Text

Forwards 931108 Application for Renewal of NPDES Permit IL0048151,per Section 3.2 of App B of Licenses NPF-11 & NPF-18
	ML20058K194
Person / Time
Site:	LaSalle
Issue date:	12/03/1993
From:	Benes G; COMMONWEALTH EDISON CO.
To:	Martin J; NRC OFFICE OF INSPECTION & ENFORCEMENT (IE REGION III)
References
	NUDOCS 9312140467
	Download: ML20058K194 (104)
	v • d • e

{{#Wiki_filter:. _ C:mm:nwrith Edisin .2! 1400 Opus Placs Downers Grove, Illinois 60515 i i t t l December 3,1993 l i Mr. J. B. Martin t l Regional Administrator, Region lil I i U.S. Nuclear Regulatory Commission 799 Roosevelt Road Glen Ellyn, IL 60137 1 l

Subject:

LaSalle County Station Units 1 and 2 f Renewal of NPDES Permit i NRC Docket Nos. 50-373 and 50-374

Dear Mr. Martin:

3 t Commonwealth Edison Company is the holder of National Pollutant Discharge - Elimination System (NPDES) Permit No. ILOO48151 for LaSalle County Station. Section 3.2 of Appendix B (Environmental Protection Plan) of Facility Operating Licenses NPF-11 and NPF-18 requires that a copy of the application for renewal of the NPDES permit be provided to the NRC. Enclosed is LaSalle County Station's November 8,1993 applicatio for renewal of NPDES Permit ILOO48151. i Please direct any questions regarding this matter to this office. I i Respectfully, t i Su-9 EBw Gary G. Benes Nuclear Licensing Administrator Enclosure cc: NRC Document Control. Desk 7 i A. T. Gody, Jr., Project Manager - NRR l D. Hills, LaSalle Senior Resident inspector - NRC i a NPDES.LTR J 9312140467 931203 35 PDR ADDCK 05000373 9 1 P PDR Q li f L I

Commonwealth Ed!aon One First Natonal Plaza. Cheago, Illinoes Adcress Reply to: Post Offee Box 767 i Chcago, lihnois 60690 0767 November 8, 1993 CERTIFIED MAII: Mr. Thomas G. McSwiggin, P. E. Manager, Permit.Section Division of Water Pollution Control Illinois Environmental Protection Agency 2200 Churchill Road Springfield, Illinois 62706

Subject:

Renewal of NPDES Permit No. ILOO48151 LaSalle County Generating Station

Dear Mr. McSwiggin:

Commonwealth Edison Company hereby submits two copies of Consolidated Permit Application Forms 1 and 2C for the renewal of the subject permit. As confirmed by your letter dated April 22, 1993, the only Form 2C--Part V-A pollutants reported are those required by the station's existing NPDES permit, and no analytical data is presented for outfalls 001(d)--Cooling Water Intake Screen Backwash (Cooling Pond), 001(f)--Auxiliary Reactor Equipment Cooling and Flushing Water and 002--I111nois River Make-Up Water Intake Screen Backwash. Pollutant levels for all permit-required parameters were derived from station data reported from August, 1992 thrcugh July, 1993. In most cases, all other pollutant data. only one analysis was conducted for All color analyses were performed as i "true" (i.

e. the samples were centrifuged prior to analysis).

Mass load values were calculated using average flows. No recent analytical data is available for outfall 001(a)-- Radwaste Treatment System. The last discharge'from this outfall occurred in June, 1992. Form 2C, Part V-A information is provided from this single occurrence. While discharge from this outfall is expected to remain a very infrequent event, we do wish to retain the ability to use thin outfall point in the future. Therefore, the last permit renewal round have been included. analytical results from While this data is too old to be considered " valid", we believe that the parameter values are still representative of the discharge. Should this discharge resume on an intermittent barsis in the future, we will provide new Form 2C data for the Agency's review. 1 i j

8 l l . j Form 2C--Part IIB requires descriptions of wastewater treatment processes. While outfall.001--Cooling Pond Blowdown, receives no treatment as wastewater, the circulating water is treated with carbon dioxide for scaling control prior to entry j. into the station's main condensers. i House service water, which is a subwaste stream of outfall 001, is. treated with sodium hypochlorite, sodium bromide and polyacrylate for macrofouling control. No chemical treatment is applied to outfall 001(d)--Cooling Water Intake Screen Backwash, 001(f)--Auxiliary Reactor Equipment Cooling and Flushing Water or outfall 002--Illinois-River Make-Up 3 Water Intake Screen Backwash. I - i Domineralizer Regenerant Wastes (outfall 001(a)) consist of excess sulfuric acid, excess caustic and rinse water used to regenerate the ion exchange resin beds which supply ultra-pure i water required for the generating process. In addition, hydrogen peroxide is applied for iron removal, as needed, at a rate of i 0.2 gallons per minute. However, due to hydrogen peroxide's reactivity, it is not expected to be present in the discharge. As noted in the permit application, chlorine is applied as a 4 disinfectant to outf all 001(b)--Sewage Treatment Plant Effluent. Anionic and cationic polymers are applied as treatment chemicals I to outf all 001(c)--Wastewater Treatment Plant Effluent. In addition, a small amount of sulfuric acid or caustic may be used I if pH adjustment is required. i There also exists the slight possibility that m'small amount i of nitrites may be discharged from outfall 001(c) when the station's closed cycle bearing cooling water system is drained-for service. This system is treated with 400'ag/L nitrites occurrences of release are expected to be very rare.. In the-- past, the' system's 5000 gallon holding tank has discharged, at most, once per year. Due to the fact that the system discharges into outfall 001(c) and that nitrites degrade rapidly under aerobic conditions, we believe that the-environmental impact of this discharge is minimal. 1 A dilute organic cleaning solution may be discharged through outfall 001(e)--Radwaste Treatment System Effluent. Due to the small amount used (approx. 5 gallons per month), ane*_ the fact that it combines with an average discharge flow hem this cutfall of 0.005 MGD, it is not expected that large amounts of this solution will be present. (copies of all pertinent Material Safety Data Sheets.(MSDSs) have been included in this submittal). r

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9 I I We have voluntarily elected to perform polychlorinated { biphenyl (PCB) aroclor screenings of all wastewater discharge points as part of our NPDES permit renewal' sampling program. (Analytical data is presented under Part V-C--Pesticides). While we do not expect any PCBs to be present in any of these outfalls, I we felt that this screening would provide definitive information i to justify our belief and provide evidence that we are in full compliance with all NPDES regulations in this regard. If there are any questions regarding this submittal, please contact Ms. Julia Wozniak of my staff at (312) 394-4468. Sincerely, f i ,? v/ Jeffrey P. Smith Supervisor of Water Quality Attachments (2 copies) 1scaper.ltr jpw/jps/dc i i

I 1 We have voluntarily elected to perform'polychlorinated f biphenyl (PCB) aroclor screenings of all wastewater discharge points as part of our NPDES permit renewal sampling program. j (Analytical data is presented under Part V-C--Pesticides). While [ we do not expect any PCBs to be present in any of these outfalls, i we felt that this screening would provide definitive information i to justify our belief and provide evidence that we are in full compliance with all NPDES regulations in this regard. If there are any questions regarding this submittal, please contact Ms. Julia Wozniak of my staff at (312) 394-4468. lincerely, l [/1 r off P. Smith Supervisor of Water Quality Attachments (2 copies) j i bec: J. V. Schmeltz P. T. Nottingham R. H. Varju J. P. Wozniak (2 copies) Director of Nuclear Licensing Files W-01-PER-H2 l i 1sesper.ltr l jpw/jps/dc 1 (

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a,,., i e i i .s . i i... i i i i i 9(Rt i I9 I - e; .i. m i l Attrcn to this appucation a topographic map of the area extending to at least one male beyond property boundenes. The map must shour the outhne of the fachty, the location of each of its existing and proposed intake and discharge structures, each of its hazardous weete { treatment, storage, or disoosal incalities, and each well where it injects fluids unoerground include all springs, revers and other surfeos j water bodies m the map aros. See instructions for preose requirements. GDIERATIOR AND DISTRIIRITION OF ELECTRIC POER 4 1 1 4 I I certsty unorr peneMy of low that I how personauy examoned and am familier wrth the informenon submitted in this a0ptication and all strachments and that, based as my inquiry of thour persons smmediately reaponenbde for obamming the informenon contained in the applocation, I beliew that the informenon is true, accurr's and compsete. I am senere that there are significant penatoen for submrttmr false information, including the possrbility of fine arv. nonsonment. A

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f y,g,*Q,j"**' .. o e se n ice... 001(b) l Sewage Treatment Plant Effluent I 0.0228 MGD l Equalization.ActivatedSludge. l x-I l 3-A l l Sedimentation. l lI-U l l l Sedissentation Disinfection. l 1-U l2-F j l l l Sludge to Aerobic Digestion.. l 5-A l l Drying Beds. On-Site Storage { 5-H l I-I I l l l I i l I I I l 001(c) ; Wastewater Treatment System Effluent l 0.018 MGD l Gil/hter Separation, g I-T g > (Turbine Building Fire and Miscellaneous l Oil /hter Separation. l I-I l Nonradioactive Waste Sime. l Equalization. Coagulation l I-I l 2-) Demineralfier Make-up Water Filter i l Flocculation. Sedimentation. l 1-G ll-U l Backwash. Diesel Fuel Stoarge l l Multimedia Filtration. l l-Q l l and Service Water Building Susso. l l Sludge to Drying Beds, l 5-H 1 l Auxiliary Boiler Blowdown. l On-Site Storage l I-I Demineralizer Rm.; rant Waste. I l l Water Sof tener Regenerant Waste). l l l l l I I I I l l l 001(d)l Cooling Water Intate Screen l l Screening g 1-1 g ! Backwash (Cooling Pond) j g g g i I l l l i I l 001(e] Unit I and 2 Radwaste Treatament l0.0050MGD** Fabric Filtration or tvaporation, g.g gp lSystemEffluent

# l(Yalue froe l Equalization or Evaporation, g

A-A 4-t l (Equipment drains in the Turbine l previous permit llonExchange.lonExchange g z-d z-J l Building. Auxiliary Building and j application) Equalization. Recycle Reuse of A-A 4-L l Reactor Building. Floor Drains in [ Treated Effluent g g } the Turbine Building. Raowaste Building l g l Auxiliary Building and Reactor l l l ! Building. EMnsate Polisher Wastes l g l from the Turbine Building; Decontamination } l g l and Laundry Maste l l { l i i i i l i I J l sea so-m n.tr o. v esi

1 * .,n ..u. a. = can.c.,ynr.m e m ,o,,. -,

-= a.or asssas e eat or evos sa me uawumma erums on,,

ILD000803643 O_7u paans ^ apruoavsourpour pumarrTaasuusenses naarannvan i u.a. e =via r. _., a m - _. -.. -.asse, sp p. 'arr '4g- @ , EXIST 1NSMMRAFACTURgggg twinanammes a e nasasssamaasn gLyggggg, N Conmemensa permars hoorer, j ..our I 2 * * * " ' " * " ' C O "'" '

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'*II,N .. oes =aeso esass l * ^ ",, * " * * ", ',, ', * " f T,**,98j"*" .. os c.,,,.. 001(f) e Auxiliary Reactor Equipment l Evaporative Heat Dissipation l K-I l l Cooling and Flushing Water l l l l I i i I 1 l l 002 Illinois River Make-Up Water l Screening. Discharge to Surface l 1-T l 4-A 4 Intake Screen Backwesh l Water l l i l l l I I l 1 l l I i l l l l l l l l 1 l l 1 l l I I l I I l l l l l l i I I I l I I I I I l I i I I I I I I I l i l i l I I u I i l l I I l [ l l l I I j t I l l 4 i t I I l l l l l l 1 l l i l l o........ o .. ~...,... EPA Form 3510-2C (Rev. 2 86) e a e c- .a- .r

]

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.>rm,,coroveo g.pA e.o. nuustn ocopy trom stem a ur f orm t o s

MB tio 20404086 CONTINUED FROM PAGE 2 A. B. & C: Les enstructions oefore proceeoing - Comoiete one set of taoles for eacn outtatt - Annotare the outtall numoer m the soace proveceo.

NOTE: Tabies V.A. V B. ano V-C are mcruaro on seoarate snects numoerea V.1 througn V-9. i D Use tne soace Deiow to sist any of tne posiutants testeo m Table 2c 3 of the instructions, wnicn you know or nove reason to beneve as ursenaroeo or may De J a.scnargeo from any outtail. For every poHutant you sist. Driefly cescrioe tne reasons you beierve st to be present ano report any analytical cata en yout 4 Dossession. I 2 ' PO LL UT a N T - sOURct i poLLufANT I . SOURCE d ? i H/A N/A 4 i 1 l l .I i l 1 l d i l is any ponutant sisteo in stem V-C a suostance or a component of a substance wnsen you currentry use or manuracture as an intermooiste or final proouct or byproduct? T vgo that en suen coautants attown T mo tso no item VI-Bb 4 4 6 1 I } N/A \\ 5 ) i I i f l J i l i t i i i t a ? I ] EPA Form 3510-2C (Rev. 2 85) P AGE 3 Cr a CONTINUE ON REVERSE

CONTINUED FROM THE FRONT .M i 1 00 vou neve any etnomneogo or receon to boicwe tiet sny osonogicas t%st for acute or cntonic scascaty nas poen moos on env of your cancharges or on s ] eceeving wat*r in reistoon to your Erscharge witnen the Rs13 veers? j

vts ennenrefv ihr restens ana descesbe these cuenoses briows (No tea to Seetson VT!!b i

j i i l ft/A 8 i

s h

) 4 J e i l l l s l i l 2 l q l ..ere any of tne aneivses reoortec'en 6 tem V oertorrnea Oy a contract saporatory or consusting term? l' v s s elast the name. audress. anu retronone numser or..and poolutan ts . No eso 80 becewn LXI anamra kv. sacn nuen naoororoev ne rurws ortown a

6. T E LE P H O N E U. FR bbW T AN T E AN A Lv Z ED a %AME g AQOgggg

'orre root at .o rs # ersf e EP:S Heritage Laboratories. Inc. 1319 Harquette Drive (815) 378-1600 All Outfalls: Romeoville. Illinois 60441-4054 Radioactivity { .l i a j i l l i ) 1 i i 1 i, 4 IX. CE RTIFICA TION i a i cecrity unoer pensolv re ow ahet this cocument ena sit attachments were prevered unoer my arreCroon or supervossen on ectorcance worn a system oesignec to assure ther custofordpersonneraroverty gather sna rvatuste the ontormation submarred. Besoc on mv eneurry of the nerson er persons who manage une s ystem or inose persons offeCilv responsible for gatherong Ene informstron. tne entormstron submittedIs. to Ene best of my knowoedge gnobeforf. True. OCCurate. and Comotete. i om eware snat there are sognitocent pensstres for submityg terse mtormaroon. oncrucong the possobrirty of tone enc omprisonment for snowar>g vuototrons. q' - g o.. o e o ... c. o r e, c. r i r u., w....,.., .a r,,o,...... Robert J.14anning y 74 - // /Gk ! (312) 39h-2901 Senior Vice President (18 'a f I / o oave sinuto j e s ec, = a v u a r 4 4 EPA Form 3510 2C (Flev. 2 851

actsora ii

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ill et n t s em-awme das-l ,E5g# ogjl5wE $! t t n aey nrS-f,'" 58g*c=[ i E* ia l 0S i y T n t =; ga;" I n n ere ni o ie m li a WWa t tak at l s zn r r in eo a e aT tI " r a taa u T n Wa r q /p _C E tie l Os !%)m$";,2a d f nn fi r c e )5 ow m)e a a 9 d" 0 Po 1 i e r g ' n" i m ",S ol 00 0 gdt3 o ) oi t t o ro 0 in 8 t r ar c n S ac co S .d .( t r ( l 6 j a o e,t Snn q*44 i e ( o eWt i o e (3 e I aee l c E r C wr,0 M C f fv l l 0 cga e O mo f

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oi s cv ~ &ne e. n r r g s e r e dpn e epes r yo e v eu a c eS n mh U S imro h ni o ne s u R H s o c at e sPP cO- ~ r pac "P du sH-id mtt n o ~ i ~ t o oH ~ n CSam c e c e n ye ~ o r ot ) s h b8 s nc n i 2 e 1 l u S,g k

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lasalle Station Cooling Pond Blowdown ~ i o nuM us u,,..o., tr.;m ri.:,. s or vorm i l'lE ASE PitINI Ofi I yl'l If a iHL hrOH ALJL O AHL A5 OfJt Y Y u.e ni.n H poe I wme..e.sH id pp,,,,4,,,,,,,,, thes infoemat.on on seper.He sl. eels fuse the serp.< forntar1 ensteJef ni cumptermg th se pa pes Ill1000803643 rw8

1mo ms9 St t INS 19tt tC1 trMJS Amve' * *swe s 9 2 J I 8 5 uu s e AL t. No V. lNJAKE AND E FF L UENT CH AR ACTE RISilCS kontmued from page.7 of Fr><.n 2 C1 001 l

PART A You must provide the results of at least one analysts for every pullutant in this table. Complete one table for each outfaff. See instructions for additional details. l 2 E F Ft_ tj E N T

3. If NITS 4 IN T A M E (optremalt b iiani

{sgv vaLui TWWyMdg'VAEUE terwr, er bsmH I. Q' t. UTANT e mea n0MteM onet y vatus g _, u._me e. 6cet ..... eL.... ul -... -. eL.,.- o f -... ~""- V-a"= " ~ ~ ~ .... r,...... ul -.. ~ " " ' Uemend l (. C*' n Demend

c. Tant Orsen6c coresen (70C3

8. Tstet ev.pende.8 sothea(Tass

s. Ammero (es us

f. RW.

v an ut v m s' u t vatut vatut 61.68 51.45 36.83 365 ItGD g.T., e,,,, u vre 5.90 3.50 2.75 365

C v^'"'-

a,. V a t tit V altiL VaLuL 7;,T N '" vaLUL 33.05 30.69 27.66 365 'C b. MSNtMifM Ma ntMuM MONtMuM M a M 0 mum e pH, 77 8.7 7.7 8.7 52 ST AND ARD UNITS ~_

p. which le limited either ditoctfy. or indirectly txe agressly. in en oNIuent limitotions Guideline.You must p columia 2e, you must provide quantitative dote or en e9 enetion of their presence in your discherge. Complete one table for each outfell. See the snetructione for addit 6onal dete at.

5 i. e g

a. n;mseet 'a

3. EFFt.U E'N T

a. UNITS

5. TNT AKE (opshmai)

C O. ,e,y b,yy

e. Maxemeuhe pasLv vaLuz

b. M a n tegegogyvaLut c.LONG Tygg. Y ALL,E 4 go o,.

4Long T4sv g,,, (fr ese; n.. ....,,,,,l',8,,,,,,, pl -e.. ,,,,,, t,l.,,,,, bl.... ,,,,,,l',,,,,,,,, vi-... veea a n n L. b Mass . " a, 'o " a se m a. ,,,,,, !,'J..,,,,, of... yeae a premhse fassee<,7 e, I 0.5 153.58 I og/l Ib/ day 0.5 1

b. Chlorine, I

0.14 43.00 totes gei 4 og/1 lb/ day 0.21 4 a.cygt I 18 I Pt-Co 25 1

f.f, ej I

.. + fi I 0.50 153.58 1 ag/l Ib/ day 0.32 1 e

f. N8erece--

I 0.45 138.22 tioque ppe N) I ag/l Ib/ day 3.76 1 EPA Form 3510 2C (Rev. 2 85) P AG E V CONTINUE ON REVERSE

g ITEM V tl CONilNtif D $ imM f HON T 8 MAKM 4.,Q,, 'A'

3. EF FLUENT

4. U NIT 3

5. INT AME (oprimerff

3. POLg.Uy.

CTDNET N EEUI~ D " A"'%,$%,Y V 3'LU'l , @% Q'y yIg

e. unatuuM D Alt.T V ALut u

y .g e p o ..... f,i..... i.i... .... DJ..,.. i.... ..., t!,,,,. i,i... yuo .... E!.... ..i... yeeo tv =*w

==a I.me.e.n. I 1.6 491.46 I ag/l Ib/ day 1.1 1 ew ore ng le NI

a. n w.e

("yh [f'ay I 0.08 24.57 I ag/l Ib/ day 0.41 1 l.nesseeetwey I11 Alpbe. Yew I <3 I pCl/l Ib/ day <3 I (21 Sete. Tow I 5.5 1 pCl/l Ib/ day <4 I O meetum, T** I (1.0 1 pCi/l Ib/ day <l.0 I p radium ate. Totes I (1.0 1 pCi/I ib/ day ( 1.0 I si. 9= ween "enes '7e el d I 98 30.101.9 I ag/l Ib/ day 55 1 ti L Sulfide fee #1 I I stenose al e.eurfectente I <0.01 <21.50 I ag/l Ib/ day <0.G7 I a Ahasselnum. [,*,*,,',,,, I 0.4 122.86 1 mg/l Ib/ day 1.9 1 ,T,** I <0.1 (30.71. I ag/l Ib/ day 0.2 1 , 3, t,oged I 0.11 52.22 1 mg/l Ib/ day 0.11 1 m,

f. GeheIL 7,'W I

<0.05 (15.36 I mg/l Ib/ day <0.05 1

teen. Totet

[yessee e3 I 0.33 101.36 I mg/l Ib/ day 2.08 I s --- T*W I 35.4 10,873.5 I ag/l Ib/ day 22.4 I (743s 98 4) u_ _., _ _- _. _. I <0.2 (61.43 I ag/l Ib/ day <0.2 1 Teene tress se il i I <0.03 <9.21 I ag/l Ib/ day 0.07 1 g,,,'

e. Ten. Teest (74 etat-si I

<0.8 (245.73 1 mg/l Ib/ day (0.8 1

s. Yleenham, f***'

I <0.8 (245.73 I ag/l Ib/ day <0.8 1 (7440 334) j. EPA Form 3510-2C (Mov. 2 85) """'I " * " # #" Y'3 i

Cooling I'ond Blowdown trA e o auust n chiitr'om frem J of Form #; ouir ALT riuuu't u o.e m Appro.ed 11D000803643 001 U"3 *o N W5 9 CONitNtflD F 7 TOM P AGE 3 OF F 084M 2 C dPP'" or e peres 72 3 r s$ l' ART C - if you ere a primary indusery and this ouiteticontems process westeaeter. :efer to f abis 2c-2 in the instructions to determine which of the GC/Ms frecieons you must test for Mark X"in c 2 e for all such GC /MS fractions that opply to your industry and for ALL tousc metals, cyonidos. and totalphenots if you are not required to mark column 2 e(secondary industries, nonpsoces westoweter ourforts. end nonregterred GC/MS frectronsl, mark **Xin column 2 b f or each pollutent you know or have reeson to behave is present Mark X"in column 2 e for each postutent y believe is absent if you merk column 2e for any pollutent. you must provede the to suits of et least one snelysis for that pollutant if you merk column 2b for any pollut ent, you must provide the t of et least one enetysis for that pollutant if you know or have reesen to beheve et wot be descharged m concenuations of 10 ppb or greater. If you mark column 2b for acrotem, scrytom dinitrophenol, or 2-methyt 4,6 dinitrophenol. you must provide the results of et least one snelysis for each of these pollutants whech you know or have ressort to believe that you discha ccficentrations of 100 ppb or greeier Otherwise. for pollutents for wtnch you mark column 2b.you must either submit et toast one enetysis or bristly describe the reasons the pollutantis espected to t be discharged Note that there are 7 pages to this part, please review each carefully Complete one tobte(ett 7 peges) for each outteil See instructions for additional details and requirements I. LLtJTANT a.uann*x*

3. ErrtutHT

4. UNITS

5. INT AM E foprioereif E

!JJ' I. * *d.01. * " " " ' " " " * * ' " " " "

