ML18019A725
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-16778-2 Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Mr. Martin Swanson Authorized for release by:
4/28/2016 12:41:27 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-16778-2 Page 2 of 16 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
4 Receipt Checklists.........................................
5 Definitions/Glossary.......................................
6 Method Summary.........................................
7 Sample Summary.........................................
8 Client Sample Results......................................
9 QC Sample Results........................................
14 QC Association Summary...................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16778-2 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16778-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: HDP RFP-CBA-022 (7 DAY TAT)
Report Number: 160-16778-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 4/4/2016 11:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 20.0º C.
RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)
Samples L05-04-01-T-S-S-00 (160-16778-1), L05-04-02-T-R-S-00 (160-16778-2), L05-04-02-T-R-Q-00 (160-16778-3),
L05-04-04-T-E-S-00 (160-16778-4), L05-04-05-T-S-S-00 (160-16778-5), L05-04-06-T-R-S-00 (160-16778-6), L05-04-08-T-S-S-00 (160-16778-7), L05-04-09-T-R-S-00 (160-16778-8), L05-04-11-T-S-S-00 (160-16778-9) and L05-04-12-T-R-S-00 (160-16778-10) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 04/04/2016, prepared on 04/06/2016 and analyzed on 04/27/2016.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 4 I
Page 1 of 11 Westingho11se Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instruct.ions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain ofCutody ID No. I F-040116-01 Page 1/1 Project Name:
Westinghouse Electric Company Contact Person:
Clark Evers Phone Number:
314-810-3336 Sampler Name Mike Dekeyser Sample ID L05-04-0 l -T-S-S-00 L05-04~02-T-R-S-OO L05-04-02-T-R-Q-OO L05-04-04-t-E-S-00 L05-04-05* t-S-S-00 L05-04-06-T-R-S-00 L05-04-08-T-S-S-OO L05-04-09-T-R-S-OO L05-04-l l-T-S-S-OO IL05-04-12-T-R-S-OO Date 4/1/2016 4/1/2016 4/1/2016 4/1/2016 4/1/2016 4/1/2016 4/1/2016 4/1/2016 4/1/2016 4/1/2016 Relinquished by: -i....--=--
t--1 -~ t.t'..w$-
Company Name~tf C...
Received by:
Company Name:
by:,3 \\ \\. ~
Time 8:30 12:40 12:40 8:40 8:55 12:55 9:00 10:45 9:05 13:25 Date/Time lf-y-f(.,
o,;;oo Date/Time Matrix s
s s
s s
s s
s s
s Relinquishecl by:
Company Name:
q.-4-,,1,,
() Gt ; OC.,
Laboratory Name:
TA-MO Laboratory Address:
13715 Rider Trail North
"' i,1---------------------l
-~ Phone No.
8 314-298-8566
]i Laboratory Contact Person:
~ Ivan Vania Phone No.
