Text

Westinghouse Hematite Decommissioning Project - Final Status Survey Final Report Volume 3, Chapter 16, Survey Area Release Record for Land Survey Area 05, Survey Units 01, 02, 03 and 04, Revision 1, J3482-1 Uds Level 2 Report Final Report
	ML18019A702
Person / Time
Site:	07000036
Issue date:	08/30/2013
From:	Vania I; TestAmerica Labs - St. Louis, Westinghouse
To:	Swanson M; Office of Nuclear Material Safety and Safeguards, Westinghouse
Shared Package
ML18019A532	List: ML18019A541; ML18019A556; ML18019A584; ML18019A585; ML18019A611; ML18019A613; ML18019A628; ML18019A643; ML18019A645; ML18019A658; ML18019A660; ML18019A666; ML18019A669; ML18019A671; ML18019A673; ML18019A676; ML18019A677; ML18019A680; ML18019A682; ML18019A683; ML18019A685; ML18019A687; ML18019A689; ML18019A695; ML18019A696; ML18019A697; ML18019A702; ML18019A704; ML18019A705; ML18019A706; ML18019A707; ML18019A708; ML18019A709; ML18019A710; ML18019A711; ML18019A712; ML18019A713; ML18019A722; ML18019A723; ML18019A724; ML18019A725; ML18019A726; ML18019A728; ML18019A730; ML18019A733; ML18019A735; ML18019A736; ML18019A737; ML18019A738; ML18019A739; ... further results
References
	HEM-18-2 160-3482-1
	Download: ML18019A702 (50)
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3482-1 Client Project/Site: RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

8/30/2013 3:38:43 PM Ivan Vania, Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-3482-1 Page 2 of 50 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

6 Receipt Checklists.........................................

9 Definitions/Glossary.......................................

10 Method Summary.........................................

11 Sample Summary.........................................

12 Client Sample Results......................................

13 QC Sample Results........................................

38 QC Association Summary...................................

44 Tracer Carrier Summary....................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3482-1 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-3482-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)

Report Number: 160-3482-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 08/22/2013; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 3 coolers at receipt time were 20.0º C, 20.0º C and 20.0º C.

TECHNETIUM-99 (ICPMS)

Samples L050301PRS00 (160-3482-1), L050302PES00 (160-3482-2), L050303PRS00 (160-3482-3), L050304PEQ00 (160-3482-4),

L050304PES00 (160-3482-5), L050305PRS00 (160-3482-6), L050306PES00 (160-3482-7), L050307PRS00 (160-3482-8),

L050308PES00 (160-3482-9), L050309PRS00 (160-3482-10), L050310PES00 (160-3482-11), L050311PRS00 (160-3482-12),

L050312PES00 (160-3482-13), L050313PRS00 (160-3482-14), L050314PES00 (160-3482-15), L050315PRS00 (160-3482-16),

L050316PES00 (160-3482-17), L050317PRS00 (160-3482-18), L050318PES00 (160-3482-19), L050319PRS00 (160-3482-20),

L050320PES00 (160-3482-21), L050321PRS00 (160-3482-22), L050322PES00 (160-3482-23), L050323PUB00 (160-3482-24),

L050324PUB00 (160-3482-25), L050325PUB00 (160-3482-26), L050326PUB00 (160-3482-27), L050327PUB00 (160-3482-28),

L050328PUB00 (160-3482-29), L050329PUB00 (160-3482-30), L050330PUB00 (160-3482-31), L050331PUB00 (160-3482-32) and L050332PUB00 (160-3482-33) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 08/23/2013 and analyzed on 08/27/2013.

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3482-1 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-3482-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

No difficulties were encountered during the Tc-99 analysis. All quality control parameters were within the acceptance limits.

PERCENT SOLIDS Samples L050301PRS00 (160-3482-1), L050302PES00 (160-3482-2), L050303PRS00 (160-3482-3), L050304PEQ00 (160-3482-4),

L050304PES00 (160-3482-5), L050305PRS00 (160-3482-6), L050306PES00 (160-3482-7), L050307PRS00 (160-3482-8),

L050308PES00 (160-3482-9), L050309PRS00 (160-3482-10), L050310PES00 (160-3482-11), L050311PRS00 (160-3482-12),

L050312PES00 (160-3482-13), L050313PRS00 (160-3482-14), L050314PES00 (160-3482-15), L050315PRS00 (160-3482-16),

L050316PES00 (160-3482-17), L050317PRS00 (160-3482-18), L050318PES00 (160-3482-19), L050319PRS00 (160-3482-20),

L050320PES00 (160-3482-21), L050321PRS00 (160-3482-22), L050322PES00 (160-3482-23), L050323PUB00 (160-3482-24),

L050324PUB00 (160-3482-25), L050325PUB00 (160-3482-26), L050326PUB00 (160-3482-27), L050327PUB00 (160-3482-28),

L050328PUB00 (160-3482-29), L050329PUB00 (160-3482-30), L050330PUB00 (160-3482-31), L050331PUB00 (160-3482-32) and L050332PUB00 (160-3482-33) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 08/24/2013.

