ML19295G702

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Revised Final Status Survey (FSS) Report - Phase 2, Eberline Analytical Reports
ML19295G702
Person / Time
Site: Zion  File:ZionSolutions icon.png
Issue date: 02/13/2018
From:
ZionSolutions
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML19295G627 List:
References
ZS-2019-0090
Download: ML19295G702 (42)
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Text

[192]

EBERLINE EBS-OR-43348 February 13, 2018 Alex Bohacheff Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099 SAMPLE RECEIPT SERVICES CASE NARRATIVE Work Order# 18-02001-0R EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TENNESSEE 37830 PHONE (865) 481-0683 FAX (865) 483-1+621 This work order contains three solid samples received 02/01/2018. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.

CLIENT ID B 1021101FIFC005CV B 1021101FIFC006CV B 102110IFIFC008CV ANALYTICAL METHODS LAB ID 18-02001-04 18-02001-05 18-02001-06 Total Strontium was analyzed using EIChroM Method SRWOI Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.

Gamma Spectroscopy was performed using EPA Method 901.1 Modified.

Laboratory qualifiers are as follows:

U - Result is less than the MDA.

ANALYTICAL RES UL TS Combined Standard Uncertainty is reported at 2-sigma value.

Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific.

MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.

TOT AL STRONTIUM Samples were prepared by aliquoting as appropriate and leaching in HN03* Samples were diluted appropriately. Strontium recovery carriers were added to each sample. Chemical separations were conducted using selective extractions. Strontium precipitated was mounted on tared filter media.

Chemical recovery was determined by Strontium carrier mass determinations. Sample was counted by gas flow proportional counting and corrected for Yttrium-90 ingrowth.

Page 1 of 3

[193]

ANALYTICAL RESULTS CONTINUED TOT AL STRONTIUM CONTINUED Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are reported from Total Strontium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.

TRITIUM A representative aliquot of each sample was equilibrated with Tritium free water. Equilibrates were transferred into round-bottomed distillation flasks and attached to single stage stills. A portion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were then counted by beta liquid scintillation.

Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.

NICKEL-63 A representative aliquot of each sample was leached in HN03* Leachates were placed in an appropriately sized beaker. Stable elemental Nickel carrier was added to each sample prior to digestion. Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.

Samples demonstrated acceptable results for all Nickel-63 analyses. All results except the laboratory control sample demonstrated slightly high method detection limits. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.

GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass/aliquot of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.

Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. Some results demonstrated slightly high method detection limits. Some sample results are greater than the method detection limits. These results are rep01ied from the Canberra Gamma Apex "Nuclide MDA Report" and are not positive. These results are qualified as non-detect (U). The method blank demonstrated acceptable results for all radionuclides as rep01ied. Results for the Cobalt-60 and Europium-152 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.

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[194]

CERTIFICATION OF ACCURACY I ce1iify that this data rep01i is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her designee to be accurate as verified by the following signature.

Date: 2/13/2018 Eberline J\\nalytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please visit http://cbcrlineanalytical.com/ to provide us with feedback on our services.

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[195]

Printed: 211312018 8:53 AM Page 1 of 6 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02001

____ Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis

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    • --------*-----------*--~
-----~-----"'"'

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pCi/g 18-02001-01 LCS SPIKE 02/01/18 00:00 2/1/2018 2/2/2018 18-02001,

Tritium LANL ER-210 Modified 2.42E+02 5.76E+OO 1.47E+01 3.63E+OO 18-02001-02 ;

MBL BLANK 02/01/18 00:00 2/1/2018 2/2/2018 18-02001 Tritium LANL ER-210 Modified

-3.75E-01 2.12E+OO 2.12E+OO 3.67E+OO u

pCi/g

*-----',-"om"" ___,_,_,, _______________ '""""'"

18-02001-03 i DUP B102110IFIFC005CV 01/31/18 09:00 2/1/2018 2/2/2018 18-02001 Tritium LANL ER-210 Modified 9.25E+01 6.29E+OO 8.15E+OO 7.24E+OO 18-02001-04 DO B102110IFIFC005CV 01/31/18 09:00 2/1/2018 2/2/2018 18-02001 Tritium LANL ER-210 Modified i

9.30E+01 6.31E+OO 8.18E+OO 7.25E+OO pCi/g--

pCi/g 18-02001-05 TRG B1021101FIFC006CV 01/31/18 09:35 2/1/2018 2/2/2018 18-02001 Tritium LANL ER-210 Modified 2.04E+02 1.21E+01 1.67E+01 1.32E+01 18-02001-06 j TRG B1021101FIFC008CV 01/31/1810:12 2/1/2018 2/2/2018 18-02001 Tritium LANL ER-210 Modified 2.64E+01 9.04E+OO 9.16E+OO 1.43E+01 pCi/g

,, ___,_,_,,-,,,,,m ___________ "'"-

i 18-02001-01 LCS KNOWN 02/01 /18 00:00 2/1/2018 2/1/2018 18-02001 Nickel-63 ASTM 3500-Ni Modified : 1.50E+03 4.51E+01 pCi/g

, 2/1/2018

""""-,--,~-----~-~"

i pCi/g 18-02001-01 LCS SPIKE 02/01/18 00:00 2/1/2018 18-02001 Nickel-63 ASTM 3500-Ni Modified 1.46E+03 8.86E+OO 8.63E+01 2.00E+OO 18-02001-02 !

MBL BLANK 02/01/18 00:00

2/1/2018 2/1/2018 18-02001 ;

Nickel-63 ASTM 3500-Ni Modified : O.OOE+OO 1.18E+OO 1.18E+OO 2.03E+OO u

pCi/g 18-02001-03 i DUP B1021101FIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 Nickel-63 ASTM 3500-Ni Modified i 4.19E+OO 4.65E+OO 4.65E+OO 7.80E+OO u

pCi/g 18-02001-04 i DO B10211 OIFIFC005CV 01/31/18 09:00 I 2/1/2018 2/1/2018 18-02001 '

Nickel-63 ASTM 3500-Ni Modified I

4.36E+OO i

4.49E+OO ;

4.50E+OO 7.53E+OO u

pCi/g 18-02001-05 i TRG B102110IFIFC006CV 01/31/18 09:35 2/1/2018 18-02001 Nickel-63 ASTM 3500-Ni Modified i

4.94E+OO : 4.47E+OO 4.48E+OO 7.47E+OO u

pCi/g 18-02001-06 i TRG B102110IFIFC008CV 01/31/18 10:12 2/1/2018 2/1/2018 18-02001 Nickel-63 ASTM 3500-Ni Modified 5.99E+OO ! 4.59E+OO 4.60E+OO 7.63E+OO u

pCi/g i

i i

18-ULUU 1-U I LCS KNOWN 02/01/18 00:00 2/1/2018 2/5/2018 18-02001 Strontium-90 EIChroM SRW01 Modified j 5.22E+01 2.93E-01 pCi/g i

--,-~---------"----*----*---*-----------

EIChroM SRW01 Modified i pCi/g 18-02001-01 LCS SPIKE 02/01/18 00:00 2/1/2018 2/5/2018 18-02001 Strontium-90 5.94E+01 2.41E+OO 2.08E+01 9.77E-01

  • ---~-----,--,,-----------:

EIChroM SRW01 Modified :

18-02001-02 ;

MBL BLANK 02/01/18 00:00 2/1/2018 2/5/2018 18-02001 Strontium-90 6.74E-01 4.72E-01 5.27E-01 7.51E-01 u

pCi/g 18-02001-03 :

DUP B1021101FIFC005CV 01/31/18 09:00 2/1/2018 2/5/2018 18-02001 Strontium-90 EIChroM SRW01 Modified I 8.68E-01 i

3.79E-01 4.84E-01 5.47E-01 oCi/q 8-02001-04 EIChroM SRW01 Modified i DO B102110IFIFC005CV 01/31/18 09:00 : 2/1/2018 2/5/2018 18-02001 Strontium-90 8.51E-01 4.07E-01 5.03E-01 6.10E-01 pCi/g 18-02001-05,

TRG B1021101FIFC006CV 01/31/18 09:35 i 2/1/2018 2/5/2018 18-02001 i Strontium-90 EIChroM SRW01 Modified !

5.76E-01 4.50E-01 4.93E-01 7.32E-01 u

pCi/g 18-02001-06 i TRG B1021101FIFC008CV 01/31/18 10:12

2/1/2018 2/5/2018 18-02001 i Strontium-90 EIChroM SRW01 Modified !

8.11E-01 i

4.91E-01 i 5.66E-01 7.80E-01 pCi/g

~----,----*.

i j

18-02001-01 LCS KNOWN 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 '

Cobalt-60 EPA901.1 Modified 2.71E+02 1.06E+01 i pCi/g 18-02001-01 LCS KNOWN 02/01 /18 00:00 i 2/1/2018 2/1/2018 18-02001 ;

Cesium-137 EPA 901.1 Modified 1.69E+02 : 6.75E+OO i pCi/g 18-02001-01 LCS SPIKE 02/01/18 00:00

2/1/2018 2/1/2018 18-02001 '

Cobalt-60 EPA 901.1 Modified I

2.85E+02 1.76E+01 2.29E+01 2.08E+OO pCi/g 18-02001-01 i LCS SPIKE 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 !

Cesium-137 EPA901.1 Modified i

1.94E+02 3.21E+01 3.36E+01 2.34E+OO pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Norrnal Sample;DO=Duplicate Original;U=Non-detect

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SERVICES CAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 EBERLINE 865/481-0683 FAX 865/483-4621

[196]

Printed: 2/13/2018 8:53 AM Page 2 of 6 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02001 Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis

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101 Shiloh Blvd Analysis Category:

ENVIRONMENTAL

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so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result Report ID Type ID Date Date Date ID cu CSU MDA Qualifier Units 18-02001-02 MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 Actinium-228 EPA 901.1 Modified : -2.63E-01 '

3.12E-01 3.12E-01 3.26E-01 u

pCi/g

****---,,-,-*"-*-*-~--------""'"" _________,,_,,,-,,,,,--,----*----

18-02001-02 MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 Silver-108m EPA 901.1 Modified 3.85E-02 5.03E-02 5.03E-02 5.78E-02 u

pCi/g 18-02001-02 MBL BLANK 02/01 /18 00:00 2/1/2018 2/1/2018 18-02001 Americium-241 EPA 901.1 Modified

-1.46E-02 6.91E-02 6.91E-02 9.75E-02 u

pCi/g 18-02001-02 MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 Barium-133 EPA 901.1 Modified 1.32E-02 6.10E-02 6.10E-02 9.33E-02 u

pCi/g

~"----*----

18-02001-02 MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 Bismuth-214 EPA 901.1 Modified 1.72E-02 1.03E-01 1.03E-01 1.76E-01 u

pCi/g 18-02001-02 MBL BLANK 02/01 /18 00:00 2/1/2018 2/1/2018 18-02001,

Cobalt-60 EPA 901.1 Modified 3.95E-02 4.87E-02 4.88E-02 1.15E-01 u

i pCi/g

--*--*--*--**----~-----****-----------

18-02001-02 MBL BLANK 02/01/18 00:00 2/1/2018 '

2/1/2018 18-02001 Cesium-134 EPA 901.1 Modified 1.28E-03 6.45E-02 6.45E-02 9.29E-02 u

pCi/g

,,_.__ __,,m_, __,, ____,ow""

18-02001-02 MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 Cesium-137 EPA 901.1 Modified 4.53E-02 6.31E-02 6.31E-02 1.20E-01 u

pCUg

--~------

18-02001-02 MBL BLANK 02/01 /18 00:00 2/1/2018 2/1/2018 ' 18-02001 Europium-152 EPA 901.1 Modified

-5.14E-02 i

1.91E-01 1.91E-01 1.44E-01 u

pCi/g

*-**-'"':-"-****-*-*"-"'=--**-***---" --

18-02001-02 MBL BLANK 02/01/18 00:00

! 2/1/2018 2/1/2018 18-02001 r:=ui,,,,r--*~*11-154 EPA 901.1 Modified 2.16E-02 1.14E-01 1.14E-01 7.04E-02 '

u pCi/g 18-02001-02 MBL BLANK 02/01/18 00:00 ' 2/1/2018 2/1/2018 18-02001 LUl"'l"'~':1-EPA 901.1 Modified 5.98E-03 5.00E-02 5.00E-02 1.00E-01 u

pCi/g 18-02001-02 i MBL BLANK 02/01/18 00:00 ' 2/1/2018 2/1/2018 18-02001 ! Holmium-166m EPA 901.1 Modified 2.53E-02 1.06E-01 1.06E-01 6.81E-02 u

pCi/g 18-02001-02 MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 i lodine-129 EPA 901.1 Modified 6.95E-02 1.02E-01 1.03E-01 1.67E-01 u

pCi/g 18-02001-02 i MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 Potassium-40 EPA 901.1 Modified i

9.69E-02 '

1.90E-01 1.90E-01 7.13E-01 u

pCi/g

~------'.----

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18-02001-02 MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018, 18-02001 Manganese-54 EPA 901.1 Modified O.OOE+OO 6.80E-02 6.80E-02 1.06E-01 u

pCi/g 18-02001-02 ;

MBL BLANK 02/01/18 00:00 : 2/1/2018 2/1/2018 18-02001 Niobium-94 EPA 901.1 Modified

-3.07E-02 '

7.76E-02 7.76E-02 8.11E-02 u

pCi/g 18-02001-02 MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 i Lead-210 EPA 901.1 Modified 7.35E-01 : 7.13E-01 7.14E-01 1.22E+OO u

pCi/g

--*-**"'-*-----*-~--*,----*

18-02001-02 MBL BLANK 02/01/18 00:00 i

2/1/2018 2/1/2018 18-02001 Lead-212 EPA 901.1 Modified

-1.68E-02 : 6.19E-02. 6.20E-02 9.02E-02 u

pCi/g 10 -~=

00 18-02001 I MBL BLANK 02/01/18 00:00 '

2/1/2018 2/1/2018 Lead-214 EPA 901.1 Modified 9.50E-02 8.23E-02 8.24E-02 1.68E-01 u

pCi/g 18-02001-02,

MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018 1.3-02001_ ; n -***~:c*~:c:,-15 EPA 901.1 Modified

-8.51E-02 ! 9.21E-02 9.22E-02 1.22E-01 u

pCi/g 10 =~=

~: :

MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 Radium-226 EPA 901.1 Modified 1.72E-02 i

1.03E-01 1.03E-01 1.76E-01 u

pCi/g

--,=--

18-02001-02 MBL BLANK 02/01 /18 00:00 '

2/1/2018 2/1/2018 18-02001

~"""V"J 1£0 EPA 901.1 Modified 3.30E-02 1.07E-01 1.07E-01 1.91E-01 u

pCi/g 18-02001-02 MBL BLANK 02/01/18 00:00 '

2/1/2018 2/1/2018 18-02001 I Thorium-234 EPA 901.1 Modified 3.97E-01 6.07E-01 6.07E-01 1.00E+OO u

pCi/g 18-02001 :

i 18-02001-02 i MBL BLANK 02/01/18 00:00 '

2/1/2018 2/1/2018 Thallium-208 EPA901.1 Modified 2.72E-02 1.67E-01 1.67E-01 2.79E-01 u

pCi/g 18-02001-02 :

MBL BLANK 02/01/18 00:00 2/1/2018 2/1/2018 18-02001 :

Uranium-235 EPA 901.1 Modified

4.56E-01 i

5.82E-01 5.82E-01 3.46E-01 u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect EBERLINE Al YT!CAL CORPORATION r---------------

601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[197]

Printed: 2/13/2018 8:53 AM Page 3 of 6 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02001 Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis c

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so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 18-02001-03 DUP 81021101FIFC005CV 01/31/18 09:00 2/1/2018 : 2/1/2018 18-02001 Actinium-228 EPA 901.1 Modified i

-4.81E-01 2.41E+OO 2.41E+OO 3.52E+OO u

pCi/g

-fo-ULUU t-03 DUP 8102110IFIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 Silver-108m EPA901.1 Modified 1.35E+OO 7.68E-01 7.72E-01 5.69E-01 u

pCi/g 18-02001-03 :

DUP 8102110IFIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 Americium-241 EPA901.1 Modified i

4.48E-01 5.57E-01 5.57E-01 8.59E-01 u

pCi/g

__________________,,_, _____, __,,,, ___,,,_. _____ ~*-**----**

i pCi/g 18-02001-03 :

DUP 8102110IFIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 8arium-133 EPA 901.1 Modified

-1.10E-02 6.57E-01 6.57E-01 8.51E-01 u

,,,,m~"----**----------.,,,,,.,,,,m,~-*----'"'~"".'"'-"_"_,o,-----**

18-02001-03 DUP 8102110IFIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 8ismuth-214 EPA 901.1 Modified 8.63E-01 1.07E+OO 1.07E+OO 1.78E+OO u

pCi/g 18-02001-03 :

DUP B1021101FIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 Cobalt-60 EPA 901.1 Modified 7.89E+OO 8.15E-01 9.10E-01 6.71E-01 pCi/g 18-02001-03 DUP 8102110IFIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 Cesium-134 EPA 901.1 Modified 2.13E-01 4.30E-01 4.30E-01 8.41E-01 u

pCi/g

~-----~-------*-*-----*------

18-02001-03 DUP 81021101FIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 Cesium-137 EPA 901.1 Modified 4.22E+OO 1.12E+OO 1.14E+OO 1.34E+OO pCi/g 18-02001-03 DUP 81021101FIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001

  • Europium-152 EPA 901.1 Modified 1.61E+02 i

8.83E+OO 1.21E+01 3.53E+OO pCi/g 18-02001-03 DUP 810211 OIFIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 ;

!=cc.;'c::: 15-.

EPA 901.1 Modified

4.32E+OO :

1.41E+OO 1.42E+OO 2.71E+OO u

pCi/g DUP 8102110IFIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 1 !=cc '"'c::: 155 EPA 901.1 Modified 3.23E-01 i

9.48E-01 9.48E-01 1.42E+OO u

pCi/g

,---"----~-------

18-02001-03 :

DUP 81021101FIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 Holmium-166m EPA 901.1 Modified 1.01E+OO i

1.16E+OO 1.17E+OO 6.81E-01 u

pCi/g

    • -------~---*

18-02001-03 DUP 8102110IFIFC005CV 01/31/18 09:00 2/1/2018 : 2/1/2018, 18-02001 lodine-129 EPA 901.1 Modified 9.24E-01 2.56E-01 2.60E-01 4.23E-01 u

pCi/g 18-02001-03 DUP i

81021101FIFC005CV 01/31/18 09:00 i 2/1/2018 2/1/2018 18-02001,

Potassium-40 EPA 901.1 Modified 1.13E+01 i

4.24E+OO 4.28E+OO 8.19E+OO u

pCi/g 18-02001-03 i DUP 8102110IFIFC005CV 01/31/18 09:00 : 2/1/2018 2/1/2018 18-02001

~.~""M""""'"""" !5.A EPA 901.1 Modified

-6.28E-01 !

