17E+OO 1. 34E+Ol Am-241 59.54 35.90 3 .21E+OO 5.05E+OO 5.05E+OO

+ = Nuclide identified during the nuclide identification

= Energy iine found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2588]

0000024303.CNF Live Time :1200.000 sec Real Time :1203.410 sec 15000 start : 1: O.l(kev) stop : 4096: 2047. l(kev)

Acq. Start :Tue Mar 13 19:10:21 2018 12500 10000 V)

~

s::::

s 8 7500

[2589]

5000 2500 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/13/2018 7:54:55PM Page 1 of6

~~~pex-Gamma Analysis Report for 13-Mar-18-10015 8105100A-FSWC-151CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10015 Sample Description : 8105100A-FSWC-151CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.026E+02 grams Facility : Default Sample Taken On : 3/9/2018 3:20:00PM Acquisition Started : 3/13/2018 7:34:46PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1203.0 seconds Dead Time : 0.25%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24305 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 7:54:51PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2590]

3/13/2018 7:54:55PM Page2 of6 Analysis Report for 13-Mar-18-10015 B 1051 OOA-FSWC-151 CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 661.7 9 1317 - 1328 1323 .11 2 .43E+04 314.83 3.49E+02 1. 49 2 1173.46 2340 - 2353 23116.52 1 . 25E+03 73.81 8.36E+Ol 1. 94 3 1332.79 2658 - 2672 2665.39 l.15E+03 69.04 2 .63E+Ol 1. 72 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Co-60 0.98 1173. 23 *!:

99.85 1.35E+Ol 1. 34E+OO 1332 .49

99.98 1.36E+Ol 1.36E+OO Cs-137 0.99 661 . 66

85. 1 0 2. 09E+02 2 .52E+Ol

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2591]

3/13/2018 7:54:55PM Page 3 of6 Analysis Report for 13-Mar-18-10015 B105100A-FSWC-151CV 0.0" - 0.5 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

Co-60 0.989 1.35E+Ol 9.53E-01 Cs-137 0.997 2.09E+02 2.52E+Ol

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2592]

3/13/2018 7:54 :55PM Page 4 of6 Analysis Report for 13-Mar-18-10015 8105100A-FSWC-151CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 7:54:51PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS {°A,) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCl!grams) (pCilgrams)

(keV)

An Pk 511. 00 100.00 1.06E-01 8.75E-01 8.75E-01 BE-7 477.60 10.44 8. 2 0E+OO 1. 03E+Ol 1.03E+Ol K-40 1 460.82 10.66 3 . 2 9E+OO 3.95E+OO 3 .95E+00

+ Co-60 11 73.23

99.85 1 . 35E+Ol 2 .80E - 01 4. 2 4E-01 13 32. 49

99.98 1.36E+Ol 2 .80E-01 Nb-94 702.65 99.81 3.79E-01 4.60E-01 4.60E-01 871.09 99.89 l.09E-01 5.32E-01 Ag-108m 79. 1 3 6.60 2 .24E+OO 4.38E-01 1. 02E+Ol 433.94 90.50 -3.05E-01 1.05E+OO 614. 2 8 89.80 2 .54E-01 7.40E-01 722. 94 90.80 -4.14E-02 4. 3 8E-01 Sb-125 176.31 6.84 1. 31E+OO 3. 21E+OO 7. 3 9E+OO 380.45 1. 52 -2 .89E+Ol 5. 2 9E+Ol 427.87 2 9.60 6. 2 6E-01 3.21E+OO 463.36 10 . 49 5.41E+OO 1.02E+Ol 600 . 60 17.65 1.lOE+OO 3.80E+OO 606.71 4.98 1.45E+OO 1 . 3 5E+Ol 635.95 11. 22 1.53E+OO 5.84E+OO 671.44 1. 79 - 1.82E+OO 2 . 3 9E+Ol

[2593]

3/13/2018 7:54:55PM Page 5 of6 Analysis Report for 13-Mar-18-10015 81051 OOA-FSWC-151 CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name * (pCilgrams) (pCilgrams) (pCi/grams)

(keV)

Ba-133 79.61 2 .65 4.02E+OO 1. 2 1E+OO 2 .50E+Ol

81. 00 32 .90 -1.17E+OO 1.86E+OO 276.40 7.16 - 2 .51E+OO 8.32E+OO 302.85 18.34 6.42E-01 3.55E+OO 356.01 62.05 -5.06E-01 1. 2 1E+OO 383.85 8.94 3 .12E+OO 9.15E+OO Cs-134 475.36 1.48 7.60E+Ol 4.95E-01 7.07E+Ol 563.25 8.34 3. 2 2E+OO 8.00E+OO 569.33 15.37 3.00E+OO 4.35E+OO 604. 72 97.62 -4.61E-01 6 . 70E-01 795.86 85.46 - 2 .99E-01 4.95E-01 801. 95 8.69 -5 .00E-01 5. ~ 7E+OO 1 038.61 0.99 8.24E+OO 5.60E+Ol 1167. 97 1. 79 - 2 .lOE+O l 7. 72E+Ol 1365. 1 9 3.0 2 9.92E-01 9.26E+OO

+ Cs-137 661. 66

85.10 2 .09E+02 6.34E-01 6.34E-01 Eu-1 52 121.78 28.67 -1.83E-01 1.39E+OO 1.39E+OO 244.70 7.6 1 -9.70E-01 7.64E+OO 295.94 0.45 - 2 .45E+Ol 1. 41E+02 344. 2 8 2 6.60 1. 04E+OO 2 .79E+00 367.79 0.86 2 .58E+OO 9.0lE+Ol 411.12 2 .24 -1.15E+Ol 3.89E+Ol 443. 96 2 .83 1 .99E+Ol 3.59E+Ol 488.68 0.42 5.25E+Ol 2 .15E+0 2 563.99 0.49 5.77E+Ol 1. 3 6E+02 586. 2 6 0.46 1.61E+Ol 1. 4 7E+02 678. 62 0.47 - 2 .12E+Ol 8.65E+Ol 688.67 0.86 -7.21E+OO 4.27E+Ol 719.35 0. 2 8 7.14E+Ol 1. 42E+02 778.90 12. 96 -6.18E-01 3.08E+OO 810.45 0.32 -5.65E+Ol 1.43E+02 867.37 4. 2 6 2.92E+OO 1. 2 4E+Ol 919.33 0.43 -2.20E+Ol 1. 3 7E+02 964.08 14.65 1. 40E-01 4.13E+OO 1085.87 10.24 -1. 72E+OO 5.49E+OO 1089.74 1. 73 1.49E+Ol 3.36E+Ol 111 2 .07 13. 69 7.09E-01 4.09E+OO 1212.95 1. 43 -1.02E+Ol 2 .35E+Ol 1249.94 0 .19 3.30E+Ol 1.76E+02 1299.14 1. 63 3.50E+OO 1.69E+Ol 1 408.01 21. 07 -l.83E-01 1.39E+OO 1457.64 0.50 1 .11E+02 8.73E+Ol 15.28. 10 0.28 5 . 72E+Ol 1.00E+0 2 Eu-154 123. 0: 40.40 5.75E-01 9.53E-01 1.00E+OO 2 47.93 6.89 1. 2 8E+OO 8.39E+OO 591. 76 4.95 2 .40E+OO 1.37E+Ol 692.42 1. 78 -9.43E+OO 2 .02E+Ol 7 23.30 20.06 4.53E-01 2 .02E+OO 756.80 4.52 2. 64E+OO 9.42E+OO 873. 1 8 12.08 2 .89E+OO 4.45E+OO 996. 2 9 10.48 7.34E-01 4.99E+OO

[2594]

3/13/2018 7:54:55PM Page 6 of6 Analysis Report for 13-Mar-18-10015 B1051 OOA-FSWC-151 CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCilgrams) (pCi/grams)

(keV)

Eu- 154 1004.76 18.01 -1.21E+OO 9.83E-01 2 .83E+OO 1274.43 34.80 -5.95E-01 9.83E-01 1596.48 1. 80 1.33E+OO 1. 2 5E+Ol Eu-155 45.30 1. 3 1 -5.68E+OO 1.74E+O O 1.17E+02 60.01 1. 2 2 -8.05E-0 2 1.22E+02 86.55 3 0.70 8.91E-01 1.74E+OO 105 . 31 2 1.10 8.96E-01 2 .09E+OO Ra-226 186. 2 1 3 .64 7.13E+OO 1. 52E+Ol 1.52E+Ol Pa-231 27.36 10.30 2 .66E+Ol 1. 21E+Ol 1. 2 1E+Ol 283.69 1. 70 1.93E+Ol 3. 71E+Ol 300.07 2 .47 -1.llE+Ol 2 .60E+Ol 302.65 2 .20 5.35E+OO 2 . 96E+Ol 330 . 06 1. 40 -1.31E+Ol 5. llE+Ol U-235 143.76 10 . 96 -2 .08E+OO 9.71E-01 3.49E+OO 163.33 5.08 1 .68E+OO 9.29E+OO 185.71 57. 2 0 8.81E-01 9. 71E-01 202 .11 1. 08 -2 .12E+OO 5.02E+Ol 205.31 5.01 1.07E+OO l .lOE+Ol Am-241 59.54 35.90 5.89E-01 4. 2 9E+OO 4.29E+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

,, = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2595]

0000024305.CNF 8000 Live Time :1200.000 sec Rea1 Time : 1202. 990 sec start: 1: O.l(kev)

Stop : 4096:2047.l(kev)

Acq. start :Tue Nar 13 19:34:46 2018 7000 6000 5000 V)

§ 0

4000 u

[2596]

3000 2000 1000 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/13/2018 8:53:32PM Page I of6

~pex-Gamma Analysis Report for 13-Mar-18-10017 B105100A-FSWC-156CV o.o* - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10017 Sample Description : B105100A-FSWC-156CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 9.647E+01 grams Facility : Default Sample Taken On : 3/9/2018 3:04:00PM Acquisition Started : 3/13/2018 8:11 :46PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 2400.0 seconds Real Time : 2403.3 seconds Dead Time : 0.14 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24307 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 8:53:28PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2597]

3/13/2018 8:53:32PM Page 2 of6 Analysis Report for 13-Mar-18-10017 B 1051 OOA-FSWC-156CV 0.0" -0.5" 0.5" Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238. 7 4 473 - 482 477.67 6.67E+Ol 41.98 3 .25E+02 0.99 2 295.21 588 - 5 9 "i 590.47 4.33E+Ol 25 .75 1. 20E+02 1.12 3 35 1 .91 698 - 70 8 703.77 6.57E+Ol 30.57 1 . 41E+02 1. 06 4 661.77 1 3 17 - 1328 132 3 . 07 8. 1 0E+02 60.15 7.52E+Ol 1. 44 5 1173. 2 6 2 340 - 2353 2 346.13 6.22E+01 19 . 44 2 .36E+Ol 1. 41 6 1332.47 2 659 - 2671 2 664 . 76 6.lOE+Ol 16 . 58 6.03E+OO 1. 43 7 1460.93 2917 - 2 92 9 2 921.91 1 .06E+02 22 .18 1. 30E+01 1. 76 M = First peak In a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigrna No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA T/ON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82

10 .66 6.67E+OO 1. 52E+OO Co-60 1. 00 1173.23

99.85 3.57E-01 1.15E-01 13 32 .49

99.98 3.81E-01 1 .08E-01 Cs-137 0.99 661.66

85.10 3.69E+OO 5. 22E - 01 Pb-21 2 0.99 11 5 .18 0.60 23 8.63

43.60 2 .80E-01 l.82E-01 3 00 .09 3.30 Pb-214 1. 00 2 41.99 7.25 2 95 .22 "* 18.42 4.96E-0 1 3.06E-0 1 351.93

35.60 4.47E-0 1 2.20E-01 785.96 1. 0 6

[2598]

3/13/2018 8:53:32PM Page 3 of6 Analysis Report for 13-Mar-18-10017 B105100A-FSWC-156CV 0.0" - 0.5" 0.5"

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.998 6.67E+OO 1.52E+OO Co-60 1. 000 3 .70E-01 7.88E-02 Cs-137 0.998 3 .69E+OO 5. 2 2E-01 X Bi-211 0.893 Pb-21 2 0.998 2 .80E-01 1. 82E-01 Pb-214 1. 000 4.64E-01 1.79E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2599]

3/13/2018 8:53:32PM Page 4 of6 Analysis Report for 13-Mar-18-10017 B105100A-FSWC-156CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 8:53:28PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCilgrams) (pCi/grams) (pCi/grams)

(keV)

An Pk 511. 00 100.00 3.60E-01 2 . 23E -01 2 .23E-01 BE-7 477.60 10.44 -3.96E-01 1 .50E+OO 1.50E+OO

+ K-40 1460.82

10.66 6.67E+OO 1.08E+OO 1. 08E+OO

+ Co-60 1173.23

99.85 3.57E-01 7.71E-02 l.27E-01 1 332. 4 9

99.98 3.81E-01 7.71E-02 Nb-94 702.65 99.81 2 .02E-03 1.1 6E-01 l.16E-01 871.09 99.89 -2 .93E-02 1 .35E-01 Ag-108m 79 .13 6.60 9.45E-01 l.57E - 01 2 .52E+OO 433.94 90.50 5.24E-0 2 1.57E-01 614.28 89.80 1.68E-0 2 1.78E-01 722 . 94 90.80 6.44E-02 l.59E-01 Sb - 1 2 5 1 76.31 6.84 1 . 05E+OO 4.85E-01 1.76E+OO 3 80.45 1. 52 -4.00E+OO 8. 2 8E+OO 427.87 2 9.60 2 .51E-01 4.85E-01 463.36 10.49 -6.15E-01 l.47E+00 600.60 17.65 -2 .09E-01 8.54E-01 606.71 4.98 2 .82E+OO 3.59E+OO 635.95 11. 22 5. 2 6E-01 1. 27E+00 671.44 1. 79 -3 . llE+OO 7.53E+OO

[2600]

3/13/2018 8:53:32PM Page 5 of6 Analysis Report for 13-Mar-18-10017 B1051 OOA-FSWC-156CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%)* Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCi/grams)

(keV)

Ba-133 79.61 2 .65 7.38E-01 2 .43E-0 1 5.93E+OO

81. 00 32 .9 0 -4.00E-01 4.02E-01 27 6.40 7.16 3.84E-01 1 .65E+OO 302.85 18.34 1.15E-01 6.12E-01 356. 0 1 62.05 -8.81E-0 2 2.43E-01 383.85 8.94 -3.85E-01 1.40E+OO Cs-1 3 4 475. 3 6 1. 48 -7.51E-01 1. 5:E-01 1.04E+Ol 563.25 8.34 -2 .59E-0 1 1.57E+OO 569.33 15.37 -1. 3 4E-01 9.02E-01 604. 72 97.6 2 -1.70E-01 1.62E-01 795.86 85.46 3.34E-02 1.57E-01 801.95 8.69 -3.20E-01 1. 49E+OO 1038.61 0.99 -6.80E+OO 1. 72E+O l 1167 . 97 1. 79 3.28E-01 1. 29E+Ol 1365 . 19 3 .0 2 -1.04E+OO 3.82E+OO

+ Cs- 137 661.66

85.10 3.69E+OO l .63E-0 1 1. 63E-01 Eu-15~ 121.78 2 8.67 -3 . 98E-02 3.18E-0 1 3.18E-01 244.70 7.61 -7.71E-02 1.65E+OO 295.94 0.45 3. 31E+OO 2 .83E+Ol 344. 2 8 2 6.60 1.07E-01 5.18E-01 367.79 0.86 -3.49E-01 1. 50E+Ol 411.12 2 . 24 7.98E-01 6.27E+OO 443. 96 2 .83 1.60E+OO 4.95E+OO 488.68 0.42 -3.57E-01 3.22E+Ol 563.99 0.49 5.65E+00 2 .80E+Ol 586. 2 6 0.46 2 .47E+01 3.33E+01 678.62 0.47 6.94E+OO 2 .87E+Ol 688.67 0.86 - 1 .38E+Ol 1.37E+Ol 719.35 0.28 2.21E+OO 4.89E+Ol 778.90 12. 96 -4.19E-01 9.91E-01 810.45 0.32 8.22E+OO 4.51E+01 867.37 4.26 -1.65E+OO 2. 84E+OO 91 9.33 0.43 5.27E+OO 3.70E+Ol 964. 0 8 14.65 -2.53E-0 2 1.07E+OO 1085.87 10.2 4 -2.55E-01 1.48E+OO 1089.74 1. 73 4.33E+OO 9 . 32E+OO 1112. 07 13. 69 -6.92E-01 1. OOE+OO 1212.95 1. 43 -2.08E+OO 1.02E+Ol 1 249.94 0. 1 9 -8.74E+OO 7.52E+Ol 1 299.14 1. 63 2. 72E+OO 7.62E+OO 1408.01 21.07 -2.85E-01 5.60E-01 1457.64 0.50 -3.75E+Ol 7.33E+Ol 1528.10 0. 2 8 -5.17E-0 1 4.84E+Ol Eu - 1 54 123.07 40.40 -4. 72E-02 2.23E- 01 2 .23E-01 2 47.93 6.89 1.77E-01 1 .70E+OO 591.76 4.95 1.17E+OO 3 .03E+OO 692.42 1. 78 2.65E+OO 7.49E+OO 723. 30 20.06 4.67E-01 7 . 43E-01 756.80 4 . 52 1 . 58E+OO 2 .79E+OO 873.18 1 2. 08 2.22E-01 1. 2 0E+OO 996. 2 9 10 .48 - 1.97E-01 1. 39E+OO

[2601]

3/13/2018 8:53:32PM Page 6 of6 Analysis Report for 13-Mar-18-10017 81051 OOA-FSWC-156CV o.o* - o.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCi/grams)

(keV)

Eu-1 5 4 1004.76 18 . 01 3.07E-01 2 .23E-01 8.62E-01 1274.43 34.80 -l.83E-01 3.84E-Ol 1596.48 1. 80 1. 37E+OO 7.29E+OO Eu-155 45.30 1. 31 -l. 2 3E+OO 3.86E-01 2 .52E+Ol 60.01 1. 22 5.42E+OO 2 .66E+Ol 86.55 30.70 -7.48E-0 2 3.86E-01 105.31 21.10 -1. 72E-01 4. 71E-01 Ra-226 186.21 3.64 2.72E+00 3.54E+OO 3.54E+OO Pa- 23 1 27.36 10.30 8.96E-01 2 .46E+OO 2 .46E+OO 283.69 1. 70 3.22E+OO 6.73E+OO 300.07 2 .47 2.38E-01 4. 3 9E+OO 30 2 .65 2 . 20 9.57E-01 5.lOE+OO 33 0.06 1. 40 -9.38E+00 9.24E+OO U-2 3 5 143 . 76 10. 96 l.OlE-01 2.24 E- 01 9.35E-Ol 163.33 5.08 3.37E-01 2.16E+OO 185. 71 57.20 l.78E-01 2 . 2 4E-01 20 2 .11 1. 08 2 . 3 6E+00 l.13E+Ol 205.31 5.01 2 .68E-01 2 .41E+OO Am-241 59.54 35.90 l.55E-01 9.32E-01 9.32E-01

+ = Nuclide identified during the nuclide identification

. = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence ievel

[2602]

0000024307.CNF 500 Live Time :2400.000 sec Real Time :2403.300 sec Start: 1: O.l(kev)

Stop : 4096:2047.l(kev)

Acq. Start :Tue Mar 13 20:11:46 2018 450 400 350 300 ~

7.,,

u VI

.µ

§ 0

250 u

[2603]

200 150 100 500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/13/2018 7:30 :36PM Page I of6

~pex-Gamma Analysis Report for 13-Mar-18-10016 B105100A-FSWC-156CV 0.0" - OS 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10016 Sample Description : 81051 OOA-FSWC-156CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 9.647E+01 grams Facility : Default Sample Taken On : 3/9/2018 3:04:00PM Acquisition Started : 3/13/2018 7:10:26PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.3 seconds Dead Time : 0.11 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120- 8192 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24304 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 7:30:31PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2604]

3/13/2018 7:30:36PM Page 2 of6 Analysis Report for 13-Mar-18-10016 B 1051 OOA-FSWC-156CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 661.55 2 633 - 2655 2644.08 1 .68E+04 2 61.66 1.74E+02 1. 42 2 1172. 95 4676 - 4701 4689. 2 4 7 . 93E+02 60.48 5.75E+Ol 1. 69 3 1332.18 5313 - 5338 5326.37 7.33E+02 55.65 1.93E+Ol 2 .00 4 1460.54 5835 - 5847 5840.08 2 .53E+Ol 11. 83 7.40E+OO 0. 71 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-4 0 0.98 1460. 82

10.66 3 .62E+OO 1. 72E+OO Co-6 0 0.98 1173. 23

99.85 1.02E+Ol 1.13E+OO 1332.49

99.98 1. 03E+Ol 1.14E+OO Cs- 137 0 . 99 661. 66

85. 10 1.69E+02 2 .05E+Ol

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2605]

3/13/2018 7:30:36PM Page 3 of6 Analysis Report for 13-Mar-18-10016 B105100A-FSWC-156CV 0.0" - 0.5" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.987 3.62E+OO 1. 72E+OO Co-60 0.986 l.03E+Ol 8.0lE-01 Cs-137 0.998 1.69E+02 2.05E+Ol

? = nuclide is part of an undetermined solution X = nuclide rejected by the Interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2606]

3/13/2018 7:30:36PM Page 4 of6 Analysis Report for 13-Mar-18-10016 B105100A-FSWC-156CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 7:30:31PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide

. NI peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCVgrams) (pCi/grams)

(keV)

An Pk 511.00 100.00 -1.33E-01 8.69E-01 8.69E-01 BE-7 4'77. 60 10.44 1.04E+OO 1.04E+Ol 1.04E+Ol

+ K-40 1 460.82

10.66 3.62E+OO 1.92E+OO 1.92E+00

+ Co-60 1173.23

99.85 1.02E+Ol 3 .45E-0 1 5.18E-01 1332.49

99.98 1 .03E+Ol 3.45E-01 Nb-94 702.65 99.81 2.77E-01 4.09E-01 4.09E-01 871.09 99.89 3.15E-01 5.53E-01 A.g-1 08m 79 .13 6.60 7.14E-01 4.45E - 01 1 . 0lE+Ol 433.94 90.50 1.09E+00 1 . 12E+OO 614.28 89.80 -5.67E-01 6 . 70E-01 722. 94 90.80 2 . 2 7E-02 4.45E-01 Sb-1 25, 1"'6.31 6.84 3.98E+OO 3 . 3 3E+OO 6.34E+OO 380.45 1. 52 -5.45E+Ol 4.97E+Ol 427.87 29.60 -1.60E-0 2 3.33E+OO 463.36 10.49 7.62E+OO 1.09E+Ol 600.60 17 .. 65 2 .64E-01 3. 35E+OO 606.71 4.98 3.47E+OO 1. 24E+Ol 635.95 11. 22 - 4.58E-01 5.55E+OO 671.44 1. 79 -7.76E+OO 1.90E+Ol

[2607]

3/13/2018 7:30:36PM Page 5 of6 Analysis Report for 13-Mar-18-10016 81051 OOA-FSWC-156CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV)

(pCUgrams) (pCilgrams) (pCilgrams)

Ba-1 33 79.61 2 .65 7.69E+OO 1.19E+O O 2 .47E+Ol

81. 00 32 .90 -8.0lE-01 1 .90E+OO 276.40 7. 1 6 3.96E-01 8.04E+OO 302.85 18.34 -1.08E+OO 3.40E+OO 356. 01 62. 05 -5.99E-01 1.19E+OO 383.85 8.94 1.34E-01 8.87E+OO Cs-134 475. 3 6 1. 48 5.61E+Ol 4.58E-01 7.35E+Ol 563.25 8.34 -1.44E-01 7.65E+OO 569.33 15.37 5.73E-01 4.18E+OO 604. 72 97.6 2 -3.43E-02 6. 3 0E-0 1 7 95.86 85.46 -2.76E-01 4.58E-0 1 8 01 .95 8.69 9.43E-01 4.73E+00 10 3 8.6 1 0.99 -1.42E-01 5.23E+Ol 1167.97 1. 79 9.79E-01 9.54E+Ol 1365.19 3.0 2 -3 .58E-01 6.99E+OO

+ Cs-137 661.66

85.10 1.69E+02 6.53E-01 6.53E-01 Eu-1 5 2 12 1 .78 28 . 67 -3 .04E-01 1.09E+OO 1.36E+OO 244.70 7.6 1 7.30E-01 7.60E+OO 295.94 0.45 8.84E+Ol 1.41E+02 344. 2 8 2 6.60 5.16E-01 2 .59E+OO 367.79 0.8 6 -6.99E+Ol 8.56E+Ol 411. 12 2 .24 3.25E+OO 3. 96E+Ol 443.96 2 .83 -1.70E+Ol 3.65E+Ol 488.68 0.42 1.35E+02 2.15E+02 563.99 0.49 -1.18E+ Ol 1.30E+0 2 586.26 0.46 5.27E+Ol 1.37E+0 2 678.62 0.47 4.70E+Ol 7.64E+Ol 688.67 0.86 -2.31E+OO 4.31E+Ol 7 1 9.35 0.28 -6.24E+Ol 1. 40E+02 7 78.90 12. 96 1.82E+OO 3.12E+OO 810.45 0.32 7.31E+OO 1.28E+02 867.37 4.26 -7.43E+OO 1 . 22E+Ol 919.33 0.43 -6.21E+Ol 1.37E+02 964.08 14.65 1.0lE+OO 4.14E+OO 1085.87 10.2 4 7.39E-01 5.55E+OO 1089.74 1. 73 -2 .80E+Ol 3 . 2 2E+Ol 1112. 07 13. 69 4.05E+OO 4.00E+OO 1 2 12.95 1. 43 -l. 2 6E+Ol 2 . 2 9E+Ol 1249.94 0.19 1.71E+Ol 1 .80E+02 1299.14 1. 63 4.46E+OO 1.97E+Ol 1408.01 2 1. 07 -1.05E-01 1.09E+OO 1457.64 0.50 9.75E+Ol 1.06E+02 1528.10 0.28 -4.21E+Ol 6.28E+Ol Eu-154 1 23 .07 40.40 4.65E-02 9.31E-0 1 9.69E-01 2 47.93 6.89 -3 .03E-01 8.39E+OO 591. 7 6 4.95 2 . 2 9E+OO 1. 2 3E+Ol 692.42 1. 78 1.78E+Ol 2 .13E+Ol 723. 30 2 0.06 -5.93E-0 2 2.04E+OO 756.80 4. 52 9.93E+OO 9.75E+OO 873.1 8 12.08 5.83E+00 4.76E+OO 996. 2 9 10.48 5.06E+00 5.18E+OO

[2608]

3/13/2018 7:30:36PM Page 6 of6 Analysis Report for 13-Mar-18-10016 B105100A-FSWC-156CV o.o* -0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCi!grams) (pCilgrams)

(keV)

Eu-154 1004.76 18.01 -1.95E+00 9. 3 1E-01 2 .86E+OO 1274.43 34.80 -1.29E-02 9.31E-01 1596. 48 1. 80 4. 2 8E+00 1.65E+Ol Eu-155 45. 3 0 1. 31 3 .85E+Ol 1. 73E+OO 1.15E+02 60.01 1. 22 2 .40E+00 l.15E+02 86.55 30.70 l.05E-01 1. 73E+OO 105.31 21.10 5.47E-01 2 .09E+OO Ra-226 186.21 3 . 64 6.75E+OO 1. 36E+Ol 1. 36E+Ol Pa-231 2 7.36 10.30 2 .02E+Ol 1. 2 1E+Ol 1.21E+Ol 283.69 1. 70 9.33E+OO 3 .51E+Ol 300.07 2 .47 1. 03E+OO 2 .57E+Ol 302.65 2 . 20 -8.93E+OO 2 .84E+Ol 330.06 1. 40 2 .04E+O l 4.90E+Ol U-235 143.76 10.9 6 -l.35E+00 8.57E-01 3.70E+OO 1 63.33 5 . 08 2. 22E+00 8.0lE+OO 185.71 57.20 1.47E-01 8.57E-01 202 .11 1. 08 8.12E-01 4.59E+Ol 2 05.31 5.0 1 1.84E+OO 9.99E+OO Am-241 59.54 35.90 -1.34E+OO 3. 98E+OO 3.98E+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA vaiue is inconsistent with Currie MDA at 95'% confidence ievei

[2609]

0000024304.CNF 4000 Live Time :1200.000 sec Real Ti me :1201.320 sec start: 1: -0.0(kev) stop : 8192: 2047 .S(kev)

Acq. Start :Tue Mar 13 19:10:26 2018 3500 3000 2500 Vl

~

§0 2000 u

[2610]

1500 1000 500

~

o----L.....l....L........---l.,_---1----L.....-+--..L.....:....;.J......;,___J_---L,~;=::+/-==-""""""!Ll....J-f--.___..__..._....._-1-..............__....L...11.........._-+-....L........LJ..____.____.__-+-----'------'---'---'--+-----'------'------'----L--t___.

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/19/2018 8:12:28PM Page I of7

~~./\pex-Gamma Analysis Report for 19-Mar-18-10012 B105100A-FSWC-162CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 19-Mar-18-10012 Sample Description : B105100A-FSWC-162CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 9.081E+01 grams Facility : Default Sample Taken On : 2/15/2018 3:30:00PM Acquisition Started : 3/19/2018 7:12:17PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 3600.0 seconds Real Time : 3604.8 seconds Dead Time : 0.13 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/19/2018 Efficiency Calibration Description Sample Number : 24569 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/19/2018 8:12:24PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2611]

3/19/2018 8:12 :28PM Page 2 of7 Analysis Report for 19-Mar-18-10012 B 1051 OOA-FSWC-162CV 0.0"-0.5" o.o*

Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238 . 72 474 - 48 2 477.61 5.78E+Ol 47 . 44 4.73E+02 1.12 2 351.80 700 - 708 703.54 5.63E+Ol 36.92 2 .67E+02 1.10 3 510.64 1015 - 1026 1020.97 1.16E+02 41.67 2 .55E+02 0.95 4 609.36 1 212 - 1224 1218.30 5.33E+Ol 27.89 1.07E+0 2 1.55 5 661. 74 1317 - 1328 1323.01 2 .89E+03 110 . 2 8 1. 2 3E+02 1. 52 6 911.4 2 1819 - 1827 1822. 2 9 2 .16E+Ol 14.78 2 .87E+Ol 1 *. 24 7 1173.20 234 1 - 2 351 2346.00 5 .12E+Ol 17.29 1.95E+Ol 1.10 8 1332. 83 2658 - 2672 2665.48 5.16E+Ol 18.44 2.28E+Ol 1. 60 9 1461.08 2915 - 2929 2922.22 9.45E+Ol 21. 55 l.50E+Ol 1. 83 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty An Pk 0.97 511. 00

100.00 4 . 00E-01 1. 54E-01 K-40 0.98 1460.82

10.66 4 .2 3E+OO 1. 03E+OO Co-60 0.99 1173.23

99.85 2 . lOE-01 7.29E-02 1332.49

99.98 2 .3 1E-01 8.46E-0 2 Cs-13: 0.99 661.66

85 . 10 9.33E+O O 1 .18E+OO Bi-211 0.91 351. 07

13.02 7.43E-0 1 5. OlE-01 Pb-212 0 .99 115 .18 0.60 238.63

43.60 1 . 72E-01 1. 44E-O l 300.09 3.30 Bi-2 1 4 1. 00 609.3 2

45.49 3.03E-01 1.63E-01

[2612]

3/19/2018 8:12:28PM Page 3 of7 Analysis Report for 19-Mar-18-10012 B1051 OOA-FSWC-162CV 0.0" - 0.5" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi -2 14 1. 00 768.36 4.89 806.18 1. 2 6 934.06 3 .11 1120. 2 9 14.92 1155. 2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2 .39 1509. 2 1 2 .13 1661. 2 7 1. 05 1729.59 2 .88 1764.49 15.30 1847.43 2 .03 2 118.51 1.16 Pb-214 0.99 241.99 7.25 295. 22 18.42 351.93

35.60 2 . 72E-01 1. 83E-01 785. 96 1. 06 Ac-228 0.99 129.07 2 .4 2 209.25 3 .89 270.24 3 .46 328.00 2 .95 338.32 11. 27 409.46 1. 92 463.00 4.40 794.95 4.25 911.20

25.80 2 .88E-01 l.98E-01 964.77 4.99 968. 97 15.80 1588.20 3. 22

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

[2613]

3/19/2018 8:12:28PM Page 4 of7 Analysis Report for 19-Mar-18-10012 B1051 OOA-FSWC-162CV 0.0" - 0.5" 0.0" Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

An Pk 0.978 4.00E-01 1 .54E-01 K-40 0.989 4.23E+OO 1.03E+00 Co-60 0.991 2.19E-01 5.52E-02 Cs-137 0.999 9.33E+00 1.18E+OO

? Bi-211 0. 918 7.43E-01 5.0lE-01 Pb-21 2 0.999 1.72E-01 l.44E-01 Bi-214 1. 000 3.03E-01 1.63E-01

? Pb-214 0.998 2 . 72E-01 1. 83E-01 Ac-228 0.998 2 .88E-01 1.98E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2614]

3/19/2018 8:12:28PM Page 5 of7 Analysis Report for 19-Mar-18-10012 B105100A-FSWC-162CV 0.0" -OS o.o*

UNIDENTIFIED PEAKS Peak Locate Performed on : 3/19/2018 8:12:24PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak .CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCl/grams)

(keV)

+ An Pk 511. 00

100.00 4.00E-01 2 .19E-01 2 .19E-01 BE-7 477.60 10.44 3 .54E-02 2 .19E+OO 2 .19E+OO

+ K-40 1460.82

10.66 4.23E+OO 8.35E-01 8.35E-01

+ Co-60 1173.23

99.85 2 .lOE-01 7.93E-02 7.93E-02 133 2 .49

99.98 2 .31E-01 1. OlE-01 Nb-94 702.65 99.81 7.lOE-0 2 1.12E-01 1.12E-01 871. 09 99.89 9.89E-0 2 1.15E-01 Ag-108m 79.13 6.60 1. 2 8E+OO 1. 21E-01 2 .24E+OO 433.94 90.50 - 6.87E-02 1. 64E-01 614.28 89.80 -3 .19E-02 1. 58E-01 722 . 94 90.80 -9.98E-02 1. 21E-01 Sb-125 176.31 6 . 84 -1.0lE+OO 5.05E-01 1.57E+00 380.45 1. 52 6.12E+OO 9.56E+OO 427.87 29 .60 -2 .47E-01 5.05E-01 463.36 10.49 5.60E-01 1.66E+OO 600.60 17.65 -3.24E-01 6.59E-01 606. 71 4.98 3.28E-01 3 .llE+OO 635.95 11. 22 -l.66E-01 l.15E+OO 671. 44 1. 79 -3 .02E+OO 5.49E+OO

[2615]

3/19/2018 8:12:28PM Page 6 of7 Analysis Report for 19-Mar-18-10012 B1051 OOA-FSWC-162CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCi!grams)

(keV)

Ba-13 3 79.61 2 . 65 2 . 67E+OO 2.2 4E- 01 5 .42E+OO

81. 00 32 .90 -4.03E-01 3 .85E-01 2 76.40 7.16 -2 . 3 9E-01 1.50E+OO 302.85 18.34 -1.84E-01 6.36E-01 356 .01 62.05 - 7.44E-02 2 . 2 4E-01 383.85 8.94 4.22E-01 1.57E+OO Cs - 134 475.36 1. 48 -4.65E-01 1.36E-01 1.07E+Ol 563.25 8.34 6.90E-01 1.48E+OO 569.33 15.37 -1.llE-01 7.73E-01 604.72 97.62 -2. 72E..:.02 1.36E-01 795.86 85.46 -1.88E-04 1.38E-01 801.95 8.69 2 . 2 0E-01 1. 34E+OO 1038.61 0.99 - 1.06E+OO 1.22E+Ol 1167.97 1. 79 -1.12E+OO 9.15E+OO 1365.19 3.0 2 6.92E-01 3.67E+OO

+ Cs-137 661. 66

85.10 9.33E+OO 1.45E-01 1.45E-01 Eu-15 2 121.78 2 8.67 ~2.05E-02 2.95E - 01 2 .95E-01 244.70 7.6 1 -9.97E-01 1.48E+OO 295.94 0.45 6.25E+OO 2 .63E+Ol 344. 2 8 2 6.60 1.89E-01 4. 96E-01 367.79 0.86 6.61E+OO 1. 57E+Ol 411. 1 2 2 . 24 -7.64E-01 6.42E+OO 443.96 2 .83 -2 .43E+OO 5.49E+OO 488.68 0 .42 1.06E+Ol 3.42E+Ol 563.99 n V *

/I a

°J:..I 9.64E+OO 2 .41E+Ol 586.26 0.46 2.52E+OO 2 .69E+Ol 678.62 0.47 -3.04E+OO 1. 98E+Ol 688.67 0.86 -1.80E+OO 1. 12E+Ol 719.35 0.28 8.46E+OO 3 .96E+O l 778.90 12. 96 - 1 .07E-01 8.18E-01 810.45 0.32 1. 1 7E+Ol 3.39E+Ol 867. 3 7 4.26 -3 .73E-01 2 . 2 4E+OO 919. 33 0.43 -9.20E+OO 2 .40E+Ol 964.08 14.65 -4.42E-01 7.83E-01 1085.87 1 0 .24 -1.91E-01 1. 23E+OO 1089.74 1. 73 2 .38E-01 7.44E+OO 11 1 2 . 07 13. 69 2 .05E-0 1 9.42E-01 121 2 .95 1. 43 -3.77E-01 7.55E+OO 1249.94 0. 1 9 -4.56E+Ol 5.22E+Ol 1 299.14 1. 63 -2 .15E+00 6.08E+OO 1 408.01 2 1.07 -2 .98E-01 5.82E-01 1 457.64 0.50 -2 .86E+OO 4.93E+Ol 1 528.10 0. 2 8 -9 .54E+OO 3. 31E+Ol Eu-154 123.07 40.40 -1.37E-01 2 .00E-01 2 .00E-01 247.93 6.89 5.61E-01 1.67E+OO 591.76 4.95 2 .92E-01 2 . 39E+OO 692. 4 2 1. 78 -2 .33E+OO 5.33E+OO 723. 3 0 20.06 -2 .63E-01 5.78E-Ol 756.8 0 4.52 9.06E-01 2.28E+OO 873. 1 8 12. 0 8 9.55E-02 9. llE-01 996.29 1 0.48 -1.85E- 01 1. 05E+OO

[2616]

3/19/2018 8:12:28PM Page 7 of7 Analysis Report for 19-Mar-18-10012 81051 OOA-FSWC-162CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCl/grams) (pCi/grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.0 1 4.16E-01 2 .00 E- 01 6.95E-01 1274.4 3 34.80 -1.77E-01 3. 02E-01 1 596.48 1. 80 1. 79E+OO 6. 35E+OO Eu-155 45. 3 0 1. 31 -1.27E+OO 3 .66E-01 ~. 37E+Ol 60.01 1. 22 9.22E+00 2 .52E+Ol 86 . 55 30.70 -4.84E-02 3.66E-01 105 .31 21.10 -1.59E-02 4.46E-01 Ra-226 186.21 3.64 3.34E-01 3 .18E+OO 3 .18E+OO Pa-23 1 2 7.36 10.30 2 .17E+00 2 .38E+OO 2 . 3 8E+OO 2 83.69 1. 70 -3 .07E+OO 6. 3 6E+OO 300.07 2 .47 -2 .44E+OO 4.65E+OO 302.65 2 .20 -1.53E+OO 5.27E+OO 330.06 1. 40 5.29E-Ol 9.02E+OO U-235 143.76 10. 96 -3.42E-02 2. 00E-01 8.07E-01 163.33 5.08 3 .25E-01 1. 99E+00 185. 71 57. 2 0 -3 .81E-02 2 .00E-01 202 .11 1. 08 -4.00E-01 1.02E+Ol 205.31 5.0 1 -6.67E-01 2 .24E+OO Am-241 59.54 35.90 3.06E-01 8. 72E - 01 8. 72E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2617]

0000024569.CNF 1000 Live Time 3600.000 sec Real Time 3604.830 sec start: 1 O.l(kev)

Stop : 4096 2047. l(kev)

Acq. start Mon Mar 19 19:12:17 2018 900 800 700 600 Vl

-I-'

§ 0

500 u

[2618]

400 300 200 500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/19/2018 8:46:22PM Page I of6

~pex-Gamma Analysis Report for 19-Mar-18-10013 B105100A-FSWC-162CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 19-Mar-18-10013 Sample Description : 8105100A-FSWC-162CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 9.081 E+01 grams Facility : Default Sample Taken On : 2/15/2018 3:30:00PM Acquisition Started : 3/19/2018 8:26:14PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.6 seconds Dead Time : 0.13 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/19/2018 Efficiency Calibration Description Sample Number : 24578 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/19/2018 8:46:18PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2619]

3/19/2018 8:46:22PM Page 2 of6 Analysis Report for 19-Mar-18-1001 3 B 1051 OOA-FSWC-162CV 0.0" -0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 661. 72 1317 - 1328 1322.98 4.08E+02 42.56 3.59E+Ol 1. 28 2 14 61. 02 2918 - 2927 2922.09 2.30E+Ol 12.10 1. 21E+Ol 1. 60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82

10.66 3.09E+OO 1.65E+OO Cs-137 0.99 661.66

85.10 3. 96E+OO 6.30E-01

" = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2620]

3/19/2018 8:46:22PM Page 3 of6 Analysis Report for 19-Mar-18-10013 B105100A-FSWC-162CV 0.0" - 0.5 0.5

INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.994 3.09E+OO 1.65E+00 Cs-137 0.999 3. 96E+OO 6.30E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2621]

3/19/2018 8:46:22PM Page4 of6 Analysis Report for 19-Mar-18-10013 8105100A-FSWC-162CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/19/2018 8:46:18PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Lisee! : C:\Canberra\Apex\Root\Default\L!brary\Z!ON LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCi/grams) (pCi/grams) (pCl/grams)

(keV)

An Pk 511. 00 100.00 4.99E-01 4.SOE-01 4.80E-01 BE-7 477.60 10.44 1. 4 7E+OO 3 .41E+OO 3 .41E+OO

+ K-40 1460.82

10.6 6 3.09E+OO 2 .07E+OO 2 .07E+OO Co-60 1173.23 99.85 6.59E-02 2 .56E-0 1 2 .56E-01 1332.49 99.98 l. 47E-01 2. 79E-01 Nb-94 702.65 99.81 -8.55E-02 1.94E-01 1.95E-01 871.09 99.89 6.44E-03 1. 94E-01 Ag-108m 79.13 6.60 4.77E-01 2 .24E - 01 3 .52E+OO 433.94 90.50 -1.40E-02 2 .50E-01 614. 2 8 89.80 -2 .48E-01 2 .38E-01 722 . 94 90.80 3.73E-0 2 2 .24E-01 Sb- 125 176.31 6.84 1. 50E+00 7 .94E-01 2 .62E+00 38 0 .45 1. 52 1.03E+OO 1. 2 5E+Ol 427.87 2 9.60 2.02E-01 7.94E-01 463.36 10.49 -6.65E-01 2 .51E+OO 600.60 17.65 -2 .45E-01 1.15E+OO 606.71 4.98 4.03E+OO 5.40E+OO 635.95 11. 22 1.15E+OO 2.06E+OO 671.44 1. 79 -2 .0lE+OO 1. 0BE+Ol

[2622]

3/19/2018 8:46:22PM Page 5 of6 Analysis Report for 19-Mar-18-10013 B105100A-FSWC-162CV 0.0" -0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

Ba-133 79.61 2 .65 -1.16E+OO 3.7 4E-01 8".16E+OO

81. 00 32 .90 -1.56E-01 6.28E-01 276.40 7.16 9.46E-0 2 2 .52E+OO 302.85 18.34 -2 .04E-01 9.23E-01 356.01 62.05 l.43E-01 3.74E-01 383.85 8.94 4.79E-01 2 .06E+OO Cs-134 475.36 1. 48 2. 70E+OO 2 .12E-01 1.64E+Ol 563.25 8.34 -2 .68E-02 2 . 3 0E+OO 569.33 15.37 4.94E-01 1. 33E+OO 604. 72 97.62 -2 .70E-02 2 .55E-01 795.86 85.46 -9.31E-02 2 .12E-01 801.95 8.69 -1.19E+OO 2 .lOE+OO 10 3 8.61 0.99 7.00E+OO 2.35E+Ol 1167.97 1. 79 - 6.86E+OO 1.26E+Ol 1365. 1 9 3.0 2 -1.34E+OO 6. 2 8E+OO

+ Cs-137 661.66

85.10 3 .96E+OO 2. 48E-01 2 .48E-0 1 Eu-1 52 121.78 2 8.67 3.62E- 02 4.86E-01 4.86E-01 244.70 7.61 -2. 03E-01 2 .45E+OO 295.94 0.45 1.80E+Ol 4.38E+Ol 344. 2 8 26.60 2 .13E-0 2 7.84E-01 367.79 0.86 1. 55E-01 2 .26E+Ol 411.12 2 .24 -7.86E-01 8.65E+OO 443.96 2 .83 4.33E-01 8.lOE+OO 488.68 0.42 1. 2 9E+Ol 5.30E+01 563.99 0.49 1. 71E-01 3.81E+Ol 586.26 0.46 5.67E+OO 5.09E+Ol 678.62 0.47 1.14E+Ol 4.14E+Ol 688.67 0.86 2.91E+OO 2 . 2 4E+Ol 719. 35 0.28 -2.86E+Ol 7.12E+Ol 778. 90 12. 96 -2.63E-01 1.53E+OO 810.45 0.32 1.63E+Ol 6.36E+Ol 867. 3 7 4.26 9.55E-01 5 . 17E+OO 919. 3 3 0.43 1.65E+Ol 5.21E+Ol 964.08 14.65 9.16E-02 1. 66E+OO 1085.87 10.24 -3.16E-01 1.66E+OO 1089.74 1. 73 -1.54E+OO 9.83E+00 111 2 .07 13. 69 -8.61E-02 1.95E+OO 1212.95 1. 43 8.26E+OO 1.88E+Ol 12 49.94 0.19 -9.48E+Ol l.22E+02 1299.14 1. 63 -2 .42E+OO 1.18E+Ol 1408.01 21. 07 9.52E-0 2 8 . 26E-01 1 457.64 0.50 -1.53E+Ol 8.69E+Ol 1528.10 0. 2 8 -3 .53E+Ol 5.92E+Ol Eu-154 123.07 40.40 1. 53E-01 3 .54E-01 3.54E-01 247.93 6.89 -8.60E-02 2 . 56E+OO 591.76 4.95 8.12E-01 4 . 44E+OO 692.42 1. 78 3.54E-02 1.09E+Ol 723. 30 2 0.0 6 -l.31E-01 9.71E-01 756.80 4.52 -1.19E+00 4.06E+OO 8 7 3.18 12.08 -3 .59E-02 1.56E+OO 996. 2 9 10.48 4.lOE-01 1.97E+OO

[2623]

3/19/2018 8:46:22PM Page 6 of6 Analysis Report for 19-Mar-18-10013 B1051 OOA-FSWC-162CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 6.60E-02 3 .54E-01 1. llE+OO 1274.43 34.80 -9.13E-02 6.99E-01 1 596.48 1. 80 - 4.64E+OO 1. 08E+Ol Eu-155 45.30 1. 3 1 6.91E-01 5.62E-01 3 .66E+Ol 60.01 1. 22 -1.59E+Ol 3 .58E+Ol 86.55 30.70 -l.14E-01 5.62E-Ol 105. 3 1 21.10 -2 .74E-01 6.95E-01 Ra-226 186.21 3 .64 2 .33E+OO 5.14E+OO 5.14E+OO Pa-23 1 27.36 10.30 1. llE+OO 3.58E+OO 3 .58E+OO 283.69 1. 70 3.26E+OO 1.14E+Ol 300.07 2 .47 -3.87E+OO 6.71E+OO 30 2 .65 2 .20 -1.69E+OO 7.65E+OO 330.06 1. 40 5.60E+OO 1.57E+O l U- 235 143.76 10. 96 -2 . 3 8E-0 1 3.34E-01 1 .25E+OO 163.33 5.08 1.20E-01 3.56E+OO 185.71 57. 2 0 2 .15E-01 3.34E-01 2 02 .11 1. 08 2 .58E+OO 1. 58E+Ol 205.31 5.01 -9 . 46E-01 3.43E+OO Am-241 59.54 35.90 -5.SOE-01 1. 2 5E+OO 1.25E+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2624]

0000024578.CNF 250 Live Time 1200.000 sec Real Ti me 1201.570 sec Start: 1 O.l(kev) stop : 4096 2047. l(kev)

Acq . Start Mon Mar 19 20: 26: 14 2018 200 150 .,,

I u

I.I)

,I-'

C 0

u

[2625]

100 50 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/19/2018 5:46:20PM Page I of6

