ML18019A704
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3482-2 Client Project/Site: RFP-CBA-022 (7 DAY TAT)
Revision: 1 For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:
9/22/2013 7:35:11 PM Ivan Vania, Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-3482-2 Page 2 of 30 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
8 Definitions/Glossary.......................................
9 Method Summary.........................................
10 Sample Summary.........................................
11 Client Sample Results......................................
12 QC Sample Results........................................
27 QC Association Summary...................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3482-2 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3482-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)
Report Number: 160-3482-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client. This revision contains the case narrative for job 160-3482-2.
RECEIPT The samples were received on 08/22/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 20.0 C.
RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)
Samples L050301PRS00 (160-3482-1), L050302PES00 (160-3482-2), L050303PRS00 (160-3482-3), L050304PEQ00 (160-3482-4),
L050304PES00 (160-3482-5), L050305PRS00 (160-3482-6), L050306PES00 (160-3482-7), L050307PRS00 (160-3482-8),
L050308PES00 (160-3482-9), L050309PRS00 (160-3482-10), L050310PES00 (160-3482-11), L050311PRS00 (160-3482-12),
L050312PES00 (160-3482-13), L050313PRS00 (160-3482-14), L050314PES00 (160-3482-15), L050315PRS00 (160-3482-16),
L050316PES00 (160-3482-17), L050317PRS00 (160-3482-18), L050318PES00 (160-3482-19), L050319PRS00 (160-3482-20),
L050320PES00 (160-3482-21), L050321PRS00 (160-3482-22), L050322PES00 (160-3482-23), L050323PUB00 (160-3482-24),
L050324PUB00 (160-3482-25), L050325PUB00 (160-3482-26), L050326PUB00 (160-3482-27), L050327PUB00 (160-3482-28),
L050328PUB00 (160-3482-29), L050329PUB00 (160-3482-30), L050330PUB00 (160-3482-31), L050331PUB00 (160-3482-32) and L050332PUB00 (160-3482-33) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The TestAmerica St. Louis Page 3 of 30 1
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3482-2 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3482-2 (Continued)
Laboratory: TestAmerica St. Louis (Continued) samples were leached on 08/23/2013, prepared on 08/28/2013 and analyzed on 09/18/2013.
No other difficulties were encountered during the Radium 226 analysis. All other quality control parameters were within the acceptance limits.
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!Procedure HDP-PR-QA-006, Chain of Custody Page 1 ofl Hematite Decommissioning Project IRevisio,n: 3 I
I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the co,ntainer is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutody ID No. I F-082213-01 Page 1/3 Laboratory Name:
Project Name:
Westinghouse Electric Company Contact Person:
Gerald Rood Phone Number:
314-810-3382 Sampler Name Scott Jenkins Sample ID L05030IPRSOO L050302PESOO L050303PRSOO L050304PEQOO L050304PESOO L050305PRSOO L050306PESOO L050307PRSOO L050308PESOO L050309PRSOO L0503 IOPESOO L050311PRSOO Received bv:
Company Name:
Relinquished by:
Company Name:
Date Time 8/20/2013 15:24 8/20/2013 15:30 8/20/2013 15:44 8/20/2013 15:52 8/20/2013 15:52 8/20/2013 17:20 8/20/2013 17:30 8/20/2013 16:08 8/20/2013 16:13 8/21/2013 9:07 8/21/2013 9:19 8/21/2013 9:42 l Date/Time g-*cz-t3 I
I Date/Time Matrix s
s s
s s
s s
s s
s s
Date/Time i:'.l TA-MO Laboratory Address:
13715 Rider Trail North
~* 1--------------------l
-~ PhoneNo.
8 314-298-8566
'E Laboratory Contact Person:
~ Joe Walker 1
1 1
1 1
I 1
1 Phone No.
108-870-8453 Rush Turn Around Time (7 days)
Remarks l.51'\\ o 5-o3 Sv\\5
...v-Cooler Temperature:
Cooler ID: I Shipper and Number:
-Ol/1 Q21-o_~
Comments: Please re-analyze samples after 21-day ingrowth period.
I,,,..
I.g,1,-i,.
I Verified By:
,i*.10
~
~
CS) 01
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10 11 Procedure HDP-PR-QA-006, Chain of Custody Page 1 ofl Hematite Decommissioning Project !Revision: 3 I
I Westinghouse Non"Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutody ID No. I F-082213-01 Page 2/3 Project Name:
Westinghouse Electric Company Contact Person:
Gerald Rood Phone Number:
314-81Q-_3382 Sampler Name Scott Jenkins Sample ID L050312PESOO L050313PRSOO L050314PES00 L0503 l 5PRSOO L050316PESOO L0503 l 7PRS00 L050318PES00 L0503l9PRS00 L050320PESOO L050321PRSOO L050322PES00 L050323PUBOO Company Name:
Received by:
Company Name:
Relinquished by:
Company Name:
Date Time 8/21/2013 10:47 8/21/2013 11:21 8/21/2013 11:38 8/21/2013 13:40 8/21/2013 13:55 8/21/2013 15:15 8/21/2013 15:21 8/21/2013 16:42 8/21/2013 16:50 8/21/2013 16:19 8/21/2013 16:24 8/19/2013 16:35 Date/Time
~--zz-J:J 1,1.,,V Date/Time Date/Time Matrix s
s s
s s
s s
s s
s s
Laboratory Name:
TA-MO Laboratory Address:
13715 Rider Trail North
~--------------------!
- § Phone No.
8 314-298-8566 5 Laboratory Contact Person:
~ Joe Walker 1
1 1
1 1
1 1
- 1 Phone No.
708-870-8453
'furn_Around Time Rush (7 days)
Remarks t--s?} o 5-o~ 5*
J
!--5A oS'-o'"55~S i..SA o5-o3 ©v..,s Cooler Temperature:
Date/Time r\\l Comments: Please re-analyze samples after 21-day ingrowth
'1/'1,. 4 'period.
"' r e_"t tD i*"t"l i~~*
Verified By:
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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 3 I
Page 1 ofll Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAJN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutody ID No. I F-082213-01 Page 3/3 Project Name:
Westinghouse Electric Company Contact Person:
Gerald Rood Phone Number:
314-810-3_382 Sampler Name Scott Jenkins Sample ID L050324PUBOO L050325PUBOO L050326PUBOO L050327PUBOO L050328PUBOO L050329PUBOO L050330PUBOO L050331PUBOO L050332PUBOO Relinquished by*
Company Name:
Received by:
Company Name:
Relinquished by:
Company Name:
Date Time 8/19/2013 16:45 8/19/2013 16:55 8/20/2013 14:55 8/21/2013 9:15 8/21/2013 9:45 8/21/2013 10:50 8/21/2013 11:10 8/21/2013 11:20 8/21/2013 13:40 t? Date/Time o--Z.2-13 7w Date/Time Date/Time Matrix s
s s
s s
s s
s s
Laboratory Name:
TA-MO Laboratory Address:
13715 Rider Trail North
~-------------------!
-~ PhoneNo.
8 314-298-8566
~ Laboratory Contact Person:
'"" Joe Walker Phone No.
708-87_0-8453 Turn Around Time Rush (7 days)
Remarks 1
t,SA-oS-o3 ~a..s 1
1 1
Cooler Temperature:
Cooler ID:. Shipqer and Number:
2-o't/oS 1Df:J Date/Time I Co=ents: Please re-analyze samples after 21-day ingrowth
,;l,L'/_ ~
7 period.
It%
,g V Verified By:
Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3482-2 Login Number: 3482 Question Answer Comment Creator: Daniels, Brian J List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
False Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Qualifiers Rad Qualifier Description U
Indicates the analyte was analyzed for but not detected.
