ML18019A671
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3435-1 Client Project/Site: RFP-CBA-022 (7 DAY TAT)
Revision: 1 For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:
8/28/2013 6:04:59 PM Ivan Vania, Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-3435-1 Page 2 of 48 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
6 Receipt Checklists.........................................
9 Definitions/Glossary.......................................
10 Method Summary.........................................
11 Sample Summary.........................................
12 Client Sample Results......................................
13 QC Sample Results........................................
37 QC Association Summary...................................
43 Tracer Carrier Summary....................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3435-1 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3435-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)
Report Number: 160-3435 Revision 1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client. This revision contains revised data for the following samples. Sample 160-3435-26 was initially counted for gamma spec analysis on a detector that was not calibrated for the geometry used. The sample was recounted on a correctly calibrated detector and the recount results are reported in this revision.
Samples 160-3435-13 and 160-3435-19 were processed against an incorrect calibration. The data was reprocessed using the correct calibration and the reprocessed results are reported in this revision.
RECEIPT The samples were received on 08/20/2013; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 22.0º C and 22.0º C.
TECHNETIUM-99 (ICPMS)
Samples L050190TUB00 (160-3435-1), L050191TUB00 (160-3435-2), L050192TUB00 (160-3435-3), L050193TUB00 (160-3435-4),
L050194TUB00 (160-3435-5), L050195TUB00 (160-3435-6), L050196TUB00 (160-3435-7), L050197TUB00 (160-3435-8),
L050247PRS00 (160-3435-9), L050248PES00 (160-3435-10), L050249PRS00 (160-3435-11), L050250PES00 (160-3435-12),
L050251PRS00 (160-3435-13), L050252PES00 (160-3435-14), L050253PES00 (160-3435-15), L050254PES00 (160-3435-16),
L050255PES00 (160-3435-17), L050256PRS00 (160-3435-18), L050257PES00 (160-3435-19), L050258PES00 (160-3435-20),
L050259PRQ00 (160-3435-21), L050259PRS00 (160-3435-22), L050260PES00 (160-3435-23), L050261PRS00 (160-3435-24),
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3435-1 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3435-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
L050262PES00 (160-3435-25), L050263PES00 (160-3435-26), L050264PRS00 (160-3435-27), L050265PES00 (160-3435-28),
L050266PUB00 (160-3435-29), L050267PUB00 (160-3435-30) and L050268PUB00 (160-3435-31) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 08/22/2013 and analyzed on 08/23/2013.
No difficulties were encountered during the Tc-99 analysis. All quality control parameters were within the acceptance limits.
PERCENT SOLIDS Samples L050190TUB00 (160-3435-1), L050191TUB00 (160-3435-2), L050192TUB00 (160-3435-3), L050193TUB00 (160-3435-4),
L050194TUB00 (160-3435-5), L050195TUB00 (160-3435-6), L050196TUB00 (160-3435-7), L050197TUB00 (160-3435-8),
L050247PRS00 (160-3435-9), L050248PES00 (160-3435-10), L050249PRS00 (160-3435-11), L050250PES00 (160-3435-12),
L050251PRS00 (160-3435-13), L050252PES00 (160-3435-14), L050253PES00 (160-3435-15), L050254PES00 (160-3435-16),
L050255PES00 (160-3435-17), L050256PRS00 (160-3435-18), L050257PES00 (160-3435-19), L050258PES00 (160-3435-20),
L050259PRQ00 (160-3435-21), L050259PRS00 (160-3435-22), L050260PES00 (160-3435-23), L050261PRS00 (160-3435-24),
L050262PES00 (160-3435-25), L050263PES00 (160-3435-26), L050264PRS00 (160-3435-27), L050265PES00 (160-3435-28),
L050266PUB00 (160-3435-29), L050267PUB00 (160-3435-30) and L050268PUB00 (160-3435-31) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 08/22/2013.
No difficulties were encountered during the % solids analysis. All quality control parameters were within the acceptance limits.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L050190TUB00 (160-3435-1), L050191TUB00 (160-3435-2), L050192TUB00 (160-3435-3), L050193TUB00 (160-3435-4),
L050194TUB00 (160-3435-5), L050195TUB00 (160-3435-6), L050196TUB00 (160-3435-7), L050197TUB00 (160-3435-8),
L050247PRS00 (160-3435-9), L050248PES00 (160-3435-10), L050249PRS00 (160-3435-11), L050250PES00 (160-3435-12),
L050251PRS00 (160-3435-13), L050252PES00 (160-3435-14), L050253PES00 (160-3435-15), L050254PES00 (160-3435-16),
L050255PES00 (160-3435-17), L050256PRS00 (160-3435-18), L050257PES00 (160-3435-19), L050258PES00 (160-3435-20),
L050259PRQ00 (160-3435-21), L050259PRS00 (160-3435-22), L050260PES00 (160-3435-23), L050261PRS00 (160-3435-24),
L050262PES00 (160-3435-25), L050263PES00 (160-3435-26), L050264PRS00 (160-3435-27), L050265PES00 (160-3435-28),
L050266PUB00 (160-3435-29), L050267PUB00 (160-3435-30) and L050268PUB00 (160-3435-31) were analyzed for Cesium-137 &
Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 08/21/2013, prepared on 08/23/2013 and analyzed on 08/23/2013, 08/25/2013, and 08/28/2013.
Preparation Batch 68361:
Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of Bismuth-214.
Because the samples have not had a 21-day ingrowth, the activity for Radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between Radium-226 and Bismuth-214 by the loss of Radon-222 during sample preparation. (160-3435-31 DU), (LCS 160-68361/2-A), (MB 160-68361/1-A), L050259PRQ00 (160-3435-21), L050259PRS00 (160-3435-22), L050260PES00 (160-3435-23), L050261PRS00 (160-3435-24), L050262PES00 (160-3435-25), L050263PES00 (160-3435-26), L050264PRS00 (160-3435-27), L050265PES00 (160-3435-28), L050266PUB00 (160-3435-29), L050267PUB00 (160-3435-30), L050268PUB00 (160-3435-31)
Lead-214 analyzed by gamma spectroscopy was detected above the MDC in the method blank. Variations in Compton backgrounds and statistical analyses allow for small area counts in the ROIs of this nuclide. Other Uranium decay chain products are not present in the blank to support Lead-214 identification. The data is reported. (160-3435-31 DU), (LCS 160-68361/2-A), (MB 160-68361/1-A),
L050259PRQ00 (160-3435-21), L050259PRS00 (160-3435-22), L050260PES00 (160-3435-23), L050261PRS00 (160-3435-24),
L050262PES00 (160-3435-25), L050263PES00 (160-3435-26), L050264PRS00 (160-3435-27), L050265PES00 (160-3435-28),
L050266PUB00 (160-3435-29), L050267PUB00 (160-3435-30), L050268PUB00 (160-3435-31)
The reporting limit for Thorium-234 was not met due to insufficient sample weight available for analysis. Analytical results are reported with the MDC achieved. L050259PRQ00 (160-3435-21), L050259PRS00 (160-3435-22), L050261PRS00 (160-3435-24), L050263PES00 (160-3435-26), L050264PRS00 (160-3435-27), L050265PES00 (160-3435-28)
Preparation Batch 68149:
Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of Bismuth-214.
Because the samples have not had a 21-day ingrowth, the activity for Radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between Radium-226 and Bismuth-214 by the loss of Radon-222 during sample preparation. (160-3435-1 DU), (LCS 160-68149/2-A), (MB 160-68149/1-A), L050190TUB00 (160-3435-1), L050191TUB00 (160-3435-2),
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3435-1 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3435-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
L050192TUB00 (160-3435-3), L050193TUB00 (160-3435-4), L050194TUB00 (160-3435-5), L050195TUB00 (160-3435-6),
L050196TUB00 (160-3435-7), L050197TUB00 (160-3435-8), L050247PRS00 (160-3435-9), L050248PES00 (160-3435-10),
L050249PRS00 (160-3435-11), L050250PES00 (160-3435-12), L050251PRS00 (160-3435-13), L050252PES00 (160-3435-14),
L050253PES00 (160-3435-15), L050254PES00 (160-3435-16), L050255PES00 (160-3435-17), L050256PRS00 (160-3435-18),
L050257PES00 (160-3435-19), L050258PES00 (160-3435-20)
The reporting limit for Thorium-234 was not met due to insufficient sample weight available for analysis. Analytical results are reported with the MDC achieved. L050251PRS00 (160-3435-13), L050253PES00 (160-3435-15), L050254PES00 (160-3435-16), L050257PES00 (160-3435-19)
No other difficulties were encountered during the Gamma spec analysis. All other quality control parameters were within the acceptance limits.
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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I
Page I of!
Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HOP.
Chain of Cutodv ID No.
F-082013-01 Pal!e 1/1
. Requested Analysis Laboratorv Na.me:
Project Name:
- -.: G' TA-MO Westinghouse Electric Company N
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Contact Person:
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Laboratory Address:
Gerald Rood
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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I
Page 1 ofl Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization., a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutodv ID No.
F-081913-01 Pa2e 1/2 Reauested Analvsis Laboratorv Name:
Project Name:
TA-MO
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Contact Person:
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Laboratory Address:
Gerald Rood
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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I
Page I of l Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutodv ID No.
F-081913-01 Pa2e 2/2 Requested Analvsis Laboratorv Name:
Project Name:
>*c.c TA-MO I
'° N
Westinghouse Electric Company N
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Contact Person:
1, Laboratory Address:
Gerald Rood
<-8 13715 Rider Trail North
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bl) 314-810-3382
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Scott Jenkins
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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3435-1 Login Number: 3435 Question Answer Comment Creator: Daniels, Brian J List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
False Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Qualifiers Metals Qualifier Description J
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier Rad Qualifier Description U
Indicates the analyte was analyzed for but not detected.