6.83E-01 6.84E-01 9.41E-01 u

pCi/g 18-02001-03 DUP 81021101FIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 Niobium-94 EPA901.1 Modified

-2.24E+OO,

1.21E+OO 1.22E+OO 9.03E-01.

u pCi/g 18-02001-03 DUP B102110IFIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 :

Lead-210 EPA 901.1 Modified 1.83E+02 1.69E+01 1.93E+01 1.49E+01 pCi/g 18-02001-03 :

DUP 8102110IFIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 Lead-212 EPA 901.1 Modified 6.28E-01 9.17E-01 9.18E-01 1.11E+OO u

pCi/g 18-02001-03 '

pCi/g DUP 81021101FIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 Lead-214 EPA 901.1 Modified 6.42E-01 : 1.19E+OO 1.19E+OO 1.46E+OO u

18-02001-03 DUP 8102110IFIFC005CV 01/31/18 09:00 2/1/2018 2/1/2018 18-02001 Promethium-145 EPA 901.1 Modified

-5.65E+01 i

4.56E+OO 5.40E+OO 1.55E+OO u

pCi/g 18-02001-03 :

DUP 8102110IFIFC005CV 01/31/18 09:00 i 2/1/2018 2/1/2018 18-02001 '

Radium-226 EPA901.1 Modified i

8.63E-01 i

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[198]

Printed: 2/13/2018 8:53 AM Page 4 of 6 Report To:

Work Order Details:

J Alex Bohacheff SDG:

18-02001 Eberline Analytical Final Report of Analysis

_____ Zion Solutions,_ LLC Purchase Order:

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pCi/g EPA 901.1 Modified 1.06E+OO 7.49E-01 7.51E-01 6.26E-01 U

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[199]

Printed: 2/13/2018 8:53 AM Page 5 of 6 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02001 Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis

--~~---

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101 Shiloh Blvd Analysis Category:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

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[200]

Printed: 2/13/2018 8:53 AM Page 6 of 6 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02001 f*

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2/1/2018 2/1/2018 18-02001 Lead-214 EPA 901.1 Modified 2.06E+OO 7.72E-01 7.79E-01 2.74E+OO u

pCi/g 18-02001-06 :

TRG 8102110IFIFC008CV 01/31/18 10:12 : 2/1/2018 : 2/1/2018 18-02001 ! Promethium-145 EPA 901.1 Modified 2.54E+OO 1.39E+OO 1.40E+OO 1.85E+OO u

pCi/g

~02001-06 I i

TRG 8102110IFIFC008CV 01/31/18 10:12 2/1/2018 2/1/2018 18-02001 Radium-226 EPA 901.1 Modified 1.03E+OO 8.51E-01 8.52E-01 1.42E+OO u

pCi/g 18-02001-06 TRG 81021101FIFC008CV 01/31/18 10:12

2/1/2018 2/1/2018 18-02001 EPA901.1 Modified 9.33E-01 9.98E-01 1.00E+OO 1.62E+OO u

pCi/g

-,,..,.,v.,,,~o 02001-06 :

TRG 81021101FIFC008CV 01/31/18 10:12 2/1/2018 2/1/2018 18-02001 Thorium-234 EPA 901.1 Modified 7.40E+OO 5.74E+OO 5.76E+OO 8.09E+OO u

pCi/g

=-*----~~--*---------

18-02001-06 :

TRG 81021101FIFC008CV 01/31/1810:12 2/1/2018 2/1/2018 18-02001 Thallium-208 EPA901.1 Modified 7.91E-02 1.33E+OO 1.33E+OO 1.68E+OO u

pCi/g 18-02001-06 '

TRG 8102110IFIFC008CV 01/31/18 10:12 2/1/2018 2/1/2018 18-02001 '

Uranium-235 EPA 901.1 Modified

-5.02E-02 4.07E+OO 4.07E+OO 2.67E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect

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SERViCES I i EBERLINE ANALYTICAL CORPORA T!ON I 601 SCARBORO ROAD OAK RIDGE, TN 7-83-0--8-6-5/_4_8_1--0-6_8_3 __

F_A_X_8_65/483-4621

[201]

ZIOr~SOLUTIONSiu Sample ID Sample Matrix Log B102110IFIFC005CV NIA Concrete Bl02110IFIFC006CV NIA Concrete B102110IFIFC008CV NIA Concrete Laboratory:

Eberline Labs Relinquished by:

J. ALEX BOHACHEFF Relinquished by:

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Relinquished by:

Relinquished by:

Comments ANALYSIS 5 ROC-HTD RE: Email to Mike McDougall PRIORITY 24 hour2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> turnaround PO# 677118 RECD fEB O 1 2018 - Chain-of-Custody Form 1a-02001 Sample Sample Container Sample Date Sample Time Analysis Preservative Type Vol Unit Type Qty Type Concrete 57.94 cm3 Puck l

1/31/2018 0900 HTD None Concrete 57.94 cm3 Puck l

1/31/2018 0935 HTD None Concrete 57.94 cm3 Puck l

1/31/2018 1012 HTD None Date Submitted To Lab:

Ship Container No.:

Cooler Temperature:

Airbill Number:

NIA NIA Date Time:

Received by:

Date: (nun/dd/yyyy):

( nun/dd/yyyy):

1-=?1-ri /J./.':?f 1rJJa n+ fr JZ/cktr 'I OJ /3/ / 7.0f'&

Date Time:

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Date: (1mri/dd/yyyy):

(m1n/dd/yyyy):

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OJ/31/20/x

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Date Time:

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(1mn/dd/yyyy):

J.-1-/g' Date Time: ~

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Date: (nun/dd/yyyy):

(mm/ddlyyyy):

ZS-WM-131 Revision 0 Information Use Remarks 0.0"-0.5" 0.0"-0.5" 0.0"-0.5" Time:

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[202]

BERLINE EBS-OR-43352 February 13, 2018 Alex Bohacheff Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099 SAMPLE RECEIPT SERVICES CASE NARRATIVE Work Order# 18-02009-0R EBERLINE ANALYTICAL CORPORATIOf\\1 601 SCARBORO ROAD OAK RIDGE, TENNESSEE :57830 PHONE (865) 481-068:5 FAX (865) 483-4621 This work order contains thirteen solid samples received 02/02/2018. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.

CLIENT ID Bl021 l01FIWC001CV B 102110IFIWC003CV B 102110IFIWC004CV B 10211 OFIFC003CV B 10211 OFIFC021 CV Bl02110FIWC015CV B 102110FIWC017CV ANALYTICAL METHODS LAB ID 18-02009-04 18-02009-05 18-02009-06 18-02009-07 18-02009-08 18-02009-09 18-02009-10 CLIENT ID B102110FIWC019CV B 10211 OFIWC020CV Bl02110FIWC014CV B102l 10FIWC018CV B102l l0FIWC0l6CV Bl02l l0IFIWC019CV LAB ID 18-02009-11 18-02009-12 18-02009-13 18-02009-14 18-02009-15 18-02009-16 Total Strontium was analyzed using EIChroM Method SRWOl Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.

Gamma Spectroscopy was performed using EPA Method 901. 1 Modified.

Laboratory qualifiers are as follows:

U - Result is less than the MDA.

ANALYTICAL RESULTS Combined Standard Uncertainty is reported at 2-sigma value.

Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific.

MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.

Page 1 of 3

[203]

ANALYTICAL RESULTS CONTINUED TOT AL STRONTIUM Samples were prepared by aliquoting as appropriate and leaching in HN03* Samples were diluted appropriately. Strontium recovery carriers were added to each sample. Chemical separations were conducted using selective extractions. Strontium precipitate was mounted on tared filter media. Chemical recovery was determined by Strontium carrier mass determinations. Samples were counted by gas flow propmtional counting and corrected for Yttrium-90 ingrowth.

Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are repmted from Total Strontium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.

TRITIUM A representative aliquot of each sample was equilibrated with Tritium free water. Equilibrates were transferred into round-bottomed distillation flasks and attached to single stage stills. A portion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were then counted by beta liquid scintillation.

Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.

NICKEL-63 A representative aliquot of each sample was leached in HN03* Leachates were placed in an appropriately sized beaker. Stable elemental Nickel carrier was added to each sample prior to digestion. Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.

Samples demonstrated acceptable results for all Nickel-63 analyses. All results demonstrated slightly high method detection limits. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated a high relative percent difference and normalized difference. Results for the duplicate sample were biased positive because of chemical interferences. Due to this condition only results from the duplicate original sample should be used for all intents and purposes. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.

GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass/aliquot of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.

Page 2 of 3

[204]

ANALYTICAL RESULTS CONTINUED GAMMA SPECTROSCOPY CONTINUED Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. Some results demonstrated slightly high method detection limits. Some sample results are greater than the method detection limits. These results are rep01ted from the Canberra Gamma Apex "Nuclide MDA Report" and are not positive. These results are qualified as non-detect (U). The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Cobalt-60, Cesium-137 and Europium-152 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.

CERTIFICATION OF ACCURACY I ce1tify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her designee to be ccu ate as verified by the following signature.

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,..... -~ -10 M.R. McDougall Laboratory Manage!"

Date: 2/13/2018 Eberline /\\nalytieal wants and encourages your feedback regarding our performance providing radioanalytieal services. Please visit http://eberlineanalytical.com/ to provide us with i'eedback on our services.

Page 3 of 3

[205]

Printed: 211312018 8:54 AM Page 1 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009 Zion Solutions, LL~_

Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 18-02009-01 LCS KNOWN 02/02/18 00:00

2/2/2018 2/5/2018 18-02009 Tritium LANL ER-210 Modified 226E+02 :

8.14E+OO pCi/g

,------------------,~-------s,~,_-m, ________ '"""

18-02009-01 LCS SPIKE 02/02/18 00:00 212/2018 21512018 18-02009 Tritium LANL ER-210 Modified. 2.17E+02 7.97E+OO 1.45E+01 5-53E+OO pCilg

,__,o_,_,m, ___,_,,,_,~--------*

18-02009-02 MBL BLANK 02102/18 00:00 21212018 21512018 18-02009 Tritium LANL ER-210 Modified

-U2E+OO 3.04E+OO 3.04E+OO 5.36E+OO u

pCi/g 18-02009-03 :

DUP B102110IFIWC001CV 01/31118 13:20 2/2/2018 2/512018 18-02009 Tritium LANL ER-210 Modified 8.78E+01 1-61E+01 1-69E+01 227E+01 pCilg

-10 """"" l"\\A l

DO B102110IF1WC001CV 01131/1813:20 212/2018 21512018 18-02009 Tritium LANL ER-210 Modified i

8-33E+01 1.63E+01 UOE+01 2.33E+01 pCi/g 18-02009-05 TRG B102110IF1WC003CV 01/31/18 13:55

' 212/2018 2/5/2018 18-02009 ;

Tritium LANL ER-210 Modified 1-13E+02 1.48E+01 1.61E+01 1.92E+01 pCi/g an M

TRG B102110IFIWC004CV 01131118 14:20

212/2018 21512018 18-02009 Tritium LANL ER-210 Modified 120E+02 U7E+01 1-89E+01 2-37E+01 pCi/g 18-02009-07 TRG B102110FIFC003CV 01131118 12:37 2/212018 2/512018 18-02009 :

Tritium LANL ER-210 Modified 1-69E+02 2.04E+01 I

2.25E+01 2.59E+01 pCi/g 18-02009-08 TRG 610211 OFIFC021 CV 01/31/18 13:00 j 2/2/2018 2/5/2018 18-02009 :

Tritium LANL ER-210 Modified 129E+02 1 -88E+01 2.01E+01 2.52E+01 pCilg 18-02009 I

18-02009-09 TRG B102110FIWC015CV 01/31/18 14:43 2/2/2018 2/5/2018 Tritium LANL ER-210 Modified 122E+02 1-62E+01 U5E+01 2.11E+01 pCi/g

~--------

18-02009-10 l TRG B102110F1WC017CV 01/31/18 15:07 i 2/2/2018 2/5/2018 18-02009 Tritium LANL ER-210 Modified 121E+02 1.52E+01 1.67E+01 1.95E+01 pCi/g 18-02009-11 TRG B102110FIWC019CV 01/31/18 15:30 i 2/2/2018 2/5/2018 18-02009 '

Tritium LANL ER-210 Modified 3.86E+02 i 2.19E+01 3.08E+01 2.02E+01 pCi/g 18-02009-12 TRG B102110FIWC020CV 02/01/18 08:12 ! 2/2/2018 2/5/2018 18-02009 Tritium LANL ER-210 Modified 228E+02 2.33E+01 : 2.66E+01 2.80E+01 pCi/g 18-02009-13 I

TRG B102110FIWC014CV 02/01/18 08:56 ! 2/2/2018 2/512018 18-02009 Tritium LANL ER-210 Modified 1-52E+02 1.94E+01 2.12E+01 2.50E+01 pCilg 18-02009-14 :

TRG I

B102110FIWC018CV 02101118 09:38 / 21212018 21512018 18-02009 Tritium LANL ER-210 Modified 1.52E+02 1.82E+01 2.01E+01 2.31E+01 pCi/g

-15 TRG B102110FIWC016CV 02/01/18 10:00 i 21212018 : 2/5/20 i8 18-02009 '

Tritium LANL ER-210 1.53E+01 1.64E+01 2.05E+01 pCi/g 18-02009-16 TRG B102110IFIWC019CV 02/01/18 2/2/2018 ' 2/5/2018 18-02009 Tritium LANL ER-210 Modified ; 2.46E+02 2.14E+01 '

2.55E+01 2.42E+01 pCi/g

__,,_ *,,,,,__,,,,,,_,,,_, __ m*=-*-*--'~*-*--***

18-02009-01 :

LCS KNOWN 02/02/18 00:00 : 2/2/2018 : 2/5/2018 18-02009 :

Nickel-63 ASTM 3500-Ni Modified ;

1.49E+03 :

4.46E+01 pCilg 18-02009-01 i

LCS SPIKE 02/02/18 00:00

2/2/2018 2/5/2018 18-02009 Nickel-63 ASTM 3500-Ni Modified 1.45E+03 9.42E+OO 8.55E+01 2.26E+OO pCi/g 18-02009-02 MBL BLANK 02/02/18 00:00 2/2/2018, 2/5/2018 18-02009 f Nickel-63 ASTM 3500-Ni Modified

-4.88E-01 1.36E+OO 1.36E+OO 2.35E+OO u

pCi/g 18-02009-03 !

DUP B102110IF1WC001CV 01/31/18 13:20

2/2/2018 2/5/2018 18-02009 Nickel-63 ASTM 3500-Ni Modified '

3.36E+OO 5.32E+OO :

5.32E+OO 8.98E+OO u

i pCi/g 18-02009-04 i DO B102110IFIWC001CV 01/31/18 13:20 2/2/2018 ' 2/5/2018 18-02009 '

Nickel-63 ASTM 3500-Ni Modified : 3.36E+OO i 5.32E+OO 5.32E+OO 8.98E+OO u

pCi/g

,x.<1,0

  • ~ i B102110IFIWC003CV 01/31/18 13:55 i 2/2/2018 2/5/2018 18-02009 '

Nickel-63 ASTM 3500-Ni Modified i 2.83E+01 5.29E+OO 5.55E+OO 8.02E+OO pCi/g 18-02009-06 TRG B102110IF1WC004CV 01/31/18 14:20 : 2/2/2018 2/5/2018 18-02009 Nickel-63 ASTM 3500-Ni Modified 1.62E+01 4.90E+OO 4.99E+OO 7.78E+OO pCi/g 18-ULUU~-07 ;

TRG B102110FIFC003CV 01/31/18 12:37 2/2/2018 2/5/2018 18-02009 Nickel-63 ASTM 3500-Ni Modified 3.11E+OO 5.53E+OO 5.54E+OO 9.36E+OO u

pCi/g n

Mi TRG B102110FIFC021CV 01/31/18 13:00 : 2/2/2018 2/6/2018 18-02009 Nickel-63 ASTM 3500-Ni Modified :

4.27E+OO 5.09E+OO 5.10E+OO 8.56E+OO u

pCi/g

-*~---~--.---

18-02009-09 ;

TRG B102110FIWC015CV 01/31/18 14:43 2/2/2018 2/6/2018 18-02009 :

Nickel-63 ASTM 3500-Ni Modified 6.91E+OO i 5.00E+OO 5.02E+OO 8.31E+OO u

pCi/g 18-02009-10 '

TRG B102110FIWC017CV 01/31/1815:07 2/2/2018 2/6/2018 18-02009 Nickel-63 ASTM 3500-Ni Modified

-8.12E-01 5.68E+OO 5.68E+OO 9.76E+OO u

pCi/g 18-02009-11 TRG B102110FIWC019CV 01/31/18

2/2/2018 2/6/2018 18-02009 Nickel-63 ASTM 3500-Ni Modified 9.28E+OO 5.64E+OO 5.66E+OO 9.30E+OO u

pCi/g 18-02009-12 :

i TRG B 10211 OFIWC020CV 02/01/18 08:12 ! 2/2/2018 2/6/2018 18-02009 Nickel-63 ASTM 3500-Ni Modified 1.51E+01 5.52E+OO 5.59E+OO 8.88E+OO pCi/g 18-02009-13 '

TRG B102110F1WC014CV 02/01/18 08:56 i 2/2/2018 2/6/2018 18-02009 '

Nickel-63 ASTM 3500-Ni Modified : 5.61E+OO 4.76E+OO 4.77E+OO 7.94E+OO u

pCi/g 18-02009-14 i TRG i

B102110FIWC018CV 02/01/18 09:38

2/2/2018 2/6/2018 18-02009 Nickel-63 ASTM 3500-Ni Modified 3.75E+OO 5.94E+OO 5.94E+OO 1.00E+01 u

pCi/g

,,=*-,,---------

18-02009-15 TRG B102110FIWC016CV 02/01/18 10:00

' 2/2/2018 2/6/2018 18-02009 Nickel-63 ASTM 3500-Ni Modified O.OOE+OO 5.57E+OO 5.57E+OO 9.54E+OO u

pCi/g

~-~-~---------

18-02009-16 TRG B102110IF1WC019CV 02/01/18 10:38 2/2/2018 2/6/2018 18-02009 Nickel-63 ASTM 3500-Ni Modified 3.69E+OO 5.27E+OO :

5.27E+OO 8.88E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE AL YTICAL CORPOR.ATION

' 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[206]

Printed: 2/13/2018 8:54 AM Page 2 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009 Zion Solutions, LLC......