Qualifier F
Duplicate RPD exceeds the control limit Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 10 of 30 1
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Sample Summary TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-3482-1 L050301PRS00 Solid 08/20/13 15:24 08/22/13 16:45 160-3482-2 L050302PES00 Solid 08/20/13 15:30 08/22/13 16:45 160-3482-3 L050303PRS00 Solid 08/20/13 15:44 08/22/13 16:45 160-3482-4 L050304PEQ00 Solid 08/20/13 15:52 08/22/13 16:45 160-3482-5 L050304PES00 Solid 08/20/13 15:52 08/22/13 16:45 160-3482-6 L050305PRS00 Solid 08/20/13 17:20 08/22/13 16:45 160-3482-7 L050306PES00 Solid 08/20/13 17:30 08/22/13 16:45 160-3482-8 L050307PRS00 Solid 08/20/13 16:08 08/22/13 16:45 160-3482-9 L050308PES00 Solid 08/20/13 16:13 08/22/13 16:45 160-3482-10 L050309PRS00 Solid 08/20/13 09:07 08/22/13 16:45 160-3482-11 L050310PES00 Solid 08/21/13 09:19 08/22/13 16:45 160-3482-12 L050311PRS00 Solid 08/21/13 09:42 08/22/13 16:45 160-3482-13 L050312PES00 Solid 08/21/13 10:47 08/22/13 16:45 160-3482-14 L050313PRS00 Solid 08/21/13 11:21 08/22/13 16:45 160-3482-15 L050314PES00 Solid 08/21/13 11:38 08/22/13 16:45 160-3482-16 L050315PRS00 Solid 08/21/13 13:40 08/22/13 16:45 160-3482-17 L050316PES00 Solid 08/21/13 13:55 08/22/13 16:45 160-3482-18 L050317PRS00 Solid 08/21/13 15:15 08/22/13 16:45 160-3482-19 L050318PES00 Solid 08/21/13 15:21 08/22/13 16:45 160-3482-20 L050319PRS00 Solid 08/21/13 16:42 08/22/13 16:45 160-3482-21 L050320PES00 Solid 08/21/13 16:50 08/22/13 16:45 160-3482-22 L050321PRS00 Solid 08/21/13 16:19 08/22/13 16:45 160-3482-23 L050322PES00 Solid 08/21/13 16:24 08/22/13 16:45 160-3482-24 L050323PUB00 Solid 08/19/13 16:35 08/22/13 16:45 160-3482-25 L050324PUB00 Solid 08/19/13 16:45 08/22/13 16:45 160-3482-26 L050325PUB00 Solid 08/19/13 16:55 08/22/13 16:45 160-3482-27 L050326PUB00 Solid 08/20/13 14:55 08/22/13 16:45 160-3482-28 L050327PUB00 Solid 08/21/13 09:15 08/22/13 16:45 160-3482-29 L050328PUB00 Solid 08/21/13 09:45 08/22/13 16:45 160-3482-30 L050329PUB00 Solid 08/21/13 10:50 08/22/13 16:45 160-3482-31 L050330PUB00 Solid 08/21/13 11:10 08/22/13 16:45 160-3482-32 L050331PUB00 Solid 08/21/13 11:20 08/22/13 16:45 160-3482-33 L050332PUB00 Solid 08/21/13 13:40 08/22/13 16:45 TestAmerica St. Louis Page 11 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-1 Client Sample ID: L050301PRS00 Matrix: Solid Date Collected: 08/20/13 15:24 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.37 (2+/-)
0.216 (2+/-)
1 09/18/13 08:51 08/28/13 13:09 pCi/g 0.184 RL MDC 0.172 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 08:51 1
0.732 0.510 0.502 0.928 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 08:51 1
0.0963 0.173 0.139 1.06 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 08:51 1
0.0913 0.157 0.0995 1.12 Lead 212 pCi/g 08/28/13 13:09 09/18/13 08:51 1
0.0915 0.170 0.115 1.29 Lead 214 pCi/g 08/28/13 13:09 09/18/13 08:51 1
0.381 2.70 1.67 22.0 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 08:51 1
1.68 0.244 0.242 U
0.303 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 08:51 1
0.0963 1.00 0.173 0.139 1.06 Radium 226 pCi/g 08/28/13 13:09 09/18/13 08:51 1
0.184 0.216 0.172 1.37 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 08:51 1
1.24 0.483 0.471 U
1.11 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 08:51 1
0.344 0.190 0.189 U
0.140 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 08:51 1
0.133 0.0809 0.0806 U
0.0624 Americium 241 pCi/g 08/28/13 13:09 09/18/13 08:51 1
8.50 4.70 4.70 U
2.65 Protactinium 234m Lab Sample ID: 160-3482-2 Client Sample ID: L050302PES00 Matrix: Solid Date Collected: 08/20/13 15:30 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.24 (2+/-)
0.204 (2+/-)
1 09/18/13 10:32 08/28/13 13:09 pCi/g 0.109 RL MDC 0.160 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.340 0.409 0.380 1.47 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.0822 0.179 0.123 1.24 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.0659 0.173 0.0800 1.19 Lead 212 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.0906 0.174 0.105 1.34 Lead 214 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.398 2.62 1.30 22.2 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 10:32 1
1.29 0.211 0.207 U
0.387 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.0822 1.00 0.179 0.123 1.24 Radium 226 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.109 0.204 0.160 1.24 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 10:32 1
1.05 0.891 0.877 1.50 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.251 0.154 0.153 U
0.138 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.108 0.0644 0.0644 U
0.0151 Americium 241 pCi/g 08/28/13 13:09 09/18/13 10:32 1
5.80 3.32 3.32 U
1.29 Protactinium 234m Lab Sample ID: 160-3482-3 Client Sample ID: L050303PRS00 Matrix: Solid Date Collected: 08/20/13 15:44 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.14 (2+/-)
0.180 (2+/-)
1 09/18/13 10:32 08/28/13 13:09 pCi/g 0.143 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.424 0.523 0.489 1.77 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.0777 0.160 0.111 1.11 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.0785 0.159 0.0787 1.07 Lead 212 TestAmerica St. Louis Page 12 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-3 Client Sample ID: L050303PRS00 Matrix: Solid Date Collected: 08/20/13 15:44 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 1.25 (2+/-)
0.165 (2+/-)
1 09/18/13 10:32 08/28/13 13:09 pCi/g 0.0810 RL MDC 0.102 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.424 2.50 1.23 21.2 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 10:32 1
1.12 0.270 0.266 U
0.407 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.0777 1.00 0.160 0.111 1.11 Radium 226 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.143 0.180 0.137 1.14 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.995 0.390 0.378 U
0.926 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.261 0.156 0.155 U
0.0539 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 10:32 1
0.116 0.0691 0.0691 U
0.0189 Americium 241 pCi/g 08/28/13 13:09 09/18/13 10:32 1
4.57 2.97 2.90 6.65 Protactinium 234m Lab Sample ID: 160-3482-4 Client Sample ID: L050304PEQ00 Matrix: Solid Date Collected: 08/20/13 15:52 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.27 (2+/-)
0.205 (2+/-)
1 09/18/13 10:29 08/28/13 13:09 pCi/g 0.127 RL MDC 0.164 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 10:29 1
0.417 0.471 0.455 1.27 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 10:29 1
0.0828 0.179 0.130 1.26 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 10:29 1
0.0679 0.153 0.0872 1.17 Lead 212 pCi/g 08/28/13 13:09 09/18/13 10:29 1
0.0736 0.162 0.101 1.30 Lead 214 pCi/g 08/28/13 13:09 09/18/13 10:29 1
0.440 2.60 1.51 21.9 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 10:29 1
1.37 0.836 0.833 U
-0.664 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 10:29 1
0.0828 1.00 0.179 0.130 1.26 Radium 226 pCi/g 08/28/13 13:09 09/18/13 10:29 1
0.127 0.205 0.164 1.27 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 10:29 1
0.813 0.328 0.315 0.956 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 10:29 1
0.270 0.174 0.173 U
0.0917 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 10:29 1
0.109 0.0640 0.0640 U
0.00911 Americium 241 pCi/g 08/28/13 13:09 09/18/13 10:29 1
6.07 4.25 4.23 U
3.93 Protactinium 234m Lab Sample ID: 160-3482-5 Client Sample ID: L050304PES00 Matrix: Solid Date Collected: 08/20/13 15:52 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.18 (2+/-)
0.223 (2+/-)
1 09/18/13 10:30 08/28/13 13:09 pCi/g 0.180 RL MDC 0.192 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 10:30 1
0.577 0.655 0.636 1.62 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 10:30 1
0.0964 0.213 0.161 1.44 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 10:30 1
0.0824 0.166 0.101 1.23 Lead 212 pCi/g 08/28/13 13:09 09/18/13 10:30 1
