ML18019A710
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3585-2 Client Project/Site: RFP-CBA-022 (7 DAY TAT)
For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:
9/27/2013 5:13:00 PM Ivan Vania, Project Manager I (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-3585-2 Page 2 of 17 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
4 Receipt Checklists.........................................
6 Definitions/Glossary.......................................
7 Method Summary.........................................
8 Sample Summary.........................................
9 Client Sample Results......................................
10 QC Sample Results........................................
16 QC Association Summary...................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3585-2 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3585-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)
Report Number: 160-3585-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 08/30/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 20.0 C.
RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)
Samples L0501100TUB0 (160-3585-1), L0501101TUB0 (160-3585-2), L0501102TUB0 (160-3585-3), L0501103TUB0 (160-3585-4),
L0501104TUB0 (160-3585-5), L0501105TUB0 (160-3585-6), L0501106TUB0 (160-3585-7), L0501107TUB0 (160-3585-8),
L0501108TUB0 (160-3585-9), L050198TUB00 (160-3585-10), L050199TUB00 (160-3585-11), L050146TSS00 (160-3585-12) and L050147TRS00 (160-3585-13) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 09/03/2013, prepared on 09/05/2013 and analyzed on 09/26/2013.
No other difficulties were encountered during the Radium 226 analysis. All other quality control parameters were within the acceptance limits.
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,Procedure BDP-PR-QA-006, Chain of Custody Pagel ofl Hematite Decommissioning Project !Revision: 3 I
I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to BDP.
Chain of Cutod ID No_
F-083013-01 Pae 1/1 Project Name:
Westinghouse Electric Company Contact Person:
Gerald Rood
-~
Phone Number:
314-810-3382
. ' \\ *;:.
Sampler Name
<<l JeffHo:ffman; Scott Jenkins 8
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'i Sample ID Date Time Matrix 811~1~ c 0~~ ~ ~ [;'~"
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L0501100TUBO 8/29/2013 13:15 s
Ct~~';;
J S:
X L0501101 TUBO 8/29/2013 13:30 s
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q~; X
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L050I 102TUBO 8/29/2013 13:45 s
C C'J i\\-;:
- i X
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L0501103TUBO 8/29/2013 14:00 s
C ~~ k X, x '
L0501104TUBO 8/29/2013 13:00 s
C ~;@ I
- .JC X IL.
LOSO l 105TUBO 8/29/2013 13:15 s
C ~~
Jf ; X. S"
1:1.::C..
L0501106TUBO 8/29/2013 13:25 s
C J$;f? ~-*-*
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L050 l 107TUBO 8/29/2013 13:40 s
C '4(~ ?
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L050 l 108TUBO 8/29/2013 18:00 s
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- X, X :/
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L050198TUBOO 8/28/2013 11:20 s
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L050199TUBOO 8/29/2013 13:00 s
C :)~ ~I Ii~ X ****-
7,(.~e Relinquished J:,y: ---
Date/Time
&/30/!3 Company Name:,, t;L.-
Date/Time
[pi°?J n*, 10 Relinquished by:
Date/Time Received by:
Date/Time Company Name:
Company Name:
Laboratorv Name:
TA-MO
,Laboratory Address:
13715 Rider Trail North
[:'.:
"' *.s Phone No.
"' 314-298-8566 0 u
-a Laboratory Contact Person:
0 Joe Walker E-<
Phone No.
708-870-8453 Turn Around Time Rush (7 days)
~~! ";:f Remarks
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1 1 I L.SA DS--o I 13/a.S Cooler Temperature:
Shipper and Number:
Comments: Please re-analyze samples after 21-day ingrowth period.