Purchase Order:.

677118 Final Report of Analysis

--,c~

101 Shiloh Blvd Analvsis c~::;;;:;.

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch i

Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID i

Units 18-02009-01 LCS KNOWN 02/02/18 00:00 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified 5.36E+01 3.00E-01 pCi/g i----*--*--*--*

18-02009-01 SPIKE 02/02/18 00:00 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified 5.75E+01 2.36E+OO 2.02E+01 1.08E+OO pCi/g

----- f------

"*"-~"-----------*---~-----------,

18-02009-02 MBL BLANK 02/02/18 00:00 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified 5.75E-01 5.38E-01 5.74E-01 8.90E-01 u

pCi/g

  • -- I-18-02009-03 DUP 8102110IFIWC001CV 01/31/1813:20 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified

-6.26E-02. 4.09E-01 4.10E-01 7A2E-01 u

pCi/g

--"'------- """"""'-----------------------~ -------*------

,,, ________,.,,. ______________.,_,~,,-----*--

18-02009-04 DO B102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified :

4.72E-01 3.75E-01 4.09E-01 6.09E-01 u

pCi/g

-~--*----------------*------------,----*""'"'"'

18-02009-05 TRG 8102110IFIWC003CV 01/31/1813:55 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified 5.50E-01 4.14E-01 4.57E-01 6.72E-01 u

pCi/g 1----------------~---------,,--_., ___________,,, _______________ --*-,,,, ___________,,__,, ___ ~------------

---~

18-02009-06 TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified 6.88E-01 5.02E-01. 5.56E-01 8.15E-01 u

pCi/g F""""'-~--------~ -----

, --------------*-----*~_,,,_;_, _____ ~--------*,----*,--", __..........,: ____

18-02009-07 TRG B102110FIFC003CV 01/31/18 12:37 2/2/2018 2/6/2018 18-02009 ;

Strontium-90 EIChroM SRW01 Modified 2.09E-01 5.09E-01 5.14E-01 8.86E-01 u

pCi/g 18-02009-08 :

TRG 8102110FIFC021CV 01/31/18 13:00 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified i 6.83E-01 4.51E-01 5.10E-01 7.18E-01 u

pCi/g

  • ---m=,_,,,

'.--*--*-"==---*----*=------*-'""*=--*------*---* ~ r----*---w.--m,,_ * '""'

_______,,,,, _____ ~ ___,,,_

18-02009-09 TRG 8102110FIWC015CV 01/31/18 14:43 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified :

4.50E-01 4.42E-O 4.69E-01 7.35E-01 u

pCi/g 18-02009-10 TRG 8102110FIWC017CV 01/31/1815:07 2/2/2018 2/6/2018 18-02009 :

Strontium-90 EIChroM SRW01 Modified 5.13E-01 4.98E-01 5.29E-01 8.27E-01 u

pCi/g

--**-----*~

18-02009-11 TRG 8102110FIWC019CV 01/31/18 15:30 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified 9.00E-01 i 4.96E-01 5.87E-01 7.74E-01 pCi/g B 10211 OFIWC020CV 02/01/18 08:12 2/2/2018 2/6/2018 18-02009 '

Strontium-90 EIChroM SRW01 Modified 5.64E-01 :

4_16E-01 4.60E-01 6.72E-01 u

pCi/g 18-02009-13 TRG B102110FIWC014CV 02/01/18 08:56 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified 3.55E-01 4.39E-01 4.56E-01 7.41E-01 u

pCi/g 18-02009-14 ;

TRG 8102110FIWC018CV 02/01/18 09:38 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified 4.56E-01 4.55E-01 4.81E-01 7.57E-01 u

pCi/g

~--

18-02009-15 '

TRG 8102110FIWC016CV 02/01 /18 10:00 2/2/2018 2/6/2018 18-02009 Strontium-90 EIChroM SRW01 Modified 5.59E-01 : 5.06E-01 5.42E-01 8.35E-01 u

pCi/g 18-02009-16 TRG 81021101FIWC019CV 02/01/18 10:38 2/2/2018 2/6/2018 18-02009 i Strontium-90 EIChroM SRW01 Modified 1.77E-01 4.90E-01 4.93E-01 8.54E-01 u

pCi/g l

*-----~------*------

18-02009-01 LCS KNOWN 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 Cobalt-60 EPA 901.1 Modified 2.71E+02 1.06E+01 pCi/g 18-02009-01 LCS KNOWN 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 :

Cesium-137 EPA 901.1 Modified 1.69E+02 6.75E+OO pCi/g an na LCS SPIKE 02/02/18 00:00 2/2/2018 2/2/2018 18-02009,

Cobalt-60 EPA 901-1 Modified 2.89E+02 1.78E+01 2.32E+01 2.27E+OO pCi/g 18-02009-01 LCS SPIKE 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 Cesium-137 EPA 901.1 Modified 1.91E+02 3.15E+01 3_30E+01 2,33E+OO pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE ALYT!CAL ON 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/ 481-0683 FAX 865/483-4621

[207]

Printed: 2/13/2018 8:54 AM Page 3 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SOG:

18-02009

_____ Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis

--* ""-'"'"-,-~---

101 Shiloh Blvd Analysis Category:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU Qualifier Report ID Type ID Date Date Date ID MDA Units 18-02009-02 MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 Actinium-228 EPA 901-1 Modified 5AOE-02 1AOE-01 1AOE-01 2A2E-01 u

pCi/g

,---*-----'---------~------------

18-02009-02 MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 00,v~, *,uoH, EPA901.1 Modified

-3A6E-02 5A2E-02 i 5A2E-02 4.97E-02 u

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__________,,;; ___________ ~""'"" _____

  • ----------~-----*------- '""" __,_,, ____

18-02009-02 MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 Americium-241 EPA 901. 1 Modified

-3A2E-03 1.56E-02 1.56E-02 6.45E-02 u

pCi/g

  • --*-s----- ---~

18-02009-02 '

MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 Barium-133 EPA 901.1 Modified

-1A9E-02 4.28E-02 4.28E-02 6.27E-02 u

pCi/g

~------*-----*------------- ----------- ____

, ____,,,,,,,,=-*--

18-02009-02.

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Bismuth-214 EPA 901. 1 Modified 4.35E-02 8A1E-02 8A1E-02 1A5E-01 u

pCi/g

-~---

18-02009-02 :

MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 Cobalt-60 EPA 901. 1 Modified. -1.88E-02 4.67E-02 4.67E-02 5.14E-02 u

pCi/g

,-----~_,, ________ ----------.........,;--

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18-02009-02 '

MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 Cesium-134 EPA901.1 Modified

-1.08E-02 4.30E-02 '

4.30E-02 6.30E-02 u

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,m_,e_, _____

V _______

,-------,-,-------~---*-

18-02009-02 MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 Cesium-137 EPA 901. 1 Modified 4A4E-02. 3.81E-02 3.82E-02 7A8E-02 u

pCi/g 18-02009-02

  • MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009,
u, -,*-* "- i 52 EPA 901.1 Modified i

4.66E-02 1.25E-01 1.25E-01 1.12E-01 u

pCi/g

-10 "'-'"'"'"' fVl MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009

~~.-,.~:- 154 EPA 901. 1 Modified i

-9.79E-02 : 1.13E-01 1.13E-01 5.91E-02 u

pCi/g 18-02009-02 !

MBL BLANK 02/02/18 00:00. 2/2/2018 2/2/2018 18-02009 Europium-155 EPA 901.1 Modified

. -2.76E-02. 3A7E-02 3A7E-02 6A3E-02 u

pCi/Q

,--~--

18-02009-02

  • MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 Holmium-166m EPA 901. 1 Modified

! -3.89E-02 9.36E-02 9.37E-02 4.28E-02 u

pCi/g 18-02009-02 :

MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 i lodine-129 EPA 901.1 Modified

/

1.60E-02 6.74E-02. 6.74E-02 1.04E-01 u

pCi/g 18-02009-02 MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 Potassium-40 EPA 901. 1 Modified I -4.04E-03 :

3.14E-01 3.14E-01 5.82E-01 u

pCi/g 18-02009 ; iL..,_.. ___ '

i pCi/g 18-02009-02 ;

MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 EPA 901.1 Modified 1A3E-02 '

3.96E-02 3.96E-02 6.59E-02 '

u

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MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 i Niobium-94 EPA 901.1 Modified 6.20E-03 1.54E-02 1.54E-02 6.22E-02 u

pCi/g 18-ULUW-02 /

MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 i Lead-210 EPA901.1 Modified 2.46E-01 4.79E-01 4.79E-01 7A8E-01 u

pCi/g

-~------,

18-02009-02 MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009,

Lead-212 EPA 901.1 Modified

. 4.56E-02 4.61E-02 4.61E-02 7.93E-02 u

pCi/g 18-02009-02 MBL BLANK 02/02/18 00:00 : 2/2/2018 2/2/2018 18-02009

  • Lead-214 EPA901.1 Modified 1.65E-03 6.78E-02 6.78E-02 1.06E-01 u

pCi/g 18-02009-02 :

MBL BLANK 02/02/18 00:00 2/2/2018

  • 2/2/2018 18-02009 ; Promethium-145 EPA 901.1 Modified i

5.17E-03 6.62E-02.

6.62E-02 1.01E-01.

u pCi/g 18-02009-02 i MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 '

Radium-226 EPA 901. 1 Modified

4.35E-02 8.41E-02 8A1E-02 1A5E-01.

u pCi/g 18-02009-02 MBL BLANK 02/02/18 00:00. 2/2/2018 2/2/2018 18-02009 '

Antimony-125 EPA 901. 1 Modified i

7.14E-03 4.55E-02 4.55E-02 1.SOE-01 u.

pCi/g

~----i 18-02009 i 18-02009-02 MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 Thorium-234 EPA 901.1 Modified 4.65E-01 '

4A5E-01 4A6E-01 7.29E-01 u

pCi/g 18-02009-02 :

MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02Q09 i Tham,*- OM EPA 901. 1 Modified 6.76E-02 1.07E-01 1.07E-01 1.93E-01 u

pCi/g 18-02009-02 ;

MBL BLANK 02/02/18 00:00 2/2/2018 2/2/2018 18-02009 Uranium-235 EPA 901.1 Modified 1.06E-01 3A1E-01 i

3A1E-01. 2.33E-01 u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect I

I EBERLINE ANALYTICAL CORPOR1~ TION I 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[208]

Printed: 2/13/2018 8:54 AM Page 4 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009 Zion. Solutions, LLC Purchase Order:

677118 Final Report of Analysis

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101 Shiloh Blvd Analysis

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ENVIRONMENTAL

.... '.":',[';!..!.:..

Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis '

Batch Analyte Report Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 18-02009-03 DUP 81021101FIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Actinium-228 EPA901.1 Modified 7.76E-01 1.91E+OO 1.91E+OO 3.18E+OO u

pCiiQ r-""'----*-*------~-...,....,----

18-02009-03 DUP B102110IFIWC001CV 01/31/18 13:20 2/2/2018 21212018 18-02009 Silver-108m EPA901.1 Modified 7.85E-01 6.43E-01 6.45E-01 6.01E-01 u

pCi/g

"-"v---,---* -*-*-------* ---------*-*-----,--,--------- ""'--

18-02009-03 DUP B102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Americium-241 EPA901.1 Modified

-1.23E+OO 6.92E-01 6.95E-01 8.02E-01 u

pCi/Q 18-02009-03 :

DUP B102110IFIWC001CV 01/31/1813:20 2/212018 2/2/2018 18-02009,

Barium-133 EPA 901. 1 Modified

-2.32E+OO 7.14E-01 7.24E-01 8.14E-01 u

pCi/g

-~--~----*--------

18-02009-03 DUP 8102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Bismuth-214 EPA 901.1 Modified 6.42E-01 1.06E+OO 1.06E+OO 1.58E+OO u

pCi/Q

.. --*--*--------*'---*-~-*--------~------*----*--- --------,,,-----*------*-

      • ------*---------~------

18-02009-03 DUP 81021101FIWC001CV 01/31/18 13:20 2/2/2018 212/2018 18-02009 Cobalt-60 EPA 901.1 Modified

1.74E+01 1.22E+OO 1.51E+OO 8.80E-01 pCi/g

---.. ---.-------- m>>.-**""""-*"*-------------*----

18-02009-03 DUP 8102110IFIWC001CV 01/31/18 13:20 2/2/2018, 2/2/2018 18-02009 :

Cesium-134 EPA901.1 Modified

-8.82E-02 '

5.04E-01 5.04E-01 7.26E-01 u

pCi/Q 18-02009-03 OUP B102110IFIWC001CV 01/31/18 13:20 2/2/2018 18-02009 Cesium-137 EPA 901. 1 Modified 2.21E+OO 8.16E-01 8.24E-01 1.19E+OO pCi/g

_,_,,, ______..,,w, _____________,, ___ -

18-02009-03 DUP 81021101FIWC001CV 01/31/18 13:20 212/2018 2/2/2018 18-02009

c:c 0,_,,,. 152 EPA 901.1 Modified i

1.60E+02 i

7.25E+OO 1.10E+01 3.27E+OO pCi/Q

- ________.. ____,.... ____ -----"*----.. ~*------,----~----*--.. --*-*-

18-02009-03 DUP B1021101FIWC001CV 01/31/1813:20 2/2/2018 2/2/2018 18-02009 Europium-154 EPA 901. 1 Modified

6.57E+OO 1.46E+OO 1.50E+OO 2.58E+OO u

pCiig 18-02009-03 OUP 8102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 CC, --

155 EPA901.1 Modified l

1.33E+OO 9.25E-01 9.27E-01 1.47E+OO u

pCi/Q

--* *a*-*

18-02009-03 ;

DUP 81021101FIWC001CV 01/31/18 13:20 2/2/2018 '

2/2/2018 18-02009 Holmium-166m EPA 901.1 Modified

5.04E-01 9.40E-01 '

9.40E-01 5.18E-01 u

pCi/g 18-02009-03 DUP 8102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 :

lodine-129 EPA 901. 1 Modified 1.47E+OO 3.80E-01 3.87E-01 1.49E+OO u

pCiig 18-02009-03 DUP B102110IFIWC001CV 01/31/1813:20 2/2/2018 2/2/2018 ' 18-02009 Potassium-40 EPA 901.1 Modified i

5.06E+OO '

3.50E+OO 3.51E+OO 6.82E+OO u

pCi/g 18-02009-03 :

DUP 8102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 C

EPA 901.1 Modified

-5.95E-02 5.53E-01 5.53E-01 8.00E-01 u

pCiig 18-02009-03 DUP B102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Niobium-94 EPA 901. 1 Modified i

-1.52E+OO '

8.68E-01 8.71E-01 7.53E-01 u

pCi/g

. -..... ~-------------------*-----***------------*

18-02009-03 DUP B1021101FIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Lead-210 EPA 901.1 Modified 2.79E+02 2.37E+01 '

2.77E+01 1.88E+01 u

pCiig

~------*.. ---->--*

  • --~----------

18-02009-03 DUP 81021101FIWC001CV 01/31/18 13:20 2/2/2018 2/212018 18-02009 Lead-212 EPA 901. 1 Modified 4.21E-01 5.84E-01 5.85E-01 9.39E-01 u

pCi/g 18-02009-03 :

OUP B1021101FIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009,

Lead-214 EPA 901.1 Modified l 2.75E+OO 1.06E+OO 1.07E+OO 1.61E+OO u

pCi/g 18-02009-03 DUP B1021101FIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Promethium-145 EPA901.1 Modified 5.25E+OO 1.90E+OO 1.92E+OO 2.44E+OO u

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-*---.. =*-*----*-

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18-02009-03 DUP B102110IFIWC001CV 01/31/1813:20 2/2/2018 2/2/2018 18-02009 Radium-226 EPA 901.1 Modified 6.42E-01 1.06E+OO 1.06E+OO 1.58E+OO u

pCi/g 18-02009-03 OUP B1021101FIWC001CV 01/31/18 13:20 2/2/2018 212/2018 18-02009 Antimony-125 EPA 901.1 Modified

-4.83E-01 1.25E+OO 1.25E+OO 1.79E+OO u

pCiig 18-02009 i i

18-02009-03 DUP 8102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 Thorium-234 EPA 901.1 Modified 4.65E+OO 6.75E+OO 6.75E+OO 8.73E+OO u

pCi/g 18-02009-03 DUP B102110IFIWC001CV 01/31/18 13:20 i 2/212018 ' 2/2/2018 18-02009 '

Thallium-208 EPA 901.1 Modified i

1.67E+OO 1.65E+OO :

1.65E+OO 1.45E+OO u

pCi/g 18-02009-03 '

DUP 8102110IFIWC001CV 01/31/1813:20 2/2/2018 2/2/2018 18-02009 Uranium-235 EPA 901. 1 Modified

-3.06E-01 4.98E+OO 4.98E+OO 3.22E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

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EBERLINE

~

SERVJCES EBERUNE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[209]

Printed: 2/13/2018 8:54 AM Page 5 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SOG:

18-02009

..... Zion Solutions,_LLC -**-********-***

Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analvsis Category:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU Qualifier Report ID Type ID Date Date Date ID MDA Units 18-02009-04 DO 8102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Actinium-228 EPA 901.1 Modified

1.75E+OO 2.03E+OO 2.04E+OO 3.09E+OO u

pCi/g

...... f-18-02009-04 DO B102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Silver-108m EPA 901.1 Modified 7.08E-01 6.13E-01 6.14E-01 5.67E-01 u

pCi/g 18-02009-04 DO. 810211 OIFIWC001 CV 01/31/18 13:20. 2/2/2018 2/2/2018 18-02009 Americium-241 EPA901.1 Modified

