ML19295G625

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Revised Final Status Survey (FSS) Report - Phase 2, Isocs Analytical Reports, Part 3
ML19295G625
Person / Time
Site: Zion  File:ZionSolutions icon.png
Issue date: 03/06/2018
From:
ZionSolutions
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML19295G627 List:
References
ZS-2019-0090
Download: ML19295G625 (323)
v • d • e


Text

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          • GAMM A S P E C T R U M ANALYSIS *****

Filename: C:\GENIE2K\CAMFILES\00002470. CNF Report Generated On 3/6/2018 5:39:18 AM Sample Title B10lll 0AFSFC005GD Sample Description Ul CTMT Sample Identification 00 5 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"'2 Sample Taken On 3/3/2018 9:25: 00 AM Acquisition Started 3/3/2018 9 :17: 40 AM Live Time 600.0 seconds Real Time 601.3 seconds Dead Time 0.21 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 BCM [1136]

Peak Analysis Report 3/6/2018 5:39:18 AM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSFC005GD Peak Analysis Performed on: 3/6/2018 5:39:17 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 136 129.76 32.03 1.47 3.88E+002 66.15 1.80E+002 2 283- 308 301.48 75.02 1. 33 5.69E+002 140 .45 1.03E+003 3 952- 966 956.52 238.98 0.62 5.21E+001 50.57 2.02E+002 4 2635- 2659 2647.43 662.07 1. 59 2.92E+003 113.75 7.77E+001 5 3639- 3650 36 44 .62 911.47 0.48 1.85E+001 13.79 1 .16E+001 6 4477- 4488 4482.36 1120.93 0.56 1.76E+001 12.03 7.44E+OOO 7 4683- 4703 4694.30 1173.91 1. 76 1.29E+002 27.92 l .83E+001 8 5320- 5342 5331.60 1333.21 0.42 1. 34E+O 02 25.94 8.68E+OOO 9 5837- 5856 5845.94 1461. 75 0.67 9.68E+001 25.79 2.02E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F Fitted singlet Errors quoted at 2 . 000 sigma [1137]

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Sample

Title:

BlOlllOAFSFCOOSGD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  '"' ., * * * * *
  • e * * * * * * * * ~ *
  • IDENTIFIED NUCLIDES *
  • Iii .. * * * * * * * * *
  • I f' f I .,.
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M"2 ) Uncertainty K-40 0.999 1460.82* 10.66 1 .20279E+006 3.37003E+OOS Co-60 0.999 1173.23* 99.85 1 .59028E+005 3_67581E+004 1332.49* 99.98 1 .72240E+005 3.60012E+004 Cs-137 1.000 661.66* 85. 10 3.64209E+006 4.59772E+OOS Pb-212 1. 000 238.63* 43.60 9.39034E+004 9.23733E+004
             *=Energy line found in the spectrum.
             @=Energy line not used for Weighted Mean Activity Energy Tolerance :                    10.000 keV Nuclide confidence index threshold ~                        0.30 Errors quoted at 2. 000 sigma

[1138]

Interference Corrected Activity Report 3/6/20 18 5:39:18 AM Page 4

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M" 2 ) uncertainty K-40 0 .999 l.202786E+006 3.370029E+OOS Co-60 0 .999 1. 6 57715E+005 "*** 2.572010E+004 Cs-137 1 .000 3.642088E+006v" 4.597721E+OOS Pb-212 1 .000 9.390342E+004 9.237326E+004 

       ? = Nuclide is part of an undetermined solution X  =  Nuclide rejected by the interference analysis
      @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2.000 sigma
  **********     U N I D E N T I F I E D           P E A K S        **********

Peak Locate Performed on: 3/6/20 18 5:39:17 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.03 6.4653E-001 1 7.05 2 75.02 9.4794E-001 24.69 5 911.47 3 .. 07 SOE-0 02 74.72 Tol. Ac-228 6 1120.93 2.9267E-002 68.53 Tol. Bi-214 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1139]

Nuclide MDA Report 3/6/2018 5:39:18 AM Page 5

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSFC005GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       1460.82*   10.66  3.743E+005    3.74E+005     1. 203E+006   1.703E+D05
 +      Co-60      1173.23*   99.85  3.638E+004    2.BOE+004     1. 590E+005   1.652E+004 1332.49*   99.98  2.802E+004                  1. 722E+005   1.228E+004 Nb-94       702.65    99.81  4.023E+004    3.98E+004     4.752E+003    1.865E+004 87 1 .09  99.89  3.982E+004                 -3.561E+003    1.837E+004 Ag-108m     433.90    90.50  7.943E+004    4. 1 8E+004   1. 416E+004   3.831E+004 614.30    89.80  6.251E+004                 -1. 365E+004   2.969E+004 722.90    90.80  4.182E+004                 -3.004E+003    1.929E+004 Cs-134      60 4 .72  97.62  5.543E+D04    4.51E+004    -2.072E+004    2.628E+004 795.86    85.46  4.507E+004                  1.526E+004J   2.077E+004
 +      Cs-137      661.66*   85.10  7.688E+004    7.69E+D04     3.642E+006    3.675E+004 Eu-152      121.78    28.67  3.845E+OD5    1 . 6 4E+005  1.329E+0D5 v  1.888E+D05 344.28    26.60  2.638E+005                  1.044E+OD4    1.274E+005 1408.01    21.07  1.639E+005                  1.613E+005    7.35BE+004 Eu-154      123.07    40.40  2.686E+005    8.73E+004    -1.560E+004    1.319E+005 723.30    20.06  1.893E+005                 -7.786E+004    8.733E+004 1274.43    34.80  8.732E+004                  5. 438E+004 / 3. 874E+004 Eu-155       86 . 55  30.70  4.856E+D05    4.86E+005     6.485E+005    2.392E+005 105.31    21.10  5.711E+005                  1.256E+005    2.B07E+005 Tl-208      583. 19   85.00  6.115E+004    6.12E+004     3.552E+004    2.894E+004 Bi-212      727.33     6.67   5.477E+005   5.48E+005     3.221E+D05    2.518E+005
 +      Pb-212      238.63*   43.60  1.485E+005    1. 49E+005    9.390E+004    7.182E+004 Bi-214      609.32    45.49  1. 231E+005   1. 23E+005    3.055E+003    5.847E+004 1120.29    14.92   3.115E+005                 1.679E+005    1.447E+005 1764.49    15.30  2.148E+005                  9.801E+004    9.477E+004 Pb-214     295.22    18.42  4.016E+005    2. 06E+005    1 .255E+005   1.946E+005 351.93    35.60   2.060E+005                 8.937E+004    9.962E+004 Ra-226      186.21     3.64   2.542E+006   2.54E+006     1 .287E+006   1.244E+006 Ac-228      338.32    11.27   6.061E+005   1.75E+005    -1.555E+005    2.926E+005 911.20    25.80  1.747E+005                  7.506E+004    B.128E+004 968.97    15.80   2.877E+005                 1.424E+005    1 .338E+005 Am-241       59.54    35.90   4.261E+005   4.26E+005    -9.937E+004    2.085E+005
       + : Nuclide identified during the nuclide identification
       *: Energy line found in the spectrum
       >    Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @: Half-life too short to be able to perform the decay correction

[1140]

      • ~**********************************************************************
          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002478 .CNF Report Generated On 3/6/?.018 7:24:48 AM Sample Title Bl01110AFSFC006GD Sample Description Ul CTMT Sample Identification 006 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 1.256E+001 M" 2 Sample Taken On 3/3/2018 3: 00 : 00 PM Acquisition started 3/3/2018 2:52 :41 PM Live Time 600 . 0 seconds Real Time 601.9 seconds Dead Time 0 . 31 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 1/30/2018 Efficiency ID 2M90D ECP 1 7 8CM [1141]

Peak Analysis Report 3/6/2018 7:2 4 :48 AM Page 2

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Detector Name: 54 52 Sample

Title:

B101110AFSFC006GD Peak Analysis Performed on: 3/6/2018 7:24:48 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. counts 1 122- 136 129.35 31. 93 1. 25 4.50E+002 79.04 3.85E+002 2 286- 308 301.50 75.03 1. 25 7.70E+002 164.84 1.55E+003 3 334- 347 34 0 .45 84.78 0.75 7.13E+001 112.46 1.11E+003 4 482- 498 489.50 122.09 0.96 2.71E+002 112. 11 9.16E+002 5 841- 850 846.65 211.49 0.44 -1.69E+001 55.65 3.49E+002 6 1371- 1384 1377.72 344.39 1.20 9.21E+001 52.58 2.15E+002 7 1403- 1415 1409.09 352.24 0.32 2.94E+001 44.10 1.73E+002 8 1540- 1550 1545.72 386.43 0.67 1.73E+001 35.69 1.26E+002 9 2634- 2658 2646.60 661.86 1. 69 6.33E+003 165.24 1.21E+002 10 3109- 3123 3116.97 779.51 1. 10 4.55E+001 24.78 3.75E+001 11 3572- 3583 3577.57 894.70 0.51 5.58E+OOO 12.53 1.34E+001 12 3847- 3863 3855.22 964.13 1. 68 4.84E+001 23.20 2.76E+001 13 4337- 4351 4343.58 1086.24 0.34 3.35E+001 21.24 2.75E+001 14 4441- 4457 4448.50 1112.47 0.36 5.17E+001 23.16 2.63E+001 15 4683- 4704 4693.72 1173.77 0.97 1.98E+002 33.95 2.43E+001 16 5318- 5343 53 31. 25 1333.12 1. 25 2.27E+002 32.74 9.62E+OOO 17 5624- 5644 5633.78 1408.73 1. 07 1.02E+002 22.77 7.62E+OOO 18 5834- 5855 5845.11 1461.54 2. 14 1.23E+002 24.77 8.08E+OOO 19 7055- 7068 7061.23 1765.38 0.48 2.30E+001 11.93 3.98E+OOO M = First peak in a multiplet region m ; Other peak in a multiplet region F ~ Fitted singlet Errors quoted at 2 . 000 sigma [1142]

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Sample

Title:

B101110AFSFC006GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * * * * * * " I * * * * * * * *
  • IDENTIFIED NUCLIDES . . . . . . .. . . .. ..
                                                                                ,;                    ... ~ ~ . ...

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) uncertainty K-40 0. 999 1460.82* 10 .66 1.51053E+006 3.31445E+005 Co-60 0. 999 1173.23* 99.85 2.42296E+005 4. 58932E t*O 04 1332.49* 99.98 2.88607E+005 4.75389E+004 Cs-137 1. 000 661.66* 85 .10 7.88035E+006 9.68353E+005 Eu-152 1. 000 121.78* 28.67 6.94368E+OOS 3.19108E+005 344.28* 26.60 3.04553E+005 1.80917E+005 14 08.01* 21.07 6.28507E+005 1.48542E+005 Eu-155 0.331 86.55* 30.70 1.96963E+OOS 3.13205E+OOS 1 05 .31 21 .10 Pb-214 0.445 295.22 18 .42 351.93* 35.60 7.31540E+004 1.10320E+OOS 

          * ; Energy line found in the spectrum.
          @ = Energy line not used for Weighted Mean Activity Energy Tolerance :                     10.000 keV Nuclide confidence index threshold =                          0.30 Errors quoted at 2 .000 sigma

[1143]

Interference Correcte d Activity Report 3/6/2018 7:24:48 AM Page 4

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 0.999 1.510532E+006 3.3144SSE+OOS Co-60 0.999 2.646361E+OOS.I 3.301787E+004 Cs-137 1.000 7.880354E+006.I 9.683527E+OOS Eu-152 1. 000 S.205552E+D05,/ 1 .080254E+OOS Eu-155 0.331 1.969633E+OOS 3.1320SOE+OOS Pb-214 0.445 7.315402E+004 1.103203E+005 

       ? ~ Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2.000 sigma

[1144]

Int~rference Corrected Activity Report 3/6/2018 7:24:48 AM Page 5 

  **********    U N I D E N T I F I E D     P E AK S       **********

Peak Locate Performed on: 3/6/2018 7:24:48 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31.93 7.4923E-001 17.58 2 75.03 1.2827E+OOO 2 1. 42 5 211.49 -2.8092E-002 -33 0. 17 Sum 8 386.43 2.8765E-002 206.81 D-Esc . 10 779.51 7.5833E-002 54.46 Sum 11 894.70 9.2982E-003 224.51 S-Esc . 12 964.13 8.0740E-002 47.89 13 1086.24 5.5806E-002 63.43 14 1112.47 8.6122E-002 44.82 Tol. Bi-214 19 1765.38 3.8364E-002 51. 83 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1145]

Nuclide MDA Report 3/6/2018 7:24:48 AM Page 6

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Detector Name: 5452 Sample Geometry: Sample

Title:

B10ll10AFSFC006GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) K-40 1460.82* 10.66 2.564E+005 2. 5 6E+OD5 1.511E+006 1. 116E+O 05 

 +

co-60 1173.23* 99.85 4.164E+004 3. 0 0E+004 2.423E+OOS 1.916E+004 

 +

1332.49* 99.98 3.004E+004 2.886E+OOS 1.330E+004 Nb-94 702.65 99. 81 4.967E+004 4.97E+004 2.724E+004 2.338E+004 8 71. 09 99.89 5.446E+004 6.277E+004 2.570E+D04 Ag-108m 433.90 90.50 1. 0 91E+O 05 5.87E+004 -6.335E+004 5.315E+004 614.30 89.80 8.132E+004 -3.290E+003 3.909E+004 722.90 90.80 5.870E+004 3.875E+004 2.774E+D04 Cs-134 604.72 97.62 7.277E+004 5.14E+004 -5.444E+D04 3.495E+004 795.86 85.46 5.138E+004 t.ec 'f:.-t-{?f-2. 027E+OD3 2.394E+004 Cs-137 661. 66

  • 85. 10 9.494E+004 9.49E+004 7.8BOE+006 4 .579E+004
 +

Eu-152 121. 78* 28.67 4 .586E+005 1. 22E+OOS 6.944E+D05 2.2SBE+005 

 +

344.28* 26.60 2.752E+D05 3.046E+005 1.331E+OOS 1408. 01* 21.07 1.220E+005 6.285E+OOS 5.269E+004 Eu-154 123.07 40.40 3.653E+005 9.99E+004 3.515E+005 1 .802E+005 723.30 20.06 2.657E+005 1. 350E+005 1 . 256E+005 127 4 .43 34.80 9.994E+004 5.400E+003 4.51 0E+OD4 Eu-155 86.55* 30.70 5.128E+D05 S.13E+OOS 1.970E+OOS 2.527E+005 

 +                                                                        -7.379E+004  3.605E+D0 5 105.31     21.10   7.310E+005 Tl-208     583.19     85.00   8.5B6E+OD4      8.59E+004 -3.572E+003           4 .130E+OD4 Bi-212     727.33      6.67   7.694E+OD5      7.69E+005 4.629E+004            3.627E+005 Pb-212     238.63     43.60   2.682E+005      2.68E+005 1.607E+005            1.317E+OOS Bi-214     609.32     45.49   1.631E+OD5      1.63E+005 1.988E+005            7.845E+004 1120.29     14.92   3.441E+OD5                          5.446E+004  1. 611E+005 1764.49     15.30   2.715E+005                          2.257E+OOS  1. 233E+D05 Pb-214     295.22     18.42   5.449E+005      1 .82E+OOS 4.432E+004           2.663E+005
 +

35 1 .93* 35.60 1. 816E+005 7.315E+004 8.74 5E+D04 Ra-226 186.21 3.64 3.329E+OD6 3.33E+006 4.493E+OOS 1.637E+006 Ac-228 338.32 11. 27 8.367E+OD5 2.16E+OOS -8.513E+004 4.079E+005 911.20 25.80 2.158E+005 1 .853E+005 1 .019E+005 968.97 15.80 3.959E+OD5 -7.015E+004 1 .BBOE+005 Am-241 59.54 35.90 5.46DE+005 5.46E+005 -3.633E+OOS 2.684E+005 

       + = Nuclide identified during the nuclide identification
  • Energy line found in the spectrum
       > ; Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ = Half-life too short to be able to perform the decay correction

[1146]

      • ~*********************************************************************
          • GAMM A S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002469.CNF Report Generated On 3/6/2018 5:36:27 AM Sample Title B101110AFSWC007GD Sample Description Ul CTMT Sample Identification 007 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.l40E+OOO M"2 Sample Taken On 3/3/2018 9:00:00 AM Acquisition Started 3/3/2018 8:53:08 AM Live Time 600 . 0 seconds Real Time 602.1 seconds Dead Time 0.36 % Energy Calibration used Done On 1/13/2015 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 1 7 8CM [1147]

Peak Analysis Report 3/6/2018 5:36:27 AM Page 2

          • P E A K A N A L Y S I S REPORT *****

Detector Name: 5452 Sample

Title:

B101110AFSWC007GD Peak Analysis Performed on: 3/6/2018 5:36:27 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 136 129.21 31.90 1. 85 1.07E+003 90.97 2.65E+002 2 298- 310 302.45 75.27 0.58 1.74E+002 111 .28 1.09E+003 3 332- 348 340.40 84 .77 1. 04 1.74E+002 130.17 1.29E+003 4 2635- 2659 2647.25 662.02 1. 93 9.88E+003 207.76 2.23E+002 5 4684- 4706 4694.35 1173.93 1. 82 1. 27E+002 25.95 1.09E+001 6 5322- 5343 5331. 99 1333.31 2.44 1. 35E+002 25.52 7.59E+OOO 7 5837- 5857 5845.58 1461. 66 0. 43 1.07E+002 23.31 8.58E+OOO M = First peak in a mul tiplet region m _.. Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2.000 sigma [1148]

Interference Corrected Activity Report 3/6/2018 5:36:27 AM Page 3

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Sample

Title:

B101110AFSWC007GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES . .... . ....... ..... - .. - .... 

                                                               ~

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M"2 ) Uncertainty K-40 0.999 1460.82* 10.66 1.33449E+006 3.11894E+005 Co-60 0.999 1173.23* 99.85 1.57002E+005 3.44307E+004 1332.49* 99.98 1.73636E+005 3.55523E+004 Cs-137 1.000 661.66* 85.10 1.23467E+007 1 .50490E+006 Eu-155 0.332 86.55* 30.70 4.72162E+005 3.66209E+005 105.31 21.10 

       *=Energy line found in the spectrum.
       @=Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold=         0.30 Errors quoted at 2 .000 sigma

[1149]

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 0.999 1.334488E+006 3.118937E+005 Co-60 0.999 1. 650525E+005 v~ 2.473320E+004 Cs-137 1. 000 1. 234667E+007./ 1.504898E+006 Eu-155 0.332 4.721615E+005 3.662094E+005 

       ? ~ Nuclide is part of an undetermined solution X ~ Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at          2.000 sigma
  **********        U N I D E N T I F I E D           P E A K S      **********

Peak Locate Performed on: 3/6/2018 5:36:27 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 90 1.7831E+OOO 8.50 2 75.27 2.9018E-001 63.91 M = First peak in a multiplet region m .... Other peak in a multiplet region F a= Fitted singlet Errors quoted at 2 . 000 sigma [1150]

Nuclide MDA Report 3/6/2018 5:36:27 AM Page 5

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSWC007GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       1460.82*   10.66   2.515E+005     2. 5 1E+D05  1.334E+006       1.089E+005
 +      Co-60      1173.23*   99.85   2 . 945E+004   2. 5 6E+004  1.570E+005       1.305E+004 1332.49*   99.98   2.556E+004                  1. 736E+005      l.105E+004 Nb-94       702.65    99.81   3.268E+004     3.27E+004   -2.836E+004       1.488E+004 871.09    99.89   3.445E+004                  1.989E+004       1.568E+004 Ag-108m     433.90    90.50   1.301E+005     4.02E+004   -l.854E+004       6.364E+004 614.30    89.80   8.410E+004                 -1 .408E+004      4.048E+004 722.90    90.80   4.018E+004                 -2.812E+004       1 .847E+004 Cs-134      604.72    97.62   7.244E+004     3.38E+004    3. 453E+O 03...- 3.478E+004 795.86    85.46   3.382E+004                 -1. 993E+O 04     1 .515E+004
 +      Cs-137      661.66*   85.10   1. 272E+D05    1.27E+005    1. 235E+D07      6.191E+OD4 Eu-152      121.78    28.67   4.952E+005     l.72E+005   -7.730E+004       2.442E+005 344.28    26.60   4. 129E+005                 4.691E+oo5.r     2.020E+005 1408 .01   21.07   1. 722E+O 05                9.459E+004       7.771E+004 Eu-154      123.07    40.40   3.SOOE+OOS     8.73E+004   -6.506E+003       l.726E+005 723.30    20.06   1. 856E+OOS                 5.771E+003       8.549E+004 1274 .43   34.80   8.732E+004                  2.682E+OD3"      3.874E+004
 +      Eu-155       86.55*   30.70   5.773E+OOS     5.77E+005    4.722E+005       2.850E+005 105.31    21.10   7.356E+005                 -3.835E+005       3.629E+OOS Tl-208      583.19    85.00   7.849E+004     7.85E+004    4.933E+004       3.761E+004 Bi-212      727.33     6.67   5.362E+005     5.36E+005    4.666E+005       2.460E+005 Pb-212      238.63    43.60   2.799E+005     2.80E+005    1. 195E+005      1.375E+005 Bi-214      609.32    45.49   1.613E+OOS     1.61E+005     l.588E+005      7.758E+004 1120.29    14 .92  2.987E+005                 -2.765E+005       1. 383E+005 176 4 .49  15 .30  2.512E+005                  2.523E+005       1. 13 OE+O 05 Pb-214      295.22    18 .42  5.914E+OOS     3.03E+005     8.307E+003      2.895E+005 351.93    35.60   3.026E+OOS                  2.018E+005       1.479E+005 Ra-226      186.21     3.64   3.720E+006     3.72E+006     B.420E+005      1.833E+D06 Ac-228      338.32    11.27   9.556E+005     1.62E+005   -5.730E+005       4.673E+005 91 1. 20  25.80   1 .622E+OOS                -1.096E+005       7.505E+004 968.97    15.80   2.619E+005                   2.752E+005      1.209E+005 Am-241       59.54    35.90   5.242E+005     5.24E+005   -4.228E+005       2.57 5E+005
       +=Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1151]

          • GAMM A S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002477.CNF Report Generated On 3/6/2018 5:48: 40 AM Sample Title BlOlllOAFSWCOOBGD Sample Description Ul CTMT Sample Identification 008 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) BS - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO MA2 Sample Taken On 3/3/2018 2: 3 0: 00 PM Acquisition Started 3/3/2018 2: 21: 52 PM Live Time 600.0 seconds Real Time 602.0 seconds Dead Time 0 .33 % Energy Calibration Used Done on 1/13/2015 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 1 7 8CM [1152]

Peak Analysis Report 3/6/2018 5:48:40 AM Page 2

          • PE AK A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC008GD Peak Analysis Performed on: 3/6/2018 5:48:39 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 136 129.31 31.92 2.35 1 .03E+003 101 . 34 1.86E+002 2 284- 308 301.84 75. 11 1. 20 9.36E+002 178.64 1 .71E+003 3 483- 495 488.29 121.79 1. 32 2.87E+002 97.66 7.95E+002 4 589- 596 592.61 147 .90 0 .38 4.3DE+001 54.37 3.45E+002 5 1188- 1197 1192.07 297.94 0 .47 7.95E+OOO 39.52 1.66E+002 6 1371- 1387 1377.84 344.42 0 .65 2.46E+002 65.77 2.66E+002 7 1837- 1846 1841.61 460.47 0 .42 1 .74E+001 36.55 1. 3 8E+O 02 8 2634- 2659 2646.80 661.91 1. 72 6.58E+OD3 168. 54 1 .25E+002 9 3105- 3129 3117.08 779.54 1. 29 1 .44E+OD2 32. 18 2.78E+001 10 3463- 3474 3468.96 867.54 1. 07 2.79E+001 22.66 3.91E+001 11 3844- 3866 3857.03 964.59 1. 43 1 .10E+OD2 37.68 6.31E+001 12 4335- 4349 4342.97 1086.08 1. 20 S.75E+OD1 25.27 3.55E+001 13 4440- 4459 4448.59 1112.49 0 .67 1 .14E+002 30.59 3.43E+001 14 4682- 4705 4693.48 1173. 71 1. 49 2.43E+OD2 37.84 2.91E+001 15 5318- 5342 5331.20 1333. 11 1. 55 2.27E+OD2 30.97 3.llE+OOO 16 5623- 5643 5632.99 1408.54 1. 72 1 .84E+OD2 31. 29 1 .72E+001 17 5836- 5852 5843.64 1461.18 1. 50 9.04E+OD1 26.33 2.66E+001 M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2.000 sigma [1153]

Interference Correcte d Activity Report 3/6/2018 5:48:40 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC008GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) uncertainty K-40 1.000 1460.82* 10. 66 1.12228E+006 3.41262E+005 Co-60 1.000 1173.23* 99.85 3.00005E+005 5.25466E+004 1332.49* 99.98 2.90935E+OOS 4.60257E+004 Cs-137 1.000 661.66* 85.10 8.21534E+006 1. 00864E+006 Eu-152 1.000 121.78* 28.67 7.29984E+005 2.88325E+005 344.28* 26.60 8.13796E+005 2.55151E+005 1408.01* 21. 07 1.14001E+006 2.14448E+005 

       * ~ Energy line found in the spectrum.
       @ ~ Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold            0 .30 Errors quoted at 2.000 sigma

[1154]

Interference Corrected Activity Report 3/6/2018 5:48:40 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 1. 000 1 .122281E+006 3.412618E+005 Co-60 1 .000 2. 948725E+OOS .., 3.462235E+004 Cs-137 1 .000 8. 215344E+006 V 1 .008635E+006 Eu-152 1 .000 9. 3 76463E+005 ../ 1 .426613E+OOS X Pb-214 0 .939 

       ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1155]

Interference Corrected Activity Report 3/6/2018 5:48:40 AM Page 5 

  **********      U N I D E N T I F I E D      P E A K S     **********

Peak Locate Performed on: 3/6/2018 5:48:39 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 92 1.7142E+OOO 9.85 2 75. 11 1. 5593E+OOO 19.09 4 147.90 7.1602E-002 126.55 D-Esc . 5 297.94 1. 3247E-002 497.16 7 460.47 2.8917E-002 210.66 Sum 9 779.54 2. 4031E-001 22.32 Sum 10 867.54 4.6517E-002 81.17 11 964.59 1.8316E-001 34 .28 12 1086.08 9.5874E-002 43.93 13 1112.49 1.8942E-001 26.92 M "" First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1156]

Nuclide MDA Report 3/6/2018 5:48:40 AM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B10ll10AFSWC008GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/M"2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10 .66  4.058E+005     4.0 6E+005  1. 122E+006    1 .861E+005
 +      Co-60      1173.23*    99.85   4.695E+004     1.86E+004   3.000E+OOS     2.180E+004 1332.49*    99.98   1.858E+004                 2.909E+OOS     7.557E+003 Nb-94       702.65     99.81   5.169E+004     5.17E+004  -2.613E+004     2.438E+004 87 1 .09   99.89   6.931E+004                 6.812E+004     3.311E+004 Ag-108m     433.90     90.50   1.171E+005     6.03E+004   7.449E+004     5.712E+004 614.30     89.80   8.571E+004                -4.969E+004     4.128E+004 722.90     90.80   6.030E+004                -1.566E+004     2.853E+004 Cs-134      604.72     97.62   7.834E+004     7.0SE+004  -2.994E+004     3.773E+004 795.86     85.46   7.046E+004                 4.336E+OQ4 /   3.347E+004
 +      Cs-137      661.66*    85.10   9.753E+004     9.75E+004   8.215E+006     4.708E+004
 +      Eu-152      121. 78*   28.67   3.903E+005     1.76E+OOS   7.300E+OOS     1 .917E+005 34 4 .28*  26.60   3.230E+005                 8.138E+OOS     1 .570E+005 1408.01*    21.07   1.761E+005                 1.140E+006     7.967E+004 Eu-154      123.07     40. 40  3.816E+005     1. 22E+005  6. 575E+O 05-' 1 .884E+005 723.30     20.06   2.791E+005                 4.812E+004     1 .322E+005 1274.43     34.80   1.220E+005                 8.563E+004     5.608E+004 Eu-155       86.55     30.70   6.068E+005     6.07E+OOS   7.141E+005     2.998E+005 105.31     21.10   7.290E+005                -3.500E+005     3.596E+005 Tl-208      583.19     85.00   8.835E+004     8.83E+004   1.004E+004     4.254E+004 Bi-212      727.33      6.67   8.109E+005     8.11E+005  -4.511E+004     3.834E+005 Pb-212      238.63     43.60   2.795E+005     2.80E+OOS   4.947E+004     1.373E+005 Bi-214      609.32     45.49   1. 709E+005    1.71E+005   6.930E+004     8.235E+004 1120.29     14.92   3.885E+005                 3.445E+OOS     1 .832E+005 1764.49     15.30   2.635E+005                 2.804E+005     1 .191E+005 Pb-214      295.22*    18.42   3.059E+005     2.41E+OOS   3.627E+004     1 .468E+005 35 1 .93*  35.60   2.414E+005                 6.081E+OOS     1 .173E+OOS Ra-226      186.21      3.64   3.315E+006     3.31E+006   2.987E+OOS     1 .630E+006 Ac-228      338.32     11.27   9.150E+005     2.27E+OOS  -7.792E+005     4.470E+005 911. 20    25.80   2.274E+005                -1.647E+004     1 .077E+005 968.97     15.80   5.195E+005                 4.649E+004     2.497E+OOS Am-241       59.54     35.90   5.557E+005     5.56E+005   3.218E+OOS     2.733E+005
       + =Nuclide identified during the nuclide identification
       * - Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1157]

          • GAMMA S P E C T R U M ANALYSIS *****

Filename: C:\GENIE2K\CAMFILES\00002476.CNF Report Generated On 3/6/2018 5:46:43 AM Sample Title B101110AFSWC009GD Sample Description Ul CTMT Sample Identification 009 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) BS - 8192 Identification Energy Tolerance 10.000 keV Sample Size 1.256E+001 M"2 Sample Taken On 3/3/2018 2:06:00 PM Acquisition Started 3/3/2018 2:02:09 PM Live Time 600.0 seconds Real Time 604.8 seconds Dead Time 0 . 80 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration used Done On 1/30/2018 Efficiency ID 2M90D ECP 17 8CM [1158]

Peak Analysis Report 3/6/2018 5:46:43 AM Page 2

          • P E A K A N A L Y S I S REPORT *****

Detector Name: 5452 Sample

Title:

B1 01ll0AFSWC009GD Peak Analysis Performed on: 3/6/2018 5:46:43 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 119 116.40 28.69 0.57 1.61E+002 50.35 1 .91E+002 2 153- 168 161.10 39.88 1.42 8.96E+002 139.40 1 .32E+003 3 284- 309 301.23 74.96 1. 51 2.68E+003 307.52 4.93E+003 4 331- 347 340.10 84.69 1.54 8.09E+002 218 .19 3.53E+003 5 479- 496 488.42 121.82 1. 54 2.20E+003 220.98 3.08E+003 6 971- 987 979.82 244.81 1. 88 4. 45E+002 128.90 1 .19E+003 7 1105- 1114 1108.88 277. 11 0.32 -2.84E+OOO 68.55 5.18E+002 8 1367- 1388 1378.02 344.47 1. 72 1. 90E+O 03 143.18 8.61E+002 9 1768- 1786 1776.85 444.27 1. 27 2.23E+002 93.91 5.86E+002 10 2634- 2659 2646.83 661.92 1. 84 6.77E+003 186.05 4.45E+002 11 3103- 3128 3115.89 779.24 1. 76 7.88E+002 90.26 2.94E+002 12 3457- 3482 3469.86 867.77 0.93 3.22E+002 73.22 2.38E+002 13 3843- 3869 3856.58 964.47 1. 90 8.28E+002 88.88 2.62E+002 14 4010- 4030 4019.18 1005.13 0.39 9.83E+001 50.85 1.49E+002 15 4330- 4365 4343.42 1086.20 2.26 6.30E+002 93.49 2.77E+002 16 4434- 4462 4448.51 1112.47 1. 97 7.97E+002 78 .45 1.61E+002 17 4679- 4707 4693.44 1173.70 1. 90 1. 03E+O 03 85.11 1 .69E+002 18 5090- 5109 5099.29 1275.15 1. 89 1. 08E+O 02 32.81 4.61E+001 19 5189- 5205 5197.22 1299.63 0.76 6.65E+001 24.22 2.55E+001 20 5316- 5345 5331.01 1333.06 1. 93 1. 05E+003 71.32 4.76E+001 21 5618- 5646 5633.20 1408.59 2.31 1. 29E+O 03 76.98 4.0lE+OOl 22 5837- 5854 5844.80 1461.47 0.84 1. OOE+O 02 29 .23 3.40E+001 M. First peak in a multiplet region m ~ Other peak in a mul tiplet region F Fitted singlet Errors quoted at 2 , 000 sigma [1159]

Interference Corrected Activity Report 3/6/20 18 5:46:43 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSWC009GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB t * * * * * * * * "' * * * * * *

  • I *
  • IDENTIFIED NUCLIDES * "" * * ,.. * * * * * * *
  • I '"' * ,. * *
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/M"'2 ) uncertainty K-40 0.999 1460.82* 10.66 1.22861E+006 3.74762E+005 Co-60 1 .000 11 73.23* 99.85 1.2617SE+006 1 .45145E+005 1332.49* 99.98 1. 33067E+006 1 .39742E+005 Cs-137 1 .000 661.66* 85.10 8.43691E+006 1 .03918E+006 Eu-152 1 .000 121.78* 28.67 5.64754E+006 1 .26500E+006 344.28* 26.60 6.2719SE+006 1 .13439E+006 1408.01* 21.07 7.94270E+006 7.91875E+005 Eu-154 0 .682 123.07* 40.40 4.00779E+006 9.00236E+OOS 723.30 20.06 1274.43* 34.80 3.88489E+005 1.22322E+005 Eu-155 0. 330 86.55* 30.70 2.23735E+006 7.51275E+005 1 05 .31 21.10 Pb-212 0 .941 238.63* 43.60 8.11116E+005 2.68932E+005
          *=Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                      10.000 keV Nuclide confidence index threshold=                           0. 30 Errors quoted at 2. 000 sigma

[1160]

Interference Corrected Activity Report 3/6/2018 5:46:43 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 0.999 1.228613E+006 3.747621E+005 Co-60 1. 000 1.297519E+006 ,, 1 .006684E+005 Cs-137 1. 000 8 .436914E+006 *f . 1 .039183E+006 Eu-152 1. 000 6.915232E+006 / 5.752654E+OOS Eu-154 0.682 3. 650281E+005 / 1 .212489E+005 Eu-155 0.330 2.237350E+006 7.512754E+OOS Pb-212 0.941 8.111156E+005 2.689320E+OOS X Pb-214 0.388 

      ? - Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ ~ Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2. 000 sigma

[1161]

Interference Corrected Activity Report 3/6/2018 5:46:43 AM Page 5 

  **********     U N I D E N T I F I E D     P E A K S     **********

Peak Locate Performed on: 3/6/2018 5:46:43 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 28.69 2.6755E-001 31.36 2 39.88 1.4927E+OOO 15.57 3 74.96 4.4703E+OOO 11. 47 7 277.11 -4.7379E-003 -2411.5 9 444.27 3.7116E-001 42.17 D-Esc. 11 779.24 1 .3130E+OOO 11. 46 Sum 12 867.77 5.3624E-001 22.76 Tol. Nb-94 13 964.47 1 .3792E+OOO 10.74 14 1005.13 1 .6391E-001 51.71 Sum 15 1086.20 1.0497E+OOO 14.85 16 1112.47 1.3282E+OOO 9. 84 Tol. Bi-214 19 1299.63 1.1083E-001 36.42 Sum M  := First peak in a multiplet region m "" Other peak in a multiplet region F ; Fitted singlet Errors quoted at 2 . 000 sigma [1162]

Nuclide MDA Report 3/6/2018 5:46:44 AM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSWC009GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/M"2 ) 

 +      K-40       1460.82*   10.66   4.643E+005     4.64E+005            1.229E+006  2.15SE+005
 +      Co-60      1173.23*   99.85   1. 16 OE+005   6.58E+004            1.262E+006  5.634E+004 1332.49*   99.98   6.585E+004                          1.331E+006  3.121E+004 Nb-94       702.65    99.81   1.221E+OOS     l. 22E+005          -6.285E+004  5.957E+004 871.09    99.89   1. 526E+005                         6.676E+004  7.476E+004 Ag-108m     433.90    90.50   1. 693E+005    1.47E+005            2.756E+004  8.326E+004 614.30    89.80   1. 513E+005                        -2.891E+003  7.410E+004 722.90    90.80   1.467E+005                          9.660E+004  7.174E+004 Cs-134      604.72    97.62   1. 357E+OOS    1. 36E+005          -6.135E+004  6.642E+004 795.86    85.46   l.389E+005        ,J,c;(} ; ,. 0 / -2.871E+004  6.770E+004
 +      Cs-137      661.66*   85. 10  1. 811E+005    1.81E+005            8.437E+006  8.884E+004
 +      Eu-152      121.78*   28.67   8.506E+OOS     2.93E+005            5.648E+006  4.218E+005 344.28*   26.60   6.272E+005                          6.272E+006  3.091E+005 1408.01*   21.07   2.933E+005                          7.943E+006  1.383E+OOS
 +      Eu-154      123.07*   40 .40  6.036E+OOS     1.60E+005            4.008E+006  2.994E+005 723.30    20.06   6.632E+005                          5.066E+005  3.243E+OOS 1274.43*   34.80   1. 601E+005                         3.88SE+OOS  7.519E+004
 +      Eu-155       86.55*   30.70   9.659E+OOS     9.66E+005            2.237E+006  4.792E+OOS 105.31    21.10   1. 261E+006                        -1.077E+006  6.253E+005 Tl-208      583.19    85.00   1. 587E+005    1 .59E+005           1.288E+OOS  7.770E+004 Bi-212      727.33     6.67   1. 939E+006    l .94E+006           3.928E+005  9.476E+OOS
 +      Pb-212      238.63*   43.60   3.699E+OOS     3.70E+005            8.111E+005  l.825E+OOS Bi-214      609.32    45.49   2.926E+OOS     2.56E+005            2.031E+OOS  1.432E+005 1120.29    14.92   6.923E+005                          7.172E+004  3.352E+OOS 1764.49    15.30   2.560E+005                          2.675E+005  1.155E+OOS Pb-214      295.22    18.42   8.776E+005     4.69E+005           -5.753E+OOS  4 .326E+005 351.93*   35.60   4.686E+005                          4.686E+006  2.310E+005 Ra-226      186.21     3.64   5.311E+006     5.31E+006            1.691E+006  2.628E+006 Ac-228      338.32    11. 27  1. 421E+006    4.57E+005           -6.673E+OOS  7.000E+OOS 911. 20   25.80   4.567E+005                         -3.441E+004  2.223E+005 968.97    15.80   1. 21SE+006                        -1. 751E+OOS 5.974E+005 Am-241       59.54    35.90   9.009E+005     9.01E+005            2.163E+005  4.458E+005
       + ~ Nuclide identified during the nuclide identification
       * = Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ = Half-life too short to be able to perform the decay correction

[1163]

          • GAMMA S P E C T R U M li1'-JliLYS I S *****

Filename: 5452 Report Generated On 3/5/2018 10:17:21 AM Sample Title BlOlllOAFSWCOlOGD Sample Description Ul CTMT Sample Identification 010 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 1.256E+001 MA2 Sample Taken On 3/5/2013 10:05:00 PM Acquisition Started 3/5/2018 10:07:15 AM Live Time 600.0 seconds Real Time 604.6 seconds Dead Time 0 . 76 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 1/30/2018 Efficiency ID 2M90D ECP 17 8CM [1164]

Peak Analysis Report 3/5/2018 10:17:21 AM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC010GD Peak Analysis Performed on: 3/5/2018 10 :17:21 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 135 128.39 31.69 1. 80 5.98E+002 119.69 7.03E+002 2 153- 168 160.73 39.79 1. 33 1 .08E+003 140. 75 1.29E+003 3 177- 189 182. 00 45.11 1. 46 2.96E+002 105.53 9.46E+002 4 284- 308 300.78 74.85 1. 15 2.56E+003 302.49 4.93E+003 5 332- 346 340.25 84.73 1. 02 4.27E+002 205.78 3.52E+003 6 479- 496 488.08 121.73 1.24 2.50E+003 217.96 2.88E+003 7 972- 985 979.13 244.64 1.03 4.43E+002 102.57 7.95E+002 8 1366- 1398 1376.67 344.13 1. 39 1.72E+003 166.87 9.86E+002 9 1454- 1463 1458.22 364.54 0.67 3.28E+001 46.70 2.26E+002 10 1632- 1649 1643. 71 410 .95 1. 14 1.14E+002 74.62 3.93E+002 11 1767- 1781 1775.37 443.90 1. 23 l.98E+002 63.97 2.87E+002 12 2248- 2261 2252.76 563. 3 4 0.93 4 .16E+001 48.78 2.00E+002 13 2430- 2443 2437.70 609.60 0.91 6.53E+001 48.49 1.90E+002 14 2634- 2655 2644.64 661. 3 7 1. 30 1.04E+003 93.97 3.13E+002 15 2746- 2759 2751.09 688. 00 0.39 1.46E+001 47.50 1.97E+002 16 3101- 3123 3113.29 778.59 1. 86 7.27E+002 80.19 2.27E+002 17 3454- 3478 3466.71 866.98 1. 48 2.97E+002 68 .12 2.09E+002 18 3842- 3866 3853.64 963. 74 1. 57 7.68E+002 78.07 1 .84E+002 19 4007- 4024 4016.89 1004 .56 1. 05 8.05E+001 43.65 1. 22E+002 20 4326- 4366 4340.36 1085.43 1. 65 6.58E+002 91.70 2.35E+002 21 4431- 4455 4445.42 1111. 70 1. 69 7.15E+002 75.74 1 .71E+002 22 4675- 4700 4689.86 1172.81 1. 96 9.99E+002 73.45 8.15E+001 23 4743- 4754 4748.81 1187.54 0 .48 2.lOE+OOl 19.12 2.80E+001 24 4840- 4857 4848.23 1212.39 1. 30 7.48E+001 30. 64 4.92E+001 25 5084- 5103 5094.84 1274.04 1. 44 1.00E+002 30.99 4.00E+OOl 26 5184- 5203 5193.28 1298.64 0.54 9.50E+001 28.76 3.20E+001 27 5311- 5339 5326.88 1332.03 1. 91 9.52E+002 65.59 2.61E+001 28 5615- 5642 5629.15 1407.58 1. 72 1. 26E+003 73.41 2.05E+001 29 5831- 5849 5839.85 1460.23 0 .84 9.95E+001 29.05 3.25E+001 M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F ~ Fitted singlet Errors quoted at 2 . 000 sigma [1165]

Interference Corrected Activity Report 3/5/2018 10 :17:21 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSWC010GD Nuclide Library used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * * *
  • I * * ** * * '"' * * * * *
  • IDENTIFIED NUCLIDES .................... . .

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/M'.'2 ) Uncertainty K-40 0 .999 1460.82* 10.66 1. 22254E+006 3.72311E+005 Co-60 0 .995 1173.23* 99.85 2.36264E+006 2.56667E+005 1332.49* 99.98 2.33067E+006 2.46078E+OOS Ag-108m 0 .417 4 33.90* 90.50 2.09313E+005 7.44155E+004 614.30* 89.80 7.60347E+004 5.71809E+004 722.90 90.80 Cs-137 1. 000 661.66* 85.10 1. 44658E+006 2.17763E+005 Eu- 152 0 .999 121.78* 28.67 8.28136E+006 1 .80885E+006 344.28* 26.60 7.34762E+006 1 .40219E+006 1408.01* 21. 07 9.96037E+006 9.86713E+005 Eu- 154 0 .681 123.07* 40.40 6.80664E+006 1 .49114E+006 723.30 20.06 1274.43* 34.80 5.38696E+005 1.72583E+005 Eu- 155 0.329 86.55* 30.70 2.44906E+006 1.27694E+006 105.31 21. 10 Pb-212 0.944 238.63* 43.60 8.07168E+005 2.27859E+005 Bi-214 0.687 609.32* 45.49 1.49181E+005 1.12194E+005 1120.29* 14.92 5.79294E+006 7.69579E+005 1764.49 15.30 

          * = Energy line found in the spectrum.
          @ = Energy line not used for Weighted Mean Activity Energy Tolerance :                       10.000 keV Nuclide confidence index threshold=                             0.30 Errors quoted at 2.000 sigma

[1166]

Interference Corrected Activity Report 3/5/2018 10 :17:21 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 0.999 1.222540E+006 3.723112E+005 Co-60 0.995 2. 34 5984E+O O6v' 1 .776290E+OOS Ag-108m 0.417 1. 041663E+005 7.313673E+004 Cs-137 1.000 1.446579E+006 / 2.177634E+005 Eu-152 0.999 8.836828E+006v'" 7.335286E+005 Eu-154 0.681 5. 254711E+005 / 1. 713711E+005 Eu-155 0.329 2.449062E+006 1. 2 7694 OE+ 006 Pb-212 0.944 8.071680E+005 2.278587E+005 Bi-214 0.687 6.661256E+004 1. 790708E+005 X Pb-214 0.383 

       ?  =   Nuclide is part of an undetermined solution X   =   Nuclide rejected by the interference analysis
      @   ;;: Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2.000 sigma

[1167]

Interference Corrected Activity Report 3/5/2018 10: 17 :21 AM Page 5 

  **********      U N I D E N T I F I E D      P E A K S       **********

Peak Locate Performed on: 3/5/2018 10 :17:21 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 69 9.9678E-001 20. 01 2 39.79 1.7950E+OOO 13.07 3 45.11 4.9263E-001 35.70 4 74.85 4.2631E+OOO 1 1.83 9 364.54 5.4628E-002 142.48 Sum 10 410.95 1. 8973E-001 65.54 12 563.34 6.9251E-002 117.39 Sum 15 688.00 2.4347E-002 325.12 Sum 16 778.59 l .2114E+OOO 1 1 .03 Sum 17 866.98 4.9443E-001 22.96 Tol. Nb-94 18 963.74 1.2797E+OOO 10 . 17 Tol. Ac-228 19 1004 .56 1.3415E-001 54.23 Sum 20 1085.43 1.0961E+OOO 13.94 23 1187.54 3.5009E-002 91.01 Sum 24 1212.39 1. 2464E-001 40.98 Sum 26 1298.64 1 .5831E-001 30.27 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted*singlet Errors quoted at 2.000 sigma [1168]

Nuclide MDA Report 3/5/2018 10:17:21 AM Page 6

          • N U C L I D E MDA REPORT *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSWC010GD Nuclide Library Used : C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2 ) (pCi/M"2 ) (pCi/M"'2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10 .66  4.599E+005    4.60E+OOS      1 .223E+006    2.133E+005
 +      Co-60      1173.23*    99.85   1.518E+005    9.62E+004      2.363E+006     7.269E+004 1332.49*    99.98   9.618E+004                   2.331E+006     4.478E+004 Nb-94       702.65     99.81   1 .151E+005   1 . 1 5E+OOS   1 .274E+002    5.610E+004 8 71. 09   99.89   1 .491E+005                  7.672E+004     7.303E+004
 +      Ag-108m     433.90*    90.50   1 .026E+005   9.07E+004      2.093E+005     4.989E+004 614.30*    89.80   9.070E+004                   7.603E+004     4.377E+004 722.90     90.80   1.366E+005                   2.014E+004     6.666E+004 Cs-134      604.72     97.62   6.634E+005    6.63E+OOS     -1.200E+005     3.240E+005 795.86     85.46   7.428E+005                   5. 542E+005 v' 3.620E+005
 +      Cs-137      661.66*    85.10   1.612E+005    1. 61E+OOS     1.447E+006     7.870E+004
 +      Eu-152      121. 78*   28.67   1.064E+006    2.70E+005      8.281E+006     5.276E+005 344 . 28*  26.60   1.029E+006                   7.348E+006     5.085E+OOS 1408.01*    21. 07  2.700E+005                   9.960E+006     1 .243E+005
 +      Eu-154      123.07*    40 .40  8.747E+005    2.24E+005      6.807E+006     4.336E+005 723.30     20.06   9.125E+005                  -5.204E+005     4.453E+005 1274.43*    34.80   2.242E+005                   5.387E+005     1 .048E+005
 +      Eu-155        86.55*   30.70   1. 916E+006   1 .92E+006     2.449E+006     9.501E+005 105 .31    21.10   2.653E+006                  -1.833E+004     1.316E+OD6 Tl-208      583.19     85.00   1.448E+005    1 .45E+005     2.044E+004     7.076E+004 Bi-212      727.33       6.67  1.826E+006    1.83E+006      9.287E+005     8.909E+OOS
 +      Pb-212      238.63*    43.60   2.851E+005    2.85E+005      8.072E+005     1. 401E+O 05
 +      Bi-214      609.32*    45. 49  1.779E+005    1.78E+005      1.492E+005     8.588E+004 1120.29*    14.92   7.373E+005                   5.793E+006     3.577E+005 1764.49     15.30   2.221E+005                   1. 941E+005    9.854E+004 Pb-214      295.22     18.42   7.846E+005    5.96E+OOS      2.254E+005     3.861E+005 35 1 .93*  35.60   5.963E+005                   4.260E+006     2.948E+D05 Ra-226      186.21       3.64  5.124E+006    5.12E+006      1. 625E+006    2.534E+006 Ac-228      338.32     11.27   1. 246E+006   4.25E+005     -1. 537E+006    6.125E+005 911. 20    25.80   4.253E+005                   2.112E+005     2.066E+005 968.97     15.80   1 .133E+006                  5.295E+005     5.566E+005 Am-241        59.54    35.90   9.310E+005    9.31E+005     -2.609E+OOS     4 .608E+005
       +=Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1169]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002484.CNF Report Generated On 3/7/2018 6:14:26 AM Sample Title B101110AFSWC011GD Sample Description Ul CTMT Sample Identification 011 Sample Type GAMMA DIRECT sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels} 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"2 Sample Taken On 3/5/2018 9:45:00 PM Acquisition Started 3/5/2018 9:43:50 AM Live Time 600.0 seconds Real Time 601.7 seconds Dead Time 0. 29 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1170]

Peak Analysis Report 3/7/2018 6: 14 :26 AM Page 2

          • P E A K ANALYSIS REPORT *****

Detector Name: 5452 Sample

Title:

BlOlllOAFSWCOllGD Peak Analysis Performed on: 3/7/2018 6: 14 :26 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 153- 167 160.36 39. 70 0.99 1.53E+002 67.52 3.43E+002 2 285- 307 301 .16 74.94 1.12 7.27E+002 159.64 1.46E+003 3 456- 463 459.92 114.68 0.30 -2.74E+001 58.92 4.43E+002 4 481- 496 488. 12 121. 74 1. 09 3.78E+002 105.86 8.05E+002 5 993- 1002 996. 71 249. 04 0.28 5.61E+OOO 37.50 1.51E+002 6 1367- 1386 1376.85 344. 18 1. 39 2.87E+002 62.81 2.00E+002 7 2430- 2445 2435.83 609. 14 1. 55 5.92E+001 27.23 4.18E+001 8 2634- 2657 2645.08 661.48 1. 75 l .48E+003 84.95 8.12E+001 9 2938- 2950 2943.99 736.25 0.47 3.75E+OOO 18.06 2.93E+OD1 10 3104- 3125 3114.79 778.97 0.81 1 .44E+002 37.38 5.53E+001 11 3463- 3474 3468.00 867.30 0.91 3.32E+D01 17.26 1.48E+001 12 3843- 3879 3853.87 963.79 1. 55 1.50E+OD2 46.59 6.89E+OD1 13 4330- 4349 43 4 1 . 77 1085 . 79 0.76 9.43E+001 30.60 3.97E+001 14 4436- 4456 4445. 71 1111 .77 1. 70 1.46E+D02 34. 11 3.99E+001 15 4679- 4701 4690.48 1172.96 0.59 1.69E+OD2 31.39 2.00E+OOl 16 5090- 5101 5095.92 1274.31 0.53 1.81E+001 11.54 5.94E+OOO 17 5318- 5338 5327.07 1332. 08 0.93 1.69E+OD2 30.90 1 .87E+001 18 5617- 5640 5629.07 1407.56 1. 73 2.12E+OD2 33.69 1 .79E+OD1 19 5832- 5851 5841.13 1460.55 0.62 1 .21E+002 23.81 6.50E+OOO M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1171]

Interference Corrected Activity Report 3/7/2018 6: 14: 27 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

BlOlllOAFSWCOllGD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * * * * *
  • I II *
  • t
  • I a .. *
  • IDENTIFIED NUCLIDES . . . . . . . . . .. . . . .. ~ ... . . ..

