ML18019A683
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3571-2 Client Project/Site: RFP-CBA-022 (7 DAY TAT)
For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:
9/26/2013 4:30:35 PM Ivan Vania, Project Manager I (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-3571-2 Page 2 of 28 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
8 Definitions/Glossary.......................................
9 Method Summary.........................................
10 Sample Summary.........................................
11 Client Sample Results......................................
12 QC Sample Results........................................
25 QC Association Summary...................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3571-2 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3571-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)
Report Number: 160-3571-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 08/29/2013; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 20.0º C and 20.0º C.
RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)
Samples L050119TSQ00 (160-3571-1), L050119TSS00 (160-3571-2), L050120TRS00 (160-3571-3), L050121TSS00 (160-3571-4),
L050122TRS00 (160-3571-5), L050125TRS00 (160-3571-6), L050127TRS00 (160-3571-7), L050128TES00 (160-3571-8),
L050131TRS00 (160-3571-9), L050132TES00 (160-3571-10), L050133TRS00 (160-3571-11), L050139TES00 (160-3571-12),
L050140TRS00 (160-3571-13), L050148TRS00 (160-3571-14), L050154TRS00 (160-3571-15), L050155TES00 (160-3571-16),
L050156TRS00 (160-3571-17), L050157TES00 (160-3571-18), L050162TRQ00 (160-3571-19), L050162TRS00 (160-3571-20),
L050163TES00 (160-3571-21), L050164TRS00 (160-3571-22), L050165TEQ00 (160-3571-23), L050165TES00 (160-3571-24),
L050169TSS00 (160-3571-25), L050170TRS00 (160-3571-26), L050171TRS00 (160-3571-27) and L050172TES00 (160-3571-28) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 08/30/2013, prepared on 09/04/2013 and analyzed on 09/25/2013.
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3571-2 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3571-2 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
No other difficulties were encountered during the Radium 226 analysis. All other quality control parameters were within the acceptance limits.
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Procedw:e HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 3 I
Page.I of l j Westinghouse Non"Proprieta,y Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cntody ID No. I F-082913-02 Page 1/3 Project Name:
Westinghouse Electric Company Contact Person:
Geralq. Rood Phone Number:
- 314-810-3382 Sampler Name Scott Jenkins Sample ID L050119TSQOO IL050119TSS00 L050120TRS00 L050121TSSOO IL050122TRS00 L050l25TRS00 L050l27TRS00
.L050128TES00 L05013 l TRSOO
'L050132TES00 L050l33TRS00 L050l39TES00 Company Name:
Received by:
Company Name:
Relinquished by:
Company Name:
Date Time 8/28/2013 8:50 8/28/2013 8:50 8/28/2013 10:15 8/28/2013 8:40 8/28/2013 9:15
,8/28/2013 10:10 8/28/2013 8:33 8/28/2013 8:45 8/28/2013 10:35 8/28/2013 10:40 8/28/2013 8/28/2013
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Date/Time Matrix s
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s 1 l 1 -I 1 1 Laboratorv Name:
TA-MO Laboratory Address:
13715 Rider Trail North Phone No.
314-298-8566 Laboratory Contact Person:
Joe Walker Phone No.
708-870-8453 Rush TlllJl Around Time (7 days)
Remarks 1 I L-.5 F\\
v os-o Cooler Temperature:
Comments: Please re-analyze samples after 21 day ingrowth period.
Verified By:
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!Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 3 I
Page I of 11 Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAlN OF CUSTODY
,J.nstructions: Each time the container is transferred to another organization, a person from eaeh organization should sign the CoC. The Laboratozy/End User must verify that the. sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutody ID No. l F-082913-02 Page 2/3 Project Name; Westinghouse Electric Company Contact Person:
Gerald Rood Phone Number:
0 314-810"3382 Sampler Name Scott Jenkins n
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Sample ID iL050 l 40TRSOO L050148TRSOO L050154TRSOO L050155TESOO L0501S6TRSOO LOS01S7TESOO LOS0162TRQOO LOSO I 62TRSOO
,LOSO l 63TESOO LOS0164TRSOO L050165TEQOO LG50 l 65TESOO Relinquished by:
Company Name: w Received by:
Company Name:
Reljnquished by:
Company Name:
!Date Time 8/28/2013 8:35 8/28/2013 16:25 8/28/2013 13:05 8/28/2013 13:10 8/28/2013 13:15 8/28/2013 13:40 8/28/2013 11:10 8/28/2013 11:10 8/28/2013 14:00 8/28/2013 10:55 8/28/2013 11:05 8/28/2013 Date/Time Matrix s
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Laboratory Name:
,TA-MO Laboratory Address:
13715 Rider Trail North Phone No.
314-298-8566 Laboratory Contact Person:
Joe Walker Phone No.
708-870-8453 Turn Al"_ou11d T_ime Rush (7 days)
Remarks Li L
Cooler Temperature:
Shipper and Number:
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Comments: Please re-analyz:isamples after 21 day ingrowth period.
Verified By:
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10 11 Procedure HDP-PR-QA-006, Chain of Custody Page l ofl Hematite Decommissioning Project !Revision: 3 I
I WestinghoUse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organizatiQn, a person from each organization should sign the CoC. The Laboratory/End User must verify lhat the sample is correctly identified
'before the sample is releasei;l. for use or analysis and send the completed CoC to HDP.
Chain of Cutod ID No, F-082913-02 Pa e 3/3
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Company Nam\\_,o t,L-Received by:
Company Name:
Relinquished bv:
Company Name:
Date/fiine Date/fiine ct. ()0 e?..,1.,,
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Comp?IlY Name:
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(&':j.fj Coo I er Temperature:
Cooler ID: I Shio.oer and Number:
Comments: Pleas~re-analyze samples after 21 day ingrowth period.