"""NI N N NEI 4 "u,.' ecoacan ddt(($"nTC "fd? filmessiew .g W .. J. w,,,, j,'),,,,,,,,, so.... ,,,,,, j, ),,,,,, so.... ,,,,,,1,'),,,,,,, ses.... vses '"*N" t, I' Qyy,c ',e t.t... vses RAWMLS, CYANIDE, AND TOTAL PHENOLS h.fg",$"$o, a <0.5 (153.58 I ag/l Ib/ day <0,5 1 f, 'a"s"h' **' X 0.003 0.921 I sig/l Ib/ day 0.002 1 Wo. Iir) X <0. <3.01 1 ~_ og/l Ib/ day <0.01 1 '",,,((,%3,, I <0.0002 <0.0614 1 mg/l Ib/ day 0.0006 3 47 3) X 0.003 0.921 I ag/l Ib/ day 0.004 3 .if x <0.002 (0.614 1 ag/l Ib/ day 0.009 I x <0.003 (1.536 1 og/l Ib/ day <0.005 1 _. _. ~ h*8 ',y. Totei I <0.00005 <0.on'$e I ag/l Ib/ day 0.00039 1 f y, **' _X _ 0.004 1.2286 1 mg/l Ib/ day 0.010 1 '2 S2p I <0.001 (0.301 7 I ag/l Ib/ day <0.001 1 mee f,%s X 0.0001 0.2150 I ag/l Ib/ day (0.0006 1 t 2u. Theemm. I <0.001 <0.301 Tew 0940 as os I sig/l Ib/ day <0.001 1 l,%zg,me' X <0.02 <6.14 I agh Ib/ day 0.05 1 .1 i ees. cyenso.. I <0.006 <2.457 ,,jrI lb/ day <0.006 4 toeot {pa st i 4 f***. I <0.005 <l.536 4 agi/1 lb/ day (0.005 4 . 2,3,7,B.7,ers osecnesanasutis . shlorossemento P- ' Dieuln f17940t el g i f EPA Forwt 3510 2C (Rev. 2-96l PAGEV.3 CONTINUE ON REVERSE

g cONTINtlE D F HOM THE F HONT 1.POLLUTCMT

a. mann n-

3. EF FLUENT

4. UNITS

5. INT AM E poprioneff Ef4 MSS

.:r ". ::.J.m a =a =ua na v a'um " ""i0 510'/# ""' ** "".AWX5Mrf"..". '7's. o'

~ _aM&'inVa" dug g? . conc ~ mav'oa ore ..w, 3

n

.=,,,,,,, e),,,,,,, i.i.... i.g,, n-- i,i... v.e. ,,,,,, t),,,,,,,, ,,,,,f,,,,_ i,. v. GCJteS FR ACTION -VOLATELE COMPOUNDS x <100 <30.716 1 og/l Ib/ day (100 1 ,',V,^y*," -. ~. 3v. Acrytonftrete X <100 00.726 1 ug/l Ib/ day (100 I (ty121) sv. mennene (71-48 1' I <5 (1.536 I ug/l Ib/ day <5 1 ev. (.ie tonsoro. m eenyr; seer g is434811 Sv. eremotorm (7s se si I (5 <1.536 I ug/l Ib/ day <5 1 ev. Corben 7 "',*7,'" I (5 <l.536 I ug/l Ib/ day <5 1 Fv. cheer.nennene (tos ee 71 X (5 <l.536 I ug/l Ib/ day 45 1 ev. Chlorods-X <5 <l.536 1 og/l Ib/ day <5 1 ov, chaereethene (7s4641 I <10 <3.072 I ug/l Ib/ day (10 I tov. s nos o-8 '**' I <10 <3.072 1 og/l Ib/ day <10 1 3 11v. cheeretorm L7404) X ($ <l.536 1 og/l Ib/ day <5 1 tav. otshooro-N I <5 <l.536 1 og/l Ib/ day <5 1 III-II4 tav. Olsbloro-effhseremechene 3 (75 71 49 14V.1.1-Olchloro-eihene ps-344ts I (5 <1.536 1 og/l Ib/ day <5 1 tev, t.ssolchsore. g lje74e4) X (5 <l.536 1 ug/l Ib/ day <5 1 t#V.1.IDechloro; eevieng (7s se 41 X <5 <l.536 1 og/l Ib/ day <5 1 17V.1 Diehlero-(?p47 el I (5 <1.536 1 og/l Ib/ day <5 1 ter.11aesseme-psyves9 pes M48 I (5 (1.536 I seg/l Ib/ day <5 1 tev. E mysbeneene X <5 <l.536 1 og/l Ib/ day (5 I gloseg4: sov,ase m ys

e q l740sel I

(10 <3.012 1 og/l Ib/ day (10 I siv'. hvi Cheeries g74 a7 3) I (10 <3.072 1 ug/l Ib/ day (10 1 epa Form 3610 2C (Mev. 2 est PAogv.a CONTINUE ON PAGE V

I ...,,....a, u t.. i -. i

e. o e i...

6 CON IINt16 Ie & 640M PAGE V.4 I1D0008030643 00I ""^'d-Anne.W e.".ruo g rJ H w I. POLLUTANT a m a n.i a - AND C AS a

t. t f L e s L N T 4 UNITS 5 IN T A M E (.,pra.=wl; N U M ZE ft

l,1 l'

','. M, h *','. f MAm!uug past, yatut b u n n eu t)u,,, s,$M,y c a.o rn, s,e,, te,u,., Oj W s a t it s a t.as t p ie ie 4 a n u r, i s n u s i.t.e.o.a.c.% L mn _ .',",(( ' ter me846h s .t T.*.. ..L e.s .__a,,. l e,.... .to.. ,o.... ........a. : e (unu n a v u! ,,,,3, 'aama ,a , s. 5 e,s... vsas OCAAS FC ACTION ~ VOL ATILE COMPOUNOS ag,.iro.._.o .~ 22v. u2thvien. chio,ide 17s ce 2: I (5 <1.536 1 ug/l Ib/ day -<5 1 23V.1.1,2.2 Tetra lEQ'"* I <5 <l.536 1 ug/l Ib/ day <5 1 2tV. Tttrechloro ethvten star.1e 4: I <5 <l.536 I ug/l Ib/ day <5 1 26V. Tohsene (tosas si I <5 <1.536 1 ug/l Ib/ day <5 1 20V.1.2 - T r ens ~ ~ ~ ,D,'d* ,jjhY'*"* I <5 <1.536 I ug/l Ib/ day <5 1 2 7 V.1.1.1 - T r 4 jy,'*g')f** I (5 <1.536 I ug/l Ib/ day <5 1 28V 1.1.2 Tst jyyy'"' I <5 <l.536 1 ug/l Ib/ day (5 I 29V. Talch8ero-

thvien. gip os e I

<5 <l.536 1 ug/l Ib/ day <5 I 3oV. Trichtoeo-theorometitane g (76-est) 31V. vin I chiorio.[rs os ai X (10 <3.072 1 ug/l Ib/ day <10 1 GCAS FftACTION - ACID COMPOUNDS ~ ~ - ~ i 1 A. 2-Chloropheno sesaFce X <10 <3.072 1 ug/l Ib/ day <10 1 2 A. 2.4 Dichloro ch.noe t t20 s3 2 I <10 <3.012 1 ug/l it / day <10 1 e_.._

34. 2.4 D6 methyl-ph.not (10s 87 96 X

<10 <3.012 .I ug/l Ib/ day (10 1-(A 4.8 Olrutto O. Cresos asse s2 sp I <50 <l5.358 I ug/l Ib/ day (g I ~ s4. 2.6 Dinitro. ph.nos is3 2s s X <50 <l5.358 1 og/l Ib/ day <g i ISA. 2 Nittwhenot j gee is si I <10 <3.012 1 og/l Ib/ day (10 I ' F A 4 Nitrwhenot

80002 :

I (50 <15.358 1 og/l Ib/ day <50 I ' C A P Chloes M ' ~

creenetoo sa 7:

I (IO <3.072 1-og/l Ib/ day (10 1 CA Pensechemo ~ I ph.*tol C786 5: I <50 <l5.358 1 og/l Ib/ day <b0 1 124. Phenol ce es al X (10 <3.072 I og/l Ib/ day (10 1 j ca8******ao8 I (10 <3.072 I og/l Ib/ day (10 'l ree oe-2 _c, s,.,,._, ,n, y

001-gig cONTINtfl'o F ROM THE F 640NT i s errt urnt a units s inv a n c t.. rem so

1. cou.uT A NT

.====a- ""JJU

.:-2 ::-.:.n.: -

=~"-aa'" ~ "* *"'"JlntW""'Ar my :""' 4 ~,ay _ g el m '/,ac u,~, y a e m.,e. <.,e.. . q. =... =..... w......I ' - ~ ~ ..... w..... n:. =- ..ee ..._.v...... .s., ocJasS FRACTION BASE /NEUT R A L. COMPOUNDS 1s. Aeeasonmeae (33 2241 I (10 <3.077 I og/l _ Ibiday <10 I 2s. Ae.aeontyw (20sesel I <10 < 3.072 1 ug/l Ib/ day (10 1

33. Aathreceae It2S12 75 X

<10 <3.072 I ug/l Ib/ day <10 1 4a.saaeknae gesq741 2 <50 <l5.358 1 og/l Ib/ day <50 I so, sease vos Aa*reem I <10 <3.072 1 og/l Ib/ day <10 1 (5695-31 SS. esato fel ryceae tso.32 e p I (10 <3.072 I ug/l Ib/ day (10 1 ~ t 7s. 3.4 searo-7,,*," I (1.0 <3.072 1 ug/l Ib/ day (10 I se. saare (sho Pwyemae I <10 <3.072 I og/I Ib/ day <10 1 (1s124-2)

93. Seate f 6)

F 8varea*=a* I (10 <3.072 I vg/l Ib/ day <10 1 (707-08-87 too. sie esosom e q11

3'"

I (10 <3.072 1 og/l Ib/ day (10 1 (1 g$gch8a= s1a see I <10 <3.072 1 og/l Ib/ day <10 I laut emph pip,ggemenosasti I <10 <3.072 1 ug/l Ib/ day <10 1 tae. 9s rs.sen,s. g,8r{f I <10 '<3.072 I ug/l Ib/ day <10 I s as. 4erorao. powap eneay' I <10 <3.072 I ug/l Ib/ day (10 1 Eteier i10146-36 re.e,sen vs seaeve 100. sut l tes.es.71 I <10 <3.072 1 ug/l Ib/ day (10 1 l l.. } see. s o aero-f914Es-?). - - - - - I <10 <3.072 I ug/l Ib/ day (10 i ??3. 4Chiero-08=aW P*eav' se,, _ _.. _ __i I (10 <3.012 1 og/l Ib/ day <10 1 esmer 170as ico.chev eae (2p01 el I <10 <3.072 I og/l Ib/ day (10 1 sea.om aso(ans ... ~ - (Q I <10 <3.072 1 og/l Ib/ day (10 1 2ee.1.2-oscheere-beareastes-eS11 I <10 <3.d72 1 og/l Ib/ day <10 1 atc. 1.3 caensero-toesprene(set-73 fl I (10 <3.072 1 ug/l Ib/d y (10 1 EPA Form 3510-2C (Rev. 2 85) pegg v.s CONTINt!E ON PAGE V ;

Looling Pond a en i o numen u....n irom s,. m a of aorm is ou r e a t i. nuMat " Bloeedown ~ '"tra" *e.w'"o mw

- J o" s coNTeNut u F ROM PAGE V "i 11D000803643 001 a g,o..i e.

,,i r2 a s as n

f. POLLUTANT a m a ss et m'

3 L f f LleLie T 4 titel T S S IN T A 94 E (oppmfff c.No c as I'-" * "'% Q,{hy w a t_u E- - - -cLONGT F VatuE- - < r inu //,1

M a n su ou o m is., v a t.u s.

NUMBEM g, F set e-..sah s

M O.'.;

e l

q.i..% ..- t,6... o,., ... ~...t. : v s. s ' a a mm

1. s..o --

e,s.... .y ..... ~ GCDAS FR ACTION - BASE /NEUTH AL COMPOUNDS tcunement' 223.1.4 okh'oeo-X bensene (106 46 7. (10 <3.072 I ug/l Ib/ day (10 1 238. 3,3' tjechiaro beas wa* X (20 <6.143 248. Diethyi._ _. I ug/l Ib/ day (20 i f 1NI Ph* *** X <10 <3.072 zow own.ihvi-- 1 og/l Ib/ day (10 I to See 21 Ph **** X <10 <3.012 (111 11 36 M I'fIeutvt~ I ug/l Ib/ day <10 I Ph * *'* X <10 <3.012 804 74 2) ' ~ 1 og/l Ib/ day <10 1 273. 2 4 D6nstro. iosues. Itzt 3 4 2i X <10 <3.072 I ug/l th/ day < f oi I 283. 2,0 umitro noiv.noteo6 20 2, I (10 <3.012 I ug/l Ib/ day <10 I 283. Di N 06tyl Phtheseti I (10 < 3.012 1 ug/l Ib/ day <10 1 tit 7CoC! 30s.1,2-Diphenyk hymesine (as Aso-X (20 (6.143 bessene) 122 66-7, 1 ug/l Ib/ day (20 I $$d'[,'*"'"" X <10 <. o I ug/l Ib/ day (10 1 321 P hnoesn> gee.7s r I <10 <3.b.' ug/l Ib/ day <10 I l _$7"__" X (10 <3.012 I ug/l Ib/ day <10 I see. He.s-ehe edue o.a* X (10 <3.012

7 es.31_ _

I og/l Ib/ day <10 1 352 Howe <.heore-tve8cp*atadien* I <10 <3.072 ( 77-47-Q -. - - - - 1 ug/l Ib/ day (10 1 3ee. He..chiaro- .mene ter.72 il I (10 <3.072 1 ug/l Ib/ day <10 1 37% Indeno (8.8.3 ed) Pveen* X <10 <3.012 (173 38 54 1 ug/l Ib/ day <10 1 38 3. Isophorone (7s 63 11 I (10 <3.012 I ug/l Ib/ day <10 1 f, $ ""*"* I <10 <3.012 I ug/l .Ib/ day (10 i @ $""*"' ". _X (IO <3.072 1 og/l Ib/ day <10 I Cia N Nitto. soasenethve <nen. I (10 <3.012 I*I'I* L I 1 og/l ~ Ib/ day (10 1 423. N 80ttoosodl- ~ ~ ~- ~ ~ - - N etopylernene X (10 <3.072 (621-64 7) I ug/l Ib/ day (10 'l

trpo Fn, is e n sf eep.

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m m m

s 001-LOOling FOnQ Blowdoist CONTINUED FCOM THE FHONT 3.POLLUTENT e m a ase

a*

3. Ep 7 Lut H T 4 UNITS 5 IN T A M E (.epenwff

b. A m pgP d

c h s g oYshjf. I i MU ER ".'

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( b. L (M L ecoNcaN N '"a me W. = = y ..t.'...... [ ' u=~ ii- - ><= i.i - - .....t,'......- .....r,.....- i.- vs - m PRACTION - BASE /NEUTR AL COhrOUNDS (continised) 438. ;3 Nitro-n- -,Ismine X <10 <3.012 1 og/l Ib/ day <10 I esass) 44s. Phonenthreae X (10 < 3.012 I ug/l Ib/ day <10 I ses.ot t) g%*"* I <10 <3.012 I ug/l ib/ day <10 I est.1,3.4 - Tr0 - - - eae 1 (10 <3.012 (13s43 1) 1 ug/l lj/ day (10 1 GCM FRACTION - PESilCIDES IP. AkerM g i30048;) 2P. SC HC (319444) I 39.f9HC g (31y 45 7) ee. k-oHC g see en se. 8.sHC g 131945p) SP. Chloedene g ,C7 7%; i FP d. g (e+3.4* DDT 9-er. 4ff. ope I !77 9G9) 'T 4//.000 g (73544) ior. Deseda I (99571) t 1P. C E ndomitfen g ($15-30-7) 13P.$ Endosutten I (195 19-7) t 3P. E ndoeuif en g suffese (1981-07 0 4 ter. maa in 3 (73394) toe. swin g Aldehyde (742 t-93/l teP. Heptochlot I t 17s 44 4 EP3 Form 3610 2C (Mew 2-951 P AGE V-8 CONTINUE ON PAGE V-3

i t.u.,iing runo l s ea s' u m uu u......p rn.m n,..m s of P oem s, o.., n i t ,* " u u t a Blowdown "'"d'""*' l CONIING at D I 640M PAtil V 8 IL0 000803643 00I " * * ' ' ^ * ' " " depr. '*' e* pere-s fl 8 8 8S

t. POLLUTANT a manos a-r.Nt3 C AS I L e f I ts L ta i 4 UNITS in IN T A M E g..t're.m.et)

,,l.1 {. ',1, e mamsuism Omsty vmLut g, u a n sM }i u, e8'oN'3n " ~ v V ii.Isi NUMECM po cCon6v,s,,[nuj %gI valut u i 'N 38 a e nur. i s nu ret se. s.6fr # .,".I. O.'.i 40 e CONCEN g, _ g M (Bi% ( V3(M L _,,g"g,' i l

1. _ g a g g...

-..48..... c., ......4.4..... g,,... ,sa 5 1 R a m8" l e t.e. .a.=.<..* = g,s... vsts l GCJhet F H ACTION - PESTICIDES trontuimeds 7 17P, Heptact.for l E poalde X (1023 87 Ji, _ 1!P.PC3 1242 (;34ee 2s 9: X <0.2 <0.061 I ug/l Ib/ day <0.2 1 19P. PCS 8764 (stoerew ti X (0.2 (0.061 I ug/l Ib/ day <0.2 1 20P. PCS 1221 It t 504 2e al X (0.2 <0.061 I ug/l Ib/ day (0.2 1 2 tP. PCS 1232 (11:41 16 s8 X <0.2 <0.061 I ug/l Ib/ day <0. 2 1 ,l I 22P PCS 4248 ( " '" _ _ lf X <0.2 (0.061 I ug/l Ib/ day <D.2 1 23P. PC31260 F4 (l109602 Si g <0.2 <0.061 1 ug/l Ib/ day 50.2 1 24P.PCS 1016 I267 4 t 2: g (0.2 <0.061 j I seg/l Ib/ day (0.2 .l. 26P. Tsesptione fe00s.3s 2) X EPA Form 3510-2C (Rev 4 84l PAGE V 9 ' EPA Form 3510 2C tRev 2 85)

.. _ ~. _._ 145alle Stetton ~~ S tva i 82 te u M ts t se to. m fr<a*e it. ree i s.f Veersen i n PLE Ast riitr4: on t vi t sie uit inAi, tit is Atti AN or48 Y ) ou u m u p -ei. s..,,,,4,y.,,,,,, Weste 44 a..i thes information utt sesser.H. stedes tuse she same forrrtar) inste.sti of co,siples.r>J tie. se pa p;s $EE INSTfblCllONS I D OMM3 8 "" #U' *' '">* " ApWwaf eepnes r2dr SS ouf&Ett.NO V. INT AKE AND EF F t ULNi CllAFt ACTEHISitCS (conrunned tront page 3 of F onn 2 Cl 001(a) PART A You must provule the results of at least one analysis for every pullutant in this table. Complete one table for each outfall. See instructions for additional details.

2. CFYt.tsE N T

4. IN T A K E fopas.neet; UAAi%g~Qgg,v val'uiTLWWYgMQg wujg-g.,,,

I. POL $.0 T A N T e ua asuum oaeLv val.ua . t o ~ <. m. u .,u

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=g, s m... ie., ....e!.. _ i.-... _ ej.,,,, ,c,,,,= o I.,=... ,, u m,, (90 i ts. Chomscal Ouysen Doniend tcops

c. Tstil Ore.aic c.rean (To cs d Tnei co.g.n.s NI8d' fT:s3 15 12.73 6.92 4.99 2.81 2.38 52 sig/l Ib/ day

e. Ammons. (.e Ne vaa tre v a' t u t

~' vas ut v a n. u t O.17 0.14 0.1018 365 MGD V " L "I ~ -~~' - - ~' g;g g

o. Temperature vntut vatut (urbiter) -

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8. IrH ST AND A RD UNITS m

PART $. Mark "X"in column 2.s for each pollutent you know or have rn to believe le present. Mark X"in column 2-b for each pollutant you believe to be obeent. lf you merk column 2 which le timitad elther dir ectly. or indtractly btA egroseh. in en effluent timitations ouidefine.you must provide the result s of ei leest one enetysis for that potiutant f or othor poltutent column 2s, you must provide quantitative date or en emplenetton of their presence in your deschergo Complete one table for each outf all. See the instructions for additional details and re g, pog,g,gy.

d. to a n et x -

3 EFFLUENT

4. UNITS

5. IN T A M E (cretioteell C

NO

'EI* **=*<

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e. e,omade (240SX7 el I

ts. Ch8erInc. _ ~. -. Total Meefdoel I

c. coo' X

cl 1 Pt-Co

d. Pecol coetterm X

e. Fluoride possuses X

0.46 0.390 I ing/l Ib/ day

f. Nitroto-Nitrite (es NJ X

0.16 0.136 1 ag/l Ib/ day EPA Form 3610-2C (Rev. 2 86) PAGE V*8 CONTINUE ON REVER$E i

ww.t., w.......+...m litu v ts CONilNtf ED f REIM F HONI f. POLLU T.

a. M a se et *m -

3. EF FLUENT

a. UNITS S. INT AME (oprirnes)

[ a.CL, P *j,

s. Maxeuum omsty vatut c LoHG TjgggVHUi

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T H A t TON [ g,g.... ,,,,,,,p),,,,,,,, ,,,,,, p),,,,,,,, g, g,,,, g,,,., g,,,,,,, .,,t. y,0*" I <0.4 <0.340 I ag/l Ib/ day IL Ottand oresse 1 I 0.849 I ag/l Ib/ day ree rs. Toin' I 0.03 0.025 I ag/l Ib/ day (7723 140) l.cediometwev (1) A4tte. Total I <3 I pCl/l (2) sets. Tetel I 5.0 1 PCi/I m neesum. Totel X 2.2 I PCl/I qo coowm 22s. Toisi X 2.6 I PCI/1 ree so ; I 680 577.33 I og/1 1b/ day a Itges 7e el L Suffkle tee 8s x (es ) g 11 38 I <0 I ag/l Ib/ day .__.059 <0.07 Teest I peso cost <0 3 <0.255 1 ag/l Ib/ day 1reiss I peess-31 <0.1 <0.085 1 mg/l Ib/ day [,*e*s*' aa el I t 0.31 0.263 I ag/l Ib/ day m.___ [y*4ea, as I <0.05 <0.042 1 ag/l Ib/ day a pen. Tessa passee-s3 X 0.82 0.6% 1 ag/l Ib/ day 7 [,'M,, a, I 15.4 11.075 1 ag/l Ib/ day

n. =. :. - -

I [,*,*,*,',,,, <0.2 <0.170 1 ag/1, Ib/ day peso se si <0.003 <0.025 1 . Q n/ day I er. Tin, Tetel (7444314 I <0.8 <0.679 1 eB/1 lb/ day

e. Yleenlum.