V eri.fied By:
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10 11 Procedure HDP-PR-QA-006, Chain of Custody Page 1 of 1 Hematite Decommissioning Project !Revision: 3 I
I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006*1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign 1he CoC. The Labonrtory/End User must verify that 1he sample is correctly identified before 1he sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutody ID No. I F-083013-02 Page Project Name:
Westinghouse Electric Company Contact Person:
Gerald Rood Phone Number:
314-81{)-3_3 82 Sampler Name Thomas Yardy Sample JD L050146TSSOO L050147TRS00 Relinquished by;,
Company Namelc.) pl.,
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Compan~:
Relinquished by:
Company Name:
Date Time 8/30/2013 8:10 8/30/2013 8:30 Date/Time g/y;/13 Date/Time
<:g/-;;0//3 J )~,o Date/Time 1/1
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Matrix 8
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Date/Time 12.4>
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Date/Time g,30(\\~
Date/Time Total Laboratory Name:
TA-MO Laboratory Address:
13715 Rider Trail North t ct---------------------i
- .s Phone No.
C 8 314-298-8566 "El Laboratory Contact Person:
~ Joe Walker Phone No.
708-870-8_453 Rush Turn Around Tune (7 days)
Remarks DS'-D3 0YD3 Cooler Temperature:
Cooler ID: I Shipper and Number:
Comments: Please re-analyze samples after 21-day ingrowth period.
Verified By: c
Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3585-2 Login Number: 3585 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
False Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-3585-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Qualifiers Rad Qualifier Description U
Indicates the analyte was analyzed for but not detected.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-3585-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 17 1
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Sample Summary TestAmerica Job ID: 160-3585-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-3585-1 L0501100TUB0 Solid 08/29/13 13:15 08/30/13 18:00 160-3585-2 L0501101TUB0 Solid 08/29/13 13:30 08/30/13 18:00 160-3585-3 L0501102TUB0 Solid 08/29/13 13:45 08/30/13 18:00 160-3585-4 L0501103TUB0 Solid 08/29/13 14:00 08/30/13 18:00 160-3585-5 L0501104TUB0 Solid 08/29/13 13:00 08/30/13 18:00 160-3585-6 L0501105TUB0 Solid 08/29/13 13:15 08/30/13 18:00 160-3585-7 L0501106TUB0 Solid 08/29/13 13:25 08/30/13 18:00 160-3585-8 L0501107TUB0 Solid 08/29/13 13:40 08/30/13 18:00 160-3585-9 L0501108TUB0 Solid 08/29/13 18:00 08/30/13 18:00 160-3585-10 L050198TUB00 Solid 08/29/13 11:20 08/30/13 18:00 160-3585-11 L050199TUB00 Solid 08/29/13 13:00 08/30/13 18:00 160-3585-12 L050146TSS00 Solid 08/30/13 08:10 08/30/13 18:00 160-3585-13 L050147TRS00 Solid 08/30/13 08:30 08/30/13 18:00 TestAmerica St. Louis Page 9 of 17 1
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Client Sample Results TestAmerica Job ID: 160-3585-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-1 Client Sample ID: L0501100TUB0 Matrix: Solid Date Collected: 08/29/13 13:15 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.249 (2+/-)
0.0847 (2+/-)
1 09/26/13 08:15 09/05/13 12:05 pCi/g 0.127 RL MDC 0.0808 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 08:15 1
0.193 0.226 0.221 0.459 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 08:15 1
0.0552 0.0926 0.0784 0.474 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 08:15 1
0.0481 0.0619 0.0467 0.315 Lead 212 pCi/g 09/05/13 12:05 09/26/13 08:15 1
0.0608 0.0807 0.0606 0.514 Lead 214 pCi/g 09/05/13 12:05 09/26/13 08:15 1