Qualifier F
Duplicate RPD exceeds the control limit Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 11 of 48 1
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Sample Summary TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-3435-1 L050190TUB00 Solid 08/19/13 13:45 08/20/13 16:06 160-3435-2 L050191TUB00 Solid 08/19/13 13:55 08/20/13 16:06 160-3435-3 L050192TUB00 Solid 08/19/13 14:05 08/20/13 16:06 160-3435-4 L050193TUB00 Solid 08/19/13 14:15 08/20/13 16:06 160-3435-5 L050194TUB00 Solid 08/19/13 14:25 08/20/13 16:06 160-3435-6 L050195TUB00 Solid 08/19/13 14:35 08/20/13 16:06 160-3435-7 L050196TUB00 Solid 08/19/13 14:45 08/20/13 16:06 160-3435-8 L050197TUB00 Solid 08/19/13 14:55 08/20/13 16:06 160-3435-9 L050247PRS00 Solid 08/16/13 15:40 08/20/13 16:06 160-3435-10 L050248PES00 Solid 08/16/13 15:55 08/20/13 16:06 160-3435-11 L050249PRS00 Solid 08/16/13 14:15 08/20/13 16:06 160-3435-12 L050250PES00 Solid 08/16/13 14:25 08/20/13 16:06 160-3435-13 L050251PRS00 Solid 08/19/13 08:35 08/20/13 16:06 160-3435-14 L050252PES00 Solid 08/19/13 10:15 08/20/13 16:06 160-3435-15 L050253PES00 Solid 08/19/13 08:45 08/20/13 16:06 160-3435-16 L050254PES00 Solid 08/19/13 08:40 08/20/13 16:06 160-3435-17 L050255PES00 Solid 08/16/13 13:50 08/20/13 16:06 160-3435-18 L050256PRS00 Solid 08/19/13 08:55 08/20/13 16:06 160-3435-19 L050257PES00 Solid 08/19/13 10:20 08/20/13 16:06 160-3435-20 L050258PES00 Solid 08/16/13 13:40 08/20/13 16:06 160-3435-21 L050259PRQ00 Solid 08/19/13 15:20 08/20/13 16:06 160-3435-22 L050259PRS00 Solid 08/16/13 15:20 08/20/13 16:06 160-3435-23 L050260PES00 Solid 08/16/13 15:30 08/20/13 16:06 160-3435-24 L050261PRS00 Solid 08/16/13 09:05 08/20/13 16:06 160-3435-25 L050262PES00 Solid 08/19/13 10:30 08/20/13 16:06 160-3435-26 L050263PES00 Solid 08/19/13 13:30 08/20/13 16:06 160-3435-27 L050264PRS00 Solid 08/16/13 14:50 08/20/13 16:06 160-3435-28 L050265PES00 Solid 08/16/13 15:00 08/20/13 16:06 160-3435-29 L050266PUB00 Solid 08/16/13 11:50 08/20/13 16:06 160-3435-30 L050267PUB00 Solid 08/16/13 11:55 08/20/13 16:06 160-3435-31 L050268PUB00 Solid 08/16/13 12:00 08/20/13 16:06 TestAmerica St. Louis Page 12 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-1 Client Sample ID: L050190TUB00 Matrix: Solid Date Collected: 08/19/13 13:45 Percent Solids: 77.9 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00071 0.000021 mg/Kg
08/22/13 08:34 08/23/13 17:48 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.234 U
(2+/-)
0.0869 (2+/-)
1 08/23/13 17:48 08/22/13 08:34 pCi/g 0.244 1.43 RL MDC 0.0756 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 17:48 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.932 (2+/-)
0.150 (2+/-)
1 08/23/13 16:19 08/23/13 09:35 pCi/g 0.112 RL MDC 0.116 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 16:19 1
0.103 0.0616 0.0615 U
-0.0189 Americium 241 pCi/g 08/23/13 09:35 08/23/13 16:19 1
0.307 0.422 0.394 1.48 Bismuth 212 pCi/g 08/23/13 09:35 08/23/13 16:19 1
0.0691 0.124 0.0968 0.752 Bismuth 214 pCi/g 08/23/13 09:35 08/23/13 16:19 1
0.0574 0.139 0.0696 0.931 Lead 212 pCi/g 08/23/13 09:35 08/23/13 16:19 1
0.0725 0.121 0.0845 0.832 Lead 214 pCi/g 08/23/13 09:35 08/23/13 16:19 1
0.373 2.03 1.11 16.7 Potassium 40 pCi/g 08/23/13 09:35 08/23/13 16:19 1
1.00 0.311 0.306 U
0.518 Protactinium 231 pCi/g 08/23/13 09:35 08/23/13 16:19 1
0.0691 1.00 0.124 0.0968 0.752 Radium 226 pCi/g 08/23/13 09:35 08/23/13 16:19 1
0.757 1.00 0.578 0.566 1.08 Thorium 234 pCi/g 08/23/13 09:35 08/23/13 16:19 1
0.194 0.151 0.150 U
0.155 Uranium 235 pCi/g 08/23/13 09:35 08/23/13 16:19 1
5.44 2.07 2.02 U
4.37 Protactinium 234m pCi/g 08/23/13 09:35 08/23/13 16:19 1
0.112 0.150 0.116 0.932 Thorium 232 Tl-208 0.299 0.0438 0.0537 0.0325 pCi/g 08/23/13 09:35 08/23/13 16:19 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-2 Client Sample ID: L050191TUB00 Matrix: Solid Date Collected: 08/19/13 13:55 Percent Solids: 78.4 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000090 J
0.00071 0.000021 mg/Kg
08/22/13 08:34 08/23/13 18:00 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.54 (2+/-)
0.165 (2+/-)
1 08/23/13 18:00 08/22/13 08:34 pCi/g 0.242 1.42 RL MDC 0.0452 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:00 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 TestAmerica St. Louis Page 13 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-2 Client Sample ID: L050191TUB00 Matrix: Solid Date Collected: 08/19/13 13:55 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.842 (2+/-)
0.147 (2+/-)
1 08/23/13 16:20 08/23/13 09:35 pCi/g 0.108 RL MDC 0.119 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 16:20 1
0.106 0.0631 0.0631 U
0.0231 Americium 241 pCi/g 08/23/13 09:35 08/23/13 16:20 1
0.555 0.384 0.378 0.632 Bismuth 212 pCi/g 08/23/13 09:35 08/23/13 16:20 1
0.0819 0.130 0.109 0.690 Bismuth 214 pCi/g 08/23/13 09:35 08/23/13 16:20 1
0.0701 0.119 0.0743 0.723 Lead 212 pCi/g 08/23/13 09:35 08/23/13 16:20 1
0.0691 0.116 0.0896 0.710 Lead 214 pCi/g 08/23/13 09:35 08/23/13 16:20 1
0.197 1.75 1.17 12.7 Potassium 40 pCi/g 08/23/13 09:35 08/23/13 16:20 1
1.18 0.285 0.283 U
0.349 Protactinium 231 pCi/g 08/23/13 09:35 08/23/13 16:20 1
0.0819 1.00 0.130 0.109 0.690 Radium 226 pCi/g 08/23/13 09:35 08/23/13 16:20 1
0.923 1.00 0.372 0.355 1.05 Thorium 234 pCi/g 08/23/13 09:35 08/23/13 16:20 1
0.282 0.171 0.171 U
0.0829 Uranium 235 pCi/g 08/23/13 09:35 08/23/13 16:20 1
5.20 3.04 3.04 U
1.69 Protactinium 234m pCi/g 08/23/13 09:35 08/23/13 16:20 1
0.108 0.147 0.119 0.842 Thorium 232 Tl-208 0.250 0.0617 0.0670 0.0521 pCi/g 08/23/13 09:35 08/23/13 16:20 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-3 Client Sample ID: L050192TUB00 Matrix: Solid Date Collected: 08/19/13 14:05 Percent Solids: 74.2 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00096 0.00074 0.000022 mg/Kg
08/22/13 08:34 08/23/13 18:04 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 16.5 (2+/-)
1.77 (2+/-)
1 08/23/13 18:04 08/22/13 08:34 pCi/g 0.254 1.48 RL MDC 0.505 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:04 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.317 (2+/-)
0.0797 (2+/-)
1 08/23/13 16:31 08/23/13 09:35 pCi/g 0.0708 RL MDC 0.0728 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 16:31 1
0.0797 0.0470 0.0469 U
0.00657 Americium 241 pCi/g 08/23/13 09:35 08/23/13 16:31 1
0.315 0.217 0.214 U
0.310 Bismuth 212 pCi/g 08/23/13 09:35 08/23/13 16:31 1
0.0548 0.110 0.0851 0.664 Bismuth 214 pCi/g 08/23/13 09:35 08/23/13 16:31 1
0.0447 0.0539 0.0416 0.265 Lead 212 pCi/g 08/23/13 09:35 08/23/13 16:31 1
0.0331 0.103 0.0722 0.708 Lead 214 pCi/g 08/23/13 09:35 08/23/13 16:31 1
0.264 0.610 0.506 3.32 Potassium 40 pCi/g 08/23/13 09:35 08/23/13 16:31 1
0.854 0.150 0.149 U
0.150 Protactinium 231 pCi/g 08/23/13 09:35 08/23/13 16:31 1
0.0548 1.00 0.110 0.0851 0.664 Radium 226 TestAmerica St. Louis Page 14 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-3 Client Sample ID: L050192TUB00 Matrix: Solid Date Collected: 08/19/13 14:05 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 1.36 (2+/-)
0.329 (2+/-)
1 08/23/13 16:31 08/23/13 09:35 pCi/g 0.673 1.00 RL MDC 0.297 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 16:31 1
0.176 0.131 0.126 0.371 Uranium 235 pCi/g 08/23/13 09:35 08/23/13 16:31 1
3.91 2.14 2.08 4.94 Protactinium 234m pCi/g 08/23/13 09:35 08/23/13 16:31 1
0.0708 0.0797 0.0728 0.317 Thorium 232 Tl-208 0.103 0.0282 0.0302 0.0263 pCi/g 08/23/13 09:35 08/23/13 16:31 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-4 Client Sample ID: L050193TUB00 Matrix: Solid Date Collected: 08/19/13 14:15 Percent Solids: 75.5 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00025 J
0.00073 0.000022 mg/Kg
08/22/13 08:34 08/23/13 18:08 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 4.32 (2+/-)
0.573 (2+/-)
1 08/23/13 18:08 08/22/13 08:34 pCi/g 0.249 1.45 RL MDC 0.332 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:08 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.748 (2+/-)
0.133 (2+/-)
1 08/23/13 17:04 08/23/13 09:35 pCi/g 0.122 RL MDC 0.109 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 17:04 1
0.103 0.0623 0.0621 U
0.0416 Americium 241 pCi/g 08/23/13 09:35 08/23/13 17:04 1
0.287 0.384 0.365 1.14 Bismuth 212 pCi/g 08/23/13 09:35 08/23/13 17:04 1
0.0665 0.125 0.104 0.668 Bismuth 214 pCi/g 08/23/13 09:35 08/23/13 17:04 1
0.0625 0.119 0.0733 0.721 Lead 212 pCi/g 08/23/13 09:35 08/23/13 17:04 1
0.0865 0.117 0.0892 0.731 Lead 214 pCi/g 08/23/13 09:35 08/23/13 17:04 1
0.356 1.84 1.25 13.2 Potassium 40 pCi/g 08/23/13 09:35 08/23/13 17:04 1
1.22 0.314 0.310 U
0.455 Protactinium 231 pCi/g 08/23/13 09:35 08/23/13 17:04 1
0.0665 1.00 0.125 0.104 0.668 Radium 226 pCi/g 08/23/13 09:35 08/23/13 17:04 1
0.937 1.00 0.745 0.727 1.58 Thorium 234 pCi/g 08/23/13 09:35 08/23/13 17:04 1
0.214 0.178 0.176 0.270 Uranium 235 pCi/g 08/23/13 09:35 08/23/13 17:04 1
7.46 2.30 2.29 U
2.52 Protactinium 234m pCi/g 08/23/13 09:35 08/23/13 17:04 1
0.122 0.133 0.109 0.748 Thorium 232 Tl-208 0.243 0.0469 0.0533 0.0317 pCi/g 08/23/13 09:35 08/23/13 17:04 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-5 Client Sample ID: L050194TUB00 Matrix: Solid Date Collected: 08/19/13 14:25 Percent Solids: 69.3 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000066 J
0.00081 0.000024 mg/Kg
08/22/13 08:34 08/23/13 18:12 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.12 (2+/-)
0.193 (2+/-)
1 08/23/13 18:12 08/22/13 08:34 pCi/g 0.276 1.61 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:12 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.887 (2+/-)
0.138 (2+/-)
1 08/23/13 17:08 08/23/13 09:35 pCi/g 0.0741 RL MDC 0.104 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 17:08 1
0.0990 0.0587 0.0587 U
0.0102 Americium 241 pCi/g 08/23/13 09:35 08/23/13 17:08 1
0.217 0.330 0.307 1.17 Bismuth 212 pCi/g 08/23/13 09:35 08/23/13 17:08 1
0.0597 0.102 0.0804 0.605 Bismuth 214 pCi/g 08/23/13 09:35 08/23/13 17:08 1
0.0478 0.136 0.0670 0.914 Lead 212 pCi/g 08/23/13 09:35 08/23/13 17:08 1
0.0596 0.114 0.0819 0.759 Lead 214 pCi/g 08/23/13 09:35 08/23/13 17:08 1
0.318 1.81 1.03 14.6 Potassium 40 pCi/g 08/23/13 09:35 08/23/13 17:08 1
0.883 0.317 0.313 U
0.461 Protactinium 231 pCi/g 08/23/13 09:35 08/23/13 17:08 1
0.0597 1.00 0.102 0.0804 0.605 Radium 226 pCi/g 08/23/13 09:35 08/23/13 17:08 1
0.782 1.00 0.622 0.606 1.33 Thorium 234 pCi/g 08/23/13 09:35 08/23/13 17:08 1
0.204 0.125 0.124 U
0.113 Uranium 235 pCi/g 08/23/13 09:35 08/23/13 17:08 1
4.85 2.87 2.86 U
1.59 Protactinium 234m pCi/g 08/23/13 09:35 08/23/13 17:08 1
0.0741 0.138 0.104 0.887 Thorium 232 Tl-208 0.246 0.0412 0.0485 0.0311 pCi/g 08/23/13 09:35 08/23/13 17:08 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-6 Client Sample ID: L050195TUB00 Matrix: Solid Date Collected: 08/19/13 14:35 Percent Solids: 72.4 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00010 J
0.00077 0.000023 mg/Kg
08/22/13 08:34 08/23/13 18:16 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.77 (2+/-)
0.224 (2+/-)
1 08/23/13 18:16 08/22/13 08:34 pCi/g 0.265 1.55 RL MDC 0.118 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:16 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 TestAmerica St. Louis Page 16 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-6 Client Sample ID: L050195TUB00 Matrix: Solid Date Collected: 08/19/13 14:35 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.539 (2+/-)
0.125 (2+/-)
1 08/23/13 17:09 08/23/13 09:35 pCi/g 0.112 RL MDC 0.112 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 17:09 1
0.0862 0.0512 0.0512 U
0.0181 Americium 241 pCi/g 08/23/13 09:35 08/23/13 17:09 1
0.512 0.310 0.309 U
0.229 Bismuth 212 pCi/g 08/23/13 09:35 08/23/13 17:09 1
