ML18019A673

Westinghouse Hematite Decommissioning Project - Final Status Survey Final Report Volume 3, Chapter 16, Survey Area Release Record for Land Survey Area 05, Survey Units 01, 02, 03 and 04, Revision 1, 3435-2 Uds Level 2 Report Final Report

ML18019A673
Person / Time
Site:	07000036
Issue date:	01/09/2018
From:	Westinghouse
To:	Office of Nuclear Material Safety and Safeguards
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HEM-18-2
Download: ML18019A673 (29)

Text

ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3435-2 Client Project/Site: RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

9/19/2013 6:05:33 AM Ivan Vania, Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-3435-2 Page 2 of 29 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

5 Receipt Checklists.........................................

8 Definitions/Glossary.......................................

9 Method Summary.........................................

10 Sample Summary.........................................

11 Client Sample Results......................................

12 QC Sample Results........................................

26 QC Association Summary...................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3435-2 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-3435-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)

Report Number: 160-3435-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 08/20/2013; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 22.0º C and 22.0º C.

TECHNETIUM-99 (ICPMS)

Samples L050190TUB00 (160-3435-1), L050191TUB00 (160-3435-2), L050192TUB00 (160-3435-3), L050193TUB00 (160-3435-4),

L050194TUB00 (160-3435-5), L050195TUB00 (160-3435-6), L050196TUB00 (160-3435-7), L050197TUB00 (160-3435-8),

L050247PRS00 (160-3435-9), L050248PES00 (160-3435-10), L050249PRS00 (160-3435-11), L050250PES00 (160-3435-12),

L050251PRS00 (160-3435-13), L050252PES00 (160-3435-14), L050253PES00 (160-3435-15), L050254PES00 (160-3435-16),

L050255PES00 (160-3435-17), L050256PRS00 (160-3435-18), L050257PES00 (160-3435-19), L050258PES00 (160-3435-20),

L050259PRQ00 (160-3435-21), L050259PRS00 (160-3435-22), L050260PES00 (160-3435-23), L050261PRS00 (160-3435-24),

L050262PES00 (160-3435-25), L050263PES00 (160-3435-26), L050264PRS00 (160-3435-27), L050265PES00 (160-3435-28),

L050266PUB00 (160-3435-29), L050267PUB00 (160-3435-30) and L050268PUB00 (160-3435-31) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 08/22/2013 and analyzed on 08/23/2013.

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3435-2 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-3435-2 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

No difficulties were encountered during the Tc-99 analysis. All quality control parameters were within the acceptance limits.

PERCENT SOLIDS Samples L050190TUB00 (160-3435-1), L050191TUB00 (160-3435-2), L050192TUB00 (160-3435-3), L050193TUB00 (160-3435-4),

L050194TUB00 (160-3435-5), L050195TUB00 (160-3435-6), L050196TUB00 (160-3435-7), L050197TUB00 (160-3435-8),

L050247PRS00 (160-3435-9), L050248PES00 (160-3435-10), L050249PRS00 (160-3435-11), L050250PES00 (160-3435-12),

L050251PRS00 (160-3435-13), L050252PES00 (160-3435-14), L050253PES00 (160-3435-15), L050254PES00 (160-3435-16),

L050255PES00 (160-3435-17), L050256PRS00 (160-3435-18), L050257PES00 (160-3435-19), L050258PES00 (160-3435-20),

L050259PRQ00 (160-3435-21), L050259PRS00 (160-3435-22), L050260PES00 (160-3435-23), L050261PRS00 (160-3435-24),

L050262PES00 (160-3435-25), L050263PES00 (160-3435-26), L050264PRS00 (160-3435-27), L050265PES00 (160-3435-28),

L050266PUB00 (160-3435-29), L050267PUB00 (160-3435-30) and L050268PUB00 (160-3435-31) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 08/22/2013.

No difficulties were encountered during the % solids analysis. All quality control parameters were within the acceptance limits.

RADIUM-226 & OTHER GAMMA EMITTERS (GS)

Samples L050190TUB00 (160-3435-1), L050191TUB00 (160-3435-2), L050192TUB00 (160-3435-3), L050193TUB00 (160-3435-4),

L050194TUB00 (160-3435-5), L050195TUB00 (160-3435-6), L050196TUB00 (160-3435-7), L050197TUB00 (160-3435-8),

L050247PRS00 (160-3435-9), L050248PES00 (160-3435-10), L050249PRS00 (160-3435-11), L050250PES00 (160-3435-12),

L050251PRS00 (160-3435-13), L050252PES00 (160-3435-14), L050253PES00 (160-3435-15), L050254PES00 (160-3435-16),

L050255PES00 (160-3435-17), L050256PRS00 (160-3435-18), L050257PES00 (160-3435-19), L050258PES00 (160-3435-20),

L050259PRQ00 (160-3435-21), L050259PRS00 (160-3435-22), L050260PES00 (160-3435-23), L050261PRS00 (160-3435-24),

L050262PES00 (160-3435-25), L050263PES00 (160-3435-26), L050264PRS00 (160-3435-27), L050265PES00 (160-3435-28),

L050266PUB00 (160-3435-29), L050267PUB00 (160-3435-30) and L050268PUB00 (160-3435-31) were analyzed for Cesium-137 &

Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 08/21/2013, prepared on 08/23/2013 and analyzed on 08/23/2013, 08/25/2013 and 08/28/2013.

No other difficulties were encountered during the Gamma spec analysis. All other quality control parameters were within the acceptance limits.

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I

Page I of!

Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HOP.

Chain of Cutodv ID No.

F-082013-01 Pal!e 1/1

. Requested Analysis Laboratorv Na.me:

Project Name:

• • -.: G' TA-MO Westinghouse Electric Company N

I.

N I*

Ji I

Contact Person:

~.*:

Laboratory Address:

Gerald Rood

<8 13715 Rider Trail North

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Phone Number:

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tlJ) 314-810-3382

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" 314-298-8566 8

Sampler Name

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Thomas Y ardy 8

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Joe Walker

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ciate/fime '.) ~..,!ived by: /2, fl Date/fime Total Cooler Temperature:

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Cooler ID: Shipper and Number:

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ed b'klL Date/fime Comments: Please re-analyze samples after 21-day ingrowth

(!}_ /io t' "J

period.

Company Name:

!Company N~s I f':..f;,;s~v-n 5

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Company Name:

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I

Page 1 ofl Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization., a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutodv ID No.

F-081913-01 Pa2e 1/2 Reauested Analvsis Laboratorv Name:

Project Name:

TA-MO

\\C Westinghouse Electric Company N

N

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Contact Person:

I>

Laboratory Address:

Gerald Rood

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C X

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~inq~ed by:? £l, Date/Time Comments: Please re-analyze samples after 2l"day ingrowth

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I

Page I of l Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutodv ID No.

F-081913-01 Pa2e 2/2 Requested Analvsis Laboratorv Name:

Project Name:

>*c.c TA-MO I

'° N

Westinghouse Electric Company N

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Contact Person:

1, Laboratory Address:

Gerald Rood

<-8 13715 Rider Trail North

~

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0 C:

Phone Number:

• i Phone No.

bl) 314-810-3382

.5 314-298-8566

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Scott Jenkins

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Phone No.

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Date/Time Total Cooler Temperature:

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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3435-2 Login Number: 3435 Question Answer Comment Creator: Daniels, Brian J List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

False Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Qualifiers Rad Qualifier Description U

Indicates the analyte was analyzed for but not detected.

Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 10 of 29 1

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Sample Summary TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-3435-1 L050190TUB00 Solid 08/19/13 13:45 08/20/13 16:06 160-3435-2 L050191TUB00 Solid 08/19/13 13:55 08/20/13 16:06 160-3435-3 L050192TUB00 Solid 08/19/13 14:05 08/20/13 16:06 160-3435-4 L050193TUB00 Solid 08/19/13 14:15 08/20/13 16:06 160-3435-5 L050194TUB00 Solid 08/19/13 14:25 08/20/13 16:06 160-3435-6 L050195TUB00 Solid 08/19/13 14:35 08/20/13 16:06 160-3435-7 L050196TUB00 Solid 08/19/13 14:45 08/20/13 16:06 160-3435-8 L050197TUB00 Solid 08/19/13 14:55 08/20/13 16:06 160-3435-9 L050247PRS00 Solid 08/16/13 15:40 08/20/13 16:06 160-3435-10 L050248PES00 Solid 08/16/13 15:55 08/20/13 16:06 160-3435-11 L050249PRS00 Solid 08/16/13 14:15 08/20/13 16:06 160-3435-12 L050250PES00 Solid 08/16/13 14:25 08/20/13 16:06 160-3435-13 L050251PRS00 Solid 08/19/13 08:35 08/20/13 16:06 160-3435-14 L050252PES00 Solid 08/19/13 10:15 08/20/13 16:06 160-3435-15 L050253PES00 Solid 08/19/13 08:45 08/20/13 16:06 160-3435-16 L050254PES00 Solid 08/19/13 08:40 08/20/13 16:06 160-3435-17 L050255PES00 Solid 08/16/13 13:50 08/20/13 16:06 160-3435-18 L050256PRS00 Solid 08/19/13 08:55 08/20/13 16:06 160-3435-19 L050257PES00 Solid 08/19/13 10:20 08/20/13 16:06 160-3435-20 L050258PES00 Solid 08/16/13 13:40 08/20/13 16:06 160-3435-21 L050259PRQ00 Solid 08/19/13 15:20 08/20/13 16:06 160-3435-22 L050259PRS00 Solid 08/16/13 15:20 08/20/13 16:06 160-3435-23 L050260PES00 Solid 08/16/13 15:30 08/20/13 16:06 160-3435-24 L050261PRS00 Solid 08/16/13 09:05 08/20/13 16:06 160-3435-25 L050262PES00 Solid 08/19/13 10:30 08/20/13 16:06 160-3435-26 L050263PES00 Solid 08/19/13 13:30 08/20/13 16:06 160-3435-27 L050264PRS00 Solid 08/16/13 14:50 08/20/13 16:06 160-3435-28 L050265PES00 Solid 08/16/13 15:00 08/20/13 16:06 160-3435-29 L050266PUB00 Solid 08/16/13 11:50 08/20/13 16:06 160-3435-30 L050267PUB00 Solid 08/16/13 11:55 08/20/13 16:06 160-3435-31 L050268PUB00 Solid 08/16/13 12:00 08/20/13 16:06 TestAmerica St. Louis Page 11 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-1 Client Sample ID: L050190TUB00 Matrix: Solid Date Collected: 08/19/13 13:45 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.874 (2+/-)

0.157 (2+/-)

1 09/13/13 16:24 08/23/13 09:35 pCi/g 0.109 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 16:24 1

0.385 0.511 0.484 1.57 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 16:24 1

0.0725 0.147 0.107 0.963 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 16:24 1

0.0786 0.129 0.0725 0.820 Lead 212 pCi/g 08/23/13 09:35 09/13/13 16:24 1

0.0784 0.141 0.0892 1.06 Lead 214 pCi/g 08/23/13 09:35 09/13/13 16:24 1

0.342 2.08 1.10 17.3 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 16:24 1

1.03 0.167 0.166 U

0.184 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 16:24 1

0.0725 1.00 0.147 0.107 0.963 Radium 226 pCi/g 08/23/13 09:35 09/13/13 16:24 1

0.109 0.157 0.129 0.874 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 16:24 1

0.760 0.575 0.566 0.986 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 16:24 1

0.244 0.140 0.140 U

0.0664 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 16:24 1

0.0757 0.0574 0.0569 U

0.0736 Americium 241 pCi/g 08/23/13 09:35 09/13/13 16:24 1

5.09 2.90 2.90 U

0.499 Protactinium 234m Lab Sample ID: 160-3435-2 Client Sample ID: L050191TUB00 Matrix: Solid Date Collected: 08/19/13 13:55 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.785 (2+/-)

0.140 (2+/-)

1 09/13/13 16:25 08/23/13 09:35 pCi/g 0.110 RL MDC 0.115 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 16:25 1

0.548 0.337 0.335 U

0.289 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 16:25 1

0.0596 0.143 0.104 0.949 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 16:25 1

0.0576 0.124 0.0693 0.791 Lead 212 pCi/g 08/23/13 09:35 09/13/13 16:25 1

0.0737 0.152 0.101 1.10 Lead 214 pCi/g 08/23/13 09:35 09/13/13 16:25 1

0.287 1.77 1.11 13.5 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 16:25 1

1.14 0.192 0.189 U

0.313 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 16:25 1

0.0596 1.00 0.143 0.104 0.949 Radium 226 pCi/g 08/23/13 09:35 09/13/13 16:25 1

0.110 0.140 0.115 0.785 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 16:25 1

0.767 0.316 0.299 0.988 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 16:25 1

0.184 0.137 0.137 U

0.136 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 16:25 1

0.100 0.115 0.115 U

-0.0236 Americium 241 pCi/g 08/23/13 09:35 09/13/13 16:25 1

5.19 2.29 2.25 U

4.40 Protactinium 234m Lab Sample ID: 160-3435-3 Client Sample ID: L050192TUB00 Matrix: Solid Date Collected: 08/19/13 14:05 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.249 (2+/-)

0.0999 (2+/-)

1 09/13/13 16:26 08/23/13 09:35 pCi/g 0.0785 RL MDC 0.0966 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 16:26 1

0.490 0.276 0.275 U

0.0807 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 16:26 1

0.0723 0.138 0.112 0.782 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 16:26 1

0.0558 0.0576 0.0482 0.244 Lead 212 TestAmerica St. Louis Page 12 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-3 Client Sample ID: L050192TUB00 Matrix: Solid Date Collected: 08/19/13 14:05 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 0.964 (2+/-)

0.138 (2+/-)

1 09/13/13 16:26 08/23/13 09:35 pCi/g 0.0612 RL MDC 0.0947 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 16:26 1

0.383 0.667 0.595 2.94 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 16:26 1

0.876 0.411 0.410 U

0.159 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 16:26 1

0.0723 1.00 0.138 0.112 0.782 Radium 226 pCi/g 08/23/13 09:35 09/13/13 16:26 1

0.0785 0.0999 0.0966 0.249 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 16:26 1

0.859 0.480 0.453 1.50 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 16:26 1

0.167 0.151 0.146 0.347 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 16:26 1

0.0774 0.0465 0.0464 U

0.0279 Americium 241 pCi/g 08/23/13 09:35 09/13/13 16:26 1

5.82 3.19 3.19 U

0.468 Protactinium 234m Lab Sample ID: 160-3435-4 Client Sample ID: L050193TUB00 Matrix: Solid Date Collected: 08/19/13 14:15 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.672 (2+/-)

0.117 (2+/-)

1 09/13/13 16:27 08/23/13 09:35 pCi/g 0.0951 RL MDC 0.0944 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 16:27 1

0.262 0.345 0.327 1.07 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 16:27 1

0.0712 0.142 0.104 0.939 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 16:27 1

0.0532 0.114 0.0625 0.741 Lead 212 pCi/g 08/23/13 09:35 09/13/13 16:27 1

0.0691 0.128 0.0774 0.983 Lead 214 pCi/g 08/23/13 09:35 09/13/13 16:27 1

0.228 1.53 0.924 12.0 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 16:27 1

0.932 0.238 0.236 U

0.278 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 16:27 1

0.0712 1.00 0.142 0.104 0.939 Radium 226 pCi/g 08/23/13 09:35 09/13/13 16:27 1

0.0951 0.117 0.0944 0.672 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 16:27 1

0.833 0.347 0.327 1.12 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 16:27 1

0.153 0.113 0.109 0.291 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 16:27 1

0.0654 0.0383 0.0383 U

-0.00487 Americium 241 pCi/g 08/23/13 09:35 09/13/13 16:27 1

4.53 2.60 2.60 U

1.28 Protactinium 234m Lab Sample ID: 160-3435-5 Client Sample ID: L050194TUB00 Matrix: Solid Date Collected: 08/19/13 14:25 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.872 (2+/-)

0.152 (2+/-)

1 09/13/13 17:06 08/23/13 09:35 pCi/g 0.104 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:06 1

0.320 0.365 0.346 1.11 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 17:06 1

0.0711 0.147 0.106 0.982 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 17:06 1

0.0753 0.124 0.0707 0.788 Lead 212 pCi/g 08/23/13 09:35 09/13/13 17:06 1

0.0697 0.143 0.0890 1.07 Lead 214 pCi/g 08/23/13 09:35 09/13/13 17:06 1

0.266 1.94 1.04 16.0 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 17:06 1

1.19 0.368 0.365 U

0.463 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 17:06 1

0.0711 1.00 0.147 0.106 0.982 Radium 226 TestAmerica St. Louis Page 13 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-5 Client Sample ID: L050194TUB00 Matrix: Solid Date Collected: 08/19/13 14:25 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 0.872 (2+/-)

0.152 (2+/-)

1 09/13/13 17:06 08/23/13 09:35 pCi/g 0.104 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:06 1

1.02 0.613 0.611 U

0.447 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 17:06 1

0.216 0.136 0.136 U

0.0708 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 17:06 1

0.108 0.0637 0.0637 U

-0.00259 Americium 241 pCi/g 08/23/13 09:35 09/13/13 17:06 1

4.65 2.84 2.83 U

2.27 Protactinium 234m Lab Sample ID: 160-3435-6 Client Sample ID: L050195TUB00 Matrix: Solid Date Collected: 08/19/13 14:35 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.678 (2+/-)

0.130 (2+/-)

