ML18019A712

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Westinghouse Hematite Decommissioning Project - Final Status Survey Final Report Volume 3, Chapter 16, Survey Area Release Record for Land Survey Area 05, Survey Units 01, 02, 03 and 04, Revision 1, J4091-2 Uds Level 2 Report
ML18019A712
Person / Time
Site: 07000036
Issue date: 12/04/2013
From: Vania I
TestAmerica Labs - St. Louis, Westinghouse
To: Swanson M
Office of Nuclear Material Safety and Safeguards, Westinghouse
Shared Package
ML18019A532 List: ... further results
References
HEM-18-2 160-4091-2
Download: ML18019A712 (13)
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-4091-2 Client Project/Site: RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

12/4/2013 1:07:27 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-4091-2 Page 2 of 13 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

4 Receipt Checklists.........................................

5 Definitions/Glossary.......................................

6 Method Summary.........................................

7 Sample Summary.........................................

8 Client Sample Results......................................

9 QC Sample Results........................................

12 QC Association Summary...................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-4091-2 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-4091-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)

Report Number: 160-4091-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 10/11/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 2.0 C.

RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)

Samples L050343PUB00 (160-4091-1), L050344PUB00 (160-4091-2), L050345PUB00 (160-4091-3), L050346PUB00 (160-4091-4),

L050347PUB00 (160-4091-5) and L050348PUB00 (160-4091-6) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 12/02/2013, prepared on 10/16/2013 and analyzed on 12/03/2013.

No difficulties were encountered during the Radium 226 analysis. All other quality control parameters were within the acceptance limits.

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10 11 Procedure HDP-PR-QA-006, Chain o(Cu.stody Hematite Decommissioning Project Revision: 3 I

Page I ofl Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutodv ID No_

F-101013-01 Pa2:e 1/1 Reauested Analysis Laborato.-v Name:

Project Name:

TA-MO

\\0 Westinghouse Electric Company N

N Contact Person:

-* : ~

Laboratory Address:

Gerald Rood

'8 13715 Rider Trail North

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Phone Number:

  • ea Phone No_

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314-810-3382

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314-298-8566

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u Sampler Name

'El Laboratory Contact Person:

"O I Andrew Schooley

§:

E

~ Joe Walker

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Phone No_

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708-870-8453 0

Q.

Q.

00..

00 Turn Around Time Q I>

u c,j "f -O'i: E Rush (7 days)

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Sample ID Date Time

.Matrix s

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Remarks 0

C::,..

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u L050343PUBOO 10/9/2013 16:05 s

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X X

1 LSA-o<- 0~

{<., ;Q' L050344PUBOO 10/9/2013 16:15 s

C X

X X

1

'J

L050345PUBOO 10/9/2013 16:25 s

C X

X X

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L050346PUBOO 10/9/2013 16:10 s

C X

X X

1 L050347PUBOO 10/9/2013 16:20 s

C X

X X

1

\\.V L050348PUBOO 10/9/2013 16:30 s

C X

X X

1 L.SA-oS-, n3

(<. '-ti <:.

Relinquished by: C...

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Date/Time Receiv~y:

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Date/Time Total Cooler Temperature:

~ [ 0-/f--t 3

,/"",t.,,., :, - --

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6 Amhie,nt Comoany Name: W CL--

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,, Company Name:

ifj.,.v,<o\\O Cooler ID: Shipper and Number:

Cross 4> ads-1 OJ 0-01 Received bv:

Date/Time

~~dby:/d D,ate/Time Comments: Please re-analyze samples after 21-day ingrowth

- ~u'"t,bc~ period.

Company Name:

.,, Company N~~

(-

i/7'""9.

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\\ l Relinquished by:

Date/Time

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Date/Time

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c'-'-<<-r s Verified By:

Company Name:

Co~a:ny Name:

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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-4091-2 Login Number: 4091 Question Answer Comment Creator: Daniels, Brian J List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-4091-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Qualifiers Rad Qualifier Description U

Indicates the analyte was analyzed for but not detected.

Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-4091-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 7 of 13 1

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Sample Summary TestAmerica Job ID: 160-4091-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-4091-1 L050343PUB00 Solid 10/09/13 16:05 10/11/13 17:45 160-4091-2 L050344PUB00 Solid 10/09/13 16:15 10/11/13 17:45 160-4091-3 L050345PUB00 Solid 10/09/13 16:25 10/11/13 17:45 160-4091-4 L050346PUB00 Solid 10/09/13 16:10 10/11/13 17:45 160-4091-5 L050347PUB00 Solid 10/09/13 16:20 10/11/13 17:45 160-4091-6 L050348PUB00 Solid 10/09/13 16:30 10/11/13 17:45 TestAmerica St. Louis Page 8 of 13 1

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Client Sample Results TestAmerica Job ID: 160-4091-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4091-1 Client Sample ID: L050343PUB00 Matrix: Solid Date Collected: 10/09/13 16:05 Date Received: 10/11/13 17:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.987 (2+/-)

0.165 (2+/-)

1 12/03/13 21:45 10/16/13 11:32 pCi/g 0.175 RL MDC 0.131 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.417 0.542 0.514 1.66 Bismuth 212 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.0858 0.181 0.128 1.23 Bismuth 214 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.0618 0.164 0.0783 1.11 Lead 212 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.0847 0.175 0.103 1.36 Lead 214 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.362 2.58 1.36 21.4 Potassium 40 pCi/g 10/16/13 11:32 12/03/13 21:45 1

1.21 0.253 0.250 U

0.368 Protactinium 231 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.0858 1.00 0.181 0.128 1.23 Radium 226 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.175 0.165 0.131 0.987 Thorium 232 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.948 0.794 0.765 2.02 Thorium 234 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.252 0.160 0.160 U

0.102 Uranium 235 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.105 0.0623 0.0623 U

-0.00173 Americium 241 pCi/g 10/16/13 11:32 12/03/13 21:45 1

7.39 2.58 2.55 U

3.60 Protactinium 234m Lab Sample ID: 160-4091-2 Client Sample ID: L050344PUB00 Matrix: Solid Date Collected: 10/09/13 16:15 Date Received: 10/11/13 17:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.16 (2+/-)

0.205 (2+/-)

1 12/03/13 21:45 10/16/13 11:32 pCi/g 0.124 RL MDC 0.168 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.378 0.384 0.372 0.920 Bismuth 212 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.101 0.174 0.134 1.07 Bismuth 214 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.0711 0.166 0.0836 1.11 Lead 212 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.0849 0.176 0.115 1.28 Lead 214 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.632 2.42 1.39 19.3 Potassium 40 pCi/g 10/16/13 11:32 12/03/13 21:45 1

1.36 0.305 0.297 U

0.614 Protactinium 231 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.101 1.00 0.174 0.134 1.07 Radium 226 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.124 0.205 0.168 1.16 Thorium 232 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.986 0.827 0.805 1.78 Thorium 234 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.296 0.177 0.177 U

0.115 Uranium 235 pCi/g 10/16/13 11:32 12/03/13 21:45 1

0.126 0.0756 0.0756 U

-0.0285 Americium 241 pCi/g 10/16/13 11:32 12/03/13 21:45 1

5.69 3.49 3.48 U

2.88 Protactinium 234m Lab Sample ID: 160-4091-3 Client Sample ID: L050345PUB00 Matrix: Solid Date Collected: 10/09/13 16:25 Date Received: 10/11/13 17:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.882 (2+/-)

0.140 (2+/-)

1 12/03/13 21:46 10/16/13 11:32 pCi/g 0.144 RL MDC 0.108 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 10/16/13 11:32 12/03/13 21:46 1