Verified By:
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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3571-2 Login Number: 3571 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
False Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Qualifiers Rad Qualifier Description U
Indicates the analyte was analyzed for but not detected.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 10 of 28 1
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Sample Summary TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-3571-1 L050119TSQ00 Solid 08/28/13 08:50 08/29/13 18:38 160-3571-2 L050119TSS00 Solid 08/28/13 08:50 08/29/13 18:38 160-3571-3 L050120TRS00 Solid 08/28/13 10:15 08/29/13 18:38 160-3571-4 L050121TSS00 Solid 08/28/13 08:40 08/29/13 18:38 160-3571-5 L050122TRS00 Solid 08/28/13 09:15 08/29/13 18:38 160-3571-6 L050125TRS00 Solid 08/28/13 10:10 08/29/13 18:38 160-3571-7 L050127TRS00 Solid 08/28/13 08:33 08/29/13 18:38 160-3571-8 L050128TES00 Solid 08/28/13 08:45 08/29/13 18:38 160-3571-9 L050131TRS00 Solid 08/28/13 10:35 08/29/13 18:38 160-3571-10 L050132TES00 Solid 08/28/13 10:40 08/29/13 18:38 160-3571-11 L050133TRS00 Solid 08/28/13 09:20 08/29/13 18:38 160-3571-12 L050139TES00 Solid 08/28/13 10:20 08/29/13 18:38 160-3571-13 L050140TRS00 Solid 08/28/13 08:35 08/29/13 18:38 160-3571-14 L050148TRS00 Solid 08/28/13 16:25 08/29/13 18:38 160-3571-15 L050154TRS00 Solid 08/28/13 13:05 08/29/13 18:38 160-3571-16 L050155TES00 Solid 08/28/13 13:10 08/29/13 18:38 160-3571-17 L050156TRS00 Solid 08/28/13 13:15 08/29/13 18:38 160-3571-18 L050157TES00 Solid 08/28/13 13:40 08/29/13 18:38 160-3571-19 L050162TRQ00 Solid 08/28/13 11:10 08/29/13 18:38 160-3571-20 L050162TRS00 Solid 08/28/13 11:10 08/29/13 18:38 160-3571-21 L050163TES00 Solid 08/28/13 14:00 08/29/13 18:38 160-3571-22 L050164TRS00 Solid 08/28/13 10:55 08/29/13 18:38 160-3571-23 L050165TEQ00 Solid 08/28/13 11:05 08/29/13 18:38 160-3571-24 L050165TES00 Solid 08/28/13 11:05 08/29/13 18:38 160-3571-25 L050169TSS00 Solid 08/28/13 13:10 08/29/13 18:38 160-3571-26 L050170TRS00 Solid 08/28/13 13:30 08/29/13 18:38 160-3571-27 L050171TRS00 Solid 08/28/13 11:00 08/29/13 18:38 160-3571-28 L050172TES00 Solid 08/28/13 11:15 08/29/13 18:38 TestAmerica St. Louis Page 11 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-1 Client Sample ID: L050119TSQ00 Matrix: Solid Date Collected: 08/28/13 08:50 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.00 (2+/-)
0.156 (2+/-)
1 09/25/13 09:42 09/04/13 12:59 pCi/g 0.100 RL MDC 0.118 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 09:42 1
0.389 0.438 0.426 0.972 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 09:42 1
0.0588 0.130 0.0935 0.865 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 09:42 1
0.0561 0.137 0.0682 0.922 Lead 212 pCi/g 09/04/13 12:59 09/25/13 09:42 1
0.0706 0.134 0.0854 0.996 Lead 214 pCi/g 09/04/13 12:59 09/25/13 09:42 1
0.294 2.11 1.12 17.6 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 09:42 1
0.984 0.291 0.282 U
0.636 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 09:42 1
0.0588 1.00 0.130 0.0935 0.865 Radium 226 pCi/g 09/04/13 12:59 09/25/13 09:42 1
0.100 0.156 0.118 1.00 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 09:42 1
0.828 0.676 0.657 1.51 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 09:42 1
0.187 0.151 0.149 0.219 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 09:42 1
0.0978 0.0580 0.0580 U
-0.00808 Americium 241 pCi/g 09/04/13 12:59 09/25/13 09:42 1
4.83 2.81 2.81 U
0.958 Protactinium 234m Lab Sample ID: 160-3571-2 Client Sample ID: L050119TSS00 Matrix: Solid Date Collected: 08/28/13 08:50 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.894 (2+/-)
0.195 (2+/-)
1 09/25/13 11:49 09/04/13 12:59 pCi/g 0.130 RL MDC 0.172 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 11:49 1
0.304 0.373 0.351 1.22 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 11:49 1
0.0666 0.143 0.101 0.971 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 11:49 1
0.0599 0.149 0.0735 1.00 Lead 212 pCi/g 09/04/13 12:59 09/25/13 11:49 1
0.0713 0.144 0.0964 1.03 Lead 214 pCi/g 09/04/13 12:59 09/25/13 11:49 1
0.329 2.23 1.17 18.5 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 11:49 1
1.31 0.814 0.809 U
-0.871 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 11:49 1
0.0666 1.00 0.143 0.101 0.971 Radium 226 pCi/g 09/04/13 12:59 09/25/13 11:49 1
0.130 0.195 0.172 0.894 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 11:49 1
0.944 0.380 0.362 1.09 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 11:49 1
0.212 0.198 0.194 0.395 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 11:49 1
0.114 0.0678 0.0678 U
0.0151 Americium 241 pCi/g 09/04/13 12:59 09/25/13 11:49 1
5.71 1.85 1.81 U
3.71 Protactinium 234m Lab Sample ID: 160-3571-3 Client Sample ID: L050120TRS00 Matrix: Solid Date Collected: 08/28/13 10:15 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.906 (2+/-)
0.139 (2+/-)
1 09/25/13 11:50 09/04/13 12:59 pCi/g 0.0990 RL MDC 0.104 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 11:50 1
0.308 0.353 0.333 1.12 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 11:50 1
0.0597 0.133 0.0908 0.938 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 11:50 1
0.0707 0.122 0.0659 0.798 Lead 212 TestAmerica St. Louis Page 12 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-3 Client Sample ID: L050120TRS00 Matrix: Solid Date Collected: 08/28/13 10:15 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 1.08 (2+/-)
0.142 (2+/-)
1 09/25/13 11:50 09/04/13 12:59 pCi/g 0.0667 RL MDC 0.0863 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 11:50 1
0.419 2.07 1.07 17.4 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 11:50 1
0.755 0.451 0.450 U
0.243 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 11:50 1
0.0597 1.00 0.133 0.0908 0.938 Radium 226 pCi/g 09/04/13 12:59 09/25/13 11:50 1
0.0990 0.139 0.104 0.906 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 11:50 1
0.825 0.329 0.314 0.934 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 11:50 1
0.229 0.143 0.142 U
0.123 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 11:50 1
0.0947 0.0561 0.0561 U
0.000300 Americium 241 pCi/g 09/04/13 12:59 09/25/13 11:50 1
4.11 2.21 2.16 4.76 Protactinium 234m Lab Sample ID: 160-3571-4 Client Sample ID: L050121TSS00 Matrix: Solid Date Collected: 08/28/13 08:40 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.826 (2+/-)
0.148 (2+/-)
1 09/25/13 11:46 09/04/13 12:59 pCi/g 0.0923 RL MDC 0.122 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 11:46 1
0.356 0.390 0.380 0.833 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 11:46 1
0.0753 0.138 0.108 0.826 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 11:46 1
0.0593 0.116 0.0672 0.735 Lead 212 pCi/g 09/04/13 12:59 09/25/13 11:46 1
0.0649 0.125 0.0841 0.892 Lead 214 pCi/g 09/04/13 12:59 09/25/13 11:46 1
0.279 1.55 1.01 11.5 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 11:46 1
0.986 0.213 0.207 U