-3.90E-01 6.47E-01 6.47E-01 7.99E-01 u

pCi/g 18-02009-04 DO 8102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Barium-133 EPA 901.1 Modified

-9.45E-02 2.72E-01 2.72E-01 8.08E-01 u

pCi/g

,,,,,,.,,,.a,,, __,,,,,,,,,,,"-**-*-*w* ______,,,_,,,,

18-02009-04 DO 8102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Bismuth-214 EPA 901.1 Modified 2.03E-01 1.01E+OO 1.01E+OO 1.48E+OO u

pCi/g 18-02009-04 DO 81021101FIWC001CV 01/31/1813:20 2/2/2018 2/2/2018 18-02009 Cobalt-SO EPA 901.1 Modified 1.51E+01 1.09E+OO 1.34E+OO 8.04E-01 pCi/g

,,,,,,.,,,,,,,,,,,,,, __,_,,,,,,,,,,_,,,,,, '"'""-~w---

1"-Mnna n DO 8102110IFIWC001CV 01/31/18 13:20 I 2/2/2018 2/2/2018 18-02009 Cesium-134 EPA901.1 Modified

-4.15E-01 4.87E-01 4.87E-01 6.74E-01 u

pCi/g

---** ----------*----***--~*-*---------------*

18-02009-04 DO 8102110IFIWC001CV 01/31/1813:20 2/2/2018

  • 2/2/2018 18-02009 Cesium-137 EPA 901.1 Modified 2.48E+OO 9.07E-01 9.16E-01 1.32E+OO I

pCi/g 18-02009-04 '

DO 8102110IFIWC001CV 01/31/18 13:20 2/2/2018 : 2/2/2018 18-02009 Europium-152 EPA 901.1 Modified 1.55E+02 6.36E+OO 1.02E+01 3.34E+OO pCi/g 18-02009-04 DO 81021101FIWC001CV 01/31/1813:20 2/2/2018 2/2/2018 18-02009 Europium-154 EPA901.1 Modified 6.87E+OO 1.44E+OO 1.48E+OO 2.55E+OO u

pCi/g ---

18-02009-04 DO 8102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Europium-155 EPA 901.1 Modified 9.86E-01 8.77E-01 8.78E-01 1.40E+OO u

pCi/g

-*------~---*-*-

18-02009-04

  • DO 81021101FIWC001CV 01131/18 13:20 : 2/2/2018 2/2/2018 18-02009 Holmium-166m EPA901.1 Modified 7.86E-01. 8.94E-01 8.95E-01 5.13E-01 u

pCi/g - *--

/"\\A DO 81021101FIWC001CV 01/31/1813:20

2/2/2018, 2/2/2018 18-02009 lodine-129 EPA 901.1 Modified 1.26E+OO 3.39E-01 3.45E-01 1.51E+OO u

pCi/g 18-02009-04 DO 81021101FIWC001CV 01/31/18 18-02009 Potassium-40 EPA 901.1 Modified 6.78E+OO 2.89E+OO 2.91E+OO 9.53E+OO u

pCi/g I

18-02009-04 DO 81021101FIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018, 18-02009 EPA 901.1 Modified

-5.69E-02 5.27E-01 5.27E-01 7.66E-01 u

pCi/g

... ---.--------~--

01/31/18 3:20 i

-1.81E+OO !

pCi/g 18-02009-04 DO B 10211 OIFIWC001 CV 2/2/2018 2/2/2018 18-02009 Niobium-94 EPA 901.1 Modified 8.53E-01 '

8.59E-01 7.18E-01 u

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pCi/g 18-02009-04 DO 8102110IFIWC001CV 01/31/1813:20 2/2/2018 2/2/2018 18-02009 Lead-210 EPA 901.1 Modified 2.40E+02 2.09E+01 2.43E+01 1.77E+01 u

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5.58E-01 8.95E-01 u

18-02009-04 '

DO 81021101FIWC001CV 01/31/18 1320 i 2/2/2018 2/2/2018 18-02009 Lead-214 EPA 901.1 Modified 2.00E+OO 8.77E-01 8.83E-01 1.64E+OO pCi/g 18-02009-04 DO 81021101FIWC001CV 01/31/18 13:20

2/2/2018 2/2/2018 18-02009 1 Promethium-145 EPA 901.1 Modified 4.33E+OO 1.79E+OO 1.80E+OO 2.29E+OO u

pCi/g 18-02009-04 :

DO 81021101FIWC001CV 01/31/18 13:20 I 2/2/2018, 2/2/2018 18-02009 Radium-226 EPA 901.1 Modified 2.03E-01 1.01E+OO 1.01E+OO 1.48E+OO u

pCi/g 18-02009-04 DO 8102110IFIWC001CV 01/31/1813:20 i 2/2/2018 : 2/2/2018 18-02009 Antimony-125 EPA 901.1 Modified

-1.20E-01 1.19E+OO 1.19E+OO 1.72E+OO u

pCi/g

  • n n

DO 81021101FIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Thorium-234 EPA 901.1 Modified

! 7.78E+OO 6.28E+OO : 6.30E+OO 8.33E+OO u

pCi/g

*,,,,,,~----

18-02009-04 l DO 8102110IFIWC001CV 01/31/18 13:20 2/2/2018 2/2/2018 18-02009 Thallium-208 EPA901.1 Modified

-1.99E-01 8.20E-01 8.20E-01 1.32E+OO u

pCi/g 18-02009-04 DO 8102110IFIWC001CV 01/31/1813:20 ' 2/2/2018 2/2/2018 18-02009 :

Uranium-235 EPA 901.1 Modified

-2.50E-01 4.85E+OO 4.85E+OO 3.16E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

(

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[210]

Printed: 2/13/2018 8:54 AM Page 6 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009 Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method cu Report ID Type ID Date Date Date ID Result CSU MDA Qualifier Units 18-02009-05 TRG 8102110IFIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18--02009 Actinium-228 EPA 901.1 Modified i

2.89E-01 1.33E+OO 1.33E+OO 1.98E+OO u

pCi/g 18-02009-05 TRG 81021101FIWC003CV 01/31/1813:55 2/2/2018 2/2/2018 18-02009 Silver-108m EPA 901.1 Modified 6.49E-01 4.28E-01 4.29E-01 4.35E-01 u

pCi/g

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18-02009-05,

TRG 8102110IFIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18-02009 Americium-241 EPA 901.1 Modified

-6.91E-02 3.21E-01 i

3.21E-01 4.68E-01 u

pCi/g 18-02009-05 TRG 81021101FIWC003CV 01/31/1813:55 2/2/2018 2/2/2018 18-02009 8arium-133 EPA 901.1 Modified

-1.64E-02

  • 4.21E-01 4.21E-01 5.37E-01 u

pCi/g

-**-------~---,_., ___________

m ___

m 18-02009-05 TRG 8102110IFIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18-02009 8ismuth-214 EPA 901.1 Modified 5.85E-01 7.19E-01 7.19E-01 1.20E+OO u

pCi/g 18-02009-05 TRG 8102110IFIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18-02009 Cobalt-60 EPA 901.1 Modified 4.85E+OO 4.77E-01 5.38E-01 4.42E-01 pCi/g

=------*

~--------------

18-02009-05 TRG 81021101FIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18-02009 Cesium-134 EPA 901.1 Modified

-1.91E-02 2.59E-01 2.59E-01 4.88E-01 u

pCi/g 18-02009-05 '

137 EPA 901.1 Modified "'"".-------*--""!-----

TRG 8102110IFIWC003CV 01/31/1813:55 2/2/2018 2/2/2018 18-02009 3.74E+01 5.90E+OO 6.20E+OO 8.62E-01 pCi/g

**------------~------,,m ___,_, ________ ------------------------------------,,,, ___

18-02009-05 TRG 81021101FIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18-02009 Europium-152 EPA 901.1 Modified 1.05E+02 5.49E+OO 7.70E+OO 2.06E+OO pCi/g 18-02009-05 '

TRG 810211 OIFIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18-02009 LUl~r--*-,11-154 EPA 901.1 Modified 3.88E+OO 9.23E-01 9.44E-01 1.68E+OO u

pCi/g 18-02009 i Europium-155 i

i 18-02009-05 :

TRG 810211 OIFIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 EPA901.1 Modified 1.22E+OO 8.83E-01 8.85E-01 1.42E+OO u

pCi/g 18-02009-05 TRG 81021101FIWC003CV 01/31/1813:55 2/2/2018 2/2/2018 18-02009 Holmium-166m EPA 901.1 Modified 6.60E-02 6.38E-01 6.39E-01 3.94E-01 u

oCi/g 18--02009-05 :

TRG 81021101FIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18-02009 ;

lodine-129 EPA 901.1 Modified 1.07E-01 1.83E-01 :

1.83E-01 2.46E-01 u

i pCi/g 18-02009-05 TRG B102110IFIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18-02009 Potassium-40 EPA 901.1 Modified i

6.76E+OO 1.97E+OO 2.00E+OO 5.06E+OO pCi/g 18-02009-05 /

TRG 810211 OIFIWC003CV 01/31/18 13:55

2/2/2018 : 2/2/2018 18-02009 ! ***-* *o-*.* ** '

EPA 901.1 Modified i 2.47E-01 3.45E-01 3.45E-01 5.25E-01 u

pCi/g 18-02009-05 :

TRG 8102110IFIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18-02009 '

Niobium-94 EPA 901.1 Modified i

-2.07E+OO !

6.89E-01 6.97E-01 5.00E-01 u

pCi/g 18--02009-05 :

TRG 81021101FIWC003CV 01/31/18 13:55 i 2/2/2018 2/2/2018 18-02009 Lead-210 EPA901.1 Modified 1.26E+02 1.06E+01 1.25E+01 8.17E+OO pCi/g 18-02009-05 :

TRG 81021101FIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18-02009 Lead-212 EPA901.1 Modified 4.36E-02 5.35E-01 5.35E-01 6.82E-01 u

pCi/g 18-02009-05 :

TRG B102110IF1WC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18-02009 i Lead-214 EPA 901.1 Modified 1.29E-01 7.13E-01 i

7.13E-01 9.02E-01 u

pCi/g 18-02009-05 TRG 810211 OIFIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 : 18-02009, Promethium-145 EPA 901.1 Modified

-3.87E+01 2.86E+OO 3.49E+OO 8.47E-01 u

oCi/Q

,N ______

18-02009-05 j TRG B1021101FIWC003CV 01/31/18 13:55 : 2/2/2018 2/2/2018 18-02009 Radium-226 EPA 901.1 Modified i

5.85E-01 7.19E-01 7.19E-01 1.20E+OO u

pCi/g 18-02009-05 i TRG 81021101FIWC003CV 01/31/1813:55

2/2/2018 2/2/2018 18-02009 EPA 901.1 Modified

-8.12E-02 1.01E+OO 1.01E+OO 1.28E+OO u

oCi/g

'""""'" *~-

18-02009-05 :

TRG 81021101FIWC003CV 01/31/18 13:55 : 2/2/2018 2/2/2018 18-02009 Thorium-234 EPA 901.1 Modified 1.49E+OO 3.17E+OO 3.17E+OO 4.74E+OO u

pCi/g

**-*"'"""'----------------~--

18-02009-05,

TRG 8102110IFIWC003CV 01/31/18 13:55 ; 2/2/2018 2/2/2018 18-02009 Thallium-208 EPA 901.1 Modified

4.48E-01 8.78E-01 8.78E-01 6.96E-01 u

pCi/g 18-02009-05 TRG 81021101FIWC003CV 01/31/18 13:55 2/2/2018 2/2/2018 18--02009 Uranium-235 EPA 901.1 Modified 3.50E-01 4.67E+OO 4.67E+OO 2.40E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect I I NE Al YT!CAL ON

~SCARBORO ROAD OAK RIDGE: TN 37830

**--------l---

865/481-0683 FAX 865/483-4621

[211]

Printed: 2/13/2018 8:54 AM Page 7 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009 Zion Solutions, LLC **---

Purchase Order:

677118 Final Report of Analysis

,, _____,w, rn,*,--,-"'" _____ """""'

101 Shiloh Blvd Ana/vsis Garegory.

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU Report ID Type ID Date Date Date ID MDA Qualifier Units 18-02009-06 TRG B1021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Actinium-228 EPA 901.1 Modified i

9.67E-01 2.24E+OO 2.24E+OO 3.31E+OO u

pCi/q 18-02009-06 TRG 81021101FIWC004CV 01/31/18 14:20. 2/2/2018 2/2/2018 18-02009 Silver-108m EPA 901.1 Modified 7.87E-01 7.08E-01 7.09E-01 6.11E-01 u

pCi/g an M:

TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009

-1.29E-01 6.24E-01 6.24E-01 7.82E-01 u

pCi/g 18-02009-06 TRG 81021101FIWC004CV 01/31/1814:20 2/2/2018 2/2/2018 18-02009 Barium-133 EPA 901.1 Modified

-1.23E-01 2.22E-01 2.22E-01 8.00E-01 u

pCi/g 18-02009-06 TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Bismuth-214 EPA901.1 Modified 1.61E+OO 1.08E+OO 1.08E+OO 1.98E+OO u

pCi/g 18-02009 '

18-02009-06 TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 Cobalt-60 EPA 901.1 Modified 1.13E+01 9.06E-01 1.08E+OO 7.32E-01 pCi/g 18-02009-06,

TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Cesium-134 EPA 901.1 Modified 2.02E-01 3.35E-01 3.35E-01 7.52E-01 u

pCi/g 18-02009-06 TRG i

81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Cesium-137 EPA 901.1 Modified 1.58E-01 ;

6.44E-01 6.44E-01 9.48E-01 u

pCi/g r-*-*---**---.-.,,

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~u, *-*

152 EPA 901.1 Modified 1.69E+02 7.04E+OO 1.12E+01 3.25E+OO pCi/g t--*------------"*---------

18-02009-06.

TRG B102110IFIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009

!:'cc**'c:- 154 EPA 901.1 Modified 5.51E+OO 1.38E+OO 1.41E+OO 2.52E+OO u

pCi/g 18-02009-06 '

TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Europium-155 EPA 901.1 Modified i

1.61E+OO 7.94E-01 7.98E-01 1.27E+OO u

pCi/g 18-02009-06 :

TRG B1021101FIWC004CV 01/31/18 14:20 ! 2/2/2018 2/2/2018 : 18-02009 : Holmium-166m EPA 901.1 Modified

-6.20E-01 1.08E+OO 1.08E+OO 4.93E-01 u

pCi/g 18-02009-06 ;

TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 : 18-02009 :

lodine-129 EPA 901.1 Modified 9.30E-01 6.37E-01 '

6.39E-01 8.20E-01 u

pCi/g 18-02009-06 TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018

  • 2/2/2018 18-02009 Potassium-40 EPA 901.1 Modified 5.65E+OO 3.48E+OO 3.49E+OO 5.57E+OO u

pCi/g 18-02009-06 TRG B102110IFIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 EPA 901.1 Modified 2.13E-02 5.98E-01 5.98E-01 8.77E-01 u

pCi/g

-*--0-,------------~---------------------------*

18-02009-06 TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Niobium-94 EPA 901.1 Modified

-1.16E+OO :

9.22E-01 9.24E-01 8.14E-01 u

pCi/g

<--:n n~

TRG B1021101FIWC004CV 01/31/1814:20 2/2/2018 2/2/2018 18-02009 Lead-210 EPA 901.1 Modified

2.70E+02 2.39E+01 2.76E+01 1.87E+01 u

pCi/g

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18-02009-06 TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Lead-212 EPA901.1 Modified 2.16E-01 5.35E-01 5.35E-01 1.01E+OO u

pCi/g 18-02009-06 :

TRG B1021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Lead-214 EPA 901.1 Modified

-1.37E+OO 9.72E-01 9.75E-01 1.31E+OO u

pCi/q 18-02009-06 ;

TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Promethium-145 EPA 901.1 Modified 1.57E+01

/

2.75E+OO 2.86E+OO 3.23E+OO u

pCi/g

'--------*-------:------~---

18-02009-06 TRG B1021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Radium-226 EPA 901.1 Modified 1.61E+OO '

1.08E+OO 1.08E+OO 1.98E+OO u

pCi/g

~Mnna_nc.

TRG

~------*-

B1021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Antimony-125 EPA 901.1 Modified 6.12E-01 1.26E+OO 1.26E+OO 1.85E+OO u

pCi/g 18-02009-06 TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Thorium-234 EPA 901.1 Modified 4.47E+OO 6.05E+OO 6.06E+OO 7.84E+OO u

pCi/g 18-02009-06 TRG 81021101FIWC004CV 01/31/18 14:20 2/2/2018 2/2/2018 18-02009 Thallium-208 EPA 901.1 Modified

-1.09E-01.