No difficulties were encountered during the % solids analysis. All quality control parameters were within the acceptance limits.

CESIUM-137 & OTHER GAMMA EMITTERS (GS)

Samples L050301PRS00 (160-3482-1), L050302PES00 (160-3482-2), L050303PRS00 (160-3482-3), L050304PEQ00 (160-3482-4),

L050304PES00 (160-3482-5), L050305PRS00 (160-3482-6), L050306PES00 (160-3482-7), L050307PRS00 (160-3482-8),

L050308PES00 (160-3482-9), L050309PRS00 (160-3482-10), L050310PES00 (160-3482-11), L050311PRS00 (160-3482-12),

L050312PES00 (160-3482-13), L050313PRS00 (160-3482-14), L050314PES00 (160-3482-15), L050315PRS00 (160-3482-16),

L050316PES00 (160-3482-17), L050317PRS00 (160-3482-18), L050318PES00 (160-3482-19), L050319PRS00 (160-3482-20),

L050320PES00 (160-3482-21), L050321PRS00 (160-3482-22), L050322PES00 (160-3482-23), L050323PUB00 (160-3482-24),

L050324PUB00 (160-3482-25), L050325PUB00 (160-3482-26), L050326PUB00 (160-3482-27), L050327PUB00 (160-3482-28),

L050328PUB00 (160-3482-29), L050329PUB00 (160-3482-30), L050330PUB00 (160-3482-31), L050331PUB00 (160-3482-32) and L050332PUB00 (160-3482-33) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 08/23/2013, prepared on 08/28/2013 and analyzed on 08/28/2013 and 08/29/2013.

Preparation Batch 69096:

Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of Bismuth-214.

Because the samples have not had a 21-day ingrowth, the activity for Radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between Radium-226 and Bismuth-214 by the loss of Radon-222 during sample preparation. (160-3482-19 DU), (LCS 160-69096/2-A), (MB 160-69096/1-A), L050301PRS00 (160-3482-1), L050302PES00 (160-3482-2), L050303PRS00 (160-3482-3), L050304PEQ00 (160-3482-4), L050304PES00 (160-3482-5), L050305PRS00 (160-3482-6),

L050306PES00 (160-3482-7), L050307PRS00 (160-3482-8), L050308PES00 (160-3482-9), L050309PRS00 (160-3482-10),

L050310PES00 (160-3482-11), L050311PRS00 (160-3482-12), L050312PES00 (160-3482-13), L050313PRS00 (160-3482-14),

L050314PES00 (160-3482-15), L050315PRS00 (160-3482-16), L050316PES00 (160-3482-17), L050317PRS00 (160-3482-18),

L050318PES00 (160-3482-19), L050319PRS00 (160-3482-20)

The reporting limit for thorium-234 was not met due to insufficient sample weight available for analysis. Analytical results are reported with the MDC achieved. L050302PES00 (160-3482-2), L050308PES00 (160-3482-9), L050310PES00 (160-3482-11), L050314PES00 (160-3482-15)

Preparation Batch 69129:

The detection goal for thorium-234 analyzed by gamma spectroscopy was not met for the following samples due to insufficient sample weight available for analysis: 160-3482-A-21-F, 160-3482-A-28-D, 160-3482-A-29-D, 160-3482-A-30-D, 160-3482-A-31-D, 160-3482-A-32-D, 160-3482-A-32-E DU. Analytical results are reported with the detection limit achieved.

In addition, sample 160-3482-A-27-D did not meet the detection goal for thorium-234 due to the activity of other isotopes in the sample.

Analytical results are reported with the detection limit achieved.

Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of Bismuth-214.

Because the samples have not had a 21-day ingrowth, the activity for Radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between Radium-226 and Bismuth-214 by the loss of Radon-222 during sample TestAmerica St. Louis Page 4 of 50 1

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3482-1 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-3482-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued) preparation. (160-3482-32 DU), (LCS 160-69129/2-A), (MB 160-69129/1-A), L050320PES00 (160-3482-21), L050321PRS00 (160-3482-22), L050322PES00 (160-3482-23), L050323PUB00 (160-3482-24), L050324PUB00 (160-3482-25), L050325PUB00 (160-3482-26), L050326PUB00 (160-3482-27), L050327PUB00 (160-3482-28), L050328PUB00 (160-3482-29), L050329PUB00 (160-3482-30), L050330PUB00 (160-3482-31), L050331PUB00 (160-3482-32), L050332PUB00 (160-3482-33)

No other difficulties were encountered during the Gamma spec analysis. All other quality control parameters were within the acceptance limits.

