ML21067A184

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Gamma Spectroscopy Report for L2-10214C-RJGS-001-SM
ML21067A184
Person / Time
Site: Zion  File:ZionSolutions icon.png
Issue date: 05/08/2020
From: Mcdougall M
Eberline Analytical
To: Wood G
Office of Nuclear Material Safety and Safeguards, ZionSolutions
Shared Package
ML21067A225 List:
References
20-04072-OR, EBS-OR-47182, ZS-2021-0001
Download: ML21067A184 (27)
v • d • e


Text

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ANALYTICAL EBS-OR-47182 May 8, 2020 Gerald Wood Zion Solutions, LLC 2701 Deborah Avenue Zion, IL 60099 SAMPLE RECEIPT CASE NARRATIVE Work Order # 20-04072-OR EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TENNESSEE 37830 PHONE (865) 481--0683 FAX (865) 483-1+621 This work order contains nine solid samples received 04/25/2020. Samples were analyzed for Isotopic Plutonium, Plutonium-241, Neptunium-237, Americium~241/243, Curium-243/244, Total Strontium, Technetium-99, Tritium, Carbon-14, Promethium-147, Nickel-59/63, Iron-55 and by Gamma Spectroscopy.

CLIENT ID B 1-06202A-FSWC-040-CV B l-06214A-FSFC-001-CV B2-08101A-BJFC-007-CV 0 0-0 5 B2-08101A-BJFC-007-CV 0 5-1 0 B2-08201-CJWC-A018-CV 0 0-0 5 ANALYTICAL METHODS LABID 20-04072-04 20-04072-05 20-04072-06 20-04072-07 20-04072-08 CLIENT ID B2-08201-CJWC-A0 18-CV 0 5-1 0 L2-l 02 l 4C-RJGS-00 1-SM-A Ll-12109L-CJGS-001-SB-A Ll-12106L-CJGS-00 1-SB-A LAB ID 20-04072-09 20-04072-10 20-04072-11 20-04072-12 Isotopic Plutonium and Plutonium-241 were analyzed using Method EML Pu-02 Modified. Neptunium-237 was analyzed using EIChroM Method ACW08 Modified. Americium and Curium were analyzed using Method EML Am-01 Modified. Total Strontium was analyzed using EIChroM Method SRW0l Modified. Technetium-99 was analyzed using EIChroM Method TCS0l Modified. Tritium was performed using Method LANL ER-210 Modified. Carbon-14 was perfonned using EPA Method 520.0 Modified. Promethium-147 was performed using Method EML Pm-01 Modified. Nickel-59/63 was performed using Method ASTM 3500-Ni Modified. Iron-55 was performed using EML Method Fe-01-01 Modified. Gamma Spectroscopy was performed using EPA Method 901.1 Modified.

Laboratory qualifiers are as follows:

U - Result is less than the MDA.

ANALYTICAL RESULTS Combined Standard Uncertainty is reported at 1-sigma value.

Page 1 of 6

ANALYTICAL RESULTS CONTINUED Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific. MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.

ISOTOPIC PLUTONIUM Samples were prepared by removing representative aliquots followed by mixed acid digestions as appropriate. Plutonium was selectively extracted by ion exchange. Plutonium was eluted, micro-precipitated and mounted on micro-porous filter media. Sample activities were determined by alpha spectroscopy using energy specific regions of interest for Plutonium-238 and Plutonium-239. Chemical recovery was determined using a Plutonium-242 tracer. Activity of the Plutonium-242 tracer was determined by alpha spectroscopy using an energy specific region of interest.

Samples demonstrated acceptable results for all Plutonium analyses Chemical recovery was acceptable for all samples. The Plutonium-238 and Plutonium-239/240 method blank demonstrated acceptable results. Results for the Plutonium-238 and Plutonium-239/240 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Plutonium-238 and Plutonium-239 laboratory control sample demonstrated an acceptable percent recovery.

PLUTONIUM-241 Following sample analysis for Isotopic Plutonium, filter media used was dissolved. Dissolved samples were placed into scintillation vials, scintillation cocktail was added and Plutonium-241 was detennined by liquid scintillation counting. Analytical tracer recovery was determined by yields from the Isotopic Plutonium tracer.

Samples demonstrated acceptable results for all Plutonium-241 analyses. All sample results demonstrated slightly high method detection limits. Chemical recovery was acceptable for all samples. The Plutonium-241 method blank demonstrated an acceptable result. Results for the Plutonium-241 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Plutonium-241 laboratory control sample demonstrated an acceptable percent recovery.

NEPTUNIUM-23 7 Samples were prepared by removing representative aliquots followed by mixed acid digestions as appropriate. Sample residues were dissolved in dilute acid and Neptunium was selectively separated using EIChroM stabilized selective resins. Neptunium was eluted, micro-precipitated and mounted on micro-porous filter media. Sample activities were determined by alpha spectroscopy using an energy specific region of interest for Neptunium-237 activity. A Neptunium-239 tracer was used for chemical yields, which was determined by beta proportional counting.

Samples demonstrated acceptable results for all Neptunium-237 analyses. Chemical recovery was acceptable for all samples. The Neptunium-237 method blank demonstrated an acceptable result. Results for the Neptunium-237 duplicate demonstrated a high relative percent difference; however, nonnalized difference is within acceptable limits for the analytical technique. Results for the Neptunium-237 laboratory control sample demonstrated an acceptable percent recovery.

Page 2 of 6

ANALYTICAL RESULTS CONTINUED AMERICIUM-241 Samples were prepared by removing representative aliquots followed by mixed acid digestions as appropriate. Samples were co-precipitated with Calcium Phosphate. Precipitates were nitrate converted using Nitric acid and Aluminum Nitrate. The Americium fractions were separated from other elements using the EIChroM, TRU and UTEV A resins. The separated Americium fractions were mounted on a membrane filter by micro-precipitation and counted on the alpha spectroscopy system. Analytical tracer recovery was determined using an Americium-243 standard and subsequent activity determination by alpha spectroscopy.

Samples demonstrated acceptable results for all Americium-241 analyses. Chemical recovery was acceptable for all samples. The Americium-241 method blank demonstrated an acceptable result. Results for the Americium-241 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Americium-241 laboratory control sample demonstrated an acceptable percent recovery.

AMERICIUM-243 Samples were prepared by removing representative aliquots followed by mixed acid digestions as appropriate. Samples were co-precipitated with Calcium Phosphate. Precipitates were nitrate converted using Nitric acid and Aluminum Nitrate. The Americium fractions were separated from other elements using the EIChroM, TRU and UTEV A resins. The separated Americium fractions were mounted on a membrane filter by micro-precipitation and counted on the alpha spectroscopy system. Analytical tracer recovery was determined using a Curium-244 standard and subsequent activity determination by alpha spectroscopy.

Samples demonstrated acceptable results for all Americium-243 analyses. Chemical recovery was low for laboratory fraction -06 (Client ID: B2-08101A-BJFC-007-CV O 0-0 5). Chemical recovery was acceptable for all other samples. The Americium-243 method blank demonstrated an acceptable result.

Results for the Americium-243 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Americium-243 laboratory control sample demonstrated an acceptable percent recovery.

CURIUM-243/244 Samples were prepared by removing representative aliquots followed by mixed acid digestions as appropriate. Samples were co-precipitated with Calcium Phosphate. Precipitates were nitrate converted using Nitric acid and Aluminum Nitrate. The Curium fractions were separated from other elements using the EIChroM, TRU and UTEV A resins. The separated Curium fractions were mounted on a membrane filter by micro-precipitation and counted on the alpha spectroscopy system. Analytical tracer recovery was determined using an Americium-243 standard and subsequent activity determination by alpha spectroscopy.

Samples demonstrated acceptable results for all Curium-243/244 analyses. Chemical recovery was acceptable for all samples. The Curium-243/244 method blank demonstrated an acceptable result. Results for the Curium-243/244 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Curium-244 laboratory control sample demonstrated an acceptable percent recovery.

Page 3 of 6

ANALYTICAL RESULTS CONTINUED TOTAL STRONTIUM Samples were prepared by acid digestion as appropriate for the matrix. Digested samples were acidified and selectively extracted and precipitated. Precipitates were then mounted on 47mm filters. Filters were reweighed to detennine aliquot size. Sample activities were determined by gas flow proportional counting.

Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 is reported from Total Strontium assuming secular equilibrium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated a high relative percent difference; however, nonnalized difference is within acceptable limits for the analytical technique. Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.

TECHNETIUM-99 A representative aliquot was removed from each sample followed by leaching in acids. Samples were prepared by oxidative reactions with Nitric acid and Hydrogen Peroxide. After complete oxidization, Technetium was selectively extracted using EIChroM stabilized resins. Special cleanup chemistry was conducted for complete removal of interferences associated with Uranium. Processed resins were transferred to liquid scintillation vials, scintillation cocktail was added, and samples were counted by beta liquid scintillation.

Samples demonstrated acceptable results for all Technetium-99 analyses. The Technetium-99 method blank demonstrated an acceptable result. Results for the Technetium-99 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Technetium-99 laboratory control sample demonstrated an acceptable percent recovery.

TRITIUM A representative aliquot of each sample was equilibrated with Tritium free water. Equilibrates were transferred into round-bottomed distillation flasks and attached to single stage stills. A portion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were counted by beta liquid scintillation.

Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique.

Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.

CARBON-14 A representative aliquot of each sample was placed into a I-liter reaction vessel. A carbonate solution was added. Samples were oxidized using Potassium Permanganate. Carbon Dioxide was evolved and Carbon-14 was captured into Harvey brand, Carb-Sorb cocktail. Carbon-14 beta emissions were then determined by beta liquid scintillation using an energy selective region.

Page 4 of 6

ANALYTICAL RESULTS CONTINUED CARBON-14 CONTINUED Samples demonstrated acceptable results for all Carbon-14 analyses. The Carbon-14 method blank demonstrated an acceptable result. Results for the Carbon-14 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Carbon-14 laboratory control sample demonstrated an acceptable percent recovery.

PROMETHIUM-147 Samples were prepared by leaching in HNO3. Aliquots were taken to near dryness. Sample residues were dissolved in deionized water. The pH of each sample was adjusted with HNO3. Samples were extracted with scintillation extractant. Organic phase of each sample was transferred to scintillation vials.

Promethium-14 7 was determined by liquid scintillation counting.

Samples demonstrated acceptable results for all Promethium-147 analyses. The Promethium-147 method blank demonstrated an acceptable result. Results for the Promethium-14 7 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Promethium-147 laboratory control sample demonstrated an acceptable percent recovery.

NICKEL-63 A representative aliquot of each sample was prepared by leaching in acids. Aliquots were placed into appropriately sized beakers. Stable elemental Nickel carrier was added to each sample prior to digestion.

Samples were digested in concentrated Nitric acid. After digestion, each sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added, and Nickel-63 activity was determined by beta liquid scintillation.

Samples demonstrated acceptable results for all Nickel-63 analyses. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.

NICKEL-59 Representative aliquots were removed from samples and placed into Petri geometry containers. Samples were counted by low-energy photon spectroscopy.

Samples demonstrated acceptable results for all Nickel-59 analyses. The Nickel-59 method blank demonstrated an acceptable result. Results for the Nickel-59 replicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the lron-55 laborato1y control sample demonstrated a statistically acceptable percent recovery.

Page 5 of 6

ANALYTICAL RESULTS CONTINUED IRON-55 Representative aliquots were removed from samples and placed into Petri geometry containers. Samples were counted by low-energy photon spectroscopy.

Samples demonstrated acceptable results for all Iron-55 analyses. The Iron-55 method blank demonstrated an acceptable result. Results for the Iron-55 replicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique.

Results for the Iron-55 laboratory control sample demonstrated an acceptable percent recovery.

GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.

Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. Cobalt-60 results for laboratory fraction -08 (Client ID: B2-08201-CJWC-A0 18-CV 0 0-0 5) demonstrated a slightly high method detection limit. The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Bismuth-214 and Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Thorium-234 replicate demonstrated a high relative percent; however, normalized difference is within acceptable limits for the analytical technique.

Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.

CERTIFICATION OF ACCURACY I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her

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ac te as verified by the following signature.

M.R. McDougall Laboratory Manager Date: 11/13/2019 Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please visit http://eberlineanalytical.com/ to provide us with feedback on our services.

Page 6 of 6

Printed: 5/7/2020 9:24 PM Eberline Analytical Final Report of Analysis I

ReE_orf To:

Gerald Wood Zion Solutions

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20-04072 Purchase Order:

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-- ------1 Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID I

Date Date Date ID Analyte Method Result CU CSU MDA Qualifier Units 20-04072-01,

LCS KNOWN 04/25/20 00:00 4/25/2020 4/30/2020 20-04072 Americium-241 EML Am-01 Modified 5.55E+OO 1.66E-01 pCi/g 20-04072-01 '

LCS SPIKE 04/25/2000:00 4/25/2020 4/30/2020 20-04072 Americium-241 EMLAm-01 Modified 5.47E+OO

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---1.10E+OO 1.40E-01 pCi/g 20-04072-02 MBL BLANK 04/25/20 00:00 4/25/2020 4/30/2020 20-04072 Americium-241--

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Americium-241 EMLAm-01 Modified 6.44E-02 8.10E-02 8.12E-02 1.29E-01 U

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20-04072-05.

