ML18019A705
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3504-1 Client Project/Site: RFP-CBA-022 (7 DAY TAT)
For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:
9/10/2013 2:26:58 PM Rhonda Ridenhower, Customer Service Manager rhonda.ridenhower@testamericainc.com Designee for Ivan Vania, Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-3504-1 Page 2 of 21 TestAmerica St. Louis 9/10/2013 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
6 Definitions/Glossary.......................................
7 Method Summary.........................................
8 Sample Summary.........................................
9 Client Sample Results......................................
10 QC Sample Results........................................
16 QC Association Summary...................................
19 Tracer Carrier Summary....................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3504-1 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3504-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)
Report Number: 160-3504-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 08/23/2013; the samples arrived in good condition, properly preserved. The temperature of the coolers at receipt was 18.0 C.
TECHNETIUM-99 (ICPMS)
Samples L050333PUB00 (160-3504-1), L050334PUB00 (160-3504-2), L050335PUB00 (160-3504-3), L050336PUB00 (160-3504-4),
L050337PUB00 (160-3504-5), L050338PUB00 (160-3504-6), L050339PUB00 (160-3504-7) and L050340PUB00 (160-3504-8) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 08/26/2013 and analyzed on 08/27/2013.
No difficulties were encountered during the Tc-99 analysis.
All quality control parameters were within the acceptance limits.
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3504-1 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3504-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
Samples L050333PUB00 (160-3504-1), L050334PUB00 (160-3504-2), L050335PUB00 (160-3504-3), L050336PUB00 (160-3504-4),
L050337PUB00 (160-3504-5), L050338PUB00 (160-3504-6), L050339PUB00 (160-3504-7) and L050340PUB00 (160-3504-8) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 08/26/2013.
No difficulties were encountered during the % solids analysis.
All quality control parameters were within the acceptance limits.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L050333PUB00 (160-3504-1), L050334PUB00 (160-3504-2), L050335PUB00 (160-3504-3), L050336PUB00 (160-3504-4),
L050337PUB00 (160-3504-5), L050338PUB00 (160-3504-6), L050339PUB00 (160-3504-7) and L050340PUB00 (160-3504-8) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were dried on 08/26/2013, prepared on 08/28/2013 and analyzed on 08/28/2013 and 08/29/2013.
Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of Bismuth-214.
Because the samples have not had a 21-day ingrowth, the activity for Radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between Radium-226 and Bismuth-214 by the loss of Radon-222 during sample preparation.
Bismuth-214/Radium-226 analyzed by gamma spectroscopy was detected above the MDC but below the CRDL in the method blank. The data is reported. (160-3504-1 DU), (LCS 160-69152/2-A), (MB 160-69152/1-A), L050333PUB00 (160-3504-1), L050334PUB00 (160-3504-2), L050335PUB00 (160-3504-3), L050336PUB00 (160-3504-4), L050337PUB00 (160-3504-5), L050338PUB00 (160-3504-6),
L050339PUB00 (160-3504-7), L050340PUB00 (160-3504-8)
The reporting limit for Thorium-234 was not met due to insufficient sample weight available for analysis. Analytical results are reported with the MDC achieved. L050334PUB00 (160-3504-2), L050335PUB00 (160-3504-3), L050338PUB00 (160-3504-6), L050339PUB00 (160-3504-7), L050340PUB00 (160-3504-8)
No other difficulties were encountered during the Gamma spec analysis.
All other quality control parameters were within the acceptance limits.
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10 11 12 IProcedure HDP-PR-QA-006, Chain of Custody Page 1 ofl Hematite Decommissioning Project !Revision: 3 I
I Westinghouse Non-Proprietruy Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the con1ainer is transferred to another organization, a person from each organization should sign the Coe. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutody ID No. I F-082313-01 Page 1/1 Project Name:
Westinghouse Electric Company Contact Person:
Gerald Rood Phone Number:
314-810-3382 Sampler Name Scott Jenkins Sample ID L050333PUBOO L050334PUBOO L050335PUBOO L050336PUBOO L050337PUBOO L050338PUBOO L050339PUBOO L050340PUBOO Company Na.me:
Received by:
Company Name:
Relinquished by:
Comoany Name:
Date Time 8/22/2013 11:20 8/22/2013 11:25 8/22/2013 11:33 8/22/2013 11:40 8/22/2013 11:45 8/23/2013 8:20 8/23/2013 8:25 8/23/2013 8:30 Date/Time g-z:;-11 _
/(d)S Date/Time Date/Time Matrix s
s s
s s
s s
s Rece~by:
Comp~y Name:
el Laboratory Name:
TA-MO Laboratory Address:
13715 Rider Trail North
~!----------------------!