0.0680 0.0946 0.0838 0.421 Bismuth 214 pCi/g 08/23/13 09:35 08/23/13 17:09 1
0.0642 0.0968 0.0644 0.558 Lead 212 pCi/g 08/23/13 09:35 08/23/13 17:09 1
0.0557 0.0970 0.0780 0.554 Lead 214 pCi/g 08/23/13 09:35 08/23/13 17:09 1
0.184 1.64 1.09 11.9 Potassium 40 pCi/g 08/23/13 09:35 08/23/13 17:09 1
1.06 0.352 0.350 U
0.307 Protactinium 231 pCi/g 08/23/13 09:35 08/23/13 17:09 1
0.0680 1.00 0.0946 0.0838 0.421 Radium 226 pCi/g 08/23/13 09:35 08/23/13 17:09 1
0.821 1.00 0.674 0.666 0.972 Thorium 234 pCi/g 08/23/13 09:35 08/23/13 17:09 1
0.221 0.131 0.131 U
0.0459 Uranium 235 pCi/g 08/23/13 09:35 08/23/13 17:09 1
5.62 3.23 3.23 U
1.30 Protactinium 234m pCi/g 08/23/13 09:35 08/23/13 17:09 1
0.112 0.125 0.112 0.539 Thorium 232 Tl-208 0.209 0.0434 0.0485 0.0326 pCi/g 08/23/13 09:35 08/23/13 17:09 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-7 Client Sample ID: L050196TUB00 Matrix: Solid Date Collected: 08/19/13 14:45 Percent Solids: 80.8 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00067 0.000020 mg/Kg
08/22/13 08:34 08/23/13 18:19 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.299 (2+/-)
0.0765 (2+/-)
1 08/23/13 18:19 08/22/13 08:34 pCi/g 0.228 1.33 RL MDC 0.0651 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:19 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.600 (2+/-)
0.108 (2+/-)
1 08/23/13 17:10 08/23/13 09:35 pCi/g 0.0481 RL MDC 0.0888 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 17:10 1
0.0724 0.0424 0.0424 U
-0.000662 Americium 241 pCi/g 08/23/13 09:35 08/23/13 17:10 1
0.207 0.274 0.258 0.896 Bismuth 212 pCi/g 08/23/13 09:35 08/23/13 17:10 1
0.0613 0.0966 0.0799 0.522 Bismuth 214 pCi/g 08/23/13 09:35 08/23/13 17:10 1
0.0445 0.0860 0.0513 0.534 Lead 212 pCi/g 08/23/13 09:35 08/23/13 17:10 1
0.0538 0.0929 0.0688 0.601 Lead 214 pCi/g 08/23/13 09:35 08/23/13 17:10 1
0.302 1.68 0.962 13.4 Potassium 40 pCi/g 08/23/13 09:35 08/23/13 17:10 1
0.853 0.523 0.521 U
-0.464 Protactinium 231 pCi/g 08/23/13 09:35 08/23/13 17:10 1
0.0613 1.00 0.0966 0.0799 0.522 Radium 226 TestAmerica St. Louis Page 17 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-7 Client Sample ID: L050196TUB00 Matrix: Solid Date Collected: 08/19/13 14:45 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 0.749 (2+/-)
0.413 (2+/-)
1 08/23/13 17:10 08/23/13 09:35 pCi/g 0.594 1.00 RL MDC 0.406 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 17:10 1
0.145 0.0992 0.0988 U
0.0864 Uranium 235 pCi/g 08/23/13 09:35 08/23/13 17:10 1
3.84 2.21 2.21 U
0.857 Protactinium 234m pCi/g 08/23/13 09:35 08/23/13 17:10 1
0.0481 0.108 0.0888 0.600 Thorium 232 Tl-208 0.166 0.0360 0.0399 0.0305 pCi/g 08/23/13 09:35 08/23/13 17:10 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-8 Client Sample ID: L050197TUB00 Matrix: Solid Date Collected: 08/19/13 14:55 Percent Solids: 72.0 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00076 0.000023 mg/Kg
08/22/13 08:34 08/23/13 18:23 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.195 U
(2+/-)
0.0206 (2+/-)
1 08/23/13 18:23 08/22/13 08:34 pCi/g 0.260 1.52 RL MDC 0.00543 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:23 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.604 (2+/-)
0.150 (2+/-)
1 08/23/13 16:21 08/23/13 09:35 pCi/g 0.106 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 16:21 1
0.0957 0.112 0.112 U
-0.0126 Americium 241 pCi/g 08/23/13 09:35 08/23/13 16:21 1
0.448 0.324 0.318 0.637 Bismuth 212 pCi/g 08/23/13 09:35 08/23/13 16:21 1
0.0699 0.107 0.0918 0.570 Bismuth 214 pCi/g 08/23/13 09:35 08/23/13 16:21 1
0.0533 0.0978 0.0640 0.687 Lead 212 pCi/g 08/23/13 09:35 08/23/13 16:21 1
0.0673 0.102 0.0804 0.642 Lead 214 pCi/g 08/23/13 09:35 08/23/13 16:21 1
0.415 1.70 1.11 13.3 Potassium 40 pCi/g 08/23/13 09:35 08/23/13 16:21 1
0.796 0.412 0.411 U
0.285 Protactinium 231 pCi/g 08/23/13 09:35 08/23/13 16:21 1
0.0699 1.00 0.107 0.0918 0.570 Radium 226 pCi/g 08/23/13 09:35 08/23/13 16:21 1
0.733 1.00 0.557 0.550 0.898 Thorium 234 pCi/g 08/23/13 09:35 08/23/13 16:21 1
0.177 0.117 0.117 U
0.117 Uranium 235 pCi/g 08/23/13 09:35 08/23/13 16:21 1
5.10 2.95 2.94 U
1.22 Protactinium 234m pCi/g 08/23/13 09:35 08/23/13 16:21 1
0.106 0.150 0.138 0.604 Thorium 232 Tl-208 0.222 0.0381 0.0438 0.0285 pCi/g 08/23/13 09:35 08/23/13 16:21 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-9 Client Sample ID: L050247PRS00 Matrix: Solid Date Collected: 08/16/13 15:40 Percent Solids: 86.1 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00064 0.000019 mg/Kg
08/22/13 08:34 08/23/13 18:35 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.171 U
(2+/-)
0.111 (2+/-)
1 08/23/13 18:35 08/22/13 08:34 pCi/g 0.220 1.28 RL MDC 0.0982 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:35 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.20 (2+/-)
0.199 (2+/-)
1 08/23/13 17:11 08/23/13 09:35 pCi/g 0.141 RL MDC 0.161 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 17:11 1
0.114 0.209 0.209 U
-0.0193 Americium 241 pCi/g 08/23/13 09:35 08/23/13 17:11 1
0.425 0.549 0.523 1.73 Bismuth 212 pCi/g 08/23/13 09:35 08/23/13 17:11 1
0.0639 0.135 0.104 0.883 Bismuth 214 pCi/g 08/23/13 09:35 08/23/13 17:11 1
0.0680 0.144 0.0821 1.10 Lead 212 pCi/g 08/23/13 09:35 08/23/13 17:11 1
0.0781 0.116 0.0848 0.823 Lead 214 pCi/g 08/23/13 09:35 08/23/13 17:11 1
0.311 2.33 1.33 19.8 Potassium 40 pCi/g 08/23/13 09:35 08/23/13 17:11 1
0.966 0.574 0.574 U
0.300 Protactinium 231 pCi/g 08/23/13 09:35 08/23/13 17:11 1
0.0639 1.00 0.135 0.104 0.883 Radium 226 pCi/g 08/23/13 09:35 08/23/13 17:11 1
0.823 1.00 0.643 0.625 1.56 Thorium 234 pCi/g 08/23/13 09:35 08/23/13 17:11 1
0.221 0.151 0.148 0.331 Uranium 235 pCi/g 08/23/13 09:35 08/23/13 17:11 1
5.31 3.58 3.57 U
2.00 Protactinium 234m pCi/g 08/23/13 09:35 08/23/13 17:11 1
0.141 0.199 0.161 1.20 Thorium 232 Tl-208 0.336 0.0551 0.0640 0.0436 pCi/g 08/23/13 09:35 08/23/13 17:11 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-10 Client Sample ID: L050248PES00 Matrix: Solid Date Collected: 08/16/13 15:55 Percent Solids: 84.2 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00065 0.000019 mg/Kg
08/22/13 08:34 08/23/13 18:39 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0845 U
(2+/-)
0.0420 (2+/-)
1 08/23/13 18:39 08/22/13 08:34 pCi/g 0.222 1.30 RL MDC 0.0373 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:39 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 TestAmerica St. Louis Page 19 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-10 Client Sample ID: L050248PES00 Matrix: Solid Date Collected: 08/16/13 15:55 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.20 (2+/-)
0.203 (2+/-)
1 08/23/13 17:30 08/23/13 09:35 pCi/g 0.0852 RL MDC 0.167 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 17:30 1
0.0993 0.0596 0.0595 U
0.0359 Americium 241 pCi/g 08/23/13 09:35 08/23/13 17:30 1
0.303 0.400 0.379 1.33 Bismuth 212 pCi/g 08/23/13 09:35 08/23/13 17:30 1
0.0736 0.127 0.105 0.743 Bismuth 214 pCi/g 08/23/13 09:35 08/23/13 17:30 1
0.0693 0.148 0.0858 1.12 Lead 212 pCi/g 08/23/13 09:35 08/23/13 17:30 1
0.0853 0.127 0.0920 0.897 Lead 214 pCi/g 08/23/13 09:35 08/23/13 17:30 1
0.182 2.39 1.41 20.0 Potassium 40 pCi/g 08/23/13 09:35 08/23/13 17:30 1
1.14 0.261 0.255 U
0.543 Protactinium 231 pCi/g 08/23/13 09:35 08/23/13 17:30 1
0.0736 1.00 0.127 0.105 0.743 Radium 226 pCi/g 08/23/13 09:35 08/23/13 17:30 1
0.925 1.00 0.743 0.731 1.36 Thorium 234 pCi/g 08/23/13 09:35 08/23/13 17:30 1
0.236 0.130 0.129 U
0.100 Uranium 235 pCi/g 08/23/13 09:35 08/23/13 17:30 1
6.46 3.54 3.52 U
3.58 Protactinium 234m pCi/g 08/23/13 09:35 08/23/13 17:30 1
0.0852 0.203 0.167 1.20 Thorium 232 Tl-208 0.349 0.0569 0.0663 0.0451 pCi/g 08/23/13 09:35 08/23/13 17:30 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-11 Client Sample ID: L050249PRS00 Matrix: Solid Date Collected: 08/16/13 14:15 Percent Solids: 82.6 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00066 0.000020 mg/Kg
08/22/13 08:34 08/23/13 18:43 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0977 U
(2+/-)
0.119 (2+/-)
1 08/23/13 18:43 08/22/13 08:34 pCi/g 0.226 1.32 RL MDC 0.110 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:43 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.14 (2+/-)
0.174 (2+/-)
1 08/25/13 20:56 08/23/13 09:35 pCi/g 0.104 RL MDC 0.134 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/25/13 20:56 1
0.109 0.0657 0.0656 U
-0.0433 Americium 241 pCi/g 08/23/13 09:35 08/25/13 20:56 1
0.398 0.444 0.423 1.37 Bismuth 212 pCi/g 08/23/13 09:35 08/25/13 20:56 1
0.0617 0.133 0.102 0.885 Bismuth 214 pCi/g 08/23/13 09:35 08/25/13 20:56 1
0.0648 0.140 0.0793 1.07 Lead 212 pCi/g 08/23/13 09:35 08/25/13 20:56 1
0.0732 0.137 0.100 0.969 Lead 214 pCi/g 08/23/13 09:35 08/25/13 20:56 1
0.289 2.32 1.28 20.0 Potassium 40 pCi/g 08/23/13 09:35 08/25/13 20:56 1
1.24 0.183 0.181 U
0.314 Protactinium 231 pCi/g 08/23/13 09:35 08/25/13 20:56 1
0.0617 1.00 0.133 0.102 0.885 Radium 226 TestAmerica St. Louis Page 20 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-11 Client Sample ID: L050249PRS00 Matrix: Solid Date Collected: 08/16/13 14:15 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 1.32 (2+/-)
0.588 (2+/-)
1 08/25/13 20:56 08/23/13 09:35 pCi/g 0.800 1.00 RL MDC 0.574 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/25/13 20:56 1
0.251 0.158 0.158 U
0.124 Uranium 235 pCi/g 08/23/13 09:35 08/25/13 20:56 1
5.21 3.63 3.62 U
1.72 Protactinium 234m pCi/g 08/23/13 09:35 08/25/13 20:56 1
0.104 0.174 0.134 1.14 Thorium 232 Tl-208 0.310 0.0516 0.0598 0.0414 pCi/g 08/23/13 09:35 08/25/13 20:56 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-12 Client Sample ID: L050250PES00 Matrix: Solid Date Collected: 08/16/13 14:25 Percent Solids: 83.1 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00066 0.000020 mg/Kg
08/22/13 08:34 08/23/13 18:46 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0562 U
(2+/-)
0.0577 (2+/-)
1 08/23/13 18:46 08/22/13 08:34 pCi/g 0.226 1.32 RL MDC 0.0525 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:46 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.15 (2+/-)
0.179 (2+/-)
1 08/25/13 21:32 08/23/13 09:35 pCi/g 0.107 RL MDC 0.135 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/25/13 21:32 1
0.116 0.0689 0.0689 U
0.00416 Americium 241 pCi/g 08/23/13 09:35 08/25/13 21:32 1
0.425 0.438 0.419 1.22 Bismuth 212 pCi/g 08/23/13 09:35 08/25/13 21:32 1
0.0739 0.145 0.107 0.940 Bismuth 214 pCi/g 08/23/13 09:35 08/25/13 21:32 1
0.0638 0.168 0.0787 1.15 Lead 212 pCi/g 08/23/13 09:35 08/25/13 21:32 1
0.0770 0.138 0.0902 1.00 Lead 214 pCi/g 08/23/13 09:35 08/25/13 21:32 1
0.325 2.51 1.25 21.2 Potassium 40 pCi/g 08/23/13 09:35 08/25/13 21:32 1
1.14 0.259 0.255 U
0.434 Protactinium 231 pCi/g 08/23/13 09:35 08/25/13 21:32 1
0.0739 1.00 0.145 0.107 0.940 Radium 226 pCi/g 08/23/13 09:35 08/25/13 21:32 1
0.807 1.00 0.331 0.312 1.05 Thorium 234 pCi/g 08/23/13 09:35 08/25/13 21:32 1
0.251 0.146 0.146 U
0.113 Uranium 235 pCi/g 08/23/13 09:35 08/25/13 21:32 1
5.33 3.25 3.24 U
2.62 Protactinium 234m pCi/g 08/23/13 09:35 08/25/13 21:32 1
0.107 0.179 0.135 1.15 Thorium 232 Tl-208 0.370 0.0483 0.0617 0.0356 pCi/g 08/23/13 09:35 08/25/13 21:32 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-13 Client Sample ID: L050251PRS00 Matrix: Solid Date Collected: 08/19/13 08:35 Percent Solids: 84.9 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00067 0.000020 mg/Kg
08/22/13 08:34 08/23/13 18:50 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0536 U
(2+/-)
0.0761 (2+/-)
1 08/23/13 18:50 08/22/13 08:34 pCi/g 0.228 1.33 RL MDC 0.0671 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:50 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.26 (2+/-)