~~~pex-Gamma Analysis Report for 19-Mar-18-10014 B105100A-FSWC-163CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 19-Mar-18-10014 Sample Description : B105100A-FSWC-163CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 9.773E+01 grams Facility : Default Sample Taken On : 2/15/2018 1:50:00PM Acquisition Started : 3/19/2018 5:26:13PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.02 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120- 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/19/2018 Efficiency Calibration Description Sample Number : 24570 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/19/2018 5:46:16PM Peak Analysis From Channel 120 Peak Analysis To Channel : 8192

[2626]

3/19/2018 5:46:20PM Page 2 of6 Analysis Report for 19-Mar-18-10014 B105100A-FSWC-163CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 352.04 1400 - 1412 1407.17 2.51E+Ol 14.36 1.97E+Ol 0.69 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi-211 0.86 351.07

1 3 .02 1 .00E+OO 5 . 96E-01 Pb-214 0.99 2 41.99 7.25 2 95. 22 18.42 351.93

35.60 3 .67E-0 1 2 .18E-01 785.96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2627]

3/19/2018 5:46:20PM Page 3 of6 Analysis Report for 19-Mar-18-10014 B105100A-FSWC-163CV 0.0" - 0.5" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

? Bi-211 0.860 1. OOE+OO 5.96E-01

? Pb-214 0.999 3.67E-01 2.18E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2628]

3/19/2018 5:46:20PM Page 4 of6 Analysis Report for 19-Mar-18-10014 8105100A-FSWC-163CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/19/2018 5:46:16PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Librar/ Used : C:\Canberra\Apex\Root\Default\Library\Z!ON L!B-BNL.NLB Nuclide Energy Yield{%) Activity Nuc/ideMDA LlneMDA Name (pCVgrams) (pCVgrams) (pCl/grams)

(keV)

An Pk 511.00 100.00 3 .32E-01 3.62E-01 3 .62E-01 BE-7 477.60 10.44 6. 96E-01 2.12E+OO 2 .12E+OO K-40 1460.8 2 10.6 6 3 .09E+OO 3.99E+OO 3.99E+OO Co-60 1173. 2 3 99.85 -2 .21E-02 2.22E- 01 2 . 2 2E- 01 1332.49 99.98 4.78E-02 2 .31E-01 Nb-94 702.65 99.8 1 6.43E-02 1.51E-01 2. 0lE-01 871.09 99.89 5 .17E-03 1.51E-01 Ag- 108m 79.13 6 . 60 -5.95E-01 1. 2 2E-01 2 .40E+00 433.94 90.50 3.98E-02 1. 2 2E-01 614.28 89.80 -5.67E-02 2 .02E-01 722. 94 90.80 -1. 28E-01 2 . OlE-01 Sb-125 176.31 6.84 5.95E-01 3.44E-01 1.44E+00 380.45 1. 52 -1.46E+OO 8.44E+OO 427.87 2 9.60 -2 .90E-01 3 .44E-Ol 463.36 10.49 -6.05E-01 1. 27E+OO 600.60 17.65 -2 . 2 3E-01 1.03E+OO 606 . 71 4.98 1.30E+OO 4.45E+OO 635.95 11. 22 -4.63E-01 l.23E+00 671. 44 1. 79 5.76E-01 7.61E+OO

[2629]

3/19/2018 5:46:20PM Page 5 of6 Analysis Report for 19-Mar-18-10014 B1051 OOA-FSWC-163CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCl/grams)

(keV)

Ba-133 79.61 2.65 -1.60E+OO 2 .40E-01 5.82E+OO

81. 00 32 .90 1. 50E-0 2 4.41E-01 276.40 7.16 -2 .12E-01 1. 45E+00 302.85 18.34 -4.46E-02 6. 2 0E-01 356.01 62.05 - 1.22E-01 2 .40E-01 383.85 8.94 1.52E-01 1. 34E+OO Cs-134 475.36 1. 48 -1.82E-01 l.92E-01 1. 04E+Ol 563. 2 5 8.34 -5 .82E-01 1.52E+OO 569.33 15.37 2 .91E-01 9.14E-01 604. 72 97.62 -9 .71E-0 2 2 . 2 4E-01 795.86 85.46 -2 .62E-02 l.92E-01 801.95 8.69 4.25E-01 1. 90E+OO 1038.61 0.99 9. 72E+OO 2 .00E+Ol 1167.97 1. 79 - 1.0lE+OO 1.26E+Ol 1365.19 3.0 2 O.OOE+OO 1. 39E+OO Cs-137 661.66 85.10 6.78E-02 1.87E-01 1.87E-01 Eu-152 121. 78 2 8.67 1.30E-01 3 .17E-01 3.17E-01 244.70 7.61 -5.56E-01 1. 3 8E+OO 295.94 0.45 -2 .93E+OO 2 .85E+Ol 344. 2 8 2 6.60 2 .14E-01 4.14E-Ol 367.79 0.86 8.78E+OO l . 31E+Ol 411.12 2 .24 1.25E+OO 5 . 32E+OO 443.96 2 .83 -1.44E+OO 4.16E+OO 488.68 0.42 8.03E+OO 2.18E+Ol 563.99 0.49 -l. 2 8E+01 2.52E+Ol 586.26 0.46 -1. 3 6E+Ol 3.82E+Ol 678.62 0.47 4.59E-01 3 .31E+Ol 688.67 0.86 5.35E+OO 2 .19E+Ol 719. 3 5 0. 2 8 -8.47E+OO 6.53E+Ol 778.90 12.96 -2 .68E-01 1. 21E+OO 810.45 0.32 -5.06E+OO 5.54E+Ol 867.37 4.26 -l.32E-01 3.55E+OO 919.33 0.43 5.05E+OO 2 .44E+Ol 964.08 14.65 1.07E+OO 1.59E+OO 1085.87 10. 2 4 -7.59E-02 1. 84E+OO 1089.74 1. 73 -3 .33E+OO 1.09E+Ol 1112. 07 13. 69 2 .69E-01 l.40E+OO 1 2 12.95 1. 43 -3.48E+OO 1.24E+01 1249.94 0.19 -2 .06E+OO 1.03E+02 1299.14 1. 63 4.21E+OO 1.15E+Ol 1408.01 21.07 4.17E-01 l.02E+OO 1457.64 0.50 8.69E+01 8.61E+Ol 1528.10 0.28 l.67E+Ol 6.23E+Ol Eu-154 123.07 40.40 -7.45E-02 2 . llE - 01 2 .llE-01 247.93 6.89 -3 .62E-01 1.51E+OO 591.76 4.95 -6.26E-01 2. 86E+OO 692.42 1. 78 -1.85E+OO 1. 03E+Ol 723. 30 20.06 1. 50E-01 9 . 73E-01 756.80 4.52 -1.51E+OO 2 .33E+00 873.18 1 2 .08 -3 .67E-01 1. 34E+00 996. 2 9 10.48 5.95E-Ol 2 .05E+OO

[2630]

3/19/2018 5:46:20PM Page 6 of6 Analysis Report for 19-Mar-18-10014 B1051 OOA-FSWC-163CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCUgrams) (pCilgrams)

(keV)

Eu-154 1004.76 18.01 7.03E-01 2 . ll E-01 1.20E+OO 1274.4 3 3 4.80 1.95E-01 5.29E-01 1596.48 1. 80 O.OOE+OO 2.62E+00 Eu-155 45.30 1. 31 -9 .83E+OO 3.99E- 01 2.04E+0 1 60.01 1. 22 - 7 . 92E+OO 2 .63E+Ol 86.55 30.70 3. 45E-01 4.90E-01 105.31 21.10 1. 2 9E-02 3.99E-01 Ra-226 186. 2 1 3.64 4.55E-01 2 .65E+OO 2 .65E+OO Pa-231 2 7.36 10.30 1.42E+OO 3.3 6E+OO 3 .36E+OO 283.69 1. 70 -3.24E+OO 6.33E+OO 300.07 2 .47 -3.34E+OO 4.54E+OO 302.65 2 . 20 4.80E-01 5.13E+OO 330.06 1. 4 0 6.19E-0 1 8.79E+OO U-235 143.76 10. 96 6.59E-02 1.73E-01 8.55E-01 163.33 5.08 8.03E-01 1. 96E+OO 185.71 57.20 1.29E-01 1. 73E-01 202 .11 1. 08 -4.52E+OO 7.86E+OO 205.31 5.01 -7.04E-02 1.86E+OO Am-2 41 59.54 35.90 -2 .43E-01 8.93 E- 01 8.93E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2631]

0000024570.CNF Live Time :1200.000 sec Real Ti11e :1200.290 sec 60 start: 1: -0.0(kev) stop : 8192:2047.S(kev)

Acq. Start :Mon Mar 19 17:26:13 2018 55 so 45 40 35

[2632]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/19/2018 7:32:37PM Page I of6

~pex-Gamma Analysis Report for 19-Mar-18-10015 B105100A-FSWC-163CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANAL YS/S Sample Identification : 19-Mar-18-10015 Sample Description : B105100A-FSWC-163CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 9.773E+01 grams Facility : Default Sample Taken On : 2/15/2018 1:50:00PM Acquisition Started : 3/19/2018 7:12:30PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.03%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120- 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/19/2018 Efficiency Calibration Description Sample Number : 24572 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/19/2018 7:32:33PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2633]

3/19/2018 7:32:37PM Page 2 of6 Analysis Report for 19-Mar-18-10015 B105100A-FSWC-163CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 1460.34 5833 - 5845 5839.30 2.98E+Ol 12.43 6.48E+OO 0.54 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0. 96 1460.82

10.66 4.20E+OO 1.79E+OO

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2634]

3/19/2018 7:32:37PM Page 3 of6 Analysis Report for 19-Mar-18-10015 B105100A-FSWC-163CV 0.0" - 0.5" 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0. 963 4.20E+00 1.79E+OO

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2635]

3/19/2018 7:32:37PM Page 4 of6 Analysis Report for 19-Mar-18-10015 B105100A-FSWC-163CV o.o* - OS 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/19/2018 7:32:33PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuciide Library Used : C:\Canberra\Apex\Root\Defauit\Library\Z!ON L!B-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LlneMDA Name (pCUgrams) (pCUgrams) (pCl/grams)

(keV)

An Pk 511. 00 100.00 3 .34E-01 3.34E-01 3 .34E-01 BE-7 477.60 10.44 -1.07E+OO 1.81E+OO 1.81E+OO

+ K-40 1460.82

10.66 4. 2 0E+OO 1. 83E+OO 1. 83E+OO Co-60 1173 . 23 99.85 -6.lOE-0 2 1. 88E- 01 1 .88E-0 1 1332.49 99.98 1.40E-01 2 .53E-01 Nb-94 70 2 .65 99.81 1.99E-02 1.41E-01 1.73E-01 871. 09 99 . 89 5.17E-02 1. 41E-01 Ag-108m 79 .13 6.6 0 1. 28E+OO 1.1 7E-0 1 2 .68E+00 433.94 90.50 -5.76E-02 1.17E-01 614. 2 8 89.80 -7.88E-02 l .97E-01 722. 94 90.80 -l.49E-0 2 1.72E-01 Sb-125 176. 3 1 6.84 2.43E-0 2 3.93E-01 1.58E+OO 380.45 1. 52 -4.00E-01 8 .44E+OO 427.87 29.60 -1.43E-01 3.93E-01 463.36 1 0.49 -4.50E-01 1.18E+OO 600 . 60 17.65 -6.33E-01 8.57E-01 606. 7 1 4.98 1.57E+OO 4.22E+00 635.95 11. 22 2 .41E-01 1.23E+00 671. 44 1. 79 3 .91E+OO 8.04E+OO

[2636]

3/19/2018 7:32:37PM Page 5 of6 Analysis Report for 19-Mar-18-10015 B1051 OOA-FSWC-163CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

Ba-1 3 3 79.61 2 .65 1. 20E+OO 2 . llE-01 6.44E+OO

81. 00 32 .9 0 -1.94E-01 3.86E-01 2 76.40 7.16 1.07E-01 1. 42E+OO 3 02.85 18.34 2 .79E-01 5.46E-01 356.01 62 .05 -2 . 2 1E-02 2 . llE-01 383.85 8.94 7.52E-02 1. 34E+OO Cs - 134 475.36 1. 48 -7.71E-01 1.84E-01 8.61E+OO 563.25 8.34 1.26E+OO 2 .15E+OO 569.33 15.37 -6.02E-01 1. 02E+00 604. 72 97.6 2 -1.90E-0 1 1. 84E-01 795.86 85.46 1.97E-02 1. 92E- 01 8 01 .95 8.69 7.89E-01 2 .17E+OO 1 038.6 1 0.99 -1. 2 3E+Ol 2 .00E+Ol 11 67. 97 1. 79 -4.18E+OO 1.06E+Ol 1365.19 3.02 -2 .86E+OO 5.41E+OO Cs-137 661.66 85.10 6.23E-03 1 .46E-0 1 1.46E-01 Eu-152 121.78 2 8.67 -1. 06E-01 3 .07E-01 3 .07E-01 2 44.70 7.61 2 . 61E-01 1. 3 8E+OO 2 95.94 0.45 1. 39E+Ol 2 .70E+Ol 344. 2 8 26.60 1.53E-01 4.70E-01 367.79 0.86 -1.49E-01 1.49E+Ol 411.12 2 .24 9.89E-01 5.14E+OO 443.96 2 .83 1. 38E+OO 4.75E+OO 488 . 68 0.42 - l.50E+Ol 2.77E+01 563.99 0.49 -2.30E+OO 3.48E+Ol 586.26 0.46 2 .43E+Ol 4. 2 8E+Ol 678.62 0.47 1.65E+Ol 3.17E+Ol 688.67 0.86 -2 .04E-01 1. 3 9E+Ol 719.35 0.28 1.94E+Ol 4.74E+Ol 778.90 12. 96 -9 . 23E-02 1.28E+OO 810 . 45 0. 32 -2 .92E+Ol 5.77E+Ol "867.37 4.26 4.05E-02 3.55E+OO 919.33 0.43 -3.74E+Ol 3.69E+Ol 964. 08 14.65 5.71E-02 1 .48E+OO 1085.87 10. 2 4 -9.74E-01 2 .13E+00 1089.74 1. 73 7.71E+OO 1. 32E+Ol 1112. 0 7 13.69 l . 20E-0 1 1 .00E+OO 1 2 12.95 1. 43 -1.19E+Ol 1. 34E+Ol 1 2 49.94 0.19 3 .52E+Ol 9.59E+Ol 1299.14 1. 63 -5.79E+OO 8.14E+OO 1408.01 2 1. 07 4.17E-01 1. 02E+OO 1457.64 0.50 1.0 8E+02 9.49E+O l 1528.10 0. 2 8 3.90E+Ol 8.67E+Ol Eu-154 123.07 40.40 1.07E- 01 2 . 42E-0 1 2 .42E-01 247.93 6.89 -4.05E-01 1.39E+OO 591.76 4.95 -3.67E+OO 3.09E+OO 692.42 1. 78 -4.81E+OO 6.75E+OO 723. 30 20.06 3.58E-01 8.52E-01 756.80 4.52 -3.17E+00 3.04E+OO 873.18 1 2 .08 3.45E-01 1.08E+OO 996.29 10.48 -2 .46E-01 1.89E+OO

[2637]

3/19/2018 7:32:37PM Page 6 of6 Analysis Report for 19-Mar-18-10015 B1051 OOA-FSWC-163CV 0.0"

0.5" 0.5" Nuclide Energy Yield("/o) Activity Nuc/ideMDA LineMDA Name (pCUgrams) (pCilgrams) (pCilgrams)

(keV)

Eu-154 1004.76 18.01 1.lOE-01 2 .42E-01 9.95E-01 1274.43 3 4.80 -1.30E-0 2 4.35E-01 1596.48 1. 80 4.55E+OO 1. 24E+Ol Eu-155 45.30 1. 31 - 1 .44E+Ol 4.18 E- 01 2 .49E+Ol 60.01 1. 22 1.90E+Ol 2 . 78E+Ol 86 . 55 30.70 2 .33E-01 4 . 90E-01 105.31 21.10 1.35E-01 4.18E-01 Ra-226 186.21 3.64 1. 07E+OO 2 .81E+OO 2 .81E+OO Pa-231 27.36 10.30 1.46E+OO 3.64E+OO 3.64E+OO 283.69 1. 70 -1.lOE+OO 5.58E+OO 300.07 2 .47 -5.88E+OO 3.89E+OO 302.65 2 . 20 2.26E+00 4.53E+OO 330.06 1. 40 -6.99E+OO 8.42E+OO U-235 143.76 10. 96 5.93E-02 1.81E-01 7.92E-01 163.33 5.08 -5 .63E-02 1.74E+OO 185.71 57.20 9.39E-02 1. 81E-01 202 .11 1. 08 -5.98E+OO 7.69E+OO 205.31 5.01 -3.56E-01 1. 99E+OO Am-241 59.54 35.90 3 . 66E-01 9.62E-01 9.62E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2638]

0000024572.CNF Live Time :1200.000 sec Real Time :1200.340 sec 60 start: 1: -0.0(kev) stop : 8192:2047 .8(kev)

Acq. Start :Mon Mar 19 19: 12: 30 2018 55 50 45 40 35

[2639]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: l

3/13/2018 7:54:58PM Page I of6

~pex-Gamma Analysis Report for 13-Mar-18-10018 B105100A-FSWC-179CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10018 Sample Description : B105100A-FSWC-179CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.005E+02 grams Facility : Default Sample Taken On : 3/9/2018 8:39:00AM Acquisition Started : 3/13/2018 7:34:51PM Procedure : Puck_half_inch Operator : Administrator Detector Name :P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.1 seconds Dead Time : 0.09 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24306 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:QO:OOPM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 7:54:54PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2640]

3/13/2018 7:54:58PM Page 2 of6 Analysis Report for 13-Mar-18-10018 B 105100A-FSWC-179CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 661.54 2633 - 2655 2 644. 0 7 1.13E+04 214.50 1. 22E+0 2 1. 41 2 1173.00 4677 - 4':'00 4689.43 4.58E+02 44.99 2 .40E+Ol 1. 83 3 1332.15 5315 - 5338 5326. 2 4 4.38E+02 42.38 5.64E+OO 1. 85 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Co-60 0.98 1173. 2 3

99.85 5.66E+OO 7.18E-01 1332.49

99.98 5. 91E+OO 7 . 42E-01 Cs-137 0.99 661.66

85.10 1.09E+02 1.33E+Ol

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2641]

3/13/2018 7:54:58PM Page 3 of6 Analysis Report for 13-Mar-18-10018 B105100A-FSWC-179CV 0.0" - 0.5" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

Co-60 0.986 5.78E+00 5.16E-01 Cs-137 0.998 1. 09E+02 l.33E+Ol

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2642]

3/13/2018 7:54:58PM Page 4 of6 Analysis Report for 13-Mar-18-10018 B105100A-FSWC-179CV o.o* - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 7:54:54PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCl/grams)

(keV)

An Pk 511. 00 100.00 1.15E-01 7 .32E- 01 7.32E-01 BE-7 477.60 10.4 4 1.0lE+Ol 8.75E+OO 8.75E+00 K-40 1460.82 10.66 5.08E+OO 4.40E+OO 4.40E+OO

+ Co-60 1173.23

99.85 5.66E+OO 1.89E-0 1 3 . 2 6E-01 1332.49

99.98 5.91E+OO 1.89E-01 Nb-94 702.65 99.81 l.14E-01 3 .37E-01 3 .37E-01 871.09 99.89 1. 81E-01 4.58E-01 Ag-108m 79 .13 6.60 -1.66E+OO 3.99E-01 8.39E+OO 433.94 90.50 1.90E-01 9.22E-01 614.28 89.80 6 . 66E-03 6.54E-01 722. 94 90.80 1. 2 3E-01 3.99E-01 Sb-1 2 5 176.31 6.84 l.76E+OO 2 .73E+OO 5.43E+OO 380.45 1. 52 - l.74E+Ol 4.52E+Ol 427.87 2 9.60 l.23E-0 1 2 .73E+OO 463.36 10.49 8.85E-01 8 . 47E+OO 600.60 17.65 1. 30E+OO 3.12E+OO 606.71 4.98 -l.91E+OO 1.16E+Ol 635.95 11. 22 2 .35E+OO 5.04E+OO 671. 4 4 1. 79 9.64E+00 1.63E+Ol

[2643]

3/13/2018 7:54:58PM Page 5 of6 Analysis Report for 13-Mar-18-10018 B1051 OOA-FSWC-179CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCl/grams) (pCl/grams)

(keV)

Ba-13 3 79.61 2 .65 -3.56E+00 9.76E- 01 2 .05E+Ol

81. 00 32 .90 2.07E-01 1.59E+OO 276.40 7.16 5. 2 0E+OO 7.08E+OO 302.85 18.34 5.51E-01 2 .88E+OO 356.01 62.05 - 4.93E-01 9.76E-01 383.85 8 . 94 -1. 24E+OO 7.75E+OO Cs-134 475. 3 6 1. 48 6.32E+Ol 3.99E-01 6.21E+Ol 563.25 8.34 -2 .46E+OO 6.79E+OO 569.33 1 5.37 -1.92E-01 3 .46E+OO 604. 72 97.62 -3 .73E-01 5.87E-0 1 795.86 85.46 2. 50E-01 3 .99E-01 801.95 8.69 l. 2 8E-01 3.76E+OO 10 38.61 0.99 3.16E+Ol 4.04E+Ol 11 67.97 1. 79 -9.00E+OO 6.96E+01 1365.19 3.0 2 l.83E+00 5.72E+OO

+ Cs-137 661. 66

85.10 l.09E+0 2 5.27E-01 5.27E- 01 Eu-152 121.78 2 8.67 6.63E-0 2 9.84E-01 1.17E+00 244.70 7.6 1 -2 . llE+OO 6. 2 2E+OO 295.94 0.45 -2 .75E+OO l. l 6E+0 2 344. 2 8 26.60 -3 .90E-01 2 . 2 4E+OO 367.79 0.86 1 .55E+Ol 7.49E+Ol 411.12 2.24 8.59E+OO 3.25E+Ol 44 3 . 96 2.83 -6.lOE-01 3.00E+Ol 488.68 0.42 9.99E+Ol 1. 74E+02 563.99 0.49 -8.40E+OO l.15E+02 586.26 0.4 6 5.41E+Ol 1.25E+02 678.62 0.47 2 .02E+Ol 6.90E+Ol 688.67 0.86 -3.90E+Ol 3.39E+Ol 719. 35 0.28 1. 29E+02 1. 29E+02 778.90 1 2 .96 -7.94E-01 2.43E+OO 810.45 0 .32 -7.93E+Ol l.09E+02 867.37 4.26 -6.48E+OO 9.85E+OO 919.33 0.43 -4. 1 6E+Ol 1.07E+02 964. 0 8 14.65 - 6.20E-01 3 .09E+OO 10 85.8 7 10.24 2.29E-01 4.17E+OO 10 89.74 1. 73 -l.47E+Ol 2 .61E+Ol 1112. 0 7 13. 69 l.85E+00 3 .56E+OO 1212.95 1. 43 -1.67E+OO 2 . 2 9E+Ol 1249.94 0 . 19 -7.30E+Ol l.18E+02 1299.14 1. 63 8.97E+O O 1. 53E+Ol 14 0 8.01 21. 07 -4.54E-0 1 9.84E-01 1457.64 0.50 8.56E+Ol 9.42E+Ol 1 528.10 0.28 1.08E+Ol 5.21E+Ol Eu-154 123.07 40.40 5.lOE-01 7 .0 6E-01 8.50E-01 247.93 6.89 1 .21E+OO 7.0lE+OO 591.76 4.95 -3 .83E-01 1.07E+Ol 692.42 1. 78 1.92E+OO 1. 71E+Ol 723.30 20.06 5.37E-01 1.80E+OO 756.80 4.52 1.81E+OO 7.40E+OO 873. \8 12.08 2.14E+OO 3.99E+OO 996.29 1 0.48 - 7.91E-01 4. 2 2E+OO

[2644]

3/13/2018 7:54:58PM Page 6 of6 Analysis Report for 13-Mar-18-10018 B1051 OOA-FSWC-179CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCVgrams) (pCl!grams)

(keV)

Eu-154 1004.76 18.01 -2 .62E-01 7.06E- 01 2 .31E+OO 1274.43 34.80 -2 .82E-01 7.06E-01 1596.48 1. 80 -8.90E+OO 1.lOE+Ol Eu-155 45.30 1. 31 1.90E+Ol l.43E+OO 9 . 54E+Ol 60.01 1. 22 -3.98E+Ol 9.61E+Ol 86.55 30.70 2 .04E-01 1.43E+00 105.31 2 1.10 2 .27E-01 l.75E+OO Ra-226 186. 2 1 3.64 5.31E+OO l.08E+Ol 1.08E+Ol Pa-231 2 7.36 10.30 1.44E+Ol 1 . 04E+Ol 1. 04E+Ol 283.69 1. 70 1. 36E+Ol 3.00E+Ol 300.07 2 .47 -2 .13E+Ol 2 .05E+Ol 302.65 2 . 20 8.06E+OO 2 .40E+Ol 330.06 1. 40 9.19E+OO 4. 1 4E+Ol U-235 143.76 10. 96 -9.57E-01 6.82E-01 3.14E+OO 163.33 5.08 -5.54E-01 6.77E+00 185.7 1 57.20 4.66E-01 6.82E-01 202.11 1. 08 - 2 .21E+Ol 3.71E+01 205.31 5.01 3 .05E-01 8.17E+00 Arn-241 59.54 35.90 1.36E+OO 3.42E+00 3.42E+00

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2645]

0000024306.CNF 2000 Live Time :1200.000 sec Real Time :1201.050 sec start: 1: -0.0(kev) stop : 8192: 2047 .S(kev)

Acq. Start :Tue Mar 13 19:34:51 2018 1750 1500 1250 Vl

+-'

§0 1000 I...)

[2646]

750 500 250 g

8 1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/13/2018 9:17:04PM Page 1 of6

~s~pex-Gamma Analysis Report for 13-Mar-18-10019 8105100A-FSWC-179CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10019 Sample Description : B105100A-FSWC-179CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.005E+02 grams Facility : Default Sample Taken On : 3/9/2018 8:39:00AM Acquisition Started : 3/13/2018 8:56:56PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.2 seconds Dead Time : 0.02 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120-8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24308 Certificate Name : Eu 155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on 3/13/2018 9:16:58PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2647]

3/13/2018 9:17:04PM Page 2 of6 Analysis Report for 13-Mar-18-10019 B 1051 OOA°FSWC-179CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238 .70 948 - 961 954.39 4.07E+Ol 18.06 2 .85E+Ol 1.12 2 661. 62 263 6 - 2653 2644.36 1.79E+02 28.87 l.80E+Ol 1. 38 3 1459.95 5831 - 5844 5837.74 2 .72E+Ol 14.48 l.76E+Ol 1. 07 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.88 1 460.82

10.66 3 .73E+OO 2 .0lE+OO Cs-137 1.00 661.66

85. 10 1. 73E+OO 3.48E-01 Pb-212 0.99 115 .18 0.60 238.63

43.60 3 .53E-01 1.67E-01 300.09 3.30

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2648]

3/13/2018 9:17:04PM Page 3 of6 Analysis Report for 13-Mar-18-10019 8105100A-FSWC-179CV 0.0" - 0.511 0.511 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.886 3.73E+OO 2.0lE+OO Cs-137 1. 000 1.73E+OO 3.48E-01 Pb-212 0.999 3.53E-01 1.67E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2649]

3/13/2018 9:17:04PM Page 4 of6 Analysis Report for 13-Mar-18-10019 8105100A-FSWC-179CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 9:16:58PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCi!grams)

(keV)

An Pk 511.00 100.00 2 .46E-01 2 .59E-01 2 .59E-01 BE-7 477.60 10. 4 4 8.70E-01 1. 81E+00 1. 81E+OO

+ K-40 1 460.82

10.66 3.73E+OO 2 .73E+OO 2. 73E+OO Co-60 1173.23 99.85 2 .00E-01 2 .90E-01 3. 14E-01 1332.49 99.98 -6 .17E-02 2 .90E-01 Nb-94 702. 65 99.81 1.15E-01 1. 82E-01 2 .00E-01 871.09 99.89 1.76E-02 1. 82E-01 Ag-108m 79.13 6 . 60 l.55E+OO 1. 41E-01 3 .20E+OO 433.94 90.50 2 .79E-02 1.80E-01 614.28 89.80 -1.76E-01 1.91E-01 72 2 . 94 90.80 -4. llE-0 2 1.41E-01 Sb-125 176.31 6.84 -3 . 13E-01 5.27E- 01 1.43E+OO 380.45 1. 52 -5.42E-01 l.05E+Ol 427.87 2 9.60 -4.49E-02 5.27E-01 463. 3 6 1 0.49 7.54E-02 1.85E+OO 600.60 17.65 -4.35E-02 8.78E-01 606 . 71 4.98 1.21E+OO 4.53E+OO 635.95 11. 22 5.90E-01 1.66E+OO 671.44 1. 79 -4. 2 0E+OO 9.09E+OO

[2650]

3/13/2018 9:17:04PM Page 5 of6 Analysis Report for 13-Mar-18-10019 B105100A-FSWC-179CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi!grams) (pCilgrams) (pCi/grams)

(keV)

Ba-133 79.61 2 .65 3 .40E+OO 2 .88E-01 7.73E+OO

81. 00 32 .90 -2 .18E-0 2 5.38E-01 276.40 7.16 1.02E+OO 1.94E+OO 302.85 18. 3 4 9.41E-02 7.18E-01 356.01 62 .05 -3.36E-01 2 .88E-01 383.85 8.94 -7.98E-01 1.74E+OO Cs-134 475.36 1. 48 4 .13E+OO 2 . 00E-01 1.21E+01 563.25 8.34 1.19E+OO 2 .09E+OO 569.33 15.37 1.20E-01 1.19E+OO 604. 72 97. 62 7.64E-0 2 2 .24E-01 795.86 85.46 7.55E-02 2 .00E-01 801.95 8.69 6.15E-01 1.97E+OO 1038.61 0.99 -3.74E+OO 1.89E+01 1 167.97 1. 79 -1. 1 7E+Ol 1. 60E+Ol 1365.19 3.0 2 4.59E-01 3 .52E+00

+ Cs-137 661.66

85.10 l.73E+OO 2 .06E - 01 2 .06E-0 1 Eu-152 121. 78 2 8.67 -l.63E-01 2 . T'E - 01 2 .77E-01 244.70 7.61 7.67E-01 1.86E+OO 295.94 0.45 2 .35E+OO 3 .48E+Ol 344. 2 8 2 6.60 -4.18E-01 4.65E-01 367.79 0.8 6 -l.31E+Ol 1.63E+Ol 411.1 2 2 .24 1. 72E+OO 7.22E+OO 443. 96 2 .83 -1.lOE+OO 6.34E+OO 488 . 68 0.4 2 1.28E+Ol 3.52E+O l 563.99 0.49 9.78E+OO 3.54E+Ol 586.26 0.46 -4.25E-Ol 4.39E+Ol 67 8. 62 0.47 l.92E+Ol 3 .92E+Ol 688.67 0.86 -5.77E+OO 1 .99E+Ol 719.35 0. 2 8 - 2 .67E+O l 3 .91E+Ol 778.90 12. 96 6.44E-01 1. 2 4E+OO 810.45 0.32 2 . 3 8E+Ol 4.89E+Ol 867.37 4.26 2 .35E+OO 4. 2 5E+OO 919.33 0.43 3.42E+Ol 5.09E+Ol 964.08 14.65 -l.36E+OO 1.75E+OO 1085.87 10.24 -6.58E-01 1. 67E+OO 1089.74 1. 73 -5.07E+OO 1.27E+Ol 1112. 07 13. 69 5.80E-01 1. 7 5E+OO 1 2 12.95 1. 43 -2.37E+Ol 9.91E+OO 1 2 49.94 0. 1 9 3.41E+Ol 9.29E+Ol 1 2 99.14 1. 63 -9.94E+OO 1.27E+Ol 1408.01 2 1. 07 -1.44E+OO 6.50E-01 1457.64 0.50 l.19E+02 9.75E+Ol 1528.10 0.28 2 .16E+Ol 6. 72E+Ol Eu-154 12 3 .07 40.40 -2.08E-02 2 .07E-01 2.07E-0 1 247.93 6.89 -1.02E-0 2 1.79E+OO 591. 7 6 4.95 3.90E-01 3.38E+OO 692.42 1. 78 -5.91E+OO 9.67E+OO 723.30 20.06 -2 . 81E-Ol 6.41E-01 756.80 4. 52 -l.50E+OO 3.47E+00 873.18 12.08 -l.04E-0 1 1.51E+OO 996. 2 9 10.48 -2 .37E-01 1.82E+OO

[2651]

3/13/2018 9:17:04PM Page 6 of6 Analysis Report for 13-Mar-18-10019 81051 OOA-FSWC-179CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)

Eu-154 1004.76 18.01 -3 .16E-01 2 .07E-01 1.07E+OO 1274.43 34.80 1 .50E-01 4.69E-01 1 596.48 1. 80 O.OOE+OO 2 .53E+OO Eu-155 45.30 1. 31 l.94E+OO 4.67 E- 01 2 .87E+Ol 60.01 1. 2 2 3 .15E+OO 2 .58E+Ol 86.55 3 0.70 7.66E-02 4.76E-01 105. 3 1 2 1.10 5.52E-02 4.67E-01 Ra- 22 6 186. 2 1 3 .64 -3 .20E-01 2. 83E+OO 2.83E+OO Pa- 231 27.36 10.30 1.65E+OO 3 .69E+OO 3.69E+OO 28 3 .69 1. 70 l.04E+OO 8.0lE+OO 300.07 2 .47 -6.16E+OO 4.88E+OO 30 2 .65 2 . 20 - 6.47E-01 5.89E+OO 330.06 1. 40 -l.79E+OO l.OOE+Ol U-235 143.76 10. 96 l.90E-01 l .84E-01 9.09E-01 1 63.33 5.08 2 .99E-01 1.85E+OO 185.71 57.20 2.61E-02 1. 84E-01 2 02 .11 1. 08 -5.17E-01 9.02E+OO 205.31 5.0 1 -9.12E-02 l . 90E+OO Arn-241 59.54 35.90 2 .31E-01 9.19E-01 9.19E-0 1

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

'? = CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level

[2652]

0000024308.CNF Live Time 1200.000 sec 60 Real Time 1200.230 sec start: 1 -0.0(kev) stop : 8192 2047 .S(kev)

Acq. Start Tue Mar 13 20: 56: 56 2018 55 50 45 r-I V,

u

[2653]

1000 2000 3000 4000 5000 6000 7000 8000 Channel

~

ROI Type: 1

3/29/2018 8:37:14AM Page I of6

.~ ~~pex-Gamma Analysis Report for 29-Mar-18-10012 B105100A-FSWC-190CV 0.0" -1.0" 0.0" GAMMA SPECTRUM ANAL YS/S Sample Identification : 29-Mar-18-10012 Sample Description : B105100A-FSWC-190CV 0.0" - 1.0" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.806E+02 grams Facility : Default Sample Taken On : 3/10/2018 1:00:00PM Acquisition Started : 3/29/2018 7:52:19AM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch

.Live Time : 1200.0 seconds Real Time : 1201.4 seconds Dead Time : 0.12 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/29/2018 Efficiency Calibration Description Sample Number : 24820 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2018 8:37:11AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2654]

3/29/2018 8:37:14AM Page 2 of6 Analysis Report for 29-Mar-18-10012 B105100A-FSWC-190CV 0.0" - 1.0" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 1460.38 2914 - 2927 2920.81 4.66E+Ol 17.34 2.07E+Ol 2.44 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0. 96 1460.82

10.66 3.15E+OO 1. 20E+OO

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2655]

3/29/2018 8:37:14AM Page 3 of6 Analysis Report for 29-Mar-18-10012 8105100A-FSWC-190CV 0.0" - 1.0" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0. 969 3.15E+OO 1.20E+OO

? = nuclide.is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2656]

3/29/2018 8:37:14AM Page 4 of6 Analysis Report for 29-Mar-18-10012 B105100A-FSWC-190CV o.o* - 1.0" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/29/2018 8:37:11AM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS {°/a) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi!grams) (pCilgrams) (pCl/grams)

(keV)

An Pk 511. 00 100.00 2 .79E-01 2 .08E-01 2. 08E-01 BE-7 477.60 10.44 -7.62E-01 1.05E+OO l .OSE+OO

+ K-40 1460.82

10.66 3.15E+OO l.42E+OO 1. 42E+OO Co- 60 1 173.23 99.8 5 -1. OlE-01 1. 35E-01 1.40E-01 13 32 .49 99.98 8.73E-02 l.35E-01 Nb-94 702.65 99.81 - 2 .63E-0 2 1.03E-01 1.03E-01 871. 09 99.89 2.47E-0 2 1.04E-01 Ag-108m 79.13 6.60 -5.32E-01 8.52E-02 1.74E+OO 433.94 90.50 6 . 87E-04 8. 5 2 E-0 2 614.28 89.80 -1.81E-01 1. 2 4E-01 72 2 . 94 90.80 -5.08E-03 1.07E-01 Sb-1 2 5 176.31 6.84 -'.2 .08E-01 2.61E- 01 l . 15E+OO 380.45 1. 52 1.64E-01 5.44E+OO 427.87 2 9.60 -1.03E-01 2 .61E-01 463.36 10.49 2 .05E-0 1 8.56E-01 600.60 17.65 -8.34E-02 6.27E-01 606.71 4.98 2.42E+OO 2 .99E+OO 635.95 11. 22 3.43E-02 7.34E-01 671.44 1. 79 -9.47E-01 5.08E+00

[2657]

3/29/2018 8:37:14AM Page 5 of6 Analysis Report for 29-Mar-18-10012 B1051 OOA-FSWC-190CV 0.0" - 1.0" 0.0" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi!grams) (pCl/grams) (pCl/grams)

(keV)

Ba-133 79.61 2 . 65 -2 .20E+OO 1. 76E-0 1 4.03E+OO

81. 00 32.9 0 -1.32E-01 3.20E-01 276.40 7.16 2 .37E-01 1.20E+00 302.85 18.34 3.56E-01 5.36E-01 356.01 62.05 3.53E-0 2 1. 76E-01 383.85 8.94 1.31E-0 1 9.06E-01 Cs-134 475.36 1. 48 - 1.lOE+OO l.09E-0 1 6.33E+OO 563.25 8.34 3.17E-01 1.19E+OO 569.33 15.37 4.24E-01 7.17E-01 604.7 2 97. 62 7.91E-02 1.49E-01 795.86 85.46 -1.07E-02 1.09E-01 8 01 .95 8.69 -6 .13E-01 1.04E+OO 1038.61 0.99 -3.0lE+OO 1. 05E+Ol 1167.97 1. 79 2 .84E+OO 8.79E+OO 1365.19 3.0 2 -5.16E-01 2 .86E+OO Cs-13 7 661. 66 85.10 6.67E-02 1 .38E-0 1 1.38E-01 Eu-152 121.78 2 8.67 2 .70E-02 2 .62E-0 1 2 .62E-01 244.70 7.6 1 -1.04E+00 1. 07E+OO 295.94 0.45 7.82E+00 2.08E+Ol 344. 2 8 2 6.60 -1.59E-01 3.04E-01 367.79 0.86 4.37E-01 9.22E+OO 411.12 2.24 -1.83E+OO 3.64E+OO 44 3 .96 2.83 5.32E-01 3.14E+OO 488.68 0.42 -1.38E-01 2.05E+Ol 563.99 0.49 5.81E+OO 2 .02E+Ol 586. 2 6 0.46 -1.19E+OO 2 .lOE+Ol 678. 62 0.47 -1.15E+Ol 1.75E+Ol 688.67 0.86 5.63E+OO 1.18E+Ol 719.35 0.28 2.09E+OO 3.29E+Ol 778.90 12.96 4. 2 8E-01 8.92E-01 810.45 0.32 1. 2 3E+Ol 3 .46E+Ol 867.37 4.26 -3 .42E-0 1 2 . 2 1E+00 919.33 0.43 2 .74E+00 2 .83E+Ol 964. 08 1 4.65 -l . 49E-0 1 8.33E-01 1085.87 1 0. 2 4 6.25E-01 1.07E+OO 1089.74 1. 73 6.75E-02 6.09E+OO 1112. 07 13. 69 -4.67E-01 7.80E-01 1 2 12.95 1. 43 -4.02E+OO 6.84E+OO 1249.94 0.19 2 .79E+Ol 7.05E+Ol 1299.14 1. 63 3.03E-01 6.30E+00 1408.01 21. 07 2 .66E-02 6.00E-01 1457.64 0.50 1. 31E+OO 5.87E+Ol 152 8.10 0. 2 8 2 .13E+Ol 4.37E+Ol Eu-154 1 23 .07 40.40 -4.0lE-02 1. 78E-0 1 1.78E-01 2 47.93 6.89 4.0lE-01 1. 1 8E+OO 591.76 4.95 3.51E-01 2.08E+OO 692.42 1. 78 -2 .64E+OO 5.47E+OO 723.30 2 0.06 3.93E-02 5.00E-01 756.80 4.52 -6.23E-01 2 .46E+OO 873. 1 8 12.08 3. 71E-01 9.21E-01 996.29 10.48 2 .89E-01 1.16E+OO

[2658]

3/29/2018 8:37:14AM Page 6 of6 Analysis Report for 29-Mar-18-10012 B105100A-FSWC-190CV o.o* - 1.0* 0.0" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCl/grams) (pCUgrams) (pCUgrams)

(keV)

Eu-154 1004.76 18.01 -2. 79E-01 1.78E-01 5.55E-01 1274.43 34.80 -3 .58E-02 3. 2 2E-01 1596.48 1. 80 -1.51E+OO 4.84E+00 Eu-15 5 45.30 1. 31 1. 3 1E+OO 3.2 5E-01 1. 83E+Ol 60.01 1. 22 3 .89E+OO 2.19E+Ol 86 . 55 30.70 -1.45E-0 2 3.25E-01 105.31 21.10 1.31E-01 3.74E-01 Ra-226 186. 2 1 3.64 1.08E+OO 2 .52E+OO 2 .52E+OO Pa-23 1 2 7.36 10.30 1.12E+OO 1.94E+OO 1.94E+OO 283.69 1. 70 6.07E-01 4.61E+00 300.07 2 .47 -2 .72E+00 3.56E+OO 302.65 2 . 20 2 .95E+OO 4.45E+00 330~06 1. 40 -2.57E+OO 5.87E+OO U- 2 35 143.76 10. 96 -1.65E-Ol l.60E-Ol 6.57E-01 163.33 5.08 1.78E-01 l.46E+OO 185.71 57.20 8.38E-02 l.60E-01 2 02 .11 1. 08 - 5.63E+OO 7.06E+OO 2 05.31 5.01 -4.70E-02 1.67E+00 Am-241 59.54 35.90 4.82E-01 7.67E-01 7.67E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

, = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2659]

0000024820.CNF Live Time :1200.000 sec Real Ti11e :1201.440 sec Start: 1: 0. l(kev) stop : 4096:2047.l(kev)

ACq. Start :Thu Mar 29 07 :52:19 2018

[2660]

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/29/2018 8:44:42AM Page I of6

~pe>c-Gamma Analysis Report for 29-Mar-18-10013 B105100A-FSWC-190CV 0.0" - 1.0" 1.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 29-Mar~ 18-1 0013 Sample Description : B105100A-FSWC-190CV 0.0" - 1.0" 1.0" Sample Type : Puck Unit Sample Point Sample Size 1.806E+02 grams Facility : Default Sample Taken On : 3/10/2018 1:00:00PM Acquisition Started : 3/29/2018 8:24:28AM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.6 seconds Dead Time : 0.13 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/29/2018 Efficiency Calibration Description Sample Number : 24816 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2018 8:44 :38AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2661]

3/29/2018 8:44:42AM Page 2 of6 Analysis Report for 29-Mar-18-10013 B105100A-FSWC-190CV 0.0" - 1.0" 1.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 1460.44 2915 - 2925 2920.94 3.75E+Ol 14.22 1.lOE+Ol 1. 55 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.97 1460.82

10.66 2.53E+OO 9.86E-01

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2662]

3/29/2018 8:44:42AM Page 3 of6 Analysis Report for 29-Mar-18-10013 B105100A-FSWC-190CV 0.0" - 1.0" 1.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.977 2.53E +OO 9.86E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@* - nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2663]

3/29/2018 8:44:42AM Page 4 of6 Analysis Report for 29-Mar-18-10013 B105100A-FSWC-190CV 0.0" - 1.0" 1.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/29/2018 8:44:38AM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M :a First peak in a multiplet region m :a Other peak in a multiplet region F :a Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCi/grams)

(keV)

An Pk 511. 00 100.00 2 . 2 1E-01 1.82E-01 1.82E-01 BE-7 477.60 10.44 -7.56E-0 1 9.27E-01 9.27E-01

+ K-40 1460.8 2

10.66 2.53E+00 1. 02E+OO l.02E+OO Co-60 1173. 23 99.85 8.16E-02 1 .21E-01 1. 4 7E-01 1332. 49 99.98 -5.04E-04 1. 2 1E-01 Nb-94 70 2 .65 99 . 81 7.97E-02 9.78E-02 1.08E-01 871.09 99.89 -3 .51E-02 9.78E-0 2 Ag-108m 79.13 6.60 1.33E-01 1. 04E-01 1.70E+OO 433.94 90.50 -2 .35E-03 1. 05E-01 614.28 89.80 -7 . llE-02 1.39E-01 722 . 94 90.80 -1.94E-02 1.04E-01 Sb- 125 176.31 6.84 2 .14E-01 3 .30E-01 1. 2 6E+OO 380.45 1. 52 -3 .86E+OO 5.59E+OO 427.87 29.60 1.09E-01 3.30E-01 463.36 10.49 2 .39E-01 1. 02E+OO 600.60 17.65 3.88E-02 4.89E-Ol 606.71 4.98 2 .51E+OO 2 .89E+OO 635.95 1 1. 22 -l.89E-01 8.02E-01 671. 44 1. 79 -8.12E-01 4.93E+OO

[2664]

3/29/2018 8:44:42AM Page 5 of6 Analysis Report for 29-Mar-18-10013 B1051 OOA-FSWC-190CV 0.0" -1.0" 1.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCilgrams) (pCl/grams)

(keV)

Ba-133 79.61 2 .65 -9.91E-01 1.47E-01 3.89E+OO

81. 00 32.90 -1.69E-01 2 .77E-01 276.40 7.16 2.38E-01 1. 14E+OO 302 . 85 1 8.34 1.93E-01 4.72E-01 356 . 01 62.05 -1 . 59E-02 1. 4 7E-01 383.85 8.94 - 1. 56E-01 1. OlE+OO Cs-134 475.36 1. 48 2 . 66E+O*O 1. 09E-0 1 6.12E+OO 563.25 8.34 6.89E-01 1.19E+OO 569.33 15.37 -2 .87E-01 5.98E-01 604. 72 97.6 2 1.28E-0 2 1. 27E-01 795.86 85.46 4.67E-04 1 . 09E-01 801.95 8.69 1.16E-01 9. llE-01 1038.61 0.99 -2 .15E+OO 1.09E+Ol 1167.97 1. 79 3 .40E+OO 7.84E+OO 1365.19 3.0 2 -5.16E-01 2 .86E+OO Cs-137 661.66 85.10 -1.59E-03 1.33E-01 1. 33E-01 Eu-1 52 12 1. 78 28.67 -3.00E-02 2 . 39E-01 2 .39E-01 2 44.7 0 7.61 4.02E-01 l .17E+OO 295.94 0.45 5.37E+OO 2 .05E+Ol 344. 2 8 26.60 -2 .20E-01 2 .84E-Ol 367.79 0.86 -1.12E+OO 9.87E+OO 411 . 12 2.24 1.31E+OO 4.09E+OO 443 . 96 2.83 -1.30E+OO 2 .66E+OO 488.68 0.42 2.86E+OO 2.24E+Ol 563.99 0.49 8.45E+OO 1. 91E+Ol 586. 2 6 0. 46 7.86E+OO 2 .41E+Ol 678.62 0.47 -3.00E+OO 1.92E+Ol 688 . 67 0.86 -5 . 80E-01 1.07E+Ol 719.35 0.28 1. 24E+O l 3.84E+Ol T:7 8.90 12. 96 -4 . 49E-02 7.24E-01 810 . 45 0. 32 -1.99E+OO 2 .57E+Ol 867.37 4.26 -4. 70E-01 2.52E+OO 919.33 0.43 -2. 15E+OO 3 . 03E+O l 964. 08 14.65 -4.58E-01 7.66E-Ol 1085.87 10.24 -4.08E-Ol 1.07E+OO 1089.74 1. 73 -4.15E+OO 6.58E+OO 1112.07 13. 69 - 6.91E-01 7.46E-01 1212.95 1. 43 2.42E+00 9.96E+OO 1249.94 0. 1 9 -9.31E+OO 5.27E+01 1299.14 1. 63 -5.18E+OO 5.50E+OO 1408.01 2 1. 07 -8. 31E-02 6.00E-01 1457.64 0.50 4.19E+Ol 5.18E+Ol 1528.10 0. 2 8 - 8.64E+OO 2 .97E+Ol Eu-154 123.07 40.40 -1.60E-02 1 . 72E-01 1. 72E-01 247.93 6.89 9.82E-02 l.22E+OO 591.76 4.95 -5.62E-01 1 .71E+OO 692.4 2 1. 78 -1.21E+OO 5.03E+OO 723. 3 0 2 0.06 1.65E-02 4 . .73E-01 756.80 4.52 3.38E-01 1.82E+OO 873. 1 8 12.08 5.24E-01 8.95E-01 996. 2 9 10.48 - 6.lOE-01 1.13E+OO