0.462 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 11:46 1
0.0753 1.00 0.138 0.108 0.826 Radium 226 pCi/g 09/04/13 12:59 09/25/13 11:46 1
0.0923 0.148 0.122 0.826 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 11:46 1
0.755 0.610 0.586 1.61 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 11:46 1
0.243 0.101 0.101 U
0.0513 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 11:46 1
0.0904 0.225 0.225 U
-0.0119 Americium 241 pCi/g 09/04/13 12:59 09/25/13 11:46 1
5.91 3.28 3.28 U
-0.145 Protactinium 234m Lab Sample ID: 160-3571-5 Client Sample ID: L050122TRS00 Matrix: Solid Date Collected: 08/28/13 09:15 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.28 (2+/-)
0.244 (2+/-)
1 09/25/13 11:47 09/04/13 12:59 pCi/g 0.164 RL MDC 0.206 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 11:47 1
0.659 0.461 0.452 0.846 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 11:47 1
0.0754 0.184 0.133 1.23 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 11:47 1
0.0775 0.179 0.0931 1.18 Lead 212 pCi/g 09/04/13 12:59 09/25/13 11:47 1
0.122 0.170 0.119 1.17 Lead 214 pCi/g 09/04/13 12:59 09/25/13 11:47 1
0.489 2.29 1.45 17.4 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 11:47 1
1.48 0.330 0.323 U
0.634 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 11:47 1
0.0754 1.00 0.184 0.133 1.23 Radium 226 TestAmerica St. Louis Page 13 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-5 Client Sample ID: L050122TRS00 Matrix: Solid Date Collected: 08/28/13 09:15 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 232 1.28 (2+/-)
0.244 (2+/-)
1 09/25/13 11:47 09/04/13 12:59 pCi/g 0.164 RL MDC 0.206 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 11:47 1
1.00 0.771 0.755 1.50 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 11:47 1
0.329 0.156 0.155 U
0.0625 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 11:47 1
0.130 0.0769 0.0769 U
-0.000224 Americium 241 pCi/g 09/04/13 12:59 09/25/13 11:47 1
10.5 4.16 4.16 U
0.000 Protactinium 234m Lab Sample ID: 160-3571-6 Client Sample ID: L050125TRS00 Matrix: Solid Date Collected: 08/28/13 10:10 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.500 (2+/-)
0.191 (2+/-)
1 09/25/13 11:48 09/04/13 12:59 pCi/g 0.272 RL MDC 0.184 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.791 0.533 0.528 U
0.723 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.0977 0.235 0.180 1.47 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.133 0.158 0.120 0.796 Lead 212 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.130 0.246 0.177 1.65 Lead 214 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.696 1.76 1.37 10.8 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 11:48 1
1.23 0.691 0.682 U
0.992 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.0977 1.00 0.235 0.180 1.47 Radium 226 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.272 0.191 0.184 0.500 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 11:48 1
1.92 0.545 0.541 U
0.658 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.462 0.283 0.282 U
0.120 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.210 0.125 0.124 U
0.0502 Americium 241 pCi/g 09/04/13 12:59 09/25/13 11:48 1
9.27 5.03 5.03 U
0.363 Protactinium 234m Lab Sample ID: 160-3571-7 Client Sample ID: L050127TRS00 Matrix: Solid Date Collected: 08/28/13 08:33 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.13 (2+/-)
0.169 (2+/-)
1 09/25/13 11:48 09/04/13 12:59 pCi/g 0.111 RL MDC 0.124 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.384 0.420 0.398 1.31 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.0690 0.153 0.105 1.07 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.0561 0.157 0.0704 1.08 Lead 212 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.0688 0.168 0.103 1.28 Lead 214 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.338 2.18 1.11 18.3 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 11:48 1
1.10 0.236 0.232 U
0.397 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.0690 1.00 0.153 0.105 1.07 Radium 226 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.111 0.169 0.124 1.13 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.769 0.325 0.307 1.03 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.185 0.113 0.113 U
0.107 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 11:48 1
0.104 0.0622 0.0621 U
-0.0104 Americium 241 TestAmerica St. Louis Page 14 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-7 Client Sample ID: L050127TRS00 Matrix: Solid Date Collected: 08/28/13 08:33 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Protactinium 234m
-0.506 U
(2+/-)
14.2 (2+/-)
1 09/25/13 11:48 09/04/13 12:59 pCi/g 4.98 RL MDC 14.2 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Lab Sample ID: 160-3571-8 Client Sample ID: L050128TES00 Matrix: Solid Date Collected: 08/28/13 08:45 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.29 (2+/-)
0.187 (2+/-)
1 09/25/13 13:59 09/04/13 12:59 pCi/g 0.121 RL MDC 0.133 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 13:59 1
0.434 0.474 0.453 1.33 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 13:59 1
0.0851 0.161 0.119 1.04 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 13:59 1
0.0609 0.185 0.0817 1.28 Lead 212 pCi/g 09/04/13 12:59 09/25/13 13:59 1
0.0874 0.163 0.102 1.23 Lead 214 pCi/g 09/04/13 12:59 09/25/13 13:59 1
0.410 2.48 1.28 20.8 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 13:59 1
1.39 0.844 0.841 U
-0.615 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 13:59 1
0.0851 1.00 0.161 0.119 1.04 Radium 226 pCi/g 09/04/13 12:59 09/25/13 13:59 1
0.121 0.187 0.133 1.29 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 13:59 1
0.945 0.747 0.730 1.55 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 13:59 1
0.191 0.119 0.118 U
0.134 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 13:59 1
0.123 0.0734 0.0734 U
-0.00894 Americium 241 pCi/g 09/04/13 12:59 09/25/13 13:59 1
6.26 2.79 2.67 8.19 Protactinium 234m Lab Sample ID: 160-3571-9 Client Sample ID: L050131TRS00 Matrix: Solid Date Collected: 08/28/13 10:35 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.433 (2+/-)
0.0900 (2+/-)
1 09/25/13 13:57 09/04/13 12:59 pCi/g 0.0564 RL MDC 0.0784 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.286 0.297 0.292 0.559 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.0561 0.106 0.0812 0.662 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.0371 0.0677 0.0414 0.414 Lead 212 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.0525 0.102 0.0719 0.693 Lead 214 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.252 1.32 0.800 10.3 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.696 0.211 0.209 U
0.269 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.0561 1.00 0.106 0.0812 0.662 Radium 226 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.0564 0.0900 0.0784 0.433 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.524 0.215 0.202 0.715 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.128 0.0961 0.0951 0.137 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.0668 0.0397 0.0397 U