<0.8 <0.679 1 mg/l Ib/ day To e peas' sa-el I i WPA Foem 3510 2C (Rev. 2 86l r Aorv.2 CO*MINUE ON PAGE V. 3

ira's o htN4 et H re,s.[ fes.m h.m I Nf MErviE ou t e AL L NuMut u N' Reg. Waste ILD000803643 00la ,,,,,,,4,,,,,,,, 040 % mu mS9 CONilNtlE D F HOM PAGE 3 OF F OHM 2 C Approvsf ereeres f 2Jf #$ PART C. If you are a primary industry and shis outf all eontains process westewater. ref ec to Table 2c-2 in theinstructions to determme which of the GC/MS fractions you must lest for Merk '"X"in column 2.s for all such GC/MS fractions that apply to your industry and for At L tonec metals. cyonedes, and totof phenols if you ere not required to mark column 2 a(secondary mdustriet. nonprocess avesrewster outfaffs. endnonrequired GC/MS fractions), merk "X" m column 2 b for each pollutant you know or havis reeson to beheve is present Mark **X"in column 2 e for each potiutant you believe is et.ent if you mark column 2a for any pollutant. you must provide the results of at least one analysis for that pollutant if you merk column 2b for any poHietant. you must provide the results of et least one analysis for that pollutant of you know or have reason to believe et wdl be descharged m concentrations of 10 ppb or greater if you merk column 2b for acroteirt acrytomteste. 2.4 dinitrophenol, or 2 methyl 4. 6 dmitrophenol. you must provide the eesults of at least one analysis for each of these pollutants wfuch you know ur have reason to beheve that you discharge m concentrations of 100 ppb or greater Otherwise. for pollutents los which you mark column 2b. you must either submit a t least one analys < or brsefly desce ebe the reasons the pollutant as expected to be discharged Note that there are 7 pages to this part, please review ech carefully Comotete one tablelatt 7pages) for each outfall See instructions for additionaldetails and requirements I. POLLUTANT a Mann x'

3. EFFLUENT

4. UNITS

5. IN T A M E (optioneff

b. Ma negggY V ALUE UMBE

". '. *,. "I.*si. *. E

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,g O G ER b O F III *3**# c.... bI...... I*I***** c oa t. b -...... I*I***** c o-c e I,'=. e.o* I'3"*** aE E teETALS, CYANIDE, AND TOTAL PHENOLS }";j,"y'$"fgo, I <0.5 O.424 1 ag/l Ib/ day - - - - ~ 2,M ny ' I <0 00I (0.0008 4e 2 1 og/1 lb/ day

"fj,*E'7'"i t, 4 4 I

<0.01 <0.0084 1 ag/l Ib/ day $jN"aj e, X <0.0002 <0.0002 1 ag/l Ib/ day $$$o"'731 1 0.022 0.0181 4 1 og/l Ib/ day h T "" X 0.004 <0.0034 1 mg/l Ib/ day N" X <0.005 <0.0042 1 mg/l Ib/ day $3 Tg[. Tow I 0.00009 <0.00008 ~. i ag/l 1b/ day hy, T *'*' x 0.029 0.024f. I ag/l Ib/ day X ~~ @[y*g"2h I <0.001 <0.0008 1 og/l Ib/ day g@y*y '*'*' I <0.0006 <0.0005 1 mg/l Ib/ day ~ 12M. Theittom-X <0.001 <0.0008 Tates (7640 28 Oi 3 "Ify yb/ day ~ ~ ".30% 13M. Zinc, Totes 0 (1440 ee ci y g,36 1 ag/l 1b/ day t 4M. cvanio.. I .<0.006 (0.0068 1eies te ra2 si 1 ag/l ib/ day ~ }*g*8 Ph*"** I <0.005 <0.0042 1 ag/l Ib/ day peonIN 2,3.7,94stre-omscassa maeuLYs shaoredesenso P. DionIn (1784 01 el g EPA Feene 3810-2C (Rev. 2 SSI PAGEv.3 CONTINUE ON REVERSE ~___

00ln - Dennin. Itegen. Wasta CONiiNut D FROM THE FHONT

3. POL.LUTCNT

a. M AMM *E'

3. EF FLUENT

a. UNITS

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3 osas x

<100 <0.065 lrg,^,';-l;"""'- x <iOO <0.085 f[t N2t I <5 <0.004 I ug/l Ib/ day j av. C: (Chtoro. swenyss etbar X isasse il f[s X <5 <0.004 I ug/l Ib/ day ev. coeven g <5 (0.004 I ug/l Ib/ day Toerschoseks. (se23el l[cie e*N ^ <5 <0.004 1 ug/l Ib/ day X ev, c.he coat g <5 <0.004 I og/l Ib/ day on meen.n. (82*-48 11- ((, M **'"*"* g (10 (0.008 I ug/l Ib/ day i 10V. tv-chiore-I l,'7d7*'*"",_g <5 (0.004 1 ug/l Ib/ day I <5 <0.004 I og/l Ib/ day w memesi.a. (79-37 4) 3 2v. pasm.,

'"e*71f I I

(7 - EQ'M' *'. _x_ <5 <0.004 1 og/l Ib/ day Mf,$*E,'[ X <5 <0.004 1 ug/l Ib/ day LVgg,$'f, D I . <5 <0.004 1 og/l Ib/ day e_ 17v.1.2 oichio I <5 <0.004 1 ug/l .lb/ day pr. pen. (7e 87 51 p.,,e 3.oise ist 1 gse: a se I (5 <0.004 1 og/l Ib/ day I l,27f j,'*j,"'*"'*"" X- <5 <0.004 1 ns5/1 1b/ day ',',.'.ne, /4 s3,3 X CO (0.005 I og/l Ib/dey 7' $",,,, g"j,',, 3, I (10 (0.008 1 lug/l Ib/ day i EPA Form 3610 2C lMov. 2 85) PAGEV.a CONTINUE ON PAGE V-6 i L

ts5alla Demin. u a e u n u u..........,,,..,,,....,.., e,.,,,, e, us,.....u......,, ,...4, CONTINtis t FROM PAGf V 4 IID 000803643 001c R89*3 ","..*e*i..".",',,n /* 4w . 2

f. POLLUTANT s m a n ni s-3 t p rt.ts E N T 4 UNITS S IN T A M E (<epte.+nefs AND C AS te w a m paQ u,,s,f.,h,in,v v a L u a

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- ','o'*o*e'"s *"*

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=*'*'aseh*

x (7s-se et 3 v. vin a chseeks.[ts os en I

(IO <0.008 1 GCAS F. ACTION - ACIO COMPOUNOS og/l Ib/ day l 1 A. 2 Chloropheno too sici X gle $0.008 1 og/8 lb/ day 2 A. 2.4 Cichloro phenol (120 83 2: I <10 <0.008 I og/1 lb/ day MgYos"*eU, g <10 <0.008 1 og 1 ib/ day 4 A. 4,0 Dinetto O cre e t:3a s2 ii X (50 ,0.042 I isg/l Ib/ day S A 2 4 D6aeseo whende set as si I (50 <0.042 1 og/l Ib/ day $ h"$'*""*" ' _I (10 (0.008 1 g/l Ib/ day g',oo E"*"*' I <50 <0.042 I og/l Ib/ day ^* M Ns$ I (10 (0.008 i I isg/l Ib/ day m.Penee hi onenes t7es s I (50 <e 042 I og/l Ib/ day j < ISA Phon (goes os.z es I (IO <0.008 1 og/l Ib/ day S t A. 2.0.S-Tel - ~~ ^ ~~^ choseeenenes I (10 (0.005 I ug/l Ib/ day f98-OS-2) m.- m. --~ ..,... ~,

tesease a t u uuoou.m43 Outtal Deman. CONTINHED Ff"OM THE FHONI t. Pot.t.U Trt NT 3 emanes m-3 E.FFLUENT

4. UNITS S. IN T AM E (eepreneff f."J.Eai ea r 3.:: a.r.. = " = ~ " =a ' - * **"'"flia.Wf f" "'#r"41si!".%,:,r

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- fy,',*"*

<50 <0.042 1 ug/l Ib/ day C").mensetel A;mr. cone <10 <0.006 I ug/l Ib/ day roses 31 $;,8*"g'so$ ai (10 <0.006 I ug/1 1b/ day

72. 3.4 sento-neerea*ea*

<10 (0.008 1 ug/l Ib/ day taes so al ee.eensete ts s Pervosae (10 (0.008 I ug/l Ib/ day (1013421 ee.eenset6I pu e --: <10 <0.008 I ug/l Ib/ day tas? ee el See. Senit Chiaro emonys uemmae <10 (0.008 I og/l Ib/ day 4 lit t4811 venyss sibChloro. t 2 ese (10 <0.008 1 og/l Ib/ day

l. " ' d* di hd,%, *is y (10 (0.008 1

og/1 lb/dey tae.t. se #2 Eehrt-hasye;enseiste <10 (0.008 1 ug/1 lb/ day IH768 78 tee. 4-Stomo paeave Pheave <10 <0.008 1 ug/l Ib/ day-seer Itot es.ai M g'.*,*e" d <10 (0.008 I ug/l Ib/ day _.I l. 185. 2 Chloro neemeen ne <10 <0.008 1 og/l Ib/ day 19148-71 4 17s. ochiaro-oneare rt eave <10 (0.008 I og/l Ib/ day emer troos 7 3: g","f [,"',[,'*"* (10 (0.008 1 og/l Ib/ day Aneremone (le (0.008 1 og/l Ib/ day M7*88 EMisNii <le (0.008 1 og/l Ib/ day av a t a oe=*iere- <le (0.008 1 . og/l ' Ib/ day meseene see s.7311 EPA Foem 3610 2C (Rev. 2 85) P Act v.s CONTINUE ON PAGE V 7

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m m .m_ L4541I2 ILD 000803643 00l(e) Demia. CONilNilt D F HOM THE FitONT 4 IJ NI T S S IN T Alt t. p.g'se.m.rf t

3. POLLtJTf.NT em a nu a-a t r e's isLNT

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, M * " 8M L'u ta m e L v {A LtJ,J Wun,igf.,4,,f,7) des AND C AS p ass um a r onn e n a y L!t M, L y al,VL 8 NUMBER ,,u,n , u,,, T- ___ i., i. f ' a a * "> " It;,:r i,i -... v si s i.e ,us . a a. 5.a-u ti-?"aal._,,,._... t e '" - ' + -'r " *m i OCJMS FRACTION - B ASE/NEUTR AL COMPOUNDS ec mtma< ds ".39. N Nlteo so sichenye mine X (10 <0.008 I ug/l Ib/ day vos so s 44s Phen.nibeen. I <10 <0.008 I og/l Ib/ day tes414 4s1 Py'o*"* I (10 <0.006 I og/l Ib/ day (tas co-n 468. l.2,4 - Tel-2 ^- - - - - s eae X (10 <0.008 1 ug/l Ib/ day it2osa.se OCJMB FR ACTION - PESTICIDES 1P. Asdrea 3 (309 00 2) 2P. C CHC g (31s C4 61 3P. $ EHC 3 (3:e es 7 4P. 7 CHC I (see>on 5P. 6 -C HC I (als es si GP. Chlord.no g (57 7f,-ol 7P. 4.000T X (50 29 al eP. C.4'-D DE I (72859) 9P. 4.4'-DDD X (72 s&s) 10P. Oleidein X (60071) t P. El Endoeuffen X (183-29-7) 12P. $ Endoeultan X (f t$ 29 7) 13P. E ndoeuif en ~ g Suffete (10elC7 el 14P. E nterin X (72-29 Sl ISP.Endem g 2.Issootyde (742143 4p tee. Heptschter X Fe 44 u I EP.3 Form 3510 2C (Rev. 2 es) PAGE V 8 CONT 8NUE'ON PAGE V-9 l a ~. - - - -.,. ---.~u,

ic5alle a en e u n uu ur e<....e, ca..m su.-m n ut F um, s o ou s e a n a unMun,e

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CONilNtsLD F HOM PAGL V e ILD000803643 001(a) Demin. As.gia..n/ e.g,,,g g p 2 J r 3 a, I. POLLUTANT a Mann m-3 Eff1ULNT

4. UNITS 5 IN T A K E (esper.neff; CND C AC

~ 7me m M I ]M3 NU M BER

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a. mea nsuuM oneLY V ALUE Y V ALUE C.LONG T L M 4 ' VALUE Le s

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f a.l.*.*.=.e..*. + s.t...g vsEs a GCJteS FR ACTION - PESTICIDES teorissamed) E poside I t 192 *e 87 3) SSP.PC3 1242 te34ee an el X <0.2 <0.0002 1 ug/l Ib/ day t DP. PC31264 I (s toer-se.tl I <0.2 <0.0002 I og/l Ib/ day 20P. PC31221 ( t11042e-21 X <0.2 <0.0002 I ug/l Ib/ day 21P. PCO 1232 f t stes le-si X <0.2 <0.0002 1 ug/l Ib/ day 22P.PC1 42e8 (12e r2.as si X <0.2 <0.0002 1 ug/l Ib/ day 23P.PC's12eo a1toose2 el I <0.2 <0.0002 1 ug/l Ib/ day see.PCO 1 ole (1247'+18 28 X <fl. 2 <0.0002 I ug/l Ib/ day 29P. Ton eestsene seco t-as-2) X EPA Form 3510-2C (Rev. 4 84) "A G E V t 4 a 1 l ' PeDC Pete e 1E 10 SP 809 = 9 #PS

(.45a I I t'

t E ASE PitirJ t UH t ' Pt Ife l tti Ilfbil ADL D A6tL A$ UfJn y E P A e u NuM ht te s..+ s fr.em item I of Form ' l SIP l

n i ne.e.q u pi n l. i os..n. a th,s intoernation on seper.ste sf cet6 iuse t ee sa<ne form. pts inste.nl of compleisnij sle. se pa.g.3 11D0008030643 p,,,,,,,q,,,,,,,,,,, i it t tNSt'Ent sC llOrJS ous %.tm n,w Approvat e.pwe g 12 p t 89 V. INTAKE AND EFF LUEN T CHAF4 ACTEF41SilCS tsonemued tro.n ragr 3 of for,re 2 Cl uss t t At L No 00l(b) PART A You must provide the results of at least one analysts f or evesy p21$ tant in this table. Complete one table for each outfall See instructions for additional details. 2 E FFL tJ E N T 3.UHtTS 4 IN T A K E (opnemelf E""*'1y",[bydi

1. POL {UTANT e M AmsMoM onsty vmLua vvnLut e L6H{.7 VAEdE-(etws/, if tpfenb) p d NO OD

,,,m lL, m. i i-~. ..... LL.... t o -.- ..>., LL... - so-~. A M LjiAss L MALM E , h NO OF "A a"* E"i .... fl..... io--. NM5'e'ad 31 5.89 14.7 2.79 12.9 2.45 12 mg/l Ib/ day

LEODI W. Chemical Oxygen Osmond (CCD1: e. Tstal Oreenic

. Cernon (TOCl d Tat:18uspendait sandstrail 35 6.65 14.0 2.66 11.9 2.26 12 auj/1 lb/ day

e. ammente (e. Ni v'a' i u t vaint~

v ni ut ' M**' vatut O.0886 0.0522 0.0228 365 MGD V A t.t# E

3. Tempt'sture VA4ut VALUt VAoUk (e.hoterp

.,g 7g v a ttst v nList vmLut vmLut -sunumerf4 C k-MtNtMUM M A M4 MUM MIN 0 MUM M A M0 MUM Pf 7.2 8.3 7.2 8.3 12 ST ANDARD UNITS fANT$ # which ie limitod elther dir ectly. or instractly btg enpressly,ln en offluent limitations guideline.you must p column 28 you must provide quantitative dote or en emplenetson of their presence in your discharge Complete one table for each outf all See the metructions I. POLpUT.

a. Manet n-3, E FFLUENT

4. UNITS

5. INT A K E (optioevall h pg

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rates fteeduce g 0.6 I.635 1.67 1.46 4 sig/1 Ib/ day . cas*' g 34 6.465 I Pt-Co IdU 9 3 3 12 Mg g . Faueride sess usC) I 0.53 0.101 1 og/l Ib/ day - Nltrete-twlte feo NJ x 1.89 0.359 I M U Pa Form 3510-2C (Rev. 2-86l PAGEv.s CONTINUE ON REVERSE

-+=-e liLM V tf CONisNLst o e nog 4 nony

3. P O Lg.U T.

a. mar.se *m-

3. EFFLUENT

4. UNIT 3 5.1HT A v(E (optionef) hf

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h. oss and Oessee I

6 1.14I 4 4 og/l Ib/ day tee ro, Teses (772J 140) 2.07 0.394 I ag/l Ib/ day l._ Messeeettetty (1) t tphe, ~~ Tweet I (3 I ag/l Ib/ day sat o te. T Tetel ' ' I 15 I ag/l Ib/ day C medlwn. Tesel - I (1.0 I ag/l Ib/ day ('0 nedsen i 22e. Totes I <l.0 I ag/l Ib/ day 80a8 I 210 39.932 I ag/l Ib/ day N' esse 7e el it L suertoe (se(J I

m. evenne ten so t s

y 1142es46 3B n eerfect*"" I 0.07 0.013 1 og/l Ib/(ay [y*4,,',,,, I <0.3 <0.057 1 mg/l Ib/ day [y*44o' as 3, I 0.1 0.019 I ag/l Ib/ day [,%4as I 0.41 0.078 I ag/l Ib/ day [,%4e-al I <0.05 (0.009* I ag/l Ib/ day n from. Total 174aseo-op I 0.25 0.047 1 mg/l Ib/ day [,e,*8,,,, I 38.8 7.378 1 og/l Ib/ day (_ Teees I <0.2 (0.038 1 og/l Ib/ day (7439 98 78 iL ____ _ _ L = _,,,, i I a.iG 0.0i9 I sy/i i ibid.1

w. tin. Tetsi I? M iles I

<0.8 (0.152 1 og/l Ib/ day [,*gp I <0.8 <0.152 1 og/l Ib/ day EPA Foren 3810 2C (Rev. 2 85) P A G E'V-2 i CONTINUE ON PAGE V,.3

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W 001(b) SIP CONTINIfED FFOM THE FRONT I enLLUTC.NT

a. mann 'a' 3 ErrLUENT

4. UNI TS

5. INT AM E forrionef;

" " TQ,,Q %,vVALut c e.ONG T M .VALuE O C [.'. IaiS.U.. a.unnewuu OAeLv vaLug U EF2 N3 F O , g g <a . m . g :::,e .;*.:...., !-),,,,,. i. i.... ... t-),.,,.. ' a av'aa ,,,,,,pi.,,,,,, vue s u ;;g - i. i.... v.s.1 ggAm FftACT90N -VOLATILE COeWOUNOS iv. Accelein (187434) X <100 (0.019 1 og/l Ib/ day 3V. Acrylongtelle (107 134) X (100 <0.019 I ug/l yb/ day sv. eenseae (7tesi I <5 <0.0009 3 ug/l Ib/d8Y . ___ a sways; emer g jee te il

v. eremoverm (75 2s.z X

(5 <0.0009 I ug/l Ib/ day ev. certion I Ib/ day veersem e h'* I (5 (0.0009 ug/l fee-33 el Fv.c uorebe"'*"* I lb/ day (18e40'7) X <5 <0.0009 ug/l ev. cuerods-I Ib/ day N X (5 <0.0009 ug/l (13+48-il ev. cMoroethene (7s-063) X (10 (0.0019 1

9/y Ib/ day I

(10 <0.0019 I ug/l Ib/ day gg',E'#*' 11v. cMetoform te74e 3) X <5 <0.0009 1

9/I ib/ day
"s.37-es "a*

I <5 <0.0009 1 og/1 Ib/ day

=*8 (7

88#es-wine,= x (7s.71el tev.1.1-os Mo<e-emene (70 s*wb I (5 <0.0009 1

9/y Ib/ day

,sov.1.z,.osemero. I (5 (0.0009 1 ugfg Ib/ day g g746 3 feV 1 f-DieMete-M g7s-as-46 I (5 <0.0009 1

9/I ib/ day 17v 1.2 ote u ero-I

<5 <0.0009 1

9f3 lb/ day presone (7p47.el ter. i.sensame-p ys megnes. 3 4:

I (5 <0.0009 1

9/3 lb/ day u

g','g[f[,*','""*U I (5 <0.0009 I

9/I ib/ day sov sesenv 9,es.aes (74 e3 el I

<10 <0.0019 1

9fy lb/ day Ea'er-a, I

<10 <0.0019 1

9/I ib/ day EP.1 Pome 3810-2C (Rev. 2.eSt P AGE V.a CONTINUE ON PAGE V m

s - CONilNt8E D Fl4OM Tite F FtONT 001(b) 9.POLLUTAMT

a. m a nos m-3 E. F f' t U C H T Nht

!af'. . Ef. E * " ^ " ' " " " " ' " ' ' " ' " "

a. UNITS S s N T A t< E (.*presen4##

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m... u.......

o,-. s ' a ^ "a" i ur. n-i.i-... v OCAN F2f.CTION _ SASE/NEUTH AL COMPOUNDS

13. Aconesihthone ges aatl I

(10 <0.0019 I "9/I Ib/ day 2a. Aceaophtviene (20s ser,p I (10 <0.0019 I ugfy Ib/ day 3,* X <5 (0.0009 I ug/l Ib/ day 20 27l h*7c,"""* I <50 <0.0095 1 "9/1 lb/ day

O. eens e las Annrecane I

(10 (0.0019 1 ug/l Ib/ day too es-3)

s; oe"g"'

I <10 (0.0019 I ug/l Ib/ day , n e,

73. 3.4 Bento.

nuorenrh*a* X (10 <0.0019 I ug/l Ib/ day (205'99-2) I rer. Sents (shil__ CO viene I (10 (0.0019 (l's-212) I ug/1-Ib/ day CO. eenr2 f t) Fluorontemeno I <10 (0.0019 I ug/l' lb/ day (207.eee t , emesys Mothene X <10 0.0019 I ug/l Ib/ day lit t# t,tL t 2 piees calore

<mpu silwr I

(10 <0.0019 1 i'9/I lb/ day . 11 1 44-41 hY$13 I <10 <0.0019 I ug/l Ib/ day tae.ses(* Een d. Ph m eiste I <10

<0.0019 nesys;t-71 titre 1

"9/3 Ib/ day f ee. 4-ero,no- '~-" ~ . osiaavlPheavt I (10 (0.0019

Ettieri1216s 3)

I "9/I lb/ day i 'd*Mg'a'sY s X <1 <0.0 9 I ug/1 jb/ day ~ ~ "

9es. 2 chiaro

~ neohmesone X <10 (0.0019 1 ug/I Ib/ day 'pheavsrhenyt I <10 <0.0019 I

9/3 lb/ day Etsier a7005 72 31 g'ad bNs""

X <10 <0.0019 1 889/3 lb/ day Aashreenne I <10 <0.0019 is*7S3 I "9/I Ib/ day i,enneneses se sp I (10 <0.0019 1 "9/ Ib/ day 28 1 1. M 8ch o'o~ baserene (541.'73.t l X <10 (0.0019 1 "9/1 lb/ day ~ PA Form 3510 2C (Rev. 2 85) rac t v.s t'nNTsNIsp oN earv **

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'geg ',,,,.'..,,,,. g j CONTINHen FHOM PAGF V a 11D000603643 001(b) SIP 4,,,,,.,, j

t. POLLUTitNT asaman n*

C H"4 C fig 3 Ef F Lt8ENT C UHlTS S IN T A M E (optsonsfl l MuMcca '.: ' 't. ::.mi. 1, 3 a a =u= o a v atu t __ __ _,Ji M.,,3,,t.,t'c,v v a t u t c Lonc. i,t,/,eu,...L'illr w A t. elt b Ma n sM l pr .som, opm. :::; ian. r e 4 O N fs TERM .n; ,,,,,, t),,,,,.,,. l .. umg uum _ bygg? . o m u,. a _,,,, p,i.,,,,. iaa m a ,,,,,, p i,,,,, 3;,; i.i.... vee. . n l GCAes F? ACTION - VOLATitE COMPOUNOS teon,in..o 2av. M*thv a* cheartse 17s'*-oe as X (10 (0.0019 I ug/l Ib/ day I gi .2 rme-g,, X <5 <0.0009 I 178-34c1 og/g Ib'/ day aav. Teir=hiero-X (5 <0.0009 othesnet}a7isai I ug/y Ib/ day sov. Tosuone X <5 (0.0009 I ug/l Ib/ day (18e 48-81 2ev. s.2 Treae-. _ _. ,D,ggY"' I <5 <0.000g i 89/I ib/ day i 27v.1.1.1 Tri-chiocoethen. 1 (5 <0.0009 (7:4e-e) I ug/l Ib/ day 3ev.1.1.2 Tri-e m e*' hone X <5 (0.0009 ~~ ~' pe4 set I ug/l Ib/ day 2ev. Trichs. ,,n, n, p,oeo, e, I <5 <0.0009 o I og/l Ib/ day 30V. Triehsero-N ererneihen. I ~' 17e48-41 kes see X (10 (0.0019 e on-al. I ug/l Ib/ day ecAss FRACTION - ACID COMPOUNOS $h"p*"*"" X (10 <0.0019 1 ug/l Ib/ day 3 A. 2.0 Olehtoro. phones (14.s43 2, I <10 <0.0019 1 ug/l Ib/ day M3* U ',', I (10 <0.0019 I ug/l Ib/ day '^d;},Dyj',*, e I <50 <0.0095 I og/l Ib/ day MIN s's X <$0 (0.0095 1 ug/1 1b/ day fo^e fsT X <10 <0.0019 1 ug/l Ib/ day 7 A. CNitrophenot stooea.73 X <50 (0.0095 I og/l It'/ day 'A. r chier. M. ca aese'so-7, X <10 <0.0019 I og/l 'Ib/ day e A. Pen,=Mo<e. phones terme op X <50 <0.0095 I og/l Ib/ day 10 A. rhenol stesse-a) X (10 <0.0019 1

97y lb/ day 11 A. 3.a.e-Trt.

X <10 <0.0019 Il69/I lb/ day Ce

m. e CONTINilt D F ROM THE F HONT

3. POLLUTANT a w a ee n

n L t t t s it te l 4 UNIT S

$ IN T A M l' g.eg.te..nJ4 C H 3. C A S -~ .=ua uantvvatu't y. '/.n,.a.n. ! =ar".J... I 'b-ummiugu,sJ.M.ywatast c L ont. 7 3,/.eu 4#'t v ai e nt, ;;p,;" p]

e..