0.288 1.09 0.813 7.15 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 08:15 1
0.781 0.0633 0.0628 U
0.0745 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 08:15 1
0.0552 1.00 0.0926 0.0784 0.474 Radium 226 pCi/g 09/05/13 12:05 09/26/13 08:15 1
0.127 0.0847 0.0808 0.249 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 08:15 1
0.635 0.290 0.277 0.821 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 08:15 1
0.167 0.0932 0.0928 U
0.0862 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 08:15 1
0.0618 0.0364 0.0364 U
0.0193 Americium 241 pCi/g 09/05/13 12:05 09/26/13 08:15 1
4.98 2.72 2.71 U
1.90 Protactinium 234m Lab Sample ID: 160-3585-2 Client Sample ID: L0501101TUB0 Matrix: Solid Date Collected: 08/29/13 13:30 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.19 (2+/-)
0.215 (2+/-)
1 09/26/13 08:11 09/05/13 12:05 pCi/g 0.132 RL MDC 0.178 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 08:11 1
0.550 0.667 0.643 1.70 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 08:11 1
0.154 0.257 0.215 1.36 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 08:11 1
0.140 0.205 0.141 1.15 Lead 212 pCi/g 09/05/13 12:05 09/26/13 08:11 1
0.0850 0.236 0.163 1.65 Lead 214 pCi/g 09/05/13 12:05 09/26/13 08:11 1
0.921 2.66 1.92 18.1 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 08:11 1
2.26 0.593 0.588 U
0.745 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 08:11 1
0.154 1.00 0.257 0.215 1.36 Radium 226 pCi/g 09/05/13 12:05 09/26/13 08:11 1
0.132 0.215 0.178 1.19 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 08:11 1
2.14 1.81 1.79 2.79 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 08:11 1
0.519 0.292 0.290 U
0.346 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 08:11 1
0.205 0.119 0.119 U
0.0113 Americium 241 pCi/g 09/05/13 12:05 09/26/13 08:11 1
11.4 7.14 7.14 U
1.95 Protactinium 234m Lab Sample ID: 160-3585-3 Client Sample ID: L0501102TUB0 Matrix: Solid Date Collected: 08/29/13 13:45 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.231 (2+/-)
0.0883 (2+/-)
1 09/26/13 08:16 09/05/13 12:05 pCi/g 0.105 RL MDC 0.0851 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 08:16 1
0.153 0.273 0.259 0.810 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 08:16 1
0.0601 0.0864 0.0764 0.388 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 08:16 1
0.0478 0.0555 0.0452 0.249 Lead 212 TestAmerica St. Louis Page 10 of 17 1
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Client Sample Results TestAmerica Job ID: 160-3585-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-3 Client Sample ID: L0501102TUB0 Matrix: Solid Date Collected: 08/29/13 13:45 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 0.432 (2+/-)
0.0806 (2+/-)
1 09/26/13 08:16 09/05/13 12:05 pCi/g 0.0608 RL MDC 0.0669 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 08:16 1
0.335 1.21 0.923 7.58 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 08:16 1
0.944 0.356 0.355 U
0.243 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 08:16 1
0.0601 1.00 0.0864 0.0764 0.388 Radium 226 pCi/g 09/05/13 12:05 09/26/13 08:16 1
0.105 0.0883 0.0851 0.231 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 08:16 1
0.745 0.240 0.236 U
0.437 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 08:16 1
0.192 0.110 0.109 U
0.105 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 08:16 1
0.0792 0.0471 0.0470 U
0.0192 Americium 241 pCi/g 09/05/13 12:05 09/26/13 08:16 1
4.15 2.73 2.70 U
3.40 Protactinium 234m Lab Sample ID: 160-3585-4 Client Sample ID: L0501103TUB0 Matrix: Solid Date Collected: 08/29/13 14:00 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.583 (2+/-)