0.0139 Americium 241 pCi/g 09/04/13 12:59 09/25/13 13:57 1
2.01 2.10 2.06 3.75 Protactinium 234m TestAmerica St. Louis Page 15 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-10 Client Sample ID: L050132TES00 Matrix: Solid Date Collected: 08/28/13 10:40 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.742 (2+/-)
0.136 (2+/-)
1 09/25/13 13:57 09/04/13 12:59 pCi/g 0.0847 RL MDC 0.114 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.695 0.454 0.449 U
0.613 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.0883 0.186 0.140 1.18 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.0858 0.111 0.0782 0.613 Lead 212 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.101 0.158 0.109 1.09 Lead 214 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.335 1.93 1.26 14.2 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 13:57 1
1.42 0.862 0.859 U
-0.653 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.0883 1.00 0.186 0.140 1.18 Radium 226 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.0847 0.136 0.114 0.742 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 13:57 1
1.30 0.503 0.470 1.71 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.326 0.185 0.185 U
0.138 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 13:57 1
0.159 0.0952 0.0951 U
-0.0327 Americium 241 pCi/g 09/04/13 12:59 09/25/13 13:57 1
6.33 3.69 3.69 U
1.84 Protactinium 234m Lab Sample ID: 160-3571-11 Client Sample ID: L050133TRS00 Matrix: Solid Date Collected: 08/28/13 09:20 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.797 (2+/-)
0.143 (2+/-)
1 09/25/13 13:58 09/04/13 12:59 pCi/g 0.0856 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 13:58 1
0.381 0.372 0.364 0.730 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 13:58 1
0.0531 0.141 0.0951 1.00 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 13:58 1
0.0486 0.118 0.0602 0.783 Lead 212 pCi/g 09/04/13 12:59 09/25/13 13:58 1
0.0635 0.126 0.0780 0.948 Lead 214 pCi/g 09/04/13 12:59 09/25/13 13:58 1
0.289 1.69 0.957 13.6 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 13:58 1
0.919 0.217 0.214 U
0.311 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 13:58 1
0.0531 1.00 0.141 0.0951 1.00 Radium 226 pCi/g 09/04/13 12:59 09/25/13 13:58 1
0.0856 0.143 0.117 0.797 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 13:58 1
0.721 0.548 0.538 0.991 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 13:58 1
0.195 0.120 0.120 U
0.104 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 13:58 1
0.0832 0.0497 0.0496 U
-0.0170 Americium 241 pCi/g 09/04/13 12:59 09/25/13 13:58 1
5.07 13.8 13.8 U
-0.346 Protactinium 234m Lab Sample ID: 160-3571-12 Client Sample ID: L050139TES00 Matrix: Solid Date Collected: 08/28/13 10:20 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.374 (2+/-)
0.105 (2+/-)
1 09/25/13 18:31 09/04/13 12:59 pCi/g 0.123 RL MDC 0.0979 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 18:31 1
0.207 0.311 0.296 0.928 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 18:31 1
0.0477 0.117 0.0905 0.717 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 18:31 1
0.0559 0.0665 0.0501 0.338 Lead 212 TestAmerica St. Louis Page 16 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-12 Client Sample ID: L050139TES00 Matrix: Solid Date Collected: 08/28/13 10:20 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 0.842 (2+/-)
0.127 (2+/-)
1 09/25/13 18:31 09/04/13 12:59 pCi/g 0.0577 RL MDC 0.0917 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 18:31 1
0.168 1.38 0.947 9.85 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 18:31 1
0.800 0.400 0.399 U
0.200 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 18:31 1
0.0477 1.00 0.117 0.0905 0.717 Radium 226 pCi/g 09/04/13 12:59 09/25/13 18:31 1
0.123 0.105 0.0979 0.374 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 18:31 1
0.681 0.356 0.318 1.52 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 18:31 1
0.154 0.114 0.112 0.243 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 18:31 1
0.0983 0.0580 0.0580 U
0.00125 Americium 241 pCi/g 09/04/13 12:59 09/25/13 18:31 1
4.35 2.80 2.78 U
2.98 Protactinium 234m Lab Sample ID: 160-3571-13 Client Sample ID: L050140TRS00 Matrix: Solid Date Collected: 08/28/13 08:35 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.430 (2+/-)
0.0911 (2+/-)
1 09/25/13 18:25 09/04/13 12:59 pCi/g 0.0499 RL MDC 0.0799 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.173 0.233 0.222 0.703 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0560 0.102 0.0772 0.643 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0491 0.0770 0.0486 0.462 Lead 212 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0685 0.111 0.0749 0.784 Lead 214 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.265 1.15 0.725 8.71 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.557 0.324 0.324 U
0.109 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0560 1.00 0.102 0.0772 0.643 Radium 226 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0499 0.0911 0.0799 0.430 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.622 0.516 0.503 1.13 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.178 0.106 0.106 U
0.0498 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0774 0.0456 0.0456 U
0.00136 Americium 241 pCi/g 09/04/13 12:59 09/25/13 18:25 1
4.16 1.70 1.67 U
3.15 Protactinium 234m Lab Sample ID: 160-3571-14 Client Sample ID: L050148TRS00 Matrix: Solid Date Collected: 08/28/13 16:25 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.136 (2+/-)
0.0547 (2+/-)
1 09/25/13 18:27 09/04/13 12:59 pCi/g 0.0693 RL MDC 0.0529 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 18:27 1
0.246 0.158 0.157 U
0.183 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 18:27 1
0.0391 0.0980 0.0674 0.684 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 18:27 1
0.0393 0.0330 0.0289 0.124 Lead 212 pCi/g 09/04/13 12:59 09/25/13 18:27 1
0.0449 0.101 0.0626 0.762 Lead 214 pCi/g 09/04/13 12:59 09/25/13 18:27 1
0.256 0.487 0.399 2.73 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 18:27 1
0.568 0.243 0.243 U
0.0615 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 18:27 1
0.0391 1.00 0.0980 0.0674 0.684 Radium 226 TestAmerica St. Louis Page 17 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-14 Client Sample ID: L050148TRS00 Matrix: Solid Date Collected: 08/28/13 16:25 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 232 0.136 (2+/-)
0.0547 (2+/-)
1 09/25/13 18:27 09/04/13 12:59 pCi/g 0.0693 RL MDC 0.0529 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 18:27 1
0.614 0.614 0.578 1.99 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 18:27 1
0.125 0.0911 0.0883 0.220 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 18:27 1
0.0621 0.0369 0.0369 U
-0.00937 Americium 241 pCi/g 09/04/13 12:59 09/25/13 18:27 1
2.56 1.83 1.81 U