0.106 0.189 0.134 1.38 Lead 214 pCi/g 08/28/13 13:09 09/18/13 10:30 1
0.533 2.81 1.75 22.8 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 10:30 1
1.68 0.473 0.468 U
0.632 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 10:30 1
0.0964 1.00 0.213 0.161 1.44 Radium 226 TestAmerica St. Louis Page 13 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-5 Client Sample ID: L050304PES00 Matrix: Solid Date Collected: 08/20/13 15:52 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 232 1.18 (2+/-)
0.223 (2+/-)
1 09/18/13 10:30 08/28/13 13:09 pCi/g 0.180 RL MDC 0.192 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 10:30 1
1.11 0.922 0.901 2.02 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 10:30 1
0.278 0.233 0.230 0.398 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 10:30 1
0.133 0.0469 0.0469 U
0.000 Americium 241 pCi/g 08/28/13 13:09 09/18/13 10:30 1
8.99 4.46 4.42 U
6.32 Protactinium 234m Lab Sample ID: 160-3482-6 Client Sample ID: L050305PRS00 Matrix: Solid Date Collected: 08/20/13 17:20 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.17 (2+/-)
0.197 (2+/-)
1 09/18/13 10:31 08/28/13 13:09 pCi/g 0.133 RL MDC 0.161 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 10:31 1
0.448 0.477 0.462 1.23 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 10:31 1
0.0738 0.152 0.112 1.06 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 10:31 1
0.0560 0.153 0.0808 1.21 Lead 212 pCi/g 08/28/13 13:09 09/18/13 10:31 1
0.0782 0.166 0.103 1.35 Lead 214 pCi/g 08/28/13 13:09 09/18/13 10:31 1
0.414 2.43 1.35 21.1 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 10:31 1
1.21 0.362 0.359 U
0.497 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 10:31 1
0.0738 1.00 0.152 0.112 1.06 Radium 226 pCi/g 08/28/13 13:09 09/18/13 10:31 1
0.133 0.197 0.161 1.17 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 10:31 1
0.903 0.734 0.716 1.62 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 10:31 1
0.215 0.146 0.145 U
0.170 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 10:31 1
0.0805 0.0475 0.0475 U
0.00812 Americium 241 pCi/g 08/28/13 13:09 09/18/13 10:31 1
5.78 3.58 3.53 5.78 Protactinium 234m Lab Sample ID: 160-3482-7 Client Sample ID: L050306PES00 Matrix: Solid Date Collected: 08/20/13 17:30 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.12 (2+/-)
0.160 (2+/-)
1 09/18/13 12:54 08/28/13 13:09 pCi/g 0.101 RL MDC 0.112 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 12:54 1
0.316 0.392 0.371 1.22 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 12:54 1
0.0753 0.156 0.110 1.06 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 12:54 1
0.0590 0.160 0.0743 1.10 Lead 212 pCi/g 08/28/13 13:09 09/18/13 12:54 1
0.0782 0.143 0.0924 1.05 Lead 214 pCi/g 08/28/13 13:09 09/18/13 12:54 1
0.384 2.28 1.18 19.0 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 12:54 1
1.23 0.265 0.260 U
0.462 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 12:54 1
0.0753 1.00 0.156 0.110 1.06 Radium 226 pCi/g 08/28/13 13:09 09/18/13 12:54 1
0.101 0.160 0.112 1.12 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 12:54 1
0.883 0.675 0.662 1.29 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 12:54 1
0.181 0.0706 0.0705 U
0.0368 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 12:54 1
0.115 0.0689 0.0688 U
0.0165 Americium 241 TestAmerica St. Louis Page 14 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-7 Client Sample ID: L050306PES00 Matrix: Solid Date Collected: 08/20/13 17:30 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Protactinium 234m 3.35 U
(2+/-)
1.73 (2+/-)
1 09/18/13 12:54 08/28/13 13:09 pCi/g 5.54 RL MDC 1.70 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Lab Sample ID: 160-3482-8 Client Sample ID: L050307PRS00 Matrix: Solid Date Collected: 08/20/13 16:08 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.08 (2+/-)
0.190 (2+/-)
1 09/18/13 12:52 08/28/13 13:09 pCi/g 0.156 RL MDC 0.155 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 12:52 1
0.463 0.484 0.470 1.15 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 12:52 1
0.0806 0.183 0.134 1.20 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 12:52 1
0.0745 0.169 0.0888 1.11 Lead 212 pCi/g 08/28/13 13:09 09/18/13 12:52 1
0.0771 0.172 0.120 1.19 Lead 214 pCi/g 08/28/13 13:09 09/18/13 12:52 1
0.324 2.59 1.49 20.7 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 12:52 1
1.35 0.434 0.431 U
0.512 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 12:52 1
0.0806 1.00 0.183 0.134 1.20 Radium 226 pCi/g 08/28/13 13:09 09/18/13 12:52 1
0.156 0.190 0.155 1.08 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 12:52 1
1.10 0.938 0.923 1.57 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 12:52 1
0.236 0.158 0.157 U
0.185 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 12:52 1
0.128 0.0765 0.0764 U
0.0270 Americium 241 pCi/g 08/28/13 13:09 09/18/13 12:52 1
7.25 4.37 4.36 U
1.93 Protactinium 234m Lab Sample ID: 160-3482-9 Client Sample ID: L050308PES00 Matrix: Solid Date Collected: 08/20/13 16:13 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.12 (2+/-)
0.208 (2+/-)
1 09/18/13 12:53 08/28/13 13:09 pCi/g 0.126 RL MDC 0.174 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 12:53 1
0.465 0.555 0.534 1.42 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 12:53 1
0.0639 0.161 0.108 1.14 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 12:53 1
0.0581 0.162 0.0746 1.11 Lead 212 pCi/g 08/28/13 13:09 09/18/13 12:53 1
0.0617 0.161 0.0913 1.28 Lead 214 pCi/g 08/28/13 13:09 09/18/13 12:53 1
0.498 2.64 1.33 22.3 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 12:53 1
1.18 0.708 0.707 U
-0.379 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 12:53 1
0.0639 1.00 0.161 0.108 1.14 Radium 226 pCi/g 08/28/13 13:09 09/18/13 12:53 1
0.126 0.208 0.174 1.12 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 12:53 1
0.853 0.640 0.625 1.32 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 12:53 1
0.253 0.142 0.142 U
0.107 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 12:53 1
0.108 0.0652 0.0650 U
-0.0406 Americium 241 pCi/g 08/28/13 13:09 09/18/13 12:53 1
5.64 3.25 3.25 U
1.30 Protactinium 234m TestAmerica St. Louis Page 15 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-10 Client Sample ID: L050309PRS00 Matrix: Solid Date Collected: 08/20/13 09:07 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.991 (2+/-)
0.195 (2+/-)
1 09/18/13 13:51 08/28/13 13:09 pCi/g 0.122 RL MDC 0.167 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.408 0.466 0.450 1.17 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.0668 0.141 0.0989 0.969 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.0618 0.160 0.0748 1.09 Lead 212 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.0816 0.161 0.101 1.21 Lead 214 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.306 2.36 1.17 20.0 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 13:51 1
1.20 0.268 0.260 U
0.585 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.0668 1.00 0.141 0.0989 0.969 Radium 226 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.122 0.195 0.167 0.991 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.818 0.637 0.619 1.44 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.266 0.123 0.123 U
0.0345 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.111 0.0666 0.0666 U
0.0187 Americium 241 pCi/g 08/28/13 13:09 09/18/13 13:51 1
5.93 91.1 91.1 U
-0.625 Protactinium 234m Lab Sample ID: 160-3482-11 Client Sample ID: L050310PES00 Matrix: Solid Date Collected: 08/21/13 09:19 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.08 (2+/-)
0.188 (2+/-)
1 09/18/13 13:51 08/28/13 13:09 pCi/g 0.130 RL MDC 0.152 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.493 0.519 0.501 1.30 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.0963 0.184 0.143 1.12 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.0766 0.176 0.0907 1.16 Lead 212 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.0922 0.167 0.121 1.10 Lead 214 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.322 2.62 1.50 21.0 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 13:51 1