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/MA2) Uncertainty K-40 1.000 1460.82* 10. 66 1. 49654E+ 006 3.22952E+005 Co-60 1.000 1173.23* 99.85 2.08706E+ 005 4 .22005E+004 1332.49* 99.98 2.16999E+ 005 4 .32424E+004 Cs-137 1 .000 661.66* 85. 10 1. 85452E+006 2.46696E+005 Eu-152 1 .000 121.78* 28.67 9.61477E+ 005 3.31127E+005 344.28* 2 6 .60 9.48749E+ 005 2.59513E+OD5 1408.01* 21. 07 1. 31526E+006 2.33912E+OD5 Eu- 154 0.683 123.07* 40.40 6.82288E+ 005 2.35256E+005 723.30 20.06 1274.43* 34.80 6.56307E+004 4 .22599E+OD4 Bi-212 0.881 727.33* 6.67 6.13752E+004 2.9569BE+OD5 Bi-214 0.689 609.32* 45.49 1.35187E+005 6.43069E+004 1120.29* 14.92 1.19042E+006 2.93885E+OD5 1764.49 15.30 

          *=Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                      10.000 keV Nuclide confidence index threshold=                            0.30 Errors quoted at 2.000 sigma

[1172]

Interference Corrected Activity Report 3/7/2018 6: 14 : 27 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1. 000 1 .496542E+006 3.229521E+005 Co-60 1.000 2 .127513E+Oo5 / 3.020188E+004 Cs-137 1. 000 1. 854524E+O 06 / 2.466957E+005 Eu-152 1. 000 1. 090592E+006 ../ 1.538396E+005 Eu-154 0 .683 6. 070269E+O 04 /' 4.171804E+004 Bi-212 0 .881 6.137516E+004 2.956977E+005 Bi-214 0 .689 1 .834040E+005 6.282055E+004 X Pb-214 0 .383 

      ? = Nuclide is part of an undetermined solution X ~ Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2. 000 sigma

[1173]

Interference Corrected Activity Report 3/7/2018 6: 14 :27 AM Page 5 

  **********    u N I D E N T I F I E D     p E A K     s  **********

Peak Locate Performed on: 3/7/2018 6: 14 :26 AM Peak Locate Frorn Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 39.70 2.5472E-001 44.18 2 74.94 l. 2110E+OOO 2 1. 97 3 114.68 -4.5721E-002 -214.78 Tol. Eu-155 s 249.04 9.3418E-003 669. 10 D-Esc. 10 778.97 2.3956E-0Dl 26.01 Sum 11 867.30 S.5295E-D02 52.04 Sum 12 963.79 2.5018E-001 3 1. 04 13 1085.79 1. 5725E-001 32.43 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2. 000 sigma [1174]

Nuclide MDA Report 3/7/2018 6:14:27 AM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B10ll10AFSWC011GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/M"2 ) (pCi/M"2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*   10 .66  2.217E+005    2.22E+005    1 .497E+006  9.402E+004
 +      Co-60      1173.23*   99.85   3.905E+004    3.86E+004    2.087E+005   1. 785E+004 1332.49*   99.98   3.860E+004                 2 .170E+005  1. 756E+004 Nb-94       702.65    99.81   5.347E+004    5.35E+004    5.036E+003   2.527E+004 871.09    99.89   6. 307E+004                2.186E+004   2.999E+004 Ag-108m     433.90    90.50   8.094E+004    6.65E+004    5.247E+003   3.906E+004 61 4 .30  89.80   7.734E+004                 3.655E+004   3.710E+004 722.90    90.80   6.648E+004                -l .409E+004  3.162E+004 Cs-134      604.72    97.62   6.731E+004    6.73E+004   -3.478E+004   3.222E+004 795.86    85.46   6.819E+004                 3.506E+004v' 3.234E+004
 +      Cs-137      661 .66*  85.10   7.680E+004    7.68E+004    1. 855E+O 06 3.671E+004
 +      Eu-152      121 .78*  28.67   4.191E+005    1. 89E+005   9.615E+005   2.061E+005 344.28*   26.60   2.962E+005                 9.487E+005   l.436E+005 1408.01*   21. 07  1. 894E+005                1. 315E+006  8.633E+004
 +      Eu-154      123.07*   40. 40  2.974E+005    5.65E+004    6.823E+005   1.462E+005 723.30    20.06   3.053E+005                 1. 888E+004  1.453E+005 1274.43*   34.80   5.645E+004                 6.563E+004   2.331E+004 Eu-155       86.55    30.70   5.692E+005    5.69E+005    5.428E+005   2.810E+005 105.31    21.10   6.690E+005                -9.923E+004   3.296E+005 Tl-208      583.19    85.00   8.436E+004    8.44E+004    6.615E+004   4.054E+004
 +      Bi-212      727.33*    6.67   5.193E+005    5. 1 9E+005  6.138E+004   2.375E+D05 Pb-212      238.63    43.60   2.250E+005    2.25E+005    4.184E+004   1 .101E+005
 +      Bi-214      609.32*   45.49   9.064E+004    9.06E+004    1.352E+005   4.223E+004 1120.29*   14.92   3.447E+005                 1.190E+006   1.613E+005 1764 .49   15.30   2.674E+005                 2.233E+005   1.211E+005 Pb-214      295.22    18.42   4.277E+005    2.21E+005    4 .248E+004  2.077E+005 351. 93*  35.60   2.213E+005                 7.089E+005   1.073E+005 Ra-226      186.21     3.64   2.916E+006    2.92E+006    2.840E+006   1.431E+006 Ac-228      338.32    11. 27  7.037E+005    2.27E+005    9.189E+004   3.413E+005 911.20    25.80   2.274E+005                -1. 457E+005  l.077E+005 968.97    15.80   5.147E+005                -1. 087E+005  2.473E+005 Am-241       59.54    35.90   5.045E+005    5.04E+005   -5.528E+004   2.477E+005
       +=Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       > - calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1175]

      • W*********************************************************************
          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002468.CNF Report Generated On 3/6/2018 5:35:15 AM Sample Title B101110AFSWC012GD Sample Description Ul CTMT Sample Identification 012 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO MA2 Sample Taken On 3/3/2018 8:45:00 AM Acquisition Started 3/3/2018 8:34:14 AM Live Time 600.0 seconds Real Time 602.1 seconds Dead Time 0.35 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 1 7 BCM [1176]

Peak Analysis Report 3/6/2018 5:35:15 AM Page 2

          • P E A K A N A L Y S I S REPORT *****

Detector Name: 5452 Sample

Title:

B101110AFSWC012GD Peak Analysis Performed on: 3/6/2018 5:35:15 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area Uncert. Counts 1 113- 136 129.30 31.92 1. 57 9.60E+002 85.84 2.37E+002 2 283- 309 3 01. 46 75.02 1. 09 9.37E+002 187.95 1.80E+003 3 332- 348 340.92 84.90 0 .43 1.22E+002 130.83 1.33E+003 4 952- 964 956.42 238.96 0 .67 4.74E+001 66.83 4.05E+002 5 2634- 2659 2647.11 661.99 1. 70 9.10E+003 196.95 1. 42E+O 02 6 4687- 4702 4694.23 1173.90 0 .52 8.32E+001 23.59 1. 88E+O 01 7 5324- 5341 5331. 25 1333.13 1. 36 9.04E+001 21. 33 7.61E+OD0 8 5835- 5854 5845.33 1461.60 1. 72 1.03E+002 24.83 1.45E+D01 M = First peak in a multiplet region m == Other peak in a multiplet region F "" Fitted singlet Errors quoted at 2 . 000 sigma [1177]

Interference Corrected Activity Report 3/6/2018 5:35:16 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSWC012GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * ., * * *
  • I " * * * * * .., " ~ +
  • IDENTIFIED NUCLIDES
  • ill ..... . . . . . . . . . .......... t Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M"2 ) uncertainty K-40 0 .999 1460.82* 10.66 1.27379E+006 3.27673E+OOS Co-60 0 .999 1173.23* 99.85 1.02730E+005 3.02791E+004 1332.49* 99.98 1.15902E+005 2.88744E+004 cs-137 1.000 661. 66* 85.10 1.13678E+007 l.38686E+006 Eu-155 0.332 86.55* 30.70 3.29839E+005 3.61197E+005 105.31 21.10 Pb-212 1.000 238.63* 43.60 8.53393E+004 l.21212E+OOS
           *=Energy line found in the spectrum.
           @=Energy line not used for Weighted Mean Activity Energy Tolerance :                      10.000 keV Nuclide confidence index threshold ~                         0 .3 0 Errors quoted at 2.000 sigma

[1178]

Interference Corrected Activity Report 3/6/20 18 5:35:16 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"'2 ) Uncertainty K-40 0.999 1.273793E+006 3.276732E+005 Co-60 0.999 1 . 096289E+oos ...~ 2.089626E+004 Cs-137 1. 000 1 .136783E+007v 1.386862E+006 Eu-155 0.332 3.298388E+005 3.611968E+005 Pb-212 1.000 8.533927E+004 1.212119E+OOS 

       ? = Nuclide is part of an undetermined solution X . Nuclide rejected by the interference analysis
       @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2.000 sigma
  * *********    U N I D E N T I F I E D            P E AK S         **********

Peak Locate Performed on: 3/6/2018 5:35: 15 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 92 1 .5993E+OOO 8.95 2 75.02 1 .5614E+OOO 2 0 .06 M = First peak i n a multiplet region m = Other peak i n a multiplet region F - Fitted singlet Errors quoted at 2 . 000 sigma [1179]

Nuclide MDA Report 3/6/2018 5:35: 16 AM Page 5

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B10ll10AFSWC012GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/M"'2 ) (pCi/M"'2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       1460.82*   10. 66  3.271E+005    3.27E+005       1. 274E+006    1.468E+005
 +      Co-60      1173 .23*  99.85   3.375E+004    2.38E+004       1. 027E+005    1.520E+004 1332.49*   99.98   2.384E+004                    1. 159E+005    1.018E+004 Nb-94       702.65    99.81   3.741E+004    3.74E+004       2.649E+004     1.724E+004 87 1 .09  99.89   4. 132E+004                  -l.200E+003     1.912E+004 Ag-108m     433.90    90.50   1.299E+005    4.60E+004      -1.978E+004     6.354E+004 614.30    89.80   8.535E+004                    2.243E+004     4 .111E+004 722.90    90.80   4.601E+004                   -2.937E+004     2.139E+004 Cs-134      604.72    97.62   7.227E+004    4 .09E+004     -4.512E+004     3.470E+004 795.86    85.46   4.088E+004        6,CC i\o / -2. 995E+004    1. 868E+004
 +      Cs-137      661.66*   85.10   1 .039E+005   1.04E+005       1. 137E+007    S.026E+004 Eu-152      121 .78   28.67   5.337E+005    1. 77E+005      5. 885E+Oos../ 2. 634E+005 344.28    26.60   3.971E+005                   -2.135E+004     1.941E+OOS 1408.01    21.07   1 .775E+005                   1. 494E+005    8.034E+004 Eu-154      123.07    40.40   3.741E+005    1. 0lE+OOS     -1. 528E+005    1.846E+005 723.30    20.06   2.066E+OOS                   -1. 255E+OOS    9.599E+004 1274 .43   34.80   1.009E+005                    1. 054E+005 ./ 4. 553E+004
 +      Eu-155       86.55*   30.70   5.832E+005    5.83E+005       3.298E+005     2.879E+005 105.31    21. 10  7.483E+005                   -3.675E+005     3.693E+005 Tl-208      583.19    85.00   8.138E+004    8.l4E+004       7.220E+004     3.905E+004 Bi-212      727.33     6.67   6.173E+005    6.17E+005       9.483E+004     2.866E+OOS
 +      Pb-212      238.63*   43.60   1 .987E+005   1.99E+005       8.534E+004     9.693E+004 Bi-214      609.32    45 .49  1. 602E+005   1 .6 0E+005     1.169E+005     7.703E+004 1120.29    14 .92  3.065E+005                    8.469E+004     1 .422E+OOS 1764.49    15.30   2.383E+005                    1.531E+005     1. 065E+005 Pb-214      295.22    18 .42  6.100E+005    3.02E+005       1.841E+005     2.989E+005 351.93    35.60   3.024E+OOS                    1.125E+OOS     1. 478E+005 Ra-226      186.21     3.64   3.599E+006    3.60E+006       1.157E+006     1.772E+006 Ac-228      338.32    11. 27  9.653E+005    1.61E+005      -4.024E+004     4. 722E+005 91 1. 20  25.80   1. 608E+005                  -2.691E+004     7.432E+004 968.97    15.80   2.643E+005                    1.388E+OOS     1.221E+005 Am-241       59.54    35.90   5.563E+005    5.56E+OOS      -6.996E+004     2.736E+OOS
       + = Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       > ~ Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ = Half-life too short to be able to perform the decay correction

[1180]

      • w*********************************************************************
          • GAMM A S P E C T R U M ANALYSIS *****

Filename: C:\GENIE2K\CAMFILES\00002474.CNF Report Generated On 3/6/2018 5:44:54 AM Sample Title B1011l0AFSCC013GD Sample Description Ul CTMT Sample Identification 013 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"2 Sample Taken On 3/3/2018 1:00:00 PM Acquisition Started 3/3/2018 12:54:24 PM Live Time 600 . 0 seconds Real Time 604.4 seconds Dead Time 0 . 73 % Energy Calibration used Done On 1/13/2015 Efficiency Calibration used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1181]

Peak Analysis Report 3/6/2018 5:44:54 AM Page 2

          • P E A K A N A L Y S I S REPORT *****

Detector Name: 5452 Sample

Title:

B101110AFSCC013GD Peak Analysis Performed on: 3/6/2018 5:44:54 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 2637- 2660 2648.09 662.23 2.56 4. 63E+002 53.42 6.27E+001 2 5833- 5859 5844.92 1 461.50 1. 81 1.38E+002 28.84 1 .61E+001 M ~ First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1182]

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Sample

Title:

B101110AFSCC013GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 0.999 1460.82* 10 .66 1 .71318E+006 3.87913E+005 Cs-137 0.999 661.66* 85. 10 5.78872E+005 9.63525E+004 

       *=Energy line found in the spectrum.
       @=Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold=           0.30 Errors quoted at 2.000 sigma

[1183]

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          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 0 .999 1.713179E+006 3.879131E+OOS Cs-137 0 .999 S. 78872 OE+OOS v* 9.635247E+004 

       ?  = Nuclide is part of an undetermined solution X   = Nuclide  rejected by the interference analysis
      @= Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2.000 sigma
  **********     U N I D E N T I F I E D         P E A K S      **********

Peak Locate Performed on: 3/6/2018 5:44:54 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide All peaks were identified. [1184]

Nuclide MDA Report 3/6/2018 5:44:54 AM Page 5

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSCC013GD Nuclide Library Us ed ; C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuc lide MDA Activity Dec . Level Name (keV) (%) (pCi/M"2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/M"2 ) 

 +      K-40       1460 . 82*  10 .66 3.756E+005     3.76E+005    1 .713E+006    1.710E+005 Co-60      1173.23     99.85  5.038E+004     4.93E+004    5.805E+004     2.352E+004 1332.49     99.98  4 .929E+004                 3. 095E+004 v  2 .291E+004 Nb-94       702.65     99.81  3.741E+004     3.74E+004   -1 .608E+004    1 .724E+004 87 1 .09   99.89  3.865E+004                  1 .111E+004    1 .778E+004 Ag-108m     433.90     90.50  5.127E+004     4.38E+004    2.309E+004     2.423E+004 614.30     89.80  5. 8 18E+004                3.260E+004     2.752E+004 722.90     90.80  4 .378E+004                -1 .735E+004    2.027E+004 Cs-134      604.72     97.62  5.182E+004     5.05E+004   -4.588E+004     2.447E+004 795.86     85.46  5.046E+004                  5.517E+004~    2.347E+004
 +      Cs-137      66 1 .66*  85.10  6.840E+004     6.84E+004    5.789E+005     3.251E+004 Eu-152      12 1 .78   28.67  4 .1SOE+005    2. 22E+O 05  1. 442E+O 05 v 2. 040E+OOS 344.28     26.60  2.219E+005                  1.937E+005     1.065E+005 1408.01     21. 07 2.308E+005                  1.457E+005     1.070E+005 Eu-154      123.07     40.40  2.905E+005     1.13E+005   -6.794E+004     1.428E+005 723.30     20.06  1.982E+OOS                 -1.127E+005     9.176E+004 1274.43     34.80  1.127E+005                  1.125E+004 ~   5.142E+004 Eu-155       86.55     30.70  5.129E+005     5.13E+005    8.031E+005     2.529E+005 105 .31    21.10  6.046E+005                 -1.669E+005     2.974E+005 Tl-208      583.19     85.00  5.260E+004     S.26E+004    3.093E+004     2.467E+004 Bi-212      727.33      6.67  6.020E+005     6. 02E+005   5.312E+005     2.789E+005 Pb-212      238.63     43.60  1.842E+005     1 .8 4E+OOS  1.637E+005     8.967E+004 Bi-214      609.32     45.49  1.212E+005     1.21E+005    1.359E+005     5.750E+004 1120.29     14.92  3.308E+005                  7.065E+004     1.543E+005 1764.49     15.30  2.635E+005                  2.804E+005     1.191E+005 Pb-214      295.22     18.42  3.271E+005     1.64E+005    2.517E+005     1.574E+005 351. 93    35.60  1.640E+005                  8.249E+004     7.863E+004 Ra-226      186.21      3.64  2.399E+006     2.40E+006   -l.676E+005     l.172E+006 Ac-228      338.32     11 .27 4.731E+005     1.69E+005   -3.669E+005     2.260E+005 911.20     25.80  1.693E+005                  3.086E+004     7.857E+004 968.97     15.80  3.112E+005                  3.194E+OOS     l.455E+OOS Am-241       59.54     35.90  4.452E+005     4.4SE+005    l.45 8 E+OOS   2.180E+005
       +=Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       > ~ Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1185]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002460.CNF Report Generated On 3/5/2018 5:28:59 PM Sample Title B101110AFSWC014GD Sample Description Ul CTMT Sample Identification 014 sample Type GAMMA DIRECT Sample Geometry 3M90D ECP 17.8CM Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 2.830E+001 M"2 Sample Taken On 3/2/2018 2:35 :00 PM Acquisition Started 3/2/2018 3: 01 :10 PM Live Time 600. 0 seconds Real Time 612.6 seconds Dead Time 2 . 06 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done on 1/30/2018 Efficiency ID 3M90D ECP 17 8CM [1186]

Peak Analysis Report 3/5/2018 5:28:59 PM Page 2

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Detector Name: 5452 Sample

Title:

B101110AFSWC014GD Peak Analysis Performed on: 3/5/2018 5: 28: 59 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area Uncert. Counts 1 113- 123 116.24 28.65 1.16 7.03E+002 115. 61 9.07E+002 2 153- 167 160.55 39.74 1.45 6.66E+003 267.99 3.92E+003 3 176- 189 182.36 45 .20 1. 37 l.93E+003 204.24 3.09E+003 4 284- 309 301.18 74.95 1.16 7.40E+003 522.96 1 .43E+004 5 332- 358 340.29 84.74 1. 32 2.92E+003 557.57 1 .71E+004 6 479- 496 488.15 121.75 1. 27 1.23E+004 401. 29 8.60E+003 7 972- 989 979.64 244.77 1. 21 2.33E+003 228.13 3.27E+003 8 1179- 1191 1184.32 295.99 0 .63 2.07E+002 126.58 1.44E+003 9 1367- 1387 1377.51 344.34 1. 44 8.51E+003 248.77 1.92E+003 10 1467- 1478 14 71. 33 367.82 0.99 1.96E+002 99.35 8.96E+002 11 1633- 1655 1644.64 411.19 1. 16 7.09E+002 158. 15 1. 43E+003 12 1766- 1785 1776. 00 444 .06 1. 45 9.20E+002 144.28 1.22E+003 13 2037- 2049 2042.43 510.72 0.48 6.21E+001 88.10 7.12E+002 14 2249- 2261 2254.78 563.84 0.59 1.07E+002 84.30 6.31E+OD2 15 2340- 2355 2344.27 586.23 0.38 1.37E+002 94.85 6.99E+002 16 2618- 2656 2646.09 661.73 1.32 1.20E+003 203.87 l.56E+003 17 2703- 2721 2713.99 678.72 0.85 5.59E+001 105.50 8.07E+OD2 18 2747- 2763 2754.47 688.84 1. 02 2.47E+002 96.48 6.64E+002 19 2885- 2901 2892.44 723.35 0.67 1.73E+002 93.85 6.46E+002 20 3054- 3071 3059.03 765.02 0.72 -l.79E+001 96.52 7.19E+002 21 3102- 3125 3114.95 779. 01 1. 61 3.20E+003 165.54 9.12E+OD2 22 3233- 3259 3253.05 813.55 0.74 1.02E+002 126.06 8.84E+002 23 3457- 3502 3469.09 867.57 1. 70 1.13E+OD3 217. 52 l.55E+003 24 3842- 3869 3855.64 964.24 1. 74 3.71E+003 164.57 6.82E+D02 25 4007- 4031 4018.81 1005.04 1.64 3.89E+002 96.34 4 .67E+D02 26 4271- 4285 4276.42 1069.45 0.86 4.58E+001 56.59 2.60E+002 27 4328- 4368 4342.74 1086.03 1. 82 3.05E+D03 172.36 7.20E+002 28 4433- 4461 4447.82 1112.30 1. 79 3.43E+D03 154.73 5.54E+D02 29 4678- 4706 4692.59 1173.49 1.83 2.54E+003 138.03 4 .82E+002 30 4840- 4861 4850.98 1213.08 1. 56 3.13E+002 69.91 2.42E+D02 31 5085- 5109 5097.70 1274.75 1. 86 3.75E+D02 62.29 1.44E+002 32 5183- 5209 5196.39 1299.42 1. 80 4 .21E+002 58.54 1.00E+OD2 33 5314- 5344 5329.86 1332.78 1 .99 2.74E+003 113.34 9.66E+D01 34 5616- 5647 5632.19 1408.34 2.00 5.31E+003 155.62 1.50E+002 35 5821- 5854 5830.99 1458.02 1. 20 2.28E+OD2 38.87 2.BBE+OOl 36 6103- 6118 6111.07 1528.00 0 .60 4 .21E+OD1 18.35 1.39E+D01 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1187]

Interference Corrected Activity Report 3/5/2018 5:28:59 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC014GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . ........ ... .... ..... .. IDENTIFIED NUCLIDES             * * * * * * * * * * * * * * * * *
  • I*

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pci/MA2 ) Uncertainty K-40 0.987 1460.82* 10.66 2.80891E+006 5.37003E+005 Co-60 1.000 1173.23* 99 . 85 3 . 12417E+006 3.02234E+005 1332.49* 99.98 3.48413E+006 3.13754E+005 Cs-137 1.000 661.66* 85. 10 1.51143E+006 3.13774E+005 Eu-152 1.000 121.78* 28.67 3.18705E+007 6.46724E+006 344.28* 26.60 2.84354E+007 4.74691E+006 1408.01* 21. 07 3.26479E+007 2.78170E+006 Eu-154 0.999 123.07* 40.40 2.26170E+007 4.60523E+006 723.30* 20.06 9.38706E+005 5.21779E+005 1274.43* 34.80 1.35368E+006 2.50619E+005 Eu-155 0.330 86.55* 30.70 8.19754E+006 2.26611E+006 105.31 21.10 Tl-208 0.985 583.19* 85.00 1.66876E+005 l.17171E+005 Pb-212 0. 941 238.63* 43.60 4.30229E+006 8.12713E+005 Pb-214 0. 941 295.22* 18.42 9.54774E+005 6.03828E+005 351.93* 35.60 2.12466E+007 3.45674E+006 

        *=Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :            10.000 keV Nuclide confidence index threshold=                   0.30 Errors quoted at 2.000 sigma

[1188]

Interference Corrected Activity Report 3/5/20 18 5:28:59 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 0.987 2.808913E+006 5.370032E+005 Co-60 1 .000 3. 29741BE+006 ..I 2.176703E+005 Cs-137 1 .000 1. 511426E+006 v*-* 3.137740E+OD5 Eu-152 1 .000 3 .108287E+007,.,~ 2.244418E+006 Eu-154 0.999 1. 274639E+006 v 2.248497E+OOS Eu-155 0.330 8.197544E+006 2.266106E+006 Tl-208 0.985 1.668757E+OOS 1 .17 1715E+OD5 X Bi-212 0.975 Pb-212 0.941 4 .302291E+006 8.127127E+005 Pb-214 0.941 8.678837E+005 5.968739E+005 

       ?  :, Nuclide is part of an undetermined so lution X   ;- Nuclide rejected by the interference analysis
      @   = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2. 000 sigma

[1189]

Interference Corrected Activity Report 3/5/2018 5: 28: 59 PM Page 5 

  **********     U N I D E N T I F I E D       P E A K S    **********

Peak Locate Performed on: 3/5/2018 5: 28: 59 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) counts per Second  % Uncertainty Type Nuclide 1 28.65 1.1714E+OOO 16.45 2 39.74 1.1104E+001 4.02 3 45.20 3.2120E+OOO 10.60 4 74.95 1. 233 7E+001 7.07 10 367.82 3.2676E-001 50.68 Sum 11 411. 19 1.1811E+OOO 22.32 Sum 12 444.06 1. 533 6E+OOO 15.68 D-Esc. 13 510.72 1. 0357E-001 141.78 14 563.84 1. 7916E-001 78.42 17 678.72 9.3170E-002 188.73 Sum 18 688.84 4. 1184E-001 39.04 Sum 20 765.02 -2.9853E-002 -538.87 S-Esc. 21 779. 01 5.3353E+OOO 5.17 Sum 22 813.55 1. 7060E-001 123.15 S-Esc. 23 867.57 1. 8834E+OO 0 19.25 Tol. Nb- 94 24 964.24 6.1835E+OOO 4.44 Sum 25 1005.04 6.4897E-001 24.74 Sum 26 1069.45 7.6348E-002 123.54 Sum 27 1086.03 5.0791E+OOO 5.66 28 1112.30 5.7104E+OOO 4.52 Tol. Bi-214 30 1213.08 5.2136E-001 22.35 32 1299.42 7.0164E-001 13.91 Sum 36 1528.00 7.0223E-002 43.55 Sum M = First peak in a multiplet region m ~ Other peak in a multiplet region F ~ Fitted singlet Errors quoted at 2 . 000 sigma [1190]

~uclide MDA Report 3/5/2018 5: 28: 59 PM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: 3M90D- ECP- 17.8CM Sample

Title:

B101l10AFSWC0l4GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/M"'2 ) 

 +      K-40       1460.82*   10.66   5.284E+005    5.28E+005    2.809E+006   2.475E+005
 +      Co-60      1173.23*   99.85   1 .944E+005   9.41E+004    3.124E+006   9.553E+004 1332.49*   99.98   9.412E+004                 3.484E+006   4.534E+004 Nb-94       702.65    99.81   2.140E+005    2 .14E+005  -2.713E+005   1.055E+005 871.09    99.89   2.790E+005                 1.644E+004   1.380E+005 Ag-108m     433.90    90.50   2.397E+005    2.40E+005   -6.016E+004   1.184E+005 614.30    89.80   2.444E+005                 1.831E+005   1.206E+005 722.90    90.80   2.507E+005                 2.747E+005   1.237E+005 Cs-134      60 4 .72  97.62   2.157E+005    2. 1 6E+005 -3.581E+005   1.064E+005 795.86    85.46   2.420E+005                 1.015E+004 ~ 1.193E+OOS
 +      Cs-137      661.66*   85 .10  3.993E+005    3.99E+005    1.511E+006   1.980E+OOS
 +      Eu-152      121.78*   28.67   1. 435E+006   5.70E+005    3.187E+007   7.142E+005 344.28*   26.60   9.263E+005                 2.844E+007   4.586E+005 1408.01*   21. 07  5.695E+005                 3.265E+007   2.764E+005
 +      Eu-154      123.07*   40.40   1.019E+006    2.99E+005    2.262E+007   S.068E+005 723.30*   20.06   8.205E+005                 9.387E+005   4.029E+005 1274.43*   34.80   2.994E+005                 1.354E+006   1.448E+005
 +      Eu-155       86.55*   30.70   2.532E+006    2.21E+006    8.198E+006   1.262E+006 105.31    21.10   2.207E+006                 7.549E+004   1.099E+006
 +      Tl-208      583.19*   85.00   1. 873E+005   1.87E+005    1.669E+005   9.201E+004 Bi-212      727.33*    6.67   2.467E+006    2.47E+006    2.823E+006   1.212E+006
 +      Pb-212      238.63*   43.60   6.318E+005    6.32E+005    4.302E+006   3.134E+005 Bi-214      609.32    45.49   4.710E+005    2.79E+005    5.328E+005   2.324E+005 1120.29    14.92   1.181E+006                -5.028E+004   5.796E+005 1764.49    15.30   2.794E+005                 2.486E+OOS   1.272E+005
 +      Pb-214      295.22*   18.42   9.483E+005    6.92E+OOS    9.548E+005   4.679E+005 351.93*   35.60   6.921E+005                 2.125E+007   3.427E+005 Ra-226      186.21     3.64   8.573E+006    8.57E+006    5.997E+006   4.259E+006 Ac-228      338.32    11. 27  2.270E+006    7.94E+005   -l .792E+006  1.125E+006 911.20    25.80   7.939E+005                -7.677E+005   3.909E+005 968.97    15.80   2.380E+006                 4.380E+005   1.180E+006 Am-241       59.54    35.90   1.570E+006    1 .57E+006   1 .340E+006  7.803E+005
       + ; Nuclide identified during the nuclide identification
       * ~ Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ = Half-life too short to be able to perform the decay correction

[1191]

          • GAMM A S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002461.CNF Report Generated On 3/5/2018 5: 45: 14 PM Sample Title B101110AFSWC015GD Sample Description Ul CTMT Sample Identification 015 Sample Type GAMMA DIRECT Sample Geometry 3M90D ECP 17.8CM Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 2.830E+001 M... 2 Sample Taken On 3/2/2018 3:35: 00 PM Acquisition Started 3/2/2018 3:23: 18 PM Live Time 600.0 seconds Real Time 609.3 seconds Dead Time 1. 52 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 1/30/2018 Efficiency ID 3M90D ECP 17 8CM [1192]

Peak Analysis Report 3/5/2018 5:45 :14 PM Page 2

          • P E A K A N A L Y S I S REPORT *****

Detector Name: 5452 Sample

Title:

B101110AFSWC015GD Peak Analysis Performed on: 3/5/2018 5: 45: 1 4 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 135 128.74 31.78 1. 58 1 .85E+003 173.60 l.42E+003 2 153- 168 160.68 39.78 1. 30 2.55E+003 205 .04 2.65E+003 3 177- 190 182.57 45.26 1. 05 7.29E+002 162.17 2.12E+003 4 284- 309 301.26 74.97 1.15 5.73E+003 444.43 1.03E+004 5 332- 358 340.28 84.74 1. 53 2.46E+003 468.10 1. 19E+004 6 479- 496 488.22 121.77 1.18 5.87E+003 321.50 6.14E+003 7 970- 987 979.69 244.78 1. 29 1 .1SE+003 190. 64 2.44E+OD3 8 1370- 1387 1377.46 344.33 1. 34 4.09E+003 178.72 1 .19E+D03 9 1634- 1653 1644.96 411.27 1. 81 4.42E+002 126.08 1.01E+003 10 1694- 1703 1698.41 424.64 0.46 -2.44E+001 66.56 S.01E+002 11 1766- 1784 1775.95 444.04 1. 19 4.80E+002 119. 42 9.14E+002 12 2249- 2261 2253.62 563.55 0.57 3.90E+001 72.23 4 .76E+002 13 2633- 2658 2646.13 661.74 1. 57 7.15E+003 202.26 7.25E+002 14 2705- 2724 2714.17 678.76 1.19 1.60E+002 85.70 4.78E+002 15 2885- 2901 2893.55 723.63 0.89 9.96E+001 81.78 5.02E+002 16 3102- 3127 3115.07 779.04 1. 78 1.66E+003 129.39 5.95E+OD2 17 3461- 3481 3468.90 867.53 1. 62 5.27E+002 94.90 4.71E+OD2 18 3841- 3869 3855.50 964.20 1. 68 1 .83E+003 131. 43 5.3BE+002 19 4005- 4032 4019.20 1005.13 1. 68 2.92E+002 83.97 3.26E+002 20 4328- 4368 4342.68 1086.01 1. 79 1. 63E+003 139.24 5.07E+002 21 4433- 4460 4447.70 1112.27 1. 96 1. 83E+003 116.52 3.47E+002 22 4678- 4706 4692.49 1173.46 1. 86 2.31E+003 123.27 3.23E+002 23 4841- 4865 4851. 34 1213.17 1. 19 2.06E+002 56.78 1. 45E+002 24 5087- 5108 5097.93 1274.81 1. 58 2.11E+002 49.33 1.D6E+002 25 5186- 5206 5197.24 1299.63 1. 54 2.24E+002 44.95 7.77E+OD1 26 5314- 5343 5329.88 1332.78 1. 80 2.41E+003 107.77 1.D3E+002 27 5616- 5646 5632. 00 1408 .29 2.01 2.90E+003 114.93 8.15E+001 28 5823- 5852 5843.96 1461 .26 1. 70 1.85E+002 32.02 1. 50E+001 29 6106- 6119 6112.72 1528 .41 0.64 1.83 E+001 10.84 3*. 66E+O 00 M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1193]

Interference Corrected Activity Report 3/5/2018 5: 45: 14 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC015GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * .. * * * *
  • l e I f * * * * * * * *
  • IDENTIFIED NUCLIDES . . . . .. " ...... .. . .. . .

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M ... 2 ) Uncertainty K-40 1 .000 1460.82* 10.66 2.27902E+006 4.41314E+005 Co-60 1 .000 11 73.23* 99.85 2.84913E+006 2.73833E+005 1332.49* 99.98 3.06064E+006 2.80556E+005 Cs-137 1 .000 661.66* 85.10 8.97358E+006 1.10710E+006 Eu-152 1 .000 121.78* 28.67 1.52449E+007 3.16512E+006 344.28* 26.60 1.36534E+007 2.32214E+006 1408.01* 21.07 1.78527E+007 l .59358E+006 Eu-154 0.999 123. 07* 40. 40 l.08186E+007 2.25349E+006 723.30* 20.06 5.41319E+005 4.49089E+005 1274.43* 34.80 7.61446E+005 1.88619E+OOS Eu-155 0.330 . 86.55* 30.70 6.88924E+006 1.90350E+006 105.31 21. 10 Pb-212 0 .941 238.63* 43.60 2.12163E+006 4.91070E+005 

           *=Energy line found in the spectrum.
           @=Energy line not used for Weighted Mean Activity Energy Tolerance :                     10.000 keV Nuclide confidence index threshold =                         0.30 Errors quoted at 2. 000 sigma

[1194]

Interference Corrected Activity Report 3/5/2018 5: 45: 14 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1.000 2.279018E+006 4.413138E+005 Co-60 1.000 2.952318E+006./ 1 .959629E+005 X Ag-108m 0.430 Cs-137 1.000 8. 973579E+006 .I' 1 .107100E+006 Eu-152 1.000 1 .613769E+007 Y"' 1 .205404E+006 Eu-154 0.999 7.204558E+005 V 1 .730954E+005 Eu-155 0.330 6.889239E+006 1 .903501E+006 X Bi-212 0.978 Pb-212 0.941 2.121635E+006 4.910699E+005 X Pb-214 0.386 

      ? =  Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @  = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2. 000 sigma

[1195]

Interference Corrected Activity Report 3/5/20 18 5: 45: 14 PM Page 5 

  **********      UN I D E N T I F I E D       P E A K S     **********

Peak Locate Performed on: 3/5/2018 5: 45: 14 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 78 3.0775E+OOO 9.40 2 39.78 4.2522E+OOO 8.04 3 45.26 1 .2150E+OOO 22.25 4 74.97 9.5570E+OOO 7.75 9 411. 27 7.3668E-001 28.52 10 424.64 -4.0744E-002 -272.25 Sum 11 444.04 8.0018E-001 24.87 D-Esc . 12 563.55 6.4943E-002 185.37 14 678.76 2.6673E-001 53.55 Sum 16 779. 04 2.7586E+OOO 7.82 Sum 17 867.53 8.7837E-001 18.01 Tol. Nb-94 18 964.20 3.0547E+OOO 7.17 Sum 19 1005. 13 4.8657E-001 28.76 Sum 20 1086.01 2.7235E+OOO 8.52 21 1112.27 3.0575E+OOO 6.35 Tol. Bi-2 1 4 23 1213.17 3.4349E-001 27.55 25 1299.63 3.7381E-001 20.04 Sum 29 1528.41 3.0 568E-002 59 .11 Sum M ,,, First peak in a multiplet region m == Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1196]

N-.1clide MDA Report 3/5/2018 5: 45: 14 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 3M90D ECP 17.8CM Sample

Title:

B10l110AFSWC015GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) (%) (pCi/MA2 ) (pCi/M"2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +       K-40       1460.82*    10.66   3.756E+OOS     3.76E+005   2.279E+006   1 . 711E+005
 +       Co-60      1173.23*    99.85   l.594E+OOS     9.65E+004   2.849E+006   7.803E+004 1332.49*    99.98   9.651E+004                 3.061E+006   4.653E+004 Nb-94       702.65     99.81   1.760E+005     1.76E+005   6.123E+004   8.655E+004 87 1. 09   99.89   2.214E+OOS                 7.098E+005   1.091E+005 Ag-108m     433.90*    90.50   1.184E+005     1.18E+005  -2.553E+004   5.779E+004 614.30     89.80   2.078E+005                 5.610E+003   1.023E+005 722.90*    90.80   1.600E+OOS                 1.196E+005   7.836E+004 Cs-134      604.72     97.62   1.880E+OOS     1.88E+005   1.774E+OOS / 9.254E+004 795.86     85.46   2.036E+005                -6.282E+004   1.001E+005
 +       Cs-137      66 1 .66*  85. 10  2.326E+005     2.33E+005   8.974E+006   1.146E+005
 +       Eu-152      121 .78*   28.67   1.214E+006     4 .21E+005  1 .524E+007  6.033E+005 344.28*    26.60   6.955E+005                 1 .365E+OD7  3.432E+005 1408.01*    21.07   4 .212E+005                1 .785E+007  2.023E+005
 +       Eu-154      123.07*    40 .40  8.612E+OOS     2.46E+005   1 .082E+007  4.281E+005 723.30*    20.06   7.241E+005                 5.413E+005   3.547E+005 1274 .43*   34.80   2.464E+005                 7.614E+005   1 .183E+005
 +       Eu-155       86.55*    30.70   2.119E+006     1.87E+006   6.889E+006   1 .056E+006 105.31     21.10   1. 875E+006                5.288E+005   9.323E+005 Tl-208      583.19     85.00   2.226E+005     2.23E+005   2.066E+OD5   1 .097E+005 Bi-212      727.33*      6.67  2.178E+006     2.18E+006   1.628E+006   1 .067E+006
 +       Pb-212      238.63*    43.60   5.453E+005     5.45E+005   2.122E+006   2.702E+005 Bi-214      609.32     45.49   3.967E+005     2.36E+005   1.680E+004   1 .952E+005 1120.29     14.92   1.011E+006                -1.324E+005   4.944E+005 1764.49     15.30   2.357E+005                 2.21BE+005   1 .053E+005 Pb-214      295.22     18.42   1.213E+006     S.20E+005  -2.090E+005   6.005E+005 351.93*    35.60   5.197E+005                 1.020E+007   2.565E+OD5 Ra-226      186.21       3.64  7.414E+006     7.41E+006  -1.252E+006   3.679E+006 Ac-228      338.32     11.27   1. 911E+006    6.54E+005  -6.417E+006   9.451E+OOS 911.20     25.80   6.545E+005                -2.470E+005   3.212E+005 968.97     15.80   1. 774E+O 06               1.327E+004   8.768E+005 Am-241       59.54     35.90   1. 345E+006    l .34E+006 -8.910E+005   6.67BE+005
        + - Nuclide identified during the nuclide identification
        * = Energy line found in the spectrum
        >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
        @ - Half-life too short to be able to perform the decay correction

[1197]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002456.CNF Report Generated On 3/5/2018 5: 05: 16 PM Sample Title B101110AFSWC016GD Sample Description Ul CTMT Sample Identification 016 Sample Type GAMMA DIRECT Sample Geometry 3M90D ECP 17.8CM Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 2.830E+001 MA2 Sample Taken On 3/2/2018 1:19:00 PM Acquisition Started 3/2/2018 1 :58:50 PM Live Time 600 . 0 seconds Real Time 610.0 seconds Dead Time 1 . 64 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 1/30/2018 Efficiency ID 3M90D ECP 1 7 8CM Dlt le. vl( l,clc. ff J 

                                                          .--i., I c;, I, ~   , , ,r
                                                         &~11ll~

5c,f::'-= o3;~Q~ [1198]

Peak Analysis Report 3/5/2018 5:05:16 PM Page 2

          • PE AK A N A L Y S I S REPORT *****

Detector Name: 5452 Sample

Title:

B101110AFSWC016GD Peak Analysis Performed on: 3/5/2018 5: 05:16 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 124 117.27 28.91 1. 65 6.97E+002 107.06 7.32E+002 2 153- 168 160.63 39.76 1.45 4.56E+003 239.85 3.27E+003 3 177- 189 182.15 45.15 1. 26 1 .38E+003 174.25 2.36E+003 4 284- 309 301.19 74.95 1. 26 6.57E+003 487 .14 1.24E+004 5 332- 346 340.52 84.80 1.23 1.51E+003 323.19 8.52E+003 6 480- 496 488.25 121.78 1.20 8.60E+003 341.65 6.58E+003 7 969- 987 979.65 244.77 1.21 1. 78E+003 204.37 2.57E+003 8 1367- 1387 1377.50 344.34 1. 42 6.08E+003 211.48 1.41E+003 9 1464 - 1480 1471.40 367.84 1. 33 2.28E+002 116.14 1.00E+003 10 1638- 1653 1644.57 411.17 1. 10 4.31E+002 109.76 8.52E+002 11 1768 - 1784 1776.10 444.08 1. 55 6.16E+002 109.28 7.57E+002 12 2639- 2653 2645.88 661.68 1. 29 3.17E+002 86.96 5.46E+002 13 2745- 2762 2755.13 689. 01 1. 52 1 .36E+002 89.33 5.69E+002 14 2886- 2902 2892.40 723.34 0.83 l.56E+002 87.03 5.54E+002 15 3104- 3127 3115.08 779.04 1. 65 2.25E+003 145.99 7.72E+002 16 3455- 3478 3469. 04 867.56 1. 73 8.53E+002 115.32 6.17E+002 17 3842- 3868 3855.68 964.25 1. 86 2.70E+003 144.81 5.81E+002 18 3976- 3995 3984.82 996.54 0. 45 1. 03E+002 69.42 3.14E+002 19 4011- 4027 4020.06 1005.35 1. 88 1. 81E+002 69.20 3.24E+002 20 4330- 4368 4342.93 1086.07 1. 80 2.23E+003 158.82 6.8SE+002 21 4433- 4460 4447.89 1112.31 1. 83 2.61E+003 134.21 4.21E+002 22 4678- 4703 4692.72 1173.52 1. 81 1.89E+003 118.42 3.77E+002 23 4840- 4864 4852.02 1213.34 1. 87 2.67E+002 63.67 1.81E+002 24 5086- 5108 5098.19 1274.87 1.62 2.39E+002 56. 36 1.43E+002 25 5185- 5208 5196.48 1299.44 1.99 2.68E+002 53.18 1. 10E+002 26 5315- 5343 5330.16 1332.85 1. 88 2.04E+003 104.85 1.53E+002 27 5616- 5646 5632.18 1408.33 2. 14 4.13E+003 136.42 1.06E+002 28 5822- 5853 5830.41 1457.87 1. 34 2.29E+002 36.29 2.00E+OOl 29 6106- 6120 6113.09 1528.51 1. 70 5.05E+001 17.01 7.SlE+OOO M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2.000 sigma [1199]

Interference Correcte d Activity Report 3/5/2018 5:05:16 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

Bl01110AFSWC016GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * * * *
  • I
  • I * * * ,. II: * * *
  • IDENTIFIED NUCLIDES * .. I * * '" t * * * * * * * *
  • I 4
  • r Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M"2 ) Uncertainty K-40 0.986 1460.82* 10.66 2.81849E+006 S.09307E+005 Co-60 1. 000 1173.23* 99.85 2.32308E+006 2.36205E+OD5 1332.49* 99.98 2.59320E+006 2.46572E+005 Cs-137 1 .000 661. 66* 85.10 3.97789E+OOS 1 .19165E+OOS Eu-152 1 .000 121. 78* 28.67 2.23301E+OD7 4.55918E+006 344.28* 26.60 2.03298E+007 3.41526E+006 1408.01* 21. 07 2.54182E+007 2.19978E+006 Eu-154 0.999 123.07* 40.40 l.58467E+007 3.24640E+006 723.30* 20.06 8.49061E+OOS 4.83377E+OOS 1274.43* 34.80 8.61130E+OOS 2.15281E+005 Eu-155 0.330 86.55* 30.70 4.2361SE+006 1.24052E+006 1 05.31 21 .10 Pb-212 0 .941 238.63* 43.60 3.29097E+006 6.51877E+005
          *=Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                       10.000 keV Nuclide confidence index threshold ~                           0.30 Errors quoted at 2.000 sigma

[1200]

Interference Corrected Activity Report 3/5/2018 5: 05: 16 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 0.986 2.818494E+006 5.093072E+005 Co-60 1.000 2. 4 52345E+006 ../ 1.705693E+005 Cs-137 1.000 3.977887E+005./ l.191647E+005 Eu-152 1.000 2.348804E+007"' l.702600E+006 Eu-154 0.999 8. 529611E+005 -/' 1.959396E+005 Eu-155 0.330 4.236149E+006 1.240517E+006 X Bi-212 0.975 Pb-212 0.9 41 3.290965E+006 6.518766E+005 X Pb-214 0.386 

      ?  = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
         = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2. 000 sigma

[1201]

Interference corrected Activity Report 3/5/20 18 5:05 : 16 PM Page 5 

  **********    UN I D E N T I    F I E D    P E A K S      **********

Peak Locate Performed on: 3/5/2018 5:05 :16 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 28.91 1.1617E+OOO 15.36 2 39.76 7.5925E+OOO 5.27 3 45.15 2.2919E+OOO 12.67 4 74.95 1.0956E+001 7.41 9 367.84 3.8046E-001 S O. BB Sum 10 411.17 7.1781E-001 25.48 11 444.08 1 .0264E+OOO 17.75 D-Esc. 13 689. 01 2.2681E-001 65.64 Sum 15 779.04 3.7438E+OOO 6.50 Sum 16 867.56 1.4210E+OOO 13.53 Tol. Nb-94 17 964.25 4.5043E+OOO 5.36 Sum 18 996.54 1. 7156E-001 67.44 Sum 19 1005.35 3.0087E-001 38.33 Sum 20 1086.07 3.7200E+OOO 7.12 21 1112.31 4.3439E+OOO 5.15 23 1213.34 4.4419E-001 23.89 25 1299.44 4.4670E-001 19.84 Sum 29 1528.51 8.4152E-002 33.70 Sum M "' First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1202]

Nuclide MDA Report 3/5/2018 5:05:16 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 3M90D ECP 1 7. 8CM Sample

Title:

B101110AFSWC016GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/M"2 ) (pCi/M"2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       146 0 .82*  10. 66  4.387E+005     4.39E+OOS   2.818E+006   2.027E+005
 +      Co-60      1173.23*    99.85   1.663E+005     1.15E+OOS   2.323E+006   8.148E+004 1332.49*    99.98   1.147E+005                 2.593E+006   5.564E+004 Nb-94       702.65     99. 81  1.920E+005     1.92E+005   8.284E+004   9.454E+004 871.09     99.89   2.494E+005                 1.152E+005   1. 232E+005 Ag-108m     433.90     90.50   2.109E+005     2.11E+005   6.415E+004   1. 040E+005 614.30     89.80   2.200E+005                -5.694E+004   1. 084E+005 722.90     90.80   2.317E+005                 3.928E+005   1. 142E+005 Cs-134      604.72     97.62   1.969E+005     1.97E+OOS   1.213E+005 v 9.701E+004 795.86     85.46   2.199E+005                -5.973E+003   1. 082E+005
 +      Cs-137      661.66*    85.10   1. 6 72E+005   1 .67E+005  3.978E+005   8.192E+004
 +      Eu-152      121.78*    28.67   1. 232E+006    4.78E+OOS   2.233E+007   6.124E+005 344 .28*   26.60   7.939E+005                 2.033E+007   3.925E+005 1408 .01*   21.07   4.782E+005                 2.542E+007   2.308E+005
 +      Eu-154      123.07*    40 .40  8.742E+005     2.90E+OOS   1.585E+007   4. 346E+005 723.30*    20.06   7.603E+005                 8.491E+005   3.728E+005 1274.43*    34.80   2.896E+005                 8.611E+005   1.399E+005
 +      Eu-155       86.55*    30.70   l. 454E+006    1.45E+006   4 .236E+006  7 .234E+005 105.31     21.10   1.995E+006                -9.678E+005   9.925E+005 Tl-208      583.19     85.00   2.310E+005     2.31E+005   2.396E+005   1.138E+005 Bi-212      727.33*      6.67  2.287E+006     2.29E+006   2.554E+006   1.121E+006
 +       Pb-212     238.63*    43.60   5.694E+005     5.69E+OOS   3.291E+006   2.822E+005 Bi-214      609.32     45.49   4.233E+005     2.07E+OOS   4.159E+004   2.085E+005 1120.29     14.92   1.071E+006                -4.429E+005   5.247E+005 1764.49     15. 30  2.074E+005                 1.664E+005   9.122E+004 Pb-214     295.22     18.42   1. 242E+006    5.93E+005   2.125E+005   6.150E+005 35 1 .93*  35.60   5.932E+005                 1.519E+007   2.932E+005 Ra-226     186.21       3.64  7.626E+006     7.63E+006  -6.647E+006   3.785E+006 Ac-228      338.32     11. 27  1.950E+006     6.97E+005   5.482E+004   9.643E+OOS 911.20     25.80   6.968E+005                -3.0l7E+005   3.424E+OOS 968.97     15.80   2.065E+006                -1 .331E+005  1.023E+006 Am-241       59.54     35.90   1. 436E+006    1 .44E+006 -4.471E+005   7.133E+005
       + ~ Nuclide identified during the nuclide identification
  • Energy line found in the spectrum
       > : Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ -  Half-life too short to be able to perform the decay correction

[1203]

      • k*********************************************************************
          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002466. CNF Report Generated On 3/6/2018 5:29: 44 AM Sample Title B101110AFSWC017GD Sample Description Ul CTMT Sample Identification 017 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 2.830E+001 MA2 Sample Taken On 3/3/2018 7 :55: 00 AM Acquisition Started 3/3/2018 7:47:47 AM Live Time 600.0 seconds Real Time 607.5 seconds Dead Time 1. 24 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration used Done On 1/30/2018 Efficiency ID 3M90D ECP 17 8CM Q& {&. V hcf~ i-eJ 0. f~t!j;cLla_ so F = e:" 'l&:>6~:-'t,~ o.. 'I t<e ~~ [1204]

Peak Analysis Report 3/6/2018 5:29:44 AM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC017GD Peak Analysis Performed on: 3/6/2018 5:29:44 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 119 1 16 .13 28.62 0.36 2.10E+002 66.28 3.42E+002 2 153- 167 160.39 39.70 1.57 2.06E+003 186.33 2.30E+003 3 176- 189 182 . 12 45.14 1.19 6.74E+002 152.72 1.87E+003 4 286- 309 3 01. 27 74.97 1. 12 3.94E+003 384.54 8.25E+003 5 332- 346 340.63 84.82 1. 20 8.71E+002 269.07 5.98E+003 6 481- 497 488.46 121.83 1. 14 4. 73E+003 280.70 4.78E+003 7 972- 988 979.89 244.83 1. 34 8.60E+002 161. 94 1. 81E+003 8 1367- 1388 1378.24 344.52 1.27 3.37E+003 173.57 1. 11E+003 9 1464- 1480 1472.30 368.06 0.97 1. 31E+002 98.52 7.32E+002 10 1634- 1651 1645.57 411.42 1. 54 2.45E+002 10 0. 62 7.02E+002 11 1765- 1785 1776.39 444 .15 1. 50 3.63E+002 111.24 7.52E+002 12 2635- 2658 26 47 .28 662.03 1.48 1. 12E+003 122.94 6.63E+002 13 2747- 2761 2755. 15 689.02 0.51 5.08E+001 68.98 3.95E+002 14 2784- 2795 2788.40 697.33 0.38 3.31E+001 52 .39 2.60E+002 15 2885- 2905 2892.70 723.42 0.61 4.50E+001 88.09 5.22E+002 16 3105- 3127 3116.03 779.28 1. 77 1.39E+003 117.31 5.30E+002 17 3362- 3374 3367.40 842.15 0.36 2.76E+001 53.53 2.61E+002 18 3456- 3482 34 70 .14 867.84 1. 63 4.27E+002 103.64 5.16E+002 19 3843- 3869 3857.20 964.63 1. 73 1. 70E+003 119.40 4.25E+002 20 3979- 3992 3985.02 996.59 0.68 5.34E+001 48. 82 l.97E+002 21 4009- 4029 4020.65 1005.50 0.76 1.43E+002 69 .26 2.91E+002 22 4330- 4369 4344.32 1086.42 1. 87 1.33E+003 130.58 4.89E+002 23 4435- 4463 4449.57 1112.73 1. 83 1. 57E+003 112.57 3.47E+002 24 4680- 4708 4694.41 1173.94 1. 70 2.19E+003 113.58 2.25E+002 25 4846- 4863 4853.07 1213.60 0.87 1 .52E+002 48.84 l.36E+002 26 5090- 5110 5099.29 1275.15 1.39 1 . 89E+002 41. 85 6.90E+001 27 5187- 5208 5198.11 1299.85 1. 09 1 .66E+002 43.23 8.00E+OOl 28 5318- 5346 5331.99 1333.31 2.10 2.04E+003 101. 55 1.19E+002 29 5619- 5648 5634.38 1408.88 2.05 2.52E+003 108.81 9.27E+001 30 5825- 5854 5845.72 1461.70 0.95 1 .74E+002 27.86 4.00E+OOO 31 6107- 6120 6113.99 1528.73 1. 02 1 .09E+001 14.18 l. 41E+001 M First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1205]

Interference Corrected Activity Report 3/6/2018 5:29:44 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC017GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB t

  • e ***** II * * *
  • I I * * ** IDENTIFIED NUCLIDES * * , I * * * * * * * * * * * * * ~ *
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/MA2 ) Uncertainty K-40 0.999 1460.82* 10 .66 2.14373E+006 3.90517E+005 Co-60 0.999 11 73.23* 99.85 2.70007E+006 2.57324E+OOS 1332.49* 99.98 2.59477E+006 2.44443E+OOS Nb-94 0.969 702.65* 99.81 3.58262E+004 S.69137E+004 871.09* 99.89 4.85910E+OOS 1 .28098E+005 Cs-137 1. 000 661.66* 85.10 l.41236E+006 2.29307E+005 Eu-152 1. 000 121.78* 28.67 1.22635E+007 2.56180E+006 344.28* 26.60 1. 12494E+O 07 1.93779E+006 14 08.01* 21.07 1. 55041E+007 1.40942E+006 Eu-154 0.999 1 23.07* 40.40 8.70285E+006 1.82387E+006 723.30* 20.06 2.44841E+005 4.79765E+OOS 1274.43* 34.80 6.82087E+005 1. 61058E+005 Eu-155 0 .331 86.55* 30.70 2.44246E+006 8.98553E+005 105.31 21.10 Pb-212 0 .940 238.63* 43.60 l.58598E+006 3.93547E+OOS
         *=Energy line found in the spectrum.
         @=Energy line not used for Weighted Mean Activity Energy Tolerance :               10.000 keV Nuclide confidence index threshold=                    0. 30 Errors quoted at 2. 000 sigma

[1206]

Interference Corrected Activity Report 3/6/20 18 5:29 :44 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 0.999 2.14372BE+006 3.90516BE+OOS Co-60 0.999 2. 644 722E+O 06 v"' 1 .772263E+OOS Nb-94 0.969 1. 100258E+OOS S.201120E+004 Cs-137 1.000 1. 4123 56E+006 ,,/ 2.293070E+OOS Eu-152 1.000 1. 355948E+007 1.034328E+006 Eu-154 0.999 6.271252E+OOS 1.518703E+OOS Eu-155 0.331 2.442463E+006 8.985526E+005 X Bi-212 0.976 Pb-212 0.940 1.585977E+006 3.935474E+OOS X Pb-214 0.389 

      ?  ;: Nuclide is part of an undetermined so lution X  "' Nuclide rejected by the interference analysis
      @  = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at    2. 000 sigma

[1207]

Inberference Corrected Activity Report 3/6/2018 5:29:44 AM Page 5 

  **********      UN I D E N T I F I E D       P E AK S     **********

Peak Locate Performed on: 3/6/2018 5:29:44 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol . No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 28.62 3.4944E-001 31.61 2 39. 70 3.4256E+OOO 9.07 3 45.14 1.1226E+OOO 22.67 4 74.97 6.5738E+OOO 9.75 9 368.06 2.1764E-001 75.45 Sum 10 411. 42 4 .0813E-001 41.09 11 444.15 6.0572E-001 30.61 D-Esc. 13 689.02 8.4608E-002 135.88 Sum 16 779.28 2.3099E+OOO 8.46 Sum 17 842.15 4.6005E-002 193.94 Sum 19 964.63 2.8398E+OOO 7.01 Sum 20 996.59 8.8973E-002 91.45 Sum 21 1005.50 2.3773E-001 48.56 Sum 22 1086.42 2.2200E+OOO 9.80 23 1112.73 2.6144E+OOO 7.18 Sum 25 1213.60 2.5300E-001 32.17 Sum 27 1299.85 2.7666E-001 26.04 Sum 31 1528.73 1. 8233E-002 129.65 Sum M  ; First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1208]

Nuclide MDA Report 3/6/2018 5:29:44 AM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSWC017GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) (%) (pCi/M"2 ) (pCi/M"2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*     10. 66  2.151E+005    2.15E+005     2.144E+006   9.086E+004
 +      Co-60      1173.23*     99.85  1.335E+005     1. 0 0E+OOS   2.700E+006   6.506E+004 1332.49*     99.98  1.003E+OOS                  2.595E+006    4 .845E+004
 +      Nb-94        702.65*    99.81  9.402E+004     9.40E+004     3.583E+004   4.555E+004 87 1 .09*  99.89  1.811E+005                  4.859E+005    8.902E+004 Ag-108m      433.90     90.50  1. 878E+OOS    1.88E+005    1. 102E+005   9.249E+004 614.30     89.80  1 .930E+005                -8.147E+004    9.494E+004 722.90     90.80  1 .926E+005                 6.320E+004    9.466E+004 Cs-134       604.72     97.62  1 . 682E+OOS   1 .68E+005  -3.670E+004    8.263E+004 795.86     85.46  1.952E+005                  2. 787E+004 v 9. 583E+004
 +      Cs-137       661.66*    85.10  2.162E+005     2.16E+005    1 .412E+006   1.064E+005
 +      Eu-152       121.78*    28.67  1.052E+006     4.41E+005    1 .226E+007   5.223E+005 344.28*    26.60   7.187E+005                 1.125E+007    3.548E+005 1408.01*     21. 07 4.410E+005                  1. 550E+007   2.122E+005
 +      Eu-154       123.07*    40 .40  7.463E+005    1. 97E+005   8.703E+006    3.707E+005 723.30*    20.06   7.933E+OOS                 2.448E+005    3.893E+005 1274.43*     34.80  1.972E+005                  6.821E+005    9.369E+004
 +      Eu-155        86.55*    30.70  1.218E+006     1. 22E+006   2.442E+006    6.052E+005 105.31     21.10  1.700E+006                  1.104E+006    8.450E+005 Tl-208       583.19     85.00  1.993E+005     1.99E+005   -5.406E+004    9.799E+004 Bi-212       727.33*     6.67  2.386E+006     2.39E+006    7.364E+005    1.171E+006
 +      Pb-212       238.63*    43.60  4 .628E+005    4.63E+005    1. 586E+006   2.289E+005 Bi-214       609.32     45.49  3.694E+OOS     2.40E+005    1. 322E+005   l.816E+005 1120.29      14.92  9.962E+005                 -1.850E+005    4.871E+005 1764.49      15. 30 2.400E+005                  2.310E+005    1 .075E+005 Pb-214       295.22     18.42  1.066E+006     5.37E+005    1.983E+004    5.267E+005 351.93*    35.60  5.370E+005                  B.405E+006    2.651E+005 Ra-226       186.21      3.64  6.629E+006     6.63E+006    8.312E+005    3.287E+006 Ac-228       338.32     11. 27 1.712E+006     6.46E+005   -1. 477E+005   8.452E+005 911. 20    25.80  6.456E+005                  2.965E+005    3.168E+005 968.97     15.80  1.710E+006                 -1.075E+005    8.452E+005 Am-241        59.54     35.90  1.234E+006     1.23E+006    2.200E+005    6.123E+005
       + = Nuclide identified during the nuclide i dentification
       * = Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1209]

  • *** GAMM A S P E C T R U M ANALYSIS *****

Filename: C:\GENIE2K\CAMFILES\00002458.CNF Report Generated On 3/5/2018 5:34: 01 PM Sample Title B101110AFSWC018GD Sample Description Ul CTMT Sample Identification 018 Sample Type GAMMA DIRECT Sample Geometry 3M90D ECP 17.8 CM Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 2.830E+001 MA2 Sample Taken On 3/2/2018 2:35: 00 PM Acquisition Started 3/2/2018 2:25: 50 PM Live Time 600.0 seconds Real Time 613.9 seconds Dead Time 2.27 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 1/30/2018 Efficiency ID 3M90D ECP 1 7 BCM [1210]

Peak Analysis Report 3/5/2018 5:34:01 PM Page 2

          • PE AK A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B1 01110AFSWC018GD Peak Analysis Performed on: 3/5/2018 5:34: 01 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area Uncert. Counts 1 113- 124 117.25 28.90 1.29 8.68E+002 127.56 1. 06E+003 2 153- 168 160.68 39.78 1. 39 7.11E+003 286.40 4.46E+003 3 176- 189 182.45 45.22 1.18 2.08E+003 212.92 3.36E+003 4 284- 309 301.07 74.92 1.19 7.98E+003 543.03 l.55E+004 5 332- 359 340.56 84.81 1. 34 3.72E+003 589.30 1. 84E+D04 6 481- 496 488.24 121.77 1. 27 1.35E+004 392.76 8.34E+003 7 873- 883 877.94 219.32 0 .71 1 .30E+001 155.95 2.54E+003 8 970- 988 979. 74 244.79 1. 30 3.18E+003 247.44 3.59E+003 9 1367- 1387 1377.51 344.34 1.40 9.99E+003 265.43 2.10E+003 10 1466- 1481 1471.63 367.89 1. 05 3.19E+002 132.93 1. 36E+003 11 1639- 1655 1644 . 69 411. 20 1. 09 7.18E+002 137.28 1. 26E+003 12 1767- 1784 1775.57 443.95 1.45 9.63E+002 142.38 1. 26E+O 03 13 1943- 1965 1955. 16 488.88 0 .55 1.42E+002 146.62 1 .35E+003 14 2250- 2261 2255.91 564.13 0 .71 5.67E+001 87.66 7.43E+002 15 2637- 2656 2646.26 661.78 1. 64 6.56E+002 123.16 8.93E+002 16 2704- 2723 27 13 .69 678.64 0.67 5.16E+001 119.79 1.01E+003 17 2745- 2762 2753.71 688.65 0.45 2.19E+002 110. 24 8.66E+D02 18 2885- 2900 2892.93 723.48 1. 08 l.99E+D02 101.50 7.91E+002 19 2955- 2967 2961.97 740 .75 0. 65 -1. 13E+001 78.49 5.86E+002 20 3102- 3127 3115.06 779.04 1. 67 3.76E+003 184.62 1 .12E+003 21 3456- 3478 3469.26 867.62 1. 78 1. 16E+003 137.22 9.14E+002 22 3670- 3686 3677.25 919.63 1. 05 9.56E+001 86.06 5.60E+002 23 3842- 3868 3855.82 964.28 1. 74 4.36E+003 175.86 7.71E+002 24 4011- 4030 4018 .86 1005.05 1.29 3.62E+002 94.05 5.23E+002 25 4329- 4369 4343.09 1086.12 1. 84 3.44E+003 196.21 9.89E+002 26 4433- 4461 4447.89 1112.32 1. 87 3.94E+003 170 .92 7.27E+002 27 4634- 4646 464 0 .60 1160.49 0.49 3.23E+001 48.67 2.13E+002 28 4678- 4706 4692.61 1173.49 1. 74 3.01E+003 151.41 5.89E+002 29 4839- 4863 4851.80 1213.29 1. 90 4 .21E+002 76.09 2.49E+002 30 4963- 4976 4968.64 1242.49 0. 46 l.86E+001 34.71 1.02E+002 31 5082- 5111 5097.38 1274.67 1. 32 4 . 10E+002 70.09 1. 72E+002 32 5185- 5209 5196.71 1299.50 1. 91 4 .77E+002 60.84 1.09E+002 33 5315- 5344 5329.98 1332.81 2.08 3.24E+003 120.27 8.09E+001 34 5617- 5647 5632.21 1408.34 1. 88 6.12E+003 163.42 1.18E+002 35 5818- 5855 5830. 44 1457.88 1. 57 3.10E+002 36.63 4. 50E+OOO 36 6105- 6122 6113.48 1528.60 0 .95 7.22 E+001 21.66 1.38E+001 M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1211]

Interference Corrected Activity Report 3/5/2018 5:34: 01 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

Bl01110AFSWC018GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * * *
  • I * * "' * * * * * * * *
  • IDENTIFIED NUCLIDES .. .. ......... . .. ......