-~ PhoneNo.
8 314-298-8566
~ Laboratory Contact Person:
e-Joe Walker Phone No.
708-870-8453 Turn Around Time Rush (7 days)
Remarks LSA 05-03 Bias LSA 05-03 Bias LSA 05-03 Bias LSA 05-03 Bias LSA 05-03 Bias LSA 05-03 Bias LSA 05-03 Bias LSA 05-03 Bias Cooler Temperature:
Cooler ID: jShipper and Number:
21-Date/Time I Comments: Please re-analyze samples after 21-day ingrowth j""Z 'S
!SD period.
Verified By:
<A
~
~
Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3504-1 Login Number: 3504 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
False Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Qualifiers Rad Qualifier Description U
Indicates the analyte was analyzed for but not detected.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 21 9/10/2013 1
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Sample Summary TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-3504-1 L050333PUB00 Solid 08/22/13 11:20 08/23/13 17:50 160-3504-2 L050334PUB00 Solid 08/22/13 11:25 08/23/13 17:50 160-3504-3 L050335PUB00 Solid 08/22/13 11:33 08/23/13 17:50 160-3504-4 L050336PUB00 Solid 08/22/13 11:40 08/23/13 17:50 160-3504-5 L050337PUB00 Solid 08/22/13 11:45 08/23/13 17:50 160-3504-6 L050338PUB00 Solid 08/23/13 08:20 08/23/13 17:50 160-3504-7 L050339PUB00 Solid 08/23/13 08:25 08/23/13 17:50 160-3504-8 L050340PUB00 Solid 08/23/13 08:30 08/23/13 17:50 TestAmerica St. Louis Page 9 of 21 9/10/2013 1
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Client Sample Results TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3504-1 Client Sample ID: L050333PUB00 Matrix: Solid Date Collected: 08/22/13 11:20 Percent Solids: 91.9 Date Received: 08/23/13 17:50 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00062 0.000019 mg/Kg
08/26/13 10:00 08/27/13 18:40 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.112 U
(2+/-)
0.0480 (2+/-)
1 08/27/13 18:40 08/26/13 10:00 pCi/g 0.213 1.24 RL MDC 0.0408 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/26/13 10:00 08/27/13 18:40 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.718 (2+/-)
0.132 (2+/-)
1 08/29/13 03:03 08/28/13 15:38 pCi/g 0.0962 RL MDC 0.110 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 15:38 08/29/13 03:03 1
0.107 0.0633 0.0633 U
0.00103 Americium 241 pCi/g 08/28/13 15:38 08/29/13 03:03 1
0.410 0.417 0.408 0.807 Bismuth 212 pCi/g 08/28/13 15:38 08/29/13 03:03 1
0.0735 0.115 0.0956 0.622 Bismuth 214 pCi/g 08/28/13 15:38 08/29/13 03:03 1
0.0553 0.119 0.0624 0.784 Lead 212 pCi/g 08/28/13 15:38 08/29/13 03:03 1
0.0576 0.104 0.0718 0.721 Lead 214 pCi/g 08/28/13 15:38 08/29/13 03:03 1
0.228 1.98 1.04 16.5 Potassium 40 pCi/g 08/28/13 15:38 08/29/13 03:03 1
1.03 0.623 0.621 U
-0.454 Protactinium 231 pCi/g 08/28/13 15:38 08/29/13 03:03 1
0.0735 1.00 0.115 0.0956 0.622 Radium 226 pCi/g 08/28/13 15:38 08/29/13 03:03 1
0.963 1.00 1.11 0.900 6.17 Thorium 234 pCi/g 08/28/13 15:38 08/29/13 03:03 1
0.210 0.188 0.157 1.01 Uranium 235 pCi/g 08/28/13 15:38 08/29/13 03:03 1
4.08 3.30 3.24 6.13 Protactinium 234m pCi/g 08/28/13 15:38 08/29/13 03:03 1
0.0962 0.132 0.110 0.718 Thorium 232 Tl-208 0.236 0.0356 0.0432 0.0266 pCi/g 08/28/13 15:38 08/29/13 03:03 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3504-2 Client Sample ID: L050334PUB00 Matrix: Solid Date Collected: 08/22/13 11:25 Percent Solids: 89.2 Date Received: 08/23/13 17:50 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00066 0.000020 mg/Kg
08/26/13 10:00 08/27/13 18:51 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0178 U
(2+/-)
0.0477 (2+/-)
1 08/27/13 18:51 08/26/13 10:00 pCi/g 0.225 1.31 RL MDC
-0.0409 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/26/13 10:00 08/27/13 18:51 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 86 TestAmerica St. Louis Page 10 of 21 9/10/2013 1