7J28-870-8453 Turn Around Time Rush 1 ILSA 05-04 1 ILSA 05-04 l
- ILSA 05-04 1, ILSA 05-04 l ILSA 05-04 1' ILSA 05-04 1 ILSA 05-04 lJ ILSA 05-04 f ILSA 05-04 1 ILSA05-04 Cooler Temperature:
Cooler ID: I Shipper and Number:
1401-01 (7 days)
Remarks Ambient Date/Time I Comments: NIA Verified By:
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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-16778-2 Login Number: 16778 Question Answer Comment Creator: Dedner, Connie L List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
N/A Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time (excluding tests with immediate HTs)
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-16778-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Qualifiers Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-16778-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 7 of 16 1
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Sample Summary TestAmerica Job ID: 160-16778-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-16778-1 L05-04-01-T-S-S-00 Solid 04/01/16 08:30 04/04/16 11:00 160-16778-2 L05-04-02-T-R-S-00 Solid 04/01/16 12:40 04/04/16 11:00 160-16778-3 L05-04-02-T-R-Q-00 Solid 04/01/16 12:40 04/04/16 11:00 160-16778-4 L05-04-04-T-E-S-00 Solid 04/01/16 08:40 04/04/16 11:00 160-16778-5 L05-04-05-T-S-S-00 Solid 04/01/16 08:55 04/04/16 11:00 160-16778-6 L05-04-06-T-R-S-00 Solid 04/01/16 12:55 04/04/16 11:00 160-16778-7 L05-04-08-T-S-S-00 Solid 04/01/16 09:00 04/04/16 11:00 160-16778-8 L05-04-09-T-R-S-00 Solid 04/01/16 10:45 04/04/16 11:00 160-16778-9 L05-04-11-T-S-S-00 Solid 04/01/16 09:05 04/04/16 11:00 160-16778-10 L05-04-12-T-R-S-00 Solid 04/01/16 13:25 04/04/16 11:00 TestAmerica St. Louis Page 8 of 16 1
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Client Sample Results TestAmerica Job ID: 160-16778-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16778-1 Client Sample ID: L05-04-01-T-S-S-00 Matrix: Solid Date Collected: 04/01/16 08:30 Date Received: 04/04/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.07 (2+/-)
0.160 (2+/-)
1 04/27/16 08:31 04/06/16 10:29 pCi/g 0.116 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/06/16 10:29 04/27/16 08:31 1
0.386 0.447 0.424 1.36 Bismuth 212 pCi/g 04/06/16 10:29 04/27/16 08:31 1
0.0570 0.171 0.109 1.27 Bismuth 214 pCi/g 04/06/16 10:29 04/27/16 08:31 1
0.0636 0.159 0.0789 1.07 Lead 212 pCi/g 04/06/16 10:29 04/27/16 08:31 1
0.0759 0.167 0.0939 1.33 Lead 214 pCi/g 04/06/16 10:29 04/27/16 08:31 1
0.317 2.27 1.20 18.9 Potassium 40 pCi/g 04/06/16 10:29 04/27/16 08:31 1
1.10 0.266 0.258 U
0.606 Protactinium 231 pCi/g 04/06/16 10:29 04/27/16 08:31 1
0.0570 1.00 0.171 0.109 1.27 Radium 226 pCi/g 04/06/16 10:29 04/27/16 08:31 1
0.116 0.160 0.117 1.07 Thorium 232 pCi/g 04/06/16 10:29 04/27/16 08:31 1
0.782 0.310 0.289 1.05 Thorium 234 pCi/g 04/06/16 10:29 04/27/16 08:31 1
0.193 0.157 0.154 0.307 Uranium 235 pCi/g 04/06/16 10:29 04/27/16 08:31 1
