Text

Revised Final Status Survey (FSS) Report - Phase 2, Eberline Analytical Reports
	ML19295G612
Person / Time
Site:	Zion File:ZionSolutions icon.png
Issue date:	04/04/2018
From:	; ZionSolutions
To:	; Office of Nuclear Material Safety and Safeguards
Shared Package
ML19295G627	List: ML19295G587; ML19295G611; ML19295G612; ML19295G617; ML19295G621; ML19295G625; ML19295G670; ML19295G674; ML19295G699; ML19295G702; ML19295G705; ML19295G726; ML19295G728; ML19295G734; ML19295G738; ML19295G742; ML19295G747; ML19295G751; ML19295G758; ML19295G764; ML19295G768; ML19295G788; ML19295G791; ML19295G795; ML19295G816; ML19295G818; ML19295G820; ML19295G822; ML19295G826; ML19295G828; ML19295G831; ML19295G837; ML19295G841; ML19295G843; ML19295G846; ML19295G850; ML19295G853; ML19295G855; ML19295G857; ML19295G859; ML19295G863; ML19295G866; ML19295G870; ZS-2019-0090, Revised Final Status Survey (FSS) Report - Phase 2, Release Record - Waste Water Treatment Facility Survey Unit 09100;
References
	ZS-2019-0090
	Download: ML19295G612 (37)
	v • d • e

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EBERLINE ANALYTICAL CORPORATION 601 SCARBORO RO/\\D OAK RIDGE, TENNESSEE 37830 PHONE (865) 1+81-068:5 FAX (865) L.,83--/.,.6?1 EBS-OR-43591 April 4, 2018 Alex Bohacheff Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099 SAMPLE RECEIPT CASE NARRATIVE Work Order# 18-03104-0R This work order contains ten solid samples received 03/22/2018. Samples were analyzed for Strontium-90, Tritium, Nickel-63 and by Gamma Spectroscopy.

CLIENT ID Bl01 l 10FIWC001CV B101 l 10FIWC003CV B 10111 OFIWC004CV B 10111 OFIFC005CV B 1011 1 OFIFC006CV ANALYTICAL METHODS LAB ID 18-03 104-04 18-03104-05 18-03104-06 18-03104-07 18-03 104-08 CLIENT ID B 10111 OFIFC008CV Bl01 l 10FIWC010CV Bl01110FIWC011CV Bl01 l 10FIWC018CV Bl01 l 10FIWC019CV LAB ID 18-03 104-09 18-03104-10 18-03 104-11 18-03 104-12 18-03104-13 Strontium-90 was analyzed using EIChroM Method SRW01 Modified. Tritium was perfonned using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.

Gamma Spectroscopy was performed using EPA Method 901.1 Modified.

Laboratory qualifiers are as follows:

U - Result is less than the MDA.

ANALYTICAL RES UL TS Combined Standard Unce11ainty is reported at I-sigma value.

Minimum Detectable Activity (MDA) values for data represented in this rep011 are sample-specific.

MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.

Page 1 of 3

[205]

ANALYTICAL RESULTS CONTINUED STRONTIUM-90 Samples were prepared by aliquoting as appropriate and leaching in HN03* Samples were diluted appropriately. Strontium recovery carriers were added to each sample. Chemical separations were conducted using selective extractions. Strontium precipitated was mounted on tared filter media.

Chemical recovery was determined by Strontium carrier mass detenninations. Samples were counted by gas flow proportional counting and corrected for Yttrium-90 ingrowth and decay.

Samples demonstrated acceptable results for all Strontium-90 analyses. Chemical recovery was acceptable for all samples. The Strontium-90 method blank demonstrated an acceptable result. Results for the Strontium-90 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Strontium-90 laboratory control sample demonstrated an acceptable percent recovery.

TRITIUM A representative aliquot of each sample was equilibrated with Tritium free water. Equilibrates were transferred into round-bottomed distillation flasks and attached to single stage stills. A portion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were then counted by beta liquid scintillation.

Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.

NICKEL-63 A representative aliquot of each sample was leached in HN03* Leachates were placed in appropriately sized beakers. Stable elemental Nickel carrier was added to each sample prior to digestion. Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.

Samples demonstrated acceptable results for all Nickel-63 analyses. All results demonstrated slightly high method detection limits. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated a high relative percent difference and normalized difference. In this case duplicate variations were caused by the heterogeneous sample nature. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.

GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass/aliquot of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.

Page 2 of 3

[206]

ANALYTICAL RES UL TS CONTINUED GAMMA SPECTROSCOPY CONTINUED Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. Some results demonstrated slightly high method detection limits. Some samples demonstrated results that are greater than the method detection limit. These results are reported from the Canberra Gamma Apex "Nuclide MDA Report" and are not positive. These results are qualified as non-detect (U). The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Cesium-13 7 replicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Cobalt-60 and Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-13 7 laboratory control sample demonstrated an acceptable percent recovery.

CERTIFICATION OF ACCURACY I ce1iify that this data rep01i is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her esignee to be accurate as verified by the following signature.

M.R. McDougall Laboratory Manager Date: 4/4/2018 Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please visit http://cberlineanalytical.com/ to provide us with feedback on our services.

Page 3 of 3

[207]

Printed: 4/4/2018 1:08 PM Page 1 of 14 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03104

. Zion __ Solutions,LLC Purchase Order 677118 Final Report of Analysis 101 Shiloh Blvd Analy~is Catt:ffCJry*..

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units LCS KNOWN 3/27/2018 18-03104 Tritium LANL ER-210 Modified 2.24E+02 8.06E+OO 18-03104-01 LCS SPIKE 03/22/18 00:00 3/22/2018 3/27/2018 18-03104 1.93E+02 18-03104-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/27/2018 18-03104 Tritium LANL ER-210 Modified

-2.27E+OO 18-03104-03 B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/27/2018 18-03104 Tritium LANL ER-210 Modified 8.21E+01 18-031 04-04 B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/27/2018 18-03104 Tritium LANL ER-210 Modified 8.80E+01 18-03104-05 TRG B101110FIWC003CV 03/14/18 14:13 3/22/2018 3/27/2018 18-03104 Tritium LANL ER-210 Modified 3.40E+01 18-031 04-06 TRG B101110FIWC004CV 03/15/18 08:15 3/22/2018 3/27/2018 18-03104 Tritium LANL ER-210 Modified 8.87E+01 1.21 E+02 1.09E+01 18-03104-08 TRG B101110FIFC006CV 03/15/18 09:50 3/22/2018 3/27/2018 18-03104 Tritium LANL ER-210 Modified 1.09E+02 18-031 04-09 TRG B 10111 OFIFC008CV 03/14/18 14:40 3/22/2018 3/28/2018 18-03104 Tritium LANL ER-210 Modified 2.29E+02 18-03104-10 TRG B101110FIWC010CV 03/14/1813:56 3/22/2018 3/28/2018 18-03104 Tritium LANL ER-210 Modified 3.44E+01 18-03104-11 TRG B101110FIWC011CV 03/14/18 13:29 3/22/2018 3/28/2018 18-03104 Tritium 18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/28/2018 18-03104 Tritium 18-03104-13 TRG B101110FIWC019CV 03/14/18 10:30 3/22/2018 3/28/2018 18-03104 Tritium LANL ER-210 Modified 3.01E+03 3.63E+01 18-031 04-01 LCS KNOWN 03/22/18 00:00 3/22/2018 3/27/2018 18-03104 Nickel-63 ASTM 3500-Ni Modified 1.49E+03 4.48E+01 18-03104-01 LCS SPIKE 03/22/18 00:00 3/22/2018 1.50E+03 9.47E+OO 18-03104-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/27/2018 18-03104 Nickel-63 ASTM 3500-Ni Modified 8.82E-01 1.28E+OO 18-03104-03 B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/27/2018 18-03104 Nickel-63 ASTM 3500-Ni Modified 2.95E+OO 9.98E-01 18-03104-04 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/27/2018 ASTM 3500-Ni Modified 6.94E+OO 1.06E+OO 18-03104-05 TRG B101110FIWC003CV 03/14/18 14:13 3/22/2018 3/27/2018 18-03104 Nickel-63 18-031 04-06 TRG B101110FIWC004CV 03/15/18 08:15 3/22/2018 3/27/2018 18-03104 Nickel-63 18-03104-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/27/2018 18-03104 Nickel-63 ASTM 3500-Ni Modified 18-031 04-08 B101110FIFC006CV 03/15/18 09:50 3/22/2018 3/27/2018 18-03104 Nickel-63 ASTM 3500-Ni Modified 1.19E+OO 7.31E-01 B10111 OFIFC008CV 03/14/18 14:40 3/22/2018 3/27/2018 18-03104 Nickel-63 ASTM 3500-Ni Modified 6.08E-01 1.25E+OO 18-03104-10 TRG B101110FIWC010CV 03/14/18 13:56 3/22/2018 3/27/2018 18-03104 Nickel-63 ASTM 3500-Ni Modified 7.01E-01 1.13E+OO u

18-03104-11 TRG 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/27/2018 18-03104 18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/28/2018 18-03104 Nickel-63 ASTM 3500-Ni Modified 1.89E+OO 18-03104-13 TRG B101110FIWC019CV 03/14/18 10:30 3/22/2018 3/28/2018 18-03104 Nickel-63 ASTM 3500-Ni Modified 4.10E+01 2.12E+OO 2.38E+OO CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect e

EBERLINE SER iCES 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/ 481-0683 FAX 865/483-4621

[208]

Printed: 4/4/2018 1 :08 PM Page 2 of 14 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03104

....... Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Anatr.sis Cat~Jl.o_ry:....-..

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 18-03104-01 LCS KNOWN 03/22/18 00:00 3/22/2018 3/30/2018 18-03104 Strontium-90 EIChroM SRW01 Modified 5.01E+01 2.81E-01 18-03104-01 LCS SPIKE 03/22/18 00:00 3/30/2018 18-03104 Strontium-90 2.68E+OO 6.67E+OO 1.11E+OO pCiig 18-03104-02 MBL BLANK 03/22/18 00:00 3/30/2018 7.33E-01 u

pCiig 18-03104-03 DUP B101110FIWC001CV 03/15/18 08:35 5.73E-01 u

pCiig 18-031 04-04 DO B101110FIWC001CV 03/15/18 08:35 2.84E-01 2.89E-01 5.62E-01 u

18-031 04-05 TRG B101110F1WC003CV 03/14/18 14:13 3/22/2018 3/30/2018 18-03104 Strontium-90 EIChroM SRW01 Modified 7.87E-02 2.73E-01 2.73E-01 5.75E-01 u

18-03104-06 TRG B 10111 OFIWC004CV 03/15/18 08:15 3/22/2018 3/30/2018 18-03104 Strontium-90 EIChroM SRW01 Modified 3.23E-01 2.76E-01 2.79E-01 5.53E-01 u

pCiig

_m ___ "'"-"'18-031 04-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/30/2018 18-03104 Strontium-90 E!ChroM SRW01 Modified 2.89E-01 2.89E-01 6.12E-01 u

18-031 04-08 TRG B101110F1FC006CV 03/15/18 09:50 4.59E-01 u

18-03104-09 TRG B101110FIFC008CV 03/14/1814:40 6.37E-01 u

18-03104-10 TRG B101110FIWC010CV 03/14/18 13:56 6.59E-01 u

18-03104-11 TRG B101110FIWC011CV 03/14/18 13:29 5.88E-01 u

18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 6.46E-01 u

B101110FIWC019CV 03/14/18 10:30 3/22/2018 3/30/2018 18-03104 Strontium-90 EIChroM SRW01 Modified 9.11E-01 3.73E-01 3.93E-01 6.93E-01 18-03104-01 LCS KNOWN 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 Cobalt-60 EPA 901.1 Modified 2.71E+02 1.06E+01 18-03104-01 LCS KNOWN 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 Cesium-137 EPA 901.1 Modified 1.69E+02 6.75E+OO 18-03104-01 LCS SPIKE 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 Cobalt-60 EPA901.1 Modified 2.72E+02 2.26E+01 2.66E+01 7.87E+OO pCiig

,--- ----'"-~----,

18-03104-01 LCS SPIKE 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 Cesium-137 EPA 901.1 Modified 1.94E+02 1.99E+01 2.22E+01 4.94E+OO pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE SER JCES 865/481-0683 FAX 865/483-4621

[209]

Printed: 4/4/2018 1 :08 PM Page 3 of 14 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03104 Zion Solutions,LLC Purchase Order:

677118 Final Report of Analysis w

101 Shiloh Blvd Analy_sis-Cat~!JOl)I~

ENVIRONMENT AL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units18-031 04-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 Actinium-228 EPA901.1 Modified BLANK 03/22/18 00:00 3/22/2018

,_oo-*--------*----.----,-,

18-03104-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 Americium-241 18-031 04-02 MBL BLANK 03/22/18 00:00 18-031 04-02 MBL BLANK 3/22/2018 18-03104 MBL BLANK 03/22/18 00:00 3/22/2018 18-03104 18-03104-02 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 18-031 04-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 18-03104-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/22/2018 18-03104

,~---*-------~-

18-03104-02 MBL BLANK 18-03104-02 MBL BLANK 18-03104-02 BLANK 03/22/18 00:00 3/22/2018 3/22/2018 18-031 04-02 BLANK 03/22/18 00:00 3/22/2018 3/22/2018 4.59E-02 18-03104-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 EPA 901.1 Modified 4.72E-02 pCi/g 18-03104-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 Niobium-94 EPA901.1 Modified 4.25E-02 18-03104-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 Lead-210 EPA 901.1 Modified 2.28E-01 3.77E-01 18-03104-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 Lead-212 EPA 901.1 Modified 5.47E-02 18-031 04-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 Lead-214 EPA 901.1 Modified 7.80E-02 18-03104-02 MBL BLANK 3.33E-02 18-03104-02 MBL BLANK 9.56E-02 u

18-031 04-02 03/22/18 00:00 3/22/2018 1.05E-01 18-03104-02 MBL BLANK 03/22/18 00:00 3/22/2018 4.64E-01 18-03104-02 MBL BLANK 03/22/18 00:00 3/22/2018 9.07E-02 1.39E-01 18-03104-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/22/2018 18-03104 Uranium-235 EPA 901.1 Modified

-1.54E-02 2.60E-01 1.46E-01 u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect E

601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[210]

Printed: 4/4/2018 1 :08 PM Page 4 of 14 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SOG:

18-03104 Zion Solutions,_ LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Anc3Jy~i~ Cat13-!l._ory:..

ENVIRONMENTAL

~---,--,,,--*---.,,,,-,-,+--"""'-

Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units 18-03104-03 DUP B101110FIWC001CV 03115/18 08:35 3122/2018 3/22/2018 18-03104 Actinium-228 EPA 901.1 Modified 1.53E-01 8.79E-01 1.28E+OO u

pCi/g 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Silver-108m EPA 901.1 Modified 8.84E-01 2.85E-01 18-031 04-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Americium-241 EPA 901.1 Modified

-1.98E-01 3.01E-01 3.69E-01 u

pCi/g 18-031 04-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Barium-133 EPA901.1 Modified 3.55E-02 1.83E-01 1.83E-01 3.49E-01 u

pCiig 18-03104-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Bismuth-214 EPA 901.1 Modified 5.89E-01 18-03104-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Cobalt-60 EPA901.1 Modified 3.07E-01 18-031 04-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Cesium-134 EPA 901.1 Modified 2.99E-01 u

pCi/g 18-03104-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Cesium-137 4.51E-01 18-031 04-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 1.56E+OO 18-03104-03 DUP 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 1.07E+OO 18-031 04-03 B10111 OFIWC001 CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 18-031 04-03 B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 18-031 04-03 B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Potassium-40 EPA901.1 Modified 7.43E+OO 1.88E+OO 1.92E+OO B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Manganese-54 EPA901.1 Modified 3.43E-01 u

18-03104-03 B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Sodium-22 EPA901.1 Modified 1.32E+OO 2.57E-01 3.34E-01 18-031 04-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Niobium-94 EPA901.1 Modified 3.00E-01 u

pCi/g B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Lead-210 EPA 901.1 Modified 9.48E+OO u

18-03104-03 DUP B101110F1WC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Lead-212 EPA901.1 Modified 5.19E-01 2.51E-01 1.01E+OO u

18-03104-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Lead-214 EPA901.1 Modified 9.04E-01 4.70E-01

.72E-01 6.72E-01 u

18-03104-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Promethium-145 EPA 901.1 Modified 1.51E+OO 1.61E+OO 1.59E+OO u

18-03104-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Radium-226 EPA 901.1 Modified

.71E-01 5.89E-01 B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Antimony-125 EPA 901.1 Modified 7.57E-01 u

pCi/g 18-031 04-03 DUP B 101110FIWC001 CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Thorium-234 EPA 901.1 Modified 18-031 04-03 DUP B101110F1WC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Thallium-208 EPA 901.1 Modified

.82E-01 18-03104-03 DUP B101110FIWC001CV 03/15/18 08:35 3/22/2018.