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Client Sample Results TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3504-2 Client Sample ID: L050334PUB00 Matrix: Solid Date Collected: 08/22/13 11:25 Date Received: 08/23/13 17:50 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.04 (2+/-)
0.154 (2+/-)
1 08/28/13 22:43 08/28/13 15:38 pCi/g 0.0822 RL MDC 0.112 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.164 0.0992 0.0991 U
0.0570 Americium 241 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.301 0.388 0.356 1.49 Bismuth 212 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.0640 0.120 0.0902 0.757 Bismuth 214 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.0678 0.154 0.0750 1.04 Lead 212 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.0754 0.140 0.0998 0.945 Lead 214 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.353 2.51 1.22 21.4 Potassium 40 pCi/g 08/28/13 15:38 08/28/13 22:43 1
1.23 0.304 0.296 U
0.611 Protactinium 231 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.0640 1.00 0.120 0.0902 0.757 Radium 226 pCi/g 08/28/13 15:38 08/28/13 22:43 1
1.43 1.00 2.84 1.45 23.4 Thorium 234 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.308 0.567 0.311 4.66 Uranium 235 pCi/g 08/28/13 15:38 08/28/13 22:43 1
3.55 6.21 5.40 30.4 Protactinium 234m pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.0822 0.154 0.112 1.04 Thorium 232 Tl-208 0.362 0.0532 0.0651 0.0404 pCi/g 08/28/13 15:38 08/28/13 22:43 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3504-3 Client Sample ID: L050335PUB00 Matrix: Solid Date Collected: 08/22/13 11:33 Percent Solids: 85.3 Date Received: 08/23/13 17:50 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00069 0.000021 mg/Kg
08/26/13 10:00 08/27/13 18:55 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0494 U
(2+/-)
0.00982 (2+/-)
1 08/27/13 18:55 08/26/13 10:00 pCi/g 0.236 1.38 RL MDC
-0.00703 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/26/13 10:00 08/27/13 18:55 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 85 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.03 (2+/-)
0.165 (2+/-)
1 08/28/13 22:42 08/28/13 15:38 pCi/g 0.119 RL MDC 0.128 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.140 0.0841 0.0840 U
-0.0326 Americium 241 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.317 0.389 0.365 1.29 Bismuth 212 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.0821 0.140 0.113 0.797 Bismuth 214 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.0861 0.142 0.0786 0.917 Lead 212 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.0630 0.125 0.0826 0.909 Lead 214 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.389 2.55 1.26 21.6 Potassium 40 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.725 0.383 0.370 0.886 Protactinium 231 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.0821 1.00 0.140 0.113 0.797 Radium 226 TestAmerica St. Louis Page 11 of 21 9/10/2013 1
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Client Sample Results TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3504-3 Client Sample ID: L050335PUB00 Matrix: Solid Date Collected: 08/22/13 11:33 Date Received: 08/23/13 17:50 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 6.43 (2+/-)
1.28 (2+/-)
1 08/28/13 22:42 08/28/13 15:38 pCi/g 1.15 1.00 RL MDC 1.09 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.253 0.214 0.186 1.05 Uranium 235 pCi/g 08/28/13 15:38 08/28/13 22:42 1
5.10 3.57 3.50 6.75 Protactinium 234m pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.119 0.165 0.128 1.03 Thorium 232 Tl-208 0.393 0.0514 0.0656 0.0380 pCi/g 08/28/13 15:38 08/28/13 22:42 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3504-4 Client Sample ID: L050336PUB00 Matrix: Solid Date Collected: 08/22/13 11:40 Percent Solids: 85.6 Date Received: 08/23/13 17:50 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00068 0.000020 mg/Kg