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 0.986 1460.82* 10.66 3.82178E+006 5.59802E+005 Co-60 1. 000 1173.23* 99.85 3.70538E+006 3.50167E+OOS 1332.49* 99.98 4.11279E+006 3.62793E+005 Cs- 137 1.000 661.66* 85.10 8.23299E+005 1.83535E+005 Eu-152 1 .000 121.78* 28.67 3.51203E+007 7.10715E+006 344.28* 26.60 3.33896E+007 5.55903E+006 1408.01* 21.07 3.76494E+007 3.17526E+006 Eu-154 0.999 123.07* 40.40 2.49232E+007 5.06098E+006 723.30* 20.06 1. 08214E+006 5.66007E+005 1274.43* 34.80 1.47833E+006 2.80422E+OD5 Eu-155 0.331 86.55* 30.70 1.04369E+007 2.66203E+006 105.31 21.10 Pb-212 0 .941 238.63* 43.60 5.86960E+006 1.05273E+006 Ac-228 0. 925 338.32* 11. 27 7.88078E+007 1 .30551E+007 911.20* 25.80 4.28486E+OOS 3.87363E+OOS 968.97* 15.80 3.22742E+007 3.14086E+006 

          * ~ Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                     10.000 keV Nuclide confidence index threshold =                         0.30 Errors quoted at 2.000 sigma

[1212]

Interference Corrected Activity Report 3/5/2018 5:34:01 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 0.986 3.821781E+006 5.598022E+OOS Co-60 1.000 3. 901872E+006 v 2.519508E+OOS Cs-137 1.000 8. 232993E+OOS .,/ 1. 8353SOE+OOS Eu-152 1.000 3. 602536E+007 "* 2.556108E+006 Eu-154 0.999 1. 395647E+006 i/ 2.501363E+005 Eu-155 0.331 1.043686E+007 2.662027E+006 X Bi-212 0.977 Pb-212 0.941 5.869598E+006 1 .052731E+006 X Pb-214 0. 386 Ac-228 0. 925 9.826629E+OOS 3.835780E+OOS 

      ?

X = 

         - Nuclide is part of an undetermined solution Nuclide rejected by the interference analysis
      @ =  Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1213]

Interference Corrected Activity Report 3/5/2018 5: 34: 01 PM Page 5 

  **********    U N I D E N T I F I E D        P E A K S       **********

Peak Locate Performed on: 3/5/2018 5:34: 01 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . (kev) Counts per Second  % Uncertainty Type Nuclide 1 28.90 1 .4465E+OOO 14.70 2 39.78 l .1848E+001 4.03 3 45.22 3.4728E+OOO 1 0.22 4 74.92 1.3304E+001 6.80 7 219.32 2.1742E-002 1195.45 10 367.89 5.3174E-001 41. 66 Sum 11 411.20 1.1968E+OOO 19. 12 12 443.95 1.6047E+OOO 14 .79 D-Esc . 13 488.88 2.3584E-001 103 . 62 Sum 14 564.13 9.4432E-002 154 . 71 16 678.64 8.5928E-002 232.34 17 688.65 3.6442E-001 5 0 .42 Sum 19 740.75 -1 .8867E-002 -693.36 Sum 20 779.04 6.2640E+OOO 4.91 Sum 21 867.62 1. 94 08E+O 00 11 .78 Tol. Nb- 94 24 1005.05 6.0280E-001 26.00 Sum 25 1086.12 5.7385E+OOO 5.70 Sum 26 1112.32 6.5691E+OOO 4.34 Tol. Bi-214 27 1160.49 5.3906E-002 15 0 .49 Sum 29 1213.29 7.0232E-001 18.06 Sum 30 1242.49 3.0961E-002 186.87 32 1299.50 7.9560E-001 12.75 Sum 36 1528.60 1. 2031E-001 3 0 . 00 Sum M - First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1214]

Nuclide MDA Report 3/5/2018 5:34:02 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 3M90D ECP 17.8CM Sample

Title:

B101110AFSWC018GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10.66   2.353E+005    2.35E+005          3.822E+OD6    1.010E+005
 +      Co-60      1173.23*    99.85   2.146E+005    8.49E+004          3.705E+006    1. 056E+O 05 1332.49*    99.98   8.493E+004                       4. 113E+006   4 .075E+004 Nb-94       702.65     99.81   2.319E+005    2.32E+005 -1.731E+005            l.145E+005 87 1 .09   99.89   2.981E+005                       1. 734E+004   l. 475E+005 Ag-lOBm     433.90     90.50   2.543E+005    2.54E+005 5.098E+004             1 .257E+OD5 614.30     89.80   2.657E+005                       2.204E+OOS    1.313E+OD5 722.90     90.80  2.762E+005                        4.425E+OOS    1.365E+D05 Cs-134      604.72     97.62  2.303E+005     2.30E+OOS -3.463E+003            1.137E+005 795.86     85.46  2.653E+D05         O,to ~-t-1> /- 5. 481E+004   1.309E+005
 +      Cs-137      661.66*    85.10  2.347E+D05     2.3SE+005 8.233E+005             1.157E+005
 +      Eu-152      121.78*    28.67   1. 358E+006   4 .94E+005 3.512E+007            6.75SE+005 34 4 .28*  26.60   9.687E+005                       3.339E+OD7    4.799E+005 1408.01*    21. 07 4 .938E+005                       3.76SE+007    2.386E+005
 +      Eu-154      123.07*    40. 40  9.637E+005    3.SOE+OOS 2.492E+007             4.794E+005 723.30*    20.06   8.867E+005                       1. 0 82E+O 06 4.360E+005 1274.43*    34.80  3.495E+005                        1. 4 78E+006  1.699E+005
 +      Eu-155       86.55*    30.70  2.666E+006     2.29E+006 1 .044E+007            1.329E+006 105.31     21.10  2.295E+006                        1 .138E+006   1.142E+006 Tl-208      583.19     85.00  2.833E+005     2.83E+005 9.752E+004             1.40DE+005 Bi-212      727.33*     6.67  2.667E+006     2.67E+D06 3.255E+D06             1. 311E+006
 +      Pb-212      238.63*    43.60  6.729E+005     6.73E+OOS 5.870E+006             3.340E+D05 Bi-214      609.32     45.49  4.968E+005     2.57E+OOS 9.463E+004             2.453E+005 1120.29     14.92  1.257E+006                      -2.882E+OD4     6.177E+005 1764.49     15.30  2.566E+D05                        2.680E+005    1.158E+005 Pb-214      295.22     18.42  1.488E+006     7.24E+005 l.055E+005             7.376E+005 351.93*    35.60  7.238E+005                        2.495E+007    3.585E+005 Ra-226      186.21      3.64  8.971E+006     8.97E+006 -2.465E+006            4.458E+006
 +      Ac-228      338.32*    11. 27 2.286E+006     6.30E+005 7.881E+007             1.133E+006 911. 2 O*  25.80  6.299E+005                       4.285E+005     3.089E+005 968.97*    15.80  1.435E+006                        3.227E+007    7.077E+005 Am-241       59.54     35.90  1.579E+OD6     1 .58E+006 -1.479E+OD5           7.849E+005
       +=Nuclide identified during the nuclide i dentification
       *=Energy line found in the spectrum
       > ; Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1215]

          • GAMMA S P E C T R U M ANALYSIS *****

Filename: C:\GENIE2K\CAMFILES\00002467.CNF Report Generated On 3/6/2018 5:32: 13 AM Sample Title B101110AFSWC019GD Sample Description Ul CTMT Sample Identification 019 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 2.830E+001 M"2 Sample Taken On 3/3/2018 8:15: 00 AM Acquisition Started 3/3/2018 8:07:14 AM Live Time 600.0 seconds Real Time 606.9 seconds Dead Time 1.13 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 1/30/2018 Efficiency ID 3M90D ECP 17 8CM [1216]

Peak Analysis Report 3/6/2018 5:32 : 13 AM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B1 0l110AFSWC019GD Peak Analysis Performed on: 3/6/2018 5:32:13 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 120 116.69 28.76 0.84 2.19E+002 66.05 3.30E+002 2 153- 167 160.59 39.75 1. 33 2.04E+003 176.03 1 .98E+003 3 177- 189 182.32 45.19 0.92 5.42E+002 139.95 1 .65E+003 4 284- 309 301.38 75.00 1. 31 3.85E+003 395.16 8.28E+003 5 332 - 346 3 40. 73 84.85 1. 20 8.17E+002 263.13 5.72E+003 6 482 - 497 488.62 121.87 1.19 4. 25E+003 258. 24 4.12E+003 7 548- 555 551.50 137.61 0.45 6.47E+OOO 115.61 1. 65E+003 8 972 - 989 979.98 244.85 1. 21 9.23E+002 158.95 1. 65E+003 9 1368 - 1388 1378. 10 344.49 1. 37 2.95E+003 164.16 1. 05E+003 10 1637- 1652 1645.02 411.28 0.89 1.76E+002 88.66 5.95E+002 11 1769- 1787 1777.09 444.33 1. 54 3.66E+002 100.95 6.45E+002 12 2351- 2360 2355.53 589.05 0.34 1.94E+001 49. 48 2.59E+002 13 2636- 2659 2647.14 662.00 1. 55 l.40E+003 122.40 5.84E+002 14 3103- 3127 3116.17 779.31 1. 64 1.25E+003 114.65 4 .94E+002 15 3426- 3440 3433.36 858.64 0.73 5.62E+001 52.09 2.15E+002 16 3458- 3480 3470.01 867 .81 1. 65 3.74E+002 89.46 4.20E+002 17 3843- 3868 3857.01 964.58 1. 61 1.42E+003 113.14 4.15E+002 18 4007- 4028 4019.70 1005.26 1. 18 1.71E+002 65.67 2.42E+002 19 4332- 4371 4344.58 1086.49 1. 83 1.16E+003 123.97 4.44E+002 20 4435- 4462 4449.36 1112.68 1. 59 1.34E+003 106.19 3.29E+002 21 4563- 4574 4568.20 1142.39 0.53 1.00E+OOl 30.29 8.70E+001 22 4679- 4706 4694.27 1173.91 1. 86 1.67E+003 102 .14 2.07E+002 23 4842- 4863 4852.24 1213.40 1. 52 1.52E+002 48 .61 l. 17E+002 24 5088- 5108 5099.45 1275.19 1. 21 1.96E+002 42.96 7.34E+001 25 5186- 5208 5198.12 1299.85 0.90 1.73E+002 40 . 88 6.33E+001 26 5317- 5346 53 31. 95 1333.30 1. 79 1.78E+003 93 .05 8.15E+001 27 5618- 5648 5634.18 1408.83 2.09 2.33E+003 105.89 9.68E+001 28 5825- 5855 5831.71 1458.20 0.92 1.63E+002 28.40 7.78E+OOO 29 6109- 6122 6115.22 1529.04 0.73 2.52E+001 11.43 2.BOE+OOO M : First peak in a multiplet region m : Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1217]

Interference Corrected Activity Report 3/6/2018 5:32:13 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC019GD Nuclide Library used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . . ........ . ......... IDENTIFIED NUCLIDES              * **** ******** iii- ..... '
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/M ... 2 ) Uncertainty K-40 0 .989 1460.82* 10 .66 2.00917E+006 3.90711E+OOS Co-60 0 .999 1173.23* 99.85 2.05970E+006 2.07283E+005 1332.49* 99.98 2.26318E+006 2.16265E+OOS Cs-137 1. 000 661.66* 85. 10 1.75869E+006 2.61165E+OOS Eu-152 1. 000 121. 78* 28.67 1.10176E+007 2.30602E+006 344.28* 26.60 9.86342E+006 1.71144E+006 1408.01* 21.07 1.43223E+007 1.31801E+006 Eu-154 0.682 123.07* 40.40 7.81864E+006 1.64174E+006 723.30 20.06 1274.43* 34.80 7.06203E+005 1.65489E+005 Eu-155 0 .331 86.55* 30.70 2.29029E+006 8.68025E+005 105.31 21.10 Tl-208 0.947 583.19* 85.00 2.36446E+004 6.03679E+004 Pb-212 0.940 238.63* 43.60 1. 70118E+006 4.01890E+005
        *=Energy line found in the spectrum.
        @=Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuclide confidence index threshold=            0.30 Errors quoted at 2.000 sigma

[1218]

Interference corrected Activity Report 3/6/2018 5:32: 13 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 0.989 2.009168E+006 3.907109E+OOS Co-60 0.999 2.157126E+006 ..t 1.496460E+005 Cs-137 1.000 1. 758695E+006v 2.611650E+OOS Eu-152 1.000 1. 218067E+007 v 9.446987E+OOS Eu-154 0.682 6. 907434E+005 ./ 1 .643448E+OOS Eu-155 0.331 2.290285E+006 8.680250E+005 Tl-208 0.9 47 2.364462E+004 6.036794E+004 Pb-212 0.9 40 1.701184E+006 4.018896E+005 X Pb-214 0.388 

       ?  = Nuclide is part of an undetermined solution X   =o Nuclide rejected by the interference analysis
      @   =  Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2.000 sigma

[1219]

Interference Corrected Activity Report 3/6/2018 5:32:13 AM Page 5 

  **********       U N I D E N T I F I E D      P E A K S     **********

Peak Locate Performed on: 3/6/2018 5:32:13 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak To l. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 28.76 3.6560E-001 30.11 2 39.75 3.4015E+OOO 8.62 3 45.19 9.0378E-001 25.81 4 75. 00 6.4087E+OOO 10.28 7 137. 61 1 .0788E-002 1786.10 10 411. 28 2.9350E-001 50.35 11 444.33 6.0984E-001 27.59 D-Esc. 14 779.31 2.0802E+OOO 9.19 Sum 15 858.64 9.3702E-002 92.66 16 867.81 6.2402E-001 23.89 Tol. Nb-94 17 964.58 2.3695E+OOO 7.96 Tol. Ac-228 18 1005.26 2.8518E-001 38.38 Sum 19 1086.49 1.9344E+OOO 10.68 20 1112.68 2.2357E+OOO 7.92 Tol. Bi-21 4 21 1142.39 1. 6667E-002 302.88 23 1213.40 2.5361E-001 31 .95 25 1299.85 2.8792E-001 23.67 Sum 29 1529.04 4.1994E-002 45.34 Sum M = First peak in a multiplet region m  ::: Other peak in a multiplet region F  ; Fitted singlet Errors quoted at 2 . 000 sigma [1220]

Nuclide MDA Report 3/6/2018 5:32:13 AM Page 6

          • N U C L I D E MDA REPORT *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSWC019GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/M"2 ) 

 +      K-40       1460.82*    10 .66  2.843E+005     2.84E+005     2.009E+006    1.255E+005
 +      Co-60      1173.23*    99.85   1 .272E+005    8.54E+004     2.060E+006    6.194E+004 1332.49*    99.98   8.541E+004                   2.263E+006    4.099E+004 Nb- 94      702.65     99. 81  1 .533E+005    1 .53E+OOS   -1.311E+005    7.520E+004 87 1 .09   99.89   1 .947E+OOS                  1.631E+OOS    9.581E+004 Ag- 108m    433.90     90.50   1.802E+OOS     1 .80E+005   -2.415E+005    8.870E+004 614.30     89.80   1.823E+OOS                   8.483E+004    8.955E+004 722.90     90.80   1. 877E+005                  1.787E+OOS    9.224E+004 Cs-134      604.72     97.62   1.632E+005     1.63E+005    -4.415E+004    8.016E+004 795.86     85.46   1. 834E+O 05                 1.611E+005v"' 8.993E+004
 +      Cs-137      66 1. 66*  85. 10 2.034E+005      2.03E+005     1 .759E+006   1.000E+OOS
 +      Eu- 152     12 1. 78*  28.67   9.586E+005     4.58E+005     l .102E+007   4 .758E+005 344.28*    26.60   6.855E+005                   9.863E+006    3.383E+005 1408.01*    21. 07 4.577E+005                    1 .432E+007   2.205E+005
 +      Eu-154      123.07*    40.40   6.803E+005     2. 0 3E+005   7.819E+006    3.376E+005 723.30     20.06   8.537E+005                   1.177E+006    4.195E+005 1274.43*    34.80  2.034E+OOS                    7.062E+005    9.680E+004
 +      Eu-155       86.55*    30.70   1.192E+006     1.19E+006     2.290E+006    5.920E+005 105.31     21.10   1.621E+006                  -6.855E+005    8.057E+00 5
 +      Tl-208      583.19*    85.00   1.009E+005     1. OlE+OOS    2.364E+004    4.881E+004 Bi-212      727.33      6.67  2.559E+006      2.56E+006     4 .742E+006   1. 257E+006
 +      Pb-212      238.63*    43.60  4 .505E+005     4 . 5 1E+005  1.701E+006    2.228E+005 Bi-214      609.32     45.49  3.546E+005      2.27E+OOS    -6.595E+004    1.742E+005 1120.29     14.92   9.663E+005                   2.222E+005    4.721E+005 1764.49     15.30  2.267E+005                    2.033E+005    1.00BE+OOS Pb-214      295.22     18.42   1.025E+006     5. 12E+005    9.635E+005    5.064E+005 351. 93*   35.60   5.122E+005                   7.370E+006    2.527E+005 Ra-226      186.21      3.64   6.257E+006     6.26E+006     9.673E+005    3.101E+006 Ac-228      338.32     11. 27  1. 627E+006    5.97E+005    -8.454E+005    8.031E+005 91 1. 20   25.80   5.974E+OOS                   4.498E+005    2.926E+005 968.97     15.80   1.604E+006                   2.715E+005    7.919E+005 Am-241       59. 54    35.90   1.201E+006     1.20E+006    -5.503E+OOS    5.958E+005
       + ~ Nuclide identified during the nuclide i dentification
       * : Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ ~ Half-life too short to be able to perform the decay correction

[1221]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002459.CNF Report Generated On 3/5/2018 5:35 : 49 PM Sample Title B101110AFSWC020GD Sample Description Ul CTMT Sample Identification 020 Sample Type GAMMA DIRECT Sample Geometry 3M90D ECP 17.8 CM Peak Locate Threshold 3 .00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 2.830E+001 MA2 Sample Taken On 3/2/2018 2:35:00 PM Acquisition Started 3/2/2018 2:44:34 PM Live Time 600. 0 seconds Real Time 613.1 seconds Dead Time 2 . 14 % Energy Calibration used Done On 1/13/2015 Efficiency Calibration Used Done On 1/30/2018 Efficiency ID 3M90D ECP 17 8CM [1222]

Peak Analysis Report 3/5/2018 5:35:49 PM Page 2

          • P E A K A N A L Y S I S REPORT *****

Detector Name: 5452 Sample

Title:

B101110AFSWC020GD Peak Analysis Performed on: 3/5/2018 5:35:48 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area Uncert. Counts 1 113- 119 116.37 28.68 0.61 3.70E+002 84.37 5.55E+002 2 153- 168 160.73 39.79 1.42 6 . 64E+003 286.39 4.62E+003 3 176- 189 182.44 45.22 1. 32 2.09E+003 209.36 3.22E+003 4 284- 309 301. 26 74.97 1. 25 8.19E+003 531. 81 1.47E+004 5 332- 3 57 3 40 .37 84.76 1. 40 3.09E+003 548. 55 l.69E+004 6 382- 389 385.17 95.97 0.59 -1.31E+002 197.93 4 .93E+003 7 479- 496 488.26 121.78 1.28 l.28E+004 410.35 8.99E+003 8 971- 989 979.67 244.78 1.26 2.56E+003 244.27 3.65E+003 9 1367- 1387 1377.54 344.35 1.36 8.84E+003 248.58 1.82E+003 10 1464- 1477 1470.47 367.60 1.10 2.57E+002 114. 47 1.09E+003 11 1636- 1651 1644.30 411. 10 1.17 7.08E+002 123.77 l.04E+003 12 1766- 1785 1775.86 444.02 1. 39 1.02E+003 143.79 1.18E+003 13 1947- 1961 1954.18 488.64 1. 31 l.95E+002 98.23 7.68E+002 14 2361- 2370 2365.86 591.63 0 .86 5.98E+001 68.67 4.95E+002 15 2633- 2658 2645.96 661.70 1. 64 1.03E+003 151. 3 0 1 .10E+003 16 2706 - 2722 2713.96 678.71 0.78 1.04E+002 99.60 7.60E+002 17 2746- 2764 27 54 .79 688.92 1. 75 1.85E+002 107.56 8.00E+002 18 2884- 2900 2892.39 723.34 0.66 1. 41E+002 101.27 7.73E+002 19 3102- 3127 31 15 . 05 779.03 1.65 3.43E+003 169.72 8.89E+002 20 3455- 3502 3468.94 867.54 1. 81 1. 23E+003 22 7. 04 1. 65E+003 21 3663- 3685 3676.91 919.55 1. 26 1. 45E+002 103.62 6.55E+002 22 3842- 3869 3855.61 964.23 1. 79 3.77E+003 171.68 8.02E+002 23 4005- 4029 4019 . 49 1005.21 1. 23 4.24E+002 101 .99 5.28E+002 24 4328- 4372 4342.94 1086.08 1. 89 3.17E+003 186.09 8.14E+002 25 4433- 4461 4447.72 1112.27 1. 89 3.46E+003 160 .41 6.44E+002 26 4678- 4706 4692.67 1173.51 1. 95 3.10E+003 147 .15 5.00E+002 27 4839- 4861 4851.72 1213.27 1. 32 3.08E+002 70.51 2.41E+002 28 5022- 5034 5027.99 1257.33 0.88 l.99E+001 29.66 7.61E+001 29 5086- 5109 5097.80 1274.78 1. 60 4.53E+002 59.84 1 .11E+002 30 5185- 5209 5196.05 1299.33 1.42 4.15E+002 59.73 1 .17E+002 31 5315- 5344 5330.09 1332.84 1. 90 3.05E+003 121. 44 1 .36E+002 32 5575- 5588 55 81 .29 1395.62 0.29 l .16E+001 19.14 2.84E+001 33 5616- 5647 5632. 17 1408.33 2.14 5.32E+003 155.94 1.54E+002 34 5822- 5854 5829.84 1457.73 0.68 2.48E+002 37.08 1. 94E+001 35 6105- 6122 6113.35 1528.57 0.90 6.51E+001 18.76 6.90E+OOO 36 7051- 7064 7057.13 1764.36 0.44 l.45E+001 11.26 5.47E+OOO M ; First peak in a mul tiplet region m ~ Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2.000 sigma [1223]

Interference Corrected Activity Report 3/5/2018 5:35:49 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSWC020GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . ...... ... . ... .... .. IDENTIFIED NUCLIDES           * * * * * * * * .. * * * * * * * * * *
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M"2 ) Uncertainty K-40 0.985 1460 .82* 10.66 3.04808E+006 5.27633E+005 Co-60 1.000 11 73 .23* 99.85 3.81751E+006 3.55091E+005 1332.49* 99.98 3.87244E+006 3.46116E+005 Cs-137 1.000 661.66* 85.10 1 .29157E+006 2.45230E+005 Eu-152 1.000 121 .78* 28.67 3.33191E+007 6.75738E+006 344.28* 26.60 2.95421E+007 4.92600E+006 1408.01* 21.07 3.26934E+007 2.78579E+006 Eu-154 0.999 123.07* 40.40 2.36450E+007 4.81185E+006 723.30* 20.06 7.67166E+005 5.57730E+005 1274.43* 34.80 1.63337E+006 2.53999E+005 Eu-155 0 .942 86.55* 30.70 8.67648E+006 2.31923E+006 105.31* 21.10 -4.99759E+005 7.63248E+005 Tl-208 0 .892 583.19* 85.00 7.29715E+004 8.42406E+004 Pb-212 0 .941 238.63* 43.60 4.72637E+006 8.86821E+005 Ac-228 0 .925 338.32* 11. 27 6.97267E+007 1.15686E+007 911.20* 25.80 6.47812E+005 4 .67608E+005 968.97* 15.80 2.79476E+007 2.78242E+006
       * ~ Energy line found in the spectrum.
       @  - Energy line not used for Weighted Mean Activity Energy Tolerance :          10.000 keV Nuclide confidence index threshold =              0.30 Errors quoted at 2. 000 sigma

[1224]

Interference Corrected Activity Report 3/5/2018 5: 35 :49 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 0. 985 3.048081E+006 5.276334E+005 Co-60 1 . 000 3. 845679E+O 06 v' 2.478531E+005 Cs-137 1 . 000 1. 291568E+006../ 2.452303E+005 Eu-152 1 . 000 3 .168018E+O 07 ;/ 2.269742E+006 Eu-154 0 .999 1. 485269E+006..r 2.297257E+005 Eu-155 0 .942 8.676478E+006 2.319232E+006 Tl-208 0 .892 7.297147E+004 8.424061E+004 X Bi-212 0 .975 Pb-212 0 .941 4. 726366E+006 8.868210E+005 X Pb-214 0. 386 Ac-228 0. 925 1. 508905E+006 4 .593624E+005 

      ?  '= Nuclide is part of an undetermined solution X  =  Nuclide rejected by the interference analysis
      @  =  Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2.000 sigma

[1225]

Interference Corrected Activity Report 3/5/2018 5:35:49 PM Page s 

  **********    U N I D E N T I F I E D      P E A K S      **********

Peak Locate Performed on: 3/5/2018 5:35:48 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 28.68 6.1746E-001 22.77 2 39.79 1 .1062E+001 4.32 3 45. 22 3.4823E+OOO 10.02 4 74. 97 1 .3657E+001 6.49 10 367.60 4.2818E-001 44.56 Sum 11 411. 10 1.1795E+OOO 17.49 12 444.02 1. 7035E+OOO 14 . 07 D-Esc. 13 488.64 3.2528E-001 50.33 Sum 16 678.71 1. 7339E-001 95.73 Sum 17 688.92 3.0799E-001 58 . 20 Sum 19 779.03 5.7086E+OOO 4.96 Sum 20 867.54 2.0427E+OOO 18.52 Tol. Nb-94 23 1005.21 7.0746E-001 24.03 Sum 24 1086.08 5.2755E+OOO 5.88 Sum 25 1112.27 5.7639E+OOO 4.64 27 1213.27 5.1312E-001 22.90 Sum 28 1257.33 3.3112E-002 149.30 Sum 30 1299.33 6.9169E-001 14.39 Sum 32 1395.62 1.9312E-002 165.15 Sum 35 1528.57 1. 0851E-001 28.82 Sum 36 1764.36 2.4208E-002 77.52 Sum M = First peak in a multiplet region m ~ Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1226]

Nuclide MDA Report 3/5/2018 5: 35 :49 PM Page 6

          • N U C L I D E MD A REPORT ****
  • Detector Name: 5452 Sample Geometry: 3M90D- ECP- 17.8CM Sample

Title:

B101110AFSWC020GD Nuclide Library used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuc lide MDA Activity Dec. Level Name (keV) (%) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       1460.82*   10 .66  4.304E+005      4.30E+005   3.048E+006    1.986E+005
 +      Co-60      1173.23*   99.85   1 .981E+005     l. 09E+005  3.818E+006    9.738E+004 1332.49*   99.98   1 .092E+005                 3.872E+006    5.29 0E+004 Nb-94       702.65    99.81   2.208E+005      2.21E+OOS   2.650E+005    1 .090E+OOS 871. 09   99. 89  2.829E+005                 -3.650E+002    1.399E+005 Ag-108m     433.90    90.50   2.478E+005      2.48E+005   5.516E+003    1.225E+005 614. 3 0  89.80   2.594E+005                  1 .267E+005   1.281E+005 722.90    90.80   2.637E+005                  1 .623E+005   1.302E+005 Cs-134      604.72    97.62   2.266E+005      2.27E+005  -3.478E+004    1. 119E+005 795.86    85.46   2.544E+005                  6.051E+003v~  1. 254E+OOS
 +      Cs-137      661.66*   85 .10  2.864E+005      2.86E+OOS   1.292E+006    1.415E+OOS
 +      Eu-152      121.78*   28.67   l.468E+006      5. 76E+OOS  3.332E+007    7.303E+005 344 .28*  26.60   9.027E+005                  2.954E+007    4.468E+005 1408. 01*  21. 07  5.759E+005                  3.269E+007    2.796E+005
 +      Eu-154      123.07*   40. 40  1.041E+006      2.60E+005   2.365E+007    5.182E+005 723.30*   20.06   8.951E+005                  7.672E+005    4.402E+005 1274.43*   34.80   2.596E+005                  1.633E+006    1 .249E+005
 +      Eu-155       86.55*   30 .70  2.486E+006      1 .26E+006  8 . 676E+006  1 .239E+006 105.31*   21. 10  1. 263E+O 06               -4.998E+005    6.262E+005
 +      Tl-208      583.19*   85. 00  1. 3 76E+O 05   1 .38E+005  7.297E+004    6.714E+004 Bi-212      727.33*    6.67   2.692E+006      2.69E+006   2.307E+006    1. 324E+O 06
 +      Pb-212      238.63*   43.60   6.792E+005      6.79E+005   4.726E+006    3.371E+OOS Bi-214      609.32    45.49   4.921E+005      2.64E+005   4.700E+005    2.430E+005 1120 .29   14.92   1. 217E+006                 2.063E+OOS    5.976E+005 176 4 .49  15.30   2.644E+005                  2.865E+OOS    1 .197E+005 Pb-214      295.22    18.42   l. 450E+006     6.74E+OOS   4.946E+005    7.188E+005 351.93*   35.60   6.745E+005                  2.207E+007    3.339E+005 Ra-226      186.21     3.64   8.818E+006      8.82E+006  -2.106E+006    4.381E+006
 +      Ac-228      338.32*   11.27   2.131E+006      7.SSE+OOS   6.973E+007    1.055E+006 911.20*   25.80   7.550E+005                  6.478E+OOS    3.715E+005 968.97*   15.80   1.481E+006                  2.795E+007    7.305E+005 Am-241       59.54    35.90   1.584E+006      1.58E+006   7.796E+005    7.875E+OOS
       + =Nuclide identified during the nuclide i dentification
       *=Energy line found in the spectrum
       > ~ Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1227]

~**** GAMM A S P E C T R U M ANALYSIS ***** Fi lename: 5452 Report Generated On 3/5/2018 1:20: 00 PM Sample Title B101110AFSFC021GD Sample Description Ul CTMT Sample Identification 021 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 1.256E+001 M"2 Sample Taken On 3/5/2013 1 :09:00 PM Acquisition Started 3/5/2018 1:09:54 PM Live Time 600 . 0 seconds Real Time 605.5 seconds Dead Time 0.91 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 1/30/2018 Efficiency ID 2M90D ECP 1 7 8CM Da f G Vu. I," cla {-e cP 3( ~ / I8 t 'ii '~'~ ~ 

                                                       /i~'71*lJ~~

s a~ ::: o. )) ~3q [1228]

Peak Analysis Report 3/5/2018 1 :2 0 : 00 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSFC021GD Peak Analysis Performed on: 3/5/2018 1 :20: 00 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 123 116 .14 28.62 1. 15 2.55E+002 74.22 3.84E+002 2 153- 168 160.66 39.77 1.44 1.78E+003 166.08 1.70E+003 3 176- 190 183.42 45.47 0. 61 4 .24E+002 136. 01 l .46E+003 4 286- 326 301 .70 75.08 1. 48 3.60E+003 517.73 1 .02E+004 5 332- 356 3 40 .48 84.79 1. 27 1.33E+003 340.57 6.69E+003 6 480- 497 488.45 121.83 1. 38 3.24E+003 248.24 3.74E+003 7 576- 587 579.10 144 .52 0 .27 -6.66E+001 141.06 2.01E+003 8 970- 988 979.30 244.68 1. 25 7.66E+002 153.96 l.53E+003 9 1224- 1234 1228.51 307.05 0 .50 2.28E+001 72.21 5.36E+002 10 1366- 1387 1376.99 344.21 1. 51 2.51E+003 152.66 8.86E+002 11 1637- 1652 1643.38 410 .87 0.43 1.41E+002 87.60 5.90E+002 12 1767- 1806 1775.04 443.81 1. 58 2.91E+002 178. 71 1.26E+003 13 2632- 2657 2645.04 661.47 1. 79 3.33E+003 146. 91 4. 85E+002 14 2746- 2763 2752.57 688.37 0.35 1.32E+002 59. 91 2.35E+002 15 2883- 2900 2890.46 722.86 1. 21 1 .13E+002 63.26 2.72E+002 16 3100- 3124 3113.44 778.63 1. 67 9.70E+002 101.66 3.92E+002 17 3454- 34 80 3467.36 867.14 1. 82 3.89E+002 86.73 3.41E+002 18 3841- 3866 3853.58 963.72 1. 88 1.07E+003 102.81 3.72E+002 19 3920- 3931 3925.07 981.60 0.27 -4.35E+OOO 32.89 1. 09E+002 20 4006- 4029 4017.67 1004.75 0.76 1.62E+002 60.63 1.89E+002 21 4256- 4267 4261.19 1065.64 0.37 1.60E+001 31.15 9.00E+OOl 22 4329- 4365 43 40 .55 1085.48 1. 74 8.78E+002 104.60 3.19E+002 23 4431- 4459 4445.48 1111.71 1. 79 1. llE +O03 95.39 2.52E+002 24 4675- 4703 4690.31 1172.92 2.08 1.56E+003 107.23 2.83E+002 25 4838- 4856 4848.06 1212.35 0.80 5.69E+001 40.97 1.07E+002 26 5087- 5105 5095.52 1274.21 0.97 1.14E+002 37.08 6.82E+001 27 5182- 5203 5193.20 1298.62 1. 06 1 .01E+002 35.64 5.77E+001 28 5312- 5342 5327.21 1332.11 2. 00 1 .63E+003 87.22 5.68E+001 29 5537- 5550 5543.64 1386.21 0 .51 5.85E+OOO 12.86 1.llE+OOl 30 5614- 5644 5629.24 1407 .60 2.03 1 .69E+003 87.99 5.14E+001 31 5830- 5852 5840. 05 1460.28 2 .14 1 .53E+002 30.28 2.llE+OOl M ~ First peak in a multiplet region m ~ Other peak in a multiplet region F ~ Fitted singlet Errors quoted at 2 . 000 sigma [1229]

Interference Corrected Activity Report 3/5/2018 1:20:00 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSFC021GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . ....... .. . ... . . .. .. IDENTIFIED NUCLIDES           a ., t * * * * * * * * * * * * * * '" I
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/M"2 ) Uncertainty K-40 1. 000 1460.82* 10 .66 1 .87867E+006 4.06153E+005 Co-60 0.995 1173.23* 99.85 3.69014E+006 3.89139E+005 1332.49* 99.98 3.98976E+006 3.84051E+OOS Ag-108m 0.424 433.90* 90.50 3.07751E+OOS l.94214E+OOS 614.30 89.80 722.90* 90.80 1.35820E+OOS 7.76349E+004 Cs-137 1. 000 661. 66* 85.10 4 .65842E+006 5.95925E+005 Eu-152 0.999 121.78* 28.67 1.07160E+007 2.29817E+006 344.28* 26.60 1.07087E+007 1 .87694E+006 14 08.01* 21. 07 1 .34259E+007 1 .28072E+006 Eu-154 0.997 123.07* 40. 40 8.80804E+006 1 .89481E+006 723.30* 20.06 9.12214E+OOS 5.21709E+OOS 1274.43* 34.80 6.12979E+OOS 2.05931E+005 Eu-155 0.329 86.55* 30.70 7.60712E+006 2.47410E+006 105.31 21.10 Pb-212 0.943 238.63* 43.60 1 .39564E+006 3.59896E+005
       *=Energy line found in the spectrum.
       @=Energy line not used for Weighted Mean Activity Energy Tolerance :            10.000 keV Nuclide confidence index threshold=                 0 .30 Errors quoted at 2 .000 sigma

[1230]

Interference Corrected Activity Report 3/5/2018 1: 20: 00 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M ... 2 ) Uncertainty K-40 1.000 1.878669E+006 4.061528E+005 Co-60 0.995 3. 841922E+006 / 2.733464E+005 Ag-108m 0.424 8.811055E+004 7.663361E+004 Cs-137 1.000 4. 658425E+006 ./ 5.959254E+005 Eu-152 0.999 1. 2103 01E+007*/ 9.557187E+005 Eu-154 0.997 5.561545E+OQ5 / 2.025189E+005 Eu-155 0.329 7.607121E+006 2.474098E+006 X Bi-212 0.969 Pb-212 0.943 1 .395644E+006 3.598960E+005 X Pb-214 0.384 

       ? = Nuclide is part of an undetermined solution X ~ Nuclide rejected by the interference analysis
      @ ~ Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1231]

Interference Corrected Activity Report 3/5/2018 1 :20:00 PM Page 5 

  **********     U N I D E N T I F I E D      PE AK S        **********

Peak Locate Performed on: 3/5/2018 1 :20: 00 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV} Counts per Second  % Uncertainty Type Nuclide 1 28.62 4.2567E-001 29.06 2 39.77 2.9729E+OOO 9.31 3 45.47 7.0707E-001 32.06 4 75.08 5.9950E+OOO 14.39 7 144 .52 -1. llOlE-001 -211.79 D-Esc . 9 307.05 3.7996E-002 316.74 D-Esc . 11 410 .87 2.3458E-001 62.23 14 688.37 2.2036E-001 45. 31 Sum 16 778.63 1. 6171E+OOO 10 .48 Sum 17 867.14 6.4865E-001 22.28 Tol. Nb-94 18 963.72 1. 7756E+OOO 9.65 Sum 19 981.60 -7.2540E-003 -755.66 20 1004.75 2.7031E-001 37. 3 9 Sum 21 1065.64 2.6667E-002 194.67 Sum 22 1085.48 1.4625E+OOO 11. 92 23 1111 .71 1 .8553E+OOO 8.57 Sum 25 1212.35 9.4891E-002 71.97 27 1298.62 1 .6889E-001 35.17 Sum 29 1386.21 9.7549E-003 219.74 Sum M First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1232]

Nuclide MDA Report 3/5/2018 1 :20:00 PM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSFC021GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10.66  3.862E+005      3.86E+005    1. 879E+006           1.765E+005
 +      Co-60      1173.23*    99.85  2.883E+005      1.40E+005    3.690E+006            1.410E+005 1332.49*    99.98  1 .396E+005                  3.990E+006            6.650E+004 Nb-94       702.65     99.81  1 .423E+005     1.42E+005    1.294E+OOS            6.969E+004 871. 09    99.89  1 .713E+005                  4.087E+004            8.413E+004
 +      Ag-108m     433.90*    90.50  3.076E+005      1.21E+005    3.078E+005            1 .524E+005 614.30     89.80  1.632E+005                  -4.547E+004            8.004E+004 722.90*    90.80  1.211E+005                   1.358E+OD5            5.892E+004 Cs-134      60 4 .72   97.62  8.100E+005      8. lOE+O 05  9. 54 OE+OOS ..,..... 3. 973E+OOS 795.86     85.46  8.523E+005                  -1 .878E+005           4.167E+005
 +      Cs-137      661. 66*   85.10  2.125E+005      2.13E+005    4.658E+D06            1.044E+005
 +      Eu-152      12 1. 78*  28.67  1.211E+006      4.27E+005    1.072E+007            6.009E+005 344.28*    26.60  8.210E+005                   1.071E+007            4 .047E+005 1408.01*    21.07  4.273E+005                   1.343E+OD7            2.029E+005
 +      Eu-154      123.07*    40.40  9.953E+005      2.83E+D05    8.808E+006            4.939E+005 723.30*    20.06  8.132E+005                   9.122E+OD5            3.957E+OOS 1274.43*    34.80  2.833E+005                   6.130E+005            1 .344E+005
 +      Eu-155       86.55*    30.70  3.150E+006      2.9SE+006    7.607E+006            1 .567E+006 105.31     21.10  2.947E+006                  -1 .076E+006           1.463E+D06 Tl-208      583.19     85.00  1.804E+005      1. BOE+OOS   2.934E+005            8.857E+OD4 Bi-212      727.33*     6.67  1.635E+006      1. 63E+006   1.834E+D06            7.954E+005
 +      Pb-212      238.63*    43.60  4.354E+005      4.3SE+005    1.396E+006            2.152E+OOS Bi-214      609.32     45.49  3.176E+005      2.72E+005   -7.309E+003            1.557E+OOS 1120.29     14.92  7.420E+005                  -6.704E+D05            3.600E+OD5 1764.49     15.30  2.721E+005                   3.0SOE+OOS            1.235E+OD5 Pb-214      295.22     18.42  9.397E+005      4.76E+OOS   -8.554E+005            4.637E+OD5 351.93*    35.60  4 .759E+005                  6.208E+006            2.346E+OOS Ra-226      186.21      3.64  5.802E+006      5.BOE+D06   -2.844E+OD6            2.874E+006 Ac-228      338.32     11. 27 1.544E+006      S.17E+OOS    4 .507E+005           7.613E+OD5 911. 20    25.80  5.166E+005                  -2.147E+005            2.523E+005 968.97     15.80  1.362E+006                   8.954E+004            6.708E+OOS Am-241       59.54     35.90  1. 03 9E+O 06   1.04E+D06   -1 .949E+005           5.149E+005
       + ; Nuclide identified during the nuclide identification
       * = Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ = Half-life too short to be able to perform the decay correction

[1233]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002487.CNF Report Generated On 3/6/2018 7 :1 6 :46 AM Sample Title B101110AFSFC022GD Sample Description Ul CTMT Sample Identification 022 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 1.256E+001 M"2 Sample Taken On 3/5/2013 12:37:00 PM ~cquisition Started 3/5/2018 12:37:15 PM Live Time 600 . 0 seconds Real Time 601.3 seconds Dead Time 0.21 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 1/30/2018 Efficiency ID 2M90D ECP 1 7 8CM [1234]

Pe~k Analysis Report 3/6/2018 7:16:46 AM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSFC022GD Peak Analysis Performed on: 3/6/2018 7: 16 :45 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 123 117 .29 28.91 0.84 l.OOE+002 39.83 l .04E+002 2 294- 310 302.39 75.25 1. 56 4.07E+002 134.51 l .31E+003 3 1369- 1386 1380.43 345 .07 0.92 7.17E+001 47. 84 1 .51E+002 4 1465- 1474 1469. 13 367.27 0.34 -1.71E+D01 25.82 8.llE+OOl 5 2633- 2658 2646. 01 661. 71 2.09 1 .25E+003 84.38 1.24E+002 6 4439- 4454 4447. 11 1112.12 0.69 5.18E+001 25.86 3.82E+001 7 5316- 5338 5327.68 1332.23 1. 70 1 .19E+002 27. 25 1. 73E+O 01 8 5620- 5640 5629.25 1407.60 0.38 l.07E+002 28.30 2.58E+001 M = First peak in a mul tiplet region m "" Other peak in a mul tiplet region F ; Fitted singlet Errors quoted at 2.000 sigma [1235]

Interference Corrected Activity Report 3/6/2018 7:16:46 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSFC022GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activi t y Activity Name Confidence (keV) (%) (pCi/M" 2 ) Uncertainty Cs-137 1.000 661.66* 85 .10 1.75019E+006 2.40997E+OOS Eu-152 0.333 121.78 28.67 344.28* 26.60 3.06518E+OOS 2.10580E+OOS 1408. 01* 21.07 8.50073E+OOS 2.34438E+005 

       * = Energy line found in the spectrum.
       @=Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold ~         0.30 Errors quoted at 2.000 sigma

[1236]

Interference Corrected Activity Report 3/6/2018 7:16:46 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuc;:lide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty Cs-137 1.000 1 . 75018 6 E+ 0 0 6 ./ 2.409973E+OOS Eu-152 0.333 5. 492380E+005 ./ 1. 56660 lE+OOS X Pb-214 0.397 

       ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2.000 sigma
  **********      U N I D E N T I F I E D             P E A K S       **********

Peak Locate Performed on: 3/6/2018 7:16:45 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 28.91 1.6725E-001 39.69 2 75.25 6.7831E-001 33.05 4 367.27 -2.8503E-002 -150.98 6 1112.12 8.6394E-002 49.89 Tol. Bi -214 7 1332.23 1.9792E-001 22.94 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1237]

Nuclide MDA Report 3/6/2018 7: 16 :46 AM Page 5

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

Bl01110AFSFC022GD Nuclide Library Used : C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) K-40 1460.82 10 .66 6.698E+005 6.70E+OOS 1.429E+006 3.183E+005 Co-60 1173.23 99.85 1.451E+005 l .45E+OOS 2.044E+005 6.936E+004 1332.49 99.98 1.476E+005 3.267E+005V""' 7.047E+004 Nb-94 702.65 99.81 5.178E+004 5.18E+004 4.850E+004 2.443E+004 871.09 99.89 5.685E+004 -6.572E+003 2.689E+004 Ag-108m 433.90 90.50 7.188E+004 5.86E+004 -5.060E+004 3.452E+004 614.30 89.80 7.181E+004 1.326E+004 3.433E+004 722.90 90.80 5.863E+004 -l.084E+004 2.769E+004 Cs-134 604.72 97.62 3.535E+005 2.97E+OOS 1.033E+004v 1.691E+005 795.86 85.46 2.966E+005 1.523E+005 l.389E+005 

 +       Cs-137     661.66*    85.10  1.094E+005    l .09E+OOS   l.750E+006     5.280E+004
 +       Eu-152     121. 78    28.67  6.252E+005    2.73E+OOS    5.161E+005     3.081E+005 344.28*    26.60  3.261E+005                 3.065E+005     l.573E+005 1408. 01*   21. 07 2.730E+005                 8.501E+005     1.258E+005 Eu-154     123.07     40.40  5.153E+005    1. 45E+OOS   4. 102E+005 /  2.540E+005 723.30     20.06  3.976E+005                 1.167E+005     l.879E+005 1274.43     34.80  1.448E+005                -4.877E+004     6.511E+004 Eu-155       86.55    30.70  1.218E+006    1. 22E+006   1.649E+006     6.015E+OOS 105.31     21.10  1.443E+006                 4. 162E+005    7.111E+005 Tl-208     583.19     85.00  7.078E+004    7 . 08E+004  7.616E+004     3.376E+004 Bi-212     727.33      6.67  8.263E+005    8.26E+OOS    9.111E+005     3.912E+005 Pb-212     238.63     43.60  2.133E+005    2.13E+OOS   -5.429E+003. 1.042E+005 Bi-214     609.32     45.49  1.459E+005    l .46E+OOS   1.968E+005     6.988E+004 1120.29     14.92  3.022E+005                -2.710E+005     1.401E+005 1764.49     15.30  2.758E+005                 3.143E+005     1.254E+005 Pb-214     295.22     18.42  4.435E+005    1 .89E+OOS   5.047E+005     2.155E+OOS 35 1. 93*  35.60  l.891E+005                 1.777E+005     9.117E+004 Ra-226     186.21      3.64  2.674E+006    2.67E+006    l.076E+006     1 .310E+006 Ac-228      338.32     11. 27 5.875E+005    2.06E+OOS   -l.001E+004     2.833E+005 911.20     25.80  2.061E+005                 1.000E+004     9.703E+004 968.97     15.80  4.098E+005                 l.055E+005     1 .949E+005 Am-241        59.54    35.90   5.463E+005   5.46E+OOS    2.354E+OOS     2.685E+005
       + = Nuclide identified during the nuclide identification
       *  = Energy line found in the spectrum
       >  = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @  = Half-life  too short to be able to perform the decay correction

[1238]

          • GAMM A S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/5/2018 2:59:22 PM Sample Title B101110AFSCC023GD Sample Description Ul CTMT Sample Identification 023 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size Sample Taken On 3/5/2013 2:48:00 PM Acquisition Started 3/5/2018 2:49:20 PM Live Time 600.0 seconds Real Time 602.0 seconds Dead Time 0 . 33 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 1/30/2018 Efficiency ID 2M90D ECP 1 7 8CM f)c. f ~ Ve L- cl u l f c/ 3/>/!'8 til3,. 

                                                                         ,,.. j l)t< /7tc~,. CJ;;.
                                                          )o i=' :::. c. f ~ :i. /.';J

[1239]

Feak Analysis Report 3/5/2018 2:59:22 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

Bl 01110AFSCC023GD Peak Analysis Performed on: 3/5/2018 2:59:22 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 155- 168 161. 36 39.95 1. 37 2.40E+002 68.49 3.39E+002 2 293- 309 301. 72 75.08 1.41 7.30E+002 142.52 1. 39E+003 3 482- 498 489.55 122. 10 1. 60 4 .64E+002 119.26 9.88E+002 4 973- 987 980.08 244.88 1. 33 1.32E+002 65.65 3.28E+002 5 1368- 1388 1377.70 344.39 1. 63 3.88E+002 70.08 2.31E+D02 6 2431- 2445 2438.34 609.76 0 .86 6.56E+001 31. 14 6 .14E+001 7 2633- 2657 2645.73 661.64 1. 95 1.23E+003 83. 17 1.22E+002 8 3104- 3126 3113.39 778.62 1. 96 1.83E+002 41.69 6.52E+001 9 3841- 3866 3854.59 963.98 2 .12 2.02E+002 46.76 8.12E+D01 10 4331- 4350 43 41 .61 1085.74 1. 31 1.17E+002 33.49 4.66E+001 11 4437- 4457 44 46 .19 1111.89 1. 71 1.59E+002 38.75 5.96E+001 12 4680- 4704 4691.70 1173.26 1. 91 2.78E+002 40 .92 3.41E+D01 13 5315- 5340 5327.63 1332.22 2. 13 2.89E+002 37.06 1.28E+001 14 5620- 5643 5630.45 1407.90 1. 80 2.61E+002 35.97 1. 65E+001 15 5830- 5852 5841.06 1460.53 2.06 1.40E+002 28.40 1.63E+001 M ~ First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1240]

Interference Corrected Activity Report 3/5/2018 2:59:22 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSCC023GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . ....... 1 * " . .... ...... IDENTIFIED NUCLIDES             . . .. ......... ' ** *
  • f * '

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 1.000 1460.82* 10.66 1 .71624E+006 3.79366E+005 Co-60 0.995 1173.23* 99.85 6.57123E+005 1.10114E+005 1332.49* 99.98 7.08343E+005 1. 06986E+005 Cs-137 1.000 661.66* 85.10 1 .71676E+006 2.36682E+OOS Eu-152 0.999 121.78* 28.67 1 .53510E+006 5.00253E+005 344.28* 26.60 1 .6559SE+006 4. 04578E+005 1408.01* 21.07 2.06534E+006 3.29610E+005 Pb-212 0.939 238.63* 43.60 2.40073E+005 1. 25734E+005 Bi-214 0.688 609.32* 45.49 l.49756E+005 7.33659E+004 11 20.29* 14.92 1.29221E+006 3.30727E+005 1764.49 15 . 30 

        * = Energy line found in the spectrum.
       @=Energy line not used for Weighted Mean Activity Energy Tolerance :             10.000 keV Nuclide confidence index threshold =                   0 .30 Errors quoted at 2.000 sigma

[1241]

Interference Corrected Activity Report 3/5/2018 2: 59: 22 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1.000 1. 7162 38E+O 06 3.793656E+005 Co-60 0.995 6.834708E+005 ./ 7.673229E+004 Cs-137 1.000 1. 716764E+Oo6 / 2.366819E+OOS Eu-152 0.999 1. 826086E+006/ 2.275680E+005 Pb-212 0.939 2.400728E+OOS 1.257336E+OOS Bi-214 0.688 2.033390E+005 7.162475E+004 X Pb-214 0.387 

       ? = Nuclide is part of an undetermined so lution X = Nuclide rejected by the interference analysis
      @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2. 000 sigma

[1242]

Interference Corrected Activity Report 3/5/2018 2:59:22 PM Page 5 

  **********    U N I D E N T I F I E D      P E A K S    **********

Peak Locate Performed on: 3/5/2018 2:59:22 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 39.95 4.0003E-001 28.53 2 75.08 1.2173E+OOO 19.51 8 778.62 3.0474E- 001 22.80 Sum 9 963.98 3.3639E- 001 23.17 Sum 10 1085 .74 1.9566E- 001 28.53 M "" First peak in a multiplet region m  ; Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1243]

Nuclide MDA Report 3/5/2018 2: 59: 22 PM Page 6

          • N U C L I D E MDA REPORT *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSCCD23GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/M"'2 ) 

 +       K-40      1460.82*    10.66   3.512E+OOS     3.51E+OOS    1.716E+006     1. 590E+OOS
 +       Co-60 . 1173.23*    99.85   9.867E+004     6.58E+004    6.571E+005     4.613E+004 1332.49*    99.98   6.585E+004                  7.083E+005     2.961E+004 Nb-94       702.65     99. 81  6.223E+004     6.22E+004    2.307E+004     2.966E+004 871.09     99.89   7.303E+004                  5.242E+OD4     3.498E+004 Ag-108m     433.90     90.50   9.071E+004     7.60E+004   -8.274E+003     4.394E+004 614.30     89.80   8.811E+004                 -3.565E+004     4.248E+004 722.90     90.80   7.597E+004                  9.602E+004     3.636E+004 Cs-134     604.72     97.62   3.979E+OOS     3.98E+OOS   -1.014E+005     1 .913E+005 795.86     85.46   4 .077E+005       o.co ~~u -1.114E+OOS     1 .945E+005
 +       Cs-137     661.66*    85.10   1.067E+005     1.07E+OOS    1.717E+OD6     5.146E+004
 +       Eu-152     12 1 .78*  28.67   6.143E+OOS     2.29E+OOS    1.535E+006     3.027E+005 344.28*    26.60   4.189E+005                  1.656E+006     2.037E+005 1408.01*    21. 07  2.285E+005                  2.065E+006     1.035E+005 Eu-154     123.07     40.40   S.903E+005     2.29E+OOS    1. 670E+O 06 J 2. 915E+O OS 723.30     20.06   4.986E+005                  1.127E+OOS     2.384E+OOS 1274.43     34.80   2.287E+005                  2.825E+OOS     1.071E+005 Eu-155      86.55     30.70   1 .314E+006    1 .31E+006   2.634E+006     6.492E+OOS 105.31     21.10   1 .534E+006                -1.098E+006     7.568E+005 Tl-208     583.19     85.00   8.959E+004     8.96E+004    8.839E+004     4 .316E+004 Bi-212     727.33      6.67   1.021E+006     1.02E+006    8.814E+005     4 .887E+005
 +       Pb-212     238.63*    43. 60  1. 892E+O 05   1.89E+OOS    2.401E+005     9.216E+004
 +       Bi-214     609.32*    45.49   1. 06 lE+O 05  1.06E+OOS    1.498E+005     4.996E+004 1120.29*    14.92   4.139E+005                  1.292E+006     1.960E+005 1764. 49    15. 30  2.645E+005                  2.865E+005     l.197E+OOS Pb-214     295.22     18.42   5.037E+005     2.43E+OOS    2.008E+005     2.457E+OOS 351.93*    35.60   2.428E+005                  9.599E+OOS     1.181E+005 Ra-226     186.21      3.64   3.077E+006     3.08E+006   -8.542E+OOS     1.511E+006 Ac-228     338.32     11. 27  7.SlSE+OOS     2.68E+OOS   -1.775E+005     3.653E+005 91 1. 20   25.80   2.679E+OOS                  1 .550E+005    1. 279E+005 968.97     15.80   6.444E+005                 -9.523E+004     3.122E+005 Am-241      59.54     35.90   5.387E+005     5.39E+005   -1.336E+004     2.647E+005
       +    Nuclide identified during the nuclide identification
  • Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ ~ Half-life too short to be able to perform the decay correction

[1244]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/5/2018 3: 14 :16 PM Sample Title B101110AFSCC024GD Sample Description Ul CTMT Sample Identification 024 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3 .00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size Sample Taken On 3/5/2013 3:08:00 PM Acquisition Started 3/5/2018 3:04:09 PM Live Time 600.0 seconds Real Time 604.9 seconds Dead Time 0. 81 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 1/30/2018 Efficiency ID 2M90D ECP 17_ 8CM [1245]

Peak Analysis Report 3/5/2018 3:14:16 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSCC024GD Peak Analysis Performed on: 3/5/2018 3:14:15 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 123 116.74 28.78 1.44 2.77E+002 61. 61 2.41E+002 2 154- 169 161.84 40. 07 1. 77 1.03E+003 133.84 l.15E+003 3 178- 192 184.55 45.75 1. 04 2.22E+002 109.92 9.72E+002 4 284- 310 302.12 75.18 1. 86 2.81E+003 286.45 4.0SE+003 5 333- 348 341.80 85.12 1. 03 4 .92E+002 199.86 3.15E+003 6 386- 396 391.05 97.45 0.51 3.37E+001 132.78 1.83E+003 7 480- 497 489.42 122.07 1. 83 2.38E+003 213.14 2.76E+003 8 971- 989 979.92 244.84 1. 88 6.22E+002 127.58 1. 02E+O 03 9 1066- 1075 1071.95 267.87 0.69 3.34E+001 61. 01 3.99E+002 10 1369- 1388 1377.77 344 .41 1. 78 1.95E+003 122. 17 5.09E+002 11 1768- 1786 1775.75 443.99 1.26 1.44E+002 77.76 4.04E+002 12 1847- 1859 1854. 51 463 .70 0.32 1.42E+001 49. 33 2.26E+002 13 2236- 2245 2240.62 560.30 0.30 2.69E+001 36 .25 1. 33E+O 02 14 2634- 2656 2645.59 661.61 1. 78 3.73E+002 81.64 3.33E+002 15 3101- 3127 3114 . 32 778.85 1. 54 7.73E+002 83.61 2.23E+002 16 3458- 3478 3467.86 867.27 1.38 2.75E+002 60.95 1. 79E+O 02 17 3844- 3868 3854.93 964.06 1. 94 8.10E+002 80.59 1. 98E+O 02 18 4010- 4030 4017 . 35 1004.67 1.13 1.29E+002 47 .12 1. 16E+O 02 19 4165- 4178 4170.98 1043.08 0.31 2.64E+001 27. 33 5.76E+001 20 4331- 4355 4341. 50 1085.72 2.22 5.97E+002 80.85 2.49E+002 21 4434- 4460 4445.94 1111.83 1. 96 7.87E+002 73.87 1. 34E+O 02 22 4677- 4704 4690.60 1172.99 2.03 9.17E+002 76.85 1.25E+002 23 4842- 4858 4850.88 1213.06 0.81 5.19E+001 29 .12 5.llE+OOl 24 5086- 5107 5095.20 1274.13 1.10 1.21E+002 34.24 4.65E+001 25 5186- 5206 5194.86 1299.04 0 .69 1. OOE+002 27.49 2.47E+001 26 5314- 5342 5328.01 1332. 31 2.22 8.86E+002 69.19 6.77E+001 27 5617- 5645 5630.13 1407.82 2.09 1. 13E+003 75. 31 6.45E+001 28 5833- 5852 5840.90 1460.49 1. 53 8.57E+001 27.67 3.03E+001 M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1246]

Interference corrected Activity Report 3/5/2018 3: 14 : 16 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101l10AFSCC024GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . ....... ... ......... IDENTIFIED NUCLIDES          * * * ~ * * * * * * * * * * .. Ill * ..
  • ti Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 1. 000 1460 .82* 10.66 l.05260E+006 3.52023E+005 Co-60 0.995 1173 .23* 99.85 2.16902E+006 2.51251E+005 1332.49* 99.98 2.17055E+006 2.42609E+005 Cs-137 1 . 000 661.66* 85.10 5.20703E+005 1.30102E+005 Eu-152 0 .999 121.78* 28.67 7.87649E+006 1 .72797E+006 344.28* 26.60 8.33628E+006 l .46615E+006 1408.01* 21.07 8.96256E+006 9.33025E+005 Eu-154 0.682 123.07* 40.40 6.47412E+006 1 .42449E+006 723.30 20.06 1274.43* 34.80 6.49206E+005 1 .91896E+005 Eu-155 0 .953 86.55* 30.70 2.80757E+006 1 .27114E+006 1 05.31* 21.10 2.61916E+OOS 1 .03276E+006 Pb-212 0 .940 238.63* 43.60 1 .13359E+006 2.95959E+005
       *=Energy line found in the spectrum.
       @=Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuclide confidence index threshold=            0.30 Errors quoted at 2.000 sigma