0.212 (2+/-)
1 08/25/13 21:33 08/23/13 09:35 pCi/g 0.132 RL MDC 0.174 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.119 0.0704 0.0704 U
0.00396 Americium 241 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.438 0.545 0.523 1.56 Bismuth 212 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0747 0.165 0.119 1.17 Bismuth 214 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0901 0.148 0.0885 1.11 Lead 212 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0922 0.161 0.107 1.24 Lead 214 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.386 2.83 1.45 25.3 Potassium 40 pCi/g 08/23/13 09:35 08/25/13 21:33 1
1.33 0.316 0.314 U
0.379 Protactinium 231 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0747 1.00 0.165 0.119 1.17 Radium 226 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.973 1.00 0.356 0.348 U
0.751 Thorium 234 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.286 0.154 0.153 U
0.102 Uranium 235 pCi/g 08/23/13 09:35 08/25/13 21:33 1
6.47 2.82 2.81 U
3.14 Protactinium 234m pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.132 0.212 0.174 1.26 Thorium 232 Other Detected Radionuclide None pCi/g 08/23/13 09:35 08/25/13 21:33 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-14 Client Sample ID: L050252PES00 Matrix: Solid Date Collected: 08/19/13 10:15 Percent Solids: 83.3 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00067 0.000020 mg/Kg
08/22/13 08:34 08/23/13 18:54 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0721 U
(2+/-)
0.0559 (2+/-)
1 08/23/13 18:54 08/22/13 08:34 pCi/g 0.229 1.34 RL MDC 0.0500 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:54 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 TestAmerica St. Louis Page 22 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-14 Client Sample ID: L050252PES00 Matrix: Solid Date Collected: 08/19/13 10:15 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.17 (2+/-)
0.197 (2+/-)
1 08/25/13 21:33 08/23/13 09:35 pCi/g 0.127 RL MDC 0.161 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.115 0.0752 0.0752 U
-0.000438 Americium 241 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.610 0.414 0.409 0.661 Bismuth 212 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0948 0.173 0.139 1.05 Bismuth 214 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0878 0.165 0.0976 1.23 Lead 212 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.112 0.159 0.108 1.20 Lead 214 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.199 2.84 1.61 24.1 Potassium 40 pCi/g 08/23/13 09:35 08/25/13 21:33 1
1.43 0.329 0.322 U
0.675 Protactinium 231 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0948 1.00 0.173 0.139 1.05 Radium 226 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.973 1.00 0.383 0.370 0.985 Thorium 234 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.293 0.176 0.176 U
0.0654 Uranium 235 pCi/g 08/23/13 09:35 08/25/13 21:33 1
6.96 3.96 3.96 U
1.06 Protactinium 234m pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.127 0.197 0.161 1.17 Thorium 232 Tl-208 0.422 0.0756 0.0861 0.0603 pCi/g 08/23/13 09:35 08/25/13 21:33 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-15 Client Sample ID: L050253PES00 Matrix: Solid Date Collected: 08/19/13 08:45 Percent Solids: 81.6 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00067 0.000020 mg/Kg
08/22/13 08:34 08/23/13 18:58 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0497 U
(2+/-)
0.00972 (2+/-)
1 08/23/13 18:58 08/22/13 08:34 pCi/g 0.228 1.33 RL MDC 0.00761 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 18:58 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.44 (2+/-)
0.333 (2+/-)
1 08/23/13 16:12 08/23/13 09:35 pCi/g 0.268 RL MDC 0.299 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 16:12 1
0.287 0.586 0.586 U
-0.0513 Americium 241 pCi/g 08/23/13 09:35 08/23/13 16:12 1
1.42 0.846 0.844 U
0.540 Bismuth 212 pCi/g 08/23/13 09:35 08/23/13 16:12 1
0.215 0.252 0.238 0.790 Bismuth 214 pCi/g 08/23/13 09:35 08/23/13 16:12 1
0.149 0.248 0.185 1.28 Lead 212 pCi/g 08/23/13 09:35 08/23/13 16:12 1
0.200 0.255 0.228 1.10 Lead 214 pCi/g 08/23/13 09:35 08/23/13 16:12 1
0.653 3.41 2.69 20.5 Potassium 40 pCi/g 08/23/13 09:35 08/23/13 16:12 1
3.36 0.428 0.425 U
0.453 Protactinium 231 pCi/g 08/23/13 09:35 08/23/13 16:12 1
0.215 1.00 0.252 0.238 0.790 Radium 226 TestAmerica St. Louis Page 23 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-15 Client Sample ID: L050253PES00 Matrix: Solid Date Collected: 08/19/13 08:45 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 0.782 U
(2+/-)
0.654 (2+/-)
1 08/23/13 16:12 08/23/13 09:35 pCi/g 2.70 1.00 RL MDC 0.649 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/23/13 16:12 1
0.574 0.289 0.289 U
0.177 Uranium 235 pCi/g 08/23/13 09:35 08/23/13 16:12 1
14.0 1.66 1.66 U
-0.472 Protactinium 234m pCi/g 08/23/13 09:35 08/23/13 16:12 1
0.268 0.333 0.299 1.44 Thorium 232 Tl-208 0.459 0.104 0.114 0.0581 pCi/g 08/23/13 09:35 08/23/13 16:12 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-16 Client Sample ID: L050254PES00 Matrix: Solid Date Collected: 08/19/13 08:40 Percent Solids: 83.3 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00066 0.000020 mg/Kg
08/22/13 08:34 08/23/13 19:02 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0347 U
(2+/-)
0.0526 (2+/-)
1 08/23/13 19:02 08/22/13 08:34 pCi/g 0.227 1.32 RL MDC 0.0474 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 19:02 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.19 (2+/-)
0.229 (2+/-)
1 08/25/13 21:34 08/23/13 09:35 pCi/g 0.144 RL MDC 0.198 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/25/13 21:34 1
0.136 0.0805 0.0805 U
0.0131 Americium 241 pCi/g 08/23/13 09:35 08/25/13 21:34 1
0.794 0.516 0.512 U
0.670 Bismuth 212 pCi/g 08/23/13 09:35 08/25/13 21:34 1
0.111 0.185 0.153 1.07 Bismuth 214 pCi/g 08/23/13 09:35 08/25/13 21:34 1
0.0810 0.189 0.109 1.43 Lead 212 pCi/g 08/23/13 09:35 08/25/13 21:34 1
0.117 0.184 0.140 1.23 Lead 214 pCi/g 08/23/13 09:35 08/25/13 21:34 1
0.484 2.75 1.78 21.7 Potassium 40 pCi/g 08/23/13 09:35 08/25/13 21:34 1
1.89 0.436 0.429 U
0.807 Protactinium 231 pCi/g 08/23/13 09:35 08/25/13 21:34 1
0.111 1.00 0.185 0.153 1.07 Radium 226 pCi/g 08/23/13 09:35 08/25/13 21:34 1
1.19 1.00 0.971 0.957 1.70 Thorium 234 pCi/g 08/23/13 09:35 08/25/13 21:34 1
0.340 0.186 0.186 U
0.153 Uranium 235 pCi/g 08/23/13 09:35 08/25/13 21:34 1
8.70 2.44 2.44 U
0.000 Protactinium 234m pCi/g 08/23/13 09:35 08/25/13 21:34 1
0.144 0.229 0.198 1.19 Thorium 232 Tl-208 0.461 0.0712 0.0841 0.0526 pCi/g 08/23/13 09:35 08/25/13 21:34 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 24 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-17 Client Sample ID: L050255PES00 Matrix: Solid Date Collected: 08/16/13 13:50 Percent Solids: 82.3 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00065 0.000020 mg/Kg
08/22/13 08:34 08/23/13 19:06 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0444 U
(2+/-)
0.0102 (2+/-)
1 08/23/13 19:06 08/22/13 08:34 pCi/g 0.223 1.30 RL MDC 0.00855 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 19:06 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 93 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.38 (2+/-)
0.226 (2+/-)
1 08/25/13 21:33 08/23/13 09:35 pCi/g 0.165 RL MDC 0.182 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0948 0.0547 0.0547 U
0.0141 Americium 241 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.462 0.501 0.484 1.34 Bismuth 212 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0875 0.166 0.129 1.08 Bismuth 214 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0784 0.164 0.0910 1.27 Lead 212 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0906 0.157 0.107 1.19 Lead 214 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.311 2.82 1.50 24.7 Potassium 40 pCi/g 08/23/13 09:35 08/25/13 21:33 1
1.45 0.882 0.880 U
-0.686 Protactinium 231 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.0875 1.00 0.166 0.129 1.08 Radium 226 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.987 1.00 0.733 0.726 1.05 Thorium 234 pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.320 0.192 0.192 U
0.115 Uranium 235 pCi/g 08/23/13 09:35 08/25/13 21:33 1
5.71 3.27 3.26 U
2.51 Protactinium 234m pCi/g 08/23/13 09:35 08/25/13 21:33 1
0.165 0.226 0.182 1.38 Thorium 232 Tl-208 0.450 0.0575 0.0722 0.0412 pCi/g 08/23/13 09:35 08/25/13 21:33 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-18 Client Sample ID: L050256PRS00 Matrix: Solid Date Collected: 08/19/13 08:55 Percent Solids: 84.0 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00066 0.000020 mg/Kg
08/22/13 08:34 08/23/13 19:10 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0312 U
(2+/-)
0.0411 (2+/-)
1 08/23/13 19:10 08/22/13 08:34 pCi/g 0.226 1.32 RL MDC 0.0367 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 19:10 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 TestAmerica St. Louis Page 25 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-18 Client Sample ID: L050256PRS00 Matrix: Solid Date Collected: 08/19/13 08:55 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.38 (2+/-)
0.202 (2+/-)
1 08/25/13 22:09 08/23/13 09:35 pCi/g 0.133 RL MDC 0.150 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/25/13 22:09 1
0.114 0.0677 0.0677 U
-0.00474 Americium 241 pCi/g 08/23/13 09:35 08/25/13 22:09 1
0.651 0.792 0.771 1.83 Bismuth 212 pCi/g 08/23/13 09:35 08/25/13 22:09 1
0.0868 0.167 0.126 1.12 Bismuth 214 pCi/g 08/23/13 09:35 08/25/13 22:09 1
0.0710 0.212 0.0889 1.27 Lead 212 pCi/g 08/23/13 09:35 08/25/13 22:09 1
0.0863 0.175 0.107 1.27 Lead 214 pCi/g 08/23/13 09:35 08/25/13 22:09 1
0.381 2.77 1.46 24.5 Potassium 40 pCi/g 08/23/13 09:35 08/25/13 22:09 1
1.29 0.359 0.352 U
0.574 Protactinium 231 pCi/g 08/23/13 09:35 08/25/13 22:09 1
0.0868 1.00 0.167 0.126 1.12 Radium 226 pCi/g 08/23/13 09:35 08/25/13 22:09 1
0.975 1.00 0.794 0.783 1.39 Thorium 234 pCi/g 08/23/13 09:35 08/25/13 22:09 1
0.222 0.156 0.156 U
0.155 Uranium 235 pCi/g 08/23/13 09:35 08/25/13 22:09 1
5.98 3.57 3.57 U
2.29 Protactinium 234m pCi/g 08/23/13 09:35 08/25/13 22:09 1
0.133 0.202 0.150 1.38 Thorium 232 Tl-208 0.373 0.0598 0.0699 0.0461 pCi/g 08/23/13 09:35 08/25/13 22:09 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-19 Client Sample ID: L050257PES00 Matrix: Solid Date Collected: 08/19/13 10:20 Percent Solids: 82.1 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00069 0.000021 mg/Kg
08/22/13 08:34 08/23/13 19:21 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.117 U
(2+/-)
0.0672 (2+/-)
1 08/23/13 19:21 08/22/13 08:34 pCi/g 0.238 1.39 RL MDC 0.0575 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 19:21 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.31 (2+/-)
0.212 (2+/-)
1 08/25/13 22:11 08/23/13 09:35 pCi/g 0.137 RL MDC 0.170 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/25/13 22:11 1
0.112 0.0671 0.0671 U
0.0207 Americium 241 pCi/g 08/23/13 09:35 08/25/13 22:11 1
0.434 0.463 0.447 1.25 Bismuth 212 pCi/g 08/23/13 09:35 08/25/13 22:11 1
0.0842 0.166 0.125 1.13 Bismuth 214 pCi/g 08/23/13 09:35 08/25/13 22:11 1
0.102 0.159 0.0951 1.19 Lead 212 pCi/g 08/23/13 09:35 08/25/13 22:11 1
0.0908 0.157 0.112 1.13 Lead 214 pCi/g 08/23/13 09:35 08/25/13 22:11 1
0.458 2.92 1.50 26.0 Potassium 40 pCi/g 08/23/13 09:35 08/25/13 22:11 1
1.36 0.295 0.293 U
0.401 Protactinium 231 pCi/g 08/23/13 09:35 08/25/13 22:11 1
0.0842 1.00 0.166 0.125 1.13 Radium 226 TestAmerica St. Louis Page 26 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-19 Client Sample ID: L050257PES00 Matrix: Solid Date Collected: 08/19/13 10:20 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 1.35 (2+/-)
