ULNRC-06367, Submittal of 2016 Annual Radiological Environmental Operating Report

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Submittal of 2016 Annual Radiological Environmental Operating Report
ML17117A652
Person / Time
Site: Callaway Ameren icon.png
Issue date: 04/27/2017
From: Geyer J
Ameren Missouri, Union Electric Co
To:
Document Control Desk, Office of Nuclear Reactor Regulation
References
ULNRC-06367
Download: ML17117A652 (105)


Text

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WAmeren Callaway Plant MISSOURI

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April27, 2017 ULNRC-06367 U.S. Nuclear Regulatory Commission Attn: Document Control Desk Washington, DC 20555-0001 40 CFR 190 10 CFR 72.44(d)

Ladies and Gentlemen:

DOCKET NUMBER 50-483 CALLAWAY PLANT UNIT 1 UNION ELECTRIC CO.

RENEWED FACILITY OPERATING LICENSE NPF-30 2016 ANNUAL RADIOLOGICA L ENVIRONMENT AL OPERATING REPORT Please find enclosed the 2016 Annual Radiological Environmental Operating Report for Callaway Plant. This report is submitted in accordance with Section 5.6.2 of the Callaway Plant Technical Specifications and Appendix B to the Callaway Plant Operating License.

This letter does not contain new commitments.

If there are any questions, please contact JohannS. Geyer at (314) 225-1589 SfficiL~

l hann S. Geyer irector, Radiation Protection JPK Enclosure

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ULNRC-06367 April27, 2017 Page2 cc: Mr. Kriss M. Kennedy Regional Administrator U.S. Nuclear Regulatory Commission Region IV 1600 East Lamar Boulevard Arlington, TX 76011-4511 Senior Resident Inspector Callaway Resident Office U.S. Nuclear Regulatory Commission 8201 NRC Road Steedman, MO 65077 Mr. L. John Klos Project Manager, Callaway Plant Office ofNuclear Reactor Regulation U.S. Nuclear Regulatory Commission Mail Stop 08H4 Washington, DC 20555-0001

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ULNRC-06367 April27, 2017 Page 3 Index and send hardcopy to QA File Al60.0761 Hardcopy:

Certrec Corporation 6100 Western Place, Suite 1050 Fort Worth, TX 76107 (Certrec receives ALL attachments as long as they are non-safeguards and may be publicly disclosed.)

Electronic distribution for the following can be made via Responses and Reports ULNRC Distribution:

F. M. Diya T. E. Herrmann B. L. Cox R. C. Wink T. B. Elwood G. P. Gary Corporate Communications NSRB Secretary Mr. Greg Voss, REP Manager (SEMA)

STARS Regulatory Affairs Mr. Jay Silberg (Pillsbury Winthrop Shaw Pittman LLP)

Mr. Chris Wieberg (DNR) .

Mr. Steve Feeler (DNR)

Mr. Robert Stout (DNR)

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AMEREN MISSOURI CALLAWAY ENERGY CENTER FULTON, MISSOURI Docket Numbers 50-483 and 72-1045 ANNUAL RADIOLOGICAL ENVIRONMENTAL OPERATING REPORT to THE UNITED STATES NUCLEAR REGULATORY COMMISSION Part I January 1 to December 31, 2016 Prepared by ENVIRONMENTAL, Inc.

Midwest Laboratory and Ameren Missouri Callaway Energy Center Submitted by UNION ELECTRIC CO.

dba Ameren Missouri Project No. 8036

PREFACE This Annual Radiological Environmental Operating Report (AREOR) describes the Ameren Missouri Callaway Energy Center Radiological Environmental Monitoring Program (REMP), and the program results for the calendar year 2016. It is submitted in accordance with section 5.6.2 of the Callaway Energy Center Technical Specifications.

Staff members of the Environmental, Inc., Midwest Laboratory were responsible for the acquisition of data presented in this report. Environmental samples were collected by Ameren Missouri personnel or contractors to Ameren Missouri and shipped to Environmental, Inc. - Midwest Laboratory and Stanford Dosimetry, LLC, for analysis.

The report was prepared by Environmental, Inc., Midwest Laboratory and the Ameren Missouri Callaway Energy Center.

ii

TABLE OF CONTENTS No. Page PREFACE ..................................................................................................................... ii List of Tables ................................................................................................................. v List of Figures ............................................................................................................... vi

1.0 INTRODUCTION

........................................................................................................... 1 2.0

SUMMARY

.................................................................................................................... 2 3.0 RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM ............................... 3 3.1 Program Design and Data Interpretation ......................................................... 3 3.2 Program Description ........................................................................................ 4 3.3 Program Execution........................................................................................... 5 3.4 Laboratory Procedures ..................................................................................... 6 3.5 Program Modifications ..................................................................................... 6 3.6 Detection and Reporting Limits ........................................................................ 7 3.7 Land Use Census ............................................................................................. 7 4.0 RESULTS AND DISCUSSION ...................................................................................... 8 4.1 Atmospheric Nuclear Detonations and Nuclear Accidents .............................. 8 4.2 Program Findings ............................................................................................. 8 5.0 TABLES ...................................................................................................................... 11

6.0 REFERENCES

CITED ................................................................................................ 23 APPENDICES A Interlaboratory Comparison Program Results .......................................................... A-1 B Data Reporting Conventions .................................................................................... B-1 C Non-Radiological Monitoring Program ..................................................................... C-1 D Sampling Location Maps .......................................................................................... D-1 iii

TABLE OF CONTENTS (continued)

PART II Page Data Tabulations and Analyses...................................................................................... i iv

LIST OF TABLES No. Page 5.1 Sampling Locations, Ameren Missouri, Callaway Energy Center ............................... 12 5.2 Collection Frequencies and Required Analyses.......................................................... 16 5.3 Minimum Required Detection Capabilities for REMP Sample Analysis ...................... 17 5.4 Results of the Land Use Census................................................................................. 18 5.5 Missed Collections and Analyses ................................................................................ 19 5.6 Radiological Environmental Monitoring Program Summary........................................ 20 5.7 Direct Radiation Dose (mrem/91 days) for the Period 2000-2015 .............................. 22 In addition, the following tables are in the Appendices:

Appendix A A-1 Environmental Resource Associates (substitute program for EPA)......................... A1-1 A-2 Interlaboratory Comparison Program Results, Thermoluminescent Dosimeters (TLDs) ................................................... A2-1 A-3 In-house Spiked Samples ........................................................................................ A3-1 A-4 In-house "Blank" Samples ........................................................................................ A4-1 A-5 In-house "Duplicate" Samples .................................................................................. A5-1 A-6 Department of Energy MAPEP comparison results ................................................. A6-1 A-7 Environmental Resource Associates (substitute program for EML) ........................ A7-1 Attachment A: Acceptance criteria for spiked samples ............................................ A-2 Appendix C C-1 Introduction............................................................................................................... C-1 C-2 Unusual or Important Events .................................................................................... C-1 C-3 EPP Non-compliances ............................................................................................. C-1 C-4 Non-routine Reports ................................................................................................. C-1 C-5 Plant Design and Operation Environmental Evaluations.......................................... C-2 v

LIST OF FIGURES No. Page Appendix D D-1 Radiological Environmental Sampling Locations 1, 2, 3 mile radius from site location ................................D-2 D-2 Radiological Environmental Sampling Locations 3, 4, 5, 6 mile radius from site location. .............................................................................................................. D-3 D-3 Radiological Environmental Sampling Locations 5, 10, 15 mile radius from site location ...................................................................................................................... D-4 D-4 Non-Potable Groundwater Monitoring Wells, 600 ft radius ....................................... D-5 D-5 Non-Potable Groundwater Monitoring Wells Collection ............................................ D-6 vi

1.0 INTRODUCTION

This report presents an analysis of the results of the Radiological Environmental Monitoring Program (REMP) conducted during 2016 for the Union Electric Company (dba Ameren Missouri ) Callaway Energy Center.

The objectives of the REMP are to monitor potential critical pathways of radioactive effluent to man and determine the radiological impact on the environment caused by operation of the Callaway Energy Center. The Radiological Environmental Monitoring Program was initiated in April 1982.

The Callaway Energy Center consists of one 3565 MWt pressurized water reactor, which achieved initial criticality on October 2, 1984. The plant is located on a plateau approximately ten miles southeast of the City of Fulton in Callaway County, Missouri and approximately eighty miles west of the St. Louis metropolitan area. The Missouri River flows by the site in an easterly direction approximately five miles south of the site at its closest point.

Tabulation of the individual analyses for the year 2016 is included in Part II of this report.

1

2.0

SUMMARY

The Radiological Environmental Monitoring Program, as required by the U.S. Nuclear Regulatory Commission (NRC) Technical Specifications for the Callaway Energy Center is described herein.

Results for the year 2016 are summarized and discussed.

For the year, the Callaway Energy Center was operated in compliance with Offsite Dose Calculation Manual (ODCM) and Radiological Effluent Controls (REC) requirements. Results from the REMP indicate the Callaway Energy Center has had no significant radiological impact on the health and safety of the public or on the environment.

2

3.0 RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 3.1 Program Design and Data Interpretation The purpose of the Radiological Environmental Monitoring Program at the Callaway Energy Center is to assess the impact of the plant on its environment. For this purpose, samples are collected from waterborne, airborne, ingestion and terrestrial pathways and analyzed for radioactive content. Direct radiation levels are monitored by thermoluminescent dosimeters (TLDs).

Sources of environmental radiation can include the following:

(1) Natural background radiation arising from cosmic rays and primordial radionuclides; (2) Fallout from atmospheric nuclear detonations; (3) Releases from nuclear power plants, planned or accidental; and (4) Industrial and medical radioactive waste.

Effects due to operation of the Callaway Energy Center must be distinguished from those due to other sources in interpreting the data.

The indicator-control concept is a major interpretive aid; where feasible the design of the Callaway Energy Center program has both indicator and control stations. Most types of samples are collected at indicator locations (nearby, downwind, or downstream) and at control locations (distant, upwind, or upstream). A station effect would be indicated if the radiation level at an indicator location was significantly larger than that at the control location. The difference would have to be greater than could be accounted for by typical fluctuations in radiation levels arising from other sources.

The monitoring program includes analyses for iodine-131, a fission product, and tritium, which is produced by cosmic rays, atmospheric nuclear detonations, and also by nuclear power plants.

Most samples are analyzed for gamma-emitting isotopes, with results for the following groups quantified: zirconium-95, cesium-137, and cerium-144. These three gamma-emitting isotopes are selected as radiological impact indicators because of the different characteristic proportions in which they appear in the fission product mix produced by a nuclear reactor and that produced by a nuclear detonation. Each of the three isotopes is produced in roughly equivalent amounts by a reactor: each constitutes about 10% of the total activity of fission products ten days after reactor shutdown. On the other hand, ten days after a nuclear explosion, the contributions of zirconium-95, cerium-144, and cesium-137 to the activity of the resulting debris are in the approximate ratio 4:1:0.03 (Eisenbud,1963).

The other group quantified consists of niobium-95, ruthenium-103 and -106, cesium-134, barium-lanthanum-140, and cerium-141. These isotopes are released in small quantities by nuclear power plants, but to date their major source of injection into the general environment has been atmospheric nuclear testing. Nuclides of the next group, manganese-54, cobalt-58 and-60, and zinc-65, are activation products and arise from activation of corrosion products. They are typical components of nuclear power plant effluents, but are not produced in significant quantities by nuclear detonation.

Nuclides of the final group, beryllium-7, which is of cosmogenic origin, and potassium-40, a naturally-occurring isotope, were chosen as analytical monitors and should not be considered radiological impact indicators.

Other means of distinguishing sources of environmental radiation can be employed in interpreting the data. Current radiation levels can be compared with previous levels, including pre-operational data. Results of the monitoring program can be related to those obtained in other parts of the world. Finally, results can be related to events known to cause elevated levels of radiation in the environment, e.g., a nuclear accident.

3

3.2 Program Description The sampling and analysis schedules for the environmental radiological monitoring program at the Callaway Energy Center are summarized in Tables 5.1 and 5.2 and briefly reviewed below. Table 5.1 identifies sampling locations and specifies as to type (indicator or control) and its distance, and direction relative to the reactor site. The types of samples collected at each location, required analyses and the frequency of collections are presented in Table 5.2.

To monitor the air environment, airborne particulate and airborne iodine samples are collected by continuous pumping, at five locations. The airborne particulates are collected on glass fiber filters and the airborne iodine through activated charcoal cartridges. Both filters and cartridges are exchanged weekly. Airborne particulates are analyzed for gamma-emitting isotopes. Charcoal cartridges are analyzed for iodine-131.

The ingestion pathway is monitored by sampling of milk (if available), fish and green leafy vegetation.

Milk samples are collected semimonthly when animals are on pasture and monthly the rest of the year. There were no milk indicator stations identified by the Land Use Census for the subject year.

The control station continued to be collected. Samples are analyzed for iodine-131 and gamma-emitting isotopes.

Monthly during the growing season, edible green leafy vegetation is collected from both indicator and control locations. Vegetation samples typically consist of mustard greens, turnip greens, cabbage, lettuce, collards, radish greens, Swiss chard, broccoli and poke. Other edible broad leaf vegetation is collected if primary varieties are not available. The samples are analyzed for iodine-131 and other gamma-emitting isotopes.

Feed crops (soybeans, sorghum, corn) are collected from locations FC-1 through FC-4. FC-1, FC-2 and FC-3 are located on Ameren property traversed by the discharge pipeline. The samples are collected at harvest and analyzed for tritium and gamma emitting isotopes. FC-4 is a control location, beyond the influence of plant operations. Feed crops are grown for animal feed and not for human consumption. The soybean field for sample FC-1 is planted by the Missouri State Department of Conservation (MODOC) to provide feed to wildlife living in the Reform Wildlife Conservation Area. MODOC did not plant the field this year and there was no crop to sample.

The waterborne pathway is monitored by sampling surface water, groundwater and drinking water, and bottom and shoreline sediments. Water samples are analyzed for tritium and gamma-emitting isotopes, and sediments are analyzed for gamma-emitting isotopes.

The waterborne pathway is also monitored by upstream and downstream semiannual collections of fish. The five most abundant recreational or commercial fish species are collected. Samples are analyzed for gamma-emitting isotopes.

Monthly composite samples of surface water from the Missouri River are collected from one indicator location (S02) and from one control location (S01). The surface water samples are composites of daily collections by automatic river samplers.

Onsite surface water from ten ponds is analyzed for tritium and gamma-emitting isotopes. The collection frequencies are either semiannually or quarterly.

To monitor possible sources of ground water contamination due to plant operations, non-potable ground water was collected monthly or quarterly from well locations both onsite and along the discharge pipeline. The samples were analyzed for tritium and gamma-emitting isotopes.

Potable well water samples are collected quarterly from the plant drinking water supply, neighboring property owners, and from the town of Portland, MO. The samples were analyzed for tritium and gamma-emitting isotopes.

4

3.2 Program Description(continued)

River bottom sediment is collected semiannually at the plant's intake (A) and discharge (C). The samples are taken from water at least 2 meters deep to prevent influence of bank erosion.

Shoreline sediments are collected semiannually in the same area as bottom sediment. These samples are collected within two feet of the edge of the water. The samples are analyzed for gamma-emitting isotopes.

The direct ambient gamma radiation pathway is also considered. This exposure is monitored by thermoluminescent dosimeters (TLDs) at forty-eight locations in and around the Callaway site.

The TLDs are placed in 16 sectors around the plant as specified in the ODCM-RECS. Five of the TLD stations have neutron monitoring capability and three locations are designated as controls.

TLDs are exchanged and analyzed quarterly.

Soil is collected annually from seven indicator locations (F2, PR3, F6, PR7, W2, W3, and W4) and two control locations (M9, W1) to monitor the terrestrial environment. The samples are analyzed for gamma-emitting isotopes.

3.3 Program Execution The program was executed as described in the preceding section with the following exceptions.

(1) Surface Water:

The sampler at S01 was out of service 8 days; the sampler at S02 was out-of service 32 days.

(2) Ground Water:

No groundwater was available from location 937B for the 1/14/16 scheduled collection due to construction in the area limiting safe access to the well.

(3) Drinking Water:

No drinking water sample was available at location DWA-05 for the 2/2/16 scheduled collection. The provider residence was unoccupied on the scheduled collection date. The new owner subsequently joined program.

(4) Broadleaf Vegetation:

Edible broadleaf vegetation, collected at the four area gardens was available for harvest from May through October, 2016 with the following exceptions: Location V-9 was unavailable in May (CR201604623) and August (Conditions too wet for planting CR201606827). Locations V-11 and V-16 started producing in May but were done producing in September. See Table 5.5.

The growing season is defined as April 1 through November 1 (ref: Hammer, Gregory R.). A vegetation sample unavailable after October 31 is not considered a missed sample.

(5) Inedible Crops:

Inedible crops were not collected at location FC-1 during the 2016 collection due to the field not being planted.(CR201607652)

(6) Direct Radiation:

The second quarter TLD at location IDM-33 was found missing (CR201606360).

5

3.3 Program Execution (continued)

(7) Airborne Particulates and Iodine.

Air sample station B-3 was permanently shut down on 12/28/16 and the sampling equipment was relocated to new location A-10. The program had one less than the required number of air sampling stations during this seven day transitional period. (CR201700071).

3.4 Laboratory Procedures The iodine-131 analyses in milk were made using a sensitive radiochemical procedure involving separation of the iodine by ion-exchange, solvent extraction and subsequent beta counting.

Gamma-spectroscopic analyses were performed with HPGe detectors. Levels of iodine-131 in vegetation and concentrations of airborne iodine-131 in charcoal samples were also determined by gamma spectroscopy.

Tritium was measured by liquid scintillation.

Analytical Procedures used by Environmental, Inc. are on file at the laboratory and are available for inspection. Procedures are based on those prescribed by the Health and Safety Laboratory of the U.S. Dep't of Energy, Edition 28, 1997, U.S. Environmental Protection Agency for Measurement of Radioactivity in Drinking Water, 1980, and the U.S. Environmental Protection Agency, EERF, Radiochemical Procedures Manual, 1984.

Environmental, Inc., Midwest Laboratory has a comprehensive quality control/quality assurance program designed to assure the reliability of data obtained. Details of the QA Program are presented elsewhere (Environmental, Inc., Midwest Laboratory, 2012). The QA Program includes participation in Interlaboratory Comparison (crosscheck) Programs. Results obtained through Quality control samples and crosscheck program results are presented in Appendix A.

Environmental TLDs are processed by Stanford Dosimetry, LLC.

3.5 Program Modifications The drinking water sample at location CA-DWA-05 was added back into the program. This location was previously deleted when the property was sold and left vacant for several months.

The location was added back to the program after the new owners were located and agreed to participate in the sampling program (CR201601894).

Leafy green vegetables at location CA-FPL-V-17 were deleted from the program when the provider decided to discontinue broadleaf vegetation in his garden. Location CA-FPL-V-11 previously designated as a backup sample was re-designated as a primary sample and an ODCM required sample(CR201601894)

Air sampler station CA-APT/AIO-B3 was deleted and air sampler stations CA-APT/AIO-A10 and CA-APT/AIO-A11 were added as a result of the re-evaluation of long-term dispersion parameters.

Refer to HPCI 1506, Evaluation of Air Sampler Locations with Respect to the Recalculated Dispersion Parameters.

A neutron sensitive TLD was added to the program at location IDM-60N which is collocated with TLD IDM-60. (CR201604129).

6

3.6 Detection and Reporting Limits Table 5.3 gives the minimum required detection limits for radiological environmental sample analysis. For each sample type, the table lists the detection level for each isotope. The lower limit of detection (LLD) used in this report is described in NRC Regulatory Guide 4.1 Rev. 1, "Program for Monitoring Radioactivity in the Environs of Nuclear Power Plants" and the NRC Radiological Assessment Branch Technical Position, Rev. 1, November 1979, "An Acceptable Radiological Environmental Monitoring Program".

3.7 Land Use Census The Land Use Census is performed annually during the growing season. In 2016, the survey was conducted within a five mile canvassing radius of the Callaway Energy Center. The location of the nearest resident, nearest milk animal, and nearest garden of greater than 50 square meters producing broadleaf vegetation was identified by aerial photography and by contacting residents by phone, mail and/or in field surveys for each of the sixteen meteorological sectors using the midpoint of the two units. Residences in the vicinity of the plant were surveyed in person and by telephone.

The field inspection of the sectors was conducted on September 23, 2016. The results of the census are presented in Table 5.4. The table includes radial direction and distance from the Callaway Energy Center for each location, determined by a Global Positioning System (GPS) receiver.

No new well water sources were identified along the Callaway Energy Center pipeline corridor. No irrigation uses of the Missouri River, within 10 miles downstream, were identified during the survey.

The Missouri Department of Natural Resources confirmed that no new drinking water intakes have been located along the Missouri River within ten (10) river miles downstream from the plant.

7

4.0 RESULTS AND DISCUSSION All collections and analyses were made as scheduled, except for the listing in Table 5.5.

Results are summarized in Table 5.6 as recommended by the Nuclear Regulatory Commission.

For each type of analysis and sample medium, the table lists the mean and range of all indicator and control locations, as well as that location with the highest mean and range.

The tabulated results of all measurements are not included in this section, although references to these results will be made in the discussion. A complete tabulation of results for 2016 is contained in Part II of the Annual Report on the Radiological Environmental Monitoring Program for the Callaway Energy Center.

4.1 Atmospheric Nuclear Detonations and Nuclear Accidents The Fukushima Daiichi nuclear accident occurred March 11, 2011. There were no reported accidents involving significant release to the environment at nuclear reactor facilities in 2016. The last reported atmospheric test was conducted on October 16, 1980 by the Peoples Republic of China. There were no reported atmospheric nuclear tests in 2016.

4.2 Program Findings Airborne Particulates and Iodine No gamma emitting isotopes were identified other than naturally occurring Be-7.

There was no I-131 activity detected in any of the charcoal canister samples.

Air sampling for 2016 indicates no radiological effects of plant operation.

Direct Radiation (TLDs)

Forty-three gamma sensitive TLDs were placed in 16 sectors around the Callaway site.

Measurements from forty indicator locations averaged 15.6 mrem/quarter and the three control locations averaged 14.8 mrem/quarter. Readings ranged from 11.1 to 18.7 mrem /quarter, with the highest from the indicator location CA-IDM-11A, averaging 17.7 mrem/quarter. The differences are statistically insignificant. The TLD readings were consistent with the results for the years 2000 through 2015 as detailed in table 5.7.

Four neutron sensitive TLDs were placed in locations at the Site Boundary closest to the Independent Spent Fuel Storage Facility Installation (ISFSI) and at a control location approximately 14 miles from the site. There was no measureable neutron dose and there was no effect from the ISFSI.

Milk There are no milk indicator stations. No iodine-131 was detected in samples from the control station. No gamma-emitting isotopes, with the exception of naturally occurring potassium-40, were detected in milk. Milk data for 2016 show no radiological effects of plant operation.

Broadleaf Vegetation There was no I-131 activity detected in broadleaf vegetation samples. No gamma-emitting isotopes were detected in broadleaf vegetation samples excepting naturally occurring potassium-

40. Vegetation data for 2016 show no radiological effects of plant operation.

8

Non-Food Crops Soybean samples were analyzed for tritium and gamma-emitting isotopes. No tritium activity was detected. No gamma-emitting isotopes, excepting naturally occurring potassium-40, were detected in non-food crops.

Fish Edible portions of fish were analyzed by gamma spectroscopy. No gamma-emitting isotopes, excepting naturally occurring potassium-40, were detected in fish.

Soil Cesium-137 activity was detected at thirteen of the eighteen sample locations at an average concentration of 264 pCi/kg dry. 306 pCi/kg dry was the average activity for the ten of fourteen positive indicator locations and 108 pCi/kg dry was the average activity for the three of four positive control locations. The cesium-137 activity is consistent with levels observed from 1999 through 2015; these levels are attributable to the deposition of fallout from previous decades.

Surface Water Low level tritium was detected in two of the twelve samples collected at the downstream location S02 at an average concentration of 304 pCi/L. There was no tritium detected in the remaining ten samples from S02. No gamma-emitting isotopes were detected.

Surface Water, Ponds Eighteen pond samples were analyzed for 2016. No tritium activity or gamma activity was detected.

Drinking Water Wells (potable water)

Quarterly samples from fourteen locations were analyzed for tritium and gamma-emitting isotopes. No tritium or gamma-emitting isotopes were detected.

Wells and Ponds (non-potable water)

Groundwater samples from deep wells F-05 and F-15 were analyzed for tritium and gamma-emitting isotopes. There were no tritium or gamma emitting isotopes detected.

Wells MW-31, MW-34, MW-36, MW-39, MW-47, MW-58, and MW-59 were installed during the 2014 LSI (the 2014 LSI is described in detail in the Callaway Energy Center 2014 Annual Radioactive Effluents Release Report). These wells continue to monitor the natural attenuation of tritium which decreased significantly during 2015 and continued to decrease in 2016. Tritium activity was detected in 20 of 29 samples from these wells. The highest concentration was measured in MW-31 which peaked at 4,448 pCi/L in October. By years end, the concentration in MW-31 had fallen to 1,944 pCi/L. The average concentration among positive results for these wells was 1,072 pCi/L. The contamination is being remediated by monitored natural attenuation.

There are no active leaks.

Wells GWS, 936, 937B, 937D, 939R, 940, 941 and IFSFI Sump are located in the Plant Protected Area, adjacent to the power block. Tritium activity in these wells is believed to be the result of washout from gaseous effluents. The low level tritium activity observed in wells MW-014, MW-018 and MW-019 is due to residual low level contamination from moisture carryover during normal operation of air release valves (ARVs) in manholes 5 and 6B on the now-retired discharge pipeline. The pipeline was replaced in 2008 and there has been no new contamination of this area since then. The existing contamination is being remediated by monitored natural attenuation.

There are no active leaks and the results are consistent with 2015..

9

Sediments Samples of shoreline and bottom sediments were analyzed for gamma-emitting isotopes.

Cesium-137 was detected in one of the two bottom sediment control samples at a concentration of 74 pCi/kg dry weight, but measured below detection limits at both of the samples from the indicator location. Cesium-137 was also detected in one of the two shoreline sediment indicator samples at a measured concentration of 87 pCi/kg dry weight. These results are consistent with results from previous years. There were no other gamma-emitting isotopes excepting naturally occurring potassium-40 in any of the sediment samples.

10

5.0 TABLES 11

Table 5.1. Sampling Locations. (TLDs)

Location Distance / Sample Code Direction 1 Description Types 2 1a 10.8 mi. 310 o NW City of Fulton on Hwy Z, 0.65 mi. E of Bus. 54, W of Campus Apartments. IDM 3 1.2 mi. 308 o NW 0.1 mi. West of Hwy CC on Gravel Rd., 0.8 mi. South Hwy O, Pole No. 18559. IDM 5 1.3 mi. 79 o ENE Primary Meteorological Tower. IDM 6 2.0 mi. 274 o W Cty Rd. 428, 1.2 mi. West of Hwy CC, Utility Pole No. 18609. IDM 7 1.4 mi. 184 o S Cty Rd. 459, 2.6 mi. North of Hwy 94, Utility Pole No. 35097. IDM 9 3.8 mi. 183 o S NW Side of the Cty Rd. 459 and Hwy 94 Junction, Utility Pole No. 06754. IDM 10 3.9 mi. 159 o SSE Hwy 94, 1.8 mi. East of Cty Rd. 459, Utility Pole No. 12182. IDM 11a 4.7 mi. 139 o SE City of Portland, Utility Pole No. 12110. IDM 14 4.9 mi. 122 o ESE SE Side of Intersection D and 94, Utility Pole No. 11940. IDM 17 3.8 mi. 88 o E Cty Rd. 4053, 0.3 mi. E of Hwy 94, Kingdom Telephone Co., Pole No. 3X12. IDM 18a 3.7 mi. 67 o ENE East side of Hwy D, 0.5 mi. South of O, Utility Pole No. 38579. IDM 20 4.7 mi. 46 o NE City of Readsville, Utility Pole No. 12830. IDM 21 3.8 mi. 23 o NNE Cty Rd. 155, 1.9 mi. North of Hwy O, Utility Pole No. 19100. IDM 22a 0.9 mi. 10 o NNE North side of Hwy O, 100 feet East of Cty Rd. 150, Utility Pole No. 31094. IDM 23 6.6 mi. 15 o NNE City of Yucatan, Utility Pole No. 12670. IDM 26 3 11.7 mi. 82 o E Town of Americus, Utility Pole No. 11159. IDM 27 3 9.3 mi. 114 o ESE Town of Bluffton, Utility Pole No. 11496. IDM 30a 4.4 mi. 206 o SSW City of Steedman, Utility Pole No. 06557. IDM City of Mokane, Hwy C and Cty Rd. 400, 0.9 mi. N. of Hwy 94, Utility 31a 7.8 mi. 224 o SW Pole.52071 IDM 32 5.4 mi. 250 o WSW Hwy VV, 0.6 mi.West of Cty Rd. 447, Utility Pole No. 27031. IDM 32a 5.0 mi. 243 o WSW Cty Rd. 447, Utility Pole No. 06357. IDM 33 7.4 mi. 272 o W City of Hams Prairie, SE of Hwy C and AD Junction. IDM 34 9.5 mi. 292 o WNW NE Side of Hwy C and Cty Rd. 408 Junction. IDM 35 5.8 mi. 340 o NNW City of Toledo, Utility Pole No. 17684. IDM 36 4.9 mi. 7 o N Cty Rd. 155, 0.8 mi. South of Cty Rd. 132, Utility Pole No. 19137 IDM 37 0.5 mi. 195 o SSW Cty Rd. 459, 0.9 mi. South of Hwy CC, Utility Pole No. 35077. IDM 38 4.6 mi. 334 o NNW Cty Rd. 133, 1.5 mi. South of Hwy UU, Utility Pole No. 34708. IDM 39 5.4 mi. 312 o NW Cty Rd. 111, Utility Pole No. 17516. IDM 39a 5.0 mi. 308 o NW Cty Rd. 111, Utility Pole No. 17526. IDM 40 4.2 mi. 292 o WNW NE Side of Cty Rd. 112 and Hwy O, Utility Pole No. 18145. IDM 41 4.9 mi. 277 o W Hwy AD, 2.8 mi. East of Hwy C, Utility Pole No. 18239. IDM 42 4.4 mi. 231 o SW Cty Rd. 447, 2.6 mi. North of Cty Rd. 463, Utility Pole No. 06326. IDM 43 0.5 mi. 223 o SW Cty Rd. 459, 0.7 mi. South of Hwy CC, Utility Pole No. 35073. IDM 44 1.7 mi. 254 o WSW Hwy CC, 1.0 mi. South of Cty Rd. 459, Utility Pole No. 1877. IDM 45 1.0 mi. 285 o WNW Cty Rd. 428, 0.1 mi. West of Hwy CC, Utility Pole No. 18580. IDM 46 1.5 mi. 328 o NNW NE Side of Hwy CC and Cty Rd. 466 Intersection, Utility Pole No. 28242. IDM 47 1.0 mi. 10 o N Cty Rd. 448, 0.9 mi. South of Hwy O, Utility Pole No. 28151. IDM 48 0.4 mi. NE Cty Rd. 448, 1.5 mi. South of Hwy O, Plant Security Sign Post. IDM 49 1.6 mi. 94 o E Cty Rd. 448, Utility Pole No. 06959, Reform Wildlife Mgmt. Parking Area. IDM 50 0.9 mi. 168 o SSE Cty Rd. 459, 3.3 mi. North of Hwy 94, Utility Pole No. 35086 IDM 51a 0.3 mi. 150o SE Owner Control Fence, SE of the Water Treatment Plant. IDM 52 0.4 mi. 111 o ESE Light Pole Near the East Plant Security Fence. IDM 60 3 13.5 mi. 224 o SW Utility Pole No. 43744, just past Tebbetts City sign. IDM 12

Table 5.1. Sampling Locations. (TLDs, continued)

Location Distance / Sample Description Code Direction 1 Types 2 60N 3 13.5 mi 224 o SW Co-located with location with IDM-60. IDM 61N 1.9 mi 334 o NNW Corner of CC and O. IDM 62N 1.2 mi. 308 o NW Co-located with location 3 IDM 63N 0.9 mi. 10 o NNE Co-located with location 22a IDM 64N 1.0 mi. 285 o WNW Co-located with location 45 IDM Table 5.1. Sampling Locations (Airborne Radioiodine and Particulate samples, Surface Ponds, Potable Water)

A1 1.3 mi. 79 o ENE Primary Meteorological Tower. APT, AIO A7 9.5 mi. 312 o NW C. Bartley Farm, Fulton, MO. APT, AIO A8 0.9 mi. 10 o NNE Cty Rd. 448, 0.9 miles South of Hwy 0. APT, AIO A9 1.9 mi. 334 o NNW Community of Reform. APT, AIO B3 1.8 mi. 341 o NNW 0.3 mi. East of the O and CC Junction, Utility Pole No. 50422. APT, AIO 3 2.9 mi. 168 o Potable water, County Road 448 DWA 4 2.6 mi. 158 o Potable water, County Road 448 DWA 5 2.5 mi. 153 o Potable water, County Road 448 DWA 6 2.2 mi. 141 o Potable water, County Road 448 DWA 7 2.1 mi. 108 o Potable water, County Road 448 DWA 8 3.4 mi. 193 o Potable water, County Road 457 DWA 9 2.9 mi. 204 o Potable water, County Road 457 DWA 10 2.7 mi. 208 o Potable water, County Road 457 DWA 12 3.6 mi. 165 o Potable water, County Road 464 DWA 21 2.4 mi. 120 o Potable water, County Road 469 DWA 22 2.4 mi. 140 o Potable water, State Road 94 DWA V16 1.64 mi. 255 o WSW Wallendorf Farm, Steedman, MO DWA D01 5.0 mi. 136 o Potable water, Riverside Bar and Grill (Portland, MO). DWA PW1 Inside OCA Potable water, Unit 1 Construction well #3 open from 400-1400 DWA Pond 01 0.6 mi. 264 o Fishing Pond SWA Pond 02 0.7 mi. 232 o Fishing Pond SWA Outfall 010 0.6 mi. 42 o Stormwater Run-Off Pond SWA Outfall 011 1.0 mi. 60 o Stormwater Run-Off Pond SWA Outfall 012 0.5 mi. 178 o Stormwater Run-Off Pond SWA Outfall 013 0.5 mi. 189 o Stormwater Run-Off Pond SWA Outfall 014 0.6 mi. 343 o Stormwater Run-Off Pond SWA Outfall 015 0.7 mi. 4 o Stormwater Run-Off Pond SWA Sludge Lagoon, 0.8 mi. 153 o On service Sewage Sludge Lagoon SWA

  1. 4 S01 3 4.8 mi. 150 o SSE 555 feet Upstream of Discharge North Bank SWA S02 4.9 mi. 138 o SE 1.1 River Miles Downstream of Discharge North Bank SWA 13

Table 5.1. Sampling Locations, Non-potable Groundwater Wells Location Distance / Sample Description Code Direction 1 Types 2 936 Inside OCA Diesel Fuel Remediation Well, NW of SFSB WWA 937B Inside OCA Monitoring Well, West of the Turbine Bldg. WWA 937D Inside OCA Monitoring Well, North of Discharge Monitor Tanks. WWA 939R Inside OCA Monitoring Well, East of the Fuel Bldg. WWA 940 Inside OCA Monitoring Well, West of the Radwaste Bldg. WWA 941 Inside OCA Monitoring Well, West of the Radwaste Bldg. WWA GWS Inside OCA Ground Water Sump, West of Reactor Bldg and SFSB WWA ISFSI Inside OCA ISFSI Sump WWA U1MW-001 0.3 mi. 334o Outside OCA , Groundwater Monitoring Well WWA U1MW-002 0.4 mi. 206 o Outside OCA , Groundwater Monitoring Well WWA U1MW-004 3.7 mi. 165 o Dillon, Groundwater Monitoring Well WWA U1MW-005 3.8 mi. 160 o Brownlee / Hudson, Groundwater Monitoring Well WWA U1MW-006 3.0 mi. 171 o Ward, Groundwater Monitoring Well WWA U1MW-010 3.1 mi. 173 o Pipeline, Groundwater Monitoring Well WWA U1MW-012 3.0 mi. 172 o Ward, Groundwater Monitoring Well WWA U1MW-013 0.8 mi. 159 o Pipeline Corridor WWA U1MW-014 3.7 mi. 171 o Pipeline Corridor WWA U1MW-015 3.9 mi. 162 o Pipeline Corridor WWA U1MW-016 4.5 mi. 151 o Pipeline Corridor WWA U1MW-018 3.75 mi. 172 o Pipeline Corridor WWA U1MW-019 3.71 mi.172 o Pipeline Corridor WWA U1MW-020 3.88 mi.164 o Pipeline Corridor WWA U1MW-031 0.2 mi. ENE ~1m from manhole 86-2 WWA U1MW-034 0.2 mi. E ~130m from manhole 86-2 WWA U1MW-036 0.3 mi. ESE ~300m from manhole 86-2 WWA U1MW-039 0.6 mi. SSE ~1100m from manhole 86-2 WWA Upstream side of HDPE Gate Valve Vault inside HDPE U1MW-047 4.6 mi. SSE WWA pipeline bedding U1MW-058 0.3 mi. SE ~400m from manhole 86-2 WWA U1MW-059 1.0 mi. SSE ~1700m from MH86-2 WWA Inside Old BDL 1.4 mi. SSE Sampled through hole in Techite blowdown line WWA U2 MW 2S 1.8 mi. 5 o Groundwater Monitoring Well WWA U2 MW 5S 1.1 mi. 261 o Groundwater Monitoring Well WWA U2 MW 8 0.4 mi. 12 o Groundwater Monitoring Well WWA U2 MW 10 0.4 mi. 163 o Groundwater Monitoring Well WWA U2 MW 16 2.9 mi. 203 o Groundwater Monitoring Well WWA F05 0.9 mi. 169 o Groundwater Monitoring Well WWA F15 0.4 mi. 29 o Groundwater Monitoring Well WWA 14

Table 5.1. Sampling Locations, Soil, Food Products, Milk, Fish, Bottom Sediments and Inedible Crops.