[1247]

Interference Corrected Activity Report 3/5/2018 3: 14: 16 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"'2 ) Uncertainty K-40 1. 000 1 .052601E+006 3.520226E+005 Co-60 0.995 2 .169812E+006 v* 1.745258E+005 Cs-137 1. 000 5.207033E+OO S\I l.301016E+005 Eu-152 0.999 8.492681E+006 / 7.132214E+005 Eu-154 0.682 6.285113E+005.i' l.901367E+005 Eu-155 0.953 1. 2742 03E+O 06 8 .01 5575E+005 Pb-212 0.940 1 .133585E+006 2.959590E+005 X Pb-214 0.387 

       ? - Nuclide is part of an undetermined so lution X = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1248]

Interference Corrected Activity Report 3/5/2018 3:14: 16 PM Page 5 

  **********     U N I D E N T I F I E D       P E A K S      **********

Peak Locate Performed on: 3/5/2018 3:14:15 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 28.78 4.6178E-001 22.24 2 40. 07 1.7088E+OOO 13.05 3 45.75 3.6963E-001 49.56 4 75.18 4.6913E+OOO 10 . 18 9 267.87 5.5596E-002 182.90 11 443.99 2.3918E- 001 54. 18 D-Esc . 12 463.70 2.3726E-002 346. 54 Sum 13 560.30 4.4854E-002 134.69 15 778.85 1 .2888E+OOO 10 .81 Sum 16 867.27 4.5792E-001 22.18 Tol. Nb-94 17 964.06 1 .3494E+OOO 9.95 Tol. Ac-228 18 1004 .67 2.1487E-001 36.55 Sum 19 1043.08 4.4048E-002 103.42 20 1085.72 9.9520E-001 13 .54 21 1111.83 1. 312 lE+OOO 9.38 23 1213.06 8.6517E-002 56.10 25 1299.04 1. 6 721E-001 27. 40 Sum M = First peak i n a multiplet region m = Other peak i n a multiplet region F 

          - Fitted singlet Errors quoted at    2 . 000 sigma

[1249]

Nu.elide MDA Report 3/5/2018 3: 14: 16 PM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Ge*ometry: Sample

Title:

B101110AFSCC024GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/MA2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +       K-40      1460.82*    10 .66 4.489E+OOS    4.49E+005     1. 053E+006  2.078E+005
 +       Co-60     1173.23*    99.85  1. 903E+005   1. 49E+005    2.169E+006   9.196E+004 1332.49*    99.98  1.486E+005                  2.171E+006   7.097E+004 Nb-94      702.65     99.81  1.14BE+005    1.15E+005    -7.048E+004   5.594E+004 871.09     99.89  1.449E+005                  5.385E+003   7.090E+004 Ag-108m    433.90     90.50  1.341E+005    1. 34E+OOS    1.734E+004   6.563E+004 614. 3 0   89.80  1.393E+005                 -2.809E+004   6.806E+004 722.90     90.80  1.367E+005                  2.971E+004   6.672E+004 Cs-134     604.72     97.62  6.610E+005    6. 6 1E+OOS  -6.897E+005   3.228E+005 795.86     85.46  6.978E+005                  2.912E+005v  3.395E+005
 +       Cs-137     66 1 .66*  85. 10 1.691E+005    1. 6 9E+005   5.207E+005   8.268E+004
 +       Eu-152     12 1 .78*  28.67  1.041E+006    4. 6 4E+OOS   7.876E+006   5.158E+005 344.28*    26.60  6.044E+005                  8.336E+006   2.964E+005 140 8.01*   21.07  4.635E+005                  8.963E+006   2.210E+005
 +       Eu-154     123.07*    40.40   8.553E+005   2.47E+005     6.474E+006   4.240E+005 723.30     20.06   9.142E+005                -1.125E+005   4.462E+005 1274.43*    34.80  2.473E+005                  6.492E+005   1.164E+005
 +       Eu-155      86.55*    30.70   1.844E+006   1.71E+006     2.808E+006   9.145E+OOS 105.31*    21.10   1.711E+006                 2.619E+005   8.450E+OOS Tl-208     583.19     85.00   1.469E+005   1.47E+005     1 .233E+005  7.181E+004 Bi-212     727.33      6.67   1.832E+006   1.83E+006     7.355E+005   8.941E+005
 +       Pb-212     238.63*    43.60   3.568E+005   3.57E+005     1.134E+006   1. 759E+O 05 Bi-214     609.32     45. 49 2.707E+005    2.17E+005     9.451E+004   1 .323E+005 1120.29     14.92   6.395E+005                -5.654E+005   3.08BE+005 1764. 49    15. 30  2.173E+005                 1.076E+005   9.616E+004 Pb-214     295.22     18.42   7.977E+OOS   3 . 5 0E+005  4.499E+005   3.927E+005 351.93*    35.60   3.504E+005                 4.832E+006   1.718E+005 Ra-226     186.21      3.64   4 .740E+006  4.74E+006     1 .184E+006  2.342E+006 Ac-228     338.32     11. 27  1.253E+006   4.32E+OOS    -1 .720E+006  6.159E+005 911. 20    25.80   4.324E+005                 1 .486E+OOS  2.102E+005 968.97     15.80   1 .169E+006               -l.122E+005   S.745E+005 Am-241      59.54     35.90   8.304E+005   8.30E+005     1.608E+005   4.105E+005
       +=Nuclide identified during the nuclide identification
       * =Energy line found in the spectrum
        > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1250]

          • GAMMA S P E C T R U M ANALYSIS *****

Filename: 5452 Report Generated On 3/7/2018 10:26:50 AM Sample Title Bl01110AFSWC025GD Sample Description Ul CTMT Sample Identification 025 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO M"2 Sample Taken On 3/7/2018 10:23:00 AM Acquisition Started 3/7/2018 10:16:47 AM Live Time 600.0 seconds Real Time 601.7 seconds Dead Time 0 . 28 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1.5M90DECP17 BCM [1251]

Peak Analysis Report 3/7/2018 10 :26:50 AM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B1 01110AFSWC025GD Peak Analysis Performed on: 3/7/2018 10:26:49 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 155 130.14 32.13 2.04 9.08E+002 12 8. 84 4 .75E+002 2 297- 309 301. 72 75.08 1.12 3.01E+002 109.65 1 .01E+003 3 335- 348 3 40 .09 84.69 1. 36 2.12E+002 107.33 9.57E+002 4 1544- 1559 1554. 16 388.55 0.38 5.09E+001 51.55 2.04E+002 5 1954- 1963 1958. 51 489.72 0.86 1.17E+001 29.32 8.93E+001 6 2483- 2492 2487.09 621.96 0.33 1.00E+OOl 19.38 3.70E+001 7 2632- 2656 2644.66 661. 38 1. 80 7.53E+003 179.22 1.22E+002 8 3650- 3661 3655.10 914 .09 0.33 9.60E+OOO 9.70 5.40E+OOO 9 4679- 4698 4689.47 1172.71 1. 96 8.30E+001 23.28 1.50E+001 10 5316- 5335 5324.70 1331. 49 1.47 7.55E+001 22.44 1.45E+001 11 5829- 5850 5839.61 1460.17 2.02 1.40E+002 25.99 7.81E+OOO 12 7046- 7059 7052.20 1763.13 0 .33 2.40E+001 9.80 O.OOE+OOO M :::; First peak in a multiplet region m = Other peak in a multiplet region F :::; Fitted singlet Errors quoted at 2 . 000 sigma [1252]

Interference Corrected Activity Report 3/7/2018 10:26:50 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

Bl01110AFSWC02SGD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 0 .999 1460.82* 10 .66 l.72481E+006 3.53144E+005 Co-60 0 .999 11 73.23* 99.85 1. 01773E+O 05 2.96873E+004 1332.49* 99.98 9.58261E+004 2.95077E+004 Cs-137 1. 000 661.66* 85.10 9.35088E+006 l.14482E+006 Eu-155 0 .331 86.55* 30.70 5.79552E+005 3.15029E+005 105.31 21.10 

       * ~ Energy line found in the spectrum.
       @=Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold =           0.30 Errors quoted at 2. 000 sigma

[1253]

Interference Corrected Activity Report 3/7/2018 10:26:50 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M ... 2 ) Uncertainty K-40 0.999 l .724808E+006 3.531441E+005 Co-60 0.999 9.878145E+0041 2.092829E+004 Cs-137 1.000 9. 350884E+006,1 l.144817E+006 Eu-155 0.331 5.795518E+005 3.150293E+005 

       ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ ~ Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2. 000 sigma

[1254]

Interference Corrected Activity Report 3/7/2018 10 :26:50 AM Page 5 

  **********      U N I D E N T I F I E D     P E A K S     **********

Peak Locate Performed on: 3/7/2018 10:26:49 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.13 1. 5129E+OOO 14.19 2 75.08 5.0183E-001 36.42 4 388.55 8.4869E-002 101. 24 5 489.72 1. 9435E-002 251.45 6 621. 96 l. 6684E-002 193.55 Tol. Ag-108m 8 914.09 1.6000E-002 101. 09 Tol. Ac-228 12 1763.13 4.0000E-002 40.82 Tol. Bi-214 M = First peak in a multiplet region m = Other peak in a multiplet region F 

         -  Fitted singlet Errors quoted at     2.000 sigma

[1255]

Nuc.l ide MDA Report 3/7/2018 10:26:50 AM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

Bl01110AFSWC025GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/M ... 2 ) (pCi/M ... 2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +       K-40       1460.82*     10.66   2.502E+005       2.50E+005       1. 725E+O 06  1.085E+005
 +       Co-60      1173.23*     99.85   3.255E+004       3.26E+004       1. 018E+O 05  l .462E+004 1332.49*     99.98   3.310E+004                       9.583E+004    1 .483E+004 Nb-94        702.65     99. 81  4.132E+004       3.38E+004       1.013E+004    l.921E+004 871. 09    99. 89  3.379E+004                       1 .189E+004   l.536E+004 Ag-108m      433.90     90.50   1.211E+005       3.87E+004       2.488E+004    5.913E+004 614 .30    89.80   7.740E+004                     -l.059E+005     3.714E+004 722.90     90.80   3.867E+004                     -2.043E+004     1. 773E+004 Cs-134       604.72     97.62   7.162E+004       4 . 5 7E+004    3.456E+004J   3.438E+004 795.86     85.46   4.567E+004                       1 .780E+004   2.108E+004
 +       Cs-137       66 1 .66*  85.10   9.488E+004       9.49E+004       9.351E+006    4 .576E+004 Eu-152       12 1 .78   28.67   4 .863E+005      1. 48E+005      7. 959E+004 / 2.397E+005 344.28     26.60   3.747E+005                       1.408E+005    l .829E+005 1408 .01     21. 07  l.477E+005                       5.341E+004    6.552E+004 Eu- 154      123.07     40.40   3.45SE+OOS       8.66E+004       2.508E+005 ~  1.703E+005 723.30     20.06   1 .770E+005                      1.725E+004    8.122E+004 127 4 .43    34.80   8.657E+004                       2.831E+004    3.841E+004
 +       Eu-155        86.SS*    30.70   4.712E+005       4.71E+OOS       5.796E+005    2.319E+005 105.31     21 .10  6.958E+OOS                       l.886E+005    3.430E+005 Tl-208       583.19     85. 00  7.653E+004       7.6SE+004     -5.329E+004     3.663E+004 Bi-212       727.33      6.67   5.614E+OOS       5.61E+OOS       1.976E+004    2.587E+005 Pb-212       238.63     43.60   2.648E+005       2.65E+OOS       l.333E+004    1.300E+005 Bi-214       609.32     45.49   1.532E+OOS       1. 5 3E+OOS     4 . 366E+004  7.354E+004 1120 .29     14. 92  2.940E+005                       2.149E+005    l .360E+005 1764.49      15. 30  2.441E+005                       1 .573E+005   1.095E+005 Pb-214       295.22     18.42   5.393E+005       2.9SE+005       2.623E+005    2.635E+005 351. 93    35.60   2.948E+OOS                     -1.133E+O 05    1.440E+005 Ra-226       186.21      3.64   3.413E+Oo6*      3.41E+006       7.028E+005    1.679E+006 Ac-228       338.32     11. 27  8.614E+005       1.77E+005     -3.578E+005     4.202E+005 91 1. 2 0  25.80   1.775E+005                       8.780E+004    8.272E+004 968.97     15.80   2.697E+OOS                     -6.018E+003     1. 249E+005 Am-241        59.54     35.90   S.147E+OOS       S.15E+005       3.194E+005    2.528E+005
        += Nuclide identified during the nuclide i dentification
        *=Energy line found in the spectrum
        > ~ Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
        @=Half-life too short to be able to perform the decay correction

[1256]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/7/2018 12:49:04 PM Sample Title B101110AFSWC026GD Sample Description Ul CTMT Sample Identification 026 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO MA2 Sample Taken On 3/7/2018 12:23:00 AM Acquisition started 3/7/2018 12:39:01 PM Live Time 600.0 seconds Real Time 602.4 seconds Dead Time 0 . 41 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1.5M90DECP17 BCM [1257]

Peak Analysis Report 3/7/2018 12:49:04 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 54 52 Sample

Title:

B10lll0AFSWC026GD Peak Analysis Performed on: 3/7/2018 12:49: 04 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 137 129.99 32.09 1. 57 8.83E+002 95.76 3.49E+002 2 293- 309 3 01. 77 75.10 1. 72 6.72E+002 149.25 1.56E+003 3 333 - 348 3 41. 90 85.14 0.79 2.47E+002 134.13 1.41E+003 4 1401- 1417 1407.79 351.92 1.52 1.28E+002 65.55 3.01E+002 5 2632- 2657 2645.22 661.52 1.95 l.04E+004 209.21 l.33E+002 6 4472- 4485 4477.94 1119.83 1.11 2.90E+001 13.91 7.00E+OOO 7 4680- 4699 4690.82 1173.05 0.39 9.80E+001 24.54 1.50E+001 8 5317- 5335 5326.34 1331.90 1.03 9.43E+001 21. 00 4.75E+OOO 9 5828- 5852 5839.92 1460.25 1. 08 1 .51E+002 27.47 9.24E+OOO 10 7049- 7062 7055.65 1763.99 0.63 1 .60E+001 8.00 O.OOE+OOO M First peak in a mul tiplet region m ;: Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1258]

Inte'rference Corrected Activity Report 3/7/2018 12 :49: 04 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC026GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

   * * * * * * *
  • I I * * * * * * * * *
  • IDENTIFIED NUCLIDES .,. * ._ * "' * * "' * * * * *
  • I ** '"'
  • I
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 0.999 1460.82* 10. 66 1. 85494E+006 3.74355E+005 Co-60 1.000 1173.23* 99.85 l. 20197E+005 3.15937E+004 1332.49* 99.98 1. 19718E+005 2.83457E+004 Cs-137 1 .000 661. 66* 85. 10 1. 28871E+007 1.56931E+006 Eu-155 0 .332 86.55* 30.70 6.70630E+005 3.88141E+005 105.31 21.10 Pb-214 0 .445 295.22 18.42 351.93* 35.60 3.16151E+005 1.70057E+005
           * = Energy line found in the spectrum.
           @=Energy line not used for Weighted Mean Activity Energy Tolerance :                     10.000 keV Nuclide confidence index threshold=                           0.30 Errors quoted at 2. 000 sigma

[1259]

Interference Corrected Activity Report 3/7/2018 12:49 :04 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 0.999 1. 8 5493 BE+O 06 3.743548E+005 Co-60 1.000 1.199318E+005 / 2.109859E+004 Cs-13 7 1.000 1.288712E+007v 1. 5693 08E+006 Eu-155 0.332 6.706303E+005 3.881412E+005 Pb-214 0.445 3.161514E+005 1 . 70 0565E+005 

      ?
  • Nuclide* is part of an undetermined solution X ~ Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1260]

Interference Corrected Activity Report 3/7/2018 12: 49: 04 PM Page 5 

  **********      U N I D E N T I    F I E D    P E A K S     **********

Peak Locate Performed on: 3/7/2018 12:49: 04 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.09 l.4714E+OOO 10.85 2 75.10 1.1194E+OOO 22.22 6 1119.83 4.8333E-002 47.96 Tol. Bi-214 10 1763.99 2.6667E-002 50.00 Tol. Bi-214 M = First peak in a multiplet region m ~ Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1261]

Nuclide MDA Report 3/7/2018 12: 49: 04 PM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSWC026GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) ( %) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       146 0 .82*  10.66   2.822E+005    2 . 82E+OOS      1.855E+006      1.245E+005
 +      Co-60      1173.23*    99.85   3.256E+004    2 . 02E+004      1 .202E+005     1.462E+004 1332.49*    99.98   2.017E+004                     1 .197E+005     8.367E+003 Nb-94       702.65     99.81   3.646E+004    3.65E+004       -3.777E+004      1 .67BE+004 87 1 .09   99.89   3.722E+004                     7.645E+003      1 .708E+004 Ag-108m     433.90     90.50   l. 353E+005   4.82E+004        4.291E+004      6.624E+004 614.30     89.80   9.192E+004                     5.941E+004      4.440E+004 722.90     90.80   4.820E+004                     1.162E+004      2.249E+004 Cs-134      604.72     97.62   7.934E+004    4.61E+004       -l.654E+004      3.824E+004 795.86     85.46   4.612E+004        0 .oct-'u J -1. 357E+004     2 .131E+004
 +      Cs-137      66 1. 66*  85.10   1. 008E+005   l. 0 1E+005      1.289E+007      4 .869E+004 Eu-152      12 1. 78   28.67   5.367E+005    1. 73E+005      -3.227E+005      2.649E+005 344.28     26.60   4.248E+005                     1.733E+Oos~     2.0BOE+OOS 1408. 01    21. 07  1. 733E+005                    4 .630E+004     7.831E+004 Eu-154      123.07     40.40   3.795E+005    9. 6 9E+004     -1.340E+005      1 .873E+005 723.30     20.06   2.135E+005                    -8.956E+004      9.94BE+004 1274.43     34.80   9.687E+004                     5. 4 05E+004 v' 4. 356E+004
 +      Eu-155       86.55*    30.70   5.898E+005    5.90E+OOS        6.706E+005      2.912E+005 105. 31    21.10   8.117E+005                     2.233E+005      4.010E+005 Tl-208      583.19     85.00   9.255E+004    9.26E+004        5.357E+004      4.465E+004 Bi-212      727.33      6.67   6.383E+005    6.38E+OOS        2.787E+005      2.972E+005 Pb-212      238.63     43.60   3.055E+005    3.0SE+OOS        1.830E+005      l.503E+OOS Bi-214      609.32     45.49   1.801E+005    1. BOE+OOS       9.797E+004      8.69BE+004 1120.29     14.92   3.117E+005                     2.717E+OOS      1.449E+005 1764.49     15. 30  2.171E+005                     l.847E+005      9.607E+004
 +      Pb-214      295.22     18.42   6.235E+005    2.57E+OOS       -l.381E+004      3.056E+005 351. 93
  • 35.60 2.574E+005 3.162E+005 1.254E+005 Ra-226 186.21 3.64 3.849E+006 3.85E+006 1.680E+006 1.898E+006 Ac-228 338.32 11. 27 9.813E+005 l.71E+OOS -2.400E+OOS 4.802E+OOS 911. 20 25.80 1.709E+005 1.229E+OOS 7.942E+004 968.97 15.80 3.400E+005 3.705E+005 1.600E+OOS Am-241 59.54 35.90 5.889E+005 5.89E+005 3.931E+OOS 2.899E+005
       + ; Nuclide identified during the nuclide identification
       * = Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ = Half-life too short to be able to perform the decay correction

[1262]

          • GAMMA S P E C T R U M ANALYSIS * ****

Filename: 5452 Report Generated On 3/7/2018 1:07:44 PM Sample Title Bl01110AFSWC027GD Sample Description Ul CTMT Sample Identification 027 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO M" 2 Sample Taken On 3/7/2018 1:03: 00 PM Acquisition Started 3/7/2018 12:57:41 PM Live Time 600 . 0 seconds Real Time 601.9 seconds Dead Time 0 . 31 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done on 3/7/2018 Efficiency ID 1.SM90DECP17 8CM ['Jci f<:,. Va/; cf c.. {r c! 

                                                     **-;i,j ~( / 8    C9 ~ ~
                                                       /Jt:Z ./7'Zlc.iZcJ£L, so F = o. -J;;-r 3 G

[1263]

Peak Analysis Report 3/7/2018 1:07:44 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC027GD Peak Analysis Performed on: 3/7/2018 1 : 07: 44 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area uncert. Counts 1 113- 137 129.87 32.06 1. 84 7.31E+002 79.48 2.15E+002 2 296- 309 301.72 75.08 1.15 3.98E+002 126.53 1 .29E+003 3 1404- 1413 1408. 61 352.12 0.49 -5.42E+OOO 36.82 1 .51E+002 4 2633- 2657 2645.55 661.60 1. 87 5.58E+003 155.65 1 .16E+002 5 4679- 4702 4691. 03 1173. 10 1. 31 1.06E+002 25. 73 l .49E+001 6 5317- 5337 5327.02 1332.07 1. 35 1.17E+002 26.41 1 .58E+001 7 5831- 5852 5840.62 1460.42 1. 02 1. 37E+002 27 .42 1.44E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2. 000 sigma [1264]

Interference Corrected Activity Report 3/7/2018 1 : 07 :.44 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101ll0AFSWC027GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) uncertainty K-40 1.000 1460.82* 10.66 1. 68087E+006 3.67645E+005 Co-60 1 .000 11 73.23* 99.85 1.30111E+005 3.32270E+004 1332.49* 99.98 1.48911E+005 3.55976E+004 Cs-137 1. 000 661.66* 85.10 6.92775E+006 8.54137E+005 Pb-214 0 .445 295.22 18.42 351.93* 35.60 -l.34246E+004 9.12382E+004 

       * : Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold:            0. 30 Errors quoted at 2.000 sigma

[1265]

Interference Corrected Activity Report 3/7/2018 1:07:44 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Unc ertainty K-40 1.000 1.680865E+006 3.676446E+005 Co-60 1.000 1. 388641E+005 / 2.428989E+004 Cs-137 1.000 6. 927749E+006,/ 8.541373E+005 Pb-214 0.445 -1. 342458E+004 9.123821E+004 

      ?     Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2.000 sigma
  **********     U N I D E N T I F I E D         P E A K S      **********

Peak Locate Performed on: 3/7/2018 1:07:44 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.06 1.2177E+OOO 10.88 2 75.08 6.6382E-001 31.77 M ~ First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1266]

Nuclide MDA Report 3/7/2018 1 : 07: 44 PM Page 5

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSWC027GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL .NLB Nuclide Energy Yield Line MDA Nuc lide MDA Activity Dec. Level Name (keV) ( %) (pCi/M"'2 ) (pCi/M"'2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10 .66  3.235E+005   3.24E+005    1.681E+006    l.451E+005
 +      Co-60      1173.23*    99.85   3.442E+004   3.44E+004    1.301E+005    1 .555E+004 1332.49*    99.98   3.503E+004                1. 489E+005   1 .580E+004 Nb-94       702.65     99.81   3.792E+004   3.79E+004   4.300E+003     1.750E+004 8 7 1. 09  99.89   4.320E+004               2.577E+004     2.007E+004 Ag-108m     433.90     90.50  1.115E+005    4.39E+004   3.664E+004     5.435E+004 614.30     89.80   7.989E+004               7.444E+003     3.838E+004 722.90     90.80  4.391E+004                2.479E+004     2.034E+004 Cs-134      60 4 .72   97.62   7.215E+004   5.17E+004  -1.153E+004     3.464E+004 795.86     85.46   5.169E+004               5.329E+004v    2.410E+004
 +      Cs-137      66 1 .66*  85.10   9.284E+004   9.28E+004   6.928E+006     4.474E+004 Eu-152      12 1 .78   28.67   5.145E+005   2.15E+005   7.612E+005 /   2.538E+005 344.28     26.60  3.731E+005                2.448E+005     1.821E+005 1408.01     21. 07 2.147E+005                2.553E+005     9.905E+004 Eu-154      123.07     40.40  3.592E+005    1 .10E+005  1.979E+OOSJ    1. 772E+005 723.30     20.06  1. 936E+005               5.545E+002     8.950E+004
                 ' 1274 .43    34.80  1. 103E+005              -6.395E+004     5.029E+004 Eu-155        86.55    30.70  6.311E+005    6.31E+005   8.631E+005     3.119E+005 105.31     21.10  7.439E+005                1 .116E+005    3.671E+005 Tl-208      583.19     85. 00 7.716E+004    7.72E+004   5.105E+004     3.695E+004 Bi-212      727.33      6.67  5.777E+005    5.78E+OOS  -l.012E+005     2.669E+005 Pb-212      238.63     43.60  2.692E+005    2.69E+005   9.849E+004     l.322E+005 Bi-214      609.32     45.49  1 .628E+005   1 .63E+005  1.727E+005     7.834E+004 1120.29     14.92  3.376E+005                1.137E+005     l .578E+005 1764.49     15. 30 2.603E+005                2.770E+005     1.177E+005
 +      Pb-214      295.22     18.42  5.239E+005    l.58E+005  -2.499E+005     2.558E+005 351.93*    35.60  1.579E+005               -1 .342E+004    7.562E+004 Ra-226      186.21      3.64  3.323E+006    3.32E+006   2.403E+006     l.634E+006 Ac-228      338.32     11. 27 8.260E+005    l.77E+005  -9.021E+005     4 .025E+005 91 1. 20   25. 80 1.775E+005               -3.118E+004     8.272E+004 968.97     15 .80 3.363E+005                3.880E+005     1 .582E+005 Am-241       59.54     35.90  5.344E+005    5.34E+005  -1.684E+005     2.626E+005
       +=Nuclide identified during the nuclide i dentification
       *=Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1267]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/7/2018 1:29: 43 PM Sample Title B101110AFSWC028GD Sample Description Ul CTMT Sample Identification 028 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3 .00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO MA 2 Sample Taken On 3/7/2018 1:26:00 PM Acquisition Started 3/7/2018 1:19:40 PM Live Time 600 . 0 seconds Real Time 601.9 seconds Dead Time 0 .32 % Energy Calibration used Done On 1/13/2015 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1 .5M90DECP17 8CM [1268]

Peak Analysis Report 3/7/2018 1:29:43 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC028GD Peak Analysis Performed on: 3/7/2018 1:29:43 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area Uncert. Counts 1 113- 136 129.52 31.98 0 .96 4.75E+002 72.77 2.07E+002 2 286- 309 301 .04 74 . 91 1.25 8.95E+002 168.80 1.56E+003 3 331- 346 339.71 84.59 1. 02 1.62E+002 120.90 1.16E+003 4 482- 495 489.47 122.08 0 .77 1.48E+002 95.44 7.72E+002 5 786- 793 789.07 197.07 0 .69 3.36E+001 42.67 2.09E+002 6 1370- 1387 1376.70 344.14 1. 52 1.53E+002 51. 18 1. 52E+002 7 2426- 2442 2435.21 608.98 1. 12 6.76E+001 30. 02 5.04E+001 8 2632- 2656 2644.49 661.33 1. 49 3.13E+003 118.53 9.34E+001 9 3844- 3863 3853. 11 963.61 0 .65 8.lOE+OOl 25.97 2.50E+001 10 4334- 4348 4341.51 1085.72 0 .37 3.99E+001 20. 35 2.21E+001 11 4438- 4454 4445.16 1111 .63 1. 55 3.91E+001 22.20 2.69E+001 12 4679- 4699 4689.95 1172.83 1.48 1.39E+002 26.55 1.04E+001 13 5317- 5335 5326.19 1331.86 1. 40 1.29E+002 26.22 1.23E+001 14 5619- 5638 5628.79 1407.49 1. 79 1.03E+002 22.82 7.57E+OOO 15 5830- 5851 5840.29 1460.34 2.16 l.02E+002 26.22 1.87E+001 M c First peak in a mul tiplet region m = Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1269]

Interference Corrected Activity Report 3/7/2018 1: 29: 43 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC028GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * * *
  • I e * * * *
  • I * * *
  • I IDENTIFIED NUCLIDES . . .. . ........... .. ..

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M'.'2 ) Uncertainty K-40 1.000 1460.82* 10 .66 1. 25859E+006 3.40643E+OOS Co-60 1.000 11 73. 23* 99.85 1. 69952E+005 3. 52842E+004 1332.49* 99.98 1.63421E+005 3.57730E+004 Cs-137 1.000 661.66* 85 .10 3.88459E+006 4.89186E+005 Eu-152 1.000 121.78* 28.67 3.74358E+OOS 2.53337E+OOS 344.28* 26.60 5.02774E+005 1.87667E+005 1408.01* 21.07 6.35520E+005 1.49163E+005 Eu-155 0 .330 86.55* 30.70 4.43103E+005 3.41991E+005 105.31 21 .10 Bi-214 0.687 609.32* 45.49 1. 53907E+005 7.07592E+004 1120.29* 14.92 3.16717E+005 1 .81401E+005 1764.49 15.30 

          * ~ Energy line found in the spectrum.
          @ = Energy line not used for Weighted Mean Activity Energy Tolerance :                    10.000 keV Nuclide confidence index threshold~                          0.30 Errors quoted at 2. 000 sigma

[1270]

Interference Corrected Activity Report 3/7/2018 1:29:43 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1.000 1.258592E+006 3.406429E+005 Co-60 1.000 1 .667316E+005 J 2.512075E+004 Cs-137 1.000 3.884593E+006 ,/ 4.891865E+005 Eu-152 1.000 5.473686E+005 J 1. 060475E+005 Eu-155 0.330 4.431026E+005 3.419913E+005 Bi-214 0.687 1.754078E+005 6.592156E+004 X Pb-214 0 .383 

      ? = Nuclide is part of an undetermined solution x = Nuclide rejected by the interference analysis
      @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2.000 sigma

[1271]

Interference Corrected Activity Report 3/7/2018 1 :29:43 PM Page 5 

  **********      U N I D E N T I F I E D      P E A K S     **********

Peak Locate Performed on: 3/7/2018 1:29:43 PM Peak Locate From Channel : 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Pea k CPS Peak Tol. No. (keV) Counts per Second  % uncertainty Type Nuclide 1 31. 98 7.9113E - 001 15.33 2 74.91 1 .4916E+OOO 18 .86 5 197.07 5.6053E-002 126.87 Sum 9 963.61 1. 3500E-001 32.06 Tol. Ac-228 10 1085.72 6.6425E-002 51.06 M ~ First peak in a multiplet region m Other peak in a multiplet region F ~ Fitted singlet Errors quoted at 2. 000 sigma [1272]

Nuclide MDA Report 3/7/2018 1 :29:43 PM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSWC028GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) ( %) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10.66   3.710E+005    3.71E+OOS    1. 259E+006     1.689E+OOS
 +      Co-60      1173.23*    99.85   2.808E+004    2.81E+004    1 .700E+005     1.238E+004 1332.49*    99.98   3.089E+004                 l .634E+005     1.373E+004 Nb-94       702.65     99.81   4.415E+004    4.42E+004   -3.944E+004      2.062E+004 871. 09    99.89   4.961E+004                 3.511E+004      2.327E+004 Ag-108m     433.90     90.50   8.930E+004    5.27E+004   -5.075E+002      4.325E+004 614.30     89.80   7.642E+004                -5.995E+004      3.665E+004 722.90     90.80   5.274E+004                 1. 245E+O 04    2.476E+004 Cs-134      60 4 .72   97.62   6.947E+004    5. 5 7E+004  2. 3 2 9E+004.J 3.330E+004 795.86     85.46   5.567E+004                -1 .113E+003     2.608E+004
 +      Cs-137      661.66*    85.10   8.351E+004    8.35E+004    3.885E+006      4.007E+004
 +      Eu-152      12 1 .78*  28.67   3.918E+005    1.21E+OOS    3.744E+OOS      1.925E+OOS 344.28*    26.60   2.516E+005                 5.028E+005      1. 214E+OOS 140 8.01*   21.07   1. 212E+005                6.355E+005      5.231E+004 Eu-154      123.07     40.40   3.505E+005    1. 05E+OOS   5.979E+005J     1. 728E+OOS 723.30     20.06   2.359E+005                 5.656E+004      1. 107E+OOS 1274.43     34.80   1.046E+005                -4.926E+003      4.742E+004
 +      Eu-155       86.55*    30.70   5.386E+005    5.39E+OOS    4 .431E+005     2.656E+005 105.31     21. 10  6.946E+005                 l.887E+005      3.424E+005 Tl-208      583.19     85.00   7.346E+004    7.35E+004    1.610E+004      3.510E+004 Bi-212      727.33      6.67   7.316E+005    7.32E+005    2.515E+005      3.43BE+005 Pb-212      238.63     43.60   2.345E+005    2.35E+OOS    2.130E+005      1.148E+005
 +      Bi-214      609.32*    45.49   l.001E+005    1. 0 0E+OOS  1 .539E+005     4. 699E+004 112 0 .29*  14.92   2.660E+005                 3.167E+005      1. 220E+005 1764.49     15. 30  2.310E+005                 2.124E+005      1.030E+005 Pb-214      295.22     18.42   4. 577E+005   1. 88E+OOS   7.429E+004      2.227E+005 35 1 .93*  35.60   1.880E+005                 3.757E+005      9.068E+004 Ra-226      186.21      3.64   2.934E+006    2.93E+006    9.916E+005      1 .440E+006 Ac-228      338.32     11.27   7.554E+005    2.03E+005   -2.014E+005      3.672E+005 91 1. 20   25 . 80 2.027E+005                 1. 551E+O OS    9.533E+004 968.97     15.80   4.259E+005                -4.641E+004      2.030E+005 Am-241       59.54     35.90   5.254E+005    5.25E+005   -1.716E+005      2.581E+005
       +=Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1273]

          • GAMM A S P E C T R U M A N A L Y S I S *****

Filename : 5452 Report Generated On 3/7/2018 2:02:57 PM Sample Title B101110AFSWC029GD Sample Description Ul CTMT Sample Identification 029 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7. 070E+OOO M"'2 Sample Taken On 3/7/2018 1 :52: 00 PM Acquisition Started 3/7/2018 1 :52:54 PM Live Time 600 . 0 seconds Real Time 601.9 seconds Dead Time 0 . 32 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1.5M90DECP17 8CM [1274]

Peak Analysis Report 3/7/2018 2 : 02:57 PM Page 2

          • PE AK A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

Bl01110AFSWC029GD Peak Analysis Performed on: 3/7/2018 2:02:57 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 135 128.54 31.73 1. 56 5.40E+002 70.85 1. 85E+002 2 286- 306 300 .89 74.88 1. 54 9.81E+002 156.80 1. 42E+003 3 332- 345 339.18 84.46 1.17 3.18E+002 113. 11 l. 04E+003 4 483- 495 487.83 121.67 1. 01 2.19E+002 91. 81 7.14E+002 5 545- 558 549.89 137.21 0 .49 S.37E+001 83.75 6.16E+002 6 1368- 1384 1376.12 343.99 1. 61 l .84E+002 54.46 1. 78E+002 7 2427- 2442 2434.58 608.82 0 .58 5.86E+001 32.23 6.64E+001 8 2632- 2656 2644.69 661 .38 1. 54 2.64E+003 109.16 8.llE+OOl 9 3106- 3119 3112.50 778.40 0 .82 4.73E+001 24.35 3.67E+001 10 3346- 3357 3351. 28 838.11 0 .54 1.26E+001 10.98 6.42E+OOO 11 3843- 3862 3853.71 963.76 0 .86 8.56E+001 29.42 3.74E+001 12 4332- 4348 4339.83 1085.30 0 .45 6.89E+001 19.36 8.07E+OOO 13 4436- 4452 4444.81 1111.54 0 .65 6.35E+001 23.93 2.55E+001 14 4679- 4699 4689.95 1172.83 0 .39 1 .33E+002 29.45 2.33E+001 15 5317- 5337 5326. 00 1331. 81 2.06 1 .59E+002 28.37 1.21E+001 16 5618- 5640 5629.03 1407.55 2.20 1 .52E+002 28.96 1.46E+001 17 5831- 5849 58 40.12 1460.30 0 .40 1.17E+002 29.30 2.89E+001 18 7049- 7062 7055. 03 1763.83 0 .28 1.79E+001 10.32 3.lOE+OOO M ; First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1275]

Interference Corrected Activity Report 3/7/2018 2:02:57 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSWC029GD Nuclide Library used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * * * * * * * * * * * *
  • I * *
  • IDENTIFIED NUCLIDES . . . . .......... . ......

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/MA2 ) uncertainty K-40 1 .000 1460.82* 10.66 l .44078E+006 3.81645E+005 Co-60 1 .000 11 73.23* 99.85 1.62715E+OOS 3.83924E+004 1332.49* 99.98 2.01757E+005 3.94849E+004 Cs-137 1.000 661.66* 85. 10 3.28385E+006 4.17021E+005 Eu-152 1.000 121.78* 28.67 5.55603E+005 2.58232E+005 344.28* 26.60 6.04707E+005 2.04967E+005 1408.01* 21. 07 9.36695E+005 1 .93078E+005 Eu-155 0.330 86.55* 30.70 8.69347E+005 3.54988E+005 105.31 21. 10 Bi-214 0.976 609.32* 45.49 1.33358E+005 7.50514E+004 11 20.29* 14.92 5.13873E+005 1.97999E+005 1764.49* 15.30 1. 65315E+005 9.61716E+004 

          *=Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                    10.000 keV Nuclide confidence index threshold ~                         0.30 Errors quoted at 2.000 sigma

[1276]

Interference Corrected Activity Report 3/7/2018 2:02:57 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1. 000 1. 440782E+006 3.816454E+005 Co-60 1.000 1. 816886E+005 ./ 2.752564E+004 Cs-137 1.000 3.283853E+006 .r 4.170211E+005 Eu-152 1.000 7.291909E+OOS,1' 1.234437E+005 Eu-155 0.330 8.693473E+005 3.549878E+005 Bi-214 0.976 1.756552E+005 5.669001E+004 X Pb-214 0.381 

      ? = Nuclide is part of an undetermined solution X - Nuclide rejected by the interference analysis
      @ ~ Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2.000 sigma

[1277]

Interference Corrected Activity Report 3/7/2018 2:02:57 PM Page 5 

  **********     UN I D E N T I F I E D       P E A K S     **********

Peak Locate Performed on: 3/7/2018 2:02:57 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 73 8.9919E-001 13.13 2 74.88 1 .6353E+OOO 15.98 5 137.21 8.9530E-002 155.90 9 778.40 7.8810E-002 51. 50 Sum 10 838 .11 2.0965E-002 87.30 11 963.76 1. 4272E-001 34.36 12 1085.30 l.1489E-001 28.09 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1278]

Nuclide MDA Report 3/7/2018 2:02:57 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSWC029GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*     10.66   4 .332E+005   4.33E+005   1.441E+006     1 .999E+005
 +      Co-60      1173.23*     99.85   4.034E+004    3.06E+004   1.627E+005     1.851E+004 1332.49*     99.98   3.065E+004                2.018E+005     1.361E+004 Nb-94        702.65     99.81   5.440E+004    5.44E+004  -2.776E+004     2.575E+004 87 1. 09   99.89   5.681E+004               -8.576E+003     2.687E+004 Ag-108m      43 3 .90   90.50   9.209E+004    5.24E+004   1.085E+003     4.464E+004 614.30     89.80   8.119E+004               -7.828E+003     3.903E+004 722.90     90.80   5.243E+004               -3.506E+004     2.461E+004 Cs-134       604.72     97.62   7.091E+004    6. 10E+004  1.32 3 E+004 J 3.402E+004 795.86     85.46   6.097E+004               -4.305E+004     2.873E+004
 +      Cs-137       661.66*    85.10   7.817E+004    7.82E+004   3.284E+006     3.740E+004
 +      Eu- 152      12 1. 78*  28.67   3.697E+OOS    1.70E+005   5.556E+005     1.814E+OOS 344.28*    26.60   2.647E+005                6.047E+005     1 .279E+005 1408 .01*    21. 07  1. 695E+005               9.367E+005     7.645E+004 Eu- 154      123.07     40.40   3.584E+005    1.lOE+OOS   3.506E+005v    l .768E+005 723.30     20.06   2.388E+005               -2.390E+005     1.121E+005 1274.43      34.80   1. 103E+005               5.855E+003     5.029E+004
 +      Eu-155        86.55*    30.70   4.906E+005    4.91E+005   8.693E+005     2.416E+005 105.31     21.10   7.389E+005                3.593E+005     3.646E+OOS Tl-208       583.19     85. 00  7.413E+004    7.41E+004   6.937E+004     3.544E+004 Bi-212       727.33      6.67   7.796E+005    7.80E+005   9.023E+005     3.679E+OOS Pb-212       238.63     43.60   2.296E+005    2.30E+OOS  -1.019E+005     l. 124E+OOS
 +      Bi-214       609.32*    45.49   1. 123E+005   1.12E+OOS   1.334E+005     5.306E+004 1120.29*     14.92   2.596E+005                5.139E+005     1. 188E+005 1764.49*     15. 30  1. 146E+005               1 .653E+005    4.481E+004 Pb-214       295.22     18.42   4.710E+005    1.98E+005   2.167E+005     2.294E+005 351.93*    35.60   1.977E+005                4.518E+005     9.555E+004 Ra-226       186.21      3.64   2.971E+006    2.97E+006   5.117E+OOS     1.459E+006 Ac-228       338.32     11.27   6.986E+005    2.39E+005  -3.693E+005     3.388E+005 911. 20    25.80   2.386E+005                2.315E+005     1.133E+005 968.97     15 . 80 4 .317E+005               l.124E+OOS     2.059E+OOS Am-241        59.54     35.90   5.493E+005    5.49E+005   2.380E+005     2.701E+OOS
       + =Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       > - Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1279]

          • GAMM A S P E C T R U M ANALYSIS *****

Filename: 5452 Report Generated On 3/7/2018 2:23:20 PM Sample Title B101110AFSWC030GD Sample Description Ul CTMT Sample Identification 030 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO M"'2 Sample Taken On 3/7/2018 2:19:00 PM Acquisition Started 3/7/2018 2:13:17 PM Live Time 600.0 seconds Real Time 602.0 seconds Dead Time 0.33 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID l .SM90DECP17 8CM [1280]

Peak Analysis Report 3/7/2018 2:23:20 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC030GD Peak Analysis Performed on: 3/7/2018 2:23:20 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV) Area Uncert. Counts 1 113- 134 129.37 31.94 1. 75 5.90E+002 75.73 2.20E+002 2 154- 165 161.22 39.91 0.55 3.51E+001 56.29 3.01E+002 3 284 - 308 301.15 74.94 1. 35 1.08E+003 179.03 1 .68E+003 4 334- 346 340.12 84.70 1. 04 2.BOE+002 106.99 9.80E+002 5 364 - 375 371.89 92.65 0 .73 5.83E+001 91.18 8.07E+002 6 481- 496 488.18 121.76 0 .88 1 .91E+002 109.94 9.43E+002 7 1371- 1386 1376.33 344.04 1. 43 1.36E+002 50. 11 1.62E+002 8 1401- 1413 1406.60 351.62 0 .62 2.73E+001 41. 31 1.52E+002 9 2426 - 2442 24 34 .29 608.75 1. 08 6.20E+001 29.76 5.lOE+OOl 10 2632- 2656 26 44 .60 661.36 1.71 3.39E+003 123.21 9.94E+001 11 3102 - 3121 3112.98 778.52 0.83 6.55E+001 26.77 3.25E+001 12 4437 - 4453 44 44 .57 1111.48 0.83 6.20E+001 23.13 2.30E+001 13 4681- 4700 4689.69 1172.76 1. 60 1.51E+002 31. 88 3.0lE+OOl 14 5316- 5337 5326.06 1331.83 1. so 1. 55E+002 29.05 1. 54E+001 15 5619- 5639 5628.69 1407.46 0 .39 l. 07E+002 23.61 9.40E+OOO 16 5830- 5850 5839.35 1460. 11 1. 96 1. 36E+002 26.81 1. 25E+001 M First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1281]

Interference Corrected Activity Report 3/7/2018 2:23:20 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC030GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB 

  . ...... .... ..... .... .. IDENTIFIED NUCLIDES             . ....... ....... ....... . .

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M"2 ) Uncertainty K-40 0.999 1460.82* 10.66 1 .66761E+006 3.60290E+005 Co-60 0.999 1173.23* 99.85 1 .85054E+005 4.18017E+004 1332.49* 99.98 1.96277E+005 4.00910E+004 Cs-137 1 .000 661.66* 85 .. 10 4.20506E+006 5.27672E+005 Eu-152 1.000 1 21.78* 28.67 4.85245E+005 2.95415E+005 344.28* 26.60 4.48175E+005 1 .80656E+005 1408. 01* 21.07 6.55042E+005 1 .54238E+005 Eu-155 0.331 86.55* 30.70 7.64162E+005 3.29545E+005 105.31 21. 10 Bi-214 0.686 609.32* 45.49 1. 41043E+005 6.97856E+004 1120.29* 14 .92 5.02084E+005 1.91420E+005 1764.49 15.30 Pb-214 0.445 295.22 18.42 351.93* 35.60 6.76092E+004 1 .02861E+005 

       * ~ Energy line found in the spectrum.
       @ ~ Energy line not used for Weighted Mean Activity Energy Tolerance :           10.000 keV Nuclide confidence index threshold =                 0.30 Errors quoted at 2.000 sigma

[1282]

Interference Corrected Activity Report 3/7/2018 2:23:20 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 0.999 1.667608E+006 3.602899E+005 Co-60 0.999 1. 908998E+005 v,. 2.893451E+004 Cs-137 1. 000 4. 2 05056E+006 " 5.276715E+005 Eu-152 1. 000 5.565789E+005 v 1. 090216E+D05 Eu-155 0.331 7.641622E+005 3.295455E+005 Bi-214 0.686 1.833991E+005 6.556442E+004 Pb-214 0.445 6.760921E+004 1. 028609E+005 

      ?    Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1283]

Interference Corrected Activity Report 3/7/2018 2:23:20 PM Page 5 

  **********    U N I D E N T I F I E D      P E A K S     **********

Peak Locate Performed on: 3/7/2018 2:23:20 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31 .94 9.8285E-001 12.84 2 39.91 5.8560E-002 160.21 3 74.94 1.8012E+OOO 16.57 5 92.65 9.7196E-002 156.35 D-Esc. 11 778.52 1 .0923E-001 40 .84 Sum M ~ First peak in a multiplet region m : Other peak in a multiplet region F ~ Fitted singlet Errors quoted at 2 . 000 sigma [1284]

Nuclide MDA Report 3/7/2018 2:23:20 PM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSWC030GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/M"2 ) (pCi/M"2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10 .66  3.024E+005    3.02E+005     1.668E+006   l.346E+005
 +      Co-60      1173.23*    99.85   4.430E+004    3.48E+004     1.851E+005   2.049E+004 1332.49*    99.98   3.481E+004                  1.963E+005   1.569E+004 Nb-94       702.65     99.81   5.140E+004    5.02E+004     9.517E+003   2.424E+004 87 1 . 09  99.89   5.020E+004                  2.564E+004   2.357E+004 Ag-108m     433.90     90.50   9.516E+004    5.89E+D04     8.662E+004   4.618E+004 614.30     89.80   7.463E+004                 -1 .862E+OD4  3.575E+004 722.90     90.80   5.886E+004                  1 .972E+004  2.782E+004 Cs-134      604.72     97.62   7.180E+004    5.53E+004    -6.450E+003   3.447E+004 795.86     85.46   5.532E+004       o.oc~~O*/ -2.869E+OD3   2.591E+004
 +      Cs-137      661.66*    85.10   8.605E+004    8.61E+004     4.205E+006   4.135E+004
 +      Eu-152      121.78*    28.67   4.510E+005    1.32E+005     4.852E+005   2.221E+005 344.28*    26.60   2.490E+OOS                  4.482E+OOS   l.201E+OOS 1408.01*    21.07   1.323E+005                  6.5SOE+005   5.783E+004 Eu-154      123.07     40.40   3.641E+005    1 .1 3E+005   5.289E+005 v 1.796E+005 723.30     20.06   2.627E+OOS                  4. 310E+D04  1 .241E+005 1274 .43    34.80   1.131E+005                  3.783E+004   5.167E+004
 +      Eu-155       86.55*    30.70   4.636E+005    4.64E+OD5     7.642E+005   2.281E+005 10 5. 31   21. 10  7.514E+005                  7.300E+D05   3.708E+005 Tl-208      583.19     85. 00  7.301E+004    7.30E+004     8.021E+002   3.488E+004 Bi-212      727.33      6.67   7.398E+005    7.4DE+005     4.962E+004   3.480E+005 Pb-212      238.63     43.60   2.411E+005    2.41E+005    -8.765E+004   1.181E+005
 +      Bi-214      609.32*    45.49   l .006E+OOS   1 .01E+OD5    l.410E+OOS   4.724E+004 1120.29*    14.92   2.473E+005                  5.021E+005   1.127E+005 1764.49     15.30   1.969E+005                  1.478E+OOS   8.593E+004
 +      Pb-214      295.22     18.42   4.863E+005    1.69E+005     2.491E+005   2.370E+005 351.93*    35.60   l.695E+005                  6.761E+004   8.140E+004 Ra-226      186.21      3.64   3.105E+006    3. 1 1E+D06   4.911E+OOS   1.526E+006 Ac-228      338.32     11. 27  7.668E+005    2.27E+005    -1. D22E+006  3.729E+005 91 1 .20   25.80   2.269E+005                  1.533E+OOS   1. 075E+005 968.97     15.80   4.096E+005                  4. 383E+004  1.948E+005 Am-241       59.54     35.90   5.591E+005    5.59E+005    -2.859E+005   2.750E+005
       + ; Nuclide identified during the nuclide i dentification
       * = Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ - Half-life too short to be able to perform the decay correction

[1285]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002537.CNF Report Generated On 3/8/2018 5:03:29 PM Sample Title B101110AFSWC031GD Sample Description Ul CTMT Sample Identification 031 Sample Type GAMMA DIRECT Sample Geometry 1. 5M9 OD ECP 1 7 . 8 Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO MA2 Sample Taken On 3/8/2018 9:11:00 PM Acquisition Started 3/8/2018 9:12:37 AM Live Time 600. 0 seconds Real Time 601.5 seconds Dead Time 0 .25 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1.5M90DECP17 8CM [1286]

Peak Analysis Report 3/8/2018 5: 03: 29 PM Page 2

          • PE AK A N A L Y S I S REPORT *****

Detector Name: 5452 Sample

Title:

B1 01110AFSWC031GD Peak Analysis Performed on: 3/8/2018 5:03:28 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 151 129.60 32. 00 1.43 7.13E+002 119.88 4.60E+002 2 296- 308 300.90 74.88 0.87 2.53E+002 100.24 8.40E+002 3 332- 347 3 40. 62 84.82 1. 06 1.03E+002 104.92 8.82E+002 4 1404- 1414 1409.19 352.27 0.36 3.98E+001 36.13 1.20E+002 5 2635- 2660 2647.89 662.18 1. 54 4.81E+003 144.15 9.24E+001 6 4685- 4704 4695.59 1174.24 2.02 l.34E+002 25.23 7.28E+OOO 7 5324- 5344 5332.71 1333.49 0.42 l. 16E+002 23.24 5.2SE+OOO 8 5839- 5857 5846.18 1461.81 0.93 9.25E+001 24.20 1 .6SE+001 M = First peak in a mu ltiplet region m = Other peak in a multiplet region F : ; Fitted singlet Errors quoted at 2. 000 sigma [1287]

Interference Corrected Activity Report 3/8/2018 S: 03: 29 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSWC031GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB I * * * * ,.. . * * * * * * "' * * * * * * .. IDENTIFIED NUCLIDES *

  • 1 * *- * * * * * * * * * * *
  • 11 *
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 0 .998 1460.82* 10 .66 1. 13872E+006 3.13856E+005 Co-60 0 .998 1173.23* 99.85 l.63999E+005 3.36068E+004 1332.49* 99.98 l.47032E+005 3.17793E+004 Cs-137 1. 000 661.66* 85.10 S.97172E+006 7.38918E+005 Eu-155 0 .331 86.55* 30.70 2.79841E+005 2.91280E+005 105.31 21.10 Pb-214 0 .445 295.22 18.42 351.93* 35.60 9.86158E+004 9.08892E+004
          * ~ Energy line found in the spectrum.
          @~Energy line not used for Weighted Mean Activity Energy Tolerance :                           10.000 keV Nuclide confidence index threshold =                               0.30 Errors quoted at 2.000 sigma

[1288]

Interference Corrected Activity Report 3/8/20 18 5:03:29 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"'2 ) Uncertainty K-40 0.998 l.138722E+006 3.138564E+OOS Co-60 0.998 1 . 550418E+OOS .r 2.309039E+004 Cs-137 1.000 5. 9 71716E+006../ 7.389179E+005 Eu-155 0 .331 2.79841SE+005 2.912798E+OOS Pb-214 0 .445 9.861576E+004 9.088916E+004 

      ?
         -  Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2. 000 sigma
  **********     U N I D E N T I F I E D          P E A K S     **********

Peak Locate Performed on: 3/8/2018 5: 03: 28 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.00 1.1879E+OOO 16.82 2 74.88 4.2145E-001 39.64 M ~ First peak in a multiplet region m ~ Other peak in a multiplet region F = Fitted singlet Errors quoted at 2. 000 sigma [1289]

Nuclide MDA Report 3/8/2018 5:03:29 PM Page 5

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 1.5M90D ECP 17.8 Sample

Title:

B101110AFSWC031GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) (%) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       1460 .82*   10 .66  3.306E+005   3.31E+005         l.139E+006    l.486E+005
 +      Co-60      1173.23*    99.85   2.365E+004   2 .1 8E+004       1.640E+OOS    1 .017E+004 1332.49*    99.98  2.179E+004                      l.470E+005    9.177E+003 Nb-94        702.65    99.81   3.608E+004   3.60E+004 2.559E+003            1.659E+004 871.09    99.89  3.597E+004                    -1. 472E+004    1 .645E+004 Ag-108m      433.90    90.50   9.888E+004   3.78E+004 7.761E+004            4.803E+004 614 .30   89.80   7.110E+004                     3.910E+004    3.399E+004 722 . 90  90.80  3.780E+004                    -7.628E+001     1.729E+004 Cs-134       604.72    97.62  6.151E+004    3.70E+004 -1.130E+005           2.932E+004 795.86    85.46  3.703E+004          ~.coe ~ 6/- 8. 422E+O 03 1.676E+004
 +      Cs-137       661.66*   85.10  8.389E+004    8.39E+004 5.972E+006            4 .026E+004 Eu-152       121 . 78  28.67  4.379E+005    1. 44E+O O5 3. 523E+O 05,:      2.155E+005 344.28    26.60  3.240E+005                      2.498E+D05   1.575E+005 1408.01     21.07  1.445E+005                      7.889E+D04    6.393E+004 Eu-154       123.07    40.40  3.111E+005    9.36E+D04 9.363E+004J          1 .531E+005 723.30    20.06  1 .711E+005                    2.828E+004     7.825E+004 1274.43     34.80  9.356E+004                      3.397E+004   4.190E+004
 +      Eu-155        86.55*   30.70  4.687E+005   4 .69E+005 2.798E+005           2.307E+005 105.31    21.10  6.185E+OOS                    -1. 389E+005   3.044E+005 Tl-208       583.19    85.00  6.763E+004   6.76E+004 4.895E+004            3.219E+004 Bi-212       727.33     6.67  5.559E+005   5.56E+005 1.927E+OOS            2.560E+005 Pb-212       238.63    43.60  2.322E+OOS   2.32E+005 8.290E+004            1. 137E+005 Bi-214       609.32    45.49  1. 375E+005  1.38E+OOS 5.713E+004            6.569E+004 1120.29     14.92  2.860E+005                    -l.277E+OOS    l.321E+005 1764.49     15.30  2.603E+005                     1 .895E+OOS   1.177E+005
+       Pb-214       295.22    18.42  4.720E+005   l.45E+005 -2.271E+005           2.299E+005 351.93*   35.60  1.447E+005                     9.862E+004    6.898E+004 Ra-226      186.21      3.64  2.911E+006   2.91E+006 -4.160E+005           l.428E+006 Ac-228      338.32     11. 27 7.330E+005   l .72E+005 -6.759E+005          3.561E+OOS 911. 20   25.80  l .722E+005                    8.731E+004    8.009E+D04 968.97     15.80  2.6SOE+005                     2.449E+005    l.225E+OOS Am-241        59.54    35.90  4.752E+005   4 .75E+OOS -2.179E+OOS          2.330E+005
       + - Nuclide identified during the nuclide identification
       * ~ Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
      @ ~ Half-life too short to be able to perform the decay correction

[1290]

          • GAMM A S P E C T R U M ANALYSIS *****

Filename: C:\GENIE2K\CAMFILES\00002538.CNF Report Generated On 3/8/2018 5:22:12 PM Sample Title B101110AFSWC032GD Sample Description Ul CTMT Sample Identification 032 Sample Type GAMMA DIRECT Sample Geometry 1.SM90D ECP 17.8 Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO M"2 Sample Taken On 3/8/2018 9:34:00 PM Acquisition Started 3/8/2018 9:28:37 AM Live Time 600 . 0 seconds Real Time 602.2 seconds Dead Time 0 . 37 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1 .5M90DECP17 8CM [1291]

~eak Analysis Report 3/8/2018 5:22:12 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC032GD Peak Analysis Performed on: 3/8/2018 5:22:12 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 136 129.49 31.97 1. so 9.70E+002 88.22 2.57E+002 2 208- 216 212.67 52.79 0.27 -2.46E+001 52.61 3.32E+002 3 284- 307 301.88 75.12 1. 50 1. 00E+ 003 179.70 1. 77E+003 4 336- 346 3 40 .45 84.78 1. 16 2.63E+002 98.15 8.96E+002 5 470- 477 473.45 118.07 0 .52 2.77E+001 64.53 5.02E+002 6 2429- 2443 2438.28 609.75 0.40 5.39E+001 31.62 6.81E+001 7 2635- 2660 2647.87 662.18 1. 60 1 .06E+004 211. 76 1 .39E+002 8 4685- 4706 4695.45 1174.20 1. 64 1.22E+002 27.09 1.65E+001 9 5324- 5343 5333. 17 1333.60 0.94 1.09E+002 24.50 1.19E+001 10 5837- 5858 5847.33 1462.10 1. 98 1 .37E+002 26. 54 1.05E+001 M .,,._ First peak in a multiplet region m = Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1292]

~nterference Corrected Activity Report 3/8/2018 5:22:12 PM Page 3

          • NU CL .IDE I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC032GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  ' . . . . .. . . . . . . . . . . . ~ .. IDENTIFIED NUCLIDES            . . . . . . . . . . . . . . . "' ' *
  • i, **

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 0 .997 1460.82* 10 .66 1 .69253E+006 3.58201E+005 Co-60 0 .998 1173.23* 99.85 1. 4 9007E+O 05 3.52960E+004 1332.49* 99.98 1.38598E+005 3.30333E+004 Cs-137 1 . 000 661.66* 85.10 1. 32050E+007 1 .60691E+006 Eu- 155 0 .331 86.55* 30.70 7.16332E+OOS 3.D3467E+OOS 105.31 21. 10 Bi-214 0.405 609.32* 45.49 1.22573E+005 7.34513E+004 1120.29 14.92 1764.49 15. 30 Am-241 0 .930 59.54* 35.90 -8.32797E+004 1 .78904E+OOS 