TRG 81-06214A-FSFC-001-CV 05/05/18 15:15 4/25/2020 4/30/2020 20-04072 Americium-241 EML Am-01 Modified

-4.34E-04 4.60E-02 4.60E-02 1.37E-01 U

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05/09/12 14:22

4/25/2020 4/30/2020 20-04072 '

Americium-241 EML Am-01 Modified 4.23E-02 5'.'-iiic:02 5.14E-02

---6.24E-02 u

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  • 20:04072-07 TRG B2-08101A-BJFC-007-CV O 5-1 0 05/09/12 14:22 4/25/2020 4/30/2020 20-04072 Americium-241 EML Am-01 Modified 2.06E-02 5.15E-02 5.16E-02 1.07E-01 U

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4.50E-02 4.50E-02 1.27E-01 U

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20-04072-09 TRG 82-08201-CJWC-A018-CVO 5-1 0 05/10/1212:56 4/25/2020 4/30/2020 20-04072 Americium-241 EMLAm-01 Modified 1.73E-02 i 5.61E-02 5.61E-02 1.16E-01 U

pCi/g 20-04072-10 TRG L2-10214C-RJGS-001-SM-A___

05/07/19 07:45 4/25/2020 4/30/202Ci" 20-04072

,,;,;:;;;;,;~;~;;;:241 EML Am-01 Modified I 3.36E-02 5.17E-02**+-*;;;:;-~:02 8.85E-02 i

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4/25/2020 4/30/2020 20-04072 Americium-243 EML Am-01 Modified 6.05E+OO 1.82E-01 pCi/g 20-04072-01 LCS -----SPIKE 04/25/20 00:00 4/25/2020 4/30/2020 20-04072 Americium-243 EML*;;;;:a,*M~dified 5.41E+OO 7.46E-01 1.10E+OO 9.62E-02 pCi/g 20-04072-02 :,,, -MBL BLANK 04/25/20 00:00
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pCi/g 20-04072-03 DUP 81-06202A-FSWC-040-CV 06/18/1810:30 f 4/25/2020 4/30/2020 20-04072

  • Americium-243 EML Am-01 Modified 7.10E-02 i 7.33E-02 7.40E-02 7.74E-02 U

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pCi/g 20-04072-06 TRG B2-08101A-BJFC-007-CVO 0-0 5 05/09/1214:22 4/25/2020 4/30/2020 20-04072.

Americium-243 EML Am-01 Modified 2.02E-01 3.46E-01 3.47E-01 6.07E-01 U

pCi/g 20-04072-07 TRG B2-08101A-BJFC-007-CV05-10 05/09/1214:22 4/25/2020 i 4/30/2020 20-04072 Americium-243 EMLAm-01 Modified 5.82E-02 7.03E-02 7.09E-02 8.58E-02 U

pCi/g 20-04072-08 7 - TRG___

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Americium-243 EMLAm-01 Modified 6.77E-02 7.96E-02 8.03E-02 1.17E-01 U

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ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 5/7/2020 9:23 PM Eberline Analytical Final Report of Analysis Rep_ort To:

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Report ID Type ID Date Date Date ID na yte et o esu t M

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LCS KNOWN 04/25/20 00:00 4/25/2020 4/30/2020 20-04072 Curium-243/244 EML Am-01 Modified 5.99E+00 1.08E-01 pCilg l-~0_:?~?.72-01 i LCS SPIKE 04/25/20 00:00 4/25/2020 4/30/2020

  • 20-::-04072 Curium-243/244 EML Am-01 Modified

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DUP B1-06202A-FSWC-040-CV 06/18/18 10:30 4125/2020 4/30/2020 20-04072 Curium-243/244 EML Am-01 Modified 2.29E-o£***

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pCi/g I 20-04072-08 TRG B2-08201-CJWC-A018-CV00-05 05/10/1212:56

4/25/2020 4/30/2020 20-04072 Curium-243/244 EMLAm-01 Modified 4.05E-02 6.63E-02 6.64E-02 i

1.16E-01 U

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20-04072-01 LCS KNOWN 04/25/20 00:00 4125/2020 4127/2020 20-04072 Carbon-14 EPA520.0 Modified 1.32E+03 3.70E+01 1

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.*... 1.:.3_~E+03 9.67E+00 1.81 E+02 I 4.08E+00 pCi/g...

20-04072-02 MBL BLANK 04/25/20 00:00 4/25/2020 4/27/2020 20-04072 Carbon-14 EPA 520.0 Modified

-3.73E-01 4.65E-01 4.68E-01 7.99E-01 U

pCi/g 20-04072-03,

DUP B1-06202A-FSWC-040-CV 06/18/1810:30 4/25/2020 4/27/2020 20-04072 '

Carbon-14 EPA520.0 Modified

. -5.57E-01

. 3.64E-01 3.72E-01 6.32E-01 U

pCi/g 20-04072-04.

DO **:****;:;J~~202A-FSWC-040-CV 06/18/1810:30 4/25/2020 4/27/2020 20-04072 '

Carbon-14 EPA~~?:.~_1".lodified

-4.31E-01 3.70§:01 3.75E-01 6.39E-01 --:** ***u*-*

pCi/g I 20-04072-05 TRG B1-06214A-FSFC-001-CV 05/05/1815:15 4/25/2020 4/28/2020 20-04072 Carbon-14 EPA520.0 Modified

-6.32E-01 3.49E-01 3.60E-01 6.09E-01 i

U pCi/g 20-04072-06 TRG B2-08101A-BJFC-007-CV00-05 05/09/1214:22 4/25/2020' 4/28/2020. 20-04072 :

Carbon-14 EPA520.0 Modified

-456E=o1***:* 3.63E-01 3.69E-01--~* 6.28E-01 i U

pCi/g 1---*-

20-04072-07 TRG B2-08101A-BJFC-00~:_<:_V 0 5-1 0 05/09/12 14:22 4/25/2020 4/28/2020 20-04072 Carbon-14 EPA 520.0 Modified

-2.87E-01 4.0~§:_01 4.04E-01 6.91 E-01 U

pCilg 20-04072-08 TRG B2-08201-CJWC-A018-CV 0 0-0 5 05/10/12 12:56 4/25/2020 4/28/2020 20-04072 Carbon-14 EPA 520.0 Modified

-6.71 E-01 3.91 E-01 4.02E-01 6.81 E-01 U

pCi/g I 20-04072-09 TRG B2-08201-CJWC-A018-CV05-10 05/10/1212:56 4/25/2020 4/28/2020 20-04072 Carbon-14

      • -EPA520.0Modified

-5.32E-O~9E:01 3.77E-01 6.41E-01 U

pCi/g 20-04072-10

  • TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45 4/25/2020 4/28/2020 : 20-04072 :

Carbon-14 EPA520.0 Modified

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U i

pCVg 20-04072-11 j

TRG l1-12109L-CJGS-001-SB-A 08/21/1910:25 4/25/2020 4/28/2020 20-04072

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3.91E-01 3.97E-01 6.77E-01 U

pCi/g 20-04072-12 i TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30 4/25/2020 4/28/2020 20-04072j Carbon-14

. ~520.0 Modified

-3.28E-01 3.68E-01 3.71E-01 i

6.33E-01 j U

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

(

EBERLINE

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ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 5/7/2020 9:23 PM Eberline Analytical Final Report of Analysis Lab ID 20-04072-01 :

Page 3 of 19 ReE_ort To:

Work Order Details:

Gerald Wood SOG:

20-04072 Zion Solutions Purchase Order 677116 1,,, ______,,,,,, ___

2701 Deborah Ave Zion, IL 60099 Analysis Category:

ENVIRONMENTAL

,,,,,,,,_t_,,_,,,_,,,,,,<,,,__,::,:_:_::,,:__;,,;_:,,_--=:,:_--,,-,,

Sample Matrix:

SO Receipt Analysis Batch Analyte I Method Result CU Date Date ID Sample Date CSU MDA Qualifier Report Units 04/25/20 00:00 4125/202 lron-55 EML Fe-01-01 Modified 4,08E+03 3,50E+02 04/25120 00:00 4/,

lron-55 EML Fe-01-01 Modified 3A1E+03 2,32E+02 6,33E+02 2,51E+02 pCi/g 04125120 00:00 3,01E+01 u

1 ___ -,,;::_c~=-..:,:,:=__;___:::==_:___;_==-=---=:._c,__:::::,c,,,,,,_,,,, _ __;_l_ro,__;_n_-5_5 __,I-EML Fe-01-01 Modified 5,18E+00 1,92E+01 1,92E+01 3,01E+01 U

pCilg

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DUP 81-06202A-FSWC-040-CV 06/18/1810:30

,, ___________,,,, lron-55 EML Fe-01-01 Modified 3,19E-02 U1E-01 U1E-01 2,15E-01 U

pCi/g 06/18/18 10:3C 2,15E-01 20-04072-04 DO 81-06202A-FSWC-040-CV 06/18118 10:30 20-04072 lron-55 EML Fe-01-01 Modified

-3,00E-02 1A1E-01 1A1E-01 2,23E-01 u

81-06214A-FSFC-001-CV 05105/1815:15 20-04072 lron-55 EML Fe-01-01 Modified 6,56E-02 L89E-01 1,89E-01 3,14E-01 U

3,14E-01 u

___,_,_~----

20-04072-09 20-04072-10,

20-04072-11 TRG TRG TRG 82-08101A-BJFC-007-CV 0 0-0 5 82-08101A-BJFC-007-CV 0 5-1 0 82-08201-CJWC-A018-CV 0 0-0 5 82-08201-CJWC-A018-CV 0 5-1 0 L2-10214C-RJGS-001-SM-A L 1-12109L-CJGS-001-SB-A 20-04072-12 TRG L1-12106L-CJGS-001-SB-A

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LCS KNOWN LCS SPIKE MBL BLANK DUP 05/09/12 14:22 20-04072 lron-55 EML Fe-01-01 Modified 7,56E-01 2,76E+00 2,76E+00 4A6E+00 U

pCi/g 4A6E+00 u

I 05/09112 14:22 4/2912020_,,, 20-04072_

lron-55 EML Fe-01-01 Modified

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pCilg 05/0!

3,04E+00 u

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pCi/g I 05/1(

5,12E+00 u

05110/12 12:56 4129/2020, 20-04072 lron-55 EML Fe-01-01 Modified L34E+00 2,55E+00 2,56E+00 4,30E+0C u

05107/19 07:45 4/2912020 20-04072 lron-55 EML Fe-01-01 Modified 5,91E-02 6,71E-02 6,79E-02 U5E-01 u

08/21/19 10:25 4/2912020 20-04072 lron-55 EML Fe-01-01 Modified ! -1,82E-02 3,86E-01 3,86E-01 6,15E-01 U

pCi/g 08114119 13:30 4/25/2020 4129/2020 20-04072 lron-55 EML Fe-01-01 Modified I L85E-01 2,37E-01 2,39E-01 4,04E-01 U,

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~------,,,,-_,,,_,_,,,,,,,,,_,,,,,,_, ____,,~---f-,--,,,~--,,_,_______

_ ____,,_/ ____,,,,, ----------

1 04/25/20 00:00 4/2512020 4130/2020 20-04072 Tritium LANL ER:210M~difi~d 1 i61E:;,02

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I 06/18/18 10:30 4/25/2020 4/30/2020 20-04072 Tritium LANL ER-210 Modified 3,70E+00 B1-06202A-FSWC-040-CV --+

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TRG B1-06214A-FSFC-001-CV 2A0E+00 2A1E+00 3,94E+00 u

pCilg TRG B2-08101A-BJFC-007-CV 0 0-0 5 I

05/09/1214:22 4/25/2020 5/1/2020 20-04072 Tritium T LANL ER-210 Modified_,____4,-9-7E_+_o_o~1-----,

05/09112 14:22

4/25/2020,

3A3E+00 3A4E+00 5,67E+00 u

pCilg I

TRG B2-08101A-BJFC-007-CV 0 5-1 0 05/09/12 14:22 4/2512020 5/1/2020 20-04072 Tritium

_LA_N_L_ER_-_2_10_M_o_difi_1e_d __ +-j _6_,3_5_E+_0_0--i-------<-----~-------'----~----'--'----I 05110/12 12:56 4/25/2020 511/2020 20-04072 Tritium LANL ER-210 Modified i 4,02E+00 5.68E+00 5,69E+00 9A8E+00 u

pCi/g TRG B2-08201-CJWC-A018-CV 0 0-0 5 3,34E+00 3,35E+00 5-56E+00 u

pCi/g TRG B2-08201-CJWC-A018-CV 0 5-1 0 I 05/10/12 12:56

4125/2020, 5/11202

*=

TRG L2-10214C-RJGS-001-SM-A I

05/10/12 12:56 4125/2020, 5/112020 20-04072 Tritium I LANL ER-210 Modified J 6A1E+00 1

-- I 05/07/19 07:45 4125/2020 5/1/2020 20-04072- *.

Tritium LANL ER-210 Modified 2,74E+00 3A6E+00 3.47E+00 5.64E+00 pCi/g 2-28E+00 2.28E+00 3,79E+00 u

pCi/g TRG L1-12109L-CJGS-001-SB-A I 08121/1910:25 4125/2020 511/2020 20-04072 Tritium LANL ER-210 Modified 8-51E+00 L 1-12109L-CJGS-001-SB-A 2,36E+00 2.41E+00 3,67E+00 pCi/g TRG L 1-12106L-CJGS-001-SB-A 172-12 TRG L1-12106L-CJGS-001-SB-A I 08/1411913:30 4/2512020 51112020 20-04072 Tritium I

LANL ER-210 Modified 1.50E+00 2,16E+00 2,16E+00 3.64E+00 u

pCilg CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect

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ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 5/7/2020 9:23 PM Page 4 of 19 Report To:

Work Order Details:

Eberline Analytical Gerald Wood SDG.