[2665]

3/29/2018 8:44:42AM Page 6 of6 Analysis Report for 29-Mar-18-10013 81051 OOA-FSWC-190CV 0.0" -1.0" 1.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCl/grams) (pCilgrams)

(keV)

Eu-154 1004.76 18.01 2 .05E-01 1. 72E-01 6.60E-01 1274.43 34.80 -1.91E-01 2 .33E-01 1596.48 1. 80 1.27E+OO 7.12E+OO Eu-155 45.30 1. 31 4.79E+OO 2 .92E-01 1.78E+Ol 60.01 1. 22 -5.36E+OO 1. 84E+Ol 86.55 30.70 5. 2 5E-0 2 2 .92E-01 105. 3 1 2 1.10 -8.51E-02 3.40E-01 Ra-226 186. 2 1 3.64 -7.14E-Ol 2 . 2 5E+OO 2 .25E+OO Pa-231 2 7. 3 6 10.30 5.67E-01 1.77E+OO 1.77E+00 283 .69 1. 70 9.94E-01 4.92E+OO 300.07 2 .47 -3 .lOE+OO 3 .14E+OO 3 02.65 2 . 20 1.60E+OO 3 .92E+OO 330.06 1. 40 3.63E+OO 6.38E+OO U- 23 5 143.76 10. 96 -2 .09E-01 1.48E-01 6.42E-01 163. 33 5.08 4.36E-01 1.67E+OO 185. 71 57.20 -7.79E-03 1.48E-01 202 .11 1. 08 -1.14E+OO 7.06E+OO 205. 3 1 5.01 -6.63E-01 1. 54E+OO Am-241 59.54 35.90 -4.15E-01 6.03E-01 6.03E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2666]

0000024816.CNF Live Time 1200.000 sec Real Time 1201.620 sec 60 Start : 1 O.l(kev)

Stop : 4096 2047. l(kev)

Acq. start Thu Mar 29 08: 24 : 28 2018 55 50 45 40 35

[2667]

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/14/2018 5:55:52PM Page 1 of6

~~~pex-Gamma Analysis Report for 14-Mar-18-10034 B105100A-FSWC-201CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10034 Sample Description : B105100A-FSWC-201CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 9.668E+01 grams Facility : Default Sample Taken On : 3/10/2018 8:00:00AM Acquisition Started : 3/14/2018 5:35:45PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.03 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description Sample Number : 24362 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 5:55:48PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2668]

3/14/2018 5:55:52PM Page 2 of6 Analysis Report for 14-Mar-18-10034 B1051 OOA-FSWC-201 CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 661.43 2636 - 2651 2643.62 7.00E+Ol 17.43 3.95E+OO 0.88 2 1460.05 5831 - 5846 5838.12 3.30E+Ol 13. 43 8.00E+OO 1. 69 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.90 1460.82

10.66 4.70E+OO 1. 96E+OO Cs-137 0.99 661.66

85.10 7.0SE-01 1. 95E-01

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2669]

3/14/2018 5:55:52PM Page 3 of6 Analysis Report for 14-Mar-18-10034 B105100A-FSWC-201CV 0.0" - 0.5" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.908 4.70E+OO 1. 96E+OO Cs-137 0. 992. 7.05E-01 1.95E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2670]

3/14/2018 5:55:52PM Page4 of6 Analysis Report for 14-Mar-18-10034 B105100A-FSWC-201CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 5:55:48PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCl/grams) (pCi/grams)

(keV)

An Pk 511.00 100.00 1.85E-01 2 .61E-01 2 .61E-01 BE-7 477.60 10.44 2 .88E-01 1. 36E+OO 1.36E+OO

+ K-40 1460.82

10.66 4.70E+OO 2 .09E+OO 2 .09E+OO Co-60 1173.23 99.85 8 . 25E-02 2 .SlE-01 2.SlE-01 1 332 .49 99.98 1.83E-01 2 .83E-01 Nb-94 702.65 99.81 1.07E-01 1. 96E-01 1.98E-01 871.09 99.89 6.68E-02 1. 96E-01 Ag-108m 79 .13 6.60 -1.40E+OO 1.66E-01 2.74E+OO 433.94 90.50 l.71E-02 l.66E-01 614.28 89.80 7.27E-02 2 .63E-01 722 . 94 90.80 4.78E-02 2 .16E-01 Sb-1 2 5 176. 3 1 6.84 3.23E-01 4.58E-01 l.34E+OO 380.45 1. 52 4.13E+OO 9.57E+OO 427.87 2 9.60 6.03E-02 4.58E-01 463.36 10.49 -3 .98E-01 1. 41E+OO 600.60 17.65 5.0SE-01 9.42E-01 606.71 4.98 4.24E+OO 4.85E+OO 635.95 11. 22 3 .92E-01 1.34E+OO 671.44 1. 79 1.58E+OO 9.78E+OO

[2671]

3/14/2018 5:55:52PM Page 5 of6 Analysis Report for 14-Mar-18-10034 B105100A-FSWC-201CV o.o* - o.5" 0.0" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCilgrams) (pCi!grams) (pCi/grams)

(keV)

Ba- 133 79.61 2 .65 2 .22E-01 2. 71E - 01 7 . 04E+OO

81. 00 32 .9 0 -2 .18E-01 4.93E-01 2 76.40 7.16 -9.37E-01 1.65E+OO 302.85 18 . 3 4 2 .80E-01 7.35E-01 356. 01 62. 05 -2 .77E-01 2 .71E-01 383.85 8 . 94 -6.50E-01 1. 31E+00 Cs - 134 475.36 1. 48 1 . 08E+OO 1. 91E-01 l . 05E+Ol 563. 2 5 8.34 1.54E-01 1.78E+OO 569.33 15.37 - 7.48E-02 8. 2 1E-01 604. 72 97.62 -2 .50E-01 1.91E-01 795.86 85.46 7.52E-03 2 .32E-01 80 1 .95 8.69 5.31E-01 l .96E+OO 1038.61 0.99 -1.50E+OO 2 .16E+Ol 1167. 97 1. 79 3 .53E+OO 1. 45E+Ol 1365.19 3.0 2 3 .81E+OO 7.84E+OO

+ Cs-137 661.66

85.10 7.05E-01 l.12E-01 l.12E-01 Eu-15 2 121. 78 2 8.67 -1.61E-01 3.39E-01 3.39E- 01 244.70 7.6 1 8.45E-01 l.51E+ OO 295.94 0.45 8.45E+OO 3.18E+Ol 344.28 26.60 -2.27E-01 5.03E-01 367.79 0 .86 -4.29E+OO l. 43E+Ol 411.12 2 .24 l.59E+OO 7.39E+OO 443. 96 2 .83 1. 2 7E+00 5.30E+OO 488.68 0.42 -l.15E+Ol 4.02E+Ol 563.99 0.49 2 .70E -t 00 2 .90E +Ol 586. 2 6 0.46 2 .18E+Ol 4.57E+Ol 678.62 0.47 l. 2 9E+Ol 2 .88E+Ol 688.67 0.86 -8.90E+OO l.77E+Ol 719.35 0.28 -3.75E+Ol 5.63E+Ol 778.90 12. 96 5.42E-01 l.45E+OO 810.45 0.32 -2 . 95E+Ol 5.58E+01 867.37 4.26 1. 32E+OO 4.59E+OO 919.33 0.43 1.91E+00 4.95E+Ol 964. 08 14.65 -1.73E-01 l. 26E+OO 1 085.87 10. 2 4 -3. 96E-01 1.33E+OO 1 089.74 1. 73 -l.20E+00 9.60E+OO 111 2 .07 13.69 1.86E-01 l.49E+OO 1212.95 1. 43 2 .lOE+OO 1. 59E+Ol 1249.94 0.19 2 .13E+Ol 7.94E+Ol 1 299.14 1. 63 2. 54E+OO 9.49E+00 1 408.01 2 1.07 -4.19E-0 2 9.51E-01 1 457.64 0.50 1. 2 1E+02 1.00E+02 1528.10 0. 2 8 -2 .41E+Ol 7.62E+Ol Eu-154 123.07 40.40 5.14E-02 2 .46E-01 2 .46E-01 247.93 6.89 -1. 79E+OO 1. 30E+OO 591.76 4.95 -7.62E-01 3.21E+OO 692.42 1. 78 -2 .82E+O O 8.61E+OO 723. 3 0 2 0.06 4.26E-0 1 l.OlE+OO 7 56 _. 8 0 4.52 -1.69E+OO 4. 2 1E+OO 873.18 12.08 -6 . 3 4E-0 1 1.63E+OO 996. 2 9 10.48 4.41E-01 1.98E+OO

[2672]

3/14/2018 5:55:52PM Page 6 of6 Analysis Report for 14-Mar-18-10034 B 1051 OOA-FSWC-201 CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCi/grams) (pCilgrams)

(keV)

Eu-154 1004.76 18.01 5. 13E-01 2 .46E-01 1.06E+OO 1274.43 34.80 -3 .03E-01 5.32E-01 1596.48 1. 80 3 .65E+OO 1 .14E+Ol Eu-155 45. 3 0 1. 31 1.28E+Ol 3.99E-01 3. 2 2E+Ol 60.01 1. 22 1. 2 9E+00 3 .05E+Ol 86.55 30.70 - 1 .3 3E-01 4 . 45E-01 105.31 21.10 - 1.73E-01 3.99E-01 Ra-22 6 186. 2 1 3.64 3.70E+OO 3.65E+OO 3.65E+OO Pa-231 2 7. 3 6 10.30 2 .78E+OO 3 .84E+OO 3.84E+OO 2 83.69 1. 70 4.67E-01 7.31E+OO 300.07 2 .47 -5.49E+OO 5.07E+OO 302.65 2 . 20 4.34E+OO 6 .3 1E+OO 330.06 1. 40 -1. 22E+OO 9. 2 6E+OO U-235 143.76 10. 96 4.02E-02 2 .34E-01 8.88E-01 163. 33 5 .08 9.94E-01 2 .13E+OO 185.7 1 57.20 1.83E-01 2 .34E-01 202 .11 1. 08 4.02E-01 8.93E+OO 205.31 5.01 -4.51E-01 1.77E+OO Am-241 59.54 35.90 2 .07E-01 1.07E+OO 1.07E+OO

+ = Nuclide identified during the nuclide identification

=Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level

[2673]

0000024362.CNF Live Time :1200.000 sec Rea1 Ti r,e : 1200. 310 sec 60 start: 1: -0.0(kev) stop : 8192: 2047 .8(kev)

Acq. Start :Wed Mar 14 17:35:45 2018 55 50 45

[2674]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/14/2018 11 :04:03PM Page I of6

~~~pex-Gamma Analysis Report for 14-Mar-18-10035 B105100A-FSWC-201CV o.o* - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10035 Sample Description : B105100A-FSWC~201CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 9.668E+01 grams Facility : Default Sample Taken On : 3/10/2018 8:00:00AM Acquisition Started : 3/14/2018 10:43:56PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.03 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120-8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description Sample Number : 24384 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : .3/14/2018 11 :03:59PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2675]

3/14/2018 11:04:03PM Page 2 of6 Analysis Report for 14-Mar-18-10035 B 1051 OOA-FSWC-201 CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (keV) 1 238.61 949 - 960 954.00 2.50E+Ol 14.85 2.40E+Ol 0.40 2 661.39 2637 - 2651 2643.45 5.93E+Ol 16.75 7.50E+OO 1.18 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Cs-137 0.98 661.66

85.10 5.96E-0 1 1.83E-01 Pb-212 1. 00 115 .18 0.60 2 38.63

43.60 2 . 2 5E-0 1 1. 3 9E-01 300.09 3.30

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2676]

3/14/2018 11:04:03PM Page 3 of6 Analysis Report for 14-Mar-18-10035 B105100A-FSWC-201CV 0.0" - 0.5" 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

Cs-137 0.988 5. 96E-01 1.83E-01 Pb-212 1. 000 2.25E- 01 1.39E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2677]

3/14/2018 11 :04:03PM Page 4 of6 Analysis Report for 14-Mar-18-10035 B105100A-FSWC-201CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 11 :03:59PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCl/grams) (pCi/grams)

(keV)

An Pk 511. 00 100.00 1.00E-01 2 .56E-0 1 2. 56E-01 BE-7 477.60 10.44 - 2 .53E-01 1. 58E+OO 1.58E+OO K-40 1460.8 2 10.66 3 .28E+OO 4.16E+OO 4.16E+00 Co-6 0 1173. 2 3 99.85 9.42E-02 2 . 3 1E- 01 2 .59E-01 1332 .49 99.98 1.12E-0 1 2 . 3 1E-01 Nb-94 702.65 99.81 -8.82E-02 1.62E-01 1.62E-01 871.09 99.89 2.91E-02 l.72E-01 Ag-108m 79.13 6.60 1.99E+OO 1.70E-01 2 .61E+OO 433.94 90.50 -7.llE-02 1.70E-01 614. 2 8 89.80 -2.57E-01 2.2 4E-01 72.2.94 90.80 2 . 51E-0 2 1 .81E-01 Sb-125 176.31 6.84 -2.04E-01 5.16E-01 1.41E+OO 380 . 45 1. 52 2.12E+O O 9.57E+OO 427.87 2 9.60 -1.16E-02 5.16E-01 463.36 10.49 7.53E-01 1.67E+OO 600.60 17.65 3.0SE-01 9.98E-01 606.71 4.98 5.SlE+OO 5.37E+OO 635.95 11. 2 2 3 . 87E-Ol l.40E+OO 671. 44 1. 79 6.79E+OO 1.0lE+Ol

[2678]

3/14/2018 11 :04:03PM Page 5 of6 Analysis Report for 14-Mar-18-10035 B1051 OOA-FSWC-201 CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCi/grams)

(keV)

Ba- 133 79. 61 2 .65 2 .07E+OO 2 .49E-01 6.13E+OO

81. 00 32 .90 -4.64E-01 4. 2 1E-01 276.40 7.16 - 1.14E+OO 1. 3 9E+OO 302.85 18. 3 4 2 . 2 4E-01 6.76E-01 356.01 62.05 -1. 2 1E-01 2 .49E-01 383.85 8.94 -5.30E-01 1. 57E+OO Cs-134 475.36 1. 48 -1.04E+Ol 1 .99E-01 9.97E+OO 563.25 8.34 -4.83E-01 2 .12E+OO 569.33 15.37 1. 09E-01 1.13E+OO 604. 72 97. 62 -6.95E-02 2 .47E-01 795.86 85.46 3. 2 6E-02 1. 99E-01 801.95 8 . 69 6.82E-01 1.66E+OO 1038.61 0.99 -7.49E+OO 1 .63E+O l 1167.97 1. 79 6.53E+OO 1.35E+Ol 1365.19 3.0 2 9.54E-01 4.61E+OO

+ Cs-137 661.66

85.10 5. 96E-01 1. 42E-01 1. 42E-01 Eu-152 121. 78 2 8.67 -8.78E-02 2 .93E-01 2.93E-01 244.70 7.6 1 8.32E-01 1 .51E+OO 295.94 0.45 1.96E+OO 3.22E+Ol 344.28 2 6.60 4.86E-0 3 3.20E-01 367.79 0.86 1.49E+OO 1 .60E+Ol 411.1 2 2 .24 3 . 3 9E+OO 6.60E+OO 443.96 2 .83 3 .14E+OO 6.30E+OO 488.68 0.42 -1.98E+OO 2 .79E+Ol 563.99 0.49 -1.82E+Ol .3 . 41E+Ol 586.26 0.46 2 .68E+Ol 4.57E+Ol 678.62 0.47 -2 .31E+Ol 2.88E+Ol 688.67 0.8 6 1 .06E+OO 2.27E+Ol 719.35 0.28 1. 27E+Ol 6.79E+Ol 778.90 12.96 -5 . l lE-01 1. 34E+00 810.45 0.32 1. 2 9E-01 4.52E+Ol 867.37 4. 2 6 -4. 3 8E+OO 3 .81E+OO 919.33 0.43 -5.72E+OO 4.39E+Ol 964.08 14.65 8.63E-02 1.26E+OO 1 085.87 10.24 7.13E-01 1.74E+OO 1 089.74 1. 73 5.64E+OO 1. 1 6E+Ol 111 2. 07 13. 69 -4.63E-01 1.13E+OO 1 2 12.95 1. 43 8.29E+OO 1.59E+Ol 1249.94 0.19 -7.lOE+OO 6.86E+Ol 1299.14 1. 63 3.39E+OO 1 . 06E+Ol 1408.01 21. 07 -2.18E-02 8. 72E-01 1 457.64 0.50 7.67E+Ol 8.80E+Ol 1528.10 0.28 1.12E+Ol 5.42E+Ol Eu-154 123.07 40.40 -5.89E-02 2 .08E-01 2 .08E-01 247.93 6.89 -7.57E-01 1.43E+OO 591.76 4. 95 -3,41E-Ol 3.lOE+OO 692.4 2 1. 78 3.61E+OO 1.13E+Ol 723. 30 20.06 -1.25E-0 1 7.87E-01 756.80 4 .52 -2.79E-0 1 3.06E+OO 873. 1 8 12.08 -4.55E-01 1. 2 7E+OO 996. 2 9 1 0.48 7.36E-01 2 .14E+OO

[2679]

3/14/2018 11:04:03PM Page6 of6 Analysis Report for 14-Mar-18-10035 B 105.100A-FSWC-201 CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCi/grams) (pCi/grams)

(keV)

Eu-154 10 04.76 18.01 -4. 3 3E-01 2 . 0 8E- 01 1. llE+OO 1274.43 3*4. 80 3.91E-0 2 6 . 09E-01 1596.48 1. 80 -1.44E+Ol 8.82E+OO Eu-155 45.30 1.31 1 .27E+Ol 4.45E-01 2. 94E+Ol 60.01 1. 22 -3 .83E+OO 2 .53E+Ol 86.55 30.70 2 .16E-01 4.95E-01 105.31 2 1.10 -3 . 0lE-01 4.45E-01 Ra-2 2 6 186.2 1 3.64 1.80E+OO 3.12E+OO 3.12E+OO Pa-231 27.36 10.30 2 .43E+OO 4.13E+OO 4 . 13E+OO 283.69 1. 70 1.84E+OO 8.00E+OO 300 . 07 2 .47 -8.91E-02 5.25E+OO 302.65 2 . 20 4.80E-01 5.63E+OO 330.06 1. 40 5.49E+OO 9.26E+OO U-235 143.76 10.96 -1.41E-01 1.98E-0 1 8. 1 4E-Ol 163.33 5.08 1.12E+OO 2 .03E+OO 185.71 57. 2 0 1.16E-01 1.98E-01 202.11 1. 08 -8 .93E+OO 7.77E+OO 205.31 5.01 1.34E-01 2 .13E+OO Am-241 59.54 35.90 1. 33E-02 9.03E-01 9.03E-01

+

. == Energy Nuclide identified during the nuclide identification line found in the spectrum

> = MDA va!ue not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2680]

0000024384.CNF Live Time :1200.000 sec 60 Real Time :1200.310 sec start: 1: -0.0(kev) stop : 8192:2047.S(kev)

Acq. Start :wed Mar 14 22:43:56 2018 55 50 45

[2681]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/14/2018 5:55:59PM Page 1 of7 Analysis Report for 14-Mar-18-10036 B105100A-FSWC-210CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10036 Sample Description : B105100A-FSWC-210CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.204E+02 grams Facility : Default Sample Taken On : 3/10/2018 8:22:00AM Acquisition Started : 3/14/2018 5:35:52PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 352 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.02 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120-8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 3/12/2018 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description : install Sample Number : 24363 Certificate Name : Eu155-Na22 Certificate Date : 12/20/2011 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 5:55:55PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2682]

3/14/2018 5:55:59PM Page 2 of7 Analysis Report for 14-Mar-18-10036 B105100A-FSWC-210CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 185.77 739 - 750 743.79 2 .17E+Ol 16.76 3 .86E+Ol 0.76 2 351.98 1 403 - 1412 1407.92 2 .46E+Ol 12.52 l.27E+Ol 0.46 3 609.29 2 431 - 2442 2436.43 2 .31E+Ol 11. 50 7.72E+00 0.35 4 661.70 2 638 - 2653 2645.97 8.22E+O l 19.34 7.63E+OO 1. 40 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Cs-137 1. 00 661.66

85.10 6.73E-01 l.78E-01 Bi-211 0.87 351.07

13. 02 8.25E-Ol 4.40E-Ol Bi-214 1. 00 609.32

45.49 3.34E-01 1. 71E-01 768.36 4.89 806.18 1. 26 934.06 3 . 11 1120.29 14.92 1155.2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385. 31 0.79 1401. 5 2 1. 33 1407.99 2 .39 1509. 2 1 2 .13

[2683]

3/14/2018 5:55:59PM Page 3 of7 Analysis Report for 14-Mar-18-10036 B 1051 OOA-FSWC-21 OCV 0.0" - 0.5" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1. 00 1661. 27 1. 05 1729.59 2 .88 1764.49 15.30 1847.43 2 .03 2118.51 1.16 Pb-214 1. 00 2 41.99 7.25 2 95. 22 1 8.42 351.93

35.60 3 .02E-01 1.61E-01 785. 96 1. 06 Ra-22 6 0. 96 186.21

3.64 1.70E+OO 1. 3 4E+OO U-235 1. 00 143.76 10.96 163. 33 5.08 185.71

57. 2 0 1.08E-01 8.53E-02 202.11 1. 08 205.31 5.01

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

Cs-137 1.000 6.73E-01 1 . 78E-01

? Bi-211 0.876 8.25E-01 4.40E-01 Bi-214 1. 000 3.34E-01 1.71E-01

? Pb-214 1.000 3 .02E-01 1.61E-01

0. 969 1 .70E+OO 1. 34E+OO

~ R();- ~~

?

? 1...,..o.e-o 1 .08E-0 1 8.53E-02 D-d3b ~\~ \ \Je:cJQ. i 6/~-1i

[2684]

3/14/2018 5:55:59PM Page4 of7 Analysis Report for 14-Mar-18-10036 B105100A-FSWC-210CV 0.0" - 0.5" 0.0"

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2685]

3/14/2018 5:55:59PM Page 5 of7 Analysis Report for 14-Mar-18-10036 B105100A-FSWC-210CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 5:55:55PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCl/grams)

(keV)

An Pk 511. 00 1 00.00 2. 36E-01 2.22E- 01 2 .22E-01 BE-7 477.60 10.44 -5 .08E-02 1.44E+00 1. 44E+OO K-40 1460.82 10.66 3 .66E+OO 3 .77E+OO 3. 77E+OO Co-60 1173.23 99.85 1.24E-01 2 .0lE-01 2 .0lE-01 1 332 .49 99.98 6.46E-02 2 .73E-01 Nb-94 70 2 .65 99.81 - 1 .47E-02 1.31E-01 1.51E-01 871. 09 99.89 2 .70E-03 1.31E-01 Ag-108m 79 .13 6.60 2 .35E-01 1 .34E-01 2 . 96E+OO 433.94 90.50 -l.09E-01 1.34E-01 614.~8 89.80 -3.74E-02 2 .30E-01 722.94 90.80 7.53E-02 1.98E-01 Sb-125 176.31 6.84 1.07E-01 4.60E - 01 1.40E+OO 380.45 1. 52 4.78E-01 8.07E+00 427.87 29.60 6.16E-0 3 4.60E-01 463.36 10.49 1.18E+OO 1. 58E+OO 600.60 17.65 1.74E-01 8.98E-01 606.71 4. 98 3.97E-01 4.33E+OO 635.95 11. 22 3.69E-01 1. 54E+OO 671.44 1. 79 -1.28E+OO 6.48E+OO

[2686]

3/14/2018 5:55:59PM Page 6 of7 Analysis Report for 14-Mar-18-10036 B1051 OOA-FSWC-21 OCV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCi/grams) (pCilgrams)

(keV)

' Ba-1 33 79 . 61 2 .65 1 . 82E+OO 2 .51E-01 7.31E+OO 81 . 00 32 .90 -3 .33E-02 5.12E-01 276.40 7.16 -2 .67E-01 1. 58E+OO 30 2 .85 18.34 -4. llE-01 5.94E-01 356.01 62.05 -1 . 42E-01 2 .51E-01 383.85 8.94 2 .17E-01 1.45E+OO Cs-134 475.36 1. 48 -5.57E+OO 1.93E-01 9.80E+OO 563.25 8.34 -1.12E-01 1. 78E+OO 569.33 15.37 -4.49E-01 9.93E-01 604. 72 97.62 -1.85E-01 2 .26E-01 795.86 85.46 1 .30E-01 1 .93E-01 801.95 8.69 -4.45E-01 1 .66E+OO 1038.61 0.99 -1. 2 7E+Ol 1. 41E+Ol 1167.97 1. 79 -2 .73E+OO 9.92E+OO 1365.19 3 .0 2 l.07E+OO 6.87E+OO

+ Cs-137 661.66

85.10 6.73E-01 1.1 7E-01 1.1 7E-01 Eu-1 52 121.78 2 8.67 1. 2 6E-0 1 3 .59E-01 3.59E-01 244.70 7.61 7.40E-01 1.74E+OO 295.94 0.45 -8.30E-01 2 .95E+Ol 344.28 26.60 -9.31E-0 3 4.41E-01 367.79 0.86 2 .88E+OO 1.38E+Ol 411.12 2 .24 -l.75E+OO 6.00E+OO 443. 96 2 .83 l.07E+OO 4.84E+OO 488.68 0.42 1 .69E+0 1 3.44E+Ol 563.99 0.49 - 6.62E-0 1 3.14E+01 586. 2 6 0.46 1. 32E+Ol 4.05E+Ol 678.62 0.47 -3 .18E-01 3.03E+Ol 688.67 0.86 6.91E+OO l.68E+Ol 719.35 0. 2 8 -2 .49E+Ol 5.50E+Ol 778.90 12 . 96 2 .94E-01 1. 04E+OO 810.45 0. 32 1.31E+O l 4.30E+Ol 867.37 4. 26 4.64E-01 3 .06E+OO 919.33 0.43 - 5.61E+OO 3 .68E+Ol 964.08 14.65 2 .00E-01 l. 3 6E+OO 1085.87 10. 2 4 -6.87E-01 1. 79E+OO 1089.74 1. 73 9.90E-01 1. lOE+Ol 111 2 . 07 13. 69 -6.75E-01 1. 41E+OO 1212.95 1. 43 -6.36E+OO 1. 21E+Ol 1249.94 0.19 4.54E+Ol 9.34E+Ol 1299.14 1. 63 -4.17E+OO l.06E+Ol 1408.01 2 1.07 -6.27E-01 6.24E-01 1 457.64 0.50 :. 2 8E+Ol 7.99E+Ol 1 528.10 0.28 -7.14E+O l 6.07E+Ol Eu-154 123.07 40.40 -4.88E-02 2.32E- 01 2. 32E-01 247.93 6.89 4. 3 1E-01 1.64E+OO 591.76 4.95 1 .31E+00 2 .79E+OO 692.42 1. 78 -2 .63E+OO 7.89E+OO 723.30 20.06 3. 60E-01 9.18E-01 756.80 4. 52 7.80E-0 2 3.41E+OO 873. 1 8 12.08 -l.31E+OO l.15E+OO 996. 2 9 10.48 4.42E-01 1 . 72E+OO

[2687]

3/14/2018 5:55:59PM Page 7 of7 Analysis Report for 14-Mar-18-10036 B1051 OOA-FSWC-21 OCV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCUgrams) (pCilgrams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 -5 .41E-01 2 . 32E-01 8.90E-01 1274.4 3 34.80 -2 .79E-02 4.87E-01 1596.48 1. 80 1 . 45E+OO 7.0lE+OO Eu-155 45.30 1. 31 -2. 17E+OO 4.06E-01 3.16E+Ol 60.01 1. 2 2 -3 .lOE+Ol 2.89E+Ol 86.55 30.70 -6 .14E-01 4.06E-01 105.31 21.10 -1.59E-01 5.12E-01

+ Ra-226 186. 2 1

3.64 1.70E+OO 2 .07E+OO 2 .07E+OO Pa-231 2 7. 3 6 10. 3 0 3 .23E+OO 4.16E+OO 4.16E+OO 2 83.69 1. 70 6.34E-01 7 . 22E+OO 300.07 2 .47 -3 .73E+OO 4.59E+OO 302.65 2 . 20 5.21E-02 5. llE+OO 330.06 1. 40 -4.16E+OO 7.84E+OO

+ U- 235 143.76 10. 96 5.54E-01 l. 32E-01 9.39E-01 163.33 5.08 1. 1 7E+OO 1.93E+OO 185.71

57. 2 0 1.08E-01 1. 32E-01

~02 .11 1. 08 -3.79E+00 9.21E+00 205.31 5.01 8.75E-02 2 .00E+OO Am-241 59.54 35.90 -1.89E-01 1.lOE+OO 1.lOE+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform lhe decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence ievei

[2688]

0000024363.CNF Live Time :1200.000 sec 60 Real Time :1200.250 sec start: 1: -0.2(kev) stop : 8192:2046.9(kev)