         *=Energy line found in the spectrum.
         @=Energy line not used for Weighted Mean Activity Energy Tolerance :                     10.000 kev Nuclide confidence index threshold=                           0.30 Errors quoted at 2.000 sigma

[1293]

Interference Corrected Activity Report 3/8/2018 5:22:12 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"'2 ) Uncertainty K-40 0 .997 1.692533E+006 3.582006E+005 Co-60 0.998 1 . 434583E+oos., 2. 4l l835E+OD4 Cs-137 1.000 1.320502E+007..t 1.606911E+006 Eu-155 0.331 7.16331BE+005 3.034675E+OOS Bi-214 0.405 l .225733E+005 7.345126E+004 Am-241 0.930 -8.327968E+004 1.789044E+OOS 

      ? ~ Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2.000 sigma

[1294]

Interference Corrected Activity Report 3/8/2018 5:22:12 PM Page s 

  **********    UN I D E N T I F I E D       P E A K S    **********

Peak Locate Performed on: 3/8/2018 5:22:12 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 97 1 .6170E+OOO 9.09 3 75.12 1.6726E+OOO 17.91 5 118.07 4.6135E-002 233 .11 M = First peak in a multiplet region m - Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1295]

Nuclide MDA Report 3/8/2018 5: 22: 12 PM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: 1.5M90D ECP 17.8 Sample

Title:

B101110AFSWC032GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/M ... 2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +       K-40       1460.82*   10.66  2.848E+005       2.BSE+OOS    1.693E+006     l .257E+005
 +      Co-60       117 3.23*  99.85  3.508E+004       3.02E+004    1. 490E+OOS    l .588E+004 1332.49*   99.98  3.017E+004                    1.386E+005    1.336E+OD4 Nb-94        702.65    99.81  4 .067E+004      4.07E+004    6.808E+003    1.888E+004 87 1 .09  99.89  4.070E+004                    4.653E+003    1.882E+004 Ag-108m      433.90    90.50  l.280E+005       4.39E+004   -8.446E+004    6.262E+D04 614.30    89.80  8.827E+004                   -8.695E+004    4.257E+D04 722.90    90.80  4.391E+004                   -4.639E+003    2.034E+004 Cs-134       60 4 .72  97.62  7.316E+004       4.73E+004    4.231E+003-1  3.515E+004 795.86    85. 46 4.734E+004                    3.430E+004    2.192E+004
 +      Cs-137       661.66*   85. 10 1.020E+005       1.02E+005    1.321E+007    4.932E+D04 Eu-152       121. 78   28.67  5.193E+005       1.81E+005    2.418E+004""  2.562E+005 344.28    26.60  4.133E+OOS                    1. SOlE+OOS   2.022E+OOS 1408.01     21.07  1.809E+005                    1.183E+005    8.212E+004 Eu-154       123.07    40.40  3.673E+005       8.28E+004    2. 700E+OOS/  1 .812E+005 723.30    20.06  2.004E+OOS                  -1. 874E+005    9.293E+004 1274 . 43   34.80  8.281E+004                  -4.930E+003     3.653E+OD4
 +      Eu-155        86.55*   30.70  4.227E+005       4.23E+005    7.163E+005    2.077E+005 105.31    21.10  7.680E+005                  -1.954E+005     3.791E+005 Tl-208       583.19    85.00  8.579E+004       8.58E+004    1 .718E+004   4.127E+OD4 Bi-212       727.33     6.67  5.882E+005       5.88E+005  -1. 562E+O 05   2.722E+D05 Pb-212       238.63    43.60  2.954E+005       2.95E+005    5.782E+004    1.453E+005
 +      Bi-214       609.32*   45.49  1. llOE+O 05     1.11E+005    1. 226E+005   5.242E+004 1120.29     14.92  3.465E+005                  -1 .152E+005    1. 623E+005 1764.49     15.30  2.310E+005                    2.124E+OOS    1. 030E+005 Pb-214       295.22    18.42  6.181E+005      3. 1 3E+005 -2.027E+OOS     3.029E+005 351.93    35.60  3.131E+OOS                    5.463E+004    l.532E+OOS Ra-226       186.21     3.64  3.775E+006      3.78E+006   -1.464E+OOS     1.861E+006 Ac-228       338.32    11. 27 9.657E+005      1 .60E+005    1. 8 70E+O 05 4.724E+005 911. 20   25.80  1. 597E+005                   4.196E+004    7.384E+004 968.97    15.80  2.835E+005                    2.073E+005    1 .318E+OOS
+       Am-241        59.54*   35.90  3.073E+005      3. 0 7E+005 -8.328E+004     1.491E+D05
       + - Nuclide identified during the nuclide i dentification
       * : Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
      @=Half-life too short to be able to perform the decay correction

[1296]

          • GAMM A S P E C T R U M ANALYSIS *****

Filename: C:\GENIE2K\CAMFILES\00002539.CNF Report Generated On 3/8/2018 5:26:34 PM Sample Title B101110AFSWC033GD Sample Description Ul CTMT Sample Identification 033 Sample Type GAMMA DIRECT Sample Geometry 1.5M90D ECP 17.8 Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO MA2 Sample Taken On 3/8/2018 9:41:00 PM Acquisition Started 3/8/2018 9:44:36 AM Live Time 600 - 0 seconds Real Time 601.5 seconds Dead Time 0.26 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1.5M90DECP17 8CM Va (;*~(e: {e c( 119..? [1297]

Peak Analysis Report 3/8/2018 5: 26: 34 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

Bl01110AFSWC033GD Peak Analysis Performed on: 3/8/2018 5:26:33 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 136 129.54 31.98 1.29 4.48E+002 69 .14 l. 90E+002 2 241- 248 244.88 60.85 0.44 -1. 64E+001 52.16 3.40E+002 3 285- 306 3 01. 92 75.13 1.26 8.17E+002 148.62 l.25E+003 4 333- 348 340 .85 84.88 0 .83 9.19E+001 115.79 1.08E+003 5 1373- 1383 1378.31 344.54 1.07 3.49E+001 32.69 9.71E+001 6 1400- 1419 1408.60 352.12 0.67 8.24E+001 51.16 l .63E+002 7 2431- 2444 2438.62 609.83 0.36 4.13E+001 23.30 3.37E+001 8 2635- 2660 2647.86 662.18 1. 68 3.74E+003 126.15 5.74E+001 9 4687- 4702 4694.31 1173.92 0.69 5.83E+001 19.38 l.17E+001 10 5323- 5342 53 31. 78 1333.26 0.33 7.97E+001 20.49 7.30E+OOO 11 5628- 5641 5634.33 1408.87 1. 05 3.60E+001 15.23 8.02E+OOO 12 5837- 5857 5846.62 1461.92 1. 59 l. 36E+002 24.73 4.82E+OOO M = First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1298]

Interference Corrected Activity Report 3/8/2018 5: 26: 34 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

Bl01110AFSWC033GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 0. 998 1460.82* 10 .66 1 .67634E+006 3.37381E+005 Co-60 0.999 11 73.23* 99.85 7.15115E+004 2.44436E+004 1332.49* 99.98 1.01227E+005 2.72590E+004 Cs-137 1. 000 661.66* 85.10 4.64357E+006 5.79064E+005 Eu-152 0 .332 121 . 78 28.67 344.28* 26. 6-0 1.14942E+005 1.09301E+005 14 08.01* 21. 07 2.21166E+005 9.52458E+004 Eu-155 0 .331 86.55* 30.70 2.50324E+005 3.19205E+005 105.31 21.10 Bi-214 0 .405 609.32* 45.49 9 . 39954E+004 5.42111E+004 112 0.29 14 .92 1764.49 15. 3 0 Pb-214 0.445 295.22 18.42 351.93* 35.60 2.04068E+005 1.30876E+005 Am-241 0.997 59.54* 35.90 -5.36414 E+004 1. 71454E+005 

       *=Energy line found in the spectrum.
       @=Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuclide confidence index threshold=             0 .30 Errors quoted at 2. 000 sigma

[1299]

Interference Corrected Activity Report 3/8/2018 5:26:34 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 0.998 1.676342E+006 3.373806E+005 Co-60 0 .999 8.475609E+004 1 .819847E+D04.J Cs-137 1.000 4.643573E+006 5.790638E+005./ Eu-152 0.332 1.753188E+005 7.180743E+004 Eu-155 0.331 2.503244E+005 3.192047E+OD5 Bi-214 0.405 9.399538E+004 5.421115E+004 Pb-214 0.445 2.040677E+005 1.308755E+005 Am-241 0.997 -5.364139E+004 1.714541E+OD5 

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2.000 sigma

[1300]

Interference Corrected Activity Report 3/8/20 18 5:26:34 PM Page s 

  **********    U N I D E N T I F I E D      P  EA   K S  **********

Peak Locate Performed on: 3/8/2018 5: 26: 33 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31.98 7.4653E-001 15.44 3 75.13 1.3609E+OOO 18.20 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singl et Errors quoted at 2 . 000 sigma [1301]

Nuclide MDA Report 3/8/2018 5:26:34 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 1. 5M9 OD ECP 1 7 . 8 Sample

Title:

B10l110AFSWC033GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) ( %) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       1460.82*   10.66    l.986E+005     l.99E+005                  1.676E+006    8.265E+004
 +      Co-60      1173.23*   99.85    2.738E+004     2.44E+004                  7.151E+004    1.203E+004 1332.49*   99.98    2.445E+004                                1. 012E+O 05  1. 051E+O 04 Nb-94        702.65   99.81    3.756E+004     3.76E+004                 -8.868E+003    1 .733E+OD4 871.09   99.89    3.802E+004                                8.16DE+003    1 .748E+004 Ag-108m      433.90   90.50    8.822E+004     4. 4 3E+004                4.087E+004   4.270E+004 614.30   89.80    7.237E+004                                2.076E+004   3.462E+OD4 722.90   90.80    4.428E+004                                1.91SE+OD4   2.D53E+004 Cs-134       604.72   97.62    5.745E+004     4 .69E+004               -1 .083E+OD4   2.729E+004 795.86   85.46    4.692E+004         (..J,;.\..,,_:;,.o.J
                                                                       ,7
                                                                               -8.486E+003    2.171E+OD4
 +      Cs-137       661.66*  85.10    6.683E+004     6.68E+004                  4.644E+006   3.173E+004
 +      Eu-152       121.78   28.67    4.558E+005     1. l lE+OOS                7.554E+D04.J 2.245E+005 344.28*  26.60    1. 74 OE+005                              1. 149E+005  8.256E+OD4 1408.01*   21. 07   1 .114E+005                               2.212E+OD5   4.740E+004 Eu-154       123.07   40.40    3.198E+005     8.28E+004                  2.756E+OD5   1.575E+005 723.30   20.06    2.004E+005                                S.386E+OD4   9.293E+004 1274.43    34.80    8.281E+004                                2.152E+D04   3.653E+004
 +      Eu-155        86.55*  30.70    5.188E+005     5.19E+OD5                  2.503E+OOS   2.557E+005 105.31   21.10    6.703E+005                                6.195E+OOS   3.303E+005 Tl-208       583.19   85.00    6.615E+004     6.62E+004                  4.D78E+004   3.14SE+004 Bi-212       727.33    6.67    6.237E+005     6.24E+005                  2.255E+OOS   2.899E+OOS Pb-212       238.63   43.60    2.252E+005    2.25E+OD5                   1.305E+005   1.102E+OD5
 +      Bi-214       609.32*  45.49    7.890E+004     7.89E+004                  9.400E+004   3.637E+004 1120.29    14. 92   2.860E+005                              -3.972E+005    1.321E+OOS 1764.49    15.30    2.219E+OOS                                1. 939E+OOS  9.845E+004
 +      Pb-214       295.22   18.42    4.455E+005    2.02E+OD5                 -2.712E+005    2.166E+OOS 351.93*  35.60    2.016E+005                                2.041E+005   9.746E+004 Ra-226       186.21    3.64    2.946E+006    2.95E+006                   l. 191E+006  1.446E+006 Ac-228       338.32   11. 27   6.832E+OOS    l .75E+D05                -3.722E+OD5    3.311E+005 911. 20  25.80    1 .749E+005                               5.778E+004   8.141E+004 968.97   15.80    2.901E+005                                2.931E+OOS   l .351E+OOS
+       Am-241        59.54*  35.90    2.937E+005    2.94E+005                 -5.364E+004    1.424E+OOS
       + = Nuclide identified during the nuclide i dentification
       * = Energy line found in the spectrum
       >~Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ ; Half-life too short to be able to perform the decay correction

[1302]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002540.CNF Report Generated On 3/8/2018 5:27:38 PM Sample Title B101110AFSWC034GD Sample Description Ul CTMT Sample Identification 034 Sample Type GAMMA DIRECT Sample Geometry 1. 5M90D ECP 17. 8 Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO MA2 Sample Taken On 3/8/2018 10:11:00 PM Acquisition Started 3/8/2018 1 0 :12:02 AM Live Time 600.0 seconds Real Time 601.6 seconds Dead Time 0 , 26 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1.SM90DECP17 8CM [1303]

Peak Analysis Report 3/8/2018 5: 27: 38 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC034GD Peak Analysis Performed on: 3/8/2018 5:27:37 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113 - 134 129.35 31. 93 1.20 3.64E+002 65. 41 1.87E+002 2 284- 309 301.32 74.98 1. 09 8.20E+002 171. 60 l.54E+003 3 332- 346 3 40 . 15 84.70 0.81 1 .99E+002 107.37 9.29E+002 4 1374- 1388 1378.99 344.71 1.48 1.10E+002 43.79 1 .27E+002 5 1400- 1414 1409.29 352.29 0.53 2.49E+001 38.08 1.15E+002 6 2431- 2445 2438.59 609.83 0.62 5.59E+001 24.55 3.21E+001 7 2635- 2658 264 8 .13 662.24 1. 54 1.96E+003 94.33 6.56E+001 8 3110- 3125 311 7 .53 779.65 1. 55 5.00E+OOl 20.42 1. 80E+001 9 3850- 3866 3858.37 964.92 0 .38 4.49E+001 24.22 3.21E+001 10 4442- 4459 44 51. 03 1113 .10 1. 08 6.49E+001 22.83 2.0lE+OOl 11 4481- 4493 4486.57 1121.98 0 .31 1.31E+001 16.39 1.99E+001 12 4685- 4704 4695.88 1174.31 2.12 1.14E+002 25.81 1 .SOE+OOl 13 5324- 5341 5333 .14 1333.60 1. 39 1.21E+002 24.52 9.00E+OOO 14 5627- 5646 5636.89 1409.51 0. 98 7.70E+001 24.26 2.00E+OOl 15 5837- 5857 5846.99 1462.01 1. 23 1.28E+002 25.00 7.78E+OOO M First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1304]

Interference Corrected Activity Report 3/8/2018 5: 27: 3 8 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

Bl01110AFSWC034GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . . ....... . . . ... .. . . . . IDENTIFIED NUCLIDES           . . . ............ . . ..

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/M"2 ) Uncertainty K-40 0.998 1460.82* 10.66 1.57833E+006 3.36895E+005 Co-60 0.998 1173.23* 99.85 1 .39813E+005 3.35753E+004 1332.49* 99.98 1 .53705E+005 3.34822E+004 Cs-137 0 .999 661.66* 85.10 2.43817E+006 3.15275E+005 Eu-152 0.331 121.78 28.67 344.28* 26.60 3.63124E+005 1.56101E+005 1408.01* 21.07 4.73349E+005 1.53852E+005 Eu-155 0 .331 86.55* 30.70 5.43077E+D05 3.12416E+005 1 05.31 21. 10 Bi-214 0.709 609.32* 45.49 1. 2732 8E+005 5.79406E+004 1120.29* 14.92 1. 06 012E+O 05 1.33246E+005 1764.49 15. 30 Pb-214 0.445 295.22 18.42 351.93* 35.60 6. 17061E+004 9.48566E+004 

        * . Energy line found in the spectrum.
        @=Energy line not used for Weighted Mean Activity Energy Tolerance :               10.000 keV Nuclide confidence index threshold=                    0. 30 Errors quoted at 2. 000 sigma

[1305]

Interference Corrected Activity Report 3/8/2018 5: 27: 38 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 0.998 l.578328E+006 3.368951E+OOS Co-60 0.998 1.467783E+005 2. 370835E+004v" Cs-137 0.999 2.438172E+006 3.152749E+005../ Eu-152 0.331 4.190364E+OOS 1 .095763E+005J Eu-155 0.331 5.430772E+OOS 3.124163E+OOS Bi-214 0.709 1.239384E+005 5.313450E+004 Pb-214 0.445 6.170613E+004 9.485663E+004 

      ? ; Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2.000 sigma

[1306]

Interference Corrected Activity Report 3/8/2018 5:27:38 PM Page 5 

  **********    U N I D E N T I F I E D     P E A K S     **********

Peak Locate Performed on: 3/8/20 18 5:27:37 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 93 6.0660E-001 17.97 2 74.98 1.3663E+OOO 20.93 8 779.65 8.3266E-002 40. 87 9 964.92 7.4816E-002 53.95 Sum 10 1113.10 1. 0809E-001 35.20 M ; First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000 sigma [1307]

Nµclide MDA Report 3/8/2018 5:27:38 PM Page 6

          • N U C L I D E MD A RE PORT *****

Detector Name: 5452 Sample Geometry: 1.SM90D- ECP- 17.8 Sample

Title:

B101110AFSWC034GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nucl ide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10 .66  2.478E+005    2. 4 8E+005          1.578E+006   1 .072E+005
 +      Co-60      1173.23*    99. 85  3.258E+004    2.60E+004            1.398E+005   1.463E+004 1332.49*    99.98   2.604E+004                         1.537E+005   1.130E+004 Nb-94       702.65     99. 81  4.475E+004    4.48E+004 -l. 447E+004            2.092E+004 871. 09    99.89   4.931E+004                        -2.151E+004   2.312E+004 Ag-108m     433.90     90.50   7.760E+004    5.30E+004 -6.130E+003             3.739E+004 614.30     89.80   7.068E+004                        -2.289E+004   3.378E+004 722.90     90.80   5.305E+004                        -7.492E+002   2.491E+004 Cs-134      604.72     97.62   5.722E+004    5.72E+004 -2.002E+004             2.718E+004 795.86     85.46   5.769E+004       ....,~ c.... c./ -8. 867E+002  2.709E+004
 +      Cs-137      66 1 .66*  85. 10  6.953E+004    6.95E+004 2.438E+006              3.309E+004
 +      Eu-152      121.78     28.67   4.SOOE+OOS    1.86E+005 9.229E+004              2.216E+005 344.28*    26.60   2.171E+OOS                         3.631E+005   1.041E+005 1408.01*    21. 07  1.860E+OOS                         4.733E+OOS   8.467E+004 Eu-154      123.07     40.40   3.232E+005    1. 03E+005 6.238E+005,            l. 591E+OOS 723.30     20.06   2.443E+005                         3.272E+004   1. 148E+005 1274.43     34.80   1. 031E+005                        6.214E+004   4.666E+004
 +      Eu-155       86.55*    30.70   4 .723E+005   4.72E+005 5.431E+005              2.325E+005 105.31     21.10   6.521E+005                        -3.346E+005   3.212E+005 Tl-208      583.19     85.00   7.049E+004    7.05E+004 1.380E+004              3.362E+004 Bi-212      727.33      6.67   7.796E+OOS    7.BOE+OOS 4.lOOE+OOS              3.679E+005 Pb-212      238.63     43.60   2.192E+005    2.19E+005 2.138E+005              l .072E+005
 +      Bi-214      609.32*    45.49   7.905E+004    7.91E+004 1. 2 73E+O 05           3.645E+004 1120.29*    14 .92  2.183E+OOS                         1. 060E+O 05 9.816E+004 1764.49     15 .30  2.603E+005                         2.770E+OOS   l.177E+005
 +      Pb-214      295.22     18.42   4 .217E+OOS   1.56E+OOS 3.858E+004              2.047E+005 351.93*    35.60   1 .565E+005                        6.171E+004   7.488E+004 Ra-226      186.21      3.64   2.714E+006    2.71E+006 2.037E+004              1.330E+006 Ac-228      338.32     11. 27  6.281E+005    2.14E+OOS -4.093E+005             3.036E+OOS 911.20     25.80   2.136E+005                         2.813E+005   1. OOBE+OOS 968.97     15.80   4. lllE+OOS                        1.217E+005   1.956E+OOS Am-241       59.54     35.90   5.159E+OOS    5.16E+OOS 2.162E+OOS              2.534E+OOS
       + = Nuclide identified during the nuclide i dentification
       *=Energy line found in the spectrum
       > - Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1308]

          • ~*******************************************************************
          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002541.CNF Report Generated On 3/8/2018 5:28:36 PM Sample Title B101110AFSWC035GD Sample Description Ul CTMT Sample Identification 035 Sample Type GAMMA DIRECT Sample Geometry 1.5M90D ECP 17.8 Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO M"'2 Sample Taken On 3/8/2018 10:45:00 PM Acquisition Started 3/8/2018 10:33:21 AM Live Time 600.0 seconds Real Time 601.8 seconds Dead Time Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1.5M90DECP17 8CM f"\ -1.~ {)( i ( 4 ,VI.:'( ItI*- ./( .-4 (' _ Q C C l /q /!B r~u c 

                                                       ~rr{--*Jz{ 0/~{~(~

So F .= o, ~o3 o 1;- [1309]

Peak P..nalysis Report 3/8/2018 5:28:36 PM Page 2

          • PE AK A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC035GD Peak Analysis Performed on: 3/8/2018 5:28:35 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 122- 136 129.53 31.98 1. 05 3. 41E+ 002 72.10 3.29E+002 2 285- 307 3 01 .36 74. 99 1. 31 8.88E+002 169.01 1.61E+003 3 333- 347 341.11 84.94 0 .72 1.83E+002 118.30 1.15E+003 4 481- 496 488.95 121. 95 0 .78 1. 87E+002 105.80 8.69E+002 5 615- 622 618.98 154.50 0 .34 -2.67E+OOO 48.63 2.95E+002 6 954- 989 979.69 244 .78 0 .59 2.17E+001 130.68 7.72E+002 7 1371- 1388 1378.40 344.56 0 .94 2.26E+002 52.39 1.40E+002 8 2328- 2337 2332.23 583.22 0 .93 l.62E+001 20.23 3.78E+001 9 2636- 2660 26 48 .28 662.28 1 .58 2.93E+003 116.16 1.08E+002 10 3109- 3127 3116.35 779.36 1. 73 8.13E+001 28.07 3.37E+001 11 3850- 3867 3858.83 965.04 1. 14 9.00E+OOl 26.67 2.70E+001 12 4340- 4353 4345.88 1086.81 1. 07 3.87E+001 19.47 2.03E+001 13 4444- 4462 4451.89 1113.32 1. 32 8.90E+001 22.97 l.30E+001 14 4686- 4706 4696. 04 1174.35 0.73 l. 56E+002 31. 23 2.39E+001 15 5323- 5343 5333.47 1333.68 1. 96 1.85E+002 29.23 7.80E+OOO 16 5626- 5646 5636.07 1409.31 1. 75 1.09E+002 28.27 2.48E+001 17 5840- 5858 5847.18 1462.06 1. 38 9.61E+001 25.18 1. 89E+001 18 7059- 7072 7065.94 1766.56 0.76 2.48E+001 12.52 5.22E+OOO M = First peak in a multiplet region m = Other peak in a multiplet region F - Fitted singlet Errors quoted at 2 . 000 sigma [1310]

Interference Corrected Activity Report 3/8/2018 5: 28: 36 PM Page 3

                                                                                                                                                • ~
          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

Bl01110AFSWC035GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * * * * ' * * * * * * * *
  • I *
  • IDENTIFIED NUCLIDES * * * * * * * * * * *
  • 1 * *
  • I I ..
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 0 .998 1460.82* 10 .66 1.18254E+006 3.26585E+005 Co-60 0 .998 11 73.23* 99.85 1.91484E+005 4.12558E+004 1332.49* 99.98 2.35263E+005 4.16318E+004 Cs-137 0 .999 661.66* 85.10 3.64020E+006 4.60180E+005 Eu-152 0 .999 121.78* 28.67 4.74235E+005 2.84633E+005 344.28* 26.60 7.42851E+005 2.11369E+005 1408 .01* 21. 07 6.71154E+005 1.81882E+OOS Eu-155 0. 332 86.55* 30.70 4.98363E+005 3.36908E+005 105.31 21.10 Tl-208 1.000 583.19* 85.00 1.95350E+004 2.44746E+004 Pb-212 0.941 238.63* 43.60 3.92928E+004 2.36819E+005 Pb-214 0.389 295.22 18.42 351.93* 35.60 5.55091E+005 1. 56574E+005
          *=Energy line found in the spectrum.
          @ ~ Energy line not used for Weighted Mean Activity Energy Tolerance :                    10.000 keV Nuclide confidence index threshold :                        0.30 Errors quoted at 2.000 sigma

[1311]

Interference Corrected Activity Report 3/8/2018 5: 28: 36 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 0.998 1.182545E+006 3.265846E+005 Co-60 0.998 2 .131752E+005 / 2.930426E+004J Cs-137 0.999 3.640200E+006v 4.601800E+005..t Eu-152 0.999 6.140475E+OOS.1 1.532563E+005v Eu-155 0.332 4.983628E+005 3.369076E+005 Tl-208 1 .000 1.953500E+004 2.447455E+004 Pb-212 0.941 3.929277E+004 2.368190E+005 Pb-214 0.389 9.624729E+004 1.939731E+OOS 

      ? = Nuclide is part of an undetermined solution x = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2.000 sigma

[1312]

Interference Corrected Activity Report 3/8/2018 5:28:36 PM Page 5 

  **********     U N I D E N T I F I E D        P E A K S    **********

Peak Locate Performed on: 3/8/2018 5 : 28: 35 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 98 5.6845E-001 21.14 2 74.99 1.4808E+OOO 19.02 5 154.50 -4.4464E-003 -1822.7 D-Esc. 10 779.36 1. 3551E-001 34.53 Sum 11 965.04 1 .5000E-001 29.63 12 1086.81 6.4492E-002 50.33 13 1113.32 1. 4 826E- 0 01 25.82 18 1766.56 4. 1306E-002 50.52 Sum M 

         -  First peak in a multiplet region m = Other peak in a multiplet region F : Fitted singlet Errors quoted at    2. 000 sigma

[1313]

Nuclide MDA Report 3/8/2018 5: 28: 36 PM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: 1.5M90D ECP 17.8 Sample

Title:

B101110AFSWC035GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nucl ide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/M"2 ) (pCi/MA2 ) 

 +      K-40       1460.82*  10. 66  3.535E+005   3.53E+005    1.183E+006    1.601E+OOS
 +      Co-60      1173.23*  99.85   4.112E+004   2.57E+004    1.915E+005    1 .890E+004 1332.49*  99.98   2.572E+004                 2.353E+005   1.114E+004 Nb-94       702.65   99.81   5.367E+004   5.37E+004    1 .970E+004   2.538E+004 871. 09  99.89   6.127E+004                 3.662E+004   2.91DE+004 Ag-108m     433.90   90.50   8.890E+004   6.05E+004    4.738E+003    4 .304E+D04 614.30   89.80   8.063E+004                1.204E+005    3.875E+004 722.90   90.80   6.049E+004               -1.055E+OD4    2.864E+004 Cs-134      604.72   97.62   6.294E+004   6. 1 3E+004 -8.859E+004    3.004E+004 795.86   85.46   6.125E+004                5.061E+004;   2.888E+OD4
 +      Cs-137      661.66*  85.10   8.941E+004   8.94E+004    3.640E+006    4.303E+004
 +      Eu-152      121.78*  28.67  4.332E+005    2.09E+005    4.742E+D05    2.132E+005 344.28*  26.60  2.415E+005                 7.429E+005    1.163E+OOS 1408.01*  21. 07 2.091E+005                 6.712E+D05    9.626E+OD4 Eu-154      123.07   40. 40 3.522E+OOS    1.25E+OOS    3.240E+D05o1  1. 737E+OD5 723.30   20.06  2.750E+005                -7.910E+004    l.302E+005 1274.43   34.80  1 .247E+005                1.439E+OD5    5.746E+004
 +      Eu-155       86.55*  30.70  5.227E+OD5    5.23E+005    4.984E+D05    2.577E+005 105.31   21.10  7.131E+005                 2.674E+005    3.517E+005
 +      Tl-208      583.19*  85.00  4.002E+004    4.00E+004    1.953E+004    1. 838E+004 Bi-212      727.33    6.67  8.569E+005    8.57E+D05    4.137E+OOS    4.065E+OOS
 +      Pb-212      238.63*  43.60  3.933E+005    3.93E+OOS    3.929E+004    l .942E+005 Bi-214      609.32   45.49  1.525E+005    1.52E+OOS    1.436E+005    7.316E+004 1120.29   14.92  3.954E+005                 7.607E+004    1.868E+005 1764.49   15.30  2.933E+005                 3.601E+OOS    1.342E+D05
 +      Pb-214      295.22   18.42  4.720E+005    1. 8DE+005  -8.109E+004    2.299E+005 351.93*  35.60  l.804E+005                 5.551E+005    8.689E+004 Ra-226      186.21    3.64  2.956E+006    2.96E+OD6    6.514E+003    1 .451E+006 Ac-228      338.32   11.27  6.938E+005    2.17E+OOS    1. 546E+O 04  3.364E+OOS 911.20   25.80  2.167E+005                 8.779E+004    1.024E+OOS 968.97   15.80  4.620E+005                -1. 398E+OOS   2.210E+OOS Am-241       59.54   35.90  5.504E+005    5.SOE+OOS   -2.629E+OOS    2.706E+005
       + =Nuclide identified during the nuclide i dentification
       *=Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1314]

          • GAMM A S P E C T R U M ANALYSIS *****

Filename: 5452 Report Generated On 3/8/2018 12 :56:47 PM Sample Title B101110AFSWC036GD Sample Description Ul LOWER CTMNT Sample Identification 036 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO M"2 Sample Taken On 3/8/2018 1:00 : 00 PM Acquisition Started 3/8/2018 12 :46:44 PM Live Time 600. 0 seconds Real Time 601.8 seconds Dead Time 0 . 29 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1. 5M90DECP1 7 BCM [1315]

Peak Analysis Report 3/8/2018 12 :56:47 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

Bl01110AFSWC036GD Peak Analysis Performed on: 3/8/2018 12:56:47 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 112 - 168 129.16 32. 00 1. 01 1.11E+ 003 154.13 5.54E+002 2 296 - 307 301.12 74.99 0. 84 2.64E+002 98.28 8.43E+002 3 334 - 345 3 40 .05 84.73 0.89 1.05E+002 92.50 8.08E+002 4 482- 497 488.65 121.88 1. 61 l.98E+002 99.60 7.56E+002 5 663- 675 667.88 166.70 0 .33 4.97E+OOO 63.86 3.84E+002 6 1368- 1416 1377.71 344.19 1. 03 2.30E+002 108.90 3.83E+002 7 2364- 2377 2370.83 592.51 0.48 7.83E+OOO 20.53 3.52E+001 8 2431- 2444 2437.03 609.06 0.98 4.12E+001 24.12 3.78E+001 9 2631- 2659 2646.86 661.52 1. 60 4.27E+003 136.51 8.2SE+001 10 3109- 3123 3116.33 778.91 0 . 31 5.97E+001 22.25 2.23E+001 11 3463- 3476 3469.04 867. 10 0.26 8.59E+OOO 20.56 3.04E+001 12 3848- 3866 3857.49 964.23 0.41 5.28E+001 24.49 2.72E+001 13 4336- 4351 4344.39 1085.98 0.94 4.78E+001 23.27 2.92E+001 14 4440- 4457 4449.22 1112.19 0.33 6.14E+001 21.21 1.56E+001 15 4684- 4704 4694.13 1173.43 1. 35 1.53E+002 31. 72 2.66E+001 16 5320- 5342 5331.30 1332.74 1. 82 l. 64E+ 002 29.57 1.42E+001 17 5623- 5643 5633.09 1408.21 1. 73 l. 35E+002 26.21 1.03E+001 18 5836- 5855 5844.79 1461.14 1.43 8.73E+001 24.62 1. 87E+001 M = First peak in a multiplet region m = Other peak in a mu ltiplet region F - Fitted singlet Errors quoted at 2.000 sigma [1316]

Interference Corrected Activity Report 3/8/2018 12:56:47 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC036GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . ...... ... . ... . .... .. IDENTIFIED NUCLIDES           * *
  • fl * * * * * * * *
  • l I I
  • t *
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 1.000 1460.82* 10.66 1.07498E+006 3.16999E+OOS Co-60 1.000 1173.23* 99.85 1 .88079E+OOS 4.17079E+004 1332.49* 99.98 2.0802SE+OOS 4 .10871E+004 Cs-137 1.000 661. 66* 85.10 5.29834E+006 6.58495E+OOS Eu-152 1.000 121.78* 28.67 5.02271E+OOS 2.71934E+005 344.28* 26.60 7.58195E+005 3.79579E+005 14 08.01* 21.07 8.27914E+005 1. 74157E+OOS Eu-155 0 .331 86.55* 30,70 2.86302E+005 2.58752E+005 105.31 21. 10 Tl-208 0.870 583.19* 85.00 9.46176E+003 2.48484E+004 Bi-214 0.690 609.32* 45. 49 9.38151E+004 5.60163E+004 11 20.29* 14. 92 4.97001E+OOS 1. 76205E+005 1764.49 15.30 Pb-214 0.383 295.22 18.42 351.93* 35.60 5.66517E+OOS 2.82827E+OOS
       * ~ Energy line found in the spectrum.
       @~Energy line not used for Weighted Mean Activity Energy Tolerance :            10.000 keV Nuclide confidence index threshold=                 0. 30 Errors quoted at 2. 000 sigma

[1317]

Interference Corrected Activity Report 3/8/2018 12:56: 47 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1. 000 1 .074984E+006 3.169990E+OOS Co-60 1.000 1.982016E+OOS~ 2.926998E+004 Cs-137 1. 000 5.298342E+006..J 6.584952E+OOS Eu-152 1.000 7.331719E+OOSJ 1.466504E+OOS Eu-155 0.331 2.863016E+OOS 2.587522E+OOS Tl-208 0.870 9.461762E+003 2.484837E+004 Bi-214 0.690 1.308221E+OOS 5.338363E+004 Pb-214 0.383 1.869688E+004 3.033032E+OOS 

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2.000 sigma

[1318]

Interference Corrected Activity Report 3/8/2018 12:56:47 PM Page 5 

  **********     U N I D E N T I F I E D       P E A K S     * *********

Peak Locate Performed on: 3/8/2018 12:56:47 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % uncertainty Type Nuclide 1 32 .00 1. 8420E+OOO 13.95 2 74.99 4.3981E-0Dl 37.24 5 166.70 8.2862E-003 1284.46 Sum 10 778.91 9.9482E-OD2 37.28 Sum 11 867. 10 1. 4316E- 002 239.31 12 964.23 8.8021E-002 46.36 13 1085.98 7.9713E-D02 48.65 M :. First peak in a multiplet region m ::, Other peak in a multiplet region F == Fitted singlet Errors quoted at 2 . 000 sigma [1319]

Nuclide MDA Report 3/8/2018 12:56:48 PM Page 6

          • N U C L I D E MD A REPORT *** **

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSWC036GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL . NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/M"'2 ) (pCi/MA2 ) (pCi/M"'2 ) (pCi/M A2 ) 

 +      K-40       1460.82*    10.66  3.576E+005    3.58E+005     l. 075E+006 1.621E+005
 +      Co-60      1173.23*    99.85  4. 329E+004   3. 4 4E+004   l. 881E+005 1.999E+004 1332.49*    99.98  3.440E+004                 2.080E+005   1. 548E+O 04 Nb-94        702.65    99.81  5.677E+004    5.68E+004   -2.849E+004   2.693E+004 871.09    99.89  6.007E+004                 4 .615E+004  2.850E+004 Ag-108m      433.90    90.50  l.101E+005    6. 4 1E+004  6.992E+004   5.365E+004 614.30    89.80  8.248E+004                 4.005E+004   3.967E+004 722.90    90.80  6.412E+004                 4.224E+004   3.045E+004 Cs-134       604.72    97.62  7.422E+004    6.64E+004    5.808E+004./ 3.568E+004 795.86    85.46  6.639E+004                 3.156E+004   3.145E+004
 +      Cs-137       661.66*   85.10  8.441E+004    8.44E+004    5.298E+006   4 .053E+004
 +      Eu- 152      121.78*   28.67  4.055E+005    1. 4 0E+005  5.023E+005   1 .993E+005 344.28*   26.60  5.753E+005                 7.582E+005   2.832E+005 1408.01*    21. 07 1. 396E+005                8.279E+005   6.150E+004 Eu-154       123.07    40 .40 3.899E+005    1 .20E+005   l.551E+005J  1.925E+005 723.30    20.06  2.880E+005                 1.403E+005   1. 367E+005 1274.43     34.80  1 .197E+005                3.708E+003   5.496E+004
 +      Eu-155        86.55*   30.70  4.122E+005    4.12E+005    2.863E+005   2.024E+005 105.31    21.10  7.981E+005                 3.726E+005   3.942E+005
 +      Tl-208       583.19*   85.00  4.256E+004    4 .26E+004   9.462E+003   1 .964E+004 Bi-212       727.33     6.67  8.392E+005    8.39E+005    8.989E+004   3.976E+005 Pb-212       238. 6 3  43.60  2.641E+005    2.64E+005   -1.521E+005   1 .296E+005
 +      Bi-214       609.32*   45.49  8.255E+004    8.26E+004    9.382E+004   3.820E+004 1120.29*    14 .92 2.121E+005                 4. 970E+005  9.512E+004 1764.49     15. 30 2.523E+005                 1.650E+005   1.137E+005
 +      Pb-214       295.22    18.42  5.548E+005    4.30E+005   -1.171E+005   2.712E+005 351.93*   35.60  4.299E+005                 5.665E+005   2.116E+005 Ra-226       186.21     3.64  3.420E+006    3.42E+006    2.100E+006   1.683E+006 Ac-228       338.32    11.27  9.165E+005    2.26E+005    1. 759E+005  4 .478E+005 911.20    25.80  2.259E+005                -2.429E+004   1 .070E+005 968.97    15.80  4.245E+005                 5.035E+005   2.023E+005 Am-241        59.54    35.90  6.333E+005    6.33E+005    2.520E+005   3.121E+005
       + = Nuclide identified during the nuclide identification
       * = Energy line found in the spectrum
       > ; Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ = Half-life too short to be able to perform the decay correction

[1320]

          • GAMMA S P E C T R U M ANALYSIS *****

Filename: C:\GENIE2K\CAMFILES\00002559.CNF Report Generated On 3/9/2018 4 : 46:42 PM Sample Title B101110AFSFC037GD Sample Description Ul LOWER CTMNT Sample Identification 037 Sample Type GAMMA DIRECT Sample Geometry 1. 5M90D ECP 17. 8 Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO M .... 2 Sample Taken On 3/9/2018 9:09:00 AM Acquisition Started 3/9/2018 9:19:33 AM Live Time 600 . 0 seconds Real Time 601.4 seconds Dead Time 0.23 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1.5M90DECP17 8CM [1321]

,Peak Analysis Report 3/9/2018 4:46:42 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B10l110AFSFC037GD Peak Analysis Performed on: 3/9/2018 4: 4 6:42 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 112- 135 128.86 31.92 1. 61 4.63E+002 63.09 1.41E+002 2 287- 312 301.33 75.05 1.07 7.56E+002 143.00 1.02E+003 3 335- 345 340. 01 84.72 1. 26 1 .52E+002 76.09 5.43E+002 4 441- 452 447.18 111 .51 0.54 7.59E+001 67.88 4.27E+002 5 1898- 1910 1903.99 475.78 0.78 1.91E+001 30.79 8.29E+001 6 2631- 2661 2645.76 661.25 1. 65 3.42E+003 120.88 4 .92E+001 7 4683- 4700 4690.89 1172.62 0.69 9.55E+001 25.19 1.95E+001 8 4931- 4946 4938.29 1234.48 0.54 1 .09E+001 8.47 2.13E+OOO 9 5318- 5340 5328.77 1332.11 2.41 1.15E+002 26.04 l.42E+001 10 5832- 5852 5842.18 1460.49 1. 59 1. 24E+O 02 26.12 1. 29E+001 11 7051- 7066 7058.88 1764.71 0.81 1. 90E+001 8.72 O.OOE+OOO M -..: First peak in a mul tiplet region m = Other peak in a mul tiplet region F 

 -    Fitted singlet Errors quoted at       2 . 000 sigma

[1322]

Inte~ference Corrected Activity Report 3/9/2018 4 :46:42 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

Bl01110AFSFC037GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV} ( %} (pCi/MA2 } Uncertainty K-40 1 .000 1460 .82* 10.66 l.52724E+006 3.47661E+005 Co-60 1.000 1173 .23* 99.85 1 .17125E+005 3.22824E+004 1332.49* 99.98 1 .45800E+005 3.50722E+004 Cs-137 1.000 661. 66* 85.10 4.24371E+006 5.31288E+OOS Eu-155 0.972 86.55* 30.70 4.15206E+OOS 2.23584E+OOS 105.31* 21. 10 2.69026E+005 2.46987E+005 

       *=Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold -           0 .30 Errors quoted at 2.000 sigma

[1323]

Interference Corrected Activity Report 3/9/2018 4 :46:42 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1 .000 1 .527239E+006 3.476608E+005 Co-60 1.000 1 . 3 02766E+OOS .I 2.375223E+004 Cs-137 1.000 4.243707E+006J 5.312883E+005 Eu-155 0.972 3.493676E+005 1.657557E+005 

      ?  = Nuclide is part of an undetermined solution X ;  Nuclide rejected by the interference analysis
      @  - Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1324]

Interference Corrected Activity Report 3/9/20 18 4: 46: 42 PM Page 5 

  **********      U N I D E N T I F I E D     P E A K S    **********

Peak Locate Performed on: 3/9/2018 4:46:42 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 92 7.7167E-001 13.63 2 75.05 1. 2604E+OOO 18.91 5 475.78 3.1785E-002 161. 46 8 1234.48 1. 8109E-002 77.98 11 1764.71 3.1667E-002 45.88 Tol. Bi-214 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1325]

Nuclide MDA Report 3/9/2018 4:46:42 PM Page 6

          • N U C L I D E MD A REPORT ****
  • Detector Name: 5452 Sample Geometry: 1. 5M9 OD ECP 1 7 . 8 Sample

Title:

B101110AFSFC037GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nucl ide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2 ) (pCi/M"2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*   10 .66   3.091E+005    3.09E+OOS        1. 527E+006     1.379E+005
 +      Co-60      1173.23*   99.85    3.538E+004    3 .44E+004       1 .171E+005     1. 603E+004 1332.49*   99.98    3.436E+004                     1 .458E+005     1. 546E+004 Nb-94       702.65    99.81    3.863E+004    3.86E+004        7.377E+002     1.786E+004 8 71. 09  99.89    4.354E+004                     5.697E+003     2.024E+004 Ag-108m     433.90    90.50    9.654E+004    4.85E+004        1.353E+003     4 .687E+004 614 .30   89.80    6.321E+004                     1 .168E+004    3.004E+004 722.90    90.80    4.854E+004                     4.263E+003     2.266E+004 Cs-134      604.72    97.62    6.216E+004    4. 25E+004       4. 308E+OQ4../ 2.965E+004 795.86    85.46    4.254E+004                     1. 617E+004    1.952E+004 Cs-137      661.66*   85. 10   6.613E+004    6.61E+004        4. 244E+006    3.139E+004 Eu-152      121.78    28.67    4.670E+005    1. 48E+005      -5.837E+005     2.301E+OOS 34 4 .28  26.60    3.292E+005       o,oo&... o J -6.659E+005     1 .601E+005 1408 . 01  21. 07   1.477E+005                    -5.948E+004     6.552E+004 Eu-154      123.07    40.40    3.341E+005    1.03E+005        9.449E+004-.t  1.646E+005 723.30    20.06    2.243E+005                     1.389E+OOS     1.049E+005 127 4 .43  34.80    1. 031E+005                   -9.007E+003     4.667E+004
 +      Eu-155        86.55*  30.70    3.304E+005    3.30E+OOS        4.152E+OOS     1 .615E+OOS 105.31*   21.10    3.923E+005                     2.690E+005     1 .914E+005 Tl-208      583.19    85.00    6.955E+004    6.96E+004       -2.154E+004     3.315E+004 Bi-212      727.33      6.67   6.709E+005    6.71E+OOS        4.259E+005     3.135E+OOS Pb-212      238.63    43.60    2.480E+005    2.48E+005        1.197E+005     1. 216E+005 Bi-214      609.32    45.49    1.273E+005    1.27E+005        7.287E+004     6.059E+004 1120.29    14.92    3.043E+005                     2.137E+005     l. 412E+OOS 1764.49    15. 30   2.265E+005                     2.032E+005     1. 008E+OOS Pb-214      295.22    18.42    5.142E+005    2.58E+005        6.240E+004     2.510E+005 351.93    35.60    2.581E+005                     2.163E+005     1.257E+005 Ra-226      186.21      3.64   3.118E+006    3. 1 2E+006      l.457E+006     l.532E+006 Ac-228      338.32    11.27    7.797E+005    1 .85E+005       3.302E+OOS     3.794E+005 911.20    25.80    1.850E+005                     7.581E+004     8.651E+004 968.97    15.80    3.070E+005                     2.913E+005     l .435E+005 Am-241       59.54    35.90    5.309E+005    5.31E+OOS       -2.071E+005     2.609E+005
       + ~ Nuclide identified during the nuclide identification
       * ~ Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ ~ Half-life too short to be able to perform the decay correction

[1326]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002560 .CNF Report Generated On 3/9/2018 4:47 : 56 PM Sample Title B101110AFSFC038GD Sample Description Ul LOWER CTMNT Sample Identification 038 Sample Type GAMMA DIRECT Sample Geometry 1. 5M9 OD ECP 1 7 . 8 Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO M"2 Sample Taken On 3/9/2018 9:38: 00 AM Acquisition Started 3/9/2018 9:38:26 AM Live Time 600 . 0 seconds Real Time 601. 8 seconds Dead Time 0.30 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1.SM90DECP17 8CM Dat~ vCf. /idC< te e/ 3/ to ( 18 oc::; o ~ 

                                                 &-z1. u~~.

s O /.= = cs. 3~ 3 () 8 [1327]

Peak Analysis Report 3/9/2018 4 : 47: 56 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B1 01110AFSFC038GD Peak Analysis Performed on: 3/9/2018 4:47:56 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 112- 150 128. 54 31. 84 1. 68 6.81E+002 127.81 5.39E+002 2 284- 312 3 01. 08 74.98 1. 27 9.41E+002 183.69 1.62E+003 3 328- 346 339.63 84.62 1.15 1. 86E+002 132.38 1.24E+003 4 1176- 1187 1181.76 295.19 0.33 1. 85E+001 43.14 1.79E+002 5 1401- 1415 1406.51 351.39 0.98 6.llE+OOl 45.90 1.60E+002 6 2430- 2444 2436.96 609 .04 0.37 3.37E+001 25.26 4.33E+001 7 2630- 2659 2645.79 661.26 1. 72 5.12E+003 148.72 8.44E+001 8 3638- 3651 3644 .35 910.94 0.50 l .77E+001 12.47 7.26E+OOO 9 4681- 4701 46 9 1 .29 1172.72 0.92 1 .32E+002 26. 23 1.07E+001 10 5318- 5340 5329.50 1332.29 0.96 1.26E+002 25.93 1. llE+O 01 11 5830- 5854 5842.52 1460.57 1. 22 1.39E+002 24.60 3.03E+OOO 12 7049- 7064 7056.61 1764.14 0.58 1. 89E+O 01 10.16 2.13E+OOO M "" First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000 sigma [1328]

Interference Corrected Activity Report 3/9/2018 4 : 47 : 56 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSFC038GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . .. . . . . . ~ ... . - . . . ... . ... . ...
                                          '"         IDENTIFIED NUCLIDES           * *
  • I ., * * * * * * * * *
  • I * ,
  • Ill' Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 1.000 1460.82* 10.66 1.71004E+006 3.37125E+005 Co-60 1.000 1173.23* 99.85 1 .62193E+005 3.46837E+004 1332 .49
  • 99.98 1. 59951E+O 05 3.53281E+004 Cs-137 1.000 661.66* 85. 10 6.35986E+006 7.85786E+005 Eu-155 0.330 86.55* 30.70 5.07809E+005 3.75554E+005 1 05.31 21.10 Bi-214 0.695 609.32* 45.49 7.66242E+004 5.82091E+004 1120.29 14.92 1764.49* 15.30 l.74231E+005 9.48035E+004 Pb-214 1.000 295.22* 18.42 8.37319E+004 1 .96223E+005 351.93* 35.60 1.51350E+OOS 1 .16189E+005
          *=Energy line found in the spectrum.
          @ ;      Energy line not used for Weighted Mean Activity Energy Tolerance :                           10.000 kev Nuclide confidence index threshold=                                0.30 Errors quoted at 2 .000 sigma

[1329]

Interference Corrected Activity Report 3/9/2018 4:47:56 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1. 000 1.710038E+D06 3.371247E+OOS Co-60 1. 000 1. 610926E+OOS/ 2.474975E+004 Cs-137 1. 000 6.359862E+006J 7.857864E+OOS Eu-155 0.330 S.078086E+OOS 3.755535E+OOS Bi-214 0.695 l.033468E+OOS 4.960497E+004 Pb-214 1 .000 1.337965E+OOS 9.997653E+004 

      ?  = Nuclide is part of an undetermined solution X  ~ Nuclide rejected by the interference analysis
      @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2 .000 sigma

[1330]

Interference Corrected Activity Report 3/9/2018 4:47:56 PM Page 5 

  **********    U N I D E N T I F I E D     P E A K S      **********

Peak Locate Performed on: 3/9/2018 4:47:56 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 84 1.1356E+OOO 18.76 2 74.98 1.5676E+OOO 19 . 53 8 910.94 2.9567E-002 70 .29 Sum M = First peak in a multiplet region m - Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1331]

Nuclide MDA Report 3/9/2018 4: 47:57 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 1.5M90D ECP 17.8 Sample

Title:

B101110AFSFC038GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +       K-40      1460.82*  10.66  1.751E+005    1.7SE+005        1.710E+006  7.092E+004
 +       Co-60     1173.23*  99.85  2.875E+004    2.BBE+004        1.622E+005  1.272E+004 1332.49*  99.98  3.0SSE+004                     1.600E+005  1.356E+004 Nb-94      702.65   99.81  4. 415E+004   4 .42E+004       2.714E+004  2.062E+004 871.09   99.89  4. 809E+004                    2.249E+004  2.251E+004 Ag-108m     433.90   90.50  1.153E+OOS    4.95E+004       -5.833E+003  5.625E+004 614.30   89.80  7.681E+004                    -1 .446E+004 3.684E+004 722.90   90.80  4.954E+004                     7.565E+003  2.316E+004 Cs-134     604.72   97.62  7.14SE+004    4.82E+004       -4.326E+003  3.429E+004 795.86   85.46  4.818E+004          O,ooE.~b/ -7. 768E+003 2. 234E+004
 +       Cs-137     661.66*  85. 10 8.597E+004    8.60E+004        6.360E+006  4.130E+004 Eu-152     121. 78  28.67  5.645E+OOS    1.54E+005        2.407E+005J 2.788E+005 344.28   26.60  3.891E+005                    -9.120E+004  1 .901E+005 1408.01   21. 07 l.538E+005                     8.617E+004  6.857E+004 Eu-154     123.07   40. 40 3.944E+005    1.00E+005       -4.193E+004  1 .948E+005 723.30   20.06  2.243E+005                     3.350E+004  1 .049E+005 1274 .43  34.80  1.000E+005                     l.941E+004J 4.514E+004
 +       Eu-155      86.55*  30.70  5.894E+OOS    5.89E+005        5.07BE+005  2.910E+005 105.31   21.10  8.174E+005                     9.988E+003  4.038E+005 Tl-208     583.19   85.00  8.170E+004    8. 1 7E+004      5.929E+004  3.922E+004 Bi-212     727.33     6.67 6.799E+005    6.80E+005       -1.189E+OOS  3.lBOE+OOS Pb-212     238.63   43.60  2.881E+005    2.88E+005        1 .680E+005 1.416E+005
 +       Bi-214     609.32*  45.49  9.013E+004    9.01E+004        7.662E+004  4.199E+004 1120 .29  14.92  3.142E+005                     2.313E+OOS  1.461E+OOS 1764.49*  15.30  1. 049E+005                    1 .742E+005 3.994E+004
 +       Pb-214     295.22*  18.42  3.279E+005    1 .82E+005       8.373E+004  l.578E+005 351.93*  35.60  1.824E+005                     1 .513E+005 8.787E+004 Ra-226     186.21     3.64 3.755E+006    3.76E+006        l .713E+006 1.851E+006 Ac-228      338.32   11. 27 9.027E+005    1 .74E+005       2.651E+005  4.409E+005 911. 20  25.80  l.73SE+005                     1 .621E+003 8.075E+004 968.97   15.80  3.472E+005                     5.768E+OOS  1.636E+005 Am-241       59.54   35.90  6.293E+005    6.29E+005        4.371E+OOS  3.101E+005
       + = Nuclide identified during the nuclide identification
  • Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ ; Half-life too short to be able to perform the decay correction

[1332]

          • GAMM A S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002561.CNF Report Generated On 3/9/2018 4:49:03 PM Sample Title B101110AFSFC039GD Sample Description Ul LOWER CTMNT Sample Identification 039 Sample Type GAMMA DIRECT Sample Geometry 1.5M90D ECP 17.8 Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO MA2 Sample Taken On 3/9/2018 9:58:00 :AM Acquisition Started 3/9/2018 9:58:56 AM Live Time 600.0 seconds Real Time 601.7 seconds Dead Time 0 . 28 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration used Done On 3/7/2018 Efficiency ID 1.5M90DECP17 8CM Sotc- - [1333]

Peak, Analysis Report 3/9/2018 4:49:03 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSFC039GD Peak Analysis Performed on: 3/9/2018 4:49:03 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid {keV) {keV) Area Uncert. Counts 1 112- 136 128.86 31.92 1. 61 6.25E+002 78.56 2.35E+002 2 283- 312 3 01. 00 74 .96 1. 29 1.02E+003 193.78 1.76E+003 3 332- 356 340.82 84 .92 1.12 2.95E+002 165.61 1.59E+003 4 827- 839 832.84 207.95 0.56 4.54E+OOO 64.51 3.93E+002 5 1561- 1572 1566.65 391.43 0.75 1 .87E+001 34.25 1.08E+002 6 2428- 2445 2436.29 608.87 1. 71 6.75E+001 28.30 4.05E+001 7 2630- 2659 2645.82 661.27 1. 66 4.32E+003 13 7. 4 7 8.37E+001 8 4474- 4487 4480 . 71 1120.06 1. 09 3.16E+001 12.85 3.43E+OOO 9 4683- 4703 4691. 72 1172.83 0.73 1.04E+002 27.22 2.26E+001 10 5318- 5339 5328 . 96 1332.16 1.45 1.32E+002 24.60 5.30E+OOO 11 5623- 5638 5630 . 97 1407.67 0.58 2.30E+001 11.96 4.02E+OOO 12 5832- 5853 5842.97 1460.69 0.69 l.16E+002 24.02 7.66E+OOO M = First peak in a multiplet region m "" Other peak in a multiplet region F -,; Fitted singlet Errors quoted at 2 . 000 sigma [1334]

Interference Corrected Activity Report 3/9/2018 4:49:03 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSFC039GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . ...... . .... ... . ........ IDENTIFIED NUCLIDES           ~ ..,
  • I * * * * * * * * * * * * * ,
  • I Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/MA2 ) Uncertainty K-40 1.000 1460.82* 10 .66 1 .43163E+006 3.20641E+005 Co-60 1.000 1173.23* 99.85 1. 28052E+005 3.49179E+004 1332.49* 99.98 1.67263E+OOS 3.39910E+004 Cs-137 1.000 661.66* 85.10 5.36708E+006 6.66773E+005 Eu-155 0.331 86.55* 30.70 8.04010E+005 4.78582E+005 105.31 21.10 Bi-214 0.710 609.32* 45.49 1 .53563E+005 6.69807E+004 1120.29* 14.92 2.55999E+005 l .06209E+005 1764.49 15.30
       * ~ Energy line found in the spectrum.
       @ ~ Energy line not used for Weighted Mean Activity Energy Tolerance :              10.000 keV Nuclide confidence index threshold=                    0.30 Errors quoted at 2.000 sigma

[1335]

Interference Corrected Activity Report 3/9/2018 4:49:03 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 1 .000 1. 4 3162 8E+006 3.206412E+OOS Co-60 1.000 1.481851E+005J 2.435635E+004 Cs-137 1. 000 5.367079E+006.J 6.667733E+OOS Eu-155 0.331 8.040100E+005 4.785815E+005 Bi-214 0.710 l.827108E+005 5.665524E+004 

      ?    Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ ~ Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1336]

Interference Corrected Activity Report 3/9/2018 4:49:03 PM Page 5 

  **********    U N I D E N T I F I E D       P E A K S    * *********

Peak Locate Performed on: 3/9/2018 4:49:03 PM Peak. Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 92 1.0420E+OOO 12.56 2 74.96 1 .6922E+OOO 19.09 4 207.95 7.5681E-003 1420.63 5 391. 43 3.1086E-002 183.65 11 1407.67 3.8302E-002 52.03 Sum M = First peak in a multiplet region m . Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1337]

Nuclide MDA Report 3/9/2018 4:49:03 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 1. 5M9 OD ECP 1 7 . 8 Sample

Title:

B101110AFSFC039GD Nuclide Library used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nucl ide MDA Activity Dec. Level Name (keV) ( %) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       146 0 .82*  10.66    2.471E+005      2.47E+005   1.432E+006   1.069E+005
 +      Co-60      1173.23*    99.85    3.959E+004      2.19E+004   1.281E+OOS   1.814E+004 1332.49*    99.98    2.195E+004                  1.673E+005   9.254E+003 Nb-94       702.65     99.81    4.229E+004      4.23E+004   1.285E+004   1.969E+004 871.09     99.89    4.684E+004                  1.504E+004   2.189E+004 Ag-108m     433.90     90.50    1.127E+005      4.57E+004   4.845E+004   5.494E+004 614.30     89.80    8.045E+004                  2.808E+004   3.866E+004 722.90     90.80    4. 575E+004                -5.027E+003   2.126E+004 Cs-134      604.72     97.62    7.354E+004      5.28E+004   1 .119E+005~ 3.534E+004 795.86     85.46    5.281E+004                  7.768E+003   2.465E+004
 +      Cs-137      661.66*    85. 10   8.539E+004      8.54E+004   5.367E+006   4.101E+004 Eu-152      121.78     28.67    S.611E+005      1.97E+005   1.148E+005v  2.771E+005 344.28     26.60    3.756E+OOS                 -4.138E+OOS   1 .834E+OOS 1408.01     21.07    1.975E+005                  2.002E+OOS   9.042E+004 Eu-154      123.07     40.40    3.957E+005      9.85E+004   1.462E+Oos.J 1 .954E+005 723.30     20.06    2.0SSE+OOS                 -1.081E+005   9.544E+004 1274.43     34.80    9.846E+004                 -1.422E+004   4.435E+004
 +      Eu-155        86.55*   30.70    7.327E+005      7.33E+005   8.040E+005   3.627E+005 10 5.31    21. 10   8.191E+005                 -5.182E+005   4.047E+005 Tl-208      583.19     85. 00   7.843E+004      7.84E+004   8.630E+003   3.758E+004 Bi-212      727.33       6.67   5.882E+OOS      5.88E+OD5  -3.123E+005   2.722E+005 Pb-212      238.63     43.60    2.729E+005      2.73E+005   2.080E+005   1.340E+005
 +      Bi-214      609.32*    45.49    9.239E+004      9.24E+004   1.536E+005   4.312E+004 1120.29*    14. 92   l. 051E+OOS                 2.560E+005   4.159E+004 1764.49     15.30    2.680E+OOS                  2.100E+005   1.215E+005 Pb-214      295.22     18.42    5.621E+005      2.87E+005  -6.760E+005   2.749E+005 3 51. 93   35.60    2.871E+005                  4 .520E+004  1.402E+005 Ra-226      186.21       3.64   3.672E+006      3.67E+006  -1.277E+006   1.809E+006 Ac-228      338.32     11.27    8.560E+005      1.70E+005  -1.707E+005   4.175E+005 911.20     25.80    1. 695E+005                 1.295E+005   7.874E+004 968.97     15.80    3.008E+005                 -1.115E+005   l .404E+OOS Am-241        59.54    35.90    6.480E+005      6.48E+005   3.038E+005   3.194E+OOS
       + ; Nuclide identified during the nuclide i dentification
       * ; Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @; Half-life too short to be able to perform the decay correction

[1338]

        • ~********************************************************************
          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002562.CNF Report Generated On 3/9/2018 4:49:55 PM Sample Title B101110AFSFC040GD Sample Description Ul LOWER CTMNT Sample Identification 040 Sample Type GAMMA DIRECT Sample Geometry 1.5M90D ECP 17.8 Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO MA2 Sample Taken On 3/9/2018 10 :10 :00 AM Acquisition Started 3/9/2018 10:30:15 AM Live Time 600.0 seconds Real Time 602. 1 seconds Dead Time 0.35 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration used Done On 3/7/2018 Efficiency ID l .5M90DECP17 BCM Oe:.t4 V(;J;J u -&d 3/to(/8 (Of~ 

                                                     /j-)4__
                                                            ~ oF - 0.,1-1~03.f"

[1339]

Peak Analysis Report 3/9/2018 4:49:55 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSFC040GD Peak Analysis Performed on: 3/9/2018 4: 49: 54 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area Uncert. Counts 1 112- 169 129.03 31. 96 1. 42 1 .45E+003 189.98 8.33E+002 2 283- 312 301.39 75.06 1. 34 l.10E+003 214.65 2.19E+003 3 331- 357 341.07 84.98 1. 07 5.23E+002 194.93 2.05E+003 4 484- 495 488.51 121.85 1. 09 1.38E+002 90.62 7.59E+002 5 1370- 1386 1377.60 344.16 0.49 7.65E+001 63.53 2.98E+002 6 2430- 2443 2436.32 608.88 0.61 4 .96E+001 27.05 4.84E+001 7 2630- 2661 2645.69 661.23 1. 63 7.44E+003 178.81 1.13E+002 8 3107- 3123 3114.48 778.45 0.65 3.89E+001 21.66 2.51E+001 9 3846- 3864 3854.89 963.58 0.49 7.36E+001 22.98 1.74E+001 10 4336- 4349 4342.85 1085.59 0.35 2.0lE+OOl 20.67 3.09E+001 11 4440- 4456 4447.34 1111.72 0.63 5.36E+001 19.84 1.44E+001 12 4680- 4702 4691. 52 1172.78 1. 72 2.34E+002 40.58 4 .58E+001 13 5316- 5341 5328.34 1332.00 2.01 2.62E+002 34.58 9.lOE+OOO 14 5623- 5640 5631.31 1407.76 1.26 6.75E+001 18.79 6.47E+OOO 15 5833 - 5853 5841.65 1460.36 1.18 1.05E+002 27.10 2.25E+001 M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1340]

Interference Corrected Activity Report 3/9/2018 4:49:55 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSFC040GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  .., ...... .. .. . ... ... t ! .. i     IDENTIFIED NUCLIDES           . " . ........
                                                                             ~          . ... . . ..