20-04072

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677116 Final Report of Analysis

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ID Date Date Date ID Units 20-04072-01

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20-04072-02 MBL BLANK 04/25/20 00:00 i 4/25/2020 4/2812020 20-04072 Nickel-59 ASTM 3500-Ni Modified

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pCi/g

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4/25/2020 4/2812020 20-04072 Nickel-59 ASTM 3500-Ni Modified 1.46E-02 7.26E-02 7.27E-02 1.15E-01 u

pCi/g

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20-04072-05 TRG B1-06214A-FSFC-001-CV 05105/18 15:15

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pCi/g

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20-04072-06 TRG B2-08101A-BJFC-007-CV 0 0-0 5 05/09/12 14:22 4/2512020 4/2812020 20-04072 Nickel-59 ASTM 3500-Ni Modified 1.10E-02 2.98E-01 2.98E-01 4.67E-01 u

pCi/g 20-04072-07 TRG B2-08101A-BJFC-007-CV 0 5-1 0 05109/12 14:22

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3.17E-01 u

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---**---*--s*****

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pCi/g 20-04072-09 TRG B2-08201-CJWC-A018-CV 0 5-1 0 05/10112 12:56 4/2512020 4/2912020 20-04072 Nickel-59 ASTM 3500-Ni Modified 3.79E-02 2.76E-01 2.76E-01 4.38E-01 u

pCilg

,._,m 20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05107119 07:45 4/25/2020 4/29/2020 20-04072 Nickel-59 ASTM 3500-Ni Modified

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pCilg

---~*~~*--*--<-*~ ***-'*-*****

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pCilg

~-*--*-*---------*------**-

20-04072-12

L 1-12106L-CJGS-001-SB-A 08/14119 13:30 4125/2020 4/2912020 20-04072 Nickel-59 ASTM 3500-Ni Modified

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pCi/g i

j 20-04072-01 LCS KNOWN 04125/20 00:00 4/25/2020 4130/2020 20-04072 :

Nickel-63 ASTM 3500-Ni Modified 1.46E+03 4.39E+01 i

pCilg 20-04072-01

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4125/2020 4130/2020 20-04072 Nickel-63 ASTM 3500-Ni Modified 1.48E+03 9.06E+00 8.76E+01 2.19E+00 pCi/g 20-04072-02 MBL BLANK 04/25/20 00:00 i 4/2512020
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pCi/g 20-04072-04 DO. B1-06202A-FSWC-040-CV 06/18/18 10:30 4/2512020 4/3012020 20-04072 Nickel-63 ASTM 3500-Ni Modified 1.45E+00 1.32E+00 1.32E+00 2.20E+00 u

pCi/g 20-04072-05 TRG B1-06214A-FSFC-001-CV 05/05/18 15:15 4125/2020 4130/2020

  • 20-04072 '

Nickel-63 ASTM 3500-Ni Modified 2.70E-01 1.37E+00 1.37E+00 2.33E+00 u

pCi/g 20-04072-06

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pCi/g 20-04072-07

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pCilg 20-04072-08 ;

TRG B2-08201-CJWC-A018-CV 0 0-0 5 05/10/12 12:56 l 412512020 4130/2020 20-04072 j Nickel-63 ASTM 3500-Ni Modified

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pCi/g

*-*-v-********-*---*

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pCilg 20-04072 !

20-04072-10 :

TRG L2-10214C-RJGS-001-SM-A 05107119 07 :45 4/25/2020 : 4/30/2020 Nickel-63 ASTM 3500-Ni Modified

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pCilg

--t---*--*

20-04072-11 TRG L 1-12109L-CJGS-001-SB-A 08121/19 10:25 4/2512020 4130/2020 20-04072 Nickel-63 ASTM 3500-Ni Modified 7.13E-01 1.36E+00 1.36E+00 I 2.30E+00 u

pCi/g 20-04072-12 TRG L 1-12106L-CJGS-001-SB-A 08/14/19 13:30 4125/2020 4/3012020 20-04072 Nickel-63 ASTM 3500-Ni Modified I -1.09E+00 1.24E+00 1.24E+00 2.16E+00 !

u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

(

EBERLINE

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ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 5/7/2020 9:23 PM I

Gerald Wood Zion Solutions ReE_ort To:

Page 5 of 19 Work Order Details:

SDG:

20-04072 Purchase Order::

677116 Eberline Analytical Final Report of Analysis i---------"--*--~--~-~-

--1--A~~ly~;~_Category* : _____ ENVIRON_MENTAC _____ -

2701 Deborah Ave Zion, IL 60099 Samp/e Matrix: '

SO Lab Sample Client I

Sample Receipt Analysis Batch A

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M h d I R I

CU CSU MDA Q rn Report ID Type ID Date Date Date ID na e

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' 4/25/2020 4/29/2020 20-0407:i Neptuniu,;;--237 EIChroM ACW08 Mod 1.17E+01 _____ 9.71 E-01 1.67E+OO 1.19E-01 pCi/g *--

20-04072-02 MBL BLANK 04/25/20 00:00 4/25/2020-- 4/29/2020 20~04072 Nept~~ium:237.. ** -* E1Ch;~M-ACW08 Mod 5.84E-02 8.35E-02 8.37E-02 1.37E-01 U

pCi/g 20-04072-03 DUP B1:06202A-FSWC-040-CV 06/18/18 10:30 4/25/2020 4/29/2020***-20:04072 --* Neptunium-237 EIChroM ACW08 Mod

-2.75E-03 3.22E-02 3.22E-02 1

6.75E-02 U

pCi/g 20-04072-04 DO B1-06202A-FSWC-040-CV 06/18/18 10:30

' 4/25/2020 4/29/2020 20-04072 Neptunium-237 EIChroM ACW08 Mod 4.76E-02 5.74E-02 i

5.76E-02 7.02E-02 U

pCi/g TRG I

B1-06214A-FSFC-001-CV 05/05/18 15:15

. 4/25/2020 4/29/2020 20-04072 ;.. Neptunium-2:37 EIChroM ACW08 Mod 2.94E-02 4:98E=02-- -

4.99E-02 8.80E=o2*

u

- pCVg TRG B2-08101A-BJFC-007-CV00-05

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Neptunium-237 EIChroMACW08Mod 7.53E-02 7.65E-02 7.70E-02 1.03E-01 U

pCi/g I 20-04072-07 TRG B2-08101A-BJFC-007-CV O 5-1 0 05/09/12 14:22

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pCi(Q__ _

20-04072-05 20-04072-06 20-04072-08 TRG B2-08201-CJWC-A018-CV00-05 05/10/1212:56

. 4/25/2020 4/29/2020

  • 20-04072 Neptunium-237 EIChroMACW08Mod 4.18E-02 5.04E-02 5.07E-02 6.17E-02 U

pCi/g 20-04072-09 TRG B2-08201-CJWC-A018-CVO 5-1 0 05/10/1212:56 4/25/2020 4/29/2020 20-04072.

Neptunium-237 EIChroM ACW08 Mod 4.72E-02 7.22E-02 7.24E-02

_ 1.23E-01 U

pCi/g 20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45 4/25/2020 4/29/2020*---*20:04012**

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pCi/g 20-04072-11 :

TRG L 1-12109L-CJGS-001-SB-A 08/21/19 10:25 4/25/2020 4/29/2020 20-04072 Neptunium-237 *

- EIChr~MACW08 Mod 4.14E-02 4:99E-02 5.01 E-02 6.1 OE-02 U

pCi/g L 1-12106L-CJGS-001-SB-A 08/14/1913:30 ______ 4/25/2020 4/29/2020 20-04072 Neptunium-237 EIChroM ACW08 Mod 1.52E-02 5.68E-02 5.68E-02 1.23E-01 ***------:~u*

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ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621

Printed: 517/2020 9:23 PM Page 7 of 19 Report To:

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ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621

Printed: 517/2020 9:23 PM Eberline Analytical Final Report of Analysis r**

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2701 Deborah Ave Zion, IL 60099 SDG:

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pCi/g v

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20-04072, 10 TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45 4/25/2020 4/29/2020 20-04072 Strontium-90 EIChroM SRW01 Modified

-9.40E-03 3.41E-02 3.42E-02 7_39E-02 U

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-2_56E -*-----3_76E +

3.86E-02 8_28E-02 U

pCi/g---t 20-04072-12 TRG L 1-12106L-CJGS-001-SB-A 08/14/19 13:30 4/25/2020 4/29/2020 20-04072 Strontium-90 EIChroM SRW01 Modified 2.42E-02 3.09E-02 3.20E-02 6.34E-02 U

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  • 4/2512,?2,9 ____ 4/27/2020 20-04072 Cesium-137 EPA901.1 Modified 1.94E+0,2,__

7.96E+OO pCi/g 20-04072-01 LCS SPIKE 04/25/20 00:00 4/25/2020 4/27/2020 20-04072 1 Cobalt-60 EPA 901.1 Modified 2.37E+02 1.45E+01 1.89E+01 2.39E+00 1

pCi/g ----t 20-04072-01 LCS SPIKE 04/25/2000:00

4/25/2020 4/27/2020 20--04072 Cesium-137

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Printed: 517/2020 9:23 PM Page 9 of 19 Report To:

Work Order Details:

Eberline Analytical I

G_eraldW~_?d_

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Zion Solutions............................

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7.02E*02 *.

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  • 1.07E*02 3.23E*02 3.23E*02 3.11E*02 U

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MBL BLANK

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  • 1.49E*02 3.36E*02 3.36E*02 3.93E*02 U

pCi/g 20.04072.02 MBL ! s°LANK 04/25/200()'.oo 4/25/2020 4/27/2020 20*04072 Bismuth*214 EPA 901.1 Modified

  • 1.14E*02 6.22E*02 6.22E*02 9.39E*02 u

pCi/g 20*04072*02 MBL BLANK 04/25/2000:00 4/25/2020 4/27/2020 20*04072 Cobalt*60 EPA901.1 Modified 5.05E*03 2.55E*02 2.55E*02 4.40E*02 U

pCi/g 20.04072.02 :

MBL BLANK 04/25/2000:00 ! 4/25/2020 4/27/2020 20*04072 ;

Cesium*134 EPA901.1 Modified 2:i2E:03*

2.89E:02*

2.89E*02 3.62E*02 U

pCi/g ***

20*04072*02 MBL BLANK 04/25/2000:00 i 4/25/2020 4/27/2020 20*04072 i Cesium.137 EPA901.1 Modified 1.42E*02 2.86E*02 2.87E*02 5.01E*02 U

pCi/g

.** 20*04072*02 MBL BLANK 04/25/2000:00 4/25/2020 4/27/2020 20*04072 Europium*152 EPA901.1 Modified 7.98E*02 7.05E*02 7.06E*02 9.37E*02 1

U pCi/g 20*04072*02 MBL BLANK 04/25/2000:00 4/25/2020, 4/27/2020 20*04072 Europium*154 EPA901.1 Modified 1.97E*02 6.70E*02 6.70E*02 i 4.51E*02 U

pCi/g

  • -20-0!072:02 MBL
      • BLANK 04/25/2000~0()

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.*... 4.73E*02 4.73E*02 6.30E*02 U

I pCi/g 20*04072*02 MBL BLANK 04/25/2000:00

,.4/25/2020 4/27/2020 20*04072 Holmium*166m EPA901.1 Modified..*..

3.65E*02 4.29E*02 4.29E*02 3.72E*02 U

pCi/g

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, 4/25/2020 4/27/2020 2CJ:04072 lodine.129

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  • 2.51E-03 5.23E*02 i

5.23E*02 7.37E-02 U

pCi/g 20*04072-02 !

MBL BLANK 04/25/20 00:00 4/25/2020 4/27/2020 20*04072 Potassium-40 EPA 901.1 Modified 3.19E-01 2.51 E-01 2.52E*01 5.75E*01 U

pCi/g 20-04072*02 :

MBL BLANK 04/25/2000:00 4/25/2020 4/27/2020 20-04072 Manganese-54 EPA901.1 Modified 7.72E*03 2.13E*02 2.13E*02 3.63E-02 U

pCi/g I* 20:04072-02 :

MBL BLANK 04/25/20 00:00

4/25/2020 *. 4/27/2020 : 20*04072 Molybdenum-93 EPA 901.1 Modified

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. 2.12E*02 2.12E*02 3.08E*02 U

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pCi/g 20-04072*02 MBL BLANK 04/25/20 00:00 4/25/2020 4/27/2020 20*04072 :

Lead*210 EPA901.1 Modified 3.17E*01 4.58E*01 4.58E*01 ! 6.69E*01 U

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2.73E*02 1

4.45E*02 4.45E*02 6.52E*02 U

i pCi/g 20-04072*02 !

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Lead*214 EPA 901.1 Modified 2.00E*02 j

5.02E*02 5.02E*02 i 7.53E*02 U

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j pCi/g 20.04072.02 MBL BLANK 04/25/2000:00 4/25/2020 4/27/2020 20-04072 :

Radium*226 EPA901.1 Modified

  • 1.14E*02 6.22E*02 6.22E*02 9.39E*02 U

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1.99E*02 4.96E*02 4.96E*02 9.23E*02 U

J pCi/g 20*04072*02 !