Location Distance / Sample Description Code Direction 1 Types 2 F2 1.0 mi. 235 o SW Callaway Plant Forest Ecology Plot F2. SOL F6 1.6 mi. 51 o NE Callaway Plant Forest Ecology Plot F6. SOL PR3 0.95 mi. 108 o ESE Callaway Plant Forest Ecology Plot PR3. SOL PR7 0.5 mi. 320 o NNW Callaway Plant Forest Ecology Plot PR7. SOL W1 3 0.52 mi. 150 o SE Callaway Plant Wetlands, High Ground. SOL W2 0.52 mi. 149 o SSE Callaway Plant Wetlands, Inlet Area. SOL W3 0.65 mi. 152 o SSE Callaway Plant Wetlands, Discharge Area. SOL W4 0.63 mi. 155 o SSE Callaway Plant Wetlands, SW Bank. SOL M9 3 13 mi. 228 o SW Ferguson Farm, Tebbetts, MO. SOL V9 1.9 mi. 294 o WNW Meehan Farm, Steedman, MO FPL V11 3.2 mi. 325 o NW Hickman Farm, Steedman, MO FPL V12 3 18.7 mi. 255 o WSW Kissock Farm, South of New Bloomfield, MO FPL V16 1.6 mi. 255 o WSW Wallendorf Farm, Steedman, MO FPL M9 3 13 mi. 228 o SW Ferguson Farm, Tebbetts, MO. MLK Between 0.6 and 10.0 river miles upstream of the plant A 3,4 AQF discharge.

A 3, Upstream of the plant intake. AQS Downstream,of the plant discharge, between the confluence C4 of the Missouri River and Logan Creek(longitude -91.7365o AQF and the Portland boat ramp)..

C Vicinity of Portland - north bank AQS FC1 3.4 mi. S Between discharge pipeline MH-8 and the Katy Trail FC FC2 3.8 mi. ESE Between discharge pipeline MH-5 and MH-3B. FC FC3 4.1 mi. SSE Between Hwy 94 and the barge loading dock access road. FC FC4 3 7.9 mi. SW South Callaway High School FC 1 Distances are measured from the midpoint of the two reactors as described in Final Safety Analysis Report (FSAR) Sec.

2.1.1.1.

2 AIO = Air Iodine, APT = Air Particulate, AQF = Fish, AQS = Sediment, FPL = Leafy Green Vegetables, FC = Food Crops, IDM = TLD, MLK = Milk, SOL = Soil, SWA = Surface Water, DWA = Drinking Water, WWA = Ground Water.

3 Control Location.

4 The expanded collection areas provide sufficient habitat to collect the required number of species.

15

Table 5.2. Collection Frequencies and Required Analyses 1 (January 1 through December 31, 2016)

Media Sample Type Collection Frequency Required Analyses Code Direct radiation IDM Quarterly Deep Dose Equivalent (DDE)

Airborne iodine AIO Weekly 131I Air particulate APT Weekly PGE5 each sample Surface water (river) SWA Monthly composite PGE and 3H PGE and 3H. If contaminated with Surface water (except UHS SWA Semiannually gamma emitting nuclides of plant

& Unit 2 ponds) origin, analyze for HTD6 nuclides.

Surface water (UHS and SWA Semiannually PGE and 3H Unit 2 ponds)

PGE and 3H. If contaminated with Groundwater (not potable) WWA Quarterly gamma emitting nuclides of plant origin, analyze for HTD nuclides.

PGE and 3H. If contaminated with Well water-potable DWA Monthly gamma emitting nuclides of plant origin, analyze for HTD nuclides.

Shoreline sediment AQS Semiannually PGE Bottom sediment 2 AQS Semiannually PGE Sludge pond sediment SOL Annually PGE Soil SOL Annually PGE Semimonthly when Milk animal MLK animals are on pasture, PGE and 131I monthly other times 3 Leafy green vegetables FPL Monthly when available 4 PGE and 131I Inedible crops FC At time of harvest PGE and 3H Fish AQF Semiannually PGE on edible portion 1 Samples required by ODCM unless specified otherwise.

2 Required by NPDES permit.

3 The grazing season is defined as April 15- December 15, but will vary according to weather conditions.

4 The growing season is defined as the months April 1- November 1, but will vary according to weather conditions.

5 Principal Gamma Emitters (PGE) are defined as 54Mn, 59Fe, 58Co, 60Co, 65Zn, 95Zr/Nb, 134Cs, 137Cs, 140Ba/La and other gamma- emitting nuclides that may be identified during the gamma spectroscopy analysis.

6 Hard to Detect (HTD) nuclides are defined as 89Sr, 90Sr, 55Fe, 63Ni, 237Np, 238Pu, 239/240Pu, 241Pu, 241Am, 242Cm and 243/244Cm.

16

Table 5.3. Minimum Required Detection Capabilities for REMP Sample Analysis1 Food Non-Food Soil and Water Airborne Fish Milk Analysis Products Products Sediment (pCi/L) (pCi/m3) (pCi/kg wet) (pCi/L)

(pCi/kg wet) (pCi/kg wet) (pCi/kg dry)

H-3 3000/20003 3000 Mn-54 15 130 Fe-59 30 260 Co-58/60 15 130 Zn-65 30 260 Zr-Nb-95 2 15 I-131 1000/13 0.07 1 60 Cs-134 15 0.05 130 15 60 60 150 Cs-137 18 0.06 150 18 80 80 180 Ba-La-140 2 15 15 1 This list does not mean only these nuclides will be detected and reported. Other peaks which are measurable and identifiable will be reported.

2 Total activity, parent plus daughter activity.

3 LLDs for Surface and Drinking / Ground water are the same, with the exception of H-3 and I-131. The Drinking / Ground water LLDs for H-3 and I-131 are 2000 and 1 pCi/liter respectively.

17

Table 5.4 2016 Land Use Census Results Closest Receptor in Miles Sector Residence Garden 1, 2 Milk 1 N(A) 1.84 NI NI NNE(B) 2.16 NI NI NE(C) 2.26 NI NI ENE(D) 1.66 2.86 NI E(E) 3.51 3.94 NI ESE(F) 2.11 4.33 NI SE(G) 3.64 NI NI SSE(H) 3.17 3.57 NI S(J) 2.86 2.86 NI SSW(K) 2.38 NI NI SW(L) 2.63 2.63 NI WSW(M) 1.20 1.96 3.23*

W(N) 1.56 3.55 NI WNW(P) 1.93 1.93 NI NW(Q) 2.07 3.16 NI NNW(R) 1.81 NI NI 1 NI = None Identified.

2 Broadleaf Vegetation

  • Declined to participate in the program.

18

Table 5.5. Missed collections and analyses, Callaway Energy Center Sample Collection Date Type Analysis Location(s) or Period Comments WWA H-3, Gamma WWA-937B 01-14-16 Construction in area. Not safely accessible.

DW H-3, Gamma CA-DWA-5 02-02-16 Property unoccupied at this time.

VE Gamma CA-FPL-V-9 05-09-16 Vegetables not available at this time.

IDM Gamma CA-IDM-33 06-30-16 TLD missing in field.

VE Gamma CA-FPL-V-9 08-09-16 Vegetables not available at this time.

FC Gamma CA-FC-1 09-12-16 Field not planted.

12-28 Air station permanently shut down and AIO I-131 CA-AIO-B-3 1-05-17 moved to new location A-10.

12-28 Air station permanently shut down and APT Gamma CA-APT-B-3 01-05-17 moved to new location A-10.

19

Table 5.6 Radiological Environmental Monitoring Program Summary Number Indicator Location with Highest Control Non-Sample Type and Locations Annual Mean Locations Routine Req'd Results(e)

Type Number of Mean, Mean, LLD(b)

(Units) Analyses(a) Fraction, Mean, Fraction, Range (c) Location (d) Fraction, Range (c)

Range (c)

Waterborne Pathway 304 (2/12) SWA-S02 304 (2/12)

Surface Water H-3 24 3000 ND 0 (283-324) 4.9 mi SE (283-324)

(pCi/L)

GS 24 (b) ND - - ND 0 Surface Water, H-3 18 3000 ND none 0 Ponds (pCi/L) GS 18 (b) ND - - ND 0 H-3 55 2000 ND - - ND 0 Potable Wells (pCi/L) GS 55 (b) ND - - ND 0 Wells 533 (63/204) 1747 (5/5)

H-3 204 3000 CA-U1MW-31 None 0 (non-potable) (181-4448) (680-4448)

(pCi/L)

GS 140 (b) ND - - ND 0 Cs-134 8 150 ND - - ND 0 Sediments (pCi/kg) dry 80 (2/4) CA-AQS-C 80 (2/4)

Cs-137 8 180 ND 0 (74-87) 4.9 mi SE (74-87)

Airborne Pathway Airborne Particulates GS 260 (b) ND - - None 0 (pCi/m3)

Airborne I-131 260 0.07 ND - - None 0 Iodine (pCi/m3)

Soil Cs-134 18 150 ND - - ND 0 Soil (pCi/kg) dry Cs-137 18 180 306 (10/14) F-002 501 (2/2) 108 (3/4) 0 (116-576) 1.0 mi. SW (425-576) (56-184) 20

Table 5.6 Radiological Environmental Monitoring Program Summary Indicator Location with Highest Control Annual Mean Number Sample Type and Locations Locations Req'd Non-Type Number of Mean, Mean, LLD(b) Mean, Routine (Units) Analyses(a) Fraction, Fraction, Location (d) Fraction, Results(e)

Range (c) Range (c)

Range (c)

Ingestion Pathway Food Products Leafy Green GS 42 (b) ND - - ND 0 Vegetables (pCi/kg wet)

Non- food H-3 (f) 7 3000 ND - - ND 0 Products Soybeans (pCi/kg) wet GS 7 (b) ND - - ND 0 Fish Edible Flesh GS 20 (b) ND - - ND 0 (pCi/kg) wet I-131 20 1 none - - ND 0 Milk (pCi/L)

GS 20 (b) ND - - ND 0 Direct Radiation 15.6 (Quarterly CA-IDM-11A, 17.7 (4/4) 14.8 (12/12) 171 (159/159) 0 TLDs) Gamma 4.7 mi. SE (16.3-18.7) (11.1-18.3)

(11.1-18.7)

(mrem/Qtr)

Neutron 20 - - ND 0 (a) GS = gamma spectroscopy.

(b) LLD = nominal lower limit of detection based on a 4.66 sigma counting error for background sample. LLD's for gamma spectroscopy are in Table 5.3.

(c) Mean and range are based on detectable measurements only. Fraction of detectable measurements at specified locations is indicated in parentheses (F). ND= not detected.

(d) Locations are specified by station code (Table 5.2) and distance (miles) and direction relative to reactor site.

(e) Non-routine results are those which exceed ten times the control station value. If no control station value is available, the result is considered non-routine if it exceeds ten times the preoperational value for the location.

(f) Units: pCi/L.

21

Table 5.7 Direct Radiation Dose (mrem/91 days) for the Period 2000-2015 Station Code Mean 3 Mean + 3 Max CA-IDM-1A 16.0 3.0 19.0 18.0 CA-IDM-3 17.0 3.0 20.0 20.0 CA-IDM-5 14.4 2.9 17.3 17.1 CA-IDM-6 16.6 3.5 20.0 19.0 CA-IDM-7 16.3 3.3 19.5 19.0 CA-IDM-9 15.1 2.6 17.7 17.0 CA-IDM-10 17.1 2.8 19.9 19.3 CA-IDM-11A 17.2 2.7 19.9 19.3 CA-IDM-14 15.9 3.0 18.9 18.7 CA-IDM-17 16.2 3.1 19.3 18.3 CA-IDM-18A 16.2 5.1 21.3 18.9 CA-IDM-20 16.6 3.1 19.7 19.3 CA-IDM-21 16.5 3.4 20.0 19.0 CA-IDM-22A 14.9 4.7 19.7 18.0 CA-IDM-23 16.6 2.9 19.5 19.0 CA-IDM-26(C) 11.4 2.4 13.8 13.1 CA-IDM-27(C) 17.2 2.9 20.2 20.0 CA-IDM-30A 15.7 2.8 18.6 18.2 CA-IDM-31A 17.0 2.8 19.9 19.0 CA-IDM-32 16.7 2.9 19.6 19.0 CA-IDM-32A 16.3 4.0 20.3 20.0 CA-IDM-33 16.0 2.9 18.9 18.0 CA-IDM-34 15.4 3.1 18.5 18.0 CA-IDM-35 14.9 2.7 17.6 17.3 CA-IDM-36 15.7 3.3 19.0 18.7 CA-IDM-37 15.9 2.9 18.8 18.0 CA-IDM-38 11.5 2.4 13.8 13.9 CA-IDM-39 16.0 3.1 19.1 19.0 CA-IDM-39A 16.7 2.9 19.5 19.0 CA-IDM-40 17.2 3.0 20.2 19.2 CA-IDM-41 15.9 3.1 19.0 19.0 CA-IDM-42 13.7 2.6 16.3 15.6 CA-IDM-43 16.1 2.9 19.0 18.7 CA-IDM-44 16.4 3.1 19.6 19.0 CA-IDM-45 14.9 3.3 18.2 20.0 CA-IDM-46 16.5 2.9 19.4 19.9 CA-IDM-47 15.8 2.7 18.5 18.0 CA-IDM-48 16.7 2.8 19.5 19.0 CA-IDM-49 15.6 2.7 18.3 18.0 CA-IDM-50 16.3 2.9 19.3 20.0 CA-IDM-51A 17.1 2.8 20.0 19.8 CA-IDM-52 16.9 2.6 19.4 19.1 CA-IDM-60(C) 16.2 2.4 18.6 18.0 22

6.0 REFERENCES

Arnold, J. R. and H. A. Al-Salih. 1955. Beryllium-7 Produced by Cosmic Rays. Science 121: 451-453.

Eisenbud, M. 1963. Environmental Radioactivity, McGraw-Hill, New York, New York, pp. 213, 275-276.

Environmental, Inc., Midwest Laboratory. 2001 - 2016. Environmental Radiological Monitoring Program for the Callaway Energy Center, Annual Report - Part II, Data Tabulations and Analyses, January - December, 2000 - 2016 2016. Quality Manual, Rev. 2, 6 May 2016.

2016. Quality Control Procedures Manual, Rev. 3, 03 March 2016.

2012. Quality Assurance Program Manual, Rev. 3, 14 November 2012.

2009. Quality Control Program, Rev. 2, 12 November 2009.

Gold, S., H. W. Barkhau, B. Shlein, and B. Kahn, 1964. Measurement of Naturally Occurring Radionuclides in Air, in the Natural Environment, University of Chicago Press, Chicago, Illinois, 369-382.

Hammer, Gregory R.,Climate of Missouri, monograph available from the National Climatic Data Center (NCDC) of the National Oceanic and Atmospheric Administration (NOAA). January, 2006.

National Center for Radiological Health, 1968. Radiological Health and Data Reports, Vol. 9, Number 12, 730-746.

Stanford Dosimetry, LLC, 2014. Environmental Dosimetry Company, Annual Quality Assurance Status Report, January-December, 2013.

Teledyne Brown Engineering Environmental Services, Midwest Laboratory. 1999 - 2000. Environmental Radiological Monitoring Program for the Callaway Plant, Annual Report - Part II, Data Tabulations and Analyses, January - December, 1998 - 1999.

U.S. Environmental Protection Agency, 2007. RadNet, formerly Environmental Radiation Ambient Monitoring System, Gross Beta in Air (MO) 1981 - 2006, Gross Beta in Drinking Water (MO) 1982- 2004.

Wilson, D. W., G. M. Ward and J. E. Johnson. 1969. Environmental Contamination by Radioactive Materials, International Atomic Energy Agency. p.125.

23

APPENDIX A INTERLABORATORY COMPARISON PROGRAM RESULTS NOTE: Environmental Inc., Midwest Laboratory participates in intercomparison studies administered by Environmental Resources Associates, and serves as a replacement for studies conducted previously by the U.S. EPA Environmental Monitoring Systems Laboratory, Las Vegas, Nevada. Results are reported in Appendix A. TLD Intercomparison results, in-house spikes, blanks, duplicates and mixed analyte performance evaluation program results are also reported. Appendix A is updated four times a year; the complete Appendix is included in March, June, September and December monthly progress reports only.

January, 2016 through December, 2016

Appendix A Interlaboratory Comparison Program Results Environmental, Inc., Midwest Laboratory has participated in interlaboratory comparison (crosscheck) programs since the formulation of its quality control program in December 1971. These programs are operated by agencies which supply environmental type samples containing concentrations of radionuclides known to the issuing agency but not to participant laboratories. The purpose of such a program is to provide an independent check on a laboratorys analytical procedures and to alert it of any possible problems.

Participant laboratories measure the concentration of specified radionuclides and report them to the issuing agency. Several months later, the agency reports the known values to the participant laboratories and specifies control limits. Results consistently higher or lower than the known values or outside the control limits indicate a need to check the instruments or procedures used.

Results in Table A-1 were obtained through participation in the RAD PT Study Proficiency Testing Program administered by Environmental Resources Associates, serving as a replacement for studies conducted previously by the U.S. EPA Environmental Monitoring Systems Laboratory, Las Vegas, Nevada.

Table A-2 lists results for thermoluminescent dosimeters (TLDs), via irradiation and evaluation by the University of Wisconsin-Madison Radiation Calibration Laboratory at the University of Wisconsin Medical Radiation Research Center.

Table A-3 lists results of the analyses on in-house spiked samples for the past twelve months. All samples are prepared using NIST traceable sources. Data for previous years available upon request.

Table A-4 lists results of the analyses on in-house blank samples for the past twelve months. Data for previous years available upon request.

Table A-5 lists REMP specific analytical results from the in-house duplicate program for the past twelve months. Acceptance is based on the difference of the results being less than the sum of the errors.

Complete analytical data for duplicate analyses is available upon request.

The results in Table A-6 were obtained through participation in the Mixed Analyte Performance Evaluation Program.

Results in Table A-7 were obtained through participation in the MRAD PT Study Proficiency Testing Program administered by Environmental Resources Associates, serving as a replacement for studies conducted previously by the Environmental Measurement Laboratory Quality Assessment Program (EML).

Attachment A lists the laboratory precision at the 1 sigma level for various analyses. The acceptance criteria in Table A-3 is set at +/- 2 sigma.

Out-of-limit results are explained directly below the result.

A1

Attachment A ACCEPTANCE CRITERIA FOR SPIKED SAMPLES a

LABORATORY PRECISION: ONE STANDARD DEVIATION VALUES FOR VARIOUS ANALYSES One standard deviation Analysis Level for single determination Gamma Emitters 5 to 100 pCi/liter or kg 5.0 pCi/liter

> 100 pCi/liter or kg 5% of known value b

Strontium-89 5 to 50 pCi/liter or kg 5.0 pCi/liter

> 50 pCi/liter or kg 10% of known value b

Strontium-90 2 to 30 pCi/liter or kg 5.0 pCi/liter

> 30 pCi/liter or kg 10% of known value Potassium-40 0.1 g/liter or kg 5% of known value Gross alpha 20 pCi/liter 5.0 pCi/liter

> 20 pCi/liter 25% of known value Gross beta 100 pCi/liter 5.0 pCi/liter

> 100 pCi/liter 5% of known value Tritium 4,000 pCi/liter +/- 1 =

0.0933 169.85 x (known)

> 4,000 pCi/liter 10% of known value Radium-226,-228 0.1 pCi/liter 15% of known value Plutonium 0.1 pCi/liter, gram, or sample 10% of known value Iodine-131, 55 pCi/liter 6 pCi/liter b

Iodine-129 > 55 pCi/liter 10% of known value Uranium-238, 35 pCi/liter 6 pCi/liter b

Nickel-63 > 35 pCi/liter 15% of known value b

Technetium-99 b

Iron-55 50 to 100 pCi/liter 10 pCi/liter

> 100 pCi/liter 10% of known value b

Other Analyses --- 20% of known value a

From EPA publication, Environmental Radioactivity Laboratory Intercomparison Studies Program", Fiscal Year, 1981-1982, EPA-600/4-81-004.

b Laboratory limit.

A2

a TABLE A-1. Interlaboratory Comparison Crosscheck program, Environmental Resource Associates (ERA) .

RAD study Concentration (pCi/L)

Lab Code Date Analysis Laboratory ERA Control Result Result Limits Acceptance ERW-1392 4/4/2016 Sr-89 43.5 +/- 4.3 48.2 37.8 - 55.6 Pass ERW-1392 4/4/2016 Sr-90 27.5 +/- 1.9 28.5 20.7 - 33.1 Pass b

ERW-1394 4/4/2016 Ba-133 65.2 +/- 3.8 58.8 48.7 - 64.9 Fail c

ERW-1394 4/4/2016 Ba-133 57.8 +/- 5.3 58.8 48.7 - 64.9 Pass ERW-1394 4/4/2016 Cs-134 43.7 +/- 3.0 43.3 34.6 - 47.6 Pass ERW-1394 4/4/2016 Cs-137 86.1 +/- 5.3 78.4 70.6 - 88.9 Pass ERW-1394 4/4/2016 Co-60 108 +/- 44 102 91.8 - 114 Pass ERW-1394 4/4/2016 Zn-65 240 +/- 13 214 193 - 251 Pass ERW-1397 4/4/2016 Gr. Alpha 52.0 +/- 2.2 62.7 32.9 - 77.8 Pass ERW-1397 4/4/2016 Gr. Beta 33.9 +/- 1.2 39.2 26.0 - 46.7 Pass ERW-1400 4/4/2016 I-131 24.7 +/- 0.6 26.6 22.1 - 31.3 Pass ERW-1402 4/4/2016 Ra-226 15.6 +/- 0.5 15.2 11.3 - 17.4 Pass ERW-1402 4/4/2016 Ra-228 5.28 +/- 0.76 5.19 3.12 - 6.93 Pass ERW-1403 4/4/2016 Uranium 4.02 +/- 0.42 4.64 3.39 - 5.68 Pass ERW-1405 4/4/2016 H-3 8,150 +/- 270 7,840 6,790 - 8,620 Pass SPW-2845 7/7/2015 Ba-133 60.3 +/- 5.7 64.7 53.9 - 71.2 Pass SPW-2845 7/7/2015 Cs-134 48.8 +/- 9.3 50.1 40.3 - 55.1 Pass SPW-2845 7/7/2015 Cs-137 101 +/-8 89.8 80.8 - 101 Pass SPW-2845 7/7/2015 Co-60 65.1 +/- 5.8 59.9 53.9 - 68.4 Pass SPW-2845 7/7/2015 Zn-65 288 +/- 29 265 238 - 310 Pass ERW-3485 7/11/2016 Sr-89 43.3 +/- 6.5 53.3 42.3 - 60.9 Pass ERW-3485 7/11/2016 Sr-90 39.0 +/- 2.8 39.2 28.8 - 45.1 Pass ERW-3487 7/11/2016 Ba-133 83.3 +/- 4.9 82.9 69.7 - 91.2 Pass ERW-3487 7/11/2016 Cs-134 62.5 +/- 4.4 65.3 53.1 - 71.8 Pass ERW-3487 7/11/2016 Cs-137 98.1 +/- 5.6 95.2 85.7 - 107 Pass ERW-3487 7/11/2016 Co-60 122 +/-5 117 105 - 131 Pass ERW-3487 7/11/2016 Zn-65 124 +/-9 113 102 - 134 Pass ERW-3490 7/11/2016 Gr. Alpha 46.6 +/- 2.2 48.1 25.0 - 60.5 Pass ERW-3490 7/11/2016 Gr. Beta 26.8 +/- 1.1 28.6 18.2 - 36.4 Pass ERW-3492 7/11/2016 I-131 23.7 +/- 1.0 24.9 20.7 - 29.5 Pass ERW-3493 7/11/2016 Ra-226 12.9 +/- 0.4 12.3 9.2 - 14.2 Pass ERW-3493 7/11/2016 Ra-228 5.8 +/- 0.8 5.8 3.5 - 7.6 Pass ERW-3493 7/11/2016 Uranium 32.8 +/- 0.8 25.2 28.4 - 39.3 Pass ERW-3495 7/11/2016 H-3 12,400 +/- 334 12,400 10,800 - 13,600 Pass a

Results obtained by Environmental, Inc., Midwest Laboratory as a participant in the crosscheck program for proficiency testing in drinking water conducted by Environmental Resources Associates (ERA).

b No reason determined for failure of Ba-133 result.

c The result of reanalysis (Compare to original result, footnoted "b" above).

A1-1

TABLE A-2. Table has been intentionally omitted.

A2-1

TABLE A-3. In-House "Spiked" Samples a

Concentration b

Lab Code Date Analysis Laboratory results Known Control c d 2s, n=1 Activity Limits Acceptance SPW-290 1/21/2016 Sr-90 38.6 +/- 1.5 37.3 22.4 - 52.2 Pass SPW-292 1/21/2016 Sr-90 35.8 +/- 1.6 37.3 22.4 - 52.2 Pass SPW-294 1/21/2016 C-14 4,689 +/- 18 4,735 2,841 - 6,629 Pass SPW-414 2/1/2016 Ra-228 18.4 +/- 2.2 17.7 10.6 - 24.8 Pass W-020416 2/4/2016 Gr. Alpha 20.8 +/- 0.4 20.1 12.0 - 28.1 Pass W-020416 2/4/2016 Gr. Beta 29.7 +/- 0.3 28.9 17.3 - 40.4 Pass W-021716 2/17/2016 Ra-226 17.9 +/- 0.5 16.7 10.0 - 23.4 Pass W-030716 3/7/2016 Gr. Alpha 16.3 +/- 0.8 20.1 12.0 - 28.1 Pass W-030716 3/7/2016 Gr. Beta 27.0 +/- 0.7 28.9 17.3 - 40.4 Pass SPDW-70046 3/29/2016 Ra-226 13.4 +/- 0.4 16.7 10.0 - 23.4 Pass SPW-1163 3/22/2016 Ra-228 4.2 +/- 0.7 4.4 2.6 - 6.2 Pass SPW-1235 3/29/2016 Gr. Alpha 21.0 +/- 0.4 20.1 12.0 - 28.1 Pass SPW-1235 3/29/2016 Gr. Beta 29.4 +/- 0.3 28.9 17.3 - 40.4 Pass SPW-1739 4/21/2016 Ra-228 16.2 +/- 2.0 17.7 10.6 - 24.8 Pass SPW-2052 4/21/2016 Ra-226 16.0 +/- 0.5 16.7 10.0 - 23.4 Pass W-042616 4/21/2016 Fe-55 1,519 +/- 61 1,482 889 - 2,075 Pass SPW-1823 4/23/2016 Gr. Alpha 21.0 +/- 0.4 20.1 12.0 - 28.1 Pass SPW-1823 4/23/2016 Gr. Beta 26.6 +/- 0.3 28.9 17.3 - 40.4 Pass SPW-1998 4/29/2016 Cs-134 35.9 +/- 6.0 36.2 21.7 - 50.6 Pass SPW-1998 4/29/2016 Cs-137 82.5 +/- 7.6 71.9 43.1 - 100.6 Pass SPW-2097 5/3/2016 H-3 3,349 +/- 184 3,280 1,968 - 4,592 Pass SPW-2132 5/4/2016 H-3 3,174 +/- 178 3,280 1,968 - 4,592 Pass SPW-2229 5/7/2016 H-3 3,182 +/- 179 3,280 1,968 - 4,592 Pass SPW-2313 5/13/2016 H-3 3,183 +/- 179 3,280 1,968 - 4,592 Pass SPW-2341 5/13/2016 H-3 3,201 +/- 178 3,280 1,968 - 4,592 Pass SPW-2374 5/14/2016 H-3 3,037 +/- 175 3,280 1,968 - 4,592 Pass SPW-2411 5/17/2016 Sr-90 37.3 +/- 1.6 37.3 22.4 - 52.2 Pass SPW-2455 5/19/2016 Gr. Alpha 19.3 +/- 0.4 20.1 12.0 - 28.1 Pass SPW-2455 5/19/2016 Gr. Beta 28.6 +/- 0.3 28.9 17.3 - 40.4 Pass SPW-2457 5/19/2016 U-238 48.2 +/- 2.4 41.7 25.0 - 58.4 Pass SPW-2504 5/20/2016 H-3 3,181 +/- 178 3,280 1,968 - 4,592 Pass SPW-2528 5/23/2016 H-3 2,998 +/- 175 3,280 1,968 - 4,592 Pass SPW-2566 5/24/2016 Gr. Alpha 19.8 +/- 0.5 20.1 12.0 - 28.1 Pass SPW-2566 5/24/2016 Gr. Beta 30.4 +/- 0.3 28.9 17.3 - 40.4 Pass W-053116 4/29/2016 Cs-134 34.0 +/- 5.0 36.2 21.7 - 50.6 Pass W-053116 4/29/2016 Cs-137 78.8 +/- 7.0 71.9 43.1 - 100.6 Pass SPW-2704 6/1/2016 Sr-90 38.0 +/- 1.6 37.3 22.4 - 52.2 Pass SPW-2719 6/2/2016 Ra-228 18.1 +/- 2.1 17.7 10.6 - 24.8 Pass SPW-2749 6/3/2016 H-3 3,197 +/- 180 3,280 1,968 - 4,592 Pass SPW-2843 6/7/2016 H-3 3,133 +/- 179 3,280 1,968 - 4,592 Pass SPW-3227 6/17/2016 Ra-226 18.6 +/- 0.4 16.7 10.0 - 23.4 Pass W-061716 4/29/2016 Cs-134 37.3 +/- 8.2 36.2 21.7 - 50.6 Pass W-061716 4/29/2016 Cs-137 79.7 +/- 10.8 71.9 43.1 - 100.6 Pass SPW-3240 6/28/2016 Gr. Alpha 25.3 +/- 0.5 20.1 12.0 - 28.1 Pass SPW-3240 6/28/2016 Gr. Beta 27.1 +/- 0.3 28.9 17.3 - 40.4 Pass A3-1