Num nca 4 eone,etseu mum vain. o a;> e .ue . r o n.. n l ter -a.6*, ' " ' " " ~ . r..... ' in..:c.- OCAN F.! ACTION - BASE /NEUTH AL COMPOUNDS #c.mtenueds 439.N dtph Citto-nvl meae X <10 (0.0019 1 "9/I lb/ day l goe zoe) 44e. Ph.nanihe.n. I (10 <0.0019 1 ug/l Ib/ day (es.cies eso. Pyr n. (san ceFog I (10 <0.0019 I og/l Ib/ day est.1,2,4 Tel- ~

- - - 'e'*3-9)

I (10 <0.00l9 I ug/l Ib/ day (13e GCAS FRACTION - PESTICIDES _.. tP. Aldeln 1300402) I 2P. S-G HC (31* e4GI X 3P. $ CHC ~ (399 85 7) X SP T9HC (se eect 1 sP. S. enc (39384$1 I SP. Chloedene E7 74t,) X FP C.4* DD T (50 $9-3) I SP. O.4*-DDE e (73 es e) X OP. f 4*-DDD ^ 173 844) I 10P. Oleadeln (90 ~.,7 t) I t IP. C E ndosulf en (l95-29 7) I ~ 12P $ E ndoeulfen (118 29 7) I ~ 13P. E ndosutien s.w.e* I (103147 CI 14P. E ndrIn (72 204l I ~~ Aldehyde X (74217 3 48.. _ ... ~. - - ler. Heptochlot (7s 44.) I FP.3 Fnem 3510 2C fRev 7 RMI PAGE V 8 CONTINUE ON FAGE V 9

eva e o n u us,s u s...e>sr...os.m s.1ro m, o

w m Arm m>

ouseatbnuuusn SIP 04G4 amunw l 110000003643 001( ) l i ONTINut O FTOM PAGE Va d#t"o'G' e*res f 2 3 7 85

8. POLLUTANT s maman n-3 te e a us N1 4 UH6TS 5 S N T A M E (,*ternmef; 5"UN

" """'"J"lf.M2 M"' * ' " " W." M[ ' ' " ' ' " "y

.:r ?.::..t.::.. e a a =ua oa>< - uus 4,"'ITLVii"v t._ %"yy

. conc. ~ -iE 9_ A ..... th.... l t = " so - - ... tt.... m-- ......r...... u-- e 812.* ::.:.- ii-** ms GCAS F.*. ACTION - e ASE/NE UT R AL COMPOUNDS ecentmved' dy,",'*,;I (10 <0.0019 I ug/l Ib/ day o 238. 3.3'-OlchlovO- ~~ teasidow I (20 <0.0038 I og/l Ib/ day 0.14411 Pametese I <10 (0.0019 1 ug/l Ib/ day estes.23 30s. Demethya ~~ ~ - ~~ Phthesene I <10 (0.0019 I og/l Ib/ day (9.t.11-31 M W ivtyt 5 Pbeslote I (10 (0.0019 I ug/l Ib/ day fe4 7Jr.2) 271 2 e iu.n 4 Dinsero. s t 21 14 2, I (10 <0.0019 I ug/l Ib/ day see. a.C.Dineiro. see e geos 2a2 I <10 <0.0019 1 og/l Ib/ day 2ee. De nocry P*sheaste I (10 <0.0019 1 ug/l Ib/ day 18874+#1 300.1.34tpheny6__ hvierseene re. Aso-I (20 (0.003s I og/l Ib/ day beassaelt122 se 71

M Q *"'

I (10 (0.0019 1 og/l Ib/ day N$Y" I <10 <0.0019 I og/l Ib/ day 7.hi. - I <10 (0.0019 I ug/l Ib/ day e eswereenre m.no I (10 <0.0019 I ug/l Ib/ day 3.L#" Sse. Nee.cnsero. -. :eae I (10 (0.0019 1 ug/l Ib/ day ff74-4) emone (e7 7211 X <10 (0.0019 I ag/l 1b/ day tr.s sed; Pv'*a* I (10 (0.0019 1 og/l Ib/ day ites-3s-s)

- - M7" p,

I <10 (0.0019 1 ug/l Ib/ day (10 <0.0019 I M. $g**'*"* I lb/ day . }..._ _ 4 I <10 (0.0019 1 og/l Ib/ day -- - r. L..ane I (10 <0.0019 1 og/l Ib/ day iss-7een Mr.-,1. ~ X (10 (0.0019 1 ug' 1 lb/ day / te2144 7) _ EP.'1 Form 3610 2C (Maw 2 m8u

waTo noust a e.on troo. suen i or sow si ouvr att nuun a '. ~ 4 rr. at CONilNUED FCOM PAGE V B ILD00(M10 % 43 001(b) 5yP mes 4.,,icoo m,sv,,,3 4,,,,,,, 5.POLLUTENT e mann m* 3 L F F t. SAL N T

4. UNITS

$ IN T A M E (esprumilj NUMLE ". ' *,. ' ', *,*. 01., *.!!.

e. Maatsuum casty vaLu2 fk.h)

]"'UE " '""" Yife" Ne g tH

i. a....a$$ _","g, f. I

_)M ,.r . w, .= :n. .u;. .. ~... ......i i.. .....i.i..... mg = = = ~ aconcam .m vs. GCAN F.: ACTION - PESTICIDES feoasia.ed) 179'. Heptschler e E perkee I (192 % 7 31 g','d' y,t((2 X <0.2 (0.00004 I ug/l Ib/ day g'ff,",$M,2,s4 X <0.2 <0.00004 1 ug/l Ib/ day 2 gge:2,21 I <0.2 (0.00004 1 ug/l Ib/ day g,tj {,qg,32 a X (0.2 <0.00004 1 og/l Ib/ day 2, i fe X <0.2 (0.00004 I ug/l Ib/ day 3,Nh',2,88 I <0.2 <0.00004 1 ug/l Ib/ day a pg,sp,sa X <0.2 <0.00004 ~ g, 1 ug/l Ib/ day 2SP. T!*aphone g (9001 35-3) SPA Form 3610-2C (Rev. 4 84) PAGE V 9 l e 'A Form 3310 2C fR** 7 RM

I.aSalle Station o no u nt .r...... tr.. tr,, .y r.,rm si . Pt E ASE Pit lNI OH ivPt th f elt 18hbil AIJLis AHl. AS ONL Y Y ou me etpo t u.m. t a.au of this informsteon on sverdte sl.eets suse the same forrn,st) eristead int comptetmg flh se gea pin p,,,,,, ap,.,,.,,,.,j SH INSTWC1 TONS II.D00080364 3 W8 % m) e door ver eo.et s r2 Ji 8$ MI, e c V. INTA8(E AND EFF LULNT CHAR ACTERISTICS kont,nuect fro.re page J of forrn 2 CJ outaXL4.No 001(c) PART A. You must erovnie the results of at least one analysis for every pollutant in this table, Complete one table gr each outfall. See instructions for edditional 2 E f"Ft.U E N T

3. UNITS I* " * '"*$ ",$M,Y V " "

\\MMf

4. IN T a M E (<> pre,maff 1.POQUTANT e un nettuu past.v vaLua t

til ,jL g-( Q,Qs. 8 g,g... 4+1 g.3... t.) . h e o oe

AO,","j"g comm a ssm a n aso g,p u.

aNatvtrs to unss t.1 g,,,... 4NaLVote 6 cal emered r Dg,,o-e-d

c. Totel Oreenic ceraron (TOCS d Totalfuspendest

- "d*' " #

13

1. 9_5

_3_. _5_ __0_ _. _5_ 2_ 1_.75 0.26 52 mg/I. Ib/ day

e. Ammonta (es N7 V a L is t WAttft

. t. F eo.s nr a t is t. V et tat 0.082 T _0.056 0.018 365 HGD r,s.e, chte rer .C Twee tammers 'C MineMuu um a suum u ste s u um um meMuu w '4. PH ~p 4 7.6 8.2 7.6 8.2 52 STAND ARD UNITS PA g y Mort ~~X"* in column 2 e for each pollutent you know or have rxx-, to believe le present. Mort **X"in column 2 b for each pollutant you be Column 20. you must provide quentitative dete or en oitplanetton eltheir presence in your discherge Co equirem9nte .g,hg,ggy.

s. u a n st n 3 E FFL.U EN T A

,T a..::; 3. :..

a. =a a'aua pav v a'un

4. UNITS S. IN T A K E (opriemsif

"^ * 1 Wit.W " ^ " I "" MA" WF"' 4,",a,3' a'rk " M *A L %gr c or emeue> t.t.,,,,. rA.,,,,, io -em ey'o ~ c a - .... ! L.... i.i -~ ...P,'..... i.i-~ vne a=~ ....E'..... io -- vne

s. eremees

'24999C7 El y

cuorine, rstes neesduce

.X . Cslor Z 4 0.600 t l't -Co I. Facel tollform y . Fluoride teessaecs .I_ _ _._5 5.. _. 0 0.083 1 mg/I. Ib/ day

Nitress-cnrie (** "#

I 0.70 0.105 1 mg/1. Ib/ day IP.S Form 3610-2C (Rev. 2-95) PAGEVs CONTINUE ON REVERSE ~

=., ITEM V U CONilNHf D F HOM F HONT I b } EI' I 1. POLLUT. 2.MRam n 3 F F F L tJ E N T

4. tJNIT3

5. IN T A K E (oprirmaff se a a eg n,e,y,

,vveLui'FE6H7Yg g p T KL tit', ggg yg, b C ' ik![ E....r,.."...."A """"g o, i, o, e..... .... t1..... i.i.... ... 11......, i,... v es orosmoe e -- 'aa"a" .... LV.....

4. i....

vsea g Mftressa. Togos Orsoner t= wn I 1.0 0.150 I ag/L _ lb[ day _

h. Off end L Phoekwe_

. I.__. 8.3 ._ ], 2 4 6 _ __ L 6_4 0.696 2.I _0.315 52 mg/L lb/ day. fes PJ, Teint 17723140) I 0.02 0.003 I ag/I. Ib/ day

i. nweseetwey til Aspbe.

X _i3 I PC![I-

seio.

Tetel ' X 11 1 pCi/L (7 noctum. M I 3.9 i PCi/L (:s neek,m aze. Totes X 3.9 1 pCi/L k.Suffets tee 00 1 4 tiepos te e X 1200 180.14 I . eg /I. Ib/ day

t. SwlMee ten 9I

. _.g tee l' _ti es, . __x -si e,. r,,,6 . _X_ _ <Q. Ql_ <0.010 1 .ng/L lb/ day II* ' 3 I_ P. seri-a. M 3_04_5 _ 1 mg/l. Ib/ day . 0.3 Total __0:0l$ 1 treessoal _I_ _ . _0 1, _. _"6_I: _ lb/ day / <3

. use*P.

Total I ag/I. Ib/ day (74eo4a si _X__ _.0_ 3_9_ -.._0 058 Total 174 esse as I <0.05 <0.0d7 1 mg/I. Ib/ day M esa. Tete I'*8' ** '8 _. 013 _. Ib/ day 0 1 mg/I. _I

0. 0_9_. _

Teest' (7ess os 4: I 58 8.707 1 mg/I. Ib/ day li.. [Ose1: I <0.2 (0.030 I ag/L lb/ day g_- 1 mg/L lb/ day trese se st X 0.08 _ 0.012

a. Ten. Total II*** * ' '

.._ _. 8 <0.120 1 mg/L lb/ day <0 I [7eessa s I <0.8 (0.120 1 mg/L lb/ day EPA Form 3510 2C (Rev. 2 361 PAGE*v2 CONTINUE ON PAGE V*.3

$.lra I i l l I I l l 03 i I C 3 3

v. E S.

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9 m e r5 5 u 2 <=rt cg

s .o s E,. E, s,w, ~ 1 ,s-je g '2d y*- g*= 4 2 ><ws E e. ER o a j e ~o R gg s-2g 2! '13 ..y::. g. auea u t-2 n se o j u n ozg gR g, E s "I g -e s et g> t~ 2* tt I s s -I

g* zg 97 "6

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LaSa1le 001(c )ln(TP CONisNtit O FROM THE FRONT 3.POLLUTnNT

a. maern A'

3. L F F t.U EN T

4. UNITS

5. INT AM E (espefonef;

b. M A m egg ggy v aLug c Lons igm gg vmLua

! h,",0j' U)40EI , '.*. i.I.4 e unzewuu umety vmLut ""O'

V concan ben a

LvaLuc (#f. amin ay,,- W ,,,,,,, t)...,,, i i -a.. .... t!.,,,,,,, s.i-... ,,,,,,p,1,,,,,,,,, i.e-... vses '""T'*" l'! *.*;;* *,"- t ai = =.. vses GCASS Ffl ACTION - VOL ATILE COtrOUNDS iv. Aerei.ia .I f100 <0.Q15 I ug/I.. Ib/ day _ l av. a.cymaaris. H 8- ' ' ( x <100 <0.015 ug/L IbLday_ ev. e.. 87'- " x 15 .50.007 1 ug/L _ IbLday. .ev..eNoem.er.- tche m ($43 40 1: I !V. eremof orm I O <0.0007 I sig/L lb/ day. ~ ev. c T.trashloe ks. twas es x 0 s0.0007 ug/I. IbLday 7V. Cheerob.ns.a. x 0 50.0007 1 ug/L. Ib/ day ev c.h .oi. er. n + + ii x <5 50.0007 I us/L lb/ day ev. ch.... '" M x $10 .f0.0015 1 ug/I. I b/ day.. 1ev. Sf.hwro-NN: _I <10 <0.0015 1 ug/L lb/ day. 11v. Closeroform I (5 <0.0007 I ug/L ib/ day. iav. ove i7'Fai.4 ~ ' I <5 30.0007 1 uB/L lb/ day ein osphoore iav .eenismen. I"'I E f

- - "* f7* 88 '

1 ug/L r.v. t.s.oschoore. lb/ day _ . 0_.0007 .. __5 . _x etheng l}ti?4941 x. . - -.(5 ._0. 00_07_ 1 ug/L lb/ day wvl s.i.nienwr..

- vi=at (7s.se-41 I

(5 <0.0007 ug/L lb/ day 1 F., 1.2 Dichooro 1 Fv. . sw e7 s' l <5 <0.0007 _ _1 _ _ug/L lb/ day ISV. l.3 Shoese-I <5 <0.0007 1 ug/L lb/ day tev. Ethyn ne.a. tio** Mi I <5 (0.0007 1 ug/L lb/ day mov. w.mve **'** 8 7 d * * * ' I <10 <0.0015 1 ug/L lb/ day aiv. wanvi cabrks.s7eers' I <10 <0.0015 1 ug/L lb/ day EPA Form 3810-2C (Rev. 2 851 pAog v.e CONTINUE ON FACE V t m

1.aSaiIe t*a e o e...u ........,,.,. n..

..,e....

4, ou.i aa i

r.. e $ 4....

UNIIN4fEl) i etOM P?GF V 4 M j;g,, ILD000803643 001(c) Wrl' avor.-us e.n-.. r r e r.vs 1.POLLUTRMT a em ann *m-3 E. 7 F t.u r N T 4 UNITS 5 IN T A k E fopruunat; NUM E ". ' ' ' '.'. *li h*1; e 54m m emassee (D AIL V V A LUE I#' " ' g h, hp WALUE C L O N C. T p vatut a

f. y m4 m,

.=

n

..t................. I

1. P. 3 0 9

_m ...i.i... ..._..i.i..... i n a T~~ ,s, ....... ~ v.e. 3CAAS F.': ACTION - VOLATILE COMPOUNDS teontinue.#1 ...r - - ~ 2v. u..hvi.n. ~~

- 'ies tim a X

<5 <0.0007 1 ug/I. Ib/ day . *3V. 9.1.2.2 T otre hooroethene 7:>=m x <5 <0.0007 I us/I. Ib/ day . 4V. Tetrachlore-

"'"* ' 18 " ' ' ' x

<5 <0.0007 I "al' lb/d Y SV. Tehsene '**D 'g <5 <0.0007 I ug/L lb/ day SV.1.2-Trono-

88chteroethylene

. tes ent.: I < 5_ <0..0007- - - I ug/_L lb/. day hooreethene i t.sse s - g <5 <0. 0. 00. 7_. I ug/L lb/ day hooresenene 'Fje&s)** I <5 <0. 00_0 7_. I _ -_ / L. _. lb/ day ug SV. Trlehtors-I (5 <0. 00g i ug/L . / day 1te . GV. Trishfors. wer neensae s-es.41 x ~~ ~ ' - ~ ~ ~ ' ~ ~ . s v. vany w ies tis 4 3 43 x <10 <0.0015 1 ug/L lb/ day .As PRACTiose - ACID COMPOUNDS . t aihaeropheno ~ 4 ' '79 1 t 2,oderhoore. <10 <0.0015 I ug/L lb/ day Atsse2 2: I <10 .<0.0015 1 ug/L lb/ day L 24 oemethys.

- - - W 7'l 1

<10 (0.0015 1 ug/L lb/ day 't. c.e.oivistr e-o. '"' '*i8 ' ' ' 1 _ 50

<0.0075 1

ug/L lb/ day 3 2.C+ Denier 2 "*'*C' X_ <50 <0.0075 1 ug/L lb/ day i.2I%.a!.--4 ' I l I (10 <0.0015 1 ug/L Ib/ day . 4 Nitrophenot " 8I _I _..__5_0__ <0.0075 ug/L lb/ day 1 . P4htece M. + , Pontoshoor+ _. (10 <0.0015 I 'nes sepasa ug/L lb/ day 1 I <50 <0.0075 ' Pa*"*' 1 ug/L lb/ day 0**-81 x <10 <0.0015 1 ug/L lb/ day L 2/.STri-Ice 'I <10 <0.0015 3 "P /I-Ib/dav

e .aane 001(c) WIP CONilNtfED FROM Tete FHONT

3. POLLUTANT

a. sa ann a" 3 L t Ft t#ENT

4. tJNITS

684 8 A M E I..peomer; M'f4N y q.y,qp..
" " 17 E 2b7 - - " = 3/'3. w f "...."' 4r.;..e..

'-a--"~ A.u,:i m yt m _ef,s,.e.- e_. t,,s ,,,..n.,, z............ w...... I .., e_..... OCAS FRACTION - G ASC/NEUTR AL COMPOUNDS ,z. Ac.n.ph,h.n. 08 ** *' .I. <!Q 30 0015 1.._ ug/L lb/ day. 2*J. Acenophtylene '2"" _x 110 30 0015

1..

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InUalle Station luntwas'te Trea tmen t. System t r a e n n uu m s u es..g., trom Item I ut Form t o 4. PLE ASE PHINI OH I YFE IN THL UNSH AOLD aHE AS ONL Y You.ney eepo,e son.e ue a:s of so,.n mm.,., j thes enfoernation on negerete theets fuse the smwe forater) enfeed of Covepithhg these pe Jet 4 Mt INSTRtJCitONS jg g g g g,j 04f84e / tan 00$y j Appre.ver e.p,pg pp,g g g5 g ouveXLLwu o V. INT AKE AND E FF t UENT CHAR ACTE RISTICS frontmued from page 3 of Fonn 2 c' 001(e) PART A You inust peovstle the results of at least une analysis for e_vesy 3,ollutant in this table. Complete one table for each outfall. See instructions for edditional details. 2 EFFluttst

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1 f BT BY:t AsalLE 57ATl0N 0-23-33

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[ $ f20 W2-i ses CORPORATION "~ 1300 DOlJWEWOOO ENWE SUGAR LAN.D. TEXAS 7747s (essee Manages penseusseien)

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1. bromo.S.chlere 5.S<smothytnydentnin PR'IIUCTt M Dlowrfecting agent for weaseweser NIOSH* RATINGS.__

3 HGH PEALTH HAZAfC o N13dnfmant seTR.E 1 2 MODERATE.YPEACTIVE .mannys samme een.meneenessa syews for ^-- -r; twaseous aanseness (teral. 1 CEPARTENT & TRANSPORTATION ff0fE4ATION Proper Shipping Name Calcium Hypeonteres Whnre. Dry RQ j Hasens Clase - Ouldtser ~ i ._ L '.2.~ ~ w urue*~ ~ m { MANUFACTURER NFOptAATONt Compery Name _. EES Corporemen. A sieessary er ELTECH Svosoms Carperemon Street Address ___ 12850 Baumeweed Drhre City. Stase. 21p -. Sugar Lane. Tesee 7747B ( Emergency Phone.. 1 800 424 9300 i l Omos Phone - (713) 274 4444 or tex Free 1 464 431.gitt Dao Revesers.~ 4/1 0 % Chemenal Nante % or Mirmare TLV PR. CASE Catalum Hypochterne i 88.30 % N/A N/A 7778 54 8 1 breme.3. chloro.s.S-cimethythysanteln 0.94% to 15 57BS.48.A A j SOILNERPOf0fT _ None; sary esed imLTNG PODiT N/A SPECPICGRAVfTY - { 1.8 enin (1stust) VAPOR DGSfrY N/A { VAPORPfESE7E - N/A i PERCENT WX.ATILEs N/A { SOLUBIL7TY N WATER 0% ipr weight (tmal i { pH s.s (i% eenesons DENSITY W EPC) 1.0 cou:n _ whe. es is GER - Begna enesNne. N4 rome sempeonete have a stench.Niis oeer. k te not me ' emeer as eftlerins. l FUW9Wif N/A ) ALfro llMITETBAP N/A R.AMMASLffY LB4ffB N AIR N/A EXPLOSIVEUMIT - L0nst N/A i LPPWt N/A EXTINGUIBMING MEDIA. Weser ONLY sasCw.som PommannoCrouRea { This preshes is a strong onesser. Use OM.Y weenr m tne overs of a fire er 3 a VMulert re400en may f6 Ipy 96 Wear eth breactists apparesus, i l =iesenerer The B R EN C O Corporation '** ** varie e ee-

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1 4 i 5ST BY:LASAllE STATION