Acq. Start :wed Mar 14 17:35:52 2018 55 50 45

[2689]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/14/2018 6:18 :28PM Page 1 of 6

~~~pex-Gamma Analysis Report for 14-Mar-18-10037 B105100A-FSWC-210CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10037 Sample Description : B105100A-FSWC-210CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.204E+02 grams Facility : Default Sample Taken On : 3/10/2018 8:22:00AM Acquisition Started : 3/14/2018 5:58:13PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 352 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 3/12/2018 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description : install Sample Number : 24366 Certificate Name : Eu155-Na22 Certificate Date : 12/20/2011 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 6:18:24PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2690]

3/14/2018 6:18:28PM Page 2 of6 Analysis Report for 14-Mar-18-10037 81051 OOA-FSWC-210CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.68 949 - 960 955.21 3 .66E+Ol 16.7 8 2 .68E+Ol 0. 71 2 294.94 1176 - 1184 1179.97 2 .05E+Ol 11.0 2 9.06E+OO 0.91 3 608.83 2430 - 2 442 24 3 4.58 2 .65E+Ol 13. 2 4 1. 30E+Ol 0.82 4 661.61 2636 - 2 655 2645.61 1.82E+02 30 .13 2 .52E+Ol 1. 56 5 1460.28 5834 - 5848 5841.47 2 .21E+Ol 14.78 2 .18E+Ol 1. 36 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.95 1460.82

10.66 2 .SlE+OO 1.69E+OO Cs-137 1. 00 661 . 66

85.10 1.49E+OO 3 .0SE-0 1 Pb-212 1. 00 115 .18 0.60 238.63

43.60 2.77E-01 1. 35E-01 300.09 3.30 Bi-214 0.98 609.32

45.49 3.82E-01 1.96E-01 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120. 2 9 1 4.92 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99

[2691]

3/14/2018 6:18:28PM Page 3 of6 Analysis Report for 14-Mar-18-10037 B 105100A-FSWC-21 OCV 0.0" - 0.5" 0.5" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi - 2 14 0.98 1385. 31 0.79 1401.52 1. 33 1407.99 2 .39 1509. 2 1 2 .13 1661. 2 7 1. 05 1729. 5 9 2 .88 1764.49 15.30 1847.43 2 .03 2 118. 51 1.16 Pb-2 14 0.99 2 41. 99 7.25 2 95. 22

18.42 4.22E-0 1 2 . 3 7E-01 351.93 35.60 785.96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.953 2 .51E+OO 1 .69E+OO Cs-137 1.000 1.49E+OO 3 .05E-01 Pb-212 1. 000 2 .77E-01 1.35E-01 Bi-214 0.984 3 .82E-01 1. 96E-01 Pb-214 0.996 4 .22E- 01 2 .37E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2692]

3/14/2018 6:18:28PM Page 4 of6 Analysis Report for 14-Mar-18-10037 8105100A-FSWC-210CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 6:18:24PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (ke V) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCUgrams) (pCi!grams)

(keV)

An Pk 511. 00 100.00 1.21E-01 2 .37E-01 2 .37E-01 BE-7 477.60 10.44 6.50E-01 1.78E+00 1.78E+OO

+ K-40 1460.82

10.6 6 2 .51E+OO 2 .52E+OO 2 .52E+OO Co-60 1173.23 99.85 2 .88E-0 2 1.86E-01 1.86E-01 133 2 .49 99.98 2 .13E-01 2 .67E-01 Nb-94 702.65 99.81 - 2 .54E-02 1.64E-01 1.73E-01 871. 09 99.89 -4.73E-02 1.64E-01 Ag-108m 79.1 3 6.60 2.29E-01 1.70E-01 3.44E+OO 433.94 90.50 -6.63E-02 1.81E-01 614.28 89.80 -2.63E-01 2 .44E-01 722. 94 90.80 1. 32E-02 1.70E-01 Sb-125 176.31 6.84 -2 .43E-01 5.49E-01 1.56E+OO 380.45 1. 52 1.86E+OO l.OoE+Ol 427.87 2 9.60 -3 . 72E-01 5.49E-01 463.36 10.49 5 .50E-01 1.70E+OO 600.60 17.65 5 .44E-01 9.91E-01 606.71 4.98 4.26E+OO 4.85E+OO 635.95 11. 22 1.06E-01 1. 22E+OO 671. 44 1. 79 7.09E+OO 9.15E+OO

[2693]

3/14/2018 6:18:28PM Page 5 of6 Analysis Report for 14-Mar-18-10037 B1051 OOA-FSWC-21 OCV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCUgrams) (pCi/grams) (pCi/grams)

(keV)

Ba-133 79.61 2 .65 8. 3 6E-02 2 .35E-01 8.32E+OO

81. 00 32 .90 -4.48E-01 5.91E-01 2 76.40 7.16 5.60E-01 1.80E+OO 302.85 18.34 7.98E-0 2 6.61E-01 356.01 62.05 -1.20E-01 2 .35E-01 383.85 8.94 1.06E+OO 1. 81E+OO Cs-134 475.36 1. 48 1. llE+OO 1. 60E-01 1.19E+Ol 563.25 8.34 6. 2 3E-01 1.82E+OO 569.33 15.37 - 8.13E-01 9.00E-01 604. 72 97. 62 - 1.47E-01 2 .38E-01 795.86 85.46 2 .81E-02 1.60E-01 801.95 8.69 -5.24E-02 1.91E+OO 1038.61 0.99 2 .69E+OO 2 .06E+Ol 1167.97 1. 79 3.95E+OO 1.04E+O l 1365.19 3.0 2 3.05E+OO 6.26E+OO

+ Cs-137 661.66

85.10 1. 49E+OO 2 . 0 9E-01 2 .09E-01 Eu- 1 52 12 1 .78 2 8.67 7. 1 5E-02 3.89E-01 3 .89E-01 244.70 7.61 7.32E-01 1.59E+OO 295.94 0.45 2 .37E+Ol 3.13E+Ol 344. 2 8 2 6.60 -1.07E-01 5.lOE-0 1 367.79 0.86 4.27E+OO 1 .68E+Ol 411.12 2 .24 4.45E+OO 7. 2 0E+OO 443.96 2 .83 2 .36E+OO 6.24E+OO 488.68 0.42 -1.70E+OO 3 .57E+Ol 563.99 0.49 --1. 09E+Ol 2 .94E+Ol 586.26 0.46 1.54E+Ol 4.51E+Ol 678.62 0.47 4. 72E+OO 3 .13E+Ol 688.67 0.86 -2.19E+Ol 1 .57E+Ol 719.35 0.28 3.17E+Ol 5.15E+Ol 778.90 12.96 -1.05E-01 1.08E+00 810.45 0.32 2 .35E+Ol 5.19E+Ol 867.37 4.26 -6.35E-01 3.70E+OO 919.33 0.43 -8.37E+00 3.68E+Ol 964. 08 14.65 -1.80E-01 1.28E+OO 1085.87 1 0.24 9.54E-01 1 . 72E+OO 1089.74 1. 73 -2 . 51E+OO 9.77E+OO 1112. 07 13. 69 1. OlE-01 1.13E+OO 1212.95 1. 43 -1.0lE+Ol 1.39E+Ol 1 249.94 0.19 -9.37E+Ol l.07E+0 2 1299.14 1. 63 7.46E+00 l. 2 7E+Ol 1408.01 21.07 2 .23E-01 6.95E-0 1 1457.64 0.50 1.03E+0 2 8 .2 6E+Ol 1528.10 0.28 2 .23E+Ol 6.07E+Ol Eu-154 123.07 40.40 -1. 28E-01 2 .52E-01 2 .52E-01 247.93 6.89 - l.60E-01 1.60E+OO 591.76 4.95 - 6.73E-01 3.30E+OO 692.4 2 1. 78 6.52E+OO 1.0lE+Ol 723. 30 2 0.06 2 .33E-01 7.92E-0 1 756.80 4. 52 2 .70E-01 3 .05E+OO 873. 1 8 12.08 1.92E-01 1. 50E+OO 996. 2 9 10.48 1.50E+OO 1.99E+OO

[2694]

3/14/2018 6:18:28PM Page 6 of6 Analysis Report for 14-Mar-18-10037 B 1051 OOA-FSWC-21 OCV o.o* -o.s* 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCVgrams) (pCl/grams)

Eu-154 1004.76 18.01 -3.82E-Ol 2 .52E-0 1 1.04E+OO 1274.43 34.80 -7.23E-01 3.90E-01 1596.48 1. 80 2.90E+00 9.05E+OO Eu-155 45.30 1. 31 -3.66E+OO 5. llE-01 3.40E+Ol

60. 01 1. 22 -1.18E+Ol 3 .17E+Ol 86.55 30 . 70 - 3.17E-Ol 5. llE-01 105.31 2 1.10 - 1. 2 5E-01 5.29E-01 Ra-22 6 186.21 3.64 1. 3 1E+OO 3.39E+O O 3.39E+OO Pa- 23 1 27.36 10. 3 0 1.49E+OO 4.0lE+OO 4.0lE+OO 2 83.69 1. 70 4.57E-02 6.44E+OO 300.07 2. 47 -5.14E+OO 5.18E+00 302.65 2 . 20 8.65E-01 5.58E+OO 330. 0 6 1. 40 3.61E+OO 9.25E+OO U-235 143.76 10. 96 1 . 87E-01 2. 1 7E-0 1 9.64E-01 163.33 5.08 1.69E+OO 2 .06E+OO 185.71 57. 2 0 6.67E-0 2 2 .17E-01

.202.11 1. 08 1. 40E+oo

l.13E+Ol 205.31 5.01 -4.76E-01 2 .38E+OO Am-241 59.54 35.90 -7.82E-01 1.05E+OO 1 . 05E+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2695]

0000024366.CNF Live Time :1200.000 sec Real Time :1200. 270 sec 60 Start: 1: -0 .2(keV)

Stop : 8192: 2046. 9(kev)

Acq. start :wed Mar 14 17 :58:13 2018 55 50 45

[2696]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/14/2018 7:05:16PM Page I of7

~pex-Gamma Analysis Report for 14-Mar-18-10038 B105100A-FSWC-231 CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10038 Sample Description : B105100A-FSWC-231CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.327E+02 grams Facility : Default Sample Taken On : 3/10/2018 8:30:00AM Acquisition Started : 3/14/2018 6:45:08PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.4 seconds Dead Time : 0.12 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description Sample Number : 24367 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 7:05:12PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2697]

3/14/2018 7:05:16PM Page 2 of7 Analysis Report for 14-Mar-18-10038 B 1051 OOA-FSWC-231 CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.55 473 - 480 477.28 2.92E+Ol 24.91 1. 24E+02 0.69 2 609.4 1 1214 - 1:23 1218.4 1 3.24E+Ol 15.4 2 2 .32E+O l 1. 22 3 661. 7 9 1318 - 1327 1323 .12 6.52E+Ol 17.17 7 . 52E+OO 1. 66 4 911.29 1818 - 1826 1 822.02 1.41E+Ol 10.08 9.71E+OO 0.94 5 1461. 25 2916 - 2927 2 922.55 5.54E+Ol 16 . 37 9 .13E+OO 1. 64 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.97 1460.82

10 .66 5.lOE+OQ 1 .57E+OO Cs-137 0.99 661.66

85.10 4.32E-01 1 .25E-01 Pb-21 2 0.99 115 .18 0 .60 238.63

43.60 1. 78E-01 1.54E-01 30 0 . 0 9 3.30 Bi-21 4 0.99 609.3 2

45.49 3.79E-01 1 .86E-0 1 768.36 4.89 806.18 1. 2 6 934.06 3.11 112 0 . 2 9 1 4.92 1155. 2 1 1. 63 1238.1 2 5.83 1 2 8 0 .98 1. 43 1 377.67 3 .99

[2698]

3/14/2018 7:05:16PM Page 3 of?

Analysis Report for 14-Mar-18-10038 B105100A-FSWC-231CV 0.0" - 0.5" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi -2 14 0.99 1385. 31 0.79 1401. 52 1. 33 1407.99 2.39 1509. 2 1 2.13 1661. 2 7 1. 05 1729 . 59 2.88 1764.49 15.30 1847.43 2 .03 2118.51 1.16 Ac-228 1. 00 1 2 9.07 2 .42 2 09. 2 5 3.89 2 70. 2 4 3.46 328.00 2.95 338 . 32 11 .2 7 409.46 1. 92 463.00 4.40 794.95 4. 25 911.20

2 5.80 3.86E-01 2 .77E-01 964. 77 4.99 968.97 15.80 1588.20 3. 22

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy iine not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0. 9 72 5.lOE+OO 1.57E+OO Cs - 1 3 7 0.99 7 4.32E-01 1.25E-01 Pb -2 1 2 0.999 1.78E-01 1.54E-01 Bi-214 0.999 3.79E-01 1.86E-01 Ac-228 1.000 3.86E-01 2.77E-01

[2699]

3/14/2018 7:05:16PM Page 4 of7 Analysis Report for 14-Mar-18-10038 B105100A-FSWC-231CV 0.0" - 0.5" 0.0"

? ::; nuclide is part of an undetermined solution X ::; nuclide rejected by the interference analysis

@ ::; nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2700]

3/14/2018 7:05:16PM Page 5 of7 Analysis Report for 14-Mar-18-10038 B105100A-FSWC-231CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 7:05:12PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCUgrams) (pCilgrams)

(keV)

An Pk 511. 00 100.00 3 .66E-01 2 .40E-01 2 .40E-01 BE-7 477.60 10.44 7.88E-02 1. 2 7E+OO 1. 2 7E+OO

+ K-40 1460.82

10.66 5.lOE+OO 1. 33E+OO 1. 33E+OO Co-6 0 1173. 2 3 99.85 -1.22E-03 1. 83E-01 2 .20E-01 1332.49 99.98 6.61E-02 1.83E-01 Nb- 94 702.65 99.81 2 . 2 1E-02 1 .37E-01 1.37E-0 1 87 1. 09 99.89 6.58E-0 2 l.55E-01 Ag-108m 79 .13 6.60 3 .74E-0 1 1. 43E-0 1 2 .46E+OO 433.94 90.50 -1.15E-02 1.43E-01 614.28 89.80 -5.41E-03 2 .02E-01 722. 94 90.80 2 .70E-02 1.53E-01 Sb-125 176.31 6.84 6.57E- 01 4.33E - 01 1. 86E+OO 380.45 1. 52 -1.95E+OO 7.43E+OO 427.87 2 9.60 -1.55E-0 2 4.33E-01 463.36 10.49 -6.05E-01 1.03E+OO 60 0 .60 17.65 -l.15E-01 6.94E-01 606.71 4.98 -8.18E-01 4.14E+OO 635.95 11. 22 8.65E-01 1. 45E+OO 671.44 1. 79 3.22E+OO 7.22E+OO

[2701]

3/14/2018 7:05:16PM Page 6 of7 Analysis Report for 14-Mar-18-10038 B1051 OOA-FSWC-231 CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

Ba- 133 79.61 2 .65 -1.45E+OO 2 .33E-01 5 . 60E+OO

81. 00 3 2 .9 0 -1. 2 9E-01 4.lOE-01 276.40 7. 1 6 3.59E-01 1.64E+OO 302.85 1 8.34 4.25E-01 6.79E-01 356.01 62.05 6.94E-04 2 .33E-01 383.85 8.94 4.88E-0 2 1. 32E+OO Cs-134 475. 3 6 1. 48 -6.73E-01 l . 52E-01 8.22E+OO 563. 2 5 8.34 -2.llE-01 1.40E+OO 569.33 1 5.37 -1.55E-01 7.48E-01 604. 72 97. 62 -3. 2 7E-02 1.87E-01 795.86 85.46 9.40E-03 1. 52E-01 801.95 8.69 -1. 39E-02 1.45E+OO 1 038.61 0.99 -2 .81E+OO 1.21E+Ol 1167.97 1. 79 2 .44E+OO 1. 16E+Ol 1 365. 1 9 3.02 -2 .00E+OO 4.51E+OO

+ Cs-137 661.66

85.10 4.32E-01 8.46E-02 8.46E-02 Eu-152 121.78 2 8.67 4.39E-03 3.16E-0 1 3. 1 6E-01 244.70 7.61 -4.45E-01 1.41E+OO 2 95.94 0 . 45 8.29E+OO 2 .88E+0 1 344. 2 8 26 .60 -2 .75E-01 4.67E-01 367.79 0.86 7.57E-01 1.39E+01 411.12 2 .24 1 .64E+OO 6.09E+OO 443.96 2 .83 3.80E-01 4.70E+OO 488.68 0.42 3 . 23E+OO 3.13E+Ol 563.99 0.49 -1.40E+OO 2 . 3 8E+Ol 586.26 0.46 -l.50E+OO 3. 2 3E+01 678.62 0.47 6.28E+OO 2 .75E+Ol 688.67 0.86 3.44E+OO 1.53E+Ol 719. 35 0.28 -9.41E+OO 4 . 17E+Ol 778.90 12. 96 2.28E-0 1 9.83E-0 1 810.45 0.32 - 4.55E+OO 3.94E+Ol 867.37 4. 2 6 -2.87E-01 3.52E+OO 919.33 0.43 4.14E+OO 3.34E+Ol 964. 0 8 14.65 -1.16E+OO 9.0lE-01 1085.87 10.24 -7.44E-0 2 1. 61E+OO 1089.74 1. 73 -8.78E-0 1 8.93E+OO 1112. 07 13. 69 8.47E-02 1.0lE+OO 1212.95 1. 4 3 3.68E+OO 1. 16E+Ol 1249.94 0.19 2 .74E+Ol 9.86E+Ol 1299.14 1. 6 3 3.24E+OO 9.91E+OO 1 408.01 2 1. 07 1.87E-01 7.02E-01 1457.64 0.50 -6.32E+OO 8 . 09E+Ol 1 528.10 0.28 3.61E+01 7.03E+Ol Eu-154 123.07 40.40 9.90E-0 3 2 .19E-01 2. 19E-01 247.93 6.89 -3.55E-01 1. 42E+OO 591.76 4.95 -4.82E-Ol 2.32E+OO 692.42 1. 78 -6.55E-01 7.42E+OO 723. 30 2 0.06 3.83E-01 7.44E-01 756.80 4.52 1. 50E-01 2 .76E+OO 873.18 12.08 -l.18E-01 1.18E+OO 996. 2 9 10.48 -4.46E-01 1.49E+00

[2702]

3/14/2018 7:05:16PM Page 7 of7 Analysis Report for 14-Mar-18-10038 B105100A-FSWC-231 CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCi!grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 3.20E-02 2 .19E-01 9.21E-01 1274.43 34 .80 -7.38E-02 4.37E-01 1596. 48 1. 80 1.17E+OO 1.0lE+Ol Eu-155 45.30 1. 31 - 8. 2 4E+00 3. 96£-01 2 .33E+Ol

60. 0 1 1. 22 8.54E+OO 2 .81E+Ol 86.55 30.70 8.48E-0 2 3. 96E-01 1 05.31 21.10 3. 2 0E-01 5.51E-01 Ra-226 186. 2 1 3.64 1.12E+OO 3.37E+OO 3.37E+OO Pa-231 2 7.36 10.30 9.86E-01 2 .56E+OO 2 .56E+00 2 83.69 1. 70 6.20E-01 7.20E+OO 300.07 2 .47 -5.19E+OO 4.63E+OO 302.65 2 . 20 3.54E+00 5.66E+OO 330.06 1. 4 0 -2.45E+OO 7.98E+OO U-2 35 143.76 10. 96 -3. 3 6E-0 1 2 . llE-01 8.16E-01 163. 33 5 . 08 -8.lOE-01 2. 19E+OO 185.7 1 57.20 9.66E-02 2 . llE-01 202 .11 1. 08 3.42E+OO 1. 09E+Ol 205.31 5.01 -8.77E-01 2 .16E+OO Am-241 59.54 35.90 3.48E-01 9.71E-01 9. 71E-01

+

. = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA vaiue is inconsistent with Currie MDA at 95% confidence level

[2703]

0000024367 .CNF Live Time :1200.000 sec Real Time :1201.400 sec start: 1: 0. l(kev)

Stop : 4096:2047.l(kev)

Acq. start :wed Mar 14 18:45:08 2018

[2704]

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/14/2018 7:31:57PM Page l of6

~pex-Gamma Analysis Report for 14-Mar-18-10039 8105100A-FSWC-231CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10039 Sample Description : 8105100A-FSWC-231CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.327E+02 grams Facility : Default Sample Taken On : 3/10/2018 8:30:00AM Acquisition Started : 3/14/2018 7:11:49PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.4 seconds Dead Time : 0.11 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description Sample Number : 24369 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 7:31 :53PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2705]

3/14/2018 7:31 :57PM Page 2 of6 Analysis Report for 14-Mar-18-10039 8105100A-FSWC-231CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 661.85 1319 - 1328 1323.24 3.14E+Ol 16.06 2.92E+Ol 1. 09 2 1460.72 2916 - 2929 2921.49 6.14E+Ol 16.19 3.12E+OO 2.10 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82

10.66 5.65E+OO 1. 57E+OO Cs-137 0.99 661.66

85.10 2.08E-01 l.09E-01

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2706]

3/14/2018 7:31:57PM Page 3 of6 Analysis Report for 14-Mar-18-10039 B105100A-FSWC-231CV 0.0" - 0.5" 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.998 5.G5E+00 1.57E+OO Cs-137 0.994 2.08E-01 1.09E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2707]

3/14/2018 7:31:57PM Page 4 of6 Analysis Report for 14-Mar-18-10039 B105100A-FSWC-231CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 7:31:53PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCUgrams) (pCi/grams)

(keV)

An Pk 511.00 100.00 3 .24E-01 2 .40E-01 2 .40E-01 BE-7 477.60 10.44 6.02E-Ol 1. 23E+OO 1. 23E+OO

+ K-40 1460.8 2

10.66 5.65E+OO 8.93E-01 8.93E-01 Co-60 1173.23 99.85 7.92E-02 2 .06E-01 2 .07E-01 1332.49 99.98 9.77E-02 2 .06E-01 Nb-94 702.65 99.81 5.84E-02 9.98E-02 1 . 66E-01 871. 09 99.89 -2.39E-02 9.98E-02 Ag-108m 79.13 6.60 -l.43E-01 1. llE - 01 2.34E+OO 433.94 90.50 -3.68E-0 2 1. llE-01 614. 2 8 89.80 -1.lOE-01 1. 71E-01 722.94 90.80 7.22E-02 1. 53E-01 Sb-125 176. 3 1 6.84 5.24E-01 3.14E-01 1.70E+00 380.45 1. 52 2.22E+OO 8.31E+OO 427.87 2 9.60 -2.32E-01 3.14E-01 463.36 10.49 -3.53E-01 1.23E+OO 600.60 17.65 -6.59E-02 7.73E-01 606.71 4.98 2.04E+OO 3.62E+00 635.95 11. 22 -3.88E-01 1. 2 4E+OO 671. 44 1. 79 -3 .61E+OO 6.84E+OO

[2708]

3/14/2018 7:31:57PM Page 5 of6 Analysis Report for 14-Mar-18-10039 B1051 OOA-FSWC-231 CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) .(pCi/grams) (pCilgrams)

(keV)

Ba-13 3 79.61 2 . 65 -8.37E-01 2. 07E-01 5.60E+OO

81. 00 32 .90 -8.85E-02 4.17E-01 276.40 7.16 -1.00E+OO l. 36E+OO 302.85 1 8.34 l.84E-01 6.96E-01 356.01 62.05 -3 .17E-02 2 .07E-01 383.85 8.94 -7 .74E-0 2 1. 34E+OO Cs-134 475.36 1. 48 -3 . 2 8E-01 l . 30E-01 7 . 15E+OO 563.25 8.34 l. 2 4E+OO 1 .79E+OO 569.33 15.37 2 . 96E-01 8.55E-01 604. 72 97.62 2 .34E-02 1.70E-01 795.86 85.46 -1.16E-01 1 .3 0E-01 801.95 8.69 -l.39E-01 1. 45E+OO 1038.61 0.99 1.57E+OO 1.46E+Ol 11 67. 97 1. 79 1. 54E+OO 1. 05E+Ol 1365.19 3.0 2 -l.61E-01 5.79E+OO

+ Cs- 137 661.66

85.10 2 .08E-01 l.48E-01 l.48E-01 Eu-15 2 121.78 2 8.67 6.26E-02 3.42E-01 3.42E-01 244.70 7.61 -l. 2 5E-01 l.51E+OO 295.94 0.45 8.39E+OO 2 .78E+Ol 344.28 2 6.60 -3 .98E-02 4.43E-01 367.79 0.86 l.79E+OO l.41E+Ol 411 .12 2.24 2.70E+OO 6.09E+OO 443.96 2.83 2.52E+OO 4.58E+OO 488.68 0.42 -2 .90E+OO 2 .SOE+Ol 563.99 0.49 1. 2 3E+Ol 2 .94E+Ol 586. 2 6 0.46 3.59E+Ol 4.06E+Ol 678.62 0.47 4.25E+OO 2 .96E+Ol 688.67 0.86 -4.86E+OO 1.40E+Ol 719.35 0.28 1. 04E+Ol 4.46E+Ol 778.90 12. 96 5.28E-02 8.41E-01 810.45 0.32 7.64E+OO 4.58E+Ol 867 . 37 4.26 -l.08E+OO 2 . 62E+OO 919.33 0.43 2 .07E+OO 3.45E+Ol 964.08 14.65 5.37E-01 l.lOE+OO 1 085.87 10. 2 4 9.65E-02 1. 2 0E+OO 1 089.74 1. 73 l.93E+OO 7.13E+OO 11 12. 07 13. 69 -3 .28E-01 7.98E-01 1 2 12.95 1. 43 -3.92E+OO 9. 2 9E+OO 1249.94 0.19 -2 .76E+Ol 7. 1 6E+Ol 1299.14 1. 63 -6.77E+OO 9.48E+OO 1408.01 2 1.07 3.61E-01 7.42E-01 1457.64 0.50 -9.73E+OO 8.03E+Ol 1528.10 0. 2 8 l.80E+Ol 4.91E+Ol Eu-154 123.07 40.40 -8.45E-0 2 2 . 2 8E-01 2 . 2 8E-O l 247.93 6.89 2 .86E-01 1. 70E+OO 591.76 4.95 l.OlE+OO 2.97E+OO 692.42 1. 78 -3 .48E+OO 6.61E+OO 72 3. 30 2 0.06 3.35E-01 6.95E-01 756.80 4.52 6.85E-02 '.2.47E+OO 873. 1 8 12.08 -1.98E-01 8. 2 7E-01 996. 2 9 10.48 3 .39E-01 1 .29E+OO

[2709]

3/14/2018 7:31:57PM Page 6 of6 Analysis Report for 14-Mar-18-10039 81051 OOA-FSWC-231 CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCl/grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 4.42E-01 2 . 2 8E-01 9.93E-01 1274.43 34.80 1. 2 8E-01 4.16E-01 1596.48 1. 80 - 1.lOE-01 7.32E+OO Eu-155 45. 3 0 1. 31 2 .0BE+OO 4 . llE-01 2 .33E+Ol 60.01 1. 22 4.85E+OO 2. 79E+Ol 86.55 30.70 1.55E-01 4. llE-01 105.31 21.10 -l.53E-01 4.32E-01 Ra-226 186. 2 1 3 .64 3.04E+OO 3 .63E+OO 3.63E+OO Pa-231 2 7. 3 6 10. 3 0 1.49E+OO 2 .77E+OO 2 .77E+OO 283.69 1. 70 2 . 3 1E+OO 6.76E+OO 300.07 2 .47 - 2 .46E+OO 4.89E+OO 302.65 2 .20 l.53E+OO 5.79E+OO 330.06 1. 40 l.27E+OO 7.80E+OO U-235 143.76 10.96 -2 . 2 0E-01 2 . 2 9E-01 8.73E-01 163.33 5.08 -l.2 0E+OO 2 .05E+OO 185.71 57. 2 0 1.77E-01 2 .29E-01 2 02 .11 1. 08 4.60E+OO l. llE+Ol 205.31 5 .01 3.39E-01 2 .32E+OO Am-241 59.54 35.90 1.18E-Ol 9.55E-01 9.55E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2710]

0000024369.CNF Live Time :1200.000 sec Real Ti me :1201.370 sec start : 1: O.l(kev) stop : 4096 :2047.l(kev)

Acq. Start :wed Mar 14 19:11:49 2018

[2711]

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/14/2018 7:05:32PM Pagel of6

~pex-Gamma Analysis Report for 14-Mar-18-10040 B1051 OOA-FSFC-239CV 0.0" - 1.0" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10040 Sample Description : B105100A-FSFC-239CV 0.0" - 1.0" 0.0" Sample Type : Puck Unit Sample Point Sample Size 2.099E+02 grams Facility : Default Sample Taken On : 3/10/2018 1:35:00PM Acquisition Started : 3/14/2018 6:45:24PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 352 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.02 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120- 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 3/12/2018 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description : install Sample Number : 24368 Certificate Name : Eu155-Na22 Certificate Date : 12/20/2011 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 7:05:27PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2712]

3/14/2018 7:05:32PM Page 2 of6 Analysis Report for 14-Mar-18-10040 B 1051 OOA-FSFC-239CV 0.0" - 1.0" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.59 951 - 960 954.83 3 .80E+Ol 18.63 4.00E+Ol 0.70 2 351.98 1403 - 1415 1407.91 5.85E+Ol 17.43 1.30E+Ol 0.84 3 609.47 2430 - 2443 2 437.16 3.83E+Ol 13 .12 3.42E+OO 1. 11 4 1460.79 5837 - 5850 5843.52 3.57E+Ol 1 4. 22 1.07E+Ol 0.43 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE IDENTIF/C,4 T/ON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION UB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 1. 00 1460.82

10 .66 2 .32E+OO 9.49E-01 Bi-211 0.87 351.07

13.02 1 .12E+OO 3.80E-01 Pb-212 1. 00 115 .18 0.60 238.63

43.60 1.65E-01 8.52E-02 300.09 3.30 Bi-214 0 .99 609. 32

45.49 3.17E-0 1 1.15E-01 768.36 4.89 806.18 1. 26 934.06 3 . 11 1120. 2 9 1 4.92 1155. 2 1 1. 63 1238.12 5.83 128 0 .98 1. 43 1377. 67 3.99 1385. 3 1 0.79

[2713]

3/14/2018 7:05:32PM Page 3 of6 Analysis Report for 14-Mar-18-10040 B 105100A-FSFC-239CV 0.0" - 1.0" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-2 14 0. 99 1401. 52 1. 33 1407.99 2.39 1509 . 2 1 2 .13 1661. 2 7 1. 05 1729.59 2 .88 1764.49 1 5.30 1847.43 2 .03 2 118.51 1. 1 6 Pb- 214 1. 00 241.99 7.25 295. 22 18.42 351.93

35.60 4 . llE-01 1.39E-01 785. 96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 1. 000 2.32E+OO 9.49E-01

? Bi - 211 0.876 1.12E+OO 3.80E-01 Pb- 2 12 1.000 l.65E-01 8.52E-02 Bi-214 0.998 3.17E-01 1 .15E-01

? Pb-214 1. 000 4. llE-01 1.39E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2714]

3/14/2018 7:05:32PM Page 4 of6 Analysis Report for 14-Mar-18-10040 8105100A-FSFC-239CV 0.0" -1.0" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 7:05:27PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCUgrams) (pCl!grams)

(keV)

An Pk 511. 00 100.00 1.38E-01 1.34E-01 1 .3 4E-01 BE-7 477.60 10.44 2 .99E-01 7. 3 9E-0 1 7. 3 9E-01

+ K-40 1460.82

10.66 2 .32E+OO 1.04E+OO 1.04E+OO Co-60 117 3 . 23 99.85 1.48E-03 1. OOE-01 1.23E-01 1332.49 99 . 98 4.51E-02 1. OOE-01 Nb-94 702.65 99.81 5.84E-0 2 8.68E-02 8.68E-02 871.09 99.89 6. 2 1E-02 1.09E-01 Ag-108m 79.13 6.60 5 . 75E-01 8 .2 1E-02 2 . 2 2E+OO 433.94 90.50 -8.07E-02 8. 2 1E-02 614.28 89.80 -3.15E-02 1.55E-01 722 .94 90.80 3.83E-02 9.43E-02 Sb-125 176.31 6.84 7.08E-01 2 .73E-01 9.61E-01 380.45 1. 52 2. 06E+OO 4.36E+OO 427.87 29.60 1.66E-01 2 .73E-01 463.36 10.49 1.08E-01 7.61E-01 600.60 17.65 -l.67E-01 4.92E-01 606. 71 4 .98 1 . 70E+OO 2 .86E+OO 635.95 11. 22 -7.87E-02 7.45E-01 671.44 1. 79 -7.91E-0 2 4.08E+OO

[2715]

3/14/2018 7:05:32PM Page 5 of6 -

Analysis Report for 14-Mar-18-10040 B1051 OOA-FSFC-239CV 0.0" - 1.0" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

Ba-133 7 9.61 2.65 4.64E+00 1.70E-01 5.46E+00

81. 00 32.90 -5.12E-01 3 .42E-01 276.40 7. 1 6 1.90E-03 8.70E-01 302.85 18.34 3.39E-0 3 3 . 93E- 01 356.01 62 .05 - 4.42E-02 1.70E-01 383.85 8.94 -2 .60E-03 7.74E-01 Cs-134 475.36 1. 48 -1.80E+OO 1.07E-01 4.44E+OO 563.25 8.34 -2 . llE-01 8.91E-01 569.33 15.37 2 .28E-01 5.69E-01 604. 72 97. 62 -6.93E-0 2 1.34E-01 795.86 85.46 -9.41E-0 3 1.07E-01 801. 95 8.69 4.51E-02 1.lOE+OO 1038.61 0.99 1.56E+OO 9.52E+OO 1167.97 1. 79 -2 .0lE+OO 6.86E+OO 1365.19 3.0 2 -6.73E-01 3 .19E+OO Cs- 137 661.66 85.10 1.lOE-02 l.09E-01 1.09E-01 Eu-152 121. 7 8 2 8.67 '"'.2 . 4 7E-0 2 2 .04E-01 2. 04E-01 244.70 7.61 - 4.66E-02 8 .9 8E- 01 295.94 0.45 4.41E+OO 1. 85E+Ol 344. 2 8 26.60 5.82E-02 2 .66E-01 367.79 0.86 -3.23E+OO 6.80E+OO 411.12 2 .24 -1.13E+OO 3 . 3 8E+OO 443. 96 2 .83 -1.55E+OO 2 .83E+OO 488.68 0.42 3.14E+OO 1.81E+Ol 563.99 0.49 -3.48E+OO 1. 51E+01 586.26 0.46 1. 59E+01 2 .55E+01 678.62 0.47 2 .37E+OO 1.79E+01 688.67 0.86 -8.53E-01 1.03E+Ol 719.35 0.28 7.62E+OO 2 .85E+Ol 778.90 1 2 . 96 2 .40E-01 7.18E-01 810.45 0.3 2 -3 .93E+OO 2.47E+Ol 867.37 4.26 -2 .02E-01 2.56E+00 919.33 0.43 -2 .46E+Ol 2 .85E+Ol 964. 08 14.65 1.85E-01 8.20E-01 1085.87 10. 2 4 -3. 99E-01 7.44E-01 1089.74 1. 73 1.62E+OO 4.41E+OO 1112. 07 13.69 -5 .60E-01 6.83E-01 1212.95 1. 43 -S.14E-01 6.59E+OO 1249.94 0.19 1.68E+Ol 6.12E+Ol 1299.14 1. 63 -3.36E-01 7.31E+OO 1408.01 2 1. 07 -2 .63E-02 4.98E-01 1457.64 0.50 6.48E+Ol 4.93E+Ol 15 2 8.10 0. 2 8 -5.76E+OO 3.48E+Ol Eu-154 123.07 40.40 1.05E-01 l. SSE-01 1. 55E-01 247.93 6.89 -6. 71E-01 8.72E-01 591. 76 4.95 - 1.68E-01 1. 73E+OO 692.4 2 1. 78 2. 03E+OO 4.98E+OO 723. 30 2 0.06 5 . 05E-02 4.27E-01 756.80 4.52 4.12E-01 2 .14E+00 873.18 12.08 -3. 71E-01 7.79E-01 996. 2 9 10.48 -3 .62E-01 1.05E+OO

[2716]

0000024368.CNF Live Time :1200.000 sec 60 Real Tille :1200 .250 sec start: 1: -0.2(keV) stop : 8192: 2046. 9(kev)

Acq. start :wed Mar 14 18:45:24 2018 55 50 45

[2717]

=

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/14/2018 7:32:18PM Page 1 of7

~pex Gamma Analysis Report for 14-Mar-18-10042 B105100A-FSFC-239CV 0.0" - 1.0" 1.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10042 Sample Description : B105100A-FSFC-239CV 0.0" - 1.0" 1.0" Sample Type : Puck Unit Sample Point Sample Size 2.099E+02 grams Facility : Default Sample Taken On : 3/10/2018 1:35:00PM Acquisition Started : 3/14/2018 7:12:12PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 352 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.02 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 3/12/2018 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description : install Sample Number : 24370 Certificate Name : Eu155-Na22 Certificate Date : 12/20/2011 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 7:32:14PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2718]

3/14/2018 7:32:18PM Page 2 of7 Analysis Report for 14-Mar-18-10042 8105100A-FSFC-239CV 0.0" -1.0" 1.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (keV) 1 186.04 739 - 749 744.86 3 .05E+Ol 16. 72 3.30E+Ol 0.35 2 238.68 950 - 960 955.19 2 . 78E+Ol 16.03 3.04E+Ol 0.94 3 351.80 1401 - 1414 1407.19 4.00E+Ol 17.00 2 .19E+Ol 0.76 4 609.28 2431 - 2 442 2436.40 2 .96E+Ol 13. 86 1.48E+Ol 1. 03 5 1460.92 5838 - 5852 5844.05 3. 31E+Ol 15. 72 1.98E+Ol 1. 47 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA T/ON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82

10 .66 2 . 1 6E+OO 1. 04E+OO Bi-2 11 0.91 351.07

13. 02 7 . 68E-01 3.49E-0 1 Pb-212 1. 00 115.18 0.60 238.63

43.60 1. 2 1E- 01 7.23E-02 30 0 .09 3.30 Bi-214 1. 00 609.32

45.49 2.4 5E-01 1.18E-Ol 768.36 4.89 8 0 6. 1 8 1. 26 934. 0 6 3 . 11 1120. 2 9 1 4.92 1155.21 1. 63 1238.12 5.83 128 0 .98 1. 43 1377. 67 3.99

[2719]

3/14/2018 7:32:18PM Page 3 of7 Analysis Report for 14-Mar-18-10042 B105100A-FSFC-239CV o.o* - 1.0" 1.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi - 214 1. 00 1385. 31 0.79 1401.52 1. 33 1 407.99 2 .39 1509. 2 1 2 .13 1661. 2 7 1. 05 17 2 9.59 2 .88 1764.49 15.30 1 847.43 2 .03 2 118.51 1.16 Pb-214 0. 99 241.99 7.25 295. 22 18.42 351.93

35.60 2 .81E-01 l. 2 7E-01 785.96 1. 06 Ra-226 0.99 186.21

3.64 1.37E+OO 7.81E - 01 U-23 5 0.98 143.76 10. 96 163.33 5.08 185. 71

57.20 8.69E-02 4.97E-0 2 202 .11 1. 08 205.31 5.01

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Toierance : i .000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.998 2.16E+OO 1.04E+OO

? Bi-211 0.919 7.68E-01 3 .49E-01 Pb-21 2 1. 000 1 .21E-01 7. 2 3E-02 Bi-214 1. 000 2.45E-01 1.18E-01

? Pb-214 0.998 2.81E-01 1.27E-01

? Ra-2 2 6 0.995 1.37E+OO 7.81E-01

? u~ ~. -~)(, 0~ 8.69E-02 4.97E-02

\), lli {X\\l\ ~~e ~ ~}\~-\e.[2720]

3/14/2018 7:32:18PM Page4 of7 Analysis Report for 14-Mar-18-10042 B105100A-FSFC-239CV 0.0" - 1.0" 1.0"

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2721]

3/14/2018 7:32:18PM Page 5 of7 Analysis Report for 14-Mar-18-10042 B105100A-FSFC-239CV 0.0" - 1.0" 1.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 7:32:14PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield('Y.n) Activity Nuclide MDA LineMDA Name (pCi!grams) (pCilgrams) (pCilgrams)

(keV)

An Pk 511.00 100.00 1.30E-01 1.38E-01 1.38E-01 BE-7 477.60 10.44 2 .15E-01 7.21E-01 7.21E-01

+ K-40 1460.82

10.66 2 .16E+OO 1.37E+OO 1. 37E+00 Co-60 1173.23 99.85 3 .55E-02 8.03E-02 8.64E-02 1332.49 99.98 -6.84E-03 8.03E-02 Nb-94 702.65 99.81 2 .46E-02 8.95E-02 8.95E-0 2 871.09 99.89 3.54E-02 9.40E-02 Ag-1 08m 79.13 6.60 1.44E-01 7.14E - 02 1.99E+OO 433.94 90.50 5.97E-0 3 7.14E-02 614.28 89.80 -9.86E-0 2 1.65E-01 722. 94 90.80 4.77E-0 2 1 .00E-01 Sb- 125 176.31 6.84 -8. 2 8E-02 2.28E-01 7.85E-01 380.45 1. 52 2 .03E+OO 5.48E+OO 427.87 2 9.60 -1. 2 1E-01 2 .28E-01 463.36 10.49 3.16E-01 7.90E-01 600.60 17.65 8.44E-02 5.15E-01 606.71 4.98 1.70E+OO 2 .86E+OO 635.95 11 .22 9.54E-0 2 7.86E-01 671.44 1. 79 1.69E-01 4.40E+OO

[2722]

3/14/2018 7:32:18PM Page 6 of7 Analysis Report for 14-Mar-18-10042 B105100A-FSFC-239CV 0.0" - 1.0" 1.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCilgrams) (pCilgrams)

(keV)

Ba-133 79.61 2 .65 3.50E+OO 1. 55E-01 4.87E+OO

81. 00 32.90 -6.21E-0 1 2 .97E-01 2 76.40 7. 1 6 -1.39E-01 9.07E-01 3 02.85 18.34 1 .79E-01 3.88E-01 356.01 62.05 -1.76E-02 1. 55E-01 383.85 8.94 -1. 56E-01 9.lOE-01 Cs-134 475.36 1. 48 -l.43E+OO 9.60E-02 4.44E+OO 563.25 8.34 -7.92E-0 2 l.04E+OO 569.33 15.37 -6.14E-02 5.16E-01 604. 72 97.62 -7.68E-02 1.36E-01 795.86 85.46 1.92E-02 9.60E-02 801. 95 8.69 -7. 1 3E-01 1. 03E+OO 1038.61 0.99 5.51E+OO 9.95E+OO 1167. 97 1. 79 2 .31E+OO 5.13E+OO 1365.19 3.02 -1.36E+OO 3 .59E+OO Cs-137 661.66 85 . 10 5.89E-02 1.06E-01 l.06E-0 1 Eu-1 52 121. 7 8 2 8.67 -3 .19E-02 2 .lOE-01 2 . l OE-01 2 44.70 7.6 1 7 . 2 1E-01 1.05E+OO 2 95.94 0.45 1.56E+Ol 1. 90E+Ol 3 44.28 2 6. 60 -1.75E-01 2 .25E-01 367.79 0.86 1.54E+OO 7.77E+OO 411.12 2 .24 3 .68E-01 3. 2 6E+OO 443. 96 2 .83 1.39E-03 2 .50E+OO 488.68 0.42 -4.76E+OO 1. 63E+ Ol 563.99 0.49 -5.68E+OO 1. 72E +01 586. 2 6 0.46 1.29E+ Ol 2 .42E+Ol 678.62 0.4 7 4.09E+OO 1.90E+Ol 688.67 0.86 -1.63E+Ol 8.98E+00 7 1 9 . 35 0.28 1. 1 4E+Ol 3.06E+Ol 778.90 12 .96 1.25E-01 5.95E-01 810.45 0.32 -1.18E+OO 3 .24E+Ol 867.37 4 . 26 5.49E-01 2 .12E+OO 919.33 0.43 1. 29E+Ol 2 . 2 0E+Ol 964.08 14.65 2 .90E-0 2 8.78E-01 1085.87 10. 2 4 7.98E-02 8.00E-01 1089.74 1. 73 -3.00E+OO 4.05E+OO 1112.07 13. 69 6.65E-01 9.17E-01 121 2 .95 1. 43 5.92E+00 8.81E+OO 1249.94 0.19 -1.02E+OO 4.06E+Ol 1299.14 1. 63 1.06E+OO 6.06E+OO 1 408.01 21. 07 2 .24E-01 4.98E-01 1457.64 0.5 0 6.87E+Ol 5.26E+Ol 1528 . 10 0.28 -8.06E+OO 3.48E+Ol Eu-154 123.07 40.40 -6.68E-03 1.51E- 01 1. 51E-0 1 247.93 6.89 - 5.06E-01 9.06E-01 591.76 4.95 -1. OlE-01 1.77E+OO 692.42 1. 78 2 . 2 9E+OO 4.98E+OO 723 . 30 20.06 2 . 0 6E-Ol 4.54E-01 756.8 0 4. 52 -6.61E-02 1. 82E+OO 873. 1 8 1 2 .08 5.60E-01 8. 3 3E-0 1 996. 2 9 10.48 - 6.00E-0 1 9.49E-01

[2723]

0000024370.CNF Live Time :1200.000 sec Real Time :1200.250 sec 60 Start: 1: -0 .2(kev)

Stop : 8192:2046.9(kev)

Acq. start :wed Mar 14 19:12:12 2018 55 50 45 40 35

[2724]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/14/2018 8:01 :45PM Page I of6

~ ~ ~pex-Gamma Analysis Report for 14-Mar-18-10043 B105100A-FSFC-250CV 0.0" - 0.5 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10043 Sample Description : B105100A-FSFC-250CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.301E+02 grams Facility : Default Sample Taken On : 3/10/2018 1: 15:00PM Acquisition Started : 3/14/2018 7:41 :38PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.7 seconds Dead Time : 0.14 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description Sample Number : 24372 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 8:01:41PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2725]

3/14/2018 8:01:45PM Page 2 of6 Analysis Report for 14-Mar-18-10043 81051 OOA-FSFC-250CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 2 38.68 473 - 481 477.54 4.52E+Ol 25.82 1.12E+02 1.13 2 351.99 701 - 708 703.93 5.37E+Ol 20 .13 4.66E+Ol 1. 38 3 661.7 2 1317 - 1328 1322. 97 1. 01E+02 23 .90 3.30E+Ol 0. 92 4 14 61. 28 2 916 - 2928 2922 . 62 5.65E+Ol 15.55 3.08E+OO 1. 60 M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

I\JUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0. 96 1460.82

10.66 5. 3 0E+OO 1. 53E+OO Cs-137 0.99 661. 66

85 . 10 6 . 86E-01 1.81E-Ol Bi-211 0.87 351.07

13.02 1 . 48E+OO 6.05E-0 1 Pb-212 1. 00 115.18 0.60 238.63

43.60 2 .81E-01 1.67E-01 300.09 3.30 Pb-214 1. 00 241.99 7.25 295. 22 18.42 351.93

35.60 5.43E-01 2 .21E-01 785. 96 1. 06

[2726]

3/14/2018 8:01 :45PM Page 3 of6 Analysis Report for 14-Mar-18-10043 B105100A-FSFC-250CV 0.0" - 0.5" 0.0"

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0. 967 5.30E+OO 1. 53E+OO Cs-137 0.999 6.86E-01 1. 81E-01

? Bi-211 0.873 1. 48E+OO 6.0SE-01 Pb-21 2 1.000 2 .81E-0 1 l.67E-Ol

? Pb-214 1. 000 5.43E-0 1 2 .21E-Ol

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2727]

3/14/2018 8:01 :45PM Page 4 of6 Analysis Report for 14-Mar-18-10043 B105100A-FSFC-250CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 8:01 :41 PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F "' Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCUgrams) (pCUgrams) (pCi/grams)

(keV)

An Pk 511. 00 100.00 3.03E-0 1 2.46E-01 2 .4oE-01 BE-7 477.60 10.44 2 .65E-0 3 1. 2 5E+OO 1. 25E+O O

+ K-40 1460.82

10.6 6 5 . 30E+OO 9.04E-01 9.04E-0 1 Co-60 1173.23 99.85 5.42E-02 1 .99E-01 2 . llE-0 1 1332 . 49 99.98 8.47E-02 l.99E-0 1 Nb-94 702.65 99.8 1 -l.93E-02 1. 25E-Ol 1.25E-01 871. 09 99.89 -5.61E-0 2 1.26E-01 Ag-108m 79.13 6.60 1.67E+OO l .25E-01 2.93E+OO 433.94 90.50 - 9. llE-02 l.25E-01 614.28 89.80 6.0lE-02 2 .21E-01 72 2 . 94 90 .80 -1.85E-02 l .67E-01 Sb-1 2 5 176 . 31 6.84 -5.98E-02 4.42E-01 1.80E+00 380.45 1. 52 -3 .25E+OO 8. OOE+.00 427.87 29.60 -2 .54E-01 4.4 2E-01 463.36 10.49 3. 2 7E-01 l.34E+OO 600.60 17.65 2 .30E-01 8.04E-01 606. 71 4.98 3.09E+OO 4.29E+OO 635.95 11. 22 4.08E-01 1. 27E+OO 671.44 1. 79 -2 .23E+OO 6.98E+OO

[2728]

3/14/2018 8:01 :45PM Page 5 of6 Analysis Report for 14-Mar-18-10043 B1051 OOA-FSFC-250CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCVgrams) (pCVgrams) (pCilgrams)

(keV)

Ba-133 79.61 2 .65 3.68E+OO 2 .70E-01 6.94E+OO

81. 00 32 .90 -3.0lE-01 4.40E-01 2 76.40 7.16 7.96E-01 1 .80E+OO 302.85 18.34 8. 77E-02 7.21E-01 356. 01 62.05 -1. 24E-01 2 .70E-01 383.85 8.94 3.65E-02 1.52E+OO Cs-134 475,36 1. 48 - 2 .36E-01 1 .50E-01 8.38E+OO 563. 2 5 8.3 4 3 .07E-01 1 .60E+OO 569. 3 3 15.3 7 4.32E-01 9.21E-01 604. 72 97.6 2 -3.55E-02 1.82E-01 795.86 85 . 46 -4.17E-02 1 . 50E-01 801. 95 8 . 69 -l.6 2E-01 1 . 43E+OO 1038.61 0.99 -1.57E+OO l.43E+Ol 1167. 97 1. 79 -2 .85E+OO l.13E+Ol 1365 .19 3.0 2 -1.28E+OO 4.60E+OO

+ Cs-137 661.66

85. 10 6.86E-01 l .67E-0 1 1.67E-01 Eu-152 12 1. 78 2 8.67 1. 30E-01 3.63E-01 3.63E-01 2 44.70 7.61 -l.14E+OO 1.55E+OO 2 95. 94 0.45 2.86E+Ol 3 .64E+Ol 344.28 26.60 -3.84E-01 4.62E-01 367.79 0.8 6 -3.57E+OO 1 .35E+Ol 411.12 2 .24 9.90E-01 6.22E+OO 443.96 2 .83 1.93E+OO 5.32E+00 488.68 0.4 2 -1.70E+Ol 3.05E+Ol 563.99 0.49 -4. 96E+00 2 .60E+Ol 586.26 0.46 4.43E+O l 4.02E+Ol 678.62 0.47 -1.06E+Ol 2. 50E+Ol 688.67 0.86 -1. 23E+OO 1.82E+Ol 719.35 0.28 1.17E+Ol 5.55E+Ol 778.90 1 2 .96 4.69E-01 1.13E+OO 810.45 0.32 -4.36E+OO 4.16E+Ol 867.37 4. 2 6 3 .90E-01 3.39E+OO 919.33 0.43 2. 75E+OO 3.52E+Ol 964.08 14.65 -5.32E-01 1. 18E+OO 1085.87 10. 2 4 -1.43E+OO 1. 07E+00 1089.74 1. 73 1. 23E+OO 6.84E+OO 1112. 07 13.69 4.34E- 01 l.39E+OO 121 2 .95 1. 43 2 .83E+OO 1. 31E+Ol 1249.94 0.19 2 .58E+OO 1.01E+02 1299.14 1. 63 6.46E+OO 1. 2 7E+Ol 1 4 0 8.01 2 1.07 2 .86E-01 9.88E-01 1457.64 0.50 -3 .97E+OO 8.0lE+Ol 1 523.10 0. 2 8 1.47E+Ol 4.59E+Ol Eu- 1 54 123.07 40.40 6.83E-02 2 .62E-0 1 2 .62E-01 247.93 6.89 1. 46E+OO 1.83E+OO 591.76 4.95 -l.15E+OO 2 . 72E+OO 692.4 2 1. 78 8.36E-02 8.82E+OO 723. 30 2 0.06 -7.49E-02 7.59E-01 756.80 4.52 l .77E-0 1 3.00E+OO 873. 1 8 12.08 2 .53E-01 1.13E+OO 996. 2 9 10.48 1. 82E-0 1 1. 47E+OO

[2729]

3/14/2018 8:01 :45PM Page 6 of6 Analysis Report for 14-Mar-18-10043 B1051 OOA-FSFC-250CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams)' (pCilgrams) (pCl/grams)

(keV)

Eu-154 1004.76 18.01 -1.76E-01 2 .62E-01 1.06E+OO 12 1 4.43 3 4.80 -9 .69E-03 4.25E-01 1596.48 1. 80 1.0lE+OO 9.85E+OO Eu-155 45.30 1. 31 5 .66E+OO 4 . 34E-01 2 .62E+Ol 60.01 1. 22 -6 .88E+OO 2 .42E+Ol 86.55 30.70 1.25E-01 4.34E-01 105.31 21.10 -3.63E-01 4.95E-01 Ra-226 186.21 3.64 l.80E+00 3 .71E+00 3.71E+OO Pa-23 1 27.36 1 0.30 1. 52E+OO 2 .83E+OO 2.83E+OO 283.69 1. 70 4.76E-01 6.84E+OO 300.07 2 .47 -5.32E+OO 5.35E+OO 302.65 2 . 20 7.30E-01 6.00E+OO 330.06 1. 40 4.12E+OO 9.82E+OO U-235 14 3 .76 10. 96 l.20E-01 2 .39E-01 8.91E-01 163.33 5 . 08 -3. 0lE-0 1 2 .42E+00 185.71 57.20 1 . 69E-01 2 . 3 9E-01 2 02 .11 1. 08 l.12E+OO 1.16E+Ol 205.31 5.01 6.17E-02 2 .37E+OO Am-241 59.54 35.90 -3. llE-01 8.19E-01 8.19E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is Inconsistent with Currie MDA at 95% confidence level

[2730]

0000024372.CNF Live Time :1200.000 sec Real Time :1201.680 sec start: 1: O.l(kev) stop : 4096:2047.l(kev)

Acq. Start :wed Mar 14 19:41:38 2018

[2731]

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/14/2018 8:24:31 PM Page 1 of6

~pex-Gamma Analysis Report for 14-Mar-18-10044 B105100A-FSFC-250CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANAL YS/S Sample Identification : 14-Mar-18-10044 Sample Description : B105100A-FSFC-250CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.301 E+02 grams Facility '. Default Sample Taken On : 3/10/2018 1:15:00PM Acquisition Started : 3/14/2018 8:04:22PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.6 seconds Dead Time : 0.14 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description Sample Number : 24375 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 8:24:26PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2732]

3/14/2018 8:24:31PM Page2 of6 Analysis Report for 14-Mar-18-10044 81 051 OOA-FS FC-250CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.64 473 - 481 477.47 4.29E+Ol 2 7.20 l.24E+02 1.14 2 295.08 586 - 594 590. 22 2 .16E+Ol 2 0.18 7.27E+Ol 0.69 3 352.13 699 - 707 704.21 4.84E+Ol 19.65 4.51E+Ol 1. 07 4 609.59 1214 - 1224 1218.76 3.79E+Ol 15.44 l.82E+Ol 1.16 5 661. 77 1318 - 1328 1323.06 3.57E+Ol 17.12 3.05E+Ol 0.99 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE IDENTIFIC14 TION REPORT Nuclide Library Used * : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Cs-137 0 .99 661.66

85.10 2 .42E-01 l.19E-Ol Pb-212 1. 00 115 .18 0.60 238.63

43.60 2 .67E-01 l.75E-Ol 300.09 3.30 Bi -21 4 0.99 609.3 2

45.49 4.52E-01 l.92E-01 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120. 2 9 14.92 1155. 2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79

[2733]

3/14/2018 8:24:31PM Page 3 of6 Analysis Report for 14-Mar-18-10044 B 1051 OOA-FSFC-250CV 0.0" - 0.5" 0.5" Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi-214 0.99 1401.52 1. 33 1407.99 2 .39 1509.21 2 .13 1661.27 1. 05 1729.59 2 .88 1764.49 15.30 1847.43 2.03 2 118.51 1. 16 Pb-214 0.99 241. 99 7.25 295. 22

18.42 3 .68E-01 3 .48E-01 351.93

35.60 4.90E-01 2 .14E-01 785.96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

Cs-137 0.998 2 .42E-01 1.19E-0 1 Pb-21 2 1. 000 2 .67E-01 1.75E-0 1 Bi-214 0.995 4.52E-01 l .92E-01 Pb-214 0.995 4.57E-01 1.82E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2734]

3/14/2018 8:24:31PM Page 4 of6 Analysis Report for 14-Mar-18-10044 B105100A-FSFC-250CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 8:24:26PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi!grams) (pCilgrams)

(keV)

An Pk 5 11. 00 100.00 2.15E-01 2 .25E-01 2 .25E-01 BE-7 477.60 10.44 1. 72E-01 1.16E+OO 1.16E+OO K-40 1 460.82 10.66 3.69E+OO 3.42E+OO 3.42E+OO Co-60 1173.23 99.85 2 .25E-02 2.05E-01 2 .07E-01 133 2 .49 99.98 6.17E-02 2 .05E-01 Nb-94 702.65 99.81 -5.28E-02 1. 2 6E-01 1. 64E-01 871. 0 9 99.89 -1.38E-02 l. 2 6E-01 Ag-108m 79.13 6.60 8.lOE-01 l .42E - 01 2 .86E+OO 433.94 90.50 -6.67E-0 3 l.42E-01 614.28 89.80 -2 .47E-0 2 2 .09E-01 722. 94 90.80 3 .85E-0 2 1.74E-01 Sb-125 176.31 6.84 -1.74E-01 4.30E-0 1 1. 80E+00 380.45 1. 52 -3.26E+OO 7 . 79E+OO 427.87 29.60 -l.47E-01 4 . 30E-01 463.36 10.49 -5.lOE-01 1.18E+OO 600.60 1 7.65 2 .93E-01 8.75E-01 606. 71 4.98 -9.23E-01 4. 2 6E+00 635.95 11. 22 -1.60E-01 1.16E+OO 671. 44 1. 79 - 5.33E+OO 6. llE+OO

[2735]

3/14/2018 8:24:31 PM Page 5 of6 Analysis Report for 14-Mar-18-10044 B105100A-FSFC-250CV 0.0" - 0.5 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

Ba-13 3 79.61 2 .G5 -9.63E-01 2 .52E-01 6.68E+OO

81. 00 32 .90 -4.29E-01 4.64E-01 276.4 0 7.16 -2 .04E-01 1.62E+OO 302.85 18.34 -2 .35E-02 6.60E-01 356. 01 62 .05 -1.85E-01 2 .52E-01 38 3 .85 8.9 4 -5.55E-02 l.40E+OO Cs- 134 475.36 1. 48 -3.87E+OO 1. 86E-01 7.12E+00 563. 2 5 8.34 -8.17E-01 1.0lE+OO 569.33 1 5.37 -3.61E-02 7.02E-01 604.72 97. 62 -3.53E-02 1 .86E-01 795.86 85.46 1.47E-01 1.91E-01 801.95 8.69 -5.50E-01 1.37E+OO 1 038.61 0.99 -2 .58E+OO 1.16E+Ol 1167. 97 1. 79 -6.60E-01 1.0SE+O l 1365.19 3.0 2 -1.63E+OO 3.92E+OO

+ Cs-137 661.66

85.10 2.42E-01 l . 60E-01 1.60E-01 Eu-1 52 121.78 2 8.67 8.99E-02 3.57E-01 3.57E-01 244.70 7.61 1 . 18E+OO 1.77E+00 295.94 0.45 4.50E+OO 3.06E+Ol 344. 28 2 6.60 4 .13E-0 2 5.24E-01 367.79 0.86 4. 72E+OO 1.54E+Ol 411.12 2 .24 2 .85E+OO 6.15E+OO 443. 96 2 .83 -4.lOE-01 4.61E+OO 488.68 0.42 -1.16E+Ol 3.15E+Ol 563.99 0.49 -4 . 6.S E: +00 l . 88E+O l 586.26 0.46 1. 24E+01 3.49E+Ol 678.62 0.47 9.31E-01 2 .66E+Ol 688.67 0.86 -4.90E+OO 1 .43E+Ol 719.35 0.28 -2 .30E+Ol 5.08E+Ol 778.90 12 .96 9. 2 3E-02 1.04E+OO 810.45 0 .32 -7.32E+OO 3 .72E+Ol 867.37 4. 2 6 - 1 . 57E+OO 3. 06E+OO 919.33 0.43 -2 . 33E+Ol 3 .41E+Ol 964. 08 1 4.65 -5.69E-01 l.15E+OO 10 85.87 10 .24 -5.78E-01 1 .54E+OO 10 89 . 74 1. 73 -1.09E-01 9.73E+OO 1 112.07 1 3.69 4.17E-01 1.28E+OO 121 2 .95 1. 43 1.39E+OO 1.lOE+Ol 1249.94 0.19 l.19E+01 6.86E+Ol 1 299.14 1. 63 -2. 52E+OO 9.21E+OO 1 408.0 1 21. 07 1 . 27E-01 7.95E-0 1 1 457.64 0.50 9.77E+Ol 7. 3 7E+Ol 1 528.10 0. 2 8 -4.60E+OO 5.0lE+Ol Eu-154 123.07 40.40 2.lOE-02 2 .50E-01 2 .50E-01 247.93 6.89 -1.18E+OO 1.62E+OO 591.76 4.95 3.22E-01 2 . 72E+OO 692.42 1. 78 -7.94E-01 8.82E+OO 723. 30 20.06 4.44E-0 1 8.34E-01 7 56.80 4.52 3.81E-01 3. 2 5E+OO 873.18 12. 0 8 2 . 2 7E-01 1. 08E+OO 996. 2 9 10.48 -3 . 2 6E-01 1. 2 6E+OO

[2736]

3/14/2018 8:24:31PM Page 6 of6 Analysis Report for 14-Mar-18-10044 B105100A-FSFC-250CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi!grams) (pCi!grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.0 1 2 .lOE-01 2 .SOE-01 9.40E-01 1274.43 34.80 2 .84E-01 4.85E-01 1596.48 1. 80 - 2 .97E+OO 8.15E+OO Eu-155 45.30 1. 31 -5 .18E+OO 4 . 6,E-0 1 2 . 3 6E+O l 60.01 1. 22 -1.33E+O l 2 .47E+Ol 86.55 30.70 -6.99E-02 4.67E-01 105. 3 1 21.10 5.37E-03 5.36E-01 Ra-226 186. 2 1 3.64 1. 33E+00 3.45E+OO 3.45E+OO Pa-231 27. 3 6 10.30 5.24E-01 2 .38E+OO 2 . 3 8E+OO 283.69 1. 70 -1.96E-02 6.90E+OO 300.07 2 .47 7.56E-03 4.99E+OO 302.65 2.20 -l.95E-01 5.49E+OO 330.06 1. 40 3.56E+OO 8.91E+OO U-2 3 5 143.76 10. 96 2 .82E-01 2 . 19E-01 9.70E-01 163.33 5.08 -2 .61E-01 2.36E+OO 185.71 57.20 4.53E-02 2.19E-01 2 02.11 1. 08 -8.60E-01 1.08E+Ol 205.31 5.01 -9.00E-01 2. 2 7E+OO Am-241 59 . 54 35.90 -2.06E-01 9.0lE-0 1 9.0lE-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

, = MDA value not calculated

@ ;;;; Haff-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2737]

0000024375.CNF Live Time :1200.000 sec Real Time :1201.630 sec start: 1: O.l(kev)

Stop : 4096: 2047. l(kev)

Acq. start :wed Mar 14 20:04:22 2018

[2738]

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/14/2018 8:01:51PM Page 1 of6 Analysis Report for 14-Mar-18-10046 B105100A-FSFC-255CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10046 Sample Description : B105100A-FSFC-255CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.343E+02 grams Facility : Default Sample Taken On : 3/10/2018 8:45:00AM Acquisition Started : 3/14/2018 7:41 :45PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description Sample Number : 24373 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANAL YS/S REPORT Peak Analysis Performed on : 3/14/2018 8:01:47PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2739]

3/14/2018 8:01 :51 PM Page 2 of6 Analysis Report for 14-Mar-18-10046 B105100A-FSFC-255CV o.o* - o.5" 0.0" Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 23 8.74 949 - 961 954.54 4.56E+Ol 18.85 3.07E+Ol 0.82 2 29 5.08 1175 - 1187 1179.59 3 .38E+Ol 17.58 3.25E+Ol 0.79 3 609.13 2429 - 2 439 2434.54 2 .89E+Ol 14.00 l.63E+Ol 1. 31 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA T/ON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb - 2 1 2 0.99 11 5 .18 0.60 2 38.63

43.60 2.96E-01 1. 31E-Ol 300.09 3.30 Bi - 214 0.99 609. 32

45.49 3.67E-01 1.84E-01 768.36 4.89 806.18 1. 2 6 934.06 3 .11 1120.29 14.92 1155.21 1. 63 1238.12 5.83 1 2 8 0 .98 1. 43 1 3 77.67 3.99 1 3 85.3 1 0.79 1401. 52 1. 33 1407.99 2 .39 1509. 2 1 2 .13

[2740]

3/14/2018 8:01 :51PM Page3 of6 Analysis Report for 14-Mar-18-10046 B105100A-FSFC-255CV 0.0" - 0.5" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi- 214 0.99 1661. 27 1. 05 1729.59 2 .88 1764.49 1 5.30 1847.43 2.03 2118.51 1. 16

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

Pb-21 2 0.998 2.96E-01 1.31E-01 Bi-214 0.998 3.67E-01 l.84E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2741]

3/14/2018 8:01 :51PM Page 4 of6 Analysis Report for 14-Mar-18-10046 B105100A-FSFC-255CV 0.0"

0.5 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 8:01 :47PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide 2 295.08 2.81250E-02 26. 05 Tol. Eu-~

r 214 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCilgrams) (pCilgrams) (pCi/grams)

(keV)

An Pk 511. 00 100.00 l.22E-01 1.70E-01 1. 70E-01 BE-7 477.60 10.44 -1.79E-01 8.42E-01 8 . 42E-01 K-40 1460.82 10.66 4.31E+OO 3 .49E+OO 3.49E+00 Co-60 1173.23 99.85 3.18E-0 2 1.57E-01 1.74E-0 1 1332.49 99.98 -7.98E-02 1. 57E-01 Nb-94 702.65 99.8 1 3 .95E-02 1. 42E-01 1. 42E-01 871. 0 9 99.89 5.63E-02 1. 52E-01 Ag-108m 79. 1 3 6.6 0 1. 57E+OO 1 .14E - 01 2. 65E+OO 433.94 90 . 50 8.89E-03 1.14E-01 614.28 89.80 -2 .51E-01 l.71E-01 722.94 90 . 80 -1.81E-0 2 1.68E-01 Sb-125 176.31 6 . 84 -7.19E-0 2 3.71E-Ol l.18E+OO 380.45 1. 52 2 . 72E+00 6.75E+00 4 2 7.87 2 9.60 -1. 71E-02 3.71E-01 463.36 10. 49 3.54E-02 1. 2 3E+OO 600.60 17.65 6.51E-01 7.92E-0 1 606.71 4.98 3.08E+OO 4. 2 4E+00

[2742]

3/14/2018 8:01:51PM Page 5 of6 Analysis Report for 14-Mar-18-10046 B105100A-FSFC-255CV o.o* - o.s" 0.0" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCl/grams)

(keV)

Sb-125 635.95 1 1. 22 -1.04E+OO 3 . 71E-01 7.27E-01 671. 4 4 1. 79 3.49E+OO 6.30E+OO Ba-133 79.61 2.65 2.57E+00 1.85E-01 6.33E+OO

81. 00 32 .90 -4.05E-01 4.15E-01 276.40 7.16 5.50E-01 1. 30E+OO 302.85 18.34 3.06E-01 5.09E-01 356.01 62.05 -4.48E-0 1 l .85E-01 383.85 8.94 - 4.54E-01 1. 1 7E+OO Cs-134 475.36 1. 48 6.50E-01 l.29E-0 1 6.77E+OO 563.25 8.34 - 6.40E-01 l.28E+OO 569.33 15.37 1.18E-01 6.20E-01 604.7: 97.6 2 -1.05E-01 2 .05E - 01 795.86 85.46 2.22E-02 1. 2 9E-Ol 801.95 8.69 2.05E-0 2 1. 2 0E+OO 1038.61 0.99 - 3.09E+OO 1. 2 6E+Ol 1167.97 1. 79 - 3.48E+OO 7.02E+OO 1365. 1 9 3.0 2 6.86E-01 3.32E+OO Cs-137 661.66 85.10 1.56E-01 2. 0lE - 01 2 .0lE-01 Eu-152 121.78 2 8.67 2 .00E-02 2 .44E-01 2 .44E-01 244.70 7.61 8.65E-01 l .35E+OO 295.94 0.45 2 .69E+Ol 3.lOE+Ol 344.28 26.60 -l.19E-01 3.55E-01 367.79 0.86 -2 .02E+OO 7.48E+OO 4 11 .12 2.24 7.96E-01 4.33E+OO

,1,1-

- .)*-v 4h 2.83 l. 2 9E-01 3 .34E+OO 488.68 0.42 1.08E+Ol 2 .70E+Ol 563.99 0.49 2 .92E+OO 2 .17E+Ol 586.26 0.46 4.62E+OO 2 .91E+Ol 678.62 0.47 -8.50E+OO 2 .50E+01 688.67 0.86 -8.89E+OO 1. 72E+Ol 719.35 0.28 -6.0lE+OO 4 . 74E+01 778.90 12. 96 3.03E-01 l .04E+OO 810.45 0. 32 -1.00E+Ol 2 .77E+Ol 867.37 4. 2 6 2 . llE+OO 3 .43E+OO 919.33 0.43 -2 .03E+Ol 3 .81E+Ol 964.08 14.65 4.58E-01 1.25E+OO 1 085.87 10. 2 4 -6.63E-01 1.07E+OO 1089.74 1. 73 5.26E-01 7.91E+OO 1112.07 13. 69 -l.14E-01 l. l 7E+00 1212.95 1. 43 -6.90E+OO l.09E+Ol 1249.94 0.19 -5.38E+Ol 7.95E+Ol 1 2 99.14 1. 63 4.27E+OO 9.51E+OO 1 408.01 2 1. 07 - 8.81E-02 7.36E-01 1457.64 0.50 4.68E+Ol 7.05E+Ol 1528.10 0. 2 8 2 . 02E+Ol 5.49E+Ol Eu-1 5 4 12 3.07 40 . 40 2 .57E-02 l . 70E-01 l.70E-01 247.93 6.89 -1. 4 7E+OO 1.09E+OO 591.76 4.95 4.30E-01 2 .31E+OO 692.4 2 1. 78 7.12E-01 8.13E+OO 723. 3 0 2 0.06 5.47E-02 7 . 62E-01 756.80 4. 52 4.55E-01 3.58E+OO

[2743]

3/14/2018 8:01 :51PM Page 6 of6 Analysis Report for 14-Mar-18-10046 81051 OOA-FSFC-255CV o.o* -o.s* 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCi/grams) (pCl/grams)

(keV)

Eu-154 873.18 12.08 -1.22E-01 1.70E-01 1.26E+OO 996.29 10.48 -2 .00E-01 1. 23E+OO 1 004.76 18.01 4.29E-02 9.62E-01 1274.43 34.80 -1.06E-01 4.86E-01 1596. 48 1. 80 -9.95E+OO 8. 2 0E+00 Eu-155 45.30 1. 31 2 .36E+OO 3.66E-0 1 2 . 06E+01 60.01 1.~2 1.45E+OO 2.23E+Ol 86.55 30.70 -1.39E-01 3.82E-01 105.31 21.10 1.09E-01 3.66E-01 Ra-226 186. 2 1 3.64 - 9.84E-0 2 2 .20E+OO 2 . 2 0E+OO Pa-231 2 7. 3 6 10. 3 0 1.92E+00 3.0lE+OO 3.0lE+OO 2 83.69 1. 70 2 .74E+OO 5. 72E+OO 3 00.07 2 .47 6.53E-01 3.93E+00 3 02.65 2 .20 3.30E+OO 4.30E+00 330.06 1. 40 -6.82E+OO 7.25E+OO U-235 14 3 .76 10.96 -2 . 2 3E-01 1.35E-01 6.04E-01 16 3 .3 3 5.08 8. 2 0E-0 2 l .44E+OO 185.71 57. 2 0 -8. 0 9E-02 l .35E-01 202 .11 1. 08 4.79E-01 7.35E+OO 205.31 5.01 -7.94E-01 1. 30E+OO Am-241 59.54 35.90 3.22E-01 7.90E-0 1 7.90E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2744]

0000024373.CNF Live Time :1200.000 sec Real Time :1200.290 sec 60 start: 1: -0.0(kev)

Stop: 8192 :2047.S(keV)

Acq. start :wed Mar 14 19:41:45 2018 55 50 45 40 35 V)

.µ s::::

8 30

[2745]

25 1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/14/2018 8:24:36PM Page I of6 Analysis Report for 14-Mar-18-10047 B105100A-FSFC-255CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10047 Sample Description : B105100A-FSFC-255CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.343E+02 grams Facility : Default Sample Taken On : 3/10/2018 8:45:00AM Acquisition Started : 3/14/2018 8:04:28PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120-8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description Sample Number : 24376 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 8:24:31PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2746]

3/14/2018 8:24:36PM Page 2 of6 Analysis Report for 14-Mar-18-10047 81051 OOA-FSFC-255CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.79 949 - 960 954. 72 3.06E+Ol 18.51 4.28E+Ol 0.90 2 351.81 1401 - 1413 1406.27 4.30E+Ol 15. 72 1.40E+Ol 0.55 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi-211 0. 91 351. 07

13. 02 l. 2 5E+OO 4.99E-01 Pb-212 0.99 115.18 0.60 23 8.63

43.60 l.99E-01 1. 2 4E-01 300.09 3.30 Pb-214 0.99 2 41.99 7. 2 5 295.22 18.42 351. 93

35.60 4.57E-01 1.82E-O l 785.96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2747]

3/14/2018 8:24:36PM Page 3 of6 Analysis Report for 14-Mar-18-10047 B105100A-FSFC-255CV 0.0" - 0.5" 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

? Bi-211 0.915 l.25E+OO 4.99E-01 Pb-21 2 0.997 l.99E-01 l.24E-01

? Pb-214 0.999 4.57E-01 l.82E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2748]

3/14/2018 8:24:36PM Page 4 of6 Analysis Report for 14-Mar-18-10047 8105100A-FSFC-255CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 8:24:31PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

An Pk 511. 00 100 . 00 2 .71E-01 2 .20E-01 2 .20E-01 BE-7 477.60 10.44 4.55E-01 9.83E-01 9.83E-01 K-40 1460.8 2 10.6 6 4. llE+OO 3.41E+OO 3.41E+OO Co-60 1173.23 99.85 3.74E-02 1.66E-01 1. 74E-01 1332.49 99.98 - 6.70E-02 1.66E-01 Nb-94 702.65 99.81 2.90E-03 1. 2 4E-01 1.38E-01 871.09 99.89 6.02E-02 1. 2 4E-01 Ag-108m 79.13 6.60 2 .60E+OO 1.12E-01 2 .53E+OO 433.94 90.50 -2 .13E-0 2 1.12E-01 614.28 89.80 -1.19E-01 1.43E-01 722. 94 90.80 -5.33E-02 1.46E-01 Sb-125 176.31 6.84 -3.79E-01 3 .79E-01 1.06E+OO 380.45 1. 52 -1. 2 0E+OO 7.02E+OO 427.87 2 9.60 4.92E-03 3.79E-01 463.36 1 0.49 1.89E-02 1.07E+OO 600.60 17.65 2. 90E-01 6.78E-01 606.71 4. 98 3.00E+OO 3.82E+OO 635.95 11. 22 -3.58E-01 8.79E-01 671.44 1. 79 5. 2 3E-02 7.48E+OO

[2749]

3/14/2018 8:24:36PM Page 5 of6 Analysis Report for 14-Mar-18-10047 B105100A-FSFC-255CV o.o* - o.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCilgrams)

(keV)

Ba-133 79.61 2 .65 5.62E+OO l.82E-01 6.02E+OO

81. 00 32 .90 -l.99E-02 3.86E-01 2 76.40 7.16 -l.'27E-01 l.14E+OO 3 02.85 18.34 -l.91E-01 4.58E-01 356.01 62.05 -9.22E-02 1. 82E-Ol 38 3 .85 8.94 l.93E-01 1. 30E+OO Cs-134 475.36 1. 48 -2 .03E-01 l.43 E- 01 6.34E+OO 563.25 8.34 l.12E+OO l.49E+OO 569.33 15.37 -2 .13E-01 8.14E-01 604. 72 97. 62 5.43E-03 l.73E-01 795.86 85.46 -1. 56E-01 l.43E-01 801.95 8.69 8.19E-01 l.48E+OO 1038.61 0.99 -l .94E+OO l.49E+Ol 1167.97 1. 79 1. 72E-01 8. 91E+OO 1365.19 3.02 -2 .66E+OO 4.67E+OO Cs-137 661.66 85.10 9.53E-02 2 .05E-01 2 .05E-01 Eu-152 121. 78 28.67 4.52E-02 2 .40E-01 2 .40E-01 244.70 7.61 3.80E-01 l.35E+OO 295.94 0.45 l.78E+Ol 2.80E+Ol 344.28 2 6.60 4.90E-02 3.33E-01 367.79 0.86 - 4.80E-01 1. 06E+01 411.12 2 . 24 -5.79E-01 4.44E+OO 443. 96 2 .83 -8.82E-01 3 .13E+OO 488 . 68 0 . 42 9.02E+OO 2.77E+Ol 563.99 0.49 -3.75E+OO 2.45E+Ol 586 . 26 0.46 -8.09E+OO 3. 2 9E+Ol 678.62 0.47 8.32E+OO 3.31E+Ol 688.67 0.86 3.13E-01 l.49E+Ol 719.35 0.28 2 .lOE+Ol 4.89E+Ol 778.90 12. 96 2 .81E-01 9.66E-01 810.45 0.32 4.87E+00 3.66E+Ol 867.37 4.26 6.99E-01 2 .90E+OO 919.33 0.43 8.19E+OO 3.30E+Ol 964.08 14.65 4.98E-Ol l. llE+OO 1 085.87 10.24 -9.63E-0 2 1. 07E+OO 1 089.74 1. 73 -l .46E+OO 8.35E+OO 1 112.07 13.69 9. llE-01 1. 35E+OO 1 2 12.95 1. 43 -1.88E+00 1.25E+Ol 1249.94 0.19 l.53E+Ol 5 . 71E+Ol 1299.14 1. 63 3.05E+OO 8.31E+OO 1408.01 21. 07 7.86E-03 8.27E-01 1457.64 0.50 7.42E+Ol 7.05E+Ol 1528.10 0.28 l.08E+Ol 6.64E+Ol Eu-154 123.07 40.40 7.63E-0 3 l .6 3E- 01 1.63E-01 247.93 6.89 2.37E-01 1. 23E+OO 591. 7 6 4.95 -4.94E-Ol 2 . 72E+OO 692.42 1. 78 1 . 82E+OO 6.19E+OO 72 3. 30 20.06 -2 .86E-01 6.39E-01 756.80 4. 52 -1.43E+OO 2 .83E+OO 873.18 1 2 .08 -5.88E-01 9. 72E-01 996.29 10.48 -1.78E-01 1.36E+OO

[2750]

3/14/2018 8:24:36PM Page 6 of6 Analysis Report for 14-Mar-18-10047 B1051 OOA-FSFC-255CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCilgrams)

(keV)

Eu-154 1004.76 18.01 9 . 11E-02 1.63E-01 7.98E-01 1 274.43 34.80 3.lOE-01 5. 2 9E-0 1 1596.48 1. 80 1.97E+OO 7. 3 5E+OO Eu-155 45.30 1. 3 1 -2 .67E+OO 3.60E-01 2 .02E+01 60.01 1. 22 8.80E+OO 2 .00E+Ol 86.55 3 0.70 7.07E-02 3.60E-01 105.3 1 2 1.10 9.08E-02 3. 96E-01 Ra-226 186.2 1 3 .64 -4.63E-02 2 .44E+OO 2 .44E+OO Pa-231 2 7.36 10 .3 0 1. 72E+OO 2 .83E+OO ~ .83E+OO 283 .69 1. 70 5.54E-01 5.60E+OO 300.07 2 .47 -2 . 36E+OO 4.02E+OO 302.65 2 .20 -1.77E-01 3 .97E+OO 330. 0 6 1. 40 3.45E+OO 7.27E+OO U-235 143.76 10 .96 -2.93E- 01 1.60E-01 6.64E-01 163. '.?3 5.08 -5.41E- 01 1.31E+OO 185.71 57. 2 0 8.17E-02 1. 60E-01 202 .11 1. 08 3.28E+OO 7.54E+OO 205.31 5.01 5.44E-02 1.62E+OO Am-241 59.54 35.90 1. 32E-01 6.76E-01 6.76E-01

+ ;;; Nuclide identified during the nuclide identification

"' Energy line found in the spectrum MDA value not calculated Half-life too short to be able to perform the decay correction

? ;;;

CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2751]

0000024376.CNF Live Time* :1200.000 sec Real Tille :1200. 300 sec 60 start: 1: -0 .0(kev)

Stop : 8192: 2047. B(kev)

Acq . start :wed Mar 14 20:04:28 2018 55 50 45 40 35

[2752]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: l

3/14/2018 12:45:17AM Page 1 of6

-~pex-Gamma Analysis Report for 14-Mar-18-10001C.

B105100A-FSF'/-263CV

~ \a~

0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10001 Sample Description : B105100A-FSFW-263CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.104E+02 grams Facility : Default Sample Taken On : 3/10/2018 12:15:00PM Acquisition Started : 3/14/2018 12:25:09AM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.6 seconds Dead Time : 0.13 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description Sample Number : 24324 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 12:45:13AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2753]

3/14/2018 12:45:17AM Page2 of6 Analysis Report for 14-Mar-18-10001 B1051 OOA-FSFW-263CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 352 .01 700 - 708 703.97 3 . 2 6E+Ol 1 7.76 4. 2 8E+Ol 1. 0 3 2 609 . 51 12] 4 - 1223 1218.60 2 . 3 9E+Ol 13. 73 ')

.03E+Ol 1. 2 0 3 661.68 132 0 - 1328 1322.89 4. 3 6E+Ol 18.03 3 .08E+Ol 1. 48 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Cs- 1 37 1. 00 66 1 .66

85. 10 3.47E-01 l.49E-01 Bi -2 11 0.86 351.07 *:~: 13. 02 1.06E+OO 6 . 03E-01 Bi -2 14 0.99 609.32 45.49 3 .35E-01 1.97E-01 768.36 4.89 806.18 1. 26 934.06 3 .11 1120.29 14. 92 1155.21 1. 63 1238.12 5.83 1 2 8 0 .98 1. 43 1377.67 3.99 1385. 3 1 0.79 1401.52 1. 33 1407.99 2 .39 1509.21 2.13 1661. 2 7 1. 0 5

[2754]

3/14/2018 12:45:17AM Page 3 of6 Analysis Report for 14-Mar-18-10001 B105100A-FSFW-263CV 0.0" - 0.5" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1729.59 2 .88 1764.49 15.30 1847.43 2.03 2 118.51 1.16 Pb-214 0.99 241.99 7.25 2 95.22 18.42 3 51.93

35.60 3.88E-01 2.20E - 01 785.96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

Cs-137 1. 000 3.47E-01 l.49E-01

? Bi-211 0.867 1.06E+OO 6.03E-01 Bi-21 4 0.998 3.35E-01 1.97E-01

? Pb-214 0.999 3.88E-01 2 . 2 0E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2755]

3/14/2018 12:45:17AM Page4 of6 Analysis Report for 14-Mar-18-10001 B105100A-FSFW-263CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 12:45:13AM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region_

m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi!grams) (pCilgrams) (pCl!grams)

(keV)

An Pk 511.00 100.00 4.29E-01 2. 84E-01 2 .84E-01 BE-7 477.60 10.44 4.53E-01 1.58E+00 1.58E+OO K-40 1460.82 10.66 3 .93E+OO 3 .87E+OO 3. 87E+OO Co-60 1173.23 99.85 1.04E-01 :.21E-01 2 . 2 1E-01 13 32 .49 99.98 8.88E-02 2 .47E-01 Nb-94 702.65 99.81 -4.93E-02 1 .4~E-01 1.43E-01 871.09 99.89 -5.88E-02 1.42E-01 Ag-108m 79.13 6.60 4.56E-01 1.62E-01 2 .93E+OO 433.94 90.50 -1.06E-03 1.62E-01 614. 2 8 89.80 -4.44E-0 2 2° .09E-01 722 . 94 90.80 6.18E-0 2 l .93E-01 Sb-125 1'76.31 6.84 - 7.53E-01 3.47E- 01 1.98E+OO 3 80.45 1. 5 2 - 4.46E+OO 8.67E+00 427.87 2 9.60 -2 .31E-01 3 . 47E-01 463.36 10.49 -l.27E-01 1 . 45E+OO 600.60 17.65 4 .13E-01 8 . 92E-01 606.71 4.98 1.75E-01 4.49E+OO 635.95 11. 22 3.97E-01 1 . 46E+OO 671. 44 1. 79 -3.lOE+OO 9. llE+OO

[2756]

3/14/2018 12:45:17AM Page 5 of6 Analysis Report for 14-Mar-18-10001 B105100A-FSFW-263CV o.o*: - 0.5 0.0" Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCVgrams) (pCi/grams) (pCi!grams)

(keV)

Ba-13 3 79.61 2.65 1.35E+OO 2 .74E-01 6.99E+OO

81. 00 32 .90 -2 .83E-01 4.70E-01 2 76.40 7.16 -8.94E-01 1.83E+OO 302.85 18.34 3.69E-02 7.34E-01 356.01 62.05 -5.89E-0 2 2 .74E-0 1 383.85 8.94 -2 . 2 8E-01 1.54E+OO Cs-134 475.36 1. 48 -2.44E+OO 1.84E-01 1.00E+Ol 563. 2 5 8.34 -3.81E-01 1.60E+OO 569.33 1 5.37 -2 . 3 6E-01 9.21E-01 604. 72 97.6 2 -4.09E-02 1 .84E-01 795.86 85.46 9.00E-02 2.05E-01 801.95 8.69 5.65E-01 1.80E+OO 1038.61 0.99 -5.09E+OO l.61E+Ol 1167.97 1. 79 -1.71E+OO 1.13E+Ol 1365.19 3 .0 2 l.64E+OO 6.09E+OO

+ Cs-137 661.66

85.10 3.47E-Ol 1. 89E- 01 1.89E-01 Eu-152 121 . 78 28.67 -1.54E-0 2 3 .90 E- 01 3.90E-01 244.70 7.61 -1.84E-01 1. 81E+OO 295.94 0.45 2 .86E+Ol 3.73E+Ol 344.28 2 6.60 -1.47E-01 5. 3 8E-01 367.79 0.86 1 .09E+Ol 2 .02E+Ol 411.12 2.24 l .69E+OO 6.40E+OO 443.96 2.83 -2.37E-01 5.21E+OO 488.68 0.42 - l.68E+Ol 3 . 21E+Ol 563.99 0.49 7.38E+OO 2 .92E+Ol 586.26 0.46 2 .25E+Ol 4.49E+Ol 678.62 0.47 3.32E+OO 3 . 71E+Ol 688.67 0.86 -6.29E+OO 1.79E+Ol 719.35 0. 2 8 1.48E+OO 5.83E+Ol 778.90 12. 96 -9.74E-0 1 9.12E-01 810.45 0 . 32 -1.66E+Ol 5.06E+O l 867.37 4.26 2.24E+OO 4.46E+OO 919.33 0.43 2.40E+Ol 5.35E+Ol 964. 0 8 14.65 2.59E-01 1. 55E+OO 1085.87 1 0.24 2.66E-01 1.74E+OO 1089.74 1. 73 -l. 2 4E+OO 1.07E+Ol 1112.07 13. 69 3.70E-Ol l.32E+OO 1212.95 1. 43 -6.lOE+OO l.40E+Ol 1 2 49.94 0.19 -9.67E+OO 6.89E+Ol 1 2 99.14 1. 63 -5 . llE+OO 1. 2 4E+Ol 1408.01 2 1.07 -3 .42E-01 6. 7.6E-01 1457 . 64 0.50 8.69E+Ol 3.28E+Ol 1528.10 0. 2 8 -9 .76E+OO 5.41E+Ol Eu-154 1 2 3.07 40.40 l.06E-01 2 .94E-01 2 .94E-01 247.93 6.89 - 9. 72E-01 1. 72E+OO 591. 76 4.95 7.54E-01 3. 2 1E+OO 692.42 1. 78 l.67E+OO 9. 1 5E+OO 723.30 2 0.06 4.16E-Ol 8.94E-01 756.80 4.5 2 -9.42E-0 1 3.92E+OO 873.18 12.08 -9.41E-Ol 9.95E-01 996. 2 9 10.48 4.00E-0 1 1.67E+OO

[2757]

3/14/2018 12:45:17AM Page 6 of6 Analysis Report for 14-Mar-18-10001 B105100A-FSFW-263CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCilgrams) (pCl/grams) (pCl/grams)

(keV)

Eu-154 1004.76 18.01 -3.53E-01 2 .94E-01 7.81E-01 1274.43 3 4.80 6.08E-02 2 .94E-01 1596.48 1. 80 4.94E+OO 1.lOE+Ol Eu-155 45.30 1. 31 1. 52E-01 4.90 E- 0 1 2 .56E+01 60.01 1. 22 -1.02E+0 1 3.14E+Ol 86.55 30.70 1.0SE-0 1 4.90E-01 1 05.31 2 1. 10 -2 .22E-0 1 5.lOE-01 Ra-226 186.21 3.64 2 .50E+OO 4.18E+OO 4.18E+OO Pa-23 1 27.36 10. 3 0 1.lOE+OO 2 .90E+OO 2 .90E+OO 2 83.69 1. 70 2 .94E+OO 8.40E+OO 300.07 2 .47 -7.08E+OO 4. 96E+00 302.65 2 .20 3.08E-01 6. llE+OO 330.06 1. 40 4.69E+OO 1. 03E+01 U-235 143. 7 6 10.96 -3 . 2 8E-01 2. 61E-0 1 1.04E+00 163.33 5.08 -5.23E-01 2. 50E+OO 185.71 57.2 0 1.16E-01 2. 61E-01 202 .11 1. 08 5.85E+OO 1.27E+01 205.31 5.01 -1 . 33E+OO 2 .50E+OO Am-241 59.54 35.90 -4.llE-01 1. 07E+OO 1.07E+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2758]

0000024324.CNF Live Tine :1200 .000 sec 60 Real Tille :1201.620 sec start: 1: O.l(kev) stop : 4096 :2047. l(kev)

Acq. Start :wed Mar 14 00:25:09 2018 55 50 45 40 35

[2759]

a>

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/14/2018 1:15:13AM Page I of6