TABLE A-3. In-House "Spiked" Samples a

Concentration b

Lab Code Date Analysis Laboratory results Known Control c d 2s, n=1 Activity Limits Acceptance SPW-3241 7/1/2016 H-3 8,821 +/- 283 8,650 5,190 - 12,110 Pass SPW-3309 7/1/2016 H-3 8,619 +/- 278 8,650 5,190 - 12,110 Pass SPW-3313 7/1/2016 Ra-228 16.6 +/- 2.0 17.7 10.6 - 24.8 Pass SPW-3328 7/6/2016 Sr-89 13.4 +/- 9.2 14.8 8.9 - 20.7 Pass SPW-3328 7/6/2016 Sr-90 12.3 +/- 1.3 11.4 6.8 - 16.0 Pass SPAP-3365 7/7/2016 Gr. Beta 39.7 +/- 0.1 42.2 25.3 - 59.0 Pass SPAP-3367 7/7/2016 Cs-134 1.2 +/- 0.7 1.2 0.7 - 1.7 Pass SPAP-3367 7/7/2016 Cs-137 94.4 +/- 2.8 94.0 56.4 - 131.6 Pass SPW-3370 7/7/2016 C-14 4,444 +/- 17 4,735 2,841 - 6,629 Pass SPW-3373 7/7/2016 Ni-63 446 +/-5 401 241 - 561 Pass SPW-3375 7/7/2016 Tc-99 545 +/-9 539 324 - 755 Pass SPW-3519 7/14/2016 H-3 8,621 +/- 279 8650 5,190 - 12,110 Pass SPW-3688 6/29/2016 Ra-226 17.5 +/- 0.4 16.7 10.0 - 23.4 Pass SPW-3711 7/20/2016 H-3 44,368 +/- 612 43,766 26,260 - 61,273 Pass SPW-3774 7/22/2016 H-3 45,259 +/- 619 43,766 26,260 - 61,273 Pass SPW-3776 7/22/2016 Gr. Alpha 23.3 +/- 0.5 20.1 12.0 - 28.1 Pass SPW-3776 7/22/2016 Gr. Beta 27.5 +/- 0.3 28.9 17.3 - 40.4 Pass SPW-3884 7/26/2016 H-3 45,850 +/- 623 43,766 26,260 - 61,273 Pass SPW-3950 7/28/2016 Ra-228 17.8 +/- 1.8 16.7 10 - 23 Pass SPW-3982 7/29/2016 H-3 45,273 +/- 619 43,766 26,260 - 61,273 Pass W-073016 4/29/2016 Cs-134 36.5 +/- 6.1 36.2 21.7 - 50.6 Pass W-073016 4/29/2016 Cs-137 80.6 +/- 7.5 71.9 43.1 - 100.6 Pass SPW-4134 8/4/2016 Ra-228 5.5 +/- 0.8 6.7 4.0 - 9.3 Pass SPW-4340 8/17/2016 Ra-228 19.9 +/- 2.0 16.7 10.0 - 23.4 Pass SPW-4386 7/15/2016 Ra-226 18.0 +/- 0.4 16.7 10.0 - 23.4 Pass W-082716 4/29/2016 Ra-228 32.5 +/- 5.2 36.2 21.7 - 50.6 Pass W-082716 4/29/2016 Ra-226 78.5 +/- 8.3 71.9 43.1 - 100.6 Pass SPW-4642 9/6/2016 U-238 45.8 +/- 2.5 41.7 25.0 - 58.4 Pass SPW-4999 9/26/2016 Sr-90 35.1 +/- 2.2 36.8 22.1 - 51.5 Pass SPW-5091 9/12/2016 Ra-226 18.2 +/- 0.4 16.7 10.0 - 23.4 Pass W-092716 4/29/2016 Cs-134 37.3 +/- 11.8 36.2 21.7 - 50.6 Pass W-092716 4/29/2016 Cs-137 78.3 +/- 11.2 71.9 43.1 - 100.6 Pass SPW-5165 9/30/2016 Gr. Alpha 22.2 +/- 0.4 20.1 12.0 - 28.1 Pass SPW-5165 9/30/2016 Gr. Beta 27.2 +/- 0.3 28.9 17.3 - 40.4 Pass SPW-5426 9/28/2016 Ra-226 18.2 +/- 0.4 16.7 10.0 - 23.4 Pass SPW-5510 10/18/2016 H-3 44,398 +/- 618 43,766 26,260 - 61273 Pass SPW-5553 10/19/2016 U-238 50.0 +/- 2.6 41.7 25.0 - 58.4 Pass SPW-5555 10/19/2016 Ra-228 17.4 +/- 1.9 16.7 10.0 - 23.4 Pass SPW-5612 10/20/2016 H-3 44,681 +/- 622 43,766 26,260 - 61,273 Pass SPW-5741 10/25/2016 H-3 44,946 +/- 624 43,766 26,260 - 61,273 Pass SPU-5833 10/26/2016 H-3 10,018 +/- 946 8,622 5,173 - 12,071 Pass SPW-5862 10/28/2016 H-3 18,061 +/- 374 17,244 10,346 - 24,141 Pass W-103116 4/29/2016 Cs-134 36.0 +/- 4.6 36.2 21.7 - 50.6 Pass W-103116 4/29/2016 Cs-137 81.1 +/- 7.3 71.9 43.1 - 100.6 Pass A3-2

TABLE A-3. In-House "Spiked" Samples a

Concentration b

Lab Code Date Analysis Laboratory results Known Control c d 2s, n=1 Activity Limits Acceptance SPW-5984 11/2/2016 H-3 17,727 +/- 399 17,244 10,346 - 24,141 Pass SPW-6008 11/4/2016 H-3 17,854 +/- 402 17,244 10,346 - 24,141 Pass SPW-6124 11/8/2016 Ra-228 14.4 +/- 1.9 16.0 9.6 - 22.4 Pass SPW-6132 11/9/2016 H-3 18,135 +/- 374 17,243 10,346 - 24,140 Pass SPW-6135 10/12/2016 Ra-226 18.9 +/- 0.4 16.7 10.0 - 23.4 Pass SPW-6146 11/10/2016 H-3 17,488 +/- 398 17,243 10,346 - 24,140 Pass SPW-6222 11/12/2016 H-3 17,787 +/- 408 17,243 10,346 - 24,140 Pass SPW-6318 11/16/2016 H-3 17,379 +/- 408 17,243 10,346 - 24,140 Pass SPW-6349 11/17/2016 H-3 17,893 +/- 371 17,243 10,346 - 24,140 Pass SPW-6424 11/19/2016 H-3 18,258 +/- 379 17,243 10,346 - 24,140 Pass W-112616 4/29/2016 Cs-134 35.0 +/- 6.0 36.2 21.7 - 50.6 Pass W-112616 4/29/2016 Cs-137 75.0 +/- 7.1 71.9 43.1 - 100.6 Pass SPW-6456 11/28/2016 Sr-90 41.9 +/- 2.5 36.8 22.1 - 51.5 Pass SPW-6486 11/30/2016 Sr-90 35.6 +/- 2.2 36.6 21.9 - 51.2 Pass SPW-6490 11/29/2016 Ra-226 18.8 +/- 0.4 16.7 10.0 - 23.4 Pass SPW-6519 11/30/2016 Ni-63 438 +/-4 400 240 - 560 Pass SPW-6527 12/1/2016 U-238 49.5 +/- 2.5 41.7 25.0 - 58.4 Pass SPW-6616 12/3/2016 H-3 18,018 +/- 374 17,243 10,346 - 24,140 Pass SPW-6669 12/5/2016 H-3 18,237 +/- 377 17,243 10,346 - 24,140 Pass SPW-6735 12/9/2016 H-3 17,939 +/- 396 17,243 10,346 - 24,140 Pass SPW-6880 12/21/2016 H-3 17,835 +/- 396 17,243 10,346 - 24,140 Pass SPW-6947 12/22/2016 Ni-63 450 +/-4 400 240 - 560 Pass W-122316 4/29/2016 Cs-134 36.0 +/- 2.2 36.2 21.7 - 50.6 Pass W-122316 4/29/2016 Cs-134 76.1 +/- 2.9 71.9 43.1 - 100.6 Pass SPW-6948 12/30/2016 H-3 17,999 +/- 398 17,243 10,346 - 24,140 Pass SPW-6974 12/29/2016 Ra-226 17.6 +/- 0.4 16.7 10.0 - 23.4 Pass a

Liquid sample results are reported in pCi/Liter, air filters ( pCi/m3), charcoal (pCi/charcoal canister), and solid samples (pCi/kg).

b Laboratory codes : W (Water), MI (milk), AP (air filter), SO (soil), VE (vegetation), CH (charcoal canister), F (fish), U (urine).

c Results are based on single determinations.

d Control limits are established from the precision values listed in Attachment A of this report, adjusted to +/- 2s.

NOTE: For fish, gelatin is used for the spike matrix. For vegetation, cabbage is used for the spike matrix.

A3-3

TABLE A-4. In-House "Blank" Samples a

Concentration b

Lab Code Sample Date Analysis Laboratory results (4.66) Acceptance c

Type LLD Activity Criteria (4.66 )

SPW-289 Water 1/21/2016 Sr-90 0.55 0.28 +/- 0.29 1 SPW-291 Water 1/21/2016 Sr-90 0.61 0.15 +/- 0.30 1 SPW-293 Water 1/21/2016 C-14 147 -12 +/- 89 200 SPW-413 Water 2/1/2016 Ra-228 0.86 1.86 +/- 0.60 2 W-020416 Water 2/4/2016 Gr. Alpha 0.43 -0.17 +/- 0.28 2 W-020416 Water 2/4/2016 Gr. Beta 0.73 0.36 +/- 0.53 4 W-020916 Water 2/9/2016 Ra-226 0.02 0.01 +/- 0.01 2 W-030716 Water 3/7/2016 Gr. Alpha 0.90 -0.36 +/- 0.32 2 W-030716 Water 3/7/2016 Gr. Beta 1.59 -0.62 +/- 0.71 4 SPDW-70045 Water 3/29/2016 Ra-226 0.03 0.01 +/- 0.02 2 SPDW-1234 Water 3/30/2016 Gr. Alpha 0.44 -0.05 +/- 0.30 2 SPDW-1234 Water 3/30/2016 Gr. Beta 0.79 -0.54 +/- 0.54 4 SPW-1738 Water 4/21/2016 Ra-228 1.05 0.13 +/- 0.50 2 SPW-1822 Water 4/23/2016 Gr. Alpha 0.50 -0.18 +/- 0.33 2 SPW-1822 Water 4/23/2016 Gr. Beta 0.08 -0.35 +/- 0.51 4 SPW-2051 Water 4/12/2016 Ra-226 0.02 0.03 +/- 0.02 2 SPW-2069 Water 5/3/2016 I-131 0.15 0.06 +/- 0.09 1 SPW-2133 Water 5/4/2016 H-3 148 55 +/- 76 200 SPW-2230 Water 5/7/2016 H-3 149 -11 +/- 73 200 SPW-2314 Water 5/13/2016 H-3 150 -29 +/- 72 200 SPW-2342 Water 5/13/2016 H-3 143 50 +/- 74 200 SPW-2364 Water 5/13/2016 I-131 0.22 -0.03 +/- 0.12 1 SPW-2375 Water 5/14/2016 H-3 146 1 +/- 70 200 SPW-2410 Water 5/17/2016 Sr-90 0.59 0.10 +/- 0.29 1 SPW-2454 Water 5/19/2016 Gr. Alpha 0.47 -0.21 +/- 0.31 2 SPW-2454 Water 5/19/2016 Gr. Beta 0.77 -0.49 +/- 0.52 4 SPW-2456 Water 5/19/2016 U-238 0.15 0.00 +/- 0.09 1 SPW-2485 Water 5/20/2016 I-131 0.18 -0.01 +/- 0.10 1 SPW-2505 Water 5/20/2016 H-3 144 64 +/- 75 200 SPW-2529 Water 5/23/2016 H-3 152 -3 +/- 75 200 SPW-2530 Water 5/23/2016 Ra-228 0.96 -0.12 +/- 0.43 2 SPW-2565 Water 5/24/2016 Gr. Alpha 0.47 0.03 +/- 0.33 2 SPW-2565 Water 5/24/2016 Gr. Beta 0.77 -0.23 +/- 0.53 4 SPW-2703 Water 6/1/2016 Sr-89 0.68 -0.13 +/- 0.50 5 SPW-2703 Water 6/1/2016 Sr-90 0.55 0.11 +/- 0.27 1 SPW-2718 Water 6/2/2016 Ra-228 0.67 0.23 +/- 0.34 2 SPW-2720 Water 6/2/2016 I-131 0.16 0.01 +/- 0.09 1 SPW-2750 Water 6/3/2016 H-3 151 -31 +/- 73 200 SPW-2844 Water 6/7/2016 H-3 148 -55 +/- 75 200 SPMI-2959 Milk 6/14/2016 I-131 0.16 0.09 +/- 0.10 1 SPW-3137 Water 6/23/2016 I-131 0.15 -0.03 +/- 0.08 1 SPW-3226 Water 6/17/2016 Ra-226 0.02 -0.01 +/- 0.04 2 SPW-3239 Water 6/28/2016 Gr. Alpha 0.40 -0.15 +/- 0.26 2 SPW-3239 Water 6/28/2016 Gr. Beta 0.73 0.14 +/- 0.52 4 SPW-3687 Water 6/29/2016 Ra-226 0.04 0.03 +/- 0.03 2 a 3 Liquid sample results are reported in pCi/Liter, air filters ( pCi/m ), charcoal (pCi/charcoal canister), and solid samples (pCi/g).

b I-131(G); iodine-131 as analyzed by gamma spectroscopy.

c Activity reported is a net activity result.

A4-1

TABLE A-4. In-House "Blank" Samples Concentration a b

Lab Code Sample Date Analysis Laboratory results (4.66) Acceptance c

Type LLD Activity Criteria (4.66 )

SPW-3312 Water 7/1/2016 Ra-228 0.67 0.35 +/- 0.35 2 SPW-3327 Water 7/6/2016 Sr-89 0.67 0.51 +/- 0.51 5 SPW-3327 Water 7/6/2016 Sr-90 0.60 -0.14 +/- 0.26 1 SPAP-3364 AP 7/7/2016 Gr.Beta 0.002 0.005 +/- 0.001 0.01 SPW-3370 Water 7/7/2016 C-14 115 49 +/- 71 200 SPW-3372 Water 7/7/2016 Ni-63 122 115 +/- 76 200 SPW-3374 Water 7/7/2016 Tc-99 6.07 1.00 +/- 3.70 10 SPW-3710 Water 7/20/2016 H-3 147 35 +/- 75 200 SPW-3775 Water 7/22/2016 Gr. Alpha 0.73 0.41 +/- 0.53 2 SPW-3775 Water 7/22/2016 Gr. Beta 0.45 -0.14 +/- 0.30 4 SPW-3884 Water 7/26/2016 H-3 151 -1 +/- 73 200 SPW-3949 Water 7/28/2016 Ra-228 0.76 0.32 +/- 0.39 2 SPW-3982 Water 7/29/2016 H-3 145 49 +/- 75 200 SPW-4133 Water 8/4/2016 Ra-228 0.80 0.26 +/- 0.40 2 SPW-4257 Water 8/11/2016 I-131 0.17 -0.01 +/- 0.10 1 SPW-4339 Water 8/17/2016 Ra-228 0.73 0.36 +/- 0.39 2 SPW-4385 Water 7/15/2016 Ra-226 0.09 0.75 +/- 0.09 2 SPW-4641 Water 9/6/2016 U-238 0.21 0.00 +/- 0.13 1 SPW-4684 Water 9/8/2016 H-3 151 48 +/- 78 200 SPW-4872 Water 9/16/2016 I-131 0.21 0.05 +/- 0.11 1 SPW-4998 Water 9/26/2016 Sr-89 0.54 0.06 +/- 0.39 5 SPW-4998 Water 9/26/2016 Sr-90 0.53 -0.03 +/- 0.24 1 SPW-5090 Water 8/19/2016 Ra-226 0.03 0.03 +/- 0.02 2 SPW-5164 Water 9/30/2016 Gr. Alpha 0.46 -0.05 +/- 0.32 2 SPW-5164 Water 9/30/2016 Gr. Beta 0.74 -0.02 +/- 0.52 4 SPW-5425 Water 9/28/2016 Ra-226 0.02 0.07 +/- 0.05 2 SPW-5323 Water 10/7/2016 H-3 157 -12 +/- 75 200 SPW-5552 Water 10/19/2016 U-238 0.18 0.00 +/- 0.11 1 SPW-5554 Water 10/19/2016 Ra-228 0.72 0.22 +/- 0.36 2 SPW-5611 Water 10/20/2016 H-3 153 67 +/- 80 200 SPW-5613 Water 10/21/2016 Gr. Alpha 0.76 -0.55 +/- 0.51 2 SPW-5613 Water 10/21/2016 Gr. Beta 0.42 0.02 +/- 0.29 4 SPW-5740 Water 10/25/2016 H-3 154 -2 +/- 72 200 SPW-5743 Water 10/25/2016 Sr-90 1.26 0.72 +/- 0.67 1 SPW-5861 Water 10/28/2016 H-3 179 129 +/- 91 200 SPW-5983 Water 11/2/2016 H-3 156 8 +/- 78 200 SPW-6007 Water 11/4/2016 H-3 156 -34 +/- 73 200 SPW-6131 Water 11/9/2016 H-3 180 80 +/- 92 200 SPW-6134 Water 10/12/2016 Ra-226 0.05 -0.02 +/- 0.12 2 SPW-6145 Water 11/10/2016 H-3 171 -46 +/- 80 200 SPW-6317 Water 11/16/2016 H-3 180 -43 +/- 82 200 SPW-6348 Water 11/17/2016 H-3 182 -45 +/- 88 200 SPW-6423 Water 11/19/2016 H-3 181 8 +/- 95 200 SPW-6455 Water 11/28/2016 Sr-89 0.58 -0.15 +/- 0.46 5 SPW-6455 Water 11/28/2016 Sr-90 0.67 0.09 +/- 0.32 1 SPW-6489 Water 11/29/2016 Ra-226 0.03 0.03 +/- 0.02 2 a 3 Liquid sample results are reported in pCi/Liter, air filters ( pCi/m ), charcoal (pCi/charcoal canister), and solid samples (pCi/g).

b I-131(G); iodine-131 as analyzed by gamma spectroscopy.

c Activity reported is a net activity result.

A4-2

TABLE A-4. In-House "Blank" Samples a

Concentration b

Lab Code Sample Date Analysis Laboratory results (4.66) Acceptance c

Type LLD Activity Criteria (4.66 )

SPW-6529 Water 12/1/2016 I-131 0.18 -0.03 +/- 0.10 1 SPW-6616 Water 12/3/2016 H-3 180 72 +/- 92 200 SPW-6670 Water 12/5/2016 H-3 174 28 +/- 92 200 SPW-6735 Water 12/9/2016 H-3 152 2 +/- 73 200 SPW-6792 Water 12/15/2016 I-131 0.17 0.03 +/- 0.12 1 SPW-6819 Water 12/16/2016 H-3 158 14 +/- 77 200 SPW-6879 Water 12/21/2016 H-3 147 80 +/- 75 200 SPW-6947 Water 12/22/2016 Ni-63 93 26 +/- 57 200 SPW-6973 Water 12/29/2016 Ra-226 0.03 0.03 +/- 0.02 2 a

Liquid sample results are reported in pCi/Liter, air filters ( pCi/m3), charcoal (pCi/charcoal canister), and solid samples (pCi/g).

b I-131(G); iodine-131 as analyzed by gamma spectroscopy.

c Activity reported is a net activity result.

A4-3

TABLE A-5. In-House "Duplicate" Samples a

Concentration Averaged Lab Code Date Analysis First Result Second Result Result Acceptance AP-010416 1/4/2016 Gr. Beta 0.044 +/- 0.006 0.051 +/- 0.006 0.047 +/- 0.004 Pass SPS-62, 63 1/7/2016 K-40 21.1 +/- 1.9 21.2 +/- 2.1 21.2 +/- 1.4 Pass WW-125, 126 1/7/2016 H-3 659 +/- 102 748 +/- 106 703 +/- 74 Pass SPS-199, 200 1/7/2016 Cs-137 0.09 +/- 0.02 0.08 +/- 0.03 0.08 +/- 0.02 Pass SPS-199, 200 1/7/2016 K-40 7.60 +/- 0.60 8.62 +/- 0.62 8.11 +/- 0.43 Pass AP-011116 1/11/2016 Gr. Beta 0.024 +/- 0.005 0.027 +/- 0.005 0.026 +/- 0.003 Pass AP-011216 1/12/2016 Gr. Beta 0.030 +/- 0.004 0.034 +/- 0.004 0.032 +/- 0.003 Pass WW-262, 263 1/14/2016 H-3 153 +/- 78 141 +/- 78 147 +/- 55 Pass WW-346, 347 1/14/2016 H-3 1,036 +/- 117 959 +/- 115 997 +/- 82 Pass WW-283, 284 1/18/2016 H-3 437 +/- 92 427 +/- 91 432 +/- 65 Pass AP-011916 1/19/2016 Gr. Beta 0.042 +/- 0.005 0.037 +/- 0.004 0.040 +/- 0.003 Pass AP-012016 1/20/2016 Gr. Beta 0.023 +/- 0.003 0.030 +/- 0.004 0.027 +/- 0.002 Pass AP-020116 2/1/2016 Gr. Beta 0.023 +/- 0.005 0.023 +/- 0.005 0.023 +/- 0.004 Pass SWU-472, 473 2/2/2016 Gr. Beta 4.37 +/- 0.47 4.60 +/- 0.49 4.49 +/- 0.34 Pass SG-493, 494 2/6/2016 Ac-228 2.10 +/- 0.20 2.13 +/- 0.20 2.12 +/- 0.14 Pass SG-493, 494 2/6/2016 K-40 5.79 +/- 0.57 5.50 +/- 0.69 5.65 +/- 0.45 Pass SG-493, 494 2/6/2016 Pb-214 1.84 +/- 0.11 1.91 +/- 0.11 1.88 +/- 0.08 Pass AP-020816 2/8/2016 Gr. Beta 0.020 +/- 0.004 0.019 +/- 0.004 0.020 +/- 0.003 Pass AP-020916 2/9/2016 Be-7 0.032 +/- 0.005 0.041 +/- 0.006 0.036 +/- 0.004 Pass SPS-619, 620 2/18/2016 K-40 20.0 +/- 1.8 19.1 +/- 1.6 19.5 +/- 1.2 Pass WW-640, 641 2/18/2016 H-3 90.1 +/- 75.0 153.6 +/- 78.4 121.8 +/- 54.2 Pass AP-021916 2/19/2016 Gr. Beta 0.021 +/- 0.003 0.025 +/- 0.004 0.023 +/- 0.002 Pass WW-822, 823 2/26/2016 H-3 2,770 +/- 173 2,974 +/- 178 2,872 +/- 124 Pass DW-70010, 70011 2/29/2016 Ra-226 4.88 +/- 0.29 4.93 +/- 0.28 4.91 +/- 0.20 Pass DW-70010, 70011 2/29/2016 Ra-228 3.00 +/- 0.77 1.90 +/- 0.62 2.45 +/- 0.49 Pass SW-934, 935 3/1/2016 Gr. Beta 0.94 +/- 0.52 1.36 +/- 0.60 1.15 +/- 0.40 Pass SPS-913, 914 3/3/2016 Cs-137 0.08 +/- 0.03 0.10 +/- 0.03 0.09 +/- 0.02 Pass SPS-913, 914 3/3/2016 K-40 17.45 +/- 0.94 16.83 +/- 0.95 17.14 +/- 0.67 Pass SPS-913, 914 3/3/2016 Ra-226 1.02 +/- 0.08 1.13 +/- 0.17 1.07 +/- 0.09 Pass SPS-913, 914 3/3/2016 Ra-228 1.09 +/- 0.15 1.13 +/- 0.17 1.11 +/- 0.11 Pass AP-030716 3/7/2016 Gr. Beta 0.018 +/- 0.005 0.021 +/- 0.005 0.019 +/- 0.003 Pass F-1303,1304 3/7/2016 K-40 3.320 +/- 0.475 3.508 +/- 0.396 3.414 +/- 0.309 Pass SG-976, 977 3/8/2016 Ra-226 6.75 +/- 0.25 6.28 +/- 0.22 6.52 +/- 0.17 Pass SG-976, 977 3/8/2016 Ra-228 9.21 +/- 0.49 9.09 +/- 0.49 9.15 +/- 0.35 Pass PM-1094, 1095 3/9/2016 K-40 14.01 +/- 0.68 14.47 +/- 0.72 14.24 +/- 0.49 Pass MI-1042,1043 3/7/2016 K-40 1,684 +/- 124 1,804 +/- 119 1,744 +/- 86 Pass DW-70023, 70024 3/7/2016 Ra-226 3.40 +/- 0.43 2.68 +/- 0.35 3.04 +/- 0.28 Pass DW-70023, 70024 3/7/2016 Ra-228 4.46 +/- 0.83 5.74 +/- 0.94 5.10 +/- 0.63 Pass DW-70014, 70015 3/7/2016 Gr. Alpha 13.38 +/- 1.58 11.40 +/- 1.43 12.39 +/- 1.07 Pass DW-70026, 70027 3/7/2016 Gr. Alpha 3.46 +/- 0.79 3.08 +/- 0.74 3.27 +/- 0.54 Pass DW-70038, 70039 3/8/2016 Gr. Alpha 1.14 +/- 0.89 1.73 +/- 0.95 1.44 +/- 0.65 Pass DW-70035, 70036 3/8/2016 Ra-226 0.47 +/- 0.10 0.45 +/- 0.09 0.46 +/- 0.07 Pass DW-70035, 70036 3/8/2016 Ra-228 0.56 +/- 0.45 0.47 +/- 0.44 0.52 +/- 0.31 Pass AP-031516 3/15/2016 Gr. Beta 0.014 +/- 0.003 0.016 +/- 0.004 0.015 +/- 0.002 Pass AP-032116 3/21/2016 Gr. Beta 0.014 +/- 0.004 0.020 +/- 0.004 0.017 +/- 0.003 Pass AP-1218,1219 3/24/2016 Be-7 0.135 +/- 0.065 0.167 +/- 0.081 0.151 +/- 0.052 Pass AP-1719,1720 3/28/2016 Be-7 0.075 +/- 0.008 0.076 +/- 0.007 0.076 +/- 0.005 Pass AP-033016 3/30/2016 Gr. Beta 0.023 +/- 0.004 0.025 +/- 0.004 0.024 +/- 0.003 Pass SPS-1260, 1261 3/30/2016 K-40 18.00 +/- 1.92 19.67 +/- 1.77 18.84 +/- 1.30 Pass XW-1467, 1468 3/30/2016 H-3 310 +/- 87 295 +/- 86 303 +/- 61 Pass XWW-1530, 1531 3/30/2016 H-3 198 +/- 84 162 +/- 82 180 +/- 59 Pass AP-1827, 1828 3/30/2016 Be-7 0.069 +/- 0.011 0.072 +/- 0.011 0.071 +/- 0.008 Pass AP-1323,1324 3/31/2016 Be-7 0.206 +/- 0.120 0.197 +/- 0.091 0.202 +/- 0.076 Pass LW-1446,1447 3/31/2016 Gr. Beta 2.36 +/- 0.93 2.23 +/- 1.01 2.29 +/- 0.69 Pass A5-1

TABLE A-5. In-House "Duplicate" Samples a

Concentration Averaged Lab Code Date Analysis First Result Second Result Result Acceptance WW-1740,1741 4/2/2016 H-3 21,162 +/- 120 21,091 +/- 427 21,126 +/- 222 Pass SPS-1344, 1345 4/4/2016 K-40 17.98 +/- 0.93 17.14 +/- 0.96 17.56 +/- 0.67 Pass SPS-1344, 1345 4/4/2016 Pb-214 1.12 +/- 0.09 1.04 +/- 0.08 1.08 +/- 0.06 Pass SPS-1344, 1345 4/4/2016 Ac-228 1.23 +/- 0.15 1.33 +/- 0.19 1.28 +/- 0.12 Pass SPS-1344, 1345 4/4/2016 Cs-137 0.13 +/- 0.03 0.13 +/- 0.03 0.13 +/- 0.02 Pass P-1509,1510 4/8/2016 H-3 1,084 +/- 120 1,038 +/- 119 1,061 +/- 85 Pass AP-041116 4/11/2016 Gr. Beta 0.020 +/- 0.004 0.019 +/- 0.004 0.019 +/- 0.003 Pass SS-1551,1552 4/12/2016 Gr. Beta 8.71 +/- 1.11 8.88 +/- 1.13 8.80 +/- 0.79 Pass SS-1551,1552 4/12/2016 K-40 3.50 +/- 0.25 3.06 +/- 0.28 3.28 +/- 0.19 Pass SS-1551,1552 4/12/2016 Tl-208 0.05 +/- 0.02 0.05 +/- 0.02 0.05 +/- 0.01 Pass SS-1551,1552 4/12/2016 Bi-214 0.10 +/- 0.02 0.09 +/- 0.02 0.10 +/- 0.02 Pass SS-1551,1552 4/12/2016 Pb-212 0.13 +/- 0.02 0.11 +/- 0.02 0.12 +/- 0.01 Pass SS-1551,1552 4/12/2016 Ra-226 0.35 +/- 0.17 0.30 +/- 0.17 0.32 +/- 0.12 Pass SS-1551,1552 4/12/2016 Ac-228 0.16 +/- 0.05 0.17 +/- 0.05 0.17 +/- 0.04 Pass SS-1593,1594 4/12/2016 K-40 14.80 +/- 0.73 14.89 +/- 0.78 14.85 +/- 0.53 Pass WW-1677, 1678 4/14/2016 Ra-226 0.23 +/- 0.13 0.35 +/- 0.15 0.29 +/- 0.10 Pass WW-1783,1784 4/14/2016 H-3 768 +/- 111 632 +/- 107 700 +/- 77 Pass BS-1804,1805 4/18/2016 K-40 0.79 +/- 0.02 0.87 +/- 0.19 0.83 +/- 0.10 Pass WW-2021,2022 4/18/2016 H-3 5,548 +/- 221 5,707 +/- 224 5,627 +/- 157 Pass XWW-2240, 2241 4/18/2016 H-3 638 +/- 104 543 +/- 101 591 +/- 72 Pass XWW-2109, 2110 4/19/2016 H-3 3461 +/- 185 3250 +/- 180 3356 +/- 129 Pass SPS-2130, 2131 4/25/2016 K-40 7.80 +/- 0.84 6.80 +/- 0.60 7.30 +/- 0.52 Pass AP-042516 4/25/2016 Gr. Beta 0.020 +/- 0.004 0.023 +/- 0.004 0.022 +/- 0.003 Pass BS-2065, 2066 4/25/2016 K-40 14.40 +/- 1.50 14.72 +/- 1.19 14.56 +/- 0.96 Pass AP-042716 4/27/2016 Gr. Beta 0.023 +/- 0.003 0.019 +/- 0.003 0.021 +/- 0.002 Pass SPS-1999, 2000 4/28/2016 K-40 19.84 +/- 1.76 18.963 +/- 2.42 19.40 +/- 1.50 Pass SO-2153,2154 5/2/2016 K-40 21.80 +/- 0.81 21.17 +/- 0.85 21.48 +/- 0.59 Pass SO-2153,2154 5/2/2016 Cs-137 0.11 +/- 0.03 0.11 +/- 0.07 0.11 +/- 0.04 Pass SO-2153,2154 5/2/2016 Ra-226 1.50 +/- 0.29 1.22 +/- 0.29 1.36 +/- 0.21 Pass SO-2153,2154 5/2/2016 Pb-214 0.56 +/- 0.06 0.57 +/- 0.06 0.57 +/- 0.04 Pass W-2394,2395 5/5/2016 H-3 736 +/- 106 631 +/- 102 683 +/- 74 Pass VE-2284,2285 5/9/2016 K-40 3.50 +/- 0.25 3.06 +/- 0.28 3.28 +/- 0.19 Pass AP-051016 5/10/2016 Gr. Beta 0.020 +/- 0.005 0.018 +/- 0.005 0.019 +/- 0.003 Pass SG-2261, 2262 5/10/2016 Ac-228 34.4 +/- 1.2 34.4 +/- 1.4 34.4 +/- 0.9 Pass SG-2261, 2262 5/10/2016 Pb-214 29.5 +/- 3.0 31.9 +/- 3.3 30.7 +/- 2.2 Pass BS-2439, 2440 5/12/2016 K-40 9.96 +/- 0.91 10.27 +/- 0.76 10.11 +/- 0.59 Pass WW-2534,2535 5/16/2016 H-3 14,342 +/- 354 14,613 +/- 357 14,477 +/- 252 Pass AP-051716 5/17/2016 Gr. Beta 0.014 +/- 0.004 0.015 +/- 0.004 0.014 +/- 0.003 Pass SPS-2945, 2946 5/19/2016 K-40 30.71 +/- 0.74 31.75 +/- 0.78 31.23 +/- 0.54 Pass SPS-2945, 2946 5/19/2016 Be-7 1.55 +/- 0.24 1.90 +/- 0.35 1.73 +/- 0.21 Pass SPS-2578, 2579 5/24/2016 Pb-214 0.96 +/- 0.12 0.80 +/- 0.14 0.88 +/- 0.09 Pass AP-052516 5/25/2016 Gr. Beta 0.022 +/- 0.004 0.022 +/- 0.004 0.022 +/- 0.003 Pass G-2642,2643 5/26/2016 Be-7 0.443 +/- 0.178 0.247 +/- 0.247 0.345 +/- 0.152 Pass SO-2663, 2664 5/26/2016 Cs-137 0.08 +/- 0.03 0.07 +/- 0.03 0.07 +/- 0.02 Pass SO-2663, 2664 5/26/2016 K-40 12.44 +/- 0.68 11.64 +/- 0.63 12.04 +/- 0.46 Pass SO-2663, 2664 5/26/2016 Tl-208 0.13 +/- 0.02 0.14 +/- 0.03 0.14 +/- 0.02 Pass SO-2663, 2664 5/26/2016 Pb-212 0.43 +/- 0.04 0.41 +/- 0.04 0.42 +/- 0.03 Pass SO-2663, 2664 5/26/2016 Ra-226 1.19 +/- 0.34 0.87 +/- 0.28 1.03 +/- 0.22 Pass SO-2663, 2664 5/26/2016 Ac-228 0.45 +/- 0.09 0.53 +/- 0.10 0.49 +/- 0.07 Pass SPS-2817, 2818 5/31/2016 K-40 12.10 +/- 0.70 11.05 +/- 0.70 11.58 +/- 0.49 Pass DW-70091, 70092 6/1/2016 Ra-226 5.61 +/- 0.29 5.53 +/- 0.30 5.57 +/- 0.21 Pass DW-70091, 70092 6/1/2016 Ra-228 1.45 +/- 0.58 1.91 +/- 0.62 1.68 +/- 0.42 Pass BS-2925,2926 6/3/2016 K-40 7.74 +/- 0.44 7.86 +/- 0.42 7.80 +/- 0.30 Pass SPS-2796, 2797 6/2/2016 K-40 20.91 +/- 2.38 21.16 +/- 1.82 21.04 +/- 1.50 Pass SPS-2882, 2883 6/7/2016 K-40 14.64 +/- 0.52 14.60 +/- 0.52 14.62 +/- 0.37 Pass SPS-2882, 2883 6/7/2016 Be-7 2.00 +/- 0.25 1.94 +/- 0.20 1.97 +/- 0.16 Pass DW-70102, 70103 6/13/2016 Ra-226 0.34 +/- 0.09 0.36 +/- 0.08 0.35 +/- 0.06 Pass A5-2