10-29-93 2:58Bf. COWOMEWDi EDIS0W COWMDITH ED! SON:t ti I

i E m a3FF ORATICH SANURL til 8 MATEMIAL SAFETY DATA SHEET { PAGE2

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f LNUSUAA.PIPEEXPLDGION HAZAFD. ,,,g } Centem6nenen wnh ergenies, mees, elkales, and strong redac6ng egents wis 1 result m fire or raped desemposeen. Spontaneoue seeempeelgen lerneerature l ter true proaset le 350*F. In lesgo fires fueled by other motettale the presuet j i '"er 9m911ber '9' DNenned.mentet l THS ECTION DESMS THE NATUI4E OF T>EE M4EAPOQUE EPPECT MER.LTNG FROM EEPOSURE 70 Tw o an O o u er. 1 RtMTES On EMPORJE. 1 ) NGEgTION: ) HigMy telde by Ingesten. May cause severe 3rdlemmation and ermeen to the knirig 1 of me esconopse ene storr. ash. Prompey ineusee vomiting. EYE COP (TACT: uts to meeerses espesure to auet eeuses irritenen of the eyes. Severe espesure i f can ceues permanent Grreversible) captage. SION CONTACT: i j WSd to meeerste esseeure a cuet may Wreme the enda. Greater espeauro een asues ( severe irrit Gen. IPeiALATION: l une = mes., ..se... ie aunt cou i,,eissen e in.,m.ou. ren.e se m....p.,eary ] possegee (namei erie throst). SENelTIZWG AGENTT __ NO I i A830fMDTPMOUGHT4 SWd? HO SYSTEMICPoaOsa __ NO EMBCTS OF DVEfExposupE-ACUTE. { ingestion may remun in eromaan et me essenegue ene esornseh. Vensent. 9esets bleeeng end i posse 6e creusseery codepee. Exposure may eeuse temporary or permeent seeue camage to sadet. eyes. and reoperatory passages. CW40MC. Psionged ens intoneswe esposure mer reeuw in seeue cameos to body surveses un6ese ( q premogy tresses. iDWWNCYAPCFWWTADMIOCEDURES: { tyee: IMMEDIATELY ilush eyse weh large amouse et weser for et least 15 i renutes, heiding Tate apart to ensure flushing of etere eye surface. SEEK MEDICAL AT'TENTIONI Sun: We&h win pionry of soap and weear. Remove eensaminated elashing one leetweer. Wash meshing before reuse. Feesapeer should be demontaminated i belere reuse. Seek moment efteralen if symptome passeet. 1 4 Irinaletten: Ost pereen out et centermnease eroa to trash air. 6f bremseing hem esassped j l reeusertete and eendnister asypen if reedly ovellehte. SEEKMEDICALATTUmONI b. tr.gestion: NEVER oive any1Nng by enousi to en urioenne6eue pereen. Feed breed =~ 4 J in reek, fellowed try oevo er seeeeg etL DO MT immane veertap. Cet a 1 phyenelen immedletelyl i l i 042490/dd j i

i 1 261 fn :LuAul MATION ~10-29-93 0:MPM COWOWEALTH EDIS0W C0WOMULTH EDIS@:: 7 i i l* EE8 CDFGHTDi t 4AS4URE. til I MATERIAL SAFETY (MTA SMET I PAGE3 i 1 6. le .n. % 2: -Gi 4*tEie.L - -~ ~ -- --ts' ' M ' " " ""*!'"lReGeEB4 s t Conoinone contnbuen6 to instabutty: k Canartenalen watrt flernmeWee, Organico ener cause fire er emplessen. W l well ro6eese dniertne and trerverie gas. incompettblety (Materiefs to eved): f Aside, flammetdee, ergenic anatoriale, reeady cueelaeWe matortete and strong 6 } rosademg agente j Hazardous decorupeestion er bypreewate: { Chiertne gas, hyeregon bremmes, brenthe ene G4^.. ordenes Hezerdous polymenaasen: .._Ihis nroduct is ret knowrt to morrmartte.. J i I Neuvenains Chemmese. Seeum suefile, sosiinam biedtne er somum restabiouNfts. i stepe in to Taken a wesenes no Renessed enwer sesee i i Wear sopropness protocewe gear: rueber gaewee ens heets. Chemies aplash gegpee and } L J er.emin, se,..us n nees...y. 4.eid es,sem m.m ca g-a,e may re.un. i ,d Dilute seHI area witt twge quenuties of seter, et least 100 geene of water per pound of n metenet. Awees contees weert reeussng assumen. Neuereltre WIlh sedhon oudlie, sedum bleurfke er eseum rnatabeleua#te. Collessed neueregese oosuelen shoutel be W et through i newege wommerit pient. Prior soprowel trem plant pereennet se wed as Lesel. steen one j Federal entarenmental agenones oneuid be oMainest Rio ortwironmental spie nashcesions if neesseery. Weste 06eeseel Weineste .I I 00 NOT espose of meterial in cry term in weets eerstelper.. tire may resuet. Proceed wah spiu a,s ur. ovoin.d see.. 1 Additional Preceuunne: 3 i Do not asempt to recover need metenet. De not etapene of menertal in weses conseiner. I Do not rouse empty container bwt psano en trasen esteesen. i Q{'T'.][ - ' [ ^~-~ T ,7 7 ; ', - - ' 9--~, g // g3g.,% yy .f, Ventlemen Requiremente: Werk in wet vonessed etees. Storage eres ehened be well venslated. Specific Personal Presseeve Etudpenent: Reapsesary prosessen is not resumed unser nennel use, howower when j ' - rp. use NIOSWW94A anyoved roepireest tallowing manuteaturer's resemmeneesene. NIOSH esproved east mean is eeeensief wn o aseeng may oesur. Eye Pressamen. Chenseel sehMy glasses eheidd be worn. Preasseve Gloves:Gioves sheed he usern. Ruhter er emer enemloety feelstant mater 6 ele are tenommerHeme as nestadste motorted. Other Clothing and Etadomasit-Pfuesellae elettirig shewhi he sem se as to m6niedse ehen corsteet. Aveld centest wetri eleth mg Pire may roeuel from eerstems of ey menenal weth clean er femmettes. 0488DB/ del I

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ENT BY:LbAllE STATION 10-29-33 2:59PM. COWO9EETH EDl5# COWONEETH E. DISON : 8 J

EESCCHIG MTEN } SANURIL 115 { MATERIAL SAFETY DATA etEET PAGE 4 [ 9. [S ilf er r U. 7CT 6tfMf.hcW;shee-e'. . : -- ri ; --- It - s= w-m..----5.e _e -- e e i DAMER: l hegrey corressee. Causes shan and eye esmoge. May be heel N esenswee. DO NOT j get in eyes or on cesshhg. Wear gogg6es one CLEAN presseeve giewee when handing. Irruaung to nose and mroet. DO NOT breesne sust ene Gustwo. Wenn thoroughty we toep ens water ener hane6ng. Remove ene ween contanteneses meeting before roues. ) i This seesuet le sonic to teh. 4 i M aceeroonas we an NPDER pernet.Do not doenerge tene lahee. eseems, pense er pWise water j i d Strong anastalny agent. Mia this product enty weth weser. Une maan dry.asseesta. Coen contener onfy where oossueno veneNeden te evaBeble. Do not add mio pseuct e any eewise eenimewag torneene of any other proeust. j h case of cornenenmMovessempeemen. so not ,eems eenwiner. is poemmis. re... concen.r in op.n e., ano moea we ierg. vem. o,.amr. sTamaE: j Keep preeaet dry stia in a nghey aseos eenasmer when not in use. Store en cost cry, wel \\ verrstated area. keeperig it away from heet seuroes ansMur o 4 j cars-00 NOT drop, rol or skie. M case se escomposeen, pen Bemes. Herode conteher with flood we large amounes of enter to stesehe au masomet. namese contener (tf posesse) me 3 se eusined h season 7 of mie Ceta sheet. Fenou 'Spel ans Laan hee" i 4 Kees in eraginal container. etthout the approval /aushenzstion of EEE Coepereden.DO NOT storenransfertrop i I, Ol8POSAL-1 l Follow *Soll one Leak Procomaree* an ouemme in Gespen 7 of 1his Ossa sheet 00 NOT reuse empty cornener. Wash maroughly we meter ano sketerd seen centainer in a safe peace DO NCT CCNTAM5nTE POCO CR RiED BY STORAGE. N OR Q2Ahpe3 Oft Ecuresed 1 i ) i AN irtformanen on thee firm 6e f.arreshes seisy ter me puppees of comptanee unm 00HAD Corrv'sc m sta=2 ggra 3e10.1200 ars i ene shen not he -- for erw ~ z - i i I i 5 1 i l 1 1 4 4 0 1 042690/ed d i J i

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m. 4- --- a RiW ~ I Cowomen j cAs No. s i PEL/TLV - SOURCE Socium Mitra te, Pw 7432-00 0 se ein. 2 a'5/e3 SA5F Corp. ecc. l I All caugnaremrrts are tre T5CA t... .bE y, SAAA Title 111 Sect. 313: Dept listed. i' i f f ? SCILIN8/8ELT2188 PCIIfT #790 sua regt w/A / 280 C pett -0.0 (Ass. sol.I f WAPOR Pett$3uile em peg cyc C: N/A l Desemp. tems.. 330 C 'saectric anAvm on suuc newstrY: 2.ss na isoo-tsoeng/. SOLUSILITY 190teATER: 5dlumit # 30C 818g/C ' ~ l AMlAAAfdC8: Yelleg Cryytels MIM ;geogus 19ff13SITY

t

' =tidWaa Milkm i } FLA5et POI 8tf (T127 IKTM101: et/A MITales1713e Tsite: N/A f PLAan6482LITY L! art?S 1N AIR(1 SY )CL) LOIER: N/A N: N/A i exrzmaurs,a I u.e w. =,og.,1in,,1enin,e s.r., we w wint,tr. j aEDIUM l te eti11 emusIl. If 1arge seelant8 are irweIweid. rittritm eey SPtC1AL fuse or seuIt. t n writ era canet t f ort. weter amey name erterutIwe ) FIas P1ertIMS Amanes scattering 09 asI ten anytaI. Ft PefIWBteGro emet tus godisques i with self _ ;s trung L _tpttete emmergtess arW M. Jt meer'. m pggg A strong canelatng aguret ta captiedrt wi th erTente matter. Abe OtPLcS!tDi 48111 tgnt te try f etction or rtest. N ( _m 5""7 5:.5 t x =t. C oo.rc.teoo 20t-sw-sooo - i ~>s -. rs..r.au o.,s. w s.. m c s. m uo.,s wint u o DAGEE 1 OF 4 i I

1 4, sENI BY:Lua.tif sIM10N

19-23-93 3:u0PM CO.WOWEALTH EDISON-COMdONWEALDi EDISOM*10

,1 d l PRODUCT NUMBER-491392 sootue wetette. sti NU W-[- !E*-E M M M M M E M Y [' 5 M.: q t TOXICOLOGICAL. TEST DATA: f RESULT: Seef tsu N e tri te, Ptf -} 4 Ast. Oral LDL50 i atamen, orel LDLo 85 mg/kg. 'very tental 3 3 og/kg. 4 k l EFFECTS OP OVEREXPOSURE: eeutes et i enosaure to tnte estersal inclues eye one amen contact er 5 enhelstion. Seetus Mttrite one eseammas soluttene of eastue nitrite stay les severely derstating to the eyes. Tne pouser'esy else act se a esenenecal Irettent et 3 the suln erus reestratory tract. Ingeett e of targe essete se tnte maternet any cause nemmes, venttine, cyaneses les a result of ameneaeglehen preewettent, eenwulesene one emes. nesseense, vtausI preeIese one mooressee Mese pressure.Ceoente easpeare to neerttes say seues l Nitritem asy react i j wt tre memonsory ane tertiery sesnos te fera nitreesetruse, wetten are enemel carctnoenne. Seetue nitette vos not enretnagente taten fee to rete in the a etet et 0.2 er e.5% f or km to t te weeke. 1 Eatetirug eseicol cone tione omrevetae try eesseure to enie meteetei i k fee informatten feures por tftte etarture. FIRST A10 PROCEDURES: j tree-Iseeststely wenn eyes with rwettne water for te menutes. 4 1, Get temastete emelcel ettenttert. j 'l 3RIn-wenn affoctee ereos w6tti weter. temove one Iawneer* eenteeietstes clo ththq hef eet eguse. If trrt totten seweseon GeneWlt e perys acien. j trigestsen If swallowse. Wilute with water one temestetely Iraeuse 4 vestting. Desver give ()utes se tasase vetttfg tf the victes 4 1e uneenseteue er Peevine comwIelen. eet iessetato meelesI ettanttan. } Inreistien-seve to #reen ate. ate tn erwetetirg, if namessary, one yet senestate meetsel ettentsen. 4 l 1 f ( .!b==-- '= = r~~ --' a - -- m - _ s

. n. :r: e..,.

.. ;. ::. = ?,T v= r.+t~r- ~ ' ' 4 ~ 1 M.= ,-t.t r 14_; 42 -,, m y STA88UTY: stmete. ostetaes estertete, a f tre se eieplesten ser ensur.avete strong estetsers. In ee ) Cotem0NS TO AVOID, CN BdCOhrATISLATY:

eensatas, tectets., eyensene, ergente metter.as j

NAZARDOUR DeConrosmON PROOUCTS: seu *uesa. se euttttoe. estemtausfatee. l HAZARDOUS POLMERIZATIOft g n.,,,,,,, CCDeffl005 TO AVOer redusse er preennes of anierseas one malestes, CORROSNE 70 NETAt: sie j om yee AESPIRATORY PROTECT 10ft t 4 thast assu. I f earte t t lene werv"ont. If tne remessenese P.E.L. se emeenene. weer en appewves esos roeptreter. I t h EYE PROTBCTIOft stes-entese safety gleeses or eneeseen geeses. 1 PROTECTNE CLOTHING: Cl***e.== ene, apron, timets as namessary to prevent sain contact. VENT 1LATIO82 use secos sem to cente I seaste. OTHER. ufa f PAOfr *A mer 4

, 5ENT BY:LMALLE STATION

10 ^9-90 3:n!PV COWOw3*LTS EDIS0W CCERALTd Edison: ell a

PRODUCT MJMER: 491392 see1us Nttetto. 84W ig s f2 ; M a m i d # m m e! m ii C ~ 2 P f S F J s W 5 s i n ni t M ;; 4 ENVIRONMENTAL TOXICITY DATA: ..ie. SPILL APO LEAK PROCEDURES: s.o..,_ is - se,,t.t n.e.,,. e.i nees i r, su, l t.m.i. eent.,n.c...e e. es., n. eCea it n.ee, 1itty. 1,.. se t er.l. t. e - -e to I t. 4 - 1.e.. HAZARDOUS SUBSTANCE SUPERPUp Yes R Q (lost 100 WASTE DISPOSAL METHOD: !nertnerate er ensey se e seile artly in a a(RA I f our,see fooMt ty. De not elecherye Into tasterwys er esaser ey.tems witneut propee autnertty, i HAZARDOUS WASTE 40CFR261: Yes HAZARDOUS WASTE NURASER:e 001 CONTAINER DISPOSAL: tapty containers with less then t snan et restaus eey me lanettites at a 1eeenees factItty, meeenseed erwentny er other aumens to prevertt unauteter1seg Other eentasnees ause me etseemme of a n a acmA i e amanes f mee a e ty. reme. i Sedlue Nt tre te _R _A _ t ves--sestaan attrete REPORTABLE QUANFffY (RQ) D.O.T. HAZARD CLASSFICATION (CPR172.101-102) m PRIIRARY ontaeser SECCISARY i D.O.T. LAmpt_3 ps'OUIRED 449CFR172.101-t o2) 0.0.7. PLACARDS 'POtSON CONSTITimtT j R (CFR172.504) M9CPR172.20390) Ossesser ser I (1906) l SILL OF t.ADehG DESCRIPTION t Sectnas Mitrete--Outstaer --t.Di 1900 he CC NO. tse ' UN/NA CODE 8800 i DATE PREPARED: 2/ 13 / se gpDAs uzr; 5/ ts / so l

t!LE BASF CCRPC#ATioN etLIEvts TM CATA SET FORTH HERE!te SSE ACCUBATE a5 0F Tat Qatt *(et0P. BA SP CDePORATIO81
TAKES M3 WARR6NTv wtTH atSPECT TwittTO A@ iL>#E55t v D25CLAlors ALL LI A51LITY FOR etLIANCE THEllEON.

SUCH DATA aat OFrtatD SOLILY FOR roue CON 510E R AT I ON. I NVE STIGAT3 Cle, aND WEDIFICATION. s een a e

P AGE 3 OF 4 I

RM BY:LtS.EE STAT 10N

m-?*-9?

Tc:PM : Ofs3MDdId EDl.%9 umWNCEALTH EDf50N;*12 PRODUCT NLMBER 491392 senius Mitette. EW b Soolum filtrite, ow 4 DaNGte: OXIDIZCR. H&eldet)b CR FATAL IF StiaLLDetc. P!At AND/04 EXPLC110N mat DCCue 2F P90 DUCT coasts IN CONT CXIC12ED EAftRfALS. Y { CNTACT titTH SOD!Uas ntTEITE aNO ITS 50LUT!045 neaY RESULT CF ffES, C08f7ACT MAY IeRITATE THE 3stIN AND RESPIRATORY TRACT. itpf DeIONIC f tp0SURE 70 ad!Te!TES haV CAUSE M'Nr".INatstit># stav RES t. 4881888510 F0sel NIT 8h05AftINES, set!CM ARE ANI8tAL CastctacesseG WIS43aL peacettes-ANs j f84TE: setTHgunas nagsegatIA. 3PaE9dAfff W0 teen MAY tt ESPECIALLT StadSITIVE TO NETRITE-SEN use wsen iemal emnswet.avete contact with eyes, skin er cteeming. Avees enreatning tseste trear a art 0 set /sesMa-asescoves mast reemerater. cnemical necessary to prevent contact.peggles, glares. coverat ts, moren, emets anos etner protec I 3 Fle57 AIO: tyee-!amestately wash eyes with rurvisng watee fee 15 etnutes Get sammeeste susescal attentsen. l skin-Ween ef fectee areas with wtee. i Remove one launoer contassinates cletnerig snevece eewse. If I pays ieiart, scritetten movetese eensult a l f Ingeotten-If swallouse. estute with water one teametately sneuce } veesting. is uneenectaus ce neweng convutsioneasever gewe e tutsss er ensases weetting si the viette I tretalatten-teeve to f resa air. . Get temas1ete emelesI attentiet. j get temmelste meccal attentlen.Als en armatning, if nemeenaer, ane IN CASE OF $# ILLS 04 Ltaats: estereat ts a eaub-regulateel prec.act. eneute age sentaines, assereas ans planes in sof tsele mentenners for etspos l settis in a eCRA.4iconses eoctIity, a i !N CASE OF Flet: Use water fog. saattering et smelten eatertal wnen larTe iluentitles are trastree in f tresasolleetten m Preshet we ll esspleos wnen neates to 538 C oc uppen montact ( Fireflytters shoule see seweppes with self*eentaines areething ap i witn cyantees. turnmut gear. l paratees one i F9PTY CWNTAINERS; all staring ane traneserting easty containere asse to preekset restamassIatseles p cause this container urtiers et is profeestenelly cleanne one recen. De not si t t ories. otsp0$AL seeItest estertat. unuseus centente.ans empty centaenere mast sue casesses of te menoreerse wete temet. to mar statertal Safety Data Sheet far seesteto stonemalssete anse femoret reyetstsene. aeter Instrisettene. i III CASE OF OGet! CAL meneflCT: enferestien concernany sealleo seeseeaI. Call CNE8ff90C doy or night fee aeststense aree q asstaante. 600-434=5300 fIce, essseeure ans other annotceI aTTElfr!as: Thie> preekset is sets solely fee use my oneustesal ina t t tut t ores, Refer to amar Teormical nullettn ene testortal Safety Dat safety, usage, asuplicat i Caneult youe supervenes tene, hasares, prgeseArea arte disspetal ofa Sheet rugstging I

er asettienel-tr m tles.

tnis preshact. NJ/PA/ eta /ca. RTM stevtow: 7632 00-0 SeetuneIdttrite I woon en tseet eereony 4 Preser Shisetvg Messe: See1um ititrite-= tad 1500 Ib0 Iritereeseate Cneuntc4Ie C990 i

Pe0% 4 6 8 f

PAGE 4 OF 4 7M db i i /hhf - i

i i - ST BY:LISALLE STATION 0-29-83 a:0?PM CMTMECU I:Dlh C'Mun.ALTH 2Di$0N: 13 e,fu no mummmmuse 1 MATERIAL SAFETY DATA SHEET } ~ PRODUCT { j NALC3 9249 LIQUID j N ALC O l n==gency Teleenone Namser neesleet(708) 93o 151O(34 heurup SECTION 1 PRODUCT IDENTIFICATION '"RADE NAME: NALCD 9249 LIQUID { OESCRIPTICK: An aqueous solution of a polyacrylate s j WFPA 70sMAD(IS RATING 1/1 HZALTH 1/1 FLA306ARILITY 0/0 REACTIVITY 0 orHER C=Insignificaat, l= Slight 2=Moderata 3=Migh awEstreme ~ j SECTION 2 NAIARDOUS INGREDIENTS l i cur hazard evaluation cf the ingredient (s) under 0$RA's Easard Communication Rule, 29 CFR 1910.1200 has found none of the ingredient (s) hasardous. ( SECTION 3 PRECAUTIONARY LABEL INFORMATION J CAUTION: May cause irritatico to skin and eyes. Avoid contact with sxin, ) eyes and clothing. Do not take internally. nupty containers may contain residual product. Do not reuse contatner unless properly reconditioned. i SECTION 4 FIRST A!D INFORMATION rYts: Plush with water for 15 minutes. Call a physician. SKIN: Plush with watar for 15 minutes. INGESTION: Do not induce vaalting. Give water. Call a physician. INHALATION: Remove to fresh air. Trent symptcas. Call a pnysician. NOTE TO FMYSICIAN: Based on the individual reacticas of the patient, physician's judgment should be used to control symptans and clinical condition. the j CAUTICN If ur. conscious, having trouble breathing or in convulsions, do not induce vomiting or give. water. SECTION 5 NEALTE EFFECTS INFORMATION FRIMERT ROUTE (S) 0F EXPOSURE: Eye, Skin EYE CONTACT: May cause irritation with prolonged contact. SKIN CONTAC:t May cause irritation with krolonged contact. SYMPTOMS OF EEPOSURI: symptoms free exposure not previously mentioned.A review of available data does not i AGGRAVATION OF EXISTING CONDIT! Cats: s' not identify any worsening of amisting con:11tions.A review of available data does PAGE 1 OF 7 peas.co GMemelGA&, CosWWAfeY ONE NALCO CENTER e NAPE 8WE LEL ILLINOIS B05831198 AREA 7D5-305-1 CXX3

5ENT BY:LASALLF ST4T!OY

G <3-33 eoasi COWoWEALDI EDISON-Coh0doMEALTH EI)! SON: 21 MATERIAL SAFETY DATA SHEET i

IPRODUCT i, NALCO 9249 LIQUID I NALCO i. i { Emerreur Telegeene Number na. eases poop 330 tst o (24 hourup SECTION i 6 TOK!COLOGY INFORMATION 4 1 } ACUTI TCXICITY STUDIES: l The results are shown below. Acute toxicity studies have been conducted on this prcduct. 5 ACUTE ORAL 10XICITY (ALBINO RATS): i

D.,

I a Greater then 5,000 mg/kg i ACUTE DERNAL TCXICITY (ALBINO RABsITS): i k LD., = Greater than 2,000 se/kg PRIMARY SKIN IRRITATICN TEST (ALBINO RABBITS): I SKIN IRhiITATION INDEX DRAIZE RATING: 0.0/C.0 Non-Lfritating i } } FRIMARY EYE IRRITATION TEST (ALBINO RABRITS): _ETE IRRITATICM INDEX DRAIZE RATINGS { 2.7/110.0 MirN11y irritating j SECTION 7 PEYSICAL AND CHEMICAL PROPERTIES COLOR: Clear water-white F0EM: Liquid

ENSITY:

10.2 lbs/ gal. ODOR: Organic SOLU 31LITY IN WATER: j SPECIFIC GRAVITY: Completely .2L - 1.23 8 60 Degrees P ) pH (NEAT)

3.6 - 4.0 ASTN 0-1298 VISCCSITY:

FREE 22 POINT: 51 eps S 60 Degrees F ASTM E-70 20 Degrees F ASTN D-2983 FLASE POINT: Wone (PleCC) ASTM D-Ll77 i A52N D-93 j morE These physical properties are typical values for this product 3 SECTION { 8 FIRE AND EXPLOSION INFONOLTION FLASE POINTr None (PMCC) ASTN 3-93 i EXTINGUISHING MsDIA: water is boiled away. 'The remaining organics'aey be ignitablThis prod i ool containers exposed to fire. i e. Use water to s j UNUSUAL FIRE AND EKPLOSION HAZARD: containers esposed in a fire should be cooled with water to prevent va I i pressure buildup leading to a rupture. A i 4 j SECTION S REACTIVITY INFORMATION i INCOMPATIBILITY: Avoid contact with strong oxidizers (eg. chlorine I which con generate heat. fires, emplosions and the releas l percaldes, j ) THERMAL DECOMPOSITION PRODUCTS: umes. In the event of combustion CD, CDs, Nor mer i PACE 2 OF 7 NALOG CMWestCAA COhedR4818Y QNE NALCO OFNTEM e 484EA 7ceNsos-s occ NAPE 8tMLLE. ILLINOS SOSes.119e

- - - -. - ' ~ " - ET EY:LiSALII simon q0-23 33 3:g3pg g,.)W.MEALE EDIS0W COWONWEALE EI)isoy;45 MATERIAL SAFETY DATA SHEET i PRODUCT j NALCO 9249 L QUID i l NALCO i Emergency Teleahone Number I Meetset(70s) esd>1s10(s4 hevfel SECTION 9 REACTIVITY INFORMATION i ( CONTINUED ) i i be formed. Do not creathe smoke or fuses. Near suitable protective equipment. j SECTION 10 PERSONAL PROTECTION EQU!FMENT i i i RESPIRATORT PROTECTION i the volatility and tericity are icw. Respiratory protection is not normally needed since If significant vapors, mists cr aerosols j are generated, wear a NIC5H approved or equivalent respirater, i For large spills, entry into large tanks, vessels or enclosed small i spaces with inadequate ventilation, a pressure-demand, self-contained breathing apparatus is reconnended. r VIvT:LAT:oE General ventilation is recommended. PROTICTIVE EQUIFMENT: when attehing f eeding equipment or doing metatanmee.Use impermeable gicves j The availability of an eye wash fountai.n and safety shower is recommended. 4 If clothing is contaminated, remove clothing and thoroughly wash the aff ected area. Launder contaminated clothing before reuse. SECTION 11 SPILI. AND DISPOSAL INFORMATION i IN CASE OF TRANSPORTATICK ACCIDENTS, CALL THE FOLLOWING 24-HOUR i i HLEPtElWE NUMEEE (7C8-920-1510) 4 SPILL CONTROL AND RECOVERY: i Small liquid spills: Contain with absorbent material, such as clay, soil or any cosearcially available abscrbent. into recovery or salvage drums for disposal. Shovel reclaimed liquid and absorDent Refer to CERCLA in Section 14 Large 11guld spills Dike to prevent further movusent and reclaim into recovery or salvage drums or tank truca for disposal. in Section it. P'afer to CERCLA 015POSAL: If this product becomes a weste, it does not meet the criteria of a hazardous waste as defined under the Resource Conservation and Recovery Act (HCRA) 40 CFR 251, since it does not have the characteristics cf Subpart C, nor is it listed under Subpart D. 1 As a non-hasardous liquid isaste, it should be solidified with stabilizing i agents (such as sand, fly ash, or cement) so that no free liquid reemins 1 PAGE 3 OF 7 ma ten esementoAL ceasesuseY CNE NALCO CENvEA e NAMERVILLE. ILLINCIS 80583-119Q uneA 7os-aos-s coa

i et ei v M.if afATivi w-23-93 3:03PN COWOWEALTH EDISOS-COWOMEALTH FDISON:s16 i MATERIAL SAFETY DATA @HEET PRODUCT NALCO NALCO 9249 LIQUID n z....e., ru a.- aseeno 1(70s)0301ato(s4 noem SECTION 11 SPILL AND DISPOSAL INFORMATION i ( CONTINUED ) before disposal to an industrial waste landfill. A non-nasardous liquid eraste can also be incinerated in accordance with local, state and federal r egulations. SECTION 12 ENVIRONMENTAL INFORMATION AQUATIC 3LTA: 96 hour static acute LC,, to B1 cog 111 Sunfish = Greater t.m 1,000 ppe i i 96 hour no observed effect concentration is 1,000 pga based on no mortality or abnormal effocts. l 96 hour static acuta LC,, to Rair.bew Trout = Greater than 1,000 ppa i 96 hour no observed effect concentration is 1,000 ppe based on no nortality or abnormal offocts. 9

48. hour static acute LC. to Daphnia Magna = Greater than 1,000 pps 48 hour no observed eff ect concentration is 560 ppe based en ro mortalit abnormal effocts.

y or l 4 T3XICITY RATING: Essentially non-tesic 96 herir static ecuta LC,. to Mystd Shrimp = 464 mg/L TOXICITT RATING: Slightly toxic 96 hour static acute tc,', to silversides (Menidia beryllina) Greater than 1,000 mg/L = %IICITT RATING: tssentially non-toalc

1 released into the environment, see CIRCLA in Section 14.