0.821 (2+/-)
1 08/25/13 22:11 08/23/13 09:35 pCi/g 0.986 1.00 RL MDC 0.810 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/25/13 22:11 1
0.233 0.189 0.188 U
0.220 Uranium 235 pCi/g 08/23/13 09:35 08/25/13 22:11 1
6.10 2.31 2.31 U
0.696 Protactinium 234m pCi/g 08/23/13 09:35 08/25/13 22:11 1
0.137 0.212 0.170 1.31 Thorium 232 Other Detected Radionuclide None pCi/g 08/23/13 09:35 08/25/13 22:11 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-20 Client Sample ID: L050258PES00 Matrix: Solid Date Collected: 08/16/13 13:40 Percent Solids: 82.6 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00068 0.000021 mg/Kg
08/22/13 08:34 08/23/13 19:25 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0872 U
(2+/-)
0.114 (2+/-)
1 08/23/13 19:25 08/22/13 08:34 pCi/g 0.234 1.37 RL MDC 0.101 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:34 08/23/13 19:25 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.12 (2+/-)
0.180 (2+/-)
1 08/25/13 22:10 08/23/13 09:35 pCi/g 0.152 RL MDC 0.143 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 09:35 08/25/13 22:10 1
0.109 0.306 0.306 U
-0.00766 Americium 241 pCi/g 08/23/13 09:35 08/25/13 22:10 1
0.389 0.420 0.403 1.21 Bismuth 212 pCi/g 08/23/13 09:35 08/25/13 22:10 1
0.0779 0.152 0.119 0.962 Bismuth 214 pCi/g 08/23/13 09:35 08/25/13 22:10 1
0.0712 0.165 0.0930 1.26 Lead 212 pCi/g 08/23/13 09:35 08/25/13 22:10 1
0.0902 0.163 0.121 1.12 Lead 214 pCi/g 08/23/13 09:35 08/25/13 22:10 1
0.195 2.62 1.53 22.1 Potassium 40 pCi/g 08/23/13 09:35 08/25/13 22:10 1
1.57 0.964 0.960 U
-0.908 Protactinium 231 pCi/g 08/23/13 09:35 08/25/13 22:10 1
0.0779 1.00 0.152 0.119 0.962 Radium 226 pCi/g 08/23/13 09:35 08/25/13 22:10 1
0.974 1.00 0.383 0.371 0.979 Thorium 234 pCi/g 08/23/13 09:35 08/25/13 22:10 1
0.288 0.155 0.154 U
0.115 Uranium 235 pCi/g 08/23/13 09:35 08/25/13 22:10 1
7.00 4.22 4.21 U
3.04 Protactinium 234m pCi/g 08/23/13 09:35 08/25/13 22:10 1
0.152 0.180 0.143 1.12 Thorium 232 Tl-208 0.406 0.0604 0.0721 0.0435 pCi/g 08/23/13 09:35 08/25/13 22:10 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-21 Client Sample ID: L050259PRQ00 Matrix: Solid Date Collected: 08/19/13 15:20 Percent Solids: 81.1 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00067 0.000020 mg/Kg
08/22/13 08:38 08/23/13 19:37 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.112 U
(2+/-)
0.104 (2+/-)
1 08/23/13 19:37 08/22/13 08:38 pCi/g 0.229 1.34 RL MDC 0.0950 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:38 08/23/13 19:37 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.22 (2+/-)
0.270 (2+/-)
1 08/23/13 16:14 08/23/13 11:49 pCi/g 0.233 RL MDC 0.240 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.223 0.129 0.129 U
-0.00450 Americium 241 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.811 0.904 0.881 1.94 Bismuth 212 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.159 0.206 0.184 0.897 Bismuth 214 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.149 0.235 0.167 1.29 Lead 212 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.189 0.208 0.188 0.842 Lead 214 pCi/g 08/23/13 11:49 08/23/13 16:14 1
1.06 2.72 1.97 18.3 Potassium 40 pCi/g 08/23/13 11:49 08/23/13 16:14 1
2.49 0.728 0.727 U
0.306 Protactinium 231 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.159 1.00 0.206 0.184 0.897 Radium 226 pCi/g 08/23/13 11:49 08/23/13 16:14 1
2.31 1.00 1.69 1.68 U
1.72 Thorium 234 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.460 0.252 0.251 U
0.228 Uranium 235 pCi/g 08/23/13 11:49 08/23/13 16:14 1
11.5 6.92 6.91 U
4.76 Protactinium 234m pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.233 0.270 0.240 1.22 Thorium 232 Tl-208 0.417 0.0978 0.107 0.0862 pCi/g 08/23/13 11:49 08/23/13 16:14 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-22 Client Sample ID: L050259PRS00 Matrix: Solid Date Collected: 08/16/13 15:20 Percent Solids: 80.5 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00072 0.000022 mg/Kg
08/22/13 08:38 08/23/13 19:48 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0960 U
(2+/-)
0.0305 (2+/-)
1 08/23/13 19:48 08/22/13 08:38 pCi/g 0.245 1.43 RL MDC 0.0252 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:38 08/23/13 19:48 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 TestAmerica St. Louis Page 28 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-22 Client Sample ID: L050259PRS00 Matrix: Solid Date Collected: 08/16/13 15:20 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.17 (2+/-)
0.317 (2+/-)
1 08/23/13 16:14 08/23/13 11:49 pCi/g 0.175 RL MDC 0.294 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.229 0.138 0.138 U
0.0945 Americium 241 pCi/g 08/23/13 11:49 08/23/13 16:14 1
1.21 0.719 0.717 U
0.456 Bismuth 212 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.200 0.218 0.205 0.735 Bismuth 214 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.134 0.211 0.151 1.14 Lead 212 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.164 0.214 0.189 0.958 Lead 214 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.847 3.01 2.21 20.0 Potassium 40 pCi/g 08/23/13 11:49 08/23/13 16:14 1
2.70 0.545 0.544 U
0.311 Protactinium 231 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.200 1.00 0.218 0.205 0.735 Radium 226 pCi/g 08/23/13 11:49 08/23/13 16:14 1
2.24 1.00 1.38 1.37 U
1.91 Thorium 234 pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.523 0.267 0.266 U
0.256 Uranium 235 pCi/g 08/23/13 11:49 08/23/13 16:14 1
12.2 7.08 7.07 U
3.58 Protactinium 234m pCi/g 08/23/13 11:49 08/23/13 16:14 1
0.175 0.317 0.294 1.17 Thorium 232 Tl-208 0.399 0.101 0.110 0.0921 pCi/g 08/23/13 11:49 08/23/13 16:14 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-23 Client Sample ID: L050260PES00 Matrix: Solid Date Collected: 08/16/13 15:30 Percent Solids: 80.3 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00069 0.000021 mg/Kg
08/22/13 08:38 08/23/13 19:52 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0332 U
(2+/-)
0.0297 (2+/-)
1 08/23/13 19:52 08/22/13 08:38 pCi/g 0.235 1.37 RL MDC 0.0265 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:38 08/23/13 19:52 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.33 (2+/-)
0.195 (2+/-)
1 08/25/13 20:14 08/23/13 11:49 pCi/g 0.121 RL MDC 0.146 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/25/13 20:14 1
0.113 0.144 0.144 U
-0.0194 Americium 241 pCi/g 08/23/13 11:49 08/25/13 20:14 1
0.475 0.552 0.531 1.56 Bismuth 212 pCi/g 08/23/13 11:49 08/25/13 20:14 1
0.100 0.164 0.134 0.971 Bismuth 214 pCi/g 08/23/13 11:49 08/25/13 20:14 1
0.0682 0.160 0.0890 1.24 Lead 212 pCi/g 08/23/13 11:49 08/25/13 20:14 1
0.0931 0.152 0.106 1.13 Lead 214 pCi/g 08/23/13 11:49 08/25/13 20:14 1
0.182 2.62 1.49 22.3 Potassium 40 pCi/g 08/23/13 11:49 08/25/13 20:14 1
1.19 0.253 0.248 U
0.492 Protactinium 231 pCi/g 08/23/13 11:49 08/25/13 20:14 1
0.100 1.00 0.164 0.134 0.971 Radium 226 TestAmerica St. Louis Page 29 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-23 Client Sample ID: L050260PES00 Matrix: Solid Date Collected: 08/16/13 15:30 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 1.32 (2+/-)
0.600 (2+/-)
1 08/25/13 20:14 08/23/13 11:49 pCi/g 0.833 1.00 RL MDC 0.586 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/25/13 20:14 1
0.276 0.168 0.167 U
0.101 Uranium 235 pCi/g 08/23/13 11:49 08/25/13 20:14 1
7.40 4.44 4.44 U
1.49 Protactinium 234m pCi/g 08/23/13 11:49 08/25/13 20:14 1
0.121 0.195 0.146 1.33 Thorium 232 Tl-208 0.376 0.0603 0.0705 0.0498 pCi/g 08/23/13 11:49 08/25/13 20:14 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-24 Client Sample ID: L050261PRS00 Matrix: Solid Date Collected: 08/16/13 09:05 Percent Solids: 82.6 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00069 0.000021 mg/Kg
08/22/13 08:38 08/23/13 19:56 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0503 U
(2+/-)
0.0174 (2+/-)
1 08/23/13 19:56 08/22/13 08:38 pCi/g 0.236 1.38 RL MDC 0.0147 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:38 08/23/13 19:56 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.23 (2+/-)
0.226 (2+/-)
1 08/25/13 20:16 08/23/13 11:49 pCi/g 0.129 RL MDC 0.188 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/25/13 20:16 1
0.132 0.0785 0.0785 U
0.0110 Americium 241 pCi/g 08/23/13 11:49 08/25/13 20:16 1
0.405 0.558 0.522 1.89 Bismuth 212 pCi/g 08/23/13 11:49 08/25/13 20:16 1
0.0969 0.160 0.130 0.900 Bismuth 214 pCi/g 08/23/13 11:49 08/25/13 20:16 1
0.0800 0.177 0.0941 1.16 Lead 212 pCi/g 08/23/13 11:49 08/25/13 20:16 1
0.0901 0.169 0.119 1.16 Lead 214 pCi/g 08/23/13 11:49 08/25/13 20:16 1
0.211 2.91 1.64 23.5 Potassium 40 pCi/g 08/23/13 11:49 08/25/13 20:16 1
1.57 0.951 0.948 U
-0.689 Protactinium 231 pCi/g 08/23/13 11:49 08/25/13 20:16 1
0.0969 1.00 0.160 0.130 0.900 Radium 226 pCi/g 08/23/13 11:49 08/25/13 20:16 1
1.16 1.00 0.967 0.952 1.60 Thorium 234 pCi/g 08/23/13 11:49 08/25/13 20:16 1
0.300 0.210 0.209 U
0.192 Uranium 235 pCi/g 08/23/13 11:49 08/25/13 20:16 1
7.12 4.04 4.04 U
1.09 Protactinium 234m pCi/g 08/23/13 11:49 08/25/13 20:16 1
0.129 0.226 0.188 1.23 Thorium 232 Tl-208 0.339 0.0570 0.0670 0.0450 pCi/g 08/23/13 11:49 08/25/13 20:16 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-25 Client Sample ID: L050262PES00 Matrix: Solid Date Collected: 08/19/13 10:30 Percent Solids: 80.5 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00070 0.000021 mg/Kg
08/22/13 08:38 08/23/13 20:08 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.127 U
(2+/-)
0.0715 (2+/-)
1 08/23/13 20:08 08/22/13 08:38 pCi/g 0.238 1.39 RL MDC 0.0628 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:38 08/23/13 20:08 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.24 (2+/-)
0.182 (2+/-)
1 08/25/13 20:17 08/23/13 11:49 pCi/g 0.123 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/25/13 20:17 1
0.100 0.0590 0.0590 U
-0.000130 Americium 241 pCi/g 08/23/13 11:49 08/25/13 20:17 1
0.523 0.598 0.572 1.79 Bismuth 212 pCi/g 08/23/13 11:49 08/25/13 20:17 1
0.0779 0.150 0.112 1.02 Bismuth 214 pCi/g 08/23/13 11:49 08/25/13 20:17 1
0.0702 0.173 0.0905 1.37 Lead 212 pCi/g 08/23/13 11:49 08/25/13 20:17 1
0.0739 0.142 0.0935 1.10 Lead 214 pCi/g 08/23/13 11:49 08/25/13 20:17 1
0.386 2.72 1.45 24.0 Potassium 40 pCi/g 08/23/13 11:49 08/25/13 20:17 1
1.31 0.219 0.216 U
0.350 Protactinium 231 pCi/g 08/23/13 11:49 08/25/13 20:17 1
0.0779 1.00 0.150 0.112 1.02 Radium 226 pCi/g 08/23/13 11:49 08/25/13 20:17 1
0.943 1.00 0.790 0.769 1.88 Thorium 234 pCi/g 08/23/13 11:49 08/25/13 20:17 1
0.257 0.154 0.153 U
0.176 Uranium 235 pCi/g 08/23/13 11:49 08/25/13 20:17 1
5.64 3.21 3.21 U
0.899 Protactinium 234m pCi/g 08/23/13 11:49 08/25/13 20:17 1
0.123 0.182 0.137 1.24 Thorium 232 Tl-208 0.378 0.0566 0.0675 0.0420 pCi/g 08/23/13 11:49 08/25/13 20:17 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-26 Client Sample ID: L050263PES00 Matrix: Solid Date Collected: 08/19/13 13:30 Percent Solids: 82.6 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00069 0.000021 mg/Kg
08/22/13 08:38 08/23/13 20:12 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.132 U
(2+/-)
0.0405 (2+/-)
1 08/23/13 20:12 08/22/13 08:38 pCi/g 0.237 1.39 RL MDC 0.0336 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:38 08/23/13 20:12 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 TestAmerica St. Louis Page 31 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-26 Client Sample ID: L050263PES00 Matrix: Solid Date Collected: 08/19/13 13:30 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.14 (2+/-)
0.169 (2+/-)
1 08/28/13 11:05 08/23/13 11:49 pCi/g 0.138 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/28/13 11:05 1
0.105 0.0626 0.0626 U
0.0112 Americium 241 pCi/g 08/23/13 11:49 08/28/13 11:05 1