TABLE A-5. In-House "Duplicate" Samples a

Concentration Averaged Lab Code Date Analysis First Result Second Result Result Acceptance DW-70102, 70103 6/13/2016 Ra-228 0.93 +/- 0.47 1.11 +/- 0.53 1.02 +/- 0.35 Pass AP-061416 6/14/2016 Gr. Beta 0.026 +/- 0.004 0.023 +/- 0.004 0.024 +/- 0.003 Pass SG-3144, 3145 6/17/2016 Be-7 2.23 +/- 0.12 2.24 +/- 0.12 2.24 +/- 0.08 Pass SG-3144, 3145 6/17/2016 K-40 7.57 +/- 0.25 7.09 +/- 0.23 7.33 +/- 0.17 Pass SPS-3165, 3166 6/22/2016 K-40 21.14 +/- 2.27 22.88 +/- 1.60 22.01 +/- 1.39 Pass SPS-3323, 3324 6/24/2016 K-40 18.67 +/- 1.57 21.53 +/- 1.65 20.10 +/- 1.14 Pass WW-3231, 3232 6/27/2016 H-3 414 +/- 104 498 +/- 108 456 +/- 75 Pass AP-3830,3831 6/29/2016 Gr. Beta 0.088 +/- 0.012 0.093 +/- 0.015 0.091 +/- 0.010 Pass AP-070516A 7/5/2016 Gr. Beta 0.018 +/- 0.002 0.014 +/- 0.002 0.016 +/- 0.002 Pass AP-070516B 7/5/2016 Gr. Beta 0.025 +/- 0.005 0.026 +/- 0.005 0.025 +/- 0.004 Pass XWW-3605,3606 7/7/2016 H-3 3,316 +/- 186 3,316 +/- 181 3,316 +/- 130 Pass DW-70135,70136 7/8/2016 Gr. Alpha 3.68 +/- 1.01 2.76 +/- 0.98 3.22 +/- 0.70 Pass DW-70132,70133 7/8/2016 Ra-226 1.32 +/- 0.14 1.11 +/- 0.15 1.22 +/- 0.10 Pass DW-70132,70133 7/8/2016 Ra-228 3.92 +/- 0.94 2.94 +/- 0.90 3.43 +/- 0.65 Pass AP-071216 7/12/2016 Gr. Beta 0.014 +/- 0.004 0.018 +/- 0.004 0.016 +/- 0.003 Pass DW-70150,70151 7/14/2016 Gr. Alpha 5.00 +/- 1.06 4.43 +/- 1.04 4.72 +/- 0.74 Pass SPS-3649,3650 7/15/2016 Cs-137 0.12 +/- 0.03 0.12 +/- 0.03 0.12 +/- 0.02 Pass SPS-3649,3650 7/15/2016 K-40 16.68 +/- 0.79 16.52 +/- 0.86 16.6 +/- 0.58 Pass SPS-3649,3650 7/15/2016 Pb-214 1.20 +/- 0.08 1.17 +/- 0.08 1.19 +/- 0.06 Pass SPS-3649,3650 7/15/2016 Ac-228 1.28 +/- 0.16 1.28 +/- 0.16 1.28 +/- 0.11 Pass AP-071816 7/18/2016 Gr. Beta 0.022 +/- 0.005 0.024 +/- 0.005 0.023 +/- 0.003 Pass DW-70163,70164 7/19/2016 Gr. Alpha 1.08 +/- 0.66 1.36 +/- 0.70 1.22 +/- 0.48 Pass WW-3761,3762 7/20/2016 H-3 347 +/- 90 466 +/- 96 407 +/- 66 Pass SPS-4003,4004 7/23/2016 K-40 7.15 +/- 1.59 6.86 +/- 1.21 7.00 +/- 1.00 Pass AP-072516 7/25/2016 Gr. Beta 0.023 +/- 0.004 0.020 +/- 0.004 0.022 +/- 0.003 Pass VE-3936,3937 7/25/2016 Sr-90 0.048 +/- 0.007 0.058 +/- 0.010 0.053 +/- 0.006 Pass VE-3936,3937 7/25/2016 Be-7 0.49 +/- 0.15 0.51 +/- 0.15 0.50 +/- 0.10 Pass VE-3936,3937 7/25/2016 K-40 4.70 +/- 0.35 4.86 +/- 0.37 4.78 +/- 0.25 Pass VE-3959,3960 7/27/2016 Sr-90 0.002 +/- 0.002 0.003 +/- 0.001 0.003 +/- 0.001 Pass VE-3959,3960 7/27/2016 Be-7 0.30 +/- 0.14 0.25 +/- 0.12 0.27 +/- 0.09 Pass VE-3959,3960 7/27/2016 K-40 4.01 +/- 0.37 4.16 +/- 0.34 4.08 +/- 0.25 Pass DW-70169,70170 7/28/2016 Ra-226 0.83 +/- 0.11 0.69 +/- 0.11 0.76 +/- 0.08 Pass DW-70169,70170 7/28/2016 Ra-228 1.85 +/- 0.63 1.31 +/- 0.84 1.58 +/- 0.53 Pass AP-080116 8/1/2016 Gr. Beta 0.029 +/- 0.003 0.033 +/- 0.003 0.031 +/- 0.002 Pass SS-4131,4132 8/1/2016 K-40 12.47 +/- 0.71 13.24 +/- 0.81 12.86 +/- 0.54 Pass SS-4131,4132 8/1/2016 Cs-137 0.10 +/- 0.03 0.13 +/- 0.04 0.12 +/- 0.02 Pass SPS-4087,4088 8/2/2016 K-40 17.06 +/- 1.58 19.5 +/- 1.97 18.28 +/- 1.26 Pass WW-4976,4977 8/4/2016 H-3 17,043 +/- 390 16,821 +/- 388 16,932 +/- 275 Pass SPS-4266,4267 8/10/2016 K-40 1.06 +/- 0.47 1.69 +/- 0.52 1.375 +/- 0.35 Pass AP-081616 8/16/2016 Gr. Beta 0.029 +/- 0.005 0.025 +/- 0.004 0.027 +/- 0.003 Pass VE-4399,4400 8/18/2016 K-40 3.85 +/- 0.23 3.27 +/- 0.41 3.56 +/- 0.24 Pass VE-4399,4400 8/18/2016 Be-7 0.30 +/- 0.08 0.45 +/- 0.20 0.37 +/- 0.11 Pass WW-5394,5395 8/18/2016 H-3 947 +/- 122 846 +/- 119 896 +/- 85 Pass SPS-4441,4442 8/22/2016 K-40 20.55 +/- 2.23 19.69 +/- 1.74 20.12 +/- 1.41 Pass AP-082216 8/22/2016 Gr. Beta 0.021 +/- 0.005 0.015 +/- 0.005 0.018 +/- 0.003 Pass VE-4462,4463 8/22/2016 Be-7 0.91 +/- 0.09 0.89 +/- 0.11 0.90 +/- 0.07 Pass VE-4462,4463 8/22/2016 K-40 7.48 +/- 0.26 7.60 +/- 0.23 7.54 +/- 0.17 Pass WW-4594,4595 8/26/2016 H-3 675 +/- 107 788 +/- 111 731 +/- 77 Pass WW-4663,4664 8/26/2016 H-3 607 +/- 104 501 +/- 100 554 +/- 72 Pass SPS-4529,4530 8/26/2016 K-40 21.98 +/- 2.52 21.85 +/- 1.56 21.92 +/- 1.48 Pass AP-083016A 8/30/2016 Gr. Beta 0.030 +/- 0.003 0.035 +/- 0.004 0.033 +/- 0.002 Pass AP-083016B 8/30/2016 Gr. Beta 0.032 +/- 0.009 0.026 +/- 0.004 0.029 +/- 0.005 Pass VE-4615,4616 8/31/2016 K-40 2.96 +/- 0.16 3.11 +/- 0.17 3.03 +/- 0.11 Pass A5-3

TABLE A-5. In-House "Duplicate" Samples Concentration a Averaged Lab Code Date Analysis First Result Second Result Result Acceptance AP-090216 9/2/2016 Gr. Beta 0.022 +/- 0.004 0.027 +/- 0.004 0.024 +/- 0.003 Pass AP-090616 9/6/2016 Gr. Beta 0.023 +/- 0.005 0.023 +/- 0.005 0.023 +/- 0.003 Pass MI-4751,4752 9/7/2016 K-40 1,693 +/- 112 1,760 +/- 99 1,726 +/- 75 Pass MI-4751,4752 9/7/2016 Sr-90 1.23 +/- 0.38 1.00 +/- 0.33 1.11 +/- 0.25 Pass SW-4772,4773 9/8/2016 H-3 196 +/- 91 236 +/- 93 216 +/- 65 Pass WW-5285,5286 9/13/2016 H-3 18,010 +/- 400 18,686 +/- 407 18,348 +/- 286 Pass MI-4826,4827 9/14/2016 K-40 1,372.6 +/- 105 1,198.1 +/- 97 1,285.4 +/- 71 Pass VE-4868,4869 9/15/2016 Gr. Beta 2.50 +/- 0.06 2.57 +/- 0.06 2.53 +/- 0.04 Pass VE-4868,4869 9/15/2016 K-40 2.20 +/- 0.17 2.30 +/- 0.17 2.25 +/- 0.12 Pass CF-4934,4935 9/19/2016 K-40 11.47 +/- 0.82 11.76 +/- 0.50 11.61 +/- 0.48 Pass CF-4934,4935 9/19/2016 Be-7 0.43 +/- 0.22 0.46 +/- 0.13 0.45 +/- 0.13 Pass AP-092016 9/20/2016 Gr. Beta 0.021 +/- 0.004 0.017 +/- 0.004 0.019 +/- 0.003 Pass DW-70196,70197 9/20/2016 Gr. Alpha 13.8 +/- 1.36 15.28 +/- 1.36 14.54 +/- 0.96 Pass F-4955,4956 9/20/2016 K-40 3.40 +/- 0.44 2.86 +/- 0.39 3.13 +/- 0.30 Pass VE-5044,5045 9/20/2016 Be-7 0.46 +/- 0.05 0.50 +/- 0.11 0.48 +/- 0.06 Pass VE-5044,5045 9/20/2016 K-40 4.37 +/- 0.12 4.68 +/- 0.24 4.53 +/- 0.13 Pass WW-5219,5220 9/20/2016 H-3 63,744 +/- 743 64,755 +/- 749 64,250 +/- 527 Pass SPS-5087,5088 9/23/2016 K-40 21.04 +/- 2.32 18.84 +/- 1.88 19.94 +/- 1.49 Pass AP-092716 9/27/2016 Gr. Beta 0.031 +/- 0.005 0.032 +/- 0.005 0.031 +/- 0.003 Pass AP-5660,5661 9/28/2016 Be-7 0.093 +/- 0.014 0.086 +/- 0.019 0.089 +/- 0.012 Pass AP-5681,5682 9/27/2016 Be-7 0.079 +/- 0.019 0.071 +/- 0.015 0.075 +/- 0.012 Pass VE-5110,5111 9/28/2016 K-40 1.82 +/- 0.15 2.14 +/- 0.18 1.98 +/- 0.12 Pass AP-5154,5155 9/29/2016 Be-7 0.237 +/- 0.116 0.195 +/- 0.096 0.216 +/- 0.075 Pass AP-5702,5703 9/30/2016 Be-7 0.084 +/- 0.015 0.070 +/- 0.018 0.077 +/- 0.012 Pass MI-5264,5265 10/4/2016 K-40 1,636 +/- 128 1,610 +/- 124 1,623 +/- 89 Pass MI-5264,5265 10/4/2016 Sr-90 2.00 +/- 0.44 1.28 +/- 0.37 1.64 +/- 0.29 Pass SS-5547,5548 10/11/2016 Gr. Beta 11.27 +/- 1.19 9.47 +/- 1.20 10.37 +/- 0.84 Pass SS-5547,5548 10/11/2016 K-40 8.03 +/- 0.45 7.23 +/- 0.46 7.63 +/- 0.32 Pass SS-5547,5548 10/11/2016 Tl-208 0.04 +/- 0.02 0.04 +/- 0.02 0.04 +/- 0.01 Pass SS-5547,5548 10/11/2016 Bi-214 0.14 +/- 0.03 0.12 +/- 0.03 0.13 +/- 0.02 Pass SS-5547,5548 10/11/2016 Pb-212 0.12 +/- 0.02 0.11 +/- 0.02 0.11 +/- 0.01 Pass SS-5547,5548 10/11/2016 Ac-228 0.10 +/- 0.05 0.16 +/- 0.05 0.13 +/- 0.04 Pass AP-101116 10/11/2016 Gr. Beta 0.032 +/- 0.004 0.028 +/- 0.004 0.030 +/- 0.003 Pass WW-5526.5527 10/11/2016 H-3 18,865 +/- 408 18,904 +/- 408 18,884 +/- 289 Pass WW-5639,5640 10/19/2016 H-3 192 +/- 103 52 +/- 98 122 +/- 71 Pass WW-5723,5724 10/18/2016 H-3 36,012 +/- 560 36,207 +/- 561 36,110 +/- 396 Pass F-5811,5812 10/20/2016 K-40 0.91 +/- 0.30 0.75 +/- 0.22 0.83 +/- 0.19 Pass SO-5900,5901 10/22/2016 Cs-137 0.05 +/- 0.02 0.03 +/- 0.02 0.04 +/- 0.02 Pass SO-5900,5901 10/22/2016 K-40 9.82 +/- 0.60 10.77 +/- 0.61 10.29 +/- 0.43 Pass SO-5900,5901 10/22/2016 Tl-208 0.10 +/- 0.02 0.14 +/- 0.03 0.12 +/- 0.02 Pass SO-5900,5901 10/22/2016 Pb-212 0.32 +/- 0.03 0.33 +/- 0.03 0.32 +/- 0.02 Pass SO-5900,5901 10/22/2016 Bi-214 0.20 +/- 0.04 0.27 +/- 0.04 0.23 +/- 0.03 Pass SO-5900,5901 10/22/2016 Ac-228 0.41 +/- 0.08 0.48 +/- 0.09 0.44 +/- 0.06 Pass SO-5900,5901 10/22/2016 Ra-226 0.45 +/- 0.23 0.61 +/- 0.27 0.53 +/- 0.18 Pass SO-5900,5901 10/22/2016 Gr. Beta 16.49 +/- 1.01 17.71 +/- 1.03 17.10 +/- 0.72 Pass SS-5879,5880 10/25/2016 K-40 14.94 +/- 0.83 15.26 +/- 0.84 15.10 +/- 0.59 Pass SS-5879,5880 10/25/2016 Cs-137 0.06 +/- 0.03 0.09 +/- 0.04 0.08 +/- 0.02 Pass LW-6072,6073 10/27/2016 Gr. Beta 0.88 +/- 0.49 1.53 +/- 0.56 1.21 +/- 0.37 Pass BS-6009, 6010 10/27/2016 Cs-137 0.14 +/- 0.08 0.13 +/- 0.06 0.13 +/- 0.05 Pass BS-6009, 6010 10/27/2016 K-40 17.04 +/- 1.58 18.30 +/- 1.42 17.67 +/- 1.06 Pass F-6211,6212 10/28/2016 Gr. Beta 3.25 +/- 0.07 3.27 +/- 0.07 3.26 +/- 0.05 Pass F-6211,6212 10/28/2016 K-40 2.45 +/- 0.33 2.49 +/- 0.37 2.47 +/- 0.25 Pass DW-70230, 70231 10/28/2016 Ra-226 4.00 +/- 0.20 4.10 +/- 0.30 4.05 +/- 0.18 Pass DW-70230, 70231 10/28/2016 Ra-228 5.30 +/- 0.80 5.20 +/- 0.80 5.25 +/- 0.57 Pass F-6093,6094 10/31/2016 K-40 3.77 +/- 0.50 3.51 +/- 0.44 3.64 +/- 0.33 Pass A5-4

TABLE A-5. In-House "Duplicate" Samples a

Concentration Averaged Lab Code Date Analysis First Result Second Result Result Acceptance AP-110116 11/1/2016 Gr. Beta 0.021 +/- 0.004 0.024 +/- 0.004 0.023 +/- 0.003 Pass S-5963, 5964 11/1/2016 K-40 20.35 +/- 2.29 18.59 +/- 1.90 19.47 +/- 1.49 Pass SG-6119, 6120 11/1/2016 Ac-228 5.70 +/- 0.44 6.28 +/- 0.57 5.99 +/- 0.36 Pass SG-6119, 6120 11/1/2016 Gr. Alpha 21.59 +/- 1.88 24.35 +/- 1.93 22.97 +/- 1.35 Pass SG-6119, 6120 11/1/2016 K-40 4.89 +/- 1.10 5.90 +/- 1.08 5.40 +/- 0.77 Pass SG-6119, 6120 11/1/2016 Pb-214 3.99 +/- 0.21 4.35 +/- 0.32 4.17 +/- 0.19 Pass S-6051, 6052 11/4/2016 K-40 7.05 +/- 0.60 7.56 +/- 0.53 7.31 +/- 0.40 Pass WW-6297, 6298 11/8/2016 H-3 207 +/- 98 165 +/- 97 186 +/- 69 Pass WW-6341,6342 11/8/2016 H-3 1,356 +/- 140 1,404 +/- 141 1,380 +/- 99 Pass SO-6406,6407 11/9/2016 Cs-137 0.36 +/- 0.04 0.43 +/- 0.05 0.40 +/- 0.03 Pass SO-6406,6407 11/9/2016 K-40 10.90 +/- 0.68 11.29 +/- 0.74 11.09 +/- 0.50 Pass AP-111416 11/14/2016 Gr. Beta 0.024 +/- 0.005 0.021 +/- 0.006 0.022 +/- 0.004 Pass WW-6829,6830 11/15/2016 H-3 39,982 +/- 589 40,315 +/- 591 40,149 +/- 417 Pass DW-70239, 70240 11/17/2016 Gr. Alpha 7.99 +/- 1.15 6.41 +/- 1.05 7.20 +/- 0.78 Pass AP-112216 11/22/2016 Gr. Beta 0.049 +/- 0.005 0.045 +/- 0.005 0.047 +/- 0.003 Pass S-6473, 6474 11/24/2016 K-40 19.37 +/- 1.97 23.80 +/- 3.54 21.58 +/- 2.02 Pass SG-6938, 6939 11/28/2016 Ac-228 18.99 +/- 0.59 19.92 +/- 0.79 19.46 +/- 0.49 Pass SG-6938, 6939 11/28/2016 Pb-214 15.28 +/- 0.34 14.96 +/- 0.43 15.12 +/- 0.27 Pass AP-120116 12/1/2016 Gr. Beta 0.029 +/- 0.003 0.030 +/- 0.003 0.030 +/- 0.002 Pass F-6567,6568 12/1/2016 K-40 3.76 +/- 0.40 3.83 +/- 0.46 3.80 +/- 0.30 Pass S-6522, 6523 12/1/2016 Ac-228 1.08 +/- 0.13 1.29 +/- 0.16 1.19 +/- 0.10 Pass S-6522, 6523 12/1/2016 Pb-214 1.00 +/- 0.08 1.01 +/- 0.09 1.01 +/- 0.06 Pass S-6609, 6610 12/1/2016 K-40 15.57 +/- 1.01 15.99 +/- 0.78 15.78 +/- 0.64 Pass S-6718, 6719 12/7/2016 K-40 18.19 +/- 2.13 18.76 +/- 1.80 18.48 +/- 1.39 Pass WW-6784, 6785 12/7/2016 H-3 922 +/- 117 905 +/- 116 914 +/- 82 Pass AP-121216 12/12/2016 Gr. Beta 0.026 +/- 0.005 0.028 +/- 0.005 0.027 +/- 0.003 Pass AP-7178,7179 1/3/2017 Be-7 0.047 +/- 0.015 0.062 +/- 0.017 0.054 +/- 0.012 Pass Note: Duplicate analyses are performed on every twentieth sample received in-house. Results are not listed for those analyses with activities that measure below the LLD.

a Results are reported in units of pCi/L, except for air filters (pCi/Filter or pCi/m3), food products, vegetation, soil and sediment (pCi/g).

A5-5

TABLE A-6. Department of Energy's Mixed Analyte Performance Evaluation Program (MAPEP).

a Concentration Reference Known Control b c Lab Code Date Analysis Laboratory result Activity Limits Acceptance MASO-1053 2/1/2016 Ni-63 1,206 +/- 20 1250 875 - 1625 Pass c

MASO-1053 2/1/2016 Sr-90 0.65 +/- 1.27 0.00 NA Pass c

MASO-1053 2/1/2016 Tc-99 0.1 +/- 5.5 0.0 NA Pass MASO-1053 2/1/2016 Cs-134 908 +/- 26 1030 721 - 1339 Pass c

MASO-1053 2/1/2016 Cs-137 0.10 +/- 6.20 0.00 NA Pass MASO-1053 2/1/2016 Co-57 1058 +/- 26 992 694 - 1290 Pass MASO-1053 2/1/2016 Co-60 1229 +/- 28 1190 833 - 1547 Pass MASO-1053 2/1/2016 Mn-54 1235 +/- 43 1160 812 - 1508 Pass MASO-1053 2/1/2016 Zn-65 753 +/- 64 692 484 - 900 Pass MASO-1053 2/1/2016 K-40 753 +/- 140 607 425 - 789 Pass MASO-1053 2/1/2016 Am-241 79 +/-6 103 72 - 134 Pass MASO-1053 2/1/2016 Pu-238 73.9 +/- 9.2 63.6 44.5 - 82.7 Pass d

MASO-1053 2/1/2016 Pu-239/240 0.76 +/- 1.34 0.21 NA Pass MASO-1053 2/1/2016 U-234/233 45.0 +/- 5.1 45.9 32.1 - 59.7 Pass MASO-1053 2/1/2016 U-238 129 +/-9 146 102 - 190 Pass c

MAW-989 2/1/2016 Am-241 0.018 +/- 0.015 0.00 NA Pass c

MAW-989 2/1/2016 H-3 0.2 +/- 2.8 0.0 NA Pass MAW-989 2/1/2016 Ni-63 12.8 +/- 2.7 12.3 8.6 - 16.0 Pass MAW-989 2/1/2016 Sr-90 8.70 +/- 1.20 8.74 6.12 - 11.36 Pass c

MAW-989 2/1/2016 Tc-99 -1.1 +/- 0.6 0.0 NA Pass MAW-989 2/1/2016 Cs-134 15.5 +/- 0.3 16.1 11.3 +/- 20.9 Pass MAW-989 2/1/2016 Cs-137 23.7 +/- 0.5 21.2 14.8 - 27.6 Pass e c MAW-989 2/1/2016 Co-57 1.38 +/- 0.12 0.00 NA Fail MAW-989 2/1/2016 Co-60 12.5 +/- 0.3 11.8 8.3 - 15.3 Pass MAW-989 2/1/2016 Mn-54 12.2 +/- 0.4 11.1 7.8 - 14.4 Pass MAW-989 2/1/2016 Zn-65 15.7 +/- 0.7 13.6 9.5 - 17.7 Pass MAW-989 2/1/2016 K-40 288 +/-5 251 176 - 326 Pass MAW-989 2/1/2016 Fe-55 17.3 +/- 7.0 16.2 11.3 - 21.1 Pass MAW-989 2/1/2016 Ra-226 0.710 +/- 0.070 0.718 0.503 - 0.933 Pass MAW-989 2/1/2016 Pu-238 1.280 +/- 0.110 1.244 0.871 +/- 1.617 Pass MAW-989 2/1/2016 Pu-239/240 0.640 +/- 0.080 0.641 0.449 - 0.833 Pass MAW-989 2/1/2016 U-234/233 1.39 +/- 0.12 1.48 1.04 - 1.92 Pass MAW-989 2/1/2016 U-238 1.43 +/- 0.12 1.53 1.07 - 1.99 Pass MAW-893 2/1/2016 Gross Alpha 0.600 +/- 0.050 0.673 0.202 - 1.144 Pass MAW-893 2/1/2016 Gross Beta 2.10 +/- 0.06 2.15 1.08 - 3.23 Pass MAW-896 2/1/2016 I-129 3.67 +/- 0.20 3.85 2.70 - 5.01 Pass MAAP-1056 2/1/2016 Gross Alpha 0.39 +/- 0.05 1.20 0.36 - 2.04 Pass MAAP-1056 2/1/2016 Gross Beta 1.03 +/- 0.07 0.79 0.40 - 1.19 Pass A6-1

TABLE A-6. Department of Energy's Mixed Analyte Performance Evaluation Program (MAPEP).

a Concentration Reference Known Control b c Lab Code Date Analysis Laboratory result Activity Limits Acceptance MAAP-1057 2/1/2016 Sr-90 1.34 +/- 0.15 1.38 0.97 +/- 1.79 Pass c

MAAP-1057 2/1/2016 Cs-134 -0.01 +/- 0.03 0.00 NA Pass MAAP-1057 2/1/2016 Cs-137 2.57 +/- 0.10 2.30 1.61 - 2.99 Pass MAAP-1057 2/1/2016 Co-57 3.01 +/- 0.06 2.94 2.06 - 3.82 Pass MAAP-1057 2/1/2016 Co-60 4.28 +/- 0.10 4.02 2.81 - 5.23 Pass MAAP-1057 2/1/2016 Mn-54 4.90 +/- 0.13 4.53 3.17 - 5.89 Pass MAAP-1057 2/1/2016 Zn-65 4.09 +/- 0.18 3.57 2.50 - 4.64 Pass MAAP-1057 2/1/2016 Am-241 0.059 +/- 0.015 0.0805 0.0564 - 0.1047 Pass MAAP-1057 2/1/2016 Pu-238 0.066 +/- 0.020 0.0637 0.0446 - 0.0828 Pass d

MAAP-1057 2/1/2016 Pu-239/240 0.074 +/- 0.020 0.099 NA Pass MAAP-1057 2/1/2016 U-234/233 0.151 +/- 0.026 0.165 0.116 - 0.215 Pass MAAP-1057 2/1/2016 U-238 0.160 +/- 0.026 0.172 0.120 - 0.224 Pass MAVE-1050 2/1/2016 Cs-134 9.83 +/- 0.19 10.62 7.43 - 13.81 Pass MAVE-1050 2/1/2016 Cs-137 6.06 +/- 0.19 5.62 3.93 - 7.31 Pass MAVE-1050 2/1/2016 Co-57 13.8 +/- 0.2 11.8 8.3 - 15.3 Pass c

MAVE-1050 2/1/2016 Co-60 0.022 +/- 0.040 0.00 NA Pass c

MAVE-1050 2/1/2016 Mn-54 0.009 +/- 0.044 0.000 NA Pass MAVE-1050 2/1/2016 Zn-65 10.67 +/- 0.39 9.60 6.70 - 12.50 Pass f

MASO-4780 8/1/2016 Ni-63 648 +/- 14 990 693 - 1287 Fail g

MASO-4780 8/1/2016 Ni-63 902 +/- 46 990 693 - 1287 Pass MASO-4780 8/1/2016 Sr-90 757 +/- 16 894 626 - 1162 Pass MASO-4780 8/1/2016 Tc-99 559 +/- 12 556 389 - 723 Pass c

MASO-4780 8/1/2016 Cs-134 0.93 +/- 2.92 0.00 NA Pass MASO-4780 8/1/2016 Cs-137 1061 +/- 12 1067 747 - 1387 Pass MASO-4780 8/1/2016 Co-57 1178 +/-8 1190 833 - 1547 Pass MASO-4780 8/1/2016 Co-60 841 +/-9 851 596 - 1106 Pass c

MASO-4780 8/1/2016 Mn-54 0.69 +/- 2.53 0.00 NA Pass MASO-4780 8/1/2016 Zn-65 724 +/- 19 695 487 - 904 Pass MASO-4780 8/1/2016 K-40 566 +/- 52 588 412 - 764 Pass c

MASO-4780 8/1/2016 Am-241 0.494 +/- 0.698 0.000 NA Pass MASO-4780 8/1/2016 Pu-238 69.7 +/- 7.4 70.4 49.3 - 91.5 Pass MASO-4780 8/1/2016 Pu-239/240 53.9 +/- 6.3 53.8 37.7 - 69.9 Pass h

MASO-4780 8/1/2016 U-233/234 46.8 +/- 3.9 122 85 - 159 Fail h

MASO-4780 8/1/2016 U-238 46.6 +/- 3.9 121 85 - 157 Fail MAW-4776 8/1/2016 I-129 4.40 +/- 0.20 4.54 3.18 - 5.90 Pass c

MAVE-4782 8/1/2016 Cs-134 -0.01 +/- 0.05 0.00 NA Pass MAVE-4782 8/1/2016 Cs-137 6.18 +/- 0.20 5.54 3.88 - 7.20 Pass MAVE-4782 8/1/2016 Co-57 8.13 +/- 0.16 6.81 4.77 - 8.85 Pass MAVE-4782 8/1/2016 Co-60 5.30 +/- 0.15 4.86 3.40 - 6.32 Pass MAVE-4782 8/1/2016 Mn-54 8.08 +/- 0.24 7.27 5.09 - 9.45 Pass MAVE-4782 8/1/2016 Zn-65 6.24 +/- 0.36 5.40 3.78 - 7.02 Pass A6-2

TABLE A-6. Department of Energy's Mixed Analyte Performance Evaluation Program (MAPEP).

a Concentration c

Reference Known NA b c Lab Code Date Analysis Laboratory result Activity Limits Acceptance MAAP-4784 8/1/2016 Sr-90 1.18 +/- 0.10 1.03 0.72 - 1.34 Pass MAAP-4784 8/1/2016 Cs-134 1.58 +/- 0.08 2.04 1.43 - 2.65 Pass MAAP-4784 8/1/2016 Cs-137 1.85 +/- 0.09 1.78 1.25 - 2.31 Pass MAAP-4784 8/1/2016 Co-57 2.39 +/- 0.52 2.48 1.74 - 3.22 Pass MAAP-4784 8/1/2016 Co-60 3.22 +/- 0.08 3.26 2.28 - 4.24 Pass MAAP-4784 8/1/2016 Mn-54 2.82 +/- 0.12 2.75 1.93 - 3.58 Pass c

MAAP-4784 8/1/2016 Zn-65 -0.015 +/- 0.062 0.00 NA Pass c

MAAP-4784 8/1/2016 Am-241 -0.001 +/- 0.006 0.00 NA Pass MAAP-4784 8/1/2016 Pu-238 0.075 +/- 0.022 0.069 0.049 - 0.090 Pass MAAP-4784 8/1/2016 Pu-239/240 0.048 +/- 0.015 0.054 0.038 - 0.070 Pass MAAP-4784 8/1/2016 U-234/233 0.151 +/- 0.036 0.150 0.105 - 0.195 Pass MAAP-4784 8/1/2016 U-238 0.147 +/- 0.034 0.156 0.109 - 0.203 Pass MAW-4778 8/1/2016 H-3 365 +/- 11 334 234 - 434 Pass MAW-4778 8/1/2016 Fe-55 23.6 +/- 16.3 21.5 15.1 +/- 28.0 Pass MAW-4778 8/1/2016 Ni-63 17.0 +/- 2.8 17.2 12.0 +/- 22.4 Pass c

MAW-4778 8/1/2016 Sr-90 0.17 +/- 0.28 0.00 NA Pass MAW-4778 8/1/2016 Tc-99 9.50 +/- 0.41 11.60 8.10 - 15.10 Pass MAW-4778 8/1/2016 Cs-134 22.6 +/- 0.4 23.9 16.7 - 31.1 Pass c

MAW-4778 8/1/2016 Cs-137 0.018 +/- 0.117 0.00 NA Pass MAW-4778 8/1/2016 Co-57 27.6 +/- 0.2 27.3 19.1 +/- 35.5 Pass c

MAW-4778 8/1/2016 Co-60 0.018 +/- 0.090 0.00 NA Pass MAW-4778 8/1/2016 Mn-54 16.2 +/- 0.4 14.8 10.4 - 19.2 Pass MAW-4778 8/1/2016 Zn-65 19.3 +/- 0.7 17.4 12.2 - 22.6 Pass MAW-4778 8/1/2016 K-40 286 +/-6 252 176 - 328 Pass MAW-4778 8/1/2016 Ra-226 1.48 +/- 0.09 1.33 0.93 - 1.73 Pass MAW-4778 8/1/2016 Pu-238 1.09 +/- 0.13 1.13 0.79 - 1.47 Pass d

MAW-4778 8/1/2016 Pu-239/240 0.003 +/- 0.011 0.016 NA Pass MAW-4778 8/1/2016 U-234/233 1.80 +/- 0.13 1.86 1.30 - 2.42 Pass MAW-4778 8/1/2016 U-238 1.77 +/- 0.13 1.92 1.34 - 2.50 Pass MAW-4778 8/1/2016 Am-241 0.678 +/- 0.086 0.814 0.570 +/- 1.058 Pass a

Results are reported in units of Bq/kg (soil), Bq/L (water) or Bq/total sample (filters, vegetation).

b Laboratory codes as follows: MAW (water), MAAP (air filter), MASO (soil), MAVE (vegetation).

c MAPEP results are presented as the known values and expected laboratory precision (1 sigma, 1 determination) and control limits as defined by the MAPEP. A known value of "zero" indicates an analysis was included in the testing series as a "false positive". MAPEP does not provide control limits.

d Provided in the series for "sensitivity evaluation". MAPEP does not provide control limits.

e The laboratory properly identified the Sn-75 interfering peak in the vicinity of Co-57 and stated so in the comment field. MAPEP requires results to be reported as an activity with an uncertainty. Since the calculated uncertainty was less than the activity MAPEP interpreted the submitted result as a "false positive" resulting in a failure.

f Original analysis for Ni-63 failed.

g Reanalysis with a smaller aliquot resulted in acceptable results. An investigation is in process to identify better techniques for analyzing samples with complex matrices.

h MAPEP states that samples contain two fractions of Uranium; one that is soluble in concentrated HNO3 and HCl acid and one that is "fundamentally insoluble in these acids". They also state that HF treatment can not assure complete dissolution.