1.46 0.886 0.883 U
-0.634 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.0963 1.00 0.184 0.143 1.12 Radium 226 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.130 0.188 0.152 1.08 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 13:51 1
1.20 0.391 0.381 U
0.869 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.292 0.169 0.168 U
0.101 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 13:51 1
0.119 0.0703 0.0703 U
0.00747 Americium 241 pCi/g 08/28/13 13:09 09/18/13 13:51 1
7.31 3.88 3.88 U
2.11 Protactinium 234m Lab Sample ID: 160-3482-12 Client Sample ID: L050311PRS00 Matrix: Solid Date Collected: 08/21/13 09:42 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.08 (2+/-)
0.195 (2+/-)
1 09/18/13 10:28 08/28/13 13:09 pCi/g 0.131 RL MDC 0.165 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 10:28 1
0.570 0.571 0.562 1.09 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 10:28 1
0.0890 0.169 0.127 1.15 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 10:28 1
0.0719 0.149 0.0831 1.15 Lead 212 TestAmerica St. Louis Page 16 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-12 Client Sample ID: L050311PRS00 Matrix: Solid Date Collected: 08/21/13 09:42 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 1.36 (2+/-)
0.178 (2+/-)
1 09/18/13 10:28 08/28/13 13:09 pCi/g 0.0819 RL MDC 0.120 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 10:28 1
0.420 2.68 1.40 23.6 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 10:28 1
1.28 0.237 0.234 U
0.388 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 10:28 1
0.0890 1.00 0.169 0.127 1.15 Radium 226 pCi/g 08/28/13 13:09 09/18/13 10:28 1
0.131 0.195 0.165 1.08 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 10:28 1
0.914 0.368 0.359 U
0.812 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 10:28 1
0.263 0.157 0.156 U
0.162 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 10:28 1
0.117 0.178 0.177 U
-0.0705 Americium 241 pCi/g 08/28/13 13:09 09/18/13 10:28 1
5.84 3.31 3.31 U
0.581 Protactinium 234m Lab Sample ID: 160-3482-13 Client Sample ID: L050312PES00 Matrix: Solid Date Collected: 08/21/13 10:47 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.15 (2+/-)
0.184 (2+/-)
1 09/18/13 13:52 08/28/13 13:09 pCi/g 0.115 RL MDC 0.142 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.438 0.488 0.469 1.31 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.0775 0.153 0.102 1.10 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.0599 0.175 0.0779 1.21 Lead 212 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.0721 0.157 0.0908 1.23 Lead 214 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.367 2.58 1.28 21.9 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 13:52 1
1.23 0.748 0.745 U
-0.571 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.0775 1.00 0.153 0.102 1.10 Radium 226 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.115 0.184 0.142 1.15 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.920 0.736 0.723 1.35 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.248 0.149 0.148 U
0.153 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.107 0.0633 0.0633 U
0.00626 Americium 241 pCi/g 08/28/13 13:09 09/18/13 13:52 1
6.41 3.63 3.63 U
0.413 Protactinium 234m Lab Sample ID: 160-3482-14 Client Sample ID: L050313PRS00 Matrix: Solid Date Collected: 08/21/13 11:21 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.00 (2+/-)
0.194 (2+/-)
1 09/18/13 12:51 08/28/13 13:09 pCi/g 0.102 RL MDC 0.168 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 12:51 1
0.455 0.523 0.497 1.68 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 12:51 1
0.0672 0.162 0.116 1.16 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 12:51 1
0.0625 0.162 0.0847 1.28 Lead 212 pCi/g 08/28/13 13:09 09/18/13 12:51 1
0.0950 0.177 0.128 1.27 Lead 214 pCi/g 08/28/13 13:09 09/18/13 12:51 1
0.500 2.62 1.42 22.7 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 12:51 1
1.38 0.272 0.267 U
0.529 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 12:51 1
0.0672 1.00 0.162 0.116 1.16 Radium 226 TestAmerica St. Louis Page 17 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-14 Client Sample ID: L050313PRS00 Matrix: Solid Date Collected: 08/21/13 11:21 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 232 1.00 (2+/-)
0.194 (2+/-)
1 09/18/13 12:51 08/28/13 13:09 pCi/g 0.102 RL MDC 0.168 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 12:51 1
0.859 0.657 0.645 1.33 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 12:51 1
0.278 0.163 0.162 U
0.167 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 12:51 1
0.115 0.0675 0.0675 U
0.0185 Americium 241 pCi/g 08/28/13 13:09 09/18/13 12:51 1
5.82 3.43 3.38 5.87 Protactinium 234m Lab Sample ID: 160-3482-15 Client Sample ID: L050314PES00 Matrix: Solid Date Collected: 08/21/13 11:38 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.14 (2+/-)
0.220 (2+/-)
1 09/18/13 17:43 08/28/13 13:09 pCi/g 0.191 RL MDC 0.187 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 17:43 1
0.449 0.472 0.457 1.15 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 17:43 1
0.0746 0.174 0.131 1.10 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 17:43 1
0.0755 0.162 0.0892 1.04 Lead 212 pCi/g 08/28/13 13:09 09/18/13 17:43 1
0.0792 0.168 0.122 1.12 Lead 214 pCi/g 08/28/13 13:09 09/18/13 17:43 1
0.364 2.27 1.45 17.1 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 17:43 1
1.36 0.591 0.587 U
0.649 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 17:43 1
0.0746 1.00 0.174 0.131 1.10 Radium 226 pCi/g 08/28/13 13:09 09/18/13 17:43 1
0.191 0.220 0.187 1.14 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 17:43 1
1.02 0.790 0.779 1.25 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 17:43 1
0.224 0.153 0.152 U
0.203 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 17:43 1
0.111 0.0660 0.0660 U
0.0146 Americium 241 pCi/g 08/28/13 13:09 09/18/13 17:43 1
7.83 3.05 3.05 U
1.54 Protactinium 234m Lab Sample ID: 160-3482-16 Client Sample ID: L050315PRS00 Matrix: Solid Date Collected: 08/21/13 13:40 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.17 (2+/-)
0.173 (2+/-)
1 09/18/13 17:44 08/28/13 13:09 pCi/g 0.107 RL MDC 0.126 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 17:44 1
0.364 0.410 0.394 1.06 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 17:44 1
0.0627 0.149 0.102 1.04 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 17:44 1
0.0563 0.170 0.0754 1.18 Lead 212 pCi/g 08/28/13 13:09 09/18/13 17:44 1
0.0827 0.152 0.0912 1.16 Lead 214 pCi/g 08/28/13 13:09 09/18/13 17:44 1
0.371 2.25 1.16 18.8 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 17:44 1
0.978 0.336 0.326 U
0.718 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 17:44 1
0.0627 1.00 0.149 0.102 1.04 Radium 226 pCi/g 08/28/13 13:09 09/18/13 17:44 1
0.107 0.173 0.126 1.17 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 17:44 1
0.960 0.804 0.789 1.47 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 17:44 1
0.255 0.159 0.159 U
0.123 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 17:44 1
0.101 0.0598 0.0598 U
-0.000676 Americium 241 TestAmerica St. Louis Page 18 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-16 Client Sample ID: L050315PRS00 Matrix: Solid Date Collected: 08/21/13 13:40 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Protactinium 234m
-1.14 U
(2+/-)
9.68 (2+/-)
1 09/18/13 17:44 08/28/13 13:09 pCi/g 5.68 RL MDC 9.68 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Lab Sample ID: 160-3482-17 Client Sample ID: L050316PES00 Matrix: Solid Date Collected: 08/21/13 13:55 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.27 (2+/-)
0.209 (2+/-)