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!Procedure HDP-PR-QA-006, Chain of Custody Page 1 ofl Hematite Decommissioning Project IRevisio,n: 3 I

I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the co,ntainer is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutody ID No. I F-082213-01 Page 1/3 Laboratory Name:

Project Name:

Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number:

314-810-3382 Sampler Name Scott Jenkins Sample ID L05030IPRSOO L050302PESOO L050303PRSOO L050304PEQOO L050304PESOO L050305PRSOO L050306PESOO L050307PRSOO L050308PESOO L050309PRSOO L0503 IOPESOO L050311PRSOO Received bv:

Company Name:

Relinquished by:

Company Name:

Date Time 8/20/2013 15:24 8/20/2013 15:30 8/20/2013 15:44 8/20/2013 15:52 8/20/2013 15:52 8/20/2013 17:20 8/20/2013 17:30 8/20/2013 16:08 8/20/2013 16:13 8/21/2013 9:07 8/21/2013 9:19 8/21/2013 9:42 l Date/Time g-*cz-t3 I

I Date/Time Matrix s

s s

Date/Time i:'.l TA-MO Laboratory Address:

13715 Rider Trail North

~* 1--------------------l

-~ PhoneNo.

8 314-298-8566

'E Laboratory Contact Person:

~ Joe Walker 1

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1 Phone No.

108-870-8453 Rush Turn Around Time (7 days)

Remarks l.51'\\ o 5-o3 Sv\\5

...v-Cooler Temperature:

Cooler ID: I Shipper and Number:

-Ol/1 Q21-o_~

Comments: Please re-analyze samples after 21-day ingrowth period.

I,,,..

I.g,1,-i,.

I Verified By:

,i*.10

~

CS) 01

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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Page 1 ofl Hematite Decommissioning Project !Revision: 3 I

I Westinghouse Non"Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutody ID No. I F-082213-01 Page 2/3 Project Name:

Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number:

314-81Q-_3382 Sampler Name Scott Jenkins Sample ID L050312PESOO L050313PRSOO L050314PES00 L0503 l 5PRSOO L050316PESOO L0503 l 7PRS00 L050318PES00 L0503l9PRS00 L050320PESOO L050321PRSOO L050322PES00 L050323PUBOO Company Name:

Received by:

Company Name:

Relinquished by:

Company Name:

Date Time 8/21/2013 10:47 8/21/2013 11:21 8/21/2013 11:38 8/21/2013 13:40 8/21/2013 13:55 8/21/2013 15:15 8/21/2013 15:21 8/21/2013 16:42 8/21/2013 16:50 8/21/2013 16:19 8/21/2013 16:24 8/19/2013 16:35 Date/Time

~--zz-J:J 1,1.,,V Date/Time Date/Time Matrix s

s s

Laboratory Name:

TA-MO Laboratory Address:

13715 Rider Trail North

~--------------------!

§ Phone No.

8 314-298-8566 5 Laboratory Contact Person:

~ Joe Walker 1

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1 Phone No.

708-870-8453

'furn_Around Time Rush (7 days)

Remarks t--s?} o 5-o~ 5*

J

!--5A oS'-o'"55~S i..SA o5-o3 ©v..,s Cooler Temperature:

Date/Time r\\l Comments: Please re-analyze samples after 21-day ingrowth

'1/'1,. 4 'period.

"' r e_"t tD i*"t"l i~~*

Verified By:

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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 3 I

Page 1 ofll Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAJN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutody ID No. I F-082213-01 Page 3/3 Project Name:

Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number:

314-810-3_382 Sampler Name Scott Jenkins Sample ID L050324PUBOO L050325PUBOO L050326PUBOO L050327PUBOO L050328PUBOO L050329PUBOO L050330PUBOO L050331PUBOO L050332PUBOO Relinquished by*

Company Name:

Received by:

Company Name:

Relinquished by:

Company Name:

Date Time 8/19/2013 16:45 8/19/2013 16:55 8/20/2013 14:55 8/21/2013 9:15 8/21/2013 9:45 8/21/2013 10:50 8/21/2013 11:10 8/21/2013 11:20 8/21/2013 13:40 t? Date/Time o--Z.2-13 7w Date/Time Date/Time Matrix s

s s

Laboratory Name:

TA-MO Laboratory Address:

13715 Rider Trail North

~-------------------!

-~ PhoneNo.

8 314-298-8566

~ Laboratory Contact Person:

'"" Joe Walker Phone No.