2.51 Protactinium 234m Lab Sample ID: 160-3571-15 Client Sample ID: L050154TRS00 Matrix: Solid Date Collected: 08/28/13 13:05 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.109 (2+/-)
0.0499 (2+/-)
1 09/25/13 18:25 09/04/13 12:59 pCi/g 0.0754 RL MDC 0.0486 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.258 0.140 0.140 U
-0.0109 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0442 0.120 0.0808 0.856 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0312 0.0285 0.0248 0.108 Lead 212 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0365 0.118 0.0622 0.962 Lead 214 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.287 0.387 0.358 1.45 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.656 0.264 0.263 U
0.245 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0442 1.00 0.120 0.0808 0.856 Radium 226 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0754 0.0499 0.0486 0.109 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.498 0.289 0.241 1.52 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.134 0.104 0.0990 0.301 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 18:25 1
0.0598 0.0351 0.0351 U
0.00475 Americium 241 pCi/g 09/04/13 12:59 09/25/13 18:25 1
3.12 1.89 1.89 U
1.09 Protactinium 234m Lab Sample ID: 160-3571-16 Client Sample ID: L050155TES00 Matrix: Solid Date Collected: 08/28/13 13:10 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.153 (2+/-)
0.0532 (2+/-)
1 09/25/13 18:26 09/04/13 12:59 pCi/g 0.0320 RL MDC 0.0509 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 18:26 1
0.310 0.195 0.194 U
0.187 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 18:26 1
0.0362 0.123 0.0842 0.861 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 18:26 1
0.0405 0.0339 0.0305 0.115 Lead 212 pCi/g 09/04/13 12:59 09/25/13 18:26 1
0.0515 0.124 0.0768 0.940 Lead 214 pCi/g 09/04/13 12:59 09/25/13 18:26 1
0.296 0.294 0.281 0.851 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 18:26 1
0.648 0.123 0.122 U
0.135 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 18:26 1
0.0362 1.00 0.123 0.0842 0.861 Radium 226 pCi/g 09/04/13 12:59 09/25/13 18:26 1
0.0320 0.0532 0.0509 0.153 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 18:26 1
0.580 0.322 0.291 1.32 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 18:26 1
0.143 0.131 0.126 0.347 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 18:26 1
0.0737 0.0438 0.0438 U
-0.0113 Americium 241 TestAmerica St. Louis Page 18 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-16 Client Sample ID: L050155TES00 Matrix: Solid Date Collected: 08/28/13 13:10 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Protactinium 234m 1.66 U
(2+/-)
2.01 (2+/-)
1 09/25/13 18:26 09/04/13 12:59 pCi/g 3.26 RL MDC 2.00 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Lab Sample ID: 160-3571-17 Client Sample ID: L050156TRS00 Matrix: Solid Date Collected: 08/28/13 13:15 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.364 (2+/-)
0.0704 (2+/-)
1 09/25/13 18:24 09/04/13 12:59 pCi/g 0.0493 RL MDC 0.0599 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 18:24 1
0.154 0.222 0.208 0.737 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 18:24 1
0.0428 0.0806 0.0634 0.479 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 18:24 1
0.0344 0.0621 0.0388 0.375 Lead 212 pCi/g 09/04/13 12:59 09/25/13 18:24 1
0.0430 0.0855 0.0620 0.566 Lead 214 pCi/g 09/04/13 12:59 09/25/13 18:24 1
0.171 1.03 0.648 7.85 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 18:24 1
0.697 0.0793 0.0786 U
0.0956 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 18:24 1
0.0428 1.00 0.0806 0.0634 0.479 Radium 226 pCi/g 09/04/13 12:59 09/25/13 18:24 1
0.0493 0.0704 0.0599 0.364 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 18:24 1
0.527 0.415 0.405 0.847 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 18:24 1
0.114 0.0820 0.0814 U
0.0975 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 18:24 1
0.0585 0.0343 0.0343 U
0.00136 Americium 241 pCi/g 09/04/13 12:59 09/25/13 18:24 1
3.56 31.1 31.1 U
-0.254 Protactinium 234m Lab Sample ID: 160-3571-18 Client Sample ID: L050157TES00 Matrix: Solid Date Collected: 08/28/13 13:40 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.485 (2+/-)
0.0890 (2+/-)
1 09/25/13 19:45 09/04/13 12:59 pCi/g 0.0863 RL MDC 0.0739 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 19:45 1
0.325 0.219 0.216 0.339 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 19:45 1
0.0452 0.0909 0.0665 0.596 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 19:45 1
0.0370 0.0708 0.0424 0.438 Lead 212 pCi/g 09/04/13 12:59 09/25/13 19:45 1
0.0533 0.0940 0.0646 0.657 Lead 214 pCi/g 09/04/13 12:59 09/25/13 19:45 1
0.243 1.11 0.687 8.53 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 19:45 1
0.814 0.129 0.126 U
0.236 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 19:45 1
0.0452 1.00 0.0909 0.0665 0.596 Radium 226 pCi/g 09/04/13 12:59 09/25/13 19:45 1
0.0863 0.0890 0.0739 0.485 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 19:45 1
0.535 0.207 0.196 0.616 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 19:45 1
0.161 0.0972 0.0970 U
0.0541 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 19:45 1
0.0717 0.0244 0.0244 U
0.000 Americium 241 pCi/g 09/04/13 12:59 09/25/13 19:45 1
3.79 9.24 9.24 U
-0.720 Protactinium 234m TestAmerica St. Louis Page 19 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-19 Client Sample ID: L050162TRQ00 Matrix: Solid Date Collected: 08/28/13 11:10 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.19 (2+/-)
0.203 (2+/-)
1 09/25/13 19:46 09/04/13 12:59 pCi/g 0.109 RL MDC 0.162 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 19:46 1
0.415 0.466 0.448 1.24 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 19:46 1
0.0720 0.162 0.112 1.13 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 19:46 1
0.0797 0.156 0.0785 1.04 Lead 212 pCi/g 09/04/13 12:59 09/25/13 19:46 1
0.0689 0.170 0.0970 1.34 Lead 214 pCi/g 09/04/13 12:59 09/25/13 19:46 1
0.326 2.49 1.20 21.3 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 19:46 1
1.24 0.216 0.214 U
0.313 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 19:46 1
0.0720 1.00 0.162 0.112 1.13 Radium 226 pCi/g 09/04/13 12:59 09/25/13 19:46 1
0.109 0.203 0.162 1.19 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 19:46 1
0.943 0.750 0.739 1.22 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 19:46 1
0.260 0.155 0.154 U
0.162 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 19:46 1
0.109 0.0651 0.0650 U
0.0238 Americium 241 pCi/g 09/04/13 12:59 09/25/13 19:46 1
4.91 3.03 2.99 5.15 Protactinium 234m Lab Sample ID: 160-3571-20 Client Sample ID: L050162TRS00 Matrix: Solid Date Collected: 08/28/13 11:10 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.13 (2+/-)
0.184 (2+/-)
1 09/25/13 21:23 09/04/13 12:59 pCi/g 0.0748 RL MDC 0.143 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 12:59 09/25/13 21:23 1
0.412 0.461 0.440 1.32 Bismuth 212 pCi/g 09/04/13 12:59 09/25/13 21:23 1
0.0850 0.157 0.120 0.969 Bismuth 214 pCi/g 09/04/13 12:59 09/25/13 21:23 1