MBL BLANK 04/25/2000:00 4/25/2020 4/27/2020 20*04072.,

Thorium*234 EPA901.1 Modified 7.38E*01*********4~4E-:_01 4.15E*01 6.72E.01 U

pCi/g 20*04072*02,

MBL BLANK 04/25/2000:00,-4/25/2020 ** 4/27/2020 20*04072 i Thallium*208 EPA901.1 Modified 8.23E*02 6.42E*02 6.44E*02 1.28E*01 U

pCi/g 20-04072*02 MBL BLANK 04/25/2000:00

4/25/2020 4/27/2020 20*04072 Uranium*235 EPA901.1 Modified I 8.75E*02 1.50E*01 1.50E*01 2.15E.01 U

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ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 517/2020 9:23 PM Page 10 of 19 Report To:

Work Order Details:

Eberline Analytical _ G_eraldWo_od SOG 20-04072 Final Re ort of Anal sis

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Units 20*04072*03 i DUP B1*06202A*FSWC*040-CV 06/18/18 10:30 4/25/20~()_._ 4/27/2020 20*04072

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.... 3.56E*01 2.24E*01 2.24E-01 5.24E*01 i

U pCi/g 20*04072*03

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pCi/g 20*04072*03 DUP i

B1*06202A-FSWC*040.CV 06/18/1810:30 4/25/2020 4/27/2020 20*04072

  • BarilJm.133 EPA901.1 Modified 1.50E*03 2.56E*02 2.57E*02 1.41E*01 U

pCi/g 20-04072*03 i DUP 81*06202A*FSWC-040.CV

~~ 06/18/1810:30

4/25/2020**-~~~.~~()_20 20*04072 Bismu!h*214___

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  • 1.88E*01 1.89E*01 i

2.74E*01 pCi/g 20*04072-03 DUP B1*06202A-FSWC*040-CV 06/18/1810:30 4/25/2020 4/27/2020 20*04072 Cobalt.60 EPA 901.1 Modified 3.90E*02 8.20E*02 8.21E*02 1.20E*01 U

pCi/g

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  • 2.78E*01 1.81E*01 1.82E*01 1.76E*01 U

pCi/g

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  • 3.81E*03_
  • --523E*02 5.23E*02 8.14E-02 u

i pCi/g

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4/25/2020 4/27/2020

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  • 2.06E*01 2.83E*01 2.83E-01 2.37E-01 U

pCi/g 20*04072*03 DUP B1*06202A*FSWC*040-CV 06/18/1810:30 4/25/2020 4/27/2020. 20*04072 Europium*154 EPA901.1 Modified 1.01E*01 1.56E*01 1.56E-01 1.24E*01 U

pCi/g 20-04072*03 DUP B1*06202A*FSWC*040*CV 06/18/1810:30

4/25/2020 ___ 4/27/2020
  • 20*04072 Europium*155 EPA 901.1 Modified

! 1.92E*01

--9~66E=o2*

9.71E-02 2.57E-01 U

pCi/g 20*04072*03 :

DUP B1*06202A*FSWC*040-CV 06/18/1810:30 4/25/2020 4/27/2020 20-04072 Holmium*166m EPA901.1 Modified*- ********-7.09E:o2 4.66E-02*****:-**:;:i;7E-02 9.07E-02 U

pCi/g *--

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20-04072-03 DUP B1*06202A-FSWC-040-CV 06/18/1810:30 4/25/2020 4/27/2020 20*04072 lodine*129 EPA901.1 Modified

-9.48E-02 1.40E-01 1.40E-01 2.12E-01 U

pCi/g J------,-----:-----*-*-***-***-**-------------,.-------'----------+-**--- *******--**** - -*-*-***------+------'---------------:------i--------'--=---1 20-04072-03 DUP B1*06202A-FSWC-040*CV 06/18/1810:30 4/25/2020 4/27/2020 20-04072 Potassium-40 EPA901.1 Modified 5.33E+OO 1.33E+OO 1.36E+OO 1.17E+OO pCi/g

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pCi/g 20-04072-03 DUP 81-06202A~FSW.C-040-CV

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4.05E-03

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pCi/g

.. -~?:?~72.03 '

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  • -~/25/2020 4/27/2020 20-04072 :

Lead-210 EPA901.1 Modified.

7.39E-01 J

1.03E+OO 1.03E+OO 1.73E+OO :

U pCi/g 20-04072-03 DUP B1*06202A-FSWC-040-CV 06/18/1810:30 i 4/25/2020 4/27/2020 20*04072 Lead*212 EPA901.1 Modified 3.69E-01 1.43E-01 1.44E-01 2.13E*01 pCi/g 20*04072-03 :

DUP 81-06202A-FSWC*040*CV 06/18/1810:30 4/25/2020

  • 4/27/2020 20-04072 Lead-214 EPA901.1 Modified 4.16E-01 1.57E*01 1.59E*01 2.60E-01 pCi/g 20.04072.03 i DUP 81-06202A*FSWC-040-CV 06/18/1810:30 i 4/25/2020 4/27/2020 20-04072 Promethium.145 EPA901.1 Modified 2.20E-02 i

1.30E-01 1.30E*01 2.16E-01 i

U pCi/g 20-04072-03 '

DUP 81-06202A*FSWC-040*CV 06/18/1810:30 i 4/25/2020

  • 4/27/2020 20*04072 Radium-226 EPA901.1 Modified 3.97E-01 1

1.88E-01 1.89E-01 2.74E-01 pCilg 20*04072-03 DUP 81-06202A-FSWC*040-CV 06/18/1810:30 I 4/2512020 4127/2020 20-04072 Antimony-125 EPA 901.1 Modified 1.79E-02 7.68E-02 7.68E-02 3.30E-01 U

pCi/g *-

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4/25/2020 4/27/2020 20-04072 Thorium*234 EPA 901.1 Modified 2.06E+OO 9.35E-01 9.41E-01 1.65E+OO U

pCi/g

- 20:04072.03 DUP B1*06202A-FSWC-040-CV 06/18/1.il10:30 i 4/25/2020: 4/27/2020 20*04072 Thallium*208

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20-04072-03 DUP 81-06202A-FSWC-040-CV 06118/1810:30 4/25/2020

  • 4/27/2020 20-04072 Uranium-235 EPA 901.1 Modified j

9.50E-02 2.66E-01 2.66E-01 4.10E-01 U

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ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 5/7/2020 9:23 PM Page 11 of 19 Report To:

Work Order Details:

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5.56E-01 U

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20-04072-04 DO 81-06202A-FSWC-040-CV 06/1811810:30 4/2512020 412712020 20-04072 Barium-133 EPA901.1 Modified

-1.08E-01 1.24E-01 1.25E-01 1.25E-01 U

pCilg

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20-04072-04 DO 81-06202A-FSWC-040-CV 06/18/1810:30 412512020 412712020 20-04072 Bismuth-214 EPA901.1 Modified 3.95E-01 1.24E-01 1.26E-01 2.81E-01 pCi/g c***-***-----.----'-------.. --... -----1-*------!,* -----------.....C-------+-----------+----------'------;---------*~-"--'---1

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20-04072-04 DO 81-06202A-FSWC-040-CV 06/18/1810:30 I 4125/2020 4/27/2020 20-04072 Cesium-134 EPA901.1 Modified 4.12E-02 6.30E-02 6.31E-02 1.57E-01 U

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06118118 10:30 ! 412512020 4/27/2020 20-04072 E~ropium-152 EPA 901.1 Modified

  • -*-:;;: 18E-01 2.79E-01 2.80E-01 2.32E-01
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20-04072-04 DO 81-06202A-FSWC-040-CV 0611811810:30 4/2512020 4127/2020 20-04072:,_. Europium-154 _

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-3.08E-02 1.08E-0_~

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pCilg

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06/18/1810:30 i 412512020 412712020 20-04072 Europium-155 EPA901.1 Modified 1.47E-01 1.48E-01 1.48E-01 2.41E-01 U

pCilg 20-04072-04 :

DO 81-06202A-FSWC-040-CV. ---*

06118/1810:30 412512020 4/2712020 20-04072 Holmium-166m EPA901.1 Modified 2.05E-02 9.15E-02 9.15E-02 8.70E-02 U

pCi/g 20-04072-04 DO 81-06202A-FSWC-040-CV 06118/1810:30 412512020 4/27/2020 20-04072 lodine-129 EPA901.1 Modified

-1.46E-02 1.39E-01 1.39E-01 2.25E-01 U

pCi/g 20-04072-04 :

DO 81-06202A-FSWC-040-CV

---06/18/1810:30

[ 4125/2020 4/27/2020 ' 20-04072 Potassium-40 EPA901.1 Modified 5.71E+00 1.33E+00 1.36E+00 1.03E+00 pCilg 20-04072-04 DO 81-06202A-FSWC-040-CV 06/18118 10:30 1 412512020 ' 412712020 20-04072-** Manganese-54 EPA 901.1 Modified

-3.94E-02 2.94E-01 2.94E-01 3.94E-01 U

pCilg ----

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20-04072-04 DO 81-06202A-FSWC-040-CV 06/18/1810:30 412512020

  • 412712020 20-04072, Molybdenum-93 EPA 901.1 Modified 1.65E-02 5.15E-02 5.15E-02 8.71E-02 U

pCi/g 20-04072-04 DO 81-06202A-FSWC-040-CV 0611811810:30

-4:;25/2020 4/27/2020 --20-04072-,

Niobium-94 EPA901.1 Modified

-6.70E-03 5.79E-02 5.79E-02 7.05E-02 U

pClig--

20-04072-04 DO 81-06202A-FSWC-040-CV 06/18/1810:30 412512020 412712020 20-04072 Lead-210

  • -* EPA901.1 Modified 1.52E+00 1.36E+00 1.36E+00 2.25E+00 U

pCilg 20-04072-04 '

DO I

81-06202A-FSWC-040-CV 06/1811810:30 I 412512020 412712020 20-04072 Lead-212

... iPA901.1 Modified*-

  • 3.09E-01 1.09E-01 U0E-01 2.26E-01 pCilg t---------------------*--t-------+-----;----,----~-------+---------1-------'------+------;---------,-~---"-**---

20-04072.04 :

DO 81-06202A-FSWC-040-CV 06118/1810:30 412512020 4/2712020 20-04072 Lead-214 EPA901.1 Modified 4.22E-01 1.26E-01 1.28E-01 3.22E-01 pCilg 20-04072-04 DO B1-06202A-FSWC-040-CV 06118/1810:30 4/2512020 4127/2020 20-04072 Promethium-145 EPA901.1 Modified 5.31E-02 1.32E-01 1.33E-01 2.22E-01 i

U pCi/g 20-04072-04 DO i

81-06202A-FSWC-040-CV 06/18/1810:30 4125/2020 4127/2020 : 20-04072 i Radium-226 EPA901.1 Modified 3.95E-01 1.24E-01 1.26E-01 i

2.81E-01 1

pCilg 20-04072-04 DO B1-06202A-FSWC-040-CV 06/18/1810:30 4125/2020. 412712020 20-04072--,

Antimony-125 EPA901.1 Modified 1.54E-01 i 1.81E-01 1.81E-01 3.19E-01

U-~-

pCi/g 20-04072-04 DO 81-06202A-FSWC-040-CV 06118/1810:30 4125/2020 4/2712020 20-~-~!~..

Thorium-234 EPA 901.1 Modified 1.20E+00 1.43E+00

.. _1~4~E+00 2.40E+00 U

pCilg 20-04072-04 DO B1-06202A-FSWC-040-CV 06118/1810:30 4/25/2020 4/27/2020 20-04072 1 Thallium-208 EPA901.1 Modified 3.67E-01 1.71E-01 1.72E-01 2.42E-01 I

pCi/g 20::04072-04 DO B1-06202A-FSWC-040-CV 06/18/1810:30 412512020 412712020 20-04072 !

Uranium-235 --

EPA901.1 Modified J

8.27E-02 2.71E-01 2.71E-01 4.15E-01 U

pCj/g-CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect

(

EBERLINE 1§)

ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 517/2020 9:23 PM Page 12 of 19 Report To:

Work Order Details:

Eberline Analytical G_erald wo_od SOG

?Q~Q-~072 Zion Solutions Purchase Order*

677116 Final Re ort of Anal sis 2701 Deborah Ave. -

---,... Analysis Category:

_E_N_V-IR_O_N_M-ENTAL p

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Zion, IL 60099 Sample Matrix:

SO Lab Sample Client Sample Receipt Analysis Batch A

I M h R

I CU CSU MDA

  • Q rfi Report ID Type ID Date Date Date ID na yte et od esu t ua 1,er Units 20-04072--05 TRG B1-06214A-FSFC-001-CV 05/05/1815:15
  • 4/25/2020 4/27/2020 20-04072 Actinium-228 EPA901.1 Modified

-127E-01 1A9E-01 1A9E-01 8A9E-01 U

pCi/g 20-04072-05 TRG 81-06214A-FSFC-001-CV 05/05/1815:15 4/25/2020 4/27/2020 20-04072 Silver-108m EPA90U Modified 3.17E-02 1.22E-01 L22E-01 U9E-01 U

pCi/g 20-04072-05 TRG B1-06214A-FSFC-001-CV 05/05/18 15:15 4/25/2020 4/27/2020 20-04072 Barium-133 EPA 901,1 Modified i. 1~07E:02 6.60E-02 6.60E-02 2.75E **u * *. -

pCi/g

,.20-04072-05

°TRG-:-131:-06214A-FSFC-001~CV 05/05/18 15:15 i 4/25/2020 4/27/2020 20-04072 I Bismuth-214

---EPA901 11~1~dified I 7 JJ3E:a;* i 2.65E-01 2.67E-01 2.56E-01 pCi/g 20-04072-05 1

TRG

_ ~1~0_6214A-FSFC-001-CV 05,1()_5/18_ 15:15,

_ ~/25!~?20 4/27/2020 20-04072 :

Cobalt-60 EPA 901.1 Modified i :5:4_1E-02 '

1.85E-01 1.85E-01 2.88~:0,1_ __

U pCi/g 20-04072-05 TRG B1-06214A-FSFC-001-CV

.,, 05/05/1815:15 4/25/2020 4/_2_7/~~~o,, __ _2-9*04072 Cesium-134 EPA901.1 Modified

-4.09E-02 "

9.97E-02 9.97E-02 3.59E-01 U

pG_~!l_ __

20-04072-05 I TRG B1-06214A-FSFC-001-CV 05/05/1815:15 4/25/2020 4/27/2020 20-04072 Cesium-137 EPA901.1 Modified 2.89E-03 1A8E-01 1A8E-01 2.07E-01 U

pCi/g 20-04072-05 TRG I

B1-06214A-FSFC-001-CV 05/05/1815:15 4/25/202? ___ 4l27!~020: 20-04072 J Europium-152___

EPA901.1 Modified

~3.Ei9E:01 __,_ 5.24E-01 5.25E-01 3.08E::!_1_

_ LJ

__ pCi/g 20-04072-05 TRG

[

81-06214A-FSFC-001-CV 05/05/1815:15 4/25/2020 4/27/2020 20-04072.