08/26/13 10:00 08/27/13 18:59 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0334 U
(2+/-)
0.0947 (2+/-)
1 08/27/13 18:59 08/26/13 10:00 pCi/g 0.232 1.35 RL MDC
-0.0817 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/26/13 10:00 08/27/13 18:59 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 86 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.23 (2+/-)
0.189 (2+/-)
1 08/28/13 22:43 08/28/13 15:38 pCi/g 0.132 RL MDC 0.142 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.106 0.0626 0.0626 U
0.0114 Americium 241 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.347 0.427 0.404 1.32 Bismuth 212 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.0918 0.154 0.124 0.874 Bismuth 214 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.0653 0.175 0.0855 1.18 Lead 212 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.0849 0.130 0.0904 0.901 Lead 214 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.333 2.39 1.38 19.1 Potassium 40 pCi/g 08/28/13 15:38 08/28/13 22:43 1
1.36 0.267 0.262 U
0.500 Protactinium 231 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.0918 1.00 0.154 0.124 0.874 Radium 226 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.981 1.00 0.868 0.795 3.35 Thorium 234 pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.236 0.179 0.176 0.341 Uranium 235 pCi/g 08/28/13 15:38 08/28/13 22:43 1
5.85 3.65 3.64 U
1.95 Protactinium 234m pCi/g 08/28/13 15:38 08/28/13 22:43 1
0.132 0.189 0.142 1.23 Thorium 232 Tl-208 0.392 0.0637 0.0756 0.0475 pCi/g 08/28/13 15:38 08/28/13 22:43 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 12 of 21 9/10/2013 1
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Client Sample Results TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3504-5 Client Sample ID: L050337PUB00 Matrix: Solid Date Collected: 08/22/13 11:45 Percent Solids: 84.8 Date Received: 08/23/13 17:50 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00068 0.000020 mg/Kg
08/26/13 10:00 08/27/13 19:03 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0562 U
(2+/-)
0.0492 (2+/-)
1 08/27/13 19:03 08/26/13 10:00 pCi/g 0.233 1.36 RL MDC
-0.0424 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/26/13 10:00 08/27/13 19:03 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.27 (2+/-)
0.198 (2+/-)
1 08/28/13 22:44 08/28/13 15:38 pCi/g 0.116 RL MDC 0.149 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 15:38 08/28/13 22:44 1
0.0957 0.0567 0.0566 U
-0.0141 Americium 241 pCi/g 08/28/13 15:38 08/28/13 22:44 1
0.608 0.392 0.389 U
0.470 Bismuth 212 pCi/g 08/28/13 15:38 08/28/13 22:44 1
0.0790 0.140 0.112 0.810 Bismuth 214 pCi/g 08/28/13 15:38 08/28/13 22:44 1
0.0783 0.162 0.0885 1.04 Lead 212 pCi/g 08/28/13 15:38 08/28/13 22:44 1
0.106 0.150 0.111 0.966 Lead 214 pCi/g 08/28/13 15:38 08/28/13 22:44 1
0.202 2.52 1.48 20.0 Potassium 40 pCi/g 08/28/13 15:38 08/28/13 22:44 1
1.42 0.227 0.222 U
0.421 Protactinium 231 pCi/g 08/28/13 15:38 08/28/13 22:44 1
0.0790 1.00 0.140 0.112 0.810 Radium 226 pCi/g 08/28/13 15:38 08/28/13 22:44 1
0.949 1.00 0.847 0.765 3.49 Thorium 234 pCi/g 08/28/13 15:38 08/28/13 22:44 1
0.217 0.183 0.177 0.436 Uranium 235 pCi/g 08/28/13 15:38 08/28/13 22:44 1
8.02 4.79 4.78 U
-2.99 Protactinium 234m pCi/g 08/28/13 15:38 08/28/13 22:44 1
0.116 0.198 0.149 1.27 Thorium 232 Tl-208 0.404 0.0620 0.0748 0.0441 pCi/g 08/28/13 15:38 08/28/13 22:44 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3504-6 Client Sample ID: L050338PUB00 Matrix: Solid Date Collected: 08/23/13 08:20 Percent Solids: 81.6 Date Received: 08/23/13 17:50 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00073 0.000022 mg/Kg