EPA 901.1 Modified 1.29E+OO u

pCiig CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE SER\\llCES FAX 865/483-4621

[211]

Printed: 4/4/2018 1 :08 PM Page 5 of 14 Report To*

Work Order Details:

Eberline Analytical J Alex Bohacheff SOG:

18-03104 Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis Cate_r;1_ory ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Qualifier Report ID Type ID Date Date Date ID Result cu CSU MDA Units 18-03104-04 DO 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Actinium-228 EPA901.1 Modified

-7.68E-02 4.62E-01 4.62E-01 1.28E+OO 18-031 04-04 DO B 10111 OFIWC001 CV 03/15/18 08:35 3/2212018 3/2212018 18-03104 Silver-108m EPA901.1 Modified 5.06E-01 2.79E-01 2.80E-01 2.49E-01 u

pCi/g

,,,, _____,m _____,_

18-031 04-04 DO 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Americium-241 EPA 901.1 Modified

-2.54E-01 3.01E-01 3.01E-01 3.69E-01 u

pCi/g 18-03104-04 DO 8101110FIWC001CV 03115/18 08:35 1.80E-01 1.80E-01 3.43E-01 u

pCi/g 18-03104-04 DO 8101110FIWC001 CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Bismuth-214 EPA 901.1 Modified 18-03104-04 DO 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Cobalt-60 EPA901.1 Modified 7.28E+OO 5.04E-01 6.27E-01 3.36E-01 18-03104-04 DO 8101110FIWC001CV 03/15118 08:35 3/22/2018 3/22/2018 18-03104 Cesium-134 EPA 901.1 Modified 18-03104-04 DO 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Cesium-137 EPA 901.1 Modified 18-031 04-04 DO 9.10E+01 3.75E+OO 5.99E+OO 1.36E+OO pCi/g 18-031 04-04 DO 810111 OFIWC001 CV 03/15/18 08:35 3/22/2018 18-03104 EPA 901.1 Modified 3.56E+OO 18-03104-04 DO 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Europium-155 EPA 901.1 Modified 1.23E+OO

,,,,,,,,--.~-'------------*------

18-03104-04 DO 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Holmium-166m EPA901.1 Modified

-1.67E-02 4.10E-01 4.10E-01 2.20E-01 u

pCi/g

,,,,,___,,,_m---

18-03104-04 8101110FIWC001CV 03/15/18 08:35 3/2212018 3/2212018 18-03104 lodine-129 EPA901.1 Modified 1.32E+OO 3.38E-01 3.45E-01 1.31E+OO pCi/g 18-03104-04 8101110FIWC001CV 03115/18 08:35 3122/2018 3/2212018 18-03104 Potassium-40 EPA 901.1 Modified 6.16E+OO 1.72E+OO 1.74E+OO 18-03104-04 DO 8101110FIWC001CV 03115/18 08:35 312212018 3/2212018 18-03104 Manganese-54 EPA 901.1 Modified 1.43E-01 2.32E-01 2.32E-01

"----w- ~mw,,, ___ -m~

18-03104-04 DO 8101110FIWC001CV 03115/18 08:35 3/22/2018 3/2212018 18-03104 Sodium-22 EPA901.1 Modified 1.44E+OO 2.78E-01 2.88E-01

,-----'-"'""""'" ______,,,,o,18-031 04-04 DO 8101110FIWC001CV 03115118 08:35 3122/2018 Niobium-94 3.44E-01 3.44E-01 18-03104-04 DO 8101110FIWC001CV 03115118 08:35 3122/2018 3/22/2018 18-03104 Lead-210 EPA901.1 Modified 1.72E+02 1.47E+01 1.71E+01 9.51E+OO u

pCi/g

~-------,,--,-

18-03104-04 DO B 10111 OFIWC001 CV 03115118 08:35 3122/2018 3122/2018 18-03104 Lead-212 EPA901.1 Modified 6.10E-01 2.49E-01 2.51E-01 1.07E+OO 18-03104-04 DO 8101110FIWC001CV 03115/18 08:35 3/22/2018 3/22/2018 18-03104 Lead-214 EPA901.1 Modified 8.02E-01 4.67E-01 4.69E-01 6.69E-01 18-03104-04 DO 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Promethium-145 EPA 901.1 Modified 1.27E+01 1.59E+OO 1.72E+OO 1.60E+OO 18-031 04-04 DO B101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Radium-226 EPA 901.1 Modified 8.40E-01 4.71E-01 4.73E-01 7.58E-01 18-03104-04 DO 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Antimony-125 EPA 901.1 Modified

-1.04E-01 5.23E-01 5.23E-01 7.55E-01 u

pCi/g 18-03104-04 DO 8101110FIWC001CV 03/15/18 08:35 3122/2018 3/22/2018 18-03104 Thorium-234 EPA 901.1 Modified 2.80E+OO 2.84E+OO 2.84E+OO 18-03104-04 DO 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Thallium-208 EPA901.1 Modified 4.17E-01 7.01E-01 7.01E-01 18-031 04-04 DO 8101110FIWC001CV 03/15/18 08:35 3/22/2018 3/22/2018 18-03104 Uranium-235 2.08E+OO 2.08E+OO 1.30E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect F

601 SCARBORO ROAD OAK RIDGE, TN 37830 865/ 481-0683 FAX 865/483-4621

[212]

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Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03104 Zion Solutions,_LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis Category:..

ENVIRONMENTAL

~---------"'

Zion, IL 60099 Sample Matrix:

so Lab Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID ID Date Date Date ID Units 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Actinium-228 03/14/1814:13 3/22/2018 3/22/2018 18-03104 Silver-108m 18-031 04-05 B101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Americium-241 EPA901.1 Modified

-2.49E+OO 5.14E-01 5.29E-01 9.01E-01 u

pCi/g EPA 901.1 Modified 1.51E+OO 18-031 04-05 TRG B101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Cobalt-60 EPA 901.1 Modified 1.24E+01 18-03104-05 TRG 810111 OFIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Cesium-134 EPA 901.1 Modified 2.81E-01 4.45E-01 4.46E-01 7.60E-01 pCi/g 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Cesium-137 18-031 04-05 TRG 8101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Europium-152 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Europium-154 EPA 901.1 Modified 5.86E+OO 4.52E+OO 4.53E+OO 1.66E+OO pCi/g 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 18-031 04-05 TRG 810111 OFIWC003CV 03/14/1814:13 3/22/2018 3/22/2018 18-03104 18-03104-05 TRG 8101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 18-031 04-05 8101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 18-03104-05 TRG 8101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Sodium-22 EPA901.1 Modified

-1.16E-02 18-03104-05 TRG 810111 OFIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104-05 TRG 8101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104-05 8101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Lead-212 EPA 901.1 Modified 1.56E-01 18-031 04-05 B 10111 OFIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Lead-214 EPA 901.1 Modified 7.39E+01 1.80E+01 18-03104-05 TRG 8101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Promethium-145 EPA 901.1 Modified 2.51E+02 4.26E+01 18-03104-05 TRG 810111 OFIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Radium-226 EPA 901.1 Modified 1.51E+OO 1.05E+OO 18-03104-05 TRG 8101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104

-3.07E-01 1.80E+OO 18-031 04-05 TRG 8101110FIWC003CV 03/14/1814:13 3/22/2018 3/22/2018 18-03104 Thorium-234 EPA 901.1 Modified

-4.05E+01 6.29E+OO 18-03104-05 TRG 8101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Thallium-208 EPA 901.1 Modified 7.96E-01 18-03104-05 8101110FIWC003CV 03/14/18 14:13 3/22/2018 3/22/2018 18-03104 Uranium-235 EPA 901.1 Modified

-8.58E+OO 8.06E+OO 8.07E+OO 4.08E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect EBERLINE SER iCES FAX 865/483-4621

[213]

Printed: 4/4/20181:08 PM Page 7 of 14 Report To.

Work Order Details:

Eberline Analytical J Alex Bohacheff SOG:

18-03104

.. Zion Solutions, LLC.

Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis Category:..

ENVIRONMENTAL

¥--- '"

Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch cu CSU Qualifier Report Analyte Method Result MDA ID Type ID Date Date Date ID Units 18-03104-06 TRG 8101110FIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Actinium-228 EPA901.1 Modified 5.08E-01 8.25E-01 8.25E-01 1.23E+OO u

pCi/g

,-----------¥'

18-03104-06 TRG 8101110FIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Silver-108m EPA 901.1 Modified 8.97E-01 2.86E-01 18-03104-06 TRG 8101110FIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Americium-241 EPA 901.1 Modified

-3.06E-01 3.52E-01 18-03104-06 8101110FIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 2.46E-01 3.75E-01 u

pCi/g 3/22/2018 18-03104 Bismuth-214 EPA 901.1 Modified 6.54E-01 3.26E-01 3.28E-01 7.14E-01 u

pCi/g 18-031 04-06 TRG 8101110FIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Cobalt-60 EPA 901.1 Modified 4.24E+OO 3.29E-01 3.94E-01 2.68E-01 pCi/g 18-031 04-06 TRG 8101110FIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Cesium-134 EPA901.1 Modified

-4.97E-02 8.94E-02 8.95E-02 2.71E-01 u

pCi/g 18-03104-06 TRG 8101110FIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Cesium-137 EPA901.1 Modified 4.65E+01 4.55E+OO 5.14E+OO 6.60E-01 pCi/g 18-03104-06 9.29E+01 3.67E+OO 6.02E+OO 1.14E+OO 18-03104-06 8101110FIWC004CV 03/15/18 08:15 3/22/2018 18-03104 EPA901.1 Modified 4.21E+OO 5.24E-01 5.66E-01 5.75E-01 3/22/2018 18-03104 Europium-155 EPA901.1 Modified 1.33E+OO 7.45E-01 7.48E-01 8.73E-01 pCi/g 3/22/2018 3/22/2018 18-03104 Holmium-166m EPA 901.1 Modified 4.82E-01 3.94E-01 3.94E-01 2.54E-01 u

pCi/g 3/22/2018 3/22/2018 18-03104 lodine-129 EPA901.1 Modified

-3.19E+OO 4.93E-01 5.20E-01 3.88E-01 5.07E+OO 1.48E+OO 1.50E+OO 2.60E+OO pCi/g 18-03104-06 TRG B101110FIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Manganese-54 EPA 901.1 Modified

-4.33E-02 2.37E-01 2.37E-01 3.40E-01 18-03104-06 TRG 810111 OFIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Sodium-22 EPA 901.1 Modified 2.41E-01 3.88E-01 18-03104-06 TRG 8101110FIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Niobium-94 EPA901.1 Modified 8.08E-01 3.57E-01 3.59E-01 3.24E-01 18-031 04-06 TRG 810111 OFIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Lead-210 EPA 901.1 Modified 1.64E+02 1.46E+01 1.69E+01 8.59E+OO pCi/g

-*--=*=**----*-*

18-031 04-06 TRG 810111 OFIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Lead-212 EPA 901.1 Modified 3.02E-01 3.48E-01 3.49E-01 4.50E-01 u

pCi/g

'" a nm~-------*

18-031 04-06 TRG 8101110FIWC004CV 03/15/18 08:15 3/22/2018 EPA 901.1 Modified 8.03E-01 4.01E-01 4.03E-01 7.14E-01

-~------ '-----~---*--*--,--,,,

18-03104-06 TRG 8101110FIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Promethium-145 EPA 901.1 Modified

-1.21E+OO 1.38E+OO 1.38E+OO 7.65E-01 18-03104-06 TRG 8101110FIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Radium-226 EPA 901.1 Modified 6.54E-01 3.26E-01 3.28E-01 7.14E-01

-*---*--~*-* ---*---~--**

18-03104-06 TRG 810111 OFIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Antimony-125 EPA 901.1 Modified 2.48E-01 5.63E-01 5.63E-01 9.02E-01 18-03104-06 TRG 810111 OFIWC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Thorium-234 EPA 901.1 Modified 1.02E+OO 3.32E+OO 3.32E+OO 4.23E+OO 18-03104-06 TRG 8101110FIWC004CV 03/15/18 08:15 3/22/2018 3/2212018 18-03104 Thallium-208 EPA901.1 Modified 2.17E-01 6.05E-01 6.05E-01 5.60E-01 18-03104-06 TRG B101110F1WC004CV 03/15/18 08:15 3/22/2018 3/22/2018 18-03104 Uranium-235 EPA901.1 Modified

-1.56E+OO 3.11E+OO 3.11E+OO 1.47E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

,,..,," _EBERLINE

~~

SERV*CES TN 37830 865/481-0683 FAX 865/483-4621

[214]

Printed: 4/4/2018 1 :08 PM Page 8 of 14 Report To:

Work Order Detai/s:

Eberline Analytical J Alex Bohacheff SDG:

18-03104 Zion Solutions, LLG.....

Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd AnalysisCategory: _

ENVIRONMENTAL

,,w"~-""_v_" --

Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units 18-03104-07 TRG B101110FIFC005CV u

18-03104-07 TRG B101110F1FC005CV u

pCiig 18-031 04-07 TRG B101110FIFC005CV 18-031 04-07 TRG B101110F1FC005CV u

pCi/g 18-03104-07 TRG B101110FIFC005CV u

18-03104-07 TRG B101110FIFC005CV u

18-03104-07 TRG B101110FIFC005CV 18-03104-07 TRG B101110F1FC005CV 18-03104-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Europium-152 EPA 901.1 Modified 9.04E+01 18-03104-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 EPA901.1 Modified 6.14E-02 18-031 04-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Europium-155 EPA 901.1 Modified 1.98E+OO 18-03104-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Holmium-166m 18-03104-07 B101110FIFC005CV 18-03104-07 18-03104-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Manganese-54 EPA 901.1 Modified

-3.47E-01 5.27E-01 5 28E-01 7.64E-01

--'- _,oaa-*-*"'"

18-03104-07 TRG B101110F1FC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Sodium-22 EPA 901.1 Modified 2.19E-02 9.23E-02 9 23E-02 18-03104-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Niobium-94 EPA 901.1 Modified 2.22E+OO 7.19E-01 7.28E-01 7.15E-01 u

pCi/g

'"~-,----*

18-031 04-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Lead-210 EPA901.1 Modified 8.62E+02 8.63E+01 9.70E+01 2.72E+01 u

pCi/g 18-03104-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Lead-212 EPA 901.1 Modified 1.01E+OO 7.09E-01 7.11E-01 18-03104-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 1.69E+OO 9.74E-01 9.78E-01 18-03104-07 TRG B101110F1FC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Promethium-145 EPA 901.1 Modified 1.75E+02 2.97E+01 3.10E+01 18-03104-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Radium-226 EPA901.1 Modified

-3.51E-01 1.00E+OO 1.00E+OO 18-03104-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Antimony-125 EPA901.1 Modified 1.63E-02 1.38E+OO 1.38E+OO

"'"-~*-*-*- * * -"w B 10111 OFIFC005CV 18-03104 Thorium-234 EPA 901.1 Modified 18-03104-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Thallium-208 EPA 901.1 Modified 18-031 04-07 TRG B101110FIFC005CV 03/15/18 09:30 3/22/2018 3/22/2018 18-03104 Uranium-235 EPA 901.1 Modified

-3.26E+OO 6.96E+OO 6.96E+OO 3.72E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma};MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect t:

601 SCARBORO ROAD OAK RIDGE, TN 37830 865/ 481-0683 FAX 865/483-4621

[215]

Printed: 4/4/20181:08 PM Page 9 of 14 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03104 Zion Solutions,LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis Category:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Method Units 18-03104-08 TRG 810111 OFIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Actinium-228 EPA 901.1 Modified

-7.74E-02 7.90E-01 7.90E-01 18-031 04-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 2.52E-01 1.99E-01 18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Bismuth-214 EPA 901.1 Modified 6.37E-01 4.56E-01 4.57E-01 18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Cobalt-60 EPA 901.1 Modified 3.42E+OO 2.78E-01 3.29E-01 18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Cesium-134 EPA 901.1 Modified 5.29E-02 1.03E-01 1.03E-01 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Cesium-137 EPA 901.1 Modified 5.76E-01 2.60E-01 2.62E-01 18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Europium-152 EPA 901.1 Modified 7.61E+01 3.05E+OO 4.95E+OO 18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Europium-154 EPA901.1 Modified 2.74E+OO 18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Europium-155 EPA 901.1 Modified 1.15E+OO 18-031 04-08 TRG 8101110FIFC006CV 03/15/18 09:50 EPA901.1 Modified 5.50E-02 3.75E-01 3.75E-01 2.05E-01 18-031 04-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 lodine-129 EPA 901.1 Modified 1.37E+OO 2.39E-01 2.50E-01 3.39E-01 u

18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Potassium-40 EPA 901.1 Modified 5.56E+OO 1.42E+OO 1.44E+OO 2.94E+OO 18-03104-08 TRG B101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Manganese-54 EPA901.1 Modified 4.95E-02 1.92E-01 1.92E-01 3.18E-01

,c,-,-co--, ""*---*-

18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Sodium-22 2.08E-01 2.13E-01 2.72E-01 18-031 04-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Niobium-94 EPA 901.1 Modified 3.33E-01 3.35E-01 2.87E-01 18-031 04-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Lead-210 EPA 901.1 Modified 1.55E+02 1.36E+01 1.58E+01 6.95E+OO 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Lead-212 EPA 901.1 Modified 4.18E-01 2.20E-01 2.21E-01 8.41E-01 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Lead-214 EPA901.1 Modified 7.98E-01 3.32E-01 3.35E-01 5.88E-01 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Promethium-145 EPA901.1 Modified 2.15E+OO 1.35E+OO 1.36E+OO 2.56E+OO 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Radium-226 EPA 901.1 Modified 4.57E-01 7.44E-01

,---~------------,---~------

"'""'"---~-----*--------

18-031 04-08 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 EPA 901.1 Modified 3.70E-01 5.97E-01 18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Thorium-234 EPA 901.1 Modified

-1.07E+OO 2.83E+OO 2.83E+OO 3.54E+OO 18-03104-08 TRG B 10111 OFI FC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Thallium-208 EPA 901.1 Modified 4.05E-01 2.71E-01 2.72E-01 5.23E-01 18-03104-08 TRG 8101110FIFC006CV 03/15/18 09:50 3/22/2018 3/22/2018 18-03104 Uranium-235 EPA901.1 Modified

-8.63E-01 2.45E+OO 2.45E+OO 1.20E+OO u

pCiig CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect FAX 865/483-4621

[216]

Printed: 4/4/20181:08 PM Page 10 of 14 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG.

18-03104 Zion Soluti<>DStLLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd ATlajy:sJs Cate90,y*_

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU Qualifier Report ID Type ID Date Date Date ID MDA Units 18-03104-09 TRG B10111 OFIFC008CV 03114/18 14:40 3122/2018 3/2212018 18-03104 Actinium-228 EPA 901.1 Modified 6.58E-01 1.08E+OO 1.08E+OO 1.59E+OO u

18-03104-09 TRG B101110FIFC008CV 03114/18 14:40 3122/2018 3/2212018 18-03104 Silver-108m EPA 901.1 Modified 7.19E-01 3.50E-01 18-03104-09 TRG B101110FIFC008CV 03/14118 14:40 3/2212018 3/22/2018 18-03104 Americium-241 EPA 901.1 Modified

-4.25E-01 3.95E-01 2.35E-01 18-03104-09 TRG B101110F1FC008CV 03114/18 14:40 3/2212018 3/2212018 18-03104 Bismuth-214 EPA 901.1 Modified 8.01E-01 3.86E-01 18-03104-09 TRG B101110FIFC008CV 03114/18 14:40 3/2212018 3/2212018 18-03104 Cobalt-60 EPA 901.1 Modified 7.72E+OO 5.28E-01 6.60E-01 TRG B101110FIFC008CV 03114/18 14:40 3/2212018 3/2212018 18-03104 Cesium-134 EPA901.1 Modified

-1.01E-02 1.65E-01 EPA 901.1 Modified 7.12E-01 2.94E-01 18-03104-09 TRG B101110F1FC008CV 03114/18 14:40 3/2212018 3/2212018 18-03104 Europium-152 EPA 901.1 Modified 1.37E+02 5.60E+OO

--_,-mm-""'"'"'="=*"-

18-031 04-09 TRG 8101110FIFC008CV 03114/18 14:40 3/2212018 3/2212018 18-03104 Europium-154 EPA 901.1 Modified 4.70E+OO 7.70E-01 18-031 04-09 TRG 8101110FIFC008CV 03/14/1814:40 3/2212018 3/2212018 18-03104 Europium-155 EPA901.1 Modified 1.15E+OO 4.95E-01

,,,_, ------~-"""""""18-031 04-09 TRG 8101110FIFC008CV 03/14118 14:40 3/2212018 3/2212018 18-03104 Holmium-166m EPA 901.1 Modified 1.12E-01 5.21E-01 18-031 04-09 1.94E+OO 4.04E-01 03114/1814:40 3/2212018 3/2212018 18-03104 Potassium-40 1.97E+OO 03114/18 14:40 3/2212018 3/22/2018 18-03104 Manganese-54 EPA 901.1 Modified 1.29E-02 2.92E-01

'""""'"'"' --~-----------

18-031 04-09 B101110F1FC008CV 03/14118 14:40 3/2212018 3/2212018 18-03104 Sodium-22 EPA 901.1 Modified 1.70E+OO 3.46E-01 18-03104-09 8101110FIFC008CV 03114/18 14:40 3/2212018 3/2212018 18-03104 Niobium-94 EPA 901.1 Modified

-2.09E-01 4.60E-01 18-031 04-09 TRG 8101110FIFC008CV 03114/18 14:40 3/2212018 3/2212018 18-03104 Lead-210 EPA 901.1 Modified 2.48E+02 2.10E+01 18-031 04-09 TRG 8101110FIFC008CV 03/14118 14:40 3/2212018 3/2212018 18-03104 Lead-212 2.31E-01 2.15E-01 18-031 04-09 TRG 8101110FIFC008CV 03114/18 14:40 3122/2018 3/2212018 18-03104 Lead-214 EPA 901.1 Modified 1.73E+OO 6.30E-01 18-031 04-09 TRG 8101110FIFC008CV 03/14118 14:40 3122/2018 3/2212018 18-03104 Promethium-145 EPA901.1 Modified 1.73E+01 2.14E+OO 18-03104-09 TRG 8101110FIFC008CV 03114/1814:40 3122/2018 3/2212018 18-03104 Radium-226 8.01E-01 3.86E-01 18-03104-09 TRG 8101110FIFC008CV 03114/18 14:40 3/2212018 3/2212018 18-03104 Antimony-125 EPA 901.1 Modified

-8.64E-03 6.85E-01 18-03104-09 TRG 8101110FIFC008CV 03114/18 14:40 312212018 3/2212018 18-03104 Thorium-234 EPA901.1 Modified 3.37E+OO 3.75E+OO 18-03104-09 TRG B101110FIFC008CV 03114118 14:40 312212018 3/2212018 18-03104 Thallium-208 EPA 901.1 Modified

-1.51E-01 3.59E-01 18-03104-09 TRG 8101110FIFC008CV 03114/18 14:40 3/2212018 3/2212018 18-03104 Uranium-235 EPA 901.1 Modified 3.59E-01 2.76E+OO CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect

(

EBERLINE SERV!CES 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683

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677118 Final Report of Analysis 101 Shiloh Blvd Analysis Category:_

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte cu CSU Qualifier Report ID Type ID Date Date Date ID Method Result MDA Units 18-03104-10 TRG 8101110FIWC010CV 03/14118 13:56 3/2212018 3/2212018 18-03104 Actinium-228 EPA 901.1 Modified

-6.50E-01 9.20E-01 9.21E-01 1.32E+OO u

pCi/g 18-03104-10 TRG 8101110FIWC010CV 03/14/1813:56 3/2212018 3/2212018 18-03104 Silver-108m EPA 901.1 Modified 3.90E-01 2.63E-01 2.63E-01 3.30E-01 u

pCilg 18-03104-10 TRG 8101110FIWC010CV 03/14118 13:56 3/2212018 3/2212018 18-03104 Americium-241 1.40E-01 1.43E-01 4.58E-01 18-03104-10 TRG B101110FIWC010CV 03114/18 13:56 3/2212018 3/2212018 18-03104 Barium-133 EPA901.1 Modified

-3.88E-02 6.54E-02 6.54E-02 4.85E-01 18-03104-10 TRG B101110FIWC010CV 03114/18 13:56 3/2212018 3/2212018 18-03104 Bismuth-214 EPA 901.1 Modified 1.35E+OO 4.94E-01 4.99E-01 7.04E-01 pCilg

' ---~----- ~

18-03104-10 TRG 8101110FIWC010CV 03/14/1813:56 3/2212018 3/2212018 18-03104 Cobalt-60 EPA901.1 Modified

-5.32E-02 5.75E-02 5.76E-02 4.68E-01 u

pCilg 18-03104-10 TRG 8101110FIWC010CV 03114/18 13:56 3/22/2018 3/22/2018 18-03104 Cesium-134 EPA901.1 Modified

-3.63E-02 1.17E-01 1.17E-01 3.92E-01 u

pCilg 18-03104-10 4.18E-02 1.20E-01 1.20E-01 4.43E-01 u

18-03104-10 8101110FIWC010CV 03/14/1813:56 3/2212018 3/2212018 18-03104 EPA 901.1 Modified 3.47E+01 3.67E+OO 4.08E+OO 2.88E+OO 18-03104-10 TRG 8101110FIWC010CV 03114118 13:56 3122/2018 312212018 18-03104 4.65E-01 4.68E-01 8.36E-01 u

18-03104-10 8101110FIWC010CV 03114/18 13:56 3122/2018 3/2212018 18-03104 Europium-155 EPA 901.1 Modified 1.24E+OO 3.38E-01 3.44E-01 9.56E-01 18-03104-10 8101110FIWC010CV 03/14/1813:56 3122/2018 3/2212018 18-03104 Holmium-166m EPA 901.1 Modified

-2.10E-01 18-03104-10 TRG 8101110FIWC010CV 18-03104-10 TRG 8101110FIWC010CV 18-03104-10 TRG 8101110FIWC010CV 03/14118 13:56 3122/2018 3/2212018 18-03104-10 TRG 8101110FIWC010CV 03/14118 13:56 3/2212018 3/2212018 18-03104 1.66E-01 1.67E-01 2.98E-01 u

18-03104-10 TRG 8101110FIWC010CV 03/14118 13:56 3/2212018 3/22/2018 18-03104 Niobium-94 EPA901.1 Modified 2.82E-02 7.65E-02 7.65E-02 3.56E-01 u

18-03104-10 TRG B101110FIWC010CV 03114/18 13:56 3/22/2018 3122/2018 18-03104 Lead-210 EPA 901.1 Modified 7.35E+01 9.52E+OO 1.02E+01 1.06E+01 pCilg

*"'-~.,_ """~-*--'-"""m""~'"'" ___ "'"'"" ___

18-03104-10 TRG 8101110FIWC010CV 03/14/18 13:56 3/22/2018 3/2212018 18-03104 Lead-212 EPA 901.1 Modified 7.70E-01 3.55E-01 3.58E-01 8.95E-01 u

18-03104-10 TRG 8101110FIWC010CV 3/2212018 18-03104 Lead-214 EPA 901.1 Modified 1.87E+01 4.62E+OO 4.71E+OO 1.46E+OO u

18-03104-10 TRG 8101110FIWC010CV 2.40E+OO u

18-03104-10 TRG 8101110FIWC010CV 7.04E-01 18-03104-10 TRG 8101110FIWC010CV 9.99E-01 u

pCilg 18-03104-10 TRG 8101110FIWC010CV 4.20E+OO u

TRG 8101110FIWC010CV 7.70E-01 2.68E-01 u

8101110FIWC010CV 03/14118 13:56 3122/2018 3/2212018 18-03104 Uranium-235 EPA 901.1 Modified

-1.19E+OO 3.55E+OO 3.55E+OO 1.94E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect FAX 865 !L.83-4621

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Work Order Details:

Eberline Analytical J Alex Bohacheff SDG.*

18-03104 Zion Solutions,_ LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis Category:_..