Europium-154 EPA 901.1 Modified

-3*'.:!-E::_0_1___.. __ 4.60E:?.1......*. 4.60E-01 1.72E-01 U

f:.~~9-20-04072-05 :

TRG ! 81-06214A-FSFC-001-CV 05/05/18 15:15 ! 4/25/2020 4/27/2020 ' 20-04072 Europium-155 EPA 901.1 Modified 2A4E-01

_ 2.07E-01 ___ 2.08E-01 3.25E-01 U

pCi/g 20-04072-05 TRG B1-06214A-FSFC-001-CV 05/05/1815:15 4/25/2020 4/27/2020 20-04072 Holmium-166m EPA901.1 Modified

-3A8E-02 1.83E-01 1.83E-01 1.39E--01 U

pCi/g

                    • -'"'~****-*---
  • -**---~*-~*

20-04072-05 TRG

--~1-06214A-FSFC-001-CV 05/05/1815:15 4/25/2020: 4/27/2020 20-04072 lodine-129 EPA901.1 Modified i 2.86E-02 2AOE-01 2AOE-01 3.60E-01 U

pCi/g 20-04072-05 TRG B1-06214A-FSFC-001-CV 05/05/1815:15 4/25/2020 4/27/2020 20-04072 Potassium-40 EPA901.1 Modified 6A5E+OO 1.84E+OO 1.87E+OO 8.62E-01 pCi/g

__,,__ ____,~-~

20-04072-05 TRG 81-06214A-FSFC-001-CV 05/05/1815:15 i 4/25/2020 4/27/2020 20-04072 Manganese-54 EPA901.1 Modified 4.62E-01 4.28E-01 4.28E-01 8.84E-01 U

pCi/g 20-04072-05 TRG i

B1-06214A-FSFC-001-CV 05/05/1815:15 (4/25/2020 4/27/2020 20-04072 Molybdenum-93 EPA901.1 Modified 3.42E-02 i

1.02E-01

        • 1:o:i"E-01 1.37E-01
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pCi/g 20-04072-05 TRG i

81--06214A-FSFC-001-CV 05/05/1815:15 4/25/2020 4/27/2020 20-0407:i°*

Niobium-94 EPA901.1 Modified 2.32E-02 1.21E-01 1.21E-01 1.79E-01 U

pCi/g 20-04072-05 TRG B1-06214A-FSFC-001-CV 05/05/1815:15 4/25/2020 4/27/2020 20-04072 i Lead-210 EPA 901.1 Modified 1.38E+OO 1.56E+OO 1.56E+OO 2.45E+OO U

j pCi/g 20-04072-05

  • TRG B1-06214A-FSFC-001-CV 05/05/1815:15 4/25/2020.. 4/27/2020--20-04072 Lead-212 EPA901.1 Modified 7.02E-01
      • 2:39E=01_,,_ 2.42E-01 3.38E-01 pCi/g 20-04072-05 j TRG 81-06214A-FSFC-001-CV 05/05/1815:15 4/25/2020 4/27/2020 20-04072 Lead-214 EPA901.1 Modified 5.56E-01 2.39E-01 2.41E-01 4.17E-01 i

pCi/g 20-04072-05 J

TRG i

B1-06214A-FSFC-001-CV 05/05/1815:15 i 4/25/2020 4/27/2020 20-04072 i Promethium-145...

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-2.11E-01 2.3:iii=-01--

  • 2.32E-01 3.16E-01 U

pCi/g 20-04072-05 TRG B1-06214A-FSFC-001-CV 05/05/1815:15 i 4/25/2020. 4/27/2020. 20-04072 ;

Radium-226 EPA901.1 Modified 7~03E=01 2.65E-01 2.67E-01 2.56E-01 pCi/g 20-04072-05 i TRG B1-06214A-FSFC-001-CV 05/05/1815:15 i 4/25/2020: 4/27/2020 20-04072 Antimony-125 EPA901.1 Modified 4.16E-01 4.52E-01 4.52E-01 7.29E-01 U

pCi/g 20-04072-05 :

TRG i 81-06214A-FSFC-001-CV 05/05/1815:15 J 4/25/2020 4/27/2020 20-04072 1 Thorium-234 EPA901.1 Modified i

2.43E+OO 1.33E+OO 1.33E+OO 2.19E+OO U

pCi/g 20-04072-05 '

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4.50E-01 2.41E--01 2.42E-01 4.10E-01 pCi/g 20-04072-05 TRG 81-06214A-FSFC--001-CV 05/05/18 15:15 i 4/25/2020 4/27/2020 20-04072 :

Uranium-235 EPA 901.1 Modified

! 5.84E-01 4.01E-01____

4.02E-01 6.81E-01 U

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(

EBERLINE

~

ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621

Printed: 5/7/2020 9:23 PM Page 13 of 19 Report To:

Work Order Details:

Eberline Analytical t Gerald Wood SDG.

20-04072

......,,.. -* ""~-*<S~******-***---*~-*-........ ~*.

~-_........ Zion Solutions __..... *--~---*

Purchase Order:

677116 Final Report of Analysis 2701 Deborah Ave Analysis Category:

ENVIRONMENTAL

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Report ID Type.

ID Date Date Date ID Units I 20.04012-06 TRG 82-08101A-BJFC-007-CV O 0-0 5 05/09/12 14 :22 4/25/2020 4/27/2020 20-04072 Actinium-228 EPA 901.1 Modified 7.82E-01 8.24E-01 8.25E-01 i

1.38E+OO u

oCi/q 20-04072-06 TRG i

B2-08101 A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 20-04072 Silver-108m EPA 901.1 Modified

-7.38E-02 2.77E-01 2.77E-01 2.37E-01.

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20-04072-06 TRG 82-08101A-BJFC-007-CV O 0-0 5 05/09112 14:22 4/25/2020 4/27/2020 20-04072 Barium-133 EPA 901.1 Modified 2.93E-01 5.75E-01 5.76E-01 i

7.52E-01 u

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---**~*-*

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20-04072-06

  • TRG B2-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 20-04072 Bismuth-214 EPA 901.1 Modified 1.34E+OO 4.57E-01 4.62E-01 3.37E-01 pCi/g 20-04072-06 TRG B2-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 l 4/25/2020 4/27/2020 20-04072 Cobalt-60 EPA 901.1 Modified

-5.83E-01 5.59E-01 5.60E-01 7.34E-01 u

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20-04072-06 TRG B2-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 20-04072 Cesium-134 EPA 901.1 Modified 4.82E-01 1.88E+OO 1.88E+OO 3.99E+OO.

u pCi/g

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  • ~-*"-

20-04072-06 TRG 82-08101A-BJFC-007-CV O 0-0 5 05/09/12 14 :22 4/25/2020 4/27/2020 20-04072 Cesium-137 EPA901.1 Modified 1.15E-01 2.37E-01 2.37E-01 3.78E-01 u

pCi/g 20-04072 :

I 20-04072-06 TRG B2-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 Europium-152 EPA 901.1 Modified. 2.89E-01 8.81E-01 8.81E-01 9.93E-01 u

pCi/g I

20-04072-06 TRG 82-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 20-04072 Europium-154 EPA 901.1 Modified 4.41E-01 9.70E-01 9.70E-01 6.53E-01 u

pCi/g v~~-------*~-'owo*~-*-

20-04072-06 I TRG 82-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 20-04072.

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20-04072-06,

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pCi/g 20-04072-06

  • TRG B2-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 ! 4/25/2020 4/27/2020 20-04072 Potassium-40 EPA901.1 Modified I

8.56E+OO 3.05E+OO 3.08E+OO 3.60E+OO pCi/g EPA 901.1 Modified-** _! _ -1.66E+01_ : _

1 zo-04072-06

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u pCi/g 20-04072-06 I

TRG B2-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 20-04072 Niobium-94 EPA 901.1 Modified 1.74E-02 1.98E-01 1.98E-01 2.70E-01 u

pCi/g

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  • Lead-214 EPA 901.1 Modified I

1.33E+OO 4.24E-01 4.30E-01 1.24E+OO pCi/g i

20-04072-06 TRG 82-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 20-04072 Promethium-145 EPA901.1 Modified l

3.88E-01 6.81E-01 6.81E-01 1.06E+OO u

pCi/g 20-04072-06 :

TRG B2-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 20-04072 j Radium-226 EPA 901.1 Modified 1.34E+OO 4.57E-01 4.62E-01 3.37E-01 pCi/g I 20-04012-06 TRG 82-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 20-04072 Antimony-125 EPA 901.1 Modified

-1.51E+OO 3.40E+OO 3.40E+OO 4.75E+OO u

pCi/g 20-04072-06 TRG 82-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 20-04072 Thorium-234 EPA 901.1 Modified 7.69E+OO 3.52E+OO 3.54E+OO 5.86E+OO u

pCi/g 20-04072-06 TRG 82-08101A-BJFC-007-CV O 0-0 5 05/09/12 14:22 4/25/2020 4/27/2020 I 20-04072 Thallium-208 EPA 901.1 Modified 3.SOE-01 6.33E-01 6.33E-01 9.84E-01 u

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(

EBERLINE

~

ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 517/2020 9:23 PM Page 14 of 19 Report To:

Work Order Details:

Eberline Analytical G_eraldWo_od SOG.

20-04072 Zion Solutions Purchase Order:

6771_1_6 _____ _

Final Report of Analysis 2701 Deborah Ave**

Analysis C~t~g;ry,..... ENVIRONMENTAL

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6.73E-01 6.77E-01 1.21E+00 pCi/g 20-04072-07 TRG B2-08101A-BJFC-007-CV05-10 05/09/1214:22 4/25/2020 4/27/2020 20-04072 Silver*108m EPA901.1 Modified

  • 1.03E-01 1.41E-01 1.41E-01 2.06E-01 U

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. 4/25/2020 4/27/2020 20*04072 _________ Barium-133.......,...

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' 4/25/2020 4/27/2020 20-04072 Coba\\t.60 EPA 901.1 Modified 1.19E-01 4.80E-01 4.80E-01 7.55E-01 U

pCi/g ___.,

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pCi/g 20-04072-07 :

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pCi/g 20-04072-07 :

TRG 82-08101A-BJFC*007-CV0 5-1 0 05/09/1214:22 4/25/2020 4/27/2020 20*04072 Europium*154 EPA901.1 Modified

1.58E-01 8.76E-01

--8.76E-01.*.. **6.04E*01 U

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20-04072-07 TRG 82-08101A*BJFC-007_:--CV*0--5-1 0 05/09/1214:22 4/25/2020 4/27/2020 20-04072 :

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... ~.:,5-~+01 3.01E+00 3.0?.1§:+00 1.92E+00 pCi/g 20-04072-07 TRG 82-08101A-BJFC-007-CV 0 5-1 0 05/09/12 14:22 4/25/2020 4/27/2020 20-04072 Manganese-54 EPA 901.1 Modified

-1.12E+02 1.23E+02 1.23E+02 1.52E+02 U

pCi/g

-~0=~~?2-07 TRG 82-08101A-BJFC-007-CV0 5-1 0 05/09/1214:22

4/25/2020 4/27/2020 20-04072 Mo\\ybdenum-93 EPA901.1 Modified 3.27E-02 __

,, 2.06E-01____

2.06E-01 3.48E-01 U

pC~-

20-04072-07 TRG 82-08101A-BJFC-007-CV05-1 0 05/09/1214:22 4/25/2020 4/27/2020 20-04072 Niobium-94 EPA901.1 Modified 1.51E-01 1.20E-01 1.21E-01 2.46E-01 U

pCi/g 20-04072-07 TRG 82-08101:;;_:-BJFC~007-CV 0 5-1 0 05/09/12 14:22 4/25/2020 4/27/2020 20-04072 i Lead-210 EPA 901.1 Modified 3.ssii:oo '

4.40E+00 4.40E+00 7.34E+00 j

u..,,,,

pCi/g -

~0-04072-07 TRG 82-08101A-BJFC-007-CV05-10 05/09/1214:22

'4/25/2020 412ii2oio 20-0407~

L~~d:212'""'

EPA901.1Modified,_

7.44E-01

-~~5-§-01 2.88E-01 7.47&01*--

u pCi/g 20-04072-07 TRG 82-08101A-BJFC-007-CV05-1 0 05/09/1214:22 4/25/2020 4/27/2020 20-04072 Lead-214 EPA901.1 Modified 9.94E-01 4.58E-01 4.61E-01 7.75E-01 pCi/g 20-04072-07 TRG 82-08101A-BJFC-007-CV05-1 0 05/09/1214:22 4/25/2020 4/27/2020 20-04072 i Promethium-145 EPA901.1 Modified 2.32E-01 5.73E-01 5.73E-01 7.98E-01 u *---o~

20-04072-07 i TRG B2-08101A-BJFC-007-CV0 5-1 0 05/09/1214:22

' 4/25/2020 4/27/2020

__ 20-04072 _,

Radium-226 EPA901.1 Modified 1.22E+00 :

6.96E-0~---

6.98E-01 j

1.08E+00 pCi/g ---***

20-04072-07 TRG 82-08101A-BJFC-007-CV05-10 05/09/1214:22

4/25/2020 4/27/2020 20-04072 Antimony-125 EPA901.1 Modified 1.05E+00

2.55E+00 2.55E+00 4.60E+00 U

pCi/g 20-04072-07 TRG 82-08101A-BJFC-007-CV05-10 05/09/1214:22 i 4/25/2020 4/27/2020 20-04072 Thorium-234 EPA901.1 Modified 3.08E+00 3.34E+00 3.35E+00 4.83E+00 U

pCi/g 20-04072-07 TRG 82-08101A-BJFC-007-CV 0 5-1 0 05/09/12 14:22

4/25/2020 4/27/2020 20-04072 Thallium-208 EPA 901.1 Modifi~cl ----

3.96E-01 6.22E-01 6.22E-01 1.04E+00 U

....,..,., pCi/g 20-04072-07 TRG 82-08101A-BJFC-007-CV05-10 05/09/1214:22

4/25/2020
4/27/2020 20-04072 Uranium-235**-* *-*EPA901.1 Modified... I 1.48E-01 9.48E-01 9.48E-01 1.30E+00 U

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

(

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ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 5/7/2020 9:23 PM Eberline Analytical Final Report of Analysis I

Report To:

Gerald Wood Zion Solutions 2701 Deborah Ave Zion, IL 60099 Page 15 of 19 Work Order Details:

SDG.