08/26/13 10:00 08/27/13 19:15 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0110 U
(2+/-)
0.0743 (2+/-)
1 08/27/13 19:15 08/26/13 10:00 pCi/g 0.250 1.46 RL MDC 0.0628 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/26/13 10:00 08/27/13 19:15 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 85 TestAmerica St. Louis Page 13 of 21 9/10/2013 1
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Client Sample Results TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3504-6 Client Sample ID: L050338PUB00 Matrix: Solid Date Collected: 08/23/13 08:20 Date Received: 08/23/13 17:50 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.04 (2+/-)
0.199 (2+/-)
1 08/28/13 22:42 08/28/13 15:38 pCi/g 0.118 RL MDC 0.169 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.139 0.0831 0.0831 U
-0.0130 Americium 241 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.423 0.508 0.480 1.58 Bismuth 212 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.0739 0.128 0.101 0.756 Bismuth 214 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.0658 0.169 0.0794 1.15 Lead 212 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.0706 0.127 0.0827 0.921 Lead 214 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.355 2.40 1.25 20.1 Potassium 40 pCi/g 08/28/13 15:38 08/28/13 22:42 1
1.23 0.209 0.204 U
0.396 Protactinium 231 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.0739 1.00 0.128 0.101 0.756 Radium 226 pCi/g 08/28/13 15:38 08/28/13 22:42 1
1.16 1.00 1.50 1.07 10.0 Thorium 234 pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.234 0.289 0.224 1.79 Uranium 235 pCi/g 08/28/13 15:38 08/28/13 22:42 1
5.09 4.50 4.32 12.6 Protactinium 234m pCi/g 08/28/13 15:38 08/28/13 22:42 1
0.118 0.199 0.169 1.04 Thorium 232 Tl-208 0.361 0.0483 0.0612 0.0362 pCi/g 08/28/13 15:38 08/28/13 22:42 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3504-7 Client Sample ID: L050339PUB00 Matrix: Solid Date Collected: 08/23/13 08:25 Percent Solids: 81.5 Date Received: 08/23/13 17:50 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00070 0.000021 mg/Kg
08/26/13 10:00 08/27/13 19:19 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0188 U
(2+/-)
0.0625 (2+/-)
1 08/27/13 19:19 08/26/13 10:00 pCi/g 0.241 1.41 RL MDC
-0.0547 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/26/13 10:00 08/27/13 19:19 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.13 (2+/-)
0.178 (2+/-)
1 08/28/13 22:03 08/28/13 15:38 pCi/g 0.152 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 15:38 08/28/13 22:03 1
0.152 91.0 91.0 U
-0.0365 Americium 241 pCi/g 08/28/13 15:38 08/28/13 22:03 1
0.394 0.448 0.431 1.25 Bismuth 212 pCi/g 08/28/13 15:38 08/28/13 22:03 1
0.0697 0.123 0.0975 0.764 Bismuth 214 pCi/g 08/28/13 15:38 08/28/13 22:03 1
0.0743 0.152 0.0854 1.16 Lead 212 pCi/g 08/28/13 15:38 08/28/13 22:03 1
0.0907 0.145 0.112 0.948 Lead 214 pCi/g 08/28/13 15:38 08/28/13 22:03 1
0.380 2.65 1.43 23.1 Potassium 40 pCi/g 08/28/13 15:38 08/28/13 22:03 1
1.46 0.252 0.247 U
0.484 Protactinium 231 pCi/g 08/28/13 15:38 08/28/13 22:03 1
0.0697 1.00 0.123 0.0975 0.764 Radium 226 TestAmerica St. Louis Page 14 of 21 9/10/2013 1
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Client Sample Results TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3504-7 Client Sample ID: L050339PUB00 Matrix: Solid Date Collected: 08/23/13 08:25 Date Received: 08/23/13 17:50 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 11.5 (2+/-)
1.83 (2+/-)
1 08/28/13 22:03 08/28/13 15:38 pCi/g 1.44 1.00 RL MDC 1.44 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 15:38 08/28/13 22:03 1
0.313 0.343 0.244 2.49 Uranium 235 pCi/g 08/28/13 15:38 08/28/13 22:03 1
4.27 6.12 5.80 20.3 Protactinium 234m pCi/g 08/28/13 15:38 08/28/13 22:03 1