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 18-03104-11 TRG 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 Actinium-228 EPA901.1 Modified

-3.32E-01 1.52E+OO 1.52E+OO 2.25E+OO u

pCilg 18-03104-11 TRG 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/2312018 18-03104 Silver-108m EPA901.1 Modified 1.10E+OO 4.67E-01 4.70E-01 5.57E-01 u

pCi/g

~*A-*---------*

18-03104-11 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 Americium-241 EPA 901.1 Modified

-4.12E-01 2.84E-01 2.85E-01 6.89E-01 u

pCi/g 18-03104-11 8101110FIWC011CV 03/14/1813:29 3/22/2018 3/23/2018 18-03104 Barium-133 EPA901.1 Modified

-1.91E-01 6.10E+OO 6.10E+OO 7.68E-01 u

pCilg 18-03104-11 TRG 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 Bismuth-214 EPA 901.1 Modified 4.34E-01 7.99E-01 7.99E-01 1.11E+OO u

pCilg 18-03104-11 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 Cobalt-60 EPA 901.1 Modified 5.52E+OO 6.46E-01 7.06E-01 8.29E-01 u

pCi/g 18-03104-11 8101110FIWC011CV 03/14118 13:29 3122/2018 3/23/2018 18-03104 Cesium-134 EPA901.1 Modified

-1.36E-01 3.88E-01 3.88E-01 5.85E-01 u

pCi/g 18-03104-11 TRG 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 Cesium-137 EPA 901.1 Modified 6.47E+OO 9.54E-01 1.01E+OO 1.05E+OO pCi/g 18-03104-11 EPA 901.1 Modified 9.46E+01 7.35E+OO 8.81E+OO 2.97E+OO pCilg 18-03104-11 3/23/2018 18-03104 Europium-154 EPA901.1 Modified 4.28E+OO 8.78E-01 9.0SE-01 1.51E+OO u

pCi/g

-*--,,-m-"""-

18-03104-11 TRG 8101110FIWC011CV 03/14/1813:29 3/22/2018 3/23/2018 18-03104 9.29E-01 9.95E-01 u

pCi/g 18-03104-11 TRG 8101110FIWC011CV 03/14/1813:29 3/22/2018 3/23/2018 18-03104 Holmium-166m EPA901.1 Modified

-3.83E-01 7.13E-01 7.13E-01 5.27E-01 u

pCi/g 18-03104-11 TRG B101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 lodine-129 EPA 901.1 Modified 1.44E+01 6.99E+OO 7.02E+OO 6.25E+OO pCi/g 18-03104-11 TRG 8101110FIWC011CV EPA 901.1 Modified 1.01E+01 2.35E+OO 2.41E+OO 3.75E+OO pCi/g

~-- ___,,_

18-03104-11 TRG 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 Manganese-54 EPA 901.1 Modified

-1.07E-01 4.20E-01 4.20E-01 6.19E-01 u

pCilg

,, me*---*~""'""""'

18-03104-11 TRG 8101110FIWC011CV 03/14/1813:29 3/22/2018 3/23/2018 18-03104 Sodium-22 EPA 901.1 Modified 1.53E+OO 3.13E-01 3.23E-01 5.40E-01 u

pCilg 18-03104-11 TRG 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 Niobium-94 EPA901.1 Modified 2.54E+OO 6.74E-01 6.87E-01 5.46E-01 u

pCilg 18-03104-11 TRG 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 Lead-210 2.28E+02 2.59E+01 2.84E+01 1.86E+01 18-03104-11 TRG B101110FIWC011CV 03/14/1813:29 3/22/2018 3/2312018 18-03104 Lead-212 EPA 901.1 Modified

-6.43E-02 2.17E-01 2.17E-01 1.27E+OO u

pCi/g 18-03104-11 TRG 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 Lead-214 EPA 901.1 Modified 5.59E-01 8.71E+OO 8.71E+OO 2.36E+OO u

pCilg

~---*---------,--"'--------. ----

18-03104-11 TRG 8101110FIWC011CV 03114/18 13:29 3/22/2018 3/23/2018 18-03104 Promethium-145 EPA901.1 Modified 1.82E+02 3.09E+01 3.23E+01 4.00E+OO u

pCi/g 18-03104-11 TRG 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 Radium-226 EPA901.1 Modified 7.99E-01 7.99E-01 1.11E+OO u

18-03104-11 TRG 8101110FIWC011CV 03/14/1813:29 3/22/2018 3/23/2018 18-03104 1.16E+OO 1.69E+OO u

pCi/g 18-03104-11 TRG 8101110FIWC011CV 03/14/18 13:29 3/22/2018 3/23/2018 18-03104 2.59E+OO 6.32E+OO u

pCi/g 18-03104-11 TRG 8101110FIWC011CV 03/14/1813:29 3/22/2018 3/23/2018 18-03104 Thallium-208 1.26E+OO 1.26E+OO 18-03104-11 TRG 8101110FIWC011 CV 03/14118 13:29 3/22/2018 3/23/2018 1.83E+OO 5.77E+OO 5.77E+OO 3.08E+OO pCilg CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[219]

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Work Order Details:

Eberline Analytical J Alex Bohacheff SDG.*

18-03104 Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis. Category:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Actinium-228 EPA901.1 Modified 1.08E+OO 1.14E+OO 1.14E+OO 2.54E+OO 18-03104-12 TRG B 10111 OFIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Silver-108m EPA 901.1 Modified 3.97E+OO 7.62E-01 7.88E-01 5.40E-01 18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Americium-241 EPA 901.1 Modified

-6.04E-01 6.35E-01 6.36E-01 7.83E-01 18-03104-12 TRG 8101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Barium-133 EPA 901.1 Modified

-2.59E+OO 6.74E-01 6.87E-01 7.35E-01 18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Bismuth-214 EPA 901.1 Modified

-2.71E-01 3.76E-01 3.76E-01 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Cobalt-60 EPA 901.1 Modified 2.53E+01 1.55E+OO 2.02E+OO 7.63E-01 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Cesium-134 3.91E-01 3.91E-01 6.30E-01 u

pCiig 18-03104-12 B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Cesium-137 EPA 901.1 Modified 1.11E+OO 5.37E-01 5.40E-01 8.70E-01 pCi/g 18-03104-12 TRG 8101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Europium-152 EPA 901.1 Modified 4.49E+02 1.79E+01 2.92E+01 4.41E+OO pCi/g

---~-----------,, -

18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Europium-154 EPA901.1 Modified 2.02E+01 2.05E+OO 2.30E+OO 18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 EPA901.1 Modified 8.28E+OO 1.60E+OO 1.65E+OO 18-03104-12 TRG 8101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 EPA 901.1 Modified

-6.98E-02 3.57E-01 3.57E-01 18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 EPA 901.1 Modified 5.70E+OO 7.63E-01 8.17E-01 18-03104-12 TRG 8101110FIWC018CV EPA 901.1 Modified 6.10E+OO 3.33E+OO 3.34E+OO 6.63E+OO u

pCi/g

~ ------~-

18-03104-12 TRG B101110FIWC018CV EPA 901.1 Modified

-3.02E-01 5.03E-01 5.03E-01 7.10E-01 u

0 18-03104-12 TRG B101110FIWC018CV EPA 901.1 Modified 7.72E-01 8.54E-01 6.65E-01 18-03104-12 TRG B101110FIWC018CV EPA901.1 Modified

-1.27E+OO 8.03E-01 8.06E-01 18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Lead-210 EPA 901.1 Modified 7.61E+02 6.17E+01 7.30E+01 18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Lead-212 EPA 901.1 Modified 3.58E-01 3.52E-01 3.52E-01 18-03104-12 TRG 8101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Lead-214 EPA901.1 Modified 5.30E+OO 1.25E+OO 1.28E+OO 1.44E+OO

'----*----,w-~--'-'""~----*-**---'"'"'""'"'"'~*-- *-

'""'~----------------------------~------,---

18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Promethium-145 EPA 901.1 Modified 5.71E+01 5.49E+OO 6.22E+OO 3.38E+OO 18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Radium-226 EPA 901.1 Modified

-2.71E-01 3.76E-01 3.76E-01 1.03E+OO 18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 EPA 901.1 Modified

-2.35E-01 4.60E-01 4.60E-01 1.62E+OO 18-03104-12 TRG B 10111 OFIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 EPA 901.1 Modified

-1.19E+OO 6.12E+OO 6.12E+OO 7.66E+OO

~------...:-----*-

18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 EPA901.1 Modified 8.73E-02 7.62E-01 7.62E-01 5.93E-01 u

18-03104-12 TRG B101110FIWC018CV 03/14/18 09:48 3/22/2018 3/23/2018 18-03104 Uranium-235 EPA 901.1 Modified

-2.77E+OO 4.54E+OO 4.54E+OO 2.78E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect

(

EBERLINE

~

SERVICES 865/481-0683 FAX 865/483-4621

[220]

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Eberline Analytical J Alex Bohacheff SDG:

18-03104 ZionSolutions, LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analys_is Cate[lory*

ENVIRONMENTAL

-'-"-*~----,--,

Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units 18-03104-13 TRG 8101110FIWC019CV 03/14/18 10:30 3/22/2018 3/23/2018 18-03104 Actinium-228 EPA901.1 Modified 6.21E-01 6.10E+OO 6.10E+OO 8.74E+OO u

TRG 8101110FIWC019CV 03/14/18 10:30 3/22/2018 3/2312018 18-03104 Silver-108m EPA901.1 Modified 2.23E+01 3.09E+OO 3.30E+OO 1.45E+OO u

8101110FIWC019CV 03114/18 10:30 3122/2018 3123/2018 18-03104 Bismuth-214 EPA901.1 Modified 3.03E+OO 3.03E+OO 2.69E+OO u

18-03104-13 TRG 8101110FIWC019CV 03/14118 10:30 3/22/2018 3/23/2018 18-03104 Cobalt-60 EPA 901.1 Modified 1.97E+02 1.14E+01 1.52E+01 1.98E+OO

~---

18-03104-13 TRG 8101110FIWC019CV 03/14118 10:30 3/22/2018 3/23/2018 18-03104 Cesium-134 EPA901.1 Modified 8.33E-02 1.11E+OO 1.11E+OO 1.75E+OO u

18-03104-13 TRG 8101110FIWC019CV 03/14/18 10:30 3/22/2018 3/23/2018 18-03104 Cesium-137 EPA 901.1 Modified

-2.15E-01 1.54E+OO 1.54E+OO 2.48E+OO u

18-03104-13 TRG 810111 OFIWC019CV 03/14/18 10:30 3/22/2018 3/23/2018 7.70E+OO 18-03104-13 TRG 8101110FIWC019CV 03/14/18 10:30 3/22/2018 3/23/2018 18-03104 Europium-154 EPA 901.1 Modified 8.74E+01 9.83E+OO 1.08E+01 3.90E+OO

'" "" "'"" ______, __ "'"~

18-03104-13 TRG 8101110FIWC019CV 03/14/18 10:30 3/22/2018 3/23/2018 18-03104 Europium-155 EPA901.1 Modified 4.48E+01 4.69E+OO 5.22E+OO 5.36E+OO 18-03104-13 TRG 8101110FIWC019CV 03/14118 10:30 3/22/2018 3/2312018 18-03104 Holmium-166m EPA 901.1 Modified

-1.51E+OO 1.18E+OO 1.18E+OO 1.44E+OO u

18-03104-13 TRG 810111 OFIWC019CV 03/14/18 10:30 3122/2018 3/23/2018 18-03104 lodine-129 EPA 901.1 Modified 4.89E+01 4.65E+OO 5.28E+OO 2.47E+OO u

18-03104-13 TRG 8101110FIWC019CV 03/14/18 10:30 3/2212018 3/23/2018 18-03104 Potassium-40 EPA 901.1 Modified

-2.22E+OO 1.59E+OO 1.60E+OO 1.07E+01 u

18-03104-13 TRG 8101110FIWC019CV 03/14/1810:30 3/22/2018 3/23/2018 18-03104 Manganese-54 EPA901.1 Modified

-1.70E+OO 1.74E+OO 1.74E+OO 2.44E+OO u

18-03104-13 TRG 8101110FIWC019CV 03/14/1810:30 3/22/2018 3/23/2018 18-03104 Sodium-22 EPA901.1 Modified 4.19E+OO 4.83E+OO 4.83E+OO 2.47E+OO 18-03104-13 TRG B101110FIWC019CV 03/14/18 10:30 3/22/2018 3123/2018 18-03104 Niobium-94 EPA901.1 Modified 2.51E+01 4.32E+OO 4.51E+OO 2.17E+OO u

18-03104-13 TRG B10111 OFIWC019CV 03/14/18 10:30 3/2212018 3/23/2018 18-03104 Lead-210 EPA 901.1 Modified 6.00E+03 4.85E+02 5.74E+02 6.77E+01 u

"= --

18-03104-13 TRG B101110F1WC019CV 03/14/18 10:30 3/2212018 3/23/2018 18-03104 Lead-212 EPA 901.1 Modified 1.30E+OO 1.93E+OO 1.94E+OO 2.44E+OO u

18-03104-13 TRG B101110FIWC019CV 03/14/18 10:30 3/2212018 3/23/2018 18-03104 2.09E+OO 2.09E+OO 3.15E+OO u

18-03104-13 TRG B101110FIWC019CV 03/14/18 10:30 3/2212018 3/23/2018 18-03104 Promethium-145 EPA 901.1 Modified

-5.35E+02 4.76E+01 5.49E+01 5.28E+OO u

18-03104-13 TRG B 10111 OFIWC019CV 03/14/18 10:30 3122/2018 3/23/2018 18-03104 Radium-226 EPA 901.1 Modified

-4.82E-01 3.03E+OO 3.03E+OO 2.69E+OO u

18-03104-13 TRG B101110F1WC019CV 03/14/18 10:30 3/22/2018 3/23/2018 18-03104 Antimony-125 EPA901.1 Modified

-6.26E-01 2.79E+OO 2.79E+OO 4.37E+OO u

,cc,~----------

18-03104-13 TRG 8101110FIWC019CV 03/14118 10:30 3/2212018 3/2312018 18-03104 Thorium-234 1.95E+01 1.96E+01 2.39E+01 u

18-03104-13 TRG B101110FIWC019CV 03/14/1810:30 3/22/2018 3/23/2018 18-03104 Thallium-208 EPA901.1 Modified 1.03E+OO 1.96E+OO 1.96E+OO 1.05E+OO u

18-03104-13 TRG B101110F1WC019CV 03/14/18 10:30 3/22/2018 3/23/2018 18-03104 Uranium-235 EPA 901.1 Modified

-3.62E-01 1.77E+01 1.77E+01 8.64E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[221]

ZIONSOLUTIONSLLC An EnergySoJu/ions Company Sample ID Sample Matrix Sample Type Log Vol

~

B10l l l0FIWC001CV NIA CONCRETE CONCRETE 57.94 s

B10l l l0FIWC003CV NIA CONCRETE CONCRETE 57.94

~

B 10111 OFIWC004CV NIA CONCRETE CONCRETE 57.94 B 101110FIFC005CV NIA CONCRETE CONCRETE 57.94 1

B 10111 OFIFC006CV NIA CONCRETE CONCRETE 57.94 q B10l l l0FIFC008CV NIA CONCRETE CONCRETE 57.94 B1011 l0FIWC010CV NIA CONCRETE CONCRETE 57.94 (1

B10l l l0FIWC011CV NIA CONCRETE CONCRETE 57.94

\\ l B10l l l0FIWC018CV NIA CONCRETE CONCRETE 57.94

}

Bl01 l 10FIWC019CV NIA CONCRETE CONCRETE 57.94 B 10111 OIFIFC003CV NIA CONCRETE CONCRETE 57.94 Bl0l l l0IFIWC014CV NIA CONCRETE CONCRETE 57.94 Bl0l l l0IFIWC015CV NIA CONCRETE CONCRETE 57.94 Bl01110IFIWC0l6CV NIA CONCRETE CONCRETE 57.94 REC'D MAR 2 2 20m -

Chain-of-Custody Form 1 8 - 03 1 0 4 Sample Container Sample Date Sample Time Analysis Type Preservative Unit Type Qty cm3 Puck I

0311512018 0835 5ROCIHTD1H3 NIA cm*'

Puck 1

0311412018 1413 5ROCIHTD1H3 NIA cm*'

Puck 1

03/1512018 0815 5ROCIHTD1H3 NIA Clll')

Puck 1

03/1512018 0930 5ROCIHTD1H3 NIA cm3 Puck 1

0311512018 0950 5ROCIHTD1H3 NIA cm3 Puck 1

0311412018 1440 5ROCIHTD1H3 NIA cm3 Puck I

0311412018 1356 5ROCIHTD1H3 NIA cm3 Puck 1

03/1412018 1329 5ROCIHTD1H3 NIA cm3 Puck I

0311412018 0948 5ROCIHTD1H3 NIA cm3 Puck 1

0311412018 1030 5ROCIHTD1H3 NIA cm3 Puck 1

03/1312018 0845 5ROCIHTD1H3 NIA cm*

Puck 1

03/1312018 1510 5ROCIHTD1H3 NIA cm3 Puck l

03/1312018 1325 5ROCIHTD1H3 NIA cm3 Puck 1

03/1312018 1430 5ROCIHTD1H3 NIA ZS-WM-131 Revision 0 Information Use Remarks 0.0-0S' 134.18g 0.0-0.5" 114.73g 0.0-0.5" 144.21g 0.0-0.5" 73.42g 0.0-0.5" 135.85g 0.0-0.5" 112.38g 0.0-0.5" 114.63g 0.0-0.5" 122.03g 0.0-0.5" 130.80g 0.0-0.5" 88.20g 0.0-0.5" 143.35g 0.0-0.5" 164.81g 0.0-0.5" 108.97g 0.0-0.5" 115.55g

[222]

ZIONSOLUTIONSrrc An EnergySoJutions Company Bl0l l l0IFIWC017CV NIA CONCRETE Bl01110IFIWC0l8CV NIA CONCRETE Bl0l l l0IFIWC019CV NIA CONCRETE Bl0l l l0IFIWC020CV NIA CONCRETE Bl01110IFIFC021CV NIA CONCRETE Laborato1y:

Eberline Labs Relinquished by:

ALEX BOHACHEFF Relinquished by:

~i'<h<Arrl FJ{hkr!rf Relinquished by:

CONCRETE 57.94 cm1 Puck CONCRETE 57.94 cm*'

Puck CONCRETE 57.94 cm1 Puck CONCRETE 57.94 cm1 Puck CONCRETE 57.94 cm3 Puck Date Submitted To Lab:

Date Time:

(1mn/ddlyyyy):

01/i.r/J.ot!}

//DO Date (mrn/dd/yyyy):

c;-z,fiJ/ 20!9i Date!