1 09/18/13 13:52 08/28/13 13:09 pCi/g 0.120 RL MDC 0.170 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.443 0.507 0.485 1.50 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.0756 0.159 0.116 1.13 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.0690 0.159 0.0849 1.24 Lead 212 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.0904 0.161 0.106 1.25 Lead 214 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.564 2.38 1.36 20.2 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.884 0.547 0.545 U
0.535 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.0756 1.00 0.159 0.116 1.13 Radium 226 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.120 0.209 0.170 1.27 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 13:52 1
1.01 0.396 0.387 U
0.894 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.277 0.133 0.133 U
0.0279 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 13:52 1
0.120 1.25 1.25 U
-0.0314 Americium 241 pCi/g 08/28/13 13:09 09/18/13 13:52 1
5.71 2.62 2.59 U
3.95 Protactinium 234m Lab Sample ID: 160-3482-18 Client Sample ID: L050317PRS00 Matrix: Solid Date Collected: 08/21/13 15:15 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.21 (2+/-)
0.178 (2+/-)
1 09/18/13 17:45 08/28/13 13:09 pCi/g 0.0931 RL MDC 0.135 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 17:45 1
0.605 0.400 0.395 0.653 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 17:45 1
0.0796 0.163 0.120 1.14 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 17:45 1
0.0916 0.141 0.0861 1.03 Lead 212 pCi/g 08/28/13 13:09 09/18/13 17:45 1
0.0864 0.166 0.105 1.33 Lead 214 pCi/g 08/28/13 13:09 09/18/13 17:45 1
0.450 2.53 1.35 22.2 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 17:45 1
1.30 0.397 0.388 U
0.829 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 17:45 1
0.0796 1.00 0.163 0.120 1.14 Radium 226 pCi/g 08/28/13 13:09 09/18/13 17:45 1
0.0931 0.178 0.135 1.21 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 17:45 1
0.977 0.392 0.383 U
0.867 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 17:45 1
0.305 0.103 0.103 U
0.0457 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 17:45 1
0.119 0.0713 0.0713 U
-0.0165 Americium 241 pCi/g 08/28/13 13:09 09/18/13 17:45 1
5.23 3.11 3.10 U
1.84 Protactinium 234m TestAmerica St. Louis Page 19 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-19 Client Sample ID: L050318PES00 Matrix: Solid Date Collected: 08/21/13 15:21 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.02 (2+/-)
0.163 (2+/-)
1 09/18/13 08:53 08/28/13 13:09 pCi/g 0.0910 RL MDC 0.125 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 08:53 1
0.394 0.379 0.367 0.907 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 08:53 1
0.0611 0.148 0.101 1.03 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 08:53 1
0.0599 0.171 0.0760 1.18 Lead 212 pCi/g 08/28/13 13:09 09/18/13 08:53 1
0.0697 0.157 0.0894 1.24 Lead 214 pCi/g 08/28/13 13:09 09/18/13 08:53 1
0.297 2.49 1.22 21.3 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 08:53 1
1.05 0.272 0.266 U
0.512 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 08:53 1
0.0611 1.00 0.148 0.101 1.03 Radium 226 pCi/g 08/28/13 13:09 09/18/13 08:53 1
0.0910 0.163 0.125 1.02 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 08:53 1
0.919 0.762 0.744 1.58 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 08:53 1
0.240 0.141 0.141 U
0.106 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 08:53 1
0.0953 0.0563 0.0563 U
-0.00129 Americium 241 pCi/g 08/28/13 13:09 09/18/13 08:53 1
5.66 3.36 3.36 U
2.18 Protactinium 234m Lab Sample ID: 160-3482-20 Client Sample ID: L050319PRS00 Matrix: Solid Date Collected: 08/21/13 16:42 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.10 (2+/-)
0.175 (2+/-)
1 09/18/13 17:46 08/28/13 13:09 pCi/g 0.138 RL MDC 0.139 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:09 09/18/13 17:46 1
0.478 0.587 0.562 1.75 Bismuth 212 pCi/g 08/28/13 13:09 09/18/13 17:46 1
0.0791 0.168 0.124 1.17 Bismuth 214 pCi/g 08/28/13 13:09 09/18/13 17:46 1
0.0738 0.148 0.0841 1.13 Lead 212 pCi/g 08/28/13 13:09 09/18/13 17:46 1
0.0868 0.156 0.101 1.22 Lead 214 pCi/g 08/28/13 13:09 09/18/13 17:46 1
0.533 2.63 1.45 22.7 Potassium 40 pCi/g 08/28/13 13:09 09/18/13 17:46 1
1.45 0.250 0.247 U
0.392 Protactinium 231 pCi/g 08/28/13 13:09 09/18/13 17:46 1
0.0791 1.00 0.168 0.124 1.17 Radium 226 pCi/g 08/28/13 13:09 09/18/13 17:46 1
0.138 0.175 0.139 1.10 Thorium 232 pCi/g 08/28/13 13:09 09/18/13 17:46 1
0.961 0.380 0.371 U
0.860 Thorium 234 pCi/g 08/28/13 13:09 09/18/13 17:46 1
0.290 0.140 0.140 U
0.0428 Uranium 235 pCi/g 08/28/13 13:09 09/18/13 17:46 1
0.116 0.0675 0.0675 U
0.00222 Americium 241 pCi/g 08/28/13 13:09 09/18/13 17:46 1
5.96 3.62 3.61 U
2.82 Protactinium 234m Lab Sample ID: 160-3482-21 Client Sample ID: L050320PES00 Matrix: Solid Date Collected: 08/21/13 16:50 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.795 (2+/-)
0.266 (2+/-)
1 09/18/13 03:11 08/28/13 13:20 pCi/g 0.276 RL MDC 0.253 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 03:11 1
1.03 0.636 0.633 U
0.554 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.194 0.279 0.246 1.27 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.157 0.180 0.139 0.885 Lead 212 TestAmerica St. Louis Page 20 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-21 Client Sample ID: L050320PES00 Matrix: Solid Date Collected: 08/21/13 16:50 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 1.17 (2+/-)
0.226 (2+/-)
1 09/18/13 03:11 08/28/13 13:20 pCi/g 0.168 RL MDC 0.190 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.663 2.65 1.94 17.6 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 03:11 1
1.34 0.831 0.827 U
0.734 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.194 1.00 0.279 0.246 1.27 Radium 226 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.276 0.266 0.253 0.795 Thorium 232 pCi/g 08/28/13 13:20 09/18/13 03:11 1
2.24 1.76 1.74 2.35 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.481 0.299 0.298 U
0.255 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.259 0.0493 0.0493 U
0.000 Americium 241 pCi/g 08/28/13 13:20 09/18/13 03:11 1
14.1 385 385 U
-2.52 Protactinium 234m Lab Sample ID: 160-3482-22 Client Sample ID: L050321PRS00 Matrix: Solid Date Collected: 08/21/13 16:19 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.01 (2+/-)
0.173 (2+/-)
1 09/18/13 03:11 08/28/13 13:20 pCi/g 0.156 RL MDC 0.143 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.480 0.475 0.463 1.07 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.0806 0.164 0.129 1.04 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.0743 0.136 0.0856 0.976 Lead 212 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.0893 0.149 0.0988 1.15 Lead 214 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.462 2.32 1.46 18.6 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 03:11 1
1.37 0.309 0.303 U
0.593 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.0806 1.00 0.164 0.129 1.04 Radium 226 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.156 0.173 0.143 1.01 Thorium 232 pCi/g 08/28/13 13:20 09/18/13 03:11 1
1.03 0.830 0.817 1.54 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.287 0.0856 0.0853 U
0.0743 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 03:11 1
0.115 0.482 0.482 U
-0.0114 Americium 241 pCi/g 08/28/13 13:20 09/18/13 03:11 1
6.94 3.60 3.59 U
0.751 Protactinium 234m Lab Sample ID: 160-3482-23 Client Sample ID: L050322PES00 Matrix: Solid Date Collected: 08/21/13 16:24 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.07 (2+/-)
0.180 (2+/-)
1 09/18/13 03:10 08/28/13 13:20 pCi/g 0.0509 RL MDC 0.144 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.277 0.530 0.483 2.11 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.0729 0.168 0.125 1.08 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.0749 0.160 0.0885 1.03 Lead 212 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.0992 0.184 0.133 1.22 Lead 214 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.495 2.55 1.55 19.7 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 03:10 1