0.201 (2+/-)
1 09/26/13 08:13 09/05/13 12:05 pCi/g 0.118 RL MDC 0.192 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 08:13 1
1.44 0.415 0.415 U
0.000 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 08:13 1
0.171 0.213 0.192 0.881 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 08:13 1
0.143 0.110 0.102 0.318 Lead 212 pCi/g 09/05/13 12:05 09/26/13 08:13 1
0.160 0.209 0.182 0.988 Lead 214 pCi/g 09/05/13 12:05 09/26/13 08:13 1
1.21 1.38 1.28 5.22 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 08:13 1
2.28 0.630 0.627 U
0.608 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 08:13 1
0.171 1.00 0.213 0.192 0.881 Radium 226 pCi/g 09/05/13 12:05 09/26/13 08:13 1
0.118 0.201 0.192 0.583 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 08:13 1
2.45 2.05 2.01 3.95 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 08:13 1
0.422 0.393 0.382 0.897 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 08:13 1
0.244 0.142 0.142 U
0.0348 Americium 241 pCi/g 09/05/13 12:05 09/26/13 08:13 1
14.1 7.17 7.17 U
0.235 Protactinium 234m Lab Sample ID: 160-3585-5 Client Sample ID: L0501104TUB0 Matrix: Solid Date Collected: 08/29/13 13:00 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.218 (2+/-)
0.0643 (2+/-)
1 09/26/13 09:23 09/05/13 12:05 pCi/g 0.0874 RL MDC 0.0603 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 09:23 1
0.332 0.206 0.205 U
0.188 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 09:23 1
0.0423 0.0997 0.0724 0.659 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 09:23 1
0.0356 0.0494 0.0350 0.269 Lead 212 pCi/g 09/05/13 12:05 09/26/13 09:23 1
0.0447 0.0973 0.0634 0.710 Lead 214 pCi/g 09/05/13 12:05 09/26/13 09:23 1
0.188 0.785 0.566 5.31 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 09:23 1
0.580 0.294 0.293 U
0.218 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 09:23 1
0.0423 1.00 0.0997 0.0724 0.659 Radium 226 TestAmerica St. Louis Page 11 of 17 1
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Client Sample Results TestAmerica Job ID: 160-3585-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-5 Client Sample ID: L0501104TUB0 Matrix: Solid Date Collected: 08/29/13 13:00 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 232 0.218 (2+/-)
0.0643 (2+/-)
1 09/26/13 09:23 09/05/13 12:05 pCi/g 0.0874 RL MDC 0.0603 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 09:23 1
0.505 0.260 0.243 0.895 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 09:23 1
0.109 0.0841 0.0828 0.146 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 09:23 1
0.0612 0.0796 0.0796 U
-0.0131 Americium 241 pCi/g 09/05/13 12:05 09/26/13 09:23 1
3.27 1.90 1.89 U
0.869 Protactinium 234m Lab Sample ID: 160-3585-6 Client Sample ID: L0501105TUB0 Matrix: Solid Date Collected: 08/29/13 13:15 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.731 (2+/-)
0.152 (2+/-)
1 09/26/13 09:24 09/05/13 12:05 pCi/g 0.156 RL MDC 0.132 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.519 0.321 0.319 U
0.278 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.0647 0.174 0.126 1.15 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.0772 0.104 0.0721 0.580 Lead 212 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.0975 0.173 0.122 1.18 Lead 214 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.335 2.15 1.35 16.3 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 09:24 1
1.35 0.814 0.812 U
-0.556 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.0647 1.00 0.174 0.126 1.15 Radium 226 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.156 0.152 0.132 0.731 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 09:24 1