0.373 0.488 0.454 1.74 Bismuth 212 pCi/g 08/23/13 11:49 08/28/13 11:05 1
0.0656 0.157 0.107 1.10 Bismuth 214 pCi/g 08/23/13 11:49 08/28/13 11:05 1
0.0634 0.186 0.0824 1.28 Lead 212 pCi/g 08/23/13 11:49 08/28/13 11:05 1
0.0814 0.176 0.103 1.37 Lead 214 pCi/g 08/23/13 11:49 08/28/13 11:05 1
0.263 2.85 1.35 24.5 Potassium 40 pCi/g 08/23/13 11:49 08/28/13 11:05 1
1.40 0.847 0.844 U
-0.614 Protactinium 231 pCi/g 08/23/13 11:49 08/28/13 11:05 1
0.0656 1.00 0.157 0.107 1.10 Radium 226 pCi/g 08/23/13 11:49 08/28/13 11:05 1
1.02 1.00 0.349 0.332 1.03 Thorium 234 pCi/g 08/23/13 11:49 08/28/13 11:05 1
0.184 0.115 0.115 U
0.142 Uranium 235 pCi/g 08/23/13 11:49 08/28/13 11:05 1
7.82 3.18 3.18 U
0.000 Protactinium 234m pCi/g 08/23/13 11:49 08/28/13 11:05 1
0.138 0.169 0.123 1.14 Thorium 232 Tl-208 0.425 0.0535 0.0693 0.0387 pCi/g 08/23/13 11:49 08/28/13 11:05 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-27 Client Sample ID: L050264PRS00 Matrix: Solid Date Collected: 08/16/13 14:50 Percent Solids: 80.5 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00069 0.000021 mg/Kg
08/22/13 08:38 08/23/13 20:16 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.173 U
(2+/-)
0.125 (2+/-)
1 08/23/13 20:16 08/22/13 08:38 pCi/g 0.235 1.37 RL MDC 0.112 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:38 08/23/13 20:16 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.85 (2+/-)
0.379 (2+/-)
1 08/23/13 16:15 08/23/13 11:49 pCi/g 0.244 RL MDC 0.329 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/23/13 16:15 1
0.412 0.238 0.238 U
-0.0185 Americium 241 pCi/g 08/23/13 11:49 08/23/13 16:15 1
2.01 1.27 1.26 U
1.18 Bismuth 212 pCi/g 08/23/13 11:49 08/23/13 16:15 1
0.163 0.241 0.229 0.711 Bismuth 214 pCi/g 08/23/13 11:49 08/23/13 16:15 1
0.231 0.311 0.257 1.35 Lead 212 pCi/g 08/23/13 11:49 08/23/13 16:15 1
0.170 0.273 0.246 1.14 Lead 214 pCi/g 08/23/13 11:49 08/23/13 16:15 1
1.31 3.74 3.21 18.8 Potassium 40 pCi/g 08/23/13 11:49 08/23/13 16:15 1
4.15 0.636 0.633 U
0.477 Protactinium 231 pCi/g 08/23/13 11:49 08/23/13 16:15 1
0.163 1.00 0.241 0.229 0.711 Radium 226 TestAmerica St. Louis Page 32 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-27 Client Sample ID: L050264PRS00 Matrix: Solid Date Collected: 08/16/13 14:50 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 1.16 U
(2+/-)
1.05 (2+/-)
1 08/23/13 16:15 08/23/13 11:49 pCi/g 3.03 1.00 RL MDC 1.04 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/23/13 16:15 1
0.809 0.476 0.475 U
0.284 Uranium 235 pCi/g 08/23/13 11:49 08/23/13 16:15 1
25.1 9.26 9.26 U
1.57 Protactinium 234m pCi/g 08/23/13 11:49 08/23/13 16:15 1
0.244 0.379 0.329 1.85 Thorium 232 Tl-208 0.564 0.147 0.159 0.0907 pCi/g 08/23/13 11:49 08/23/13 16:15 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-28 Client Sample ID: L050265PES00 Matrix: Solid Date Collected: 08/16/13 15:00 Percent Solids: 80.9 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00070 0.000021 mg/Kg
08/22/13 08:38 08/23/13 20:19 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.217 U
(2+/-)
0.0850 (2+/-)
1 08/23/13 20:19 08/22/13 08:38 pCi/g 0.240 1.40 RL MDC 0.0725 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:38 08/23/13 20:19 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.45 (2+/-)
0.202 (2+/-)
1 08/25/13 20:53 08/23/13 11:49 pCi/g 0.128 RL MDC 0.145 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/25/13 20:53 1
0.117 0.0703 0.0702 U
0.0270 Americium 241 pCi/g 08/23/13 11:49 08/25/13 20:53 1
0.459 0.491 0.471 1.41 Bismuth 212 pCi/g 08/23/13 11:49 08/25/13 20:53 1
0.0768 0.155 0.116 1.05 Bismuth 214 pCi/g 08/23/13 11:49 08/25/13 20:53 1
0.0705 0.222 0.0913 1.34 Lead 212 pCi/g 08/23/13 11:49 08/25/13 20:53 1
0.0982 0.170 0.112 1.17 Lead 214 pCi/g 08/23/13 11:49 08/25/13 20:53 1
0.450 2.42 1.37 20.7 Potassium 40 pCi/g 08/23/13 11:49 08/25/13 20:53 1
1.18 0.420 0.404 U
0.953 Protactinium 231 pCi/g 08/23/13 11:49 08/25/13 20:53 1
0.0768 1.00 0.155 0.116 1.05 Radium 226 pCi/g 08/23/13 11:49 08/25/13 20:53 1
1.08 1.00 0.911 0.901 1.33 Thorium 234 pCi/g 08/23/13 11:49 08/25/13 20:53 1
0.229 0.198 0.196 0.301 Uranium 235 pCi/g 08/23/13 11:49 08/25/13 20:53 1
6.83 3.88 3.88 U
0.619 Protactinium 234m pCi/g 08/23/13 11:49 08/25/13 20:53 1
0.128 0.202 0.145 1.45 Thorium 232 Tl-208 0.443 0.0667 0.0794 0.0513 pCi/g 08/23/13 11:49 08/25/13 20:53 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-29 Client Sample ID: L050266PUB00 Matrix: Solid Date Collected: 08/16/13 11:50 Percent Solids: 85.7 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00064 0.000019 mg/Kg
08/22/13 08:38 08/23/13 20:23 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0513 U
(2+/-)
0.0611 (2+/-)
1 08/23/13 20:23 08/22/13 08:38 pCi/g 0.219 1.28 RL MDC 0.0558 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:38 08/23/13 20:23 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.01 (2+/-)
0.165 (2+/-)
1 08/25/13 20:55 08/23/13 11:49 pCi/g 0.116 RL MDC 0.128 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.107 0.0632 0.0632 U
-0.00396 Americium 241 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.445 0.504 0.486 1.28 Bismuth 212 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.0823 0.138 0.107 0.840 Bismuth 214 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.0898 0.144 0.0801 0.925 Lead 212 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.0667 0.146 0.0960 1.06 Lead 214 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.381 2.62 1.28 22.4 Potassium 40 pCi/g 08/23/13 11:49 08/25/13 20:55 1
1.22 0.749 0.745 U
-0.676 Protactinium 231 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.0823 1.00 0.138 0.107 0.840 Radium 226 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.905 1.00 0.735 0.719 1.49 Thorium 234 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.264 0.150 0.150 U
0.0295 Uranium 235 pCi/g 08/23/13 11:49 08/25/13 20:55 1
5.98 2.27 2.27 U
0.000 Protactinium 234m pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.116 0.165 0.128 1.01 Thorium 232 Tl-208 0.347 0.0425 0.0557 0.0304 pCi/g 08/23/13 11:49 08/25/13 20:55 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-30 Client Sample ID: L050267PUB00 Matrix: Solid Date Collected: 08/16/13 11:55 Percent Solids: 85.6 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00066 0.000020 mg/Kg
08/22/13 08:38 08/23/13 20:27 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0320 U
(2+/-)
0.0123 (2+/-)
1 08/23/13 20:27 08/22/13 08:38 pCi/g 0.226 1.32 RL MDC 0.0105 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:38 08/23/13 20:27 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 TestAmerica St. Louis Page 34 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-30 Client Sample ID: L050267PUB00 Matrix: Solid Date Collected: 08/16/13 11:55 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.13 (2+/-)
0.183 (2+/-)
1 08/25/13 20:54 08/23/13 11:49 pCi/g 0.163 RL MDC 0.147 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/25/13 20:54 1
0.0793 0.0528 0.0527 U
0.0341 Americium 241 pCi/g 08/23/13 11:49 08/25/13 20:54 1
0.379 0.425 0.408 1.21 Bismuth 212 pCi/g 08/23/13 11:49 08/25/13 20:54 1
0.0770 0.145 0.115 0.916 Bismuth 214 pCi/g 08/23/13 11:49 08/25/13 20:54 1
0.0730 0.150 0.0875 1.13 Lead 212 pCi/g 08/23/13 11:49 08/25/13 20:54 1
0.0811 0.140 0.0937 1.08 Lead 214 pCi/g 08/23/13 11:49 08/25/13 20:54 1
0.183 2.64 1.50 22.5 Potassium 40 pCi/g 08/23/13 11:49 08/25/13 20:54 1
1.47 0.335 0.325 U
0.802 Protactinium 231 pCi/g 08/23/13 11:49 08/25/13 20:54 1
0.0770 1.00 0.145 0.115 0.916 Radium 226 pCi/g 08/23/13 11:49 08/25/13 20:54 1
0.918 1.00 0.686 0.674 1.29 Thorium 234 pCi/g 08/23/13 11:49 08/25/13 20:54 1
0.248 0.159 0.159 U
0.116 Uranium 235 pCi/g 08/23/13 11:49 08/25/13 20:54 1
7.03 3.93 3.93 U
-0.269 Protactinium 234m pCi/g 08/23/13 11:49 08/25/13 20:54 1
0.163 0.183 0.147 1.13 Thorium 232 Tl-208 0.337 0.0525 0.0618 0.0402 pCi/g 08/23/13 11:49 08/25/13 20:54 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3435-31 Client Sample ID: L050268PUB00 Matrix: Solid Date Collected: 08/16/13 12:00 Percent Solids: 93.5 Date Received: 08/20/13 16:06 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00057 0.000017 mg/Kg
08/22/13 08:38 08/23/13 20:31 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.231 (2+/-)
0.0502 (2+/-)
1 08/23/13 20:31 08/22/13 08:38 pCi/g 0.194 1.13 RL MDC 0.0427 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/22/13 08:38 08/23/13 20:31 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 95 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.207 (2+/-)
0.0681 (2+/-)
1 08/25/13 20:55 08/23/13 11:49 pCi/g 0.109 RL MDC 0.0648 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.0711 0.0417 0.0417 U
-0.00170 Americium 241 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.338 0.201 0.201 U
0.130 Bismuth 212 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.0449 0.0810 0.0684 0.417 Bismuth 214 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.0391 0.0525 0.0394 0.269 Lead 212 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.0551 0.0829 0.0618 0.532 Lead 214 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.259 0.879 0.688 5.35 Potassium 40 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.669 0.381 0.381 U
-0.0624 Protactinium 231 pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.0449 1.00 0.0810 0.0684 0.417 Radium 226 TestAmerica St. Louis Page 35 of 48 1
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Client Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3435-31 Client Sample ID: L050268PUB00 Matrix: Solid Date Collected: 08/16/13 12:00 Date Received: 08/20/13 16:06 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 0.690 (2+/-)
0.256 (2+/-)
1 08/25/13 20:55 08/23/13 11:49 pCi/g 0.649 1.00 RL MDC 0.246 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.189 0.105 0.103 0.200 Uranium 235 pCi/g 08/23/13 11:49 08/25/13 20:55 1
4.25 2.58 2.58 U
1.99 Protactinium 234m pCi/g 08/23/13 11:49 08/25/13 20:55 1
0.109 0.0681 0.0648 0.207 Thorium 232 Tl-208 0.0918 0.0261 0.0278 0.0234 pCi/g 08/23/13 11:49 08/25/13 20:55 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 36 of 48 1
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QC Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-67949/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68435 Prep Batch: 67949 RL MDL Technetium 99 ND 0.00052 0.000015 mg/Kg 08/22/13 08:34 08/23/13 17:33 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-67949/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68435 Prep Batch: 67949 Technetium 99 0.00250 0.00254 mg/Kg 102 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: L050190TUB00 Lab Sample ID: 160-3435-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 68435 Prep Batch: 67949 Technetium 99 ND 0.00335 0.00311 mg/Kg 93 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: L050190TUB00 Lab Sample ID: 160-3435-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 68435 Prep Batch: 67949 Technetium 99 ND 0.00333 0.00294 mg/Kg 88 75 - 125 6
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Client Sample ID: Method Blank Lab Sample ID: MB 160-67951/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68435 Prep Batch: 67951 RL MDL Technetium 99 ND 0.00053 0.000016 mg/Kg 08/22/13 08:38 08/23/13 19:29 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-67951/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68435 Prep Batch: 67951 Technetium 99 0.00247 0.00245 mg/Kg 99 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: L050259PRQ00 Lab Sample ID: 160-3435-21 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 68435 Prep Batch: 67951 Technetium 99 ND 0.00321 0.00304 mg/Kg 95 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: L050259PRQ00 Lab Sample ID: 160-3435-21 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 68435 Prep Batch: 67951 Technetium 99 ND 0.00320 0.00298 mg/Kg 93 75 - 125 2