20-04072 Purchase Order.*

677116

. + _'-'.!7§.'t.~i.s,.ga!EifL().'Y:..* __ ENVIRONMENTAL

              • ~=J Sample Matrix:

SO Lab Sample Client I

Sample Receipt Analysis Batch Analyte I Method I Result CU CSU MDA Qualifier Ri~i~rt ID Type ID Date Date Date ID 20*04072-08 TRG B2*08201*CJWC-A018*CV00-05 05/10/1212:56 4/25/2020 4/27/2020 20-04072 Actinium-228 EPA901.1 Modified 1.89E+OO 1.33E+OO 1.34E+OO :

2.70E+OO U

pCi/g 20-04072*08 TRG

..** B2-08201-CJWC*A018~Cv*o*o:o5 05/10/1212:56 4/25/2020 4/27/2020: 20*04072 Silver*108m EPA901.1 Modified

  • 1.60E-01 3.91E-01 3.91E*01 4.55E*01 U

pCi/g t~04072*08 TRG B2*08201-C.JWC:Ao1icvoo~o5 05/10/1212:56

4/25/2020 4/27/2020 20-04072 Barium*133 EPA901.1 Modified 1.34E*01 2.59E*01 2.59E*01 9.98E-01 u

pCi/g j_ici:()4072*0~**-**:.~. s2.6s20*,:cJWC-"2?!!l:CV_(l_?:05 05/10/1212:56 ! 4/25/2020 4/27/2020 20*04072 Bismuth*214_._,_ EPA901.1 Modified 1.31E+OO ;

6.33E*01 6.36E*01 9.56E*01 pCi/g 20.04072.os TRG B2-08201*CJWC*A018.CV00*0*5*****05/10/1212:56 4/25/2020, 4/27/2020 20*04072 Cobalt*60 EPA901.1 Modified

              • *8.17E*01 1.52E+OO

.*. 1.52E+OO 1.60E+OO *****************************P.~ii.g 20*04072*08 TRG B2*08201*CJWC*A018*CVO O*O 5 05/10/1212:56 i 4/25/2020 4/27/2020 20*04072 Cesium*134 EPA901.1 Modified

  • 5.14E+OO 6.77E+OO 6.77E+OO 7.60E+OO U

pCi/g 20~04072*08 TRG B2*08201*CJWC*A018*CV O O*O 5 05/10/12 12:56

' 4/25/2020 4/27/2020 20-04072 Cesium* 137 EPA 901'.1Mod-ifi~d

,* 8.97E*02 4.50E*01 4.50E*01 6.93E*01..

U

    • pCiig*-**

20*04072*08 TRG.,... B2*08201*CJWC*A018*CV00-05 05/10/1212:56 4/25/2020 4/27/2020 20*04072,-* Europium*152 EPA901.1 Modified

  • 1.78E+OO '

2.31E+OO 2.31E+OO 1.19E+OO

-**** U pCi/g 20-04072*08 TRG B2*08201*CJWC*A018.CV00-05 05/10/1212:56 4/25/2020 4/27/2020' 20*04072 Europium*154 EPA901.1 Modified

  • 2.01E*01 1.86E+OO 1.86E+OO 8.00E*01 U

pCi/g

~1 20.0407~* TRG B2*08201*CJWC*-"2_~1.8:E.? O*O 5 05/10/12.'..~~~ _ _;__4/25/~020 4/27/2020 20*04072

  • E~*;~;;;;;-,;,. 1.55 *
  • EPA 901.1 Modified --==*4.58E*01 1.26E+OO 1.26E+OO 1.94E+OO U

-~=y~ii_g_==~=

20*04072*08 TRG B2*08201-CJWC*A018*CV00-05 05/10/1212:56 4/25/2020 4/27/2020. 20*04072 Holmium*166m EPA901.1 Modified 3.42E-01 5.13E-01 5.13E*01 3.33E*01 U

20*04072*08 '

TRG B2*08201*CJWC-A018.CV O O*O 5 05/10/12_1_2:56 4/25/2020 4/27/2020 20-04072 *

...... l"dine*129 EPA 901:.1.. Modified

  • 1.99E*02 7.20E*01 7.20E*01 1.0SE+OO
              • ~*-****

pCi/g 20*04072*08 TRG B2*08201*CJWC*A018.CV00-05 05/10/1212:56 4/25/2020 4/27/2020 20*04072 Potassium-40 EPA901.1 Modified 6.63E+OO 4.17E+OO 4.18E+OO 5.44E+OO pCi/g 20.04072.08 TRG B2*08201*CJWC*A018*CV00-05 05/10/1212:56

4/25/2020: 4/27/2020

! -2.99E+01 :

2.03E+02 2.03E+02 3.28E+02 U

pCl/g

-~*.,**----*--*-----*-*-~--*.,*****-

  • -************--*******. ******~*-*
    • ------ --~*---

20.04072.08 TRG B2*08201*CJWC*A018-CV00*05 05/10/1212:56

4/25/2020
  • 4/27/2020 20*04072 Molybdenum.93 EPA901.1 Modified

-2.37E*01 ! 5.55E*01 5.55E-01 7.95E*01 U

pCi/g 1----*****

20*04072*08 TRG B2-08201-CJWC-A018*CV00-05 05/10/1212:56 i 4/25/2020 4/27/2020 20*04072 Niobium-94 EPA901.1 Modified 2.62E*01 3.39E-01 3.39E*01 5.03E-01 U

pCi/g 20.04072.08 TRG B2-08201-CJWC*A018-CV O 0-0 5 05/10/12 12:56 4/25/2020 4/27 /202C020-04072 T*******c;~d*210~-- -** EPA 901.1 Modified 6.20E+OO 4.99E+OO 5.00E+OO 8.26E+OO u

  • -* ****;;cilg**-*

L.2-?:?.4072-08 TRG B2-08201*CJWC-A018-CVO 0-0 5

-*05/10/1212:56*-1 4/25/2020 4/27/2020

  • 20-0407:i°*t Lead-212 EPA901.1_Modified 8.14E-01 3.71E-01 3.73E-01 1.02E+OO -

lJ pCi/g 20-04072-08 TRG B2*08201-CJWC-A018-CV O 0-0 5 05/10/12 12:56 i 4/25/2020 4/27/2020 20-04072 L:.1'_~:2-.1.~*-****

EPA 901.1 Modified 1.25E+OO i 7.13E-01 7.16E-01 1.26E+OO

-*~---*,

pCi/g 20-04072*08 TRG B2-08201-CJWC-A018*CV00-05 05/10/1212:56 ! 4/25/2020. 4/27/2020, 20-04072 Promethium-145 EPA901.1 Modified

-2.10E-01 7.80E-01 7.80E*01 1.14E+OO U

pCi/g t-******

TRG B2*08201*CJWC*A018-CV00-05 05/10/1212:56

4/25/2020. 4/27/2020 20*04072 Radium*226 EPA901.1 Modified 1.31E+OO 6.33E-01 6.36E-01 9.56E-01 pCii;;. --**

20-04072-08 I 20-04072-08 TRG B2-08201-CJWC-A018-CV00-05

    • -*05/10/1212:56 i 4/25/2020' 4/27/2020' 20-04072 Antimony*125-****

EPA901.1 Modified

-2.89E-01 6.44E+OO 6.44E+OO 9.17E+OO U

pCi/g

'L~C!:-~?.?2*08 TRG B2-08201-CJWC*A018-CV O 0-0 5 05/10/12 12:56 I 4/25/2020 4/27/2020

  • 20-04072

.721()~.ufTl:~3'.\\-***.

_ EPA.9~~~1 ~.o~i~E>d. J 7.28E+OO 4.18E+OO 4.20E+OO 6.66E+OO pCi/g I

-~*0*04072*08 TRG B2-08201*CJWC*A018-CV00*05 05/10/1212:56

4/25/2020 4/27/2020' 20*04072 Thallium-208 EPA901.1 Modified

! 5.36E*01 9.57E-01 9.58E-01 1.57E+OO U

pCi/g 20-04072-08 TRG B2-08201*CJWC-A018-CV00-05 05/10/1212:56 i 4/25/2020 4/27/2020 20*04072 Uranium-235 EPA901.1 Modified i

7.87E-01 1.10E+OO 1.10E+OO 1.81E+OO U

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1*sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

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ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 5/7/2020 9:23 PM Page 16 of 19 Report To:

Work Order Details:

Eberline Analytical.

G_erald wo_od SOG.

~Q-04072 Final Re ort of Anal sis

!~~~ ~:

1~!

1~~~Ave--*** ******- ** ******-*-*-**-*"* * ;};1;;;fj~:{!i1! :* *-*fJ~i~6NMENTAL p

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SO Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result CU CSU MDA Qualifier,

Rep.art ID Type ID Date Date Date ID Units 20*04072-09

....... !RG B2-08201-CJWC-A018-CV 0 5-1 0

---~5,l_~0/12 12:56 4/251202,~--~13!~03_°-.* 20-04072 Actinium-228 EPA 901.1 Modified

-2.94E-01 8.38E-01 8.38E-01 1.11 E+00 U

pCi/g 20-04072-09_..

TRG B2-08201-CJWC-A018-CV05-10 05/10/1212:56

. 4/25/2020 4/27/2020 20-04072 Silver-108m EPA901.1 Modified 1.31~:01 1.19E-01 1.19E-01 2.29E-01 U

.........* pCi/g.....

20-04072-09 TRG B2-08201-CJWC-A018-CV05-10 05/10/1212:56

4/25/2020 4/27/2020 20-04072 Barium-133 EPA901.1 Modified

-5.55E-02 1.21E-01 1.21E-01 6.16E-01 U

pCi/g 20-04072-09 TRG 82-08201-CJWC-A018-CV05-1 0 05/10/1212:56 ! 4/25/2020 4/27/2020 20-04072 Bismuth-214 EPA901.1 Modified 9.88E-01 4.95E-01 4.98E-01 8.46E-01 pCi/g 20-04072-09 TRG B2-08201-CJWC-A018-CV 0 5-1 0 05/10/12 12:56 4/25/2020 4/27/2020 20-04072 Cobalt-60 EPA 901.1 Modified 6.65E-02 1.81 E-01 1.81 E-01 8.74E-01 U

pCi/g 20-04072-09 TRG B2-08201-CJWC-A018-CV 0 5-1 0 05/10/12 12:56

4/25/2020
  • 4/27/2020
    • 20-04072 Cesium-134 EPA 901.1 Modified 0.00E+00... 1.33E+00
    • -1.33E+OO
    • 46E.;OO U *
  • pCi/g 20-04072-09 ***--;:izG*.

B2-08201*CJWC~ci'is:cv*o*5-10 05/10/1212:56 4/25/2020 4/27/2020 20-04072 Cesium-137 EPA901.1 Modified 2.52E-01 2.28E:01 2.28E-01 4.02E-01 u

pCi/g 1------~---...;-----------****--********* ***--**-------------*-:-****.. *******-*---*----------+----*------+-----~--------------------~--*****----*-

20-04072-09 TRG B2-08201-CJWC-A018-CV05-10 05/10/1212:56

4/25/2020 4/27/2020 20-04072
  • Europium*152 EPA901.1 Modified 8.30E-02 6.27E-01 6.27E-01 1.02E+00 U

pCi/g 20-04072-09 TRG B2-08201-CJWC:A018-CV05-10 05/10/1212:56 1 4/25/2020 4/27/2020 20-04072 r* E~;~piu~'.:;54 EPA901.1 Modified 4.39E-01 8.07E-01 8.07E-01 6.61E-Oi U

pCi/g

  • 20:04072-09 _

... TRG***** B2-08201-CJWC-A018-CV 0 5.1 0 05/10/12 12:56 4/25/2020 4/27 iio20-20~04072.

Europium-155 EPA 901.1 Modified

-8.71 E-02 1.16E+00 1.16E+00 1.69E+00

.. u*....... **~----

20-04072-09 TRG B2-08201-CJWC-A018-CV05-10 05/10/1212:56 4/25/2020 4/27/2020 20-04072 Holmium-166m EPA901.1 Modified 2.90E-02 3.43E-01 t

3.43E-01 2.93E-01 U

pCi/g 20-04072-09...

TRG B2-08201-CJWC-A018-CV05-10 05/10/1212:56 ! 4/25/2020. 4/27/2020 20-04072:

lodj~e:129 EPA901.1 Modified

-3.76E-01 i

5.87E-01 i

5.87E-01 8.14E-01 U

--pCl/g*-*****

20-04072-09 TRG B2-08201-CJWC-A018-CV05-10 05/10/1212:56

4/25/2020 4/27/2020 20-04072 Potassium-40 EPA901.1 Modified 8.11E+00 3.11E+00,

3.14E+00 3.93E+00 pCi/g

-*20-04072-09 TRG B2-08201-CJWC-A018-CV05-1 0 05/10/1212:56 i 4/25/2020

  • 4/27/2020 20-04072 Manga~;;e-54 EPA901.1 Modified

-5.06E+01 1.56E+02 :

1.56E+02 1.90E+02 U

pCi/g

  • -20:04072-09 TRG B2-08201:CJWC-A018-CV 0 5-1 0 05/10112 12:56 i 4/25/2020 4/27/2020 20-04072
  • Molybdenum-93 EPA 901.1 Modified

-8.88E-02 3.31 E-01 3.31E-01 4.46E-01 u*. **. -****pCi/g****

20-04072-09-*

TRG B2-08201-CJWC-A018-CV05-10 05/10/1212:56

4/25/2020 4/27/2020, 20-04072 Niobium-94 EPA901.1 Modified

-7.09E-02 2.12E-01 2.12E-01 2.82E-01.....

U pCi/g 20-04072-09 TRG B2-08201-CJWC-A018-CV05-10 05/10/1212:56 i 4/25/2020 4/27/2020 20-04072,

Lead-210 EPA901.1 Modified 4.42E+00 3.86E+00 3.87E+00 6.32E+00 U

pCi/g

        • 20~04072-09 TRG.. !

B2-08201-CJWC-A018-CV05-10 05/10/1212:56 i 4/25/2020

  • 4/27/2020**:**20:04072 Lead-212 EPA901.1 Modified 3.96E-01 3.85E-01 3.86E-01 i

6.35E-01 U

pCi/g 20-04072-09

  • TRG B2-08201-CJWC-A018-CV05-10 05/10/1212:56 4/25/2020 4/27/2020 20-04072
  • Lead-214 EPA901.1 Modified 9.67E-01 4.55E-01 4.57E-01 9.06E-01 i

pCi/g 20-04072-09 i TRG B2-08201-CJWC-A018-CV05-10 05/10/1212:56 4/25/2020 4/27/2020 20-04072 Promethium-145 EPA901.1 Modified 9.01E-02 6.14E-01 6.14E-01 I

9.28E-01 U

pCi/g 20-04072-09 :

TRG B2-08201-CJWC-A018-CV05-1 0 05/10/1212:56 4/25/2020 4/27/2020 20-04072.