~~~pex-Gamma Analysis Report for 14-Mar-18-10002 C:

8105100A-FSF,r.263CV

(.-,.~

0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10002 Sample Description : 8105100A-FSFW-263CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.104E+02 grams Facility : Default Sample Taken On : 3/10/2018 12: 15:00PM Acquisition Started : 3/14/2018 12:55:04AM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.5 seconds Dead Time : 0.13 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description Sample Number : 24326 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 1:15:07AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2760]

3/14/2018 1:15:13AM Page 2 of6 Analysis Report for 14-Mar-18-10002 B 105100A-FSFW-263CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 609.83 1214 - 1224 1219.23 2. 72E+Ol 16.99 3.77E+Ol 0.93 2 1461.37 2917 - 2926 2922.79 2.42E+Ol 13.31 l.77E+Ol 1. 72 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.95 1460.82

10 .66 2 .67E+OO l.49E+OO Bi-214 0.98 609. 32 :': 45.49 3 .82E-01 2 .43E-01 768.36 4.89 8 0 6. 1 8 1.26 934. 0 6 3. 11 1120. 2 9 14.92 1155.21 1. 63 1238.12 5.83 128 0 .98 1. 43 1377.67 3.99 1 3 85.3 1 0.79 1401. 52 1. 33 1407.99 2.39 1509.21 2.13 1661.27 1. 05 1729.59 2.88 1 764.49 15.30

[2761]

3/14/2018 1:15:13AM Page 3 of6 Analysis Report for 14-Mar-18-10002 8105100A-FSFW-263CV 0.0" - 0.5" 0.5" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi-214 0.98 1847.43 2.03 2118.51 1.16

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold= 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.954 2.67E+OO l.49E+OO Bi-214 0.983 3.B2E-01 2.43E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2762]

3/14/2018 1:15:13AM Page 4 of6 Analysis Report for 14-Mar-18-10002 8105100A-FSFW-263CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 1:15:07AM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

An Pk 511. 00 100.00 3.42E-01 2 .81E-01 2. 81E-01 BE-7 477.60 10.44 -9.49E-01 1.18E+OO l.18E+OO

+ K-40 1460.82

10.66 2 .67E+OO 2 .00E+OO 2 .00E+OO Co-60 11 73.23 99.85 4.79E-02 2 .49E-01 2. 49E- 01 1332.49 99.98 1.61E-01 2 .72E- 01 Nb-94 702.65 99.81 2 .39E-0 2 1 .71E-01 1. 72E-01 871.09 99.89 3.63E-02 1.71E-01 Ag-1 0 8m 79. 1 3 6.60 -7.80E-02 1.45E- 01 2 .61E+OO 433.94 90 . 50 4.32E-02 l.45E-01 614. 2 8 89.80 -2 .64E-02 2 .46E-01 722 . 94 9 0 .80 -5.75E-0 2 1.65E-01 Sb- 1 2 5 176.31 6. 8 4 1.06E+OO 4. 1 4E-01 2 .03E+OO 38 0 .45 1. 52 -4 . 1 6E+OO 8.80E+OO 4 2 7.87 29.60 -1.25E-0 1 4.14E-01 463.36 10 .49 -1.07E+OO 1.lOE+OO 600.60 17.65 8.04E-02 9.98E-01 606. 71 4.98 -6.99E-02 5.32E+OO 635.95 11. 22 -2 .94E-02 1. 2 3E+OO 671. 44 1. 79 - 3 .83E-01 8.90E+OO

[2763]

3/14/2018 1:15:13AM Page 5 of6 Analysis Report for 14-Mar-18-10002 B105100A-FSFW-263CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi!grams) (pCilgrams) (pCi/grams)

(keV)

Ba- 133 79.61 2 .65 8.07E-01 2. 61 E- 01 6 . 34E+OO 81.00 32 .9 0 -5.78E-01 3 .89E-01 2 76.40 7.16 3.02E-01 1. 88E+OO 302.85 18. 3 4 5.03E-01 8.17E-01 356.01 62 .05 6. 96E-02 2 .61E-01 383 . 85 8.94 - 3 .83E-01 1. 43E+OO Cs-13 4 475.36 1. 48 3.04E-01 l.63E-Ol 8.59E+OO 563. 25 8. 3 4 2 .02E-01 l .68E+OO 569. 33 1 5.37 l.18E-01 9. 2 1E-01 604. 72 97.6 2 - 2 .76E-02 2 . 2 4E-01

95.86 85.46 8 .13E-03 1. 63E-01 801.95 8.69 3.70E- 01 l.86E+OO 1038.61 0.99 5.54E+O O l.95E+Ol 11 67.97 1. 79 -l.62E+Ol 1.05E+Ol 1365. 1 9 3.0 2 1.15E+OO 5.76E+OO Cs-137 661.66 85.10 2 .28E-01 2.68E-01 2 .68E-01 Eu-152 121 . 78 2 8.67 l .89E-02 3. 96E-01 3 .96E-01 244.70 7.6 1 -8.68E-01 1. 83E+OO 2 95.94 0. 45 l.77E+Ol 3 .47E+Ol 3 44. 2 8 26.60 - l.15E-01 5.03E-01 3 67.79 0.86 -2 .63E+OO l .63E+Ol 4 11 .12 2.24 3. 2 0E-02 5.73E+OO 443.96 2.83 O. OOE+OO 5. 2 1E+OO 488.68 0.42 -8.25E+OO 3 .07E+Ol 563 . 99 0.49 l. 2 7E+OO 2 . 71E+Ol 586. 2 6 0.46 l. 2 5E+Ol 4.33E+Ol 678.6 2 0.47 6.73E-01 3 .48E+01 688.67 0 . 86 -1. 72E+Ol 1. 46E+Ol 719.35 0. 2 8 l.04E+01 5.68E+Ol 778.90 12 .96 2.89E-01 l.33E+OO 810.45 0. 32 -l.30E+Ol 4.56E+Ol 867 . 37 4. 26 -8.99E-03 4.2 3E+OO 919.33 0.43 -6.64E-0 2 4. 2 7E+01 964. 0 8 14.65 - 9.56E-Ol l.13E+OO 1 0 85.87 10. 2 4 7.05E-01 1.67E+OO 1089.74 1. 73 -4.05E+OO 8.57E+OO 1112.07 13. 69 -3.40E-02 l.47E+OO 1212.95 1. 43 2.84E+00 1.45E+Ol 1 2 49.94 0.19 -l.31E+Ol 8.08E+Ol 1 2 99.14 1. 63 - 3.79E+OO 8.23E+OO 1408. 01* 21. 07 - 1.57E-01 7.38E-01 1457.64 0.5 0 7.66E+Ol 7.68E+O l 1 528.10 0. 2 8 - 2 .17E+Ol 3.33E+Ol Eu-154 123.07 40.40 9.97E-02 2 .76E-0 1 2 .76E-01 2 47.93 6.89 8.92E-01 2 .07E+OO 591.76 4.95 - 7. llE-0 2 3 . 3 3E+00 692.42 1.. 7 8 - 2. 81E-02 8. 2 0E+OO 723. 30 2 0.06 -5.75E-02 7.71E-01 756.80 4. 52 2 .08E+OO 3.82E+OO 873.18 12.08 3 .59E-01 l.28E+OO 996. 29 10.48 3 .21E-01 1. 48E+OO

[2764]

3/14/2018 1:15:13AM Page 6 of6 Analysis Report for 14-Mar-18-10002 B105100A-FSFW-263CV o.o* - o.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCVgrams) (pCl/grams)

(keV)

Eu-154 1004.76 18.01 - 8 . 99E-0 2 2 .76E-01 7.34E-01 12'74.43 34.80 -1.60E-01 5.71E-01 1596.48 1. 80 6.35E+OO 1. 22E+Ol Eu-155 45.30 1. 3 1 1.llE+Ol 4 . 75E - 01 3.06E+O l

60. 01 1. 22 -7 . 49E+OO 2 .9 1E+O l 8G.55 30.70 1. 41E-01 4 .75E-01 1 0 5.31 21.10 - 1.60E-01 5.38E-01 Ra-226 186. 2 1 3.64 1. llE+OO 4. 1 3E+OO 4.13E+OO Pa-231 27.36 10. 3 0 1.06E+OO 2 . 9 0E+OO 2 .90E+OO 283.69 1. 70 -5.14E+OO 6.21E+OO 30 0 .07 2 .47 -5.09E+OO 5.77E+OO 302.65 2 .20 4.19E+OO 6.80E+OO 330. 0 6 1. 40 1.94E+OO 1. 05E+Ol U-235 143.76 10. 96 6.06E-01 2 .67E-01 1.15E+OO 1 63 . 33 5.08 6.00E-01 2 .77E+00 185.71 57. 2 0 1.61E-01 2 .67E-01 202 .11 1. 08 -1.93E+OO l .16E+Ol 205.31 5.01 8.61E-01 2 .53E+OO Am-241 59.54 35.90 -4.77E-02 1.05E+OO 1. 05E+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2765]

0000024326.CNF Live Time :1200.000 sec Real Time :1201.540 sec Start: 1: O.l(kev) stop : 4096 :2047. l(kev)

Acq. Start :Wed Mar 14 00:55:04 2018

[2766]

=

I I

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/13/2018 9:41:01PM Page I of6 Analysis Report for 13-Mar-18-10020 8105100A-FSFC-276CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10020 Sample Description : 8105100A-FSFC-276CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.227E+02 grams Facility : Default Sample Taken On : 3/9/2018 10:20:00AM Acquisition Started : 3/13/2018 9:20:53PM Procedure : Puck_half_inch.

Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.7 seconds Dead Time : 0.14 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24310 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 9:40:57PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2767]

3/13/2018 9:41:01PM Page 2 of6 Analysis Report for 13-Mar-18-10020 81051 OOA-FSFC-276CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid *Area Uncertainty Counts (keV) 1 2 38.65 473 - 481 477.49 3. 72E+Ol 26 . 85 1.28E+02 0.99 2 352.00 699 - 708 703.95 6. 72E+Ol 2 0.93 3 .76E+01 1. 51 3 609. 22 1 214 - 1 223 1 2 18.01 3.52E+Ol 16.59 2 .95E+Ol ' 1.20 4 1120. 58 2 237 - 2 244 22 40.71 1.61E+Ol 8.45 1 .76E+OO 1. 29 5 1460.82 2 916 - 2 927 2921 .70 4.45E+Ol 13. 92 3.09E+00 1. 52 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 1. 00 1460.82

10.66 4.42E+OO 1. 44E+00 Bi- 211 0.87 351.07

13. 0 2 1.97E+OO 6.90E-01 Pb - 212 1. 00 115 .18 0.60 238.63

43.60 2.45E-01 1. 81E-01 300.09 3.30 Bi - 214 0. 9 9 609.32

45.49 4.45E-01 2 .16E-01 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120. 2 9

14.92 9.43E-01 5 . 0lE-01 1155. 2 1 1. 63 1238.12 5.83 1 2 80 . 98 1. 43 13 77 . 67 3.99

[2768]

3/13/2018 9:41:01PM Page 3 of6 Analysis Report for 13-Mar-18-10020 B 105100A-FSFC-276CV 0.0" - 0.5" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi-214 0.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 1 5 09.21 2 .13 1661. 27 1. 05 1729.59 2 .88 1764.49 15.30 1847.4 3 2 .03 2118.51 1.16 Pb-214 1. 00 2 41.99 7. 2 5 2 95. 22 1 8.4 2 3 51.93

3 5.60 7. 2 0E-01 2 .52E-01 785.96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

K-40 1. 000 4.42E+OO 1.44E+OO

? Bi-211 0.870 1.97E+OO 6.90E-01 Pb-21 2 1. 000 2 .45E - 01 1.81E-01 Bi-214 0.998 5.23E- 01 1.99E-01

? Pb-214 1. 000 7.20E-01 2 .52E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2769]

3/13/2018 9:41:01PM Page4 of6 Analysis Report for 13-Mar-18-10020 8105100A-FSFC-276CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 9:40:57PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCilgrams) (pCilgrams)

(keV)

An Pk 511. 00 100.00 3.29E-01 2 .55E-01 2 .55E-01 BE-7 477.60 10.44 -6.09E-02 1.31E+OO 1.31E+OO

+ K-40 1460.82

10.66 4.42E+OO 9.59E-01 9.59E-01 Co-60 1 173. 23 99.85 -1.65E-02 1.98E-01 2 .09E-01 1 332 .49 99.98 3.48E-02 1.98E-01 Nb-94 702.65 99.81 3.37E-02 1. 3 9E-01 1.51E-01 871. 09 99.89 2 .87E-0 2 1 . 39E-01 Ag-108m 79.13 6.60 1.69E+00 1.35E-01 2. 83E+OO 433.94 90.50 -2 .lSE-02 1. 35E-01 614.28 89.80 -1.21E-01 2 .09E-01 722. 94 90.80 6.40E-02 1.77E-01 Sb-125 176.31 6.84 - 4.78E-01 4.43E- 01 1 . 71E+OO 380.45 1. 52 l .90E+OO 8.79E+00 4 2 7.87 29.60 1.14E-01 4.43E-01 463.36 10.49 2 .98E-02 1.23E+OO 600.60 17.65 -2 .80E-01 7.51E-01 606.71 4.98 -4.38E-01 4 . 69E+OO 635.95 11. 22 4.21E-01 1 . 42E+OO 671 . 44 1. 79 -2 .67E+00 8 .2 1E+OO

[2770]

3/13/2018 9:41 :01PM Page 5 of6 Analysis Report for 13-Mar-18-10020 B105100A-FSFC-276CV 0.0" - 0.5 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCi/grams)

(keV)

Ba-13~ 79.61 2.65 4.06E+OO 2. 72E-01 6.83E+OO

81. 00 3 2 .90 -4.52E-01 4.36E-01 276.40 7. 1 6 3 .82E-02 1. 53E+OO 302.85 18.34 3 .34E-02 6.73E-01 356.01 62.05 -1. 74E-01 2 .72E-01 3 83.85 8.94 7.76E-01 1.53E+OO Cs-134 475. 3 6 1. 48 -3.38E+OO 1.98E-Ol 8.73E+OO 563.25 8.34 7.lOE-01 1 .66E+OO 569. 33 1 5.37 -3 .66E-01 9. 2 4E-01 604. 72 97. 62 -7.68E-02 2 .08E-01 7 95.86 85.46 7.25E-02 1.98E-01 801 . 95 8.69 5.87E-0 2 1.57E+OO 1038.61 0.99 7.55E+OO 1 . 70E+Ol 1167. 97 1. 79 1.46E-Ol 1. 20E+Ol 1365.19 3 .0 2 -5.28E-Ol 5 .75E+OO Cs-13 7 661.66 85.10 8.65E-02 1. 89E-01 1. 89E-01 Eu-1 52 12 1 .78 2 8.67 4.20E-02 3 . 1 9E- 01 3. 19E-01 244.70 7 . 61 2 . 2 2E-01 1.67E+OO 295.94 0.45 2 .00E+Ol 3 .23E+Ol 344. 2 8 2 6.60 9.84E-02 4.95E-01 367.79 0.86 -3.15E+OO 1. 31E+Ol 411 . 12 2 . 24 6.24E-01 6.38E+OO 443.96 2 .83 -1.63E+OO 4.08E+OO 488.68 0.42 6 . 69E+OO 3. 2 3E+Ol 563 . 99 0.49 1.55E+Ol 2.81E+Ol 586.26 0.46 3.08E+Ol 3.75E+Ol 678.62 0.47 - 1 .25E+Ol 3 .13E+Ol 688.67 0.8 6 -4.87E+OO 1.74E+Ol 719.35 0. 2 8 -3.62E+Ol 5. llE+Ol 778.90 12. 96 5.0lE-0 2 9.51E-01 810 .45 0. 32 9. 1 9E+OO 4.82E+Ol 867.37 4. 26 -4. 2 7E-01 2 .98E+OO 919.33 0.43 1. OOE+Ol 3.84E+Ol 964.08 14.65 -2 .57E-01 1. 42E+OO 1 085.87 10. 2 4 2 .78E-01 l.51E+OO 1 089.74 1. 73 4.93E+OO 1 . 00E+Ol 1112.07 13.69 -3.02E-01 1 :3 6E+OO 1212.95 1. 43 -4.19E+OO 7.22E+OO 1249.94 0 .19 3.53E+Ol 1.10E+02 1 299.14 1. 63 4.24E+OO 1.03E+Ol 1408.01 2 1. 0 7 -1.02E-01 9.51E-01 1457.64 0. 5 0 O.OOE+OO 7.45E+Ol 1528.10 0. 2 8 -1.95E+Ol 2 .99E+Ol Eu-154 123. 0 7 40.40 -9.35E-0 2 2 .06E - 01 2 .06E-01 247.93 6.89 -1. 72E+OO 1.44E+OO 591.76 4.95 5.28E-01 2 .SlE+OO 692.4 2 1. 78 4.00E+OO 8.23E+OO 723. 30 2 0.06 2.31E-01 8.04E-01 7 56.80 4.52 -9.07E-01 2 .67E+OO 873. 1 8 12.08 -6. 2 6E-0 2 1.15E+OO 996.29 10.48 -3.86E-02 1. 39E+OO

[2771]

0000024310.CNF .

Live Tfae :1200.000 sec Real Tille :1201. 680 sec start: 1: O.l(kev) stop : 4096: 2047. l(kev)

Acq. start :Tue Mar 13 21:20:53 2018

[2772]

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/13/2018 10:02:45PM Page 1 of6

~pex-Gamma Analysis Report for 13--Mar-18-10021 B105100A-FSFC-276CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10021 Sample Description : B105100A-FSFC-276CV o.o* - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.227E+02 grams Facility : Default Sample Taken On : 3/9/2018 10:20:00AM Acquisition Started : 3/13/2018 9:42:36PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.7 seconds Dead Time : 0.14 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24312 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on 3/13/2018 10:02:40PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2773]

3/13/2018 10:02:45PM Page2 of6 Analysis Report for 13-Mar-18-10021 B 1051 OOA-FS FC-276CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 351.95 701 - 708 703.84 5.70E+Ol 19.79 4.00E+Ol 0.99 2 609.36 1215 - 1223 1218.29 2 .66E+Ol 13.38 1.68E+Ol 1. 35 3 1461.19 2916 - 2926 2922 .44 3 .40E+Ol 13.18 8.00E+OO 1. 54 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.97 1460. 82 *):

10.66 3.38E+OO 1. 34E+OO Bi-211 0.88 351.07

13 . 0 2 l.67E+OO 6 . 39E-01 Bi-2 1 4 1. 00 609. 32

45.49 3. 3 6E-01 1.74E-01 768.36 4.89 806.18 1. 26 934.06 3 .11 1120. 2 9 14.92 1155. 2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 1509. 2 1 2 .13 1661. 2 7 1. 05

[2774]

3/13/2018 10:02:45PM Page 3 of6 Analysis Report for 13-Mar-18-10021 8105100A-FSFC-276CV 0.0" - 0.5" 0.5" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1. 00 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1. 00 2 41. 99 7.25 2 95. 22 18.42 351.93

35.60 6.lOE-01 2.3 3E-01 785.96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.978 3.38E+OO 1. 34E+OO

? Bi-211 0.884 1.67E+OO 6.39E-01 Bi-214 1. 000 3.36E-Ol l.74E-01

? Pb-214 1.000 6.lOE-01 2 .33E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2775]

3/13/2018 10:02:45PM Page 4 of6 Analysis Report for 13-Mar-18-10021 8105100A-FSFC-276CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 10:02:40PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCilgrams) (pCi!grams)

(keV)

An Pk 511. 00 100.00 2.80E-01 2 .33E-01 2.33E-01 BE-7 477.60 10.44 -5.17E-01 1.16E+OO 1.16E+OO

+ K-40 1460.82

10.66 3.38E+OO 1.32E+OO 1.32E+OO Co-60 1173.23 99.85 3.33E-02 1.82E-01 1.82E-01 133 2 .49 99.98 5.34E-02 2 . llE-01 Nb-94 702.65 99.81 6 . 05E-02 1.44E-01 1.51E-01 871.09 99.89 2 .89E-02 1.44E-01 Ag- 108m 79 .13 6.60 3 . 3 0E-01 l.48E-01 2 .57E+OO 433.94 90.50 2 .22E-0 2 1. 48E-01 614.28 89.80 -1.58E-02 1.85E-01 72 2 . 94 90.80 -2.55E-03 1.77E-01 Sb-125 176.31 6.84 1 .81E-01 4. 2 3E- 01 1.73E+OO 380.45 1. 52 -3.32E+OO 7.44E+OO 427.87 2 9 .60 -4.15E-0 2 4.23E-01 463.36 10.49 -2.06E-01 9.90E-01 600.60 17.65 - 1.17E-01 7 . 13E-01 606.71 4.98 -2.73E+OO 4.00E+OO 635.95 11. 2 2 2.89E-01 1. 2 9E+OO 671. 44 1. 79 -5.21E+OO 7. 1 8E+OO

[2776]

3/13/2018 10:02:45PM Page 5 of6 Analysis Report for 13-Mar-18-10021 81051 OOA-FSFC-276CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl!grams) (pCUgrams) (pCi/grams)

(keV)

Ba-133 79. 61 2 .65 -1.38E+OO 2.79E-01 5. 96E+OO

81. 00 32 .9 0 -4.62E-01 4 . 06E-01 276.40 7.16 -4.58E-01 1.57E+OO 302.85 18.34 2 .49E-01 6.05E-01 356.01 62.05 -1. llE-01 2 .79E-01 383.85 8. 94 - 6. 81E-02 1. 41E+OO Cs-134 475.36 1. 48 -3 .25E+OO l .69E-01 7.17E+OO 563.25 8.34 -1 . 80E-01 1.82E+OO 569.33 15 .37 7.59E-02 9.06E-01 604. 72 97. 62 -1 . 98E-01 1. 76E-01 795.86 85.46 8. llE-02 1. 69E-01 8 01 .95 8.69 - 4.52E-01 1. 51E+OO 10 38.6 1 0.99 1.68E+Ol 2 .05E+Ol 11 67.97 1. 79 7 .36E-01 1.05E+Ol 1365. 1 9 3.0 2 -3.67E-01 4.53E+OO Cs-137 661.66 85.10 2 .97E-02 1. 85E-01 1. 85E-01 Eu-152 1 2 1 .78 2 8.67 1.48E-01 3 .76E-0 1 3.76E-01 2 44.70 7.61 4.77E-01 1.66E+OO 2 95.94 0.45 2 .00E+Ol 3.16E+Ol 344.28 26.60 -1.39E-0 1 4.95E-01 367.79 0.86 2 .51E+OO 1.41E+Ol 411.12 2 .24 3.66E+OO 6.38E+OO 443. 96 2 .83 -1.38E+OO 4.47E+OO 488.68 0.42 9.34E+OO 3 . 3 4E+Ol 563 . 99 0.49 -2.95E+OO 3.08E+Ol 586.26 0.46 1.80E+Ol 3.65E+Ol 678.62 0.47 5.62E+OO 3.53E+Ol 688.67 0.86 -3.39E+OO 1.70E+Ol 719.35 0.28 3.30E+Ol 6.33E+Ol 778.9 0 12.96 -2.05E-0 1 1 .19E+OO 810 .45 0.32 -4.04E+00 4.69E+Ol 867.37 4.26 -3.88E-01 3.37E+00 919 . 33 0.43 -2.91E+Ol 3.23E+Ol 964.08 1 4 .65 -8.12E-01 8.40E-01 1085.87 10.24 -4.99E-01 l .44E+OO 10 89.74 1. 73 -1.42E+OO 9.66E+OO 1 112. 07 13.69 -3. 2 8E-01 1.14E+OO 1212.95 1. 43 1.45E+OO l.06E+Ol 1249.94 0.19 1.45E+OO 9.69E+Ol 1 299.14 1. 63 -5.49E+00 6.64E+OO 1 408.01 21.07 9. 2 1E-02 9.17E-01 1457.64 0.50 6.40E+Ol 6.99E+Ol 1528.10 0.28 6.83E+O O 6.42E+Ol Eu-154 123.07 40.40 4.48E-03 2 .55E-0 1 2 .55E-01 247.93 6.89 -1. 2 5E+OO 1.62E+OO 591.76 ' 4.95 1. 32E+OO 2 .83E+OO 692. 4 2 1. 78 -4.16E+OO 6.91E+OO 723.30 20.06 -1.75E-01 7.70E-01 756.80 4.52 -1 . 80E+OO 3.36E+OO 873.18 12.08 - 2 .83E-01 1.0lE+OO 996.29 1 0 .48 -6.94E-0 1 1.70E+OO

[2777]

3/13/2018 10:02:45PM Page 6 of6 Analysis Report for 13-Mar-18-10021 B1051 OOA-FSFC-276CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCilgrams) (pCi/grams)

(keV)

Eu-1 5 4 1004.76 18.01 -4.48E-01 2 .55E-01 7.79E-01 1274.4 3 34.80 6.34E-02 5.14E-01 1596.48 1. 80 1.06E+OO 9 .2 8E+OO Eu-155 45.30 1. 31 1. 05E+Ol 4.89E-01 2. SOE+Ol

60. 0 1 1. 22 -5.90E+OO 2 .70E+Ol 86.55 30.70 2.07E-02 4.89E-01 105.31 2 1. 10 -8. 3 3E-02 5 .17E-01 Ra- 22 6 186.21 3.64 1 .86E+OO 3 .79E+OO 3.79E+00 Pa-231 2 7.36 10.30 1. 3 9E+OO 2 .73E+OO 2 .73E+OO 283.69 1. 70 6.59E-0 1 7. 2 5E+OO 300.07 2. 47 -5. 3 8E+OO 4.41E+OO 302.65 2 .20 2 .07E+OO 5.04E+OO 330.06 1. 40 1. 05E+OO 9.99E+OO U-2 35 143.76 1 0 .96 4.15E-02 2 .38E-01 1. 02E+OO 163.33 5.08 1.69E+OO 2 .57E+OO 185. 71 57. 2 0 8 . 92E-02 2 .38E-01 202. 11 1. 08 -5.16E+OO 1. llE+Ol 205.31 5.01 -6.96E-01 2 .40E+00 Am- 241 59 . 54 35.90 7.29E-02 9.54E-01 9.54E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Haif-life too short to be abie to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2778]