Nuclide Id Energy Yield Activity Activity Name Confidence (keV} ( %} (pCi/MA2 } Uncertainty K-40 1.000 1460.82* 10.66 1 .28587E+006 3.51649E+OD5 Co-60 1.000 1173.23* 99.85 2.87121E+OOS 5.48006E+004 1332.49* 99.98 3.32619E+005 5.13552E+004 Cs-137 1 .000 661.66* 85.10 9.23511E+006 1.131D8E+006 Eu-152 1 .000 121.78* 28.67 3.49256E+005 2.40316E+005 344.28* 26.60 2.51858E+005 2.13200E+005 14 08.01* 21. 07 4.14963E+005 1. 20144E+005 Eu-155 0.332 86.55* 30.70 1 .42333E+006 6.01788E+005 105.31 21.10 Bi-214 0.687 609.32* 45.49 1.12799E+005 6.30224E+004 1120 .29* 14.92 4. 34126E+005 1.64271E+005 1764.49 15.30 

         *=Energy line found in the spectrum.
         @=Energy line not used for Weighted Mean Activity Energy Tolerance :                 10.000 keV Nuclide confidence index threshold=                      0.30 Errors quoted at 2.000 sigma

[1341]

Interference Corrected Activity Report 3/9/2018 4: 49: 55 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1.000 1.285870E+006 3.516492E+005 Co-60 1.000 3.113452E+005v 3.747248E+004 Cs-137 1.000 9.235109E+006J' 1. 131079E+006 Eu-152 1 .000 3.714419E+OOS..I 9.596186E+004 Eu-155 0.332 1.423329E+006 6.017879E+005 Bi-214 0.687 1.540257E+OOS 5.884069E+004 X Pb-214 0.383 

       ? :; Nuclide is part of an undetermined so lution X =   Nuclide rejected by the interference analysis
      @  =  Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at    2.000 sigma

[1342]

Interference Correcte d Activity Report 3/9/2018 4:49:55 PM Page s 

  **********    U N I D E N T I F I E D      P E A K S      **********

Peak Locate Performed on: 3/9/2018 4 :49:54 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 96 2.4165E+OOO 13. 10 2 75.06 1.8325E+OOO 19.52 8 778.45 6.4883E-002 55.64 Sum 9 963.58 1. 2271E- 001 3 1. 21 Tol. Ac-228 10 1085.59 3.3578E-002 102.61 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1343]

NucJ.ide MDA Report 3/9/2018 4:49:55 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 1.5M90D ECP 17.8 Sample

Title:

B1011l0AFSFC040GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/M" 2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10 .66 3.933E+005      3.93E+005  1.286E+006   1.800E+005
 +      Co-60      1173.23*    99.85  5.706E+004      2.89E+004  2.871E+005   2.687E+004 1332.49*    99.98   2.890E+004                3.326E+005   1.273E+004 Nb-94       702.65     99.81  5.488E+004      5.49E+004  9.406E+003   2.599E+004 871.09     99.89  5.550E+004                 8.495E+003   2.622E+D04 Ag-108m     433.90     90.50  1.327E+005      5.43E+004  3.632E+003   6.495E+004 61 4. 3 0  89.80  8.673E+004                 6.106E+003   4.180E+004 722.90     90.80  5.426E+004                -1. 755E+004  2.552E+004 Cs-134      604.72     97.62  8.056E+004      6.55E+004  6.066E+004/  3.885E+004 795.86     85.46  6.552E+004                 1. 877E+004  3.101E+004
 +      Cs-137      661.66*    85.10  9.983E+004      9.98E+004  9.235E+006~  4.823E+004
 +      Eu-152      121.78*    28.67  3.722E+005      1.09E+005  3.493E+005~  1.827E+005 34 4 .28*  26.60  3.396E+005                 2.519E+OOS   1.654E+005 1408.01*    21.07  1.087E+005                 4.lSOE+OOS   4.604E+004 Eu-154      123.07     40.40   4.429E+005     1.05E+005 -3.890E+004   2.190E+005 723.30     20.06   2.457E+005               -7.946E+004   1.155E+005 127 4 .43   34.80  1.046E+005                 4 .842E+004v 4 .742E+OD4
 +      Eu-155       86.55*    30.70  8.552E+005      8.55E+005  1.423E+006   4 .239E+005 105.31     21.10  9.321E+005                 5.897E+005   4.612E+005 Tl-208      583.19     85.00  9.464E+004      9.46E+004  4 .697E+004  4.569E+004 Bi-212      727.33       6.67 7.679E+005      7.68E+005  2.197E+005   3.620E+005 Pb-212      238.63     43.60  3.238E+005      3.24E+005 -1.640E+004   l .595E+005
 +      Bi-214      609.32*    45.49  9.260E+004      9.26E+004  1.128E+005   4.322E+004 1120.29*    14 .92  2.000E+005                4.341E+005   8.905E+004 1764.49     15 .30  2.171E+005                1 .847E+005  9.607E+004 Pb-214      295.22     18 .42 6.600E+005      2.54E+005 -1 .796E+005  3.239E+005 351.93*    35.60   2.538E+005                1 .882E+005  1 .236E+005 Ra-226      186.21       3.64  4.084E+006     4.08E+006  6.663E+006   2.015E+006 Ac-228      338.32     11.27  1 .123E+006     2.37E+005  6.184E+004   5.511E+005 911. 20    25.80   2.367E+005                3.258E+005   1.123E+005 968.97     15.80   4.374E+005               -2.427E+005   2.087E+OOS Am-241       59.54     35.90   7.200E+005     7.20E+005 -4.264E+004   3.554E+005
       +=Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1344]

        • ~********************************************************************
          • GAMM A S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/9/2018 12:46:45 PM Sample Title B101110AFSFC041GD Sample Description Ul LOWER CTMNT Sample Identification 041 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.0?0E+OOO MA2 Sample Taken On 3/9/2018 12:35:00 AM Acquisition Started 3/9/2018 12:36:42 PM Live Time 600. 0 seconds Real Time 602. 0 seconds Dead Time 0 . 34 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1 .SM90DECP17 BCM [1345]

Peak*Analysis Report 3/9/2018 12: 4 6:45 PM Page 2

          • PE AK A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSFC041GD Peak Analysis Performed on: 3/9/2018 12:46:45 PM Peak Analysis From Channe.l .: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 138 117 .29 29.03 3.05 2.35E+004 689.33 2.00E+004 2 297- 311 301.42 75 .07 0. 83 2.49E+002 190.59 3.04E+003 3 1369- 1389 1376.95 344 .00 1. 47 8.75E+001 77.53 3.89E+002 4 2631- 2661 2645.86 661.28 1. 73 6.67E+003 198.98 6.64E+002 5 3107- 3121 3113.46 778 .19 0.35 3.99E+001 22.25 2.91E+001 6 3461- 3474 3467.02 866.60 0.44 3.35E+001 20.74 2.65E+001 7 3847- 3863 3854.58 963.51 0.42 5.64E+001 24.67 3.06E+001 8 4332- 4349 4339. 81 1084 .83 0.33 3.95E+001 25.38 3.65E+001 9 4439- 4457 4447.49 1111.76 1. 22 7.69E+001 24.35 2.llE+OOl 10 4681- 4704 4691.94 1172.88 2.03 2.00E+002 39.76 4.93E+001 11 5319 - 5342 5329.06 1332.19 1. 60 1.92E+002 37.74 4.19E+001 12 5623- 5640 5631.58 1407.83 1. 31 6.89E+001 21. 77 1.51E+001 13 5833 - 5852 5842.61 1460.60 1. 22 8.68E+001 26. 54 2.52E+001 M 

 -  First peak in a mul tiplet region m "' Other peak in a mul tiplet region F =  Fitted singlet Errors quoted at     2 . 000 sigma

[1346]

Interference Corrected Activity Report 3/9/2018 12:46:45 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSFC041GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB

  • I * * * "' * * * * * * * * * * * * *
  • IDENTIFIED NUCLIDES * * * * * * * * * * * * *
  • I
  • a .. ~
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/M"2 ) Uncertainty K-40 1.000 1460.82* 10.66 1.06751E+006 3.3952SE+OOS Co-60 1.000 1173.23* 99.85 2.44889E+OOS 5.25489E+004 1332.49* 99.98 2.43981E+OOS 5.17657E+004 Cs-137 1.000 661.66* 85.10 8.27988E+006 1 .02460E+006 Eu-152 0.332 121.78 28.67 344.28* 26.60 2.88052E+OOS 2.59575E+OOS 1408.01* 21.07 4.23465E+005 1.38009E+005
          * = Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                     10.000 keV Nuclide confidence index threshold ~                        0 .30 Errors quoted at 2.000 sigma

[1347]

Interference Corrected Activity Report 3/9/2018 12:46:45 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"'2 ) Uncertainty K-40 1 .000 1.067513E+006 3.395247E+OOS Co-60 1 .000 2. 4442 79E+005 ./ 3.687766E+004 Cs-137 1 .000 8.279881E+006..J 1.024602E+006 Eu-152 0.332 3.936228E+005J' 1.218567E+005 X Pb-214 0.381 

      ? : Nuclide is part of an undetermined so lution x ~ Nuclide rejected by the interference analysis
      @~Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1348]

Interference Corrected Activity Report 3/9/20 18 12: 46: 45 PM Page 5 

  **********     U N I D E N T I F I E D      P EA K S         **********

Peak Locate Performed on: 3/9/2018 12:46:45 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak To l. No . (keV) Counts per Second  % Uncertainty Type Nuclide 1 29.03 3.9177E+001 2 . 93 2 75.07 4 .1491E-001 76.56 5 778.19 6.6582E-002 55.69 6 866.60 5.5875E-002 61. 87 7 963.51 9.3922E-002 43.78 Tol. Ac-228 8 1084.83 6.5768E-002 64.32 9 1111.76 l.2817E-001 3 1. 66 Tel. Bi-214 M "' First peak in a multiplet region m -= Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1349]

Nuclide MDA Report 3/9/2018 12:46:45 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSFC041GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) ( %) (pCi/M"2 ) (pCi/M ... 2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       1460.82*    10 .66 4.161E+005    4. 16E+OD5          1.068E+006   1.914E+005
 +      Co-60      1173.23*    99.85  5.973E+004    5.70E+004           2.449E+005   2.821E+D04 1332.49*    99.98  5.697E+004                        2.440E+005   2.677E+D04 Nb-94       702.65     99. 81 7.148E+004    6.89E+004           1.787E+004   3.429E+004 87 1 .09   99.89  6.888E+OD4                        4.365E+004   3.291E+D04 Ag-108m     433.90     90.50  1.389E+OD5    6.87E+004          -2.771E+004   6.806E+004 614.30     89.80  9.941E+004                        5.347E+004   4.814E+D04 722.90     90.80  6.873E+OD4                       -3.957E+003   3.275E+D04 Cs-134      604.72     97.62  8.876E+OD4    6.70E+004           4.052E+004/  4.295E+004 795.86     85.46  6.700E+OD4                       -3.492E+004   3.175E+004
 +      Cs-137      66 1 .66*  85.10  2.357E+OD5    2.36E+005           8.280E+006   1 .162E+005
 +      Eu-152      12 1 .78   28.67  6.489E+OD5    l.59E+005           6.369E+005   3.21DE+005 344.28*    26.60  4.163E+005                        2.881E+005   2.037E+005 1408.01*    21. 07 1.590E+005                        4.235E+005   7.118E+004 Eu-154      123.07     40. 40 4.550E+005    1.17E+005          -3.362E+005   2.251E+OD5 723.30     20.06  3.101E+005             O i""tJ j -8. 589E+004  l .478E+005 1274 .43    34.80  1.171E+OOS        c,.O           -3. 234E+O 04 5.368E+OD4 Eu-155       86.55     30.70  9.114E+OOS    9.11E+005           1.253E+006   4.521E+OOS 105.31     21. 10 9.341E+OOS                        5.726E+004   4.622E+005 Tl-208      583.19     85.00  9.982E+004    9.98E+004           1.900E+004   4.828E+004 Bi-212      727.33      6.67  8.673E+005    8.67E+005          -6.124E+005   4.117E+005 Pb-212      238.63     43.60  3.299E+005    3.30E+005          -2.856E+005   l .625E+005 Bi-214      609.32     45.49  1 .9D7E+005   1 .91E+005          1.915E+005   9.230E+004 1120.29     14.92  4.352E+005                        2.138E+005   2.067E+005 1764.49     15.30  2.441E+005                        2.401E+005   1. 095E+005 Pb-214      295.22     18.42  6.814E+005    3 .l lE+OOS         5.217E+005   3.345E+005 351 .93*   35.60  3.lllE+OOS                        2.152E+005   l.522E+005 Ra-226      186.21      3.64  4 .242E+006   4.24E+006          -2.709E+006   2.094E+006 Ac-228      338.32     11. 27 1.130E+006    2. 5 2E+OOS         9.301E+004   5.543E+005 91 1. 20   25.80  2.523E+005                        l .308E+005  1. 201E+005 968.97     15.80  4.686E+005                        5.543E+OOS   2.243E+005 Am-241       59.54     35.90  1.986E+006    1.99E+006          -3.077E+006   9.884E+005
       +=Nuclide identified during the nuclide i dentification
       * ~ Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1350]

        • ~********************************************************************
          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/9/2018 1 :11:07 PM Sample Title B101ll0AFSFC042GD Sample Description Ul LOWER CTMNT Sample Identification 042 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO MA2 Sample Taken On 3/9/2018 1:00:00 PM Acquisition Started 3/9/2018 1: 01: 04 PM Live Time 600. 0 seconds Real Time 602. 1 seconds Dead Time 0.35 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1 .5M90DECP17 8CM [1351]

Peak, Analysis Report 3/9/2018 1:11:07 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

Bl01110AFSFC042GD Peak Analysis Performed on: 3/9/2018 1:11:07 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 118- 155 129.31 32.03 1. 31 7.99E+002 162.97 9.88E+002 2 281- 311 301.26 75.03 1. 54 1. 21E+003 222.93 2.30E+003 3 330- 346 341.08 84.98 0.39 1.16E+002 142.88 1. 59E+003 4 484- 496 488.89 121.94 1. 04 1.92E+002 100.70 8.87E+002 5 609- 620 614.92 153.46 0.77 4.82E+001 77.85 5.85E+002 6 702- 715 708.89 176.95 0.65 -2.34E+OOO 78.07 5.52E+002 7 975- 988 981.03 245 .00 0.58 5.43E+001 67.90 3.98E+002 8 1175- 1188 1182.34 295.33 0.80 2.84 E+001 53.71 2.52E+002 9 1363- 1387 1377.66 344.17 0.42 1.60E+002 80.99 3.59E+002 10 2430- 2444 2437.29 609.12 1. 02 5.90E+001 30.86 6.20E+001 11 2630- 2660 2646.08 661.33 1. 75 7.19E+003 175.72 1.06E+002 12 3108- 3124 3115.42 778.68 1.04 5.45E+001 25.66 3.45E+001 13 3847- 3864 3855.21 963.66 0.50 6.92E+001 24.99 2.68E+001 14 4332- 4350 4342.43 1085.49 0.30 4.68E+001 25.81 3.52E+001 15 4438- 4457 4447.81 1111.84 1. 81 5.55E+001 27.35 3.75E+001 16 4679- 4704 4692.39 1172.99 1. 94 2.49E+002 37.17 2.27E+001 17 5317- 5342 5329.89 1332.39 1. 70 2.45E+002 37.85 2.64E+001 18 5621- 5642 5631.07 1407.70 1. 41 1.29E+002 25.05 7.59E+OOO 19 5833- 5854 5842.65 1460.61 1. 68 1. 41E+ 002 25.86 7.47E+OOO M First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1352]

Inte.r ference Corrected Activity Report 3/9/2018 1:11:07 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

Bl01110AFSFC042GD Nuclide Library used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  ....................... IDENTIFIED NUCLIDES             * *
  • t ;;, * * * * * * * '" * * *
  • I I I Nuclide Id Energy Yield Activity Activity Name Confidence {keV) (%) (pCi/MA2 ) Uncertainty K-40 1. 000 1460.82* 10 .66 1 .72917E+006 3.51886E+OOS Co-60 1. 000 1173.23* 99.85 3.05752E+OOS 5.17327E+004 1332.49* 99.98 3.1073!:>E+OO!::i 5.41243E+004 Cs-137 1 . 000 661.66* 85. 10 8.93494E+006 1 .09499E+006 Eu-152 1 .000 1 21.78* 28.67 4.87212E+005 2.73405E+005 344.28* 26.60 5.27560E+005 2.80402E+005 1408.01* 21.07 7.95210E+005 1.66547E+OOS Eu-155 0.332 86.55* 30.70 3.15249E+005 3.93690E+005 105. 31 21. 10 Pb-212 0. 937 238.63* 43.60 9.84642E+OD4 1.24056E+005 Bi-214 0.688 609.32* 45.49 1 .34235E+OOS 7.20409E+004 1120.29* 14.92 4.48990E+OOS 2.24209E+005 1764.49 15.30 Ra-226 0 .872 186.21* 3.64 -4.66669 E+004 1.55546E+OD6
        *=Energy line found in the spectrum.
        @=Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold -            0.30 Errors quoted at 2.000 sigma

[1353]

Inte,r ference Corrected Activity Report 3/9/2018 1 : 11: 07 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1. 000 1 .729168E+006 3.518857E+005 Co-60 1. 000 3.081310E+005./ 3.739743E+004 Cs-137 1. 000 8.934940E+006'1 1 .094986E+006 Eu-15:2 1. 000 6.741364E+005J 1 .268488E+005 Eu-155 0 .332 3.152487E+005 3.936898E+OOS Pb-212 0 .937 9.846423E+004 1 .240557E+OOS Bi-214 0 .688 l .636893E+OOS 6.858734E+004 X Pb-214 0 .938 Ra-226 0 .872 -4.666693E+004 1 .SS5464E+006 

        ? ,e:: Nuclide is part of an undetermined so lution X = Nuclide rejected by the interference analysis
           -   Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .000 sigma

[1354]

Interference Corrected Activity Report 3/9/2018 1: 11: 07 PM Page 5 

  **********       U N I D E N T I F I E D     P E A K S     **********

Peak Locate Performed on: 3/9/2018 1 : 11 : 07 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.03 1 .3322E+OOO 20.39 2 75.03 2.0218E+OOO 18.38 5 153.46 8.0350E-002 161. 48 D-Esc . 8 295.33 4.7315E-002 189 . 20 Sum 12 778.68 9.0838E-002 47.08 Sum 13 963.66 1.1535E-001 36.11 14 1085.49 7.7978E-002 55.16 M _, First peak in a multiplet region m = Other peak in a multiplet region F .,,. Fitted singlet Errors quoted at 2 . 000 sigma [1355]

Nuclide MDA Report 3/9/2018 1: 11 :07 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSFC042GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL .NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +       K-40      1460.82*     10.66  2.425E+005    2.42E+005    1.729E+006   1. 046E+005
 +       Co-60     1173.23*     99.85  4.287E+004    4.29E+004    3.058E+OOS   1.978E+004 1332.49*     99.98  4.797E+004                 3.107E+005   2.227E+004 Nb-94       702.65     99.81  5.90SE+004    5.90E+004    4.40SE+004   2.807E+004 87 1 .09   99.89  6.031E+004                 2.620E+004   2.862E+004 Ag-108m     433.90     90.50  1.333E+005    6.39E+004  -2.243E+004    6.526E+004 614.30     89.80  9.714E+004                2.440E+004    4.701E+004 722.90     90.80  6.387E+004               -2.671E+004    3.032E+004 Cs-134      60 4 .72   97.62  8.815E+004    6.81E+004    7.975E+004.I 4.264E+004 795.86     85.46  6.810E+004                2.190E+004    3.230E+004
 +       Cs-137      66 1 .66*  85.10  9.703E+004    9.70E+004    8.935E+006   4.683E+004
 +       Eu-152      121.78*    28.67  4 .108E+005   l. 23E+005  4.872E+005    2.020E+005 344.28*    26.60  4 .256E+005               5.276E+005    2.083E+005 1408.01*     21. 07 1 .225E+005               7.952E+005    5.295E+004 Eu-154      123.07     40.40  4.564E+005    1.21E+005   4 .999E+OOSv  2.258E+005 723.30     20.06  2.914E+005                3.965E+004    1.384E+005 1274.43      34.80  1.209E+005               -2.252E+004    5.560E+004
 +       Eu-155       86.55*    30.70  6.393E+005    6.39E+005   3.152E+005    3.160E+005 105.31     21.10  9.281E+OOS               -l.123E+O 05   4.592E+OOS Tl-208      583.19     85.00  8.988E+004    8.99E+004   1.073E+003    4.331E+004 Bi-212      727.33      6.67  8.776E+OOS    8.78E+005  -1.044E+006    4.169E+005
 +       Pb-212      238.63*    43.60  2.02SE+005    2.02E+005   9.846E+004    9.878E+004
 +       Bi-214      609.32*    45.49  1. 063E+005   1.06E+005   1.342E+005    5.008E+004 1120.29*     14.92  3.272E+005                4.490E+005    1.526E+005 176 4. 49    15. 30 2.355E+005                2.216E+005    1 .052E+005 Pb-214      295.22*    18.42  4.053E+005    3.18E+005   1.289E+OOS    1 .965E+005 351.93*    35.60  3.180E+005                3.942E+005    1.557E+005
 +       Ra-226      186.21*     3.64  2.61SE+006   2.61E+006   -4.667E+004    1.280E+006 Ac-228       338.32     11. 27 1.109E+006   2. 4 0E+005  7.069E+005    5.440E+005 911. 20    25.80  2.404E+005                1.732E+005    1.142E+005 968.97     15.80  4.553E+005                7.773E+OOS    2.177E+005 Am-241        59.54     35.90  7.336E+005    7.34E+005   3.568E+005    3.622E+005
       +=Nuclide identified during the nuclide i dentification
       *=Energy line found in the spectrum
       >    Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1356]

          • GAMM A S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002547.CNF Report Generated On 3/8/2018 5:29:30 PM Sample Title B101110AFSCC043GD Sample Description Ul LOWER CTMT Sample Identification 043 Sample Type GAMMA DIRECT Sample Geometry Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO M"2 Sample Taken On 3/8/2018 3:05:00 PM Acquisition Started 3/8/2018 3:03:00 PM Live Time 600 . 0 seconds Real Time 601.3 seconds Dead Time 0 . 22 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1.5M90DECP17 8CM (_

_ -~-l /~*~ /
                                                                      !         **11 C
                                                                                  -  I f      /   ""*"*
                                                                                 . l   _(...
                                                   /\/         \        ,._....

s{' t-* [1357]

Peak Analysis Report 3/8/2018 5:29:30 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name : 54 52 Sample

Title:

B1 01110AFSCC043GD Peak Analysis Performed on: 3/8/2018 5:29:30 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 118- 138 129.29 32.03 1. 15 2.26E+002 69.67 2.70E+002 2 285- 310 301.20 75. 01 0.95 4.77E+002 149.81 1.20E+003 3 335- 345 340.68 84.89 0.85 8.86E+001 73.13 5.24E+002 4 1494- 1505 1499.52 374.64 0.36 1.09E+001 26.03 6.31E+001 5 2431- 2445 2438.17 609.34 0.84 3.35E+001 21. 63 2.85E+001 6 2634- 2659 26 47 .40 661.66 1. 60 2.00E+003 92.13 2.94E+001 7 4687- 4702 4694.68 1173.56 1. 23 4.94E+001 19.01 l.36E+001 8 5323- 5342 5332.00 1332.92 0.59 4.97E+001 17. 31 7.28E+OOO 9 5835- 5856 5845.08 1461.21 1. 79 l .10E+002 22.82 5.50E+OOO 10 7055- 7070 7062.24 1765. 55 0.50 2.SOE+OOl 10.00 O.OOE+OOO M = First peak in a multiplet region m == Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1358]

Interference Corrected Activity Report 3/8/2018 5:29:30 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSCC043GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name confidence (keV) (%) (pCi/M"'2 ) Uncertainty K-40 1.000 1460.82* 10.66 1.34762E+006 3.0423SE+OOS Co-60 1.000 1173.23* 99.85 6.05620E+004 2.38082E+004 1332.49* 99.98 6.31580E+004 2.25661E+004 Cs-137 1.000 661.66* 85. 10 2.48020E+006 3.19081E+005 Eu-155 0.331 86.55* 30.70 2.41302E+OOS 2.04887E+005 105.31 21.10 Bi-214 0 .695 609.32* 45.49 7.62551E+004 5.00645E+004 1120. 29 14.92 1764. 49* 15.30 2.30912E+005 9.41984E+004 

       *=Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold=            0.30 Errors quoted at 2. 000 sigma

[1359]

Interference Corrected Activity Report 3/8/2018 5: 29: 3 0 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1 .000 l.347617E+006 3.042352E+OOS Co-60 1 .000 6.192949E+004./ l.637817E+004 Cs-137 1 .000 2.480205E+006./ 3.190806E+OOS Eu-155 0.331 2.413016E+OOS 2.048866E+OOS Bi-214 0.695 1.103191E+OOS 4.420858E+004 

      ?    Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ ~ Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1360]

Interference Corrected Activity Report 3/8/2018 5:29:30 PM Page 5 

  **********    U N I D E N T I F I E D      P E A K S    **********

Peak Locate Performed on: 3/8/2018 5: 29: 30 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.03 3.7749E-001 30.76 2 75.01 7.9578E-001 31.38 4 374.64 1. 8176E-002 238.69 M ; First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1361]

Nuclide MDA Report 3/8/2018 5:29:30 PM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample

Title:

B101110AFSCC043GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nucl ide MDA Activity Dec. Level Name (keV) ( %) (pCi/M"'2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*   10. 66 2.174E+005    2.17E+OOS    1 .348E+006  9.205E+004
 +      Co-60      1173.23*   99.85  2.913E+004    2.44E+004     6.056E+004  1.291E+004 1332.49*   99.98  2.443E+004                  6.316E+004  1 .049E+004 Nb-94        702.65   99.81  3.863E+004    3.76E+004   -2.063E+004   l .786E+004 871.09   99.89  3.762E+004                -3.266E+004   1 .728E+004 Ag-108m      433.90   90.50  8.739E+004    3.82E+004   -1.197E+004   4.229E+004 614.30   89.80  6.487E+004                 4.339E+004   3.087E+004 722.90   90.80  3.824E+004                -3.719E+004   1. 751E+004 Cs-134       604.72   97.62  6.277E+004    4.35E+004    3.375E+004~  2.995E+004 795.86   85.46  4.346E+004                 7.923E+003   1. 998E+004
 +      Cs-137       661.66*  85.10  4.912E+004    4.91E+004    2.480E+006   2.288E+004 Eu-152       121 .78  28.67  4 .600E+005   1.60E+OOS   -3.236E+005   2.266E+005 344.28   26.60  2.859E+005                -1 .337E+005  1.385E+005 1408.01    21.07  1. 596E+005                l. 105E+005~ 7.148E+004 Eu-154       123.07   40 .40 3.247E+005    7.89E+004    5.099E+004~  1.599E+005 723.30   20.06  l .751E+005               -8.090E+004   8.024E+004 1274.43    34.80  7.887E+004                 3.455E+004   3.456E+004
 +      Eu-155        86.55*  30.70  3.239E+005    3.24E+OOS    2.413E+005   l .583E+OOS 105. 31  21.10  6.871E+005                -4.432E+005   3.387E+005 Tl-208       583.19   85.00  6.787E+004    6.79E+004    4.425E+004   3.231E+004 Bi-212       727.33    6.67  5.559E+005    5.56E+005    2.839E+005   2.560E+005 Pb-212       238.63   43.60  2.239E+OOS    2.24E+005    1.458E+005   1. 095E+O 05
 +      Bi-214       609.32*  45.49  7.455E+004    2.50E+004    7.626E+004   3.419E+004 1120.29    14.92  3.043E+005                 7.544E+004   1.412E+OOS 1764.49*   15.30  2.499E+004                 2.309E+005   O.OOOE+OOO Pb-214       295.22   18.42  4.244E+005    2. 1 2E+005 -1.032E+OOS   2.061E+OOS 351. 93  35.60  2.122E+005                 1 .125E+005  1 .027E+005 Ra-226       186.21    3.64  3.071E+006    3.07E+006    2.370E+006   l .508E+006 Ac-228       338.32   11. 27 6.613E+005    1. 71E+005  -3.035E+OOS   3.202E+OOS 911. 20  25.80  1.709E+005                 5.710E+004   7.942E+004 968.97   15.80  2.966E+005                 1. 420E+O 05 1. 383E+005 Am-241        59.54   35.90  5.421E+005    5. 4 2E+OOS  3.610E+005   2.665E+005
       + ; Nuclide identified during the nuclide identification
       * ~ Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ ~ Half-life too short to be able to perform the decay correction

[1362]

    • ~**********************************************************************
          • GAMM A S P E C T R U M A N A L Y S I S *****

Filename: C:\GENIE2K\CAMFILES\00002557.CNF Report Generated on 3/9/2018 4:44:18 PM Sample Title B101110AFSCC044GD Sample Description Ul LOWER CTMNT Sample Identification 044 Sample Type GAMMA DIRECT Sample Geometry 1. SM9 OD ECP 1 7 . 8 Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 8192 Peak Area Range (in channels) 85 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO MA2 Sample Taken On 3/9/2018 7:59:00 PM Acquisition Started 3/9/2018 8:00:06 AM Live Time 600.0 seconds Real Time 601.0 seconds Dead Time 0 . 17 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1. 5M90DECP17 BCM [1363]

Peak Analysis Report 3/9/2018 4:44:18 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSCC044GD Peak Analysis Performed on: 3/9/2018 4:44: 1 7 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 112- 126 116. 13 28.74 0.64 5.45E+001 46.68 1.44E+002 2 289- 310 301.24 75.02 1. 55 7.07E+002 139.71 1.11E+003 3 337- 347 341.20 85.01 1. 10 1.51E+002 81.21 6.21E+002 4 1372- 1412 1406.98 351.50 0.75 -1.45E+001 81. 26 2.68E+002 5 2325- 2338 2331.27 582.62 1. 33 3.78E+001 18.46 l.72E+001 6 2427- 2445 2436.34 608.89 0.61 6.37E+001 25.22 2.83E+001 7 2633- 2658 2645.85 661.27 1. 51 6.94E+002 59.95 4.84E+001 8 4684- 4700 4690.69 1172.57 0.71 5.89E+001 17.62 6.05E+OOO 9 5323- 5339 5330.23 1332.48 0.79 3.55E+001 17.74 1 .3SE+001 10 5625- 5640 5632.32 1408.01 1.17 3.12E+001 12.09 1 .83E+OOO 11 5831- 5853 5842.27 1460.51 1. 76 1 .40E+002 29.48 2.00E+OOl M m 

 =

First peak in a mul tiplet region Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1364]

Interference Corrected Activity Report 3/9/2018 4:44: 18 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSCC044GD Nuclide Li*brary Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * * * *
  • Ii I I * * * * *
  • f *
  • IDENTIFIED NUCLIDES . ........ ......... .

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 1 .000 1460.82* 10.66 1. 72299E+006 3.92344E+005 Co-60 1 .000 1173.23* 99.85 7.22634E+004 2.23579E+004 1332.49* 99.98 4.50367E+004 2.28103E+004 Cs-137 1 .000 661.66* 85.10 8.61429E+005 1.27460E+005 Eu-152 0 .304 121. 78 28.67 344.28* 26.60 -4.79366E+004 2.69339E+005 1408 . 01* 21.07 1.91522E+005 7.58354E+004 Eu-155 0.332 86.55* 30.70 4. 11371E+ 005 2.35602E+005 105 .31 21.10 Tl-208 0.999 583.19* 85.00 4.54508E+004 2.28853E+004 Bi-214 0.405 609.32* 45.49 1.44983E+005 5.99718E+004 1120 .29 14.92 1764.49 15.30 

          * ~ Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                     10.000 keV Nuclide confidence index threshold=                         0.30 Errors quoted at 2 .000 sigma

[1365]

Interference Corrected Activity Report 3/9/2018 4:44:18 PM Page 4

          • INTER FER.ENCE C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA 2 ) Uncertainty K-40 1. 000 1.722990E+006 3.923441E+005 Co-60 1. 000 5.892275E+004./ 1 .596696E+004 Cs-137 1. 000 8.614294E+005..I 1 .274600E+005 Eu-152 0.304 1.915218E+005~ 7.583539E+004 Eu-155 0.332 4 .113705E+005 2.356020E+005 Tl-208 0.999 4 .545081E+004 2.288533E+004 Bi-214 0.405 1.449826E+005 5.997182E+004 X Pb-214 0.445 

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1366]

Interference Corrected Activity Report 3/9/2018 4: 44: 18 PM Page 5 

  **********    U N I D E N T I F I E D      P E A K S     **********

Peak Locate Performed on: 3/9/2018 4: 44: 17 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 28.74 9.0819E-002 85.67 2 75.02 1.1776E+OOO 19. 77 M ; First peak in a multiplet region m ~ Other peak in a multiplet region F ~ Fitted singlet Errors quoted at 2 . 000 sigma [1367]

Nuclide MDA Report 3/9/2018 4: 44:18 PM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: 1.5M90D- ECP- 17.8 Sample

Title:

Bl01110AFSCC044GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +       K-40      1460.82*     10.66   3.890E+005    3.89E+005         1.723E+006  1.778E+005
 +       Co-60     1173.23*     99.85   2.073E+004    .2. 07 E+004,.,   7. 226E+004 8.708E+003 1332.49*     99.98   3.089E+004                     4.504E+004   1 .373E+004 Nb-94       702.65     99. 81  4.000E+004    4.00E+004       -4.686E+004   1 .855E+OD4 871. 09    99.89   3.995E+004                    -l .994E+003  1.844E+004 Ag-108m      433.90     90.50   6.368E+004    5.27E+004       -2.999E+004   3.044E+D04 61 4 .30   89.80   7.068E+004                    -1.115E+003   3.378E+004 722.90     90.80   5.274E+004                     3.449E+004   2.476E+004 Cs-134      604.72     97.62   6.233E+004    5.01E+004        3.428E+004/  2.973E+004 795.86     85.46   5.014E+004                     1.844E+004   2.332E+004
 +       Cs-137      66 1 .66*  85.10   6.186E+004    6. 1 9E+004      8.614E+005   2.925E+004
 +       Eu-152      12 1 .78   28.67   4.754E+005    6.34E+004        2.630E+005   2.342E+005 344.28*    26.60   4.538E+005                    -4.794E+004   2.224 E+005 1408.01*     21.07   6.341E+OD4                     1. 915E+O 05 2.339E+004 Eu-154      123.07     40. 40  3.351E+005    1.05E+OD5        2.128E+005   1.651E+005 723.30     20.06   2.387E+005                     1.354E+005   1.121E+005 1274.43      34.80   1.046E+005                     5.494E+004   4. 741E+004
 +       Eu-155       86.55*    30.70   3.535E+005    3.53E+005        4.114E+005   1.731E+005 105.31     21.10   7.366E+005                     5.557E+005   3.634E+005
 +       Tl-208      583.19*    85.00   3.054E+004    3.05E+004        4. 545E+004  1.364E+004 Bi-212      727.33       6.67  7.063E+005    7.06E+005       -1.713E+005   3.312E+OD5 Pb-212      238.63     43.60   2.065E+005    2.06E+005        9.709E+004   1 .00BE+OOS
 +       Bi-214      609.32*    45.49   7.923E+004    7.92E+004        1. 450E+OOS  3.654E+004 1120.29      14.92   3.093E+005                    -3.492E+005   l .437E+OD5 1764.49      15.30   2.680E+005                     2.18DE+005   1 .215E+OOS Pb-214      295.22     18.42   3.953E+005    3.39E+005       -7.408E+003   1.915E+OOS 351.93*    35.60   3.391E+005                    -3.582E+004   1.662E+005 Ra-226      186.21       3.64  2.907E+006    2.91E+006       -2.318E+006   1.426E+006 Ac-228       338.32     11. 27  6.119E+OOS    1.91E+005       -3.704E+005   2.955E+OOS 911.20     25.80   1 .911E+005                    2.357E+005   8.954E+004 968.97     15.80   2.966E+005                    -l.773E+005   l.383E+OOS Am-241        59.54     35.90   5.809E+OOS    5.81E+005        5.747E+004   2.859E+005
       +    Nuclide identified during the nuclide identification
       * = Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ = Half-life too short to be able to perform the decay correction

[1368]

          • GAMMA S P E C T R U M ANALYSIS *****

Filename: C:\GENIE2K\CAMFILES\00002558 .CNF Report Generated On 3/9/2018 4:45:23 PM Sample Title B101110AFSCC045GD sample Description Ul LOWER CTMNT Sample Identification 045 Sample Type GAMMA DIRECT Sample Geometry 1.5M90D ECP 17.8 Peak Locate Threshold 3.00 Peak Locate Range (in channels) BS - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 7.070E+OOO M ... 2 Sample Taken On 3/9/2018 8:22: 00 AM Acquisition Started 3/9/2018 8:23:04 AM Live Time 600.0 seconds Real Time 601.5 seconds Dead Time 0 . 25 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 3/7/2018 Efficiency ID 1.5M90DECP17 8CM [1369]

Peak Analysis Report 3/9/2018 4:45:23 PM Page 2

          • PE AK ANALYS I s R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSCC045GD Peak Analysis Performed on: 3/9/2018 4:45:23 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 122 117.32 29.04 1.18 6.35E+001 37.62 1.00E+002 2 153- 193 160.93 39.94 1.22 2.32E+002 153.94 9.21E+002 3 253- 265 260.62 64.87 0.72 5.56E+001 85.99 6.80E+002 4 287- 307 3 01. 10 74.99 0.92 7.56E+002 160.90 1. 58E+O 03 5 328- 346 339.92 84.69 0.69 1. 75E+002 143.89 1.47E+003 6 480- 499 487.89 121.69 0.99 4.80E+002 129.30 1.05E+003 7 621- 632 626.06 156.24 1.33 5.54E+001 65.45 4.04E+002 8 973- 987 979.67 244.66 1.15 8.16E+001 59.93 2.82E+002 9 1369- 1414 1377.22 344.06 1.41 2.72E+002 113.78 4.26E+002 10 1855- 1868 1861.95 465.27 0.33 2.70E+001 28.30 6.30E+001 11 2326- 2341 2332.80 583. 00 0.41 2.41E+001 30.87 7.09E+001 12 2428- 2443 2436.57 608.94 0.72 7.51E+001 30.78 5.39E+001 13 2633- 2655 2645.76 661.25 1. 47 7.66E+002 65.41 7.78E+001 14 3107- 3124 3114 .32 778.41 0.41 1. 53E+O 02 32.22 3.21E+001 15 3461- 3475 3468.38 866.94 1. 06 3.70E+001 21. 69 2.80E+001 16 3843- 3865 3854.28 963.43 0.89 1. 64E+O 02 37.58 4.88E+001 17 4333- 4351 4342.26 1085.44 1.16 7.81E+001 30.54 4.39E+001 18 4438- 4457 4446. 51 1111 . 51 1.61 l .13E+002 32.48 4.34E+001 19 4683- 4703 4691.90 1172.87 1. 59 2.14E+002 34.08 2.17E+001 20 5319- 5339 5328.87 1332.14 1. 91 1.77E+002 31. 93 2.19E+001 21 5620- 5643 5631.18 1407 .73 1.47 1.90E+002 33.50 2.31E+001 22 5832- 5853 5842.63 1460.60 1. 59 1.34E+002 26.40 1.08E+001 23 7048- 7063 7055.90 1763.97 0 .29 1.71E+001 11. 83 5.95E+OOO M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F ""' Fitted singlet Errors quoted at 2 . 000 sigma [1370]

Interference Corrected Activity Report 3/9/2018 4: 45 ; 23 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSCC045GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . . ......... . ....... . .      IDENTIFIED NUCLIDES             * *
  • I *
  • a * * *
  • a * * * * * * *
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/M ... 2 ) Uncertainty K-40 1. 000 1460.82* 10.66 1. 65184E+006 3.55100E+005 Co-60 1 . 000 1173.23* 99.85 2.62745E+005 4.67804E+004 1332.49* 99.98 2.24863E+005 4.43674E+004 Cs-137 1. 000 661.66* 85. 10 9.51570E+005 1.40213E+005 Eu-152 1.000 1 21 .78* 28.67 1.21701E+006 4.08772E+005 344.28* 26.60 8.93774E+005 4.02348E+005 1408.01* 21.07 1 .16725E+006 2.26064E+005 Eu-155 0 .331 86.55* 30.70 4.78322E+005 4.04144E+OOS 105.31 21.10 Tl-208 1 .000 583.19* 85.00 2.89739E+004 3.73337E+004 Pb-212 0 .944 238.63* 43.60 l.47710E+005 1 .11146E+005 Bi-214 0 .976 609.32* 45.49 1.70961E+005 7.29739E+004 1120 .29* 14.92 9.11020E+005 2.72804E+005 17 64.49* 15.30 l .57468E+005 1.09971E+005 Am-241 0.956 59.54* 35.90 1.68421E+005 2.62791E+005
         *=Energy line found in the spectrum.
         @=Energy line not used for Weighted Mean Activity Energy Tolerance :         10.000 keV Nuclide confidence index threshold=              0.30 Errors quoted at 2. 000 sigma

[1371]

Interference Corrected Activity Report 3/9/2018 4: 45: 23 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1. 000 1.651841E+006 3.551004E+005 Co-60 1. 000 2.428019E+005,J 3.219177E+004 Cs-137 1. 000 9.515696E+005.J 1 .402127E+005 Eu-152 1. 000 1.123393E+006..t l .775287E+005 Eu-155 0.331 4.783219E+OOS 4.041443E+005 Tl-208 1.000 2.897394E+004 3.733374E+004 Pb-212 0.9 44 1 .47710DE+005 1. 111463E+005 Bi-214 0.976 2.020564E+005 5.934833E+004 X Pb.:..214 0.382 Am-241 0 .956 1 .684213E+D05 2.627915E+OOS 

      ? = Nuclide is part of an undetermined so lution X "' Nuclide rejected by the interference analysis
      @  = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1372]

Interference Corrected Activity Report 3/9/2018 4: 45: 23 PM Page 5 

  **********       U N I D E N T I F I E D     P E A K S     **********

Peak Locate Performed on: 3/9/2018 4:45:23 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV) Counts per Second  % Uncertainty Type Nuclide 1 29.04 1.0587E-001 59.22 2 39.94 3.8657E-001 66.37 4 74.99 1.2593E+OOO 21. 30 7 156.24 9.2295E-002 118.18 D-Esc . 10 465.27 4 .SOOOE-002 10 4.82 Sum 14 778.41 2.5491E-001 21. 07 Sum 15 866.94 6.1603E-002 58.68 16 963.43 2.7373E-001 22.88 Tol. Ac-228 17 1085.44 1. 3012E-001 39.12 M - First peak in a multiplet region m  := Other peak in a multiplet region F ~ Fitted singlet Errors quoted at 2 . 000 sigma [1373]

Nuclide MDA Report 3/9/2018 4:45:24 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 1.5M90D- ECP- 17.8 Sample

Title:

B101110AFSCC045GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL .NLB Nuclide Energy Yield Line MDA Nucl ide MDA Activity Dec. Level Name (keV) (%) (pCi/M ... 2 ) (pCi/M ... 2 ) (pCi/M ... 2 ) (pCi/M"2 ) 

 +      K-40       1460.82*    10.66   2.893E+OOS      2.89E+OOS      1.652E+006      1 .280E+OOS
 +      Co-60      1173.23*    99.85   3.852E+004      3.85E+004      2.627E+005      1 .760E+004 1332.49*    99.98   4.031E+004                     2.249E+005      1.844E+004 Nb-94       702.65     99. 81  5.927E+004      5.93E+004      1.460E+004      2.818E+004 871.09     99.89   7.076E+004                    -2.510E+004      3.385E+004 Ag-108m     433.90     90.50   8.572E+004      7.24E+004     -5.799E+003      4.146E+004 614.30     89.80   8.878E+004                    -3.799E+004      4.283E+004 722.90     90.80   7.237E+004                     2.663E+004      3.458E+004 Cs-134      604.72     97.62   8.149E+004      7.92E+004      7.229E+004J     3.931E+004 795.86     85.46   7.922E+004                     4.550E+004      3.786E+004
 +      Cs-137      661. 66
  • 85.10 7.456E+004 7.46E+004 9.516E+005 3.560E+004
 +      Eu-152      121. 78*   28.67   S.148E+005      2.09E+OOS      1.217E+006      2.540E+OOS 344.28*    26.60   S.987E+005                     8.938E+OOS      2 . 949E+005 1408.01*    21. 07  2.091E+005                     1.167E+006      9.625E+004 Eu-154      123.07     40 .40  4.313E+005      1.43E+005      1. 049E+006 .,  2.132E+005 723.30     20.06   3.276E+OOS                     2.712E+005      1.565E+005 1274 .43    34.80   1. 428E+005                    1 .361E+OOS     6.653E+004
 +      Eu-155       86.55*    30.70   6.423E+005      6. 4 2E+OOS    4.783E+005      3.174E+OOS 105.31     21.10   8.845E+005                     2.764E+005      4.374E+OOS
 +      Tl-208      583.19*    85.00   6.123E+004      6. 1 2E+004    2.897E+004      2.899E+004 Bi-212      727.33       6.67  9.745E+005      9.75E+005      3.429E+005      4.653E+OOS
 +      Pb-212      238.63*    43.60   1. 752E+O 05    1.75E+OOS      1. 4 77E+005    8.513E+004
 +      Bi-214      609.32*    45.49   1. 013E+005     1.0lE+OOS      1.710E+OOS      4.758E+004 112 0 .29*  14.92   3.493E+005                     9.110E+005      l.637E+005 176 4 .49*  15.30   1. 537E+005                    1. 575E+005     6.434E+004 Pb-214      295.22     18.42   5.191E+005      4.47E+OOS      2.018E+005      2.534E+OOS 351. 93
  • 35.60 4.473E+005 6.678E+OOS 2.203E+005 Ra-226 186.21 3.64 3.585E+006 3.58E+006 3.065E+005 1.765E+006 Ac-228 338.32 11. 27 9.554E+005 2.68E+OOS -7.305E+004 4.672E+OOS 911. 20 25.80 2.678E+005 7.000E+004 1.279E+005 968.97 15. 80 6.112E+005 3.220E+005 2.956E+OOS
 +      Am-241       59.54*    35.90   4.304E+005      4 .30E+005     1.684E+OOS      2.lllE+OOS
       + ~ Nuclide identified during the nuclide identification
       * = Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ = Half-life too short to be able to perform the decay correction

[1374]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/10/2018 12:42:02 PM Sample Title B101110AFSWC046GD Sample Description Ul LOWER CTMNT Sample Identification 046 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"2 Sample Taken On 3/10/2018 12:32:00 AM Acquisition Started 3/10/2018 12:31:59 PM Live Time 600.0 seconds Real Time 602.3 seconds Dead Time 0 . 38 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM 5o F - [1375]

Peak'Analysis Report 3/10/2018 12:42:02 PM Page 2

          • PE AK A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B1 01110AFSWC046GD Peak Analysis Performed on: 3/10/2018 12:42:02 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area Uncert. Counts 1 113- 139 130.64 32.37 1. 92 6.32E+002 93.83 3.49E+002 2 156- 170 161.66 40.12 1.13 2.34E+002 89.81 6.12E+002 3 280- 313 301.94 75.20 1. 46 1 .41E+003 270.30 3.21E+003 4 330- 351 340.28 84.79 1. 55 4.13E+002 192.53 2.36E+003 5 481- 501 489.39 122.07 1.37 7 .04E+ 002 163.38 1.64E+003 6 976- 991 981 .01 244.99 0.87 1 .04E+002 75.04 4 .32E+002 7 1365- 1388 1378.57 344.40 1. 66 5.70E+002 84.59 3.05E+002 8 2431- 2449 2438.43 609.41 0 .35 6.33 E+001 38.49 9.07E+001 9 2631- 2662 2647. 00 661.56 1. 93 3.61E+003 130.29 1.28E+002 10 3106- 3127 3116. 12 778.86 1. 77 2.09E+002 44.26 7.53E+001 11 3460- 3477 3470.18 867.39 0. 67 6.85E+001 30.44 4.75E+001 12 3844- 3869 3855.70 963.78 1. 71 2.03E+002 46.13 7.73E+001 13 4332- 4353 4344.03 1085.89 1.78 1.39E+002 40.72 7.3SE+001 14 4437- 4460 4447.86 1111.85 0.69 2.34E+002 43.48 5.96E+001 15 4681- 4705 4692.98 1173 .14 1. 89 2.19E+002 40. 95 4 .88E+001 16 5318- 5343 5330.30 1332.50 1. 16 2.42E+002 34.96 1.55E+001 17 5618- 5645 5633.42 1408.29 1. 43 3.82E+002 42.32 1. 44E+O 01 18 5833- 5855 5843.37 1460.78 1. 87 1. 46E+002 27.26 1. OSE+OOl 19 7052- 7067 7059.03 1764.75 0.28 1 .72E+001 9.52 1. 84E+OOO M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2.000 sigma [1376]

Interference Corrected Activity Report 3/10/2018 12:42:02 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample Tit l e: B101110AFSWC046GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  ..... ...... .... .... ... . ..... IDENTIFIED NUCLIDES             * ,. * *  * " * * "' * .., ! * * * ' I * "
  • Nuclide Id Energy Yield Activit y Activity Name Confidence (keV) ( %) (pCi/MA 2 ) Uncertainty K-40 1. 000 1460.82* 10 .66 1.81914E+006 3.73607E+005 Co-60 1. 000 1173.23* 99.85 2.70754E+OOS 5.50257E+004 1332.49* 99.98 3.09698E+OOS 5.12241E+004 Cs-137 1.000 661.66* 85 .10 4.50477E+006 5.64936E+OOS Eu-152 1.000 121.78* 28.67 1.79026E+006 5.48808E+OOS 344.28* 26.60 1.88389E+006 4.17095E+005 1408. 01* 21. 07 2.36760E+006 3.23725E+005 Eu-155 0 .332 86.55* 30.70 1.12355E+006 5.69539E+005 105.31 21.10 Pb-212 0 .937 238.63* 43.60 1 .89534E+005 1.39657E+005 Bi-214 0.978 609.32* 45.49 1 .44720E+005 8.96605E+004 11 20.29* 14. 92 1.91026E+006 3.86005E+005 1764.49* 15.30 1.60370E+005 8.99208E+004
          *=Energy line found in the spectrum.
          @ : Energy line not used for Weighted Mean Activity Energy Tolerance :               10.000 keV Nuclide confidence index threshold =                    0.30 Errors quoted at 2.000 sigma

[1377]

Interference Corrected Activity Report 3/10/2018 12:42:02 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"'2 ) Uncertainty K-40 1.000 1. 819140E+006 3.736071E+005 Co-60 1. 000 2.916179E+005.J 3.749291E+004 Cs-137 1 .000 4.504773E+006.I 5.649365E+005 Eu-152 1.000 2.115200E+006J 2.318040E+005 Eu-155 0.332 1.123554E+006 5.695392E+005 Pb-212 0.937 1.895341E+005 1.396571E+005 Bi-214 0.978 l.988246E+005 6.264955E+004 X Pb-214 0.387 

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2. 000 sigma

[1378]

Interference Corrected Activity Report 3/10/2018 12:42:02 PM Page s 

  **********     U N I D E N T I F I E D             P E A K S      **********

Peak Locate Performed on: 3/10/2018 12:42:02 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.37 1. 0 5 3 7 E+ 0 0 0 14 .84 2 40 .12 3.9009E-001 38.37 3 75.20 2.3520E+OOO 19.15 10 778.86 3.4791E-001 21.20 Sum 11 867.39 1.1421E-001 44.42 To l. Nb- 94 12 963.78 3.3783E-001 22.76 Sum 13 1085.89 2.3248E-001 29.19 M = First peak in a multiplet region m = Other peak in a multiplet region F ~ Fitted singlet Errors quoted at 2 . 000 sigma [1379]

Nuclide MDA Report 3/10/2018 12:42:03 PM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

Bl01110AFSWC046GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       1460.82*    10. 66  2.898E+005    2.90E+OOS      l.819E+006 1.281E+005
 +      Co-60      1173.23*    99.85   6.082E+004    3.72E+004      2.708E+005 2.874E+004 1332.49*    99.98   3.725E+004                   3.097E+005 1 .689E+004 Nb-94        702.65    99. 81  7.262E+004    7.26E+004      9.442E+003 3.485E+004 8 71. 09  99.89   8.658E+004                   9.531E+004 4. 175E+004 Ag-108m      433.90    90.50   1 .211E+005   8.77E+004    -3.502E+004 5.914E+004 614 .30   89.80   1.006E+005                 -1.880E+004 4.873E+004 722.90    90.80   8.769E+004                   7.001E+004 4.222E+004 Cs-134       604.72    97.62   9.475E+004    9 .1 0E+004    3.455E+003v 4.594E+004 795.86    85.46   9.096E+004                 -1. 190E+004 1~~-372E+004
 +      Cs-137       661.66*   85.10   l.071E+005    l.07E+OOS      4.505E+006~V"5.188E+004
 +      Eu-152       121.78*   28.67   6.533E+005    1.83E+005      1.790E+006,...._3.232E+005 344.28*   26.60   3.884E+005                   l.884E+006 1.897E+005 1408.01*    21. 07  1 .827E+005                  2.368E+006 8.29SE+004 Eu-154       123.07    40.40   5.264E+005    1.57E+005      1.567E+006~ 2.608E+005 723.30    20.06   3.953E+005                   1.476E+005 1.903E+005 1274.43     34.80   l.573E+005                   9.450E+004 7.371E+004
 +      Eu-155        86.55*   30.70   8.488E+005    8.49E+005     1 .124E+006 4.207E+005 105.31    21.10   l. 028E+006                  4.452E+005 5.091E+005 Tl-208       583.19    85.00  1.134E+005     1.13E+OOS      8.930E+004 5.509E+004 Bi-212       727.33     6.67  1.188E+006     1 . 1 9E+006   6.090E+005 5.719E+005
 +      Pb-212       238.63*   43.60   2.206E+005    2.21E+005     1 .895E+005 1.078E+005
 +      Bi-214       609.32*   45.49  1. 379E+005    9.75E+004     1.447E+005 6.587E+004 1120.29*    14.92  4.360E+005                   1.910E+006 2.069E+005 1764.49*    15. 30  9.747E+004                  1.604E+005 3.609E+004 Pb-214       295.22    18.42   6.597E+005    2.90E+005     3.776E+005 3.237E+005 351.93*   35.60  2.902E+005                   1.408E+006 1.417E+005 Ra-226       186 . 21   3.64  4.159E+006    4.16E+006      6.833E+005 2.052E+006 Ac-228       338.32    11. 27 1 .195E+006   2.81E+OOS     -7.837E+005 5.868E+005 911.20    25.80  2.811E+005                   3.064E+004 1.345E+005 968.97    15.80  6.908E+005                   3.194E+005 3.354E+005 Am-241        59.54    35.90  7.931E+005    7.93E+005     -3.870E+004 3.920E+OOS
       +=Nuclide identified during the nuclide identification
       * : Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ ~ Half-life too short to be able to perform the decay correction

[1380]

          • GAMMA S P E C T R U M ANALYSIS *****

Filename: 5452 Report Generated On 3/10/2018 2:19:22 PM Sample Title B101110AFSWC047GD Sample Description Ul LOWER CTMNT Sample Identification 047 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"'2 Sample Taken On 3/10/2018 2:08:00 PM Acquisition Started 3/10/2018 2:09:18 PM Live Time 600. 0 seconds Real Time 602.6 seconds Dead Time 0 . 43 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1381]