Radium-226 EPA901.1 Modified 9.88E-01 4.95E-01 4.98E-01 8.46E-01 i

pCi/g 20-04072-09

  • TRG B2-08201-CJWC-A018-CV05-1 0 05/10/1212:56 4/25/2020 4/27/2020 20-04072.

Antimony-125 EPA901.1 Modified

-1.17E+00 3.21E+00 3.21E+00 4.56E+00 U

pCi/g 20-04072-09 TRG j

B2-08201-CJWC-A018-CV 0 5-1 0 05/10/12 12:56 4/25/2020 4/27/2020 20-04072 Thorium-234 EPA 901.1 Modified 5.06E+00 3.29E+00

.... 3.30E+00 5.36E+00 _ !.. _ _ U......,....... pCi/g......

20-04072-09 TRG i

82-08201-CJWC-A018-CV05-1 0 05/10/1212:56 4/25/2020 4/27/2020 20-04072 Thallium-208 EPA901.1 Modified 7.44E-01 5.68E-01 5.69E-01 9.58E-01 U

pCi/g 20-04072-09 TRG B2-08201-CJWC-A018-CV0 5-1 0 05/10/1212:56 4/25/2020 4/27/2020 20-04072 Uranium-235 EPA901.1 Modified 1.69E-01 9.78E-01 9.78E-01 1.49E+00 i

U pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect

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EBERLINE

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ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621

Printed: 5/7/2020 9:23 PM Page 17 of 19 Report To:

Work Order Details:

Eberline Analytical G_eraldWo_od SOG.

20-04072 Zion Solutions Purchase Order.*

677116 Final Re ort of Anal sis 2701 Deborah Ave Analysis Categ~;::***-

ENVIRONMENTAL p

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Zion, IL 60099 Sample Matrix.*

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I M h d R

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  • . Q rfi i Report ID Type ID Date Date Date ID na yte et O esu 1 ua 1,er Units 20-04072-10 :

TRG L2-10214C-RJGS-001-SM-A 05/07/1907:45

4/25/2020 4/27/2020 20-04072 Actinium-228 EPA901.1 Modified 2.05E-01 8.86E-02 8.92E-02 1.84E-01 pCi/g 20-04072*10 TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45 4/25/2020 4/27/2020 20-04072 Silver-108m EPA 901.1 Modified 2.26E-02 1.67E-02 1.67E-02 3.00E-02 U

i pCi/g 20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/1907:45 4/25/2020 4/27/2020 20-04072 Barium-133...* EPA901.1 Modified 4.61E-03 3.41E-02 3.41E-02 4.72E-02 U

pCi/g

--20:04072-10 TRG

-****L2=1*0214c.RJGS-001-SM-A

. 05/07/19 07:45 4/25/2020

  • 4/27/2020 20-04072 :

Bismuth-214

  • --***EPA 901.1 Modified 1.82E-01 4.48E-02 4.58E-02 1.49E-01 pCi/g 20-04072-10 :

TRG L2-10214C-RJGS-001.SM*A 05/07/19 07:45 4/25/2020 4/27/2020 20-04072 Cobalt-60 EPA 901.1 Modified 2.65E-01 3.39E-02 3.65E-02 4.51 E-02 pCi/g 20-04072-10 I TRG L2-10214C-RJGS-001-SM-A

. -*05/07/1907:45. 4/25/2020 - 4/27/2020 20:04072..

Cesium-134 EPA901.1 Modified

-1.57E-01 4.61E-02 4.68E-02 3.57E-02 U

pCi/g 20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45

4!25!2020 4/27/2020 20-04072 Cesium-137 EPA 901.1 Modified 2.18E+OO 2.50E-01 2.74E-01 5.19E-02 pCi/g 20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/1907:45 4/25/2020 4/27/2020 20-04072 Europium-152 EPA901.1 Modified 1.33E-02 6.46E-02 6.46E-02 7.87E-02 U

pCi/g

      • -**" -------------------t--------i
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  • -*--*----- ---,t----------t****

20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45 4/25/2020 4/27/2020 20-04072 Europium-154 EPA901.1 Modified 4.61E-02 5.72E-02 5.72E-02 4.12E-02 U

pCi/g

.2°.:~_()72-10 TRG-* ** L2-10214C-RJGS-001-SM-A 05/07/19 07:45

4/25/2020 4/27/2020_. __ 2?:°.~0,~~.--_E_;'.':?Eium-155 EPA901.1 Modified

-8.47E-03 4.60E-02

... ~~°.E_~~--*

6.57E-02 U

pCi/g

.2..0:0,4?:2.: 10 TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45

, 4/25/2020 4/27/2020 20-04072 Holmium-166m EPA 901.1 Modified

.. 5.:7_9§~03_

2.77E-02 2.77E-02 2.78E-02 U

pCi/g *-

20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45 4/25/2020 4/27/2020 20-04072 lodine-129 EPA901.1 Modified 9.89E-03 2.49E-02 2.49E-02 7.80E-02 U

pCi/g 20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/1907:45 4/25/2020 4/27/2020' 20-04072 Potassium-40 EPA901.1 Modified 5.09E+OO 6.51E-01 7.02E-01 4.74E-01 pCi/g

'-------+---------*-----l-----~'------------------~--*-----

20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/1907:45 4/25/2020 4/27/2020 20-04072 Manganese-54 EPA901.1 Modified 7.01E-03 3.94E-02 3.94E-02 5.91E-02 U

pCi/g

,,...,,... -.,.~****

20-04072-10 TRG

.c L2-10214C-RJGS-001-SM-A 05/07/1907:45 4/25/2020 4/27/2020 20-04072 Molybdenum-93 EPA901.1 Modified

-1.32E-02 1.69E-02 1.69E-02 2.01E-02 U

pCi/g **-

20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/1907:45 4/25/2020 4/27/2020

  • 20-04072 Niobium-94 EPA901.1 Modified 2.40E-02 1.67E-02 1.68E-02 2.53E-02 U

pCi/g 20-04072-10,

TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45 4/25/2020 4/27/2020 : 20-04072 Lead-210 EPA901.1 Modified 4.98E-01 4.11E-01 4.12E-01 6.82E-01 U

pCi/g 20-04072-10 i TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45 4/25/2020 4/27/2020-20-04072 Lead-212 EPA 901.1 Modified 2.12E-01 i

5:56E-02 5.66E-02 7.94E-02 pCi/g r-** -----t-----,-------------+----------******---------***-******---*---****"-*----+----------+-----~------

20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45 4/25/2020, 4/27/2020 20-04072 Lead-214 EPA 901.1 Modified 2.10E-01 5.98E-02 6.07E-02 1.09E-01 i pCi/g 20-04072-10 i TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45 4/25/2020 4/27/2020 20-04072 ! Promethium-145 EPA 901.1 Modified

-4.66E-02 4.65E-02 4.66E-02 c--7.14E-02 i

U pCi/g 20-04072-10 i TRG L2-10214C-RJGS-001-SM-A 05/07/1907:45 4/25/2020

  • 4/27/2020 20-04072 Radium-226 EPA901.1 Modified 1.82E-01 4.48E-02 4.58E-02 1.49E-01 pCi/g 20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/1907:45 4/25/2020 4/27/2020
  • 20-04072 i Antimony-125 EPA901.1 Modified 3.SOE-02 7.98E-02 7.99E-02 i

1.18E-01 U

pCi/g 20-04072-10 TRG L2-10214C-RJGS-001-SM-A 05/07/19 07:45 4/25/2020 4/27/2020 20-04072 Thorium-234 EPA 901.1 Modified 8.17E-01 2.93E-01 2.96E-01 i

4.86E-01 U

pCUg 20-04072-10 i TRG L2-10214C-RJGS-001-SM-A 05/07/1907:45 4/25/2020. 4/27/2020 20-04072 Thallium-208 EPA901.1 Modified 1.SOE-01 i

5.83E-02 5.91E-02 9.63E-02 pCi/g 20-04072-10 i TRG i

L2-10214C-RJGS-001-SM-A 05/07/1907:45 4/25/2020' 4/27/2020 20-04072 Uranium-235 EPA901.1 Modified 1.17E-01 1.05E-01 1.05E-01 1.57E-01 i

U pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

(

EBERLINE

~

ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 5/7/2020 9:23 PM Gerald Wood I

Zion Solutions Rep_ort To:

Page 18 of 19 Work Order Details:

SDG:

20-04072

. **.f--,*

Purchase Order:

677116

,,4,,_,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,_____

**m*_,,,, __

,,,WAW Eberline Analytical Final Report of Analysis 2701 Deborah Ave

..,,,,,,,,1 Analysis Category:.

ENVIRONMENTAL

,,,,,,,,,,,,,,,,,,,,,,,,,,,,,, __,,_.,,_ ___ ---- ------,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,, ___,, -------1 Sample Matrix:

SO Zion, IL 60099 Lab Sample Client I

Sample Receipt Analysis Batch A

I I

M h d I R I

CU CSU MDA Q

rfi Report ID Type ID Date Date Date ID na yte et O esu t ua 1,er '

Units 20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25 4/25/2020 4/27/2020 20-04072 Actinium-228 EPA901.1 Modified 1.11E+00 2.50E-01 2.57E-01 4.54E-01 pCi/g 20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/191°-~2--5__

4/25/2020 4/27/2020 20-04072; Silver-108m EPA901.1 Modified

'is1E:03 -

4.71E-02

__ 4,?1~:o~:~--:T~C.E:°-2____

U pCi/g 20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25

4/25/2020 4/27/2020 20-04072 Barium-133 EPA901.1 Modified 8.15E-03 2.98E-02 2.98E-02 1.50E-01 U

pCi/g

  • =~~_, _

,=--**""""'"'"'""'""'w'~*-""""""""-*--~-e*:*--*-

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...-,---~"'",,,

20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25 4/25/2020 4/27/2020 20-04072 Bismuth-214 EPA901.1 Modified 1.24E+00 1.90E-01 2.00E-01 2.55E-01 pCi/g 20-04072-11 :

TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25 4/25/2020 4/27/2020 20-04072,------C~b;l;:60 EPA901.1 Modified...... _9.43E-02 7:75E_:P~... ;... -7:7-6~:°-~-*- 1.1i:~=a.1__ _

U

- P.~i!9..

20-04072-11,

TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25 4/25/2020 4/27/2020 20-04072 Cesium-134 EPA901.1 Modified 4.83E-02 5.80E-02 5.81E-02 1.47E-01 U

pCi/g

'"20:0407~:.1.2, ____ 1:1'~--

L1-12109L-CJGS-001-SB-A 08/21/1910:25 4/25/2020

__ 4,1271202-0 20-04072 Cesium-137 EPA901.1 Modified - I -1~47E:o;-***r---8.15E-°-~--

8.18E-02 1.31E-01

,,_pCi/g*-~

20-04072-11

  • TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25 4/25/2020 4/27/2020 20-04072 Europium-152 EPA901.1 Modified
-2.05E-03 1.31E-01 1.31E-01 2.52E-01 U

pCi/g 20-04072-11 !

TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25 4/25/2020 4/27/2020 20-04072 Europium-154 EPA901.1 Modified

-1.19E-01 2.01E-01, __ 2.01E:,°-1 1.31E-01 U

pCi/g 20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25 4/25/2020. 4/27/2020 20-04072 Europium-155 EPA901.1 Modified 1.01E+00 1.84E-01 1.91E-01 2.67E-01 pCi/g

"" --~*m*-*-*----,,_, --

,~~-*,,,,.-~,~*...-,,~--*~~,,

~ =~~';"="

20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25

4/25/2020 4/27/2020 20-04072 Holmium-166m EPA901.1 Modified 2.38E-01 8.51E-02 8.60E-02 1.38E-01 pCi/g

20-0407i11-TRG ___

L1-12109L-CJGS-001-SB-A 08/21/1910:25 4/25/2020 4/27/2020 20-04072 1

lodine-129 EPA901.1 Modified

-1.11E-01 __, ___ 216E:01-T 2.17E-01 3.07E-01 U --.