708-87_0-8453 Turn Around Time Rush (7 days)

Remarks 1

t,SA-oS-o3 ~a..s 1

1 1

Cooler Temperature:

Cooler ID:. Shipqer and Number:

2-o't/oS 1Df:J Date/Time I Co=ents: Please re-analyze samples after 21-day ingrowth

,;l,L'/_ ~

7 period.

It%

,g V Verified By:

Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3482-1 Login Number: 3482 Question Answer Comment Creator: Daniels, Brian J List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

False Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Qualifiers Rad Qualifier Description U

Indicates the analyte was analyzed for but not detected.

Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 11 of 50 1

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Sample Summary TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-3482-1 L050301PRS00 Solid 08/20/13 15:24 08/22/13 16:45 160-3482-2 L050302PES00 Solid 08/20/13 15:30 08/22/13 16:45 160-3482-3 L050303PRS00 Solid 08/20/13 15:44 08/22/13 16:45 160-3482-4 L050304PEQ00 Solid 08/20/13 15:52 08/22/13 16:45 160-3482-5 L050304PES00 Solid 08/20/13 15:52 08/22/13 16:45 160-3482-6 L050305PRS00 Solid 08/20/13 17:20 08/22/13 16:45 160-3482-7 L050306PES00 Solid 08/20/13 17:30 08/22/13 16:45 160-3482-8 L050307PRS00 Solid 08/20/13 16:08 08/22/13 16:45 160-3482-9 L050308PES00 Solid 08/20/13 16:13 08/22/13 16:45 160-3482-10 L050309PRS00 Solid 08/20/13 09:07 08/22/13 16:45 160-3482-11 L050310PES00 Solid 08/21/13 09:19 08/22/13 16:45 160-3482-12 L050311PRS00 Solid 08/21/13 09:42 08/22/13 16:45 160-3482-13 L050312PES00 Solid 08/21/13 10:47 08/22/13 16:45 160-3482-14 L050313PRS00 Solid 08/21/13 11:21 08/22/13 16:45 160-3482-15 L050314PES00 Solid 08/21/13 11:38 08/22/13 16:45 160-3482-16 L050315PRS00 Solid 08/21/13 13:40 08/22/13 16:45 160-3482-17 L050316PES00 Solid 08/21/13 13:55 08/22/13 16:45 160-3482-18 L050317PRS00 Solid 08/21/13 15:15 08/22/13 16:45 160-3482-19 L050318PES00 Solid 08/21/13 15:21 08/22/13 16:45 160-3482-20 L050319PRS00 Solid 08/21/13 16:42 08/22/13 16:45 160-3482-21 L050320PES00 Solid 08/21/13 16:50 08/22/13 16:45 160-3482-22 L050321PRS00 Solid 08/21/13 16:19 08/22/13 16:45 160-3482-23 L050322PES00 Solid 08/21/13 16:24 08/22/13 16:45 160-3482-24 L050323PUB00 Solid 08/19/13 16:35 08/22/13 16:45 160-3482-25 L050324PUB00 Solid 08/19/13 16:45 08/22/13 16:45 160-3482-26 L050325PUB00 Solid 08/19/13 16:55 08/22/13 16:45 160-3482-27 L050326PUB00 Solid 08/20/13 14:55 08/22/13 16:45 160-3482-28 L050327PUB00 Solid 08/21/13 09:15 08/22/13 16:45 160-3482-29 L050328PUB00 Solid 08/21/13 09:45 08/22/13 16:45 160-3482-30 L050329PUB00 Solid 08/21/13 10:50 08/22/13 16:45 160-3482-31 L050330PUB00 Solid 08/21/13 11:10 08/22/13 16:45 160-3482-32 L050331PUB00 Solid 08/21/13 11:20 08/22/13 16:45 160-3482-33 L050332PUB00 Solid 08/21/13 13:40 08/22/13 16:45 TestAmerica St. Louis Page 12 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-1 Client Sample ID: L050301PRS00 Matrix: Solid Date Collected: 08/20/13 15:24 Percent Solids: 83.2 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00070 0.000021 mg/Kg

08/23/13 14:01 08/27/13 15:30 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0398 U

(2+/-)

0.0238 (2+/-)

1 08/27/13 15:30 08/23/13 14:01 pCi/g 0.240 1.40 RL MDC

-0.0201 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 15:30 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 86 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.23 (2+/-)

0.183 (2+/-)

1 08/28/13 22:44 08/28/13 10:52 pCi/g 0.163 RL MDC 0.140 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 22:44 1