1 (1mn/ddlyyyy):

Time:

ZS-WM-*131 1 a - 03 1 04 REC'D MAR 2 2 2018 Revision 0 Information Use I

03/1312018 1007 5ROCIHTDIH3 NIA 0.0-0.5" 155.47g 1

03/1312018 1400 5ROCIHTDIH3 NIA 0.0-0.5" 91.78g 1

03/1312018 0945 5ROCIHTDIH3 NIA 0.0-0.5" 162.88g I

0311412018 0911 5ROCIHTDIH3 NIA 0.0-0.5" 88.81g l

03/1312018 0900 5ROCIHTDIH3 NIA 0.0-0.5" 162.07g Ship Container No.:

Cooler Temperature:

Airbill Number: f e.J ;; X NIA NIA Received by:

Date: (mrn/dd/yyyy):

Time:

!loo Received by:

Date: (1mniddlyyyy):

Time:

Relinquished by:

Date (mrn/dd/yyyy):

Time:

v~ecei~

,,?/

Date: (mmldd/yyyy):

Time:

Comments PO# 677118 14 day turnaround 5-ROC I HTD / H-3

[223]

SEf,VICE.

EBERLINE ANALYTICAL COfxPORt\\ TION 601 SCARBORO f~Of\\rl OAK RIDGE, TENNESSEE 37!330 PHONE (!365) 481**06flj FAX (865) /483-*l,621 EBS-OR-43602 April 4, 2018 Alex Bohacheff Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099 SAMPLE RECEIPT CASE NARRATIVE Work Order# 18-03105-0R This work order contains nine solid samples received 03/22/2018. Samples were analyzed for Strontium-90, Tritium, Nickel-63 and by Gamma Spectroscopy.

CLIENT ID Bl01110IFIFC003CV B 1 0111 0 IFIW CO l 4CV B10l l l0IFIWC015CV Bl0l l l0IFIWC016CV Bl0l I l0IFIWCOl7CV ANALYTICAL METHODS LAB ID 18-03105-04 18-03105-05 18-03105-06 18-03105-07 18-03105-08 CLIENT ID BI01 l l0IFIWC018CV Bl01 l 10IFIWC019CV BIO 1110IFIWC020CV Bl01110IFIFC021CV LAB ID 18-03105-09 18-03105-10 18-03 10 5-1 1 18-03105-12 Strontium-90 was analyzed using EIChroM Method SRWOl Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.

Gamma Spectroscopy was performed using EPA Method 901.1 Modified.

Laboratory qualifiers are as follows:

U - Result is less than the MDA.

ANALYTICAL RES UL TS Combined Standard Unce1tainty is reported at I-sigma value.

Minimum Detectable Activity (MDA) values for data represented in this repo11 are sample-specific.

MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.

Pagel of 3

[224]

ANALYTICAL RES UL TS CONTINUED STRONTIUM-90 Samples were prepared by aliquoting as appropriate and leaching in HN03. Samples were diluted appropriately. Strontium recovery carriers were added to each sample. Chemical separations were conducted using selective extractions. Strontium precipitate was mounted on tared filter media. Chemical recovery was determined by Strontium carrier mass determinations. Samples were counted by gas flow propmiional counting and corrected for Yttrium-90 ingrowth.

Samples demonstrated acceptable results for all Strontium-90 analyses. Chemical recovery was acceptable for all samples. The Strontium-90 method blank demonstrated an acceptable result. Results for the Strontium-90 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Strontium-90 laboratory control sample demonstrated an acceptable percent recovery.

TRITIUM A representative aliquot of each sample was equilibrated with Tritium free water. Equilibrates were transferred into round-bottomed distillation flasks and attached to single stage stills. A portion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were then counted by beta liquid scintillation.

Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.

NICKEL-63 A representative aliquot of each sample was leached in HN03. Leachates were placed in an appropriately sized beaker. Stable elemental Nickel carrier was added to each sample prior to digestion. Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.

Samples demonstrated acceptable results for all Nickel-63 analyses. Results for laboratory fractions -03 and -04 (Client ID: B 10111 OIFIFC003CV DUP & DO) demonstrated slightly high method detection limits. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.

GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass/aliquot of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.

Page 2 of 3

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ANALYTICAL RESULTS CONTINUED GAMMA SPECTROSCOPY CONTINUED Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. Some results demonstrated slightly high method detection limits. Some samples demonstrated results that are greater than the method detection limit. These results are reported from the Canberra Gamma Apex "Nuclide MDA Repo1i" and are not positive. These results are qualified as non-detect (U). The method blank demonstrated acceptable results for all radionuclides as repo1ied. Results for the Cesium-13 7 replicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Cobalt-60 and Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.

CERTIFICATION OF ACCURACY I ce1iify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her designee to be accurate ~erified by the following signature.

~.-~~.

I~

M.R. McDougall Laboratory Manager \\

Date: 4/4/2018 Lberlinc Analytical wants and encourages your feedback regarding our perf'ormance providing radioanalytical services. Please visit http://cbcrlineanalytical.com/ to provide us with feedback on our services.

Page 3 of 3

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Printed: 4/412018 1 :08 PM Eberline Analytical Final Report of Analysis Lab Sample Client ID Type ID 18-03105-01 LCS KNOWN 18-03105-01 LCS SPIKE 18-03105-05 TRG 18-031 05-08 TRG B1011101FIWC017CV 18-03105-09 TRG B1011101FIWC018CV 18-03105-10 B101110IFIWC019CV 18-03105-11 B1011101FIWC020CV 18-03105-12 TRG 8101110IFIFC021CV 18-03105-01 LCS KNOWN 18-031 05-02 MBL BLANK 18-03105-03 DUP B1011101FIFC003CV 18-03105-04 DO B1011101FIFC003CV 18-03105-05 TRG B101110IFIWC014CV 18-031 05-06 TRG B1011101FIWC015CV 18-031 05-07 TRG B 10111 OIFIWC016CV 18-031 05-08 TRG B101110IFIWC017CV 18-03105-09 TRG B1011101FIWC018CV B101110IFIWC019CV 18-03105-11 B 10111 OIFIWC020CV 18-03105-12 B1011101FIFC021CV Report To:

J Alex Bohacheff Zfon Solution_si_l:!::~

101 Shiloh Blvd Zion, IL 60099 Sample Date Receipt Date Analysis Date Batch ID 03122118 00:00 03122118 00:00 3122/2018 3/28/2018 18-03105 3/22/2018 3128/2018 18-03105 03/13/18 15:10 3/22/2018 3/28/2018 18-03105 03113118 10:07 312212018 3129/2018 03113/18 14:00 3/22/2018 3/29/2018 03/13118 09:45 3/22/2018 3129/2018 18-03105 03/14118 09:11 3122/2018 3129/2018 18-03105 03113118 09:00 3122/2018 3/2912018 18-03105 03/22118 00:00 03122/18 00:00 3122/2018 3/2812018 18-03105 03122118 00:00 3/2212018 3/2812018 18-03105 03/13118 08:45 3122/2018 3/2812018 18-03105 03113118 08:45 3122/2018 03113118 10:07 3/2212018 3/28/2018 18-03105 03113118 09:45 3122/2018 3/2912018 18-03105 03114/18 09:11 3122/2018 3129/2018 18-03105 03113/18 09:00 3122/2018 3/2912018 18-03105 Analyte Tritium Tritium Tritium Tritium Tritium Tritium Tritium Nickel-63 Nickel-63 Nickel-63 Nickel-63 Nickel-63 Nickel-63 Nickel-63 SDG:

Purchase Order:

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Analysis_ Category:

Sample Matrix:

Method LANL ER-210 Modified LANL ER-210 Modified LANL ER-210 Modified LANL ER-210 Modified LANL ER-210 Modified LANL ER-210 Modified LANL ER-210 Modified ASTM 3500-Ni Modified ASTM 3500-Ni Modified ASTM 3500-Ni Modified ASTM 3500-Ni Modified ASTM 3500-Ni Modified ASTM 3500-Ni Modified ASTM 3500-Ni Modified ASTM 3500-Ni Modified ASTM 3500-Ni Modified ASTM 3500-Ni Modified ASTM 3500-Ni Modified Work Order Details:

18-03105 677118 ENVIRONMENT AL so Result 2.26E+02 1.96E+02 5.95E+02 7.95E+01 1.55E+02 1.53E+02 1.53E+03 1.52E+03

-8.83E-02 7.62E-01

-8.97E-02 5.22E-01 6.83E-01 4.75E+01 2.84E+01 4.79E-01 cu 8.15E+OO 5.34E+OO 1.48E+01 8.50E+OO 9.61E+OO 1.25E+01 4.58E+01 9.25E+OO 1.31E+OO 1.43E+OO 1.33E+OO 7.15E-01 8.60E-01 1.40E+OO 1.36E+OO 8.00E-01 CSU 3.64E+01 9.60E+OO 1.30E+01 1.51E+01 8.96E+01 1.31E+OO 1.43E+OO 1.33E+OO 7.16E-01 1.14E+OO 1.13E+OO 7.73E-01 8.61E-01 3.13E+OO 2.15E+OO 8.01E-01 MDA 9.73E+OO 2.20E+OO 2.24E+OO 2.42E+OO 2.28E+OO 1.20E+OO 1.86E+OO 1.92E+OO 1.23E+OO 1.45E+OO 1.22E+OO 1.51E+OO 1.35E+OO CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original EBERLINE

ER'\\/ CES 865/ 481-0683 FAX 865/483-4621 Page 1 of 13 Qualifier u

u u

Report Units pCilg

,m_*_,_, __

pCi/g

[227]

Printed: 4/4/2018 1 :08 PM Page 2 of 13 Report To Work Order Details:

Eberline Analytical J Alex Bohacheff SDG.*

18-03105 ZionSolutions, LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis Category:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID ID Date Date Date ID Units 03/22/18 00:00 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified 5.05E+01 2.83E-01 18-03105-01 LCS 03/22/18 00:00 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified 4.84E+01 1.37E+OO 6.72E+OO 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified

-1.83E-02 3.83E-01 3.83E-01 18-03105-03 DUP 81011101FIFC003CV 03/13/18 08:45 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified 4.14E-01 3.76E-01 3.80E-01 18-031 05-04 DO 9.64E-01 3.83E-01 4.05E-01 B101110IFIWC014CV 03/13/18 15:10 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified 1.86E-01 2.34E-01 2.36E-01 B101110IF1WC015CV 03/13/18 13:25 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified 5.47E-01 3.57E-01 3.65E-01 18-031 05-07 TRG B101110IFIWC016CV 03/13/18 14:30 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified 9.83E-02 3.43E-01 3.43E-01 7.22E-01 u

pCi/g 18-031 05-08 TRG B101110IFIWC017CV 03/13/18 10:07 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified 2.21E-01 2.22E-01 2.24E-01 18-03105-09 TRG B1011101FIWC018CV 03/13/18 14:00 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified 1.37E-01 2.69E-01 2.70E-01 18-03105-10 TRG B101110IFIWC019CV 03/13/18 09:45 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified 2.82E-01 2.03E-01 2.06E-01 18-03105-11 TRG B 10111 OIFIWC020CV 03/14/18 09:11 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified 7 04E-01 2.76E-01 2.92E-01 18-03105-12 TRG 81011101FIFC021 CV 03/13/18 09:00 3/22/2018 3/30/2018 18-03105 Strontium-90 EIChroM SRW01 Modified 2.99E-02 2.26E-01 2.26E-01 4.80E-01 u

pCi/g 18-03105-01 LCS KNOWN 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Cobalt-60 EPA901.1 Modified 2.71E+02 1.06E+01 18-03105-01 LCS KNOWN 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Cesium-137 18-03105-01 LCS SPIKE 03/22/18 00:00 3/22/2018 Cobalt-60 2.08E+01 18-03105-01 LCS SPIKE 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Cesium-137 EPA 901.1 Modified 1.76E+02 1.49E+01 1.75E+01 2.90E+OO pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Nonmal Sample; DO=Duplicate Original 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[228]

Printed: 41412018 1 :08 PM Page 3 of 13 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03105

...... ZionSolutio11s.,. LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis CEJte_9:ory:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Actinium-228 EPA901.1 Modified

-7 07E-02 9.49E-02 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018

-1.36E-02 3.14E-02 18-03105-02 BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Americium-241 EPA 901.1 Modified

-5.73E-02 3.44E-02 18-03105-02 BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Barium-133 EPA 901.1 Modified 1.06E-02 18-03105-02 MBL BLANK 18-031 05-02 MBL BLANK

---¥------------"~ "'18-031 05-02 MBL BLANK 03/22/18 00:00 3/22/2018 18-03105 Cesium-134 18-03105-02 MBL BLANK 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Europium-152 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Europium-154 s,avv--w--vvvv~- -~=-, _,w 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Europium-155 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Holmium-166m 18-031 05-02 BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 lodine-129 18-03105-02 BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Potassium-40 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Manganese-54 EPA 901.1 Modified

-1.36E-02 2.64E-02 3.96E-02 u

~---

18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Niobium-94 EPA901.1 Modified 9.62E-03 2.43E-02 4.25E-02 u

18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Lead-210 EPA 901.1 Modified 1.68E-01 2.36E-01 3.67E-01 u

18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Lead-212 EPA901.1 Modified 3.81E-02 3.19E-02 5.17E-02 u

*.--m=="-" *----------------------- ----------*-----------

18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Lead-214 EPA 901.1 Modified 1.83E-02 5.09E-02 8.02E-02 u

18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Promethium-145 EPA 901.1 Modified 4.48E-03 2.42E-02 u

18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 7.72E-02 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 7.62E-02 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Thorium-234 EPA901.1 Modified 6.47E-01 2.74E-01 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Thallium-208 EPA 901.1 Modified 2.86E-02 9.97E-02 18-03105-02 MBL BLANK 03/22/18 00:00 3/22/2018 3/23/2018 18-03105 Uranium-235 EPA 901.1 Modified 6.45E-02 2.71E-01 CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original EBERLINE SER CES 865/ 481-0683 FAX 865/483-4621

[229]

Printed: 4/4/2018 1 :08 PM Page 4 of 13 Eberline Analytical Final Report of Analysis Report To:

J Alex Bohacheff Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099 Lab Sample Client Sample Date Receipt Analysis Batch ID Type ID Date Date ID 18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 18-03105-03 DUP B1011101FIFC003CV 03/13/18 08:45 18-03105-03 DUP 81011101FIFC003CV 18-03105-03 DUP B1011101FIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 03/13/18 08:45 3/22/2018 3/23/2018 03/13/18 08:45 3/22/2018 3/23/2018 18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 18-03105 18-03105 18-03105 Analyte Actinium-228 Bismuth-214 Cobalt-60 Cesium-134 Cesium-137 Work Order Details:

SDG:

18-03105 Purchase Order:

677118 Analysis Catego,y: _____ ENVIRONMENTAL Sample Matrix:

SO Method Result cu EPA 901. 1 Modified

-6.91 E-01 1.43E+OO 8.61 E-01 4.26E-01

-7.28E+OO 6.86E-01 4.28E-02 1.48E+01 EPA901.1 Modified 6.81E-01 7.79E-01 EPA 901.1 Modified 5.33E+OO 4.57E-01 EPA 901.1 Modified 8.47E-03 2.05E-01 EPA 901.1 Modified 3.47E-01 4.08E-01 EPA901.1 Modified 9.89E+01 6.63E+OO CSU 1.43E+OO 4.29E-01 7.81E-01 1.48E+01 7.80E-01 5.33E-01 2.05E-01 4.09E-01 8.35E+OO MDA Qualifier 2.08E+OO U

4.90E-01 u

6.53E-01 u

7.00E-01 u

7.56E-01 u

Report Units 4.43E-01 5.55E-01 u

6.82E-01 u

2.89E+OO pCiig u

u pCiig u

18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 lodine-129 EPA 901.1 Modified

-1.34E+OO 7.56E-01 7.60E-01 5.47E+OO u

18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Potassium-40 EPA 901.1 Modified 7.98E+OO 1.99E+OO 2 04E+OO 4.62E+OO 18-03105-03 DUP B101110IFIFC003CV 3/23/2018 18-03105 Manganese-54 EPA901.1 Modified

-4.14E-01 4.11E-01 4.11E-01 5.86E-01 U

,, --+---*-*---------------------------*-----*-,,,,,,,, **--------

18-03105-03 DUP B1011101FIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Niobium-94 EPA 901.1 Modified

3. 14E+OO 7.43E-01 7.60E-01 5.22E-01 U

18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Lead-210 EPA 901.1 Modified

-2,04E+01 2.89E+OO 3.07E+OO 1.97E+01 U

.,,.,,,,,,, ____________ +**--------*-*

DUP B1011101FIFC003CV 03/13/18 08:45 3/22/2018 18-03105 Lead-212 EPA 901.1 Modified

-2.02E-01 2.98E-01 2.98E-01 1.20E+OO U

****---------------------*--***---*---*-*,, --*,..***.,j.*, **,,,.,,,,,,,.*... *---****---------------*------------------------*** -**---~----------****--*,,,,,,.,,

-----------*---------****------------*------*--*-1 18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 5.42E+01 1.32E+01 1.35E+01 2.18E+OO U

pCi/g 18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 1.79E+02 3.02E+01 3.16E+01 3.69E+OO U

18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Radium-226 EPA 901.1 Modified 6.81E-01 7.79E-01 7.80E-01 7.56E-01 U

18-03105-03 DUP 81011101FIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 3.71E-01 1.03E+OO 1.03E+OO 1.51E+OO U

18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Thorium-234 EPA 901.1 Modified

-9.39E+01 8.64E+OO 9.89E+OO 6.05E+OO U

.......,,...,,........,,,,,,,...........,... --~---------- ----

-----*----- ___,,..,.....,..,,...,........ c.,,.

18-03105-03 DUP B1011101FIFC003CV 03/13/1808:45 3/22/2018 3/23/2018 18-03105 Thallium-208 EPA901.1 Modified 7.97E-01 1.18E+OO 1.18E+OO 4.33E-01 U

18-03105-03 DUP B101110IFIFC003CV 03/13/18 08:45 3/22/2018 18-03105 Uranium-235 EPA 901.1 Modified

-6.01E+OO 5.55E+OO 5.56E+OO 2.92E+OO U

CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Nonnal Sample; DO=Duplicate Original

( EBERLINE SERV!CES E

601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[230]

Printed: 4/4/2018 1 :08 PM Page 5 of 13 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SOG:

18-03105 Zion S0lutior1~1. LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis Cat~fICJ.'Y:.

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 18-03105-04 DO 8101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Actinium-228 EPA901.1 Modified 2.32E-02 1.22E+OO 1.22E+OO 2.06E+OO u

pCi/g 18-03105-04 DO 810111 OIFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Silver-108m EPA901.1 Modified 8.45E-01 4.28E-01 4.30E-01 4.88E-01 pCi/g 18-031 05-04 DO 81011101FIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Americium-241 EPA901.1 Modified

-5.95E+OO 5.84E-01 6.59E-01 6.54E-01 pCi/g 18-031 05-04 DO 8101110IFIFC003CV 7.01E-01 u

pCi/g 18-03105-04 DO 8101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 8ismuth-214 EPA 901.1 Modified 7.19E-01 4.07E-01 4.09E-01 8.89E-01 u

pCi/g 18-03105-04 DO 81011101FIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Cobalt-60 EPA901.1 Modified 5.50E+OO 4.58E-01 5.38E-01 4.29E-01 pCi/g 18-03105-04 DO 8101110IFIFC003CV 03/13/18 08:45 3/22/2018

-3.58E-01 2.52E-01 2.53E-01 5.53E-01 u

pCi/g

*-""'~,,_, ___

18-031 05-04 DO 8101110IFIFC003CV 03/13/18 08:45 4.64E-01 6.72E-01 u

pCi/g 18-03105-04 DO 81011101FIFC003CV 03/13/18 08:45 9.30E+OO 2.89E+OO pCi/g

'"~

18-03105-04 DO 81011101FIFC003CV 03/13/18 08:45 7.97E-01 1.32E+OO u

pCi/g 18-03105-04 DO 8101110IFIFC003CV 03/13/18 08:45 7.13E-01 1.50E+OO pCi/g 18-031 05-04 DO 6.50E-01 5.00E-01 u

pCi/g 18-031 05-04 DO 810111 OIFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 lodine-129 EPA 901.1 Modified 1.39E+01 6.77E+OO 6.81E+OO 5.44E+OO pCi/g M

Sc, COS o'Y--~-~

18-031 05-04 DO 81011101FIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Potassium-40 EPA901.1 Modified 6.59E+OO 1.77E+OO 1.80E+OO 4.05E+OO pCi/g 18-03105-04 DO 81011101FIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Manganese-54 EPA901.1 Modified 3.72E-01 3.99E-01 4.00E-01 6.00E-01 18-03105-04 DO 81011101FIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Niobium-94 EPA 901.1 Modified 2.95E+OO 7.17E-01 7.33E-01 5.32E-01 18-03105-04 DO 81011101FIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Lead-210 EPA 901.1 Modified

-1.99E+01 2.87E+OO 3.05E+OO 1.97E+01 u

pCi/g 18-031 05-04 DO 8101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Lead-212 EPA901.1 Modified

-1.59E-01 2.07E-01 2.07E-01 1.22E+OO u

pCi/g 18-03105-04 DO 810111 OIFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Lead-214 EPA 901.1 Modified 5.21E+01 1.27E+01 1.30E+01 2.19E+OO u

18-03105-04 DO 1.79E+02 3.02E+01 3.16E+01 3.69E+OO u

18-03105-04 DO 81011101FIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Radium-226 EPA901.1 Modified 7.19E-01 4.07E-01 4.09E-01 8.89E-01 u

pCi/g

,--~""

18-03105-04 DO 8101110IFIFC003CV 03/13/18 08:45

-3.44E-01 5.79E-01 5.79E-01 1.52E+OO u

18-03105-04 DO 8101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 6.13E+OO 6.03E+OO u

18-03105-04 DO B101110IFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 1.16E+OO 4.65E-01 u

pCi/g 18-03105-04 DO 810111 OIFIFC003CV 03/13/18 08:45 3/22/2018 3/23/2018 18-03105 Uranium-235 EPA901.1 Modified 4.51E+OO 5.47E+OO 5.48E+OO 2.95E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Nonmal Sample; DO=Duplicate Original

.::iER lCES 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[231]

Printed: 41412018 1 :08 PM Page 6 of 13 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03105 Zion Solutions, LLC ____

Purchase Order 677118 Final Report of Analysis 101 Shiloh Blvd Analysis Category:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units18-031 05-05 TRG 81011101FIWC014CV 03/13/18 15:10 3/22/2018 3/23/2018 18-03105 Actinium-228 EPA 901.1 Modified 1.27E+OO 2.16E+OO 2.16E+OO 3.27E+OO u

---""'""-~-A--c' <

18-03105-05 TRG 81011101FIWC014CV 03/13118 15:10 3/22/2018 3/23/2018 EPA 901.1 Modified 2.78E+OO

-*---~,-,

18-03105-05 TRG 81011101FIWC014CV 03/13/18 15:10 3/22/2018 3/23/2018 18-03105 Americium-241 EPA 901.1 Modified

-7.04E-01 4.88E-01 4 89E-01 6.82E-01 u

18-03105-05 TRG 81011101FIWC014CV 03113/18 15:10 3/22/2018 3/23/2018 18-03105 8arium-133 18-03105-05 TRG 8101110IFIWC014CV 03/13/1815:10 3/22/2018 3/23/2018 18-03105 8ismuth-214 18-03105-05 TRG 8101110IF!WC014CV 03/13/18 15:10 3/22/2018 3/23/2018 18-03105 Cobalt-60 EPA 901.1 Modified 18-03105-05 TRG 81011101FIWC014CV 03/13/1815:10 3/22/2018 3/23/2018 18-03105 Cesium-134 EPA901.1 Modified

-2.70E-01 18-03105-05 TRG 81011101FIWC014CV 03/13/18 15:10 3/22/2018 3/23/2018 18-03105 Cesium-137 EPA 901.1 Modified 3.73E-01 18-031 05-05 TRG 81011101FIWC014CV 03/13/18 15:10 3/22/2018 3/23/2018 18-03105 Europium-152 EPA 901.1 Modified 18-031 05-05 TRG 81011101FIWC014CV 03/13/1815:10 3/22/2018 3/23/2018 18-03105 1.12E+01

-A--*-*-----~

18-031 05-05 TRG 810111 OIFIWC014CV 03/13/1815:10 3/22/2018 3/23/2018 18-03105

--~--**----,-* c*~

18-03105-05 TRG B101110IFIWC014CV 03/13/18 15:10 3/22/2018 3/23/2018 18-03105

~-°'~.-----*

18-03105-05 TRG 81011101FIWC014CV 03/13/1815:10 3/22/2018 3/23/2018 18-03105 18-03105-05 TRG 81011101FIWC014CV 03/13/18 15:10 3/2212018 3/23/2018 18-03105 18-03105-05 TRG 81011101FIWC014CV 03/13/18 15:10 3/22/2018 3/23/2018 18-03105 Manganese-54 EPA 901.1 Modified 18-03105-05 TRG 81011101FIWC014CV 03/13/1815:10 3122/2018 3/23/2018 18-03105 Niobium-94 EPA901.1 Modified 18-03105-05 TRG 81011101FIWC014CV 03/13/18 15:10 3/2212018 3/2312018 18-03105 Lead-210 EPA901.1 Modified 5.11E+02 3.76E+01 4.59E+01 2.58E+01 18-03105-05 TRG 81011101FIWC014CV 03/13/18 15:10 3/22/2018 3/23/2018 18-03105 Lead-212 EPA 901.1 Modified 5.33E-02 4.57E-01 18-03105-05 TRG 8101110IFIWC014CV 03/13/18 15:10 3/22/2018 3/23/2018 18-03105 Lead-214 EPA901.1 Modified 2.80E-01 6.20E-01 18-03105-05 TRG 8101110IFIWC014CV 03/13/18 15:10 3/22/2018 3/23/2018 18-03105 Promethium-145 EPA901.1 Modified 3.86E+01 2.79E+OO 18-03105-05 TRG 3/23/2018 18-03105 Radium-226 EPA 901.1 Modified 4.92E-01 1.23E+OO 18-03105-05 TRG 8101110IFIWC014CV 03/13/1815:10 3/22/2018 3/2312018 18-03105 8.30E-01 1.41E+OO 18-031 05-05 TRG 18-03105 Thorium-234 EPA 901.1 Modified

-5.41E+OO 4.71E+OO 18-03105-05 TRG 81011101FIWC014CV 03113/18 15:10 312212018 3/23/2018 18-03105 Thallium-208 EPA 901.1 Modified 2.75E-01 1.21E+OO

--"'""'"-*--=---,,--------w*-*,-*--**,18-031 05-05 TRG 81011101FIWC014CV 03113/18 15:10 3/2212018 3/2312018 2.49E+OO 5.15E+OO 515E+OO 2.74E+OO u

pCilg CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original EBERLINE 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[232]

Printed: 4/4/2018 1 :08 PM Page 7 of 13 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03105 Zion_Solutions, LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis. Category:

ENVIRONMENTAL

-r-~-

Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 18-03105-06 TRG B1011101FIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 Actinium-228 EPA901.1 Modified

-5.26E-01 1.03E+OO 1 03E+OO 18-03105-06 B1011101FIWC015CV 03/13/1813:25 3/22/2018 3/23/2018 18-03105 Silver-108m EPA 901.1 Modified 8.61E-01 3.39E-01 3.42E-01 3.01E-01 u

pCi/g 18-031 05-06 B101110IFIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 Americium-241 EPA901.1 Modified

-5.91E-01 3.64E-01 3.66E-01 4.31E-01 u

18-031 05-06 TRG B101110IF1WC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105.18-031 05-06 TRG B1011101FIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 18-03105-06 TRG B101110IFIWC015CV 03/13/1813:25 3/22/2018 3/23/2018 18-03105 18-03105-06 B101110IFIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 18-03105-06 B101110IFIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 18-031 05-06 B1011101FIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 Europium-152 EPA901.1 Modified 1.08E+02 4.45E+OO 7.10E+OO 1.82E+OO pCi/g 18-031 05-06 B10111 OIFIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 Europium-154 EPA 901.1 Modified 1.29E+OO 18-031 05-06 TRG 81011101FIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 EPA 901.1 Modified pCi/g 18-031 05-06 B101110IFIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 18-031 05-06 81011101FIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 1.57E+OO 18-03105-06 TRG B101110IFIWC015CV 03/13/1813:25 3/22/2018 3/23/2018 18-03105 Potassium-40 EPA 901.1 Modified 18-03105-06 TRG B1011101FIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 Manganese-54 EPA 901.1 Modified 3.97E-01 u

pCi/g 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 Niobium-94 EPA901.1 Modified

-2.79E-01 4.19E-01 4.19E-01 3.65E-01 81011101FIWC015CV 03/13/1813:25 3/22/2018 3/23/2018 18-03105 Lead-210 EPA901.1 Modified 2.08E+02 1.79E+01 2.08E+01 1.17E+01 18-03105-06 TRG B 10111 OIFIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 Lead-212 EPA 901.1 Modified 7.02E-02 2.86E-01 2.86E-01 4.52E-01 18-031 05-06 TRG B101110IFIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 Lead-214 EPA 901.1 Modified 1.48E+OO 5.77E-01 5.82E-01 8.13E-01 u

pCi/g 3/22/2018 3/23/2018 18-03105 : Promethium-145 EPA 901.1 Modified 1.65E+01 2.02E+OO 2.19E+OO 2.00E+OO u

B101110IFIWC015CV 03/13/18 13 :25 3/22/2018 3/23/2018 18-03105 Radium-226 EPA 901.1 Modified 4.03E-01 5.19E-01 5.19E-01 7.71E-01 u

03/13/18 13:25 3/22/2018 3/23/2018 18-03105 Antimony-125 EPA 901.1 Modified

-2.58E-01 6.39E-01 6.39E-01 9.12E-01 u

18-03105-06 TRG B101110IFIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 Thorium-234 EPA 901.1 Modified 4.27E+OO 3.43E+OO 3.44E+OO 4.46E+OO u

18-03105-06 TRG B1011101FIWC015CV 03/13/1813:25 3/22/2018 3/23/2018 18-03105 Thallium-208 EPA 901.1 Modified 3.26E-02 8.39E-01 8.39E-01 6.82E-01 u