0000024312.CNF Live Time :1200.000 sec Real Tire :1201.670 sec 60 Start: 1: O.l(kev) stop : 4096:2047 .l(kev)

Acq. start :Tue Mar 13 21:42:36 2018 55 50 45

[2779]

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/14/2018 8:02:14PM Page I of6

,~pex-Gamma Analysis Report for 14-Mar-18-10048 B105100A-FSFC-282CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10048 Sample Description : B105100A-FSFC-282CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.167E+02 grams Facility : Default Sample Taken On : 3/10/2018 1 :45:00PM Acquisition Started : 3/14/2018 7:41:51PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 352 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.2 seconds Dead Time : 0.02 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 3/12/2018 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description : install Sample Number : 24374 Certificate Name : Eu155-Na22 Certificate Date : 12/20/2011 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 8:02:10PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2780]

3/14/2018 8:02:14PM Page 2 of6 Analysis Report for 14-Mar-18-10048 8105100A-FSFC-282CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.79 950 - 961 955.61 2.46E+Ol 17 .11 3.87E+Ol 0.69 M ; First peak in a multiplet region m ; Other peak in a multiplet region F ; Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Pb-2 12 0.9 9 115.18 0.60 238.63

43.60 l.93E-0 1 l. 37E-0 1 300.09 3.30

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold= 0.30 Errors quoted at 2.000sigma

[2781]

3/14/2018 8:02:14PM Page 3 of6 Analysis Report for 14-Mar-18-10048 B105100A-FSFC-282CV 0.0" - 0.5" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

Pb-212 0.997 l.93E-01 l.37E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2782]

3/14/2018 8:02:14PM Page 4 of6 Analysis Report for 14-Mar-18-10048 B105100A-FSFC-282CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 8:02:10PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Ubrar; Used : C:\Canberra\Apex\Roct\Default\Library\Z!ON L!B-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCilgrams) (pCilgrams) (pCl/grams)

(keV)

An Pk 511. 00 100.00 2 . 2 8E-01 2 .25E-01 2.25E-0 1 BE-7 477.60 10.44 1.43E-01 1.33E+OO 1.33E+OO K-40 1460.82 10.66 3 .16E+OO 3.94E+OO 3 .94E+OO Co-60 11 73.23 99.85 1. 2 5E-02 2 .09E-01 2 .41E-01 1332.49 99.98 5.30E-02 2 .09E-01 Nb-94 702.65 99.81 -2.21E-02 1.70E-01 1. 70E-Ol 871. 0 9 99.89 6.46E-02 1.75E- 0 1 Ag-1 08m 79 .13 6.60 -4.64E-01 1.42E-0 1 3.00E+OO 433.94 90.50 6.17E-02 1.42E-01 614. 2 8 89.80 5.llE-04 2 .07E-01 72 2 . 94 90.80 -1. 0 5E-01 1. 52E-01 Sb-1 2 5 176.31 6.84 9.89E-0 2 4.66E-01 1.31E+OO 380.45 1. 52 -1.57E+OO 7.85E+OO 427.87 2 9.60 - 2 .51E-0 1 4 . 66E-01 463.36 10.49 -4. 2 8E-0 1 1 . 13E+OO 600.60 17.65 5. 3 0E-0 1 9 . 06E-01 606.71 4.98 9.84E-01 4.02E+OO 635.95 11. 22 -1.42E-01 1.38E+OO 671.44 1. 79 4.47E+OO 7.64E+OO

[2783]

0000024374.CNF Live Time :1200.000 sec 60 Real Time :1200.240 sec start: 1: -0.2(kev) stop : 8192:2046.9(kev)

Acq. start :wed Mar 14 19:41:51 2018 55 50 45

[2784]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/14/2018 8:24:50PM Page 1 of6

~~~pex-Gamma Analysis Report for 14-Mar-18-10049 8105100A-FSFC-282CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 14-Mar-18-10049 Sample Description : 8105100A-FSFC-282CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.167E+02 grams Facility : Default Sample Taken On : 3/10/2018 1:45:00PM Acquisition Started : 3/14/2018 8:04:33PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 352 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.2 seconds Dead Time : 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 3/12/2018 Efficiency Calibration Used Done On : 3/14/2018 Efficiency Calibration Description : install Sample Number : 24377 Certificate Name : Eu155-Na22 Certificate Date : 12/20/2011 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/14/2018 8:24:46PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2785]

3/14/2018 8:24:50PM Page 2 of6 Analysis Report for 14-Mar-18-10049 B 105100A-FSFC-282CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.78 951 - 961 955.58 2 .38E+Ol 15.80 3 .23E+Ol 0.34 2 352.04 1404 - 1413 1 408.14 1. 51E+Ol 9.85 7.82E+OO 0.79 3 609.11 2431 - 2441 2 435.69 1 .95E+Ol 11. 47 1.lOE+Ol 0.76 4 661.33 2639 - 264 9 2 644.50 l.42E+O l 9.24 5.53E+OO 0.70 5 1460.28 5835 - 5848 5841.50 2 .85E+Ol 12.35 7.00E+OO 0.73 M ;;; First peak in a multiplet region m ;;; Other peak in a multiplet region F ;;; Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.95 1460.82

10.66 3.34E+OO 1. 48E+OO Cs-137 0.98 661. 66

85.10 1.20E-01 7.94E-02 Bi-211 0.86 351.07

13. 02 5. 2 1E-Ol 3.51E-01 Pb-212 0.99 115 .18 0.60 2 38.63

43.60 1.86E-0 1 1 .27E-01 300.09 3.30 Bi-214 0.99 609. 32

45.49 2 .90E-01 1. 74E-01 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120. 2 9 14.92 11 55. 2 1 1. 63 1 2 38.12 5.83 1 2 80.98 1. 43

[2786]

3/14/2018 8:24:50PM Page 3 of6 Analysis Report for 14-Mar-18-10049 B 1051 OOA-FS FC-282CV 0.0" - 0.5" 0.5" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi-2 14 0.99 1377. 67 3 .99 1385. 31 0.79 1401. 52 1. 33 1407.99 2 .39 1509. 2 1 2 .13 1661. 2 7 1. 05 1729.59 2 .88 1764.49 15.30 1 847.43 2 .03 2118.51 1.16 Pb- 2 14 0.99 241.99 7. 2 5 2 95. 22 18.42 3 51. 93

35.60 l .91E-0 1 l.28E-01 785. 96 1. 06

"' Energy line found in the spectrum.

- "' Manually added nuclide.

? "' Manually edited nuclide.

@ "' Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.955 3 .34E+OO l . 48E+OO Cs-137 0.983 1. 20E-01 7.94E-02

? Bi-211 0.861 5.21E - 01 3 .51E-01 Pb-212 0 . 997 l.86E - 01 l.27E-01 Bi-214 0.997 2 .90E-01 1 .74E-01

? Pb-214 0.999 1 .91E-01 l.28E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2787]

3/14/2018 8:24:SOPM Page 4 of6 Analysis Report for 14-Mar-18-10049 B105100A-FSFC-282CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/14/2018 8:24:46PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCUgrams) (pCl!grams)

(keV)

An Pk 511. 00 100.00 3 .00E-01 2 .38E-01 2 .38E-0 1 BE-7 477.60 10.44 5.03E-01 1. 33E+OO 1.33E+OO

+ K-40 1460.8 2

10.66 3 .34E+OO 1 . 57E+OO 1.57E+OO Co-60 1173.23 99.85 -6.86E-02 1 .70E-01 2.21E-01 1 332.49 99.98 -9.56E-02 1.70E-01 Nb-94 702.65 99.81 2.81E-02 9.71E - 02 1.61E-01 871. 09 99.89 -8.03E-0 2 9. 71E-02 Ag- 1 08m 79.13 6 . 60 3.77E-01 1. 51E-Ol 2.81E+00 433.94 90.50 2.71E-02 1.51E-01 614.28 89.80 -2 .66E-02 2.37E-01 722. 94 90.8 0 -3. 90E-03 1.75E-01 Sb-125 176.31 6 . 84 9.57E-02 4.66E - 01 1.31E+OO 380.45 1. 52 3.79E+OO 6.15E+00 427.87 2 9.60 -9.31E-0 2 4.66E-01 463.36 10.49 6.45E-01 1 .56E+OO 600.60 17.65 2 .86E-0 1 7.68E-01 606.71 4.98 5. 1 7E+OO 4.41E+OO 635.95 11 . 22 -7.81E-02 1.13E+OO 671.44 1. 79 1.73E+OO 7.34E+OO

[2788]

3/14/2018 8:24:SOPM Page 5 of6 Analysis Report for 14-Mar-18-10049 81051 OOA-FSFC-282CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCi/grams)

(keV)

Ba-133 79.61 ~ .65 -3.62E-01 2 . 2 9E-0 1 6.74E+OO

81. 00 32.9 0 -5."03E-01 4.59E-01 276.40 7.16 -1.32E-02 1. 45E+OO 302.85 18.34 1.44E-01 6.33E-01 356.01 62.05 5.78E-03 2.29E-01 383.85 8.94 -1.40E+OO 1. OlE+OO Cs-134 475.36 1. 48 4.43E+OO 1. 40E-01 8.68E+OO 563.25 8.34 - 2 .52E-01 1. 50E+OO 569.33 15.37 2 . llE-02 9.78E-01 604. 72 97.6 2 -2 .03E-01 2 . llE-01 795.86 85.46 5.75E-02 1.40E-01 801. 95 8.69 - 1.37E+OO 1.63E+OO 1 038.61 0.99 6.94E+OO 1. 54E+Ol 1167. 97 1. 79 7.71E+OO 1. 20E+Ol 1365 . 19 3.02 -3 . 60E-01 5.75E+OO

+ Cs-137 66 1 .66

85.10 1.20E-01 1. OlE-0 1 1. OlE-01 Eu-152 121.78 28.67 5.09E-02 3.38E- 0 1 3.38E-01 244.70 7.6 1 1. 72E-01 1. 44E+OO 295.94 0.4 5 2.79E+O l 2 .98E+Ol 344.2 8 26.60 3.23E-02 4.39E-01 367.79 0.86 -4. 1 8E+OO 1.31E+Ol 411.12 2.24 3.91E+OO 6.19E+OO 443.96 2.83 2.32E+OO 4.81E+OO 488.68 0.42 1.66E+Ol 3.26E+Ol 563.99 0.49 2.46E+OO 2.63E+Ol 586. 2 6 0.46 1.86E+Ol 4.05E+Ol 678.62 0.47 -3.80E+OO 2 .80E+Ol 688.67 0.86 1.12E+Ol 1. 74E+Ol 719.35 0. 2 8 -5.66E+Ol 5.51E+01 778.90 12 . 96 1. 45E-01 1. 02E+OO 810.45 0.32 -8.95E+OO 5.19E+Ol 867.37 4.26 -6.60E-0 1 2 .76E+OO 919.33 0.43 1.1 9E+O l 4.39E+Ol 964.08 14.65 4 . 0 5E-01 1.32E+OO 1085.87 10. 2 4 -7.03E-03 1.53E+OO 1089.7 4 1. 7 3 5.84E+OO 1. 05E+Ol 1112. 07 13.69 -8.29E-01 1.29E+OO 1212.95 1. 43 l.69E+OO 1.31E+01 1249.94 0.19 -l.50E+Ol l .01E+02 1 2 99.14 1. 63 4.90E+00 1.09E+Ol 1408.01 21.07 9.93E-0 2 1. 04E+OO 1 457.64 0.50 5.89E+Ol 8.05E+Ol 1528.10 0. 2 8 2 .76E+Ol 6.73E+Ol Eu-154 123.07 40.40 1 .92E-02 2 . 25E-01 2 .25E-01 247.93 6.89 -l.02E+OO l.44E+OO 591.76 4.95 -1. 02E+OO 2 .42E+OO 692.42 1. 78 -1.33E-01 7.85E+OO 7 23.30 2 0.06 1.91E-03 8.18E-01 756.80 4.52 -1.19E+OO 3.15E+OO 873.18 12.08 7.49E-02 l .05E+00 996. 2 9 10.48 -4.85E-0 1 1. 33E+OO

[2789]

3/14/2018 8:24:50PM Page 6 of6 Analysis Report for 14-Mar-18-10049 B 1051 OOA-FSFC-282CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi!grams) (pCi!grams)

(keV)

Eu-154 1004.76 18.01 1.60E-01 2 .25E-01 5.95E-01 1274.43 34.80 2 . 2 6E-01 5.03E-01 1596. 48 1. 80 3 .00E+OO 9. 3 4E+00 Eu-155 45.30 1. 31 1. 72E+00 5.37E-01 3. 2 6E+Ol

60. 01 1. 22 -1 . 06E+Ol 2 .93E+Ol 86.55 3 0.70 2.64E- 01 5 . 37E-01 105.31 2 1.10 2 .90E-01 5.58E-01 Ra-226 186.2 1 3 .64 '5 . 8 6E-01 2 .89E+OO 2.89E+OO Pa-23 1 27.36 10. 3 0 4.62E+OO 4.65E+OO 4.65E+OO 2 83.69 1. 70 -4.22E+00 6.09E+00 300.07 2 .47 -5.12E+OO 4.81E+OO 302.65 2 .20 7.39E-01 5.19E+OO 330. 0 6 1. 40 4.91E+OO 8.81E+OO U- 235 143.76 10. 96 -5.76E-01 1.89E- 01 8.88E-01 163. 3 3 5.08 - 1.lOE+OO 1. 59E+OO 185.71 57.20 l.77E-01 1.89E-01 2 02 .11 1. 08 4.48E+OO 9.05E+OO 205.31 5.01 9.42E-02 2 .02E+OO Am-241 59.54 35.90 -4.59E-01 1. OlE+OO 1 .0lE+OO

+ ;:;; Nuclide identified during the nuclide identification

;:;; Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTiON: MDA vaiue is inconsistent with Currie MDA at 95% confidence ievei

[2790]

~ - - - - - - - - - - - - - - - - -0000024377.CNF Live Tire :1200.000 sec 60 Real Tire :1200.240 sec start: 1: -0.2(kev)

Stop : 8192: 2046. 9(kev)

Acq. Start :wed Mar 14 20: 04: 33 2018 55 50 45

[2791]

C>

1000 2000 3000 4000 5000 6000 7000 8000 Channel

~

ROI Type: 1

3/13/2018 9:41 :06PM Pagel of6

~pex-Gamma Analysis Report for 13-Mar-18-10022 B105100A-FSFC-289CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10022 Sample Description : B105100A-FSFC-289CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.190E+02 grams Facility : Default Sample Taken On : 3/9/2018 1:30:00PM Acquisition Started : 3/13/2018 9:20:58PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.02 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24311 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 9:41:01PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2792]

3/13/2018 9:41:06PM Page 2 of6 Analysis Report for 13-Mar-18-10022 B105100A-FSFC-289CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.47 949 - 958 953.46 2 .08E+Ol 13. 33 2 .05E+Ol 0.54 2 609.27 2430 - 2 440 2435.10 1 .83E+Ol 11. 70 1.34E+Ol 1.12 3 661.35 2636 - 2 652 2643.3 1 9.31E+Ol 20.47 7.74E+OO 1. 60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) .(pCi/grams) Uncertainty Cs-137 0.98 661.66

85.10 7.61E-01 1.91E-01 Pb-212 0.99 115 .18 0.60 2 38.63

43.60 1.52E-01 1. OlE-01 300.09 3 .30 Bi-214 1. 00 609. 32

45. 49 2 .63E-01 1. 71E-01 768.36 4.89 806.18 1. 2 6 934.06 3 .11 1120. 2 9 1 4.9 2 1155. 21 1. 63 1238.12 5.33 1280.98 1. 43 1377.67 3.99 1385. 31 0 .79 1401.52 1. 33 1407.99 2 .39

[2793]

3/13/2018 9:41 :06PM Page 3 of6 Analysis Report for 13-Mar-18-10022 8105100A-FSFC-289CV 0.0" - 0.5" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi-2 1 4 1. 00 1509. 2 1 2 .13 1661.27 1. 05 1729.59 2 .88 1764.49 15.30 1847.43 2 .03 2 118.51 1. 16

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

Cs-137 0.985 7.61E-01 1.91E-01 Pb-21 2 0.996 1.52E-01 1.0lE-01 Bi-214 1. 000 2.63E-01 1.71E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2794]

3/13/2018 9:41 :06PM Page 4 of6 Analysis Report for 13-Mar-18-10022 B105100A-FSFC-289CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 9:41:01PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (ke V) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCi!grams) (pCl/grams)

(keV)

An Pk 511. 00 100.00 1.42E-01 l.98E-01 l.98E-01 BE-7 477.60 10.44 -1.0lE+OO 1.28E+OO l.28E+00 K-40 1460.82 10.66 2 .23E+OO 3.17E+OO 3. 17E+OO Co-6 0 1173.23 99 . 85 2 .09E-01 2.38E-01 2 .54E-01 13 32 .49 99.98 l.60E-01 2 . 3 8E-01 Nb-94 ; 02.65 99.8 1 2 .36E-02 1. 40E-0 1 1.47E-01 871.09 99.89 1 . 83E-02 l.40E-01 Ag-108m 79.13 6.60 1.35E+OO 1. 44E-01 2 .43E+OO 433.94 90.50 -1.49E-02 1 .44E-01 614. 2 3 89.80 -4.68E-02 1. 82E-01 722 . 94 90.80 5 .50E-0 2 2 .07E-01 Sb-125 176.3 1 6.84 -3 .54E-0 1 4.76E-01 9.73E-01 380.45 1. 52 4.65E+OO 9.0 l E+OO 427.87 2 9.6 0 l.77E-01 4.76E-01 463.36 10.49 3. 1 6E-Ol 1 .09E+OO 600.60 17.65 1.38E-01 7.41E-01 606.71 4.98 3.70E+OO 4.lOE+OO 635.95 11. 22 -3.70E-01 1. 22E+00 671.44 1. 79 l.41E+OO 7.67E+OO

[2795]

3/13/2018 9:41:06PM Page 5 of6 Analysis Report for 13-Mar-18-10022 8105100A-FSFC-289CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCi/grams)

(keV)

Ba-133 79.61 2 .65 4.22E+00 2. 1 4E-01 5.90E+O O

81. 0 0 32 .90 -3.44E-01 3.29E-O l 276.4 0 7.16 -8.98E-01 1. 43E+OO 302.85 18. 3 4 3.47E-02 5.78E-O l 356. 0 1 62.05 -2 .89E-Ol 2.14E-01 383.85 8.94 -2 .09E-01 1.42E+OO Cs-134 4 75.36 1. 48 - 2 .63E+OO 1 .92E-01 9.31E+OO 563.25 8.34 -5.77E-0 1 l.63E+OO 569.33 15.37 9.75E-02 8.94E-01 604. 72 97. 62 -8.61E-0 2 1 .92E-01 795.86 85.46 3 .07E-02 2 . 2 2E-01 8 01 .95 8.69 1.05E+OO 2 .04E+OO 1038.61 0.99 5.84E+OO l.42E+Ol 11 67.97 1. 79 3.80E+00 l.32E+Ol 1 365.19 3 . 02 1.94E+00 5.27E+OO

+ Cs-137 661. 66

85.10 7.61E-01 1.18E-01 l.18E-01 Eu-152 12 1 .78 2 8.67 -6.53E-02 2 .86E-01 2 . 86E-01 244.70 7.6 1 8.92E-01 l.39E+OO 295.94 0.4 5 2 .80E+OO 2 .81E+Ol 344.28 2 6.60 -l.47E-02 3.29E-01 367.79 0.86 l.18E+OO 1.56E+01 411.12 2 .24 2 .78E+OO 5.48E+00 443. 96 2 .83 -4. 07E-01 4.77E+00 488.68 0.42 -8.05E+OO 2.56E+Ol 563.99 0. 49 -9 . 92E+00 2.69E+Ol 586.26 0.46 3.64E+OO 2 . 96!!:+0l 678.62 0.47 l.36E+Ol 3 .03E+Ol 688.67 0.86 - 8.76E+OO 1. 44E+Ol 719. 35 0. 2 8 l.lGE+Ol 7.12E+Ol 778.90 12.96 9. 3 6E-0 2 8.22E-0 1 810.45 0. 32 -l.62E+Ol 4.13E+Ol 867.37 4 .26 4.53E-01 3.27E+OO 919.33 0.43 2 .27E+Ol 3.88E+Ol 964.08 14.65 2 .36E-01 l.48E+00 1085.87 10. 2 4 -5.55E-01 l .41E+OO 1089.74 1. 73 3.44E+OO 8.38E+OO 1112. 07 13.69 2 .75E-01 1. 2 1E+OO 1212.95 1. 43 3.57E+OO 1.41E+Ol 1249.94 0.19 4.61E+Ol 9.48E+Ol 1299.14 1. 63 2 .80E+OO l. 1 3E+Ol 1408.01 2 1.07 -l.75E-01 6.35E-01 1 457.64 0.50 6.37E+Ol 6.70E+01 1 528.10 0.28 l .37E+Ol 5.09E+Ol Eu- 154 123.07 40.40 -3.28E-02 2.08E-0 1 2 .08E-01 247.93 6.89 -3.20E-01 1.19E+OO 591.76 4.95 -5.29E-02 2.43E+OO 692. 42 1. 78 2 . 88E+OO 7.89E+OO 723.30 20. 0 6 2.59E-01 9.39E-01 756.8 0 4.52 1.70E+OO 3.06E+OO 873. 1 8 1 2.08 5.63E-01 l.16E+OO 996. 2 9 10.48 4.08E-01 l.61E+OO

[2796]

3/13/2018 9:41:06PM Page 6 of6 Analysis Report for 13-Mar-18-10022 B 1051 OOA-FSFC-289CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCilgrams) (pCi/grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 6.52E-03 2 .08E-0 1 8.57E-01 1 2 :4.43 34.80 - 2 .06E-01 3 . 96E-01 1 596.48 1. 80 - 4.82E+00 5.69E+OO Eu-155 45.30 1. 3 1 8.75E+OO 4.0lE-0 1 2 .32E+Ol 60.01 1. 22 - 2 .22E+Ol 2 .26E+Ol 86.55 30.70 2 .52E-01 4.47E-01 105.31 2 1.10 -8.19E-02 4.0lE-01 Ra-226 186. 2 1 3.64 -3.66E-01 2 .45E+OO 2 .45E+OO Pa-23 1 27.36 10. 3 0 1.09E+OO 2 .94E+OO 2 .94E+OO 283.69 1. 70 -2 .19E+OO 5 .84E+OO 300.07 2 .47 -4.79E+OO 3 .89E+OO 302.65 2 . 20 -1. 76E+OO 4.57E+OO 330.06 1. 40 -1.22E+OO 6.75E+OO U-235 143.76 10. 96 2.0lE-01 l.58E-01 7.59E-01 163. 33 5.08 -6.76E-01 1.41E+OO 185.71 57.20 -1 . 76E-02 l.58E-01 202 .11 1. 08 - 2 .64E+OO 7.50E+OO 205.31 5.01 6.49E-01 1.61E+OO Am-24 1 59.54 35.90 -3 .69E-01 8.43E-01 8.43E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2797]

0000024311.CNF Live Time :1200.000 sec Real Tille :1200.270 sec 60 start: 1: -0.0(kev) stop : 8192: 2047 .B(kev)

Acq . start :Tue Mar 13 21:20:58 2018 55 50 45 40

[2798]

V1 u

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/13/2018 10:02:49PM Page I of6

~~~pex-Gamma Analysis Report for 13-Mar-18-10023 B105100A-FSFC-289CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANAL YS/S Sample Identification : 13-Mar-18-10023 Sample Description : B105100A-FSFC-289CV 0.0" - 0.5" 0.5" Sample Typ~ : Puck Unit Sample Point Sample Size 1.190E+02 grams Facility : Default Sample Taken On : 3/9/2018 1:30:00PM Acquisition Started : 3/13/2018 9:42:42PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds ReaiTime : 1200.3 seconds Dead Time : 0.03%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120- 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24313 Certificate Name : Eu 155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 10:02:45PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2799]

3/13/2018 10:02:49PM Page 2 of6 Analysis Report for 13-Mar-18-10023 B 1051 OOA-FSFC-289CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.85 950 - 959 954.98 3.50E+Ol 17.74 3.81E+Ol 0.80 2 352.4 2 1402 - 1414 1408. 7 1 2 .58E+Ol 15. 12 2 .25E+Ol 0 . 57 3 661. 51 2636 - 2 650 2 643.95 5.12E+Ol 15.01 3 .62E+OO 1. 25 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Cs-137 0 . 99 661.66

85.10 4.18E-01 1. 33E-01 Pb - 2 1 2 0 .99 115 .18 0 .60 2 38.63

43.60 2 .56E-01 1 .36E-01 3 00.09 3.30 Pb-2 14 0 .97 2 41.99 7.25 2 95. 22 18.42 351.93

35.60 3. 09E-0 1 1.88E-01 785. 96 1. 06

[2800]

3/13/2018 10:02:49PM Page 3 of6 Analysis Report for 13-Mar-18-10023 B105100A-FSFC-289CV 0.0" - 0.5" 0.5"

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

Cs-137 0.997 4. 1 8E-01 1.33E-01 Pb-21 2 0.993 2 .56E-01 1.36E-01 Pb-214 0.978 3 . 0 9E-01 1.88E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2801]

3/13/2018 10:02:49PM Page 4 of6 Analysis Report for 13-Mar-18-10023 B105100A-FSFC-289CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 10:02:45PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCilgrams) (pCi/grams) (pCilgrams)

(keV)

An Pk 511. 00 1 00.00 1. 55E-01 2 .26E-01 2 .26E-01 BE-7 477.60 10.44 -1.59E+OO 1 . 18E+OO 1.18E+OO K-40 1460.82 10.66 3 .47E+OO 3.38E+OO 3.38E+OO Co-60 1173. 23 99.85 1.40E-01 2.54E-01 2. 54E-01 1332.49 99.98 2.74E-01 3.0lE-01 Nb-94 702.65 99.81 5.82E-02 1. 2 0E-01 1. 2 0E-01 871.09 99.89 7.64E-0 2 1. 4 7E-01 Ag-1 08m 79 .13 6.60 2 .40E-01 1. 32E - 01 2 .66E+OO 433.94 90.50 -6.44E-03 1.32E-01 614.28 89.80 -2 .45E-01 1.66E-01 722. 94 90.80 1. 04E-01 1. 90E-01 Sb-125 176.31 6.84 -2 .18E-01 4.76E-01 1. 2 2E+OO 380.45 1. 52 3.38E-01 6.62E+OO 427.87 2 9.60 1. 59E-01 4.76E-01 463.36 1 0.49 -2 .71E-01 9.13E-01 600 . 60 17.65 3.2 1E-01 7.65E-01 606. 71 4.98 3.5 4E+OO 3.65E+OO 635.95 11. 22 2 .83E-01 1.18E+OO 671.44 1. 79 2 .46E+00 8.68E+OO

[2802]

3/13/2018 10:02:49PM Page 5 of6 Analysis Report for 13-Mar-18-10023 81051 OOA-FSFC-289CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCl/grams) (pC/lgrams) (pCi/grams)

(keV)

Ba-1 33 .,9.61 2 .65 4.02E-01 2 .20E- 01 6.42E+OO 81.00 32 .9 0 -7.06E-01 3 .95E-01 2 7 6.40 7.16 2 .18E-02 1. lOE+OO 302.85 18.34 -1.69E-01 6 . 42E-01 356. 0 1 62.05 6.06E-02 2. 20E-01 383.85 8.94 4.91E-01 1.30E+OO Cs-1 3 4 475.36 1. 48 l.84E+OO 1.76E-01 8.73E+OO 563.25 8.34 -4.82E-01 1. 44E+OO 569.33 15.37 - 4 .13E-02 8.17E-01 604. 72 97. 62 - 1.73E-02 l.76E-01 795.86 85.46 8.24E-02 1.94E-01 801.95 8.69 -8.7 1 E-Ol l.73E+OO 1 038.6 1 0.99 -2 .52E+OO 1 .83E+Ol 1167. 97 1. 79 '2 .69E+OO 1. 38E+01 1365.19 3.0 2 3.lOE+OO 6.37E+OO

+ Cs- 137 661.66

85.10 4.18E-01 8 . 65E-02 8.65E-02 Eu- 15 2 121.78 2 8.67 6.66E-02 3.lOE-01 3 .lOE-01 2 44.70 7.61 -l.89E-01 1. 2 8E+OO 2 95.94 0.45 l.62E+OO 2 . 72E+Ol 344. 2 8 2 6.60 l.61E-01 4.0lE-01 367.79 0 . 86 -1.89E-01 1.22E+Ol 411.12 2 .24 2.29E+OO 4.63E+OO 443. 96 2 .83 2.81E+OO 4.86E+00 488.68 0.42 -1.17E+OO 3.0SE+Ol 563.99 0.49 9.92E+OO 2 .53E+Ol 586. 26 0.46 9.66E+00 3.64E+Ol 678. 62 0.47 -1 . 81E+Ol 2.93E+Ol 688.67 0.86 -l . 91E+Ol l.57E+Ol 71 9.35 0.28 -l.72E+01 5.52E+Ol 77 8.90 12. 96 -2.85E-01 9.40E-01 810.45 0.32 -3.14E+OO 4.33E+Ol 867.37 4.26 -8.44E-01 2 .91E+OO 919. 33 0.43 - l.44E+OO 2 .81E+Ol 964. 08 14.65 9.73E-03 1. 3 7E+OO 1085.87 10.24 6.76E-01 1.50E+OO 1089.74 1. 73 - 6.32E+OO 8.92E+OO 111 2 . 07 13. 69 l.22E-01 1.21E+OO 1212.95 1. 43 -1.02E+00 1.16E+Ol 1249.94 0.19 -2.77E+O l 9.48E+Ol 1299.14 1. 63 8.40E-0 1 1.13E+Ol 1408.01 2 1.07 -3.83E-01 8.30E-01 1 457.64 0 . 50 6. 2 8E+Ol 7.04E+Ol 1 528.10 0. 2 8 1. 3 7E+Ol 5.09E+Ol Eu-154 123.07 40.40 -5.71E-02 2 .lOE-01 2 .lOE-01 247.93 6.89 3.79E-01 1. 30E+OO 591.76 4.95 6.46E-0 2 2 .43E+OO 692.4 2 1. 78 -6.85E-01 8.17E+OO 723 .3 0 2 0.06 4.63E-01 8.60E-01 756.8 0 4.52 l. l 9E+00 2 .64E+OO 873. 1 8 12 .08 - l.55E-01 1. 2 7E+OO 996. 2 9 10 .4 8 1.07E+OO 1.74E+00

[2803]

3/13/2018 10:02:49PM Page 6 of6 Analysis Report for 13-Mar-18-10023 B1051 OOA-FSFC-289CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCi/grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 -1. l 7E-01 2 .lOE-01 8.57E-01 1274.43 34.80 1.59E-01 4.32E-01 1596.48 1. 80 4.45E+OO 1.09E+Ol Eu-155 45.30 1. 31 5.03E+OO 4.19E-01 2.42E+Ol 60.01 1. 22 6.88E+OO 2 .51E+Ol 86.55 30.70 2 .49E-01 4.23E-01 105. 3 1 2 1.10 6.79E-02 4.19E-01 Ra-226 186.21 3.64 1.38E+OO 2.64E+OO 2 .64E+OO Pa-231 27.36 10.30 6.19E-01 2 .81E+OO 2 .81E+OO 283.69 1. 70 3 . 3 7E-02 5.08E+OO 300.07 2 .47 - 4.0lE+OO 4.54E+OO 302.65 2 . 20 4.64E-01 5.48E+OO 330.06 1. 40 -1.47E+OO 7.37E+OO U-235 143.76 10. 96 -1.0lE-01 1. 71E-01 6. 71E-01 163.33 5.08 4.97E-01 1.38E+OO 185.71 57.20 1.54E-01 1.71E-01 20 2 .11 1. 08 4.64E-01 8.07E+OO 205. 3 1 5.01 -1.85E-01 1.55E+OO Am-241 59.54 35.90 5.47E-01 9.03E-01 9.03E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? *~ CAUTION: MD/\ value is inconsistent with Currie MDA 8t 95% confidence level

[2804]

0000024313.CNF Live Time :1200.000 sec Real Time :1200.310 sec 60 start: 1: -0.0(kev) stop : 8192: 2047. 8(kev)

Acq. start :Tue Mar 13 21:42:42 2018 55 50 45 40 35

[2805]

25 1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/12/2018 6:44:24PM Page l of6 Analysis Report for 12-Mar-18-10003 B105100A-FSFC-293CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Mar-18-10003 Sample Description : B105100A-FSFC-293CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.325E+02 grams Facility : Default Sample Taken On : 2/7/2018 1:45:00PM Acquisition Started : 3/12/2018 6:24:15PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Livenme : 1200.0 seconds Real Time : 1201 .9 seconds Dead Time : 0.16 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/12/2018 Efficiency Calibration Description Sample Number : 24240 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/12/2018 6:44:20PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2806]

3/12/201 R 6:44:24PM Page 2 of6 Analysis Report for 12-Mar-18-10003 B1051 OOA-FS FC-293CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 661. 79 1317 - 1328 1323 .11 4.07E+03 128.56 5.12E+Ol 1. 46 2 14 61. 03 2917 - 2927 2922.12 4.40E+Ol 13 .27 O.OOE+OO 0. 71 M a: First peak in a multiplet region m a: Other peak in a multiplet region Fa: Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460.82

10.66 4.05E+OO 1.27E+OO Cs-137 0.99 661.66

85.10 2.70E+Ol 3.36E+OO

a: Energy line found in the spectrum.

- a: Manually added nuclide.

? a: Manually edited nuclide.

@ a: Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold a: 0.30 Errors quoted at 2.000sigma

[2807]

3/12/2018 6:44:24PM Page 3 of6 Analysis Report for 12-Mar-18-10003 B105100A-FSFC-293CV 0.0" - 0.5" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.993 4.0SE+OO 1. 27E+OO Cs-137 0.997 2.70E+Ol 3.36E+OO

? = nuclide [s part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2808]

3/12/2018 6:44:24PM Page 4 of6 Analysis Report for 12-Mar-18-10003 B105100A-FSFC-293CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/12/2018 6:44:20PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCi/grams)

(keV)

An Pk 511. 00 100 . 00 2 .27E-01 4.82E-01 4.82E-01 BE-7 477.60 10 . 44 -5.32E+OO 4.34E+OO 4. 3 4E+00

+ K-40 1460.82

10.66 4.05E+00 2. G5E-01 2 .65E-01 Co-60 1173 .23 99.85 5.02E-0 2 1 . 76E-01 1. 76E-01 1332.49 99.98 7.66E-02 l.97E-01 Nb-94 702.65 99.81 2 .64E-02 l.23E - 01 1.30E-01 871. 09 99.89 1.37E-03 1.23E-01 Ag-108m 79 .13 6.60 1.71E+OO 1.38E-01 3.97E+OO 433.94 90.50 -3.38E-02 3.43E-01 614. 2 8 89.80 -1.48E-01 2 .35E-01 722. 94 90.80 -4.16E-02 1.38E-01 Sb-1 2 5 176.31 6.84 -3 .lBE-01 1. llE+OO 2.71E+OO 380.45 1. 52 -1.31E+Ol 1.73E+Ol 4'.27. 87 2 9.60 5.58E-0 2 l.llE+OO 463.36 10.49 8.56E-01 3 .44E+OO 600.60 17.65 -3 .66E-01 1 .23E+O O 606.71 4.98 -2 .75E+00 4.36E+OO 635.95 11. 22 -2 .18E+OO 1.74E+OO 671.44 1. 79 -5.47E-01 8.lOE+OO

[2809]

3/12/2018 6:44:24PM Page 5 of6 Analysis Report for 12-Mar-18-10003 B1051 OOA-FS FC-293CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCilgrams)

(keV)

Ba-133 79.61 2 . 65 2.44E+OO 2 .92E-01 9.62E+OO

81. 00 32.9 0 -5.70E-01 6.64E-01 276.40 7.16 -9.62E-01 2 .89E+OO 302.85 1 8.34 5.58E-01 1. 22E+OO 356. 01 62.05 -2 .97E-01 3 .92E-01 383.85 8.94 -8.44E-01 2 .93E+OO Cs - 134 475.36 1. 48 1 .06E+Ol 1.45E-0 1 2 . 2 7E+Ol 563.25 8.34 -9.58E-01 2 .47E+OO 569.33 15.37 3.23E-0 2 1.41E+OO 604. 72 97.6 2 2.37E-0 2 2 .34E-01 795.86 85.46 -4.48E-0 2 1. 45E-01 801.95 8.69 - 1 . 50E-01 1.44E+OO 1 038.61 0 .99 5.78E+OO 1. 44E+Ol 1167. 97 1. 79 2 .48E+OO 1.05E+Ol 1365. 1 9 3.0 2 1. 58E+OO 4.31E+OO

+ Cs-137 661.66

85.10 2 .70E+Ol 2 .00E-01 2 .00E-01 Eu-152 121. 7 8 28.67 2 .24E-01 5.44E-01 5.44E-01 244. 7 0 7.61 5.72E-01 2 .81E+00 295.94 0.45 -1.37E+O l 4.75E+Ol 344. 2 8 2 6.60 1. 2 7E-01 9 .94E-01 367.79 0.86 7.98E+OO 3.19E+Ol 41 1.12 2.24 -1. 2 6E+OO 1.35E+Ol 443. 96 2.83 1.31E+OO 1.18E+Ol 488.68 0.42 -3.86E+Ol 6.99E+Ol 563.99 0.49 -6.66E-01 4.15E+Ol 586. 2 6 0.46 2.15E+Ol 4.92E+Ol 678.62 0.47 1.94E+Ol 3. 2 8E+Ol 688.67 0.86 -2.47E-01 1. 2 8E+Ol 71 9.35 0.28 -2.69E+OO 4.34E+Ol 778.90 12. 96 -2.03E-0 1 9.55E-01 810.45 0.3 2 1. 7 4E+Ol 4. 2 3E+Ol 867.37 4.26 -3.77E-01 2 .90E+OO 919.33 0.43 3.41E+00 3 .0lE+Ol 964. 0 8 14.65 -5.02E-01 9 .43E-01 10 85.87 10. 24 3.88E-0 2 1. 51E+OO 10 89.74 1. 73 2 .92E+OO 8.98E+OO 1112. 07 13.69 3.89E-01 1. llE+OO 1212.95 1. 43 -2.70E+OO 9.34E+OO 1249.94 0.19 6.35E+OO 5.76E+Ol 1299.14 1. 63 -1.46E+00 8.59E+OO 14 0 8.01 21. 0 7 5.90E-01 9.15E-01 1457.64 0.50 -l.94E+Ol 7.00E+Ol 1528.10 0. 2 8 2 .18E+Ol 5.31E+Ol Eu-154 123.07 40 . 40 1.33E-02 3 . 73E-01 3 . 73E-01 247.93 6.89 -2 .98E-01 2. 96E+OO 591.76 4.95 2 .31E+00 4.47E+OO 692.42 1. 78 -4.58E-01 6.20E+OO 723. 30 2 0.06 1. 85E-01 7.00E-01 756.80 4. 52 1.42E+OO 3 .13E+OO 873. 1 8 12.08 -2 .79E-01 8.88E-01 996. 2 9 10. 4 8 -1.51E-01 1. 30E+OO

[2810]

3/12/2018 6:44:24PM Page 6 of6 Analysis Report for 12-Mar-18-10003 B105100A-FSFC-293CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCUgrams) (pCUgrams) (pCi!grams)

(keV)

Eu-154 1004.76 18.01 1. 21E-01 3 .73E-01 7.90E-01 1274.43 34.80 -6.74E-02 3.97E-01 1596.48 1. 80 2 .68E+OO 9.21E+00 Eu-155 45.30 1. 31 -l.52E+Ol 6.SlE-01 3 .91E+Ol 60.01 1. 22 -l.61E+Ol 4. 21E+Ol 86.55 30.70 3 .16E-0 2 6.51E-01 105.31 2 1.10 4.47E-0 2 7.75E-01 Ra-226 186.21 3 .64 1.0lE+OO 5.66E+OO 5.66E+00 Pa-231 27.36 10. 3 0 4.31E+OO 4.27E+OO 4.27E+OO 283.69 1. 70 -3 .25E-01 1.25E+01 300.07 2. 47 -1.75E+OO 8.51E+00 302.65 2.2 0 4.62E+OO 1. OlE+Ol 330.06 1. 40 -4.50E+OO 1.76E+Ol U-235 143.76 10.96 -5.83E-02 3.61E-01 1. 40E+OO 163.33 5.08 -8.68E-01 3 .47E+OO 185.71 57. 2 0 1. 53E-01 3. 61E-01 202.11 1. 08 -4.04E+OO 1 . 90E+Ol 205.31 5.01 -2 .20E+OO 4 . 00E+OO Am-241 59.54 35.90 -2 .39E-01 l.51E+OO 1 . 51E+00

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUT!ON: MDA vaiue is inconsistent with Currie MDA at 95% confidence !evel

[2811]

0000024240.CNF 2000 Live Tfae :1200.000 sec Rea1 Ti11e :1201.890 sec start: 1: O.l(kev) stop : 4096: 2047. l(kev)

Acq. start :MOn Mar 12 18:24:15 2018 1750 1500 1250 VI

§ 0

1000 u

[2812]

750 500 250 500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/12/2018 7:07:43PM Page I of6

~~~pex Gamma Analysis Report for 12-Mar-18-10004 B105100A-FSFC-293CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Mar-18-10004 Sample Description : B105100A-FSFC-293CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.325E+02 grams Facility : Default Sample Taken On : 2/7/2018 1:45:00PM Acquisition Started : 3/12/2018 6:47:34PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.7 seconds Dead Time : 0.14 %

Peak Locate Threshold : *3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/12/2018 Efficiency Calibration Description Sample Number : 24242 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/12/2018 7:07:38PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2813]

3/12/2018 7:07:43PM Page 2 of6 Analysis Report for 12-Mar-18-10004 B105100A-FSFC-293CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.56 474 - 481 477.31 3 .70E+Ol 34.90 2.64E+02 0.69 2 661. 7 9 1317 - 1328 1323.12 3 . ~3E+0 3 114. 94 5.77E +Ol 1. 55 3 14 fil. 4 5 2 917 - 2928 2 922.95 4.44E+O l 13. 95 3.20E+00 2 .20 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0 .94 1460.82

10.66 4.09E+OO 1. 33E+OO Cs-137 0 .99 661.66

85.10 2 .15E+Ol 2 .69E+OO Pb-212 0 .99 115 .18 0.60 238.63

43.60 2 .26E-01 2 . 16E-01 300.09 3.30

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2814]

3/12/2018 7:07:43PM Page 3 of6 Analysis Report for 12-Mar-18-10004 8105100A-FSFC-293CV 0.0" - 0.5 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.940 4.09E+OO l . 33E+OO Cs-137 0.997 2 .15E+Ol 2 .69E+OO Pb-212 0.999 2 .26E-01 2 .16E-Ol

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2815]

3/12/2018 7:07:43PM Page 4 of6 Analysis Report for 12-Mar-18-10004 B105100A-FSFC-293CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/12/2018 7:07:38PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCl/grams) (pCilgrams)

(keV)

An Pk 511. 00 1 00.00 4. 2 8E-01 4.95E-01 4 . 95E-01 BE-7 477.60 10.44 3 .59E+OO 4 . 74E+OO 4.74E+OO

+ K-40 1 460.82

10.6 6 4.09E+OO 9.06E-01 9.06E-01 Co-60 1173.23 99.8 5 l.35E-0 1 l .86E-01 1.86E-01 1332.49 99.98 8.99E-02 1.86E-01 Nb-94 702.65 99.81 3 .24E-02 1.40E-01 1.40E-01 871. 0 9 99.89 7.31E-02 1 . 47E-01 Ag-108m 79 .13 6.60 -7.69E-O l 1 .71E-01 3 .45E+OO 433 . 94 90.50 -2 .12E-01 3 . 2 4E-0 1 614 . 28 89.80 -1 . 30E-01 2 .48E-01 722 . 94 90.80 -1.34E-02 1 .71E-01 Sb-1 2 5 176. 3 1 6.84 -1.16E-01 1.02E+00 2 .73E+OO 380.45 1. 52 -1.16E+00 1. 72E+Ol 427 . 87 2 9.60 4.14E-01 1. 02E+OO 463.36 10.49 -2 .84E+OO 3 .00E+OO 60 0 .60 17.65 1 . 41E-02 1 .31E+OO 606.71 4.98 3. 20E+OO 5.lOE+OO 635.95 11. 22 -2. 35E-01 1.92E+OO 671. 44 1. 79 -2 .0lE+OO 6.99E+OO

[2816]

3/12/2018 7:07:43PM Page 5 of6 Analysis Report for 12-Mar-18-10004 81051 OOA-FSFC-293CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCilgrams) (pCi/grams)

(keV)

Ba-133 79.61 2 .65 -1.70E+OO 4.05E-01 8.47E+OO

81. 00 32 .90 -3.39E-01 6.23E-01 276.40 7.16 9. 96E-01 2 . 96E+OO 302.85 18.34 3.27E-01 1.24E+OO 356.0 1 62.05 -1.43E-01 4.05E-01 383.85 8.94 7.16E-01 3 .05E+OO Cs-134 475.36 1. 48 3.69E+OO L 71E-0 1 2 . 2 7E+Ol 563.25 8.34 4. 3 9E-01 2 .79E+OO 569.33 15.37 4. 71E-01 1.49E+OO 604. 72 97.6 2 3 .68E-02 2.56E-01 795.86 85.46 6.69E-02 1. 71E-01 801.95 8.69 -1 .71E-01 1.49E+OO 1038.61 0.99 1.90E+OO 1.32E+Ol 1167.97 1. 79 .-3 . 94E+OO 8.25E+OO 1365.19 3 . 02 6 . 73E-01 3.95E+OO

+ Cs- 137 661.66

85.10 2. 15E+Ol 2 . llE-01 2 .llE-01 Eu-1 52 1 2 1. 78 28.67 -1.27E-01 5.30E-01 5.30E-01 2 44.70 7.61 -2 .13E+OO 2 .67E+00 2 95.94 0.45 -2 .13E+Ol 4.55E+Ol 344.28 2 6.60 -6 .63E-01 8 .58E-01 367.79 0.86 8.12E+OO 2 .90E+Ol 411.12 2 .24 -2 .17E+OO 1 .23E+Ol 443.96 2.83 -1.22E+OO 1.12E+Ol 488.68 0.42 1.63E+Ol 6.85E+Ol 563 . 99 0.49 1. 22E+O O 4.51E+Ol 586. 2 6 0.46 6.95E-02 4.70E+Ol 678. 62 0.47 -1.18E+Ol 2 .62E+Ol 688.67 0.86 3.lOE+OO 1. 61E+Ol 719.35 0. 28 1 .75E+Ol 5.24E+Ol 778.90 12.96 -4.04E-01 9.88E-01 810.45 0.32 -1.48E+00 3 .82E+Ol 867.37 4. 2 6 -1.50E+OO 2 .64E+OO 919.33 0.43 1.05E+Ol '.2 .88E+Ol 964. 08 14.65 -1 . 87E-01 1.22E+OO 1085.87 10.24 9.51E-01 1.80E+OO 1089.74 1. 73 -5.53E+OO 8.65E+OO 1112. 07 13. 69 -3.00E-01 1. 02E+OO 1 2 12 . 95 1. 43 -4.92E+OO 8.78E+OO 1249.94 0.19 9.00E+OO 1.10E+02 1299.14 1. 63 1.60E+OO 7.51E+OO 1408.01 2 1. 07 3.24E-02 7.06E-0 1 1 457.64 0.50 -2 .45E+Ol 7 .13E+Ol 1528. 1 0 0.28 2 .95E+OO 4.52E+Ol Eu-154 123.07 40.40 -1.36E-01 3 .69E-01 3.69E-01 247.93 6 . 89 1. 44E+OO 3.17E+OO 591.76 4.95 -1.48E+OO 4.14E+00 692.42 1. 78 -1.32E+OO 7.08E+OO 723.30 2 0.06 -1.47E-Ol 7.65E-01 756.80 4. 52 -1.27E+OO 2 .59E+OO 873.18 12 .08 1.lSE-01 1.19E+OO 996. 2 9 10.48 9.19E-0 2 1.24E+OO

[2817]

3/12/2018 7:07:43PM Page 6 of6 Analysis Report for 12-Mar-18-10004 B 1051 OOA-FSFC-293CV 0.0" - 0.5 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCUgrams) (pCi/grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 1.68E-0 2 3.69E-01 7.59E-01 -

1274.4 3 3 4.80 1.87E-01 4.79E-01 1596.48 1. 80 -6 .80E+00 4.54E+OO Eu-155 45.30 1. 31 -2 .65E+Ol 6.64E-01 3.87E+Ol 60.01 1. 22 -l .45E+Ol 4.07E+Ol 86.55 30.70 3 . 3 3E-01 6.64E-01 105.31 2 1.10 -2 .92E-01 7.45E-01 Ra-226 186.21 3 .64 3.67E+OO 5.58E+OO 5.58E+00 Pa-231 27.36 10.30 3.64E+OO 4.lOE+OO 4.lOE+OO 283.69 1. 70 3.54E+00 1.21E+Ol 300.07 2 .47 1.55E+00 8.93E+OO 302.65 2 .20 2 .71E+00 1. 03E+Ol 330.06 1. 40 1.37E+OO 1. 71E+Ol U- 2 35 143.76 10.96 -2 . 2 1E-01 3.52E-01 1.31E+OO 163.33 5.08 -4.50E-01 3.57E+OO 185.71 57. 2 0 1.87E-01 3.52E-01 202 .11 1. 08 -9.42E+OO 1. 80E+Ol 205.31 5.01 -1 . 36E+OO 3.83E+OO Am-241 59.54 35.90 2 .13E-01 1.45E+OO 1.45E+00

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

= Half-life too short to be able to perform the decay correction t = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2818]

u 0000024242.CNF 1000 Live Tire :1200.000 sec Real Tire :1201.660 sec Start: 1: O.l(kev) stop : 4096 :2047 .l(kev)

Acq. start :Mon Mar 12 18:47:34 2018 900 800 700 600 V'I

§0 500 u

[2819]

400 300 200 100 .....

a,

.**"'l,J,..i_),,, ._,*r/ca '*/ *

...,.........i............--i.........a...--+---L-....i---.1..-+-..J.......6....J.--L--U...-4-.......1.--.J...--1..---1..-'--1---J-L...._,L__.L...,..j...........1 o_L.J_L__J____i_---l...--4----L--l.____J____JJ...._+---,a::i.::....::!=~.........

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/19/2018 5:46:41PM Page I of6