9.07E-01 9.07E-01 9.51E-01 u

pCi/g 18-02009-06 TRG 81021101FIWC004CV 01/31/18 14:20 : 2/2/2018 2/2/2018 18-02009 Uranium-235 EPA 901.1 Modified

-1.90E+OO :

6.16E+OO 6.16E+OO 2.92E+OO :

u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

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[212]

Printed: 2/1312018 8:54 AM Page 8 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SOG:

18-02009

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101 Shiloh Blvd

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ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA

  • Qualifier Report ID Type ID Date Date Date ID Units 18-02009-07 TRG 8102110FIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 Actinium-228 EPA 901.1 Modified 2.36E+OO 2.11E+OO 2.12E+OO 3.06E+OO u

pCi/g 18-02009-07 TRG 8102110FIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 Silver-108m EPA 901.1 Modified 1.15E+OO 6.25E-01 6.28E-01 4.77E-01 u

pCi/g

_________,,,,,_,. __ M_,,__, __, _______,,, _______________

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18-02009-07 TRG B102110FIFC003CV 01/31/1812:37 2/2/2018 2/2/2018 18-02009 Americium-241 EPA 901.1 Modified

-2.22E-01 4.82E-01 4.82E-01 6.84E-01 u

pCi/g 18-02009-07 '

TRG 8102110FIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 8arium-133 EPA 901.1 Modified

-8.85E-02 4.36E-01 4.36E-01 6.28E-01 u

pCi/g 18-02009-07 TRG 810211 OFIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 8ismuth-214 EPA901.1 Modified 1.21E+OO 6.15E-01 6.18E-01 6.54E-01 pCi/g

-~---"'-*--

18-02009-07 ;

TRG 8102110FIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 Cobalt-60 EPA 901.1 Modified 5.47E+OO 5.99E-01 6.62E-01 5.99E-01 pCi/g

"""--*----**o* -* ---------------- ------------------*

18-02009-07 TRG 810211 OFIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 Cesium-134 EPA901.1 Modified 3.86E-03 2.12E-01 2.12E-01 5.84E-01 u

pCi/g

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pCi/g 18-02009-07 :

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pCi/g TRG 8102110FIFC003CV 01/31/18 12:37

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18-02009-07 TRG 810211 OFIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 I Europium-154 EPA 901.1 Modified

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1.81E+OO 7.24E-01 7.30E-01 1.04E+OO u

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18-02009-07 ;

TRG 8102110FIFC003CV 01/31/18 12:37 2/2/201 2/2/2018 18-02009, Holmium-166m EPA 901.1 Modified 4.44E-01 7.11E-01 7.11E-01 4.26E-01 u

pCi/g 18-02009-07 :

TRG 8102110FIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 lodine-129 EPA 901.1 Modified

-2.89E+OO :

1.15E+OO ; 1.16E+OO 1.34E+OO u

pCi/g 18-02009-07 TRG 810211 OFIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 Potassium-40 EPA 901.1 Modified 8.06E+OO I

3.00E+OO 3.03E+OO 6.09E+OO u

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TRG 8102110FIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 Lead-210 EPA 901.1 Modified 2.49E+02 2.55E+01 2.85E+01 2.75E+01 pCi/g 18-02009-07 TRG 8102110FIFC003CV 01/31/18 12:37

' 2/2/2018 2/2/2018 18-02009 :

Lead-212 EPA 901.1 Modified 9.94E-02 3.55E-01 3.55E-01 7.92E-01 u

pCi/g 18-02009-07 j TRG 8102110FIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 Lead-214 EPA 901.1 Modified 5.38E-01 6.15E-01 6.15E-01 1.02E+OO u

pCi/g 18-02009-07 TRG B102110FIFC003CV 01/31/1812:37 ; 2/2/2018 2/2/2018 18-02009 : Promethium-145 EPA 901.1 Modified 4.45E+01 5.63E+OO 6.08E+OO 3.42E+OO u

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pCi/g 18-02009-07 TRG 8102110FIFC003CV 01/31/18 12:37 2/2/2018 2/2/2018 18-02009 Radium-226 EPA 901.1 Modified I

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2/2/2018 18-02009 Antimony-125 EPA 901.1 Modified 4.34E-01 9.49E-01 9.SOE-01 1.43E+OO u

pCi/g 18-02009-07 :

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pCi/g 18-02009-07 !

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pCi/g 18-02009-0 I TRG 8102110FIFC003CV 01/31/18 12:37

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[213]

Printed: 211312018 8:54 AM Page 9 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009 Zion Solutions,_ LLC Purchase Order:

677118 Final Report of Analysis

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____,,,,, -'-- "'"'"""'_,_, '"""~'-

101 Shiloh Blvd Analysis Ca,cyv,y.

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 18-02009-08 TRG 8102110FIFC021CV 01/31/18 13:00 2/2/2018 2/2/2018 18-02009 Actinium-228 EPA901.1 Modified 1.44E+OO :

1.43E+OO 1.43E+OO 2.23E+OO u

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  • ------~ -----------

18-02009-08 TRG 8102110FIFC021CV 01/31/18 13:00 2/2/2018 2/2/2018 18-02009 Si1ver-108m EPA 901.1 Modified i

7.44E-01 4.80E-01 4.82E-01 3.70E-01 u

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pCi/Q 18-02009-08 TRG B102110FIFC021CV 01/31/18 13:00 2/2/2018 2/2/2018 18-02009 Barium-133 EPA 901.1 Modified 1.23E-01 4.21E-01 4.21E-01 5.42E-01 u

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pCi/Q 18-02009-08 TRG B102110FIFC021CV 01/31/1813:00 2/2/2018 2/2/2018 18-02009 Cobalt-60 EPA 901.1 Modified 4.49E+OO 5.00E-01 5.51E-01 5.34E-01 pCi/g

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18-02009-08 ;

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18-02009-08 '

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18-02009-08 TRG B102110FIFC021CV 01/31/18 13:00 2/2/2018 2/2/2018 18-02009, Europium-154 EPA 901.1 Modified 2.95E+OO 9.60E-01. 9.72E-01 1.80E+OO u

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>--*---"'"'~------------*--------*-----*---

18-02009-08 TRG B102110FIFC021CV 01/31/18 13:00 2/2/2018 2/2/2018 18-02009 lodine-129 EPA 901.1 Modified 6.95E-01 1.64E-01 1.68E-01 2.72E-01 u

pCi/Q 18-02009-08

  • TRG B102110FIFC021CV 01/31/18 13:00 2/2/2018 2/2/2018 18-02009 ;

Potassium-40 EPA 901.1 Modified 4.97E+OO 2.41E+OO 2.42E+OO 7.04E+OO u

pCi/g C

18-02009-08 TRG B102110FIFC021CV 01/31/18 13:00 2/2/2018 2/2/2018 18-02009 ' ***-**.:,-**-

EPA901.1 Modified

-1.28E-01 4.23E-01 4.23E-01 6.08E-01 u

pCi/g 18-02009-08 i TRG 8102110FIFC021CV 01/31/1813:00 2/2/2018 2/2/2018 18-02009 Niobium-94 EPA 901.1 Modified

-1.46E+OO :

7.41E-01 7.45E-01 5.72E-01 u

pCi/g 18-02009-08 TRG 8102110FIFC021CV 01/31/18 2/2/2018 18-02009 Lead-210 EPA901.1 Modified 1.35E+02 '

1.17E+01 1.36E+01 9.13E+OO pCi/g 18-02009-08 TRG 8102110FIFC021CV 01/31/18 13:00 2/2/2018 2/2/2018 18-02009 Lead-212 EPA901.1 Modified 2.05E-01 '

5.73E-01 5.73E-01 7.01E-01 u

pCi/g 18-02009-08 ;

TRG B102110FIFC021CV 01/31/18 13:00 2/2/2018 2/2/2018 18-02009 Lead-214 EPA 901.1 Modified 2.36E-01 :

7.16E-01 7.16E-01 9.05E-01 u

pCi/g

"-*-----~-------

  • ----- --*-------~-

18-02009-08 '

TRG B102110FIFC021CV 01/31/18 13:00 2/2/2018 2/2/2018 18-02009 ' Promethium-145 EPA 901.1 Modified

-4.14E+01 3.25E+OO 3.88E+OO 9.65E-01 u

pCi/g 18-02009-08 TRG 8102110FIFC021CV 01/31/18 13:00. 2/2/2018 2/2/2018 18-02009 Radium-226 EPA 901.1 Modified 5.92E-01 ! 8.09E-01 8.10E-01 1.23E+OO u

pCi/g

*--------*--------~ ------~--

18-02009-08 TRG B102110FIFC021CV 01/31/18 13:00. 2/2/2018 2/2/2018 18-02009 Antimony-125 EPA 901.1 Modified '

-2.44E-01 9.12E-01 9.12E-01 1.15E+OO u

pCi/g f-..-*--

18-02009-08 TRG 8102110FIFC021CV 01/31/18 13:00 2/2/2018 2/2/2018 18-02009 Thorium-234 EPA 901.1 Modified

4.09E+OO 3.13E+OO 3.13E+OO 4.94E+OO u

pCi/g 18-02009-08 i TRG B102110FIFC021CV 01/31/18 13:00

  • 2/2/2018 2/2/2018 18-02009 ;

Thallium-208 EPA 901.1 Modified 6.95E-02 9.75E-01 9.75E-01 1.15E+OO u

pCi/g 18-02009-08

  • TRG B102110FIFC021CV 01/31/18 13:00. 2/2/2018 2/2/2018 18-02009 :

Uranium-235 EPA 901.1 Modified

-1.46E+OO 4.95E+OO 4.95E+OO 2.38E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect I

I EBERUNE CAL CORPOR,ATI

~ScARsoRo RoAD OAK R1DGE, :6~--3-7-8-30--8-65/48i=-o6s_3_FAx_s_6_5_/483=4-6-2i

[214]

Printed: 2/1312018 8:54 AM Page 10 of 17 Report To:

Work Order Details:

Eberline Analytical Final Report of Analysis J Alex Bohacheff

___ Zion Solutions,LLC 101 Shiloh Blvd SDG:

Purchase Order:

Analysis Cc<<v,;viy.

18-02009 677118 ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report Units ID Type ID Date Date Date ID 18-02009-09 TRG B102110FIWC015CV 01/31/1814:43 2/2/2018 2/2/2018 18-02009 Actinium-228 EPA901.1 Modified

-3.28E-01 1.55E+OO 1.55E+OO 2.24E+OO U

pCi/g

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18-02009-09 18-02009-09 18-02009 B102110FIWC015CV 01/31/18 14:43

' 2/2/2018 2/2/2018 18-02009 Americium-241 EPA 901.1 Mo***d--ifi-,e--d--,-****_**5*-.0-6E---0**1** *****-5*.2**e***E*****_**o**1***---5-_2**-7E---0-1--*-6-.4_0_E ___

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pCi/g B102110FIWC015CV 01/31/1814:43

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18-02009-09 TRG B102110FIWC015CV 01/31/1814:43 2/2/2018 2/2/2018 18-02009 Cesium-134 EPA901.1 Modified

-1.50E-01 3.73E-01 3.73E-01 5.31E-01 U

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18-02009-09 :

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,__=: ~===*-~*~---M**-=*-=-=!==-T*-_R-_G*--~~-_-_--8~1-~2-_1__-1-~-~I-_VJ-_C_0_1*~**=C=V=*=======--*-=;::o::.:_1_i3..:1:/.:1.. 8:_1:..:4:..:4..:3_ *....::21:.::2::.:/2::.:0_1..::..8*_*_-...:.2:f2.,:.'.:2.0:_1_:_8: __ *_=-~1.:.8~-0::2:.::-0..:0.::..;;...:* _**_~E;u.=ro:;P:i~u:.:m**.-:.*.*_-_ 1:.* : 5:*..:*2*::.:*=l-[-==-=-..::E=P-:A:..:9=0:.-1=*:*1-_;M-.:o-..::d-i::.fi-,e~d*==*--~_:'=.. ~..:1*:.::*3..:1..::E+_0::2:._;--:-5::*.::..86::E:.+..::.0.0:..*....,.*....:8:.::::*92::-E_+::...:_00--:-....::2:.::3:3:..::E+_.:O::O:._; ______..*.... ___ !:'.::'.:

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6.82E+OO 1.12E+OO 1.17E+OO 2.02E+OO U

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2.15E+OO 7.23E-01 7.31E-01 1.15E+OO U

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18-02009-09 '

TRG B102110F1WC015CV 01/31/1814:43 2/2/2018 2/2/2018 18-02009 lodine-129 EPA901.1 Modified 1.16E+OO 2.73E-01 2.80E-01 1.17E+OO U

oCi/a 18-02009-09 !

TRG B102110FIWC015CV 01/31/1814:43 2/2/2018 2/2/2018 18-02009 Potassium-40 EPA901.1 Modified 6.37E+OO 2.55E+OO 2.57E+OO 4.23E+OO pCi/g I-***-----...---**--:-----------*******-*--------+----------------***-**-*----

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18-02009-09 TRG B102110FIWC015CV 01/31/18 14:43 2/2/2018 2/2/2018 18-02009 Manganese-54 EPA 901.1 Modified 3.27E-01 4.13E-01 4.14E-01 6.21E-01 U

pCi/g 18-02009-09 :

TRG B102110FIWC015CV 01/31/1814:43

2/2/2018 2/2/2018 18-02009 Niobium-94 EPA901.1 Modified
-1.40E+OO :

6.94E-01 6.98E-01 5.56E-01 U

18-02009-09 :

18-02009-09 '

18-02009-09 i 18-02009-09 !

TRG B102110F1WC015CV 01/31/1814:43 2/2/2018 2/2/2018 18-02009 Lead-210 EPA901.1 Modified 2.05E+02 1.76E+01 2.05E+01 1.40E+01 U

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pCi/g 18-02009-09 TRG B102110F1WC015CV 01/31/1814:43 2/2/2018 2/2/2018 18-02009 Radium-226 EPA901.1 Modified 4.77E-01 7.91E-01 7.92E-01 1.17E+OO U

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oCi/a 18-02009-09 i TRG B102110F1WC015CV 01/31/1814:43 2/2/2018 2/2/2018 18-02009 Uranium-235 EPA901.1 Modified

-1.84E+OO 3.83E+OO 3.83E+OO 2.43E+OO U

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EBERLINE SERVICES CAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[215]

Printed: 2/13/2018 8:54 AM Page 11 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009

-+***

Zion Solutions. LLC r... *.-:;.':;;ic Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis Category:

ENVIRONMENTAL

    • - """""'"'--~-----*-------------*-*

Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units 18-02009-10 TRG B102110FIWC017CV 01/31/18 15:07 2/2/2018 2/2/2018 18-02009

  • Actinium-228 EPA 901.1 Modified 6.62E-01 1.89E+OO 1.89E+OO 2.79E+OO u

pCiig 18-02009-10 TRG B102110FIWC017CV 01/31/18 15:07 2/2/2018 2/2/2018 18-02009 Silver-108m EPA 901.1 Modified 6.93E-01 6.13E-01 6.14E-01 5.30E-01 u

pCi/g

"'~---------*

pCi/g 18-02009-10 TRG B102110FIWC017CV 01/31/1815:07 2/2/2018 2/2/2018 18-02009 Americium-241 EPA901.1 Modified

-4.49E-01 5.74E-01 5.75E-01 7 08E-01 u

18-02009-10 :

TRG B102110FIWC017CV 01/31/1815:07 2/2/2018 2/2/2018 18-02009 Barium-133 EPA 901.1 Modified 2.48E-01 3.74E-01 3.74E-01 7.25E-01 u

pCi/g

____________,,, ____________ "'"'"--------,--~----*--'"'

18-02009-10 '

TRG B102110FIWC017CV 01/31/18 15:07 2/2/2018 2/2/2018 18-02009 Bismuth-214 EPA 901.1 Modified 1.43E+OO i

1.16E+OO 1.16E+OO 1.68E+OO u

pCi/g

  • -----,,-----------------*------.-----~--------.--

18-02009-10 TRG B102110F1WC017CV 01/31/18 15:07 2/2/2018 2/2/2018 18-02009 Cobalt-60 EPA 901.1 Modified 7.60E+OO 6.76E-01 7.80E-01 6.62E-01 pCi/g

_, ____,, __, __ ~--------

18-02009-10 TRG B102110FIWC017CV 01/31/18 15:07 2/2/2018 2/2/2018 18-02009 Cesium-134 EPA 901.1 Modified 7.41E-02 2.31E-01 2.31E-01 6.40E-01 u

pCi/g I

*=---------.

pCi/g 18-02009-10 TRG B102110FIWC017CV 01/31/18 15:07 2/2/2018 2/2/2018 18-02009 Cesium-137 EPA 901.1 Modified

2.17E+OO 8.04E-01 8.11E-01 1.14E+OO 18-02009-10 TRG B102110FIWC017CV 01/31/18 15:07 2/2/2018 2/2/2018 18-02009
u, ve,u*,.. 52 EPA 901.1 Modified 1.58E+02 5.56E+OO :

9.84E+OO 3.06E+OO pCi/g 2/2/2018 :

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---*---------------,---""~'-"'

18-02009-10 :

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. -1.01E+OO 9.50E-01 9.51E-01 4.36E-01 u

pCi/g 18-02009-10 TRG B102110FIWC017CV 01/31/18 15:07 ! 2/2/2018 2/2/2018 18-02009 lodine-129 EPA 901.1 Modified 8.32E-01 5.67E-01 5.69E-01 7.27E-01 u

oCi/q pCi/g 18-02009-10 TRG B 10211 OFIWC017CV 01/31/18 15:07 2/2/2018 2/2/2018 18-02009 Potassium-40 EPA 901.1 Modified 7.10E+OO 2.61E+OO 2.63E+OO 5.74E+OO

  • ---*-----",------~----,,,,, ______________

---*----=-m 18-02009-10 TRG B102110FIWC017CV 01/31/1815:07 ; 2/2/2018 2/2/2018 18-02009 Manganese-54 EPA901.1 Modified 1.16E-01 i 4.12E-01 i

4.12E-01 7.73E-01 u

pCi/g 18-02009-10 TRG B102110F1WC017CV 01/31/18 15:07 : 2/2/2018

  • 2/2/2018 18-02009 ;

Niobium-94 EPA 901.1 Modified

-8.36E-01 7.84E-01 7.85E-01 7.10E-01 u

pCi/g 18-02009-10 TRG B102110FIWC017CV 01/31/1815:07 i 2/2/2018 2/2/2018 18-02009 Lead-210 EPA 901.1 Modified 2.33E+02 !

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---**-----------------*"*-~-*---------~ _________,_, ____ "--*'_, _____________ _. ____ *-----*

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---*----------------~~-*

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pCi/g 18-02009-10 TRG B102110FIWC017CV 01/31/18 15:07 2/2/2018

  • 2/2/2018 18-02009 !