0.0911 0.0545 0.0544 U
0.0181 Americium 241 pCi/g 04/06/16 10:29 04/27/16 08:31 1
5.51 3.79 3.74 6.09 Protactinium 234m Tl-208 0.349 0.0480 0.0601 0.0367 pCi/g 04/06/16 10:29 04/27/16 08:31 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16778-2 Client Sample ID: L05-04-02-T-R-S-00 Matrix: Solid Date Collected: 04/01/16 12:40 Date Received: 04/04/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.03 (2+/-)
0.170 (2+/-)
1 04/27/16 08:28 04/06/16 10:29 pCi/g 0.0922 RL MDC 0.134 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/06/16 10:29 04/27/16 08:28 1
0.342 0.351 0.340 0.821 Bismuth 212 pCi/g 04/06/16 10:29 04/27/16 08:28 1
0.0596 0.129 0.0886 0.909 Bismuth 214 pCi/g 04/06/16 10:29 04/27/16 08:28 1
0.0656 0.143 0.0750 0.942 Lead 212 pCi/g 04/06/16 10:29 04/27/16 08:28 1
0.0593 0.135 0.0791 1.06 Lead 214 pCi/g 04/06/16 10:29 04/27/16 08:28 1
0.346 2.02 1.02 17.0 Potassium 40 pCi/g 04/06/16 10:29 04/27/16 08:28 1
0.905 0.223 0.219 U
0.416 Protactinium 231 pCi/g 04/06/16 10:29 04/27/16 08:28 1
0.0596 1.00 0.129 0.0886 0.909 Radium 226 pCi/g 04/06/16 10:29 04/27/16 08:28 1
0.0922 0.170 0.134 1.03 Thorium 232 pCi/g 04/06/16 10:29 04/27/16 08:28 1
0.775 0.283 0.267 0.894 Thorium 234 pCi/g 04/06/16 10:29 04/27/16 08:28 1
0.228 0.124 0.123 U
0.150 Uranium 235 pCi/g 04/06/16 10:29 04/27/16 08:28 1
0.103 0.0621 0.0620 U
-0.0356 Americium 241 pCi/g 04/06/16 10:29 04/27/16 08:28 1
4.10 2.07 2.04 U
3.52 Protactinium 234m Tl-208 0.278 0.0370 0.0469 0.0294 pCi/g 04/06/16 10:29 04/27/16 08:28 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16778-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16778-3 Client Sample ID: L05-04-02-T-R-Q-00 Matrix: Solid Date Collected: 04/01/16 12:40 Date Received: 04/04/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.574 (2+/-)
0.165 (2+/-)
1 04/27/16 08:22 04/06/16 10:29 pCi/g 0.181 RL MDC 0.155 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/06/16 10:29 04/27/16 08:22 1
0.392 0.468 0.447 1.32 Bismuth 212 pCi/g 04/06/16 10:29 04/27/16 08:22 1
0.0905 0.160 0.129 0.909 Bismuth 214 pCi/g 04/06/16 10:29 04/27/16 08:22 1
0.0774 0.160 0.0922 1.01 Lead 212 pCi/g 04/06/16 10:29 04/27/16 08:22 1
0.0790 0.140 0.101 0.941 Lead 214 pCi/g 04/06/16 10:29 04/27/16 08:22 1
0.497 2.40 1.45 18.8 Potassium 40 pCi/g 04/06/16 10:29 04/27/16 08:22 1
1.37 0.250 0.246 U
0.383 Protactinium 231 pCi/g 04/06/16 10:29 04/27/16 08:22 1
0.0905 1.00 0.160 0.129 0.909 Radium 226 pCi/g 04/06/16 10:29 04/27/16 08:22 1
0.181 0.165 0.155 0.574 Thorium 232 pCi/g 04/06/16 10:29 04/27/16 08:22 1
1.05 0.907 0.887 1.81 Thorium 234 pCi/g 04/06/16 10:29 04/27/16 08:22 1
0.269 0.187 0.187 U
0.113 Uranium 235 pCi/g 04/06/16 10:29 04/27/16 08:22 1
0.115 0.0681 0.0681 U
-0.00134 Americium 241 pCi/g 04/06/16 10:29 04/27/16 08:22 1
6.93 3.91 3.91 U