0.0644 0.160 0.0789 1.07 Lead 212 pCi/g 09/04/13 12:59 09/25/13 21:23 1
0.0880 0.159 0.0961 1.22 Lead 214 pCi/g 09/04/13 12:59 09/25/13 21:23 1
0.273 2.41 1.31 19.8 Potassium 40 pCi/g 09/04/13 12:59 09/25/13 21:23 1
1.15 0.222 0.220 U
0.281 Protactinium 231 pCi/g 09/04/13 12:59 09/25/13 21:23 1
0.0850 1.00 0.157 0.120 0.969 Radium 226 pCi/g 09/04/13 12:59 09/25/13 21:23 1
0.0748 0.184 0.143 1.13 Thorium 232 pCi/g 09/04/13 12:59 09/25/13 21:23 1
0.977 0.397 0.377 1.19 Thorium 234 pCi/g 09/04/13 12:59 09/25/13 21:23 1
0.182 0.118 0.117 U
0.153 Uranium 235 pCi/g 09/04/13 12:59 09/25/13 21:23 1
0.112 0.134 0.134 U
-0.0213 Americium 241 pCi/g 09/04/13 12:59 09/25/13 21:23 1
5.70 4.04 4.01 U
4.85 Protactinium 234m Lab Sample ID: 160-3571-21 Client Sample ID: L050163TES00 Matrix: Solid Date Collected: 08/28/13 14:00 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.11 (2+/-)
0.176 (2+/-)
1 09/25/13 03:56 09/04/13 14:28 pCi/g 0.105 RL MDC 0.135 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.436 0.487 0.466 1.36 Bismuth 212 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.0682 0.129 0.0951 0.834 Bismuth 214 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.0812 0.148 0.0770 0.973 Lead 212 TestAmerica St. Louis Page 20 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-21 Client Sample ID: L050163TES00 Matrix: Solid Date Collected: 08/28/13 14:00 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 0.979 (2+/-)
0.133 (2+/-)
1 09/25/13 03:56 09/04/13 14:28 pCi/g 0.0790 RL MDC 0.0862 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.322 2.24 1.13 18.9 Potassium 40 pCi/g 09/04/13 14:28 09/25/13 03:56 1
1.15 0.251 0.247 U
0.440 Protactinium 231 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.0682 1.00 0.129 0.0951 0.834 Radium 226 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.105 0.176 0.135 1.11 Thorium 232 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.855 0.717 0.697 1.62 Thorium 234 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.254 0.146 0.146 U
0.0766 Uranium 235 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.108 0.0648 0.0647 U
0.0316 Americium 241 pCi/g 09/04/13 14:28 09/25/13 03:56 1
5.46 3.11 3.11 U
0.420 Protactinium 234m Lab Sample ID: 160-3571-22 Client Sample ID: L050164TRS00 Matrix: Solid Date Collected: 08/28/13 10:55 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.17 (2+/-)
0.210 (2+/-)
1 09/25/13 03:56 09/04/13 14:28 pCi/g 0.0972 RL MDC 0.173 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.387 0.446 0.427 1.24 Bismuth 212 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.0654 0.146 0.105 0.981 Bismuth 214 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.0584 0.156 0.0752 1.06 Lead 212 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.0786 0.149 0.100 1.06 Lead 214 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.258 2.39 1.27 19.8 Potassium 40 pCi/g 09/04/13 14:28 09/25/13 03:56 1
1.25 0.414 0.406 U
0.745 Protactinium 231 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.0654 1.00 0.146 0.105 0.981 Radium 226 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.0972 0.210 0.173 1.17 Thorium 232 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.849 0.620 0.613 0.886 Thorium 234 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.181 0.121 0.120 U
0.176 Uranium 235 pCi/g 09/04/13 14:28 09/25/13 03:56 1
0.105 0.153 0.153 U
-0.00292 Americium 241 pCi/g 09/04/13 14:28 09/25/13 03:56 1
6.65 2.87 2.85 U
3.57 Protactinium 234m Lab Sample ID: 160-3571-23 Client Sample ID: L050165TEQ00 Matrix: Solid Date Collected: 08/28/13 11:05 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.11 (2+/-)
0.203 (2+/-)
1 09/25/13 03:57 09/04/13 14:28 pCi/g 0.137 RL MDC 0.168 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.441 0.516 0.491 1.54 Bismuth 212 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.0959 0.178 0.138 1.08 Bismuth 214 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.0741 0.166 0.0887 1.08 Lead 212 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.0983 0.154 0.112 1.02 Lead 214 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.334 2.44 1.46 19.1 Potassium 40 pCi/g 09/04/13 14:28 09/25/13 03:57 1
1.52 0.234 0.231 U
0.355 Protactinium 231 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.0959 1.00 0.178 0.138 1.08 Radium 226 TestAmerica St. Louis Page 21 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-23 Client Sample ID: L050165TEQ00 Matrix: Solid Date Collected: 08/28/13 11:05 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 232 1.11 (2+/-)
0.203 (2+/-)
1 09/25/13 03:57 09/04/13 14:28 pCi/g 0.137 RL MDC 0.168 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.964 0.363 0.356 U
0.704 Thorium 234 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.339 0.199 0.199 U
0.00575 Uranium 235 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.125 0.0748 0.0747 U
0.0256 Americium 241 pCi/g 09/04/13 14:28 09/25/13 03:57 1
6.13 4.24 4.20 U
5.12 Protactinium 234m Lab Sample ID: 160-3571-24 Client Sample ID: L050165TES00 Matrix: Solid Date Collected: 08/28/13 11:05 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.15 (2+/-)
0.205 (2+/-)
1 09/25/13 03:57 09/04/13 14:28 pCi/g 0.107 RL MDC 0.169 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.400 0.528 0.494 1.80 Bismuth 212 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.0514 0.152 0.102 1.09 Bismuth 214 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.0667 0.168 0.0797 1.14 Lead 212 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.0698 0.152 0.0953 1.13 Lead 214 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.324 2.29 1.21 19.0 Potassium 40 pCi/g 09/04/13 14:28 09/25/13 03:57 1
1.28 0.784 0.780 U
-0.658 Protactinium 231 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.0514 1.00 0.152 0.102 1.09 Radium 226 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.107 0.205 0.169 1.15 Thorium 232 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.920 0.720 0.706 1.37 Thorium 234 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.244 0.0926 0.0925 U
0.0417 Uranium 235 pCi/g 09/04/13 14:28 09/25/13 03:57 1
0.109 0.0648 0.0648 U
-0.00888 Americium 241 pCi/g 09/04/13 14:28 09/25/13 03:57 1
4.97 2.70 2.65 U
4.94 Protactinium 234m Lab Sample ID: 160-3571-25 Client Sample ID: L050169TSS00 Matrix: Solid Date Collected: 08/28/13 13:10 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.243 (2+/-)
0.0888 (2+/-)
1 09/25/13 08:40 09/04/13 14:28 pCi/g 0.0851 RL MDC 0.0853 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 14:28 09/25/13 08:40 1
0.118 0.192 0.184 0.528 Bismuth 212 pCi/g 09/04/13 14:28 09/25/13 08:40 1
0.0391 0.0776 0.0667 0.382 Bismuth 214 pCi/g 09/04/13 14:28 09/25/13 08:40 1
0.0358 0.0495 0.0377 0.248 Lead 212 pCi/g 09/04/13 14:28 09/25/13 08:40 1
0.0428 0.0745 0.0588 0.440 Lead 214 pCi/g 09/04/13 14:28 09/25/13 08:40 1
0.157 1.02 0.757 6.74 Potassium 40 pCi/g 09/04/13 14:28 09/25/13 08:40 1
0.634 0.294 0.293 U