1 09/13/13 17:07 08/23/13 09:35 pCi/g 0.114 RL MDC 0.111 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:07 1

0.559 0.354 0.352 U

0.385 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 17:07 1

0.0625 0.131 0.102 0.787 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 17:07 1

0.0629 0.0999 0.0651 0.586 Lead 212 pCi/g 08/23/13 09:35 09/13/13 17:07 1

0.0898 0.119 0.0836 0.810 Lead 214 pCi/g 08/23/13 09:35 09/13/13 17:07 1

0.493 1.53 1.09 10.5 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 17:07 1

0.979 0.242 0.241 U

0.147 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 17:07 1

0.0625 1.00 0.131 0.102 0.787 Radium 226 pCi/g 08/23/13 09:35 09/13/13 17:07 1

0.114 0.130 0.111 0.678 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 17:07 1

0.793 0.615 0.605 1.03 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 17:07 1

0.231 0.147 0.146 U

0.0837 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 17:07 1

0.101 0.0604 0.0603 U

0.0289 Americium 241 pCi/g 08/23/13 09:35 09/13/13 17:07 1

6.21 2.63 2.60 U

4.18 Protactinium 234m Lab Sample ID: 160-3435-7 Client Sample ID: L050196TUB00 Matrix: Solid Date Collected: 08/19/13 14:45 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.573 (2+/-)

0.104 (2+/-)

1 09/13/13 17:08 08/23/13 09:35 pCi/g 0.0942 RL MDC 0.0859 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:08 1

0.252 0.327 0.311 0.960 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 17:08 1

0.0564 0.119 0.0885 0.765 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 17:08 1

0.0479 0.0988 0.0557 0.630 Lead 212 pCi/g 08/23/13 09:35 09/13/13 17:08 1

0.0492 0.119 0.0773 0.876 Lead 214 pCi/g 08/23/13 09:35 09/13/13 17:08 1

0.212 1.73 0.963 14.0 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 17:08 1

0.854 0.229 0.227 U

0.270 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 17:08 1

0.0564 1.00 0.119 0.0885 0.765 Radium 226 pCi/g 08/23/13 09:35 09/13/13 17:08 1

0.0942 0.104 0.0859 0.573 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 17:08 1

0.834 0.259 0.254 U

0.487 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 17:08 1

0.156 0.101 0.101 U

0.0688 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 17:08 1

0.0771 0.0460 0.0460 U

0.0178 Americium 241 TestAmerica St. Louis Page 14 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-7 Client Sample ID: L050196TUB00 Matrix: Solid Date Collected: 08/19/13 14:45 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Protactinium 234m 2.03 U

(2+/-)

2.26 (2+/-)

1 09/13/13 17:08 08/23/13 09:35 pCi/g 3.74 RL MDC 2.26 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Lab Sample ID: 160-3435-8 Client Sample ID: L050197TUB00 Matrix: Solid Date Collected: 08/19/13 14:55 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.656 (2+/-)

0.126 (2+/-)

1 09/13/13 16:29 08/23/13 09:35 pCi/g 0.0803 RL MDC 0.109 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 16:29 1

0.480 0.301 0.299 U

0.305 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 16:29 1

0.0671 0.134 0.103 0.877 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 16:29 1

0.0594 0.0987 0.0657 0.685 Lead 212 pCi/g 08/23/13 09:35 09/13/13 16:29 1

0.0775 0.129 0.0914 0.945 Lead 214 pCi/g 08/23/13 09:35 09/13/13 16:29 1

0.361 1.69 1.07 13.5 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 16:29 1

1.08 0.401 0.400 U

0.309 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 16:29 1

0.0671 1.00 0.134 0.103 0.877 Radium 226 pCi/g 08/23/13 09:35 09/13/13 16:29 1

0.0803 0.126 0.109 0.656 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 16:29 1

0.812 0.673 0.662 1.22 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 16:29 1

0.249 0.153 0.153 U

0.0608 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 16:29 1

0.0979 0.0820 0.0820 U

-0.00606 Americium 241 pCi/g 08/23/13 09:35 09/13/13 16:29 1

4.76 2.77 2.77 U

1.34 Protactinium 234m Lab Sample ID: 160-3435-9 Client Sample ID: L050247PRS00 Matrix: Solid Date Collected: 08/16/13 15:40 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.185 (2+/-)

1 09/13/13 17:09 08/23/13 09:35 pCi/g 0.133 RL MDC 0.152 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:09 1

0.403 0.442 0.425 1.26 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 17:09 1

0.0827 0.167 0.125 1.15 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 17:09 1

0.0659 0.138 0.0798 1.04 Lead 212 pCi/g 08/23/13 09:35 09/13/13 17:09 1

0.0948 0.170 0.116 1.29 Lead 214 pCi/g 08/23/13 09:35 09/13/13 17:09 1

0.369 2.47 1.36 21.3 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 17:09 1

1.34 0.813 0.810 U

-0.626 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 17:09 1

0.0827 1.00 0.167 0.125 1.15 Radium 226 pCi/g 08/23/13 09:35 09/13/13 17:09 1

0.133 0.185 0.152 1.09 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 17:09 1

0.974 0.793 0.774 1.79 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 17:09 1

0.227 0.191 0.188 0.356 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 17:09 1

0.115 0.103 0.103 U

-0.00710 Americium 241 pCi/g 08/23/13 09:35 09/13/13 17:09 1

6.35 3.81 3.80 U

2.51 Protactinium 234m TestAmerica St. Louis Page 15 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-10 Client Sample ID: L050248PES00 Matrix: Solid Date Collected: 08/16/13 15:55 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.18 (2+/-)

0.173 (2+/-)

1 09/13/13 17:43 08/23/13 09:35 pCi/g 0.131 RL MDC 0.130 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:43 1

0.469 0.523 0.507 1.32 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 17:43 1

0.0810 0.172 0.123 1.23 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 17:43 1

0.0898 0.143 0.0853 1.07 Lead 212 pCi/g 08/23/13 09:35 09/13/13 17:43 1

0.0931 0.174 0.113 1.37 Lead 214 pCi/g 08/23/13 09:35 09/13/13 17:43 1

0.288 2.48 1.27 22.1 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 17:43 1

1.29 0.205 0.203 U

0.320 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 17:43 1

0.0810 1.00 0.172 0.123 1.23 Radium 226 pCi/g 08/23/13 09:35 09/13/13 17:43 1

0.131 0.173 0.130 1.18 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 17:43 1

1.10 0.399 0.392 U

0.745 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 17:43 1

0.293 0.171 0.170 U

0.143 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 17:43 1

0.111 0.0658 0.0658 U

-0.0114 Americium 241 pCi/g 08/23/13 09:35 09/13/13 17:43 1

5.48 3.16 3.15 U

2.51 Protactinium 234m Lab Sample ID: 160-3435-11 Client Sample ID: L050249PRS00 Matrix: Solid Date Collected: 08/16/13 14:15 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.07 (2+/-)

0.166 (2+/-)

1 09/13/13 17:44 08/23/13 09:35 pCi/g 0.132 RL MDC 0.130 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:44 1

0.574 0.414 0.406 0.846 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 17:44 1

0.0693 0.176 0.128 1.24 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 17:44 1

0.0632 0.139 0.0824 1.04 Lead 212 pCi/g 08/23/13 09:35 09/13/13 17:44 1

0.0897 0.177 0.126 1.28 Lead 214 pCi/g 08/23/13 09:35 09/13/13 17:44 1

0.322 2.44 1.44 20.3 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 17:44 1

1.44 0.270 0.268 U

0.342 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 17:44 1

0.0693 1.00 0.176 0.128 1.24 Radium 226 pCi/g 08/23/13 09:35 09/13/13 17:44 1

0.132 0.166 0.130 1.07 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 17:44 1

0.868 0.662 0.646 1.48 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 17:44 1

0.255 0.174 0.174 U

0.179 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 17:44 1

0.112 0.321 0.321 U

-0.00803 Americium 241 pCi/g 08/23/13 09:35 09/13/13 17:44 1

6.82 3.95 3.95 U

1.60 Protactinium 234m Lab Sample ID: 160-3435-12 Client Sample ID: L050250PES00 Matrix: Solid Date Collected: 08/16/13 14:25 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.32 (2+/-)

0.240 (2+/-)

1 09/13/13 17:45 08/23/13 09:35 pCi/g 0.155 RL MDC 0.198 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:45 1

0.448 0.538 0.515 1.49 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 17:45 1

0.101 0.196 0.150 1.20 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 17:45 1

0.0809 0.177 0.0936 1.16 Lead 212 TestAmerica St. Louis Page 16 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-12 Client Sample ID: L050250PES00 Matrix: Solid Date Collected: 08/16/13 14:25 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.32 (2+/-)

0.189 (2+/-)

1 09/13/13 17:45 08/23/13 09:35 pCi/g 0.0952 RL MDC 0.130 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:45 1