Results are consistent with measuring the soluble form.

A6-3

a TABLE A-7. Interlaboratory Comparison Crosscheck Program, Environmental Resource Associates (ERA) .

MRAD Study a

Concentration b

Lab Code Date Analysis Laboratory ERA Control Result Result Limits Acceptance ERAP-1101 3/14/2016 Am-241 37.3 45.9 28.3 - 62.1 Pass ERAP-1101 3/14/2016 Co-60 637 623 482 - 778 Pass ERAP-1101 3/14/2016 Cs-134 251 304 193 - 377 Pass ERAP-1101 3/14/2016 Cs-137 1,273 1,150 864 - 1,510 Pass ERAP-1101 3/14/2016 Fe-55 < 162 126 39.1 - 246 Pass ERAP-1101 3/14/2016 Mn-54 < 2.64 < 50.0 0.00 - 50.0 Pass ERAP-1101 3/14/2016 Pu-238 68.0 70.5 48.3 - 92.7 Pass ERAP-1101 3/14/2016 Pu-239/240 54.1 54.8 39.70 - 71.60 Pass ERAP-1101 3/14/2016 Sr-90 139 150 73.3 - 225.0 Pass ERAP-1101 3/14/2016 U-233/234 59.3 64.8 40.2 - 97.7 Pass ERAP-1101 3/14/2016 U-238 55.5 64.2 41.5 - 88.8 Pass ERAP-1101 3/14/2016 Zn-65 428 356 255 - 492 Pass ERAP-1101 3/14/2016 Gr. Alpha 98.0 70.1 23.5 - 109 Pass ERAP-1101 3/14/2016 Gr. Beta 78.6 54.4 34.4 - 79.3 Pass ERSO-1105 3/14/2016 Am-241 1,030 1,360 796 - 1,770 Pass ERSO-1105 3/14/2016 Ac-228 1,540 1,240 795 - 1,720 Pass ERSO-1105 3/14/2016 Bi-212 1,550 1,240 330 - 1,820 Pass ERSO-1105 3/14/2016 Bi-214 3,100 3,530 2,130 - 5,080 Pass ERSO-1105 3/14/2016 Co-60 5,600 5,490 3,710 - 7,560 Pass ERSO-1105 3/14/2016 Cs-134 3,030 3,450 2,260 - 4,140 Pass ERSO-1105 3/14/2016 Cs-137 4,440 4,310 3,300 - 5,550 Pass ERSO-1105 3/14/2016 K-40 10,300 10,600 7,740 - 14,200 Pass ERSO-1105 3/14/2016 Mn-54 < 50.8 < 1000 0.0 - 1,000 Pass ERSO-1105 3/14/2016 Pb-212 1,140 1,240 812 - 1,730 Pass ERSO-1105 3/14/2016 Pb-214 3,190 3,710 2,170 - 5,530 Pass ERSO-1105 3/14/2016 Pu-238 680 658 396 - 908 Pass ERSO-1105 3/14/2016 Pu-239/240 460 496 324 - 0,685 Pass ERSO-1105 3/14/2016 Sr-90 7,740 8,560 3,260 - 13,500 Pass ERSO-1105 3/14/2016 Th-234 3,630 3,430 1,080 - 6,450 Pass ERSO-1105 3/14/2016 U-233/234 3,090 3,460 2,110 - 4,430 Pass ERSO-1105 3/14/2016 U-238 3,280 3,430 2,120 - 4,350 Pass ERSO-1105 3/14/2016 Zn-65 2,940 2,450 1,950 - 3,260 Pass ERW-1115 3/14/2016 Gr. Alpha 105.0 117.0 41.5 - 181.0 Pass ERW-1115 3/14/2016 Gr. Beta 76.2 75.5 43.2 - 112.0 Pass ERW-1117 3/14/2016 H-3 8,870 8,650 5,800 - 12,300 Pass A7-1

a TABLE A-7. Interlaboratory Comparison Crosscheck Program, Environmental Resource Associates (ERA) .

MRAD Study a

Concentration b

Lab Code Date Analysis Laboratory ERA Control Result Result Limits Acceptance ERVE-1108 3/14/2016 Am-241 1,930 2,120 1,300 - 2,820 Pass ERVE-1108 3/14/2016 Cm-244 1,294 1,560 764 - 2,430 Pass ERVE-1108 3/14/2016 Co-60 1,164 1,100 759 - 1,540 Pass ERVE-1108 3/14/2016 Cs-134 1,056 1,070 687 - 1,390 Pass ERVE-1108 3/14/2016 Cs-137 930 838 608 - 1,170 Pass ERVE-1108 3/14/2016 K-40 32,200 31,000 22,400 - 43,500 Pass ERVE-1108 3/14/2016 Mn-54 < 24.5 < 300 0.00 - 300 Pass ERVE-1108 3/14/2016 Zn-65 3,320 2,820 2,030 - 3,960 Pass ERVE-1108 3/14/2016 Pu-238 3,410 2,810 1,680 - 3,850 Pass ERVE-1108 3/14/2016 Pu-239/240 4,120 3,640 2,230 - 5,010 Pass ERVE-1108 3/14/2016 Sr-90 8,120 8,710 4,960 - 11,500 Pass ERVE-1108 3/14/2016 U-233/234 4,350 4,160 2,740 - 5,340 Pass ERVE-1108 3/14/2016 U-238 4,220 4,120 2,750 - 5,230 Pass ERW-1111 3/14/2016 Am-241 113 121 81.5 - 162 Pass ERW-1111 3/14/2016 Co-60 1,120 1,050 912 - 1,230 Pass ERW-1111 3/14/2016 Cs-134 806 842 618 - 968 Pass ERW-1111 3/14/2016 Cs-137 1,190 1,100 934 - 1,320 Pass ERW-1111 3/14/2016 Mn-54 < 5.89 < 100 0.00 - 100 Pass ERW-1111 3/14/2016 Pu-238 159 138 102 - 172 Pass ERW-1111 3/14/2016 Pu-239/240 113 98.7 76.6 - 124 Pass ERW-1111 3/14/2016 U-233/234 46.9 52.7 39.6 - 68.0 Pass ERW-1111 3/14/2016 U-238 50.4 52.3 39.9 - 64.2 Pass ERW-1111 3/14/2016 Zn-65 1,160 1,010 842 - 1,270 Pass ERW-1111 3/14/2016 Fe-55 1,600 1,650 984 - 2,240 Pass ERW-1111 3/14/2016 Sr-90 430 434 283 - 574 Pass a

Results obtained by Environmental, Inc., Midwest Laboratory as a participant in the crosscheck program for proficiency testing administered by Environmental Resources Associates, serving as a replacement for studies conducted previously by the Environmental Measurements Laboratory Quality Assessment Program (EML).

b Laboratory codes as follows: ERW (water), ERAP (air filter), ERSO (soil), ERVE (vegetation). Results are reported in units of pCi/L, except for air filters (pCi/Filter), vegetation and soil (pCi/kg).

c Results are presented as the known values, expected laboratory precision (1 sigma, 1 determination) and control limits as provided by ERA.

A7-2

APPENDIX B. DATA REPORTING CONVENTIONS Data Reporting Conventions 1.0. All activities, except gross alpha and gross beta, are decay corrected to collection time or the end of the collection period.

2.0. Single Measurements Each single measurement is reported as follows: x+/-s where: x = value of the measurement; s = 2 counting uncertainty (corresponding to the 95% confidence level).

In cases where the activity is less than the lower limit of detection L, it is reported as: < L, where L = the lower limit of detection based on 4.66 uncertainty for a background sample.

3.0. Duplicate analyses If duplicate analyses are reported, the convention is as follows. :

3.1 Individual results: For two analysis results; x1 +/- s1 and x2 +/- s2 Reported result: x +/- s; where x = (1/2) (x1 + x2) and s = (1/2) s12 + s 22 3.2. Individual results: < L1 , < L2 Reported result: < L, where L = lower of L1 and L2 3.3. Individual results: x +/- s, < L Reported result: x +/- s if x L; < L otherwise.

4.0. Computation of Averages and Standard Deviations 4.1 Averages and standard deviations listed in the tables are computed from all of the individual measurements over the period averaged; for example, an annual standard deviation would not be the average of quarterly standard deviations. The average and standard deviation s of a set of n numbers x1, x2 . . . xn are defined as follows:

1 (x- )2

=n x s= n-1 4.2 Values below the highest lower limit of detection are not included in the average.

4.3 If all values in the averaging group are less than the highest LLD, the highest LLD is reported.

4.4 If all but one of the values are less than the highest LLD, the single value x and associated two sigma error is reported.

4.5 In rounding off, the following rules are followed:

4.5.1. If the number following those to be retained is less than 5, the number is dropped, and the retained numbers are kept unchanged. As an example, 11.443 is rounded off to 11.44.

4.5.2. If the number following those to be retained is equal to or greater than 5, the number is dropped and the last retained number is raised by 1. As an example, 11.445 is rounded off to 11.45.

B-1

Appendix C. NON-RADIOLOGICAL MONITORING PROGRAM 1.0. Introduction Union Electric Company Callaway Plant, d.b.a. Ameren Missouri Callaway Energy Center, in accordance with federal regulations and a desire to maintain the quality of the local environment around Callaway Plant has implemented an Environmental Protection Plan, (EPP) contained in Appendix B of the Callaway Plant Operating License.

The objective of the EPP is to provide for protection of non-radiological environmental values during operation of the Callaway Plant.

This report describes the conduct of the EPP for the Callaway Plant during 2016.

2.0. Unusual or Important Events No unusual or important events reportable under the EPP Section 4.1 were identified during 2016.

3.0. EPP Non-compliances During 2016, there were no non-compliances with the EPP.

4.0. Nonroutine Reports There were no nonroutine reports submitted in accordance with the EPP, Section 5.4.2 in 2016.

C-1

5.0. Plant Design and Operation Environmental Evaluations.

This section lists all changes in the plant design, operation, tests or experiments installed during 2016, which could have involved a potentially significant unreviewed environmental question in accordance with section 3.1 of Appendix B.

During 2016, three plant changes could have involved a potentially significant unreviewed environmental question. The interpretations and conclusions regarding these plant changes along with a description of the change and activity are presented below.

MP 15-0004, MP 15-0011, MP 15-0012, MP 13-0033 - Construction of the New Hardened Condensate Storage Tank Description of Change:

Modifications MP 15-0004, MP 15-0011, MP 15-0012, and MP 13-0033 include all construction and connections associated with the new Hardened Condensate Storage Tank (HCST) at Callaway Energy Center. This evaluation includes a review of the modification packages for this work as follows:

MP 15-0004 - Demolition and excavation work for placement of the new HCST MP 15-0011 - Construction of the foundation and underground piping MP 15-0012 - Construction of the tank, protective barrier system, valve house, & electrical MP 13-0033 - Connections to balance of plant equipment The 500,000 gallon stainless steel HCST was constructed on a 5.5 foot thick concrete slab, surrounded by a protective structural steel frame with a mesh barrier system to withstand a design basis accident. The foundation includes 64 drilled shafts to support the tank with 46 piers installed to a depth of 45 feet with a diameter of 3 feet and 18 piers installed to a depth of 60 feet. A 10 foot by 10 foot pipe trench was also excavated to route necessary stainless steel and fused high density polyethylene (HDPE) piping for connection to the existing secondary systems. Hydro excavation was used to remove backfill for the piping trench and connections to the current CST tunnel and turbine building.

The HCST will store demineralized water. All construction was completed within the protected area and near the existing power block.

Evaluation of Change:

As part of the Final Environmental Evaluation, both the ER and FES-OL were reviewed for any previously evaluated adverse environmental impacts and any new adverse environmental impacts not previously evaluated. No adverse environmental impacts were identified. All construction was completed within the protected area close to the power block in areas that had been previously disturbed. During construction storm water from this area was directed to two C-2

permanently permitted NPDES Outfalls. Therefore, this change does not involve an unreviewed environmental question and NRC approval is not required for this construction project.

MP 15-0018 - Replacement of Existing Transformer XPB218 at the Callaway Intake Facility Description of Change:

MP 15-0018 covers the replacement of the existing transformer XPB218 at the Callaway intake facility. The new transformer will contain 1667 gallons of refined mineral oil (approximately 588 gallons more than the original transformer). The original transformer was located above a permanent rock filled concrete pit to contain the total volume of oil should a leak develop. Rock will be removed from this pit to allow additional volume to contain the 1667 gallons should a leak occur in the new transformer. The containment pit will also contain a new double grating with an absorbent rock layer.

Evaluation of Change:

As part of the Final Environmental Evaluation, both the ER and FES-OL were reviewed for any previously evaluated adverse environmental impacts and any new adverse environmental impacts not previously evaluated. No adverse environmental impacts were identified. Although the replacement transformer will contain a larger volume on mineral oil, the concrete containment located under the transformer was redesigned to contain the entire volume of the new transformer. Therefore, should a leak develop, oil will be contained within the concrete pit and there is no increased risk of this oil being discharged to the Missouri River.

This change does not involve an unreviewed environmental question and NRC approval was not required.

RFR 201606690 - Use of BULAB 5011P a new Polymer/Coagulant Description of Change:

This change involves the use of BULAB 5011P (a new water soluble cationic polymer/coagulant) for removal of solids from makeup water withdrawn from the Missouri River.

This product will be utilized at the Water Treatment Plant (WTP) to treat makeup to plant raw water systems. Callaway was previously using BULAB 5013, Dimethyl Ammonium Chloride (DADMAC) a similar polymer/coagulant for solids removal. This change allows the use of either product or a blend of these two products to reduce solids carried to plant raw water systems.

As a result, it is expected that suspended solids will also be reduced in plant discharges from Outfalls 002 and 016. BULAB 5011P is a similar product to the current polymer but has a larger molecular weight. The new product is less toxic to aquatic life and will be used at the same treatment concentrations as previously used for BULAB 5013.

C-3

Evaluation of Change:

As part of the Final Environmental Evaluation, both the ER and FES-OL were reviewed for any previously evaluated adverse environmental impacts and any new adverse environmental impacts not previously evaluated. No adverse environmental impacts were identified. Missouri DNR approval or permit changes were not required as similar coagulants/ organic polymers were previously approved by the state. In addition, use of coagulants/organic polymers at the WTP was included in the last Callaway NPDES Permit re-application. Both products contain a similar water soluble cationic polymer which will be maintained at the same concentration range.

Aquatic toxicity data was reviewed for both BULAB products and BULAB 5011P was found to have a less toxic 48-hour LC50 and 96 hour0.00111 days <br />0.0267 hours <br />1.587302e-4 weeks <br />3.6528e-5 months <br /> LC50 than BULAB 5013. Therefore, use of BULAB 5011P for solids removal at the WTP should have no adverse effect on the environment.

This evaluation concluded that this change to utilize BULAB 5011P as a coagulant for solids removal at the WTP does not involve an unreviewed environmental question and NRC approval was not required.

C-4

APPENDIX D Sampling Location Maps D-1

Figure D-1. Radiological Environmental Sampling Locations 1, 2, 3, mile radius from site location.

D-2

Figure D-2. Radiological Environmental Sampling Locations 3, 4, 5, 6 mile radius from site location.

D-3

Figure D-3. Radiological Environmental Sampling Locations 5, 10, 15 mile radius from site location.

D-4

Figure D-4. Non-Potable Groundwater Monitoring Wells, 600 ft radius from Site.

D-5

Figure D-5. Non-Potable Groundwater Monitoring Wells Collection.

D-6

AMEREN MISSOURI, CALLAWAY ENERGY CENTER FULTON, MISSOURI Docket Numbers 50-483 and 72-1045 ANNUAL RADIOLOGICAL ENVIRONMENTAL OPERATING REPORT to THE UNITED STATES NUCLEAR REGULATORY COMMISSION Part II DATA TABULATIONS AND ANALYSES January 1 to December 31, 2016 Prepared by ENVIRONMENTAL, Inc.

Midwest Laboratory Submitted by Union Electric Co.

dba Ameren Missouri Project No. 8036 TABLE OF CONTENTS

Section Page List of Tables ............................................................................................................... iii 1.0 Introduction................................................................................................................... iv 2.0 Data Tables ................................................................................................................... v ii

LIST OF TABLES No. Title Page 1 Airborne particulates and charcoal cartridges, analysis for gamma-emitting isotopes, and iodine-131 ....................................................................................... 1-1 2 Milk, analysis for iodine-131 and gamma emitting isotopes................................................ 2-1 3 Vegetation, analysis for iodine-131 and gamma emitting isotopes ..................................... 3-1 4 Non-food Crops, analysis for tritium and gamma emitting isotopes.................................... 4-1 5 Soil, analysis for gamma-emitting isotopes......................................................................... 5-1 6 Surface water, analysis for tritium and gamma-emitting isotopes....................................... 6-1 7 Surface water (Ponds), analysis for tritium and gamma-emitting isotopes ......................... 7-1 8 Drinking water, analysis for tritium and gamma-emitting isotopes ...................................... 8-1 9 Wells (non-potable water), analysis for tritium and gamma-emitting isotopes .................... 9-1 10 Sediment 10a. Bottom sediment, analysis for gamma-emitting isotopes .................................................. 10-1 10b. Shoreline sediment, analysis for gamma-emitting isotopes .............................................. 10-2 11 Fish, analysis for gamma-emitting isotopes ...................................................................... 11-1 12 Direct Radiation 12a. Gamma dose .................................................................................................................... 12-1 12b. Neutron dose .................................................................................................................... 12-2 iii

1.0 INTRODUCTION

The following constitutes a supplement to the Annual Report for the Radiological Environmental Monitoring Program conducted at the Ameren Missouri, Callaway Energy Center, Fulton, Missouri in 2016. Results of completed analyses are presented in the attached tables.

For information regarding sampling locations, type and frequency of collection, and sample codes, refer to Part I, Tables 5.1 - 5.2 and Figures 5.1 through 5.8.

Analyses results from additional sampling may be found in Appendix A.

iv

2.0 DATA TABLES v

Table 1. Air particulates and charcoal cartridges, analyses for gamma-emitting isotopes and I-131a.

Collection: Continuous, weekly exchange.

3 Units: pCi/m Location CA-A-001 7 58 60 95 134 137 140 144 Be Co Co Zr Cs Cs BaLa Ce Required LLDs - - - - 0.050 0.060 - -

Date Collected Vol.

01-08-16 290 < 0.10 < 0.005 < 0.005 < 0.014 < 0.008 < 0.007 < 0.009 < 0.041 01-15-16 279 < 0.14 < 0.011 < 0.012 < 0.020 < 0.012 < 0.006 < 0.037 < 0.064 01-22-16 277 < 0.09 < 0.008 < 0.008 < 0.017 < 0.010 < 0.006 < 0.016 < 0.051 01-29-16 302 < 0.10 < 0.008 < 0.005 < 0.016 < 0.009 < 0.009 < 0.007 < 0.046 02-04-16 294 < 0.09 < 0.004 < 0.005 < 0.015 < 0.009 < 0.009 < 0.006 < 0.046 02-11-16 291 < 0.10 < 0.009 < 0.005 < 0.017 < 0.010 < 0.011 < 0.020 < 0.052 02-18-16 290 < 0.10 < 0.007 < 0.003 < 0.013 < 0.009 < 0.007 < 0.010 < 0.037 02-25-16 306 < 0.10 < 0.010 < 0.008 < 0.013 < 0.008 < 0.005 < 0.015 < 0.039 03-03-16 307 0.23 +/- 0.09 < 0.005 < 0.005 < 0.014 < 0.009 < 0.006 < 0.018 < 0.032 03-10-16 306 < 0.09 < 0.004 < 0.009 < 0.010 < 0.005 < 0.009 < 0.017 < 0.027 03-17-16 311 < 0.08 < 0.008 < 0.006 < 0.012 < 0.008 < 0.008 < 0.013 < 0.032 03-24-16 307 < 0.08 < 0.008 < 0.005 < 0.010 < 0.009 < 0.007 < 0.006 < 0.037 03-31-16 307 0.18 +/- 0.09 < 0.005 < 0.008 < 0.012 < 0.009 < 0.006 < 0.014 < 0.041 04-07-16 314 0.18 +/- 0.08 < 0.007 < 0.007 < 0.008 < 0.008 < 0.005 < 0.008 < 0.031 04-14-16 303 0.19 +/- 0.09 < 0.009 < 0.009 < 0.012 < 0.010 < 0.007 < 0.015 < 0.038 04-21-16 311 < 0.13 < 0.006 < 0.005 < 0.014 < 0.009 < 0.010 < 0.015 < 0.038 04-28-16 310 < 0.13 < 0.006 < 0.005 < 0.018 < 0.009 < 0.008 < 0.017 < 0.046 05-05-16 305 < 0.09 < 0.007 < 0.007 < 0.008 < 0.010 < 0.011 < 0.009 < 0.049 05-12-16 312 < 0.14 < 0.006 < 0.008 < 0.017 < 0.010 < 0.007 < 0.038 < 0.036 05-19-16 309 0.21 +/- 0.10 < 0.007 < 0.005 < 0.016 < 0.010 < 0.010 < 0.019 < 0.045 05-26-16 316 0.19 +/- 0.10 < 0.006 < 0.005 < 0.015 < 0.009 < 0.006 < 0.016 < 0.042 06-02-16 316 0.26 +/- 0.13 < 0.007 < 0.006 < 0.008 < 0.006 < 0.007 < 0.015 < 0.031 06-09-16 317 0.20 +/- 0.12 < 0.006 < 0.003 < 0.014 < 0.008 < 0.005 < 0.017 < 0.033 06-16-16 317 < 0.11 < 0.008 < 0.005 < 0.012 < 0.007 < 0.005 < 0.035 < 0.047 06-23-16 317 < 0.15 < 0.007 < 0.007 < 0.011 < 0.010 < 0.010 < 0.025 < 0.044 06-30-16 317 0.17 +/- 0.07 < 0.006 < 0.005 < 0.015 < 0.009 < 0.008 < 0.011 < 0.041 07-07-16 316 < 0.13 < 0.005 < 0.006 < 0.018 < 0.008 < 0.009 < 0.016 < 0.051 07-14-16 319 < 0.15 < 0.010 < 0.003 < 0.015 < 0.008 < 0.006 < 0.045 < 0.039 07-21-16 318 < 0.10 < 0.005 < 0.003 < 0.012 < 0.008 < 0.008 < 0.019 < 0.029 07-28-16 284 < 0.15 < 0.009 < 0.006 < 0.014 < 0.010 < 0.011 < 0.031 < 0.061 08-04-16 297 0.10 +/- 0.05 < 0.005 < 0.004 < 0.014 < 0.006 < 0.005 < 0.007 < 0.024 08-11-16 298 < 0.11 < 0.015 < 0.008 < 0.016 < 0.009 < 0.010 < 0.022 < 0.044 08-18-16 304 < 0.12 < 0.010 < 0.008 < 0.017 < 0.010 < 0.008 < 0.019 < 0.041 08-25-16 309 0.18 +/- 0.10 < 0.007 < 0.007 < 0.015 < 0.009 < 0.007 < 0.014 < 0.027 08-31-16 261 0.14 +/- 0.08 < 0.006 < 0.010 < 0.009 < 0.008 < 0.005 < 0.013 < 0.036 09-08-16 354 < 0.09 < 0.007 < 0.005 < 0.009 < 0.007 < 0.007 < 0.010 < 0.039 09-15-16 310 < 0.11 < 0.011 < 0.006 < 0.017 < 0.009 < 0.005 < 0.041 < 0.035 09-22-16 310 0.21 +/- 0.10 < 0.005 < 0.005 < 0.016 < 0.007 < 0.008 < 0.018 < 0.033 09-29-16 306 0.20 +/- 0.10 < 0.006 < 0.008 < 0.018 < 0.008 < 0.006 < 0.010 < 0.035 a 3 Iodine-131 concentrations are < 0.07 pCi/m unless noted otherwise.

1-1

Table 1. Air particulates and charcoal cartridges, analyses for gamma-emitting isotopes and I-131a.

Collection: Continuous, weekly exchange.

3 Units: pCi/m Location CA-A-001 (cont.)

7 58 60 95 134 137 140 144 Be Co Co Zr Cs Cs BaLa Ce Required LLDs - - - - 0.050 0.060 - -

Date Collected Vol.

10-06-16 311 < 0.12 < 0.010 < 0.005 < 0.016 < 0.010 < 0.009 < 0.083 < 0.049 10-13-16 313 0.18 +/- 0.10 < 0.006 < 0.007 < 0.017 < 0.009 < 0.009 < 0.075 < 0.037 10-21-16 351 < 0.11 < 0.008 < 0.007 < 0.016 < 0.007 < 0.003 < 0.039 < 0.031 10-27-16 264 < 0.11 < 0.009 < 0.008 < 0.015 < 0.010 < 0.010 < 0.057 < 0.054 11-03-16 312 < 0.11 < 0.011 < 0.006 < 0.015 < 0.008 < 0.008 < 0.041 < 0.048 11-10-16 311 < 0.12 < 0.010 < 0.008 < 0.021 < 0.011 < 0.008 < 0.058 < 0.050 11-17-16 307 < 0.14 < 0.007 < 0.008 < 0.014 < 0.009 < 0.008 < 0.060 < 0.040 11-23-16 256 < 0.11 < 0.014 < 0.009 < 0.030 < 0.010 < 0.011 < 0.052 < 0.053 12-01-16 346 < 0.10 < 0.006 < 0.010 < 0.023 < 0.012 < 0.006 < 0.037 < 0.052 12-08-16 300 < 0.07 < 0.008 < 0.009 < 0.013 < 0.008 < 0.007 < 0.017 < 0.043 12-16-16 324 < 0.09 < 0.013 < 0.008 < 0.016 < 0.009 < 0.006 < 0.032 < 0.039 12-22-16 239 0.19 +/- 0.11 < 0.008 < 0.009 < 0.014 < 0.009 < 0.006 < 0.021 < 0.055 12-29-16 301 < 0.10 < 0.008 < 0.010 < 0.007 < 0.008 < 0.005 < 0.017 < 0.047 a 3 Iodine-131 concentrations are < 0.07 pCi/m unless noted otherwise.

1-2

Table 1. Air particulates and charcoal cartridges, analyses for gamma-emitting isotopes and I-131a.

Collection: Continuous, weekly exchange.

3 Units: pCi/m Location CA-A-007 7 58 60 95 134 137 140 144 Be Co Co Zr Cs Cs BaLa Ce Required LLDs - - - - 0.050 0.060 - -

Date Collected Vol.

01-08-16 283 < 0.10 < 0.007 < 0.007 < 0.018 < 0.010 < 0.009 < 0.016 < 0.052 01-15-16 276 < 0.14 < 0.010 < 0.006 < 0.026 < 0.011 < 0.009 < 0.016 < 0.032 01-22-16 283 0.20 +/- 0.09 < 0.007 < 0.004 < 0.022 < 0.008 < 0.005 < 0.010 < 0.048 01-29-16 300 < 0.10 < 0.007 < 0.005 < 0.015 < 0.009 < 0.005 < 0.008 < 0.029 02-04-16 290 < 0.11 < 0.012 < 0.009 < 0.018 < 0.013 < 0.012 < 0.009 < 0.038 02-11-16 288 < 0.10 < 0.006 < 0.006 < 0.012 < 0.009 < 0.007 < 0.012 < 0.039 02-18-16 288 < 0.08 < 0.008 < 0.003 < 0.014 < 0.008 < 0.006 < 0.013 < 0.039 02-25-16 287 < 0.11 < 0.010 < 0.006 < 0.016 < 0.011 < 0.008 < 0.016 < 0.048 03-03-16 294 < 0.10 < 0.005 < 0.007 < 0.014 < 0.008 < 0.007 < 0.017 < 0.046 03-10-16 289 0.12 +/- 0.07 < 0.010 < 0.005 < 0.009 < 0.010 < 0.006 < 0.008 < 0.056 03-17-16 291 < 0.11 < 0.005 < 0.005 < 0.015 < 0.010 < 0.006 < 0.010 < 0.049 03-24-16 290 0.14 +/- 0.06 < 0.009 < 0.004 < 0.019 < 0.009 < 0.006 < 0.017 < 0.036 03-31-16 290 0.21 +/- 0.12 < 0.010 < 0.006 < 0.013 < 0.010 < 0.009 < 0.010 < 0.059 04-07-16 286 < 0.11 < 0.004 < 0.007 < 0.016 < 0.010 < 0.008 < 0.016 < 0.030 04-14-16 286 0.27 +/- 0.12 < 0.007 < 0.004 < 0.015 < 0.010 < 0.007 < 0.011 < 0.045 04-21-16 279 < 0.11 < 0.009 < 0.009 < 0.017 < 0.010 < 0.006 < 0.013 < 0.048 04-28-16 285 0.20 +/- 0.10 < 0.005 < 0.007 < 0.016 < 0.010 < 0.011 < 0.009 < 0.044 05-05-16 282 < 0.09 < 0.009 < 0.006 < 0.010 < 0.009 < 0.009 < 0.006 < 0.048 05-12-16 283 < 0.12 < 0.006 < 0.012 < 0.021 < 0.009 < 0.011 < 0.042 < 0.060 05-19-16 291 0.19 +/- 0.10 < 0.007 < 0.006 < 0.016 < 0.010 < 0.008 < 0.013 < 0.038 05-26-16 290 0.21 +/- 0.11 < 0.004 < 0.008 < 0.016 < 0.008 < 0.007 < 0.032 < 0.056 06-02-16 284 0.20 +/- 0.12 < 0.006 < 0.007 < 0.019 < 0.010 < 0.010 < 0.015 < 0.055 06-09-16 281 0.21 +/- 0.10 < 0.011 < 0.006 < 0.016 < 0.010 < 0.005 < 0.035 < 0.034 06-16-16 281 0.24 +/- 0.12 < 0.006 < 0.006 < 0.015 < 0.008 < 0.006 < 0.014 < 0.038 06-23-16 277 0.17 +/- 0.10 < 0.010 < 0.007 < 0.023 < 0.012 < 0.008 < 0.028 < 0.044 06-30-16 277 0.19 +/- 0.10 < 0.009 < 0.003 < 0.011 < 0.008 < 0.007 < 0.015 < 0.034 07-07-16 275 < 0.11 < 0.008 < 0.004 < 0.021 < 0.010 < 0.006 < 0.045 < 0.046 07-14-16 257 < 0.14 < 0.007 < 0.010 < 0.016 < 0.010 < 0.007 < 0.048 < 0.040 07-21-16 275 0.20 +/- 0.09 < 0.008 < 0.005 < 0.019 < 0.010 < 0.008 < 0.033 < 0.043 07-28-16 275 < 0.16 < 0.016 < 0.010 < 0.026 < 0.009 < 0.011 < 0.071 < 0.039 08-04-16 272 < 0.08 < 0.004 < 0.006 < 0.011 < 0.008 < 0.007 < 0.008 < 0.027 08-11-16 268 < 0.19 < 0.011 < 0.010 < 0.034 < 0.010 < 0.010 < 0.079 < 0.045 08-18-16 269 < 0.13 < 0.015 < 0.009 < 0.021 < 0.009 < 0.010 < 0.019 < 0.052 08-25-16 267 < 0.11 < 0.007 < 0.008 < 0.016 < 0.010 < 0.009 < 0.013 < 0.053 08-31-16 226 < 0.15 < 0.010 < 0.012 < 0.021 < 0.013 < 0.010 < 0.014 < 0.057 09-08-16 304 < 0.11 < 0.005 < 0.008 < 0.018 < 0.010 < 0.010 < 0.051 < 0.052 09-15-16 263 0.17 +/- 0.10 < 0.007 < 0.009 < 0.014 < 0.006 < 0.008 < 0.055 < 0.031 09-22-16 261 < 0.12 < 0.006 < 0.006 < 0.014 < 0.009 < 0.010 < 0.040 < 0.039 09-29-16 258 < 0.11 < 0.007 < 0.009 < 0.014 < 0.009 < 0.007 < 0.048 < 0.037 a 3 Iodine-131 concentrations are < 0.07 pCi/m unless noted otherwise.

1-3

Table 1. Air particulates and charcoal cartridges, analyses for gamma-emitting isotopes and I-131a.

Collection: Continuous, weekly exchange.

3 Units: pCi/m Location CA-A-007 (cont.)

7 58 60 95 134 137 140 144 Be Co Co Zr Cs Cs BaLa Ce Required LLDs - - - - 0.050 0.060 - -

Date Collected Vol.

10-06-16 254 < 0.14 < 0.011 < 0.008 < 0.018 < 0.011 < 0.011 < 0.086 < 0.051 10-13-16 253 < 0.14 < 0.008 < 0.006 < 0.014 < 0.011 < 0.009 < 0.036 < 0.061 10-21-16 279 < 0.12 < 0.007 < 0.008 < 0.020 < 0.010 < 0.010 < 0.072 < 0.049 10-27-16 211 < 0.18 < 0.009 < 0.008 < 0.023 < 0.012 < 0.008 < 0.093 < 0.050 11-03-16 245 0.23 +/- 0.13 < 0.012 < 0.010 < 0.017 < 0.011 < 0.010 < 0.067 < 0.059 11-10-16 241 < 0.13 < 0.009 < 0.010 < 0.016 < 0.011 < 0.008 < 0.096 < 0.047 11-17-16 239 < 0.14 < 0.007 < 0.007 < 0.021 < 0.012 < 0.012 < 0.024 < 0.071 11-23-16 196 < 0.18 < 0.009 < 0.009 < 0.023 < 0.011 < 0.015 < 0.029 < 0.057 12-01-16 241 < 0.10 < 0.006 < 0.012 < 0.022 < 0.011 < 0.012 < 0.061 < 0.058 12-08-16 265 < 0.11 < 0.012 < 0.009 < 0.015 < 0.008 < 0.006 < 0.026 < 0.055 12-16-16 301 < 0.10 < 0.006 < 0.009 < 0.018 < 0.010 < 0.007 < 0.019 < 0.031 12-22-16 224 < 0.12 < 0.014 < 0.011 < 0.021 < 0.012 < 0.007 < 0.025 < 0.052 12-29-16 263 < 0.11 < 0.004 < 0.008 < 0.019 < 0.010 < 0.009 < 0.009 < 0.049 a 3 Iodine-131 concentrations are < 0.07 pCi/m unless noted otherwise.