0.118 1.44 1.44 U

-0.0360 Americium 241 pCi/g 08/28/13 10:52 08/28/13 22:44 1

0.427 0.455 0.437 1.30 Bismuth 212 pCi/g 08/28/13 10:52 08/28/13 22:44 1

0.0756 0.136 0.108 0.859 Bismuth 214 pCi/g 08/28/13 10:52 08/28/13 22:44 1

0.0679 0.149 0.0828 1.15 Lead 212 pCi/g 08/28/13 10:52 08/28/13 22:44 1

0.0799 0.136 0.100 0.940 Lead 214 pCi/g 08/28/13 10:52 08/28/13 22:44 1

0.152 2.58 1.37 22.6 Potassium 40 pCi/g 08/28/13 10:52 08/28/13 22:44 1

1.32 0.304 0.299 U

0.515 Protactinium 231 pCi/g 08/28/13 10:52 08/28/13 22:44 1

0.0756 1.00 0.136 0.108 0.859 Radium 226 pCi/g 08/28/13 10:52 08/28/13 22:44 1

0.875 1.00 0.357 0.342 1.02 Thorium 234 pCi/g 08/28/13 10:52 08/28/13 22:44 1

0.275 0.163 0.163 U

0.0619 Uranium 235 pCi/g 08/28/13 10:52 08/28/13 22:44 1

7.07 1.30 1.30 U

0.000 Protactinium 234m pCi/g 08/28/13 10:52 08/28/13 22:44 1

0.163 0.183 0.140 1.23 Thorium 232 Tl-208 0.364 0.0504 0.0616 0.0371 pCi/g 08/28/13 10:52 08/28/13 22:44 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-2 Client Sample ID: L050302PES00 Matrix: Solid Date Collected: 08/20/13 15:30 Percent Solids: 81.6 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00070 0.000021 mg/Kg

08/23/13 14:01 08/27/13 15:42 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0483 U

(2+/-)

0.0209 (2+/-)

1 08/27/13 15:42 08/23/13 14:01 pCi/g 0.240 1.40 RL MDC

-0.0176 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 15:42 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 TestAmerica St. Louis Page 13 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-2 Client Sample ID: L050302PES00 Matrix: Solid Date Collected: 08/20/13 15:30 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.11 (2+/-)

0.217 (2+/-)

1 08/28/13 23:16 08/28/13 10:52 pCi/g 0.121 RL MDC 0.186 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:16 1

0.118 0.0704 0.0704 U

0.0282 Americium 241 pCi/g 08/28/13 10:52 08/28/13 23:16 1

0.677 0.472 0.463 0.874 Bismuth 212 pCi/g 08/28/13 10:52 08/28/13 23:16 1

0.0713 0.151 0.117 0.922 Bismuth 214 pCi/g 08/28/13 10:52 08/28/13 23:16 1

0.0825 0.172 0.0924 1.13 Lead 212 pCi/g 08/28/13 10:52 08/28/13 23:16 1

0.0979 0.160 0.126 0.953 Lead 214 pCi/g 08/28/13 10:52 08/28/13 23:16 1

0.357 2.43 1.47 18.9 Potassium 40 pCi/g 08/28/13 10:52 08/28/13 23:16 1

1.26 0.233 0.231 U

0.257 Protactinium 231 pCi/g 08/28/13 10:52 08/28/13 23:16 1

0.0713 1.00 0.151 0.117 0.922 Radium 226 pCi/g 08/28/13 10:52 08/28/13 23:16 1

1.05 1.00 0.886 0.869 1.64 Thorium 234 pCi/g 08/28/13 10:52 08/28/13 23:16 1

0.242 0.153 0.152 U

0.187 Uranium 235 pCi/g 08/28/13 10:52 08/28/13 23:16 1

7.15 4.42 4.42 U

0.696 Protactinium 234m pCi/g 08/28/13 10:52 08/28/13 23:16 1

0.121 0.217 0.186 1.11 Thorium 232 Tl-208 0.344 0.0561 0.0664 0.0444 pCi/g 08/28/13 10:52 08/28/13 23:16 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-3 Client Sample ID: L050303PRS00 Matrix: Solid Date Collected: 08/20/13 15:44 Percent Solids: 83.8 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00067 0.000020 mg/Kg

08/23/13 14:01 08/27/13 15:46 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0638 U

(2+/-)

0.0719 (2+/-)

1 08/27/13 15:46 08/23/13 14:01 pCi/g 0.231 1.35 RL MDC

-0.0628 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 15:46 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 88 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.03 (2+/-)

0.176 (2+/-)

1 08/28/13 23:18 08/28/13 10:52 pCi/g 0.110 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.0906 0.0543 0.0543 U

0.0255 Americium 241 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.314 0.333 0.308 1.22 Bismuth 212 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.0636 0.123 0.0917 0.789 Bismuth 214 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.0590 0.166 0.0759 1.14 Lead 212 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.0754 0.134 0.0975 0.879 Lead 214 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.251 2.45 1.22 20.8 Potassium 40 pCi/g 08/28/13 10:52 08/28/13 23:18 1