0.172 Protactinium 231 pCi/g 09/04/13 14:28 09/25/13 08:40 1
0.0391 1.00 0.0776 0.0667 0.382 Radium 226 pCi/g 09/04/13 14:28 09/25/13 08:40 1
0.0851 0.0888 0.0853 0.243 Thorium 232 pCi/g 09/04/13 14:28 09/25/13 08:40 1
0.637 0.222 0.219 U
0.330 Thorium 234 pCi/g 09/04/13 14:28 09/25/13 08:40 1
0.148 0.0895 0.0892 U
0.0709 Uranium 235 pCi/g 09/04/13 14:28 09/25/13 08:40 1
0.0806 0.0472 0.0472 U
-0.00600 Americium 241 TestAmerica St. Louis Page 22 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-25 Client Sample ID: L050169TSS00 Matrix: Solid Date Collected: 08/28/13 13:10 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Protactinium 234m 0.583 U
(2+/-)
1.74 (2+/-)
1 09/25/13 08:40 09/04/13 14:28 pCi/g 4.00 RL MDC 1.74 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Lab Sample ID: 160-3571-26 Client Sample ID: L050170TRS00 Matrix: Solid Date Collected: 08/28/13 13:30 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.267 (2+/-)
0.0595 (2+/-)
1 09/25/13 08:38 09/04/13 14:28 pCi/g 0.0202 RL MDC 0.0529 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 14:28 09/25/13 08:38 1
0.107 0.163 0.154 0.495 Bismuth 212 pCi/g 09/04/13 14:28 09/25/13 08:38 1
0.0341 0.0541 0.0448 0.291 Bismuth 214 pCi/g 09/04/13 14:28 09/25/13 08:38 1
0.0265 0.0377 0.0270 0.203 Lead 212 pCi/g 09/04/13 14:28 09/25/13 08:38 1
0.0322 0.0524 0.0381 0.346 Lead 214 pCi/g 09/04/13 14:28 09/25/13 08:38 1
0.241 0.799 0.534 5.81 Potassium 40 pCi/g 09/04/13 14:28 09/25/13 08:38 1
0.509 0.0464 0.0462 U
0.0448 Protactinium 231 pCi/g 09/04/13 14:28 09/25/13 08:38 1
0.0341 1.00 0.0541 0.0448 0.291 Radium 226 pCi/g 09/04/13 14:28 09/25/13 08:38 1
0.0202 0.0595 0.0529 0.267 Thorium 232 pCi/g 09/04/13 14:28 09/25/13 08:38 1
0.438 0.140 0.135 U
0.339 Thorium 234 pCi/g 09/04/13 14:28 09/25/13 08:38 1
0.114 0.0617 0.0615 U
0.0537 Uranium 235 pCi/g 09/04/13 14:28 09/25/13 08:38 1
0.0499 0.0297 0.0297 U
-0.0117 Americium 241 pCi/g 09/04/13 14:28 09/25/13 08:38 1
2.40 1.29 1.29 U
-0.00934 Protactinium 234m Lab Sample ID: 160-3571-27 Client Sample ID: L050171TRS00 Matrix: Solid Date Collected: 08/28/13 11:00 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.26 (2+/-)
0.207 (2+/-)
1 09/25/13 08:39 09/04/13 14:28 pCi/g 0.117 RL MDC 0.162 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 14:28 09/25/13 08:39 1
0.354 0.482 0.444 1.82 Bismuth 212 pCi/g 09/04/13 14:28 09/25/13 08:39 1
0.0813 0.169 0.119 1.16 Bismuth 214 pCi/g 09/04/13 14:28 09/25/13 08:39 1
0.0848 0.164 0.0830 1.09 Lead 212 pCi/g 09/04/13 14:28 09/25/13 08:39 1
0.0897 0.174 0.118 1.23 Lead 214 pCi/g 09/04/13 14:28 09/25/13 08:39 1
0.482 2.59 1.31 21.8 Potassium 40 pCi/g 09/04/13 14:28 09/25/13 08:39 1
1.32 0.252 0.249 U
0.362 Protactinium 231 pCi/g 09/04/13 14:28 09/25/13 08:39 1
0.0813 1.00 0.169 0.119 1.16 Radium 226 pCi/g 09/04/13 14:28 09/25/13 08:39 1
0.117 0.207 0.162 1.26 Thorium 232 pCi/g 09/04/13 14:28 09/25/13 08:39 1
1.00 0.787 0.779 1.09 Thorium 234 pCi/g 09/04/13 14:28 09/25/13 08:39 1
0.162 0.136 0.136 U
0.106 Uranium 235 pCi/g 09/04/13 14:28 09/25/13 08:39 1
0.105 0.0623 0.0623 U
-0.000167 Americium 241 pCi/g 09/04/13 14:28 09/25/13 08:39 1
6.39 1.90 1.90 U
0.000 Protactinium 234m TestAmerica St. Louis Page 23 of 28 1
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Client Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3571-28 Client Sample ID: L050172TES00 Matrix: Solid Date Collected: 08/28/13 11:15 Date Received: 08/29/13 18:38 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.11 (2+/-)
0.202 (2+/-)
1 09/25/13 09:36 09/04/13 14:28 pCi/g 0.165 RL MDC 0.167 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/04/13 14:28 09/25/13 09:36 1
0.534 0.605 0.585 1.45 Bismuth 212 pCi/g 09/04/13 14:28 09/25/13 09:36 1
0.104 0.215 0.163 1.34 Bismuth 214 pCi/g 09/04/13 14:28 09/25/13 09:36 1
0.0897 0.175 0.0965 1.13 Lead 212 pCi/g 09/04/13 14:28 09/25/13 09:36 1
0.0988 0.189 0.130 1.32 Lead 214 pCi/g 09/04/13 14:28 09/25/13 09:36 1
0.221 2.83 1.64 22.5 Potassium 40 pCi/g 09/04/13 14:28 09/25/13 09:36 1
1.75 1.06 1.06 U
-0.784 Protactinium 231 pCi/g 09/04/13 14:28 09/25/13 09:36 1
0.104 1.00 0.215 0.163 1.34 Radium 226 pCi/g 09/04/13 14:28 09/25/13 09:36 1
0.165 0.202 0.167 1.11 Thorium 232 pCi/g 09/04/13 14:28 09/25/13 09:36 1
1.11 0.868 0.852 1.60 Thorium 234 pCi/g 09/04/13 14:28 09/25/13 09:36 1
0.302 0.175 0.174 U
0.152 Uranium 235 pCi/g 09/04/13 14:28 09/25/13 09:36 1
0.128 0.0759 0.0759 U
-0.00837 Americium 241 pCi/g 09/04/13 14:28 09/25/13 09:36 1
8.44 5.17 5.16 U
3.67 Protactinium 234m TestAmerica St. Louis Page 24 of 28 1
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QC Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-70595/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 74710 Prep Batch: 70595 Actinium 228 Analyte U
1 09/25/13 22:56 09/04/13 12:59 pCi/g 0.0339 MDC RL 0.0199 0.0199 (2+/-)
(2+/-)
MB 0.01255 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
09/25/13 22:56 09/04/13 12:59 pCi/g 0.160 0.0289 0.0289 U
0.0000 Bismuth 212 1
09/25/13 22:56 09/04/13 12:59 pCi/g 0.0371 0.0426 0.0426 U
-0.007046 Bismuth 214 1
09/25/13 22:56 09/04/13 12:59 pCi/g 0.0241 0.0124 0.0124 U
0.004529 Lead 212 1
09/25/13 22:56 09/04/13 12:59 pCi/g 0.0306 0.0240 0.0240 U
-0.004110 Lead 214 1
09/25/13 22:56 09/04/13 12:59 pCi/g 0.210 4.21 4.21 U
-0.1053 Potassium 40 1
09/25/13 22:56 09/04/13 12:59 pCi/g 0.370 0.00202 0.00202 U
-0.0005165 Protactinium 231 1
09/25/13 22:56 09/04/13 12:59 pCi/g 0.0371 1.00 0.0426 0.0426 U
-0.007046 Radium 226 1
09/25/13 22:56 09/04/13 12:59 pCi/g 0.0339 0.0199 0.0199 U
0.01255 Thorium 232 1
09/25/13 22:56 09/04/13 12:59 pCi/g 0.250 0.262 0.262 U
-0.05987 Thorium 234 1
09/25/13 22:56 09/04/13 12:59 pCi/g 0.0591 0.0348 0.0348 U
0.006726 Uranium 235 1
09/25/13 22:56 09/04/13 12:59 pCi/g 0.0206 0.0122 0.0122 U
0.007224 Americium 241 1
09/25/13 22:56 09/04/13 12:59 pCi/g 1.29 0.592 0.592 U
0.01125 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-70595/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 74703 Prep Batch: 70595 Americium 241 Analyte 116 87 98 96.22 97.7 10.0 0.556 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 31.6 31.68 3.33 0.168 pCi/g 100 87 - 120 Cobalt 60 24.5 24.76 2.51 0.101 pCi/g 101 87 - 115 Client Sample ID: L050162TRS00 Lab Sample ID: 160-3571-20 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 74744 Prep Batch: 70595 Actinium 228 Analyte 1
0.09 1.163 1.13 0.206 0.146 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 1.32 1.570 0.484 0.334 pCi/g 0.27 1
Bismuth 214 0.969 1.019 0.163 0.0807 pCi/g 0.16 1
Lead 212 1.07 1.105 0.167 0.0701 pCi/g 0.10 1
Lead 214 1.22 1.173 0.166 0.0773 pCi/g 0.15 1
Potassium 40 19.8 18.52 2.37 0.487 pCi/g 0.27 1
Protactinium 231 0.281 U
0.3655 U
0.277 1.52 pCi/g 0.17 1
Radium 226 0.969 1.019 0.163 1.00 0.0807 pCi/g 0.16 1
Thorium 232 1.13 1.163 0.206 0.146 pCi/g 0.09 1
Thorium 234 1.19 1.414 0.473 1.14 pCi/g 0.26 1
Uranium 235 0.153 U
0.1215 U
0.160 0.295 pCi/g 0.11 1
-0.0213 U
0.02173 U
0.0718 0.120 pCi/g 0.21 1
Protactinium 234m 4.85 U
2.146 U