~~~pex-Gamma Analysis Report for 19-Mar-18-10016 B105100A-FIFC-300CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 19-Mar-18-10016 Sample Description : B105100A-FIFC-300CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 8.562E+01 grams Facility : Default Sample Taken On : 2/13/2018 12:50:00PM Acquisition Started : 3/19/2018 5:26:19PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 352 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.2 seconds Dead Time : 0.02 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120-8192 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 3/12/2018 Efficiency Calibration Used Done On : 3/19i2018 Efficiency Calibration Description : install Sample Number : 24571 Certificate Name : Eu155-Na22 Certificate Date : 12/20/2011 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on 3/19/2018 5:46:37PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2820]

3/19/2018 5:46:41PM Page 2 of6 Analysis Report for 19-Mar-18-10016 B105100A-FIFC-300CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 661.77 2640 - 2654 2646.26 3.57E+01 14.26 1.07E+Ol 0.83 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Cs-137 0.99 661.66

85.10 4. llE-01 1. 72E-01

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2821]

3/19/2018 5:46:41PM Page3 of6 Analysis Report for 19-Mar-18-10016 B105100A-FIFC-300CV 0.0" - 0.5" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

Cs-137 0.998 4. llE-01 1. 72E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2822]

3/19/2018 5:46:41 PM Page4 of6 Analysis Report for 19-Mar-18-10016 B105100A-FIFC-300CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/19/2018 5:46:37PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCilgrams) (pCi!grams)

(keV)

An Pk 511.00 1 00.00 3.53E-01 5.02E-01 5.02E-01 BE-7 477.60 10.44 1. 35E+OO 2 .61E+OO 2 .61E+OO K-40 1460.82 10.66 2.60E+OO 4.21E+00 4.21E+OO Co-60 11 73.23 99.85 6.08E-02 1 .79E-01 2. 64E-01 1332.49 99.98 -2 .93E-01 1. 7 9E-01 Nb-94 702.65 99.8 1 7.92E-0 2 1.61E-01 2 .43E-01 871. 0 9 99.89 -8.39E-02 1. 61E-01 Ag-108m 79. 1 3 6.60 -2 .45E+00 1.88E-01 3.79E+OO 433.94 90.50 3.24E-02 1.89E-01 614.28 89.80 1.22E-01 2 .68E-0 1 722. 94 90.80 9.17E-02 1. 88E-01 Sb-125 176.31 6.84 -2 .18E-01 5.98E-01 1 .59E+OO 380.45 1. 52 -9 . llE+OO 1.18E+Ol 4 2 7.87 2 9.60 1.37E-01 5 . 98E-01 463.36 10.49 - 1 . l OE-01 1.71E+OO 600.60 17.65 7.42E-01 1. lOE+OO 606.71 4.98 -9.27E-01 4.80E+OO 635.95 11. 22 -2 .79E+00 1.57E+OO 671. 44 1. 79 -8 .13E-01 1.25E+Ol

[2823]

3/19/2018 5:46:41PM Page 5 of6 Analysis Report for 19-Mar-18-10016 B105100A-FIFC-300CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi!grams) (pCUgrams) (pCi!grams)

(keV)

Ba-133 79.61 2 .65 2 .16E+00 3 .13E-01 9.65E+OO

81. 00 3 2 .90 -1.16E+OO 6.09E-01 2 76.40 7.16 4.00E-01 1. 91E+OO 3 02.85 18.34 -3 .60E-01 8.26E-01 356.01 62 .05 - 3. 1 7E-02 3 .13E-01 383.85 8.94 5.53E-01 2 .02E+OO Cs- 134 475.36 1. 48 2 .43E-01 2 . 31E-0 1 1.18E+Ol 563.25 8.34 6.20E-01 2 .38E+OO 569.33 15.37 3.98E-01 1. 34E+00 604. 72 97.62 -2 .47E-01 2 .31E-01 795.86 85.46 1.64E-01 3 . llE-01 801. 95 8.69 -8.09E-01 3 .00E+OO 1038.61 0.99 5.56E+OO 1 . .73E+.01 1167.97 1. 79 -3 .94E+OO 1. 43E+Ol 1365.19 3 .02 1 . lOE+OO 5.32E+OO

+ Cs-13 7 661 . 66

85. 1 0 4. llE-01 1.85E-01 1. 85E-01 Eu-1 52 121. 78 2 8.67 -1.31E-01 4.00E- 01 4.00E-0 1 244.70 7.6 1 6. 2 4E-01 1. 90E+OO 295.94 0.45 7. 2 9E+OO 3 .64E+Ol 344.28 26.6 0 -1.23E-01 5.90E-01 367.79 0.86 4.00E+OO 1. 80E+01 4 11 .12 2 .24 -1.24E+OO 7.70E+OO 443.96 2 .83 2 .73E+OO 6. 96E+00 488.68 0.42 1.64E+Ol 4.46E+0 1 563.99 0.49 - 9.60E+OO 3.94E+Ol 586.26 0.46 3.34E+Ol 5.17E+Ol 678.62 0.47 -1.70E+Ol 3 .66E+Ol 688.67 0.86 8.83E-01 2 . 2 9E+Ol 719.35 0. 2 8 2.99E+Ol 6.14E+Ol 778.90 1 2 . 96 2 .23E-01 1.40E+00 810.45 0 .3 2 2 .18E+Ol 6.61E+O l 867.37 4.26 3.94E-01 4.06E+OO 919.33 0.43 -2.23E+Ol 3 .92E+Ol 964. 0 8 14.65 4.96E-01 1.87E+OO 1 085.87 10.24 5.39E-01 1.68E+OO 1 0 89.74 1. 73 2 .40E+OO 8.94E+00 11 12. 07 1 3.69 -7.61E-01 1. 68E+OO 1212.95 1. 43 6. 2 5E+OO 1. 52E+Ol 1249.94 0.19 -1. 2 0E+0 2 1. 25E+0 2 1299.14 1. 63 -1.04E+OO 1. 07E+Ol 1408.01 21.07 4.73E-0 1 1.15E+OO 1457.64 0.50 4.59E+Ol 8.96E+Ol 1528.10 0. 2 8 1.89E+Ol 7.04E+01 Eu-154 123.07 40.40 7.67E-02 2 .92E-01 2 .92E-01 247.93 6.89 6.59E-Ol l.91E+OO 591.76 4.95 6.57E-03 2 . 86E+OO 692.42 1. 78 2. 1 5E+OO 1. 23E+Ol 723. 3 0 2 0.06 1.06E-01 8.13E-01 756 . 80 4.52 1. 34E+OO 4.49E+00 873.18 12.08 -7.40E-0 2 1.54E+00 996. 2 9 10.48 1.05E+OO 2 .60E+OO

[2824]

3/19/2018 5:46:41PM Page 6 of6 Analysis Report for 19-Mar-18-10016 B1051 OOA-FIFC-300CV 0.0" - 0.5" o.o*

Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.0 1 4.09E-01 2 .92E-01 1. 42E+OO 1274.43 3 4.80 2 .66E-01 6.48E-01 1596.48 1. 80 -7. 71E+OO 1.15E+Ol Eu-155 45.30 1. 31 1.04E+OO 6.32E-01 4.24E+Ol 60.01 1. 22 -2 . 2 7E+Ol 4.25E+Ol 86.55 30.70 9.30E-02 6.32E-01 105.31 21.10 6.77E-02 6.37E-01 Ra-2 2 6 186. 2 1 3.64 1.69E+00 4.09E+OO 4.09E+00 Pa-231 27.36 10.30 1. 70E+00 4.99E+OO 4.99E+OO 283.69 1. 70 -2 .82E+00 8.15E+OO 300.07 2 .47 -1.78E+OO 5.95E+OO 302.65 2 . 20 -4.lOE+OO 6. 72E+OO 330.06 1. 40 -3 .98E+OO 1. 04E+01 U-235 143.76 10.96 -3 .0lE-01 2 .67E-01 1.16E+OO 163.33 5.08 -2 .21E-01 2 .55E+OO 185.71 57.20 1.78E-01 2 .67E-01 2 02 .11 1. 08 -1.56E+OO 1.08E+Ol 2 05. 3 1 5.01 1.93E-01 2 .58E+00 Arn-241 59.54 35.90 -7.18E-01 1. 52E+OO 1.52E+00

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-iife too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2825]

0000024571.CNF Live Tille :1200.000 sec Real Time :1200. 230 sec 60 start: 1: -0 .2(kev)

Stop : 8192:2046.9(kev)

Acq. start :Mon Mar 19 17: 26: 19 2018 55 50 45 35

[2826]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/19/2018 7:32:42PM Page 1 of6

~pex-Gamma Analysis Report for 19-Mar-18-10017 B105100A-FIFC-300CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 19-Mar-18-10017 Sample Description : B105100A-FIFC-300CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 8.562E+01 grams Facility : Default Sample Taken On : 2/13/2018 12:50:00PM Acquisition Started : 3/19/2018 7:12:35PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 352 Geometry : Puck_half_inch Live Time : 1200.0 seconds Rea!Time : 1200.2 seconds Dead Time : 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 3/12/2018 Efficiency Calibration Used Done On : 3/19/2018 Efficiency Calibration Description : install Sample Number : 24573 Certificate Name : Eu155-Na22 Certificate Date : 12/20/2011 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/19/2018 7:32:38PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2827]

3/19/2018 7:32:42PM Page 2 of6 Analysis Report for 19-Mar-18-10017 8105100A-FIFC-300CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 202.51 807 - 814 810.68 7.00E+OO 8.73 1. 20E+Ol 0.54 2 661.69 2637 - 2654 2645.94 4.77E+Ol 14.87 4.53E+OO 0. 71 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams) Uncertainty Cs-137 1. 00 661. 66

85.10 5.50E-01 1. 84E-01

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2828]

3/19/2018 7:32:42PM Page 3 of6 Analysis Report for 19-Mar-18-10017 B105100A-FIFC-300CV 0.0" - 0.5" 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

Cs-137 1. 000 5.SOE-01 1.84E-01

? a: nuclide is part of an undetermined solution X a: nuclide rejected by the interference analysis

@ a: nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2829]

3/19/2018 7:32:42PM Page4 of6 Analysis Report for 19-Mar-18-10017 B105100A-FIFC-300CV 0.0" - 0.5" 0.5

UNIDENTIFIED PEAKS Peak Locate Performed on : 3/19/2018 7:32:38PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide 1 202.51 5.83333E-03 ~ Tol.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCUgrams) (pCilgrams)

(keV)

An Pk 511. 00 100.00 3.54E-01 4. l OE-01 4.lOE-01 BE-7 477.60 10.44 1.40E+OO 2 .61E+OO 2 .61E+OO K-40 1460.82 10.66 4 . 63E+OO 4.59E+OO 4.59E+OO Co-60 1173.23 99.85 3 .42E-02 2 .53E-01 2 .53E-01 1332.49 99.98 2 .99E-02 2 .63E-01 Nb-94 702.65 99.81 -3 .32E-02 l .68E-01 1.68E-01 871. 0 9 99.89 -5.03E-0 2 1.94E-01 Ag-108m 79.13 6.60 2 .85E-02 1. 75E - 01 4. 2 0E+OO 433.94 90.50 6.08E-02 1.75E-01 614.28 89.80 1.0lE-01 2 .57E-01 722. 94 90.80 -5 .70E-02 2 .07E-01 Sb-125 176.3 1 6.84 1. 4 6E-0 1 5.12E-0 1 1. 85E+OO 380.45 1. 52 -8. 2 3E-01 8.56E+OO 427.87 29 .60 9.83E-02 5.12E-01 463.36 10.49 - l.98E-01 l.67E+OO 600.60 17.65 -3. 41E-01 1. 2 9E+00 606.7 1 4.98 -1.48E+OO 4.70E+OO 635.95 11. 22 -3.91E-02 1. 5 7E+OO

[2830]

3/19/2018 7:32:42PM Page 5 of6 Analysis Report for 19-Mar-18-10017 8105100A-FIFC-300CV o.o* - o.5" 0.5" Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCl/grams) (pCi/grams)

(keV)

Sb-125 671. 44 1. 79 9.89E-01 5.12E-01 1.14E+Ol Ba-133 79.61 2 . 65 2.95E+OO 2 .88E-01 l.OlE+Ol

81. 00 32 .90 -8.0lE-02 7.48E-01 2 76 . 40 7.16 -6.52E-01 l.98E+OO 302.85 18.34 2 .52E-01 6.66E-01 356.01 62.05 l.54E-01 2 .88E-01 383.85 8.94 l.44E-01 1. 44E+OO Cs-134 475.36 1. 48 -4.19E+00 2.2 1E-01 1.15E+Ol 563.25 8.34 -1.15E+OO 2 . 3 1E+00 569.33 15.37 -3.83E-01 1.23E+OO 604.72 97.62 -2.13E-01 2 .25E-01 795.86 85.46 -5.03E-02 2 . 21E-01 801.95 8.69 -8.84E-02 2 . 2 9E+OO 1038.61 0.99 - 1.86E+Ol 2 .03E+Ol 1167.97 1. 79 3 .23E-01 1. 43E+Ol 1365.19 3.0 2 4.95E+OO 9 .50E+OO

+ Cs-137 661. 66

85.10 5.50E-01 1.40E-01 1.40E-01 Eu-152 12 1.78 28.67 3. 40E-01 4.41E-01 4. 41E-01 2 44.70 7.61 -5.51E-02 l.82E+OO 2 95.94 0.45 -2 .54E+O l 2 .89E+Ol 344.28 2 6.60 -l.65E-01 5 .42E-01 367.79 0.86 1. 74E+OO l.98E+O l 411.12 2 .24 -4.82E+OO 7.37E+OO 443.96 2 .83 -l.82E+OO 6.17E+OO 488.68 0.42 1. 83E+Ol 4.56E+Ol 563.99 0.49 2 .05E+01 4.04E+Ol 586.26 0.4 6 1.89E+Ol 4.44E+Ol 678.62 0.47 4.92E+OO 4.42E+Ol 688.67 0.86 -1.47E+OO 2 .12E+Ol 719.35 0.28 5.37E+OO 6.14E+Ol 778.90 12. 96 - l.15E+OO l.53E+OO 810.45 0.32 1.14E+Ol 6.35E+Ol 867.37 4.26 2 .22E+OO 4.57E+OO 919.33 0.43 -4.41E+Ol 3 .59E+Ol 964.08 14.65 -8.63E-01 1. 35E+OO 1085.87 10.24 -3 .03E-01 1. 83E+OO 1089.74 1. 73 7.19E+OO l. 3 8E+Ol 111 2 . 07 1 3 .69 9. 2 1E-01 1.77E+OO 1212.95 1. 4 3 1.98E+OO 1. 88E+Ol 1249.94 0.19 1. 75E+Ol l.32E+0 2 1 299.14 1. 63 9.58E+OO 1. 73E+Ol 1 408.01 21. 07 -3.94E-01 6.04E-01 1457.64 0.50 9.51E+Ol 9.60E+01 1528.10 0 .2 8 -4.41E+Ol 7.04E+Ol Eu-154 123.07 40.40 8.77E-02 3.12E-01 3.12E-01 2 47.93 6.89 3.08E-01 1.84E+OO 591.76 4.95 2 .18E+OO 4.06E+OO 692.42 1. 78 -1.32E+OO 1. 03E+01 723.30 2 0.06 2 . 2 6E-01 1 .02E+OO 756.80 4.52 2.25E+OO 5.13E+OO 873.18 12.08 -2 .94E+OO 1. 54E+OO

[2831]

3/19/2018 7:32:42PM Page 6 of6 Analysis Report for 19-Mar-18-10017 8105100A-FIFC-300CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCl/grams) (pCi/grams) (pCi/grams)

(keV)

Eu-154 996.29 10.48 -l.77E-01 3 .12E-01 2 .51E+OO 1004.76 18.01 1.38E-01 1.26E+OO 1274.4 3 34.80 8.85E-02 4.28E-01 1596.48 1. 80 -3.60E+OO 1. 50E+Ol Eu-155 45.30 1. 31 -1.27E+Ol 6.32E-01 3 .54E+O l 60.01 1. 22 -1.70E+Ol 4.04E+Ol 86.55 30.70 -3.64E-01 6.32E-01 105.31 21.10 3.26E-01 6.84E-01 Ra- 2 26 186.21 3.64 3.97E+OO 4.51E+OO 4.51E+OO Pa-231 2 7.36 10. 3 0 3.60E+OO 5.02E+00 5. 2 4E+OO 283.69 1. 70 -7.73E-0 2 8.45E+OO 300.07 2 .47 -2 .18E+OO 5.02E+OO 302.65 2 . 20 2 .06E+OO 5.67E+OO 330.06 1. 40 -4.82E+OO 1. 02E+Ol U-235 143.76 10.96 3.53E-01 2 .76E- 01 1. 30E+OO 163.33 5.08 l.18E-01 2 . 2 3E+OO 185.71 5 7.20 1.16E-01 2 .76E-01 202 .11 1. 08 5.75E+OO l. 2 6E+Ol 205.31 5.01 1. 1 6E+OO 2 . 71E+OO Am-241 59.54 35.90 3 .35E-01 1. 3 8E+OO 1. 38E+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA vaiue not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2832]

0000024573.CNF Live Time :1200.000 sec Real Time :1200 .230 sec 60 Start: 1: -0 .2(keV)

Stop : 8192: 2046. 9(kev)

Acq. Start :Mon Nar 19 19:12:35 2018 55 50 45 40 35

[2833]