,,,_,,_.,,,,,,_,,m-.-*-,*-

18-031 05-06 TRG B101110IFIWC015CV 03/13/18 13:25 3/22/2018 3/23/2018 18-03105 Uranium-235 EPA901.1 Modified

-6.31E-01 2.46E+OO 2.46E+OO 1.50E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Nonmal Sample; DO=Duplicate Original 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[233]

Printed: 4/4/20181:08 PM Page 8 of 13 Report To*

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03105

.. _ ____ Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd

__ Analysis. Category.

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch cu Report Analyte Method Result CSU MDA Qualifier ID Type ID Date Date Date ID Units 18-03105-07 TRG B101110IFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Actinium-228 EPA 901.1 Modified 1.40E-01 1.23E+OO 1.23E+OO 1.80E+OO u

pCi/g

'""~----**

18-03105-07 TRG B101110IFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Silver-108m EPA 901.1 Modified 1.41E+OO 4.16E-01 4.22E-01 3.08E-01 u

pCi/g 18-03105-07 TRG B101110IFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Americium-241 EPA901.1 Modified 5.12E-03 4.44E-01 4.44E-01 5.61E-01 u

pCi/g

""-=----

Barium-133 EPA901.1 Modified

-2.72E-02 2.16E-01 2.16E-01 18-03105 Bismuth-214 EPA 901.1 Modified 1.09E+OO 4.55E-01 4.59E-01 1.05E+OO pCi/g 18-03105-07 TRG B101110IFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Cobalt-60 EPA901.1 Modified 8.76E+OO 6.12E-01 7.59E-01 18-03105-07 TRG B1011101FIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Cesium-134 EPA 901.1 Modified

-5.77E-02 2.39E-01 2.39E-01 u

pCi/g 18-03105-07 3/22/2018 3/23/2018 18-03105 Cesium-137 EPA901.1 Modified 2.94E-01 3.64E-01 3.64E-01 5.39E-01 u

pCi/g 18-031 05-07 TRG B101110IFIWC016CV 03/13/1814:30 3/22/2018 3/23/2018 18-03105 Europium-152 EPA 901.1 Modified 1.65E+02 6.39E+OO 1.06E+01 18-031 05-07 TRG 8101110IFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Europium-154 EPA 901.1 Modified 5.79E+OO 8.33E-01 8.84E-01 8.49E-01 pCi/g

~----*--*

18-03105-07 TRG B101110IFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Europium-155 EPA 901.1 Modified 2.98E+OO 7.81E-01 7.96E-01 1.17E+OO pCVg 18-03105-07 TRG 81011101FIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Holmium-166m EPA 901.1 Modified 7.62E-01 5.92E-01 5.93E-01 18-03105-07 810111 OIFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 lodine-129 EPA901.1 Modified 2.50E+OO 3.92E-01 4.13E-01 5.17E-01 u

18-03105-07 81011101FIWC016CV 03/13/1814:30 3/22/2018 3/23/2018 18-03105 Potassium-40 EPA901.1 Modified 7.74E+OO 1.95E+OO 18-03105-07 TRG 81011101FIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Manganese-54 EPA901.1 Modified

-8.63E-02 3.60E-01 18-03105-07 TRG 8101110IFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Niobium-94 5.42E-01 18-03105-07 TRG 81011101FIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Lead-210 EPA 901.1 Modified 3.28E+02 2.78E+01 18-031 05-07 TRG 810111 OIFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Lead-212 EPA901.1 Modified 1.09E+OO 4.89E-01

--~-=----*--**-*--- -------

18-031 05-07 TRG B101110IFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Lead-214 EPA901.1 Modified 1.10E+OO 5.18E-01 5.21E-01 9.24E-01 pCi/g 18-03105-07 TRG 8101110IFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Promethium-145 EPA 901.1 Modified

-2.57E+01 2.58E+OO 2.90E+OO 1.09E+OO u

18-03105-07 TRG 8101110IFIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Radium-226 EPA 901.1 Modified 1.09E+OO 4.55E-01 4.59E-01 1.05E+OO 1S-03105-07 TRG 81011101FIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Antimony-125 EPA 901.1 Modified 2.71E-01 5.96E-01 5.96E-01 9.58E-01 u

pCi/g 18-031 05-07 TRG 81011101FIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Thorium-234 EPA901.1 Modified

-1.41E+OO 4.26E+OO 4.26E+OO 5.34E+OO u

18-031 05-07 TRG 81011101FIWC016CV 03/13/18 14:30 3/22/2018 3/23/2018 18-03105 Thallium-208 EPA901.1 Modified

-4.59E-01 8.35E-01 8.35E-01 6.27E-01 u

18-03105-07 TRG 81011101FIWC016CV 03/13/1814:30 3/22/2018

3/23/2018 18-03105 Uranium-235 EPA 901.1 Modified

-3.41E+OO 3.93E+OO 3.93E+OO 1.89E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Nonmal Sample; DO=Duplicate Original

'.::,ER\\/lCES 601 SCARBORO ROAD OAK RIDGE, 865/481-0683 FAX 865/ 483-4621

[234]

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Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03105 ZionSolutions, LLC Purchase Order 677118 Final Report of Analysis 101 Shiloh Blvd Analysis C;,te~CJ'}': _ _

ENVIRONMENTAL

, ',_ __ ~" --"-""

Zion, IL 60099 Sample Matrix:

so Lab Client Sample Receipt Analysis Batch Report ID ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 18-03105-08 6.01E-01 1.32E+OO 1.32E+OO 18-03105-08 B1011101FIWC017CV 03/13/18 10:07 3/22/2018 3/23/2018 18-03105 Silver-108m EPA901.1 Modified 9.59E-01 4.31E-01 4.34E-01 18-031 05-08 81011101FIWC017CV 03/13/18 10:07 3/22/2018 3/23/2018 18-03105 Americium-241 EPA901.1 Modified

-5.19E-01 3.03E-01 3.05E-01 2.89E-01 3.83E-01 81011101FIWC017CV 03/13/18 10:07 18-03105-08 TRG B1011101FIWC017CV 03/13/18 10:07 18-03105-08 TRG B101110IFIWC017CV 03/13/18 10:07 Cesium-134 EPA 901.1 Modified 18-031 05-08 TRG 03/13/18 10:07 18-03105 Cesium-137 EPA 901.1 Modified 18-03105-08 18-03105-08 TRG B1011101FIWC017CV 18-03105 Europium-154 EPA901.1 Modified 18-03105-08 EPA901.1 Modified 18-03105-08 18-03105-08 TRG 81011101FIWC017CV 18-03105-08 TRG B1011101FIWC017CV Manganese-54

-1.99E-01 18-03105-08 B101110IF1WC017CV 03/13/18 10:07 3/22/2018 3/23/2018 18-03105 Niobium-94 EPA 901.1 Modified 2.64E-01 18-03105-08 TRG B101110IFIWC017CV 03/13/1810:07 3/22/2018 3/23/2018 18-03105 Lead-210 EPA 901.1 Modified 2.01E+02 18-03105-08 TRG B1011101FIWC017CV 03/13/18 10:07 3/22/2018 3/23/2018 18-03105 Lead-212 EPA 901.1 Modified 2.28E-02 18-03105-08 TRG 81011101FIWC017CV 03/13/18 10:07 3/22/2018 3/23/2018 18-03105 Lead-214 EPA 901.1 Modified 5.45E-01 18-03105-08 TRG B1011101FIWC017CV 03/13/18 10:07 3/22/2018 3/23/2018 18-03105 Promethium-145 EPA 901.1 Modified 1.35E+01 18-031 05-08 TRG B101110IFIWC017CV 03/13/18 10:07 3/22/2018 3/23/2018 18-03105 Radium-226 18-03105-08 TRG B101110IFIWC017CV 03/13/18 10:07 3/22/2018 EPA 901.1 Modified 18-03105-08 TRG 81011101FIWC017CV 03/13/1810:07 18-03105-08 81011101FIWC017CV 03/13/18 10:07 03/13/18 10:07 3/22/2018 3/23/2018 18-03105 Uranium-235 EPA 901.1 Modified

-3.08E-01 3.17E+OO 3.17E+OO 1.66E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original EBERLINE SER\\/iCES FAX 865/483-4621

[235]

Printed: 41412018 1 :08 PM Report To*

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03105 Zion Solutions, LLC Purchase Order:

677118 Final Report of Analysis

""l-c---'-""'

101 Shiloh Blvd Analysis Category:

ENVIRONMENTAL

<*,~--,mn*,*--,

Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA 18-031 05-09 TRG 8101110IFIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Actinium-228 1.48E+OO 2.16E+OO 18-031 05-09 TRG 81011101FIWC018CV 03/13/1814:00 3/22/2018 3/23/2018 18-03105 Silver-108m EPA 901.1 Modified 8.19E-01 5.03E-01 5.05E-01 4.56E-01 18-03105-09 TRG 81011101FIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Americium-241 EPA 901.1 Modified

-1.19E+OO 5.54E-01 5.57E-01 6.50E-01 18-03105-09 TRG B101110IFIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Barium-133 EPA 901.1 Modified 1.16E-01 2.78E-01 2.78E-01 6.21E-01 18-03105-09 TRG 81011101FIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Bismuth-214 EPA 901.1 Modified 8.71E-01 7.70E-01 7.71E-01 1.06E+OO 18-03105-09 TRG 81011101FIWC018CV 03/13/1814:00 3/22/2018 3/23/2018 18-03105 Cobalt-60 EPA901.1 Modified 1.13E+01 7.89E-01 9.78E-01 5.64E-01 18-031 05-09 TRG 81011101FIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Cesium-134 EPA 901.1 Modified 2.38E-01 2.38E-01 5.29E-01 18-03105-09 TRG 81011101FIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Cesium-137 6.58E-01 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Europium-152 EPA 901.1 Modified 2.29E+02 9.28E+OO 1.50E+01 2.58E+OO TRG 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Europium-154 EPA 901.1 Modified 7.73E+OO 1.15E+OO 18-03105-09 TRG 81011101FIWC018CV 03/13/1814:00 3/22/2018 3/23/2018 18-03105 7.12E-01 1.09E+OO 18-031 05-09 TRG B101110IFIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Holmium-166m EPA901.1 Modified

-2.64E-02 3.03E-01 3.03E-01 3.94E-01 18-031 05-09 TRG B101110IFIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 lodine-129 EPA 901.1 Modified 3.10E+OO 5.88E-01 6.09E-01 2.39E+OO 18-031 05-09 TRG 81011101FIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Potassium-40 EPA901.1 Modified 8.82E+OO 2.37E+OO 2.42E+OO 3.93E+OO 18-031 05-09 TRG B101110IFIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Manganese-54 EPA 901.1 Modified 4.58E-01 4.26E-01 4.27E-01 6.26E-01

,--------, -~~-c',vmm,,,, __,_"_'-'"',,

18-03105-09 TRG 8101110IFIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Niobium-94 EPA 901.1 Modified

-6.82E-01 6.56E-01 6.57E-01 5.47E-01 18-03105-09 3/23/2018 18-03105 Lead-210 3.66E+01 4.31 E+01 1.81E+01 18-03105-09 TRG 81011101FIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Lead-212 EPA901.1 Modified 1.55E-01 2.95E-01 2.95E-01 6.76E-01 18-03105-09 TRG B101110IFIWC018CV 03/13/1814:00 3/22/2018 3/23/2018 18-03105 Lead-214 EPA901.1 Modified 3.19E+OO 9.41E-01 9.55E-01 1.24E+OO 18-031 05-09 TRG 81011101FIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Promethium-145 EPA 901.1 Modified 3.50E+01 3.75E+OO 4.16E+OO 3.11E+OO

"""" ---"'-~--------------------------

18-031 05-09 TRG 81011101FIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Radium-226 EPA901.1 Modified 8.71E-01 7.70E-01 7.71E-01 1.06E+OO 18-03105-09 TRG B1011101F1WC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Antimony-125 EPA901.1 Modified

-4.81E-01 9.64E-01 9.64E-01 1.37E+OO 18-03105-09 TRG 810111 OIFIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Thorium-234 EPA 901.1 Modified 4.29E+OO 5.13E+OO 5.14E+OO 6.52E+OO 18-03105-09 TRG 81011101FIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Thallium-208 EPA901.1 Modified 8.72E-02 6.67E-01 6.67E-01 7.56E-01 18-03105-09 TRG B101110IFIWC018CV 03/13/18 14:00 3/22/2018 3/23/2018 18-03105 Uranium-235 EPA 901.1 Modified 1.34E-01 3.78E+OO 3.78E+OO 2.35E+OO CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original EBERLINE SER iCES r C 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/ 481-0683 FAX 865/483-4621 Page 10 of 13 Report Qualifier Units u

u u

pCi/g pCi/g u

pCi/g u

u u

u pCi/g

[236]

Printed: 4/4/2018 1 :08 PM Page 11 of 13 Report To:

Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03105 Zion Solutions, LLC ___

Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis Cate_qory:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Method Result cu CSU MDA Qualifier Report ID Type ID Date Date Date ID Units 18-03105-10 TRG 81011101FIWC019CV 03/13/18 09:45 3/22/2018 3/23/2018 18-03105 Actinium-228 EPA 901.1 Modified 7.95E-01 8.70E-01 8.71E-01 1.29E+OO u

pCi/g m-,,-***~H SSA"¥-e<-S 18-03105-10 TRG 81011101FIWC019CV 8.25E-01 2.90E-01 2.93E-01 2.66E-01 18-03105-10 TRG 81011101FIWC019CV 03/13/18 09:45 3/23/2018 18-03105 Americium-241 EPA901.1 Modified

-1.59E-01 3.28E-01 3.28E-01 4.10E-01 u

pCi/g 18-03105-10 TRG 81011101FIWC019CV 03/13/18 09:45 3/22/2018 3/23/2018 18-03105 Barium-133 EPA901.1 Modified

-2.07E-02 2.25E-01 2.25E-01 3.39E-01 u

18-03105-10 TRG B 10111 OIFIWC019CV 03/13/18 09:45 3/22/2018 3/23/2018 18-03105 Bismuth-214 EPA 901.1 Modified 8.37E-01 3.04E-01 3.07E-01 4.62E-01 18-03105-10 TRG 8101110IFIWC019CV 03/13/18 09:45 3/22/2018 3/23/2018 18-03105 Cobalt-60 EPA 901.1 Modified 7.94E+OO 5.25E-01 6.65E-01 2.66E-01 18-03105-10 TRG 8101110IFIWC019CV 03/13/18 09:45 3/22/2018 3/23/2018 18-03105 Cesium-134 EPA 901.1 Modified 7.59E-02 1.39E-01 1.39E-01 2.64E-01 u

18-03105-10 03/13/18 09:45 3/22/2018 3/23/2018 18-03105 Cesium-137 EPA901.1 Modified 3.03E+01 2.98E+OO 3.36E+OO 5.71E-01 18-031 05-10 1.22E+OO 18-03105-10 TRG 81011101FIWC019CV 6.18E-01 pCi/g 18-03105-10 TRG 81011101FIWC019CV 4.35E-01 8.31E-01 18-03105-10 TRG 81011101FIWC019CV 4.05E-01 4.05E-01 2.40E-01 18-03105-10 TRG 8101110IFIWC019CV 2.89E-01 2.90E-01 3.54E-01 18-03105-10 TRG 8101110IFIWC019CV 1.35E+OO 1.37E+OO 2.44E+OO 18-03105-10 TRG 81011101FIWC019CV 2.43E-01 2.43E-01 3.47E-01 18-03105-10 TRG 81011101FIWC019CV 3.69E-01 3.73E-01 3.12E-01 18-03105-10 TRG 81011101FIWC019CV 18-03105 Lead-210 EPA 901.1 Modified 1.72E+02 1.51E+01 1.75E+01 8.21E+OO 18-03105-10 TRG 81011101FIWC019CV 18-03105 Lead-212 EPA901.1 Modified 5.60E-01 2.61E-01 2.63E-01 1.02E+OO 18-03105-10 TRG 8101110IFIWC019CV 03/13/18 09:45 3/22/2018 3/23/2018 18-03105 Lead-214 EPA 901.1 Modified 8.03E-01 3.80E-01 3.82E-01 6.73E-01 18-03105-10 TRG 81011101FIWC019CV 03113/18 09:45 3/22/2018 3/23/2018 18-03105 Promethium-145 EPA 901.1 Modified