0.152 0.178 0.141 1.13 Thorium 232 Tl-208 0.403 0.0568 0.0690 0.0396 pCi/g 08/28/13 15:38 08/28/13 22:03 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3504-8 Client Sample ID: L050340PUB00 Matrix: Solid Date Collected: 08/23/13 08:30 Percent Solids: 81.6 Date Received: 08/23/13 17:50 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00067 0.000020 mg/Kg
08/26/13 10:00 08/27/13 19:22 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99
-0.0516 U
(2+/-)
0.0229 (2+/-)
1 08/27/13 19:22 08/26/13 10:00 pCi/g 0.229 1.34 RL MDC
-0.0204 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/26/13 10:00 08/27/13 19:22 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.08 (2+/-)
0.196 (2+/-)
1 08/28/13 23:19 08/28/13 15:38 pCi/g 0.175 RL MDC 0.162 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/28/13 15:38 08/28/13 23:19 1
0.186 0.112 0.112 U
-0.0436 Americium 241 pCi/g 08/28/13 15:38 08/28/13 23:19 1
0.589 0.481 0.465 1.21 Bismuth 212 pCi/g 08/28/13 15:38 08/28/13 23:19 1
0.0646 0.159 0.125 0.947 Bismuth 214 pCi/g 08/28/13 15:38 08/28/13 23:19 1
0.0776 0.174 0.0947 1.13 Lead 212 pCi/g 08/28/13 15:38 08/28/13 23:19 1
0.105 0.151 0.110 0.990 Lead 214 pCi/g 08/28/13 15:38 08/28/13 23:19 1
0.587 2.70 1.70 20.5 Potassium 40 pCi/g 08/28/13 15:38 08/28/13 23:19 1
1.72 0.344 0.337 U
0.668 Protactinium 231 pCi/g 08/28/13 15:38 08/28/13 23:19 1
0.0646 1.00 0.159 0.125 0.947 Radium 226 pCi/g 08/28/13 15:38 08/28/13 23:19 1
1.70 1.00 2.11 1.64 12.7 Thorium 234 pCi/g 08/28/13 15:38 08/28/13 23:19 1
0.309 0.406 0.307 2.61 Uranium 235 pCi/g 08/28/13 15:38 08/28/13 23:19 1
4.98 5.74 5.55 14.6 Protactinium 234m pCi/g 08/28/13 15:38 08/28/13 23:19 1
0.175 0.196 0.162 1.08 Thorium 232 Tl-208 0.416 0.0673 0.0800 0.0438 pCi/g 08/28/13 15:38 08/28/13 23:19 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 15 of 21 9/10/2013 1
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QC Sample Results TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-68468/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68468 RL MDL Technetium 99 ND 0.00053 0.000016 mg/Kg 08/26/13 10:00 08/27/13 18:32 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-68468/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68468 Technetium 99 0.00253 0.00250 mg/Kg 99 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: L050333PUB00 Lab Sample ID: 160-3504-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68468 Technetium 99 ND 0.00282 0.00267 mg/Kg 94 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: L050333PUB00 Lab Sample ID: 160-3504-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68468 Technetium 99 ND 0.00295 0.00269 mg/Kg 91 75 - 125 1
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-68468/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68468 Technetium 99 Analyte U
1 08/27/13 18:32 08/26/13 10:00 pCi/g 0.183 MDC 1.07 RL 0.0347
-0.0322 (2+/-)
(2+/-)
MB
-0.03681 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 08/26/13 10:00 08/27/13 18:32 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 93 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-68468/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68468 Technetium 99 Analyte 120 80 99 42.88 43.3 4.38 1.08 0.185 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 92 LCS TestAmerica St. Louis Page 16 of 21 9/10/2013 1
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QC Sample Results TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: L050333PUB00 Lab Sample ID: 160-3504-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68468 Technetium 99 Analyte 125 75 94 45.63 48.3 0.112 U
4.92 1.21 0.207 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 90 MS Client Sample ID: L050333PUB00 Lab Sample ID: 160-3504-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68468 Technetium 99 Analyte 1