1-4

Table 1. Air particulates and charcoal cartridges, analyses for gamma-emitting isotopes and I-131a.

Collection: Continuous, weekly exchange.

3 Units: pCi/m Location CA-A-008 7 58 60 95 134 137 140 144 Be Co Co Zr Cs Cs BaLa Ce Required LLDs - - - - 0.050 0.060 - -

Date Collected Vol.

01-08-16 238 < 0.13 < 0.006 < 0.008 < 0.022 < 0.010 < 0.009 < 0.040 < 0.058 01-15-16 230 < 0.11 < 0.004 < 0.006 < 0.014 < 0.010 < 0.011 < 0.012 < 0.047 01-22-16 268 0.14 +/- 0.08 < 0.003 < 0.008 < 0.014 < 0.008 < 0.007 < 0.009 < 0.045 01-29-16 288 < 0.10 < 0.007 < 0.006 < 0.016 < 0.009 < 0.011 < 0.009 < 0.038 02-04-16 270 < 0.09 < 0.009 < 0.010 < 0.016 < 0.009 < 0.005 < 0.010 < 0.037 02-11-16 273 < 0.12 < 0.005 < 0.006 < 0.015 < 0.010 < 0.009 < 0.012 < 0.069 02-18-16 271 < 0.13 < 0.010 < 0.008 < 0.016 < 0.009 < 0.009 < 0.031 < 0.051 02-25-16 278 0.14 +/- 0.08 < 0.005 < 0.005 < 0.013 < 0.010 < 0.005 < 0.031 < 0.058 03-03-16 280 0.16 +/- 0.10 < 0.010 < 0.009 < 0.010 < 0.009 < 0.008 < 0.019 < 0.031 03-10-16 274 < 0.13 < 0.009 < 0.005 < 0.016 < 0.010 < 0.009 < 0.009 < 0.042 03-17-16 279 < 0.10 < 0.007 < 0.008 < 0.009 < 0.010 < 0.007 < 0.016 < 0.038 03-24-16 273 0.13 +/- 0.07 < 0.004 < 0.006 < 0.010 < 0.007 < 0.007 < 0.010 < 0.022 03-31-16 275 < 0.12 < 0.008 < 0.010 < 0.017 < 0.011 < 0.008 < 0.016 < 0.047 04-07-16 278 0.16 +/- 0.09 < 0.004 < 0.007 < 0.016 < 0.008 < 0.006 < 0.016 < 0.033 04-14-16 269 < 0.15 < 0.006 < 0.006 < 0.014 < 0.011 < 0.006 < 0.028 < 0.047 04-21-16 271 < 0.16 < 0.011 < 0.005 < 0.018 < 0.009 < 0.010 < 0.019 < 0.058 04-28-16 273 0.20 +/- 0.09 < 0.008 < 0.007 < 0.021 < 0.010 < 0.010 < 0.010 < 0.053 05-05-16 268 < 0.10 < 0.004 < 0.005 < 0.017 < 0.010 < 0.007 < 0.016 < 0.052 05-12-16 272 < 0.14 < 0.005 < 0.010 < 0.017 < 0.010 < 0.007 < 0.041 < 0.048 05-19-16 271 < 0.12 < 0.007 < 0.013 < 0.012 < 0.011 < 0.006 < 0.019 < 0.067 05-26-16 277 < 0.13 < 0.010 < 0.007 < 0.015 < 0.009 < 0.008 < 0.019 < 0.037 06-02-16 278 < 0.12 < 0.009 < 0.006 < 0.014 < 0.009 < 0.009 < 0.020 < 0.061 06-09-16 281 < 0.17 < 0.012 < 0.006 < 0.018 < 0.011 < 0.011 < 0.053 < 0.066 06-16-16 285 0.17 +/- 0.09 < 0.010 < 0.009 < 0.013 < 0.010 < 0.008 < 0.031 < 0.051 06-23-16 294 < 0.15 < 0.009 < 0.009 < 0.016 < 0.009 < 0.010 < 0.018 < 0.046 06-30-16 302 < 0.12 < 0.008 < 0.010 < 0.017 < 0.009 < 0.007 < 0.018 < 0.049 07-07-16 301 < 0.15 < 0.008 < 0.008 < 0.015 < 0.008 < 0.010 < 0.039 < 0.045 07-14-16 306 < 0.13 < 0.011 < 0.008 < 0.022 < 0.009 < 0.007 < 0.040 < 0.045 07-21-16 310 0.18 +/- 0.10 < 0.009 < 0.007 < 0.015 < 0.008 < 0.006 < 0.014 < 0.033 07-28-16 314 0.22 +/- 0.12 < 0.008 < 0.006 < 0.020 < 0.009 < 0.009 < 0.015 < 0.044 08-04-16 314 < 0.10 < 0.012 < 0.007 < 0.020 < 0.009 < 0.008 < 0.032 < 0.058 08-11-16 314 0.17 +/- 0.10 < 0.007 < 0.006 < 0.013 < 0.009 < 0.008 < 0.041 < 0.040 08-18-16 314 < 0.11 < 0.008 < 0.007 < 0.018 < 0.010 < 0.006 < 0.042 < 0.037 08-25-16 319 0.15 +/- 0.09 < 0.008 < 0.008 < 0.016 < 0.009 < 0.008 < 0.013 < 0.041 08-31-16 270 < 0.12 < 0.010 < 0.009 < 0.022 < 0.011 < 0.007 < 0.013 < 0.042 09-08-16 363 0.17 +/- 0.10 < 0.007 < 0.008 < 0.014 < 0.008 < 0.006 < 0.051 < 0.037 09-15-16 316 < 0.12 < 0.007 < 0.006 < 0.015 < 0.009 < 0.006 < 0.046 < 0.045 09-22-16 316 0.18 +/- 0.11 < 0.006 < 0.006 < 0.013 < 0.009 < 0.009 < 0.014 < 0.034 09-29-16 313 0.19 +/- 0.06 < 0.003 < 0.007 < 0.009 < 0.006 < 0.007 < 0.012 < 0.036 a 3 Iodine-131 concentrations are < 0.07 pCi/m unless noted otherwise.

1-5

Table 1. Air particulates and charcoal cartridges, analyses for gamma-emitting isotopes and I-131a.

Collection: Continuous, weekly exchange.

3 Units: pCi/m Location CA-A-008 (cont.)

7 58 60 95 134 137 140 144 Be Co Co Zr Cs Cs BaLa Ce Required LLDs - - - - 0.050 0.060 - -

Date Collected Vol.

10-06-16 312 < 0.12 < 0.009 < 0.009 < 0.014 < 0.008 < 0.006 < 0.069 < 0.044 10-13-16 312 < 0.14 < 0.011 < 0.008 < 0.015 < 0.010 < 0.009 < 0.084 < 0.043 10-21-16 349 < 0.09 < 0.004 < 0.006 < 0.010 < 0.007 < 0.005 < 0.053 < 0.054 10-27-16 263 < 0.12 < 0.008 < 0.008 < 0.015 < 0.011 < 0.010 < 0.069 < 0.034 11-03-16 308 0.23 +/- 0.12 < 0.008 < 0.008 < 0.014 < 0.010 < 0.010 < 0.052 < 0.029 11-10-16 284 < 0.12 < 0.011 < 0.007 < 0.019 < 0.010 < 0.009 < 0.094 < 0.032 11-17-16 282 < 0.14 < 0.012 < 0.007 < 0.018 < 0.010 < 0.008 < 0.072 < 0.051 11-23-16 232 < 0.12 < 0.006 < 0.009 < 0.020 < 0.013 < 0.010 < 0.071 < 0.053 12-01-16 310 < 0.11 < 0.009 < 0.009 < 0.012 < 0.009 < 0.006 < 0.055 < 0.039 12-08-16 265 < 0.11 < 0.010 < 0.007 < 0.013 < 0.009 < 0.008 < 0.023 < 0.053 12-16-16 293 < 0.09 < 0.008 < 0.007 < 0.017 < 0.010 < 0.007 < 0.021 < 0.046 12-22-16 217 < 0.14 < 0.012 < 0.012 < 0.018 < 0.013 < 0.012 < 0.020 < 0.056 12-29-16 267 0.18 +/- 0.10 < 0.014 < 0.010 < 0.011 < 0.011 < 0.007 < 0.019 < 0.047 a 3 Iodine-131 concentrations are < 0.07 pCi/m unless noted otherwise.

1-6

Table 1. Air particulates and charcoal cartridges, analyses for gamma-emitting isotopes and I-131a.

Collection: Continuous, weekly exchange.

3 Units: pCi/m Location CA-A-009 7 58 60 95 134 137 140 144 Be Co Co Zr Cs Cs BaLa Ce Required LLDs - - - - 0.050 0.060 - -

Date Collected Vol.

01-08-16 265 < 0.11 < 0.011 < 0.009 < 0.009 < 0.010 < 0.007 < 0.021 < 0.050 01-15-16 300 < 0.10 < 0.007 < 0.008 < 0.012 < 0.010 < 0.007 < 0.022 < 0.049 01-22-16 306 < 0.10 < 0.007 < 0.006 < 0.017 < 0.009 < 0.005 < 0.016 < 0.050 01-29-16 329 0.13 +/- 0.06 < 0.005 < 0.007 < 0.013 < 0.007 < 0.005 < 0.016 < 0.044 02-04-16 321 < 0.09 < 0.008 < 0.005 < 0.011 < 0.007 < 0.007 < 0.007 < 0.041 02-11-16 320 < 0.10 < 0.003 < 0.005 < 0.009 < 0.008 < 0.008 < 0.009 < 0.035 02-18-16 320 0.19 +/- 0.11 < 0.009 < 0.008 < 0.010 < 0.009 < 0.007 < 0.024 < 0.042 02-25-16 332 < 0.07 < 0.007 < 0.005 < 0.010 < 0.008 < 0.007 < 0.019 < 0.034 03-03-16 329 0.18 +/- 0.09 < 0.008 < 0.007 < 0.014 < 0.008 < 0.007 < 0.022 < 0.037 03-10-16 332 < 0.10 < 0.004 < 0.007 < 0.009 < 0.007 < 0.008 < 0.010 < 0.035 03-17-16 335 < 0.09 < 0.006 < 0.004 < 0.016 < 0.007 < 0.008 < 0.010 < 0.033 03-24-16 332 < 0.10 < 0.008 < 0.004 < 0.017 < 0.009 < 0.009 < 0.010 < 0.034 03-31-16 332 < 0.09 < 0.003 < 0.006 < 0.016 < 0.008 < 0.008 < 0.013 < 0.039 04-07-16 333 0.19 +/- 0.08 < 0.006 < 0.005 < 0.011 < 0.007 < 0.007 < 0.016 < 0.032 04-14-16 328 0.19 +/- 0.09 < 0.006 < 0.006 < 0.015 < 0.008 < 0.006 < 0.018 < 0.040 04-21-16 292 < 0.11 < 0.008 < 0.007 < 0.015 < 0.010 < 0.006 < 0.020 < 0.041 04-28-16 306 < 0.11 < 0.005 < 0.006 < 0.011 < 0.009 < 0.006 < 0.013 < 0.040 05-05-16 312 < 0.09 < 0.009 < 0.009 < 0.009 < 0.009 < 0.008 < 0.010 < 0.041 05-12-16 321 < 0.12 < 0.005 < 0.006 < 0.018 < 0.008 < 0.008 < 0.032 < 0.046 05-19-16 315 0.29 +/- 0.12 < 0.010 < 0.003 < 0.012 < 0.009 < 0.008 < 0.012 < 0.042 05-26-16 325 0.22 +/- 0.10 < 0.007 < 0.004 < 0.013 < 0.008 < 0.007 < 0.025 < 0.045 06-02-16 271 < 0.17 < 0.014 < 0.011 < 0.020 < 0.015 < 0.010 < 0.044 < 0.053 06-09-16 272 0.25 +/- 0.13 < 0.009 < 0.006 < 0.023 < 0.009 < 0.009 < 0.021 < 0.055 06-16-16 270 0.30 +/- 0.15 < 0.010 < 0.003 < 0.015 < 0.010 < 0.007 < 0.018 < 0.045 06-23-16 270 0.20 +/- 0.09 < 0.009 < 0.005 < 0.020 < 0.009 < 0.012 < 0.026 < 0.045 06-30-16 271 0.20 +/- 0.12 < 0.007 < 0.007 < 0.022 < 0.011 < 0.010 < 0.031 < 0.047 07-07-16 273 < 0.13 < 0.008 < 0.005 < 0.010 < 0.010 < 0.007 < 0.024 < 0.052 07-14-16 268 < 0.15 < 0.009 < 0.008 < 0.014 < 0.010 < 0.010 < 0.045 < 0.057 07-21-16 270 < 0.15 < 0.007 < 0.004 < 0.016 < 0.009 < 0.008 < 0.023 < 0.049 07-28-16 270 < 0.10 < 0.013 < 0.007 < 0.012 < 0.009 < 0.009 < 0.024 < 0.032 08-04-16 275 < 0.13 < 0.008 < 0.009 < 0.017 < 0.009 < 0.004 < 0.056 < 0.047 08-11-16 267 < 0.12 < 0.009 < 0.007 < 0.024 < 0.010 < 0.009 < 0.027 < 0.049 08-18-16 268 < 0.15 < 0.011 < 0.009 < 0.027 < 0.009 < 0.010 < 0.035 < 0.042 08-25-16 274 < 0.11 < 0.007 < 0.008 < 0.013 < 0.010 < 0.006 < 0.018 < 0.047 08-31-16 230 < 0.13 < 0.011 < 0.009 < 0.022 < 0.011 < 0.012 < 0.015 < 0.036 09-08-16 310 < 0.11 < 0.010 < 0.007 < 0.020 < 0.007 < 0.008 < 0.050 < 0.047 09-15-16 269 < 0.13 < 0.009 < 0.014 < 0.017 < 0.011 < 0.008 < 0.059 < 0.047 09-22-16 268 < 0.13 < 0.008 < 0.009 < 0.011 < 0.010 < 0.006 < 0.051 < 0.046 09-29-16 268 0.21 +/- 0.10 < 0.008 < 0.007 < 0.018 < 0.010 < 0.005 < 0.056 < 0.031 a 3 Iodine-131 concentrations are < 0.07 pCi/m unless noted otherwise.

1-7

Table 1. Air particulates and charcoal cartridges, analyses for gamma-emitting isotopes and I-131a.

Collection: Continuous, weekly exchange.

3 Units: pCi/m Location CA-A-009 (cont.)

7 58 60 95 134 137 140 144 Be Co Co Zr Cs Cs BaLa Ce Required LLDs - - - - 0.050 0.060 - -

Date Collected Vol.

10-06-16 269 < 0.13 < 0.008 < 0.009 < 0.026 < 0.010 < 0.008 < 0.075 < 0.032 10-13-16 272 < 0.12 < 0.011 < 0.007 < 0.013 < 0.010 < 0.009 < 0.045 < 0.053 10-21-16 303 < 0.13 < 0.005 < 0.007 < 0.022 < 0.010 < 0.004 < 0.067 < 0.028 10-27-16 230 < 0.14 < 0.010 < 0.011 < 0.025 < 0.010 < 0.010 < 0.086 < 0.037 11-03-16 267 0.23 +/- 0.11 < 0.010 < 0.009 < 0.013 < 0.010 < 0.010 < 0.063 < 0.035 11-10-16 273 < 0.13 < 0.015 < 0.006 < 0.017 < 0.009 < 0.010 < 0.045 < 0.036 11-17-16 269 < 0.12 < 0.006 < 0.008 < 0.017 < 0.010 < 0.009 < 0.077 < 0.056 11-23-16 224 < 0.16 < 0.010 < 0.011 < 0.020 < 0.014 < 0.012 < 0.038 < 0.063 12-01-16 300 0.18 +/- 0.10 < 0.010 < 0.008 < 0.013 < 0.009 < 0.007 < 0.047 < 0.055 12-08-16 283 < 0.10 < 0.010 < 0.008 < 0.016 < 0.010 < 0.007 < 0.021 < 0.044 12-16-16 342 0.19 +/- 0.09 < 0.006 < 0.006 < 0.011 < 0.007 < 0.005 < 0.010 < 0.047 12-22-16 258 0.28 +/- 0.14 < 0.010 < 0.011 < 0.015 < 0.011 < 0.009 < 0.020 < 0.053 12-29-16 289 < 0.11 < 0.010 < 0.007 < 0.015 < 0.009 < 0.007 < 0.009 < 0.050 a 3 Iodine-131 concentrations are < 0.07 pCi/m unless noted otherwise.

1-8

a Table 1. Air particulates and charcoal cartridges, analyses for gamma-emitting isotopes and I-131 .

Collection: Continuous, weekly exchange.

3 Units: pCi/m Location CA-B-003 7 58 60 95 134 137 140 144 Be Co Co Zr Cs Cs BaLa Ce Required LLDs - - - - 0.050 0.060 - -

Date Collected Vol.

01-08-16 265 < 0.12 < 0.007 < 0.003 < 0.015 < 0.008 < 0.004 < 0.015 < 0.054 01-15-16 256 < 0.09 < 0.005 < 0.005 < 0.020 < 0.010 < 0.010 < 0.029 < 0.033 01-22-16 256 < 0.12 < 0.005 < 0.007 < 0.013 < 0.008 < 0.007 < 0.008 < 0.039 01-29-16 268 < 0.11 < 0.005 < 0.003 < 0.017 < 0.009 < 0.007 < 0.009 < 0.050 02-04-16 268 < 0.11 < 0.010 < 0.008 < 0.022 < 0.011 < 0.006 < 0.017 < 0.063 02-11-16 262 < 0.13 < 0.005 < 0.007 < 0.017 < 0.009 < 0.009 < 0.018 < 0.046 02-18-16 258 < 0.11 < 0.007 < 0.008 < 0.019 < 0.010 < 0.010 < 0.031 < 0.035 02-25-16 272 < 0.09 < 0.008 < 0.005 < 0.011 < 0.010 < 0.011 < 0.027 < 0.063 03-03-16 272 < 0.12 < 0.010 < 0.007 < 0.016 < 0.009 < 0.007 < 0.014 < 0.061 03-10-16 271 0.17 +/- 0.10 < 0.008 < 0.009 < 0.015 < 0.010 < 0.006 < 0.016 < 0.029 03-17-16 281 < 0.10 < 0.008 < 0.011 < 0.016 < 0.013 < 0.012 < 0.015 < 0.035 03-24-16 274 < 0.12 < 0.011 < 0.010 < 0.018 < 0.010 < 0.011 < 0.026 < 0.050 03-31-16 274 0.17 +/- 0.10 < 0.011 < 0.008 < 0.013 < 0.008 < 0.009 < 0.021 < 0.038 04-07-16 276 0.19 +/- 0.10 < 0.006 < 0.005 < 0.019 < 0.009 < 0.007 < 0.019 < 0.053 04-14-16 270 < 0.12 < 0.007 < 0.006 < 0.011 < 0.008 < 0.008 < 0.023 < 0.042 04-21-16 280 < 0.11 < 0.010 < 0.009 < 0.018 < 0.009 < 0.009 < 0.017 < 0.050 04-28-16 281 < 0.13 < 0.009 < 0.005 < 0.011 < 0.009 < 0.007 < 0.015 < 0.032 05-05-16 276 < 0.09 < 0.005 < 0.006 < 0.014 < 0.010 < 0.010 < 0.012 < 0.038 05-12-16 280 < 0.14 < 0.005 < 0.007 < 0.023 < 0.011 < 0.011 < 0.035 < 0.052 05-19-16 276 < 0.12 < 0.012 < 0.010 < 0.019 < 0.012 < 0.010 < 0.021 < 0.060 05-26-16 283 < 0.17 < 0.006 < 0.006 < 0.011 < 0.010 < 0.010 < 0.027 < 0.052 06-02-16 283 < 0.12 < 0.006 < 0.007 < 0.016 < 0.009 < 0.010 < 0.022 < 0.046 06-09-16 286 < 0.16 < 0.007 < 0.009 < 0.010 < 0.009 < 0.006 < 0.029 < 0.052 06-16-16 286 0.24 +/- 0.12 < 0.007 < 0.006 < 0.017 < 0.010 < 0.006 < 0.024 < 0.049 06-23-16 286 < 0.16 < 0.005 < 0.008 < 0.019 < 0.010 < 0.009 < 0.024 < 0.058 06-30-16 291 < 0.12 < 0.008 < 0.005 < 0.014 < 0.009 < 0.006 < 0.021 < 0.039 07-07-16 258 < 0.14 < 0.011 < 0.005 < 0.023 < 0.011 < 0.008 < 0.033 < 0.050 07-14-16 250 < 0.22 < 0.015 < 0.012 < 0.029 < 0.015 < 0.011 < 0.104 < 0.073 07-21-16 254 < 0.12 < 0.010 < 0.004 < 0.018 < 0.010 < 0.005 < 0.031 < 0.033 07-28-16 258 < 0.13 < 0.010 < 0.007 < 0.017 < 0.010 < 0.007 < 0.024 < 0.067 08-04-16 255 < 0.15 < 0.012 < 0.007 < 0.022 < 0.010 < 0.010 < 0.034 < 0.034 08-11-16 246 < 0.14 < 0.010 < 0.008 < 0.016 < 0.011 < 0.006 < 0.035 < 0.045 08-18-16 276 0.25 +/- 0.12 < 0.009 < 0.009 < 0.016 < 0.009 < 0.009 < 0.050 < 0.040 08-25-16 285 < 0.11 < 0.009 < 0.009 < 0.016 < 0.009 < 0.007 < 0.016 < 0.055 08-31-16 241 < 0.12 < 0.014 < 0.010 < 0.019 < 0.012 < 0.013 < 0.016 < 0.049 09-08-16 328 0.20 +/- 0.10 < 0.003 < 0.007 < 0.015 < 0.008 < 0.005 < 0.045 < 0.024 09-15-16 286 < 0.12 < 0.009 < 0.011 < 0.015 < 0.009 < 0.008 < 0.056 < 0.048 09-22-16 288 0.20 +/- 0.09 < 0.008 < 0.005 < 0.010 < 0.008 < 0.004 < 0.020 < 0.041 09-29-16 288 < 0.13 < 0.005 < 0.006 < 0.022 < 0.010 < 0.007 < 0.037 < 0.044 a 3 Iodine-131 concentrations are < 0.07 pCi/m unless noted otherwise.

1-9

a Table 1. Air particulates and charcoal cartridges, analyses for gamma-emitting isotopes and I-131 .

Collection: Continuous, weekly exchange.

3 Units: pCi/m Location CA-B-003 (cont.)

7 58 60 95 134 137 140 144 Be Co Co Zr Cs Cs BaLa Ce Required LLDs - - - - 0.050 0.060 - -

Date Collected Vol.

10-06-16 290 < 0.13 < 0.006 < 0.005 < 0.016 < 0.008 < 0.009 < 0.070 < 0.036 10-13-16 294 0.19 +/- 0.10 < 0.012 < 0.007 < 0.022 < 0.010 < 0.006 < 0.079 < 0.042 10-21-16 327 < 0.10 < 0.008 < 0.007 < 0.018 < 0.008 < 0.005 < 0.058 < 0.034 10-27-16 251 < 0.12 < 0.011 < 0.011 < 0.021 < 0.012 < 0.009 < 0.078 < 0.038 11-03-16 298 0.24 +/- 0.12 < 0.005 < 0.010 < 0.012 < 0.008 < 0.010 < 0.054 < 0.025 11-10-16 300 0.21 +/- 0.09 < 0.006 < 0.009 < 0.021 < 0.007 < 0.005 < 0.058 < 0.033 11-17-16 299 < 0.11 < 0.009 < 0.007 < 0.011 < 0.007 < 0.006 < 0.062 < 0.043 11-23-16 249 < 0.13 < 0.010 < 0.011 < 0.014 < 0.010 < 0.012 < 0.069 < 0.059 12-01-16 336 < 0.10 < 0.010 < 0.006 < 0.014 < 0.007 < 0.009 < 0.025 < 0.049 12-08-16 290 < 0.06 < 0.005 < 0.008 < 0.018 < 0.010 < 0.009 < 0.026 < 0.043 12-16-16 324 < 0.09 < 0.006 < 0.006 < 0.014 < 0.008 < 0.004 < 0.013 < 0.047 12-22-16 246 0.22 +/- 0.13 < 0.007 < 0.012 < 0.025 < 0.011 < 0.010 < 0.019 < 0.054 12-28-16 269 0.23 +/- 0.13 < 0.008 < 0.011 < 0.021 < 0.010 < 0.007 < 0.011 < 0.046 a 3 Iodine-131 concentrations are < 0.07 pCi/m unless noted otherwise.

1-10

Table 2. Milk, analyses for iodine-131 and gamma-emitting isotopes.

Collection: Semimonthly during grazing season, monthly otherwise.

Units: pCi/L Location CA-MLK-M9 Date Lab Concentration (pCi/L)

Collected Code I-131 K-40 Zn-65 Cs-134 Cs-137 Ba-La-140 Required LLDs 1 - - 15 18 15 01-11-16 CAMI -191 < 0.3 849 +/- 43 < 3.4 < 1.8 < 1.7 < 2.1 02-09-16 CAMI -576 < 0.4 1124 +/- 101 < 6.2 < 3.2 < 3.1 < 3.0 03-08-16 CAMI -1005 < 0.3 1243 +/- 104 < 5.7 < 3.8 < 3.0 < 2.5 03-22-16 CAMI -1195 < 0.3 1135 +/- 91 < 5.4 < 3.2 < 2.9 < 1.8 04-11-16 CAMI -1537 < 0.3 947 +/- 84 < 4.4 < 3.0 < 4.1 < 1.7 04-25-16 CAMI -1954 < 0.4 1615 +/- 191 < 8.0 < 7.6 < 7.9 < 7.5 05-09-16 CAMI -2280 < 0.2 1308 +/- 124 < 4.7 < 2.9 < 3.5 < 2.4 05-23-16 CAMI -2617 < 0.5 1504 +/- 128 < 8.1 < 4.6 < 4.8 < 4.6 06-14-16 CAMI -2999 < 0.3 1375 +/- 119 < 6.2 < 4.0 < 3.4 < 2.0 06-28-16 CAMI -3247 < 0.2 1076 +/- 103 < 5.9 < 3.1 < 3.1 < 2.5 07-12-16 CAMI -3655 < 0.4 1405 +/- 124 < 3.7 < 3.6 < 4.4 < 3.7 07-26-16 CAMI -3969 < 0.3 1258 +/- 102 < 6.5 < 3.3 < 2.2 < 2.6 08-08-16 CAMI -4265 < 0.4 1370 +/- 114 < 4.5 < 4.1 < 4.4 < 2.6 08-22-16 CAMI -4471 < 0.5 1093 +/- 102 < 6.8 < 4.1 < 4.1 < 3.4 09-13-16 CAMI -4873 < 0.4 1095 +/- 152 < 6.3 < 7.6 < 4.7 < 5.7 09-26-16 CAMI -5130 < 0.4 1019 +/- 104 < 4.9 < 3.8 < 3.7 < 2.6 10-11-16 CAMI -5477 < 0.4 1105 +/- 127 < 5.6 < 4.7 < 5.4 < 2.0 10-24-16 CAMI -5858 < 0.3 1352 +/- 122 < 6.9 < 5.0 < 4.2 < 3.1 11-22-16 CAMI -6452 < 0.2 1122 +/- 108 < 8.7 < 4.9 < 3.9 < 2.3 12-13-16 CAMI -6793 < 0.2 1360 +/- 108 < 4.1 < 3.4 < 1.9 < 2.4 2-1

Table 3. Vegetation, analyses for iodine-131 and gamma-emitting isotopes.

Collection: Monthly, during growing season Units: pCi/kg wet Collection Concentration (pCi/kg wet) 40 54 58 60 131 134 137 Lab Code Date Sample Type K Mn Co Co I Cs Cs Location: CA-FPL-V9 a

5/9/2016 NS CAVE- 3000 6/14/2016 Lettuce 5821 +/- 328 < 10.3 < 9.0 < 7.0 < 22.2 < 9.4 < 10.2 CAVE- 3001 6/14/2016 Cabbage 4396 +/- 235 < 6.6 < 3.9 < 4.2 < 20.1 < 7.0 < 7.2 CAVE- 3002 6/14/2016 Mustard 4645 +/- 241 < 4.7 < 3.5 < 5.6 < 13.3 < 6.7 < 7.4 CAVE- 3003 6/14/2016 Swiss Chard 5878 +/- 342 < 6.7 < 4.9 < 7.0 < 12.4 < 7.5 < 8.1 CAVE- 3004 6/14/2016 Collard Greens 4028 +/- 284 < 5.1 < 8.6 < 7.0 < 20.4 < 8.9 < 9.1 CAVE- 3656 7/12/2016 Collard Greens 4088 +/- 298 < 9.3 < 9.2 < 9.6 < 33.2 < 7.6 < 8.2 CAVE- 3657 7/12/2016 Cabbage 4088 +/- 264 < 7.9 < 4.8 < 4.6 < 17.4 < 7.4 < 4.7 a

8/9/2016 NS CAVE- 4896 9/13/2016 Mustard Greens 3855 +/- 213 < 4.9 < 6.8 < 4.2 < 17.2 < 5.7 < 7.0 CAVE- 5486 10/11/2016 Collard Greens 3457 +/- 220 < 4.6 < 7.6 < 4.2 < 25.8 < 6.9 < 7.6 CAVE- 5487 10/11/2016 Mustard Greens 4111 +/- 237 < 4.1 < 5.5 < 4.1 < 26.5 < 6.4 < 5.6 Location: CA-FPL-V11 CAVE- 2281 5/9/2016 Lettuce 4741 +/- 364 < 9.4 < 8.0 < 7.2 < 17.1 < 8.9 < 10.0 CAVE- 2282 5/9/2016 Collard Greens 3504 +/- 247 < 6.4 < 7.3 < 7.2 < 12.6 < 6.9 < 7.0 CAVE- 3005 6/13/2016 Lettuce 6314 +/- 499 < 15.7 < 10.7 < 14.1 < 32.9 < 17.8 < 9.4 CAVE- 3006 6/13/2016 Collard Greens 4402 +/- 320 < 5.7 < 7.8 < 8.8 < 17.3 < 12.0 < 7.5 CAVE- 3658 7/12/2016 Collard Greens 3287 +/- 204 < 5.9 < 5.3 < 3.7 < 22.0 < 5.2 < 6.6 CAVE- 3659 7/12/2016 Cabbage 2103 +/- 177 < 5.2 < 6.6 < 4.6 < 14.9 < 5.5 < 5.4 CAVE- 4269 8/8/2016 Swiss Chard 4290 +/- 267 < 5.6 < 8.1 < 7.4 < 26.9 < 9.0 < 9.7 CAVE- 4270 8/8/2016 Collard Greens 3187 +/- 245 < 7.8 < 5.3 < 5.4 < 17.4 < 7.8 < 9.3 CAVE- 4897 9/13/2016 Collard Greens 3572 +/- 253 < 4.9 < 6.9 < 5.1 < 28.0 < 8.4 < 6.5 CAVE- 4898 9/13/2016 Kale 5845 +/- 392 < 7.5 < 8.0 < 11.6 < 37.0 < 11.4 < 6.6 a

"NS" = No sample; refer to Part I Table 5.5, Missed Collections and Analyses.

3-1

Table 3. Vegetation, analyses for iodine-131 and gamma-emitting isotopes.

Collection: Monthly, during growing season Units: pCi/kg wet Collection Concentration (pCi/kg wet) 40 54 58 60 131 134 137 Lab Code Date Sample Type K Mn Co Co I Cs Cs Location: CA-FPL-V12 CAVE- 2284 5/9/2016 Lettuce 4343 +/- 321 < 9.2 < 9.1 < 6.6 < 17.0 < 10.8 < 13.3 CAVE- 2285 5/9/2016 Mustard Greens 3464 +/- 408 < 13.6 < 10.8 < 7.3 < 27.8 < 14.5 < 7.9 CAVE- 2286 5/10/2016 Chard 5678 +/- 387 < 11.1 < 7.8 < 8.9 < 21.7 < 11.4 < 5.9 CAVE- 3007 6/14/2016 Swiss Chard 6694 +/- 310 < 5.5 < 6.0 < 8.6 < 13.6 < 7.1 < 9.6 CAVE- 3008 6/14/2016 Lettuce 4186 +/- 324 < 11.9 < 9.5 < 4.9 < 31.8 < 10.2 < 11.4 CAVE- 3009 6/14/2016 Cabbage 3204 +/- 235 < 5.4 < 6.1 < 4.9 < 14.7 < 9.6 < 10.5 CAVE- 3660 7/12/2016 Cabbage 3635 +/- 232 < 7.2 < 7.7 < 5.3 < 18.9 < 6.8 < 8.5 CAVE- 3661 7/12/2016 Chard 6434 +/- 314 < 6.1 < 8.8 < 6.3 < 15.9 < 8.2 < 10.4 CAVE- 3662 7/12/2016 Lettuce 6983 +/- 358 < 8.6 < 8.6 < 9.1 < 24.5 < 8.4 < 8.4 CAVE- 4271 8/8/2016 Swiss Chard 4879 +/- 312 < 4.6 < 9.5 < 5.3 < 23.1 < 8.9 < 8.5 CAVE- 4899 9/13/2016 Swiss Chard 5836 +/- 369 < 10.3 < 6.8 < 7.8 < 38.5 < 9.0 < 10.4 CAVE- 5488 10/11/2016 Swiss Chard 5806 +/- 397 < 12.3 < 12.4 < 8.5 < 45.9 < 10.3 < 8.8 Location: CA-FPL-V16 CAVE- 2287 5/10/2016 Lettuce 5112 +/- 406 < 8.3 < 12.3 < 11.6 < 21.5 < 10.9 < 11.4 CAVE- 2288 5/10/2016 Turnip greens 6433 +/- 488 < 12.4 < 7.6 < 10.4 < 27.1 < 13.5 < 13.8 CAVE- 3010 6/13/2016 Lettuce 7800 +/- 415 < 15.3 < 11.2 < 12.3 < 21.6 < 14.8 < 16.4 CAVE- 3011 6/13/2016 Turnip Greens 9059 +/- 634 < 19.8 < 10.5 < 18.6 < 45.2 < 20.7 < 28.2 CAVE- 3013 6/13/2016 Mustard 9782 +/- 699 < 21.5 < 22.7 < 24.8 < 37.4 < 22.5 < 22.1 CAVE- 3136 6/13/2016 Collard Greens 6241 +/- 419 < 14.9 < 13.1 < 7.8 < 18.8 < 11.4 < 11.9 CAVE- 3663 7/12/2016 Lettuce 3682 +/- 117 < 4.4 < 3.8 < 4.7 < 6.0 < 3.6 < 3.1 CAVE- 4272 8/8/2016 Collard Greens 6935 +/- 340 < 10.0 < 5.1 < 6.2 < 17.3 < 8.9 < 7.1 CAVE- 4273 8/8/2016 Lettuce 7567 +/- 602 < 30.3 < 19.5 < 23.1 < 55.0 < 28.6 < 31.1 CAVE- 4900 9/13/2016 Collard Greens 8228 +/- 836 < 23.2 < 29.1 < 15.4 < 31.2 < 22.4 < 24.9 3-2

Table 4. Non-food Crops, analyses for tritium and gamma-emitting isotopes.