-0.678 Protactinium 234m Tl-208 0.400 0.0611 0.0738 0.0401 pCi/g 04/06/16 10:29 04/27/16 08:22 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16778-4 Client Sample ID: L05-04-04-T-E-S-00 Matrix: Solid Date Collected: 04/01/16 08:40 Date Received: 04/04/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.14 (2+/-)
0.205 (2+/-)
1 04/27/16 11:03 04/06/16 10:29 pCi/g 0.0951 RL MDC 0.169 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/06/16 10:29 04/27/16 11:03 1
0.443 0.505 0.488 1.26 Bismuth 212 pCi/g 04/06/16 10:29 04/27/16 11:03 1
0.0764 0.170 0.120 1.17 Bismuth 214 pCi/g 04/06/16 10:29 04/27/16 11:03 1
0.0658 0.151 0.0791 0.991 Lead 212 pCi/g 04/06/16 10:29 04/27/16 11:03 1
0.0719 0.170 0.0992 1.33 Lead 214 pCi/g 04/06/16 10:29 04/27/16 11:03 1
0.223 2.21 1.18 18.2 Potassium 40 pCi/g 04/06/16 10:29 04/27/16 11:03 1
1.07 0.362 0.356 U
0.561 Protactinium 231 pCi/g 04/06/16 10:29 04/27/16 11:03 1
0.0764 1.00 0.170 0.120 1.17 Radium 226 pCi/g 04/06/16 10:29 04/27/16 11:03 1
0.0951 0.205 0.169 1.14 Thorium 232 pCi/g 04/06/16 10:29 04/27/16 11:03 1
0.761 0.272 0.261 U
0.745 Thorium 234 pCi/g 04/06/16 10:29 04/27/16 11:03 1
0.232 0.110 0.109 U
0.0909 Uranium 235 pCi/g 04/06/16 10:29 04/27/16 11:03 1
0.0961 0.0574 0.0574 U
-0.0189 Americium 241 pCi/g 04/06/16 10:29 04/27/16 11:03 1
6.08 2.30 2.28 U
3.46 Protactinium 234m Tl-208 0.338 0.0496 0.0608 0.0391 pCi/g 04/06/16 10:29 04/27/16 11:03 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16778-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16778-5 Client Sample ID: L05-04-05-T-S-S-00 Matrix: Solid Date Collected: 04/01/16 08:55 Date Received: 04/04/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.754 (2+/-)
0.117 (2+/-)
1 04/27/16 11:29 04/06/16 10:29 pCi/g 0.0740 RL MDC 0.0877 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/06/16 10:29 04/27/16 11:29 1
0.316 0.389 0.371 1.14 Bismuth 212 pCi/g 04/06/16 10:29 04/27/16 11:29 1
0.0354 0.105 0.0693 0.758 Bismuth 214 pCi/g 04/06/16 10:29 04/27/16 11:29 1
0.0575 0.107 0.0627 0.670 Lead 212 pCi/g 04/06/16 10:29 04/27/16 11:29 1
0.0613 0.107 0.0679 0.801 Lead 214 pCi/g 04/06/16 10:29 04/27/16 11:29 1
0.297 1.67 0.891 13.8 Potassium 40 pCi/g 04/06/16 10:29 04/27/16 11:29 1
0.915 0.154 0.151 U
0.313 Protactinium 231 pCi/g 04/06/16 10:29 04/27/16 11:29 1
0.0354 1.00 0.105 0.0693 0.758 Radium 226 pCi/g 04/06/16 10:29 04/27/16 11:29 1
0.0740 0.117 0.0877 0.754 Thorium 232 pCi/g 04/06/16 10:29 04/27/16 11:29 1
0.568 0.387 0.370 1.09 Thorium 234 pCi/g 04/06/16 10:29 04/27/16 11:29 1
0.156 0.0894 0.0881 U
0.147 Uranium 235 pCi/g 04/06/16 10:29 04/27/16 11:29 1
0.0846 0.0506 0.0505 U
0.0155 Americium 241 pCi/g 04/06/16 10:29 04/27/16 11:29 1
4.02 2.44 2.44 U
0.293 Protactinium 234m Tl-208 0.264 0.0393 0.0479 0.0291 pCi/g 04/06/16 10:29 04/27/16 11:29 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16778-6 Client Sample ID: L05-04-06-T-R-S-00 Matrix: Solid Date Collected: 04/01/16 12:55 Date Received: 04/04/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.06 (2+/-)