Peak Analysis Report 3/10/2018 2:19:22 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC047GD Peak Analysis Performed on: 3/10/2018 2: 1 9:21 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) {keV) Area Uncert. Counts 1 113- 133 128.94 31. 94 1. 04 3.75E+002 82.88 3.4BE+OD2 2 150- 187 161.02 39.96 1. 38 6.96E+002 199.27 1.5BE+003 3 284- 310 3 01 .63 75. 12 1. 22 1.46E+003 233.35 2.77E+003 4 333- 346 340.40 84.81 0.96 2.78E+002 140. 21 1.68E+D03 5 478- 496 488.72 121.90 1. 15 1 .21E+003 167.06 l. 71E+003 6 971- 988 980.23 244.80 1. 00 2.72E+002 91. 66 5.61E+002 7 1368- 1414 1377.63 344. 17 1. 38 9.95E+002 160.37 7.33E+002 8 1636- 1654 1645.97 411.26 0.55 l.05E+002 57.30 2.12E+002 9 1767- 1789 1776.22 443.83 1. 05 1 .02E+002 65.09 2.45E+002 10 2429- 2443 2436.63 608.96 0 .52 2.44E+001 38. 75 1.21E+OD2 11 2634- 2657 2646.56 661.45 1. 69 1.35E+003 90.61 l.75E+002 12 2887- 2900 2893. 01 723.07 1.16 5.14E+001 30.83 6.76E+001 13 3103- 3126 3115.24 778.64 1. 35 3.49E+002 62.44 1 .56E+D02 14 3459- 3480 3469.64 867.25 1. 70 1.08E+002 46.50 1 .16E+002 15 3843- 3869 3855.91 963.84 1. 55 4.20E+002 62.18 1.25E+002 16 4015- 4028 4021 .12 1005.15 0.91 3.14E+D01 28. 71 5.86E+001 17 4329- 4352 4342.76 1085.57 1. 49 2.75E+002 53.67 1 .12E+002 18 4434 - 4462 4447.72 1111.81 1. 77 4.15E+002 57.43 8.91E+001 19 4678

  • 4705 4692.93 1173. 13 1. 70 5.46E+OD2 56.43 5.56E+001 20 5090- 5107 5098.58 1274.56 1. 56 5.22E+001 21. 58 1.98E+001 21 5188- 5204 5196.38 1299.01 2.09 5.68 E+001 20.17 1.42E+D01 22 5316- 5343 5330.06 1332.43 1. 75 4.96E+D02 51.13 3.50E+D01 23 5615- 5645 5632.70 1408. 11 1. 77 6.52E+002 52.73 8.38E+OOO 24 5835- 5854 5843.44 1460.80 0.78 1. 05E+002 26.51 2.0SE+OOl M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F Fitted singlet Errors quoted at 2 . 000 sigma

[1382]

Interference Corrected Activity Report 3/10/2018 2:19 : 22 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC047GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * *
  • e *
  • e * * * .. e e * *
  • I *
  • a IDENTIFIED NUCLIDES * ,t * !t> * * * * * * * * *
  • t I t .. j
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M"2 ) Uncertainty K-40 1.000 1460.82* 10.66 1 .30985E+006 3.48299E+005 Co-60 1.000 1173.23* 99.85 6.74829E+005 8.81577E+OD4 1332.49* 99.98 6.35899E+005 8.29786E+004 Cs-137 1 .000 661.66* 85.10 1.68238E+006 2.31577E+005 Eu-152 1.000 1 21.78* 28.67 3.08761E+006 7.50333E+005 344.28* 26.60 3.28776E+006 7.56675E+005 1408.01* 21.07 4 .04197E+006 4.59950E+005 Eu-154 0.999 123.07* 40.40 2.19113E+006 5.33749E+OD5 723.30* 20.06 2.78526E+OOS l . 7014 7E+005 1274.43* 34.80 1.89809E+OOS 7.99528E+004 Eu- 155 0.332 86.55* 30.70 7.56339E+005 4.09850E+OOS 105.31 21.10 Bi-212 0 .971 727.33* 6.67 8.37667E+005 5.11970E+005 Pb-212 0 .941 238.63* 43.60 4.93524E+005 l.84516E+005 Bi-214 0.689 609.32* 45.49 5.57169E+004 8.87891E+004 1120.29* 14.92 3.38192E+006 5.40801E+OOS 1764.49 15.30
          * ~ Energy line found in the spectrum.
          @ ~ Energy line not used for Weighted Mean Activity Energy Tolerance :                        10.000 kev Nuclide confidence index threshold ~                            0.30 Errors quoted at 2.000 sigma

[1383]

Interference Corrected Activity Report 3/10/2018 2:19:22 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 1. 00.0 l .309848E+006 3.482993E+OOS Co-60 1. 000 6.541865E+OOSI 6.042271E+D04 X Ag-108m 0.934 Cs-137 1 .000 1. 6823 80E+006 ./ 2.315772E+OOS Eu-152 1.000 3.620784E+006./ 3.479106E+OOS Eu-154 0.999 l.772789E+005.t" 7.918742E+OD4 Eu-155 0.332 7.563388E+OOS 4.098497E+OOS Bi-212 0.971 3.045D09E+005 S.64l99DE+005 Pb-212 0.9 41 4.935240E+D05 l. 845158E+005 Bi-214 0.689 l.430224E+OOS 8.761607E+D04 X Pb-214 0 .383 

      ? =  Nuclide is part of an undetermined solution X  = Nuclide rejected by the interference analysis
      @  = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at    2.000 sigma

[1384]

Interference Corrected Activity Report 3/10/2018 2:19:22 PM Page 5 

  * *********     U N I D E N T I F I E D      P E A K S     **********

Peak Locate Performed on: 3/10/2018 2: 19: 21 PM Peak Locate From Channel : 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % uncertainty Type Nuclide 1 31. 94 6.2461E-001 22.12 2 39.96 1.1607E+OOO 28.61 3 75.12 2.4322E+OOO 15.99 8 411.26 l .7563E-001 54 .38 9 443.83 1 .6939E-001 64.05 D-Esc. 13 778.64 5.8177E-001 17 .89 Sum 14 867.25 1. 7917E-001 43.26 Tol. Nb-94 15 963.84 7.0054E-001 14.79 Sum 16 1005.15 5.2315E-002 91.46 Sum 17 1085.57 4.5856E-001 19.51 21 1299.01 9.4730E-002 35.49 Sum M = First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1385]

Nuclide MDA Report 3/10/2018 2:19:22 PM Page 6

          • N U C L I D E MDA R E P O R T *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B101110AFSWC047GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       1460.82*     10 .66  3.759E+005   3.76E+005     1 .310E+006 1.712E+005
 +      Co-60      1173.23*     99.85   6.754E+004   5.64E+004     6.748E+005  3.210E+004 1332.49*     99.98  5.643E+004                  6.359E+005  2.648E+004 Nb- 94       702.65     99. 81  9.444E+004   9.44E+004    -1.236E+004  4.576E+004 871.09     99.89  1 .138E+005                -2.859E+003  5.536E+004 Ag-108m      433.90*    90.50  1 .096E+005   5.70E+004     1 .065E+005 5.336E+004 614.30*    89.80   7.447E+004                 2.822E+004  3.567E+004 722.90*    90.80  5.698E+004                  6.153E+004  2.687E+004 Cs-134       604.72     97.62  1.082E+005    1.08E+005     5.974E+004v 5.267E+004 795.86     85.46  1.148E+005                  8.832E+004  5.562E+004
 +      Cs-137       661.66*    85.10   l.125E+005   1. 1 3E+O 05  1.682E+006  5.457E+004
 +      Eu-152       121. 78*   28.67   6.423E+005   1. 51E+005    3.088E+006  3.177E+005 34 4. 28*  26.60  8.100E+005                  3.288E+006  4.005E+005 1408. 01*    21. 07 1 .515E+005                 4.042E+006  6.735E+004
 +      Eu-154       123.07*    40 .40 4.558E+005    1. 06E+005    2.191E+006  2.255E+005 723.30*    20.06  2.579E+005                  2.785E+005  l.216E+005 1274.43*     34.80  1. 056E+005                 1.898E+005  4 .790E+004
 +      Eu-155        86.55*    30.70   6.159E+005   6.16E+005     7.563E+005  3.043E+OOS 105.31     21.10  1. 082E+006                -2.039E+OOS  5.361E+OOS Tl-208       583.19     85 .00 1.215E+005    1.21E+005     4.435E+004  5.910E+004
 +      Bi-212       727.33*     6.67   7.756E+005   7.76E+005     8.377E+005  3.658E+005
 +      Pb-212       238.63*    43.60  2.603E+005    2.60E+005     4.935E+005  1 .277E+005
 +      Bi-214       609.32*    45.49  1. 470E+005   1 .47E+005    5.572E+004  7.042E+004 1120.29*     14.92  5.647E+005                  3.382E+006  2.713E+005 176 4 .49    15.30  2.595E+005                  1 .853E+005 l.171E+OOS Pb-214       295.22     18.42  7.003E+005    6.05E+005     7.664E+005  3.440E+OOS 35 1 .93*  35.60  6.052E+005                  2.457E+006  2.993E+005 Ra-226       186.21      3.64  4.340E+006    4.34E+006     1. 978E+006 2.143E+006 Ac-228       338.32     11.27  l.479E+006    3.72E+005     2.937E+004  7.290E+OOS 911.20     25.80  3.720E+005                 -2.276E+004  1. BOOE+OOS 968.97     15.80  9.175E+005                  2.730E+005  4.487E+005 Am-241        59.54     35.90  8.270E+005    8.27E+005     2.174E+005  4.089E+005
       +=Nuclide identified during the nuclide i dentification
       *=Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @: Half-life too short to be able to perform the decay correction

[1386]

          • GAMMA S P E C T R U M ANALYSIS *****

Filename: 5452 Report Generated On 3/10/2018 12:54 ; 22 PM Sample Title B101110AFSWC048GD Sample Description Ul LOWER CTMNT Sample Identification 048 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"2 Sample Taken On 3/10/2018 12:44 ~00 AM Acquisition Started 3/10/2018 12 :44:20 PM Live Time 600. 0 seconds Real Time 601.9 seconds Dead Time 0.31 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1387]

Peak Analysis Report 3/10/2018 12 :54:22 PM Page 2 

*****              P E A K        ANALYSIS               R E P O R T            *****

Detector Name: 5452 Sample

Title:

B101110AFSWC048GD Peak Analysis Performed on: 3/10/2018 12:54:22 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 112- 126 116.40 28.81 0.80 7. llE +OOl 62.48 2.62E+002 2 155- 169 162.63 40. 36 1. 52 2.56E+002 78.52 4.46E+002 3 290- 313 302.24 75.27 1.76 9.76E+002 182.31 1.83E+003 4 333- 347 341. 40 85.07 0.70 2.00E+002 124.86 1.28E+003 5 481- 501 489.20 122.02 1. 52 6.61E+002 145.28 1. 27E+003 6 973- 993 9 8 0.53 244.87 1. 67 1.67E+002 83. 01 4.28E+002 7 1367- 1390 1378.73 344.44 1.92 4.32E+002 78.52 2.78E+002 8 1491- 1502 1496 .49 373.89 0. 95 2.93E+001 32.65 9.37E+001 9 2430- 2446 2436.88 609.02 0 .40 5.08E+001 32.18 6.62E+001 10 2631- 2662 26 47 .21 661.61 2.06 2.34E+003 106.65 1.00E+002 11 3105- 3127 31 16 .53 778.96 1. 52 1 .98E+002 42.02 6.15E+001 12 3844- 3869 3856.68 964.03 1. 66 2.08E+002 49 .16 9.35E+001 13 4335- 4353 4344.25 1085.94 0.41 8.86E+001 34.59 6.04E+001 14 4438- 4463 4449.26 1112.20 1.57 2.27E+002 39.02 3.42E+001 15 4682 - 4705 4693.93 1173.38 1. 81 1.89E+002 39.93 5.27E+001 16 5092- 5107 5099.31 1274.74 0.26 2.26E+001 13.13 6.37E+OOO 17 5317- 5343 5331.18 1332 .71 1.83 2.21E+002 35.43 2.06E+001 18 5620- 5645 5633.43 1408.29 1.34 3 .01E+ 002 41.26 2.93E+001 19 5834- 5856 5843.67 1460.86 1. 35 1.21E+002 29.42 2.54E+001 M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1388]

Interference Corrected Activity Report 3/10/2018 12:54:22 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

Bl01110AFSWC048GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . ...... . ......... . ..      IDENTIFIED NUCLIDES            * . . . . . . . . . . . . . . . .. .. I, .....

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pci/MA2 ) Uncertainty K-40 1. 000 1460.82* 10 .66 1.49742E+006 3.87869E+005 Co-60 1 . 000 1173.23* 99.85 2.33908E+005 5.27585E+004 1332.49* 99.98 2.83869E+005 5.07917E+004 Cs-137 1.000 661.66* 85 .10 2.92528E+006 3.75715E+OOS Eu-152 1.000 121.78* 28.67 1.68185E+006 4.99987E+005 344.28* 26.60 l. 42834E+006 3.49868E+OOS 14 08.01* 21.07 1.86561E+006 2.96278E+OOS Eu-154 0.683 1 23.07* 40.40 1.19358E+006 3.55399E+005 723.30 20.06 1274.43* 34.80 8.22510E+004 4.82016E+004 Eu-155 0.333 86.55* 30.70 5.42580E+005 3.55308E+005 1 05. 31 21.10 Pb-212 0 .940 238.63* 43.60 3.03162E+005 l .58458E+OOS Bi-214 0 .691 609.32* 45.49 1.16167E+005 7.48310E+004 1120 .29* 14.92 l.84851E+006 3.50815E+005 1764.49 15.30 

       * - Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :          10.000 keV Nuclide confidence index threshold ~               0. 30 Errors quoted at 2.000 sigma

[1389]

Interference Corrected Activity Report 3/10/2018 12:54:22 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 1.000 1 .497422E+006 3.878688E+OOS Co-60 1. 000 2.598372E+005/ 3.659070E+004 Cs-137 1 .000 2.925278E+006/ 3.757146E+OOS Eu-152 1 .000 1.661447E+006J 2.054505E+005 Eu-154 0.683 8.102251E+004./ 4.781515E+004 Eu-155 0.333 5.425797E+005 3.553082E+005 Pb-212 0.940 3.031616E+005 l.584578E+005 Bi-214 0.691 1.915576E+OOS 7.318462E+004 X Pb-214 0.387 

      ?  = Nuclide is part of an undetermined solution X  = Nuclide rejected by the interference analysis
      @  = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2. 000 sigma

[1390]

Interference Corrected Activity Report 3/10/2 018 12:54:22 PM Page 5 

  **********    U N I D E N T I F I E D        P E A K S      **********

Peak Locate Performed on: 3/10/2018 12:54:22 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV) Counts per Second  % Uncertainty Type Nuclide 1 28.81 1. 1851E- 0 01 87.86 2 40.3 6 4.2688E-001 30.65 3 75.27 1 .6269E+OOO 18 .68 8 373.89 4.8916E-002 111. 24 Sum 11 778.96 3.2919E- 001 21. 27 Sum 12 964.03 3.4585E- 001 23.69 13 1085. 94 1. 4760E- 001 39.06 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1391]

Nuclide MDA Report 3/10/2018 12:54:22 PM Page 6

          • N U C L I D E MD A R E P O R T ****
  • Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B101110AFSWC048GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL .NLB Nuclide Energy Yield Line MDA Nuc lide MDA Activity Dec . Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10 .66  4.337E+005   4.34E+005      l. 497E+006 2.000E+OOS
 +      Co-60      1173.23*    99.85   6.214E+004   4.40E+004     2.339E+005   2.940E+004 1332.49*    99.98  4.403E+004                  2.839E+005   2.028E+004 Nb-94        702.65    99.81   7.406E+004   7.41E+004    -6.944E+003   3.557E+004 871 .09   99.89   8.402E+004                 5.814E+004   4.047E+004 Ag-108m      433.90    90.50   l.086E+005   8.53E+004    -5.522E+004   5.291E+004 614.30    89.80  9.199E+004                -3.821E+003    4,443E+004 722.90    90.80  8.527E+004                -6.729E+003    4.101E+004 Cs-134       604.72    97.62  8.370E+004    8.28E+004     4.63SE+003,f 4.041E+004 795.86    85.46  8.280E+004                  4 .465E+004  3.964E+OD4
 +      Cs-137       661.66*   85.10  9.544E+004    9 .54E+004    2.92SE+006   4.603E+004
 +      Eu-152       121. 78*  28.67  5.754E+005    2.45E+005     l.682E+006   2.842E+OOS 344.28*   26.60  3.709E+005                  1. 428E+O 06 1.810E+OOS 1408.01*    21.07  2.448E+OOS                  1.866E+006   l.140E+OOS
 +      Eu-154       123.07*   40.40  4.083E+005    6.4DE+004     l. 194E+006  2.017E+OOS 723.30    20.06  3.878E+005                - 8.490E+D04   1. 865E+OOS 1274 .43*   34.80  6.395E+004                  8.225E+004   2.706E+004
 +      Eu-155        86.55*   30.70  5.494E+005    5. 4 9E+005   S.426E+005   2.710E+005 105.31    21.10  9.089E+005                  4.031E+005   4.495E+005 Tl-208       583.19    85. 00 9.565E+004    9.57E+004     3.505E+004   4.619E+004 Bi-212       727.33     6.67  l.215E+006    1.22E+006     1.669E+006   S.856E+OOS
 +      Pb-212       238.63*   43.60  2.405E+OOS    2.40E+005     3.032E+005   1 .178E+005
 +      Bi-214       609.32*   45.49  1. 146E+005   1. 1 5E+005   1 .162E+OOS  S.420E+004 1120.29*    14.92  3.546E+005                  1.849E+006   l.663E+OOS 1764.49     15.30  2.751E+005                  3.084E+OOS   1. 249E+OOS Pb-214       295.22    18.42  5.998E+005    2.77E+005     3.532E+005   2.938E+OOS 351.93*   35.60  2.771E+005                  1. 067E+006  1. 352E+005 Ra-226      186.21      3.64  3.686E+006    3.69E+006   -1. 340E+006   1.816E+006 Ac-228       338.32    11. 27 1.108E+OD6   2.81E+005    -5.017E+OOS    5.436E+OD5 911.20    25.80  2.811E+005                - 3.390E+004   1.345E+OD5 968 . 97  15.80  6.943E+OOS                  1. 287E+005  3.371E+005 Am-241        59 . 54  35.90  7.044E+005    7.04E+005     4.089E+005   3.476E+005
       + ~ Nuclide identified during the nuclide identification
       * ; Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
      @ ~ Half-life too short to be able to perform the decay correction

[1392]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/10/2018 2: 00: 51 PM Sample Title Bl01110AFSWC049GD Sample Description Ul LOWER CTMNT Sample Identification 049 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M ... 2 Sample Taken On 3/10/2018 1 :50: 00 PM Acquisition started 3/10/2018 1:50:48 PM Live Time 600.0 seconds Real Time 602.1 seconds Dead Time 0.34 % Energy Calibration used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1393]

Peak Analysis Report 3/10/2018 2:00:51 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC049GD Peak Analysis Performed on: 3/10/2018 2:00:51 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 112- 135 129.58 32.10 1.43 4 .18E+002 75.47 2.53E+002 2 153- 189 161.10 39.98 1. 37 4.03E+002 172.09 1 .23E+003 3 282- 310 301.60 75. 11 1.21 1.19E+003 218. 53 2.32E+003 4 334- 345 340.75 84.90 1. 17 1.23E+002 112.66 1.21E+003 5 365- 376 370.90 92.44 0.30 1. 92E+O 01 101.75 1.02E+003 6 480- 495 488.50 121.85 1.13 8.40E+002 128.09 1 .09E+003 7 970- 989 980.27 244. 81 0 .64 1.78E+002 85.71 4.73E+002 8 1370- 1414 1377 .81 344.21 1. 35 6.57E+002 141.68 6.07E+002 9 1639- 1652 1644.86 410.98 1. 38 3.67E+001 40.00 1. 29E+O 02 10 1769- 1782 1776.05 443.79 1. 15 8.49E+001 40. 95 1. 21E+002 11 2430 - 2444 2437.16 609.09 0.82 5.53E+001 36.33 9.47E+001 12 2633 - 2659 2646.44 661.42 1. 53 l.61E+003 93.44 1. 31E+002 13 3104- 3128 3115.23 778.64 1. 58 2.79E+002 51.53 9.33E+001 14 3461- 3477 3469.48 867.22 1. 04 8.78E+001 34.15 6.42E+001 15 3842- 3867 3855.27 963.68 1. 65 2.88E+002 51.99 9.llE+OOl 16 4333- 4365 4342.94 1085.61 2.16 1.89E+002 54.58 1 .05E+002 17 4436- 4459 4447. 81 1111 .84 1. 77 2.52E+002 48.79 8.60E+001 18 4681- 4705 4692.83 1173.10 2.13 3.18E+002 48.70 6.72E+001 19 4845- 4860 4852.06 1212.92 0.88 3.09E+001 18.14 1.71E+001 20 5318- 5342 5330.22 1332.47 1. 96 3.34E+002 44.68 4.02E+001 21 5617- 5645 5632.25 1407.99 1. 92 4 .53E+002 46.46 1.84E+001 22 5833- 5855 5844.24 1461.00 1. 27 1 .43E+002 27.67 1. 30E+001 23 7054- 7069 7061.75 1765.43 0.32 2.60E+001 10 .20 O.OOE+OOO M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1394]

Interference Corrected Activity Report 3/10/2018 2:00 : 51 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSWC049GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * *  * * * *
  • _. * * * *
  • t, I .. ** IDENTIFIED NUCLIDES * "' ... * * * * * * * * * *
  • a * ~ 'ill ,.
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M"'2 ) Uncertainty K-40 1.000 1460.82* 10 .66 1.77647E+006 3.76687E+005 Co-60 1.000 11 73.23* 99.85 3.92506E+005 6.78587E+004 1332.49* 99.98 4.27902E+005 6.67299E+004 Ag-108m 0.416 433.90* 90.50 8.90069 E+004 4.49268E+004 614.30* 89.80 6.39802E+004 4 .27415E+004 722.90 90.80 Cs-137 1 .000 661.66* 85 .10 2.01365E+006 2.68510E+005 Eu-152 1.000 121.78* 28.67 2.13632E+006 5.37837E+005 344.28* 26.60 2.16911E+006 5.88290E+005 1408 . 01* 21.07 2.80726E+006 3.65342E+005 Eu-155 0.332 86.55* 30.70 3.33953E+005 3.12968E+005 1 05.31 21. 10 Pb-212 0.941 238.63* 43.60 3.23154E+005 l.64120E+005 Bi-214 0.977 609.32* 45.49 l .26301E+005 8.43790E+004 1120.29* 14.92 2.05357E+006 4.30353E+005 17 64.49* 15.30 2.43050E+005 9.72993E+004
          * =Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                          10.000 keV Nuclide confidence index threshold =                               0.30 Errors quoted at 2. 000 sigma

[1395]

Interference Corrected Activity Report 3/10/2018 2:00:51 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 1 .000 1.776473E+006 3.766873E+005 Co-60 1.000 4 .105009E+005.J 4.757925E+004 Ag-108m 0.416 2.580686E+004 3.683272E+004 Cs-137 1.000 2.013648E+006..t 2.685104E+005 Eu-152 1 .000 2.506408E+006J 2.688162E+OOS Eu-155 0.332 3.339529E+005 3.129677E+005 Pb-212 0.941 3.231539E+OOS l .641203E+005 Bi-214 0.977 1.882753E+005 7.500058E+004 X Pb-214 0.384 

      ? ~ Nuclide is part of an undetermined so lution X = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2.000 sigma

[1396]

Interference Corrected Activity Report 3/10/2018 2: 00: 51 PM Page 5 

  **********      U N I D E N T I F I E D      P E A K S      **********

Peak Locate Performed on : 3/10/2 018 2:00:51 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol . No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32. 10 6.9624E-001 1 8. 07 2 39.98 6.7182E-001 42.69 3 75.11 1 .9876E+OOO 18. 32 5 92.44 3.1940E-002 53 0 .96 D-Esc. 9 410 .98 6.1202E-002 108.92 13 778.64 4 .6448E-001 18.49 Sum 14 867.22 1. 4627E-001 38.91 Tol . Nb-94 15 963.68 4.7979E-001 18 .06 16 1085.61 3.1443E-001 28.93 19 1212.92 5.1510E-002 58 . 71 Sum M ~ First peak in a multiplet region m = Other peak in a multiplet region F ~ Fitted singlet Errors quoted at 2 . 000 sigma [1397]

Nuclide MDA Report 3/10/2018 2: 00 : 51 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 sample Geometry: 1M90D Sample

Title:

B101110AFSWC049GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*     10.66   3.178E+005    3.18E+005    1. 776E+006       l.421E+OOS
 +      Co-60      1173.23*     99.85   7.076E+004    5.77E+004    3.925E+OOS        3.371E+004 1332.49*     99.98   5.770E+004                 4 .279E+005       2.711E+004 Nb-94        702.65     99.81   8.356E+004    8.36E+004  -l.514E+004         4.032E+004 87 1 .09   99.89   9.867E+004                 8.943E+004        4.779E+004
 +      Ag-108m      433.90*    90.50   6.589E+004    6.59E+004    8.901E+004        3.152E+004 614.30*    89.80   6.624E+004                 6.398E+004        3.155E+004 722.90     90.80   9.807E+004                 4.834E+004        4.741E+004 Cs-134       604.72     97.62   1. 008E+005   9.60E+004    1 .682E+005v      4.894E+004 795.86     85.46   9.602E+004               -3.284E+004         4.625E+004
 +      Cs-137       66 1 .66*  85. 10 1.015E+005     1 .02E+005   2.014E+006        4. 907E+004
 +      Eu-152       121. 78*   28.67  4.850E+005     2.07E+005    2.136E+006        2.391E+OOS 344.28*    26.60  7.266E+005                  2.169E+006        3.588E+005 140 8.01*    21.07  2.071E+005                  2.807E+006        9.517E+004 Eu-154       123.07     40.40  5.052E+005     1.81E+005    1. 3 76E+ 0 0 6v" 2.502E+005 723.30     20.06  4.417E+005                  4. 745E+004       2.135E+005 1274.43      34.80  1. 806E+005                 3.707E+OOS        8.538E+004
 +      Eu-155        86.55*    30.70  5.005E+005     5.00E+005    3.340E+005        2.466E+005 105.31     21.10  9.624E+005                -1.065E+005         4.763E+OOS Tl-208       583. 19    85.00  1.101E+OOS     1.10E+005    3.735E+004        5.341E+004 Bi-212       727.33      6.67  1. 315E+006    1. 31E+006  1.003E+006         6.352E+005
 +      Pb-212       238.63*    43.60  2.481E+005    2. 4 8E+005   3.232E+005        1 .216E+OOS
 +      Bi-214       609.32*    45.49  1.308E+005    2.53E+004    1.263E+005         6.229E+004 1120.29*     14.92  5.188E+OOS                 2.054E+006         2.484E+005 1764.49*     15.30  2.530E+004                 2.430E+005         O.OOOE+OOO Pb-214       295.22     18.42  6.296E+OOS    5.43E+005    3.792E+OOS         3.086E+005 351.93*    35.60  5.429E+005                 1 .621E+D06        2.681E+005 Ra-226       186.21      3.64  3.944E+006    3.94E+006    2.465E+006         1 .945E+006 Ac-228       338.32     11. 27 l. 287E+006   3.36E+005    3.585E+005         6.332E+005 911. 20    25.80  3.359E+005                -l.24DE+005         1.619E+005 968.97     15.80  7.610E+005                -1.074E+005         3.704E+005 Am-241        59.54     35.90  7.401E+005    7.40E+005   -4.721E+003         3.655E+D05
       + =Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1398]

          • GAMM A S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/10/2018 1 :07:46 PM Sample Title Bl01110AFSWC050GD Sample Description Ul LOWER CTMNT Sample Identification 050 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M... 2 Sample Taken On 3/10/2018 1:00:00 AM Acquisition Started 3/10/2018 12:57:43 PM Live Time 600.0 seconds Real Time 601.6 seconds Dead Time 0.27 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1399]

Peak Analysis Report 3/10/2018 1: 07: 46 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC050GD Peak Analysis Performed on: 3/10/2018 1 :07:45 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area uncert. Counts 1 112- 168 130.94 32.44 2. 71 1. 1 7E+O 03 156.02 6.04E+002 2 225- 244 239.65 59.62 0 .62 -9.29E+OOO 109.01 8.41E+002 3 297- 312 302.22 75.27 1.12 3.04E+002 136.98 1.44E+003 4 330- 348 341. 90 85. 19 1.43 1. 88E+002 140.88 l.41E+003 5 483- 499 489.46 122.09 1. 04 2.70E+002 106.88 8.24E+002 6 1370- 1389 1378.40 344.36 0.99 2.43E+002 54.90 1.46E+002 7 1621- 1632 1626.74 406.45 0.39 1 .80E+001 30.20 8.30E+001 8 2327- 2340 2333.79 583.24 0.28 3. 08E+ 001 24.85 4 .42E+001 9 2430- 2449 2438.93 609.53 0.42 5.90E+001 33.76 6.40E+001 10 2631- 2662 2647.41 661.66 1.93 2.01E+003 99.01 8.84E+001 11 3108- 3126 3117.02 779.09 0.72 8.26E+001 27.63 3.14E+OD1 12 3845- 3866 3856.09 963.88 1.17 1.23E+002 33.90 4.37E+001 13 4335- 4350 4342.83 1085.59 0.74 5.30E+001 22.89 2.60E+001 14 4439- 4461 4450.06 1112 .40 0.85 1 .09E+002 30.59 3.24E+D01 15 4682- 4706 4693.75 1173.33 1. 99 1. 49E+002 33.37 3.13E+001 16 5321- 5342 5330.78 1332.61 1. 68 1. 37E+002 27.42 l.44E+001 17 5622- 5645 5632.54 1408.07 2.43 2.00E+002 31. 51 1.20E+001 18 5835- 5856 5844.44 1461.05 0 .92 1 .18E+002 27.07 1. 83E+001 M = First peak in a mul tiplet region m = Other peak in a mul tiplet region F ~ Fitted singlet Errors quoted at 2 . 000 sigma [1400]

Interference Correcte d Activity Report 3/10/2018 1: 07 :46 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC050GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB I * * * * * * * * * * * * *

  • I I * '"
  • IDENTIFIED NUCLIDES
  • I , , * * * * * '" * *
  • I I *
  • J " I Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/MA2 ) Uncertainty K-40 1. 000 1460.82* 10.66 1.46162E+OD6 3.59385E+005 Co-60 1. 000 1173.23* 99.85 1.83769E+005 4.37712E+004 1332.49* 99.98 1 .75175E+005 3.78555E+004 Cs-137 1.000 661.66* 85 .10 2.50660E+D06 3.25437E+005 Eu-152 1 .000 1 21.78* 28.67 6.86792E+OD5 3.04622E+OD5 344.28* 26.60 8.02157E+OOS 2.24239E+OOS 1408.01* 21.07 1. 24066E+006 2.19245E+005 Eu-155 0 .333 86.55* 30.70 5.08758E+ 005 3.94536E+OOS 105.31 21.10 Tl-208 1 .000 583.19* 85.00 3.72791E+ 004 3.03623E+004 Bi-214 0 .692 609.32* 45.49 1.34734E+005 7.88372E+D04 1120.29* 14. 92 8.85091E+005 2.59205E+005 1764.49 15.30 Am-241 1. 000 59.54* 35.90 -3.12146E+004 3.66512E+005
          *=Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                     10.000 keV Nuclide confidence index threshold -                         0 .30 Errors quoted at 2.000 sigma

[1401]

Interference Corrected Activity Report 3/10/2018 1 :07:46 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 1.000 1.461624E+006 3.593845E+005 Co-60 1.000 1.788526E+005J 2.863273E+004 Cs-137 1.000 2.506597E+006.t 3.254366E+005 Eu-152 1 .000 9.552505E+OOS..t l.393905E+005 Eu-155 0.333 5.087583E+005 3.945357E+005 Tl-208 1.000 3.727913E+004 3.036229E+004 Bi-214 0.692 1. 982698E+OOS 7.542565E+004 X Pb-214 0.386 Am-241 1.000 -3.121464E+004 3.665120E+005 

      ?     Nuclide is part of an undetermined solution X  =, Nuclide rejected by the interference analysis
         "" Nuclide  contains energy lines not used in Weighted Mean Activity Errors quoted at     2.000 sigma

[1402]

lnterference Corrected Activity Report 3/10/2018 1 :07:46 PM Page 5 

  **********    UN I D E N T I F I E D       P E A K S     **********

Peak Locate Performed on: 3/10/2018 1:07:45 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.44 l. 9554E+OOO 1 3.30 3 75.27 5.0673E-001 45.05 7 406.45 2.9967E-002 167.96 Sum 11 779.09 1.3763E-001 33.46 Sum 12 963.88 2.0544E-001 27.51 Sum 13 1085.59 8.8381E-002 43.16 M - First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [1403]

Nuclide MDA Report 3/10/2018 1:07:46 PM Page 6

          • N U C L I D E MDA R E P O R T *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B101110AFSWC050GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/M"2 ) (pCi/M"'2 ) (pCi/M"2 ) (pCi/MA2 ) 

 +      K-40       1460.82*     10 .66  3.644E+005   3.64E+OOS    l.462E+006 1.654E+005
 +      Co-60      1173.23*     99.85  4 .963E+004   3.37E+004    1.838E+005 2.314E+004 1332.49*     99.98   3.372E+004                l.752E+005 1 .512E+004 Nb-94        702.65     99. 81 5.871E+004    5.87E+004  -4.385E+004 2.789E+004 871. 09    99.89   6.931E+D04                4.653E+004 3.311E+004 Ag-108m      433.90     90.50   9.577E+004   6.75E+004    8.705E+004 4.647E+004 61 4 .30   89.80  8.5DOE+004                 7.042E+003 4.093E+004 722.90     90.80  6.746E+OD4                1 .462E+004 3.211E+004 Cs-134       60 4 .72   97.62  7.506E+004    6. 94E+004  1. 894E+004../ 3. 609E+004 795.86     85.46  6.938E+004               -1.544E+004 3.293E+004
 +      Cs-137       661.66*    85. 10 8.998E+D04    9.00E+004   2.507E+006 4.330E+004
 +      Eu-152       121.78*    28.67  4.323E+D05    1. 59E+005  6.868E+005 2.127E+005 34 4 .28*  26.60  2.546E+005                8.022E+OOS 1.228E+005 1408.01*     21.07  l. 586E+005               1.241E+006 7.091E+004 Eu-154       123.07     40.40  4.026E+OOS    1.28E+005   3.378E+005~ l.988E+OOS 723.30     20.06  3.021E+005               -1.904E+005 l.437E+005 1274.43      34.80  1.282E+005               -6.410E+OD4 5.919E+004
 +      Eu-155        86.55*    30.70  6.224E+OOS    6.22E+005   5.088E+005 3.075E+005 105.31     21.10  8.482E+OD5                3.917E+004 4.192E+005
 +      Tl-208       583.19*    85.00  4.746E+004    4.75E+004   3.728E+004 2.209E+004 Bi-212       727.33      6.67  9.263E+005    9.26E+OOS   3.896E+OOS 4.411E+005 Pb-212       238.63     43.60  2.649E+OOS    2.65E+OOS   1 .727E+004 1 .300E+005
 +      Bi-214       609. 3 2*  45.49  1 .192E+OOS  1.19E+OOS    1 .347E+005 5.652 E+004 1120.29*     14.92  3.222E+005                8.851E+005 1.501E+005 1764.49      15.30  2.046E+005                1.589E+005 8.965E+004 Pb-214       295.22     18 .42 5.283E+OOS   1.90E+005    2.192E+005 2.580E+005 351.93*    35.60  1 .902E+005               5.993E+005 9.177E+004 Ra-226      186.21       3.64  3.378E+006   3.38E+006   -2.107E+006 1.662E+006 Ac-228       338.32     11. 27 9.288E+005   2. 4 6E+005 -2.515E+005 4.539E+OOS 911.20     25.80  2.458E+005                2.627E+004 1.168E+005 968.97     15. 80 5.508E+OOS               -1. 527E+005 2.653E+005
+       Am-241        59.54*    35.90  6.129E+005   6.13E+OOS   -3. 121E+004 3.019E+005
       + =Nuclide identified during the nuclide i dentification
       *=Energy line found in the spectrum
       > ~ Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
      @=Half-life too short to be able to perform the decay correction

[1404]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/10/2018 2:52:01 PM Sample Title Bl01110AFSWC051GD Sample Description Ul LOWER CTMNT -HIGH DEAD TIME Sample Identification 051 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"2 Sample Taken On 3/10/2018 2: 41: 00 PM Acquisition Started 3/10/2018 2:41:59 PM Live Time 600.0 seconds Real Time 601.9 seconds Dead Time 0 . 31 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1405]

Peak Analysis Report 3/10/2018 2:52: 01 PM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 54 52 Sample

Title:

B1 01110AFSWC051GD Peak Analysis Performed on: 3/10/2018 2:52: 01 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV} (keV} Area Uncert. Counts 1 113- 137 129.50 32.08 1. 57 3.83E+002 76.05 2.46E+002 2 151- 193 161.53 40.09 1. 02 3.15E+002 176.15 1. 16E+O 03 3 283- 308 301. 79 75.16 0 .93 9.88E+002 186.35 1 .81E+003 4 330- 347 339.73 84.65 1 .25 2.18E+002 137. 96 1 .39E+003 5 482- 500 488.94 121.96 1.15 6 .51E+ 002 127.95 1.02E+003 6 973- 986 979.72 244.67 1.16 1.40E+002 57.28 2.47E+002 7 1179- 1192 1185.09 296.02 0. 64 3.53E+001 46.82 1.86E+002 8 1368- 1386 1377.67 344.17 1. 44 4.21E+002 67.59 2.14E+002 9 1770- 1783 1776.13 443.81 0.39 4.33E+001 38.55 1 .16E+002 10 2430 - 2444 2436.52 608.93 0.40 3.lOE+OOl 32.53 8.00E+OOl 11 2635- 2659 2646.64 661.47 1. 68 1 .65E+003 89.07 8.22E+001 12 3105- 3125 3115. 21 778.63 1.29 1 .72E+002 41. 04 6.82E+001 13 3462- 3478 3469.33 867.18 0.31 5.61E+001 28.04 4.29E+001 14 3844- 3867 3856.30 963.94 1. 67 1.71E+002 43.37 7.48E+001 15 4333- 4351 4343.24 1085.69 1.28 1.31E+002 35.39 S.41E+001 16 4437- 4460 4448.38 1111.98 1.30 2.01E+002 36.46 3.27E+001 17 4682- 4705 4693.39 1173.24 1. 79 2.53E+002 42.56 5.02E+001 18 5316- 5343 5330.51 1332.55 1. 98 3.25E+002 38.62 1.05E+001 19 5618- 5644 5632.50 1408.06 1. 76 3.17E+002 38.88 1.37E+001 20 5834- 5854 5844.35 1461 .03 2.01 1 .09E+002 25.64 1. 54E+001 M = First peak in a multiplet region m = Other peak in a mu ltiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1406]

Interference Corrected Activity Report 3/10/2018 2:52:01 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101ll0AFSWC051GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB I * * * * *

  • I I * * * * * * *
  • 11
  • e IDENTIFIED NUCLIDES * * * * * * * * * * * * , *
  • t I I *
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/MA2 ) Uncertainty K-40 1.000 1460.82* 10.66 1. 34944E+006 3.39357E+005 Co-60 1. 000 1173.23* 99.85 3.12211E+OOS 5.82016E+004 1332.49* 99.98 4.17296E+005 5.97196E+004 Cs-137 1.000 661.66* 85. 10 2.05941E+006 2.71187E+005 Eu-152 1 .000 1 21.78* 28.67 1.65703E+006 4.64821E+005 344.28* 26.60 1.39186E+006 3.19649E+005 1408.01* 21.07 1 .96833E+006 2.88023E+005 Eu-155 0.33 1 86.55* 30.70 S.9445SE+005 3.93883E+005 105.31 21. 10 Pb-212 0.943 238.63* 43.60 2. 54124E+ OOS 1.11777E+005 Bi-214 0.690 609.32* 45.49 7.08220E+004 7.48004E+004 1120.29* 14.92 1.64105E+006 3.24930E+OOS 1764.49 15.30
          * ~ Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                     10.000 keV Nuclide confidence index threshold -                         0 .30 Errors quoted at 2.000 sigma

[1407]

Interference Corrected Activity Report 3/10/2018 2: 52: 01 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1. 000 1.349440E+006 3.393575E+005 Co-60 1.000 3.634010E+005J' 4.168105E+004 X Ag-108m 0.4 15 Cs-137 1. 000 2. 059412E+006 .J 2.711869E+005 Eu-152 1.000 1 .700750E+006../ 1.943676E+005 Eu-155 0.331 5.944551E+005 3.938834E+005 Pb-212 0.943 2.541239E+OOS 1.117771E+OOS Bi-214 0.690 1.498469E+OOS 7.289384E+004 X Pb-214 0.938 

      ? ~ Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2.000 sigma

[1408]

Interference Corrected Activity Report 3/10/2018 2:52: 01 PM Page 5 

  **********    UN I D E N T I F I E D      P E A K S      **********

Peak Locate Performed on: 3/10/2018 2:52: 01 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.08 6.3825E- 001 19.86 2 40.09 5.2561E- 001 55.86 3 75.16 1.6466E+OOO 18.86 7 296.02 S.8763E-D02 132.80 Tol. Pb-214 9 443.81 7.2233E-002 88.94 D-Esc . 12 778.63 2.8626E-001 23.90 Sum 13 867.18 9.3497E-002 49 . 98 Tol. Nb-94 14 963.94 2.8536E-001 25 . 33 15 1085. 69 2.1821E-001 27 . 03 M = First peak in a multiplet region m "' Other peak in a multiplet region F = Fitted singlet Errors quoted at 2. 000 sigma [1409]

Nuclide MDA Report 3/10/2018 2:52:02 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B10l110AFSWC051GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*     10 .66  3.387E+OOS    3.39E+005    1 .349E+006 1.525E+005
 +      Co-60      1173.23*     99.85   6.082E+004    3.25E+004    3.122E+005 2.874E+004 1332.49*     99.98   3.252E+004                 4.173E+005 1.453E+004 Nb-94       702.65      99.81   7.115E+004    7.12E+004   -4.080E+004 3.411E+004 871.09      99.89   8.454E+004                 6.839E+004 4.073E+004 Ag-108m     433.90*     90.50   6.531E+004    6. 1 3E+004  4.543E+004 3.123E+004 61 4. 30*   89.80   6.132E+004                 3.588E+004 2.909E+004 722.90      90.80   8.546E+004                 2.387E+004 4.111E+004 Cs-134      604.72      97.62   8.634E+004    8.63E+004    1.146E+005./4.173E+004 795.86      85.46   8.749E+004                 5.185E+004 4.198E+004
 +      Cs-137      66 1 . 66*  85.10   7.852E+004    7.85E+004    2.059E+006 3.757E+004
 +      Eu-152      121. 78*    28.67   4.978E+005    1.76E+005    1.657E+006 2.455E+005 344.28*     26.60   3.007E+005                 1.392E+006 1.459E+005 1408.01*     21.07   1. 756E+005                1. 968E+006 7.942E+004 Eu-154      123.07      40 .40  4.546E+005    l. 56E+005   9.821E+005/ 2.249E+005 723.30      20.06   3.869E+005                 1.838E+005 l .861E+005 1274 .43     34.80   1. 563E+005                1.508E+OOS 7.322E+004
 +      Eu-155       86.55*     30.70   6.107E+005    6.llE+OOS    5.945E+OOS 3.017E+005 105.31      21.10   8.879E+005                 1.113E+006 4.390E+005 Tl-208      583.19      85.00   1. 000E+OOS   1. OOE+OOS   5.848E+004 4.836E+004 Bi-212      727.33       6.67   1.160E+006    1. 1 6E+006  2.384E+OOS 5.579E+005
 +      Pb-212      238.63*     43.60   1.606E+005    1.61E+OOS    2.541E+OOS 7.786E+004
 +      Bi-214      609.32*     45.49   1.210E+005    1 .21E+OOS   7.082E+004 5.743E+004 1120.29*     14.92   3.289E+005                 1.641E+006 l.534E+005 1764.49      15.30   2.246E+005                 1.057E+OOS 9.964E+004 Pb-214      295.22*     18.42   3.516E+005    2.25E+005    1.606E+005 l .697E+005 351. 93*    35.60   2.247E+005                 1. 040E+006 1 .090E+005 Ra-226      186.21       3.64   3.537E+006    3.54E+006    3.738E+006 1 .741E+006 Ac-228      338.32      11. 27  1 .106E+006   2.92E+005   -2.905E+005 5.424E+005 911.20      25.80  2.921E+005                 -7.958E+004  l .400E+005 968.97      15.80   6.654E+005                 l .609E+004 3.227E+OOS Am-241       59.54      35.90   6.717E+005    6.72E+005    2.990E+004  3.313E+005
       +=Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       > ~ Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1410]

          • GAMMA S P E C T R U M .A N A L Y S I S *****

Filename: 5452 Report Generated On 3/10/2018 1 :20:52 PM Sample Title B101110AFSWC052GD Sample Description Ul LOWER CTMNT Sample Identification 052 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO MA2 Sample Taken On 3/10/2018 1:10:00 AM Acquisition Started 3/10/2018 1:10:48 PM Live Time 600.0 seconds Real Time 602. 4 seconds Dead Time 0.40 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 1 7 BCM Ou-I-CA. V,;,.J; cA {e I q 3 /I:;__ /1 r? -f/;;, Q *'!(,~ ,. I ~~6 f-)°7f11~ s oF_::: O,Jl 59tJ [1411]

Peak Analysis Report 3/10/2018 1 : 20: 52 PM Page 2

          • P E A K ANALYS I s R E P O R T *****

Detector Name: 5452 Sample

Title:

B1 01110AFSWC052GD Peak Analysis Performed on: 3/10/2018 1: 20:51 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 139 130.70 32.38 1.29 3.95E+002 74.65 2.25E+002 2 151- 172 162.07 40.22 1. 05 2.09E+002 89.90 4.83E+002 3 296- 313 302.44 75.32 1. 60 3.58E+002 141 .41 1 .42E+003 4 335- 351 342.15 85.25 0. 61 1. 16E+002 124.80 1 .20E+003 5 452- 462 456.27 113.79 0. 25 2.49E+001 73.56 5.54E+002 6 478- 500 490.24 122.28 1. 35 4.76E+002 134.45 1.04E+003 7 969- 992 980.84 244.95 0.89 1.42E+002 79.52 3.59E+002 8 1368- 1417 1378.09 344.28 1. 53 3.53E+002 115.64 4 .03E+002 9 2429- 2447 2439.45 609.66 0 .69 7.51E+001 32.68 5.69E+001 10 2632- 2662 2647.51 661.69 2.04 1. 42E+003 83.52 6.58E+001 11 3108- 3126 3116.64 778.99 1. 80 1 .07E+002 40 .35 8.88E+001 12 3848- 3867 3857.13 964.14 1 .70 1. 28E+002 33.86 4.50E+001 13 4334- 4354 4344.20 1085.93 0.87 7.63E+001 32.04 4.97E+001 14 4438- 4458 4448.91 1112. 11 1.42 1.14E+002 32.07 3.90E+001 15 4684- 4705 4693.32 1173.22 1. 67 1.71E+002 35.38 3.78E+001 16 5320- 5344 5331.10 1332.70 1.25 1.69E+002 30 .28 1.49E+001 17 5620- 5646 5633.49 1408.31 2.29 2.00E+002 35.60 2.67E+001 18 5834- 5856 5845.42 1461 . 30 0 .68 1 .27E+002 26.08 1.llE+OOl M =- First peak in a multiplet region m -"' Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1412]

Interference Corrected Activity Report 3/10/2018 1 : 20: 52 PM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC052GD Nuclide Library used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  "" .. . . . . ~ . . "" . . . . .. ... ...      IDENTIFIED NUCLIDES           . ... " "' ........ .... " , "

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/MA2 ) Uncertainty K-40 1.000 1460.82* 10.66 1.57592E+006 3.51704E+OOS Co-60 1.000 1173.23* 99.85 2.11538E+OOS 4.68693E+004 1332.49* 99.98 2.16844E+OOS 4.25278E+004 Cs-137 1.000 661. 66

  • 85.10 1.77779E+006 2.37624E+OOS Eu-152 1.000 1 21. 78* 28.67 1. 2 0970E+006 4.19004E+005 344.28* 26.60 1.16716E+006 4.27462E+005 1408.01* 21.07 1.24275E+006 2.42215E+005 Eu-155 0.953 86.55* 30.70 3.14077E+OOS 3.43244E+005 105.31* 21.10 8.77935E+004 2.60318E+OOS Pb-212 0.938 238.63* 43.60 2.57236E+005 1 .50236E+OOS Bi-214 0.690 609.32* 45.49 1.71694E+OOS 7.74901E+004 11 20.29* 14 .92 9.28827E+005 2.71816E+005 1764.49 15.30
         *=Energy line found in the spectrum.
         @ = Energy line not used for Weighted Mean Activity Energy Tolerance :                       10.000 keV Nuclide confidence index threshold -                             0.30 Errors quoted at 2.000 sigma

[1413]

Interference Corrected Activity Report 3/10/2018 1 :20:52 PM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1.000 1. 575916E+006 3.517042E+OOS Co-60 1. 000 2 .1444 82E+005./ 3.149497E+004 Cs-137 1.000 1.777788E+006J' 2.376240E+OOS Eu-152 1.000 1.221413E+006./ 1. 882650E+OOS Eu-155 0.953 1.704211E+OOS 2.07414SE+OOS Pb-212 0.938 2.572363E+OOS l.502364E+OOS Bi-214 0.690 2.286026E+OOS 7.452097E+004 X Pb-214 0.385 

      ?  ~ Nuclide is part of an undetermined solution X  = Nuclide rejected by the interference analysis
      @  - Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1414]

Interference Corrected Activity Report 3/10/2018 1 : 20: 52 PM Page 5 

  **********     U N I D E NT I F I E D        P E A K S      **********

Peak Locate Performed on: 3/10/2018 1:20:51 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty_ Type Nuclide 1 32.38 6.5821E-001 18.90 2 40.22 3.4836E-001 43.01 3 75.32 5.9706E-001 39.48 11 778.99 1. 7865E- 0 01 37.65 Sum 12 964.14 2.1333E-001 26 . 45 13 1085.93 1.2711E-001 42. 01 M m = 

         - First peak in a multiplet region Other peak in a multiplet region F =  Fitted singlet Errors quoted at    2 . 000 sigma

[1415]

Nuclide MDA Report 3/10/2018 1:20:52 PM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B101110AFSWC052GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10. 66  3.022E+005   3. 02E+005   1.576E+OD6 1.343E+005
 +      Co-60      1173.23*    99.85   5.172E+004   3.62E+004    2.115E+005 2.419E+004 1332.49*    99.98   3.618E+004                2.168E+005 1.635E+004 Nb-94       702.65     99. 81  6.793E+004   6.79E+004    1 .136E+004 3.250E+004 871. 09    99.89   7.302E+004                3.436E+004 3.497E+004 Ag-108m     433.90     90.50   9.294E+004   7.63E+004   -6.480E+004 4 .506E+004 614.30     89.80   9.000E+004               -1.137E+004 4.343E+004 722.90     90.80   7.627E+004                8.636E+004 3.651E+004 Cs-134      604.72     97.62   7.982E+004   7.88E+004    6.449E+OQ3.I" 3.847E+004 795.86     85.46   7.876E+004               -1.605E+004 3.762E+004
 +      Cs-137      66 1. 66*  85. 10  7.700E+004   7. 7 0E+004  1.778E+006 3.681E+004
 +      Eu-152      121 .78*   28.67   5.38BE+005   2.37E+005    1.210E+006 2.660E+005 344.28*    26.60   6.032E+005                1.167E+006 2.971E+005 1408.01*    21.07   2.372E+005                1.243E+006 1.102E+D05 Eu- 154     123.07     40. 40  4.11BE+005   1.32E+OOS    7.895E+005J"2.035E+005 723.30     20.06   3.443E+005                4.633E+005 1 .648E+005 1274.43     34.80  1. 318E+005                9.782E+004 6.097E+004
 +      Eu-155       86.55*    30.70   5.541E+005   4.33E+005    3.141E+005 2.734E+005 105 .31*   21. 10  4.328E+005                8.779E+004 2.116E+005 Tl-208      583.19     85. 00  8.872E+004   8.87E+004    3.326E+004 4.273E+004 Bi-212      727.33      6.67  1. 037E+006   1. 0 4E+006 -5.643E+005 4.964E+005
 +      Pb-212      238.63*    43.60   2.315E+005   2.32E+OOS    2.572E+005 1.133E+005
 +      Bi-214      609.32*    45.49  1. 103E+005   1. lOE+OOS   1 .717E+005 5.208E+004 1120.29*    14.92   3.430E+005                9.288E+005 1.605E+005 1764.49     15.30   2.470E+005                1.449E+005 1.109E+005 Pb-214      295.22     18.42   5.191E+005   4 .51E+005   2.853E+005 2.534E+005 351. 93*   35.60   4.507E+005                8.720E+OD5 2.220E+005 Ra-226      186.21      3.64   3.286E+006   3.29E+006   -l.338E+006 1.616E+006 Ac-228      338.32     11. 27  9.500E+005   2.45E+OD5   -1.574E+005 4.645E+005 91 1. 20   25.80   2.448E+005                5.133E+004 1.164E+005 968.97     15.80   5.575E+005                1.345E+006 2.687E+005 Am-241       59.54     35.90   6.151E+005   6.lSE+OOS    4.602E+004 3.030E+005
       +=Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1416]

          • GAMMA S P E C T R U M A N A L Y S J S *****

Filename: 5452 Report Generated On 3/10/2018 9:04:28 AM Sample Title B101110AFSWC053GD Sample Description Ul LOWER CTMNT Sample Identification 053 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"2 Sample Taken On 3/10/2018 9:00:00 AM Acquisition Started 3/10/2018 8:54:26 AM Live Time 600.0 seconds Real Time 602.0 seconds Dead Time 0 . 33 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1417]

Peak Analysis Report 3/10/2018 9:04:28 AM Page 2

          • PE AK A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC053GD Peak Analysis Performed on: 3/10/2018 9:04:28 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 112- 135 128.93 31.94 1.27 5.24E+002 75.86 2.30E+002 2 153- 188 160.81 39.91 1. 06 1 .78E+002 152.77 1.02E+003 3 280- 308 301.12 74.99 1. 03 1 .13E+003 190.23 1.71E+003 4 333- 347 340.43 84.82 1. 50 1 .40E+002 120.18 1.20E+003 5 483- 497 488.84 121.93 1. 29 4.53E+002 108.70 8.64E+002 6 974- 988 979.32 244.57 0 .70 5.80E+OD1 63.85 3.32E+002 7 1368- 1386 1377.25 344. 07 1. 13 3.47E+002 64.16 2.02E+002 8 1768- 1783 1774.88 443.49 0 .44 4.75E+001 45.30 1.54E+002 9 2431- 2444 2437.60 609.20 0 .66 4.59E+001 31.05 7.0lE+OOl 10 2633- 2660 2646.28 661.38 1. 44 2.79E+003 115.90 1.27E+002 11 3103- 3126 3114.87 778.55 0 .89 1.65E+002 38.41 5.09E+001 12 3463- 3479 3469.23 867.15 0 .36 3.48E+001 27.12 4.72E+001 13 3845- 3866 3855.69 963.78 1. 66 1.64E+002 38.55 5.35E+001 14 4334- 4351 4342.91 1085.61 1. 55 1.10E+002 33 .41 5.18E+001 15 4438- 4458 4448.55 1112.02 1. 69 1.43E+D02 35.84 4.93E+001 16 4681- 4704 4692.83 1173. 10 1. 95 1. 89E+002 39.39 5.00E+OOl 17 5319- 5342 5330 .11 1332.45 1. 25 2.21E+002 36.59 2.88E+001 18 5623- 5643 5632.60 1408.08 1. 25 2.19E+002 35.06 2.48E+001 19 5834- 5855 5843.47 1460.81 0.39 1.02E+002 26.10 1.87E+001 M = First peak in a multiplet region m ~ Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000 sigma [1418]

Interference Corrected Activity Report 3/10/2018 9: 04 :28 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSWC053GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . ........ . ' .. " . . .. . .. IDENTIFIED NUCLIDES           a f t a. * *
  • e t e t
  • t * "' t
  • II *
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M"2 ) Uncertainty K-40 1.000 1460.82* 10.66 1. 27083E+006 3.42447E+005 Co-60 1.000 11 73.23* 99.85 2.33432E+005 5.21111E+004 1332.49* 99.98 2.83529E+005 5.21035E+004 Ag-108m 0.420 433.90* 90.50 4.98184E+004 4.80581E+004 614.30* 89.80 5.31375E+004 3.64944E+004 722.90 90.80 cs-137 1.000 661. 66
  • 85.10 3.48841E+006 4.43234E+005 Eu-152 1.000 1 21.78* 28.67 1.15289E+006 3.60237E+005 344.28* 26.60 1.14623E+006 2.83524E+OOS 14 08.01* 21.07 1. 35941E+006 2.43175E+005 Eu-155 0.332 86.55* 30.70 3.7996BE+005 3.35194E+OOS 105.31 21.10 Pb-212 0.945 238.63* 43.60 1. 05287E+OOS 1.17105E+005 Bi-214 0.690 609.32* 45.49 1.04897E+005 7.20460E+004 11 20.29* 14 .92 1.1632BE+006 3.06639E+OOS 17 64.49 15 .30
       * - Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :               10.000 keV Nuclide confidence index threshold=                    0.30 Errors quoted at 2. 000 sigma

[1419]

Interference Corrected Activity Report 3/10/2018 9:04:28 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1. 000 1.270828E+006 3.424474E+OOS Co-60 1. 000 2.584840E+OOS./ 3.684543E+004 Ag-lOBm 0.420 1.075272E+003 4.601589E+004 Cs-137 1. 000 3. 488414E+006.I" 4.432336E+OOS Eu-152 1. 000 1 . 244902E+006./ 1.642733E+005 Eu-155 0.332 3.799676E+005 3.351936E+ODS Pb-212 0.945 1. 052869E+005 1.171046E+OOS Bi-214 0.690 1. 582613E+005 1. 11 0370E+005 X Pb-214 0.382 

       ?  = Nuclide is part of an undetermined solution X   := Nuclide rejected by the interference analysis
      @   = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2. 000 sigma

[1420]

interference Corrected Activity Report 3/10/2018 9:04:28 AM Page 5 

  **********      U N I D E N T I F I E D     P E A K S      **********

Peak Locate Performed on: 3/10/2018 9:04:28 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 3 1. 94 8.7335E-001 14. 48 2 39.91 2.9705E-001 85.72 3 74.99 1.8753E+OOO 16.91 11 778.55 2.7509E-001 23.27 Sum 12 867.15 5.7947E-002 77.99 Tol. Nb-94 13 963.78 2.7410E-001 23.44 14 1085.61 1. 8360E-001 3 0 .33 M  ; First peak in a multiplet region m = Other peak in a multiplet region F Fitted singlet Errors quoted at 2.000 sigma [1421]

Nuclide MDA Report 3/10/2018 9: 04 :28 AM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B101110AFSWC053GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/M"'2) (pCi/M"'2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*     10.66   3.706E+005   3.71E+005   1.271E+006 1. 685E+005
 +      Co-60      1173.23*     99.85   6.065E+004   4.84E+004   2.334E+005 2.865E+004 1332.49*     99.98   4.841E+004               2.835E+005 2.247E+004 Nb-94       702.65      99.81   6.965E+004   6.97E+004   3.156E+004 3.336E+004 871.09      99.89   7.918E+004               2.446E+004 3.805E+004
 +      Ag-108m     433.90*     90.50   7.723E+004   5.63E+004   4 .982E+004 3.720E+004 614.30*     89.80   5.631E+004               5.314E+004 2.659E+004 722.90      90.80   7.898E+004               6.822E+004 3.787E+004 Cs-134      604.72      97.62   8.893E+004   7.72E+004   4 .256E+004../4.303E+004 795.86      85.46   7.724E+004               2.432E+004 3.686E+004
 +      Cs-137      661. 66*    85.10   1.011E+005   l .01E+005  3.488E+006 4.884E+004
 +      Eu-152      121. 78*    28.67   4.254E+005   2.08E+005   1 .153E+006 2.093E+005 344.28*     26.60   2.927E+005               1 .146E+006 1. 419E+005 1408.01*     21. 07  2.085E+005               1 .359E+006 9.584E+004 Eu-154      123.07      40.40   4.475E+005   1. 43E+005  8.678E+005~ 2.213E+005 723.30      20.06   3.585E+005               5.465E+005 1.719E+005 1274.43      34.80   1.430E+005               4.270E+004 6.657E+004
 +      Eu-155       86.55*     30.70   5.339E+005   5.34E+005   3.800E+005 2.633E+005 105.31      21.10   8.664E+005               4.908E+005 4.283E+005 Tl-208      583.19      85.00   9.835E+004   9.84E+004  -6.070E+004 4.754E+004 Bi-212      727.33       6.67   l.057E+006   1 .06E+006  6.888E+005 5.064E+005
 +      Pb-212      238.63*     43.60   1.900E+005   1 .90E+005  1. 053E+005 9.254E+004
 +      Bi-214      609.32*     45.49   1.112E+005   1.11E+005   1. 049E+005 5.249E+004 1120.29*     14.92   3.803E+005               1. 163E+006 l.791E+005 1764.49      15. 30  2.512E+005               2.523E+005 1.130E+005 Pb-214      295.22      18.42   5.956E+005   2.19E+005  -1. 603E+005 2.917E+005 35 1. 93
  • 35.60 2.187E+005 8.565E+005 1.060E+005 Ra-226 186.21 3.64 3.647E+006 3.65E+006 8.300E+005 1.796E+006 Ac-228 338.32 11. 27 1.111E+006 2.79E+005 2.718E+005 5.448E+005 911. 20 25.80 2.795E+005 -1. 793E+005 1.337E+005 968.97 15.80 6.243E+005 1. 485E+005 3.021E+005 Am-241 59.54 35.90 6.638E+005 6.64E+005 1. 208E+005 3.274E+005
       + =Nuclide identified during the nuclide i dentification
       * ~ Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1422]

          • GAMMA S P E C T R U M ANALYSIS *****

Filename: 5452 Report Generated On 3/10/2018 10:32: 41 AM Sample Title B101110AFSWC054GD Sample Description Ul LOWER CTMNT Sample Identification 054 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"2 Sample Taken On 3/10/2018 10 :22: 00 AM Acquisition Started 3/10/2018 10 :22:37 AM Live Time 600. 0 seconds Real Time 602.8 seconds Dead Time 0.46 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1423]

Peak Analysis Report 3/10/2018 10:32:41 AM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC054GD Peak Analysis Performed on: 3/10/2018 10:32:40 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 119- 135 129.69 32.13 1. 36 3.39E+002 90.73 5.49E+002 2 152- 193 160 .82 39.91 1. 35 5.14E+002 210.03 1. 67E+003 3 281- 311 301.48 75.08 1.17 1.41E+003 243.17 2.74E+003 4 333- 346 3 40 .27 84.78 1.17 3.15E+002 131. 05 1. 44E+O 03 5 481- 498 488.30 121.80 1.21 9.83E+002 153.68 1.50E+003 6 973- 991 979.68 244.66 0.98 1 .89E+002 99.41 6.72E+002 7 1368- 1388 1377.92 344.24 1.47 9.16E+002 93.50 3.51E+002 8 1764- 1785 1776.85 443.99 0.64 1. 30E+002 71. 40 3.05E+002 9 2429- 2443 2436.00 608.80 0 .45 3.90E+001 38.05 1.12E+002 10 2633- 2660 2646.53 661. 44 1. 55 3.16E+003 129.35 2.30E+002 11 3104- 3125 3115.03 778.59 1. 58 3.33E+002 53.84 1.04E+002 12 3459- 3478 3469.05 867.11 0.70 1 .21E+002 44.67 1.08E+002 13 3845- 3868 3855.75 963.80 1. 77 4.14E+002 57.39 1.03E+002 14 4012- 4030 4020.10 1004.89 0.47 6.06E+001 31. 30 5.44E+001 15 4332- 4353 4342.88 1085.60 1. 64 2.59E+002 51. 86 1 .10E+002 16 4434- 4463 4448.18 1111.93 1. 38 3.97E+002 57.68 9.21E+001 17 4679- 4705 4693. 14 1173 . 18 1. 59 4.82E+002 53.64 5.41E+001 18 5091- 5106 5098.21 1274.46 1. 01 3.32E+001 20 .49 2.28E+001 19 5189- 5204 5196.54 1299.05 1. 16 4.16E+001 18.96 1.54E+001 20 5317- 5342 5330.20 1332.47 1.38 4.71E+002 48.76 2.91E+001 21 5617- 5645 5632.43 1408 .04 1. 89 5.86E+002 53.20 2.58E+001 22 5831- 5853 5843.57 1460.84 0.90 1.31E+002 29.66 2.26E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2. 000 sigma [1424]

Interference Corrected Activity Report 3/10/2018 10 :32 :41 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC054GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  . . .. . . . . .. . . . . . . . .. . IDENTIFIED NUCLIDES           ................ . .....