0.686 0.400 0.400 U

0.0565 Bismuth 212 pCi/g 10/16/13 11:32 12/03/13 21:46 1

0.0596 0.166 0.105 1.24 Bismuth 214 pCi/g 10/16/13 11:32 12/03/13 21:46 1

0.0590 0.152 0.0698 1.04 Lead 212 TestAmerica St. Louis Page 9 of 13 1

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Client Sample Results TestAmerica Job ID: 160-4091-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4091-3 Client Sample ID: L050345PUB00 Matrix: Solid Date Collected: 10/09/13 16:25 Date Received: 10/11/13 17:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.21 (2+/-)

0.156 (2+/-)

1 12/03/13 21:46 10/16/13 11:32 pCi/g 0.0625 RL MDC 0.0933 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 10/16/13 11:32 12/03/13 21:46 1

0.384 2.27 1.11 19.3 Potassium 40 pCi/g 10/16/13 11:32 12/03/13 21:46 1

1.08 0.660 0.658 U

-0.541 Protactinium 231 pCi/g 10/16/13 11:32 12/03/13 21:46 1

0.0596 1.00 0.166 0.105 1.24 Radium 226 pCi/g 10/16/13 11:32 12/03/13 21:46 1

0.144 0.140 0.108 0.882 Thorium 232 pCi/g 10/16/13 11:32 12/03/13 21:46 1

0.838 0.461 0.410 2.01 Thorium 234 pCi/g 10/16/13 11:32 12/03/13 21:46 1

0.175 0.144 0.140 0.326 Uranium 235 pCi/g 10/16/13 11:32 12/03/13 21:46 1

0.102 0.0614 0.0613 U

-0.0245 Americium 241 pCi/g 10/16/13 11:32 12/03/13 21:46 1

4.84 2.95 2.94 U

2.32 Protactinium 234m Lab Sample ID: 160-4091-4 Client Sample ID: L050346PUB00 Matrix: Solid Date Collected: 10/09/13 16:10 Date Received: 10/11/13 17:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.939 (2+/-)

0.174 (2+/-)

1 12/03/13 22:54 10/16/13 11:32 pCi/g 0.139 RL MDC 0.146 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.336 0.439 0.408 1.56 Bismuth 212 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.0846 0.170 0.119 1.17 Bismuth 214 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.0578 0.163 0.0736 1.13 Lead 212 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.0751 0.163 0.0934 1.28 Lead 214 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.308 2.39 1.17 20.3 Potassium 40 pCi/g 10/16/13 11:32 12/03/13 22:54 1

1.13 0.297 0.293 U

0.449 Protactinium 231 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.0846 1.00 0.170 0.119 1.17 Radium 226 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.139 0.174 0.146 0.939 Thorium 232 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.925 0.786 0.759 1.97 Thorium 234 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.179 0.130 0.129 U

0.122 Uranium 235 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.110 0.0668 0.0667 U

0.0457 Americium 241 pCi/g 10/16/13 11:32 12/03/13 22:54 1

5.59 3.20 3.20 U

1.15 Protactinium 234m Lab Sample ID: 160-4091-5 Client Sample ID: L050347PUB00 Matrix: Solid Date Collected: 10/09/13 16:20 Date Received: 10/11/13 17:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.10 (2+/-)

0.186 (2+/-)

1 12/03/13 22:55 10/16/13 11:32 pCi/g 0.116 RL MDC 0.148 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 10/16/13 11:32 12/03/13 22:55 1