0.04 125 75 91 46.03 50.4 0.112 U
4.99 1.26 0.216 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 86 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-69152/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 69120 Prep Batch: 69152 Actinium 228 Analyte U
1 08/28/13 22:04 08/28/13 15:38 pCi/g 0.0379 MDC RL 0.0268 0.0268 (2+/-)
(2+/-)
MB 0.008818 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
08/28/13 22:04 08/28/13 15:38 pCi/g 0.0353 0.00898 0.00898 U
0.0000 Americium 241 1
08/28/13 22:04 08/28/13 15:38 pCi/g 0.237 0.127 0.127 U
0.03646 Bismuth 212 1
08/28/13 22:04 08/28/13 15:38 pCi/g 0.0484 0.0469 0.0461 0.08036 Bismuth 214 1
08/28/13 22:04 08/28/13 15:38 pCi/g 0.0297 0.0271 0.0271 U
-0.002784 Lead 212 1
08/28/13 22:04 08/28/13 15:38 pCi/g 0.0443 0.0232 0.0230 U
0.02607 Lead 214 1
08/28/13 22:04 08/28/13 15:38 pCi/g 0.471 0.0430 0.0430 U
0.0000 Potassium 40 1
08/28/13 22:04 08/28/13 15:38 pCi/g 0.379 0.173 0.173 U
0.03679 Protactinium 231 1
08/28/13 22:04 08/28/13 15:38 pCi/g 0.0484 1.00 0.0469 0.0461 0.08036 Radium 226 1
08/28/13 22:04 08/28/13 15:38 pCi/g 0.307 1.00 0.164 0.164 U
0.08769 Thorium 234 1
08/28/13 22:04 08/28/13 15:38 pCi/g 0.0767 0.0439 0.0438 U
0.01639 Uranium 235 1
08/28/13 22:04 08/28/13 15:38 pCi/g 1.43 1.04 1.04 U
0.1185 Protactinium 234m 1
08/28/13 22:04 08/28/13 15:38 pCi/g 0.0379 0.0268 0.0268 U
0.008818 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 08/28/13 15:38 08/28/13 22:04 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 17 of 21 9/10/2013 1
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QC Sample Results TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-69152/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 69121 Prep Batch: 69152 Americium 241 Analyte 116 87 91 89.28 97.7 9.29 0.429 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 31.7 29.69 3.11 0.200 0.128 pCi/g 94 87 - 120 Cobalt 60 24.8 22.58 2.28 0.0771 pCi/g 91 87 - 115 Client Sample ID: L050333PUB00 Lab Sample ID: 160-3504-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 69117 Prep Batch: 69152 Actinium 228 Analyte 1
0.61 0.5614 0.718 0.124 0.105 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241 0.00103 U
0.02207 U
0.0684 0.114 pCi/g 0.16 1
Bismuth 212 0.807 1.070 0.429 0.356 pCi/g 0.31 1
Bismuth 214 0.622 0.6551 0.110 0.0612 pCi/g 0.15 1
Lead 212 0.784 0.8112 0.122 0.0532 pCi/g 0.11 1
Lead 214 0.721 0.7528 0.104 0.0584 pCi/g 0.15 1
Potassium 40 16.5 16.51 1.98 0.284 pCi/g 0
1 Protactinium 231
-0.454 U
0.09418 U
0.440 0.759 pCi/g 0.52 1
Radium 226 0.622 0.6551 0.110 1.00 0.0612 pCi/g 0.15 1
Thorium 234 6.17 6.104 1.09 1.00 0.938 pCi/g 0.03 1
Uranium 235 1.01 0.9641 0.200 0.196 pCi/g 0.12 1
Protactinium 234m 6.13 5.977 3.15 4.46 pCi/g 0.02 1
Thorium 232 0.718 0.5614 0.124 0.105 pCi/g 0.61 1
TestAmerica St. Louis Page 18 of 21 9/10/2013 1
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QC Association Summary TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Metals Prep Batch: 68468 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3504-1 L050333PUB00 Total/NA Solid None 160-3504-1 MS L050333PUB00 Total/NA Solid None 160-3504-1 MSD L050333PUB00 Total/NA Solid None 160-3504-2 L050334PUB00 Total/NA Solid None 160-3504-3 L050335PUB00 Total/NA Solid None 160-3504-4 L050336PUB00 Total/NA Solid None 160-3504-5 L050337PUB00 Total/NA Solid None 160-3504-6 L050338PUB00 Total/NA Solid None 160-3504-7 L050339PUB00 Total/NA Solid None 160-3504-8 L050340PUB00 Total/NA Solid None LCS 160-68468/2-A Lab Control Sample Total/NA Solid None MB 160-68468/1-A Method Blank Total/NA Analysis Batch: 68965 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 68468 160-3504-1 L050333PUB00 Total/NA Solid 6020A 68468 160-3504-1 MS