1.05 0.896 0.874 1.86 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.292 0.169 0.167 U
0.257 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.121 0.0724 0.0723 U
0.0329 Americium 241 pCi/g 09/05/13 12:05 09/26/13 09:24 1
7.86 3.65 3.65 U
0.217 Protactinium 234m Lab Sample ID: 160-3585-7 Client Sample ID: L0501106TUB0 Matrix: Solid Date Collected: 08/29/13 13:25 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.949 (2+/-)
0.177 (2+/-)
1 09/26/13 09:24 09/05/13 12:05 pCi/g 0.0980 RL MDC 0.149 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.329 0.356 0.340 0.998 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.0764 0.159 0.112 1.08 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.0544 0.133 0.0681 0.886 Lead 212 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.0704 0.161 0.0952 1.25 Lead 214 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.234 2.05 1.11 16.8 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 09:24 1
1.03 0.205 0.203 U
0.228 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.0764 1.00 0.159 0.112 1.08 Radium 226 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.0980 0.177 0.149 0.949 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.872 0.711 0.684 1.84 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.234 0.144 0.144 U
0.141 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 09:24 1
0.0747 0.0437 0.0437 U
-0.000888 Americium 241 TestAmerica St. Louis Page 12 of 17 1
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Client Sample Results TestAmerica Job ID: 160-3585-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-7 Client Sample ID: L0501106TUB0 Matrix: Solid Date Collected: 08/29/13 13:25 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Protactinium 234m 1.90 U
(2+/-)
2.89 (2+/-)
1 09/26/13 09:24 09/05/13 12:05 pCi/g 5.09 RL MDC 2.88 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Lab Sample ID: 160-3585-8 Client Sample ID: L0501107TUB0 Matrix: Solid Date Collected: 08/29/13 13:40 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.136 (2+/-)
0.0531 (2+/-)
1 09/26/13 09:25 09/05/13 12:05 pCi/g 0.0884 RL MDC 0.0513 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 09:25 1
0.339 0.210 0.209 U
0.189 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 09:25 1
0.0440 0.106 0.0801 0.662 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 09:25 1
0.0437 0.0359 0.0321 0.123 Lead 212 pCi/g 09/05/13 12:05 09/26/13 09:25 1
0.0494 0.106 0.0764 0.714 Lead 214 pCi/g 09/05/13 12:05 09/26/13 09:25 1
0.128 0.971 0.683 6.74 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 09:25 1
0.679 0.115 0.114 U
0.105 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 09:25 1
0.0440 1.00 0.106 0.0801 0.662 Radium 226 pCi/g 09/05/13 12:05 09/26/13 09:25 1
0.0884 0.0531 0.0513 0.136 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 09:25 1
0.549 0.212 0.206 U
0.491 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 09:25 1
0.108 0.0816 0.0806 0.124 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 09:25 1
0.0458 0.0322 0.0321 U
0.0293 Americium 241 pCi/g 09/05/13 12:05 09/26/13 09:25 1
4.43 0.933 0.932 U
0.000 Protactinium 234m Lab Sample ID: 160-3585-9 Client Sample ID: L0501108TUB0 Matrix: Solid Date Collected: 08/29/13 18:00 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.385 (2+/-)
0.194 (2+/-)
1 09/26/13 08:39 09/05/13 12:05 pCi/g 0.255 RL MDC 0.190 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 08:39 1
0.948 0.560 0.559 U
0.327 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 08:39 1
0.181 0.199 0.186 0.668 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 08:39 1