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD TestAmerica St. Louis Page 37 of 48 1
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QC Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-67949/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68436 Prep Batch: 67949 Technetium 99 Analyte U
1 08/23/13 17:33 08/22/13 08:34 pCi/g 0.177 MDC 1.03 RL 0.00886 0.00769 (2+/-)
(2+/-)
MB 0.04102 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 08/22/13 08:34 08/23/13 17:33 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 97 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-67949/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68436 Prep Batch: 67949 Technetium 99 Analyte 120 80 102 43.57 42.8 4.81 1.07 0.183 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 94 LCS Client Sample ID: L050190TUB00 Lab Sample ID: 160-3435-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 68436 Prep Batch: 67949 Technetium 99 Analyte 125 75 93 53.16 57.4 0.234 U
6.06 1.43 0.246 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 90 MS Client Sample ID: L050190TUB00 Lab Sample ID: 160-3435-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 68436 Prep Batch: 67949 Technetium 99 Analyte 1
0.24 125 75 88 50.25 57.0 0.234 U
6.16 1.43 0.244 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 90 MSD Client Sample ID: Method Blank Lab Sample ID: MB 160-67951/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68436 Prep Batch: 67951 Technetium 99 Analyte U
1 08/23/13 19:29 08/22/13 08:38 pCi/g 0.181 MDC 1.06 RL 0.0144 0.0131 (2+/-)
(2+/-)
MB 0.04180 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total TestAmerica St. Louis Page 38 of 48 1
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QC Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: Method Blank Lab Sample ID: MB 160-67951/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68436 Prep Batch: 67951 Carrier Re 30 - 110 08/22/13 08:38 08/23/13 19:29 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 94 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-67951/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68436 Prep Batch: 67951 Technetium 99 Analyte 120 80 99 41.92 42.3 4.13 1.06 0.181 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 95 LCS Client Sample ID: L050259PRQ00 Lab Sample ID: 160-3435-21 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 68436 Prep Batch: 67951 Technetium 99 Analyte 125 75 95 52.13 55.0 0.112 U
5.61 1.37 0.235 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 90 MS Client Sample ID: L050259PRQ00 Lab Sample ID: 160-3435-21 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 68436 Prep Batch: 67951 Technetium 99 Analyte 1
0.10 125 75 93 50.99 54.8 0.112 U
5.39 1.37 0.235 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 90 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-68149/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68614 Prep Batch: 68149 Actinium 228 Analyte U
1 08/26/13 21:04 08/23/13 09:35 pCi/g 0.0322 MDC RL 0.0201 0.0201 (2+/-)
(2+/-)
MB 0.004246 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
08/26/13 21:04 08/23/13 09:35 pCi/g 0.0263 0.0141 0.0141 U
0.002703 Americium 241 1
08/26/13 21:04 08/23/13 09:35 pCi/g 0.333 0.0276 0.0276 U
0.0000 Bismuth 212 1
08/26/13 21:04 08/23/13 09:35 pCi/g 0.0289 0.0175 0.0173 U
0.02545 Bismuth 214 TestAmerica St. Louis Page 39 of 48 1
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QC Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Method Blank Lab Sample ID: MB 160-68149/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68614 Prep Batch: 68149 Lead 212 Analyte U
1 08/26/13 21:04 08/23/13 09:35 pCi/g 0.0216 MDC RL 0.0142 0.0141 (2+/-)
(2+/-)
MB 0.01369 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
08/26/13 21:04 08/23/13 09:35 pCi/g 0.0413 0.00668 0.00666 U
0.005201 Lead 214 1
08/26/13 21:04 08/23/13 09:35 pCi/g 0.217 0.115 0.115 U
0.03823 Potassium 40 1
08/26/13 21:04 08/23/13 09:35 pCi/g 0.367 0.195 0.195 U
-0.004419 Protactinium 231 1
08/26/13 21:04 08/23/13 09:35 pCi/g 0.0289 1.00 0.0175 0.0173 U
0.02545 Radium 226 1
08/26/13 21:04 08/23/13 09:35 pCi/g 0.299 1.00 0.0189 0.0189 U
0.007326 Thorium 234 1
08/26/13 21:04 08/23/13 09:35 pCi/g 0.0733 0.0384 0.0382 U
0.03931 Uranium 235 1
08/26/13 21:04 08/23/13 09:35 pCi/g 3.05 1.68 1.68 U
-0.4858 Protactinium 234m 1
08/26/13 21:04 08/23/13 09:35 pCi/g 0.0322 0.0201 0.0201 U
0.004246 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 08/23/13 09:35 08/26/13 21:04 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-68149/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68409 Prep Batch: 68149 Americium 241 Analyte 116 87 98 96.19 97.7 10.1 0.898 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 31.7 31.81 3.34 0.200 0.178 pCi/g 100 87 - 120 Cobalt 60 24.8 24.77 2.51 0.109 pCi/g 100 87 - 115 Client Sample ID: L050190TUB00 Lab Sample ID: 160-3435-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 68392 Prep Batch: 68149 Actinium 228 Analyte 1
0.16 0.9822 0.932 0.169 0.115 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241
-0.0189 U
0.003815 U
0.0643 0.108 pCi/g 0.18 1
Bismuth 212 1.48 1.366 0.398 0.291 pCi/g 0.14 1
Bismuth 214 0.752 0.7715 0.122 0.0633 pCi/g 0.08 1
Lead 212 0.931 0.8332 0.131 0.0809 pCi/g 0.36 1
Lead 214 0.832 0.8105 0.118 0.0671 pCi/g 0.09 1
Potassium 40 16.7 17.17 2.06 0.227 pCi/g 0.12 1
Protactinium 231 0.518 U
-0.5099 U F 0.643 1.06 pCi/g 1.08 1
Radium 226 0.752 0.7715 0.122 1.00 0.0633 pCi/g 0.08 1
Thorium 234 1.08 1.867 0.742 1.00 0.833 pCi/g 0.59 1
Uranium 235 0.155 U
0.1289 U
0.124 0.167 pCi/g 0.1 1
Protactinium 234m 4.37 U
4.236 U
2.99 4.93 pCi/g 0.03 1
Thorium 232 0.932 0.9822 0.169 0.115 pCi/g 0.16 1
TestAmerica St. Louis Page 40 of 48 1
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QC Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Method Blank Lab Sample ID: MB 160-68361/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68418 Prep Batch: 68361 Actinium 228 Analyte U
1 08/25/13 20:14 08/23/13 11:49 pCi/g 0.0662 MDC RL 0.00790 0.00789 (2+/-)
(2+/-)
MB 0.004165 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
08/25/13 20:14 08/23/13 11:49 pCi/g 0.0257 0.0147 0.0147 U
0.003463 Americium 241 1
08/25/13 20:14 08/23/13 11:49 pCi/g 0.158 0.0859 0.0858 U
0.02943 Bismuth 212 1
08/25/13 20:14 08/23/13 11:49 pCi/g 0.0401 0.0223 0.0223 U
-0.001347 Bismuth 214 1
08/25/13 20:14 08/23/13 11:49 pCi/g 0.0219 0.0131 0.0130 U
0.01034 Lead 212 1
08/25/13 20:14 08/23/13 11:49 pCi/g 0.0285 0.0171 0.0168 0.03187 Lead 214 1
08/25/13 20:14 08/23/13 11:49 pCi/g 0.315 0.158 0.158 U
-0.009079 Potassium 40 1
08/25/13 20:14 08/23/13 11:49 pCi/g 0.358 0.197 0.197 U
-0.02795 Protactinium 231 1
08/25/13 20:14 08/23/13 11:49 pCi/g 0.0401 1.00 0.0223 0.0223 U
-0.001347 Radium 226 1
08/25/13 20:14 08/23/13 11:49 pCi/g 0.278 1.00 0.144 0.144 U
0.03659 Thorium 234 1
08/25/13 20:14 08/23/13 11:49 pCi/g 0.0627 0.0348 0.0348 U
0.004433 Uranium 235 1
08/25/13 20:14 08/23/13 11:49 pCi/g 1.68 1.05 1.05 U
0.8453 Protactinium 234m 1
08/25/13 20:14 08/23/13 11:49 pCi/g 0.0662 0.00790 0.00789 U
0.004165 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 08/23/13 11:49 08/25/13 20:14 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-68361/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68419 Prep Batch: 68361 Americium 241 Analyte 116 87 97 94.58 97.7 9.84 0.491 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 31.7 31.34 3.28 0.200 0.129 pCi/g 99 87 - 120 Cobalt 60 24.8 24.45 2.47 0.109 pCi/g 99 87 - 115 Client Sample ID: L050268PUB00 Lab Sample ID: 160-3435-31 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 68414 Prep Batch: 68361 Actinium 228 Analyte 1
0.89 0.3328 0.207 0.0729 0.0386 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241
-0.00170 U
-0.01717 U
0.0401 0.0671 pCi/g 0.19 1
Bismuth 212 0.130 U
0.3056 0.152 0.153 pCi/g 0.50 1
Bismuth 214 0.417 0.5197 0.0835 0.0401 pCi/g 0.62 1
Lead 212 0.269 0.3239 0.0557 0.0346 pCi/g 0.51 1
Lead 214 0.532 0.4982 0.0739 0.0395 pCi/g 0.22 1
Potassium 40 5.35 5.186 0.748 0.187 pCi/g 0.10 1
Protactinium 231
-0.0624 U
0.1583 U
0.121 0.560 pCi/g 0.44 1
Radium 226 0.417 0.5197 0.0835 1.00 0.0401 pCi/g 0.62 1
Thorium 234 0.690 1.292 0.501 1.00 0.576 pCi/g 0.80 1
Uranium 235 0.200 0.2728 0.0966 0.112 pCi/g 0.36 1
Protactinium 234m 1.99 U
0.9806 U
1.56 2.89 pCi/g 0.24 1
TestAmerica St. Louis Page 41 of 48 1
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QC Sample Results TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: L050268PUB00 Lab Sample ID: 160-3435-31 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 68414 Prep Batch: 68361 Thorium 232 Analyte 1
0.89 0.3328 0.207 0.0729 0.0386 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER TestAmerica St. Louis Page 42 of 48 1
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QC Association Summary TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Metals Prep Batch: 67949 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3435-1 L050190TUB00 Total/NA Solid None 160-3435-1 MS L050190TUB00 Total/NA Solid None 160-3435-1 MSD L050190TUB00 Total/NA Solid None 160-3435-2 L050191TUB00 Total/NA Solid None 160-3435-3 L050192TUB00 Total/NA Solid None 160-3435-4 L050193TUB00 Total/NA Solid None 160-3435-5 L050194TUB00 Total/NA Solid None 160-3435-6 L050195TUB00 Total/NA Solid None 160-3435-7 L050196TUB00 Total/NA Solid None 160-3435-8 L050197TUB00 Total/NA Solid None 160-3435-9 L050247PRS00 Total/NA Solid None 160-3435-10 L050248PES00 Total/NA Solid None 160-3435-11 L050249PRS00 Total/NA Solid None 160-3435-12 L050250PES00 Total/NA Solid None 160-3435-13 L050251PRS00 Total/NA Solid None 160-3435-14 L050252PES00 Total/NA Solid None 160-3435-15 L050253PES00 Total/NA Solid None 160-3435-16 L050254PES00 Total/NA Solid None 160-3435-17 L050255PES00 Total/NA Solid None 160-3435-18 L050256PRS00 Total/NA Solid None 160-3435-19 L050257PES00 Total/NA Solid None 160-3435-20 L050258PES00 Total/NA Solid None LCS 160-67949/2-A Lab Control Sample Total/NA Solid None MB 160-67949/1-A Method Blank Total/NA Prep Batch: 67951 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3435-21 L050259PRQ00 Total/NA Solid None 160-3435-21 MS L050259PRQ00 Total/NA Solid None 160-3435-21 MSD L050259PRQ00 Total/NA Solid None 160-3435-22 L050259PRS00 Total/NA Solid None 160-3435-23 L050260PES00 Total/NA Solid None 160-3435-24 L050261PRS00 Total/NA Solid None 160-3435-25 L050262PES00 Total/NA Solid None 160-3435-26 L050263PES00 Total/NA Solid None 160-3435-27 L050264PRS00 Total/NA Solid None 160-3435-28 L050265PES00 Total/NA Solid None 160-3435-29 L050266PUB00 Total/NA Solid None 160-3435-30 L050267PUB00 Total/NA Solid None 160-3435-31 L050268PUB00 Total/NA Solid None LCS 160-67951/2-A Lab Control Sample Total/NA Solid None MB 160-67951/1-A Method Blank Total/NA Analysis Batch: 68435 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 67949 160-3435-1 L050190TUB00 Total/NA Solid 6020A 67949 160-3435-1 MS L050190TUB00 Total/NA Solid 6020A 67949 160-3435-1 MSD L050190TUB00 Total/NA Solid 6020A 67949 160-3435-2 L050191TUB00 Total/NA Solid 6020A 67949 160-3435-3 L050192TUB00 Total/NA Solid 6020A 67949 160-3435-4 L050193TUB00 Total/NA TestAmerica St. Louis Page 43 of 48 1
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QC Association Summary TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Metals (Continued)