Collection: Annually, at harvest Units: pCi/kg wet Sample Collection (pCi/L) Concentration (pCi/kg wet) 3 40 54 58 60 134 137 Lab Code Type Date H K Mn Co Co Cs Cs Location: CA-FC-1 a

9/12/2016 NS a

9/12/2016 NS a

9/12/2016 NS Location: CA-FC-2 CAVE- 4884 1-Soybeans 9/12/2016 < 152 5414 +/- 385 < 9.3 < 6.7 < 10.3 < 9.7 < 10.3 CAVE- 4885 2-Soybeans 9/12/2016 < 152 5857 +/- 448 < 10.1 < 15.4 < 10.2 < 12.3 < 11.6 CAVE- 4886 3-Soybeans 9/12/2016 < 152 6521 +/- 477 < 7.2 < 10.8 < 9.3 < 13.5 < 10.1 Location: CA-FC-3 CAVE- 4887 1-Soybeans 9/12/2016 < 152 5997 +/- 433 < 10.4 < 12.7 < 11.2 < 10.9 < 12.9 CAVE- 4888 2-Soybeans 9/12/2016 < 187 5733 +/- 417 < 12.9 < 5.5 < 12.4 < 11.4 < 11.1 CAVE- 4889 3-Soybeans 9/12/2016 < 187 5308 +/- 382 < 12.1 < 12.6 < 8.1 < 11.7 < 14.2 Location: CA-FC-4(C)

CAVE- 5063 Soybeans 9/20/2016 < 187 6652 +/- 423 < 11.1 < 14.3 < 10.2 < 12.8 < 12.0 a

"NS" = No sample; refer to Part I Table 5.5, Missed Collections and Analyses.

4-1

Table 5. Soil, analyses for gamma-emitting isotopes.

Collection: Annually Collection Concentration (pCi/kg dry) 40 54 59 58 60 95 134 137 140 Lab Code Date K Mn Fe Co Co ZrNb Cs Cs BaLa Location: SOL-F-002 CASO- 6404 11/9/2016 12960 +/- 823 < 28.0 < 92.7 < 44.9 < 19.0 < 95.5 < 21.8 425 +/- 58 < 283.1 CASO- 6405 11/9/2016 11400 +/- 765 < 27.9 < 122.5 < 28.9 < 24.3 < 38.3 < 26.9 576 +/- 47 < 166.3 Location: SOL-F-006 CASO- 6406 11/9/2016 11287 +/- 744 < 26.5 < 65.2 < 45.8 < 18.7 < 50.2 < 29.4 426 +/- 49 < 201.1 CASO- 6408 11/9/2016 10593 +/- 704 < 28.9 < 43.9 < 44.2 < 19.3 < 75.4 < 21.0 421 +/- 41 < 261.5 Location: SOL-PR-003 CASO- 6411 11/9/2016 10518 +/- 633 < 27.6 < 57.2 < 30.3 < 16.3 < 62.8 < 22.1 165 +/- 30 < 132.0 CASO- 6412 11/9/2016 9790 +/- 642 < 22.8 < 98.8 < 25.6 < 12.5 < 67.5 < 16.8 349 +/- 37 < 228.4 Location: SOL-PR-007 CASO- 6413 11/9/2016 10791 +/- 598 < 25.6 < 66.5 < 23.4 < 16.0 < 59.1 < 14.8 217 +/- 30 < 203.5 CASO- 6414 11/9/2016 10595 +/- 700 < 38.3 < 87.0 < 34.9 < 18.1 < 43.7 < 27.9 228 +/- 36 < 211.7 Location: SOL-M-009 CASO- 6409 11/8/2016 14409 +/- 849 < 27.8 < 137.8 < 31.4 < 12.7 < 65.4 < 28.3 136 +/- 40 < 219.2 CASO- 6410 11/8/2016 16262 +/- 803 < 32.5 < 71.5 < 33.5 < 25.8 < 83.0 < 23.3 184 +/- 33 < 249.1 Location: SOL-W-001 CASO- 6415 11/9/2016 11317 +/- 777 < 23.7 < 78.7 < 35.9 < 15.7 < 58.4 < 21.4 < 33 < 312.2 CASO- 6416 11/9/2016 11824 +/- 628 < 22.7 < 62.0 < 25.1 < 21.1 < 50.7 < 15.2 56 +/- 23.2 < 120.7 Location: SOL-W-002 CASO- 6417 11/9/2016 14900 +/- 928 < 38.1 < 89.1 < 47.0 < 24.0 < 88.9 < 23.3 116 +/- 32 < 231.0 CASO- 6418 11/9/2016 15243 +/- 927 < 34.2 < 86.3 < 35.0 < 19.6 < 80.6 < 26.6 134 +/- 36 < 352.7 Location: SOL-W-003 CASO- 6419 11/9/2016 9137 +/- 741 < 29.6 < 88.7 < 37.9 < 22.9 < 46.1 < 24.0 < 26.9 < 105.1 CASO- 6420 11/9/2016 4891 +/- 639 < 31.0 < 103.2 < 34.8 < 20.7 < 53.2 < 31.8 < 28.6 < 216.3 Location: SOL-W-004 CASO- 6421 11/9/2016 3865 +/- 615 < 37.9 < 105.2 < 46.6 < 17.7 < 74.1 < 34.2 < 36.6 < 258.1 CASO- 6422 11/9/2016 2399 +/- 613 < 35.3 < 117.9 < 39.1 < 27.9 < 43.8 < 25.5 < 31.2 < 386.2 5-1

Table 6. Surface water, analyses for tritium and gamma-emitting isotopes.

Collection: Monthly Location: CA-SWA-S01 Units: pCi/L Lab Code Required CASW- 427 CASW- 812 CASW- 1319 CASW- 1961 Date Collected LLD 01-26-16 02-23-16 03-29-16 04-26-16 H-3 3000 < 143 < 172 < 152 < 174 Mn-54 15 < 2.7 < 1.8 < 5.3 < 2.9 Fe-59 30 < 4.7 < 5.6 < 7.1 < 5.1 Co-58 15 < 2.2 < 2.1 < 3.9 < 1.4 Co-60 15 < 2.5 < 2.5 < 5.1 < 2.7 Zn-65 30 < 4.1 < 4.6 < 5.7 < 3.9 Zr-Nb-95 15 < 2.8 < 3.2 < 5.3 < 3.5 I-131 1000 < 11.3 < 6.0 < 6.1 < 13.0 Cs-134 15 < 2.9 < 2.6 < 6.6 < 3.4 Cs-137 18 < 2.6 < 1.8 < 4.2 < 3.2 Ba-La-140 15 < 4.2 < 3.5 < 5.3 < 2.8 Lab Code Required CASW- 2771 CASW- 3303 CASW- 3974 CASW- 4573 Date Collected LLD 05-31-16 06-28-16 07-26-16 08-30-16 H-3 3000 < 183 < 150 < 145 < 155 Mn-54 15 < 2.3 < 2.0 < 1.4 < 2.6 Fe-59 30 < 5.1 < 3.0 < 4.8 < 4.3 Co-58 15 < 2.8 < 2.3 < 1.4 < 2.7 Co-60 15 < 2.3 < 1.5 < 1.1 < 2.3 Zn-65 30 < 5.4 < 3.9 < 1.3 < 3.9 Zr-Nb-95 15 < 1.9 < 2.0 < 2.3 < 2.9 I-131 1000 < 4.7 < 14.9 < 27.7 < 18.8 Cs-134 15 < 3.2 < 1.9 < 1.3 < 2.5 Cs-137 18 < 1.6 < 1.6 < 1.4 < 2.9 Ba-La-140 15 < 2.8 < 7.4 < 6.8 < 4.9 Lab Code Required CASW- 5142 CASW- 5949 CASW- 6697 CASW- 6953 Date Collected LLD 09-27-16 10-25-16 11-29-16 12-27-16 H-3 3000 < 148 < 156 < 152 < 143 Mn-54 15 < 1.3 < 1.4 < 2.5 < 1.8 Fe-59 30 < 4.7 < 3.9 < 4.3 < 3.8 Co-58 15 < 2.8 < 1.8 < 3.0 < 2.0 Co-60 15 < 2.0 < 1.2 < 2.5 < 1.3 Zn-65 30 < 1.5 < 2.5 < 4.4 < 4.2 Zr-Nb-95 15 < 4.2 < 1.7 < 3.4 < 2.8 I-131 1000 < 14.8 < 20.2 < 33.9 < 7.3 Cs-134 15 < 2.7 < 1.4 < 2.4 < 2.1 Cs-137 18 < 2.5 < 1.4 < 1.9 < 2.5 Ba-La-140 15 < 5.8 < 5.8 < 7.4 < 2.8 6-1

Table 6. Surface water, analyses for tritium and gamma-emitting isotopes.

Collection: Monthly Location: CA-SWA-S02 Units: pCi/L Lab Code Required CASW- 428 CASW- 813 CASW- 1320 CASW- 1962 Date Collected LLD 01-26-16 02-23-16 03-29-16 04-26-16 H-3 3000 < 143 324 +/- 96 < 152 283 +/- 102 Mn-54 15 < 2.1 < 2.8 < 3.2 < 5.7 Fe-59 30 < 4.5 < 6.4 < 2.5 < 8.5 Co-58 15 < 2.8 < 2.5 < 4.2 < 5.0 Co-60 15 < 2.0 < 1.5 < 2.3 < 5.2 Zn-65 30 < 2.5 < 5.5 < 3.6 < 8.6 Zr-Nb-95 15 < 2.7 < 2.7 < 4.2 < 4.4 I-131 1000 < 6.0 < 6.4 < 6.9 < 8.2 Cs-134 15 < 2.7 < 3.2 < 4.1 < 5.8 Cs-137 18 < 2.9 < 3.2 < 3.4 < 4.8 Ba-La-140 15 < 3.6 < 2.6 < 1.8 < 4.0 Lab Code Required CASW- 2772 CASW- 3304 CASW- 3975 CASW- 4575 Date Collected LLD 05-31-16 06-28-16 07-26-16 08-30-16 H-3 3000 < 183 < 150 < 145 < 155 Mn-54 15 < 4.9 < 2.2 < 2.7 < 1.8 Fe-59 30 < 8.4 < 3.2 < 4.9 < 4.8 Co-58 15 < 4.7 < 1.6 < 2.8 < 3.6 Co-60 15 < 3.0 < 1.0 < 2.1 < 2.0 Zn-65 30 < 4.0 < 2.7 < 4.4 < 2.8 Zr-Nb-95 15 < 3.7 < 2.9 < 3.8 < 3.0 I-131 1000 < 7.3 < 18.5 < 27.4 < 15.9 Cs-134 15 < 5.4 < 2.1 < 2.5 < 2.6 Cs-137 18 < 6.0 < 2.4 < 2.4 < 2.1 Ba-La-140 15 < 2.6 < 8.3 < 12.5 < 5.9 Lab Code Required CASW- 5143 CASW- 5950 CASW- 6699 CASW- 6954 Date Collected LLD 09-27-16 10-25-16 11-29-16 12-27-16 H-3 3000 < 148 < 156 < 152 < 143 Mn-54 15 < 2.4 < 1.4 < 1.5 < 1.2 Fe-59 30 < 7.0 < 1.8 < 4.5 < 3.0 Co-58 15 < 1.3 < 1.4 < 2.2 < 1.8 Co-60 15 < 2.3 < 0.9 < 1.6 < 2.1 Zn-65 30 < 3.9 < 2.5 < 2.0 < 2.1 Zr-Nb-95 15 < 3.3 < 1.6 < 2.3 < 2.4 I-131 1000 < 23.1 < 23.1 < 27.0 < 5.4 Cs-134 15 < 2.7 < 1.2 < 1.7 < 2.5 Cs-137 18 < 3.0 < 1.2 < 1.7 < 1.8 Ba-La-140 15 < 9.8 < 6.6 < 5.4 < 3.8 6-2

Table 7. Surface Water (Ponds), analyses for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa Location: CA-SWA-POND 01 CASW- 961 02/29/16 < 142 < 1.6 < 1.9 < 1.8 < 2.2 < 2.5 < 2.3 < 2.0 < 1.9 < 2.9 CASW- 4813 09/06/16 < 149 < 4.8 < 5.0 < 5.9 < 5.6 < 5.4 < 6.0 < 6.2 < 5.2 < 11.3 Location: CA-SWA-POND 02 CASW- 962 03/01/16 < 142 < 1.7 < 4.4 < 1.9 < 1.9 < 2.5 < 1.8 < 1.8 < 1.9 < 1.8 CASW- 4814 09/06/16 < 149 < 2.0 < 3.3 < 3.0 < 1.8 < 2.1 < 2.9 < 2.8 < 2.4 < 8.4 Location: CA-SWA-SLUDGE LAGOON #4 CASW- 963 02/29/16 < 146 < 2.1 < 3.9 < 1.5 < 1.3 < 2.8 < 2.4 < 1.7 < 2.6 < 3.2 CASW- 4821 09/06/16 < 149 < 2.4 < 4.8 < 3.7 < 1.7 < 4.6 < 3.7 < 2.5 < 2.0 < 10.9 7-1

Table 7. Surface Water (Ponds), analyses for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa Location: CA-SWA-OUTFALL 010 CASW- 954 02/29/16 < 146 < 2.6 < 4.0 < 1.9 < 2.6 < 2.4 < 3.9 < 3.3 < 2.8 < 4.5 CASW- 4815 09/06/16 < 149 < 2.2 < 5.1 < 2.2 < 1.5 < 2.7 < 3.0 < 2.8 < 3.1 < 10.7 Location: CA-SWA-OUTFALL 011 CASW- 955 02/29/16 < 146 < 5.1 < 8.4 < 4.4 < 4.1 < 5.3 < 6.3 < 5.1 < 5.7 < 8.6 CASW- 4816 09/06/16 < 149 < 3.8 < 4.3 < 2.2 < 2.4 < 1.8 < 5.4 < 3.5 < 2.3 < 12.4 Location: CA-SWA-OUTFALL 012 CASW- 957 02/29/16 < 146 < 2.1 < 6.1 < 1.2 < 2.3 < 3.4 < 2.4 < 2.5 < 2.8 < 4.0 CASW- 4817 09/06/16 < 149 < 2.6 < 3.6 < 3.3 < 2.1 < 5.6 < 2.7 < 2.7 < 2.0 < 7.2 Location: CA-SWA-OUTFALL 013 CASW- 958 03/01/16 < 146 < 5.0 < 5.4 < 4.1 < 3.9 < 6.4 < 5.8 < 3.8 < 3.8 < 5.4 CASW- 4818 09/06/16 < 149 < 2.7 < 8.6 < 3.7 < 1.2 < 3.8 < 5.6 < 3.1 < 3.1 < 7.8 Location: CA-SWA-OUTFALL 014 CASW- 959 02/29/16 < 146 < 1.9 < 3.3 < 1.7 < 2.2 < 3.9 < 3.4 < 3.1 < 1.8 < 3.6 CASW- 4819 09/06/16 < 149 < 1.8 < 4.9 < 3.4 < 1.6 < 4.5 < 2.9 < 2.6 < 2.0 < 12.9 Location: CA-SWA-OUTFALL 015 CASW- 960 02/29/16 < 142 < 2.0 < 5.4 < 2.3 < 1.3 < 2.8 < 2.9 < 2.6 < 2.2 < 4.4 CASW- 4820 09/06/16 < 149 < 1.8 < 7.9 < 2.7 < 1.3 < 4.6 < 3.5 < 2.4 < 2.2 < 7.1 7-2

Table 8. Drinking Water Wells, analysis for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa CA-DWA-003 (Ward)

CADW- 540 2/2/2016 < 141 < 2.2 < 3.9 < 2.8 < 2.2 < 2.5 < 3.0 < 2.6 < 2.0 < 4.9 CADW- 2081 4/27/2016 < 160 < 1.5 < 7.6 < 2.3 < 2.1 < 4.3 < 3.9 < 3.0 < 2.1 < 4.8 CADW- 4200 7/27/2016 < 149 < 2.7 < 6.2 < 3.6 < 1.1 < 2.9 < 4.6 < 2.9 < 3.3 < 9.3 CADW- 5934 10/24/2016 < 156 < 2.8 < 6.2 < 3.2 < 1.8 < 5.8 < 3.5 < 3.7 < 2.8 < 4.8 CA-DWA-004 (Miller)

CADW- 541 2/2/2016 < 141 < 1.6 < 5.3 < 2.1 < 2.2 < 3.2 < 3.2 < 2.2 < 2.4 < 3.2 CADW- 2082 4/28/2016 < 160 < 2.4 < 5.8 < 2.7 < 2.6 < 4.2 < 5.1 < 3.9 < 2.3 < 7.8 CADW- 4202 7/27/2016 < 149 < 1.4 < 4.3 < 1.1 < 1.5 < 2.6 < 2.2 < 1.2 < 1.2 < 5.4 CADW- 5935 10/25/2016 < 156 < 1.6 < 6.2 < 2.2 < 2.1 < 3.2 < 4.4 < 2.3 < 2.9 < 10.2 CA-DWA-005 (Brucker Bros.)

a 2/2/2016 NS CADW- 2083 4/27/2016 < 160 < 1.2 < 5.6 < 2.0 < 2.7 < 4.0 < 5.2 < 3.8 < 3.2 < 8.4 CADW- 4203 8/1/2016 < 148 < 2.7 < 6.1 < 3.0 < 2.5 < 4.7 < 4.4 < 3.6 < 3.3 < 4.0 CADW- 5936 10/24/2016 < 156 < 2.3 < 7.6 < 3.4 < 1.9 < 3.9 < 3.3 < 3.1 < 2.9 < 14.2 CA-DWA-006 (Lindeman)

CADW- 542 2/2/2016 < 141 < 2.6 < 9.3 < 3.0 < 2.5 < 4.3 < 3.7 < 4.7 < 3.5 < 4.5 CADW- 2084 4/27/2016 < 160 < 2.4 < 6.0 < 3.0 < 2.0 < 4.2 < 3.5 < 2.8 < 3.5 < 4.8 CADW- 4204 7/27/2016 < 149 < 1.8 < 4.6 < 2.7 < 1.7 < 3.6 < 5.2 < 2.3 < 2.9 < 9.2 CADW- 5937 10/24/2016 < 156 < 1.8 < 3.8 < 1.9 < 1.4 < 3.2 < 3.0 < 1.6 < 1.5 < 6.9 CA-DWA-007 (Kriete)

CADW- 543 2/2/2016 < 141 < 2.2 < 5.3 < 2.1 < 1.7 < 3.5 < 2.8 < 2.2 < 1.9 < 4.2 CADW- 2085 4/27/2016 < 160 < 1.3 < 3.4 < 2.2 < 2.1 < 3.8 < 4.8 < 3.3 < 2.9 < 11.9 CADW- 4205 7/27/2016 < 149 < 1.4 < 3.7 < 1.8 < 0.9 < 2.0 < 2.3 < 1.3 < 0.9 < 5.4 CADW- 5938 10/24/2016 < 156 < 1.6 < 3.7 < 4.2 < 2.5 < 3.4 < 4.8 < 2.7 < 2.0 < 7.8 CA-DWA-008 (Brandt)

CADW- 544 2/2/2016 < 141 < 1.8 < 2.1 < 1.7 < 1.5 < 1.7 < 2.5 < 2.2 < 2.4 < 3.1 CADW- 2086 4/27/2016 < 160 < 4.5 < 9.9 < 6.9 < 6.0 < 13.0 < 6.9 < 7.9 < 5.5 < 6.6 CADW- 4206 7/29/2016 < 148 < 3.1 < 8.6 < 2.6 < 2.2 < 4.8 < 3.9 < 3.9 < 2.6 < 6.8 CADW- 5939 10/24/2016 < 156 < 3.1 < 4.2 < 2.9 < 2.7 < 3.6 < 4.9 < 3.7 < 2.1 < 11.6 a "NS" = No sample; refer to Part I Table 5.5, Missed Collections and Analyses.

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Table 8. Drinking Water Wells, analysis for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa CA-DWA-009 (Clardy)

CADW- 545 2/2/2016 < 141 < 1.9 < 2.7 < 1.0 < 1.5 < 3.4 < 1.9 < 1.7 < 2.3 < 3.4 CADW- 2087 4/27/2016 < 160 < 7.1 < 6.2 < 5.1 < 3.5 < 3.5 < 6.6 < 6.7 < 7.3 < 4.0 CADW- 4207 7/27/2016 < 149 < 3.2 < 5.5 < 3.1 < 2.6 < 4.1 < 3.6 < 2.3 < 2.4 < 10.5 CADW- 5940 10/24/2016 < 156 < 1.7 < 4.6 < 2.5 < 2.6 < 3.5 < 4.6 < 2.5 < 2.8 < 9.0 CA-DWA-010 (Dillon, Susan)

CADW- 546 2/2/2016 < 141 < 1.6 < 3.3 < 2.1 < 2.2 < 3.4 < 2.3 < 1.8 < 2.4 < 4.5 CADW- 2089 4/27/2016 < 160 < 2.9 < 4.3 < 2.6 < 2.1 < 6.3 < 4.4 < 3.5 < 2.7 < 4.9 CADW- 4208 7/27/2016 < 149 < 2.1 < 5.6 < 2.6 < 2.2 < 3.8 < 5.0 < 2.7 < 2.4 < 12.1 CADW- 5941 10/24/2016 < 156 < 2.7 < 8.2 < 2.2 < 2.5 < 4.3 < 4.6 < 3.3 < 2.8 < 13.7 CA-DWA-012 (Dillon, Joe)

CADW- 547 2/2/2016 < 141 < 2.1 < 4.7 < 1.5 < 1.5 < 2.8 < 2.6 < 1.8 < 1.7 < 4.4 CADW- 2090 4/27/2016 < 160 < 3.1 < 8.0 < 2.2 < 1.5 < 5.4 < 3.7 < 2.8 < 2.0 < 4.3 CADW- 4209 7/29/2016 < 148 < 2.0 < 3.5 < 2.8 < 2.1 < 3.3 < 4.0 < 2.3 < 2.1 < 8.9 CADW- 5942 10/24/2016 < 156 < 2.2 < 4.0 < 1.8 < 1.7 < 4.2 < 4.4 < 2.9 < 2.0 < 14.6 CA-DWA-022 (Plummer)

CADW- 549 2/2/2016 < 141 < 1.8 < 3.1 < 2.7 < 1.5 < 3.6 < 2.3 < 2.3 < 2.1 < 2.2 CADW- 2092 4/27/2016 < 160 < 1.9 < 6.6 < 3.6 < 1.2 < 1.5 < 3.4 < 2.0 < 2.7 < 6.9 CADW- 4211 7/29/2016 < 148 < 2.3 < 6.6 < 1.7 < 2.0 < 5.3 < 4.6 < 2.3 < 2.5 < 5.2 CADW- 5945 10/24/2016 < 156 < 1.3 < 3.0 < 0.9 < 1.2 < 2.1 < 1.9 < 1.1 < 1.4 < 8.0 CA-DWA-D01 (Portland Bar/Grill)

CADW- 551 2/2/2016 < 141 < 1.7 < 2.9 < 1.2 < 1.9 < 3.5 < 2.9 < 1.7 < 2.0 < 5.5 CADW- 2093 4/27/2016 < 160 < 2.0 < 5.8 < 2.0 < 0.6 < 4.6 < 4.4 < 3.0 < 1.9 < 5.0 CADW- 4213 7/29/2016 < 148 < 1.3 < 2.1 < 2.0 < 0.9 < 2.2 < 1.9 < 1.3 < 1.1 < 7.0 CADW- 5947 10/24/2016 < 156 < 1.9 < 4.1 < 1.6 < 1.7 < 2.6 < 2.9 < 1.6 < 1.8 < 8.5 8-2

Table 8. Drinking Water Wells, analysis for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa CA-DWA-PW1 (Plant Cafeteria)

CADW- 552 2/3/2016 < 141 < 1.8 < 3.7 < 2.3 < 1.5 < 2.7 < 2.2 < 2.0 < 2.0 < 4.9 CADW- 2094 4/28/2016 < 160 < 1.8 < 3.4 < 2.6 < 1.8 < 4.8 < 4.7 < 2.7 < 2.7 < 6.5 CADW- 4214 7/29/2016 < 148 < 1.3 < 3.0 < 1.5 < 1.6 < 1.4 < 2.5 < 1.2 < 1.4 < 7.1 CADW- 5948 10/25/2016 < 156 < 1.1 < 3.9 < 1.2 < 1.8 < 3.4 < 3.4 < 1.6 < 1.7 < 9.1 CA-DWA-21 CADW- 548 2/2/2016 < 141 < 1.3 < 3.4 < 1.8 < 1.1 < 2.3 < 2.9 < 2.0 < 2.2 < 4.3 CADW- 2091 4/27/2016 < 160 < 2.0 < 4.1 < 1.5 < 1.6 < 2.9 < 4.8 < 2.4 < 2.4 < 10.7 CADW- 4210 7/27/2016 < 149 < 1.3 < 2.2 < 1.0 < 1.3 < 1.6 < 2.2 < 1.1 < 1.5 < 7.4 CADW- 5944 10/24/2016 < 156 < 1.7 < 2.5 < 1.9 < 1.8 < 2.8 < 3.1 < 1.6 < 1.8 < 7.6 CA-DWA-V16 CADW- 550 2/2/2016 < 141 < 1.4 < 3.9 < 0.9 < 1.7 < 3.1 < 2.3 < 2.0 < 1.9 < 2.6 CADW- 2095 4/27/2016 < 160 < 1.9 < 5.5 < 2.1 < 1.9 < 2.4 < 4.7 < 2.6 < 3.0 < 8.1 CADW- 4212 7/29/2016 < 148 < 1.8 < 6.1 < 3.0 < 2.3 < 3.5 < 3.2 < 2.4 < 3.3 < 10.0 CADW- 5946 10/25/2016 < 156 < 1.1 < 3.2 < 1.2 < 0.7 < 2.3 < 1.9 < 1.0 < 1.0 < 3.9 8-3

Table 9. Wells and Ponds (non-potable), analyses for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa Location: CA-WWA-936 CAWW- 259 1/14/2016 189 +/- 80 < 3.6 < 2.5 < 2.1 < 1.6 < 4.5 < 3.6 < 3.5 < 3.1 < 4.7 CAWW- 637 2/18/2016 288 +/- 99 < 1.7 < 4.9 < 1.6 < 2.7 < 5.3 < 2.8 < 2.9 < 1.6 < 2.1 CAWW- 1131 3/15/2016 269 +/- 91 < 3.0 < 6.6 < 2.9 < 1.9 < 3.6 < 3.6 < 3.1 < 3.3 < 2.9 CAWW- 1853 4/13/2016 189 +/- 84 < 2.0 < 3.8 < 4.7 < 2.7 < 4.1 < 4.7 < 2.8 < 2.9 < 6.3 CAWW- 2367 5/12/2016 402 +/- 91 < 3.1 < 3.5 < 1.4 < 2.5 < 5.1 < 6.0 < 3.0 < 3.3 < 7.7 CAWW- 2964 6/13/2016 338 +/- 88 < 3.4 < 11.0 < 2.8 < 3.8 < 9.2 < 4.6 < 4.3 < 3.4 < 4.2 CAWW- 3582 7/13/2016 354 +/- 91 < 3.3 < 3.3 < 3.5 < 2.2 < 5.3 < 3.7 < 3.3 < 2.8 < 8.8 CAWW- 4428 8/18/2016 298 +/- 89 < 2.2 < 7.4 < 2.5 < 2.3 < 5.5 < 4.4 < 4.0 < 3.0 < 4.3 CAWW- 4805 9/9/2016 152 +/- 86 < 5.6 < 5.9 < 3.7 < 3.4 < 8.0 < 5.1 < 5.3 < 4.8 < 7.5 CAWW- 5431 10/10/2016 222 +/- 87 < 3.6 < 4.1 < 2.1 < 2.1 < 3.0 < 5.6 < 2.9 < 1.5 < 13.0 CAWW- 6200 11/9/2016 < 180 < 2.8 < 8.4 < 3.4 < 3.1 < 3.5 < 4.6 < 3.5 < 2.8 < 12.5 CAWW- 6765 12/9/2016 < 158 < 1.8 < 2.8 < 1.3 < 1.8 < 3.4 < 3.1 < 1.9 < 1.7 < 5.0 Location: CA-WWA-937B a

1/14/2016 NS CAWW- 814 2/24/2016 < 172 < 3.6 < 5.9 < 3.1 < 2.7 < 3.8 < 2.6 < 3.4 < 3.7 < 3.8 CAWW- 1132 3/15/2016 < 149 < 3.2 < 6.1 < 2.2 < 4.2 < 7.1 < 4.0 < 3.9 < 4.3 < 5.0 CAWW- 1854 4/13/2016 < 149 < 2.8 < 6.5 < 2.6 < 1.9 < 3.9 < 2.9 < 3.2 < 3.0 < 6.8 CAWW- 2368 5/12/2016 207 +/- 82 < 3.8 < 6.3 < 3.3 < 1.7 < 3.0 < 5.6 < 4.7 < 4.7 < 9.2 CAWW- 2965 6/13/2016 236 +/- 83 < 4.6 < 8.2 < 2.7 < 2.6 < 4.6 < 4.7 < 5.3 < 4.8 < 4.7 CAWW- 3583 7/13/2016 183 +/- 83 < 2.5 < 4.4 < 1.8 < 2.6 < 3.3 < 4.7 < 2.9 < 3.6 < 10.8 CAWW- 4429 8/18/2016 < 148 < 2.3 < 5.1 < 1.3 < 2.2 < 4.1 < 2.0 < 2.2 < 2.5 < 6.5 CAWW- 4807 9/9/2016 < 149 < 3.5 < 6.9 < 1.9 < 2.4 < 3.9 < 3.6 < 4.1 < 4.2 < 5.1 CAWW- 5432 10/10/2016 < 153 < 3.2 < 4.9 < 3.9 < 2.5 < 5.2 < 5.8 < 3.3 < 2.1 < 8.1 CAWW- 6201 11/9/2016 < 180 < 2.6 < 7.2 < 2.2 < 2.1 < 3.9 < 3.7 < 2.7 < 2.7 < 6.9 CAWW- 6766 12/7/2016 < 158 < 3.2 < 3.6 < 2.6 < 2.0 < 2.2 < 4.2 < 2.7 < 1.8 < 6.4 Location: CA-WWA-937D CAWW- 260 1/14/2016 < 141 < 3.5 < 5.1 < 3.1 < 3.1 < 5.3 < 4.6 < 4.3 < 4.6 < 5.1 CAWW- 638 2/17/2016 < 142 < 3.7 < 3.3 < 2.9 < 3.7 < 3.4 < 3.5 < 3.0 < 4.4 < 4.5 CAWW- 1133 3/15/2016 < 149 < 3.3 < 6.4 < 2.9 < 3.7 < 4.8 < 5.2 < 4.5 < 3.3 < 10.4 CAWW- 1855 4/13/2016 160 +/- 82 < 3.2 < 7.6 < 2.3 < 3.5 < 5.0 < 4.2 < 3.5 < 3.6 < 8.4 CAWW- 2369 5/12/2016 205 +/- 81 < 4.6 < 6.1 < 2.5 < 2.7 < 4.8 < 4.7 < 5.3 < 6.3 < 7.4 CAWW- 2966 6/13/2016 < 146 < 1.4 < 4.2 < 3.3 < 2.0 < 3.8 < 2.3 < 3.6 < 3.1 < 4.8 CAWW- 3584 7/13/2016 < 147 < 2.9 < 9.7 < 3.4 < 4.2 < 11.6 < 6.8 < 5.4 < 5.8 < 5.4 CAWW- 4430 8/18/2016 < 149 < 3.0 < 5.8 < 4.7 < 2.7 < 7.0 < 3.8 < 4.1 < 2.3 < 10.9 CAWW- 4808 9/8/2016 < 149 < 2.8 < 7.3 < 4.0 < 1.9 < 6.7 < 5.3 < 3.3 < 3.8 < 11.5 CAWW- 5433 10/10/2016 163 +/- 85 < 3.2 < 2.5 < 2.0 < 2.6 < 3.6 < 5.6 < 2.9 < 2.9 < 14.1 CAWW- 6202 11/9/2016 < 180 < 3.5 < 3.9 < 3.2 < 2.9 < 3.2 < 3.3 < 3.2 < 3.7 < 4.9 CAWW- 6767 12/7/2016 < 158 < 1.3 < 2.9 < 1.5 < 0.9 < 2.8 < 1.3 < 1.3 < 1.4 < 6.3 a "NS" = No sample; refer to Part I Table 5.5, Missed Collections and Analyses.