0.540 2.49 1.52 19.3 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 17:45 1

0.921 0.532 0.532 U

0.153 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 17:45 1

0.101 1.00 0.196 0.150 1.20 Radium 226 pCi/g 08/23/13 09:35 09/13/13 17:45 1

0.155 0.240 0.198 1.32 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 17:45 1

1.04 0.407 0.399 U

0.770 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 17:45 1

0.322 0.208 0.208 U

0.0397 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 17:45 1

0.128 0.0771 0.0770 U

0.0375 Americium 241 pCi/g 08/23/13 09:35 09/13/13 17:45 1

6.52 3.94 3.93 U

2.85 Protactinium 234m Lab Sample ID: 160-3435-13 Client Sample ID: L050251PRS00 Matrix: Solid Date Collected: 08/19/13 08:35 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.34 (2+/-)

0.194 (2+/-)

1 09/13/13 17:46 08/23/13 09:35 pCi/g 0.0896 RL MDC 0.145 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.500 0.532 0.514 1.40 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.103 0.207 0.149 1.49 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.0705 0.172 0.0909 1.36 Lead 212 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.0672 0.198 0.122 1.62 Lead 214 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.373 2.86 1.50 25.3 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 17:46 1

1.39 0.262 0.257 U

0.513 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.103 1.00 0.207 0.149 1.49 Radium 226 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.0896 0.194 0.145 1.34 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.856 0.329 0.318 U

0.831 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.280 0.142 0.140 U

0.231 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.110 0.0657 0.0657 U

0.0149 Americium 241 pCi/g 08/23/13 09:35 09/13/13 17:46 1

4.77 21.8 21.8 U

-0.583 Protactinium 234m Lab Sample ID: 160-3435-14 Client Sample ID: L050252PES00 Matrix: Solid Date Collected: 08/19/13 10:15 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.25 (2+/-)

0.206 (2+/-)

1 09/13/13 17:46 08/23/13 09:35 pCi/g 0.173 RL MDC 0.167 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.423 0.513 0.488 1.64 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.0965 0.204 0.145 1.47 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.0800 0.174 0.0940 1.36 Lead 212 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.105 0.204 0.129 1.63 Lead 214 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.459 3.00 1.56 26.6 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 17:46 1

1.52 0.333 0.327 U

0.638 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.0965 1.00 0.204 0.145 1.47 Radium 226 TestAmerica St. Louis Page 17 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-14 Client Sample ID: L050252PES00 Matrix: Solid Date Collected: 08/19/13 10:15 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 1.25 (2+/-)

0.206 (2+/-)

1 09/13/13 17:46 08/23/13 09:35 pCi/g 0.173 RL MDC 0.167 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:46 1

1.24 0.400 0.387 U

1.03 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.315 0.193 0.193 U

0.119 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 17:46 1

0.126 0.0741 0.0741 U

0.00973 Americium 241 pCi/g 08/23/13 09:35 09/13/13 17:46 1

7.11 3.64 3.64 U

0.814 Protactinium 234m Lab Sample ID: 160-3435-15 Client Sample ID: L050253PES00 Matrix: Solid Date Collected: 08/19/13 08:45 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.26 (2+/-)

0.242 (2+/-)

1 09/13/13 17:47 08/23/13 09:35 pCi/g 0.143 RL MDC 0.205 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 17:47 1

0.485 0.756 0.715 2.36 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 17:47 1

0.116 0.214 0.175 1.19 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 17:47 1

0.142 0.203 0.141 1.13 Lead 212 pCi/g 08/23/13 09:35 09/13/13 17:47 1

0.118 0.228 0.176 1.39 Lead 214 pCi/g 08/23/13 09:35 09/13/13 17:47 1

0.946 2.80 1.99 19.2 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 17:47 1

2.66 0.379 0.375 U

0.473 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 17:47 1

0.116 1.00 0.214 0.175 1.19 Radium 226 pCi/g 08/23/13 09:35 09/13/13 17:47 1

0.143 0.242 0.205 1.26 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 17:47 1

2.34 0.625 0.613 U

1.16 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 17:47 1

0.502 0.286 0.285 U

0.250 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 17:47 1

0.243 0.146 0.146 U

0.0867 Americium 241 pCi/g 08/23/13 09:35 09/13/13 17:47 1

14.4 3.85 3.85 U

1.93 Protactinium 234m Lab Sample ID: 160-3435-16 Client Sample ID: L050254PES00 Matrix: Solid Date Collected: 08/19/13 08:40 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.31 (2+/-)

0.197 (2+/-)

1 09/13/13 18:19 08/23/13 09:35 pCi/g 0.154 RL MDC 0.150 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.514 0.508 0.495 1.14 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.0963 0.183 0.138 1.24 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.0727 0.224 0.0921 1.35 Lead 212 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.0902 0.202 0.112 1.54 Lead 214 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.459 2.65 1.44 23.0 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 18:19 1

1.65 1.01 1.00 U

-0.784 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.0963 1.00 0.183 0.138 1.24 Radium 226 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.154 0.197 0.150 1.31 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 18:19 1

1.04 0.846 0.834 1.49 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.308 0.178 0.178 U

0.0853 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.119 0.0714 0.0713 U

-0.0301 Americium 241 TestAmerica St. Louis Page 18 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-16 Client Sample ID: L050254PES00 Matrix: Solid Date Collected: 08/19/13 08:40 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Protactinium 234m 5.97 U

(2+/-)

3.55 (2+/-)

1 09/13/13 18:19 08/23/13 09:35 pCi/g 7.12 RL MDC 3.51 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Lab Sample ID: 160-3435-17 Client Sample ID: L050255PES00 Matrix: Solid Date Collected: 08/16/13 13:50 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.20 (2+/-)

0.209 (2+/-)

1 09/13/13 18:19 08/23/13 09:35 pCi/g 0.136 RL MDC 0.174 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.484 0.532 0.513 1.45 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.0954 0.189 0.136 1.35 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.0988 0.156 0.0933 1.16 Lead 212 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.100 0.194 0.133 1.46 Lead 214 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.401 2.67 1.40 23.7 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 18:19 1

1.43 0.369 0.360 U

0.801 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.0954 1.00 0.189 0.136 1.35 Radium 226 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.136 0.209 0.174 1.20 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 18:19 1

1.01 0.823 0.811 1.40 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.312 0.165 0.165 U

0.0514 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 18:19 1

0.117 0.0694 0.0694 U

-0.0104 Americium 241 pCi/g 08/23/13 09:35 09/13/13 18:19 1

6.04 3.53 3.53 U

1.47 Protactinium 234m Lab Sample ID: 160-3435-18 Client Sample ID: L050256PRS00 Matrix: Solid Date Collected: 08/19/13 08:55 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.34 (2+/-)

0.204 (2+/-)

1 09/13/13 18:20 08/23/13 09:35 pCi/g 0.160 RL MDC 0.158 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 18:20 1

0.431 0.480 0.460 1.43 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 18:20 1

0.112 0.218 0.162 1.50 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 18:20 1

0.0779 0.160 0.0934 1.20 Lead 212 pCi/g 08/23/13 09:35 09/13/13 18:20 1

0.115 0.205 0.130 1.64 Lead 214 pCi/g 08/23/13 09:35 09/13/13 18:20 1

0.592 2.86 1.69 23.9 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 18:20 1

1.46 0.276 0.270 U

0.595 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 18:20 1

0.112 1.00 0.218 0.162 1.50 Radium 226 pCi/g 08/23/13 09:35 09/13/13 18:20 1

0.160 0.204 0.158 1.34 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 18:20 1

1.06 0.820 0.810 1.34 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 18:20 1

0.297 0.174 0.173 U

0.140 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 18:20 1

0.120 0.194 0.194 U

-0.0181 Americium 241 pCi/g 08/23/13 09:35 09/13/13 18:20 1

6.77 3.88 3.87 U

1.27 Protactinium 234m TestAmerica St. Louis Page 19 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-19 Client Sample ID: L050257PES00 Matrix: Solid Date Collected: 08/19/13 10:20 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.30 (2+/-)

0.225 (2+/-)

1 09/13/13 18:21 08/23/13 09:35 pCi/g 0.166 RL MDC 0.187 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 18:21 1

0.779 0.536 0.529 0.923 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 18:21 1

0.105 0.215 0.166 1.41 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 18:21 1

0.103 0.185 0.113 1.36 Lead 212 pCi/g 08/23/13 09:35 09/13/13 18:21 1

0.107 0.199 0.147 1.38 Lead 214 pCi/g 08/23/13 09:35 09/13/13 18:21 1

0.591 3.11 1.91 25.4 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 18:21 1

2.02 0.330 0.327 U

0.499 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 18:21 1

0.105 1.00 0.215 0.166 1.41 Radium 226 pCi/g 08/23/13 09:35 09/13/13 18:21 1

0.166 0.225 0.187 1.30 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 18:21 1