0.685 0.397 0.397 U

0.0609 Bismuth 212 pCi/g 10/16/13 11:32 12/03/13 22:55 1

0.0704 0.173 0.116 1.24 Bismuth 214 pCi/g 10/16/13 11:32 12/03/13 22:55 1

0.0629 0.159 0.0742 1.09 Lead 212 pCi/g 10/16/13 11:32 12/03/13 22:55 1

0.0740 0.171 0.0972 1.36 Lead 214 pCi/g 10/16/13 11:32 12/03/13 22:55 1

0.411 2.24 1.18 18.6 Potassium 40 pCi/g 10/16/13 11:32 12/03/13 22:55 1

1.04 0.360 0.357 U

0.401 Protactinium 231 pCi/g 10/16/13 11:32 12/03/13 22:55 1

0.0704 1.00 0.173 0.116 1.24 Radium 226 TestAmerica St. Louis Page 10 of 13 1

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Client Sample Results TestAmerica Job ID: 160-4091-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4091-5 Client Sample ID: L050347PUB00 Matrix: Solid Date Collected: 10/09/13 16:20 Date Received: 10/11/13 17:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 1.10 (2+/-)

0.186 (2+/-)

1 12/03/13 22:55 10/16/13 11:32 pCi/g 0.116 RL MDC 0.148 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 10/16/13 11:32 12/03/13 22:55 1

0.862 0.343 0.330 0.888 Thorium 234 pCi/g 10/16/13 11:32 12/03/13 22:55 1

0.246 0.137 0.136 U

0.191 Uranium 235 pCi/g 10/16/13 11:32 12/03/13 22:55 1

0.0992 0.0591 0.0590 U

0.0111 Americium 241 pCi/g 10/16/13 11:32 12/03/13 22:55 1

5.40 3.35 3.33 U

3.15 Protactinium 234m Lab Sample ID: 160-4091-6 Client Sample ID: L050348PUB00 Matrix: Solid Date Collected: 10/09/13 16:30 Date Received: 10/11/13 17:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.11 (2+/-)

0.189 (2+/-)

1 12/03/13 22:54 10/16/13 11:32 pCi/g 0.100 RL MDC 0.151 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.593 0.412 0.405 0.756 Bismuth 212 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.0937 0.171 0.129 1.07 Bismuth 214 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.0820 0.146 0.0825 0.934 Lead 212 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.0678 0.162 0.109 1.15 Lead 214 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.644 2.41 1.40 19.2 Potassium 40 pCi/g 10/16/13 11:32 12/03/13 22:54 1

1.36 0.333 0.329 U

0.490 Protactinium 231 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.0937 1.00 0.171 0.129 1.07 Radium 226 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.100 0.189 0.151 1.11 Thorium 232 pCi/g 10/16/13 11:32 12/03/13 22:54 1

1.04 0.887 0.865 1.88 Thorium 234 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.196 0.153 0.150 0.283 Uranium 235 pCi/g 10/16/13 11:32 12/03/13 22:54 1

0.121 0.0725 0.0724 U

0.0207 Americium 241 pCi/g 10/16/13 11:32 12/03/13 22:54 1

5.97 3.48 3.48 U

1.64 Protactinium 234m TestAmerica St. Louis Page 11 of 13 1

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QC Sample Results TestAmerica Job ID: 160-4091-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-89240/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 89252 Prep Batch: 89240 Actinium 228 Analyte U

1 12/03/13 21:42 10/16/13 11:32 pCi/g 0.128 MDC RL 0.0225 0.0225 (2+/-)

(2+/-)