SECTION 13 TRANSPORTATION INFORMATION a DOT PROPER SHIPPING MANE /HA.tARD CODE - Pst0 DUCT IS NUT REG OURING TRANSPOItTATION PAGE 4 OF 7 MAA.co cMemmocAL SOA4sBANY ONE NALCQ CENTEpq e NAPERVILLE. aLLINQ18 801563-19 98 E 8 tea 7DS 305r 1000

5DT BY:L4SALLE STATION 10-03-93 3:0FM COWONNE.u.TH EDISON-C0!al0NNEALTH EDISON::17 l MATERIAL SAFETY DATA SHEET i i PRODUCT ) i NALCO 9249 LIQUID i NALCO Emereeney Teleehone Nunrher meneest troel e301510(s4 hevrug i t ~ a SECTION 14 REGULATORY INFORMATION 1 "he following regulations apply to this products a FEDERAL REGULATIONS: 05KA's MAZAND COMMUNICATION RULE, 29 CFR 1910.12003 Based on out hazard evaluation, none of the ingreetients in this product i i are hasardous. I i CERCLA, 40 CPR 117, 302 t Wotification of spills of this ;:roduct is not required. SARA /5UFERFUN11 AMENDNENTS AND REAUTICRIEATICK ACT OF 1986 (TITLE III) - SECTIONS 302, 311, 312 AND 313: I SECTION 302 - ECTREMELY HAZARDOUS SUBSTANCES (40 CFR 355): 1 This product does not contain ingredients listed in Appendia A and a as an Ratremely Hazarcous Substance. SECTIONS 311 and 312 - MATERIAL SAFETY DATA SEEET REQUIRE j Our hazard evaluation has found that this product is not Fazardous under 29 CFR 1910.1200. SECTION 313 - LI57 or TOXIC CEEMICALS (40 CFR 372): This product does not contain ingreaients on the List of Toxic Chemicals TOKIC SUBSTANCES CDerTROL ACT (TSCA): The enemical ingredients in this product are on the 8(b) Inventory List (40 CFR 710). RESOURCE CDNSERVATION AMD RECOVERr ACT (RCRA), 60 CFR 261 SURPART C t. Dr consult Section 11 for RCRA classtfication. FEDERAL WATER POLLUTION CONTROL ACT, CLEAN WATER ACT, 40 CFR 401 15 (formerly Sec. 307), 40 CFR 116 (formerly Sec. 311): j Mone of the infredients are specifically listed. Clean Air Act. Sec. 111 (40 CFR 60), Sec. 112 (40 CFR 61, 1990 Assendments): itis product does not contain ingredients covered try the Clean Air Act. ' STATE R3GULATIONSI CALIFORNIA PROPOSITICK 65: PAGE 5 OF 7 NALasas OMS 8ustsBAb CashesmasWY ONE NALCQ CENTER e NaimERVIL 1 s AREA 705 305-1000

_,_.._.m {- DENT BY:LASALLE STATION

10-29-93. a:04PM. CoWOMEU TH EDISOP COWONWE.U.TH EDIS 1

MATERIAL SAFETY DATA SHEET i PRODUCT i NALCD 9249 LIQUID l NALCO i ,,o er r.,.e.e,.. m,,,,.e, lese 6ost(708193o 1s10(34 heerst SECTION 14 REGULATORY INFORMATION i ( This product does not contain any caemicals which require warning under { California Proposition 65. j MICHIG&N CRITICAL MATERIALS: i "his product does not contain ingredients listed on the Michigan Critical-l Materials Register. i STATE aIGtT TO KN0sf LAWS: } The following ingredient (s) are disclosed for compliance with State Right To Know Laws: Acrylate polymer Trade secret i Inorganic salts Trade secrets j Water 7732-18-5 INTERNATIONAL REGULATIONS: I j This is not a Wit (IS controlled product under The Mouse of Commons of Canada sill C-70. SECTION 15 ADDITIONAL INFORMATION i 1 5 isone SECTION 16 USER'S RESP (1NSIBILITY j This product material safety data sheet provides bes1th and safety j intornation. j our product literature.The product is to be used in applications consistent with Individuals handling this product should be informed of the recossmanded safety precautions and should have access to this information. For any other uses, esposures should be evaluated i so that appropriate handling practices and training programs can be j established to ensura safe workplace operations. i local sales representative for any further information.Please consult your l SECTION 17 EIELIOGRAPRY j i ANNUAL REPORT ON CARCINOGENS, U.S. Department of Health and Human Services, P.2blic Health Service, PB 33-135855, 1983. a CAEAR2TT AND DOULL'S TOKICOLOGT, THE BABIC SCIENCE OF POIS0sS, Doull ) l N. Y., 2nd edition, 1960.Klaassen, C. D., and Adnaar, M. O., eds., Macmillian Publishing Company, Inc J., 1 I J i PAGE 6 0F 7 i NALCes 084See# CAL OG8u8pA8WY CNE NALCO CENTER e NAPERVILLE ILLINCH _ _ ooo E 80583-19 98 4

i n.M ci:LOALLE STATlos

10-:?3-83 3:05PM COWO'dEALDI EDISob COMMEALTH ED150N:*18 MATERIAL SAFETY DATA SHEET PRODUCT NALCO 9249 LIQUID 1

N A LC Q Emereeney Teleehone Numeer leesteel(708) S301s10(34 hourse SECTION 17 BIBLIOGRAPRY ( CONTINUED ) CHEMICAL MAZARDS OF THE WORKPLACE, Proctor, W. H., and Hugnes,.7. P., J. P. :ipincott Company, N.Y., 1981. eds., OANGDtCUS PROFERT!ES OF INDUSTRIAL MATERIALS, Sax,N. i Irving, ed., Van Nostrand Rainhold Company, X.Y., 6th edition, 1984. 1 IARC MONOGRAPHS ON THE EVALUATION OF THE CARCINOGENIC RISK CF To MAN, Geneva World Health Organization, International Agency for Research on Cancer, 1972-1977 FATTY'S IIIrJSTRIAL HYGIENE AND TOIICOLOGT, Clayton, G. D., Clayton, F. E., eds., John Wiley add Sons, N. Y., 3rd edition, Vol. 2 A <., 1981. REGISTRY CF *:OKIC EFFECTS ON CEDCICAL SUBSTANCES, U.S. Depart:nent of Health and Human Services Public Health Service, Center for Disease Control, National Institute ter occupational Safety and Health-1983 supplement of 19tf1-1982 a11 tion, Vol.1-3, OR,1964. Title 29 Code of Federal Regulations Part 1910, subpart 2, Toxic and i Mazardous Substances, Occupational Safety and Hes1th WM stration (OSHA) THRESBOLD LIMIT VALUES POR CREMICAL SUBSTANCES AND PHYSIC WORKROCDI ENVIROIOGNT WI"'8 INTEMDED CHANGES, American Conf erence of Governmental Industrial Hygienists, OH. PREPARED BY Ricky A. Startrhause PhD., Tealcologist DATE CHANGED: 07/22/92 IRTE PRINTED 11/14/92 i. 1 d 'l 4 received 1/2 /2. /92. I i PAGE 7 cr 7 NALGE3 CHEhelcAL CC3eem4NY ONE NALCO CENTEM e NAPEF%nLLE, ILLNOsa BOSS 3-11Ege wasA ros.aos.1000

2 1 x.u cr:LbAtiti siAimN 10-23-93 3:05PM COWO.WEA1.TH EDISON-COWOMEEALTH EDISON;do l' ?"gg MATERIAL Sr DrySJ SAFETY DATA m. l N.. Network E"' "GENCY PHONE 1800 OLIN 911 4 i ~ s SECTICM I IDENTIFICATION 8505 FILE **0 I @ffMICAL NAME 4 ?YNDWYMS 1 I 50e t tet 7,;p _.,_,, ], [ ,,I i l CHEMICAL FAss!' 1 lPORealLA falkal? PROERACT Naos. Lawnt:c Sees 50% Rayon Crece-DESaft!PTION Cl ear ee t er * **- a s t u t ic" CAR NO. 1310-73-2 i 4 ~* TION !! - NORMAL HANDLING PROCEDURES ? j ! PRECAUTION 5 6-" 'i r IAKEN 90LII*E AMD 5!DItAGE May to fatal gwellow*" ,' i o contact wit % eyes. eben or clotnta0 upon contset weth settn oc .ve.. ...n. - ..th ..t-- ., cre.tn.n,.t.t. sto,e ,n a.e.i-..ntti.t ..ee. s.eeret..t Je-eas, me t a l. aan esotoa-e t$e a ot'uttne tae solution, asways ace it to tme mater. d er.91ng ,=mter to tha * . i t eat ee - ncesst%e neat anct may cause selettering. Mave safety showC* me

.ye..en....-.

e l I occTtCTtvt r ew"cutarr t vtMTILATION 80gWIREDItpf73 t I j tvE5 tt ee i e - googles '*esnieto 4 a s roow tree to homo * *coorrw concentrattens GLOVE 5 *iene** 1* *Vf metow TLv. crHet

ever--

ano ee-- SECTION !!! - HAZARDOUS INGREDIENTS i BASD MattatAL 05HA PEL LD50 LC90 soo u.e nyoea-e StenrFICANT EFFECT$ h agr'i3 isso sets P*o cata I Coerpetwo to all tissues i contacteo. l l t ION IV - r!RE AND EXPLos!ON NA1ARD DATA }03MAClA35IFICATION8801 FLASM POIMf ' finame"' werwoD I"*on-$onunate F'**""*"Lf Lowtm ~'

- ,wastoe uPPet E8'Lostv.,s. o.

,s.. i EXTINGUIENIN'1 "!DIA P8cn L! sert i ettble, out may l SStef AL FIRr f"7 Aste a r ar * . *innt *t=e ana raeltgnt te comeustunne mater ials or organic sat ter geratset. 5 4 r~'..-2HL3Aff ' annaamm cantainmen_ on ,,s e r -cont s te" ersa tn t er '"aff2NG Pa0Crimmas use #10&M/MSMA s 'ratus enere ints astects) espeeves posittwo eresswee to involves in a etre, SECTION V - HEALTE RA1ARD DATA miter 10LD LI!" VALIJE See suso a een* me v 2 so. * * 'reeitae) r 19sg.g? ) 5Vk,susg5 0FIi'IR EKPD5Uf Coeecstwe ' e, * * ' **wount qactee LMERGENCY FIN 31-AID P-5-"""3 t,gtw p1usn w w a t er' ' ruutes. esit a cnvesetan lrygg fmanegin fluen > y .ater for 18 minutes = t tn eyes no tcr open. call e omveteten l b--J____. $Norgttty Or "

1 eros cru ti_s o' meter.

So - e C411 a pnveteten. L -] imgro. m- - a t r. i casi a env.ician l -i

dEM M:LuiALLE STATION 10-29-93. 3:05P.M. COWOMEALTH EDlSob Coholoh1EALTH EDISOM;;21 i n e r.= 1 C DC c>stm2 CAL NAM Caust te Soes 50E teven Crees } 1 4 "ECTION VI TOXICOLOGY (PRODUCT) j ACUTE CRae Lg So we. asev ce fatsi le cAaCINDetattCITY Not known to me carcinogensc swallow,*i anJTAetNICITT Met known to se.eutogente i ACUTE Ctf"**t LD 50 !Yf IRRIT ATION Corroe lve i no eats i painsaaY SacIN IRRITATION l j A3JTE :Po***ATION L Correstwe 1 no cats I l PRINCIPAL

COTES CP"o7204

n,s i e t,,..

oor..i 1 ) ~ a trFtCTs er acutt Exon" e a svene ee a<eesee tee-

eeowe+:t t v resul t ene in coeo ulcere t ten.

gFr! CTS M C11RONIC F. 'lat were..r.rt t e.ee s r e-sea to tissue comoge. 4 4 SECTION VI1 i SPILL AND LEAKAGE PROCEDURES (CONTROL PROCEDURES) i l AcTI:s t ri r ma tf RI AL r*sse ca SPtLL l 4 cauttew " t u Y 10w I

SL1ppgav aNo cannot!vt. eene NICSM/P5MA appeevee cust/ mist reaperator.

Fellow ** 6 regulat 'or resovretoe use fece 29 CFB '990.134). mese goggles. toweral)s one r,ecoroae Meyvtert -**ce gloves one coots. Aos non-coacttwo cry asserDent sucn es a l'woutrer.--esieve m otosse*- st earth et er sweep u0 an6 rysoce in an approveo 00T cersteiner ano ses). m iute scio sacn es ecet te t vinepor t one fiwen wetn water. se not veen .no...... m orem. .,o .e.or, or..,...e......n. i, con t....,., e.. e t s e,.e..es,o.e..,,, j e ve. - av. tam-- ceii tne e.orgency seisonone nummer enM,n en ene croot., ents sneet. I , TRANSP0r?TATION ' ~RGENCT. CONTACT CHENTREC 800-424-9300 I 4 . WA5TE DI"*'5AL NETit } l Dispose -r coritemiaa omouct. o.oty contatssere end meteetale uses in eteening up emella op a seems em 3 genmer ce" as f v ** e mater el Consult approortate seoeral. State one locat ..t ..e ...,procer ....o..t.ro _ e... J i I l I SECTION V!!I - SHIPPING DATA jD.0 T Caus t 'e t t ou ta Correstve Meterial tm ta24 1 SECTION II - REACTIVITY DATA M1 Afd AT C F MAZAmpWE i MAY ON STABLt _ POLY 3IE RIEATION

WILL NOT n :.-

r CONDifff9't TO AVDIO 93ne aon-n IteCCp8P Af f a tLITYIIIAfrf ' TO AYDIC) aetne..seny nitro-comeouries, entertnotes tverocaroons. perostoe-atumirssa HarAA00Ut CfCORIPOE!Y ' ' N8tODUCTS centset watn eerochvoretee aey resaase carbon monomtoe. Centset witn er*****

alA'.3, r e le ase a t -a t e evernema nas SECTION I - PHYSICAL DATA aet t r ING '.i TWT S S ' r t t.

t VArt3 rurgg=="

See pe low

!VULATELg5 w a SQ, LING (UINT 295 t ' 59U=ILITY 188 UATEm toIunie ICY.-v mTsuss mATsN

yi cIFIC s?.AVITT(N2(a en e, eor PM >

't a) s,."._3 a i:0 ci e VL - begmKTT I AER* t I an a. [ t.oe i SC ' r t INFORMATION: T"t"'! SHED TO m ano FURNISRED BY DATE "' ' ' ' * ' ' oes one.=.e e eaiet te,iene rese.e.e,r at* Ot PT t,AN#* 1 at&t L S AF E f t DATA SMttTS r re>V*tt DJFFE1N (18317ee test Et t 5 C1, RA CORPORATION '. t "a* ti Op 120 Long Meepe meest Stasneers. Connecticut 069C4 ~7 ? 9 2P... _ OCEADe* Waturerk ..e.ne.ee n.e t...,teto..t1

INT BY:LbALLE STATION 10-29-93 3:06PM COWONnEALDi EDISON-C0hoiOMEALTH EDISON: 22 i i dNs.stpky $bemicct{ Ynspecilon 00. P. o. sox 43. LEMONT. ILUNOIS 9043D4o43 * (7081257 6775 i togR g oael P. O. Box 1355 i Staarord CT. 069tli-1355 i REPORT OF LABORATORY ANALYSIS DATE: May 21, 1992 REGARDING: Ex-Berge OMCC 11 caustic Soda The Powell Duffryn Terminal in Lemont. IL. Barge Composite Shore Tank 219 Before Olscharge After Ofscherge NAZO 38.971 39.085 NA0H 50.231 50.385 NA 00 2 3 .03565 .03945 NACL 00205 .00165 Iron Content 0.73 PPM 0.78 PPM Arsenic Content <1 PPM Lead Content 2.12 PPM Hercury Content 0.016 PPM Heavy Metals <30 PPM 8 lbs/ Gal P 60 F: 12.7871 ) b a w V

l ~sT BY:LASAll.E STATION. w . 0-29-93 3:06P>i. C0WONME.413H SISON-C0!ciONWEALTH GiWd 3Z 11% A W ~ Maten. lSafe; DataSheet a y SGCtlOn i Product identification m _.m m T4ADE NAME i un-or a DOT $MIPPING NAME m.RODUCT TYPt P i e im mt., r....- t CDOt IDENT. Section 2 m-4an_. _ i . redients unaer 29CFR 1910.1200 0(33&(4)-Does not contata he frPoscarcarrtatA cAs NUMata 1 i i i 3 awes. a Section 3 Physicat Dato .s 1 l ?O UNG INT.760 m Me j fittitN IN T 3 pts F 3 YPfGtlCGAVITY IM20. h 37 F utt?tNG POINT _. a VAPOR PRE 15UAE u } _ VAPOR DINSfTY (At4 o 4 t i ei l . a VOLATILf5BYWOLUMF ado SatutttiTY IN M20 M ma um ] i APFtARANCE & ODOR eVAPORAflCN R ATE _ rao ac. Inr==1stm een mM ( close liquid with no specielo esoc ~ i c - 4. 7 ; Section 4 Fate & Explosion Huzard Doto flash PolNTi& mE TMoo u5f D1 t { + MA,uster-based produ.t FLAMMAntt LIMIT 51N AIR % 5Y VOLUMt l LOWER HA UP'fR . AUTO 'GNITION ihNGutiHINO wf D#A-NA TEMPERATUtf IFt CiAt f ett flGHTING PROCf DURES. NA 1 rnan efW DeYrurmem i Firefighters should weer full protective [ i clotaitig, i UNU5UAL Flat AND f EPtOS60N HAZARD: none known 1 i Section 5 Reactivity Dato ~ ~ _STAtitITYEORMAL CONOfflONS) ctmain 4NcCuPATitit:TY (MAff ttALS 10 CONDIT#CN810 MO!D wa+ AvolDl danmes,and_ Streng oxidizing agents I x AZARDOU$ DiCOMPO$iTION PEODUCT5 vict deteratted ,m AIA 20005 POLYMlatZAT60N ut11 u, n~w CONDITroNs TO WOiD we+ 2a 1e malm GRACE Dearborn t_-. OMalen W R. Grecs & Co.. Conn. 330 Gen ene. %mes. Lake Zunch, i 60047 (708) 438 1800 \\

. _. ~ qu By :Lu.A..L.L.E.ST.A.T. I.O..N..,..w: 10.w-29. wormmo' 07PX COWOMALT11 EDISON-Co.WOMEALTli EDl50N;*24 93 3 w SQ h Hezeralin{prmation _, s .s u 7 'OXIOTYINPORALATION: l~ see Seou s. 2 EFFICT3 0F OVEREXPOS URE: INHALATION: Inhalatica of vapors or sist say irritate sasal passages-INGESTION: Harmful if'suallowed SXIN OR EYE CONTACT: Prolonged or frequent skis cent.act may cause arratati 1 ca. 1 EMERGENCY AND FIRST AfD PROCEDURES !NHALATION: k Remove affected persons to fresa air asa treat sveptoms NGESTION: IP tagested assinsster eestic or crisk lar ater to neutralize and contact physician. ge amounts of allk or i SWIN CONTACT: unsh with soap and water. j 3 EYE CONTACT: Flush eyes utLh w4ter and seek medical attention. i j Section 7 special Protection information dENTILATCM EtOUtREMENTS f

1menanteal wantilattaa RESPIRAtoaf PROTECTION (SPECLPY TYPf)sha.la ha_a p aa=*ta Jens

===~imi t YE PROTECTION finmalm_a gr dans shield GLOVES d CTHEI PAOTECTIVE CLCTH.NG AND tGUlPME NT oi " asp or slantin 11 $TE r5 TO TAK E iP MATE Rt AL 15 RtLE ASED OR 5P: LLIO Wear protective clothing. spills should be soaked up on atSmall spills may De flushed to the drain. 5 for disposal. Flush area of spill uith water.1 sert absorbent and placed in a contalperLarge } AASTI Da5POSALMtTHOD Dispose of absorbed eaterial in accordasoe with applicatie F d local regulations. flag te DuPtos or landfilled, e eral, state ans i This product is met an EPA hazardous wasta. t J 1 I Section 9 Specsol Procautions PRECA'lTION5 TO BE TAKE N IN M AND(It4G AND STollAGE Protect from freeting. i Store crues closed when not in k use. \\ i OfME R PRECAUTIONS r r sneustrial use osiv. o 4 Keep out of reson of children. j pat Pant D av-5. Mores A. DATt; B/03/88 g, v 6, M** **s" *."U*.*I.*-."..'.' d ~E~/.S..Ur 7. Y.,.J.'" yy=y-.g.. a T.. w 7 7w"7 GRAG Dearborn r. i Desehern Divisten w il Grace & Co.. Com. 300 Genenes Seese tala ur c. a7 908) 438.7800

i DENT BY:LISALLE STATION l 00-29-93. 3:07PM COMEMEALTil EDIS0W C0hWOMIEALTH EDISON::25 \\ UE V&p-. i rao' uer.uurn o i 18314 Wd5:e anC OTOCESS i . mci. co. W6:Cr ': red3 ten': I AQUAFLOC' 408 i industrial and Municipal Waste Treatment i k AQUAFLOC' 408 is a liquid anionic fiossoient und esegulant aid.: AQUAFLOC 4e will inemses the efficiency of cierifiers. filters, thickeners, esperstars and softeners. AQUAFLO in the clarification of row water intended for potable use. AQUAFLOC 408 prom j faster settling floc which means a reduodon in floc carryover snel intressed filter runs i ADVANTAGES: 4 i Convenievt liouad form of a high moissaior weteht potymer lasreamus offisseney of troussent synesses I a Promotes faner settling fios ...j.... Sele-EPA soproval for use in posuble weenr Does not add solids to sludge ' hI, ( i . l. 3.- DOSAGE: .r PRIMARY COAGULANT: Use 25 to 300 ppm based upon affluent quattty requered. COAGULANT AID: Cossoas of 5 to 100 ppm are recommended. exosed 60 ppm. Cptimum doseges are best determined by ist tesu or use in th FEEDING: For best results. feed diluted solutions of the required amount of AQUAFLO t solutions of 1 part AQUAFLOC 408 to 5 or 10 paru of water should be prepared . Feed When used as a crtmary coagulant,408 should be fed to a thoroughly ag I setts or otner pnmery coagulant, whors floc formation has beg ent j ,. st { l Pump feed solution continuously or proportionally to flour with a positive disp i 5 PMODUCT DATA: Color: Coleriens; oteer ) Forut: Liquisi Frees 6ng point: 32* P (0*C) pH: 4 Densey: 8.5 bis /ss6lon (1.01 ko/L1 HANDLING: SIIghtly acid. eyes, immediately flush with uter anc get medleet ettention. Avoid contact with sk Keep container classo when not in use. PACKAGING: 55 Galton drums - Approximately 460 lbs. not 1208.68 kg) 30 Gallon crums - Approximswiy 250 lbs. riet U 13.4 kol 5 Gallon pans - Approximately 42 lbs. not (18.65 kg) i i

m. w i.