Radium-226 EPA 901.1 Modified 1.43E+OO 1.16E+OO 1.16E+OO 1.68E+OO u

pCi/g 18-02009-10,

TRG B 10211 OFIWC017CV 01/31/18 15:07 2/2/2018

  • 2/2/2018 18-02009 : ~,::':,,_.. 125 EPA 901.1 Modified

-6.38E-01 1.16E+OO 1.16E+OO 1.65E+OO u

pCi/g 18-02009-10 (

TRG B102110FIWC017CV 01/31/18 15:07 : 2/2/2018 2/2/2018 18-02009 Thorium-234 EPA 901.1 Modified 7.20E-01 5.41E+OO 5.41E+OO 6.88E+OO u

pCiig 18-02009-10 TRG B102110F1WC017CV 01/31/18 15:07 2/2/2018 2/2/2018 18-02009 '

Thallium-208 EPA 901.1 Modified 5.40E-01 9.98E-01 9.98E-01 1.02E+OO u

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,,,,,,_,, ------------*-*-*-----~*-

18-02009-10 '

TRG B102110F1WC017CV 01/31/18 15:07 2/2/2018 2/2/2018 18-02009 Uranium-235 EPA 901.1 Modified

-3.44E+OO 5.50E+OO 5.50E+OO 2.55E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect SCARBORO ROAD OAK RIDGE, 865/481-0683 FAX 865/483-4621

[216]

Printed: 2/13/2018 8:54 AM Page 12 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009

___ Zion Solutions, LLC __________

Purchase Order:

677118 Final Report of Analysis

*-------*-----,----*---------------,-------*---------,-.---------~----------------------------------

101 Shiloh Blvd

.... Analysis Category: __

ENVIRONMENTAL f-----**

Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units 18-02009-11 TRG 8102110FIWC019CV 01/31/18 15:30 2/2/2018 2/2/2018 18-02009 Actinium-228 EPA 901.1 Modified 2.31E+OO 1.71E+OO 1.72E+OO 2.65E+OO u

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18-02009-11 TRG 8102110FIWC019CV 01/31/18 15:30 2/2/2018 2/2/2018 18-02009 Silver-108m EPA 901.1 Modified 8.70E-01 5.73E-01 5.75E-01 4.42E-01 u

pCi/g 18-02009-11 TRG 8102110FIWC019CV 01/31/18 15:30 2/2/2018 2/2/2018 18-02009 Americium-241 EPA 901.1 Modified 1.36E-01 3.79E-01 3.79E-01 5.67E-01 u

pCi/g

--~-------------*--------

18-02009-11 TRG 8102110FIWC019CV 01/31/18 15:30 2/2/2018 2/2/2018 18-02009 Barium-133 EPA901.1 Modified 2.46E-01 5.06E-01 5.06E-01 6.24E-01 u

pCi/g 18-02009-11 TRG 8102110FIWC019CV 01/31/18 15:30

' 2/2/2018 2/2/2018 18-02009 Bismuth-214 EPA 901.1 Modified 1.68E+OO 7.70E-01 7.75E-01 1.53E+OO pCi/g 18-02009-11 TRG 8102110FIWC019CV 01/31/18 15:30 2/2/2018 2/2/2018 18-02009 Cobalt-60 EPA 901.1 Modified 8.89E+OO 7.44E-01 8.73E-01 6.22E-01 pCi/g

~-

i 18-02009-11 TRG 8102110FIWC019CV 01/31/18 15:30 2/2/2018 2/2/2018 18-02009 Cesium-134 EPA 901.1 Modified 1.04E-02 '

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pCi/g 18-02009-11 TRG 8102110FIWC019CV 01/31/1815:30 2/2/2018, 2/2/2018 18-02009 Cesium-137 EPA 901.1 Modified 6.75E+OO 1.35E+OO 1.39E+OO 1.25E+OO pCi/g 01/31/18 15:30 2/2/2018 :

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1.53E+02 i 2.24E+OO pCi/g 18-02009-11 TRG 8102110FIWC019CV 2/2/2018 18-02009 EPA 901.1 Modified 7.84E+OO 1.11E+01 18-02009-11 TRG 8102110FIWC019CV 01/31/18 15:30 2/2/2018 2/2/2018 18-02009 Europium-154 EPA901.1 Modified i 7.05E+OO 1.32E+OO 1.37E+OO 2.39E+OO u

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18-02009-11 TRG 8102110FIWC019CV 01/31/18 15:30 2/2/2018 2/2/2018 18-02009 Europium-155 EPA 901.1 Modified 4.31E-01 6.52E-01 6.52E-01 9.73E-01 u

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TRG 8102110FIWC019CV 01/31/18 15:30 : 2/2/2018 2/2/2018 18-02009 Holmium-166m EPA 901.1 Modified 2.56E-01 '

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18-02009-11 :

TRG 8102110FIWC019CV 01/31/18 15:30 2/2/2018 2/2/2018 18-02009 lodine-129 EPA 901.1 Modified

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pCi/g 18-02009-11 TRG 8102110FIWC019CV 01/31/18 15:30 2/2/2018 2/2/2018 18-02009 Potassium-40 EPA 901.1 Modified 9.49E+OO 2.99E+OO 3.03E+OO 7.58E+OO pCi/g r

18-02009-11 :

TRG. 8102110FIWC019CV 01/31/1815:30 2/2/2018 2/2/2018 18-02009 EPA 901.1 Modified

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TRG 8102110FIWC019CV 01/31/18 15:30. 2/2/2018 2/2/2018 18-02009 '

Uranium-235 EPA 901.1 Modified i

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[217]

Printed: 2/13/2018 8:54 AM Page 13 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009 Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis

,,e ____

101 Shiloh Blvd

<.;aregory ENVIRONMENT AL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units 18-02009-12 TRG B102110FIWC020CV 02/01/18 08:12 2/2/2018 2/2/2018 18-02009 :

Actinium-228 EPA 901-1 Modified 1.28E+OO 1.38E+OO L39E+OO 2.10E+OO u

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pCi/g 18-02009-12 TRG 810211 OFIWC020CV 02/01/18 08:12 2/2/2018 2/2/2018 18-02009 Americium-241 EPA 901-1 Modified

-1WE-01 :

4.14E-01 4.14E-01 5.15E-01 u

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1.53E+02 1.37E+01 1.58E+01 1.10E+01 u

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TRG B102110FIWC020CV 02/01/18 08:12 l 2/2/2018 2/2/2018 18-02009, Promethium-145 EPA 901.1 Modified 7.86E+OO 1.56E+OO 1.61E+OO 1.88E+OO u

oCi/q 18-02009-12 :

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6.75E-01 6.75E-01 1.00E+OO u

pCi/g 18-02009-12 TRG 8102110FIWC020CV 02/01/18 08:12 2/2/2018 2/2/2018 18-02009 Antimonv-125 EPA901.1 Modified 4.33E-01 : 8.16E-01 8.16E-01 1.20E+OO u

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18-02009-12 :

TRG 8102110FIWC020CV 02/01/18 08:12 2/2/2018 2/2/2018 18-02009 Thorium-234 EPA 901.1 Modified 47E-03 3.99E+OO 3.99E+OO 5.03E+OO u

pCi/g 18-02009-12 TRG 8102110FIWC020CV 02/01/18 08:12 2/2/2018 2/2/2018 18-02009 Thallium-208 EPA901.1 Modified 7.36E-01 1-09E+OO 1.09E+OO 6.06E-01 u

pCi/g f-.-----

' 2/2/2018 18-02009-12 TRG 810211 OFIWC020CV 02/01/18 08:12 2/2/2018 18-02009 Uranium-235 EPA 901.1 Modified 1.12E+OO 3.95E+OO 3.95E+OO 1.83E+OO u

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[218]

Printed: 211312018 8:54 AM Page 14 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009 Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis Category:

  • ENVIRONMENTAL y-=-"-

Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu Report ID Type ID Date Date Date ID CSU MDA Qualifier Units 18-02009-13 I

TRG B102110FIWC014CV 02101 /18 08:56 2/2/2018 2/2/2018 18-02009 Actinium-228 EPA901.1 Modified

-8.70E-01 1.75E+OO 1.75E+OO 2.50E+OO u

pCi/g 18-02009-13 :

TRG 8102110FIWC014CV 02/01/18 08:56

2/2/2018 2/2/2018 18-02009 Silver-108m EPA 901.1 Modified 2.42E-01 5.38E-01 5.38E-01 4.96E-01 u

pCi/g 18-02009-13 TRG 8102110FIWC014CV 02/01/18 08:56 2/2/2018 2/2/2018 18-02009 Americium-241 EPA901.1 Modified

-9.73E-01 6.00E-01 6.03E-01 7.04E-01 u

pCi/g 18-02009-13 TRG B102110FIWC014CV 02/01/18 08:56 2/2/2018 2/2/2018 18-02009 Barium-133 EPA 901.1 Modified

-1.44E-01 2.44E-01 2.45E-01 7.17E-01 u

I pCi/g

*---~-------,-----------

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2/2/2018 i 2/2/2018 18-02009 I Antimony-*125 EPA 901.1 Modified

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[219]

Printed: 2/13/2018 8:54 AM Page 15 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009

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Zion Solutions,_ LLC Purchase Order:

677118 Final Report of Analysis ms, '"*-,,*-*-----------

101 Shiloh Blvd r,,+o--

ENVIRONMENTAL

--~-:::,-Y Zion, IL 60099 Sample Matrix:

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-8.63E-01 2A4E+OO 2.44E+OO 3.22E+OO u

pCi/g 18-02009-14 TRG B102110FIWC018CV 02/01/18 09:38 2/2/2018 2/2/2018 18-02009 Silver-108m EPA 901.1 Modified 1.26E+OO 6.99E-01 7.02E-01 5.22E-01 u

pCi/g 18-02009-14 TRG 8102110FIWC018CV 02/01/18 09:38 i 2/2/201 2/2/2018 18-02009 Americium-241 EPA901.1 Modified

-4.21E-01 5.22E-01 5.22E-01 7.37E-01 u

pCi/g 18-02009-14 ;

TRG 8102110FIWC018CV 02/01/18 09:38 2/2/2018 2/2/2018 18-02009 Barium-133 EPA 901.1 Modified 3.94E-01 4.64E-01 i

4.64E-01 6.97E-01 u

pCi/g TRG B102110FIWC018CV 02/01/18 09:38 2/2/2018 2/2/2018 18-02009 Bismuth-214 EPA 901.1 Modified 4.64E-01 8.80E-01 : 8.80E-01 1.32E+OO u

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EPA 901.1 Modified 5.71E-01 : 1.04E+OO 1.04E+OO 4.72E-01 u

pCi/g 18-02009-14 i TRG B102110FIWC018CV 02/01/18 09:38 2/2/2018 2/2/2018 18-02009 lodine-129 EPA 901.1 Modified

-3.55E+OO 1.29E+OO ; 1.30E+OO 1.45E+OO u

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,rn *- -~

TRG B102110FIWC018CV 02/01/18 09:38 i 2/2/2018 2/2/2018 18-02009 Potassium-40 EPA 901. 1 Modified 4.52E+OO 3.01E+OO 3.02E+OO 7.77E+OO u

pCi/g

  • ~

18-02009-14 TRG B102110FIWC018CV 02/01 /18 09:38

2/2/2018 2/2/2018 18-02009
,.,_,,"_" ___ :

EPA 901.1 Modified 1.63E-01 6.35E-01 6.36E-01 8.64E-01 u

pCi/g 18-02009-14 '

TRG B102110FIWC018CV 02/01/18 09:38 2/2/2018 2/2/2018 18-02009 Niobium-94 EPA901.1 Modified 5.19E-02 2.31E-01 2.31E-01 7.75E-01 u

pCi/g

  • -----~--_,,_,, _____, ____

---"--~--

18-02009-14 TRG 8102110FIWC018CV 02/01/18 09:38 i

2/2/2018 2/2/2018 18-02009 Lead-210 EPA 901.1 Modified 2.55E+02 2.54E+01 2.86E+01 2.81E+01 pCi/g 18-02009-14 :

TRG 8102110FIWC018CV 02/01/18 09:38 2/2/2018 2/2/2018 18-02009 Lead-212 EPA 901.1 Modified ' 7.16E-01 5.49E-01 5.50E-01 1.80E+OO u

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-*----*-----'--=-

____________,.,,_ -~-----

18-02009-14 TRG B102110FIWC018CV 02/01/18 09:38 2/2/2018 2/2/2018 18-02009 Lead-214 EPA 901.1 Modified i

-8.42E-02 7.90E-01 '

7.90E-01 1.14E+OO u

pCi/g

~--*---*----*=*"*-------*----*"'*------,, *------------

18-02009-14 !

TRG 8102110FIWC018CV 02/01/18 09:38 2/2/2018 2/2/2018 18-02009 Promethium-145 EPA 901. 1 Modified 6.11E+01 7.55E+OO 8.18E+OO 3.81E+OO u

pCi/g 18-02009-14 i TRG B102110FIWC018CV 02/01/18 09:38 2/2/2018 2/2/2018 18-02009 Radium-226 EPA 901. 1 Modified 4.64E-01 8.80E-01 8.80E-01 1.32E+OO u

pCi/g 18-02009-14 i TRG 8102110FIWC018CV 02/01/18 09:38 '

2/2/2018 2/2/2018 18-02009 Antimony-125 EPA 901.1 Modified 1.14E+OO 1.07E+OO 1.08E+OO 1.63E+OO u

pCi/g

-~

TRG 8102110FIWC018CV 02/01/18 09:38 : 2/2/2018 ; 2/2/2018 18-02009 Thorium-234 EPA 901.1 Modified

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18-02009-14 TRG B102110FIWC018CV 02/01/18 09:38 2/2/2018 2/2/2018 18-02009 '

Thallium-208 EPA 901. 1 Modified 2.99E-01 1.49E+OO 1.49E+OO 1.37E+OO u

pCi/g 18-02009-14,

TRG B102110FIWC018CV 02/01 /18 09:38

' 2/2/2018 2/2/2018 18-02009 Uranium-235 EPA 901.1 Modified

' -1.45E+OO 3.89E+OO 3.89E+OO 2.70E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE SERViCES

, EBERLINE CAL 'v ON i 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[220]

Printed: 211312018 8:54 AM Page 16 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02009 Zion Solutions, LLC n;;,-::;.~::;:;e Order:

677118 Final Report of Analysis

,---------,,,,,,,,-,-*----,,,,,,._ -*~-*----A---*-----* ~.w-101 Shiloh Blvd Analysis Category:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units 18-02009-15 TRG B102110FIWC016CV 02/01 /18 10:00 2/2/2018 2/2/2018 18-02009 Actinium-228 EPA 901.1 Modified

-1.56E-01 1.55E+OO 1.55E+OO 2.27E+OO u

pCi/g v--**---*-*-*----***-*-------*-------

18-02009-15 TRG B102110FIWC016CV 02/01/18 10:00 2/2/2018 2/2/2018 18-02009 :

Silver-108m EPA 901.1 Modified 8.37E-01 4.77E-01 4.78E-01 4.44E-01 u

pCi/g 18-02009-15 :

TRG 8102110FIWC016CV 02/01/18 10:00. 2/2/2018 2/2/2018 18-02009 : Americium-241 EPA 901.1 Modified

-2.42E-02 3.75E-01 3.75E-01 5.76E-01 u

pCi/g 18-02009-15 TRG 8102110FIWC016CV 02/01/18 10:00 2/2/2018 2/2/2018 18-02009 Barium-133 EPA 901.1 Modified i

2.19E-02 4.06E-01 4.06E-01 5.95E-01 u

pCi/g

--~-*-*-***-**-

18-02009-15 '

TRG 8102110FIWC016CV 02/01/18 10:00 i 2/2/2018 2/2/2018 18-02009 Bismuth-214 EPA 901.1 Modified i

9.47E-01. 8.01E-01 8.02E-01 1.30E+OO u

pCi/g

--*---.--"--*------.------,,~------~*-----------

8102110FIWC016CV 18-02009-15 TRG 02/01/18 10:00 2/2/2018 2/2/2018 18-02009 Cobalt-60 EPA901.1 Modified 3.95E+OO 4.32E-01 4.77E-01 2.63E-01 pCi/g 18-02009-15 i TRG i

8102110FIWC016CV

/01/18 10:00 2/2/2018 2/2/2018 18-02009 Cesium-134 EPA 901.1 Modified 1.04E-01 2.63E-01 2.63E-01 5.06E-01 u

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/01/1810:00 2/2/2018 2/2/2018 18-02009 Cesium-137 EPA 901.1 Modified i

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TRG 8102110FIWC016CV 02/01 /18 10:00 i

2/2/2018 2/2/2018 18-02009 Holmium-166m EPA 901.1 Modified i

-2.61E-01 7.31E-01. 7.31E-01 3.45E-01 u

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"----~-------,--------"-"'~--------------,-*,

18-02009-15 i TRG 8102110FIWC016CV 02/01 /18 1 0:00 2/2/2018 2/2/2018 18-02009 lodine-129 EPA 901.1 Modified 1.43E+OO : 4.83E-01. 4.88E-01 1.96E+OO u

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18-02009-15,

TRG 8102110FIWC016CV 02/01/18 10:00 2/2/2018 2/2/2018 18-02009 Potassium-40 EPA 901.1 Modified 5.97E+OO 2.84E+OO 2.86E+OO 4.13E+OO pCiig 18-02009-15 TRG 8102110FIWC016CV 02/01/18 10:00 i 2/2/2018 2/2/2018 18-02009 :

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9.50E-02 1.91E-01 i

1.91E-01 5.98E-01 u

pCi/g 18-02009-15,

TRG B102110FIWC016CV 02/01/18 10:00 2/2/2018

  • 2/2/2018 18-02009 Lead-210 EPA901.1 Modified 1.31E+02 i

1.28E+01 1.45E+01 1.31E+01 u

pCi/g 18-02009-15 TRG 8102110FIWC016CV 02/01/18 10:00 2/2/2018 2/2/2018 18-02009 Lead-212 EPA 901.1 Modified 1.59E-01 3.76E-01 3.76E-01 7.19E-01 u

pCi/g 18-02009-15 TRG B102110FIWC016CV 02/01/18 10:00 i 2/2/2018 2/2/2018 18-02009 Lead-214 EPA901.1 Modified

-1.12E+OO,

7.14E-01 i

7.16E-01 9.43E-01 u

pCi/g 18-02009-15 TRG B102110FIWC016CV 02/01/1810:00 2/2/2018 2/2/2018 18-02009 Promethium-145 EPA 901.1 Modified 7.28E+OO i

1.82E+OO 1.85E+OO 2.28E+OO u

pCi/g i 2/2/2018 '

pCi/g 18-02009-15.