L050333PUB00 Total/NA Solid 6020A 68468 160-3504-1 MSD L050333PUB00 Total/NA Solid 6020A 68468 160-3504-2 L050334PUB00 Total/NA Solid 6020A 68468 160-3504-3 L050335PUB00 Total/NA Solid 6020A 68468 160-3504-4 L050336PUB00 Total/NA Solid 6020A 68468 160-3504-5 L050337PUB00 Total/NA Solid 6020A 68468 160-3504-6 L050338PUB00 Total/NA Solid 6020A 68468 160-3504-7 L050339PUB00 Total/NA Solid 6020A 68468 160-3504-8 L050340PUB00 Total/NA Solid 6020A 68468 LCS 160-68468/2-A Lab Control Sample Total/NA Solid 6020A 68468 MB 160-68468/1-A Method Blank Total/NA General Chemistry Analysis Batch: 68432 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3504-1 L050333PUB00 Total/NA Solid Moisture 160-3504-2 L050334PUB00 Total/NA Solid Moisture 160-3504-3 L050335PUB00 Total/NA Solid Moisture 160-3504-4 L050336PUB00 Total/NA Solid Moisture 160-3504-5 L050337PUB00 Total/NA Solid Moisture 160-3504-6 L050338PUB00 Total/NA Solid Moisture 160-3504-7 L050339PUB00 Total/NA Solid Moisture 160-3504-8 L050340PUB00 Total/NA Solid Moisture 160-3504-8 DU L050340PUB00 Total/NA Rad Leach Batch: 68464 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3504-1 L050333PUB00 Total/NA Solid Dry and Grind 160-3504-1 DU L050333PUB00 Total/NA Solid Dry and Grind 160-3504-2 L050334PUB00 Total/NA Solid Dry and Grind 160-3504-3 L050335PUB00 Total/NA TestAmerica St. Louis Page 19 of 21 9/10/2013 1
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QC Association Summary TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Rad (Continued)
Leach Batch: 68464 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3504-4 L050336PUB00 Total/NA Solid Dry and Grind 160-3504-5 L050337PUB00 Total/NA Solid Dry and Grind 160-3504-6 L050338PUB00 Total/NA Solid Dry and Grind 160-3504-7 L050339PUB00 Total/NA Solid Dry and Grind 160-3504-8 L050340PUB00 Total/NA Prep Batch: 68468 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3504-1 L050333PUB00 Total/NA Solid None 160-3504-1 MS L050333PUB00 Total/NA Solid None 160-3504-1 MSD L050333PUB00 Total/NA Solid None 160-3504-2 L050334PUB00 Total/NA Solid None 160-3504-3 L050335PUB00 Total/NA Solid None 160-3504-4 L050336PUB00 Total/NA Solid None 160-3504-5 L050337PUB00 Total/NA Solid None 160-3504-6 L050338PUB00 Total/NA Solid None 160-3504-7 L050339PUB00 Total/NA Solid None 160-3504-8 L050340PUB00 Total/NA Solid None LCS 160-68468/2-A Lab Control Sample Total/NA Solid None MB 160-68468/1-A Method Blank Total/NA Prep Batch: 69152 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 68464 160-3504-1 L050333PUB00 Total/NA Solid Fill_Geo-0 68464 160-3504-1 DU L050333PUB00 Total/NA Solid Fill_Geo-0 68464 160-3504-2 L050334PUB00 Total/NA Solid Fill_Geo-0 68464 160-3504-3 L050335PUB00 Total/NA Solid Fill_Geo-0 68464 160-3504-4 L050336PUB00 Total/NA Solid Fill_Geo-0 68464 160-3504-5 L050337PUB00 Total/NA Solid Fill_Geo-0 68464 160-3504-6 L050338PUB00 Total/NA Solid Fill_Geo-0 68464 160-3504-7 L050339PUB00 Total/NA Solid Fill_Geo-0 68464 160-3504-8 L050340PUB00 Total/NA Solid Fill_Geo-0 LCS 160-69152/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-69152/1-A Method Blank Total/NA TestAmerica St. Louis Page 20 of 21 9/10/2013 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-3504-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 88 160-3504-1 Percent Yield (Acceptance Limits)
L050333PUB00 90 160-3504-1 MS L050333PUB00 86 160-3504-1 MSD L050333PUB00 86 160-3504-2 L050334PUB00 85 160-3504-3 L050335PUB00 86 160-3504-4 L050336PUB00 87 160-3504-5 L050337PUB00 85 160-3504-6 L050338PUB00 88 160-3504-7 L050339PUB00 92 160-3504-8 L050340PUB00 92 LCS 160-68468/2-A Lab Control Sample 93 MB 160-68468/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 21 of 21 9/10/2013 1
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