1.14 0.344 0.339 U

0.513 Protactinium 231 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.0636 1.00 0.123 0.0917 0.789 Radium 226 TestAmerica St. Louis Page 14 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-3 Client Sample ID: L050303PRS00 Matrix: Solid Date Collected: 08/20/13 15:44 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.60 (2+/-)

0.693 (2+/-)

1 08/28/13 23:18 08/28/13 10:52 pCi/g 0.865 1.00 RL MDC 0.672 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.228 0.140 0.140 U

0.0973 Uranium 235 pCi/g 08/28/13 10:52 08/28/13 23:18 1

4.72 2.34 2.30 U

4.19 Protactinium 234m pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.110 0.176 0.141 1.03 Thorium 232 Tl-208 0.370 0.0502 0.0632 0.0370 pCi/g 08/28/13 10:52 08/28/13 23:18 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-4 Client Sample ID: L050304PEQ00 Matrix: Solid Date Collected: 08/20/13 15:52 Percent Solids: 82.0 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00071 0.000021 mg/Kg

08/23/13 14:01 08/27/13 15:49 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0875 U

(2+/-)

0.0119 (2+/-)

1 08/27/13 15:49 08/23/13 14:01 pCi/g 0.245 1.43 RL MDC

-0.00602 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 15:49 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 85 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.29 (2+/-)

0.199 (2+/-)

1 08/28/13 23:18 08/28/13 10:52 pCi/g 0.127 RL MDC 0.155 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.114 0.667 0.667 U

-0.0293 Americium 241 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.221 0.387 0.353 1.61 Bismuth 212 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.0712 0.136 0.106 0.875 Bismuth 214 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.0730 0.154 0.0849 1.19 Lead 212 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.0794 0.133 0.101 0.891 Lead 214 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.572 2.75 1.53 23.6 Potassium 40 pCi/g 08/28/13 10:52 08/28/13 23:18 1

1.24 0.392 0.382 U

0.891 Protactinium 231 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.0712 1.00 0.136 0.106 0.875 Radium 226 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.927 1.00 0.381 0.367 1.04 Thorium 234 pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.270 0.165 0.164 U

0.112 Uranium 235 pCi/g 08/28/13 10:52 08/28/13 23:18 1

5.67 3.37 3.36 U

1.97 Protactinium 234m pCi/g 08/28/13 10:52 08/28/13 23:18 1

0.127 0.199 0.155 1.29 Thorium 232 Tl-208 0.344 0.0542 0.0637 0.0425 pCi/g 08/28/13 10:52 08/28/13 23:18 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 15 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-5 Client Sample ID: L050304PES00 Matrix: Solid Date Collected: 08/20/13 15:52 Percent Solids: 81.8 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00076 0.000023 mg/Kg

08/23/13 14:01 08/27/13 15:53 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0618 U

(2+/-)

0.0895 (2+/-)

1 08/27/13 15:53 08/23/13 14:01 pCi/g 0.260 1.52 RL MDC

-0.0725 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 15:53 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 81 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.16 (2+/-)

0.174 (2+/-)

1 08/28/13 23:52 08/28/13 10:52 pCi/g 0.112 RL MDC 0.133 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.107 0.0637 0.0636 U

0.0141 Americium 241 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.421 0.477 0.454 1.51 Bismuth 212 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.0778 0.133 0.106 0.828 Bismuth 214 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.0658 0.191 0.0825 1.14 Lead 212 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.0888 0.140 0.0906 0.974 Lead 214 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.365 2.60 1.38 22.9 Potassium 40 pCi/g 08/28/13 10:52 08/28/13 23:52 1

1.27 0.316 0.305 U

0.677 Protactinium 231 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.0778 1.00 0.133 0.106 0.828 Radium 226 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.897 1.00 0.728 0.712 1.55 Thorium 234 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.262 0.139 0.138 U

0.172 Uranium 235 pCi/g 08/28/13 10:52 08/28/13 23:52 1

5.44 3.75 3.74 U

3.07 Protactinium 234m pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.112 0.174 0.133 1.16 Thorium 232 Tl-208 0.405 0.0523 0.0655 0.0358 pCi/g 08/28/13 10:52 08/28/13 23:52 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-6 Client Sample ID: L050305PRS00 Matrix: Solid Date Collected: 08/20/13 17:20 Percent Solids: 82.8 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00070 0.000021 mg/Kg

08/23/13 14:01 08/27/13 15:57 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0360 U

(2+/-)

0.0641 (2+/-)

1 08/27/13 15:57 08/23/13 14:01 pCi/g 0.240 1.40 RL MDC

-0.0548 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 15:57 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 86 TestAmerica St. Louis Page 16 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-6 Client Sample ID: L050305PRS00 Matrix: Solid Date Collected: 08/20/13 17:20 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.17 (2+/-)