TRG 8102110FIWC016CV 02/01/18 10:00 2/2/2018 18-02009 Radium-226 EPA 901.1 Modified 9.47E-01 8.01E-01 8.02E-01 1.30E+OO u '

18-02009-15 TRG 8102110FIWC016CV 02/01/18 10:00 2/2/2018 2/2/2018 18-02009 i n,...... -.., *--

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2.20E-01. 9.11E-01 i

9.11E-01 1.34E+OO u

pCi/g

!-----------(

18-02009-15 TRG 8102110FIWC016CV 02/01 /18 10:00 i 2/2/2018 2/2/2018 18-02009 i Thorium-234 EPA 901.1 Modified 6.18E-01 i

4.52E+OO 4.52E+OO 5.80E+OO u

pCi/g j

18-02009-15 TRG B102110FIWC016CV 02/01/18 10:00 2/2/2018 2/2/2018 18-02009 Thallium-208 EPA 901.1 Modified i

5.94E-02 8.09E-01 8.09E-01 9.42E-01 u

pCi/g r---~-------~--,

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-7.76E-01 4.19E+OO 4.19E+OO 2.08E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

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EBERLINE

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SERVICES I

I EBERLINE ANALYTICAL CORPORA Ti ON I 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[221]

Printed: 2/1312018 8:54 AM Page 17 of 17 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SOG:

18-02009 Zion_Solutions, LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd

___ Analysis Category: _

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units 18-02009-16 TRG B102110IFIWC019CV 02/01/18 10:38 2/212018 2/2/2018 18-02009 Actinium-228 EPA 901.1 Modified 1.34E-01 1.95E+OO 1.95E+OO 2.88E+OO u

pCi/g 18-02009-16 TRG B102110IFIWC019CV 02/01/18 10:38 2/2/2018 2/2/2018 18-02009 '

Silver-108m EPA 901.1 Modified 8.34E-01 5.92E-01 5.94E-01 4.44E-01 u

pCi/g

,,m,~'->" _____,_,_

18-02009-16 TRG B10211 OIFIWC019CV 02/01/1810:38 2/2/2018 212/2018 18-02009 Americium-241 EPA901.1 Modified

-1.33E-01 3.86E-01 3.86E-01 5.69E-01 u

pCiig i-------****

18-02009-16 TRG B102110IFIWC019CV 02/01/18 10:38 2/2/2018 2/2/2018 18-02009 Barium-133 EPA 901. 1 Modified

-2.37E-01 5.38E-01 5.38E-01 6.43E-01 u

pCi/g r-----

18-02009-16 TRG B102110IFIWC019CV 02/01/1810:38 2/2/2018 2/2/2018 18-02009

'Bismuth-214 EPA 901. 1 Modified

-1.40E-01 9.59E-01 9.59E-01 1.39E+OO u

pCi/g

,==------------*""-~',"""'"'"'*----------------=--*-------

18-02009-16 TRG B102110IFIWC019CV 02/01/1810:38 2/2/2018 2/2/2018 18-02009 i Cobalt-60 EPA901.1 Modified i 8.42E+OO 7.26E-01 8.45E-01 4.79E-01 pCiig 18-02009-16 TRG B102110IFIWC019CV 02/01/18 10:38 2/2/2018 2/2/2018 18-02009 Cesium-134 EPA 901. 1 Modified

' -4. 16E-01 4.66E-01 4.66E-01 6.38E-01 u

pCiig 18-02009-16 TRG B1021101FIWC019CV 02101/18 10:38 '

2/2/2018 2/2/2018 18-02009 Cesium-137 EPA901.1 Modified

6.83E-01 6.30E-01 6.31E-01 1.03E+OO u

pCi/g 18-02009-16 TRG B102110IFIWC019CV 02/01/1810:38 2/2/2018 2/2/2018 18-02009, Europium-152 EPA 901.1 Modified

1.45E+02 7.66E+OO 1.07E+01 2.57E+OO pCi/g 18-02009-16 TRG B102110IFIWC019CV 02/01/18 10:38 2/2/2018 2/2/2018 18-02009 Europium-154 EPA 901.1 Modified 2.96E+OO 1.17E+OO 1.18E+OO 2.06E+OO u

pCi/g

~-----~-

18-02009-16 TRG B1021101FIWC019CV 02/01/18 10:38 2/2/2018 2/2/2018 18-02009 Europium-155 EPA 901.1 Modified 3.39E-01 6.90E-01 6.90E-01 1.02E+OO u

pCi/g

. '""-------------~----

pCiig 18-02009-16 TRG B102110IFIWC019CV 02/01/18 10:38 : 212/2018 2/2/2018 18-02009 : Holmium-166m EPA 901.1 Modified 3.44E-01 8.59E-01 8.59E-01 4.82E-01 u

18-02009-16 TRG B102110IFIWC019CV 02/01/18 10:38 2/2/2018 i 2/2/2018 18-02009 lodine-129 EPA 901.1 Modified i.08E+OO 2.05E-01 2.13E-01 3.39E-01 u

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---~-*---"'--"""'--'-*"

18-02009-16 TRG B102110IFIWC019CV 02/01/18 10:38 212/2018 2/2/2018 18-02009,

10 EPA 901.1 Modified 6.81E+OO 3.43E+OO 3.45E+OO 6.02E+OO pCi/g 18-02009-16 :

TRG B102110IFIWC019CV 02101 /18 10:38 212/2018 2/2/2018 18-02009 ' Manganese-54 EPA901.1 Modified 1.15E-01 5.13E-01 5.13E-01 7.61E-01 u

pCi/g 18-02009-16 TRG B102110IFIWC019CV 02/01/18 10:38 I 21212018 212/2018 18-02009 Niobium-94 EPA 901.1 Modified 2.40E-01 3.07E-01 3.08E-01 7.09E-01 u

pCi/g B102110IFIWC019CV 02/01/18 10:38 2/2/2018 2/2/2018 18-02009 :

Lead-210 EPA 901.1 Modified 2.05E+02 1.67E+01 1.98E+01 1.14E+01.

pCi/g

~-----*------------*--

18-02009-16 TRG B1021101FIWC019CV 02/01/18 10:38 212/2018

  • 2/2/2018 18-02009 Lead-212 EPA 901.1 Modified 2.00E-01 4.62E-01 4.62E-01 8.20E-01 u

pCi/g 18-02009-16 B102110IFIWC019CV 02/01/18 10,38 21212018, 2/2/2018 18-02009,

Lead-214 EPA 901.1 Modified 5.20E-01 8.68E-01 8.69E-01 1.03E+OO u

pCi/g

=-------------------

~-"""

18-02009-16 :

TRG B102110IFIWC019CV 02/01/1810:38. 2/2/2018 2/2/2018 18-02009 Promethium-145 EPA901.1 Modified i -6.21E+01 '

4.57E+OO 5.57E+OO 1.27E+OO u

pCi/g 18-02009-16 !

TRG B102110IFIWC019CV 02/01/18 10:38 2/212018 2/2/2018 18-02009 Radium-226 EPA 901.1 Modified

-1.40E-01 9.59E-01 9.59E-01 1.39E+OO :

u pCi/g 18-02009-16 '

TRG B102110IFIWC019CV 02/01/18 10:38 212/2018 2/2/2018 18-02009

~,.*,,,o,,, >L~

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-7.37E-01 1.12E+OO 1.12E+OO 1.38E+OO u

pCi/g 18-02009-16 '

TRG B102110IFIWC019CV 02/01/1810:38 212/2018 2/2/2018 18-02009 j Thorium-234 EPA 901.1 Modified 2.96E+OO 4.02E+OO 4.03E+OO 6.03E+OO u

pCi/g

--**~

18-02009-16 TRG B102110IFIWC019CV 02/01/18 10:38

' 2/2/2018 2/2/2018 18-02009 i Thallium-208 EPA 901.1 Modified 4.64E-01 8.21E-01 8.21E-01 1.22E+OO i u

pCi/g 18-02009-16 TRG i

B102110IFIWC019CV 02/01/18 10,38 : 2/2/2018 2/2/2018 18-02009 ! Uranium-235 EPA 901.1 Modified 4.83E-01 5.91E+OO 5.91E+OO 2.88E+OO u

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EBERLINE

~

SERViCES EBERUNE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[222]

ZI()NSOLUTIONSru:

1

\\v

\\\\

Sample ID Bl02110IFIWCOOICV Bl02110IFIWC003CV Bl02110IFIWC004CV Bl02110FIFC003CV B102110FIFC021CV Bl02110FIWC015CV B102110FIWC017CV Bl02110FIWC019CV Bl02110FIWC020CV Bl02110FIWC014CV Bl02110FIWC018CV Bl02110FIWC016CV Bl02l10IFIWC019CV Sample Mat1ix Log NIA Concrete NIA Concrete NIA Concrete NIA Concrete NIA Concrete NIA Concrete NIA Concrete NIA Concrete NIA Concrete NIA Concrete NIA Concrete NIA Concrete NIA Concrete Sample Type Concrete Concrete Concrete Concrete Concrete Concrete Concrete Concrete Concrete Concrete Concrete Concrete Concrete 18 -02009 -

Cliain-of-Custody Form REC'D FEBO 2 2018 Sample Container Sample Date Sample Time Analysis Preservative Vol Unit Type Qty Type 57.94 cm3 Puck 1

1/31/2018 1320 HTD None 57.94 cm3 Puck 1

1/31/2018 1355 HTD None 57.94 cm3 Puck 1

1/31/2018 1420 HTD None 57.94 cm3 Puck l

1/31/2018 1237 HTD None 57.94 cm3 Puck 1

1/31/2018 1300 HTD None 57.94 cm3 Puck l

1/31/2018 1443 HTD None 57.94 cm3 Puck l

1/3112018 1507 HTD None 57.94 cm3 Puck l

1/31/2018 1530 HTD None 57.94 cm3 Puck 1

211/2018 0812 HTD None 57.94 cm3 Puck l

211/2018 0856 HTD None 57.94 cm3 Puck l

211/2018 0938 HTD None 57.94 cm3 Puck 1

211/2018 1000 HTD None 57.94 cm3 Puck l

211/2018 1038 HTD None ZS-WM-131 Revision 0 Information Use Remarks 0.0"-0.5" 0.0"-0.5" 0.0"-0.5" 0.0"-0.5" 0.0"-0.5" 0.0"-0.5" 0.0"-0.5" 0.0"-0.5" 0.0"-0.5" 0.0"-0.5" 0.0"-0.5" 0.0"-0.5" 0.0"-0.5"

[223]

ZI<)NSOLUTIONSiu:

Laboratory:

Eberline Labs Relinquished by:

J. ALEX BOHACHEFF Relinquished by:

fil'rh, rJ l ~'ltrf Relinquished by:

Relinquished by:

Comments ANALYSIS 5 ROC-HTD Date Submitted To Lab:

Date Time:

( mm/ dd/yyyy):

t>::J./o{ ~oJB

{ 3'-1 S Dae (mm/dd/yyyy):

Time:

Date Time:

( mm/ dd/yyyy):

REFERENCE:

Email to Mike McDougall PRIORITY 24 hour2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> turnaround PO# 677118

- oz O O 9 Ship Container No.:

Received by:

Received by:

ftdt:A REC'D FEB O 2 2018 ZS-WM-131 Revision 0 Information Use Cooler Temperature:

Airbill Number:

NIA Date: (rnrn/dd/yyyy):

Time:

0i/0.1 ho1 g (3L/.0 Date: (rnrn/dd/yyyy):

Time:

(6:00 Date: (min/dd/yyyy):

Time:

2.-~-i V o</ l 5 Date: (mm/dd/yyyy):

Time:

[224]

BERLINE EBS-OR-43353 February 13, 2018 Alex Bohacheff Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099 SAMPLE RECEIPT SERVICES CASE NARRATIVE Work Order # 18-02018-0R EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TENNESSEE 37830 PHONE (865) 481-0683 FAX (865) 483--L,621 This work order contains three solid samples received 02/03/2018. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.

CLIENT ID B 10211 OIFIWCOl OCV Bl02110IFIWC0l 1CV B 10211 OIFIWCO l 8CV ANALYTICAL METHODS LAB ID 18-02018-04 18-02018-05 18-02018-06 Total Strontium was analyzed using EIChroM Method SRWOl Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.

Gamma Spectroscopy was perf01med using EPA Method 901.1 Modified.

Laboratory qualifiers are as follows:

U - Result is less than the MDA.

ANALYTICAL RES UL TS Combined Standard Uncertainty is reported at 2-sigma value.

Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific.

MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.

TOT AL STRONTIUM Samples were prepared by aliquoting as appropriate and leaching in HN03. Samples were diluted appropriately. Strontium recovery carriers were added to each sample. Chemical separations were conducted using selective extractions. Strontium precipitate was mounted on tared filter media. Chemical recovery was determined by Strontium carrier mass determinations. Samples were counted by gas flow proportional counting and corrected for Yttrium-90 ingrowth.

Page 1 of 3

[225]

ANALYTICAL RESULTS CONTINUED TOT AL STRONTIUM CONTINUED Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are reported from Total Strontium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated a slightly high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.

TRITIUM A representative aliquot of each sample was equilibrated with Tritium free water. Equilibrates were transferred into round-bottomed distillation flasks and attached to single stage stills. A portion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were then counted by beta liquid scintillation.

Samples demonstrated acceptable results for all Tritium analyses. Results for laboratory fraction -05 (Client ID: B 10211 OIFIWCO 11 CV) demonstrated a slightly high method detection limit. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.

NICKEL-63 A representative aliquot of each sample was leached in HN03* Leachates were placed in an appropriately sized beaker. Stable elemental Nickel carrier was added to each sample prior to digestion. Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.

Samples demonstrated acceptable results for all Nickel-63 analyses. All results demonstrated slightly high method detection limits. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated a high relative percent difference and normalized difference. In this case duplicate variations were caused by the heterogeneous sample nature. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.

GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass/aliquot of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.

Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. Some results demonstrated slightly high method detection limits. Some sample results are greater than the method detection limits. These results are reported from the Canberra Gamma Apex "Nuclide MDA Report" and are not positive. These results are qualified as non-detect (U). The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Cesium-13 7 and Potassium-40 replicate Page 2 of 3

[226]

(

ANALYTICAL RESULTS CONTINUED GAMMA SPECTROSCOPY CONTINUED demonstrated a slightly high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Europium-152 replicate demonstrated a high relative percent difference and normalized difference. In this case duplicate variations were caused by the heterogeneous sample nature. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.

CERTIFICATION OF ACCURACY I ce1tify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her t*ig~:'.','° be accurate as verified by the following signature.

'~-~*-~\\

M.R. McDougan--*-

, \\ \\

Laboratory Manager

\\

\\

Date: 2/13/2018 Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please visit http://eberlineanalytical.com/ to provide us with feedback on our services, Page 3 of 3

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677118 Final Report of Analysis 101 Shiloh Blvd Analysis_ Category-ENVIRONMENTAL

-- ------------,-,---~,----*-w-,

Zion, IL 60099 Sample Matrix.*

so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 18-02018-01 LCS KNOWN 02/03/18 00:00 2/3/2018 2/6/2018 18-02018 Tritium LANL ER-210 Modified 2.25E+02 8.11E+OO pCiig f-----~----. -------.----------,,----~ ---------------"

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Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analvsis -~'~"'"V.

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

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18-02018

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677118 Final Report of Analysis 101 Shiloh Blvd Analysis Category:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample l

Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units 18-0201$..04 DO B1021101FIWC010CV 02/08/1813:10 2/3/2018 2/5/2018 18-02018 Actinium-228 EPA 901.1 Modified

-5.66E-01 2.74E+OO 2.74E+OO 3.99E+OO u

pCi/g

~------*0--*--". --**---------------**

02/08/18 13:10 2/3/2018 2/5/2018 18-02018 Silver-108m EPA901.1 Modified l

3.08E-01 8.50E-01 8.50E-01 6.82E-01 pCi/g 1&-02018-04 DO B1021101FIWC010CV u

18-02018 i Americium-241 18-02018-04 ;

DO 81021101FIWC010CV 02/08/18 13:10 2/3/2018 2/5/2018 EPA 901.1 Modified i

5.59E-01 : 7.05E-01 7.05E-01 1.11E+OO '

u pCi/g 18-0201$..04 I

DO I

8102110IFIWC010CV 02/08/18 13:10 2/3/2018 2/5/2018 18-02018 i 8arium-133 EPA 901.1 Modified 8.79E-01 ' 5.42E-01 5.44E-01 9.26E-01 u

pCi/g 18-0201&-04 DO 8102110IFIWC010CV 02/08/1813:10 l

2/3/2018 2/5/2018 1&-02018 8ismuth-214 EPA 901.1 Modified 1.02E+OO : 1.36E+OO 1.36E+OO 2.07E+OO u

pCi/g 18-02018-04 :

DO 81021101FIWC010CV 02/08/1813:10 2/3/2018 2/5/2018 18-02018 Cobalt-60 EPA 901.1 Modified 9.17E+OO ;

9.70E-01 1.08E+OO 6.78E-01 pCi/g 1&-02018-04 DO 8102110IFIWC010CV 02/08/18 13:10 ' 2/3/2018 2/5/2018 18-02018 Cesium-134 EPA 901.1 Modified I

1.04E-01 3.24E-01 I

3.24E-01 9.28E-01 u

pCi/g 18-02018 ;

i 18-02018-04 I

DO 8102110IFIWC010CV 02/08/18 13:10 I

2/3/2018 2/5/2018 Cesium-137 EPA 901.1 Modified 8.54E-01 I

8.59E-01 8.60E-01 1.43E+OO u

pCi/g

.. n DO B102110IFIWC010CV 02/08/1813:10 1 2/3/2018 2/5/2018 18-02018, Europium-152 EPA 901.1 Modified 1.64E+02 i

6.91E+OO 1.09E+01 3.96E+OO pCi/g 18-0201$..04 I DO 81021101FIWC010CV 02/08/1813:10 2/3/2018 2/5/2018 18-02018 j

!::~*-s*-*<<-154 EPA 901.1 Modified 4.92E+OO ! 1.64E+OO '

1.66E+OO 3.21E+OO u

pCi/g 18-0201$..04 i DO 8102110IFIWC010CV 02/08/18 13: 10

2/3/2018 2/5/2018 18-02018 cu,-~*-*,i-i 55 EPA 901.1 Modified 1.49E+OO 1.70E+OO i

1.70E+OO 2.85E+OO u

pCi/g 1&-02018-04 ;

DO 81021101FIWC010CV 02/08/18 13:10 2/3/2018 '

2/5/2018 18-02018, Holmium-166m EPA 901.1 Modified

-7.12E-01 1.22E+OO i 1.22E+OO 8.19E-01 u

pCi/g 1&-02018-04 ;

DO 81021101FIWC010CV 02/08/18 13:10 I 2/3/2018, 2/5/2018 18-02018 i lodine-129 EPA 901.1 Modified 3.87E+OO '

3.92E+OO I

3.93E+OO 5.34E+OO I

u pCi/g 18-02018-04 1 DO i

8102110IFIWC010CV 02/08/1813:10

, 2/3/2018 2/5/2018 18-02018 Potassium-40 EPA 901.1 Modified 7.15E+OO 4.48E+OO : 4.49E+OO 8.45E+OO '

u pCi/g 1&-02018-04 :

DO 810211 OIFIWC01 OCV 02/08/18 13:10 2/3/2018 2/5/2018 18-02018 l

,.,_,,M_,, ___ :

EPA 901.1 Modified

-4.26E-01 ;

6.75E-01 6.76E-01 9.57E-01 u

I pCi/g 18-02018-04 I

DO B102110IFIWC010CV 02/08/18 13:10

2/3/2018 2/5/2018 18-02018 Niobium-94 EPA901.1 Modified 4.65E-01 i

5.08E-01 I

5.09E-01 9.96E-01 u

pCi/g an *-

DO '

81021,OIFIWC010CV 02/08/18 13:10

! 2/3/2018 2/5/2018 18-02018 Lead-210 EPA901.1 Modified 3.78E+02 4.69E+01 5.07E+01 3.00E+01 pCi/g 18-02018-04 DO 8102110IFIWC010CV 02/08/18 13:10 2/3/2018 2/5/2018 18-02018 I Lead-212 EPA 901.1 Modified

-3.82E-02 f

8.55E-01 i

8.55E-01 1.33E+OO u

pCi/g 18-0201s..04 I DO B102110IFIWC010CV 02/08/1813:10 2/3/2018 2/5/2018 18-02018 I Lead-214 EPA 901.1 Modified 1.16E+OO 1.07E+OO 1.07E+OO 1.77E+OO u

I pCi/g 18-0201$..04 :

DO 81021101FIWC010CV 02/08/1813:10

, 2/3/2018 2/5/2018 18-02018 EPA 901.1 Modified

-2.09E+02 i 3.93E+01 4.07E+01 6.12E+OO u

pCi/g

~e-:::~:-G"'

i DO 81021101FIWC010CV 02/08/1813:10

! 2/3/2018 2/5/2018 18-02018 i Radium-226 EPA 901.1 Modified 1.02E+OO l~.66E+OO 1.36E+OO 2.07E+OO u

pCi/g 18-02018-04 /

DO 810211u1e1vv1,,u,vvV 02/08/18 13:10 i 2/3/2018 2/5/2018 18-02018 j Antimony-125 EPA901.1 Modified

-8.46E-01 1.66E+OO 2.03E+OO I u

i pCi/g 18-02018-04 DO 810211 OIFIWC01 OCV 02/08/18 13:10

i.