0.131 0.101 0.0947 0.280 Lead 212 pCi/g 09/05/13 12:05 09/26/13 08:39 1
0.156 0.145 0.130 0.602 Lead 214 pCi/g 09/05/13 12:05 09/26/13 08:39 1
1.52 0.760 0.758 U
0.454 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 08:39 1
1.93 1.13 1.13 U
-0.393 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 08:39 1
0.181 1.00 0.199 0.186 0.668 Radium 226 pCi/g 09/05/13 12:05 09/26/13 08:39 1
0.255 0.194 0.190 0.385 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 08:39 1
1.83 0.531 0.520 U
1.00 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 08:39 1
0.338 0.253 0.251 U
0.294 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 08:39 1
0.142 0.0837 0.0836 U
0.0295 Americium 241 pCi/g 09/05/13 12:05 09/26/13 08:39 1
10.7 5.85 5.83 U
5.71 Protactinium 234m TestAmerica St. Louis Page 13 of 17 1
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Client Sample Results TestAmerica Job ID: 160-3585-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-10 Client Sample ID: L050198TUB00 Matrix: Solid Date Collected: 08/29/13 11:20 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.934 (2+/-)
0.174 (2+/-)
1 09/26/13 10:49 09/05/13 12:05 pCi/g 0.0985 RL MDC 0.146 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.550 0.383 0.376 0.686 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.0660 0.172 0.121 1.17 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.0680 0.139 0.0760 0.900 Lead 212 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.0817 0.168 0.103 1.27 Lead 214 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.178 2.26 1.32 17.9 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 10:49 1
1.21 0.357 0.354 U
0.397 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.0660 1.00 0.172 0.121 1.17 Radium 226 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.0985 0.174 0.146 0.934 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.931 0.347 0.337 U
0.827 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.277 0.164 0.164 U
0.0197 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.114 0.0682 0.0681 U
0.0237 Americium 241 pCi/g 09/05/13 12:05 09/26/13 10:49 1
7.30 4.10 4.10 U
0.171 Protactinium 234m Lab Sample ID: 160-3585-11 Client Sample ID: L050199TUB00 Matrix: Solid Date Collected: 08/29/13 13:00 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.11 (2+/-)
0.266 (2+/-)
1 09/26/13 08:40 09/05/13 12:05 pCi/g 0.330 RL MDC 0.241 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 08:40 1
0.960 0.660 0.651 1.01 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 08:40 1
0.192 0.233 0.207 1.02 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 08:40 1
0.128 0.169 0.122 0.906 Lead 212 pCi/g 09/05/13 12:05 09/26/13 08:40 1
0.195 0.218 0.172 1.28 Lead 214 pCi/g 09/05/13 12:05 09/26/13 08:40 1
1.14 3.04 2.15 21.0 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 08:40 1
1.60 0.790 0.778 U
1.26 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 08:40 1
0.192 1.00 0.233 0.207 1.02 Radium 226 pCi/g 09/05/13 12:05 09/26/13 08:40 1
0.330 0.266 0.241 1.11 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 08:40 1
1.63 1.27 1.26 1.65 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 08:40 1
0.438 0.271 0.270 U
0.237 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 08:40 1
0.179 0.107 0.107 U
0.0443 Americium 241 pCi/g 09/05/13 12:05 09/26/13 08:40 1
10.7 6.97 6.94 U
6.41 Protactinium 234m Lab Sample ID: 160-3585-12 Client Sample ID: L050146TSS00 Matrix: Solid Date Collected: 08/30/13 08:10 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.188 (2+/-)
0.0528 (2+/-)