1.42 0.346 0.342 U
0.479 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.0729 1.00 0.168 0.125 1.08 Radium 226 TestAmerica St. Louis Page 21 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-23 Client Sample ID: L050322PES00 Matrix: Solid Date Collected: 08/21/13 16:24 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 232 1.07 (2+/-)
0.180 (2+/-)
1 09/18/13 03:10 08/28/13 13:20 pCi/g 0.0509 RL MDC 0.144 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 03:10 1
1.11 0.900 0.889 1.36 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.269 0.170 0.170 U
0.0926 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.134 0.0798 0.0798 U
0.0279 Americium 241 pCi/g 08/28/13 13:20 09/18/13 03:10 1
7.80 4.39 4.39 U
0.675 Protactinium 234m Lab Sample ID: 160-3482-24 Client Sample ID: L050323PUB00 Matrix: Solid Date Collected: 08/19/13 16:35 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.20 (2+/-)
0.188 (2+/-)
1 09/18/13 03:12 08/28/13 13:20 pCi/g 0.116 RL MDC 0.148 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 03:12 1
0.546 0.420 0.407 1.09 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 03:12 1
0.0847 0.161 0.124 1.06 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 03:12 1
0.0650 0.150 0.0840 1.16 Lead 212 pCi/g 08/28/13 13:20 09/18/13 03:12 1
0.0875 0.183 0.127 1.36 Lead 214 pCi/g 08/28/13 13:20 09/18/13 03:12 1
0.392 2.45 1.38 21.0 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 03:12 1
1.24 0.203 0.200 U
0.368 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 03:12 1
0.0847 1.00 0.161 0.124 1.06 Radium 226 pCi/g 08/28/13 13:20 09/18/13 03:12 1
0.116 0.188 0.148 1.20 Thorium 232 pCi/g 08/28/13 13:20 09/18/13 03:12 1
0.886 0.688 0.671 1.56 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 03:12 1
0.216 0.146 0.144 U
0.215 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 03:12 1
0.106 0.0626 0.0626 U
0.00369 Americium 241 pCi/g 08/28/13 13:20 09/18/13 03:12 1
9.73 18.8 18.8 U
-0.470 Protactinium 234m Lab Sample ID: 160-3482-25 Client Sample ID: L050324PUB00 Matrix: Solid Date Collected: 08/19/13 16:45 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.23 (2+/-)
0.188 (2+/-)
1 09/18/13 03:10 08/28/13 13:20 pCi/g 0.0391 RL MDC 0.146 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.431 0.573 0.540 1.96 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.0751 0.158 0.118 1.08 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.0788 0.151 0.0876 1.15 Lead 212 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.0927 0.185 0.130 1.36 Lead 214 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.455 2.63 1.44 22.8 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 03:10 1
1.43 0.872 0.868 U
-0.758 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.0751 1.00 0.158 0.118 1.08 Radium 226 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.0391 0.188 0.146 1.23 Thorium 232 pCi/g 08/28/13 13:20 09/18/13 03:10 1
1.11 0.926 0.917 1.29 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.276 0.107 0.107 U
0.0576 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 03:10 1
0.126 1.06 1.06 U
-0.0296 Americium 241 TestAmerica St. Louis Page 22 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-25 Client Sample ID: L050324PUB00 Matrix: Solid Date Collected: 08/19/13 16:45 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Protactinium 234m 2.21 U
(2+/-)
3.87 (2+/-)
1 09/18/13 03:10 08/28/13 13:20 pCi/g 6.34 RL MDC 3.86 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Lab Sample ID: 160-3482-26 Client Sample ID: L050325PUB00 Matrix: Solid Date Collected: 08/19/13 16:55 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.19 (2+/-)
0.193 (2+/-)
1 09/18/13 03:13 08/28/13 13:20 pCi/g 0.125 RL MDC 0.155 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 03:13 1
0.424 0.498 0.482 1.29 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 03:13 1
0.0873 0.165 0.124 1.12 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 03:13 1
0.0950 0.140 0.0881 1.01 Lead 212 pCi/g 08/28/13 13:20 09/18/13 03:13 1
0.0956 0.175 0.125 1.26 Lead 214 pCi/g 08/28/13 13:20 09/18/13 03:13 1
0.573 2.86 1.53 25.1 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 03:13 1
1.23 0.337 0.332 U
0.604 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 03:13 1
0.0873 1.00 0.165 0.124 1.12 Radium 226 pCi/g 08/28/13 13:20 09/18/13 03:13 1
0.125 0.193 0.155 1.19 Thorium 232 pCi/g 08/28/13 13:20 09/18/13 03:13 1
0.958 0.820 0.799 1.89 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 03:13 1
0.279 0.169 0.169 U
0.116 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 03:13 1
0.112 0.0673 0.0672 U
0.0317 Americium 241 pCi/g 08/28/13 13:20 09/18/13 03:13 1
6.09 3.60 3.60 U
1.94 Protactinium 234m Lab Sample ID: 160-3482-27 Client Sample ID: L050326PUB00 Matrix: Solid Date Collected: 08/20/13 14:55 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.373 (2+/-)
0.103 (2+/-)
1 09/18/13 03:56 08/28/13 13:20 pCi/g 0.0934 RL MDC 0.0961 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 03:56 1
0.521 0.289 0.289 U
-0.00340 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 03:56 1
0.0795 0.0992 0.0830 0.522 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 03:56 1
0.0591 0.0607 0.0488 0.280 Lead 212 pCi/g 08/28/13 13:20 09/18/13 03:56 1
0.0677 0.103 0.0810 0.615 Lead 214 pCi/g 08/28/13 13:20 09/18/13 03:56 1
0.168 0.817 0.658 4.73 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 03:56 1
0.881 0.0888 0.0885 U
0.0665 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 03:56 1
0.0795 1.00 0.0992 0.0830 0.522 Radium 226 pCi/g 08/28/13 13:20 09/18/13 03:56 1
0.0934 0.103 0.0961 0.373 Thorium 232 pCi/g 08/28/13 13:20 09/18/13 03:56 1
2.00 3.94 1.21 35.8 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 03:56 1
0.354 0.939 0.391 8.39 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 03:56 1
0.218 0.132 0.132 U
0.0800 Americium 241 pCi/g 08/28/13 13:20 09/18/13 03:56 1
1.51 8.36 6.56 51.3 Protactinium 234m TestAmerica St. Louis Page 23 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-28 Client Sample ID: L050327PUB00 Matrix: Solid Date Collected: 08/21/13 09:15 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.15 (2+/-)
0.181 (2+/-)
1 09/18/13 04:04 08/28/13 13:20 pCi/g 0.152 RL MDC 0.142 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.537 0.630 0.608 1.69 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.0943 0.149 0.110 1.03 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.0746 0.182 0.0830 1.07 Lead 212 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.0854 0.176 0.114 1.23 Lead 214 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.487 2.53 1.39 22.0 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 04:04 1
1.34 0.325 0.319 U
0.519 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.0943 1.00 0.149 0.110 1.03 Radium 226 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.152 0.181 0.142 1.15 Thorium 232 pCi/g 08/28/13 13:20 09/18/13 04:04 1
1.47 2.49 1.52 20.2 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.354 0.506 0.315 4.07 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.176 0.105 0.105 U
-0.0171 Americium 241 pCi/g 08/28/13 13:20 09/18/13 04:04 1
5.02 6.54 6.00 26.9 Protactinium 234m Lab Sample ID: 160-3482-29 Client Sample ID: L050328PUB00 Matrix: Solid Date Collected: 08/21/13 09:45 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.10 (2+/-)
0.168 (2+/-)
1 09/18/13 04:03 08/28/13 13:20 pCi/g 0.128 RL MDC 0.125 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 04:03 1
0.483 0.359 0.347 0.885 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 04:03 1
0.0808 0.177 0.122 1.24 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 04:03 1
0.0811 0.150 0.0784 0.988 Lead 212 pCi/g 08/28/13 13:20 09/18/13 04:03 1
0.0868 0.165 0.109 1.19 Lead 214 pCi/g 08/28/13 13:20 09/18/13 04:03 1
0.417 2.60 1.28 22.1 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 04:03 1