0.190 (2+/-)
1 04/27/16 11:44 04/06/16 10:29 pCi/g 0.153 RL MDC 0.156 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/06/16 10:29 04/27/16 11:44 1
0.542 0.384 0.377 0.703 Bismuth 212 pCi/g 04/06/16 10:29 04/27/16 11:44 1
0.0887 0.190 0.142 1.21 Bismuth 214 pCi/g 04/06/16 10:29 04/27/16 11:44 1
0.0882 0.166 0.0976 1.04 Lead 212 pCi/g 04/06/16 10:29 04/27/16 11:44 1
0.0915 0.174 0.114 1.26 Lead 214 pCi/g 04/06/16 10:29 04/27/16 11:44 1
0.256 2.39 1.39 18.9 Potassium 40 pCi/g 04/06/16 10:29 04/27/16 11:44 1
1.35 0.434 0.429 U
0.605 Protactinium 231 pCi/g 04/06/16 10:29 04/27/16 11:44 1
0.0887 1.00 0.190 0.142 1.21 Radium 226 pCi/g 04/06/16 10:29 04/27/16 11:44 1
0.153 0.190 0.156 1.06 Thorium 232 pCi/g 04/06/16 10:29 04/27/16 11:44 1
1.21 0.371 0.356 U
1.00 Thorium 234 pCi/g 04/06/16 10:29 04/27/16 11:44 1
0.289 0.113 0.112 U
0.109 Uranium 235 pCi/g 04/06/16 10:29 04/27/16 11:44 1
0.117 0.0693 0.0693 U
-0.00183 Americium 241 pCi/g 04/06/16 10:29 04/27/16 11:44 1
6.94 3.97 3.97 U
1.11 Protactinium 234m Tl-208 0.372 0.0638 0.0746 0.0519 pCi/g 04/06/16 10:29 04/27/16 11:44 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16778-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16778-7 Client Sample ID: L05-04-08-T-S-S-00 Matrix: Solid Date Collected: 04/01/16 09:00 Date Received: 04/04/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.908 (2+/-)
0.165 (2+/-)
1 04/27/16 12:18 04/06/16 10:29 pCi/g 0.132 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/06/16 10:29 04/27/16 12:18 1
0.518 0.332 0.330 U
0.381 Bismuth 212 pCi/g 04/06/16 10:29 04/27/16 12:18 1
0.0550 0.140 0.106 0.886 Bismuth 214 pCi/g 04/06/16 10:29 04/27/16 12:18 1
0.0722 0.135 0.0820 0.831 Lead 212 pCi/g 04/06/16 10:29 04/27/16 12:18 1
0.0822 0.152 0.105 1.05 Lead 214 pCi/g 04/06/16 10:29 04/27/16 12:18 1
0.458 1.95 1.26 14.6 Potassium 40 pCi/g 04/06/16 10:29 04/27/16 12:18 1
1.27 0.323 0.317 U
0.555 Protactinium 231 pCi/g 04/06/16 10:29 04/27/16 12:18 1
0.0550 1.00 0.140 0.106 0.886 Radium 226 pCi/g 04/06/16 10:29 04/27/16 12:18 1
0.132 0.165 0.137 0.908 Thorium 232 pCi/g 04/06/16 10:29 04/27/16 12:18 1
0.870 0.347 0.318 1.32 Thorium 234 pCi/g 04/06/16 10:29 04/27/16 12:18 1
0.236 0.186 0.178 0.513 Uranium 235 pCi/g 04/06/16 10:29 04/27/16 12:18 1
0.112 0.0668 0.0668 U
-0.0125 Americium 241 pCi/g 04/06/16 10:29 04/27/16 12:18 1
5.99 4.12 4.09 U
4.83 Protactinium 234m Tl-208 0.297 0.0477 0.0568 0.0333 pCi/g 04/06/16 10:29 04/27/16 12:18 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16778-8 Client Sample ID: L05-04-09-T-R-S-00 Matrix: Solid Date Collected: 04/01/16 10:45 Date Received: 04/04/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.857 (2+/-)
0.151 (2+/-)
1 04/27/16 11:39 04/06/16 10:29 pCi/g 0.0927 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/06/16 10:29 04/27/16 11:39 1
0.358 0.374 0.360 0.955 Bismuth 212 pCi/g 04/06/16 10:29 04/27/16 11:39 1