MB 0.0000 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

12/03/13 21:42 10/16/13 11:32 pCi/g 0.276 0.0497 0.0497 U

0.0000 Bismuth 212 1

12/03/13 21:42 10/16/13 11:32 pCi/g 0.0459 0.0249 0.0249 U

-0.005283 Bismuth 214 1

12/03/13 21:42 10/16/13 11:32 pCi/g 0.0259 0.0268 0.0268 U

-0.003650 Lead 212 1

12/03/13 21:42 10/16/13 11:32 pCi/g 0.0372 1.53 1.53 U

-0.01078 Lead 214 1

12/03/13 21:42 10/16/13 11:32 pCi/g 0.360 0.168 0.168 U

0.02478 Potassium 40 1

12/03/13 21:42 10/16/13 11:32 pCi/g 0.427 0.232 0.232 U

-0.04150 Protactinium 231 1

12/03/13 21:42 10/16/13 11:32 pCi/g 0.0459 1.00 0.0249 0.0249 U

-0.005283 Radium 226 1

12/03/13 21:42 10/16/13 11:32 pCi/g 0.128 0.0225 0.0225 U

0.0000 Thorium 232 1

12/03/13 21:42 10/16/13 11:32 pCi/g 0.290 0.454 0.454 U

-0.1068 Thorium 234 1

12/03/13 21:42 10/16/13 11:32 pCi/g 0.0575 0.0299 0.0299 U

-0.001085 Uranium 235 1

12/03/13 21:42 10/16/13 11:32 pCi/g 0.0203 0.0106 0.0106 U

-0.0004221 Americium 241 1

12/03/13 21:42 10/16/13 11:32 pCi/g 3.73 0.886 0.886 U

0.1555 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-89240/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 89040 Prep Batch: 89240 Americium 241 Analyte 116 87 95 92.45 97.7 9.62 0.480 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 31.5 30.21 3.16 0.128 pCi/g 96 87 - 120 Cobalt 60 23.9 22.26 2.25 0.0638 pCi/g 93 87 - 115 Client Sample ID: L050343PUB00 Lab Sample ID: 160-4091-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 89252 Prep Batch: 89240 Actinium 228 Analyte 1

0.62 1.251 0.987 0.262 0.148 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.66 1.592 0.619 0.552 pCi/g 0.06 1

Bismuth 214 1.23 1.253 0.201 0.100 pCi/g 0.07 1

Lead 212 1.11 1.145 0.174 0.0804 pCi/g 0.10 1

Lead 214 1.36 1.426 0.187 0.0964 pCi/g 0.18 1

Potassium 40 21.4 19.95 2.54 0.503 pCi/g 0.29 1

Protactinium 231 0.368 U

0.4554 U

0.398 1.31 pCi/g 0.13 1

Radium 226 1.23 1.253 0.201 1.00 0.100 pCi/g 0.07 1

Thorium 232 0.987 1.251 0.262 0.148 pCi/g 0.62 1

Thorium 234 2.02 1.634 0.709 0.925 pCi/g 0.26 1

Uranium 235 0.102 U

0.1355 U

0.139 0.267 pCi/g 0.11 1

Americium 241

-0.00173 U

0.02859 U

0.0711 0.119 pCi/g 0.23 1

Protactinium 234m 3.60 U

1.814 U

4.34 7.33 pCi/g 0.26 1

TestAmerica St. Louis Page 12 of 13 1

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QC Association Summary TestAmerica Job ID: 160-4091-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Rad Leach Batch: 88849 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-4091-1 L050343PUB00 Total/NA Solid Dry and Grind 160-4091-1 DU L050343PUB00 Total/NA Solid Dry and Grind 160-4091-2 L050344PUB00 Total/NA Solid Dry and Grind 160-4091-3 L050345PUB00 Total/NA Solid Dry and Grind 160-4091-4 L050346PUB00 Total/NA Solid Dry and Grind 160-4091-5 L050347PUB00 Total/NA Solid Dry and Grind 160-4091-6 L050348PUB00 Total/NA Prep Batch: 89240 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 88849 160-4091-1 L050343PUB00 Total/NA Solid Fill_Geo-21 88849 160-4091-1 DU L050343PUB00 Total/NA Solid Fill_Geo-21 88849 160-4091-2 L050344PUB00 Total/NA Solid Fill_Geo-21 88849 160-4091-3 L050345PUB00 Total/NA Solid Fill_Geo-21 88849 160-4091-4 L050346PUB00 Total/NA Solid Fill_Geo-21 88849 160-4091-5 L050347PUB00 Total/NA Solid Fill_Geo-21 88849 160-4091-6 L050348PUB00 Total/NA Solid Fill_Geo-21 LCS 160-89240/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-89240/1-A Method Blank Total/NA TestAmerica St. Louis Page 13 of 13 1

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