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 1. 000 1460.82* 10 .66 1.63234E+006 3.94685E+OOS Co-60 1. 000 1173.23* 99.85 5.95219E+005 8.15905E+004 1332.49* 99.98 6.03759E+OOS 7.90042E+004 Cs-137 1 .000 661.66* 85. 10 3.94862E+006 5.00964E+OOS Eu-152 1 .000 121. 78* 28.67 2.5019BE+006 6.35608E+OOS 344.28* 26.60 3.02632E+006 5.85486E+OOS 1408. 01* 21.07 3.63622E+006 4.39898E+005 Eu- 154 0.683 123.07* 40.40 1.77554E+006 4.52048E+005 723.30 20.06 1274.43* 34.80 1.20590E+005 7.51290E+004 Eu-155 0 .332 86.55* 30.70 8.55346E+005 3.95106E+005 1 05 .31 21.10 Pb-212 0 .944 238.63* 43.60 3.42813E+OOS 1.88731E+005 Bi-214 0 .689 609.32* 45.49 8.92070E+004 8.75841E+004 1120.29* 14. 92 3.23500E+006 5.36839E+OOS 1764.49 15.30 

        * - Energy line found in the spectrum.
        @ ~ Energy line not used for Weighted Mean Activity Energy Tolerance :                   10.000 keV Nuclide confidence index threshold=                         0.30 Errors quoted at 2.000 sigma

[1425]

Interference Corrected Activity Report 3/10/2018 10:32:41 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 1.000 1.632335E+006 3.946852E+005 Co-60 1.000 S.99626SE+Oos .l 5.675671E+004 Cs-137 1.000 3.948617E+006.I S. 00 9642E+OOS Eu-152 1. 000 3.165492E+006,1 3.069761E+005 Eu-154 0.683 1 . 046097E+OOS .I' 7.431218E+004 Eu-155 0.332 8.553455E+OOS 3.951060E+005 Pb-212 0.944 3.428129E+OOS 1 .887314E+005 Bi-214 0.689 1.707684E+OOS 8.644126E+OD4 X Pb-214 0.384 

      ?    Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ = Nuclide contains energy lines not used in weighted Mean Activity Errors quoted at   2.000 sigma

[1426]

Interference Corrected Activity Report 3/10/2018 10:32:41 AM Page 5 

  **********      U N I D E N T I F I E D        P E A K S      **********

Peak Locate Performed on: 3/10/20 18 10 :32:40 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.13 5.6519E-001 26.75 2 39. 91 8.5612E-001 40. 89 3 75.08 2.3550E+OOO 17.21 8 443.99 2.1630E-001 55. 01 D-Esc . 11 778.59 5.5417E-001 16 .19 Sum 12 867 .11 2.0227E-001 36.81 Tol. Nb-94 13 963.80 6.9025E-001 13.86 14 1004 .89 1. 010 OE- 0 01 51 .65 Sum 15 1085.60 4.3147E-001 20.03 19 1299.05 6.9298E-002 45.60 Sum M First peak i n a multiplet region m = Other peak i n a multiplet region F "" Fitted singlet Errors quoted at 2 . 000 sigma [1427]

Nuclide MDA Report 3/10/2018 10 :32:41 AM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B101110AFSWC054GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name {keV) ( %) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +      K-40       1460.82*    10.66   4 .180E+005   4.18E+005    1.632E+006 1.922E+OOS
 +      Co-60      1173.23*    99.85   6.595E+004    5. 0 4E+004   5.952E+005 3.131E+004 1332.49*    99.98   5.036E+004                  6.038E+OOS 2.344E+004 Nb-94       702.65     99.81   9.220E+004    9.22E+004   -1.081E+OOS 4.464E+004 87 1 . 09  99.89   1. 185E+005                 l .752E+005 S.772E+004 Ag-108m     433.90     90.50   1.346E+OOS    1 .09E+OOS  -9.200E+004 6.590E+004 614.30     89.80   1.208E+005                -8.239E+003 S.882E+004 722.90     90.80   1.086E+005                 1.643E+005 S.268E+004 Cs-134      604.72     97.62   1.089E+005    1. 09E+OOS   7. 261E+004/ 5. 302E+004 795.86     85.46   l.118E+005                -1.207E+004 5.412E+004
 +      Cs-137      661.66*    85.10   1 .347E+005   1.35E+OOS    3.949E+006 6.567E+004
 +      Eu-152      121.78*    28.67  5.942E+005     2.42E+005    2.502E+006 2.936E+005 344.28*    26.60  3.961E+005                  3.026E+006 1 .936E+OOS 1408. 01*   21. 07 2.416E+005                  3.636E+006 1.124E+OOS
 +      Eu-154      123.07*    40.40  4.216E+OOS     1.11E+005    1.776E+006 2.084E+005 723.30     20.06  4.910E+OOS                  6.629E+005 2.382E+005 1274.43*    34.80  1.112E+005                  l.206E+005 5.066E+004
 +      Eu-155       86.55*    30.70  5.713E+005     5.71E+005    8.553E+OOS 2.820E+OOS 105.31     21.10  1.035E+006                  1. 3 70E+OOS 5.128E+005 Tl-208      583.19     85. 00 1.290E+005     1. 29E+005   S.531E+004 6.286E+004 Bi-212      727.33      6.67  1 .456E+006    1. 4 6E+006 -6.430E+005 7.061E+OOS
 +      Pb-212      238.63*    43.60  2.901E+005     2.90E+005    3.428E+OOS 1 .426E+005
 +      Bi-214      609.32*    45.49  1 .412E+005    1. 4 1E+OOS  8.921E+004 6.753E+004 1120.29*    14.92  5.813E+005                  3.235E+006 2.796E+005 176 4 .49   15.30  2.046E+005                  7.711E+004 8.965E+004 Pb-214      295.22     18.42  7.187E+005     2.96E+OOS   -3.332E+OOS 3.53 2E+005 351 .93*   35.60  2.960E+OOS                  2.261E+006 l.447E+005 Ra-226      186.21      3.64  4.442E+006     4.44E+006    3.424E+005 2.194E+006 Ac-228      338.32     11.27  1.493E+006     3.57E+005    8.439E+OOS 7.361E+005 911.20     25.80  3.567E+005                 -2.30SE+005 1.723E+005 968.97     15.80  9.209E+005                  2.485E+005 4 .504E+005 Am-241       59.54     35.90  7.700E+OOS     7.70E+005    5.838E+OOS 3.805E+005
       + ~ Nuclide identified during the nuclide identification
       * = Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ = Half-life too short to be able to perform the decay correction

[1428]

                • ~****************************************************************
          • GAMMA S P E C T R U M ANALYSIS *****

Filename: 5452 Report Generated On 3/10/2018 9:20:27 AM Sample Title B101110AFSWC055GD Sample Description Ul LOWER CTMNT Sample Identification 055 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO MA2 Sample Taken On 3/10/2018 9: 10 : 00 AM Acquisition Started 3/10/2018 9: 10 :24 AM Live Time 600. 0 seconds Real Time 602.5 seconds Dead Time 0 .42 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1429]

Peak Analysis Report 3/10/2018 9:20:27 AM Page 2

          • PE AK A N A L Y S I S REPORT *****

Detector Name: 5452 Sample

Title:

B101110AFSWC055GD Peak Analysis Performed on: 3/10/2018 9:20:27 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 171 129.10 31.98 1. 58 1. 79E+003 183.20 7.70E+002 2 284- 308 301.48 75.08 1.18 1.12E+003 18 0. 84 1 .71E+003 3 333- 355 34 0 .11 84. 74 0.91 3.21E+002 171.41 l.81E+003 4 482 - 500 488.40 121.82 0.92 5.50E+002 13 8. 66 1. 25E+O 03 5 973- 991 980.44 244.85 0.70 1.25E+002 93.17 6.04E+002 6 1369- 1414 1377.68 344.18 0.84 3.99E+002 165.70 9.28E+002 7 2431- 2444 2437.40 609.15 1. 29 3.75E+001 32.70 8.25E+001 8 2630- 2659 2646.31 661.39 1. 52 6.23E+003 168.36 1 .80E+002 9 3106- 3126 3114.73 778.51 1. 36 l.99E+002 42.37 6.90E+001 10 3462- 3477 3469.18 867. 14 0.91 5.34E+001 28.69 5.06E+001 11 3845- 3866 3855.88 963.83 1. 76 2.16E+002 44.50 7.43E+001 12 4331- 4353 4342.99 1085.63 1.17 l.27E+002 40.83 7.41E+001 13 4437- 4458 4447.60 1111.79 1. 82 1. 84E+O 02 39. 82 5.68E+001 14 4681- 4705 4692.41 1173.00 1. 83 3.39E+002 46.75 5.00E+OOl 15 5090- 5105 5097.30 1274.24 0 .46 2.99E+001 15.58 l.OlE+OOl 16 5318- 5341 5329.31 1332.25 2.02 2.99E+002 40. 60 2.88E+001 17 5620- 5645 5631.93 1407.92 1. 96 3.27E+002 40 .53 2.06E+001 18 5834- 5853 5843.07 1460.71 0.78 l.11E+002 26. 82 2.02E+001 19 7052- 7067 7059. 11 1764.77 0.28 l.90E+001 8.72 O.OOE+OOO M ~ First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2. 000 sigma [1430]

Interference Corrected Activity Report 3/10/2018 9:20:27 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

B101110AFSWC055GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * * * * * * * * * * * *
  • I * *
  • IDENTIFIED NUCLIDES .. .. ......... ... ... . .

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/M"2 ) Uncertainty K-40 1. 000 1460.82* 10 .66 1.3765SE+006 3.53895E+005 Co-60 1. 000 1173.23* 99.85 4.1A700E+005 6.67533E+004 1332.49* 99.98 3.83636E+005 6.04277E+004 Cs-137 1.000 661.66* 85 .10 7.78427E+006 9.58186E+005 Eu-152 1.000 1 21.78* 28.67 1. 39884E+006 4.50514E+005 344.28* 26.60 1.31706E+006 5.88535E+005 1408.01* 21.07 2.03057E+006 2.99316E+005 Eu-154 0 .683 123.07* 40.40 9.92688E+OOS 3.20144E+005 723.30 20.06 1274 .43* 34.80 1.08562E+005 5.73179E+004 Eu-155 0.332 86.55* 30.70 8.73172E+005 4.97720E+005 105.31 21.10 Pb-212 0 .940 238.63* 43.60 2.27112E+005 1.73071E+005 Bi-214 0 .977 609.32* 45.49 8.57135E+004 7.54314E+004 1120 .29* 14 .92 1.50097E+006 3.46133E+005 1764 .49* 15.30 1.77588E+005 8.27151E+004 

          * - Energy line found in the spectrum.
          @ = Energy line not used for Weighted Mean Activity Energy Tolerance :                    10.000 keV Nuclide confidence index threshold                          0.30 Errors quoted at 2.000 sigma

[1431]

Interference Corrected Activity Report 3/10/2018 9:20:27 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) Uncertainty K-40 1 .000 1. 376550E+OD6 3.538951E+OOS Co-60 1.000 3.994282E+OOS~ 4.479865E+004 Cs-137 1.000 7.784266E+006v 9.581859E+OOS Eu-152 1. 000 1.721552E+006~ 2.303379E+OOS Eu-154 0.683 9.804963E+004/ S.661763E+004 Eu-155 0.332 8.731719E+OOS 4.977205E+OOS Pb-212 0.940 2 . 271123E+OOS 1.730707E+OOS Bi-214 0.977 1.621421E+OD5 5.502673E+004 X Pb-214 0.383 

      ? = Nuclide is part of an undetermined solution x = Nuclide rejected by the interference analysis
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2.000 sigma

[1432]

Interference Corrected Activity Report 3/10/2018 9:20:27 AM Page 5 

  **********      U N I D E N T I   F I E D    P E A K S    **********

Peak Locate Performed on: 3/10/2018 9:20:27 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak To l. No. (keV) Counts per Second  % uncertainty Type Nuclide 1 31. 98 2.9871E+OOO 10.22 2 75.08 1.8608E+OOO 16.20 9 778.51 3.3171E-001 21.29 Sum 10 867.14 8.8926E-002 53.78 11 963.83 3.5942E-001 20.63 12 1085.63 2.1146E-001 32.18 M  :; First peak in a multiplet region m  :; Other peak in a multiplet region F  :; Fitted singlet Errors quoted at 2 . 000 sigma [1433]

N'uclide MDA Report 3/10/2018 9:20:27 AM Page 6

          • N U C *LIDE MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B101110AFSWC055GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) (%) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       1460.82*   10.66  3.730E+005     3.73E+005    1.377E+006 1.697E+005
 +      Co-60      1173.23*   99.85   6.186E+004    4.83E+004    4.187E+005 2.926E+004 1332.49*   99.98   4. 829E+004                3.836E+OOS 2.241E+004 Nb-94       702.65    99.81   7.787E+004    7.79E+004   -9.092E+004 3.747E+004 87 1 .09  99.89   8.641E+004                 3.065E+004 4.167E+004 Ag-108m     433.90    90.50   1. 371E+005   8.68E+004   -4.376E+004 6.714E+004 614.30    89.80  1. 040E+005                -9.756E+004 5.042E+OD4 722.90    90.80  8.677E+004                 -3.898E+004 4.176E+004 Cs-134      604.72    97.62  1. 041E+005    8.39E+004    1.160E+OOSv5.060E+004 795.86    85.46  8.392E+004                 -1.460E+005 4.020E+004
 +      Cs-137      661.66*   85.10  1.234E+005     1.23E+005    7.784E+006 6.003E+004
 +      Eu-152      121.78*   28.67  5.531E+005     2.03E+005    1.399E+OD6 2.731E+OOS 344.28*   26.60  8.827E+005                  1.317E+006 4 .369E+OOS 1408.01*   21.07   2.031E+005                 2.031E+006 9.313E+004
 +      Eu-154      123.07*   40.40  3.925E+005     7.62E+004    9.927E+005 1 .938E+005 723.30    20.06  3.961E+005                  4.463E+004 1 .907E+005 1274 .43*  34.80   7.621E+004                 1. 086E+OOS 3.319E+004
 +      Eu-155       86.55*   30.70   7.571E+OOS    7 . 57E+005  8.732E+005 3.749E+OOS 105.31    21.10  9.379E+005                  9.320E+005 4.641E+OD5 Tl-208      583.19    85.00  1.144E+005     1.14E+OOS    6.987E+003 S.559E+004 Bi-212      727.33     6.67  1.223E+006     1.22E+006    9.167E+005 5.893E+005
 +      Pb-212      238.63*   43.60   2.750E+OOS    2.75E+005    2.271E+OOS 1.350E+D05
 +      Bi-214      609.32*   45.49  1. 202E+005    2.53E+004    8.571E+004 5.699E+004 1120.29*   14.92  4 .128E+005                 1.501E+D06 1.954E+005 1764.49*   15.30   2.529E+004                 1.776E+005 O.OOOE+OOO Pb-214      295.22    18.42   7.253E+005    6.60E+005    1.041E+006 3.565E+005 351.93*   35.60  6.595E+005                  9.841E+005 3.264E+005 Ra-226      186.21     3.64  4.249E+OD6     4 .25E+006   6.907E+005 2.098E+006 Ac-228      338.32    11. 27 l. 342E+006    2.91E+005    3.087E+005 6.604E+005 911.20    25.80  2.906E+005                 -2.226E+005 1. 392E+005 968.97    15. 80  7.118E+OD5                 2.266E+005 3.459E+005 Am-241       59.54    35.90  6.914E+005     6.91E+OOS   -9.038E+004 3.411E+005
       + =Nuclide identified during the nuclide identification
       *=Energy line found in the spectrum
       > ; Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1434]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/10/2018 10:20:20 AM Sample Title Bl01110AFSWC056GD Sample Description Ul LOWER CTMNT Sample Identification 056 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"2 Sample Taken On 3/10/2018 10:09:00 AM Acquisition Started 3/10/2018 10:10:17 AM Live Time 600.0 seconds Real Time 602.3 seconds Dead Time 0.37 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 1 7 8CM [1435]

Peak Analysis Report 3/10/2018 10 :20:20 AM Page 2

          • P E A K ANALYS I s REPORT *****

Detector Name: 5452 Sample

Title:

B101110AFSWC056GD Peak Analysis Performed on: 3/10/2018 10 :20:20 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area uncert. Counts 1 112- 139 129.03 31.96 1. 21 4.85E+002 99 .40 4.15E+002 2 151- 166 161.00 39.96 1. 65 3.28E+002 84.45 4.83E+002 3 280- 312 301.17 75.00 1.17 9.29E+002 229.89 2.40E+003 4 334- 357 351.31 87.54 1. 65 3.39E+002 178 .44 l.90E+003 5 481- 500 488. 44 121. 83 1.45 7.06E+002 146.61 1.33E+003 6 972- 988 979.54 244.63 0.79 1 .63E+002 78.14 4 .35E+002 7 1177- 1189 1182.85 295.46 0.89 -6.70E+OOO 52.20 2.62E+002 8 1367- 1389 1377.80 344.21 1. 32 6.98E+002 84.72 2.80E+002 9 1638- 1652 16 44 .83 410 .98 0.98 6.55E+001 46.03 1 .60E+002 10 1769- 1784 1776.26 443.84 0.55 6.96E+001 48.66 1 .73E+002 11 2431- 2445 2437.83 609.26 0.55 4.74E+001 32 .44 7.46E+001 12 2634- 2660 2646.48 661.43 1. 70 2.02E+003 100.61 1.17E+002 13 2886- 2899 2892.65 722.98 0 .57 3.46E+001 27.54 5.24E+001 14 3106- 3125 3115.66 778.75 1. 61 2.45E+002 44.58 7.21E+001 15 3461- 3478 3468.76 867.03 1. 43 7.40E+001 32.83 6.00E+OOl 16 3640- 3653 3646.51 911.48 0.87 3.77E+001 22.75 3.33E+001 17 3844- 3866 3856.00 963.86 1. Bl 3.04E+002 47. 82 6.90E+001 18 4011- 4027 4018.41 1004.47 0.80 4 .67E+001 25. 39 3.63E+001 19 4332- 4353 4343.54 1085.77 1. 48 l.57E+002 44.75 9.12E+001 20 4437- 4459 4447.99 1111.88 1.32 3.02E+002 41.18 3.24E+001 21 4679- 4705 4692.81 1173 .10 1. 62 3.54E+002 45. 99 4.00E+OOl 22 5090- 5106 5098.04 1274.42 0.47 3.63E+001 17.50 l .28E+001 23 5188- 5204 5196.29 1298.99 0.74 3.63E+001 18.21 1. 47E+001 24 5317- 5342 5330.15 1332.46 1. 50 3.04E+002 40. 04 2.27E+001 25 5618- 5646 5632.59 1408 .08 1. 96 4.45E+002 44. 44 1 .06E+001 26 5836- 5853 5844.25 1461. 0 0 1. 67 9.14E+001 25.19 2.06E+001 M =- First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1436]

Interference Corrected Activity Report 3/10/2018 10:20:20 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSWC056GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  .. ....... ' . . ... .. . . .. IDENTIFIED NUCLIDES            . . . . .......... . . . . .. .

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/M"'2 ) Uncertainty K-40 1 .000 1460.82* 10 .66 1.13470E+006 3.28067E+005 Co-60 1 .000 1173.23* 99.85 4.37216E+005 6.67048E+004 1332.49* 99.98 3.90106E+005 6.00749E+004 Cs-137 1. 000 661.66* 85.10 2.52442E+006 3.28175E+005 Eu-152 1.000 121. 78* 28.67 1 .79612E+006 5.18223E+005 344.28* 26.60 2.30395E+006 4.70855E+005 1408.01* 21.07 2.76287E+006 3.53307E+005 Eu-154 0.999 123.07* 40.40 1.27462E+006 3.68383E+OOS 723.30* 20.06 1. 8 7678E+005 l. 50782E+005 1274.43* 34.80 1. 31 734E+OOS 6.45080E+004 Eu-155 0.334 86.55* 30.70 8.94569E+005 5.03132E+005 105.31 21.10 Bi-212 0.970 727.33* 6.67 5.64442E+005 4.53606E+005 Pb-212 0.944 238.63* 43.60 2.95489E+005 l.49634E+005 Bi-214 0.689 609.32* 45.49 1. 08384E+005 7.52528E+004 1120.29* 14.92 2.45821E+006 3.89155E+005 1764.49 15.30 Ac-228 0.976 338.32* 11. 27 5.43789E+006 1.10765E+006 911.20* 25.80 1.68714E+005 1.02829E+005 968.97* 15.80 2.25409E+006 4 .06834E+005 

       *=Energy line found in the spectrum.
       @  - Energy line not used for Weighted Mean Activity Energy Tolerance :              10.000 keV Nuclide confidence index threshold ~                   0 .30 Errors quoted at 2.000 sigma

[1437]

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Uncertainty K-40 1.000 1.134704E+006 3.280670E+OOS Co-60 1.000 4 .112040E+005.,t' 4.463980E+004 X Ag-108m 0.936 Cs-137 1.000 2. 524420E+006./ 3.281745E+OOS Eu-152 1.000 2.339711E+006.J 2.480046E+005 Eu-154 0.999 1.162856E+005/ 6.371543E+004 Eu-155 0.334 8.945694E+OOS 5.031315E+OOS Bi-212 0.970 2.147133E+OOS 4.921854E+005 Pb-212 0.944 2.954888E+005 1.496345E+OD5 Bi-214 0.689 1 .93D853E+005 7.388404E+OD4 X Pb-214 0.939 Ac-228 0.976 2.959062E+005 9.914211E+004 

      ? ;  Nuclide is part of an undetermined so lution X =  Nuclide rejected by the interference analysis
      @  = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1438]

Interference Corrected Activity Report 3/10/2018 10 :20 :20 AM Page 5 

  **********     U N I D E N T I F I E D        P E A K S     **********

Peak Locate Performed on: 3/10/2018 10:20:20 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 96 8.0893E-001 20.48 2 39.96 5.4619E-001 25.77 3 75.00 1.5489E+OOO 24.74 7 295.46 -l .1162E-002 - 779.46 Tol. Pb-214 9 410.98 1. 0919E-001 70.26 10 443.84 1.1594E-001 69.95 D-Esc . 14 778.75 4.0820E-001 18.20 Sum 15 867.03 1. 2 327E- 0 01 44.39 Tol. Nb-94 18 1004.47 7.7826E-002 54.37 Sum 19 1085.77 2.6140E-001 28.53 Sum 23 1298.99 6.0441E-002 50.21 Sum M m 

         -  First peak in a multiplet region
         = Other peak in a multiplet region F  = Fitted singlet Errors quoted at    2 . 000 sigma

[1439]

Nuclide MDA Report 3/10/2018 10 :20:20 AM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B101110AFSWC056GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) (pCi/MA2 ) 

 +       K-40      1460.82*     10 .66  3.689E+005   3.69E+005   1. 135E+006 1.676E+OOS
 +       Co-60     1173.23*     99.85   5.705E+004   4 .49E+004  4.372E+005 2.685E+004 1332.49*     99.98   4.490E+004               3~901E+005 2.072E+004 Nb-94       702.65     99.81   8.214E+004   8.21E+004  -1.043E+003 3.961E+004 871. 09    99.89   9.259E+004               9.549E+004 4.476E+004 Ag-108m      433.90*    90.50   8.167E+004   5.23E+004   7.292E+004 3.941E+004 614.30*    89.80   5.905E+004               5.490E+004 2.796E+004 722.90*    90.80   5.226E+004               4.146E+004./2.451E+004 Cs-134      604.72     97.62   9.694E+004   9.52E+004   4.152E+004 4.703E+004 795.86     85.46   9.523E+004               1 .657E+005 4.585E+004
 +       Cs-137      66 1. 66*  85.10   9.613E+004   9.61E+004   2.524E+006 4.637E+004
 +       Eu-152      121. 78*   28.67   5.788E+005   1.58E+OOS   1.796E+006 2.860E+005 344.28*    26.60   3.689E+005               2.304E+006 1.800E+005 1408.01*     21.07  1.585E+005                2.763E+006 7.085E+004
 +       Eu-154      123.07*    40. 40 4 .108E+005   8.58E+004   1.275E+006 2.029E+005 723.30*    20.06   2.365E+OOS               1.877E+005 1 .109E+OOS 1274.43*     34.80   8.576E+004               1.317E+005 3.796E+004
 +       Eu-155       86.55*    30.70   7.640E+005   7.64E+OOS   8.946E+OOS 3.784E+005 105.31     21.10   9.261E+OOS              -6.310E+005 4.582E+005 Tl-208      583.19     85.00  1. 133E+005   1.13E+OOS   9.769E+004 5.501E+004
 +      Bi-212       727.33*     6.67   7.114E+005   7.llE+OOS   5.644E+005 3.336E+005
 +       Pb-212      238.63*    43.60  2.254E+OOS    2.25E+005   2.955E+OOS 1.102E+005
 +      Bi-214       609.32*    45.49  1.166E+OOS    1. 17E+OOS  1. 084E+005 5.519E+004 1120.29*     14 .92  3.187E+OOS               2.458E+006 1.483E+005 176 4 . 49   15.30  2.554E+OOS                2.617E+005 1 .151E+OOS Pb-214      295.22*    18.42  4.051E+OOS    2.76E+OOS  -3.048E+004 1 .964E+005 351. 93
  • 35.60 2.756E+005 1. 721E+006 1 .345E+005 Ra-226 186.21 3.64 3.947E+006 3.95E+006 1.117E+006 1. 94 7E+006
 +      Ac-228       338.32*    11. 27  8.706E+005   1.53E+OOS   5.438E+006 4.248E+005 911.20*    25.80  1. 531E+005               1. 687E+OOS 7.049E+004 968.97*    15.80  4.190E+005                2.254E+006 1.99SE+005 Am-241        59.54     35.90   6.788E+005   6:79E+005   1. 174E+005 3.349E+005
       + =Nuclide identified during the nuclide identification
       * - Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @    Half-life too short to be able to perform the decay correction

[1440]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/10/2018 9:36:39 AM Sample Title B101110AFSWC057GD Sample Description Ul LOWER CTMNT Sample Identification 057 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"'2 Sample Taken On 3/10/2018 9:25: 00 AM Acquisition Started 3/10/2018 9:26:36 AM Live Time 600. 0 seconds Real Time 601.7 seconds Dead Time 0 . 28 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 1 7 8CM Oai~ v41,,J<<ff?! 

                                                          .3 / f tJ- / (1l ,Q_ 0 1..r-1J!z_lJ;t~

5aF = Opf ?J~1r [1441]

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Detector Name: 5452 Sample

Title:

B1 01110AFSWC057GD Peak Analysis Performed on: 3/10/2018 9:36:39 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 112- 138 128.96 31.95 1. 31 5.58E+002 74.86 1.89E+002 2 154- 168 160.77 39.90 0.84 1.43E+002 63.09 2.96E+002 3 284- 307 301.40 75.06 1.16 7.04E+002 148.23 1. 2 OE+O 03 4 330- 345 339.14 84.50 0.52 6.99E+001 107.65 9.37E+002 5 478- 498 488.32 121.80 1. 11 3.71E+002 118.29 8.62E+002 6 975- 988 98 0 .90 244.97 0.31 4.00E+OOl 54.99 2.58E+002 7 1370- 1385 1377.78 344.20 1.45 2.05E+002 51.24 1.49E+002 8 2428- 2447 2437.23 609. 11 1. 51 6.20E+001 29. 68 4 .50E+001 9 2632- 2657 2646.50 661.44 1. 59 2.58E+003 105.40 4.61E+001 10 3105- 3126 3115.78 778.77 1. 71 1.00E+002 29 .63 3.19E+001 11 3846- 3865 3855.66 963.78 0.67 1.06E+002 31. 55 4.04E+001 12 4335- 4351 4342.19 1085.43 0.45 4.85E+001 24. 11 3.05E+001 13 4438- 4457 4448.54 1112.02 1. 75 8.43E+001 28. 89 3.47E+001 14 4636- 4649 4642.58 1160.54 0.83 1.30E+001 11. 36 7.00E+OOO 15 4683- 4703 4693. 00 1173.14 1. 75 1.57E+002 28 .15 1.18E+001 16 5191- 5206 5198.20 1299.47 0.31 1.90E+001 8.72 O.OOE+OOO 17 5319- 5340 5330.02 1332.43 1. 70 1.67E+002 27. 36 5.50E+OOO 18 5621- 5643 5632.37 1408.02 1. 02 1 .62E+002 27. 84 8.34E+OOO 19 5832- 5854 584 4. 29 1461. 01 0.61 1 .20E+002 24.80 8.51E+OOO 20 7052- 7067 7059.60 1764.89 0.27 2.12E+001 10.29 1. BOE+OOO M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1442]

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Sample

Title:

Bl01110AFSWC057GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB 

  .. ...... ' ... ... .... .. IDENTIFIED NUCLIDES           .. .. ......... ........

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 1.000 1460.82* 10.66 l .49661E+006 3.34323E+005 Co-60 1.000 1173.23* 99.85 1 .94204E+005 3.80778E+004 1332.49* 99.98 2.13462E+005 3.90165E+004 Cs-137 1.000 661.66* 85. 10 3.21981E+006 4.08469E+005 Eu-152 1.000 121.78* 28.67 9.44265E+005 3.55466E+005 344.28* 26.60 6.77243E+005 2.02557E+005 14 08.01* 21. 07 1 .00273E+006 1.90385E+005 Eu-155 0.331 86.55* 30.70 1 .90684E+OOS 2.95975E+005 1 05.31 21 .10 Pb-212 0.938 238.63* 43.60 7.25413E+004 1. 00517E+005 Bi-214 0.979 609.32* 45.49 1.41655E+005 6.99097E+004 1120.29* 14.92 6.87418E+005 2.41834E+OOS 1764.49* 15.30 1.98115E+005 9.75130E+004 

        * = Energy line found in the spectrum.
        @=Energy line not used for Weighted Mean Activity Energy Tolerance :          10.000 keV Nuclide confidence index threshold =               0.30 Errors quoted at 2. 000 sigma

[1443]

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/M"2 ) uncertainty K-40 1.000 1.496606E+006 3.343228E+005 Co-60 1 .000 2.035984E+OOS/ 2.725090E+004 Cs-137 1 .000 3.219809E+OD611 4 .084686E+005 Eu-152 1 .000 8.62512DE+005II' 1.292332E+005 Eu-155 0.331 1 .906836E+OOS 2.959751E+OOS Pb-212 0.938 7.25413DE+004 1 .005173E+005 Bi-214 0.979 1 .883690E+005 5.531077E+004 X Pb-214 0.384 

      ?  =  Nuclide is part of an undetermined solution X  =  Nuclide rejected by the interference analysis
      @  =- Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at    2 .000 sigma

[1444]

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  **********      UN I D E N T I F I E D      P E A K S      **********

Peak Locate Performed on: 3/10/2 018 9:36:39 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak To l. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 95 9.3072E-001 13.41 2 39.90 2.3888E-001 44.02 3 75.06 1 .1727E+OOO 2 1 .07 10 778.77 1.6688E-001 29.60 Sum 11 963.78 1.7601E-001 29.87 12 1085.43 8.0775E-002 49.74 14 1160.54 2.1667E-002 87.39 16 1299.47 3.1667E-002 45 . 88 Sum M First peak in a multiplet region m = Other peak in a multiplet region F ~ Fitted singlet Errors quoted at 2 . 000 sigma [1445]

Nuclide MDA Report 3/10/2018 9:36:39 AM Page 6

          • N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B101110AFSWC057GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +       K-40      1460.82*    10.66   2.693E+005     2.69E+005   1.497E+006 1.178E+005
 +       Co-60     1173.23*    99.85   2.930E+004     2.27E+004   1.942E+005 1.298E+004 1332.49*    99.98   2.265E+004                 2.135E+005 9.592E+003 Nb-94       702.65    99.81   5.848E+004     5.85E+004  -6.984E+004 2.778E+004 871.09    99.89   6.737E+004                -8.929E+003 3.214E+004 Ag-108m     433.90    90.50   9.863E+004     6.82E+004  -5.031E+004 4.790E+004 614. 3 0  89.80   8.356E+004                 4.498E+004 4.021E+004 722.90    90.80   6.818E+004                -1.660E+004 3.247E+004 Cs-134      604.72    97.62   7.537E+004     6.85E+004   1. 964E+004./ 3. 625E+004 795.86    85.46   6.851E+004                 3.061E+004 3.249E+004
 +       Cs-137      661.66*   85.10   6.140E+004     6 .14E+004  3.220E+006 2.901E+004
 +       Eu-152      121.78*   28.67   4.750E+005     1 .32E+005  9.443E+005 2.341E+005 344.28*   26.60   2.398E+005                 6.772E+005 1 .154E+005 1408.01*    21.07   1.323E+005                 1.003E+006 5.776E+004 Eu-154      123.07    40.40   3.854E+005     1 .32E+005  7.157E+oos.l 1 .9D3E+oos 723.30    20.06   3.119E+005                 l.351E+OOS l.486E+005 1274 .43    34.80   1.. 318E+005               9.966E+004 6.096E+004
 +       Eu-155       86.55*   30.70   4. 843E+005    4.84E+005   1.907E+OOS 2.385E+005 105.31    21.10   7.497E+005                 3.199E+OOS 3.700E+005 Tl-208      583.19    85.00   8.377E+004     8.38E+004  -4.408E+004 4.025E+004 Bi-212      727.33      6.67  9.583E+005     9.58E+OOS   7.097E+005 4.571E+OOS
 +       Pb-212      238.63*   43.60   1. 647E+005    1. 65E+005  7.254E+004 7.991E+004
 +       Bi-214      609.32*   45.49   1. 007E+005    9.60E+004   1.417E+OOS 4.727E+004 1120.29*    14.92   3.211E+005                 6.874E+005 1 .495E+005 1764.49*    15.30   9.604E+004                 1.981E+005 3.538E+004 Pb-214      295.22    1*9 .42 5.275E+005     1. 79E+005  6.091E+OOS 2.576E+005 351.93*   35.60   l.792E+005                 5.060E+005 8.624E+004 Ra-226      186.21      3.64  3.316E+006     3.32E+006   3.287E+006 1 .631E+006 Ac-228       338.32    11. 27  9.646E+005     2.24E+005  -3.824E+OOS 4.718E+005 911.20    25.80   2.244E+005                 1.241E+OOS l.061E+005 968.97    15.80   5.301E+005                 7.795E+004 2.550E+005 Am-241        59.54    35.90   5.592E+005     5.59E+005   3.231E+005 2.751E+005
       +    Nuclide identified during the nuclide identification
       * = Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @ = Half-life too short to be able to perform the decay correction

[1446]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/10/2018 10:06:11 AM Sample Title B101110AFSWC05 8GD Sample Description Ul LOWER CTMNT Sample Identification 058 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3. 00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO M"2 Sample Taken On 3/10/2018 9:55: 00 AM Acquisition Started 3/10/2018 9:56:08 AM Live Time 600.0 seconds Real Time 602.1 seconds Dead Time 0 . 35 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1447]

Peak Analysis Report 3/10/2018 10 :06: 11 AM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B101110AFSWC058GD Peak Analysis Performed on: 3/10/2018 10 :06:11 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 112- 137 129.44 32.07 1. 27 6.19E+002 87.60 3.06E+002 2 154- 188 160.87 39.92 1.31 2.58E+002 142.25 8.93E+002 3 284 - 307 301.52 75.09 1. 34 8.40E+002 162.89 1.45E+003 4 334- 347 340.44 84.83 1.19 2.00E+002 105.66 9.37E+002 5 481- 499 488.48 121. 84 1.22 5.36E+002 128.76 1 .06E+003 6 974- 989 979.88 244. 71 0.54 1.39E+002 67.97 3.37E+002 7 1369- 1386 1377.58 344.15 1. 13 3.78E+002 68.90 2.49E+002 8 1770- 1783 1776.55 443.91 0.75 4.97E+001 41.23 1.36E+002 9 1951- 1962 1956.44 488.89 0.38 2.63E+001 31. 67 8.97E+001 10 2631- 2658 2646.48 661.43 1. 57 2.99E+003 120.90 1.45E+002 11 3102- 3124 3115.37 778.67 1. 35 1 .66E+002 41. 66 6.90E+001 12 3461- 3478 3469.08 867. 11 1.16 6.09E+001 31.21 5.61E+001 13 3843- 3867 3855.59 963.76 0.98 2.13E+002 41.69 5.34E+001 14 4334- 4354 4342.82 1085.58 1. 07 1.05E+002 35.79 5.94E+001 15 4434- 4488 4447. 8 1 1111.84 1. 27 2.68E+002 48.51 4.20E+001 16 4680- 4706 4692.66 1173.06 1. 89 3.18E+002 40. 76 2.26E+001 17 5090- 5105 5097.77 1274.35 0.35 1.97E+001 16.09 1 .43E+001 18 5317- 5342 53 30 .73 1332.60 1. 91 3.15E+002 39.23 1 .64E+001 19 5619- 5645 5632. 18 1407.98 2.02 2.93E+002 37.36 l.30E+001 20 5834- 5854 5843.66 1460.86 1. 32 9.50E+001 29.11 3.lOE+OOl M = First peak in a multiplet region m ; Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000 sigma [1448]

Interference Corrected Activity Report 3/10/2018 10:06: 11 AM Page 3

          • N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample

Title:

B101110AFSWC058GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * .. * * * *
  • I * * *
  • a I I *
  • IDENTIFIED NUCLIDES *
  • I ll a * * * * * * * * " * * * * *
  • Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 1. 000 1460.82* 10.66 1 .1798SE+006 3.75836E+OOS Co-60 1.000 1173.23* 99.85 3.93221E+OOS 5.93628E+004 1332.49* 99.98 4.03401E+OOS 5.97655E+004 Cs-137 1.000 661.66* 85. 10 3.73834E+006 4.73659E+OOS Eu-152 1 .000 121.78* 28.67 1.36473E+006 4.26652E+OOS 344.28* 26.60 1.24898E+006 3.06472E+005 14 08.01* 21.07 1. 81 746E+O 06 2.73552E+OOS Eu-154 0 .683 1 23.07* 40.40 9.68487E+005 3.03212E+005 723.30 20.06 1274.43* 34.80 7. 14771E+ 004 5.87649E+004 Eu-155 0.332 86.55* 30.70 5.42427E+005 3.06831E+OOS 105.31 21.10 Pb-212 0.943 238.63* 43.60 2.51759E+OOS 1 .29898E+OOS
          *=Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                     10.000 keV Nuclide confidence index threshold ~                          0.30 Errors quoted at 2. 000 sigma

[1449]

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          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence {pCi/MA2 ) Uncertainty K-40 1.000 1 .179852E+006 3.758359E+OOS Co-60 1.000 3. 982764E+005v 4 .211748E+004 Cs-137 1. 000 3. 738343E+006J 4 .736594E+OOS Eu-152 1. 000 1.508622E+006J 1 .839090E+OOS Eu-154 0.683 6.517126E+OQ4/ 5 .786948E+004 Eu-155 0.332 S.424266E+OOS 3.068308E+005 Pb-212 0.943 2.517593E+OOS 1 .298984E+OOS X Pb-214 0.383 

      ?

X 

         =

Nuclide is part of an undetermined solution Nuclide rejected by the interference analysis 

      @  = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1450]

Interference Corrected Activity Report 3/10/2 018 10 :06:11 AM Page 5 

  **********    U N I D E N T I F I E D      P E AK S        **********

Peak Locate Performed on: 3/10/2018 10:06:11 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second  % Uncertainty Type Nuclide 1 32.07 1. 0317E+OOO 14 .15 2 39.92 4.2946E-001 55.20 3 75.09 1.3994E+OOO 19.40 8 443.91 8.2755E-002 83 . 03 D-Esc . 9 488.89 4 .3908E-002 120 . 23 Sum 11 778.67 2.7667E-001 25 . 09 Sum 12 867 .11 l .0148E-001 51.25 Tol. Nb-94 13 963.76 3.5428E-001 19.61 14 1085.58 1.7442E- 001 34.20 15 1111.84 4.4660E- 001 18.10 Tol. Bi-214 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1451]

Nuclide MDA Report 3 /10/2018 10 :06 :11 AM Page 6

          • N U C L I D E MD A REPORT *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B101110AFSWC058GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nucl ide MDA Activity Dec. Level Name (keV) (%) (pCi/MA2 ) (pCi/M"2 ) (pCi/M"2 ) (pCi/M"2 ) 

 +      K-40       1460.82*    10 .66  4.754E+005      4.75E+005  1.180E+006    2.209E+005
 +      Co-60      1173.23*    99.85   4.335E+004      3.88E+004  3.932E+005    2.001E+004 1332.49*    99.98   3.881E+004                 4.034E+005    1.767E+004 Nb-94       702.65     99.81   7.477E+004      7.48E+004  4.067E+003    3.592E+004 87 1. 09   99.89   8.725E+004                 7.251E+004    4 .208E+004 Ag-108m     433.90     90.50  1.163E+005       8.47E+004  3.377E+004    5.676E+004 614.30     89.80   9.725E+004                 1. 997E+004   4.705E+004 722.90     90.80   8.470E+004                -3.381E+004    4.073E+004 Cs-134      60 4 .72   97.62   9.006E+004      8.39E+004  1. 086E+OOSJ' 4.359E+004 795.86     85.46   8.392E+004                 2.070E+004    4.020E+004
 +      Cs-137      661.66*    85.10  1 .090E+005     1.09E+005   3.738E+006    5.282E+004
 +      Eu-152      121.78*    28.67   5.097E+005     1. 69E+005  1.365E+006    2.514E+005 34 4 .28*  26.60   3.179E+005                 1.249E+006    1.545E+OOS 1408 . 01*  21.07  1.693E+005                  1.817E+006    7.626E+004
 +      Eu-154      123.07*    40 .40  3.617E+005     9.01E+004   9.685E+005    1 .784E+005 723.30     20.06   3.843E+005                 4.242E+004    l .848E+OOS 1274.43*    34.80   9.009E+004                 7.148E+004    4.013E+004
 +      Eu-155       86.55*    30.70  4. 623E+005     4.62E+005   5.424E+005    2.275E+005 105.31     21. 10  8.494E+005                -5.SlOE+OOS    4.198E+005 Tl-208      583.19     85.00  1. 0 03E+O 05   1.00E+OOS  -5.523E+004    4.853E+004 Bi-212      727.33      6.67  1. 170E+O 06    1.17E+006   3.496E+005    S.630E+005
 +      Pb-212      238.63*    43.60  1. 953E+005     1.95E+005   2.51BE+005    9.518E+004 Bi-214      609.32     45.49   l. 912E+005    1 .91E+005  2.SOOE+OOS    9.253E+004 1120.29     14.92  5.262E+005                  3.219E+004    2.521E+005 176 4 .49   15.30  2.470E+005                  l .527E+OOS   1 .109E+005 Pb-214      295.22     18.42  6.127E+005      2.38E+005   5.73SE+003    3.002E+005 35 1 .93*  35.60  2.376E+005                  9.332E+005    l .154E+005 Ra-226      186.21      3.64  3.641E+006      3.64E+006   1.831E+006    1.793E+006 Ac-228      338.32     11.27  1.176E+006      2.79E+005   1.177E+OOS    5.773E+005 91 1. 20   25.80  2.787E+005                  1.615E+005    1.333E+005 968.97     15.80  6.598E+005                  8.740E+004    3.199E+OOS Am-241       59.54     35.90  6.238E+005      6.24E+005   2.759E+OOS    3.073E+OOS
       + = Nuclide identified during the nuclide i dentification
       *=Energy line found in the spectrum
       >=Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @=Half-life too short to be able to perform the decay correction

[1452]

          • GAMMA S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 3/10/2018 9:52:37 AM Sample Title B101110AFSWC059GD Sample Description Ul LOWER CTMNT Sample Identification 059 Sample Type GAMMA DIRECT Sample Geometry 1M90D Peak Locate Threshold 3.00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 3.140E+OOO MA2 Sample Taken On 3/10/2018 9:42: 00 AM Acquisition Started 3/10/2018 9:42:35 AM Live Time 600.0 seconds Real Time 601.8 seconds Dead Time 0 . 29 % Energy Calibration Used Done On 3/8/2018 Efficiency Calibration Used Done On 2/14/2018 Efficiency ID 1M90D ECP 17 8CM [1453]

Peak Analysis Report 3/10/2018 9:52:37 AM Page 2

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample

Title:

B1 01110AFSWC059GD Peak Analysis Performed on: 3/10/2018 9:52:37 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 112- 138 129.07 31.97 0.92 5.63E+002 82.01 2.58E+002 2 155- 167 160 .67 39.87 0.84 9.35E+001 60.40 3.08E+002 3 286- 309 301 .54 75.10 1. 23 7.22E+002 156.61 1. 35E+003 4 335- 347 340.35 84.80 1. 59 9.81E+001 94.84 8.10E+002 5 481- 498 488.61 121.87 1. 40 4.05E+002 110.23 8.07E+002 6 698- 710 703.97 175.72 1. 34 4.07E+001 62. 11 3.50E+002 7 973- 990 979.27 244.56 0.89 6.82E+001 68.56 3.38E+002 8 1086- 1097 1091 .10 272.52 0.58 3.51E+001 39.73 1. 43E+002 9 1178- 1189 1183.25 295.56 0.57 4.69E+001 37 .21 1. 17E+002 10 1366- 1420 1377.47 344.12 0.99 3.94E+002 126.82 4.62E+002 11 1772- 1784 1777.30 444.10 0.36 2.92E+001 34.30 9.98E+001 12 2430- 2443 2436.91 609.03 1. 06 3.51E+001 26.30 4.99E+001 13 2633- 2659 2646.50 661.43 1. 68 2.32E+003 107.05 1.25E+OD2 14 3107- 3126 3114.82 778.53 1. 56 1 .10E+002 34.22 5.24E+001 15 3463- 3478 3470.44 867.45 0 .55 3.03E+001 27.71 5.27E+001 16 3846- 3866 3855.90 963.84 1. 01 1.39E+002 34.52 4.39E+001 17 4334- 4352 4343.39 1085.73 0 .77 8.17E+001 26.75 2.73E+001 18 4438- 4459 4448.08 1111.91 1. 83 1.08E+002 30.92 3.51E+001 19 4681- 4701 4693. 14 1173.18 1. 38 2.03E+002 35.50 3.llE+OOl 20 5318- 5342 5329.68 1332.34 1. 58 1.87E+002 33.03 2.llE+OOl 21 5620- 5643 5631. 96 1407.92 1. 69 2.02E+002 31.53 1. 16E+001 22 5834- 5854 5843.63 1460.85 2.03 1 .18E+002 23.79 6.88E+OOO 23 7053- 7068 7060.36 1765.08 0.50 1 .70E+001 8.25 O.OOE+OOO M = First peak in a multiplet region m : Other peak in a multiplet region F : Fitted singlet Errors quoted at 2 . 000 sigma [1454]

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Sample

Title:

B101110AFSWC059GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB 

  * * * * * * * * * * * * * * * *
  • I
  • t IDENTIFIED NUCLIDES . ................ . .. .

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/MA2 ) Uncertainty K-40 1 .000 1460.82* 10.66 1.46702E+006 3.21743E+005 Co-60 1.000 11 73 .23* 99.85 2.50672E+005 4.82152E+004 1332.49* 99.98 2.39569E+005 4.64756E+004 Cs-137 1.000 661.66* 85.10 2.89819E+006 3.72849E+005 Eu-152 1.000 121.78* 28.67 1. 03 0 03E+O 06 3.48142E+005 344.28* 26.60 1.30175E+006 4.70344E+005 1408.01* 21.07 1 .25528E+006 2.19847E+005 Eu-155 0.332 86.55* 30.70 2.66476E+OOS 2.63142E+005 1 05.31 21.10 Pb-212 0.945 238.63* 43.60 1.23679E+005 1 .26017E+005 Bi-214 0.978 609.32* 45.49 8.01318E+004 6.08566E+004 1120.29* 14.92 8.79336E+005 2.61673E+005 1764.49* 15.30 1. 58905E+OOS 7.81241E+004 Pb-214 0.938 295.22* 18.42 2.13472E+OOS 1. 72789E+005 351.93* 35.60 9.72656E+005 3.49550E+005 

          * : Energy line found in the spectrum.
          @=Energy line not used for Weighted Mean Activity Energy Tolerance :                    10.000 keV Nuclide confidence index threshold=                          0.30 Errors quoted a t                 2.000 sigma

[1455]

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          • I N T E R F E R E N C E C O R R E C T E D REPORT *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/MA2 ) Unce rtainty K-40 1 .000 1.467025E+006 3.217431E+005 Co-60 1 .000 2. 449170E+005*/ 3.346130E+004 Cs-137 1.000 2. 898194E+006J 3.728487E+005 Eu-152 1. 000 1 .1 71325E+O 06 ../ 1.750865E+005 Eu-155 0.332 2.664760E+005 2.631417E+005 Pb-212 0.945 1.236787E+005 l .260172E+005 Bi-214 0.978 1. 349379E+005 4.722125E+004 Pb-214 0.938 1.906877E+005 1.570102E+005 

      ? =  Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @  = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   2.000 sigma

[1456]

Interference Corrected Activity Report 3/10/2018 9: 52: 37 AM Page 5 

  **********      U N I D E N T I F I E D      P E A K S      **********

Peak Locate Performed on: 3/10/2018 9:52:37 AM Peak Locate From Channel : 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak To l. No . (keV) Counts per Second  % Uncertainty Type Nuclide 1 31. 97 9.3864E-001 14 .56 2 39.87 1.5578E-001 64.62 3 75. 10 1. 2035E+OOO 2 1 .69 6 175.72 6.7903E-002 152.45 Sum 8 272.52 5.8549E-002 113 .10 11 444.10 4.8692E-002 117 .40 D-Esc. 14 778.53 1.8261E-001 31. 23 Sum 15 867.45 5.0422E-002 91.58 Tol. Nb-94 16 963.84 2.3177E-001 24.82 Sum 17 1085.73 1.3619E-001 32. 74 M -=; First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [1457]

Nuclide MDA Report 3/10/2018 9:52:37 AM Page 6

  • **** N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: 1M90D Sample

Title:

B101110AFSWC059GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/M"2 ) (pCi/M"2 ) (pCi/MA2 ) (pCi/M"2 ) 

  +       K-40      1460.82*     10 .66  2.311E+005    2.31E+005   1. 467E+O 06  9.873E+004
  +       Co-60     1173.23*     99.85   4 .637E+004   4 .25E+004  2.507E+005    2.151E+004 1332.49*     99.98   4 .254E+004               2.396E+005    1.954E+004 Nb-94       702.65     99.81  6.223E+004     6.22E+004   5.929E+004    2.965E+004 871.09     99.89   7.655E+004                9.003E+004    3.673E+004 433.90     90.50  9.924E+004     6.SOE+004  -1.119E+005    4.821E+004 614.30     89.80   7.890E+004               -1. 116E+004   3.788E+004 722.90     90.80  6.500E+004                -6.091E+004    3.088E+004 Cs-134      604.72     97.62   7.802E+004    6.82E+004   3.76SE+004.I  3.757E+004 795.86     85.46  6.822E+004                -9.791E+003    3.23SE+004
  +       Cs-137      661.66*    85.10  9.927E+004     9.93E+004   2.898E+006    4.794E+004
  +       Eu-152      121.78*    28.67  4 .364E+005    1.55E+005   1.030E+006    2.147E+005 34 4 .28*  26.60   6.633E+OOS                1. 302E+006   3.272E+005 1408.01*     21. 07 1 .554E+OOS                1. 255E+006 j 6. 932E+004 Eu-154      123.07     40 .40 4.037E+005     1 .27E+005  5.828E+005    1.994E+005 723.30     20.06  2.931E+OOS                -4.619E+005    1.392E+005 1274.43      34.80  1.270E+OOS                 9.006E+004    5.857E+004
  +       Eu-155       86.55*    30.70  4.219E+005     4.22E+OOS   2.665E+005    2.073E+005 105.31     21.10   7.879E+OOS               -5.025E+004    3.890E+005 Tl-208      583.19     85.00  8.760E+004     8.76E+004   9.941E+004    4.217E+004 Bi-212      727.33      6.67  9.552E+005     9.SSE+OOS   4.421E+005    4 .SSSE+OOS
  +       Pb-212      238.63*    43.60  2.036E+005     2.04E+005   1. 237E+005   9.933E+004
  +       Bi-214      609.32*    45.49   9.444E+004    2.53E+004   8.013E+004    4.413E+004 1120.29*     14.92  3.291E+005                 8.793E+005    1 .535E+005 1764.49*     15.30  2.529E+004                 1.589E+005    O.OOOE+OOO
  +       Pb-214      295.22*    18.42  2.714E+005     2.71E+005   2.135E+005    1. 295E+005 351.93*    35.60  4.956E+005                 9.727E+005    2.445E+005 Ra-226      186.21      3.64  3.414E+006     3.41E+006  -3.973E+004    1. 680E+006 Ac-228      338.32     11.27  1.008E+006     2.37E+OOS   6.136E+004    4.934E+005 91 1. 20   25.80  2.373E+005                -9.146E+004    1.126E+005 968.97     15.80  5.824E+005                 2.092E+005    2.812E+005 Am-241       59.54     35.90  5.958E+005     5.96E+OOS   2.288E+OOS    2.933E+005
        +=Nuclide identified during the nuclide identification
        *=Energy line found in the spectrum
        >    Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
        @=Half-life too short to be able to perform the decay correction

[1458]}}

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