1.26 0.508 0.498 U

1.07 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 18:21 1

0.365 0.221 0.220 U

0.145 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 18:21 1

0.141 0.0832 0.0832 U

0.00862 Americium 241 pCi/g 08/23/13 09:35 09/13/13 18:21 1

8.95 4.97 4.97 U

-0.274 Protactinium 234m Lab Sample ID: 160-3435-20 Client Sample ID: L050258PES00 Matrix: Solid Date Collected: 08/16/13 13:40 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.32 (2+/-)

0.193 (2+/-)

1 09/13/13 18:22 08/23/13 09:35 pCi/g 0.106 RL MDC 0.144 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 09:35 09/13/13 18:22 1

0.428 0.491 0.470 1.45 Bismuth 212 pCi/g 08/23/13 09:35 09/13/13 18:22 1

0.0825 0.185 0.132 1.33 Bismuth 214 pCi/g 08/23/13 09:35 09/13/13 18:22 1

0.0675 0.176 0.0906 1.40 Lead 212 pCi/g 08/23/13 09:35 09/13/13 18:22 1

0.0892 0.190 0.114 1.58 Lead 214 pCi/g 08/23/13 09:35 09/13/13 18:22 1

0.455 2.78 1.49 24.4 Potassium 40 pCi/g 08/23/13 09:35 09/13/13 18:22 1

1.38 0.846 0.842 U

-0.801 Protactinium 231 pCi/g 08/23/13 09:35 09/13/13 18:22 1

0.0825 1.00 0.185 0.132 1.33 Radium 226 pCi/g 08/23/13 09:35 09/13/13 18:22 1

0.106 0.193 0.144 1.32 Thorium 232 pCi/g 08/23/13 09:35 09/13/13 18:22 1

1.00 0.784 0.771 1.49 Thorium 234 pCi/g 08/23/13 09:35 09/13/13 18:22 1

0.288 0.170 0.170 U

0.111 Uranium 235 pCi/g 08/23/13 09:35 09/13/13 18:22 1

0.119 0.0705 0.0705 U

0.00492 Americium 241 pCi/g 08/23/13 09:35 09/13/13 18:22 1

6.74 3.92 3.91 U

1.81 Protactinium 234m Lab Sample ID: 160-3435-21 Client Sample ID: L050259PRQ00 Matrix: Solid Date Collected: 08/19/13 15:20 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.08 (2+/-)

0.257 (2+/-)

1 09/13/13 11:05 08/23/13 11:49 pCi/g 0.312 RL MDC 0.232 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 11:05 1

1.75 1.09 1.09 U

0.999 Bismuth 212 pCi/g 08/23/13 11:49 09/13/13 11:05 1

0.149 0.294 0.251 1.46 Bismuth 214 pCi/g 08/23/13 11:49 09/13/13 11:05 1

0.153 0.230 0.171 1.19 Lead 212 TestAmerica St. Louis Page 20 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-21 Client Sample ID: L050259PRQ00 Matrix: Solid Date Collected: 08/19/13 15:20 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.49 (2+/-)

0.280 (2+/-)

1 09/13/13 11:05 08/23/13 11:49 pCi/g 0.154 RL MDC 0.233 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 11:05 1

1.01 3.00 2.46 16.9 Potassium 40 pCi/g 08/23/13 11:49 09/13/13 11:05 1

3.43 0.253 0.252 U

0.184 Protactinium 231 pCi/g 08/23/13 11:49 09/13/13 11:05 1

0.149 1.00 0.294 0.251 1.46 Radium 226 pCi/g 08/23/13 11:49 09/13/13 11:05 1

0.312 0.257 0.232 1.08 Thorium 232 pCi/g 08/23/13 11:49 09/13/13 11:05 1

3.08 0.662 0.657 U

0.736 Thorium 234 pCi/g 08/23/13 11:49 09/13/13 11:05 1

0.506 0.339 0.338 U

0.229 Uranium 235 pCi/g 08/23/13 11:49 09/13/13 11:05 1

0.316 28.7 28.7 U

-0.0378 Americium 241 pCi/g 08/23/13 11:49 09/13/13 11:05 1

19.2 10.5 10.5 U

-0.931 Protactinium 234m Lab Sample ID: 160-3435-22 Client Sample ID: L050259PRS00 Matrix: Solid Date Collected: 08/16/13 15:20 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.281 (2+/-)

1 09/13/13 11:06 08/23/13 11:49 pCi/g 0.298 RL MDC 0.258 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 11:06 1

0.608 0.730 0.705 1.83 Bismuth 212 pCi/g 08/23/13 11:49 09/13/13 11:06 1

0.171 0.263 0.226 1.29 Bismuth 214 pCi/g 08/23/13 11:49 09/13/13 11:06 1

0.130 0.207 0.142 1.16 Lead 212 pCi/g 08/23/13 11:49 09/13/13 11:06 1

0.160 0.222 0.167 1.40 Lead 214 pCi/g 08/23/13 11:49 09/13/13 11:06 1

1.04 2.92 2.12 19.6 Potassium 40 pCi/g 08/23/13 11:49 09/13/13 11:06 1

2.86 0.511 0.503 U

0.853 Protactinium 231 pCi/g 08/23/13 11:49 09/13/13 11:06 1

0.171 1.00 0.263 0.226 1.29 Radium 226 pCi/g 08/23/13 11:49 09/13/13 11:06 1

0.298 0.281 0.258 1.09 Thorium 232 pCi/g 08/23/13 11:49 09/13/13 11:06 1

2.28 0.602 0.593 U

0.996 Thorium 234 pCi/g 08/23/13 11:49 09/13/13 11:06 1

0.657 0.209 0.209 U

0.0677 Uranium 235 pCi/g 08/23/13 11:49 09/13/13 11:06 1

0.271 0.159 0.159 U

-0.0209 Americium 241 pCi/g 08/23/13 11:49 09/13/13 11:06 1

8.48 5.02 5.01 U

3.17 Protactinium 234m Lab Sample ID: 160-3435-23 Client Sample ID: L050260PES00 Matrix: Solid Date Collected: 08/16/13 15:30 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.26 (2+/-)

0.240 (2+/-)

1 09/13/13 12:48 08/23/13 11:49 pCi/g 0.150 RL MDC 0.207 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 12:48 1

0.542 0.580 0.564 1.41 Bismuth 212 pCi/g 08/23/13 11:49 09/13/13 12:48 1

0.113 0.219 0.159 1.55 Bismuth 214 pCi/g 08/23/13 11:49 09/13/13 12:48 1

0.0750 0.159 0.0864 1.24 Lead 212 pCi/g 08/23/13 11:49 09/13/13 12:48 1

0.0887 0.192 0.110 1.62 Lead 214 pCi/g 08/23/13 11:49 09/13/13 12:48 1

0.501 2.61 1.41 22.7 Potassium 40 pCi/g 08/23/13 11:49 09/13/13 12:48 1

1.48 0.305 0.297 U

0.704 Protactinium 231 pCi/g 08/23/13 11:49 09/13/13 12:48 1

0.113 1.00 0.219 0.159 1.55 Radium 226 TestAmerica St. Louis Page 21 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-23 Client Sample ID: L050260PES00 Matrix: Solid Date Collected: 08/16/13 15:30 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 1.26 (2+/-)

0.240 (2+/-)

1 09/13/13 12:48 08/23/13 11:49 pCi/g 0.150 RL MDC 0.207 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 12:48 1

0.957 0.743 0.732 1.31 Thorium 234 pCi/g 08/23/13 11:49 09/13/13 12:48 1

0.327 0.131 0.131 U

0.0193 Uranium 235 pCi/g 08/23/13 11:49 09/13/13 12:48 1

0.125 4.12 4.12 U

-0.0324 Americium 241 pCi/g 08/23/13 11:49 09/13/13 12:48 1

5.73 3.37 3.37 U

1.74 Protactinium 234m Lab Sample ID: 160-3435-24 Client Sample ID: L050261PRS00 Matrix: Solid Date Collected: 08/16/13 09:05 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.23 (2+/-)

0.192 (2+/-)

1 09/13/13 12:53 08/23/13 11:49 pCi/g 0.133 RL MDC 0.145 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 12:53 1