-1.34E+01 1.41E+OO 1.57E+OO 7.18E-01 18-03105-10 TRG 81011101FIWC019CV 03113/18 09:45 3/22/2018 3/2312018 18-03105 Radium-226 EPA 901.1 Modified 8.37E-01 3.04E-01 3.07E-01 4.62E-01 18--03105-10 TRG 81011101FIWC019CV 03113/18 09:45 3122/2018 3/2312018 18-03105 2.69E-01 5.05E-01 5.05E-01 8.11E-01 18-03105-10 TRG 81011101FIWC019CV 03/13/18 09:45 3/22/2018 3/23/2018 18-03105 Thorium-234 3.18E+OO 3.18E+OO 3.99E+OO 18-03105-10 TRG 81011101FIWC019CV 03113/18 09:45 3122/2018 3/2312018 18-03105 Thallium-208 EPA 901.1 Modified

-4.89E-01 5.93E-01 5.93E-01 6.08E-01 18--03105-10 TRG 8101110IFIWC019CV 03/13118 09:45 3122/2018 3/2312018 18-03105 Uranium-235 EPA 901.1 Modified 2.43E-01 2.90E+OO 2.90E+OO 1.41E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[237]

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Work Order Details:

Eberline Analytical J Alex Bohacheff SDG:

18-03105 Zion_Solutions,_ LLC_

Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd Analysis Category:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Analyte Qualifier Report ID Type ID Date Date Date ID Method Result cu CSU MDA Units 18-03105-11 TRG B 10111 OIFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Actinium-228 EPA901.1 Modified 3.51E-02 1.31E+OO 1.31E+OO 1.90E+OO u

pCi/g 18-03105-11 B101110IFIWC020CV 03/14/18 09: 11 3/22/2018 3/26/2018 18-03105 Silver-108m EPA901.1 Modified 6.35E-01 4.05E-01 4.06E-01 3.76E-01 u

pCi/g 18-03105-11 B101110IFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Americium-241 pCi/g 18-03105-11 TRG B101110IFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Barium-133 pCi/g 18-03105-11 TRG B101110IFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Bismuth-214 EPA901.1 Modified 8.98E-01 7.23E-01 7.25E-01 u

pCi/g 18-03105-11 TRG B1011101FIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Cobalt-60 EPA901.1 Modified 1.38E+01 9.34E-01 1.17E+OO 5.20E-01 pCi/g

~-.'

18-03105-11 TRG 81011101FIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Cesium-134 EPA 901.1 Modified

-8.37E-03 1.98E-01 1.98E-01 4.41E-01 u

pCi/g 18-03105-11 TRG 810111 OIFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Cesium-137 EPA 901.1 Modified 4.28E-01 3.68E-01 3.69E-01 6.09E-01 u

pCi/g 3/26/2018 18-03105 Europium-152 EPA 901.1 Modified 1.32E+02 5.47E+OO 8.70E+OO 2.07E+OO pCi/g 3/26/2018 18-03105 Europium-154 EPA901.1 Modified 4.00E+OO 8.00E-01 8.26E-01 1.40E+OO u

pCi/g pCi/g pCi/g 18-03105-11 TRG 8101110IFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 lodine-129 EPA 901.1 Modified 1.93E+OO 4.77E-01 4.87E-01 1.89E+OO 18-03105-11 TRG 810111 OIFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Potassium-40 EPA 901.1 Modified 4.81E+OO 1.99E+OO 2.01E+OO 6.61E+OO u

pCi/g 18-03105-11 TRG 81011101FIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Manganese-54 EPA 901.1 Modified

-1.51E-01 3.03E-01 3.03E-01 4.89E-01 u

18-03105-11 TRG B101110IFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Niobium-94 EPA 901.1 Modified

-4.50E-01 5.32E-01 5.32E-01 4.75E-01 u

18-03105-11 TRG B101110IFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Lead-210 EPA 901.1 Modified 2.22E+02 1.92E+01 2.23E+01 1.33E+01 u

18-03105-11 TRG B101110IFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Lead-212 EPA901.1 Modified 3.16E-01 2.49E-01 2.50E-01 5.63E-01 u

pCi/g 18-03105-11 TRG B1011101FIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 1.39E+OO 6.94E-01 6.98E-01 9.88E-01 18-03105-11 TRG B1011101FIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105

Promethium-145 EPA 901.1 Modified 1.44E+01 2.05E+OO 2.18E+OO 2.24E+OO 18-03105-11 TRG B 10111 OIFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Radium-226 EPA901.1 Modified 8.98E-01 7.23E-01 7.25E-01 9.66E-01 18-03105-11 TRG B 10111 OIFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 7.95E-01 1.10E+OO 18-03105-11 TRG B1011101FIWC020CV 03/14/18 09:11 3/22/2018 EPA901.1 Modified 1.42E+OO 4.36E+OO 4.36E+OO 5.48E+OO 18-03105-11 TRG B101110IFIWC020CV 03/14/1809:11 3/22/2018 3/26/2018 18-03105 Thallium-208 EPA 901.1 Modified

-1.58E-01 1.04E+OO 1.04E+OO 8.27E-01

,,,---~-----,-- "~"="*--"---------------

18-03105-11 TRG B101110IFIWC020CV 03/14/18 09:11 3/22/2018 3/26/2018 18-03105 Uranium-235 EPA 901.1 Modified 2.35E+OO 3.13E+OO 3.13E+OO 1.92E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Nonmal Sample; DO=Duplicate Original EBERLINE SERV CES FAX 865/483-4621

[238]

Printed: 41412018 1 :08 PM Page 13 of 13 Report To:

Work Order Details*

Eberline Analytical J Alex Bohacheff SDG:

18-03105

_ Zion Solutions,_LLC Purchase Order:

677118 Final Report of Analysis 101 Shiloh Blvd

......... Analysis Category:

ENVIRONMENTAL Zion, IL 60099 Sample Matrix:

so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 18-03105-12 TRG Actinium-228 EPA901.1 Modified 5.61E-01 8.44E-01 8.45E-01 1.25E+OO u

pCi/g 18-03105-12 TRG 810111 OIFIFC021 CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Silver-108m EPA901.1 Modified 5.22E-01 2.60E-01 2.61E-01 1.97E-01 u

pCi/g v,------~---**

18-03105-12 TRG 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Americium-241 EPA 901.1 Modified 1.51E-02 2.82E-01 2.82E-01 3.56E-01 u

pCi/g 18-03105-12 TRG 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 8arium-133 EPA 901.1 Modified 2.80E-02 1.73E-01 1.73E-01 2.65E-01 u

18-03105-12 TRG 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 8ismuth-214 EPA 901.1 Modified 6.03E-01 2.76E-01 2.78E-01 6.00E-01 pCi/g 18-03105-12 TRG 810111 OIFIFC021 CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Cobalt-60 EPA901.1 Modified 8.85E+OO 5.76E-01 7.33E-01 2.83E-01 pCi/g 18-03105-12 TRG 810111 OIFIFC021 CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Cesium-134 EPA 901.1 Modified 3.89E-02 1.25E-01 1.25E-01 2.38E-01 u

pCi/g 18-03105-12 TRG 8101110IFIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Cesium-137 EPA 901.1 Modified 1.95E-03 2.35E-01 2.35E-01 3.42E-01 u

pCi/g 18-03105-12 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 pCi/g 18-03105-12 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Europium-154 EPA 901.1 Modified 2.81 E+OO 4.45E-01 4.68E-01 5.25E-01 pCi/g 18-03105-12 TRG 8101110IFIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Europium-155 EPA 901.1 Modified 1.04E+OO 4.30E-01 4.34E-01 5.55E-01 u

pCi/g

,,,.--,-~-"*-*"

emo,~M-~

18-03105-12 TRG 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Holmium-166m EPA 901.1 Modified 2.32E-01 3.83E-01 3.83E-01 2.00E-01 u

pCi/g 18-03105-12 TRG 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 lodine-129 EPA 901.1 Modified 1.05E+OO 2.07E-01 2.14E-01 2.96E-01 u

pCi/g 18-03105-12 TRG 8101110IFIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Potassium-40 EPA 901.1 Modified 8.06E+OO 1.70E+OO 1.75E+OO 2.10E+OO 18-03105-12 8101110IFIFC021 CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Manganese-54 EPA 901.1 Modified 1.74E-01 2.24E-01 2.24E-01 3.34E-01 u

pCi/g 18-03105-12 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Niobium-94 EPA 901.1 Modified 8.24E-01 3.31E-01 3.34E-01 2.91E-01 u

03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Lead-210 EPA 901.1 Modified 1.43E+02 1.27E+01 1.47E+01 7.12E+OO 18-03105-12 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Lead-212 EPA 901.1 Modified 2.72E-01 3.54E-01 u

18-03105-12 TRG 81011101FIFC021CV 03/13/18 09:00 3/22/2018 EPA 901.1 Modified 5.42E-01 2.99E-01 3.01E-01 18-03105-12 TRG 8101110!FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Promethium-145 EPA901.1 Modified

-1.06E+01 1.15E+OO 1.27E+OO 18-03105-12 TRG 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Radium-226 2.76E-01 2.78E-01 6.00E-01 pCi/g 18-03105-12 TRG 8101110IFIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Antimony-125 3.85E-01 3.85E-01 6.12E-01 u

pCi/g

*----~

18-03105-12 TRG 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Thorium-234 2.77E+OO 2.77E+OO 3.51E+OO u

pCi/g 18-03105-12 TRG 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Thallium-208 EPA 901.1 Modified 3.56E-01 3.57E-01 3.57E-01 5.12E-01 u

18-03105-12 TRG 81011101FIFC021CV 03/13/18 09:00 3/22/2018 3/26/2018 18-03105 Uranium-235 EPA 901.1 Modified

-3.18E-01 2.44E+OO 2.44E+OO 1.19E+OO u

pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621

[239]

ZIONSOLl]TIONSrrc An E' 1ergyS0/u/ions Company Sample ID Sample Matrix Sample Type Log Vol BlOl l lOFIWCOOlCV NIA CONCRETE CONCRETE 57.94 Bl01 l 10FIWC003CV NIA CONCRETE CONCRETE 57.94 B 10111 OFIWC004CV NIA CONCRETE CONCRETE 57.94 BI01110FIFC005CV NIA CONCRETE CONCRETE 57.94 Bl01 l 10FIFC006CV NIA CONCRETE CONCRETE 57.94 B 10 l l 10FIFC008CV NIA CONCRETE CONCRETE 57.94 Bl01110FIWCOI0CV NIA CONCRETE CONCRETE 57.94 BlOl l lOFIWCO! lCV NIA CONCRETE CONCRETE 57.94 Bl01110FIWCOI8CV NIA CONCRETE CONCRETE 57.94 Bl01 l 10FIWC019CV NIA CONCRETE CONCRETE 57.94 B 1 Ol l l0IFIFC003CV NIA CONCRETE CONCRETE 57.94

~

Bl01 l 10IFIWC014CV NIA CONCRETE CONCRETE 57.94 b

Bl01 l 10IFIWC015CV NIA CONCRETE CONCRETE 57.94 1

B 101 l 10IFIWC016CV NIA CONCRETE CONCRETE 57.94 REC'D MAR 2 2 2018 -

Chain-of-Custody Form 1 a-031 os Sample Container Sample Date Sample Time Analysis Type Preservative Unit Type Qty cm*

Puck I

0311512018 0835 5ROCIHTD1H3 NIA cm3 Puck I

03/1412018 1413 5ROCIHTD1H3 NIA cm3 Puck I

0311512018 0815 5ROCIHTD1H3 NIA cm3 Puck l

03/1512018 0930 5ROCIHTD1H3 NIA cm3 Puck 1

0311512018 0950 5ROCIHTD1H3 NIA cm3 Puck l

0311412018 1440 5ROCIHTD1H3 NIA cm3 Puck 1

0311412018 1356 5ROCIHTD1H3 NIA cm3 Puck I

03/1412018 1329 5ROCIHTD1H3 NIA cm3 Puck 1

0311412018 0948 5ROCIHTD1H3 NIA

'\\

cn1' Puck I

0311412018 1030 5ROCIHTD1H3 NIA cm3 Puck I

03/1312018 0845 5ROCIHTD1H3 NIA cm" Puck 1

03/1312018 1510 5ROCIHTD1H3 NIA Clll" Puck l

03/1312018 1325 5ROCIHTD1H3 NIA cm3 Puck l

03/1312018 1430 5ROCIHTD1H3 NIA ZS-WM-131 Revision 0 Information Use Remarks 0.0-0.5" 134.18g 0.0-0.5" II4.73g 0.0-0.5" 144.21g 0.0-0.5" 73.42g 0.0-0.5" 135.85g 0.0-0.5" 112.38g 0.0-0.5" 114.63g 0.0-0.5" 122.03g 0.0-0.5" 130.80g 0.0-0.5" 88.20g 0.0-0.5" 143.35g 0.0-0.5" 164.81g 0.0-0.5" 108.97g 0.0-0.5" 115.55g

[240]

¥ er lO lt l)...

ZIC>NSOLl!TIONSrrc An E nergySo/ulions Company Bl01110IFIWC017C\\'

NIA CONCRETE B!Ol l lOIFIWCOl8C\\'

NIA CONCRETE Bl0l l l0IFIWCOl9C\\'

NIA CONCRETE B 101110IFIWC020C\\'

NIA CONCRETE Bl 01110IFIFC021 CV NIA CONCRETE Laboratory:

Eberline Labs Relinquished by:

ALEX BOHACHEFF Relinquished by:

fi/<hdN{ fff[d(r,r(

Relinquished by:

CONCRETE 57.94 CONCRETE 57.94 CONCRETE 57.94 CONCRETE 57.94 CONCRETE 57.94 Date Submitted To Lab:

Date (mm/ddlyyyy):

Time:

cm3 Puck cm*'

Puck cm3 Puck cm3 Puck cm3 Puck 01f:u/.201B

//DO Date (1mn/dd/yyyy):

('J'Z,.f Z./ ! 2 ()rti Datel (1mn/ddlyyyy):

Time:

I ?.tOO Time:

l 03/1312018 1

03/1312018 l

03/1312018 1

0311412018 1

03/1312018 Ship Container No.:

Received by:

ZS-WM-131 REC'D MAR 2 2 2018 Revision 0 05 Information Use 1i :a-031

i 1007 5ROCIHTDIH3 NIA 0.0-0.5" 155.47g 1400 5ROCIHTDIH3 NIA 0.0-0.5" 91.78g 0945 5ROCIHTDIH3 NIA 0.0-0.5" 162.88g 09]1 5ROCIHTD/H3 NIA 0.0-0.5" 88.81g 0900 5ROCIHTDIH3 NIA 0.0-0.5" 162.07g Cooler Temperature:

Airbill Number: f eJ f )C Date: (1mn/ddlyyyy):

Time:

03/21/2019,

!loo Date: (1mnidd/yyyy):

Time:

03 /Jj / 2()/ H Time:

Relinquished by:

Date (m1n/dd/yyyy):

Time:

V' ~ecei~

.?"

Date: (mmldd/yyyy):

Time:

Co1mnents PO# 677118 14 day turnaround 5-ROC I HTD / H-3

ML19295G612

Text

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