Analysis Batch: 68435 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 67949 160-3435-5 L050194TUB00 Total/NA Solid 6020A 67949 160-3435-6 L050195TUB00 Total/NA Solid 6020A 67949 160-3435-7 L050196TUB00 Total/NA Solid 6020A 67949 160-3435-8 L050197TUB00 Total/NA Solid 6020A 67949 160-3435-9 L050247PRS00 Total/NA Solid 6020A 67949 160-3435-10 L050248PES00 Total/NA Solid 6020A 67949 160-3435-11 L050249PRS00 Total/NA Solid 6020A 67949 160-3435-12 L050250PES00 Total/NA Solid 6020A 67949 160-3435-13 L050251PRS00 Total/NA Solid 6020A 67949 160-3435-14 L050252PES00 Total/NA Solid 6020A 67949 160-3435-15 L050253PES00 Total/NA Solid 6020A 67949 160-3435-16 L050254PES00 Total/NA Solid 6020A 67949 160-3435-17 L050255PES00 Total/NA Solid 6020A 67949 160-3435-18 L050256PRS00 Total/NA Solid 6020A 67949 160-3435-19 L050257PES00 Total/NA Solid 6020A 67949 160-3435-20 L050258PES00 Total/NA Solid 6020A 67951 160-3435-21 L050259PRQ00 Total/NA Solid 6020A 67951 160-3435-21 MS L050259PRQ00 Total/NA Solid 6020A 67951 160-3435-21 MSD L050259PRQ00 Total/NA Solid 6020A 67951 160-3435-22 L050259PRS00 Total/NA Solid 6020A 67951 160-3435-23 L050260PES00 Total/NA Solid 6020A 67951 160-3435-24 L050261PRS00 Total/NA Solid 6020A 67951 160-3435-25 L050262PES00 Total/NA Solid 6020A 67951 160-3435-26 L050263PES00 Total/NA Solid 6020A 67951 160-3435-27 L050264PRS00 Total/NA Solid 6020A 67951 160-3435-28 L050265PES00 Total/NA Solid 6020A 67951 160-3435-29 L050266PUB00 Total/NA Solid 6020A 67951 160-3435-30 L050267PUB00 Total/NA Solid 6020A 67951 160-3435-31 L050268PUB00 Total/NA Solid 6020A 67949 LCS 160-67949/2-A Lab Control Sample Total/NA Solid 6020A 67951 LCS 160-67951/2-A Lab Control Sample Total/NA Solid 6020A 67949 MB 160-67949/1-A Method Blank Total/NA Solid 6020A 67951 MB 160-67951/1-A Method Blank Total/NA General Chemistry Analysis Batch: 67942 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3435-1 L050190TUB00 Total/NA Solid Moisture 160-3435-2 L050191TUB00 Total/NA Solid Moisture 160-3435-3 L050192TUB00 Total/NA Solid Moisture 160-3435-4 L050193TUB00 Total/NA Solid Moisture 160-3435-5 L050194TUB00 Total/NA Solid Moisture 160-3435-6 L050195TUB00 Total/NA Solid Moisture 160-3435-7 L050196TUB00 Total/NA Solid Moisture 160-3435-8 L050197TUB00 Total/NA Solid Moisture 160-3435-9 L050247PRS00 Total/NA Solid Moisture 160-3435-10 L050248PES00 Total/NA Solid Moisture 160-3435-11 L050249PRS00 Total/NA Solid Moisture 160-3435-12 L050250PES00 Total/NA TestAmerica St. Louis Page 44 of 48 1
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QC Association Summary TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
General Chemistry (Continued)
Analysis Batch: 67942 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3435-13 L050251PRS00 Total/NA Solid Moisture 160-3435-14 L050252PES00 Total/NA Solid Moisture 160-3435-15 L050253PES00 Total/NA Solid Moisture 160-3435-16 L050254PES00 Total/NA Solid Moisture 160-3435-17 L050255PES00 Total/NA Solid Moisture 160-3435-18 L050256PRS00 Total/NA Solid Moisture 160-3435-19 L050257PES00 Total/NA Solid Moisture 160-3435-20 L050258PES00 Total/NA Solid Moisture 160-3435-21 L050259PRQ00 Total/NA Solid Moisture 160-3435-22 L050259PRS00 Total/NA Solid Moisture 160-3435-23 L050260PES00 Total/NA Solid Moisture 160-3435-24 L050261PRS00 Total/NA Solid Moisture 160-3435-25 L050262PES00 Total/NA Solid Moisture 160-3435-26 L050263PES00 Total/NA Solid Moisture 160-3435-27 L050264PRS00 Total/NA Solid Moisture 160-3435-28 L050265PES00 Total/NA Solid Moisture 160-3435-29 L050266PUB00 Total/NA Solid Moisture 160-3435-30 L050267PUB00 Total/NA Solid Moisture 160-3435-31 L050268PUB00 Total/NA Solid Moisture 160-3435-31 DU L050268PUB00 Total/NA Rad Leach Batch: 67776 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3435-1 L050190TUB00 Total/NA Solid Dry and Grind 160-3435-1 DU L050190TUB00 Total/NA Solid Dry and Grind 160-3435-2 L050191TUB00 Total/NA Solid Dry and Grind 160-3435-3 L050192TUB00 Total/NA Solid Dry and Grind 160-3435-4 L050193TUB00 Total/NA Solid Dry and Grind 160-3435-5 L050194TUB00 Total/NA Solid Dry and Grind 160-3435-6 L050195TUB00 Total/NA Solid Dry and Grind 160-3435-7 L050196TUB00 Total/NA Solid Dry and Grind 160-3435-8 L050197TUB00 Total/NA Solid Dry and Grind 160-3435-9 L050247PRS00 Total/NA Solid Dry and Grind 160-3435-10 L050248PES00 Total/NA Solid Dry and Grind 160-3435-11 L050249PRS00 Total/NA Solid Dry and Grind 160-3435-12 L050250PES00 Total/NA Solid Dry and Grind 160-3435-13 L050251PRS00 Total/NA Solid Dry and Grind 160-3435-14 L050252PES00 Total/NA Solid Dry and Grind 160-3435-15 L050253PES00 Total/NA Solid Dry and Grind 160-3435-16 L050254PES00 Total/NA Solid Dry and Grind 160-3435-17 L050255PES00 Total/NA Solid Dry and Grind 160-3435-18 L050256PRS00 Total/NA Solid Dry and Grind 160-3435-19 L050257PES00 Total/NA Solid Dry and Grind 160-3435-20 L050258PES00 Total/NA Solid Dry and Grind 160-3435-21 L050259PRQ00 Total/NA Solid Dry and Grind 160-3435-22 L050259PRS00 Total/NA Solid Dry and Grind 160-3435-23 L050260PES00 Total/NA Solid Dry and Grind 160-3435-24 L050261PRS00 Total/NA TestAmerica St. Louis Page 45 of 48 1
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QC Association Summary TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Rad (Continued)
Leach Batch: 67776 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3435-25 L050262PES00 Total/NA Solid Dry and Grind 160-3435-26 L050263PES00 Total/NA Solid Dry and Grind 160-3435-27 L050264PRS00 Total/NA Solid Dry and Grind 160-3435-28 L050265PES00 Total/NA Solid Dry and Grind 160-3435-29 L050266PUB00 Total/NA Solid Dry and Grind 160-3435-30 L050267PUB00 Total/NA Solid Dry and Grind 160-3435-31 L050268PUB00 Total/NA Solid Dry and Grind 160-3435-31 DU L050268PUB00 Total/NA Prep Batch: 67949 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3435-1 L050190TUB00 Total/NA Solid None 160-3435-1 MS L050190TUB00 Total/NA Solid None 160-3435-1 MSD L050190TUB00 Total/NA Solid None 160-3435-2 L050191TUB00 Total/NA Solid None 160-3435-3 L050192TUB00 Total/NA Solid None 160-3435-4 L050193TUB00 Total/NA Solid None 160-3435-5 L050194TUB00 Total/NA Solid None 160-3435-6 L050195TUB00 Total/NA Solid None 160-3435-7 L050196TUB00 Total/NA Solid None 160-3435-8 L050197TUB00 Total/NA Solid None 160-3435-9 L050247PRS00 Total/NA Solid None 160-3435-10 L050248PES00 Total/NA Solid None 160-3435-11 L050249PRS00 Total/NA Solid None 160-3435-12 L050250PES00 Total/NA Solid None 160-3435-13 L050251PRS00 Total/NA Solid None 160-3435-14 L050252PES00 Total/NA Solid None 160-3435-15 L050253PES00 Total/NA Solid None 160-3435-16 L050254PES00 Total/NA Solid None 160-3435-17 L050255PES00 Total/NA Solid None 160-3435-18 L050256PRS00 Total/NA Solid None 160-3435-19 L050257PES00 Total/NA Solid None 160-3435-20 L050258PES00 Total/NA Solid None LCS 160-67949/2-A Lab Control Sample Total/NA Solid None MB 160-67949/1-A Method Blank Total/NA Prep Batch: 67951 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3435-21 L050259PRQ00 Total/NA Solid None 160-3435-21 MS L050259PRQ00 Total/NA Solid None 160-3435-21 MSD L050259PRQ00 Total/NA Solid None 160-3435-22 L050259PRS00 Total/NA Solid None 160-3435-23 L050260PES00 Total/NA Solid None 160-3435-24 L050261PRS00 Total/NA Solid None 160-3435-25 L050262PES00 Total/NA Solid None 160-3435-26 L050263PES00 Total/NA Solid None 160-3435-27 L050264PRS00 Total/NA Solid None 160-3435-28 L050265PES00 Total/NA Solid None 160-3435-29 L050266PUB00 Total/NA Solid None 160-3435-30 L050267PUB00 Total/NA Solid None 160-3435-31 L050268PUB00 Total/NA TestAmerica St. Louis Page 46 of 48 1
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QC Association Summary TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Rad (Continued)
Prep Batch: 67951 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None LCS 160-67951/2-A Lab Control Sample Total/NA Solid None MB 160-67951/1-A Method Blank Total/NA Prep Batch: 68149 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 67776 160-3435-1 L050190TUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-1 DU L050190TUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-2 L050191TUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-3 L050192TUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-4 L050193TUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-5 L050194TUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-6 L050195TUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-7 L050196TUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-8 L050197TUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-9 L050247PRS00 Total/NA Solid Fill_Geo-0 67776 160-3435-10 L050248PES00 Total/NA Solid Fill_Geo-0 67776 160-3435-11 L050249PRS00 Total/NA Solid Fill_Geo-0 67776 160-3435-12 L050250PES00 Total/NA Solid Fill_Geo-0 67776 160-3435-13 L050251PRS00 Total/NA Solid Fill_Geo-0 67776 160-3435-14 L050252PES00 Total/NA Solid Fill_Geo-0 67776 160-3435-15 L050253PES00 Total/NA Solid Fill_Geo-0 67776 160-3435-16 L050254PES00 Total/NA Solid Fill_Geo-0 67776 160-3435-17 L050255PES00 Total/NA Solid Fill_Geo-0 67776 160-3435-18 L050256PRS00 Total/NA Solid Fill_Geo-0 67776 160-3435-19 L050257PES00 Total/NA Solid Fill_Geo-0 67776 160-3435-20 L050258PES00 Total/NA Solid Fill_Geo-0 LCS 160-68149/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-68149/1-A Method Blank Total/NA Prep Batch: 68361 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 67776 160-3435-21 L050259PRQ00 Total/NA Solid Fill_Geo-0 67776 160-3435-22 L050259PRS00 Total/NA Solid Fill_Geo-0 67776 160-3435-23 L050260PES00 Total/NA Solid Fill_Geo-0 67776 160-3435-24 L050261PRS00 Total/NA Solid Fill_Geo-0 67776 160-3435-25 L050262PES00 Total/NA Solid Fill_Geo-0 67776 160-3435-26 L050263PES00 Total/NA Solid Fill_Geo-0 67776 160-3435-27 L050264PRS00 Total/NA Solid Fill_Geo-0 67776 160-3435-28 L050265PES00 Total/NA Solid Fill_Geo-0 67776 160-3435-29 L050266PUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-30 L050267PUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-31 L050268PUB00 Total/NA Solid Fill_Geo-0 67776 160-3435-31 DU L050268PUB00 Total/NA Solid Fill_Geo-0 LCS 160-68361/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-68361/1-A Method Blank Total/NA TestAmerica St. Louis Page 47 of 48 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-3435-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 90 160-3435-1 Percent Yield (Acceptance Limits)
L050190TUB00 90 160-3435-1 MS L050190TUB00 90 160-3435-1 MSD L050190TUB00 90 160-3435-2 L050191TUB00 91 160-3435-3 L050192TUB00 90 160-3435-4 L050193TUB00 89 160-3435-5 L050194TUB00 90 160-3435-6 L050195TUB00 92 160-3435-7 L050196TUB00 91 160-3435-8 L050197TUB00 90 160-3435-9 L050247PRS00 91 160-3435-10 L050248PES00 92 160-3435-11 L050249PRS00 91 160-3435-12 L050250PES00 88 160-3435-13 L050251PRS00 90 160-3435-14 L050252PES00 91 160-3435-15 L050253PES00 90 160-3435-16 L050254PES00 93 160-3435-17 L050255PES00 90 160-3435-18 L050256PRS00 87 160-3435-19 L050257PES00 89 160-3435-20 L050258PES00 92 160-3435-21 L050259PRQ00 90 160-3435-21 MS L050259PRQ00 90 160-3435-21 MSD L050259PRQ00 87 160-3435-22 L050259PRS00 90 160-3435-23 L050260PES00 88 160-3435-24 L050261PRS00 89 160-3435-25 L050262PES00 88 160-3435-26 L050263PES00 90 160-3435-27 L050264PRS00 89 160-3435-28 L050265PES00 92 160-3435-29 L050266PUB00 89 160-3435-30 L050267PUB00 95 160-3435-31 L050268PUB00 94 LCS 160-67949/2-A Lab Control Sample 95 LCS 160-67951/2-A Lab Control Sample 97 MB 160-67949/1-A Method Blank 94 MB 160-67951/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 48 of 48 1
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