en.m e ,,=-.ussa aa em um.. a g wy we====s assens==am enumm. e. ?OP4 310 GENESEE sinEET. (Aers rJascMsu.ueo's soodF. sta/ w - - ~ ~ ~ ~~'~~ " * ~ ~

SI tr.LuAtif MATioN

10-23-93 3:D FM COWOMEALTH EDISOF COWohWEALTH EI)lSON;@6 i

"HOMPSON-HAYWARD CHEMICAL COMPANY KANSAS CITY, KANSAS MlTERIAL .. _ _ _ _ __ _ _ _ _ _ _.. _ __ _ _ _ _ _'__ -_ _ - _ _ - S AFhTT'" DATA _ -S KEET $ h CO __: W_____________________^ i CAS e 007722-84-1 FORMULA: H(2)O(2) CHEMICAL FAMILT: :norganic Peroxide CHEMICAL NAME AND SYNONTMS: Peroxide 104, Hydrogen Dioxide SUPPLIERS NAME: Th pson-Maywa d Chemical Company 52 5 ter R i K nsa Ks 66106 SUPPLI EM } TRANSPROTAgHONE NUMEE 1 1-3131 . ION EMERGENCY PHONE NUMBER: 1-800-424-9300 4 SECTICH I Hasardous In _________________gre___dients 133E'9I'"3 $'EC'31 Ib3 HYDROGEN PEROZIDE 10% P TWA 8 HR 1 OSHA + 7 NA 8 MR 1 A H

TION II He i

--_____..____alth__ Hazards._______________________..._.---___ i Threshold Limit value: As indicated in section I. { Potential Effects of Exposure: Eyes:. Ma y terstant.cause eye burns, effects may be delayed, an extreme l Skin: Short term ex sure causen skin irritatio exposure causes tr E. tation, blasters or burns.n, longer ) Inhalation: nose and throat. Inhalation of vapor or mist may cause irritation of i

ngestions en whic:# swallowed it ma au a sudden volution of ox

. an a se in r y atention o se ch, an oca neern 1 6d ng may resu t.the esophagus or First aid: Ey Immedia flush e es i e of v r at least tes in an w per a t med at ntion.g ta t enses a not be war. h worxing vit this chealca. w a Skin Thorouchl fivsh skin v th water, rem e and wash physzczan.edc!ot contaminat ing cramp AI b41cv.t y and thoroug y. 411 a Note Inb lation: Remove utient to fresh air. If irritation of throat or nose is hpparent ref er person to a physician. Incestion: DO NOT induce vomitino. Give wate dontents. If vomsting occurs skntaneously,r to dilute stomach maintain head CONTINUED ON PAGE 02 J

j }. INT BY:LASAl.lE STATION 10-23-93. '3:06FN : COWONIEALTH EDISOW ColWOMEAl.T ""' "dHII^RTf"'Lctis "^"' c l ~ XATERIAZ. SAFETY DATA 5HEET i l giij5 55i[~56iiihiiEiH~IBi ETEF~~~~~E~riT~BUiUiilHTE~ I S'c " " L er"itlsh ni'Kf's to k c o n see Note to Physic an, ( , be ow.a.1. tion. C.ff T U ici.n. t in f Cther Informations i ) j l h( drogen peroxide and should notProtective skin creams do no offer protection from I l p otective measures given in Sect on III.-a worn also see other 1 (B) Notes.to Ph concentracionps ksiciant g,stronoox5ka!enb$ rec H r roxide at this contact sith the eve 1ssuffiegent., {foesus gernesg g gscially it i e0a15$!I$n! imitmrp$**rms:mn u =or;:me ene ommen$ -loca$# e ssg n rue i 2:*:a "it'tpttermg. u!anetiWaf*!Mi".*5t:Entfs!* m=e nor e m:e - i-i i togas [armat;3n.tmd"m'tK4! a I j I g chronic exIocureg teI rted i ob inogenic to agu ner.E5"It:0 I Pa?:r*P titt.g*TII cgegdf miP2 fill!g"': mf .e. .is t.1.it.d a.aterfsl."'lvidencetsn.tu:J*'"a2nese;nce it 'h.:=' !!!e9a sn.**Alfe " hat a2os. igd, in'ti t b

h

'N'5 '$5Ag%'" 1"g 4 or ta f ove Li

rense togeg,o1sinA ta=R.t)h :"B to a.s j.J i

cone.nuat soI 56se 'l f W 8ue t: ese acut, 5.H.5 nI!*Il n g i v fog,tt. Ie..ve to.di?*:".IsT 5"1!t n B2* lose :_.?iliW!! h oPl i 1ons s en.o 1cy. lince t in !$r a!cikN is se oral exposu! i$$$ Secogn!$2isun$!51vl.f$ $[DN$$' !"c[$,sg[eetgd khek$ "k re to 4 H sanor6vekas! 4 (Generally 8tftP?R'IBpidues.ased as sat ) I6r with.no r6 pter141 is not Yse as a'hhBan food ad ive ' B W 9irt ilt F1 38!!c'2.*** g ag" "a2 " *' 5Y i ist ~ l l Sacne"_111_ _5 Pre!!L EEa t tshee_!e 8 aE=es!ee__ _ __ t ""Si'*if61n!!jj!"?!8"4 'tjeP f!"ijtil*"iioPo! salAmitn* autb:; 5*" PE"t.gff* $o n!Ri" xI$1A*lthsable sor$ent. i otuseanos$ ~ ventilation Required;de conc 6ntratsons below exposure limitsGood oene to asep peroxi Protective Clothings j Eyest Cu pe chemical goggies and/or full face mask are i recosaa j Skin l When a possibility of contact exists, wea'r a hard hat with CONTINUED ON PAGE 03 4 4 i m..

, pEM BY:LuAllE 5TATlo\\ 10-23-93 3:ObPM : COWONIEALE EDISON-COWOMEALE EDISON:: THOMPSON-HAYWARD CHEMICM. COMPANY KANSAS CI M, KANSAS ) 1 _ __ __ __ __ _ __ ____ _ ___ _ _ _ _ _ _MATF.RI AL S AFETT DA_T_A SH_E_ET i PR O SECTION I!! bria, Iu.hal Protecticn In ormattu CONTINU4D Sp . length taca shi Id neoprene, butyl _or viny rubber watgsgoc een acrylic or po yes:ter outer clotning, chem:, cal ault boo e Additiona; Protective Me gures Where ez M eu mesible wea aS.EesteroracryIcoYter i E1 material.on oth ng o coa mov cause rein n$ ott.er prous shoes.e less su!armeSustib ts. kration or e f these synthetics ar sceptible. votR cracKe, su.. e e or v-S!cI29N {y,,,(({3,3,Esg}osion Hagagd ggta t Flash Point (Method): Will not burn Flammable Limits (% Volume in Air): t appe[c:b in a confinek,swee wi$$ position will releas$1m1Eken,d Will not hur but dec wh .cz f burning rate of fla m mle vapors. crease explosive in an Lower UNK Extinguishing Media: Flush away with water. SpecialF1eFightinginers Procedures F ood with water u sh gogo es and ictA sn eme{r aneles it hvorogen prox 2We cool

a s or cont in ang-incluinIn-in Mdrokaofsandski. rs and mistk are extremely j

inc en roxide v4 e arritafIng ot Unusual. Fire and En lo ion Hazards: x!re.r,oncecompositionreleasesoxygenwhichPeroxide is non-combu is a.strone tro may intensif r i S_ E_ CT_ _I O_N_ _V _ _ __ _ _P h y s i c__a _l Da ta_ _ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ Boiling Points 226 dag. F Specific Gravity (H(2)C=1): 1.133 i vapor Pressure (MM HG. ): 23 0 30 deg. C i Vapor Density (AIR =1): UNK Evaporation Rate (autyl Acetate =1): >l Solubility in Waters Complete Percent Volatile by Volumes 1004 i pH Apparent 2.0-3.0, 14 solution 5-6 i Appearance end odors colorless liquid, slightly pungent odor. i CONTINCED ON PAGE 04 i

- S T BY:LtiAl.if STATION

10-29-93: 0:09PM : COWONnEALTH EDISOF COMOMIEALTH EDISON:r29 4

t THOMPSONg g g gCCBIPANT 1 l MATERI ---_--------------------------- AL SAFETY DATA SHEET l 1 U PEROZIDE 10% BLK DLT-------------------------------- PRODUCf NAME: m o l PRODUCT CODE: 26-14-01 DATE: 03/09/88 PAGE 04 s5grigN y1___agge31313r_ggsa_______________________________________,,,,__,,,___ Stabilit[y: kfna such as the [$compata$Ies Skve he$elow. contaminates of l nstable when ex sed to, ces t or a ated Incompatibility: With c anides, hexavalent chromium connounds, nitric' - l cid, potassium rmano note, reduczng noents, l oys.nd other 2 5n a gavy metals, go vantze tron ,6mra r other, combustib.s articu arly v.co tre organics c

rust, iny unoa9ttJ wo ith pH s above 4. paper or.

.bs, and mattrial Hazardous Decomposition Products: None. HazardousPol[merization: Will not occur boyever.. mroxide will cataly e polymerization ancompatibality as indicated above. SECTICN VII Spill and Leak Procedures Steps to be taken if material is released or. spilled: Dilute vi h a lar e volume of.de decTseswater and hold in a and o area unti

he elow.hy bo en N [oytgon oxi Disobse of as outlined M

scape to sewers br natural watercourses be ore ecompos i Waste Disposal Method: After.d comDosition, consult with local officta s sultahl 6reatment system.to their approval disch,rge-into aand. federal hnd subject stata zN hasarcuavas! tea!". [n kCk N N1blN Na g" sw te No 9$IkghE$yfb![ckS*Ea!hea$MSnnbvYSI#ER$bT50): '22-35 mg/1) i SECTION VIII D.O.T. Shi

pp ing I n f o rma t i on Proper Shipping Names E,ROg g LUTION Hazard Class:

OKIDI2ER ID Number: j UN2 Ole Label Requirements: 01IDIZER Reportable Quantity: NONE Other Information: CONTINUED ON PAGE 05

. test.BY:LMALLE STATION 10-29-93 3:09PM COWONEF_tLDi EDISON-COWONTEALTH EDISON::30 1

*" Ei!*II^CErY M u% s **'*"'

C s MA _____________________________TERIAL SAFETY DA_TA SHEET __________________ gg g ggg_gROZIDE :.0% BLK DLT DATE: 03/09/88 PAGE 05 sECricN g___Aad!31gn 1_infggma31gn This information may be of importance to you: No smoking where material is used or stored. Minimize skin contact.. Wash-drinting, smoting or using to%th-soso -ands weter-before eating, ~1..e t fac111 ties. Safety show available. er, eye bath and washing facilities should be S'ItRAGE C*NDITIONS: Store ao roved Eulk storace f acil:r,n roperly vented container r in Q. Keg,contagetout af ties. Do not block vent in un sun and away from. heat, spar s,gand .. so. not e any et 'ter eroduct to con aner. 9 pot store withreducinoa!ents com.sustible or flamma heavy metal Sal s. liave vatar source. avail Nevet return Mused peroxide to container - [ut.or 4,auhn. teri or of water and qlscar, a w1 p water before tiscar ing. Rinse empty drums thorouch v with c.e tv l sh Protect drums from vedt &c. Never use pressure to empty drums, container is not a pressure vesse gontaigers of.this material ma be hazardous when emptf.ed anotv contain pret:ahtions out!is retaan prod et residues. Observe a..1 hazard 1ned in this s set. Utensilgusedfor ggg a :natoria{.gngg gdrogen goride shguld be of g ss, sta oss stee, al num or Consumer Use Distribution industrial sir, sales or use of drocen roxide 104 (de)o her ngth concente s 62 h or roce neroxi or consumer use,l s NOT recomene due t the kards savo ed. Also ou shou be aware that recen nerosi e ma to re ulation v the U.S Dent. I Trankoortation,y su , !%s act Cons er Produ t Saf ety doamission, and the FDA. E REFERENCES I (1) NIO gc/OSEA Pockeg5 g e to Chemical Hazards DHEW (NIOSH) G Pub ation No. { NPCAMMIS 301 I

r \\t at LuALLt siAito.\\ .ie-;u-e3. 3:10P.M. COEWOMEALTH EDISON. COWOMEALTH ED150N;;:31 a.- r- " "' x"3II^!M""dStM"*%yyf ~~1...,-- 4 ........................M. ATERI AL SAF. E. TT D. AT. A..S H.EET.......... ~~ gogg g g g g_ gROXIDE 10% BLK DLY DATE: 03/09/88 PAGE 06 END 0F REPQRT

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<=2LSSTHAN N/A = NOT APPLICAB SE:s8Tiirlisii$'D UNK

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^" been obtaIned f rom sotarces bel;,eveThe information orevided L,n t is Materia; bleSa to be rel;a The o -Hapard Chemical Co. croy es no warrantie.s either sa oseed 1 ed and assumes no resp 6nst 41tv for the accu,rac or of ta Conta10ed hete&n. This inf6rm tion offer for ur or co lateness mation, consideration ana investlostion. Tou 5 d sat fy yo tselknlor-vou nave all cu rent data relevenf to you part er use that Trompson-Havvar Chemical com v knewt o ho a al condition, other taan those hote.on this mate i safety ata a wet, recognized as oeing aggravate y exposGro to t 11s product.which are generally F 'l J I l

dM BY:LDALLE MAilm

10-2343 a:)uPM : COWOMEALTH EDISOV-C060f0WcALTH EDISO.N:332

'0-13-92 32:23?I FICM T pg Sr G83 9y7 SynTech Products Corporados - 320E.woedrudtAvenue CLASS Toises,onto 43624 2 (419)241-1215 24 Hour-CallINF0 TRAC 1400 535 5053 MatrialSadeqrDeas Shoes SecdonI-ProductIdendSendon preensin Tandrat4maa - cm w r ar manne seem 8/92 renamn.: Propriesary Minnan Seedon II-Material or Contponent CheadcalName CA38 WT% PEL TLVesmo STIL CARCEO

3ammy temet 111 76 2 1% e 50 30Ghisemaug No soeumMausmans 6834424 1% +

No Osernphmmet7 9m.nglse 9002 93.L 1% + No TdsmehnFesgesm 7601-54 9 1% 4 No i Secdon IR-PhysicalData nomsgReses(a )et N.D. F ve ,y, w mc e. as vapormanury: N.D. s.t.taar as waneraf e-spasmonwanspoavs' rec sm C*"7'" 1.o3 w,voimmeervehmeen dans ss Flaaseemset Name e IS0*FTag Opus Cup Appaummes ofSpran Wkteiban,padhasoder i Seedon IV - Fire and Explosion Hazard Data i n enarasercracrimmes=.m 7mm ammeshie nummelaLimes: WA UIL: WA mem rosa,my enemies sem esside, s,.ms nm e==ama. x pasmeness ,L areweians'=gdsed 8 g8penament sedna tupamas,ervendas Unmustna umanipless.sm.auer As elevased unspermanus (above 120"F) eenadaan may vem, rupera, or Secdon V-Rm;Miy Data Cimmsalassabr: Stable ca.easea Anett Do not expees a tempetansec above 130'F. Y N amr auben m Mammeams pelrumhsess Wil1NOTossar

~ ,{. 2ENT St:LbALLE STAil0N . M-29-93 a:11PN COWOYiEALTH EDl50% C0hol0 STEALTH EDISON:233 }

r-B-92 :::3 ?M ?i G rH

!.e l Secdon VI-Health Ravard Data i osas p. a=* Lgesaa unic N.D. wilmavaks (See Soodon n) Eska eroveruapesure Eyes: Minorirritanoa sWs: No evidesca of advares efhet kom swallable lakuutades Iasamos Can cause passnian===a=1 irritanos, voandag Pnxtuct ensu as fossa. Imbalesien of the ibus, and diarshan. j seuld amuss asphpondon. 'shamanne l l Emergesty and First Aid Frstedares Eree Flush with waar fbr at least 15 nuouses 5kan Wash er.pased eres wre water and soap, tagesnee Do notladuce vomida6. Getmedical assessan. Trentthrasphymanan. t-j Section VII - Spiti or Leak Procedures seps = a miss ia -a m a. =a w m.m d. r Clean eres Oy maneing or with ab serbest nameriale god placa la closed commisars tr cl . Canadt fWerst, nase, or local disposal audsanmas fiiiFapproved mapeant precedures. j wasm o med properly sament products do not generuss hasardous wuses. Empty %suriand canalaars not be taused and abauld be wrapped as put in trash colleoman. Cass which are pruss coctsin h, quid mum be en of a a permitted wasse management 1 Consult man, and local disposal autherties ihr procedures. I i Seedon VIII - Special Protection Information SpeciSc Pmeani Processive Iqalpensat i % p.m Under normai sendida.a r=,ussary prosesdan te quired. venssass: Normal vomitission a mam pse ai.ws: Naas mieired, be wom. Ma mar bewas. l are trs=====: Naas ratand, cal ) - Section IX -SpecialPrecautions i j Fiesmadsas e he ehemia humains and smang* bove 120*F. De met esore stiespersanos a i SamantWsusuuss: Plenas red ana follow the direetiens on the proshact label. They are you bem misdas i this productin the som ofBecive way, sad give the necessary safsy a presset i yourhentet. ne anewInsmanansa pennens a ens p rod.e: as eurvemar nrummhand,and h bm.d es she i=a==amme areasMs a th thas, 1 e Adedes of retsaus eremar adettes as als predser may sekssandsay abermessayesteen. We mais as warvaudes,empres .,tapass,and .s u.amir si n.s,esa y .t she isenemas, i e Prop red by J. Esse i nasag. Tmah 1r1% Bulle ) i ~..

j 2EM Bi;LuAL1_E STATION

10-29-93 0:11P.M. COWONAEALili EDISON-COWOMEAl.Til EDIS0N;*34 i

'3 ~:C-52 2 C.3 R.E ?<,'] n..,, ,,a w. e -,~m-FAX N -nF-S 4 an l 7 7ese Ys enx'e E E """ b2 A.A4sem-1 4 "b.urdd " ann== 81T 2n.m, 316441 6 - _ ",,7 Wr. David Moore 1 M = w.- SPQA Coorthastor j syntech Prodness corporuton 520 E. Woodruff Avenue l Telsda. Ohio 4362+ i I l {

Subject:

r%===1 Analysis of One Sample el Touch It.Up., Latsserapia. Estait a 10201, toesteed on synnch patchaus order No. 9964 l Ta wt -e - we cie* -s \\ i } The resuha of the chemical saalysts ese as fellows: 1 Eammat landta Eament Imanha Arsenic <1 5tiver <1 calemm <1 Cadaluun <1 i i i cabak <1 Chrenhan <1 Copper <1 fren < 10ppea Mareury < 1oppen uma < 10ppaa i Mangement <10ppset c 10ppra j land < 10 ppm Scientuna < 10ppem Tin < 10ppun Zlas <10ppus ) i Cblerida < 100 ppa Fluoride < 100ppus } Sulfur < 100ppen 1 l

TOC 18.500ppaa
pK: 12.1 4

j

seahes i hsed in sceerdsome wkh sandard 1^ -- _7 methods All werk was pariennad in ancordanes with the Tenkatcal and Engineering Sesvlees Quaik menmes N.m..QA Develar No. 2001.

7 1 Wrtuna krr M'M

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i i ~ENT BY:LtSALLE STATION 10-29-93 3:11Bf. C0WOVEALTH EDIS0W COWOMF.ALTH EDISON;45 sr e st Bu'A Maten. lSafetyDataSheet a 70s-43s-isoo nira8TEK 2425 Wa $_ N a 4 rsa * --.i TN DOT SHIPhNG NAmt -id) 7 1 CA5 NuM6ta t.xPCsuet CA:tras4 Hydroentario acid 7447-01-0 C5 TWA: 5 ppa (seiling) l i v I 1 3 ,su t $ .%6 e ,, i N dbudhai BO(LINO PotNT. 760 -m Ho S A FE2f NG eotNT } 212 F MELTING POINT } NA } $PtOf tC GAAvtTY fM20 0 42 F 4Apon pastaute i I VAPOR cf N117Y (Art. H 1_ 21 $fW 8 *F_TY IN Ms0 go deareciable-- l % VOLATILf 5 BY WLumE te f VA PORAFION R. ATE _ fim Ac e 41 ( 1 APPtAAANCE & 0004 MD a## 1 1_ U - L 3 ? yellow-ttown liquid Section4 Fire & Explosion Hozord Data h FLASH POINT (& Mt THOD USEDI f LAMMA4LE UMIT5 IN AIR % SY VCXUMt j MA, ua ter-based product

OWER UPPER AUlO IGNITION k

NA NA TEMPERATURE f yTINGUISHING MED(A: M4 SPECI AL FlRE HGHTING PROCE DU AES: FDAM f'ft2 DRY C)EFMIC.AL i Firefiehtets should usar Full protective gese isoluding self containes l breathing apparatus. I k j UNU5UAL fitt AND EXPLOilON HAIAAD: i j Hydroges ontoride an'd chlorine gas say ge liberated 1 Section 5 Reactivity Dato i stAltuTY INORMAL CONDmONS) CONDmON, E TO AmtD e**mt. ret -- haat INComMTIDruTY(MAff atALs TO AvotD) Avents direct costaat with strong alkali. s H A2 ARDOU$ DE COMPOSITION PROCUCTS HC1, C12, CD CO2. exides of nLtregen 1 i. HA2ARDOUS POLYM E RIZATION j uilt met -- - CONDITIONS TO Aml0 amt --ifa**1m GRACE Dearborn Deewtperve BMalen W. R. Grecs & Co.. Corm. 300 Genesee $Nas*, Lake Zunch, IL 6004 3 .._.....~,.e_r..

2r_u cI : Lu..Au._.t ~s i.A.~il.o%.e ~~.10.m-;'.3-33 1;i41. Om0.VEALTH EDISON-CWWEALTH ED150M2 .3 : ~. .cormrwea T i Sectio + azard intermatiec ~. .~2 'CIICITY INPolWAAllON: Not establishee, see section 2 for component inforeation. EFFECTS Of Ov!REXPC5URE: IMHALATIWf: Inhalatics of vapors or sist say arritate nasal passages and lungs INGESTION: Prodwet util irritate or iaJure gastreistostinal tract. SKIN C3HTACT: Prolonged or frequet.t skin centact say cause irritation or burns. k EMt AGENCY AND FIRST AfD PROCEDURES IMHALATION: Recove affected person to fresh air and treat sweptees. 1 IM3ESTIDH: If conscious, give water to dalute ano contact phystolan immediately. Do not :stuoe voetting. SKIN CONTACT: Wash with scap 1 w uash before reuse.ater. Reeeve contestnated clothing and ETE CONTACT: Flush uith water for 15 atnutes ano seek mestcal attention. Section 7 ML MML vf NTILATION REQUta EMENT5 'Jse ameauate mechanical ventilation. Et$riRATORY PPOTtCTION (5PECIFY TV PE) Mais nascial EYE PetOTECTLON Gomales or face shield T-Glovt3 rrvious .MER PROTECTlYE CLCTHING AND EQU;PMENT SoCil 'e5 STEP 5 TO TAKE JF MATERIAL 15 RELEA520 CR 5PILLE D i Wear protective clothing. Collect using absortente place la container for proper disposal. Flush area of saill unth sator. 3 j

Adit DISPOSAL Mt IMOD Dispese cf is accordamee with federal state and local regulattens.

Contains ( 52 of hydrochloric acid. CAS NO. 7447-01 0 requzre reporting under section 313 of SARA Title III and 40 CFR.Uhtoh say Section 9 5pecsol Precoutions PR f CAUTION 5 TO && TAKEN IN MANDUNG AND STORAGE .+ Open with care. Keep container closed when not in use. Store containers closed away from entreme toeperatures. OTNtR PIECAuTIONS FOR INDUSTRIAL USE 04.Y. KEEP OUT OF REACH OF CHILDREM. PREPARf D B Y: FNM i J".c: DATE: 5/@/Y1 = s. t;::.r---':':::WJ.*2:.'"'~'.. .~.3-de' :t:.