9-1

Table 9. Wells and Ponds (non-potable), analyses for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa Location: CA-WWA-939R CAWW- 261 1/14/2016 364 +/- 89 < 4.0 < 7.6 < 3.8 < 2.2 < 6.5 < 3.2 < 4.4 < 4.8 < 4.5 CAWW- 639 2/18/2016 245 +/- 97 < 2.4 < 3.3 < 2.5 < 2.1 < 5.7 < 2.5 < 2.9 < 2.5 < 2.5 CAWW- 1134 3/15/2016 < 149 < 4.1 < 8.5 < 2.5 < 3.5 < 6.7 < 4.3 < 4.0 < 3.6 < 3.4 CAWW- 1856 4/13/2016 < 149 < 2.8 < 7.0 < 2.2 < 3.3 < 5.3 < 4.5 < 3.2 < 1.8 < 2.9 CAWW- 2370 5/12/2016 181 +/- 80 < 3.7 < 6.8 < 3.7 < 3.7 < 4.1 < 6.0 < 4.3 < 5.8 < 8.5 CAWW- 2967 6/13/2016 240 +/- 83 < 2.6 < 5.3 < 1.9 < 1.2 < 2.4 < 4.1 < 2.7 < 1.6 < 4.3 CAWW- 3586 7/13/2016 283 +/- 88 < 1.2 < 3.7 < 1.3 < 0.7 < 2.2 < 1.5 < 1.5 < 1.7 < 5.9 CAWW- 4431 8/18/2016 572 +/- 101 < 3.0 < 5.1 < 2.7 < 2.4 < 6.1 < 3.9 < 3.2 < 3.9 < 4.9 CAWW- 4809 9/9/2016 190 +/- 84 < 1.5 < 7.0 < 3.3 < 2.1 < 4.6 < 4.3 < 2.3 < 3.2 < 14.4 CAWW- 5434 10/10/2016 240 +/- 89 < 3.1 < 7.5 < 4.7 < 3.2 < 3.0 < 5.5 < 3.5 < 3.7 < 6.4 CAWW- 6203 11/9/2016 < 180 < 3.6 < 5.2 < 3.3 < 2.0 < 3.5 < 5.9 < 3.9 < 2.7 < 9.4 CAWW- 6768 12/9/2016 218 +/- 87 < 2.8 < 2.9 < 3.4 < 1.9 < 4.3 < 4.2 < 2.8 < 2.7 < 8.7 Location: CA-WWA-940 CAWW- 282 1/18/2016 < 141 < 3.2 < 6.5 < 3.4 < 2.8 < 4.5 < 4.5 < 4.5 < 2.9 < 2.7 CAWW- 640 2/18/2016 < 146 < 1.9 < 4.8 < 2.4 < 2.7 < 4.0 < 2.1 < 2.8 < 2.6 < 3.6 CAWW- 1136 3/15/2016 < 149 < 1.9 < 5.7 < 2.6 < 2.7 < 2.1 < 2.2 < 2.6 < 2.6 < 5.3 CAWW- 1857 4/13/2016 < 149 < 2.4 < 6.1 < 2.6 < 2.8 < 4.8 < 2.7 < 3.3 < 4.1 < 3.6 CAWW- 2371 5/12/2016 < 146 < 4.0 < 3.9 < 4.4 < 4.0 < 7.0 < 4.5 < 4.8 < 4.4 < 4.9 CAWW- 2969 6/13/2016 < 146 < 1.7 < 3.3 < 2.0 < 1.1 < 3.1 < 2.9 < 1.6 < 1.9 < 5.0 CAWW- 3587 7/13/2016 < 147 < 3.1 < 6.3 < 2.5 < 1.6 < 3.5 < 3.0 < 2.8 < 3.4 < 5.1 CAWW- 4432 8/18/2016 < 149 < 2.3 < 6.3 < 2.6 < 2.3 < 3.2 < 5.0 < 2.9 < 3.9 < 6.6 CAWW- 4810 9/9/2016 161 +/- 87 < 2.9 < 8.4 < 2.4 < 2.3 < 3.0 < 6.1 < 4.3 < 3.8 < 13.8 CAWW- 5435 10/10/2016 < 153 < 2.6 < 6.9 < 2.1 < 1.4 < 5.2 < 4.2 < 2.9 < 2.9 < 4.8 CAWW- 6204 11/9/2016 < 180 < 2.1 < 8.5 < 1.5 < 1.7 < 3.9 < 3.5 < 2.9 < 3.0 < 6.6 CAWW- 6769 12/9/2016 < 158 < 1.7 < 5.4 < 1.0 < 1.9 < 2.8 < 3.1 < 1.9 < 1.8 < 7.4 Location: CA-WWA-941 CAWW- 263 1/14/2016 < 141 < 2.5 < 9.2 < 2.1 < 1.1 < 8.1 < 2.8 < 3.8 < 2.7 < 4.4 CAWW- 642 2/18/2016 202 +/- 95 < 2.8 < 4.0 < 1.6 < 1.5 < 5.1 < 2.4 < 2.9 < 2.6 < 2.8 CAWW- 1137 3/15/2016 184 +/- 87 < 3.8 < 7.4 < 2.8 < 3.0 < 7.2 < 3.6 < 3.8 < 3.1 < 7.0 CAWW- 1858 4/13/2016 < 149 < 1.8 < 4.0 < 3.4 < 2.6 < 5.2 < 3.2 < 3.3 < 3.3 < 3.6 CAWW- 2386 5/13/2016 207 +/- 82 < 3.8 < 6.9 < 3.8 < 4.5 < 6.0 < 5.4 < 6.4 < 4.9 < 4.2 CAWW- 2970 6/13/2016 176 +/- 80 < 1.3 < 3.4 < 1.8 < 1.6 < 2.0 < 2.4 < 1.7 < 1.8 < 6.1 CAWW- 3588 7/13/2016 < 147 < 1.3 < 2.5 < 2.0 < 1.3 < 2.7 < 2.5 < 2.0 < 1.9 < 8.2 CAWW- 4433 8/18/2016 < 148 < 2.7 < 8.1 < 3.1 < 1.9 < 7.1 < 5.5 < 3.4 < 4.1 < 10.2 CAWW- 4811 9/8/2016 < 149 < 3.8 < 4.3 < 1.9 < 2.4 < 4.6 < 4.3 < 3.6 < 3.3 < 14.1 CAWW- 5436 10/10/2016 < 153 < 2.9 < 9.7 < 3.1 < 2.5 < 4.7 < 3.3 < 3.1 < 2.7 < 6.4 CAWW- 6205 11/9/2016 < 180 < 2.6 < 7.0 < 2.2 < 2.4 < 4.1 < 5.7 < 3.2 < 3.5 < 6.8 CAWW- 6770 12/9/2016 < 158 < 1.2 < 3.3 < 1.7 < 1.5 < 1.5 < 1.9 < 1.4 < 1.7 < 6.9 9-2

Table 9. Wells and Ponds (non-potable), analyses for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa Location: CA-WWA-GWS CAWW- 264 1/14/2016 254 +/- 84 < 4.1 < 6.4 < 3.3 < 3.5 < 4.3 < 5.1 < 3.6 < 3.4 < 4.1 CAWW- 643 2/18/2016 249 +/- 97 < 2.2 < 6.5 < 1.4 < 2.8 < 4.5 < 2.1 < 3.1 < 2.3 < 2.7 CAWW- 1138 3/15/2016 < 149 < 3.7 < 4.8 < 2.9 < 3.3 < 5.1 < 4.8 < 3.8 < 4.4 < 7.5 CAWW- 1859 4/13/2016 166 +/- 83 < 3.1 < 6.2 < 4.5 < 2.5 < 4.0 < 3.3 < 3.3 < 2.2 < 5.9 CAWW- 2372 5/12/2016 224 +/- 82 < 5.1 < 7.5 < 3.6 < 3.2 < 7.1 < 4.5 < 6.1 < 4.3 < 3.3 CAWW- 2971 6/13/2016 192 +/- 81 < 1.4 < 3.4 < 1.7 < 1.0 < 2.5 < 1.8 < 1.3 < 1.5 < 5.1 CAWW- 3589 7/13/2016 223 +/- 85 < 1.7 < 2.3 < 0.8 < 1.2 < 2.6 < 2.3 < 1.5 < 1.4 < 4.4 CAWW- 4434 8/18/2016 392 +/- 94 < 2.8 < 8.1 < 1.9 < 2.9 < 3.8 < 5.1 < 3.3 < 3.8 < 6.4 CAWW- 4812 9/9/2016 727 +/- 111 < 3.5 < 8.9 < 3.7 < 2.0 < 3.8 < 3.3 < 3.9 < 3.2 < 9.6 CAWW- 5437 10/10/2016 178 +/- 85 < 1.8 < 3.3 < 1.9 < 1.6 < 3.3 < 3.5 < 2.1 < 1.3 < 4.9 CAWW- 6206 11/9/2016 < 180 < 2.9 < 3.4 < 3.2 < 2.0 < 2.1 < 4.1 < 2.6 < 2.2 < 3.8 CAWW- 6771 12/9/2016 169 +/- 85 < 1.8 < 2.7 < 1.2 < 1.6 < 3.8 < 2.6 < 1.8 < 2.2 < 7.7 ISFSI Sump CAWW- 265 1/14/2016 198 +/- 81 < 3.5 < 7.2 < 3.9 < 3.2 < 5.4 < 4.3 < 3.6 < 4.0 < 4.0 CAWW- 2041 4/29/2016 < 150 CAWW- 3760 7/20/2016 < 151 CAWW- 5782 10/21/2016 < 156 Location: CA-WWA-U1MW-001 CAWW- 81 1/6/2016 < 143 < 2.5 < 4.6 < 4.2 < 3.1 < 5.4 < 4.8 < 4.4 < 2.8 < 4.5 CAWW- 1451 4/6/2016 < 138 < 5.0 < 8.3 < 2.8 < 6.2 < 9.5 < 8.1 < 6.4 < 5.8 < 4.8 CAWW- 3412 7/6/2016 < 149 < 1.0 < 3.0 < 1.3 < 1.1 < 2.5 < 2.2 < 1.5 < 1.1 < 4.3 CAWW- 5597 10/14/2016 < 154 < 3.3 < 7.8 < 2.1 < 1.5 < 4.7 < 5.6 < 3.1 < 1.6 < 10.3 Location: CA-WWA-U1MW-002 CAWW- 258 1/15/2016 < 141 < 3.2 < 6.7 < 3.3 < 4.3 < 8.1 < 3.2 < 4.8 < 3.9 < 2.5 CAWW- 1919 4/26/2016 < 166 < 5.7 < 9.1 < 4.4 < 3.6 < 4.3 < 4.2 < 4.6 < 3.5 < 5.3 CAWW- 3552 7/11/2016 < 147 < 2.2 < 5.6 < 2.4 < 1.9 < 3.8 < 3.1 < 2.1 < 2.5 < 4.8 CAWW- 5430 10/6/2016 < 151 < 2.2 < 4.1 < 2.0 < 1.2 < 4.0 < 2.7 < 2.0 < 1.7 < 4.6 Location: CA-WWA-U1MW-004 CAWW- 85 1/6/2016 < 143 < 2.4 < 4.9 < 2.4 < 2.2 < 4.9 < 3.7 < 3.7 < 2.6 < 2.0 CAWW- 1848 4/12/2016 < 149 < 1.9 < 4.9 < 2.9 < 1.2 < 5.2 < 2.9 < 3.5 < 3.1 < 4.4 CAWW- 3410 7/5/2016 < 149 < 2.4 < 4.2 < 2.6 < 2.7 < 4.7 < 3.6 < 3.4 < 2.7 < 4.4 CAWW- 5596 10/14/2016 < 154 < 2.8 < 5.2 < 2.3 < 1.8 < 2.7 < 2.2 < 2.3 < 1.8 < 13.7 9-3

Table 9. Wells and Ponds (non-potable), analyses for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa Location: CA-WWA-U1MW-005 CAWW- 86 1/6/2016 < 143 < 3.0 < 6.8 < 4.0 < 4.1 < 7.0 < 4.2 < 4.9 < 2.5 < 10.2 CAWW- 1847 4/12/2016 < 149 < 2.5 < 7.9 < 3.3 < 1.1 < 3.4 < 2.2 < 2.9 < 2.8 < 4.4 CAWW- 3411 7/5/2016 < 149 < 1.0 < 2.5 < 1.5 < 0.8 < 3.0 < 1.6 < 1.5 < 1.3 < 3.6 CAWW- 5595 10/14/2016 < 154 < 1.7 < 3.9 < 3.6 < 1.7 < 3.4 < 3.2 < 2.8 < 2.4 < 6.4 Location: CA-WWA-U1MW-006 CAWW- 257 1/13/2016 < 141 < 2.6 < 7.0 < 3.0 < 4.4 < 7.0 < 5.8 < 3.8 < 3.8 < 2.8 CAWW- 1915 4/25/2016 < 166 < 6.2 < 5.0 < 6.8 < 6.5 < 11.1 < 8.1 < 8.1 < 8.9 < 5.4 CAWW- 3971 7/28/2016 < 145 < 3.0 < 8.3 < 2.9 < 1.9 < 3.2 < 3.3 < 3.4 < 2.6 < 14.0 CAWW- 5607 10/17/2016 < 154 < 1.9 < 4.8 < 2.4 < 1.1 < 2.7 < 3.0 < 1.9 < 1.7 < 7.6 Location: CA-WWA-U1MW-010 CAWW- 117 1/8/2016 < 145 < 4.9 < 5.5 < 3.1 < 3.5 < 2.6 < 2.6 < 4.4 < 4.5 < 8.8 CAWW- 1851 4/12/2016 < 149 < 2.8 < 6.8 < 1.4 < 2.6 < 4.0 < 4.4 < 3.7 < 2.8 < 4.8 CAWW- 3758 7/18/2016 < 152 < 3.0 < 7.1 < 3.4 < 3.6 < 5.4 < 5.3 < 2.9 < 2.7 < 10.1 CAWW- 5606 10/17/2016 < 154 < 2.9 < 4.5 < 4.1 < 2.6 < 7.3 < 5.6 < 3.1 < 1.9 < 6.6 Location: CA-WWA-U1MW-012 CAWW- 256 1/13/2016 < 141 < 3.4 < 5.4 < 3.4 < 2.9 < 5.1 < 2.5 < 3.2 < 3.4 < 2.1 CAWW- 1916 4/25/2016 < 166 < 2.8 < 9.0 < 2.3 < 2.2 < 5.0 < 4.8 < 4.6 < 2.4 < 1.8 CAWW- 3972 7/28/2016 < 145 < 1.4 < 4.8 < 1.4 < 1.1 < 1.3 < 2.3 < 1.3 < 1.4 < 6.8 CAWW- 5787 10/18/2016 < 156 < 2.5 < 3.7 < 3.0 < 2.9 < 2.9 < 5.1 < 3.5 < 2.4 < 10.0 Location: CA-WWA-U1MW-013 CAWW- 82 1/6/2016 < 143 < 2.9 < 5.6 < 3.0 < 1.9 < 2.4 < 3.3 < 2.9 < 3.1 < 2.8 CAWW- 1649 4/15/2016 < 148 < 5.7 < 6.7 < 4.2 < 2.3 < 9.3 < 5.3 < 5.4 < 4.9 < 6.2 CAWW- 3754 7/18/2016 < 152 < 2.2 < 4.9 < 2.6 < 1.9 < 4.9 < 3.7 < 2.8 < 2.3 < 10.6 CAWW- 5604 10/15/2016 < 154 < 2.4 < 4.1 < 1.5 < 2.5 < 2.0 < 3.1 < 2.0 < 2.3 < 8.7 Location: CA-WWA-U1MW-014 CAWW- 203 1/11/2016 < 146 < 3.4 < 6.5 < 2.0 < 3.5 < 7.3 < 3.8 < 3.2 < 1.9 < 3.2 CAWW- 1850 4/12/2016 313 +/- 90 < 2.9 < 6.5 < 1.8 < 1.2 < 2.1 < 4.1 < 3.2 < 3.7 < 7.5 CAWW- 3551 7/11/2016 319 +/- 93 < 1.4 < 5.7 < 2.1 < 1.3 < 4.8 < 2.1 < 2.2 < 2.0 < 8.5 CAWW- 5428 10/6/2016 211 +/- 86 < 3.5 < 4.6 < 2.1 < 2.8 < 3.7 < 3.6 < 3.4 < 2.6 < 11.0 Location: CA-WWA-U1MW-015 CAWW- 116 1/8/2016 < 145 < 2.6 < 4.5 < 2.7 < 2.5 < 7.6 < 2.2 < 4.0 < 4.2 < 6.9 CAWW- 1647 4/15/2016 < 148 < 2.4 < 6.9 < 2.9 < 1.1 < 3.9 < 3.5 < 2.5 < 3.0 < 8.1 CAWW- 3757 7/18/2016 < 152 < 1.6 < 4.9 < 2.1 < 1.6 < 3.1 < 1.7 < 2.0 < 1.8 < 9.6 CAWW- 5602 10/15/2016 < 154 < 3.0 < 7.4 < 2.2 < 2.1 < 2.3 < 4.5 < 2.4 < 2.0 < 10.0 9-4

Table 9. Wells and Ponds (non-potable), analyses for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa Location: CA-WWA-U1MW-016 CAWW- 204 1/11/2016 < 146 < 4.9 < 9.3 < 4.9 < 5.6 < 6.6 < 6.5 < 5.5 < 5.1 < 6.0 CAWW- 1648 4/15/2016 < 148 < 4.5 < 7.6 < 4.5 < 1.8 < 4.6 < 6.0 < 4.8 < 3.6 < 10.0 CAWW- 3414 7/6/2016 < 149 < 1.0 < 2.6 < 1.2 < 1.0 < 2.7 < 1.8 < 1.2 < 1.6 < 3.6 CAWW- 5598 10/14/2016 < 154 < 6.0 < 8.7 < 5.4 < 4.3 < 11.2 < 6.1 < 6.9 < 4.0 < 4.6 Location: CA-WWA-U1MW-18 CAWW- 202 1/11/2016 < 146 CAWW- 1640 4/12/2016 282 +/- 86 CAWW- 3553 7/11/2016 173 +/- 86 CAWW- 5427 10/6/2016 < 151 Location: CA-WWA-U1MW-19 CAWW- 205 1/12/2016 < 146 CAWW- 1917 4/26/2016 188 +/- 95 CAWW- 3755 7/18/2016 < 152 CAWW- 5600 10/14/2016 201 +/- 83 Location: CA-WWA-U1MW-20 CAWW- 206 1/12/2016 < 146 CAWW- 1918 4/26/2016 < 166 CAWW- 3756 7/18/2016 < 152 CAWW- 5429 10/6/2016 < 151 Location: CA-WWA-U1MW-31 CAWW- 76 1/5/2016 680 +/- 103 CAWW- 1643 4/14/2016 846 +/- 110 CAWW- 3594 7/14/2016 818 +/- 109 a

CAWW- 5592 10/13/2016 4448 +/- 208 CAWW- 6772 12/9/2016 1944 +/- 149 a

Tritium reanalyzed with a result of 4,590+/-213 pCi/L.

9-5

Table 9. Wells and Ponds (non-potable), analyses for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa Location: CA-WWA-U1MW-34 CAWW- 77 1/5/2016 755 +/- 106 CAWW- 1646 4/14/2016 743 +/- 106 CAWW- 3591 7/14/2016 536 +/- 97 CAWW- 5785 10/19/2016 620 +/- 107 Location: CA-WWA-U1MW-36 CAWW- 78 1/5/2016 1036 +/- 116 CAWW- 1644 4/14/2016 966 +/- 115 CAWW- 3592 7/14/2016 707 +/- 104 CAWW- 5786 10/19/2016 889 +/- 117 Location: CA-WWA-U1MW-39 CAWW- 80 1/5/2016 < 143 CAWW- 1641 4/14/2016 < 148 CAWW- 3554 7/11/2016 < 147 CAWW- 5601 10/15/2016 < 154 9-6

Table 9. Wells and Ponds (non-potable), analyses for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa Location: CA-WWA-U1MW-47 CAWW- 83 1/6/2016 < 143 CAWW- 1453 4/6/2016 1373 +/- 129 CAWW- 3590 7/14/2016 620 +/- 101 CAWW- 5599 10/14/2016 597 +/- 102 Location: CA-WWA-U1MW-58 CAWW- 79 1/5/2016 1302 +/- 125 CAWW- 1645 4/14/2016 997 +/- 116 CAWW- 3593 7/14/2016 847 +/- 110 CAWW- 5783 10/19/2016 717 +/- 111 Location: CA-WWA-U1MW-59 CAWW- 118 1/8/2016 < 145 CAWW- 1865 4/19/2016 < 149 CAWW- 3759 7/20/2016 < 151 CAWW- 5784 10/19/2016 < 156 Inside Old Blowdown Pipeline CAWW- 283 1/18/2016 437 +/- 92 CAWW- 1864 4/19/2016 383 +/- 93 CAWW- 3761 7/20/2016 466 +/- 96 CAWW- 5605 10/17/2016 391 +/- 93 9-7

Table 9. Wells and Ponds (non-potable), analyses for tritium and gamma-emitting isotopes.

Collection Concentration (pCi/L) 3 54 59 58 60 65 95 134 137 140 Lab Code Date H Mn Fe Co Co Zn ZrNb Cs Cs BaLa Location: CA-WWA-U2MW-2S CAWW- 75 1/5/2016 < 143 CAWW- 1650 4/15/2016 < 148 CAWW- 3314 7/1/2016 < 150 CAWW- 5589 10/13/2016 < 154 Location: CA-WWA-U2MW-5S CAWW- 72 1/4/2016 < 143 CAWW- 1452 4/6/2016 < 138 CAWW- 3315 7/1/2016 < 150 CAWW- 5590 10/13/2016 < 154 Location: CA-WWA-U2MW-8 CAWW- 73 1/4/2016 < 143 CAWW- 1642 4/14/2016 < 148 CAWW- 3555 7/11/2016 < 147 CAWW- 5593 10/13/2016 < 154 Location: CA-WWA-U2MW-10 CAWW- 74 1/4/2016 < 143 < 7.3 < 9.8 < 2.8 < 2.7 < 6.7 < 7.8 < 6.1 < 3.9 < 10.9 CAWW- 1852 4/14/2016 < 149 < 2.6 < 6.2 < 3.5 < 3.6 < 3.7 < 4.5 < 4.9 < 4.7 < 4.6 CAWW- 3413 7/6/2016 < 149 < 1.2 < 2.4 < 1.4 < 1.5 < 2.4 < 2.1 < 1.3 < 1.2 < 3.6 CAWW- 5603 10/15/2016 < 154 < 2.8 < 4.7 < 2.9 < 2.0 < 3.9 < 4.1 < 2.5 < 1.8 < 8.7 Location: CA-WWA-U2MW-16 CAWW- 71 1/4/2016 < 143 CAWW- 1913 4/25/2016 < 174 CAWW- 3409 7/5/2016 < 149 CAWW- 5591 10/13/2016 < 154 Location: CA-WWA-F-005 CAWW- 69 1/5/2016 < 143 < 2.6 < 4.5 < 4.3 < 1.0 < 4.2 < 4.9 < 3.0 < 4.3 < 5.8 CAWW- 1455 4/5/2016 < 138 < 2.3 < 4.3 < 2.2 < 1.9 < 2.8 < 3.8 < 2.5 < 3.0 < 2.8 CAWW- 3752 7/13/2016 < 152 < 1.2 < 3.0 < 1.3 < 1.0 < 2.4 < 2.0 < 1.1 < 1.3 < 8.7 CAWW- 5371 10/3/2016 < 152 < 3.3 < 8.4 < 2.1 < 1.6 < 5.7 < 4.7 < 3.2 < 2.5 < 2.4 Location: CA-WWA-F-015 CAWW- 70 1/5/2016 < 143 < 3.1 < 6.7 < 3.4 < 3.5 < 4.5 < 3.9 < 3.7 < 3.0 < 3.8 CAWW- 1454 4/5/2016 < 138 < 1.6 < 5.8 < 2.9 < 1.8 < 3.6 < 4.2 < 2.9 < 2.0 < 6.8 CAWW- 3753 7/13/2016 < 152 < 2.0 < 3.3 < 2.1 < 2.2 < 2.0 < 3.5 < 2.5 < 2.2 < 5.5 CAWW- 5372 10/3/2016 < 152 < 3.1 < 3.0 < 1.9 < 3.0 < 4.8 < 5.0 < 2.7 < 2.6 < 6.9 9-8

Table 10a. Bottom sediments, analyses for gamma-emitting isotopes.

Collection: Semiannually Units: pCi/kg dry Location CA-AQS-A Lab Code Req. LLD CABS- 1595 CABS- 5882 Date Collected - 04-12-16 10-25-16 K-40 - 12530 +/- 614 14818 +/- 1026 Mn-54 - < 17.7 < 45.7 Fe-59 - < 54.0 < 127.9 Co-58 - < 19.3 < 55.4 Co-60 - < 6.8 < 26.3 Zr-Nb-95 - < 22.6 < 63.0 Cs-134 150 < 17.1 < 35.4 Cs-137 180 < 12.8 73.5 +/- 42.3 Ba-La-140 - < 52.0 < 283.3 Location CA-AQS-C Lab Code Req. LLD CABS- 1596 CABS- 5883 Date Collected - 04-12-16 10-25-16 K-40 - 14594 +/- 754 11855 +/- 520 Mn-54 - < 29.7 < 16.5 Fe-59 - < 46.0 < 40.3 Co-58 - < 33.0 < 22.7 Co-60 - < 23.9 < 15.9 Zr-Nb-95 - < 57.0 < 41.8 Cs-134 150 < 24.5 < 12.8 Cs-137 180 < 29.5 < 15.3 Ba-La-140 - < 109.9 < 102.4 10-1

Table 10b. Shoreline sediments, analyses for gamma-emitting isotopes.

Collection: Semiannually Units: pCi/kg dry Location CA-AQS-A Lab Code Req. LLD CASS- 1592 CASS- 5879 Date Collected - 04-12-16 10-25-16 K-40 - 14609 +/- 807 15261 +/- 841 Mn-54 - < 32.0 < 29.0 Fe-59 - < 96.4 < 94.6 Co-58 - < 38.4 < 31.6 Co-60 - < 16.2 < 21.9 Zr-Nb-95 - < 57.7 < 65.3 Cs-134 150 < 26.6 < 18.8 Cs-137 180 < 34.7 86.5 +/- 38.4 Ba-La-140 - < 78.5 < 67.4 Location CA-AQS-C Lab Code Req. LLD CASS- 1593 CASS- 5881 Date Collected - 04-12-16 10-25-16 K-40 - 14796 +/- 732 15475 +/- 746 Mn-54 - < 24.3 < 25.5 Fe-59 - < 56.0 < 44.8 Co-58 - < 29.3 < 33.6 Co-60 - < 13.1 < 19.6 Zr-Nb-95 - < 45.9 < 61.4 Cs-134 150 < 25.2 < 24.8 Cs-137 180 < 29.5 < 28.0 Ba-La-140 - < 75.9 < 133.1 10-2

Table 11. Fish, analyses for gamma-emitting isotopes.

Collection: Semiannually Units: pCi/kg wet Location CA-AQF-A Lab Code Req. LLD CAF- 1597 CAF- 1598 CAF- 1599 CAF- 1600 CAF- 1601 Date Collected 04-12-16 04-12-16 04-12-16 04-12-16 04-12-16 Sample Type River Freshwater Silver Carp Common Carp Channel Catfish Carpsucker Drum K-40 - 2449 +/- 372 2650 +/- 381 2832 +/- 369 3118 +/- 401 3431 +/- 411 Mn-54 130 < 10.9 < 11.5 < 16.8 < 21.6 < 19.5 Fe-59 260 < 37.7 < 49.2 < 61.8 < 42.3 < 31.3 Co-58 130 < 21.3 < 25.5 < 11.9 < 17.4 < 25.5 Co-60 130 < 12.0 < 6.3 < 15.9 < 15.7 < 9.0 Zn-65 260 < 20.0 < 32.5 < 19.8 < 32.9 < 19.5 Cs-134 130 < 16.8 < 17.6 < 15.0 < 15.8 < 18.2 Cs-137 150 < 11.2 < 9.0 < 13.7 < 13.3 < 15.8 Lab Code Req. LLD CAF- 5869 CAF- 5870 CAF- 5871 CAF- 5872 CAF- 5873 Date Collected 10-25-16 10-25-16 10-25-16 10-25-16 10-25-16 Sample Type River Freshwater Common Carp Blue Catfish Silver Carp Carpsucker Drum K-40 - 2808 +/- 378 2400 +/- 337 2988 +/- 443 3178 +/- 364 2895 +/- 410 Mn-54 130 < 11.2 < 12.8 < 13.7 < 14.7 < 15.5 Fe-59 260 < 33.0 < 25.5 < 47.3 < 35.5 < 47.8 Co-58 130 < 9.3 < 13.3 < 14.4 < 16.2 < 13.8 Co-60 130 < 9.9 < 10.9 < 15.4 < 11.7 < 8.5 Zn-65 260 < 20.5 < 25.4 < 27.7 < 28.4 < 15.1 Cs-134 130 < 14.9 < 14.3 < 18.1 < 15.3 < 18.4 Cs-137 150 < 12.9 < 11.1 < 18.7 < 9.0 < 13.5 11-1

Table 11. Fish, analyses for gamma-emitting isotopes.

Collection: Semiannually Units: pCi/kg wet Location CA-AQF-C Lab Code Req. LLD CAF- 1602 CAF- 1603 CAF- 1604 CAF- 1605 CAF- 1606 Date Collected 04-12-16 04-12-16 04-12-16 04-12-16 04-12-16 Sample Type River Freshwater Silver Carp Common Carp Channel Catfish Carpsucker Drum K-40 - 3026 +/- 433 3231 +/- 411 2926 +/- 416 3416 +/- 381 3145 +/- 394 Mn-54 130 < 18.1 < 11.5 < 17.8 < 14.3 < 17.1 Fe-59 260 < 65.1 < 42.3 < 64.7 < 58.0 < 68.3 Co-58 130 < 21.1 < 22.5 < 28.7 < 14.3 < 25.8 Co-60 130 < 12.7 < 14.7 < 14.7 < 9.3 < 11.2 Zn-65 260 < 21.3 < 18.3 < 19.5 < 14.9 < 27.8 Cs-134 130 < 20.5 < 14.8 < 15.8 < 15.8 < 19.0 Cs-137 150 < 14.4 < 18.0 < 15.7 < 14.5 < 20.2 Lab Code Req. LLD CAF- 5874 CAF- 5875 CAF- 5876 CAF- 5877 CAF- 5878 Date Collected 10-25-16 10-25-16 10-25-16 10-25-16 10-25-16 Sample Type River Freshwater Freshwater Common Carp Blue Catfish Carpsucker Drum Drum K-40 - 3532 +/- 488 2771 +/- 433 3058 +/- 478 2593 +/- 316 1915 +/- 336 Mn-54 130 < 19.5 < 13.2 < 19.2 < 11.9 < 16.0 Fe-59 260 < 32.5 < 29.7 < 64.0 < 28.1 < 44.4 Co-58 130 < 18.2 < 18.5 < 19.3 < 10.2 < 14.5 Co-60 130 < 19.3 < 12.2 < 17.0 < 11.4 < 11.4 Zn-65 260 < 17.5 < 21.3 < 45.8 < 15.2 < 18.2 Cs-134 130 < 18.0 < 17.7 < 19.2 < 12.2 < 15.2 Cs-137 150 < 16.4 < 18.5 < 13.1 < 12.1 < 10.0 11-2

Table 12. Direct Radiation (quarterly exposure)

Location Gamma Dose (mrem/90 days)

QTR 1 QTR 2 QTR 3 QTR 4 CA-IDM-1A 16.24 15.81 15.88 16.22 CA-IDM-3 16.76 16.46 16.73 17.02 CA-IDM-5 15.19 13.35 14.50 14.27 CA-IDM-6 16.35 15.34 16.12 16.52 CA-IDM-7 16.39 15.97 15.02 16.05 CA-IDM-9 14.78 14.10 15.08 15.65 CA-IDM-10 17.69 16.23 16.43 17.28 CA-IDM-11A 18.54 16.31 18.71 17.19 CA-IDM-14 16.85 15.69 16.17 16.32 CA-IDM-17 16.16 15.15 15.62 15.77 CA-IDM-18A 16.29 15.49 15.81 16.03 CA-IDM-20 16.43 16.11 16.12 16.99 CA-IDM-21 16.35 15.31 15.94 16.10 CA-IDM-22A 13.16 13.13 12.56 12.41 CA-IDM-23 16.89 16.16 16.55 16.15 CA-IDM-26 (C) 12.20 11.14 11.32 11.84 CA-IDM-27 (C) 17.54 16.44 17.01 18.25 CA-IDM-30A 16.34 15.22 17.96 15.26 CA-IDM-31A 16.69 16.40 16.89 16.67 CA-IDM-32 17.01 15.41 16.21 16.39 CA-IDM-32A 15.86 14.80 16.54 15.20 CA-IDM-33 15.95 NSa 15.70 16.49 CA-IDM-34 16.26 15.56 16.13 15.14 CA-IDM-35 15.11 14.41 15.15 14.62 CA-IDM-36 15.36 14.32 15.07 14.53 CA-IDM-37 15.61 15.67 15.54 15.65 CA-IDM-38 11.84 11.09 11.32 11.17 CA-IDM-39 16.08 15.82 14.97 15.43 CA-IDM-39A 16.27 16.13 14.50 16.18 CA-IDM-40 17.13 17.25 15.68 16.81 CA-IDM-41 16.44 15.82 14.08 15.80 CA-IDM-42 14.56 13.27 12.58 13.44 CA-IDM-43 16.42 15.59 14.38 15.19 CA-IDM-44 16.26 15.10 14.45 15.76 CA-IDM-45 14.22 14.41 13.83 14.59 CA-IDM-46 16.69 16.03 15.26 16.30 CA-IDM-47 15.71 14.76 14.87 15.28 CA-IDM-48 16.80 15.82 16.09 16.31 CA-IDM-49 15.99 15.00 14.58 14.75 CA-IDM-50 16.38 15.77 15.45 16.07 CA-IDM-51A 17.29 16.49 15.20 17.24 CA-IDM-52 16.89 15.98 15.26 16.29 CA-IDM-60 (C) 16.17 16.12 13.80 15.79 a "NS" = No sample; refer to Part I Table 5.5, Missed Collections and Analyses.

12-1

Table 12b. Direct Radiation Neutron (quarterly exposure)

Location Neutron Dose (mrem/91 days)

QTR 1 QTR 2 QTR 3 QTR 4 CA-IDM-60N (C) 0.0 0.0 0.0 0.0 CA-IDM-61N 0.0 0.0 0.0 0.0 CA-IDM-62N 0.0 0.0 0.0 0.0 CA-IDM-63N 0.0 0.0 0.0 0.0 CA-IDM-64N 0.0 0.0 0.0 0.0 12-2