2/3/2018 2/5/2018 18-02018 i Th-"**- 00

  • EPA 901.1 Modified 7.74E-01

.02E+OO 7.02E+OO 1.04E+01 u

pCi/g 18-02018-04 !

DO 81021101FIWC010CV 02/08/18 13:10 i 2/3/2018 2/5/2018 18-02018 !

Thallium-208 EPA 901.1 Modified

-1.95E+OO

.70E+OO i 1.71E+OO 1.69E+OO 1

u pCi/g

  • n i

DO 8102110IFIWC010CV 02/08/18 13:10 2/3/2018 2/5/2018 18-02018 !

,,........ ;.,..... _?':!,t:;.

EPA 901.1 Modified 3.67E+OO 9.37E+OO 9.37E+OO 4.76E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Norrnal Sample;DO=Duplicate Original;U=Non-detect I EBERLINE AL YTI CAL CORPC_R_.A_T_I_O_N _____.

601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[231]

Printed: 2/13/2018 2:25 PM Page 5 of 6 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02018

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Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analvsis Cateaorv:

ENVIRONMENTAL

---------~---*---~ ***----------~--~--

Zion, IL 60099 Sample Matrix:

  • so Lab Sample Client Sample
Receipt Analysis Batch

/

Report ID Type ID Date Date Date ID Analyte Method l

Result cu CSU MDA Qualifier Units 18-02018-05 TRG 81021101FIWC011CV 02/08/1814:30 2/3/2018 2/5/2018 18-02018 Actinium-228 EPA 901.1 Modified 6.25E-01 6.01E-01 6.01E-01 1.10E+OO u

pCi/g 18-02018--05 TRG 81021101FIWC011CV 02/08/18 14:30 l 2/3/2018 2/5/2018 18-02018

  • Silver-108m EPA 901.1 Modified 2.49E-02 1.34E-01 1.34E-01 1.67E-01 u

pCi/g 18-02018-05 i TRG 8102110IFIWC011CV 02/08/18 14:30 2/3/2018 2/5/2018 18-02018 Arnencium-241 EPA 901.1 Modified

-2.66E-01 2.88E-01 2.88E-01 3.17E-01 u

pCi/g 18-02018-05 TRG 8102110IFIWC011CV 02/08/18 14:30 : 2/3/2018 2/5/2018 18-02018 8arium-133 EPA 901.1 Modified 7.34E-03 1.18E-01 1.18E-01 3.17E-01 u

pCi/g 18-02018-05 :

TRG 8102110IFIWC011CV 02/08/18 14:30

2/3/2018 2/5/2018 18-02018 :

8ismuth-214 EPA 901.1 Modified 8.45E-01 3.05E-01 3.09E-01 5.92E-01 I

pCi/g 18-02018-05 j TRG 810211 OIFIWC011 CV 02/08/18 14:30 2/3/2018 2/5/2018 18-02018 Cobalt-60 EPA 901.1 Modified 6.31E-02 1.96E-01 1.96E-01 3.08E-01 u

pCi/g 18-02018-05,

TRG 8102110IFIWC011CV 02/08/18 14:30 i 2/3/2018 2/5/2018 18-02018 :

Cesium-134 EPA 901.1 Modified

/

-4.12E-03 6.81E-02 6.81E-02 2.79E-01 u

pCi/g 18-02018--05 !

TRG 81021101FIWC011CV 02/08/18 14:30 2/3/2018 2/5/2018 18-02018 i Cesium-137 EPA 901.1 Modified

-3.59E-02 1.56E-01 1.56E-01 2.32E-01 u

pCi/g 18-02018-05 :

TRG 81021101FIWC011CV 02/08/18 14:30 2/3/2018 2/5/2018 18-02018 Europium-152 EPA 901.1 Modified 3.64E+OO : 4.34E-01 4.72E-01 8.63E-01 pCi/g 18-02018-05 i TRG 810211 OIFIWC011 CV 02/08/18 14:30 2/3/2018 2/5/2018 i

18-02018 Europium-154 EPA901.1 Modified

-3.80E-02 :

2.11E-01 2.11E-01 5.58E-01 u

pCi/g 18-02018--05 TRG B102110IFIWC011CV 02/08/18 14:30 2/3/2018 ! 2/5/2018 18-02018

v, veov, 155 EPA 901.1 Modified 1.22E-01 2.82E-01 2.82E-01 4.77E-01 u

pCi/g 18--02018--05 TRG 81021101FIWC011CV 02/08/18 14:30 2/3/2018 2/5/2018 18-02018 Holmium-166m EPA 901.1 Modified

-1.18E-02 :

2.19E-01 2.19E-01 2.02E-01 u

pCi/g f--*--------: -----,,----.

18-02018-05 TRG 81021101FIWC011CV 02/08/18 14 :30 2/3/2018 2/5/2018 18-02018 lodine-129 EPA 901.1 Modified

-6.36E-03 8.45E-02 8.45E-02 1.10E-01 i

u pCi/g 18-02018-05 :

TRG B102110IFIWC011CV 02/08/18 14:30 2/3/2018 2/5/2018 18-02018 Potassium-40 EPA901.1 Modified 8.79E+OO 2.33E+OO 2.37E+OO 1.18E+OO pCi/g 18-020 18-05 :

TRG 8102110IFIWC011CV 02/08/18 14:30 i

2/3/2018, 2/5/2018 18-02018 :

C EPA 901.1 Modified

-8.25E-03 I

7.65E-02 7.65E-02 1.94E-01 u

pCi/g

....... ~...................,

18-02018-05 i TRG 81021101FIWC011CV 02/08/18 14:30 2/3/2018 2/5/2018 18-02018 Niobium-94 EPA 901.1 Modified

-3.16E-02 1.53E-01 1.53E-01 2.07E-01 u

pCi/g 18-02018-05 i TRG 8102110IFIWC011 CV 02/08/18 14:30 2/3/2018 2/5/2018 18-02018 Lead-210 EPA 901.1 Modified 3.81E+OO 1

2.30E+OO 2.31E+OO 3.67E+OO :

pCi/g 18-02018-05 i TRG 8102110IFIWC011CV 02/08/18 14:30 ' 2/3/2018 2/5/2018 18-02018 I

Lead-212 EPA 901.1 Modified 2.41E-01 2.74E-01. 2.75E-01 4.58E-01 u

pCi/g 18-02018--05 :

TRG 81021101FIWC011CV 02/08/18 14:30 2/3/2018 2/5/2018 : 18-02018 I Lead-214 EPA 901.1 Modified 9.06E-01 3.03E-01 3.07E-01 1.06E+OO u

I pCi/g 18-02018--05 !

TRG 8102110IFIWC011CV 02/08/18 14:30 i 2/3/2018 2/5/2018 18-02018 I Promethium-145 EPA 901.1 Modified

-2.41E-01 '

3.56E-01 3.56E-01 4.27E-01 u

pCi/g 18-02018-05 I

TRG 8102110IFIWC011CV 02/08/18 14:30 2/3/2018 2/5/2018 18-02018 Radium-226 EPA 901.1 Modified 8.45E-01 I

3.05E-01 3.09E-01 5.92E-01 '

pCi/g 18-02018-05 TRG i

B102110IFIWC011CV 02/08/18 14:30 2/3/2018 I 2/5/2018 18--02018 :

~........... *~~

EPA 901.1 Modified

-1.10E-01 3.66E-01 3.66E-01 5.36E-01 u

I pCi/g 18-02018-05 TRG B102110IFIWC011CV 02/08/18 14:30 : 2/3/2018, 2/5/2018 18-02018 I Thorium-234 EPA 901.1 Modified 4.67E+OO 3.76E+OO 3.76E+OO 6.18E+OO u

pCi/g 18-02018-05 TRG 810211 OIFIWC011 CV 02/08/18 14:30 2/3/2018 2/5/2018 18-02018 Tt...::::~. :::

EPA901.1 Modified i

1.06E+OO 1

6.53E-01 I

6.55E-01 9.86E-01 pCi/g 18--02018--05 TRG 81021101FIWC011CV 02/08/18 14:30

! 2/3/2018 2/5/2018 18-02018 i Uranium-235 EPA 901.1 Modified

-6.70E-01 1.67E+OO 1.67E+OO 1.11E+OO u

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SERV!CES I EBERLINE AL YTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[232]

Printed: 2/13/2018 2:25 PM Page 6 of 6 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-02018

****----'""'*---*-**---*~'-**se*---..--**---*----._... ****-*---**m.. **-*-**

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677118 Final Report of Analysis

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101 Shiloh Blvd Analysis :-*-~-*

ENVIRONMENTAL

-"--------------~------------------

Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 18-02018-06 TRG B102110IFIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 18-02018 j Actinium-228 EPA 901.1 Modified

-4.18E-01 2.23E+OO 2.23E+OO 3.22E+OO u

pCi/g 18-02018-06 j TRG B102110IFIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 18-02018 !

Silver-108m EPA 901.1 Modified i

1.27E+OO 7.20E-01 7.23E-01 6.68E-01 u

pCi/g 18-02018-06 TRG B102110IFIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 18-02018 Americium-241 EPA 901.1 Modified 1.80E-01 7.93E-01 7.93E-01 1.01E+OO u

pCi/g 18-02018-06 :

TRG B102110IFIWC018CV 02/08/18 13:50

2/3/2018 2/5/2018 18-02018 Barium-133 EPA 901.1 Modified

-7.91E-02 3.27E-01 i

3.27E-01 9.71E-01 u

pCi/g 18-02018-06 :

TRG B102110IFIWC018CV 02/08/18 13:50 i 2/3/2018 2/5/2018 18-02018,

Bismuth-214 EPA 901.1 Modified 1.28E+OO 1.24E+OO : 1.24E+OO 1.42E+OO u

pCi/g 18-02018-06 TRG B102110IFIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 18-02018,

Cobalt-60 EPA 901.1 Modified 1.34E+01 9.82E-01 1.20E+OO 1.02E+OO pCi/g 18-02018-06 ;

TRG B102110IFIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 18-02018 '

Cesium-134 EPA 901.1 Modified

-1.39E-02 !

3.37E-01 3.37E-01 7.68E-01 u

pCi/g 18-02018-06 TRG B102110IFIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 18-02018 I Cesium-137 EPA 901.1 Modified 4.94E-02 :

6.40E-01 i 6.40E-01 9.34E-01 u

pCi/g

<--**----~'*--

18-02018 i 18-02018-06 TRG B1021101FIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 Europium-152 EPA 901.1 Modified 2.23E+02 7.75E+OO ;

1.38E+01 4.54E+OO pCi/g

~---------

18-02018-06 ;

TRG j

B1021101FIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 18-02018 : Europium-154 EPA 901.1 Modified 7.20E+OO 1.47E+OO 1.52E+OO 2.62E+OO u

pCi/g 18-02018-06 l TRG B1021101FIWC018CV 02/08/18 13:50 : 2/3/2018 2/5/2018 18-02018 : Europium-155 EPA901.1 Modified 2.83E+OO : 1.11E+OO i

1.12E+OO 1.77E+OO u

pCi/g 18-02018-06 i TRG B1021101FIWC018CV 02/08/18 13:50 i 2/3/2018 2/5/2018 18-02018 Holmium-166m EPA901.1 Modified

-3.13E-01 ! 1.06E+OO 1.06E+OO 6.27E-01 u

pCi/g 18-02018-06 I TRG B102110IFIWC018CV 02/08/18 13:50

2/3/2018 2/5/2018 18-02018 lodine-129 EPA901.1 Modified 1.19E+OO 3.37E-01 3.42E-01 1.59E+OO u

pCi/g

<~ :: on AC !

8102110IFIWC018CV 02/08/18 13:50 : 2/3/2018 2/5/2018 18-02018 :

Potassium-40 EPA 901.1 Modified

5.18E+OO 3.56E+OO 3.57E+OO 5.24E+OO u

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~--

18-02018-06 TRG B102110IFIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 18-02018 r

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pCi/g 18-02018-06 i TRG B102110IFIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 18-02018 '

Niobium-94 EPA 901.1 Modified

-2.90E+OO :

1.04E+OO : 1.05E+OO 7.84E-01 u

pCi/g 18-02018-06 i TRG i B10211u1c1vv1.,u1o1.,v 02/08/18 13:50

2/3/2018 2/5/2018 18-02018 Lead-210 EPA 901.1 Modified 2.85E+02 '

2.44E+01 2.85E+01 1.95E+01 u

pCi/g 18-02018-06 :

TRG 8102110IFIWC018CV 02/08/18 13:50 : 2/3/2018 2/5/2018 18-02018 :

Lead-212 EPA 901.1 Modified

-8.63E-01 !

6.84E-01 : 6.85E-01 1.04E+OO u

pCi/g 18-02018-06 I TRG 81021101FIWC018CV 02/08/18 13:50

2/3/2018 ; 2/5/2018 18-02018 :

Lead-214 EPA 901.1 Modified 4.36E+OO j 1.20E+OO 1.22E+OO 3.37E+OO pCi/g 18-02018-06 i TRG B102110IFIWC018CV 02/08/18 13:50 2/3/2018

  • 2/5/2018 18-02018 Promethium-145 EPA 901.1 Modified i

6.90E+OO ! 1.96E+OO 1.99E+OO. 2.50E+OO u

pCi/g 18-02018-06 TRG B102110IFIWC018CV 02/08/1813:50

2/3/2018 : 2/5/2018 18-02018 !

Radium-226 EPA901.1 Modified i

1.28E+OO : 1.24E+OO l 1.24E+OO 1.42E+OO u

pCi/g 18-02018 i Antimony-125 I

pCi/g 18-02018-06

~

8102110IFIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 EPA 901.1 Modified

-6.13E-03 1.40E+OO 1.40E+OO 2.02E+OO u

pCi/g 18-02018-06 j TRG B1021101FIWC018CV 02/08/18 13:50 2/3/2018, 2/5/2018 18-02018 i Thorium-234 EPA901.1 Modified 9.50E-01 7.89E+OO 7.89E+OO 1.01E+01 u

18-02018-06 TRG B1021101FIWC018CV 02/08/18 13:50

! 2/3/2018 2/5/2018 18-02018

  • Thallium-208 EPA 901.1 Modified 1.13E+OO 1.79E+OO 1.79E+OO 1.28E+OO u

pCi/g 18-02018-06 ;

TRG B102110IFIWC018CV 02/08/18 13:50 2/3/2018 2/5/2018 18-02018 :

Uranium-235 EPA 901.1 Modified

-4.75E+OO ;

5.96E+OO 5.97E+OO 3.87E+OO i u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

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EBERLINE SERVICES SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[233]

ZIONSOLUTIONSru An Energ:,-Solufiona Con1)8ny Sample ID Sample Matrix Log B102110IFIWC010CV NIA Concrete B102110IFIWC011CV NIA Concrete B102110IFIWCOI8CV NIA Concrete Laboratory:

Eberline Labs Relinquished by:

J. ALEX BOHACHEFF Relinquished by:

F:idJa 1) F Ki'Cskf;, f Relinquished by:

Relinquished by:

Comments ANALYSIS 5 ROC-HTD RE: Email to Mike McDougall PRIORITY 24 hour2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> turnaround PO# 677118 1 a-0201s REC'D FEB O 3 2018 ZS-WM-131 Revision 0 Information Use -

Chain-of-Custody Form Sample Sample Container Sample Date Sample Time Analysis Preservative Remarks Type Vol Unit Type Qty Type cm3 6 ROC.

Concrete 57.94 Puck 211/2018 1310 HTD None 0.0"-0.5" 5 Koc Concrete 57.94 cm3 Puck 211/2018 1430 HTD None 0.0"-0.5" 5 ROC.

Concrete 57.94 cm3 Puck 211/2018 1350 HTD None 0.0"-0.5" Date Submitted To Lab:

Ship Container No.:

Cooler Temperature:

Airbill Number: re.cl/}(

NIA NIA

<is! 0 7 DfifS 67r/J Date Time:

Received by:

Date: (mmlddlyyyy):

Time:

(mmlddlyyyy):

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Time:

(m1n/dd/2It O)JO

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(5)Jo2/~,rs D'700 Date I

Time:

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