1.30 0.793 0.790 U
-0.605 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 04:03 1
0.0808 1.00 0.177 0.122 1.24 Radium 226 pCi/g 08/28/13 13:20 09/18/13 04:03 1
0.128 0.168 0.125 1.10 Thorium 232 pCi/g 08/28/13 13:20 09/18/13 04:03 1
2.01 4.28 2.11 35.6 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 04:03 1
0.426 0.765 0.362 6.62 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 04:03 1
0.223 0.135 0.135 U
-0.0910 Americium 241 pCi/g 08/28/13 13:20 09/18/13 04:03 1
4.31 8.46 6.96 47.6 Protactinium 234m Lab Sample ID: 160-3482-30 Client Sample ID: L050329PUB00 Matrix: Solid Date Collected: 08/21/13 10:50 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.976 (2+/-)
0.187 (2+/-)
1 09/18/13 04:05 08/28/13 13:20 pCi/g 0.143 RL MDC 0.161 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.515 0.626 0.600 1.82 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.0969 0.170 0.133 1.09 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.0850 0.147 0.0928 1.06 Lead 212 TestAmerica St. Louis Page 24 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-30 Client Sample ID: L050329PUB00 Matrix: Solid Date Collected: 08/21/13 10:50 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 1.05 (2+/-)
0.143 (2+/-)
1 09/18/13 04:05 08/28/13 13:20 pCi/g 0.101 RL MDC 0.101 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.355 2.68 1.59 22.3 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 04:05 1
1.68 0.351 0.348 U
0.496 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.0969 1.00 0.170 0.133 1.09 Radium 226 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.143 0.187 0.161 0.976 Thorium 232 pCi/g 08/28/13 13:20 09/18/13 04:05 1
2.19 4.70 1.44 45.8 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.500 1.17 0.511 10.8 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.235 0.140 0.140 U
0.000542 Americium 241 pCi/g 08/28/13 13:20 09/18/13 04:05 1
4.35 10.5 8.73 61.1 Protactinium 234m Lab Sample ID: 160-3482-31 Client Sample ID: L050330PUB00 Matrix: Solid Date Collected: 08/21/13 11:10 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.17 (2+/-)
0.231 (2+/-)
1 09/18/13 04:06 08/28/13 13:20 pCi/g 0.203 RL MDC 0.198 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 04:06 1
0.585 0.702 0.673 1.91 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 04:06 1
0.0849 0.179 0.133 1.15 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 04:06 1
0.0802 0.173 0.0905 1.14 Lead 212 pCi/g 08/28/13 13:20 09/18/13 04:06 1
0.0963 0.175 0.122 1.20 Lead 214 pCi/g 08/28/13 13:20 09/18/13 04:06 1
0.441 2.43 1.45 19.1 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 04:06 1
1.55 0.345 0.343 U
0.317 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 04:06 1
0.0849 1.00 0.179 0.133 1.15 Radium 226 pCi/g 08/28/13 13:20 09/18/13 04:06 1
0.203 0.231 0.198 1.17 Thorium 232 pCi/g 08/28/13 13:20 09/18/13 04:06 1
2.04 5.85 2.26 51.5 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 04:06 1
0.345 0.360 0.268 2.36 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 04:06 1
0.243 0.146 0.146 U
-0.0363 Americium 241 pCi/g 08/28/13 13:20 09/18/13 04:06 1
5.33 10.9 8.83 62.8 Protactinium 234m Lab Sample ID: 160-3482-32 Client Sample ID: L050331PUB00 Matrix: Solid Date Collected: 08/21/13 11:20 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.08 (2+/-)
0.188 (2+/-)
1 09/18/13 04:04 08/28/13 13:20 pCi/g 0.111 RL MDC 0.152 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.435 0.415 0.401 1.05 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.0850 0.167 0.121 1.11 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.0703 0.170 0.0802 1.15 Lead 212 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.0915 0.159 0.101 1.19 Lead 214 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.320 2.46 1.25 20.7 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 04:04 1
1.39 0.339 0.334 U
0.566 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.0850 1.00 0.167 0.121 1.11 Radium 226 TestAmerica St. Louis Page 25 of 30 1
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Client Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3482-32 Client Sample ID: L050331PUB00 Matrix: Solid Date Collected: 08/21/13 11:20 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 232 1.08 (2+/-)
0.188 (2+/-)
1 09/18/13 04:04 08/28/13 13:20 pCi/g 0.111 RL MDC 0.152 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 04:04 1
1.92 7.16 2.20 65.2 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.383 0.439 0.283 3.30 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 04:04 1
0.234 0.140 0.140 U
0.00134 Americium 241 pCi/g 08/28/13 13:20 09/18/13 04:04 1
4.48 11.0 7.88 76.6 Protactinium 234m Lab Sample ID: 160-3482-33 Client Sample ID: L050332PUB00 Matrix: Solid Date Collected: 08/21/13 13:40 Date Received: 08/22/13 16:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.22 (2+/-)
0.184 (2+/-)
1 09/18/13 04:05 08/28/13 13:20 pCi/g 0.113 RL MDC 0.142 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.454 0.534 0.512 1.56 Bismuth 212 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.0782 0.154 0.109 1.11 Bismuth 214 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.0673 0.152 0.0842 1.18 Lead 212 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.0689 0.160 0.101 1.29 Lead 214 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.575 2.46 1.41 20.8 Potassium 40 pCi/g 08/28/13 13:20 09/18/13 04:05 1
1.37 0.317 0.314 U
0.462 Protactinium 231 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.0782 1.00 0.154 0.109 1.11 Radium 226 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.113 0.184 0.142 1.22 Thorium 232 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.934 0.770 0.731 2.48 Thorium 234 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.207 0.157 0.155 0.297 Uranium 235 pCi/g 08/28/13 13:20 09/18/13 04:05 1
0.116 1.54 1.54 U
-0.0302 Americium 241 pCi/g 08/28/13 13:20 09/18/13 04:05 1
6.09 3.39 3.35 U
5.92 Protactinium 234m TestAmerica St. Louis Page 26 of 30 1
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QC Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-69124/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 73103 Prep Batch: 69124 Actinium 228 Analyte U
1 09/18/13 20:08 08/28/13 13:09 pCi/g 0.128 MDC RL 0.0112 0.0112 (2+/-)
(2+/-)
MB 0.0000 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
09/18/13 20:08 08/28/13 13:09 pCi/g 0.130 0.0352 0.0352 U
0.0000 Bismuth 212 1
09/18/13 20:08 08/28/13 13:09 pCi/g 0.0355 0.00492 0.00492 U
0.0000 Bismuth 214 1
09/18/13 20:08 08/28/13 13:09 pCi/g 0.0293 0.0152 0.0152 U
-0.0001895 Lead 212 1
09/18/13 20:08 08/28/13 13:09 pCi/g 0.0388 0.0193 0.0193 U
-0.0000351 4
Lead 214 1
09/18/13 20:08 08/28/13 13:09 pCi/g 0.174 0.0473 0.0473 U
0.0000 Potassium 40 1
09/18/13 20:08 08/28/13 13:09 pCi/g 0.375 0.207 0.207 U
0.06965 Protactinium 231 1
09/18/13 20:08 08/28/13 13:09 pCi/g 0.0355 1.00 0.00492 0.00492 U
0.0000 Radium 226 1
09/18/13 20:08 08/28/13 13:09 pCi/g 0.128 0.0112 0.0112 U
0.0000 Thorium 232 1
09/18/13 20:08 08/28/13 13:09 pCi/g 0.260 0.0903 0.0899 U
0.08212 Thorium 234 1
09/18/13 20:08 08/28/13 13:09 pCi/g 0.0695 0.0309 0.0308 U
0.01119 Uranium 235 1
09/18/13 20:08 08/28/13 13:09 pCi/g 0.0334 0.0118 0.0118 U
0.0000 Americium 241 1
09/18/13 20:08 08/28/13 13:09 pCi/g 2.66 1.36 1.36 U
-0.2942 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-69124/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 73115 Prep Batch: 69124 Americium 241 Analyte 116 87 96 94.11 97.7 9.79 0.455 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 31.6 31.33 3.28 0.138 pCi/g 99 87 - 120 Cobalt 60 24.6 24.32 2.46 0.102 pCi/g 99 87 - 115 Client Sample ID: L050318PES00 Lab Sample ID: 160-3482-19 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 73103 Prep Batch: 69124 Actinium 228 Analyte 1
0.51 1.215 1.02 0.217 0.124 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 0.907 1.474 0.638 0.598 pCi/g 0.56 1