0.377 0.504 0.469 1.76 Bismuth 212 pCi/g 08/23/13 11:49 09/13/13 12:53 1

0.0777 0.181 0.120 1.30 Bismuth 214 pCi/g 08/23/13 11:49 09/13/13 12:53 1

0.0908 0.156 0.0838 1.02 Lead 212 pCi/g 08/23/13 11:49 09/13/13 12:53 1

0.0912 0.192 0.108 1.53 Lead 214 pCi/g 08/23/13 11:49 09/13/13 12:53 1

0.436 2.86 1.36 24.6 Potassium 40 pCi/g 08/23/13 11:49 09/13/13 12:53 1

1.32 0.226 0.222 U

0.400 Protactinium 231 pCi/g 08/23/13 11:49 09/13/13 12:53 1

0.0777 1.00 0.181 0.120 1.30 Radium 226 pCi/g 08/23/13 11:49 09/13/13 12:53 1

0.133 0.192 0.145 1.23 Thorium 232 pCi/g 08/23/13 11:49 09/13/13 12:53 1

1.02 0.846 0.833 1.39 Thorium 234 pCi/g 08/23/13 11:49 09/13/13 12:53 1

0.201 0.129 0.127 0.205 Uranium 235 pCi/g 08/23/13 11:49 09/13/13 12:53 1

0.117 0.0697 0.0697 U

0.00518 Americium 241 pCi/g 08/23/13 11:49 09/13/13 12:53 1

6.03 3.52 3.52 U

1.33 Protactinium 234m Lab Sample ID: 160-3435-25 Client Sample ID: L050262PES00 Matrix: Solid Date Collected: 08/19/13 10:30 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.37 (2+/-)

0.199 (2+/-)

1 09/13/13 13:40 08/23/13 11:49 pCi/g 0.102 RL MDC 0.149 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 13:40 1

0.638 0.461 0.449 1.08 Bismuth 212 pCi/g 08/23/13 11:49 09/13/13 13:40 1

0.0835 0.177 0.127 1.26 Bismuth 214 pCi/g 08/23/13 11:49 09/13/13 13:40 1

0.0796 0.162 0.0903 1.25 Lead 212 pCi/g 08/23/13 11:49 09/13/13 13:40 1

0.0899 0.187 0.127 1.41 Lead 214 pCi/g 08/23/13 11:49 09/13/13 13:40 1

0.544 2.84 1.53 24.7 Potassium 40 pCi/g 08/23/13 11:49 09/13/13 13:40 1

1.50 0.436 0.432 U

0.607 Protactinium 231 pCi/g 08/23/13 11:49 09/13/13 13:40 1

0.0835 1.00 0.177 0.127 1.26 Radium 226 pCi/g 08/23/13 11:49 09/13/13 13:40 1

0.102 0.199 0.149 1.37 Thorium 232 pCi/g 08/23/13 11:49 09/13/13 13:40 1

0.943 0.401 0.376 1.42 Thorium 234 pCi/g 08/23/13 11:49 09/13/13 13:40 1

0.215 0.175 0.174 U

0.190 Uranium 235 pCi/g 08/23/13 11:49 09/13/13 13:40 1

0.122 0.0801 0.0801 U

-0.00202 Americium 241 TestAmerica St. Louis Page 22 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-25 Client Sample ID: L050262PES00 Matrix: Solid Date Collected: 08/19/13 10:30 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Protactinium 234m

-0.0228 U

(2+/-)

3.73 (2+/-)

1 09/13/13 13:40 08/23/13 11:49 pCi/g 6.68 RL MDC 3.73 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Lab Sample ID: 160-3435-26 Client Sample ID: L050263PES00 Matrix: Solid Date Collected: 08/19/13 13:30 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.28 (2+/-)

0.227 (2+/-)

1 09/13/13 13:38 08/23/13 11:49 pCi/g 0.202 RL MDC 0.186 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 13:38 1

0.594 0.800 0.764 2.28 Bismuth 212 pCi/g 08/23/13 11:49 09/13/13 13:38 1

0.0898 0.204 0.150 1.32 Bismuth 214 pCi/g 08/23/13 11:49 09/13/13 13:38 1

0.0873 0.192 0.101 1.26 Lead 212 pCi/g 08/23/13 11:49 09/13/13 13:38 1

0.104 0.184 0.126 1.29 Lead 214 pCi/g 08/23/13 11:49 09/13/13 13:38 1

0.228 2.87 1.68 22.7 Potassium 40 pCi/g 08/23/13 11:49 09/13/13 13:38 1

1.20 0.554 0.534 1.34 Protactinium 231 pCi/g 08/23/13 11:49 09/13/13 13:38 1

0.0898 1.00 0.204 0.150 1.32 Radium 226 pCi/g 08/23/13 11:49 09/13/13 13:38 1

0.202 0.227 0.186 1.28 Thorium 232 pCi/g 08/23/13 11:49 09/13/13 13:38 1

0.930 0.394 0.378 1.05 Thorium 234 pCi/g 08/23/13 11:49 09/13/13 13:38 1

0.315 0.181 0.180 U

0.151 Uranium 235 pCi/g 08/23/13 11:49 09/13/13 13:38 1

0.136 0.0818 0.0817 U

-0.0392 Americium 241 pCi/g 08/23/13 11:49 09/13/13 13:38 1

7.46 4.19 4.19 U

0.896 Protactinium 234m Lab Sample ID: 160-3435-27 Client Sample ID: L050264PRS00 Matrix: Solid Date Collected: 08/16/13 14:50 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.34 (2+/-)

0.270 (2+/-)

1 09/13/13 11:07 08/23/13 11:49 pCi/g 0.187 RL MDC 0.233 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 11:07 1

1.23 0.738 0.736 U

0.510 Bismuth 212 pCi/g 08/23/13 11:49 09/13/13 11:07 1

0.195 0.272 0.234 1.34 Bismuth 214 pCi/g 08/23/13 11:49 09/13/13 11:07 1

0.171 0.224 0.165 1.17 Lead 212 pCi/g 08/23/13 11:49 09/13/13 11:07 1

0.209 0.289 0.242 1.52 Lead 214 pCi/g 08/23/13 11:49 09/13/13 11:07 1

1.03 3.01 2.28 19.2 Potassium 40 pCi/g 08/23/13 11:49 09/13/13 11:07 1

3.00 0.451 0.447 U

0.533 Protactinium 231 pCi/g 08/23/13 11:49 09/13/13 11:07 1

0.195 1.00 0.272 0.234 1.34 Radium 226 pCi/g 08/23/13 11:49 09/13/13 11:07 1

0.187 0.270 0.233 1.34 Thorium 232 pCi/g 08/23/13 11:49 09/13/13 11:07 1

2.62 1.87 1.86 U

1.48 Thorium 234 pCi/g 08/23/13 11:49 09/13/13 11:07 1

0.578 0.345 0.344 U

0.254 Uranium 235 pCi/g 08/23/13 11:49 09/13/13 11:07 1

0.290 0.172 0.172 U

-0.0630 Americium 241 pCi/g 08/23/13 11:49 09/13/13 11:07 1

16.2 48.1 48.1 U

-2.00 Protactinium 234m TestAmerica St. Louis Page 23 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-28 Client Sample ID: L050265PES00 Matrix: Solid Date Collected: 08/16/13 15:00 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.46 (2+/-)

0.259 (2+/-)

1 09/13/13 15:15 08/23/13 11:49 pCi/g 0.214 RL MDC 0.217 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 15:15 1

0.671 0.695 0.680 1.49 Bismuth 212 pCi/g 08/23/13 11:49 09/13/13 15:15 1

0.127 0.225 0.177 1.43 Bismuth 214 pCi/g 08/23/13 11:49 09/13/13 15:15 1

0.0974 0.183 0.111 1.35 Lead 212 pCi/g 08/23/13 11:49 09/13/13 15:15 1

0.129 0.218 0.155 1.59 Lead 214 pCi/g 08/23/13 11:49 09/13/13 15:15 1

0.590 2.91 1.84 23.4 Potassium 40 pCi/g 08/23/13 11:49 09/13/13 15:15 1

1.73 0.402 0.396 U

0.697 Protactinium 231 pCi/g 08/23/13 11:49 09/13/13 15:15 1

0.127 1.00 0.225 0.177 1.43 Radium 226 pCi/g 08/23/13 11:49 09/13/13 15:15 1

0.214 0.259 0.217 1.46 Thorium 232 pCi/g 08/23/13 11:49 09/13/13 15:15 1

1.21 0.995 0.978 1.85 Thorium 234 pCi/g 08/23/13 11:49 09/13/13 15:15 1

0.384 0.215 0.215 U

0.112 Uranium 235 pCi/g 08/23/13 11:49 09/13/13 15:15 1

0.145 0.0853 0.0853 U

0.00216 Americium 241 pCi/g 08/23/13 11:49 09/13/13 15:15 1

9.19 2.76 2.75 U

1.62 Protactinium 234m Lab Sample ID: 160-3435-29 Client Sample ID: L050266PUB00 Matrix: Solid Date Collected: 08/16/13 11:50 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.985 (2+/-)

0.194 (2+/-)

1 09/13/13 13:39 08/23/13 11:49 pCi/g 0.125 RL MDC 0.166 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 13:39 1