0.0674 0.146 0.102 1.01 Bismuth 214 pCi/g 04/06/16 10:29 04/27/16 11:39 1
0.0571 0.125 0.0680 0.810 Lead 212 pCi/g 04/06/16 10:29 04/27/16 11:39 1
0.0623 0.140 0.0844 1.07 Lead 214 pCi/g 04/06/16 10:29 04/27/16 11:39 1
0.200 1.77 0.996 14.4 Potassium 40 pCi/g 04/06/16 10:29 04/27/16 11:39 1
1.01 0.190 0.188 U
0.230 Protactinium 231 pCi/g 04/06/16 10:29 04/27/16 11:39 1
0.0674 1.00 0.146 0.102 1.01 Radium 226 pCi/g 04/06/16 10:29 04/27/16 11:39 1
0.0927 0.151 0.123 0.857 Thorium 232 pCi/g 04/06/16 10:29 04/27/16 11:39 1
0.702 0.267 0.258 U
0.668 Thorium 234 pCi/g 04/06/16 10:29 04/27/16 11:39 1
0.159 0.102 0.100 0.178 Uranium 235 pCi/g 04/06/16 10:29 04/27/16 11:39 1
0.0910 0.0543 0.0543 U
-0.0141 Americium 241 pCi/g 04/06/16 10:29 04/27/16 11:39 1
5.18 2.99 2.99 U
0.998 Protactinium 234m Pb-210 1.39 0.494 0.521 0.621 pCi/g 04/06/16 10:29 04/27/16 11:39 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.293 0.0489 0.0576 0.0382 pCi/g 04/06/16 10:29 04/27/16 11:39 1
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Client Sample Results TestAmerica Job ID: 160-16778-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16778-9 Client Sample ID: L05-04-11-T-S-S-00 Matrix: Solid Date Collected: 04/01/16 09:05 Date Received: 04/04/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.525 (2+/-)
0.0982 (2+/-)
1 04/27/16 12:09 04/06/16 10:29 pCi/g 0.0652 RL MDC 0.0823 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/06/16 10:29 04/27/16 12:09 1
0.306 0.197 0.196 U
0.254 Bismuth 212 pCi/g 04/06/16 10:29 04/27/16 12:09 1
0.0383 0.0825 0.0575 0.570 Bismuth 214 pCi/g 04/06/16 10:29 04/27/16 12:09 1
0.0409 0.0759 0.0465 0.464 Lead 212 pCi/g 04/06/16 10:29 04/27/16 12:09 1
0.0418 0.0955 0.0594 0.720 Lead 214 pCi/g 04/06/16 10:29 04/27/16 12:09 1
0.197 1.22 0.690 9.83 Potassium 40 pCi/g 04/06/16 10:29 04/27/16 12:09 1
0.761 0.151 0.149 U
0.229 Protactinium 231 pCi/g 04/06/16 10:29 04/27/16 12:09 1
0.0383 1.00 0.0825 0.0575 0.570 Radium 226 pCi/g 04/06/16 10:29 04/27/16 12:09 1
0.0652 0.0982 0.0823 0.525 Thorium 232 pCi/g 04/06/16 10:29 04/27/16 12:09 1
0.702 0.343 0.298 1.63 Thorium 234 pCi/g 04/06/16 10:29 04/27/16 12:09 1
0.136 0.115 0.104 0.488 Uranium 235 pCi/g 04/06/16 10:29 04/27/16 12:09 1
0.0846 0.0508 0.0507 U
-0.0187 Americium 241 pCi/g 04/06/16 10:29 04/27/16 12:09 1
3.38 1.90 1.88 U
2.72 Protactinium 234m Tl-208 0.141 0.0270 0.0307 0.0237 pCi/g 04/06/16 10:29 04/27/16 12:09 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16778-10 Client Sample ID: L05-04-12-T-R-S-00 Matrix: Solid Date Collected: 04/01/16 13:25 Date Received: 04/04/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.913 (2+/-)
0.180 (2+/-)
1 04/27/16 12:12 04/06/16 10:29 pCi/g 0.150 RL MDC 0.154 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/06/16 10:29 04/27/16 12:12 1
0.421 0.440 0.420 1.26 Bismuth 212 pCi/g 04/06/16 10:29 04/27/16 12:12 1