1 09/26/13 10:49 09/05/13 12:05 pCi/g 0.0579 RL MDC 0.0492 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.246 0.155 0.155 U
0.163 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.0386 0.0845 0.0606 0.566 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.0314 0.0352 0.0272 0.174 Lead 212 TestAmerica St. Louis Page 14 of 17 1
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Client Sample Results TestAmerica Job ID: 160-3585-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-12 Client Sample ID: L050146TSS00 Matrix: Solid Date Collected: 08/30/13 08:10 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 0.582 (2+/-)
0.0782 (2+/-)
1 09/26/13 10:49 09/05/13 12:05 pCi/g 0.0366 RL MDC 0.0496 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.193 0.973 0.579 7.64 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.558 0.118 0.118 U
0.0707 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.0386 1.00 0.0845 0.0606 0.566 Radium 226 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.0579 0.0528 0.0492 0.188 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.452 0.171 0.165 U
0.425 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.101 0.0620 0.0613 U
0.0947 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 10:49 1
0.0496 0.0299 0.0298 U
0.0187 Americium 241 pCi/g 09/05/13 12:05 09/26/13 10:49 1
3.18 5.51 5.51 U
-0.194 Protactinium 234m Lab Sample ID: 160-3585-13 Client Sample ID: L050147TRS00 Matrix: Solid Date Collected: 08/30/13 08:30 Date Received: 08/30/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.190 (2+/-)
0.0522 (2+/-)
1 09/26/13 08:17 09/05/13 12:05 pCi/g 0.0429 RL MDC 0.0484 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 12:05 09/26/13 08:17 1
0.230 0.156 0.154 0.235 Bismuth 212 pCi/g 09/05/13 12:05 09/26/13 08:17 1
0.0387 0.0727 0.0562 0.444 Bismuth 214 pCi/g 09/05/13 12:05 09/26/13 08:17 1
0.0295 0.0332 0.0258 0.162 Lead 212 pCi/g 09/05/13 12:05 09/26/13 08:17 1
0.0305 0.0683 0.0481 0.467 Lead 214 pCi/g 09/05/13 12:05 09/26/13 08:17 1
0.193 0.904 0.562 6.92 Potassium 40 pCi/g 09/05/13 12:05 09/26/13 08:17 1
0.481 0.189 0.189 U
0.0964 Protactinium 231 pCi/g 09/05/13 12:05 09/26/13 08:17 1
0.0387 1.00 0.0727 0.0562 0.444 Radium 226 pCi/g 09/05/13 12:05 09/26/13 08:17 1
0.0429 0.0522 0.0484 0.190 Thorium 232 pCi/g 09/05/13 12:05 09/26/13 08:17 1
0.390 0.148 0.142 0.424 Thorium 234 pCi/g 09/05/13 12:05 09/26/13 08:17 1
0.117 0.0726 0.0726 U
0.0119 Uranium 235 pCi/g 09/05/13 12:05 09/26/13 08:17 1
0.0492 0.0291 0.0291 U
0.00520 Americium 241 pCi/g 09/05/13 12:05 09/26/13 08:17 1
2.72 0.861 0.850 U
1.38 Protactinium 234m TestAmerica St. Louis Page 15 of 17 1
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QC Sample Results TestAmerica Job ID: 160-3585-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-70785/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 75044 Prep Batch: 70785 Actinium 228 Analyte U
1 09/26/13 19:21 09/05/13 12:05 pCi/g 0.0598 MDC RL 0.0147 0.0147 (2+/-)
(2+/-)
MB 0.002817 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
09/26/13 19:21 09/05/13 12:05 pCi/g 0.186 0.0955 0.0955 U
0.001730 Bismuth 212 1
09/26/13 19:21 09/05/13 12:05 pCi/g 0.0397 0.0803 0.0803 U
-0.01288 Bismuth 214 1
09/26/13 19:21 09/05/13 12:05 pCi/g 0.0245 0.0125 0.0125 U
0.004282 Lead 212 1
09/26/13 19:21 09/05/13 12:05 pCi/g 0.0346 0.0148 0.0148 U
-0.004057 Lead 214 1
09/26/13 19:21 09/05/13 12:05 pCi/g 0.252 5.98 5.98 U
-0.1494 Potassium 40 1
09/26/13 19:21 09/05/13 12:05 pCi/g 0.310 0.170 0.170 U
0.03673 Protactinium 231 1
09/26/13 19:21 09/05/13 12:05 pCi/g 0.0397 1.00 0.0803 0.0803 U
-0.01288 Radium 226 1
09/26/13 19:21 09/05/13 12:05 pCi/g 0.0598 0.0147 0.0147 U