---pCi/g

--1, 20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08121_1.!_~ 10:25 ° 4/25/2020 ----~'-2~/~020 20-04072 : __ Potassium-40 EPA901.1 Modified 2.59E+01 2-:~~~+.00 2.96E+00 1:93E+OO pCi/g I,

20-04072-11 i TRG____

L1:12_109L-CJGS-001-SB-A___

08/21/1910:25 4/25/2020 4/27/2020 20-04072 __ Manganese-54

_____ -~_F'A901.1 Modified

_ __1~3E:01 _,

1.23E-01 1.23E-01 1.76E-01

, _U pCi/g 20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25

, 4/25/2020 4/27/2020 20-04072 Molybdenum-93 EPA901.1 Modified 1.49E-02 6.62E-02 6.62E-02 9.11E-02 U

pCi/g L~.°-4,072-11 TRG L1-12109L-CJGS-001-SB-A

-* 08/21_/1910:25--;*4i25/2020

  • 4/27/2020 20-04072 Niobium-94 EPA901.1 Modified ___

2.92E-02 6.45E-02 6.45E-02 9.12E-02 U

pCi/g 20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25 4/25/2020 4/27/2020 20-04072 Lead-210 EPA901.1 Modified 2.40E+00 1.43E+00 1.43E+00 2.34E+00 pCi/g 20-04072-11

  • TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25

. 4/25/2020 4/27/2020_, 20-04072 Lead-212 EPA901.1 Modified

- 1:1ii:oo :

1.89E-01 1.98E-01 2.88E-01 pCi/g

,,~--

~----~-~"-------------~--

' 20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25

, 4/25/2020 4/27/2020 20-04072 Lead-214 EPA901.1 Modified 1.35E+00 2.32E-01 2.42E-01 3.27E-01 1

pCi/g 8

,20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25 i 4/25/2020 4/27/2020 20-04072 Promethium-145 EPA901.1 Modified 4.47E-02____

1.81E-01 1.81E-01 2.63E-01 j_---*

U pCi/g 20-04072-11 TRG L 1-12109L-CJGS-001-SB-A 08/21/19 10:25 4,(~~!~~~.. ---4'.~/}020 I 20-04072 Radium-226 EPA 901.1 Modified 1.24E+00 i 1.90E-01 2.00E-01 i

2.55E-01 i

pCi/g 20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25

, 4/25/2020 4/27/2020 20-04072 Antimony-125 EPA901.1 Modified

-1.85E-01 1.95E-01 1.96E-01 2.67E-01 U

pCi/g 20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25 i 4/25/2020 4/27/2020 20-04072 Thorium-234 EPA901.1 Modified

--6:9:iE:;:;;-a--*

1.33E+00 1.37E+00 ;

1.97E+00 f"------U--

pCi/g

    • e*

-.s,--~~

***---* ******~**

20-04072-11 TRG L1-12109L-CJGS-001-SB-A 08/21/1910:25 1 4/25/2020" 4/27/2020 20-04072 Thallium-208 EPA901.1 Modified 9.01E-01 1.88E-01 1.93E-01 3.50E-01 pCi/g 20-04072-11 TRG I

L1-12109L-CJGS-001-SB-A 08/21/1910:25 1 4/25/2020 4/27/2020 20-04072 Uranium-235 EPA901.1 Modified 5.96E-01 3.59E-01 3.60E-01 5.40E-01 U

I pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

(

EBERLINE

~

ANALYTICAL EBERUNE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

Printed: 5/7/2020 9:23 PM Page 19 of 19 Ref)_ort To:

Work Order Details:

Gerald Wood SOG*

20-04072 Zion Solutions Purchase Order::

677116 f

Eberline Analytical Final Report of Analysis

,,J __ ~'!afJS.iS.,C:!3!'!gory-

  • ENVIRgNryi~T::,JII:\\~_ _

_______ -~---- _

2701 Deborah Ave Zion, IL 60099 Sample Matrix:

  • SO Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result CU CSU MDA Qualifier Units 20-04072-12 TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30 4/25/2020 4/27/2020 20-04072 Actinium-228 EPA90U Modified 5,36E-01 1.52E-01 1.54E-01 i

3_38E-01 pCi/g 20-04072-12 TRG L 1-12106L-CJGS-001-SB-A 08/14/19 13:30 4/25/2020 4/27/2020 : 20-04072 Silver-108m EPA 901 _1 Modified 4.17E-03 2,76E-02 2,76E-02 4,45E-02 U

pCi/g 20-04072-12 i TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30*-, 4/25/2020 4/27/2020 20-04072 Barium-133 EPA90U Modified

-3_19E-01 1.03E-01 1.05E-01 6,63E-02 U

  • c;/~

20-04072-12 TRG L 1-12106L-CJGS-001-SB-A 08/14/19 13:30 ! 4/25/2020 4/27/2020 20-04072 Bismuth-214 EPA 901-1 Modified 6.70E-01 1,24E-01 1,29E-01 i

1,96E-01 pCi/Q 20-04072-12 TRG L1-12106L-CJGS-001-SB-::A 08/14/1913:30 i 4/25/2020 4/27/2020 20-04072,,

Cobalt-60 EPA90U Modified 2,89E-02 5,38E-02 5.38E-02 7-28E-02 U

20-04072-12 :

TRG L1-12106L-CJGS-001-SB-A 08/1411913:30 4/25/2020 4/27/2020 20-04072 Cesium-134 EPA90U Modified 1,56E-02 3,25E-02 3_25E-02 7A8E-02 U

pCi/g 20-04072-12 i TRG L1-12106L-CJGS-001-SB-A

--08/14/1913:30 4/25/2020. 4/27/2020 20-04072,,,,,,C;;i~---

EPA90UModified 1,92E-01 6A3E-02 6,50E-02 9,63E-02

__,,_,,,_ pCi/g_,,,.,,

20-04072-12 TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30 4/25/2020, 4/27/2020---20:04072 -

Europium-152 EPA901.1 Modified 1.34E-01 ______ 1'.31E-01 1.31E-01

_ 1.51E-01 U

pCi/g 20-04072-12

  • TRG L1-12106L-CJGS-001-SB-A

___ ?_~/14/1913:30 4/25/2020 4/27/2020 20:04072

  • Europi~;:;;:154-

-EP/\\9011 M~ctifi~ct 1.57E:?~ ____

1.25E-01 1~25E=o~i--

- -7~86E~c12--,,~~~-u

  • ---* pCi/g 20-04072-12 TRG L1-12106L-CJGS-001-SB-A 08114/1913:30 4/25/2020
  • 4/27/2020 20-04072 Europium-155 EPA901.1 Modified 6.02E-02 6.89E-02 6.90E-02 U5E-01 U

pCi/g 20-04072-12 '

TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30 4/25/2020, 4/27/2020. 20-04072 Hol;:;;ium-1-66;:;;--*

EPA901.1 Modified 6.21E-02 6.76E-02 6.77E-02 9.36E U pCi/g==

20-04072-12 TRG L1-12106L-CJGS-001:SB:A 08/14/191330 ! 4/2512020 4/27/2020 20-04072 lodin~:129* --

  • EPA901.1M;dified 9.17E-02

,--8.74E:02 ___

8.76E-02 1'.23&01

  • U pCi/g 20-04072-12 TRG L 1-12106L-CJGS-001-SB-A 08/14/1913:30
4/25/2020 : 4/27/2020 20-04072 :

Potassium-40 EPA 901.1 Modified 1.95E+01----2~02E+OO 2.25E+OO U4E+OO

  • c~

1--20-04072-12 TRG L1-121-06L-CJGS-001-SB-A

---,--08/14/1913:30 4/25/2020 4127/2020 20-04072 Manganese-54 EPA901.1 Modified 3.61E-02 7.05E-02 7.05E-02 i 1.09E-01 i U

pCi/g 1--20:04072-12 i TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30 ! 4/25/2020, 4/27/2020 i 20-04072 Molybdenum-93 EPA901.1 Modified 1.21E-02 2.17E-02 2.17E-02 5.50E-02 i

U pCi/g 20-04072-12 :

TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30 4/25/2020 4/27/2020 20-04072-*

Niobium-94 EPA901.1 Modified

-3.10E-03 4.05E-02 4.05E-02 5.95E-02 U

pCi/g 20~04072-12 :

TRG L1-12106L-CJGS-001-SB-A o8i14/1913:30 i 4/25/2020 4/27/2020 20-?4?7.~-

-L~ad-210_

__ E_Pll9?11fv1~difi<e~

1A1E+oo,

1.05E+OO

_ 1.06E+oo 1.75E+oo _

LJ p~ii~ ___,.

20-04072-12 TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30

_ 4/25/2020 4/27/2020' 20-04072.

Lead-212 EPA901.1 Modified 4.37E-01 9.77E-02 1.00E-01 1.33E-01 pCi/g

,,,20-04072-12 TRG L1-12106L-CJGS-001-SB-A

  • ---,,,.08/14/1913:30 o-4/25/2020 4/27/2020 20-04072 ;

Lead-214 EPA901.1 Modified 6.06E-01 1.21E-01 1.25E-01 i

2.08E-01

,c.,,,,

pCi/g 20-04072-12 ___

TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30 i 4/25/2020 4/27/2020. 20-04072 ; Promethium-145 EPA901.1 Modified

-2.10E-01 !

1-25E-01 1.25E-01 1A5E-01 U

pCi/g 20:04072-12 TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30

[ 4/25/2020 4/27/2020 i 20-04072 Radium-226 EPA901.1 Modified

6.70E-01 1.24E-01 1.29E-01 1.96E-01 pCi/g 20-04072-12 TRG-- ;

L1-12106L-CJGS-001-SB-A 08/14/1913:30 j 4/25/2020 _ 4/27/2020 20-04072 :

Antimony-125 EPA901.1 Modifi_ed 3-25E-02 j 1.02E-01 1.03E-01 i

1.69E-01 U

pCilg 20-04072-12 TRG 1

L1-12106L-CJGS-001-SB-A 08/14/1913:30 I 4/25/2020, 4/27/2020 20-04072 Thorium-234 EPA901.1 Modified 1.10E+OO i 7.84E-01 7.86E-01 1.30E+OO U

pCi/g

  • -20:04072-12 TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30

, 4/25/2020 : 4/27/2020 20-04072 Thallium-208 EPA 901.1 Modified 5.15E-01 1.24E-01 1.26E-01*T-i10E-01 pCi/g 20-04072-12 TRG L1-12106L-CJGS-001-SB-A 08/14/1913:30 i 4/25/2020 4/27/2020 20-04072 Uranium-235 EPA901.1 Modified J

-1.06E-01 2.46E-01 2A6E-01 3.09E-01 U

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

(

EBERLINE

~

ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

~

ZIONSOLUTIONSru An EnergySo/u6ons Company Sample ID Sampl Matrix eLog B2-06207C-JFCCV-002- 0.0-0.5 NA NA B2-06207C-JFCCV-002- 0.5-1.0 NA NA B2-06104C-JFCCV-003- 0.5-1.0 NA NA B2-06104C-JFCCV-003-1.0-1.5 NA NA B 1-0620 lA-FSFC-009-CV NA NA B l-0620tA-FSWC-041-CV NA NA B 1-06201A-FSWC-050-CV NA NA B l-06202A-FSFC-028-CV NA NA B 1-06202A-FSWC-033CV NA NA u,

B l-06202A-FS W C-040-CV NA NA

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Comments FULL SUITE and 5 ROC 20.... 04072 REC'D APR 2 5 2020 Attachment _l :-- _ Cbain-_of-C_ufitody_F--91111 Sample Sample Container Sample Date Sample Analysis Type Type Vol Unit Type Qty Time Concrete 120.18 gm Plastic bag 1

11-19-2012 1045 FULL SUITE and 5 ROC Concrete 129.04 gm Plastic bag 1

11-19-2012 1045 FULL SUITE and 5 ROC Concrete 115.89 gm Plastic bag 1

11-12-2012 1008 FULL SUITE and 5 ROC Concrete 118.77 Plastic bag 1

11-12-2012 1008 FULL SUITE and 5 ROC gm Concrete 298.87 Plastic bag 1

06-07-2018 1130 FULL SUITE and 5 ROC gm Concrete 231.42 Plastic bag 1

06-18-2018 0900 FULL SUITE and 5 ROC gm Concrete 259.58 Plastic bag 1

06-07-2018 1300 FULL SUITE and 5 ROC gm Concrete 244.20 Plastic bag 1

06-18-2018 1450 FULL SUITE and 5 ROC gm Concrete 274.50 Plastic bag 1

06-18-2018 1344 FULL SUITE and 5 ROC gm FULL SUITE and 5 ROC Concrete 389.08 gm Plastic bag 1

06-18-2018 1030 Concrete 298.3 Plastic bag 1

05-05-2018 1515 FULL SUITE and 5 ROC gm Date Submitted To Lab:

Ship Container No.:

Cooler Temperature:

  1. A NA NA Date:

Time:

1Zr~r:rl r Kitkt 1 Date:

04/24/2020 lt'-15

()4/Ji/J?Dm 18~Ji//~70 TimeiGOCJ rt;rt-tfl,ori-1 owN, Wate: 6¥ ;7-i I 7-6 JO Dtlte: I Time:

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EXPEDITE ZS-WM-131 Revision 0 Information Use Preser Remarks vative NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA frll211~n~

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y B2-08101A-BJFC-007-CV 0.0-0.5 NA NA j32-08101A-BJFC-007-CV 0.5-1.0 NA NA
  • ~

B2-08201-CJWC-A018-CV 0.0-0.5 NA NA

~-08201-CJWC-A018-CV 0.5-1.0 NA NA tO L2-10214C-RJGS-001-SM-A NA NA

\\\\

L 1-12109L-CJGS-001-SB-A NA NA l?-

L 1-12106L-CJGS-OO I-SB-A NA NA Laboratory:

1.1.

Eberline Labs Rj~by~

Relrrr~~~~d f_/{i ch1 f Relinquished by: :/-e,,l ~ ')(

Comments FULL SUITE and 5 ROC 20"'"04072 REC'D APR 2 5 2020 - Chain-of-Custody Fonn Sample Sample Container Sample Date Sample Analysis Type Type Vol Unit Type Qty Time Concrete 120.18 gms Plastic 1

05-09-2012 1422 FULL SUITE and 5 ROC Concrete 175.02 gms Plastic I

05-09-2012 1422 FULL SUITE and 5 ROC Concrete 123,37

!mlS Plastic 1

05-10-2012 1256 FULL SUITE and 5 ROC Concrete 132.37 gms Plastic 1

05-10-2012 1256 FULL SUITE and 5 ROC Sediment 561.53 gms Marinelli 1

05-07-2019 0745 FULL SUITE and 5 ROC Soil 145.65 gms Marinelli 1

08-21-2019 1025 FULL SUITE and 5 ROC Soil 174.32 gms Marinelli 1

08-14-2019 1330 FULL SUITE and 5 ROC Date Submitted To Lab:

Ship Container No.:

Cooler Temperature:

NA NA NA Date:

Time:

~eseJed byi ~ ~ km Date:

04/24/2020 11 '-/-S' I 1 1(11-(; -

IC.

NI) J1// JJJUJ

~~f/;o;-0 Time: / f,~c) fl~7J/Pt-,~t-r/./ ~iqm1<< ?fao If 1-/tf J 'j_{) 2o D ;;ho Time: C/i{OCUYJ Rece~e~~

f v Date:

I q

1V,11,n tt-l~~l>n J

EXPEDITE ZS-WM-131 Revision 0 Information Use Preserv Remarks ative NA NA NA NA NA NA NA NA NA NA NA NA NA NA rffc~Number:

1olf1( OiJe111'&i1 9iJ3?-. OXJ.-'f OD 0 Ti)/L/£ Tiitoo Timq,;//)a '41

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