0.511 0.347 0.341 0.599 Bismuth 212 pCi/g 08/23/13 11:49 09/13/13 13:39 1

0.0801 0.166 0.116 1.15 Bismuth 214 pCi/g 08/23/13 11:49 09/13/13 13:39 1

0.0697 0.162 0.0786 1.09 Lead 212 pCi/g 08/23/13 11:49 09/13/13 13:39 1

0.0946 0.177 0.106 1.36 Lead 214 pCi/g 08/23/13 11:49 09/13/13 13:39 1

0.391 2.72 1.32 23.2 Potassium 40 pCi/g 08/23/13 11:49 09/13/13 13:39 1

1.14 0.299 0.295 U

0.435 Protactinium 231 pCi/g 08/23/13 11:49 09/13/13 13:39 1

0.0801 1.00 0.166 0.116 1.15 Radium 226 pCi/g 08/23/13 11:49 09/13/13 13:39 1

0.125 0.194 0.166 0.985 Thorium 232 pCi/g 08/23/13 11:49 09/13/13 13:39 1

0.888 0.372 0.360 0.903 Thorium 234 pCi/g 08/23/13 11:49 09/13/13 13:39 1

0.276 0.133 0.132 U

0.0606 Uranium 235 pCi/g 08/23/13 11:49 09/13/13 13:39 1

0.114 0.0685 0.0685 U

-0.0311 Americium 241 pCi/g 08/23/13 11:49 09/13/13 13:39 1

6.01 3.38 3.38 U

0.707 Protactinium 234m Lab Sample ID: 160-3435-30 Client Sample ID: L050267PUB00 Matrix: Solid Date Collected: 08/16/13 11:55 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.13 (2+/-)

0.206 (2+/-)

1 09/13/13 15:16 08/23/13 11:49 pCi/g 0.154 RL MDC 0.175 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 15:16 1

0.383 0.446 0.427 1.33 Bismuth 212 pCi/g 08/23/13 11:49 09/13/13 15:16 1

0.0796 0.192 0.130 1.45 Bismuth 214 pCi/g 08/23/13 11:49 09/13/13 15:16 1

0.0760 0.158 0.0866 1.23 Lead 212 TestAmerica St. Louis Page 24 of 29 1

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Client Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3435-30 Client Sample ID: L050267PUB00 Matrix: Solid Date Collected: 08/16/13 11:55 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.65 (2+/-)

0.209 (2+/-)

1 09/13/13 15:16 08/23/13 11:49 pCi/g 0.0923 RL MDC 0.135 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 15:16 1

0.555 2.92 1.52 25.8 Potassium 40 pCi/g 08/23/13 11:49 09/13/13 15:16 1

1.45 0.293 0.285 U

0.650 Protactinium 231 pCi/g 08/23/13 11:49 09/13/13 15:16 1

0.0796 1.00 0.192 0.130 1.45 Radium 226 pCi/g 08/23/13 11:49 09/13/13 15:16 1

0.154 0.206 0.175 1.13 Thorium 232 pCi/g 08/23/13 11:49 09/13/13 15:16 1

0.999 0.854 0.831 1.99 Thorium 234 pCi/g 08/23/13 11:49 09/13/13 15:16 1

0.292 0.141 0.140 U

0.157 Uranium 235 pCi/g 08/23/13 11:49 09/13/13 15:16 1

0.122 0.159 0.159 U

-0.0120 Americium 241 pCi/g 08/23/13 11:49 09/13/13 15:16 1

3.84 3.80 3.75 6.26 Protactinium 234m Lab Sample ID: 160-3435-31 Client Sample ID: L050268PUB00 Matrix: Solid Date Collected: 08/16/13 12:00 Date Received: 08/20/13 16:06 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.358 (2+/-)

0.0756 (2+/-)

1 09/13/13 13:42 08/23/13 11:49 pCi/g 0.0555 RL MDC 0.0662 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/23/13 11:49 09/13/13 13:42 1

0.356 0.221 0.220 U

0.196 Bismuth 212 pCi/g 08/23/13 11:49 09/13/13 13:42 1

0.0403 0.100 0.0769 0.619 Bismuth 214 pCi/g 08/23/13 11:49 09/13/13 13:42 1

0.0511 0.0558 0.0437 0.267 Lead 212 pCi/g 08/23/13 11:49 09/13/13 13:42 1

0.0572 0.0930 0.0679 0.612 Lead 214 pCi/g 08/23/13 11:49 09/13/13 13:42 1

0.242 0.821 0.639 5.03 Potassium 40 pCi/g 08/23/13 11:49 09/13/13 13:42 1

0.801 0.132 0.132 U

0.0893 Protactinium 231 pCi/g 08/23/13 11:49 09/13/13 13:42 1

0.0403 1.00 0.100 0.0769 0.619 Radium 226 pCi/g 08/23/13 11:49 09/13/13 13:42 1

0.0555 0.0756 0.0662 0.358 Thorium 232 pCi/g 08/23/13 11:49 09/13/13 13:42 1

0.668 0.535 0.529 0.745 Thorium 234 pCi/g 08/23/13 11:49 09/13/13 13:42 1

0.194 0.117 0.115 U

0.165 Uranium 235 pCi/g 08/23/13 11:49 09/13/13 13:42 1

0.0801 0.0384 0.0384 U

0.000 Americium 241 pCi/g 08/23/13 11:49 09/13/13 13:42 1

4.14 2.26 2.26 U

0.264 Protactinium 234m TestAmerica St. Louis Page 25 of 29 1

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QC Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-68357/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 72609 Prep Batch: 68357 Actinium 228 Analyte U

1 09/16/13 20:12 08/23/13 09:35 pCi/g 0.0581 MDC RL 0.0305 0.0305 (2+/-)

(2+/-)

MB 0.01044 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

09/16/13 20:12 08/23/13 09:35 pCi/g 0.168 0.0808 0.0808 U

-0.01322 Bismuth 212 1

09/16/13 20:12 08/23/13 09:35 pCi/g 0.0454 0.676 0.676 U

-0.01691 Bismuth 214 1

09/16/13 20:12 08/23/13 09:35 pCi/g 0.0267 0.0131 0.0131 U

0.002461 Lead 212 1

09/16/13 20:12 08/23/13 09:35 pCi/g 0.0425 0.0156 0.0156 U

0.005852 Lead 214 1

09/16/13 20:12 08/23/13 09:35 pCi/g 0.260 3.50 3.50 U

-0.08742 Potassium 40 1

09/16/13 20:12 08/23/13 09:35 pCi/g 0.316 0.175 0.175 U

0.06755 Protactinium 231 1

09/16/13 20:12 08/23/13 09:35 pCi/g 0.0454 1.00 0.676 0.676 U

-0.01691 Radium 226 1

09/16/13 20:12 08/23/13 09:35 pCi/g 0.0581 0.0305 0.0305 U

0.01044 Thorium 232 1

09/16/13 20:12 08/23/13 09:35 pCi/g 0.272 0.0976 0.0975 U

0.02297 Thorium 234 1

09/16/13 20:12 08/23/13 09:35 pCi/g 0.0805 0.0476 0.0475 U

0.02750 Uranium 235 1

09/16/13 20:12 08/23/13 09:35 pCi/g 0.0294 0.0171 0.0171 U

0.007593 Americium 241 1

09/16/13 20:12 08/23/13 09:35 pCi/g 1.43 0.549 0.549 U

0.0000 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-68357/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 72490 Prep Batch: 68357 Americium 241 Analyte 116 87 95 92.91 97.7 9.67 0.500 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 31.6 31.00 3.24 0.116 pCi/g 98 87 - 120 Cobalt 60 24.6 23.72 2.39 0.0692 pCi/g 96 87 - 115 Client Sample ID: L050190TUB00 Lab Sample ID: 160-3435-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 72492 Prep Batch: 68357 Actinium 228 Analyte 1

0.04 0.8873 0.874 0.205 0.143 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.57 0.9617 0.410 0.547 pCi/g 0.66 1

Bismuth 214 0.963 0.9340 0.155 0.0812 pCi/g 0.1 1

Lead 212 0.820 0.9323 0.143 0.0671 pCi/g 0.41 1

Lead 214 1.06 1.095 0.146 0.0804 pCi/g 0.14 1

Potassium 40 17.3 16.19 2.06 0.288 pCi/g 0.26 1

Protactinium 231 0.184 U

0.2798 U

0.271 1.07 pCi/g 0.22 1

Radium 226 0.963 0.9340 0.155 1.00 0.0812 pCi/g 0.1 1

Thorium 232 0.874 0.8873 0.205 0.143 pCi/g 0.04 1

Thorium 234 0.986 1.005 0.639 0.869 pCi/g 0.02 1

Uranium 235 0.0664 U

0.09492 U

0.0997 0.269 pCi/g 0.12 1

Americium 241 0.0736 U

-0.00851 3

U 1.07 0.103 pCi/g 0.07 1

Protactinium 234m 0.499 U

1.039 U

3.30 5.77 pCi/g 0.09 1

TestAmerica St. Louis Page 26 of 29 1

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QC Sample Results TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Method Blank Lab Sample ID: MB 160-68366/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 72483 Prep Batch: 68366 Actinium 228 Analyte U