0.176 (2+/-)

1 08/28/13 23:49 08/28/13 10:52 pCi/g 0.108 RL MDC 0.135 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:49 1

0.104 0.0618 0.0618 U

0.00112 Americium 241 pCi/g 08/28/13 10:52 08/28/13 23:49 1

0.357 0.468 0.442 1.60 Bismuth 212 pCi/g 08/28/13 10:52 08/28/13 23:49 1

0.0756 0.132 0.102 0.856 Bismuth 214 pCi/g 08/28/13 10:52 08/28/13 23:49 1

0.0922 0.134 0.0842 0.969 Lead 212 pCi/g 08/28/13 10:52 08/28/13 23:49 1

0.0718 0.134 0.0975 0.944 Lead 214 pCi/g 08/28/13 10:52 08/28/13 23:49 1

0.346 2.48 1.30 21.9 Potassium 40 pCi/g 08/28/13 10:52 08/28/13 23:49 1

1.21 0.204 0.202 U

0.287 Protactinium 231 pCi/g 08/28/13 10:52 08/28/13 23:49 1

0.0756 1.00 0.132 0.102 0.856 Radium 226 pCi/g 08/28/13 10:52 08/28/13 23:49 1

0.914 1.00 0.769 0.756 1.44 Thorium 234 pCi/g 08/28/13 10:52 08/28/13 23:49 1

0.242 0.140 0.139 U

0.145 Uranium 235 pCi/g 08/28/13 10:52 08/28/13 23:49 1

5.06 2.91 2.91 U

0.946 Protactinium 234m pCi/g 08/28/13 10:52 08/28/13 23:49 1

0.108 0.176 0.135 1.17 Thorium 232 Tl-208 0.368 0.0541 0.0649 0.0431 pCi/g 08/28/13 10:52 08/28/13 23:49 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-7 Client Sample ID: L050306PES00 Matrix: Solid Date Collected: 08/20/13 17:30 Percent Solids: 81.2 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00071 0.000021 mg/Kg

08/23/13 14:01 08/27/13 16:09 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.139 U

(2+/-)

0.0678 (2+/-)

1 08/27/13 16:09 08/23/13 14:01 pCi/g 0.242 1.41 RL MDC 0.0574 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:09 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.29 (2+/-)

0.271 (2+/-)

1 08/28/13 23:54 08/28/13 10:52 pCi/g 0.135 RL MDC 0.236 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:54 1

0.129 0.0765 0.0765 U

-0.00159 Americium 241 pCi/g 08/28/13 10:52 08/28/13 23:54 1

0.440 0.563 0.539 1.56 Bismuth 212 pCi/g 08/28/13 10:52 08/28/13 23:54 1

0.0796 0.153 0.124 0.852 Bismuth 214 pCi/g 08/28/13 10:52 08/28/13 23:54 1

0.0726 0.166 0.0886 1.09 Lead 212 pCi/g 08/28/13 10:52 08/28/13 23:54 1

0.0877 0.140 0.103 0.902 Lead 214 pCi/g 08/28/13 10:52 08/28/13 23:54 1

0.491 2.47 1.52 18.9 Potassium 40 pCi/g 08/28/13 10:52 08/28/13 23:54 1

1.42 0.278 0.274 U

0.415 Protactinium 231 pCi/g 08/28/13 10:52 08/28/13 23:54 1

0.0796 1.00 0.153 0.124 0.852 Radium 226 TestAmerica St. Louis Page 17 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-7 Client Sample ID: L050306PES00 Matrix: Solid Date Collected: 08/20/13 17:30 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.16 (2+/-)

0.735 (2+/-)

1 08/28/13 23:54 08/28/13 10:52 pCi/g 0.977 1.00 RL MDC 0.725 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:54 1

0.192 0.134 0.133 U

0.131 Uranium 235 pCi/g 08/28/13 10:52 08/28/13 23:54 1

7.45 4.15 4.15 U

-0.434 Protactinium 234m pCi/g 08/28/13 10:52 08/28/13 23:54 1

0.135 0.271 0.236 1.29 Thorium 232 Tl-208 0.380 0.0592 0.0711 0.0395 pCi/g 08/28/13 10:52 08/28/13 23:54 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-8 Client Sample ID: L050307PRS00 Matrix: Solid Date Collected: 08/20/13 16:08 Percent Solids: 81.9 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00075 0.000022 mg/Kg

08/23/13 14:01 08/27/13 16:13 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0340 U

(2+/-)

0.0739 (2+/-)

1 08/27/13 16:13 08/23/13 14:01 pCi/g 0.256 1.50 RL MDC 0.0608 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:13 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 82 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.24 (2+/-)

0.190 (2+/-)