Bismuth 214 1.03 1.154 0.176 0.0677 pCi/g 0.38 1
Lead 212 1.18 1.069 0.165 0.0788 pCi/g 0.33 1
Lead 214 1.24 1.236 0.174 0.0963 pCi/g 0.01 1
Potassium 40 21.3 19.33 2.49 0.370 pCi/g 0.39 1
Protactinium 231 0.512 U
0.4096 U
0.300 1.59 pCi/g 0.18 1
Radium 226 1.03 1.154 0.176 1.00 0.0677 pCi/g 0.38 1
Thorium 232 1.02 1.215 0.217 0.124 pCi/g 0.51 1
Thorium 234 1.58 0.7291 U
0.397 1.24 pCi/g 0.73 1
Uranium 235 0.106 U
0.1270 U
0.175 0.281 pCi/g 0.07 1
-0.00129 U
-0.00709 9
U 0.0607 0.103 pCi/g 0.05 1
Protactinium 234m 2.18 U
0.2020 U
0.787 8.16 pCi/g 0.48 1
TestAmerica St. Louis Page 27 of 30 1
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QC Sample Results TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Method Blank Lab Sample ID: MB 160-69138/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 73103 Prep Batch: 69138 Actinium 228 Analyte U
1 09/18/13 02:59 08/28/13 13:20 pCi/g 0.0605 MDC RL 0.0285 0.0284 (2+/-)
(2+/-)
MB 0.02046 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
09/18/13 02:59 08/28/13 13:20 pCi/g 0.370 0.0497 0.0497 U
0.0000 Bismuth 212 1
09/18/13 02:59 08/28/13 13:20 pCi/g 0.0355 0.0166 0.0166 U
0.005487 Bismuth 214 1
09/18/13 02:59 08/28/13 13:20 pCi/g 0.0288 0.0369 0.0369 U
-0.003830 Lead 212 1
09/18/13 02:59 08/28/13 13:20 pCi/g 0.0330 0.0159 0.0159 U
0.002790 Lead 214 1
09/18/13 02:59 08/28/13 13:20 pCi/g 0.512 0.0473 0.0473 U
0.0000 Potassium 40 1
09/18/13 02:59 08/28/13 13:20 pCi/g 0.420 0.158 0.158 U
0.01715 Protactinium 231 1
09/18/13 02:59 08/28/13 13:20 pCi/g 0.0355 1.00 0.0166 0.0166 U
0.005487 Radium 226 1
09/18/13 02:59 08/28/13 13:20 pCi/g 0.0605 0.0285 0.0284 U
0.02046 Thorium 232 1
09/18/13 02:59 08/28/13 13:20 pCi/g 0.298 0.00608 0.00607 U
0.003188 Thorium 234 1
09/18/13 02:59 08/28/13 13:20 pCi/g 0.0599 0.0269 0.0268 U
0.01407 Uranium 235 1
09/18/13 02:59 08/28/13 13:20 pCi/g 0.0224 0.0124 0.0123 U
0.003036 Americium 241 1
09/18/13 02:59 08/28/13 13:20 pCi/g 2.10 1.04 1.04 U
0.2559 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-69138/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 73104 Prep Batch: 69138 Americium 241 Analyte 116 87 95 92.95 97.7 9.67 0.442 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 31.6 30.09 3.15 0.116 pCi/g 95 87 - 120 Cobalt 60 24.6 23.20 2.34 0.0752 pCi/g 94 87 - 115 Client Sample ID: L050331PUB00 Lab Sample ID: 160-3482-32 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 73104 Prep Batch: 69138 Actinium 228 Analyte 1
0.09 1.053 1.08 0.162 0.108 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 1.05 1.454 0.594 0.534 pCi/g 0.40 1
Bismuth 214 1.11 1.166 0.169 0.0824 pCi/g 0.18 1
Lead 212 1.15 1.098 0.162 0.0695 pCi/g 0.17 1
Lead 214 1.19 1.181 0.164 0.0855 pCi/g 0.02 1
Potassium 40 20.7 20.42 2.42 0.320 pCi/g 0.06 1
Protactinium 231 0.566 U
-0.6573 U F 0.855 1.41 pCi/g 1.02 1
Radium 226 1.11 1.166 0.169 1.00 0.0824 pCi/g 0.18 1
Thorium 232 1.08 1.053 0.162 0.108 pCi/g 0.09 1
Thorium 234 65.2 64.56 7.18 2.13 pCi/g 0.04 1
Uranium 235 3.30 3.139 0.445 0.313 pCi/g 0.18 1
Americium 241 0.00134 U
0.01720 U
0.155 0.258 pCi/g 0.05 1
Protactinium 234m 76.6 78.28 11.8 5.20 pCi/g 0.07 1
TestAmerica St. Louis Page 28 of 30 1
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QC Association Summary TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Rad Leach Batch: 68380 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3482-1 L050301PRS00 Total/NA Solid Dry and Grind 160-3482-2 L050302PES00 Total/NA Solid Dry and Grind 160-3482-3 L050303PRS00 Total/NA Solid Dry and Grind 160-3482-4 L050304PEQ00 Total/NA Solid Dry and Grind 160-3482-5 L050304PES00 Total/NA Solid Dry and Grind 160-3482-6 L050305PRS00 Total/NA Solid Dry and Grind 160-3482-7 L050306PES00 Total/NA Solid Dry and Grind 160-3482-8 L050307PRS00 Total/NA Solid Dry and Grind 160-3482-9 L050308PES00 Total/NA Solid Dry and Grind 160-3482-10 L050309PRS00 Total/NA Solid Dry and Grind 160-3482-11 L050310PES00 Total/NA Solid Dry and Grind 160-3482-12 L050311PRS00 Total/NA Solid Dry and Grind 160-3482-13 L050312PES00 Total/NA Solid Dry and Grind 160-3482-14 L050313PRS00 Total/NA Solid Dry and Grind 160-3482-15 L050314PES00 Total/NA Solid Dry and Grind 160-3482-16 L050315PRS00 Total/NA Solid Dry and Grind 160-3482-17 L050316PES00 Total/NA Solid Dry and Grind 160-3482-18 L050317PRS00 Total/NA Solid Dry and Grind 160-3482-19 L050318PES00 Total/NA Solid Dry and Grind 160-3482-19 DU L050318PES00 Total/NA Solid Dry and Grind 160-3482-20 L050319PRS00 Total/NA Solid Dry and Grind 160-3482-21 L050320PES00 Total/NA Solid Dry and Grind 160-3482-22 L050321PRS00 Total/NA Solid Dry and Grind 160-3482-23 L050322PES00 Total/NA Solid Dry and Grind 160-3482-24 L050323PUB00 Total/NA Solid Dry and Grind 160-3482-25 L050324PUB00 Total/NA Solid Dry and Grind 160-3482-26 L050325PUB00 Total/NA Solid Dry and Grind 160-3482-27 L050326PUB00 Total/NA Solid Dry and Grind 160-3482-28 L050327PUB00 Total/NA Solid Dry and Grind 160-3482-29 L050328PUB00 Total/NA Solid Dry and Grind 160-3482-30 L050329PUB00 Total/NA Solid Dry and Grind 160-3482-31 L050330PUB00 Total/NA Solid Dry and Grind 160-3482-32 L050331PUB00 Total/NA Solid Dry and Grind 160-3482-32 DU L050331PUB00 Total/NA Solid Dry and Grind 160-3482-33 L050332PUB00 Total/NA Prep Batch: 69124 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 68380 160-3482-1 L050301PRS00 Total/NA Solid Fill_Geo-21 68380 160-3482-2 L050302PES00 Total/NA Solid Fill_Geo-21 68380 160-3482-3 L050303PRS00 Total/NA Solid Fill_Geo-21 68380 160-3482-4 L050304PEQ00 Total/NA Solid Fill_Geo-21 68380 160-3482-5 L050304PES00 Total/NA Solid Fill_Geo-21 68380 160-3482-6 L050305PRS00 Total/NA Solid Fill_Geo-21 68380 160-3482-7 L050306PES00 Total/NA Solid Fill_Geo-21 68380 160-3482-8 L050307PRS00 Total/NA Solid Fill_Geo-21 68380 160-3482-9 L050308PES00 Total/NA Solid Fill_Geo-21 68380 160-3482-10 L050309PRS00 Total/NA Solid Fill_Geo-21 68380 160-3482-11 L050310PES00 Total/NA Solid Fill_Geo-21 68380 160-3482-12 L050311PRS00 Total/NA Solid Fill_Geo-21 68380 160-3482-13 L050312PES00 Total/NA TestAmerica St. Louis Page 29 of 30 1
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QC Association Summary TestAmerica Job ID: 160-3482-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Rad (Continued)
Prep Batch: 69124 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 68380 160-3482-14 L050313PRS00 Total/NA Solid Fill_Geo-21 68380 160-3482-15 L050314PES00 Total/NA Solid Fill_Geo-21 68380 160-3482-16 L050315PRS00 Total/NA Solid Fill_Geo-21 68380 160-3482-17 L050316PES00 Total/NA Solid Fill_Geo-21 68380 160-3482-18 L050317PRS00 Total/NA Solid Fill_Geo-21 68380 160-3482-19 L050318PES00 Total/NA Solid Fill_Geo-21 68380 160-3482-19 DU L050318PES00 Total/NA Solid Fill_Geo-21 68380 160-3482-20 L050319PRS00 Total/NA Solid Fill_Geo-21 LCS 160-69124/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-69124/1-A Method Blank Total/NA Prep Batch: 69138 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 68380 160-3482-21 L050320PES00 Total/NA Solid Fill_Geo-21 68380 160-3482-22 L050321PRS00 Total/NA Solid Fill_Geo-21 68380 160-3482-23 L050322PES00 Total/NA Solid Fill_Geo-21 68380 160-3482-24 L050323PUB00 Total/NA Solid Fill_Geo-21 68380 160-3482-25 L050324PUB00 Total/NA Solid Fill_Geo-21 68380 160-3482-26 L050325PUB00 Total/NA Solid Fill_Geo-21 68380 160-3482-27 L050326PUB00 Total/NA Solid Fill_Geo-21 68380 160-3482-28 L050327PUB00 Total/NA Solid Fill_Geo-21 68380 160-3482-29 L050328PUB00 Total/NA Solid Fill_Geo-21 68380 160-3482-30 L050329PUB00 Total/NA Solid Fill_Geo-21 68380 160-3482-31 L050330PUB00 Total/NA Solid Fill_Geo-21 68380 160-3482-32 L050331PUB00 Total/NA Solid Fill_Geo-21 68380 160-3482-32 DU L050331PUB00 Total/NA Solid Fill_Geo-21 68380 160-3482-33 L050332PUB00 Total/NA Solid Fill_Geo-21 LCS 160-69138/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-69138/1-A Method Blank Total/NA TestAmerica St. Louis Page 30 of 30 1
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