0.0753 0.140 0.106 0.877 Bismuth 214 pCi/g 04/06/16 10:29 04/27/16 12:12 1
0.0663 0.150 0.0794 0.981 Lead 212 pCi/g 04/06/16 10:29 04/27/16 12:12 1
0.0729 0.145 0.0937 1.06 Lead 214 pCi/g 04/06/16 10:29 04/27/16 12:12 1
0.329 2.12 1.18 17.2 Potassium 40 pCi/g 04/06/16 10:29 04/27/16 12:12 1
0.999 0.248 0.243 U
0.416 Protactinium 231 pCi/g 04/06/16 10:29 04/27/16 12:12 1
0.0753 1.00 0.140 0.106 0.877 Radium 226 pCi/g 04/06/16 10:29 04/27/16 12:12 1
0.150 0.180 0.154 0.913 Thorium 232 pCi/g 04/06/16 10:29 04/27/16 12:12 1
0.779 0.505 0.493 1.07 Thorium 234 pCi/g 04/06/16 10:29 04/27/16 12:12 1
0.223 0.140 0.140 U
0.115 Uranium 235 pCi/g 04/06/16 10:29 04/27/16 12:12 1
0.0863 0.0516 0.0515 U
0.0207 Americium 241 pCi/g 04/06/16 10:29 04/27/16 12:12 1
5.58 3.26 3.25 U
-1.38 Protactinium 234m Tl-208 0.328 0.0444 0.0560 0.0315 pCi/g 04/06/16 10:29 04/27/16 12:12 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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QC Sample Results TestAmerica Job ID: 160-16778-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-244684/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 248012 Prep Batch: 244684 Actinium 228 Analyte U
1 04/27/16 15:56 04/06/16 10:29 pCi/g 0.0444 MDC RL 0.0254 0.0253 (2+/-)
(2+/-)
MB 0.01339 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
04/27/16 15:56 04/06/16 10:29 pCi/g 0.130 0.0749 0.0748 U
0.04229 Bismuth 212 1
04/27/16 15:56 04/06/16 10:29 pCi/g 0.0335 0.0200 0.0200 U
0.002566 Bismuth 214 1
04/27/16 15:56 04/06/16 10:29 pCi/g 0.0231 0.0263 0.0263 U
-0.003714 Lead 212 1
04/27/16 15:56 04/06/16 10:29 pCi/g 0.0299 0.0470 0.0470 U
-0.006331 Lead 214 1
04/27/16 15:56 04/06/16 10:29 pCi/g 0.164 2.28 2.28 U
-0.05688 Potassium 40 1
04/27/16 15:56 04/06/16 10:29 pCi/g 0.292 0.155 0.155 U
-0.0009372 Protactinium 231 1
04/27/16 15:56 04/06/16 10:29 pCi/g 0.0335 1.00 0.0200 0.0200 U
0.002566 Radium 226 1
04/27/16 15:56 04/06/16 10:29 pCi/g 0.0444 0.0254 0.0253 U
0.01339 Thorium 232 1
04/27/16 15:56 04/06/16 10:29 pCi/g 0.274 0.0209 0.0209 U
0.01415 Thorium 234 1
04/27/16 15:56 04/06/16 10:29 pCi/g 0.0593 0.000605 0.000605 U
-0.0001865 Uranium 235 1
04/27/16 15:56 04/06/16 10:29 pCi/g 0.0221 0.0125 0.0125 U
0.002849 Americium 241 1
04/27/16 15:56 04/06/16 10:29 pCi/g 2.35 13.7 13.7 U
-0.3414 Protactinium 234m Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 04/06/16 10:29 04/27/16 15:56 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-244684/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 248014 Prep Batch: 244684 Americium 241 Analyte 116 87 101 101.9 101 10.6 0.502 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.0 34.06 3.57 0.172 pCi/g 100 87 - 120 Cobalt 60 31.4 31.15 3.15 0.104 pCi/g 99 87 - 115 Client Sample ID: L05-04-01-T-S-S-00 Lab Sample ID: 160-16778-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 248009 Prep Batch: 244684 Actinium 228 Analyte 1
0.28 1.169 1.07 0.195 0.159 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 1.36 1.533 0.531 0.450 pCi/g 0.17 1