.ac.~.2.: .0.1.;;!. :::!:::: r. ~

3 .y,,.,,.,. = -.~. ~ -.. _ GRAG Dearborn amerhawn IBMelon W R. G.cee & Co. - Core. 300 Genesee $trem. Lahn Zurich. 160047 (708) a381800 ~ ^ ' ' ~ ~

u n m.us.u.c sa n e au-23-ee ms.v. ceu.m sisow ceux.m sisow hi~ /c721/A. TERIAL SAFETY DATA SHEET ONLY - Phone 504-344-7147 NY Y; ,,fy g,, .no sawy trenas** *"" " "" 98.0.6 m.----.--_---- PRODUCT IDENTITICATION

RADE NAME:

50 DICE BROKIDE 38 i Sodium Bromida, Water Soaution~ CHEMICAL NAME: Not applicable-sixture CAS No.: CNENICAL TCRMUIA: NaBr/H2O CHEMICAL FAMILY: Metal Bromide THIS MATERIAL IS IN COMPLIANCE WITH THE T0XIC SUSETANCES CONTROL ACT (15 Usc 2601 - 2629).

==.._

SUMMARY

OF HAZARDS I Eye irritant. HAZARDOUS COMPONENTS CHINICAL NAME CAS NO. NOTE + EXPOSURE LIMIT sodium Bromide 7647-15-4 NL Not astablished by OSHA /ACGIM. d + NOTE: Carcinogenicity listing of components at concentrations greater than or. equal to 0.1% indicated by t=WTPt #=IARC: &=0SHAf *=0TNER NL=Not Listed u-i CHEKICAL AND PKYSICAL PROPERTIES APPEARANCE /0 DOR: Clear liquid /little or no odor. SOILING POINT: 110-112C/212-234F. 08/02/89 Ethyl Corporation - Chemicals Group F.styt Tower est mortes shnL, Beton Rouen, LA 79001 -- ---..uss cowenanom ean szoont suas

i, ) sc.Ni of :LuAuf. slATio.N

1u-;: S-93 d:13PX. COMMO. WEALTH EDISoh-COMh0MEALTH EDISON:*

}I i Page 2 of 5 EMERGENCY PMONE NUMBER "RADE NAME: 800238 BRONIDE 38 (504) 344-1147 i { es o.s CHEMICAL AND PHYSICAL PROPERTIES (Con't) i i VAPOR PRESSURE: 17.5 mm Ng 8 20C/6EF for aqueous portion of solution. SOLUBILITY IN WATER: Miscible. i SPECITIC GRAVITY: 1.47.G 21C/70F.- PERCENT VOIATILE 62% water (by weight). TIRE AND EXPIASION MAEARDS FLASH POINT (METHOD): Non-flammable. i FIAMMABLE LIMITS: Het applicable. EXTINGUISMING MEDIA: None required. KAIARDOUS THERNAL DECOMPOSITION PRODUCTS Includes bromine. SPECIAL TIRE FIGHTING PROCEDURE 5s Avoid breathing tunes. UNUSUAL FIRE AND EXPIASION MAIARDE: None known. I REACTIVITY DATA STABILITY:. Stable. CONDITIONS TO AVOID: Extrasely high heat. MATERIALE TO AVOID: Strong acids and strong oxid1Eing I agents corrosive to aluminum. l HAZARDOUS POLYMERIZATION: Will not occur. a ..ni gggg 08/02/89

3r\\1 cs :tasALLE si.4Tlus 10-23-33 3:1SPM. COWOMEALTri G150b Conol0MEALTH GISON: 33 i \\ \\ Paga 3 of 5 ENERGENCY FNONE NUMBER TRADE NAME: SODIUM BROKIDE 38 (504) 344-7147 98.0.6 REALTM MAEARDS INKA1ATION: Not expected to be a primary route of exposure. EYE CONTACT: Expected to be an eye irritant. SKIN CONTACT: Repeated or prolonged skin contact may cause irritation and superficial burns. INGESTION: Not expected to be a primary route of

exposure, i

CNRONIC EFFECTS OF OVEREXPOSURE: None known. j ENERGENCY FIRST AID PROCEDURES EYE CONTACT: Immediately flush eyes with plenty of water for at least 15 minutes. Get medical attention. l SKIN CONTACT Wash contaminated at eas with ' soap and water. INGESTION: Give two glasses of water. Do not induce vaniting. est medical attention. EXPOSURE CONTROL INPORMATION EXPOSURE LIMITS: Not established by CSMA/ACGIM. EYE PROTECTIDW Chenical goggles. PROTECTIVE G14YES: Resistant to chemical penetration. RESPIRATORY PROTECTION: None under normal conditions, UX:AI. EXEAUST VErrIIATION: Not required. NECNAMICAL VENTIIATION: Recommended. 08/02/89 1

) l 2ENT BY:LuAl.LE ST.4 Tion

10-28-33 3:13PM : COWONWEALT!i EDISO.N-COBONRALT11 EDISON: 4 i

I 1 Page 4 of 5 DG3tGENCY PHONE NUMBER TRADE NAME: SODILDt 3R00(108 38 (504) 344-7147 98.0.4 b l EXPOSURE CONTROL INFORMATION (Con't) i 2 OTNER: If repeated or prolonged skin contact or contamination of clothing is likely, protective clothing should be worn.- ENVIRONMENTAL PROTECTIolt 1 SPILLS OR LEAKS: contain any spilla with dikes or l abserDents to prevent migration and entry into eewers or straeas. Take up small spills.with dry chemical absorbent. Large spills any be taken up with pump or vacuum and finished off with dry chemical absorment. May require excavation of contaminated soil. DISPOSAL METHODS: Under the CERCIA/ RCRA regulations currently in effect, this product is not regulated as e hasardous waste or a material. Therefore, it may.be disposed of as an industrial waste in a manner acceptante to good waste management practica and in compliance with applicable local, stata and j federal reptiations. If used as a-j postioide, contest your Regional i office of EPA for guidanem in disposal of this produet. ] STORAGE REQUIREMENTS: Store in dry, well-ventilated area. i 08/02/so l i .r, wv

r-ci:LbAui sf.4rius 10-23-33. a:13FM. LOWOMFJLLTH EDISOW COWWOMEALili EDISON;;41 1 1 i I l Page 5 of 5 IMERGENCY PitONE NUN 3ER TRADE NAME: SCDIUM RROMIDE 34 (504) 344-7147 l 98.0.6 I j issue DATE: os/02/st supersedes: 10/os/a7 l MSDS prepared by: Health & Ep ironment Department a Ethyl corporation FOR ADDITIONAL NONEMEllCENCY MSDS INFORMATION, CONTACT: 1 MEALTN AND ENVIRONIEllT DEPARTMENT ETNYL CORPORATION i 481 FLORIDA ST. BAT 00f ROUGE, LA. 70d01 (504) 388-7717 TNIS MATERIAL SAFETY DATA SMEET 00ertAING AT LEAST THE INFORMATION REQUIRED BY THE FEDERAL OSNA RAEARD COMMUNICATICII RU12, 29 CFR 1910.1200(g) (2). j l W l i I I

i 2ENT BY:LuAllE 3DTl0%

10-28-93 3:14Py.. C0kNONWEALTH EDISON-C0!cKMEG ED150N;*42

{ l 57 goo 7G: i' PAGE 1 of 5 A.STEELCHEMICALS INC. i WARENESS for .M OA AFETY ] l { MATERIAL SAFETY DATA SHEET SEC 1 PRODUCT IDENTIFICATION 4 t PRODUCT NAME: i SODIUM HYPOCHLCRITE SOLUT!ON ) EFFE CIVZ DATE: j March 1, 1990 CAS NUMBER: } 7681-52-9 I 1 CHEMICAL FORMULA: l Na0CL (SOLUTION) i l HAZARDOUS INGREDIENTS: SODIUM HYPOCHLCRITE i 13.07 - 14.51 % i i EMERGENCY RESPONSE FACILITY COORDINATORS: r r menWT. T r navy. TM RRugrrr.are.wy (708) 257-3909 (219) 882-5778 (518) 432-4173 EMERGENCY TELEPHONE NUMBERS Schiller Park Office 1-708-671-5070 24 Hour Security 1-708-257-3918 LOUTHGATE C'HAAE OFFCC PLAI.A SUITE 250 4333 TfuM56LD ACAD+ SCHILLCA PAAK.I11:NOl5601M a 700 671-5070 x. G

i 3DT BY:LuaLLE STATION

10-28-SS. 3:14PM : COWOWEALTH EDISON-COBOWEALIN EDISON HYP000. QTS t

PAGE 2 of 5 03/01/90 l SEC 2 PHYSICAL DATA l t APPEARANCE:' CLEAR to YELLOW LIGUID ODOR: PUNGENT. IRRITATING. " MAT OF HOUSEHOLD BLEA i SotD5ILITY: 00teLETE BOILING POINT: i DICOMPOSES PRIOR TO BOILING SPECIFIC GRAVITY: 1.205 4 13.07X t.230 e 14.51X VAPOR PRESSURE: i APPROX. THAT OF AIR IVAPORATION RATE: NOT APPLICABLE i SEC 3 FIRE AND EXPIDSION INPORMATION V FIRE: NOT CONSIDERED TO BE A FIRE MAZARD. i EXPLOSION: NOT CONSIEDIRED AN EXPIOSION HAEAID. FIRE EXTINGUISMING MEDIA: USE ANY M M SUITABLE FOR EXIINGUISHIN i SPECIAL INPOBdATION: \\ WEAR PULLY ENCAPSULATED SUITS WITH SELF-ERRA2NING APPARATUS (POSITIVE PRESENtI) .i h 1 l

i 5ENT BY:LLSAllE STATION

10-23-93. 2:14PM : C0WONE.A1.TH EDISON-COWOMIEA!.TH EDIS i

HrPoeo. QTS l PAGE 3 of S' 03/01/90 SEC 4 REACTIVITY DATA: ~l I STABILITY: I UNSTABLE AT ELEVATED TEMPERATURESSTAB i } HAZARDOUS DECOMPOSITION PRODUCTS: l OXYGEN WHICH CAN BE 00EIC AND j i i i HAZARDOUS POLYMERIZATION: THIS SUBSTANCE DOES.NOT. POLYMERIZE. t i INCOMPATIBILITIES (MATERIALS TO AVOID): OXALATE. ACIDS AND NOST ORGANICS. REACTS VIGO } j 1 i 2 i LEAR / SPILL DISPOSAL IN50ENATION I SEC S i Rar.raans/ SPILLS: a { MOVE L3tPROTECTED PERSONNEL UPWIND OUT OF D4! j REPORTABLE QUANTITY (RQ) { (CNA/ CERCLA): 100 LBS. 454 Es DISPOSAL: 1 i l DILUTE WITH WATER AND FLUSH TO LOCAL i SEWER SYSTEM. IF ,t PERMITTED. SOLID WASTE MUST BE DISPOSED OF IN A PEttfITTED I i WASTE MANANGIMENT FACILITY. STATE AND FEDERAL REQULATIONS. ENSURE ' COMPLIANCE WITH I i SEC 6 MEALTH HAZARD INPOktATION i A. EXPOSURE /MIALTH IFFECTS i 1 INHALATION: RESPIRATORY TRACT IRRITANT. INGESTION: CAN CADE CORROSION OF THE WCOUS MiameAm. SEIN CONTACT: ~ TISSUE DESTEUCTION. IMMEDIATED i l i EYE CONTACT:' WASH EYES POR AT LEAST TWENTT i MINUTES CONTINUES AFTER FLUSHING, SIEE MEDICAL ATTENTIONIF IRRITA 1 j i

ENT BY: USA 1.LE STATION

10-23-93 3:15PM : COWONWEALTH EDISON-COW 0hTEALTH EDlWM i

HYP090. QTS PAGE 4 of 5 1 CHRONIC EXPOSUEE: 03/01/90 i NO DATk FOUND "VXICITY DATA: i M(7IAGENITY DATA:(RTECS 1983-4 SUPPLEMENT TO 81-82; NH i cyt-han:1yn 100 pps/24M ihuman) cyt-ham:ing 100 mg/L (hamster) i CHEMICAL LISTED AS CARCINOGEN OR POTENTIAL } NTP -No ; IARC -No ; OSHA -NO ; ACGIH -N0 i B. EMERGINCY/FIRST AID l INGESTION : DO NOT INDUCI VOMITING! GIVE ANYTHING BY MotJrH TO AN UNCONSCIOUS PitanngG 3 IMHAIATION: i MOVE PERSON TO FRESH AIR AT ONCE. IF.NOT GIVE ARTIFICIAL RESPIRATION. i AGIINISTER OXYGIN. BREATNING i EYE C0erIACT: IMMEDIATELY FLUSH ETES WITH PLENTY O LEAST 20 MINtJYEE. SEIN WITH PLENTY OF WATER.IN CAEE OF SEIN OCM REMOVE ANY CONTAMINATED CICIRIN SEC 7 OCCUPATIONAL CONTROL MEASURES 1 1 OSHA PERMISSARLE EXPOSURE LIMIT: NOT ESTABLISHED VENTILATION SYSTEM: 4 IDCAL E2HAUST PERSONAL RESPIRATORE:(NIOSI AFF M VED) RE0019dENDED POR ALL AREA OF POTENTIAL EXPOSURE. PERE 0mEEL WORKING IN OR ABOUT AN SEIN PROTECTION: WEAR INPERVIOUS FEDTICTIVE CIDTHING: } GLOVES: LAB COAT: INCIEDING BOOTS: APRON OR COVERALLS TO PREVENT SIIN i EYE P30 RECTI 0ti: LENSEE SHOULD 100TUEI CMBRICAL SAFETY GO 4 BI WORN 14EEN WOREING WITH TNIS COIFIACT MATERIAL. FACILITIES IN WORE AREA. MAINTAIN EYE WASH 700N AMD QUICE-DRENCE t l l 4 a -m w .p.....,,---gr--....g -._.,m., ,y,e-.,w-- ,,,w--9

i SEhi BY:LLSA11E STATION

10-29-83 3:15PM : COWONEEA1.TH EDISON-ColN0NWEALTH EDISON;46 1

HYP090. QTS i. PAGE 5 of 5 1 03/01/30 SEC 8 STORAGE AND SPECIAL INFORMATION STORE IN A COOL. DRY. VENTILATED AREA. DAMAGE. KEEP SEPARATE FROM INCOMPATIBLES. PROTECT AGAINST P SEC 9 REGULATORY INFORMATION DOT HAZARD CLASS: l DDT PLACARD REQUIRED: CORROSIVE MATERIAL l CORROSIVE 1 DOT LASEL: CORROSIVE .NA 1791 t REGULATED UNDER THE FEDERAL INSECTICIDE j ACT (FIFRA) IF ANY SANITATION OR FUNGICIDE and ROTENTICIDE { DISINFBCTION CLAIMS ARE NAM QN ~ } l NFPA/HMIS ratings: Health - 3 ; Flamatability - 0 ; Anactivity -

0. higher sikalinity R - 1.

1 SARA TITLE III-SEC. 302, 304, 311. 312. i i REPORTABLE QUANTITY (RQ) j (CWA / CERCLA): 100 LSE. 4 l i THE INFORMATION CONTAINED HEREIN IS BELIEVED TO BE CORRECT AS OF PROVIDED IN GOOD FAITH AND IS THE DATE STIEL CHEMICALS INC. MAKES NO HEREOF. HONEVII. E. A. THAT INDIVIDUALS RECEIVINGCOMPRENENSIVENE IT 15 EXPECTED INDEPENDENT JUDetRNT THE INFOBIATICBI WILL IXERCISE THEIR IN DETIIttINING ITE APPROPRIATENESS FOR A PARTICULAR PURPOSE. ACCORDINGLY. K. A. STEEL CNBRICAEJ5, WILL NOT BE RES9018EIBLE POR DAMAGES OF ANY E OF OR N An UPON SDCR INWOMATION. NO REPREERNTATICIOS. OR R WARRANTIES. IITNER EEPREES OR POR A PARTICULAR PURPOSE OR OF ANY OT i WITH RESPECT TO TIE INFORMATION SET FORTH H To WHIQi THE INFORIATION REFERS. DUCT

d iI. Matarini Scfaty Dato Shoct sdI$FURIC ACID, Genium Publishing Corporauon 1145 Catalyn Street CONCENTRATED Sch.a+My,NY 12303-1836 USA Reymon C e "( (518) 377-8855 Issued: Oceah-e 1980 i casum - - com. Revised: R,.mmy 1986 i SECTION 1 MATERIAL IDENTIFICATION i 19 2 MA1TRf AL NAME SULEURIC ACID, CONCENTRATED O OTMFR DEXfCNAT10NS: Oil of Vitnol, Hydrogen Sulfate; H SO ; CAS #7664-93-9 3 2 2 4 MANUFAC7URF_R/SUPPT YFR? Avadable imm many suppliers, including: HMIS Allied Corporanon, PO Box 2064R. Mornstown, NJ 07960; Telephone: 800 631-8050 F: 0 R1 R: 2 - I 3 PPE:

S4 See sect. 8 K0 SECE4@tbGr.4NG4HMMGP$TScANDt'A*J"E-5 ---

~C +- H AZARD DATA Hy m. Sulfate (H SO ) i 2 4 93-98 8-tr TWA: 1 myum3 Water Balace* HmWIh. 3

Maxenalis obtained by the react.on of 50 and wear. Can canten TCla: 3 myer. 24 wtr,.

3 low impunry levels, such as 0.02% maa of iros as Fe. Properuss vary @me h h) with H SO cantant. I 2 4 Rat. Oral, Carmnt OSHA standard and ACCIH (1985-86)TLV. NIOSH has a 10-fr LD50: 2140 mg/kg TWA,40 hr. work weet, of 1 mg/m. 3 SECTION 3. PHYSICAL DATA ~"o 93.19% H SO4 98.33% H SO4 100% H SO4 2 2 2 Boiling Point, I aan. C ca 28s ca 338 ca 330 (de) Specific Gravity (60/60 1.8354 1.84 1.84 Volatdes. % @ 340*C ca 100 ca 100 ca 100 i Melting Point, deg C ca.34 ca 3 10A Water Solubdity Conglese Miscible Vapor Premme, non Hg @ 100*F <1 (93.19% H40 ); reponed in degress Baume Be). Formala is Bo=145 (145/sp gr for liquads heavser than wanw[Deg 4 4 2 4 i Appearance and ador Clear, colorises, hygroscopec, ody liquid widt no oder. Mises passer that I airm3 3 seseedy l recosmzable. Those at 5 matar are distancelv oW SECTION 4. FIRE AND EXPLOSION DATAt-w -~~e LOWER UPPER { Flash Patrit and Method Aur c = Ta'a=_ Finnmahaintyllaues in Air i None - Nonfiammabis NA NA NA NA w%c acad is ~ m; no ar,26 is a soong osaamag agnet aus may cases igensa ey coment wun somensues mansnals. Sman Deus may be senemed wdh musshis dry chamacaL Cool emannerof seneses tasks of H SO wdh wasar t 2 4 i avod nipase if esposed a rne. tw nor a=== er %a am ihn -ai no end, asymmany when niissed wth wear, em 4 react wie mamm = liberans flammammis byeogue gas. Sulfune acid ama and vapors ime a rue ama me canouve (sms sess. 5). Fire fighaars ausst wear asif -w breastang supupaust and feuy passceive clodung. SECTION 5.-REACTIVITY DATA ~~we Sulfunc acid is simbis mader nonaal ra-dma== of use and storses. It does est undergo hasantous polysannasame it is a strong maeral acid reacnag wish bases and metals. The concensused acid is also a dehydrustg agust, packing up numans readily fmm the er or other maasnals. Hydrogas gas may be generend walds a H SO4 causmeer. Vent drums cas 2 This mansnal rescas emothenmcaDy with water. (Acid should always he added slowly a waar. Weser added to acid ca boding and uncoenound splashag of the med.) Sulfur osadas can result from ' sulfurac acad. and ime osadinag ressmans of EE"afmImmm*m*e Eu"ss Nammme PumEAmtpummme e amatud,

4 No.9 2/86 SULFURIC Acrn, CONCENTRATED (Rev. C) i ' SECTION 6. HEALTH HAZARD INFORMATION lTLV Concennstad sulfunc acid is a strong mmeral acad, an o**=: agent, and a dehydraung agent tha j human ussue with which it comes m contact. Ingescon may cause severe mjury or death. Eye contact i permanent injury. f*'W of mists can damage both the upper respiratory tract and the lungs. Sulfunc acid is no j a caremogen by the f(fP, IARC, or OSHA. FTDST AfD: EVE CONTACT: Immediatelv flush eyes (including under cychds) wuh plenty of runmng water for at lew = mutes. Speed in dilutmg and nasing out ac:d with water is estremely important if permanent eye damag 15 Obtam medical help as soon as possible.* ELN CONTACT: contammated clothmg y.tilg under the safety shower. Cocuoue washag with water and ge IWALATION: Remove to fresh att. Restore bresuung. Call a physacian immediately, INCESTION: Ddute acid i-meme'v wah large amounts of tmlk or waser, then give mdk of magame so neverahae. Never give anytfu an unconscious person. Do not toduce vonnung; if it occurs spontaneously, cocunne to ademisier fluid. Obtam m.d eal a::enuon as soon as possible.* Mamtam observauan of pauent for possible delayed onset of pulmonary edema. t

GET MEDICAL HELP In plant, paramedic, e-"My.

_SECrlON 7. SPILL. LEAK. AND DISPOSAL PROCEDURES Hardle ma.ior spdla by a p 5 m -4 plan. Contact supplaer for==an rance a this plannang, m meeung local regulanons, ud for disposmg of large amounts. Notify safety personnel Provide optanmas vestalanon; vapars are en Sap ieac if you can do so without rut. Cleanup personnel need protecoon agamst mhalanon or contact. Keep upwed. Contam spdl. Mmor leaks dduted wun much water and neutrahzed with soda ash or tune. If water is not avadable uries, or gravel and neutrahze caucously wuh soda ash or lime. DISPOS AU Follow Federal, state, and local regulacons. Runoff to sewer may crease hydrogen gas, which is a fire exoiosion rizzard. EPA (CWA) RQ 1000 los. (40 CFR 117). SECTION 8. SPECIAL PROTECTION INFORMATION - Provide general ventdataos a meet current TLV requarements in the -.ay1 Where nusts are up to 50 mgtm, a high-3 efficicocy paruculase resperator with full f pressurewsemand mode is used to 100 rog/m.nece ts warranted; a typc4 supplier-aar resperssor with full facepsece o Avoid eye contact by use of chemical safety goggles or face shield where sp! ashing may occur. Acid-resistant pro clopung, such as rubber glovea, aprons, boots, and suits, as recommended to avoid body contact. Eyewash foumam and safety showers with deluge type of heads should be maddg avadable where this masena stored. Contact lenses pose a special hazard; soft lenses may abaarb and all lensus casousens armanas. Co.,.: we prTn=r===# and ammaal medacal exammannes wuh emphmus se demaal womaa. C, ' mucous memhrane urganon and cough are indacated. --i systna, and SECTION 9. SPECIAL PRECAUTIONS AND COMMENTS-Sulfunc acid in carooys or drums should be aioned in clean, venidased aurige ames havmg ead-remnant floors wa dramage. Keep out of diress senhght, do not anon above 89EF (32*C). Stories facahmes as to be separnas froni o masenala, meta!!ic powders, skeomains, chloranes, aurains, carbides, candasables, etc. Soda ash, sand, or time sh m general storage or work areas for emergency use. Prosset contaaners agamst physsal damage. Glass botues need extra prosecuon. Sulfunc acid is highly corrosive to most metals, especially below 775 H SO. Avoed breathing anst or vapora 2 4 Avoid contact wuh slan or eyes. Do not ingest. Do not add water to concentrased acad. Drums may contam hydrogen g so open cauuously. Use nonapartmg tools free of oil, dat, and gra and vapar-pmof electncal fiamres DOT Clasuficataate Corrosive Malenal. ID No.: UNig30 Label: Corrosive Data Source (s) Code: 1-12,19,20,24,26,31,37-39,42,82. CK u.s . mu u.un,rnr.re n t,p.m rs,,=. Approvals %fMumccv, 0-/ffa, u..= ru, pen re mma.rn=w ssim-io - w a.=r.r w Tr sn-

5. I."*.".'.".". '." M.

.. ".M7 Indust. HygTe'ne/ Safety % /d(,- = = - - r- < = = = Medical Review MM h ( h.ra."' 7."J:llllBam:",==m .,,,em. copyrtsbc c February 1,l9W [# <}}

ML20058K194

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ML20058K194

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