1000 2000 3000 4000 5000 6000 7000 8000 Channel

~

ROI Type: 1

3/13/2018 10:26:33PM Pagel of6

~~~pex-Gamma Analysis Report for 13-Mar-18-10024 B105100A-FSFC-316CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10024 Sample Description : B105100A-FSFC-316CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.081E+02 grams Facility : Default Sample Taken On : 3/9/2018 8:57:00AM Acquisition Started : 3/13/2018 10:06:25PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Rear Time : 1201.5 seconds Dead Time : 0.13 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24314 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 10:26:29PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2834]

3/13/2018 10:26:33PM Page 2 of6 Analysis Report for 13-Mar-18-10024 B105100A-FSFC-316CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 2 38.57 475 - 480 477. 32 2 .87E+Ol 20.40 8.46E+Ol 0. 60 2 2 95.17 588 - 595 590.40 2 .70E+Ol 18.79 6.00E+Ol 0.97 3 351.99 699 - 703 703.92 4. 2 9E+O l 21. 05 6.0lE+Ol 1. 42 4 609. 5 9 1213 - 1224 1218.75 2 . 72E+O l 19.34 5.16E+Ol 1. 06 5 661.77 1319 - 1328 1323. 07 5.19E+Ol 17 . 80 2 .43E+Ol 1. 52 6 1461.31 2917 - 2928 2922.69 3.70E+Ol 12. 17 O.OOE+OO 1. 70 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0. 96 1460.82

10.66 4 . 18E+OO l.42E+OO Cs-137 0.99 661.66

85.10 4.22E-01 l.53E-Ol Pb-212 0.99 115.18 0.60 238.63

43.60 2 . 1 5E-01 l. 5 7E-01

'.:500. 09 3.30 Bi-214 0.99 609. 32

45.49 3 .90E-01 2.81E-01 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120.29 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43

[2835]

3/13/2018 10:26:33PM Page 3 of6 Analysis Report for 13-Mar-18-10024 B 1051 OOA-FSFC-316CV 0.0" - 0.5" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-2 14 0.99 1377. 67 3.99 1385.31 0.79 1401. 52 1. 3 3 1407.99 2 .39 1509. 2 1 2 .13 1661. 2 7 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2 .03 2118.51 1.16 Pb-214 1. 00 2 41. 99 7. 2 5 2 95. 22 18.42 5.53E-01 3 .95E - 01 351.93

35.60 5.22E-01 2 .69E- 01 785. 96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0. 962 4.18E+OO 1. 42E+OO Cs-137 0.998 4.22E-01 l.53E-01 X Bi-211 0.874 Pb-212 0.999 .2.15E-01 1.57E-01 Bi-214 0.995 3.90E-01 2 .81E-01 Pb-214 1.000 5.32E-01 2 .22E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2836]

3/13/2018 10:26:33PM Page 4 of6 Analysis Report for 13-Mar-18-10024 B105100A-FSFC-316CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 10:26:29PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCi/grams) (pCUgrams) (pCUgrams)

(keV)

An Pk 511. 00 100.00 2. 80E-01 2.75E-01 2 .75E-01 BE-7 477.60 10.44 8.65E-01 l.75E+OO l.75E+OO

+ K-40 1460.82

10.66 4.18E+OO 3.25E-01 3.25E-Ol Co-6 0 1173.23 99.85 l.03E-01 2.06E-01 2.06E-0 1 133 2 .49 99.98 l.32E-0 1 2.39E-0 1 Nb-94 702.65 99.81 2 .29E-02 l . 46E-01 l.46E-01 871.09 99.89 2 .97E-02 l.57E-Ol Ag - 1 08m 79.13 6.60 l.83E+OO l.66E-01 3.27E+OO 433.94 90.50 -2 .66E-02 l.66E-01 614.28 89.80 4.48E-0 2 2 .51E-01 722 . 94 90.80 -2 .43E-0 2 l.97E-01 Sb-1 2 5 176.31 6.84 -4.46E-01 4.88E - 01 l.95E+OO 380.45 1. 52 l .87E+OO 9.50E+OO 427.87 2 9 .60 -4.82E-02 4.88E-01 463. 3 6 1 0.49 2 .55E-01 l.59E+OO 600.60 17.65 -l. 2 5E-01 l. 02E+OO 606.71 4.98 - 8.59E-01 5.52E+OO 635.95 1 1. 22 4.95E-0 1 l.62E+OO 671.44 1. 79 -6.lOE+OO 8.87E+OO

[2837]

3/13/2018 10:26:33PM Page 5 of6 Analysis Report for 13-Mar-18-10024 B105100A-FSFC-316CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity .Nuclide MDA LineMDA Name (pCi!grams) (pCilgrams) (pCi/grams)

(keV)

Ba-133 79.61 2.65 l. 7 9E+OO 3.15E-01 7.70E+OO

81. 00 32.90 -5.0lE-01 5.12E-01 2 76.40 7.16 4.65E-01 1.80E+OO 3 02.85 18.34 6.44E-02 7.73E-01 356.01 62.05 -1.34E-01 3.15E-01 383.85 8.94 -1.65E-01 1.58E+OO Cs-134 475 . 36 1. 48 - 2 .63E+OO 1.67E-01 1. OlE+Ol 563.25 8.34 -3 .17E-01 1.68E+OO 569.33 15.37 4.57E-01 9.64E-01 604.72 97.6 2 -6.23E-02 2.50E-01 795.86 85.46 - 3 .93E-02 1.67E-01 801.95 8.69 -3 .97E-01 1.50E+OO 1038.61 0.99 -7.12E+OO 1.72E+O l 1167. 97 1. 79 -8.73E+OO 1.03E+Ol 1365.19 3.0 2 3.47E-01 4.23E+OO

+ Cs - 137 661.66

85.10 4.22E - 01 1 .o8E-01 1.68E-Ol Eu-15 2 121. 7 8 2 8 . 67 1.60E-01 4.44E-01 4.44E-01 244.70 7.61 6.04E-01 2 .09E+OO 295.94 0.4 5 1.90E+Ol 3.77E+Ol 344. 2 8 2 6.60 1.75E-01 6.05E-01 367.79 0.8 6 8. 2 1E+OO 1. 71E+01 411.1 2 2.24 -1.30E-01 6. 72E+OO 443.96 2 .83 -7.69E-01 5.40E+OO 488.68 0.42 8.73E-01 3.90E+Ol 563.99 0.49 -2.00E+Ol 2.62E+Ol 586.26 0.46 2 .16E+Ol 4.63E+Ol 678.62 0.47 8.92E+OO 3.47E+Ol 688.67 0.86 3. 71E-01 1.97E+Ol 719.35 0. 2 8 -3.63E+Ol 5.64E+Ol 778.90 12. 96 -2.99E-02 1. 03E+OO 810.45 0.32 6.20E-01 5.0lE+Ol 867.37 4.26 -8.15E-01 3.22E+OO 919.33 0.43 - 4.64E+Ol -l.49E+Ol 964. 08 14.65 - 6. 72E-01 1. 2 8E+OO 1 085.87 10. 2 4 -1.03E+OO 1. 85E+OO 1 089.74 1. 73 7.31E+OO 1.13E+Ol 1 112.07 13. 69 2. 81E-01 1.35E+OO 1212.95 1. 43 2 .46E+OO 1.43E+01 1249.94 0.19 4.51E+O l 9. 2 8E+Ol 1299.14 1. 63 -9.44E+00 6.51E+OO 1403.01 21. 07 -1.80E-01 6.20E-01 1457.64 0.50 -1.90E+Ol 8. llE+Ol 1528. 1 0 0. 2 8 2 .21E+Ol 6.02E+01 Eu-154 123.07 40.40 6.25E-03 3.08E- 01 3.08E-01 247.93 6.89 -l.38E-01 l.99E+OO 591.76 4.95 -8.82E-01 3.07E+OO 692.4 2 1. 78 5.81E+OO 1.00E+Ol 723. 30 2 0.06 1. 54E-01 9.32E-01 756.80 4.52 - 2. 31E-Ol 3.03E+OO 873.18 12.08 4.86E-02 1. 25E+O.O 996. 2 9 10.48 l.12E+OO 1. 88E+OO

[2838]

3/13/2018 10:26:33PM Page 6 of6 Analysis Report for 13-Mar-18-10024 B1051 OOA-FS FC-316CV 0.0" - 0.5" 0.0" Nuc/Jde Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCilgrams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 -2 .31E-01 3.08E-01 7.49E-01 1274.43 34.80 7.77E-02 4.23E-01 1596.48 1. 80 -6.66E+OO 6.96E+OO Eu-155 45. 3 0 1. 31 9.06E+00 4.46E-01 2 .74E+Ol 60.01 1. 22 1.59E+OO 3 .27E+Ol 86.55 30.70 -1.84E-01 4.46E- 01 105.31 21.10 -1.57E-01 5.87E-01 Ra-226 186. 2 1 3.64 l.77E+OO 4.19E+OO 4.19E+OO Pa-23 1 2 7.36 10.30 2 .98E+OO 3.52E+OO 3 .52E+OO 2 83.69 1. 70 2. 08E+OO 7.87E+OO 300.07 2 .47 -8.17E-01 5.74E+OO 302.65 2 . 20 5.36E-01 6.43E+OO 330.06 1. 40 9.74E-01 9.76E+OO U-23 5 143.76 10.96 -1.90E-01 2 .68E-01 1. 03E+OO 163.33 5.08 -2 .0lE-01 2 .67E+OO 185. 71 57. 2 0 1. 21E-01 2 .68E-01 2 02 .11 1. 08 6.36E-01 1.27E+Ol 205.31 5.01 -6.52E-01 2 .63E+OO Am-241 59.54 35.90 l.60E-01 1.17E+OO 1.17E+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value Is inconsistent with Currie MDA at 95% confidence level

[2839]

0000024314.CNF Live Time :1200.000 sec 60 Real Time :1201.530 sec start: 1: O.l(kev) stop : 4096: 2047. l(kev)

Acq. Start :Tue Mar 13 22:06:25 2018 55 50 45

[2840]

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/13/2018 10:48:32PM Page l of6

~pex-Gamma Analysis Report for 13-Mar-18-10025 B105100A-FSFC-316CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10025 Sample Description : B105100A-FSFC-316CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.081E+02 grams Facility : Default Sample Taken On : 3/9/2018 8:57:00AM Acquisition Started : 3/13/2018 10:28:24PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1201.5 seconds Dead Time : 0.12 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24316 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on 3/13/2018 10:48:28PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2841]

3/13/2018 10:48:32PM Page 2 of6 Analysis Report for 13-Mar-18-10025 8105100A-FSFC-316CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 661.77 1317 - 1323 1323. 08 l.51E+02 26.89 2.38E+Ol 1. 66 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCUDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Cs-13, 0.99 661.66

85.10 1.23E+OO 2.64E-01

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2842]

3/13/2018 10:48:32PM Page 3 of6 Analysis Report for 13-Mar-18-10025 B105100A-FSFC-316CV 0.0" - 0.5" 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

Cs-137 0.998 1. 23E+OO 2.64E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2843]

3/13/2018 10:48:32PM Page 4 of6 Analysis Report for 13-Mar-18-10025 B105100A-FSFC-316CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 10:48:28PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defauit\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA L/neMDA Name (pCUgrams) (pCi/grams) (pCi/grams)

(keV)

An Pk 511. 00 1 00.00 2 .71E-01 2 .58E-01 2. 58E-01 BE-7 477.60 10.44 -l.17E-01 1.56E+OO 1.56E+OO K-40 1460.8 2 10.66 5. 2 8E+OO 4.27E+OO 4.27E+00 Co-60 1173. 2 3 99.85 -4.48E-02 l,68E-01 1.6 8E- 01 1 332 .49 99.98 1.51E-01 2.53E-01 Nb-94 70 2 .65 99.8 1 2.13E-02 1 . 55E-01 1.55E-01 871.09 99.89 -2.37E-0 2 1. 63E-01 A.g-108m 79.13 6.60 2.09E+OO l.75E-01 3.2 6E+OO 433.94 90.50 1.53E-02 1 . 75E-01 614.28 89.80 5.95E-02 2. 19E-01 722 . 94 90.80 9.75E-03 1.79E-01 Sb-125 176.31 6 . 84 -4.69E- 01 5.65E-01 1. 89E+OO 380.45 1. 52 4.63E+OO 1.03E+Ol 427.87 29.60 -2 .lOE-02 5 . 65E-01 463.36 10.49 6.79E-Ol 1.57E+OO 600.60 17.65 4.59E-01 1. 1 3E+OO 606. 71 4 .98 1.67E+OO 4.68E+00 635.95 11 . 22 8.45E-Ol 1.64E+00 671.44 1. 79 8.31E-0 1 1.07E+Ol

[2844]

3/13/2018 10:48:32PM Page 5 of6 Analysis Report for 13-Mar-18-10025 B1051 OOA-FSFC-316CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCl/grams) (pCUgrams)

(keV)

Ba-1 33 79.61 2 .65 4.59E+OO 2 .93E-01 7.80E+OO

81. 00 32 .90 -l.38E-01 5.34E-01 2 76.40 7.16 3.12E-01 l.95E+OO 302.85 18.34 3.40E-01 7.93E-01 356.01 62 .05 2 . 2 9E-0 2 2 .93E-01 383.85 8.94 -1.00E+OO l.66E+OO Cs-134 475.36 1. 48 1.45E+OO 2 .15E-01 l.OlE+Ol 563.25 8.34 3 .76E-01 2 .06E+OO 569.33 15.37 l.07E+OO l. 2 5E+OO 604. 72 97.6 2 -l.41E-01 2 .16E-01 795.86 85.46 7.85E-0 2 2 .15E-0 1 801. 95 8.69 -4.90E-01 l.84E+OO 1038.61 0.99 - l.48E+OO 1.72E+Ol 1167. 97 1. 79 -4.79E+OO 1. 03E+Ol 1365.19 3.02 -9.46E-01 4. 2 3E+OO

+ Cs- 137 661.66

85.10 1. 23E+OO l .74E-01 1. 74E-01 Eu-152 121. 78 2 8.67 3.41E-02 4.15E-0 1 4.lSE-01 244.70 7.61 l. llE+OO 2 . llE+OO 2 95.94 0.45 2 .76E+Ol 3.83E+Ol 344. 2 8 2 6.60 -9.95E-02 5.89E-01 367.79 0.86 -1.67E+Ol 1. 69E+Ol 411.12 2 .24 l.04E+OO 6 . 99E+OO 44 3 . 96 2 .83 -6.69E-01 5.55E+OO 488.68 0.42 -3.96E+00 3.67E+Ol 563.99 0.49 4.66E+OO 3.55E+Ol 586.26 0.46 2.35E+01 4.37E+Ol 673.62 0.47 8.77E+OO 3.79E+01 688.67 0.86 -4.45E+OO l.83E+01 719.35 0.28 2 .76E+Ol 6.40E+Ol 778.90 12. 96 l.39E-01 1. 2 5E+OO 810.45 0.32 1.61E+Ol 5.48E+Ol 867.37 4.2 6 6.86E-01 3.95E+OO 919. 33 0.43 -9.15E+OO 3.67E+Ol 964.08 14.65 4.21E-01 1. 4 9E+OO 1085.87 10.24 -6.04E-01 l.56E+OO 1089.74 1. 73 -2.16E+OO 7.65E+OO 1112. 07 13.69 ""'.8. 84E-0 2 1. 3 5E+OO 1212.95 1. 43 1.lOE+OO 1.48E+Ol 1249.94 0. 1 9 4.65E+Ol 1.18E+02 1299.14 1. 6 3 3.88E+OO l.31E+Ol 1408.01 21.07 -3.83E-01 6.20E-01 1 457.64 0.50 l.20E+02 8.95E+Ol 1528.10 0. 28 3.63E+01 7.99E+Ol Eu-154 1 2 3.07 40.40 7.95E-0 2 3 .06E-01 3.06E-01 247.93 6.89 -l.04E+OO l.95E+OO 591.76 4.95 - 2. 89E+OO 2 .85E+OO 692.42 1. 78 -2. 65E+OO 8.63E+OO 723. 30 20.06 -3.24E-02 7.88E-Ol 756.80 4.52 -1.lOE-01 3.39E+OO 873.18 12.08 7.12E-01 1.49E+OO 996.29 10.48 - 4. 3 8E-02 1.58E+OO

[2845]

3/13/2018 10:48:32PM Page 6 of6 Analysis Report for 13-Mar-18-10025 B105100A-FSFC-316CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCUgrams) (pCilgrams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 -2 .lOE-01 3 .06E-01 9. 2 5E-01 1274.43 34.80 1 .93E-01 5.61E-01 1596.48 1. 80 -2 .34E+OO 8.06E+00 Eu-155 45.30 1. 3 1 3.46E+OO 5. 0 BE- 01 3 .04E+Ol

60. 01 1. 22 -6.42E+OO 3. 35E+Ol 86.55 30.70 9.92E-0 2 5.0BE-01 105.31 2 1.10 2 .76E-01 6.33E-01 Ra-226 186.21 3 .64 4.96E-01 4. 1 7E+O O 4.17E+OO Pa-23 1 27.36 10.30 1.82E+OO 3.36E+O O 3. 3 6E+OO 283.69 1. 70 -2 .70E+OO 8.15E+OO 300.07 2 .47 -2 . 2 2E+OO 5.63E+OO 302.65 2 . 20 2 .83E+OO 6.60E+OO 330.06 1. 40 -3 .56E+OO 1.05E+Ol U-235 14 3 .76 10. 96 7.18E-0 2 2 .o9E-01 1.0BE+OO 163.33 5.08 3. 72E-01 2 .78E+OO 185.71 57.20 6.04E-02 2 .69E-01 2 02 .11 1. 08 3.17E+00 1.32E+Ol 2 05.31 5.01 -5.63E-01 2 .84E+OO hm- 2 41 59.54 35.90 2 .67E-01 1. 2 3E+OO 1.23E+OO

+ =

=

Nuclide identified during the nuclide identification Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2846]

0000024316.CNF Live Time :1200.000 sec Real Ti me :1201. 490 sec 60 start: 1: O.l(kev)

Stop : 4096: 2047. l(kev)

Acq . start :Tue Mar 13 22:28:24 2018 55 50 45 35

[2847]

500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

3/19/2018 8:00:39PM Page I of6

~pex-Gamma Analysis Report for 19-Mar-18-10018 8105100A-FIFC-321CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANAL YSJS Sample Identification : 19-Mar-18-10018 Sample Description : 8105100A-FIFC-321CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.488E+02 grams Facility : Default Sample Taken On : 2/13/2018 2:10:00PM Acquisition Started : 3/19/2018 7:40:33PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.2 seconds Dead Time : 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120-8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/19/2018 Efficiency Calibration Description Sample Number : 24574 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/19/2018 8:00:35PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2848]

3/19/2018 8:00:39PM Page 2 of6 Analysis Report for 19-Mar-18-10018 8105100A-FIFC-321CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 1460.34 5833 - 5846

5839.29 4.82E+Ol 17.06 1.77E+Ol 0.38 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0. 96 1460.82

10.66 4.46E+OO 1.63E+OO

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2849]

3/19/2018 8:00:39PM Page 3 of6 Analysis Report for 19-Mar-18-10018 B105100A-F1FC-321CV 0.0" - 0.5" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0. 963 4.46E+OO 1.63E+OO

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2850]

3/19/2018 8:00:39PM Page 4 of6 Analysis Report for 19-Mar-18-10018 B105100A-FIFC-321CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/19/2018 8:00:35PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LlneMDA Name (pCilgrams) (pCl/grams) (pCi/grams)

(keV)

An Pk 511 . 00 100.00 1.64E-01 2 .50E-01 2 .50E-01 BE-7 477.60 10.44 -1.98E-01 1.54E+OO 1. 54E+OO

+ K-40 1460. 8 2

10.6 6 4.46E+OO 1. 82E+OO 1.82E+OO Co-60 1173. 23 99 . 85 -1.65E-0 1 1. 2 4E-01 1 .24E-01 1332.49 99.98 3.55E-02 1.67E-01 Nb-94 702.65 99.81 2 .47E-02 1 . 0 6E- 01 1 .2 1E-01 871.09 99.89 8.0lE-03 1.06E-01 Ag-108m 79 .13 6.60 5.62E-01 9.56E-02 1.94E+OO 433.94 90.50 7.94E-03 1. 2 6E-01 614.28 89.80 -1.97E-01 1.46E-01 722. 94 90.80 -3.05E-02 9.56E-02 Sb-125 176.31 6.84 -5.34E-01 3.42E-0 1 9.32E-01 380.45 1. 52 -l.90E+OO 5.83E+00 427.87 29.60 -2.55E-0 1 3.42E-01 463. 3 6 10.49 3.00E-01 9 . 12E-01 600.60 17.65 3.22E-Ol 7.30E-01 606.71 4.98 3.35E+OO 3.60E+OO 635.95 11. 22 1. llE-01 9.60E-01 671. 4 4 1. 79 l.44E+OO 6.04E+OO

[2851]

3/19/2018 8:00:39PM Page 6 of6 Analysis Report for 19-Mar-18-10018 B 1051 OOA-F IFC-321 CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCUgrams) (pCilgrams)

(keV)

Eu-154 1004.76 18.01 6.72E-01 1.46E-01 9.26E-01 1274.43 34.80 1.53E-01 3 .74E-01 1596.48 1. 80 5.38E+OO 1.03E+Ol Eu-155 45.30 1. 31 -1.45E+01 3. 15E-01 1.67E+Ol 60.01 1. 22 -2 .40E+OO 1.89E+01 86.55 30.70 -4.62E-02 3 .15E-01 105.31 21. 10 5.04E-02 3 .34E-01 Ra-226 186.21 3. 64 1.05E+OO 2 . 2 4E+OO 2 .24E+OO Pa-231 27.36 10.30 1.21E+OO 2 . 3 6E+OO 2 .36E+00 2 83.69 1. 70 1.20E+OO 5. 2 0E+OO 3 00.07 2 .47 -3 .03E+OO 3. 2 9E+OO 3 02.65 2 . 20 1. 31E+OO 3.52E+OO 330.06 1. 40 8 .13E-01 5. 78E+OO U-235 143.76 10.96 - 1.68E-01 1.42E-01 5.61E-01 163.33 5.08 - 6.77E-01 1.14E+OO 185. 71 57.20 9. 22E- 02 1.42E-01 2 02 .11 1. 08 -2 .57E+OO 6.63E+OO 2 05.31 5.01 6.19E-02 1.43E+OO Am-241 59.54 35.90 4.55E-02 6.84E-01 6.84E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life toe;> short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent *vvith Currie MDA at 95% confidence level

[2852]

0000024574.CNF Live Time 1200.000 sec Real Time 1200.190 sec 60 start : 1 -0.0(kev) stop : 8192 2047. 8(kev)

Acq. Start Mon Mar 19 19:40:33 2018 55 50 45 40 35

[2853]

....=

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/19/2018 8:23:47PM Page 1 of6 Analysis Report for 19-Mar-18-10019 B105100A-FIFC-321CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 19-Mar-18-10019 Sample Description : B105100A-FIFC-321CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.488E+02 grams Facility : Default Sample Taken On : 2/13/2018 2:10:00PM Acquisition Started : 3/19/2018 8:03:40PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.03%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120- 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/19/2018 Efficiency Calibration Description Sample Number : 24576 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/19/2018 8:23:43PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2854]

3/19/2018 8:23:47PM Page 2 of6 Analysis Report for 19-Mar-18-10019 B 105100A-FI FC-321 CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 77.29 307 - 314 309.70 l.14E+Ol 14.99 3 .51E+Ol 0.54 2 238.76 951 - 961 954.63 3.05E+Ol 17 .11 3 .51E+Ol 0 .38 3 35 1 .91 140 1 - 1412 1406.n4 3.04E+Ol 13. 00 9.23E+OO 1. 00 4 583.04 232 6 - 2335 2330.29 1.74E+Ol 10.09 7.12E+OO 0.48 5 1460.54 5833 - 5g4 7 5840.10 6.53E+Ol 17.45 7.50E+OO 1.14 M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.98 1460.8 2

10.66 6.04E+OO 1. 70E+OO Tl-208 0.99 583.19

85.00 1. 04E-01 6 .13E-02 Bi-211 0.89 351.07

13.02 7.97E-01 3. 64E-Ol Pb-21 2 0.99 115 .18 0.60 23 8.63

43.60 l .78E-0 1 1 . 04E-01 3 00.09 3.30 Pb21 2-XR 0.99 74.82 10. 2 8 77 .11

17.10 2 .35E-01 3. llE-01 87.35 3.97 89.78 1. 46 Pb- 21 4 1. 00 241.99 7. 25 295.22 18.42 351.93

35.60 2 .91E-01 1 .33E-01 785. 96 1. 06

[2855]

3/19/2018 8:23:47PM Page 3 of6 Analysis Report for 19-Mar-18-10019 B105100A-FIFC-321CV 0.0" - 0.5" 0.5" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty.

Pb~l4 -XR 0. 99 74.82 5.8 0 77 .11

9.7 0 4 .13E-01 5.49E-01 87.35 2.24 89.78 0 .82

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.987 6.04E+OO 1.70E+OO Tl-208 0.997 1 .04E-01 6 .13E-02

? Bi-211 0.894 7.97E-0 1 3 .64E-01 Pb-21 2 0.998 1.78E-0 1 1.04E-01

? Pb212-XR 0.997 2 .35E-01 3 . llE-01

? Pb-214 1. 000 2 .91E-01 1.33E-01

? Pb214-XR 0.997 4 .13E-01 5.49E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2856]

3/19/2018 8:23:47PM Page 4 of6 Analysis Report for 19-Mar-18-10019 B105100A-FIFC-321CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/19/2018 8:23:43PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCUgrams) (pCi/grams)

(keV)

An Pk 511. 00 100.00 2 .78E-01 2 .57E-01 2 .57E-01 BE-7 477.60 10.44 4.99E-0 3 1. 3 1E+00 1.31E+OO

+ K-40 1460.82

10 . 6 6 6.04E+OO 1. 3 0E+OO 1. 30E+OO Co-60 1173.23 99.8 5 3 .48E-02 1. 52E-01 1.52E-01 1332.49 99.9 8 1.02E-01 1. 73E-01 Nb-94 702.65 99.8 1 7.28E-03 1 . 09E-01 1.09E-01 8 71 . 0 9 99.89 -1.53E-02 1.12E-01 Ag- 1 0 8m 79 .13 6.60 -7.87E-02 9. 2 6E-02 1.87E+OO 433.94 90.50 -4.91E-0 2 9.26E-02 614.28 89.80 1. 0 lE-0 2 1.81E-01 722 . 94 90. 8 0 7. 0 9E-02 1.44E-01 Sb-125 176.3 1 6.8 4 - 3. 2 3E-02 3.12E-01 9.03E-01 380.45 1. 52 - 4.53E-01 6.34E+OO 4 2 7.87 29.60 2.34E-01 3 .12E-01 463.36 10.49 4. 72E-02 8 . 60E-01 6 00 .60 17 . 65 -4.48E-01 6.79E-01 606.71 4.98 2 .73E+OO 3.64E+OO 635.95 11. 22 -7.13E-01 7.67E-01 671.44 1. 79 -4. 2 4E+OO 5. 2 9E+OO

[2857]

3/19/2018 8:23:47PM Page 5 of6 Analysis Report for 19-Mar-18-10019 8105100A-FIFC-321CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCUgrams) (pCilgrams) (pCi/grams)

(keV)

Ba-1 33 79.61 2 .65 -8.87E-02 1. 68E-01 4.59E+OO

81. 00 32 .9 0 -6.66E-02 2 .99E-01 276. 40 7.16 1.42E-01 1.09E+OO 302.85 18.34 3.23E-01 4.88E-01 356. 01 62.05 -1.06E-02 1.68E-01 383.85 8.94 -1. llE-01 1.14E+OO Cs-134 475.36 1. 48 2 .19E+OO 1.12E-0 1 6.66E+OO 563.25 8.34 O.OOE+OO 1.19E+OO 569.33 1 5.37 -1.17E-0 2 6.0lE-01 604. 72 97. 62 - 1 .88E-01 1.*50E-01 7 95.86 85.46 - 1.90E-01 1.12E-01 801.95 8.69 4.04E-01 1.37E+OO 1 038.61 0.99 -4.17E+OO 1.56E+Ol 1 167.97 1. 79 -8.27E-01 8.99E+OO 1365.19 3 .0 2 1.27E+OO 3.97E+OO Cs-137 661.66 85.10 1.90E-01 1 . 88 E- 01 1.88E-01 Eu-1 52 1 2 1 .78 2 8.67 -9.60E-0 2 1 . 91E-01 1.91E-01 244.70 7.6 1 1 . 2 4E-01 1.07E+OO 295.94 0.45 5.lOE+OO 2 .18E+Ol 344.28 2 6.60 1.16E-01 3.09E-01 367.79 0.86 l. llE+OO 9.80E+OO 411.12 2.24 3 .53E+OO 4.57E+00 443. 96 2.83 3. 05E-01 3.54E+OO 488.68 0.42 1.98E-01 2 .06E+Ol 563.99 0.49 -8. 96E+OO 1.74E+Ol 586.26 0.46 l.43E+Ol 3.18E+O l 67 8. 62 0.47 -1.15E+Ol 2 . 2 7E+Ol 688.67 0.8 6 -2 . 2 6E+OO 8.35E+OO 719.35 0.28 1.91E+Ol 4.43E+Ol 778.90 12.96 -1. 2 1E-02 8.76E-01 810.45 0.3 2 -8.57E+OO 2 .95E+Ol 867.37 4.2 6 -7 . 06E-02 3 .22E+OO 919.33 0.4 3 -8.71E+OO 2 .43E+Ol 964.08 1 4.65 -1.25E-02 9.40E-01 1 0 85.87 1 0.2 4 3.67E-01 l. 40E+OO 10 89.7 4 1. 73 - 4. 2 8E+OO 6.73E+OO 111 2. 0 7 13. 69 8. 2 6E-01 1. 2 3E+OO 1212.95 1. 43 -2 .57E+OO 1.04E+Ol 1249.94 0.19 3.47E+OO 9.34E+Ol 1299.14 1. 63 -3.51E+OO 6.19E+OO 140 8. 01 21. 07 2 .74E-01 6.67E-01 1457.64 0.50 1 .42E+02 8.58E+Ol 1528.10 0. 2 8 -3 .38E+Ol 4.56E+Ol Eu-154 1 23 . 0 7 40.40 2 .27E-0~ 1. 43E-01 l.43E-01 2 47.93 6.89 -2 .00E-01 9.54E-01 591. 76 4.95 6.70E-01 2.23E+OO 692.42 1. 78 l .06E+OO 6.12E+OO 723.30 2 0.06 2 .91E-01 6.39E-01 756.80 4.52 2 .14E-01 2 .25E+OO 873.18 12.08 -5.46E-01 8.29E-01 996.29 10 .48 8.61E-01 1.40E+OO

[2858]

3/19/2018 8:23:47PM Page 6 of6 Analysis Report for 19-Mar-18-10019 B1051 OOA-FI FC-321 CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ide MDA LineMDA Name. (pCilgrams) (pCi!grams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 -4.58E-02 1.43E-01 7.89E-01 1274.43 34 .80 1.53E-01 3.74E-01 1 596.48 1. 80 -2 .39E+OO 5. 77E+OO Eu-155 45.30 1. 31 5.64E+OO 3 .08E-01 2 .19E+Ol 60.01 1. 22 -4.34E+OO 1.98E+Ol 86.55 30.70 2 . llE-02 3.08E-01 105.31 21.10 1.35E-01 3.80E-01 Ra-2 2 6 186.21 3.64 3.51E-01 2 .18E+OO 2 .18E+OO Pa-23 1 27.36 10.30 1.43E+OO 2 .53E+OO 2.53E+00 283.69 1. 70 -2 .40E+OO 3.97E+OO 300.07 2 .47 -1. 2 6E+00 3.41E+OO 302.65 2 .20 2 .02E+OO 3.98E+OO 330.06 1. 40 3 .12E+OO 6.24E+OO U-2 35 143.76 1 0.96 1.16E-01 l.41E-01 6.21E-01 163.33 5.08 5.56E-01 1.29E+OO 185.71 57. 2 0 6.37E-02 1.41E-01 2 02 .11 1. 08 -3.86E+OO 5.90E+OO 205.31 5 . 01 2 .45E-01 1.31E+OO Am-241 59.54 35. 90 -3.33E-01 6.53E-01 6.53E-0 1

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2859]

0000024576.CNF Live Time :1200.000 sec Rea1 Tille :1200 .310 sec 60 Start: 1: -0.0(kev) stop : 8192: 2047 . 8(kev)

Acq . start :Mon Mar 19 20:03:40 2018 55 50 45 40 35

[2860]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: l

3/19/2018 8:00:49PM Page 1 of6

~§~pex-Gamma Analysis Report for 19-Mar-18-10020 B105100A-FIFC-326CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 19-Mar-18-10020 Sample Description : B105100A-FIFC-326CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.344E+02 grams Facility : Default Sample Taken On : 2/14/2018 8:15:00AM Acquisition Started : 3/19/2018 7:40:39PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 352 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.2 seconds Dead Time : 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 92 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 3/12/2018 Efficiency Calibration Used Done On : 3/19/2018 Efficiency Calibration Description : install Sample Number : 24575 Certificate Name : Eu155-Na22 Certificate Date : 12/20/2011 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/19/2018 8:00:41PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2861]

3/19/2018 8:00:49PM Page 2 of6 Analysis Report for 19-Mar-18-10020 B105100A-FIFC-326CV 0.0" - 0.5" 0.0" Peak Energy . ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.71 949 - 962 955.30 2.22E+01 18.44 4.55E+Ol 0.87 2 14 61. 07 5836 - 5852 5844.64 3.99E+01 13. 65 4.24E+OO 1.23 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0 . 99 1460.82

10.66 4.06E+OO 1.43E+OO Pb- 212 0 . 99 115.18 0.60 238 . 63

43.60 1 . 51E-01 1.28E-01 300.09 3 .30

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold= 0.30 Errors quoted at 2.000sigma

[2862]

3/19/2018 8:00:49PM Page 3 of6 Analysis Report for 19-Mar-18-10020 B105100A-FIFC-326CV 0.0" - 0.5" 0.0" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.990 4.06E+00 1.43E+OO Pb-212 0.999 1.SlE-01 1.28E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2863]

3/19/2018 8:00:49PM Page 4 of6 Analysis Report for 19-Mar-18-10020 B105100A-FIFC-326CV 0.0" - 0.5 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/19/2018 8:00:41 PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

An Pk 511. 00 100.00 3.76E-01 3.12E-01 3 .12E-01 BE-7 477.60 10.44 3.51E-01 l .73E+00 l . 73E+OO

+ K-4 0 1460.82

10.66 4.06E+OO l. 19E+OO l.19E+OO Co-60 1173.23 99.85 4.67E-02 1. 27E-01 1. 27E-01 1332.49 99.98 7.63E-03 l. 2 7E-01 Nb-94 702.65 99.81 -l.57E-01 l . 2 7E-01 l. 27E-Ol 871. 09 99.89 3.43E-02 l.36E-Ol Ag-108rn 79.13 6.60 l.35E-01 1. 05E-Ol 2 .33E+OO 433.94 90.50 -2 .38E-02 l.OSE-01 614.28 89.80 l. llE-01 l.95E-01 72 2 .94 90.80 2 .74E-02 1. 52E- 01 Sb-125 176.31 6.84 -2.68E-01 2 .70E-01 l.12E+OO 380.45 1. 52 4.86E-02 7.24E+00 4.27.87 2 9.60 -4.45E-01 2 .70E-01 4 63. 3 6 10.49 7.39E-01 1.1 7E+OO 600.60 1 7.65 l.94E-01 7 . 45E-Ol 606. 71 4.98 3. llE+OO 3. 67E+OO 635.95 11. 22 -4.26E-01 9.98E-Ol 671. 44 1. 79 -1. 4 6E+OO 7.95E+OO

[2864]

3/19/2018 8:00:49PM Page 5 of6 Analysis Report for 19-Mar-18-10020 B105100A-FIFC-326CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCUgrams) (pCUgrams) (pCi/grams)

(keV)

Ba-13 3 79.61 2 .65 -1.77E+OO 2 .15E-01 5.52E+OO 81.00 32 .90 -6.02E-01 3 .69E-01 276.40 7.16 4.16E-01 1.37E+OO 302.85 18.34 1. llE-01 5.77E-01 356.01 62.05 1.16E-01 2 . 15E-01 383.85 8.94 3.72E-01 1.17E+OO Cs-134 475.36 1. 48 -1. 56E-01 1. 72E-01 7.74E+OO 563.25 8.34 6. OlE-01 1. 63E+OO 569.33 1 5.37 4.04E-01 9.34E-01 604. 72 97.6 2 -4.58E-04 1. 72E-01 795.86 85.46 6. 3 4E-02 1.78E-01 801.95 8.69 3.04E-01 1.65E+OO 10 38.61 0.99 -7.45E+OO 1.53E+0 1 11 67. 97 1. 79 -7.18E-01 8.23E+OO 1365. 1 9 3 .02 2 .80E-01 4.77E+OO Cs-137 661.66 85.10 -6.69E-0 2 1.71E-01 1 .71E-01 Eu-152 121.78 2 8.67 -8.87E-03 2 .51E-0 1 2.51E-01 2 44.70 7.61 -3.57E-01 1. 32E+OO 2 95.94 0.45 -1. 1 9E+Ol 2 .60E+D1 344.28 26.60 -6.61E-02 3.45E-01 367.79 0.86 7. 72E+00 1. 31E+Ol 411.12 2 . 24 -1. 4 7E+00 4.36E+OO 44 3 .96 2 .83 4.47E-01 4.19E+OO 488.68 0.42 - 1.46E+OO 2.91E+Ol 563.99 0.49 -1.71E+OO 2.71E+Ol 586.26 0.46 5.99E+OO 3.53E+Ol 678.62 0.47 -1.51E+Ol 2.64E+01 688.67 0.86 8.65E+OO 1. 70E+01 719.35 0.28 1.62E+Ol 4. 96E+01 778.90 12.96 4.87E-01 9.34E- 01 810.45 0.32 -1.29E+Ol 3 .28E+D1 867.37 4.26 3.lOE-01 3 .69E+OO 919.33 0.43 -4.91E+Ol 3 .02E+01 964. 0 8 14.65 5.83E-0 1 1. 2 9E+OO 1085.87 10.24 -8.21E-01 1. 34E+OO 1 089.7 4 1. 73 -1. 09E+Ol 6.93E+OO 1 112.07 1 3 .69 6.93E-0 2 1.07E+OO 121 2 .95 1. 43 4.98E-01 1.09E+Ol 1249.34 0.19 4.09E+Ol 8.41E+01 12 99.14 1. 63 2 .67E-01 1.00E+Ol 1408.01 21.07 -1.05E-01 6.83E-01 1 457.64 0.50 9.28E+01 7.74E+Ol 1 528. 1 0 0.28 -1.81E+Ol 5.46E+01 Eu-154 123.07 40.4 0 1.lOE-01 1.89E-01 1.89E-01 247.93 6.89 1.13E-01 1. 32E+OO 591.76 4 .95 -1. llE+OO 2 .20E+OO 692. 42 1. 78 4.08E+OO 8. 2 7E+OO 723. 30 2 0.06 2 .66E-01 6.72E-01 756.80 4.52 -2 . 2 7E+OO 3 .08E+OO 873. 1 8 12.08 3.33E-01 1.18E+OO 996. 2 9 10.48 1. 72E-01 1 .70E+OO

[2865]

3/19/2018 8:00:49PM Page 6 of6 Analysis Report for 19-Mar-18-10020 B105100A-FIFC-326CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity Nuclide AADA Line AADA Name (pCVgrams) (pCilgrams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 5.58E-01 1.89E-01 9.06E-01 1274.4 3 34.80 2 .54E-01 4.87E-01 1596.48 1. 80 -7.36E+OO 8.16E+00 Eu-155 45. 3 0 1. 31 1.llE+Ol 3 .98E-01 2 .90E+01 60.01 1. 22 -6.30E+OO 2 .96E+Ol 86.55 30.70 -6.71E-02 3 .98E-01 105.31 21.10 5.43E-0 2 4.06E-01 Ra-2 2 6 186.21 3 .64 1.64E+OO 2 .77E+OO 2 .77E+OO Pa-23 1 2 7.36 10. 3 0 1.06E+OO 3 .49E+OO 3.49E+OO 2 83.69 1. 70 1.16E+OO 5.57E+OO 300.07 2 .47 3.90E-01 4.41E+OO 302.65 2 .20 2 .78E-01 4.78E+OO 330.06 1. 40 -7.78E-01 7.53E+OO U- 235 143.76 10. 96 -8.42E-0 2 1.70E-0 1 8.03E-01 163.33 5.08 - 1.75E-01 1. 69E+OO 185.71 57. 2 0 5.77E-0 2 1. 70E-01 202.11 1. 08 -2 .59E+00 8.25E+OO 205.3 1 5.01 1.91E-01 1.86E+OO Am-241 59.54 35.90 -6 .04E-02 9.85E-01 9.85E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2866]

0000024575.CNF Live Time :1200.000 sec Real Time :1200.240 sec 60 Start: 1: -0 .2(kev) stop : 8192: 2046. 9(kev)

Acq. Start :Mon Mar 19 19:40:39 2018 55 50 45

[2867]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/19/2018 8:23:52PM Page I of6

~pex-Gamma Analysis Report for 19-Mar-18-10021 B105100A-FIFC-326CV 0.0" - 0.5" 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 19-Mar-18-10021 Sample Description : 8105100A-FIFC-326CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.344E+02 grams Facility : Default Sample Taken On : 2/14/2018 8:15:00AM Acquisition Started : 3/19/2018 8:03:46PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 352 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.2 seconds Dead Time : 0.02%

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) ; 120 - 8192 Peak Area Range (in channels) : 120-8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 3/12/2018 Efficiency Calibration Used Done On : 3/19/2018 Efficiency Calibration Description : install Sample Number : 24577 Certificate Name : Eu155-Na22 Certificate Date : 12/20/2011 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/19/2018 8:23:48PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2868]

3/19/2018 8:23:52PM Page 2 of6 Analysis Report for 19-Mar-18-10021 81051 OOA-FIFC-326CV 0.0" -0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.52 950 - 959 954.54 2.41E+01 17.38 4.18E+01 0.60 2 511.16 2040 - 2049 2044.13 1. 72E+Ol 13.34 2.36E+Ol 0.74 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\CanberraV\pex\Root\Default\Libmry\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty An Pk 0.99 511. 00

100.00 l.37E-01 1.08E-01 Pb-212 0.99 115.18 0.60 238.63

43.60 1.64E-01 l.21E-01 300 . 09 3 .30

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.0_00sigma

[2869]

3/19/2018 8:23:52PM Page 3 of6 Analysis Report for 19-Mar-18-10021 B105100A-FIFC-326CV 0.0" - 0.5" 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

An Pk 0.994 1.37E-01 1.0SE-01 Pb-212 0.998 1.64E-01 1.21E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2870]

3/19/2018 8:23:52PM Page 4 of6 Analysis Report for 19-Mar-18-10021 B105100A-FIFC-326CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/19/2018 8:23:48PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M ::: First peak in a multiplet region m ::: Other peak in a multiplet region F ::: Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCilgrams) (pCi/grams)

(keV)

+ An Pk 511. 00

100.00 1.37E-01 1.65E-01 1.65E-01 BE-7 477.60 10.44 1. 32E-01 1.77E+OO 1.77E+OO K-40 1460.82 10.6 6 3.77E+OO 3.53E+OO 3 .53E+OO Co-60 1173. 2 3 99.85 8.65E-0 2 1.76E-01 2.00E-01 1332.49 99.98 -5.34E-02 1.76E-01 Nb-94 702.65 99.81 - 1 .66E-02 1.36E-01 1. 3 6E-01 871.09 99.89 -l.05E-01 l. 3 6E-01 Ag-108m 79.13 6.60 1.65E+OO l.15E-0 1 2 .82E+OO 433.94 90.50 6.00E-02 1.15E-01 614.28 89.80 7.03E-02 1.77E-Ol 722. 94 90.80 -2 .47E-02 1.37E-01 Sb-125 176.31 6.84 -9.76E-01 3 .55E-01 l.07E+OO 38 0 .45 1. 52 -1.0lE+OO 6.00E+OO 427.87 29.60 -l. 3 1E-01 3.55E-01 463.36 10.49 -8.41E-01 6.86E-01 600.60 17.65 4.98E-01 8.90E-01 606.71 4.98 -5.56E-01 3.35E+00 635.95 11. 22 -2.0lE-01 l . 1 5E+OO 671. 44 1. 79 -2.08E+OO 6.22E+OO

[2871]

3/19/2018 8:23:52PM Page 5 of6 Analysis Report for 19-Mar-18-10021 B1051 OOA-F IFC-326CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCl/grams) (pCi/grams)

(keV)

Ba-133 79.61 2.65 -6.16E-02 2 .19E-01 6.47E+OO 81.00 32.90 -7.51E-02 4.56E-01 2 76.40 7.16 1.13E+OO 1. 53E+OO 302.85 18.34 6.52E-02 5.94E-Ol 356.01 62.05 8.80E-02 2. 19E-01 383.85 8.94 4.58E-01 1 .12E+OO Cs-134 475.36 1. 48 -3.51E+OO l .63E-01 8.14E+OO 563.25 8.34 -9.30E-01 1.39E+OO 569.33 15.37 -5.92E-01 8.06E-01 604. 72 97.6 2 -2.07E-01 1. 63E-01 795.86 85.46 7.03E-02 1.78E-01 801.95 8.69 -l.80E+OO 1. 96E+OO 1038.61 0.99 7.08E+OO l .45E+Ol 1167. 97 1. 79 -2 .98E+OO 9.93E+OO 1365.19 3.02 -7.0lE-01 4.77E+OO Cs-137 661.66 85.10 -4.75E-02 1.67E-01 1.67E-01 Eu-152 121.78 2 8.67 -2 .27E-01 2.95E-0 1 2 .95E-01 244.70 7.61 -6.87E-01 1. 24E+OO 295.94 0 . 45 -9.75E+OO 2 .22E+Ol 344. 2 8 26.60 4.86E-02 3.90E-01 367.79 0.86 -5.12E-01 1.22E+Ol 411.12 2 . 24 1. 04E-01 5.40E+OO 443. 96 2 .83 3.33E-01 3.65E+OO 488.68 0.42 - l. 42E+Ol 2.49E+Ol 563 . 99 0.49 5.41E+OO 2.44E+Ol 586.26 0.46 -5.03E-01 3.23E+Ol 678.62 0.47 l.49E+Ol 2 .54E+Ol 688.67 0.86 l.50E+Ol 1. 83E+Ol 719.35 0.28 l.41E+Ol 4.29E+Ol 778.90 12. 96 9.46E-02 9.76E-Ol 810.45 0. 32 -4.09E+Ol 4.05E+Ol 867.37 4. 26 -2 . 2 1E-01 3.33E+OO 919.33 0.43 1.84E+OO 1.41E+Ol 964.08 14.65 -7.74E-01 1.15E+OO 1085.87 10.24 -l.50E-01 1.61E+OO 1089.74 1. 73 -4.48E+OO 9.57E+OO 1112. 07 13.69 2.39E-01 1. 23E+OO 121 2 .95 1. 43 l.87E+OO l.09E+Ol 1249.94 0.19 l.71E+Ol 9. 2 2E+Ol 1299 .14 1. 63 l.83E+OO 1 .00E+Ol 1408.01 21. 07 -8.53E-02 6.83E-01 1457.64 0.50 7.40E+Ol 7.43E+Ol 1528.10 0. 2 8 1. 20E+Ol 4.49E+Ol Eu-154 123.07 40.40 2.99E-02 2 . llE-01 2 . llE-01 247.93 6.89 -5 . 45E-01 l .28E+OO 591.76 4.95 -4.32E-0 1 2. 59E+OO 692.42 1. 78 -2.0lE+OO 8. 2 7E+OO 723. 30 2 0.06 2.24E-01 6. 72E-01 756.80 4.52 -1. 24E+OO 2 .86E+OO 873.18 12.08 -6.25E-01 1 .03E+OO 996. 2 9 10.48 8.74E-01 1.49E+OO

[2872]

3/19/2018 8:23:52PM Page 6 of6 Analysis Report for 19-Mar-18-10021 B105100A-FIFC-326CV 0.0" - o.s- 0.5" Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCilgrams) (pCl/grams)

(keV)

Eu-154 1004.76 18.01 6.51E-01 2 .llE-01 9.68E-01 1274.43 3 4.80 -1.13E-01 2 .73E-01 1596.48 1. 80 -7.26E+OO 9.58E+00 Eu-155 45.30 1. 31 5.14E+00 3 .88E-01 2 .86E+Ol 60.0 1 1. 22 -l.36E+Ol 2 .75E+Ol 86.55 3 0.70 -6.61E-0 2 3 .88E-01 105.31 2 1.10 2.87E-0 2 4.80E-01 Ra-22 6 186.21 3. 64 2.17E-01 2.92E+OO 2 .92E+OO Pa-23 1 27.36 10.30 8. 71E-01 3.34E+OO 3.34E+OO 283.69 1. 70 -5.66E-01 5.57E+OO 300.07 2 .47 -9.47E-Ol 4. 2 9E+OO 302.65 2 .20 2 .07E+OO 4.98E+OO 330.06 1. 40 -5.18E-0 2 7.41E+OO U- 2 35 143.76 10.96 l.12E-02 l.92E-Ol 7.79E-01 163.33 5 .08 9.40E-01 1. 64E+OO 185.71 57. 2 0 1.32E-01 1. 92E-01 20 2 .11 1. 08 -4. llE+OO 8.25E+OO 205.31 5.01 -5.43E-01 l.73E+OO Am-241 59.54 35.90 -4.50E-01 9 .71 E- 01 9. 71E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Haif-iife too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2873]

0000024577 .CNF Live Time :1200.000 sec Real Time :1200.240 sec 60 start: 1: -0.2(kev) stop : 8192:2046.9(kev)

Acq. Start :Mon Mar 19 20: 03: 46 2018 55 50 45 35

[2874]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: 1

3/13/2018 10:26:38PM Pagel of6

~pex-Gamma Analysis Report for 13-Mar-18-10026 B105100A-FSFC-329CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10026 Sample Description : B105100A-FSFC-329CV 0.0" - 0.5" o.o*

Sample Type : Puck Unit Sample Point Sample Size 1.151E+02 grams Facility : Default Sample Taken On : 3/9/2018 1:10:00PM Acquisition Started : 3/13/2018 10:06:31PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.02 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24315 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 10:26:34PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2875]

3/13/2018 10:26:38PM Page 2 of6 Analysis Report for 13-Mar-18-10026 B 1051 OOA-FS FC-329CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238. *72 949 - 958 954.46 2. 16E+Ol 17 .76 4.69E+Ol 0.39 2 352.02 1 403 - 1411 1407.08 2 .23E+Ol 14 .69 2 .95E+Ol 0 .43 3 661.52 2634 - 2 653 2643.98 3.62E+02 38.48 4.95E+OO 1. 33 4 1460.78 5836 - 5848 5841.06 3.02E+Ol 12.64 7.54E+OO 0.57 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFiED NUCLiDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 1. 0 0 1460.82

10.66 3.62E+OO 1. 55E+OO Cs-137 0.99 661.66

85.10 3.06E+OO 4.90E-01 Bi-211 0.86 351.07

13 . 02 7.55E-0 1 5 .13E-01 Pb-212 0.99 11 5 .18 0.60 2 38.63

43.60 1 .63E-01 1 .3 7E-01 300. 0 9 3.30 Pb-214 0.99 241.99 7. 2 5 295. 22 1 8.4 2 351.93

35.60 2 .76E-01 1.87E-01 785. 96 1. 06

[2876]

3/13/2018 10:26:38PM Page3 of6 Analysis Report for 13-Mar-18-10026 B105100A-FSFC-329CV 0.0" - 0.5" 0.0"

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 1. 000 3.62E+OO 1.SSE+OO Cs-137 0.997 3.06E+OO 4.90E-01

? Bi-211 0.867 7.SSE-01 5.13E-01 Pb-21 2 0.999 1.63E-01 1. 37E-01

'? Pb-214 0.999 2.76E-01 1 .87E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2877]

3/13/2018 10:26:38PM Page 4 of6 Analysis Report for 13-Mar-18-10026 B105100A-FSFC-329CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 10:26:34PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA

Name (pCUgrams) (pCi/grams) (pCl/grams)

(keV)

An Pk 511. 00 100.00 2 .35E-01 2 .34E-01 2 .34E-01 BE-7 477.60 10.44 - 2 .53E-02 1. 58E+OO 1.58E+OO

+ K-40 14G0.82

10.66 3.62E+OO 1.51E+OO 1.61E+OO Co-60 1173.23 99.85 5.46E-02 1.95E-01 1.95E-01 1332.49 99.98 1.30E-01 2 . 22E- 01 Nb-94 702.65 99.81 - 4.14E-02 1.5:E-01 1.57E-01 871. 09 99.89 - 2 .40E-03 1.65E-01 Ag-108m 79 .13 6 . 60 1.69E+OO 1. 86E-01 3 .07E+OO 433.94 90.50 1 .31E- 01 2 .lOE-01 614. 2 8 89.80 -7.48E-02 2 .24E-01 722. 94 90.80 9.63E-02 1.86E-01 Sb-125 176.31 6.84 4.84E-01 6.05E-01 1.50E+OO 380.45 1. 52 - 6. 2 1E-01 9.19E+OO 42 7.87 2 9.60 -4.55E-01 6.05E-01 463.36 1 0.49 2 .62E-01 1.74E+OO 600.60 17.65 3.88E-01 1.02E+OO 606.71 4.98 1.97E+OO 4.80E+OO 635.95 11 .22 -8 . 42E-01 1.13E+OO 671.44 1. 79 4.07E+OO 7. 3 5E+OO

[2878]

3/13/2018 10:26:38PM Page 5 of6 Analysis Report for 13-Mar-18-10026 B105100A-FSFC-329CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCilgrams) (pCi/grams} (pCilgrams}

(keV)

Ba - 133 79.61 2 .65 4.36E+OO 2 .52E-01 7.44E+OO

81. 00 32 .90 -2 .19E-01 5. llE-01 2 76.40 7.16 1.93E-01 1.71E+OO 302.85 18.34 1.89E-01 6.90E-01 356.01 62.05 -1.09E-01 2 .52E-01 383.85 8.94 -3 .79E-01 1.63E+OO Cs-1 3 4 475.36 1. 48 4.82E+OO 1. 5 0E-01 1. 22E+Ol 563.25 8.34 1. 72E-01 1.91E+OO 569.33 15.37 6.29E-02 1.02E+00 604. 72 97.6 2 -1. 23E-01 2 .30E-01 795.86 85.46 2 .21E-02 1.50E-01 801.95 8.69 6.69E-01 1.49E+OO 1038.61 0.99 -8. 3 6E+OO 1.74E+Ol 1167. 97 1. 79 8.43E+OO 1. 25E+Ol 1365.19 3.02 2 .00E+OO 5.45E+OO

+ Cs-137 661.66

85.10 3.06E+OO 1. 08E-01 1.08E-01 Eu-152 121.78 28.67 -7.52E-03 3 .31E-01 3.31E-01 2 44.70 7.61 -3.96E-01 1.95E+OO 2 95.94 0.45 1.41E+Ol 3.16E+Ol 344.28 2 6.60 -5.73E-01 5. 2 3E-01 367.79 0.86 -8.47E+OO 1. 72E+Ol 411.12 2 .24 1.25E+OO 7.24E+OO 44 3 .96 2 .83 6.08E-01 5.93E+OO 488.68 0.4 2 1. 32E+Ol 4.30E+Ol 563.9Sl 0.49 1.95E+00 3.16E+Ol 586.26 0.46 2.94E+Ol 4.52E+Ol 678.62 0.47 3.88E+OO 2 .55E+Ol 688.67 0.86 2.92E+OO 1. 4 9E+Ol 719.35 0.28 3.04E+Ol 6.05E+Ol 778.90 12.96 -6.72E-01 l.03E+OO 810.45 0.32 -1.62E+OO 3.24E+Ol 867.37 4.26 3.60E-01 4 . 0lE+OO 919.33 0.43 6.76E+OO 3.69E+Ol 964.08 14.65 4.88E-01 1. 42E+OO 1085.87 10. 2 4 -1.17E+OO 1.56E+OO 1089.74 1. 73 4.74E+OO 9.75E+OO 1112. 07 13.69 -5.88E-01 9.47E-01 1 2 12 . 95 1. 43 2 .76E-02 1.20E+Ol 1249.94 0 .19 1.41E+Ol 9. 2 8E+Ol 1299.14 1. 63 4.99E+OO 1.llE+Ol 1408.01 21.07 4. llE-01 9.14E-01 1457.64 0.50 8 .13E+Ol 8.52E+Ol 1528.10 0.28 9.42E+OO 4.55E+Ol Eu- 154 1::23. 07 40.40 3.80E-02 2 .41E-01 2 .41E-01 247.93 6.89 5.85E-01 2 .06E+OO 591.76 4.95 -1.83E+OO 3 .18E+OO 692.42 1. 78 3.18E+OO 8.16E+OO 723 . 30 20.06 6.51E-01 8.67E-01 756.80 4. 52 1.16E+00 3. 30E+OO 873.18 12.08 -2.35E-01 1.26E+OO 996. 2 9 10.48 -3 .92E-01 1 . 43E+OO

[2879]

3/13/2018 10:26:38PM Page 6 of6 Analysis Report for 13-Mar-18-10026 B1051 OOA-FSFC-329CV o.o* - o.5" 0.0" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCUgrams) (pCi/grams) (pCilgrams)

(keV)

Eu-154 1004.76 18 . 01 -2 .04E-01 2 .41E-01 8.39E-01 1 2 74.43 34.80 2 .30E-01 5. llE-01 1596.48 1. 80 1.34E+00 1.12E+Ol Eu-155 45.30 1. 31 -'7.23E+OO 4.54E-01 2 .54E+Ol 60.01 1. 22 - 1.78E+Ol 2 .56E+Ol 86.55 30.70 5.76E-02 4.54E-Ol 105.31 21.10 1. 74E-01 4. 96E-01 Ra-2 2 6 186. 2 1 3.64 9.00E-01 3. 2 1E+OO 3.21E+OO Pa-231 2 7.36 10.30 1.51E+OO 3.43E+OO 3.43E+OO 283.69 1. 70 - 4.90E+OO 6. 3 4E+OO 300.07 2 .47 -5.37E+OO 5.08E+OO 302.65 2 .20 l.14E-01 5.67E+OO 330.06 1. 40 1. 22E+OO l. lOE+Ol U- 2 35 143.76 10.96 -4.03E-01 2 .02E-01 8.74E-01 163.33 5.08 1.95E-01 1 .85E+OO 185.71 57. 2 0 4.12E-02 2 .02E-01 202 .11 1. 08 6.65E-01 1 .03E+Ol 205.31 5.01 -5 .13E-01 2 .24E+OO Am-241 59.54 35.90 -6.39E-01 8 . 9'7E- 01 8.97E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2880]

0000024315.CNF Live Time :1200.000 sec 120 Real Time :1200.280 sec Start: 1: -0. O(kev) stop : 8192: 2047. B(kev)

Acq. Start :Tue Mar 13 22:06:31 2018 110 100 90 80

~

7 V,

V V)

+-'

C:

s 0

u

[2881]

1000 2000 3000 4000 7000 8000 channel

~

ROI Type: 1

3/13/2018 10:48:37PM Page 1 of6

~pex-Gamma Analysis Report for 13-Mar-18-10027 B105100A-FSFC-329CV 0.0" - 0.5 0.5" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10027 Sample Description : B105100A-FSFC-329CV 0.0" - 0.5" 0.5" Sample Type : Puck Unit Sample Point Sample Size 1.151E+02 grams Facility : Default Sample Taken On : 3/9/2018 1: 10:00PM Acquisition Started : 3/13/2018 10:28:29PM Procedure : Puck_half_inch Operator : Administrator Detector Name : P11314 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Time : 1200.3 seconds Dead Time : 0.03%

Peak Locate Threshold : 3.00 Peak Locate Range (in *channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 12/15/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24317 Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 10:48:33PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192

[2882]

3/13/2018 10:48:37PM Page 2 of6 Analysis Report for 13-Mar-18-10027 B 1051 OOA-FSFC-329CV 0.0" - 0.5" 0.5" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 242.09 963 - 972 967.93 1 .53E+Ol 13. 94 2 .95E+Ol 0.55 2 352.15 1402 - 1412 1407.62 2 .37E+Ol 15. 62 3 .07E+Ol 1. 07 3 661.51 2 638 - 2 652 2 643.93 1 .67E+02 2 7.78 1.81E+Ol 1. 36 4 1460.26 5832 - 5846 5838.99 3 .73E+Ol 13. 87 7.50E+OO 0.94 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.95 1460.82

10.66 4.46E+OO 1.71E+OO Cs-137 0.99 661.66

85.10 1.41E+OO 2 .90E-01 Pb-214 0.99 241. 99

7.25 7.02E-01 6.50E-01 295.22 18.42 351.93

35.60 2 .93E-01 1 .99E-01 785.96 1. 06

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

[2883]

3/13/2018 10:48:37PM Page 3 of6 Analysis Report for 13-Mar-18-10027 B105100A-FSFC-329CV o.o* - 0.5" 0.5" INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.951 4.46E+00 l.71E+OO Cs-137 0. 996 l.41E+OO 2.90E-01 Pb-214 0.995 3.28E-01 l.91E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2884]

3/13/2018 10:48:37PM Page 4 of6 Analysis Report for 13-Mar-18-10027 B105100A-FSFC-329CV 0.0" - 0.5" 0.5" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 10:48:33PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCi/gramsj (pCi/gramsj (pCl/grams)

(keV)

An Pk 511.00 100.00 O.OOE+OO 1.95E-01 1. 95E-01 BE-7 477.60 10.44 4.89E-01 1.55E+OO 1.55E+OO

+ K-40 1460.8 2

10.66 4.46E+OO 1.68E+OO 1.68E+OO Co-60 1173.23 99.85 -1.05E-01 1.78E-01 1.78E-01 1332.49 99.98 8. 2 6E-02 1.84E-01 Nb-94 702.65 99.81 7.19E-03 1.59E-01 l.71E-01 871.09 99.89 -2 . 2 0E-03 1. 59E-01 Ag-1 08m 79.13 6.60 2 .14E+OO 1.60E-01 2. 91E+OO 433.94 90.50 -2 .78E-02 1. 60E-01 614.28 89.80 -1.03E-01 1. 96E-01 722 .94 90.80 1.44E-01 1.91E-01 Sb-125 176.31 6.84 3.52E-01 4.93E-01 1.36E+OO 380.45 1. 52 4.47E+OO 9.19E+OO 427.87 29.60 -1.43E-01 4.93E-01 463.36 10.49 4.67E-01 1.41E+OO 600.60 17.65 -1.64E-01 7.91E-01 606.71 4.98 1.62E+OO 4.40E+OO 635.95 11. 22 -1.04E-03 1.34E+OO 671.44 1. 79 -4.87E-01 8.48E+OO

[2885]

3/13/2018 10:48:37PM Page 5 of6 Analysis Report for 13-Mar-18-10027 B1051 OOA-FSFC-329CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCi/grams) (pCi/grams)

(keV)

Ba-133 79.61 2 .65 2 .15E+00 2 .64E-01 6.81E+OO

81. 00 32.90 -7.44E-01 4.03E-01 276.40 7.16 -3 .57E-01 1.67E+OO 302.85 18.34 4.61E-02 7. 3 1E-01 356.01 62.05 -1.24E-01 2.64E-01 383.85 8.94 6.62E-01 1. 52E+OO Cs - 134 475.36 1. 48 -4.49E+OO 1. 81E-01 1. llE+Ol 563.25 8.34 -2 .87E-01 2 .02E+OO 569.33 15.37 1.53E-02 1. llE+OO 604. 72 97. 62 -3.42E-02 2 .07E-01 795.86 85. 46 1. 06E-01 1. 81E-01 801. 95 8.69 6.45E-01 2 .16E+OO 1038.61 0.99 5.51E+OO 1.89E+Ol 1167. 97 1. 79 O.OOE+OO 8.81E+OO 1365.19 3.0 2 4.0lE-01 3.07E+OO

+ Cs-137 661. 66

85.10 1.41E+OO 1.71E-01 1. 71E-01 Eu-152 121.78 2 8 . 67 -1.64E-0 2 3.21E-01 3.21E-01 2 44.70 7.61 -2 . 2 5E-01 1 .73E+OO 2 95.94 0.45 2 .76E+Ol 3.52E+Ol 344. 2 8 2 6.60 3 .88E-02 4.76E-01 367.79 0.86 3 .85E+OO 1. 66E+Ol 411.12 2 .24 8.61E-01 6.00E+OO 443. 96 2 .8 3 -1.23E+OO 5.70E+OO 488.68 0.42 9.94E+OO 3 .23E+Ol 563.99 0.49 -3.80E+Ol 3.29E+Ol 586. 2 6 0.46 -4.78E+OO 3.47E+Ol 678.62 0.47 -7.91E+OO 2 .55E+Ol 688.67 0.86 -6.87E+OO l.95E+Ol 719.35 0. 2 8 -4.57E+OO 5 . 88E+Ol 778.90 12.96 -6.80E-0 1 1.17E+OO 810.45 0.32 1.33E+Ol 4.88E+01 867.37 4.26 -8.34E-01 4.14E+OO 919.33 0.43 -2 .40E+OO 2 .06E+Ol 964.08 14.65 -7.41E-01 1. 2 1E+OO 1 085.87 10. 2 4 1.25E-01 2 .02E+OO 1 089.74 1. 7 3 - 4.03E+OO 1 . 02E+Ol 1 112.07 13.69 -7.69E-01 1.25E+OO 1212.95 1. 43 1. 02E+OO 9.65E+OO 1249.94 0.19 -8.72E+Ol 7.44E+01 1 299.14 1. 63 6.41E+00 1.23E+Ol 1408.01 21.07 4.70E-01 9.66E-01 1457.64 0. 5 0 6.36E+Ol 8.70E+Ol 1528.10 0.28 O.OOE+OO 1.35E+Ol Eu-154 123.07 40.40 l.38E-02 2 . 1 7E - 01 2 .17E-01 247.93 6.89 3.31E-01 1. 54E+OO 591.76 4.95 1.29E+OO 3.18E+00 692.4 2 1. 78 4.68E-01 8.98E+OO 723. 30 20.06 6.51E-01 8.67E-01 756.80 4. 52 - 9. 72E-01 2 .73E+OO 873.18 1 2 .08 -2 .96E-01 1. 2 0E+OO 996.29 10.48 5.51E-01 1.73E+OO

[2886]

3/13/2018 10:48:37PM Page 6 of6 Analysis Report for 13-Mar-18-10027 B105100A-FSFC-329CV 0.0" - 0.5" 0.5" Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCilgrams) (pCUgrams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 -6.74E-02 2 .17E-0 1 9.73E-01 1274 . 43 34.80 -9.50E-01 5.40E-01 1596. 48 1. 80 -4.60E+OO 9.57E+OO Eu-155 45.30 1. 31 -1.03E+Ol 4.12E-01 2 .47E+Ol 60.0 1 1. 22 8.75E-01 2 .49E+Ol 86.55 3 0.70 9.94E-02 4.12E-01 1 05.31 2 1.10 -7.39E-02 4.68E-01 Ra-226 1 86.21 3. 64 1. 71E+OO 3 .09E+OO 3 .09E+OO Pa-231 27 .36 10 . 30 1.64E+OO 3 .18E+OO 3 .18E+OO 283.69 1. 70 -2 .48E+OO 5.93E+OO 300.07 2 .47 -5.30E+OO 5. 2 0E+OO 302.65 2 .20 3 .81E+OO 6. 2 1E+OO 330. 0 6 1. 40 9.43E+OO 1.03E+ Ol U-235 143 . 76 10. 96 -4.80E-01 1.99E-O l 7.05E-01 163.33 5.08 -1.45E+OO 1.60E+OO 185.71 57.20 1.66E-01 1.99E-01 2 02. 11 1. 08 -8.02E+OO 8.69E+OO 205.31 5.01 -2.0lE-01 2 .03E+OO Arn-241 59.54 35.90 2 .50E-01 9. l OE-01 9.lOE-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2887]

0000024317 .CNF Live Time :1200.000 sec Real Tille :1200.330 sec 60 start: 1: -0.0(kev)

Stop : 8192: 2047 .8(kev)

Acq. start :Tue Mar 13 22:28:29 2018 55 50 45 40 35

[2888]

1000 2000 3000 4000 5000 6000 7000 8000 channel

~

ROI Type: l

3/13/2018 11: 11 :32PM Page 1 of6

~pex-Gamma Analysis Report for 13-Mar-18-10028 B105100A-FSFC-332CV 0.0" - 0.5" 0.0" GAMMA SPECTRUM ANALYSIS Sample Identification : 13-Mar-18-10028 Sample Description : B105100A-FSFC-332CV 0.0" - 0.5" 0.0" Sample Type : Puck Unit Sample Point Sample Size 1.235E+02 grams Facility : Default Sample Taken On : 3/9/2018 2:10:00PM Acquisition Started : 3/13/2018 10:51 :24PM Procedure : Puck_half_inch Operator : Administrator Detector Name : 324 Geometry : Puck_half_inch Live Time : 1200.0 seconds Real Tima : 1201.6 seconds Dead Time : 0.13 %

Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120-4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 8/9/2017 Efficiency Calibration Used Done On : 3/13/2018 Efficiency Calibration Description Sample Number : 24318 Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/13/2018 11 :11 :28PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096

[2889]

3/13/2018 11:11 :32PM Page 2 of6 Analysis Report for 13-Mar-18-10028 B105100A-FSFC-332CV 0.0" - 0.5" 0.0" Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.67 473 - 481 477.53 4.43E+Ol 28.85 1 .43E+02 0.91 2 609.59 1213 - 122 2 1218.75 2 .76E+Ol 16.35 3.48E+Ol 0.70 3 661.84 1317 - 1329 1323. 22 2 .57E+02 34.57 3.20E+Ol 1. 39 4 1461.05 2917 - 2928 2922 .16 5.27E+Ol 14.94 2 .64E+OO 2.28 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82

10.66 5.20E+OO 1. 54E+OO Cs-137 0.99 661.66

85.10 1.83E+OO 3. 30E-01 Pb-21 2 1. 00 115 .18 0.60 2 38.63

43.60 2.90E-01 1.95E-Ol 300.09 3.30 Bi-214 0.99 609.32

45.49 3.46E-01 2 .09E-01 768.36 4.89 806.18 1. 2 6 934.06 3 . 11 11 2 0. 2 9 14.92 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79

[2890]

3/13/2018 11 :11 :32PM Page 3 of6 Analysis Report for 13-Mar-18-10028 8105100A-FSFC-332CV 0.0"

_0.5" 0.0" Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi-214 0.99 1401.52 1. 33 1407.99 2.39 1509.21 2 .13 1661. 2 7 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2 .03 2118. 51 1.16

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.9 92 5.20E+OO 1. 54E+00 Cs-137 0.994 1. 83E+OO 3.30E-01 Pb-212 1.000 2 .90E-01 1.95E-01 Bi-214 0.995 3.46E-01 2 .09E-01

? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

[2891]

3/13/2018 11 :11 :32PM Page 4 of6 Analysis Report for 13-Mar-18-10028 B105100A-FSFC-332CV 0.0" - 0.5" 0.0" UNIDENTIFIED PEAKS Peak Locate Performed on : 3/13/2018 11:11:28PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCUgrams) (pCl/grams)

(keV)

An Pk 511. 00 100.00 l.78E-01 2 . 3 4E-01 2 .34E-01 BE-7 477.60 10.44 7.81E-Ol l.61E+OO l.61E+OO

+ K-40 1460.82

10.66 5.20E+OO 8.76E - 01 8.76E-01 Co-60 1173.2 3 99.85 l.52E-01 l.90E-01 2 .18E-01 1332.49 99.98 l . 17E-01 1. 90E-01 Nb-94 702.65 99.81 3.56E-03 l.40E-01 1.40E-01 871.09 99.89 6.97E-0~ l.62E-Ol Ag-108m 79.13 6 . 60 1.69E+OO l.65E-Ol 3.13E+OO 433.94 90.50 - 3 .77E-0 3 1.65E-01 614.28 89.80 -l.51E-01 2 .29E-01

'"7 22 . 94 90.80 4.74E-02 1. 76E-01 Sb-125 176.31 6 . 84 1. 82E-01 5.43E-01 l.86E+OO 380.45 1. 52 - 2 .41E+OO 8.73E+OO 427.87 29.60 7.90E-03 5.43E-01 463.36 10.49 5.32E-01 l . 3 7E+OO 600.60 17.65 -5.80E-0 2 8.78E-01 606.71 4 . 98 -7.16E-02 4.48E+OO 635.95 11.22 -8.22E-02 l.28E+OO 671. 44 1. 7 9 - 2.06E+OO 6.91E+OO

[2892]

3/13/2018 11 :11:32PM Page 5 of6 Analysis Report for 13-Mar-18-10028 81051 OOA-FSFC-332CV 0.0" - 0.5 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCi!grams)

(keV)

Ba- 133 79.61 2 .65 -l.67E-01 2 .75E-0 1 7.23E+OO

81. 00 32 .90 -4. 3 7E-01 4.89E-01 2 7 6.40 7.16 l.46E-01 1. 75E+OO 302.85 18.34 1. 53E-01 7.12E-01 356.01 62.05 4.89E-0 2 2 .75E-01 383.85 8.94 -6.64E-Ol l.44E+OO Cs -134 475.36 1. 48 l.14E+Ol l .52E-01 1.19E+Ol 563. 2 5 8.34 -1.04E+OO 1 .65E+OO 569.33 15.37 2 .63E-01 1.05E+OO 604. 72 97.6 2 -4.91E-02 1.85E-01 795.86 85.46 -5.02E-02 1. 52E-01 801. 95 8.69 -4.81E-01 1. 61E+oo-10 3 8 . 61 0.99 -2 .07E+OO 1. 44E+Ol 1167. 97 1. 79 -l.86E+OO 9. 3 8E+OO 1365. 1 9 3.0 2 4 .13E+OO 7.lOE+OO

+ Cs-137 661.66

85.1 0 l.83E+OO l . 77E-01 l.77E-01 Eu-152 121.78 28.67 -2 .38E-02 3. G7E-01 3 .67E-01 244.70 7. 61 2. 73E-01 l.82E+OO 295.94 0.45 2. 50E+Ol 3 .43E+Ol 344.28 2 6.60 4.36E-02 5. llE-01 367.79 0.86 - 2 .91E+OO 1.64E+Ol 411.12 2 . 24 1.05E+OO 6.41E+OO 44 3 . 96 2 .83 7.77E-01 5.54E+OO 488.68 0.42 -9.12E+00 3.27E+Ol 563.99 0 .49 -l.65E+Ol 2 .73E+Ol 586.26 0.46 3.77E+OO 3.87E+Ol 678.62 0.47 6. 3 4E+OO 2 . 96E+Ol 688.67 0.86 - 7. 3 5E+OO 1. 60E+Ol 719.35 0.28 - 1 .62E+Ol 4.94E+Ol 778.90 12.96 -1.31E-02 1.09E+OO 810.45 0.32 -5.43E-01 4.52E+Ol 867.37 4 .26 3.34E-01 3 .98E+OO 91 9. 3 3 0.43 -5.83E+OO 3. 2 1E+Ol 964.08 14.65 -2 .13E-01 1. 08E+OO 1085.87 10. 2 4 -5.07E-01 l.73E+OO 1089.74 1. 73 -2. 2 0E+OO 9 . 93E+OO 1112. 07 13. 69 7.99E-01 1. 57E+OO 1 212.95 1. 43 l .41E+OO 1. 20E+Ol 1 2 49.94 0.19 -l.40E+Ol 9. 96E+Ol 1 2 99. 1 4 1. 63 -4.42E+OO 8.03E+OO 1408.01 2 1. 07 -4.12E-01 6.05E-01 1457.64 0.50 -3 .30E+Ol 8.31E+Ol 1528.10 0. 2 8 6.78E+OO 6.37E+Ol Eu- 154 1 23 .07 40.40 1.06E-01 2 . 71E-0 1 2 .71E-01 2 47.93 6.89 l.48E-01 1. 71E+OO 591.76 4 . 95 8.97E-0 2 2 .93E+OO 692.42 1. 78 9.02E-Ol 7.77E+OO 723. 30 2 0.06 2 .13E-01 7.99E-01 756.80 4.5 2 -l.45E-01 3 . 2 5E+OO 873. 1 8 12.08 -3 . 22E- 01 1.lOE+OO 996. 2 9 10 . 48 3 .49E-01 1.38E+00

[2893]

3/13/2018 11:11:32PM Page 6 of6 Analysis Report for 13-Mar-18-10028 B 105100A-FSFC-332CV 0.0" - 0.5" 0.0" Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCi/grams)

(keV)

Eu-154 1004.76 18.01 -l.91E-01 2 . 71E-01 7.74E-01 1274.43 3 4.80 -3 .05E-01 3. 70E-01 1596.48 1. 80 3 .15E+OO 8.58E+OO Eu-155 45.30 1. 31 l .09E+Ol 4.69E-0 1 3.00E+Ol 60.01 1. 22 1. 72E+OO 2 .95E+Ol 86.55 30.70 -4.48E-0 2 4.69E-01 105.3 1 21.10 3.63E-0 2 5.65E-01 Ra-22 6 1 86.2 1 3.64 2 .32E+OO 3.65E+OO 3.65E+OO Pa-23 1 27.36 10.30 1.32E+OO 2.91E+OO 2.91E+OO 283.69 1. 70 -6 .28E-01 7.91E+OO 300.07 2 .47 -3 . 8 4E+OO 5.38E+OO 30 2 .65 2 . 20 1. 2 8E+OO 5.93E+OO 330.06 1. 40 2 . 3 6E+OO l.lOE+Ol U-235 143.76 10. 96 4.78E-01 2 . 2 9E-Ol l.OOE+OO 163.33 5.08 8.15E-01 2.67E+OO 1 85.71 57.20 8.42E-02 2.29E-01 20 2 . 11 1. 08 9.81E-01 l. 23E+Ol 205.31 5.01 -4.SOE-01 2.64E+OO Am-241 59.54 35.90 - 2 .04E-01 1. OOE+OO 1.00E+OO

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

[2894]

0000024318.CNF Live Time :1200.000 sec 120 Rea1 Time :1201.610 sec start: 1: O.l(kev)

Stop : 4096:2047.l(kev)

Acq. Start :Tue Mar 13 22:51:24 2018 110 V'I C:

s 0

u

[2895]

I 500 1000 1500 2000 2500 3000 3500 4000 channel

~

ROI Type: 1

ML19295G764

Text

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