Bismuth 214 1.27 1.065 0.177 0.0932 pCi/g 0.58 1
Lead 212 1.07 1.040 0.170 0.0917 pCi/g 0.08 1
Lead 214 1.33 1.299 0.184 0.0866 pCi/g 0.09 1
Potassium 40 18.9 18.49 2.36 0.512 pCi/g 0.08 1
Protactinium 231 0.606 U 0.5927 U 0.254 1.33 pCi/g 0.03 1
Radium 226 1.27 1.065 0.177 1.00 0.0932 pCi/g 0.58 1
Thorium 232 1.07 1.169 0.195 0.159 pCi/g 0.28 1
Thorium 234 1.05 1.105 0.353 0.944 pCi/g 0.08 1
Uranium 235 0.307 0.2470 0.195 0.245 pCi/g 0.17 1
Americium 241 0.0181 U
-0.00127 9
U 0.0724 0.122 pCi/g 0.15 1
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QC Sample Results TestAmerica Job ID: 160-16778-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: L05-04-01-T-S-S-00 Lab Sample ID: 160-16778-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 248009 Prep Batch: 244684 Protactinium 234m Analyte 1
0.54 U
1.984 6.09 3.88 6.59 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Tl-208 1
0.08 0.3591 0.349 0.0683 0.0441 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 15 of 16 1
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QC Association Summary TestAmerica Job ID: 160-16778-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Rad Leach Batch: 244065 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16778-1 L05-04-01-T-S-S-00 Total/NA Solid Dry and Grind 160-16778-1 DU L05-04-01-T-S-S-00 Total/NA Solid Dry and Grind 160-16778-2 L05-04-02-T-R-S-00 Total/NA Solid Dry and Grind 160-16778-3 L05-04-02-T-R-Q-00 Total/NA Solid Dry and Grind 160-16778-4 L05-04-04-T-E-S-00 Total/NA Solid Dry and Grind 160-16778-5 L05-04-05-T-S-S-00 Total/NA Solid Dry and Grind 160-16778-6 L05-04-06-T-R-S-00 Total/NA Solid Dry and Grind 160-16778-7 L05-04-08-T-S-S-00 Total/NA Solid Dry and Grind 160-16778-8 L05-04-09-T-R-S-00 Total/NA Solid Dry and Grind 160-16778-9 L05-04-11-T-S-S-00 Total/NA Solid Dry and Grind 160-16778-10 L05-04-12-T-R-S-00 Total/NA Prep Batch: 244684 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 244065 160-16778-1 L05-04-01-T-S-S-00 Total/NA Solid Fill_Geo-21 244065 160-16778-1 DU L05-04-01-T-S-S-00 Total/NA Solid Fill_Geo-21 244065 160-16778-2 L05-04-02-T-R-S-00 Total/NA Solid Fill_Geo-21 244065 160-16778-3 L05-04-02-T-R-Q-00 Total/NA Solid Fill_Geo-21 244065 160-16778-4 L05-04-04-T-E-S-00 Total/NA Solid Fill_Geo-21 244065 160-16778-5 L05-04-05-T-S-S-00 Total/NA Solid Fill_Geo-21 244065 160-16778-6 L05-04-06-T-R-S-00 Total/NA Solid Fill_Geo-21 244065 160-16778-7 L05-04-08-T-S-S-00 Total/NA Solid Fill_Geo-21 244065 160-16778-8 L05-04-09-T-R-S-00 Total/NA Solid Fill_Geo-21 244065 160-16778-9 L05-04-11-T-S-S-00 Total/NA Solid Fill_Geo-21 244065 160-16778-10 L05-04-12-T-R-S-00 Total/NA Solid Fill_Geo-21 LCS 160-244684/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-244684/1-A Method Blank Total/NA TestAmerica St. Louis Page 16 of 16 1
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