3.99 6.77 pCi/g 0.34 1
TestAmerica St. Louis Page 25 of 28 1
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QC Sample Results TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Method Blank Lab Sample ID: MB 160-70612/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 74703 Prep Batch: 70612 Actinium 228 Analyte U
1 09/25/13 03:49 09/04/13 14:28 pCi/g 0.0952 MDC RL 0.00987 0.00986 (2+/-)
(2+/-)
MB 0.004445 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
09/25/13 03:49 09/04/13 14:28 pCi/g 0.332 0.186 0.186 U
-0.06747 Bismuth 212 1
09/25/13 03:49 09/04/13 14:28 pCi/g 0.0291 0.0235 0.0234 U
0.02140 Bismuth 214 1
09/25/13 03:49 09/04/13 14:28 pCi/g 0.0280 0.0215 0.0215 U
-0.001932 Lead 212 1
09/25/13 03:49 09/04/13 14:28 pCi/g 0.0302 0.292 0.292 U
-0.007306 Lead 214 1
09/25/13 03:49 09/04/13 14:28 pCi/g 0.174 0.0473 0.0473 U
0.0000 Potassium 40 1
09/25/13 03:49 09/04/13 14:28 pCi/g 0.339 0.146 0.146 U
0.08279 Protactinium 231 1
09/25/13 03:49 09/04/13 14:28 pCi/g 0.0291 1.00 0.0235 0.0234 U
0.02140 Radium 226 1
09/25/13 03:49 09/04/13 14:28 pCi/g 0.0952 0.00987 0.00986 U
0.004445 Thorium 232 1
09/25/13 03:49 09/04/13 14:28 pCi/g 0.285 0.0573 0.0572 U
0.03776 Thorium 234 1
09/25/13 03:49 09/04/13 14:28 pCi/g 0.0677 0.0284 0.0284 U
0.01283 Uranium 235 1
09/25/13 03:49 09/04/13 14:28 pCi/g 0.0208 0.0117 0.0117 U
0.004500 Americium 241 1
09/25/13 03:49 09/04/13 14:28 pCi/g 1.56 0.811 0.809 U
0.5413 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-70612/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 74707 Prep Batch: 70612 Americium 241 Analyte 116 87 95 92.60 97.7 9.63 0.458 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 31.6 30.41 3.18 0.131 pCi/g 96 87 - 120 Cobalt 60 24.5 22.88 2.31 0.0618 pCi/g 93 87 - 115 Client Sample ID: Duplicate Lab Sample ID: 160-3570-A-8-G DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 74707 Prep Batch: 70612 Actinium 228 Analyte 1
0.21 0.7913 0.851 0.130 0.103 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 1.21 1.043 0.334 0.289 pCi/g 0.23 1
Bismuth 214 0.752 0.8573 0.125 0.0571 pCi/g 0.41 1
Lead 212 0.750 0.7399 0.112 0.0487 pCi/g 0.05 1
Lead 214 0.938 0.8971 0.124 0.0540 pCi/g 0.16 1
Potassium 40 13.5 15.53 1.86 0.270 pCi/g 0.55 1
Protactinium 231 0.196 U
0.3272 U
0.226 0.963 pCi/g 0.22 1
Radium 226 0.752 0.8573 0.125 1.00 0.0571 pCi/g 0.41 1
Thorium 232 0.851 0.7913 0.130 0.103 pCi/g 0.21 1
Thorium 234 2.02 2.480 0.720 0.796 pCi/g 0.28 1
Uranium 235 0.433 0.4744 0.150 0.162 pCi/g 0.13 1
-0.00073 4
U
-0.00114 3
U 0.0607 0.102 pCi/g 0
1 Protactinium 234m 1.99 U
0.4194 U
1.11 5.08 pCi/g 0.41 1
TestAmerica St. Louis Page 26 of 28 1
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QC Association Summary TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Rad Leach Batch: 69978 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3570-A-8-G DU Duplicate Total/NA Leach Batch: 69988 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3571-1 L050119TSQ00 Total/NA Solid Dry and Grind 160-3571-2 L050119TSS00 Total/NA Solid Dry and Grind 160-3571-3 L050120TRS00 Total/NA Solid Dry and Grind 160-3571-4 L050121TSS00 Total/NA Solid Dry and Grind 160-3571-5 L050122TRS00 Total/NA Solid Dry and Grind 160-3571-6 L050125TRS00 Total/NA Solid Dry and Grind 160-3571-7 L050127TRS00 Total/NA Solid Dry and Grind 160-3571-8 L050128TES00 Total/NA Solid Dry and Grind 160-3571-9 L050131TRS00 Total/NA Solid Dry and Grind 160-3571-10 L050132TES00 Total/NA Solid Dry and Grind 160-3571-11 L050133TRS00 Total/NA Solid Dry and Grind 160-3571-12 L050139TES00 Total/NA Solid Dry and Grind 160-3571-13 L050140TRS00 Total/NA Solid Dry and Grind 160-3571-14 L050148TRS00 Total/NA Solid Dry and Grind 160-3571-15 L050154TRS00 Total/NA Solid Dry and Grind 160-3571-16 L050155TES00 Total/NA Solid Dry and Grind 160-3571-17 L050156TRS00 Total/NA Solid Dry and Grind 160-3571-18 L050157TES00 Total/NA Solid Dry and Grind 160-3571-19 L050162TRQ00 Total/NA Solid Dry and Grind 160-3571-20 L050162TRS00 Total/NA Solid Dry and Grind 160-3571-20 DU L050162TRS00 Total/NA Solid Dry and Grind 160-3571-21 L050163TES00 Total/NA Solid Dry and Grind 160-3571-22 L050164TRS00 Total/NA Solid Dry and Grind 160-3571-23 L050165TEQ00 Total/NA Solid Dry and Grind 160-3571-24 L050165TES00 Total/NA Solid Dry and Grind 160-3571-25 L050169TSS00 Total/NA Solid Dry and Grind 160-3571-26 L050170TRS00 Total/NA Solid Dry and Grind 160-3571-27 L050171TRS00 Total/NA Solid Dry and Grind 160-3571-28 L050172TES00 Total/NA Prep Batch: 70595 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 69988 160-3571-1 L050119TSQ00 Total/NA Solid Fill_Geo-21 69988 160-3571-2 L050119TSS00 Total/NA Solid Fill_Geo-21 69988 160-3571-3 L050120TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-4 L050121TSS00 Total/NA Solid Fill_Geo-21 69988 160-3571-5 L050122TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-6 L050125TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-7 L050127TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-8 L050128TES00 Total/NA Solid Fill_Geo-21 69988 160-3571-9 L050131TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-10 L050132TES00 Total/NA Solid Fill_Geo-21 69988 160-3571-11 L050133TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-12 L050139TES00 Total/NA Solid Fill_Geo-21 69988 160-3571-13 L050140TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-14 L050148TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-15 L050154TRS00 Total/NA TestAmerica St. Louis Page 27 of 28 1
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QC Association Summary TestAmerica Job ID: 160-3571-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Rad (Continued)
Prep Batch: 70595 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 69988 160-3571-16 L050155TES00 Total/NA Solid Fill_Geo-21 69988 160-3571-17 L050156TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-18 L050157TES00 Total/NA Solid Fill_Geo-21 69988 160-3571-19 L050162TRQ00 Total/NA Solid Fill_Geo-21 69988 160-3571-20 L050162TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-20 DU L050162TRS00 Total/NA Solid Fill_Geo-21 LCS 160-70595/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-70595/1-A Method Blank Total/NA Prep Batch: 70612 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 69978 160-3570-A-8-G DU Duplicate Total/NA Solid Fill_Geo-21 69988 160-3571-21 L050163TES00 Total/NA Solid Fill_Geo-21 69988 160-3571-22 L050164TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-23 L050165TEQ00 Total/NA Solid Fill_Geo-21 69988 160-3571-24 L050165TES00 Total/NA Solid Fill_Geo-21 69988 160-3571-25 L050169TSS00 Total/NA Solid Fill_Geo-21 69988 160-3571-26 L050170TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-27 L050171TRS00 Total/NA Solid Fill_Geo-21 69988 160-3571-28 L050172TES00 Total/NA Solid Fill_Geo-21 LCS 160-70612/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-70612/1-A Method Blank Total/NA TestAmerica St. Louis Page 28 of 28 1
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