1 09/13/13 12:44 08/23/13 11:49 pCi/g 0.0952 MDC RL 0.0225 0.0225 (2+/-)

(2+/-)

MB 0.0000 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

09/13/13 12:44 08/23/13 11:49 pCi/g 0.276 0.0352 0.0352 U

0.0000 Bismuth 212 1

09/13/13 12:44 08/23/13 11:49 pCi/g 0.0430 0.0221 0.0221 U

-0.0002383 Bismuth 214 1

09/13/13 12:44 08/23/13 11:49 pCi/g 0.0291 0.0634 0.0634 U

-0.005378 Lead 212 1

09/13/13 12:44 08/23/13 11:49 pCi/g 0.0357 0.0783 0.0783 U

-0.004825 Lead 214 1

09/13/13 12:44 08/23/13 11:49 pCi/g 0.174 0.0473 0.0473 U

0.0000 Potassium 40 1

09/13/13 12:44 08/23/13 11:49 pCi/g 0.453 0.240 0.240 U

-0.001682 Protactinium 231 1

09/13/13 12:44 08/23/13 11:49 pCi/g 0.0430 1.00 0.0221 0.0221 U

-0.0002383 Radium 226 1

09/13/13 12:44 08/23/13 11:49 pCi/g 0.0952 0.0225 0.0225 U

0.0000 Thorium 232 1

09/13/13 12:44 08/23/13 11:49 pCi/g 0.302 0.184 0.184 U

0.03965 Thorium 234 1

09/13/13 12:44 08/23/13 11:49 pCi/g 0.0605 0.0369 0.0368 U

0.02812 Uranium 235 1

09/13/13 12:44 08/23/13 11:49 pCi/g 0.0238 0.0134 0.0134 U

-0.004336 Americium 241 1

09/13/13 12:44 08/23/13 11:49 pCi/g 1.76 0.835 0.835 U

0.2159 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-68366/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 72490 Prep Batch: 68366 Americium 241 Analyte 116 87 96 94.07 97.7 9.79 0.480 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 31.6 31.01 3.24 0.135 pCi/g 98 87 - 120 Cobalt 60 24.6 23.50 2.37 0.0590 pCi/g 95 87 - 115 Client Sample ID: L050268PUB00 Lab Sample ID: 160-3435-31 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 72490 Prep Batch: 68366 Actinium 228 Analyte 1

0.06 0.3490 0.358 0.0698 0.0573 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 0.196 U

0.1733 U

0.160 0.250 pCi/g 0.06 1

Bismuth 214 0.619 0.5104 0.0855 0.0495 pCi/g 0.59 1

Lead 212 0.267 0.3105 0.0543 0.0361 pCi/g 0.39 1

Lead 214 0.612 0.5822 0.0813 0.0500 pCi/g 0.17 1

Potassium 40 5.03 5.101 0.740 0.234 pCi/g 0.04 1

Protactinium 231 0.0893 U

0.1458 U

0.144 0.560 pCi/g 0.20 1

Radium 226 0.619 0.5104 0.0855 1.00 0.0495 pCi/g 0.59 1

Thorium 232 0.358 0.3490 0.0698 0.0573 pCi/g 0.06 1

Thorium 234 0.745 0.7734 0.224 0.518 pCi/g 0.04 1

Uranium 235 0.165 U

0.1904 0.0880 0.123 pCi/g 0.12 1

Americium 241 0.000 U

0.01365 U

0.0370 0.0621 pCi/g 0.18 1

Protactinium 234m 0.264 U

2.015 U

1.59 3.22 pCi/g 0.45 1

TestAmerica St. Louis Page 27 of 29 1

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QC Association Summary TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Rad Leach Batch: 67776 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3435-1 L050190TUB00 Total/NA Solid Dry and Grind 160-3435-1 DU L050190TUB00 Total/NA Solid Dry and Grind 160-3435-2 L050191TUB00 Total/NA Solid Dry and Grind 160-3435-3 L050192TUB00 Total/NA Solid Dry and Grind 160-3435-4 L050193TUB00 Total/NA Solid Dry and Grind 160-3435-5 L050194TUB00 Total/NA Solid Dry and Grind 160-3435-6 L050195TUB00 Total/NA Solid Dry and Grind 160-3435-7 L050196TUB00 Total/NA Solid Dry and Grind 160-3435-8 L050197TUB00 Total/NA Solid Dry and Grind 160-3435-9 L050247PRS00 Total/NA Solid Dry and Grind 160-3435-10 L050248PES00 Total/NA Solid Dry and Grind 160-3435-11 L050249PRS00 Total/NA Solid Dry and Grind 160-3435-12 L050250PES00 Total/NA Solid Dry and Grind 160-3435-13 L050251PRS00 Total/NA Solid Dry and Grind 160-3435-14 L050252PES00 Total/NA Solid Dry and Grind 160-3435-15 L050253PES00 Total/NA Solid Dry and Grind 160-3435-16 L050254PES00 Total/NA Solid Dry and Grind 160-3435-17 L050255PES00 Total/NA Solid Dry and Grind 160-3435-18 L050256PRS00 Total/NA Solid Dry and Grind 160-3435-19 L050257PES00 Total/NA Solid Dry and Grind 160-3435-20 L050258PES00 Total/NA Solid Dry and Grind 160-3435-21 L050259PRQ00 Total/NA Solid Dry and Grind 160-3435-22 L050259PRS00 Total/NA Solid Dry and Grind 160-3435-23 L050260PES00 Total/NA Solid Dry and Grind 160-3435-24 L050261PRS00 Total/NA Solid Dry and Grind 160-3435-25 L050262PES00 Total/NA Solid Dry and Grind 160-3435-26 L050263PES00 Total/NA Solid Dry and Grind 160-3435-27 L050264PRS00 Total/NA Solid Dry and Grind 160-3435-28 L050265PES00 Total/NA Solid Dry and Grind 160-3435-29 L050266PUB00 Total/NA Solid Dry and Grind 160-3435-30 L050267PUB00 Total/NA Solid Dry and Grind 160-3435-31 L050268PUB00 Total/NA Solid Dry and Grind 160-3435-31 DU L050268PUB00 Total/NA Prep Batch: 68357 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 67776 160-3435-1 L050190TUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-1 DU L050190TUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-2 L050191TUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-3 L050192TUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-4 L050193TUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-5 L050194TUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-6 L050195TUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-7 L050196TUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-8 L050197TUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-9 L050247PRS00 Total/NA Solid Fill_Geo-21 67776 160-3435-10 L050248PES00 Total/NA Solid Fill_Geo-21 67776 160-3435-11 L050249PRS00 Total/NA Solid Fill_Geo-21 67776 160-3435-12 L050250PES00 Total/NA Solid Fill_Geo-21 67776 160-3435-13 L050251PRS00 Total/NA Solid Fill_Geo-21 67776 160-3435-14 L050252PES00 Total/NA TestAmerica St. Louis Page 28 of 29 1

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QC Association Summary TestAmerica Job ID: 160-3435-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Rad (Continued)

Prep Batch: 68357 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 67776 160-3435-15 L050253PES00 Total/NA Solid Fill_Geo-21 67776 160-3435-16 L050254PES00 Total/NA Solid Fill_Geo-21 67776 160-3435-17 L050255PES00 Total/NA Solid Fill_Geo-21 67776 160-3435-18 L050256PRS00 Total/NA Solid Fill_Geo-21 67776 160-3435-19 L050257PES00 Total/NA Solid Fill_Geo-21 67776 160-3435-20 L050258PES00 Total/NA Solid Fill_Geo-21 LCS 160-68357/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-68357/1-A Method Blank Total/NA Prep Batch: 68366 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 67776 160-3435-21 L050259PRQ00 Total/NA Solid Fill_Geo-21 67776 160-3435-22 L050259PRS00 Total/NA Solid Fill_Geo-21 67776 160-3435-23 L050260PES00 Total/NA Solid Fill_Geo-21 67776 160-3435-24 L050261PRS00 Total/NA Solid Fill_Geo-21 67776 160-3435-25 L050262PES00 Total/NA Solid Fill_Geo-21 67776 160-3435-26 L050263PES00 Total/NA Solid Fill_Geo-21 67776 160-3435-27 L050264PRS00 Total/NA Solid Fill_Geo-21 67776 160-3435-28 L050265PES00 Total/NA Solid Fill_Geo-21 67776 160-3435-29 L050266PUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-30 L050267PUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-31 L050268PUB00 Total/NA Solid Fill_Geo-21 67776 160-3435-31 DU L050268PUB00 Total/NA Solid Fill_Geo-21 LCS 160-68366/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-68366/1-A Method Blank Total/NA TestAmerica St. Louis Page 29 of 29 1

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