0.002817 Thorium 232 1
09/26/13 19:21 09/05/13 12:05 pCi/g 0.292 0.0233 0.0232 U
0.01597 Thorium 234 1
09/26/13 19:21 09/05/13 12:05 pCi/g 0.0637 0.0348 0.0348 U
-0.0008006 Uranium 235 1
09/26/13 19:21 09/05/13 12:05 pCi/g 0.0247 0.0138 0.0138 U
0.001479 Americium 241 1
09/26/13 19:21 09/05/13 12:05 pCi/g 2.62 19.2 19.2 U
-0.4795 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-70785/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 75044 Prep Batch: 70785 Americium 241 Analyte 116 87 95 92.66 97.7 9.64 0.419 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 31.6 30.74 3.22 0.109 pCi/g 97 87 - 120 Cobalt 60 24.5 23.20 2.34 0.0701 pCi/g 95 87 - 115 Client Sample ID: L050147TRS00 Lab Sample ID: 160-3585-13 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 75044 Prep Batch: 70785 Actinium 228 Analyte 1
0.43 0.1477 0.190 0.0460 0.0634 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 0.235 0.1692 U
0.147 0.229 pCi/g 0.22 1
Bismuth 214 0.444 0.4597 0.0690 0.0302 pCi/g 0.11 1
Lead 212 0.162 0.1517 0.0316 0.0285 pCi/g 0.16 1
Lead 214 0.467 0.4864 0.0720 0.0507 pCi/g 0.14 1
Potassium 40 6.92 7.552 0.959 0.188 pCi/g 0.34 1
Protactinium 231 0.0964 U
0.07967 U
0.115 0.497 pCi/g 0.06 1
Radium 226 0.444 0.4597 0.0690 1.00 0.0302 pCi/g 0.11 1
Thorium 232 0.190 0.1477 0.0460 0.0634 pCi/g 0.43 1
Thorium 234 0.424 0.4659 0.176 0.374 pCi/g 0.13 1
Uranium 235 0.0119 U
0.05491 U
0.0732 0.122 pCi/g 0.29 1
Americium 241 0.00520 U
-0.00079 42 U
0.0322 0.0547 pCi/g 0.1 1
Protactinium 234m 1.38 U
0.1482 U
1.55 2.87 pCi/g 0.51 1
TestAmerica St. Louis Page 16 of 17 1
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QC Association Summary TestAmerica Job ID: 160-3585-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Rad Leach Batch: 70118 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3585-1 L0501100TUB0 Total/NA Solid Dry and Grind 160-3585-2 L0501101TUB0 Total/NA Solid Dry and Grind 160-3585-3 L0501102TUB0 Total/NA Solid Dry and Grind 160-3585-4 L0501103TUB0 Total/NA Solid Dry and Grind 160-3585-5 L0501104TUB0 Total/NA Solid Dry and Grind 160-3585-6 L0501105TUB0 Total/NA Solid Dry and Grind 160-3585-7 L0501106TUB0 Total/NA Solid Dry and Grind 160-3585-8 L0501107TUB0 Total/NA Solid Dry and Grind 160-3585-9 L0501108TUB0 Total/NA Solid Dry and Grind 160-3585-10 L050198TUB00 Total/NA Solid Dry and Grind 160-3585-11 L050199TUB00 Total/NA Solid Dry and Grind 160-3585-12 L050146TSS00 Total/NA Solid Dry and Grind 160-3585-13 L050147TRS00 Total/NA Solid Dry and Grind 160-3585-13 DU L050147TRS00 Total/NA Prep Batch: 70785 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 70118 160-3585-1 L0501100TUB0 Total/NA Solid Fill_Geo-21 70118 160-3585-2 L0501101TUB0 Total/NA Solid Fill_Geo-21 70118 160-3585-3 L0501102TUB0 Total/NA Solid Fill_Geo-21 70118 160-3585-4 L0501103TUB0 Total/NA Solid Fill_Geo-21 70118 160-3585-5 L0501104TUB0 Total/NA Solid Fill_Geo-21 70118 160-3585-6 L0501105TUB0 Total/NA Solid Fill_Geo-21 70118 160-3585-7 L0501106TUB0 Total/NA Solid Fill_Geo-21 70118 160-3585-8 L0501107TUB0 Total/NA Solid Fill_Geo-21 70118 160-3585-9 L0501108TUB0 Total/NA Solid Fill_Geo-21 70118 160-3585-10 L050198TUB00 Total/NA Solid Fill_Geo-21 70118 160-3585-11 L050199TUB00 Total/NA Solid Fill_Geo-21 70118 160-3585-12 L050146TSS00 Total/NA Solid Fill_Geo-21 70118 160-3585-13 L050147TRS00 Total/NA Solid Fill_Geo-21 70118 160-3585-13 DU L050147TRS00 Total/NA Solid Fill_Geo-21 LCS 160-70785/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-70785/1-A Method Blank Total/NA TestAmerica St. Louis Page 17 of 17 1
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