1 08/28/13 23:52 08/28/13 10:52 pCi/g 0.137 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.101 1.07 1.07 U

-0.00776 Americium 241 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.316 0.417 0.388 1.45 Bismuth 212 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.0764 0.132 0.103 0.797 Bismuth 214 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.0604 0.164 0.0803 1.10 Lead 212 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.0760 0.138 0.0955 0.958 Lead 214 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.278 2.45 1.36 19.9 Potassium 40 pCi/g 08/28/13 10:52 08/28/13 23:52 1

1.06 0.355 0.352 U

0.414 Protactinium 231 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.0764 1.00 0.132 0.103 0.797 Radium 226 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.849 1.00 0.353 0.336 1.05 Thorium 234 pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.239 0.134 0.134 U

0.116 Uranium 235 pCi/g 08/28/13 10:52 08/28/13 23:52 1

5.50 3.42 3.40 U

3.12 Protactinium 234m pCi/g 08/28/13 10:52 08/28/13 23:52 1

0.137 0.190 0.141 1.24 Thorium 232 Tl-208 0.371 0.0502 0.0633 0.0458 pCi/g 08/28/13 10:52 08/28/13 23:52 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-9 Client Sample ID: L050308PES00 Matrix: Solid Date Collected: 08/20/13 16:13 Percent Solids: 81.7 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00071 0.000021 mg/Kg

08/23/13 14:01 08/27/13 16:17 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0443 U

(2+/-)

0.0809 (2+/-)

1 08/27/13 16:17 08/23/13 14:01 pCi/g 0.243 1.42 RL MDC

-0.0696 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:17 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 86 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.10 (2+/-)

0.199 (2+/-)

1 08/28/13 23:53 08/28/13 10:52 pCi/g 0.131 RL MDC 0.164 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:53 1

0.122 0.0724 0.0724 U

0.0150 Americium 241 pCi/g 08/28/13 10:52 08/28/13 23:53 1

0.554 0.623 0.602 1.57 Bismuth 212 pCi/g 08/28/13 10:52 08/28/13 23:53 1

0.0712 0.138 0.108 0.818 Bismuth 214 pCi/g 08/28/13 10:52 08/28/13 23:53 1

0.0788 0.164 0.0884 1.07 Lead 212 pCi/g 08/28/13 10:52 08/28/13 23:53 1

0.0948 0.149 0.108 0.985 Lead 214 pCi/g 08/28/13 10:52 08/28/13 23:53 1

0.356 2.71 1.55 21.8 Potassium 40 pCi/g 08/28/13 10:52 08/28/13 23:53 1

1.42 0.306 0.301 U

0.507 Protactinium 231 pCi/g 08/28/13 10:52 08/28/13 23:53 1

0.0712 1.00 0.138 0.108 0.818 Radium 226 pCi/g 08/28/13 10:52 08/28/13 23:53 1

1.01 1.00 0.839 0.827 1.32 Thorium 234 pCi/g 08/28/13 10:52 08/28/13 23:53 1

0.282 0.168 0.168 U

0.0739 Uranium 235 pCi/g 08/28/13 10:52 08/28/13 23:53 1

6.60 4.14 4.12 U

4.09 Protactinium 234m pCi/g 08/28/13 10:52 08/28/13 23:53 1

0.131 0.199 0.164 1.10 Thorium 232 Tl-208 0.388 0.0670 0.0782 0.0504 pCi/g 08/28/13 10:52 08/28/13 23:53 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-10 Client Sample ID: L050309PRS00 Matrix: Solid Date Collected: 08/20/13 09:07 Percent Solids: 83.3 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00069 0.000021 mg/Kg

08/23/13 14:01 08/27/13 16:20 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0504 U

(2+/-)

0.0604 (2+/-)

1 08/27/13 16:20 08/23/13 14:01 pCi/g 0.236 1.38 RL MDC

-0.0519 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:20 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 86 TestAmerica St. Louis Page 19 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-10 Client Sample ID: L050309PRS00 Matrix: Solid Date Collected: 08/20/13 09:07 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.177 (2+/-)

1 08/28/13 23:51 08/28/13 10:52 pCi/g 0.0972 RL MDC 0.134 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.101 0.0601 0.0601 U

0.0133 Americium 241 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.334 0.410 0.386 1.32 Bismuth 212 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.0571 0.123 0.0897 0.806 Bismuth 214 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.0527 0.161 0.0727 1.11 Lead 212 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.0576 0.122 0.0840 0.849 Lead 214 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.328 2.30 1.18 19.3 Potassium 40 pCi/g 08/28/13 10:52 08/28/13 23:51 1

1.10 0.250 0.244 U

0.474 Protactinium 231 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.0571 1.00 0.123 0.0897 0.806 Radium 226 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.773 1.00 0.568 0.553 1.24 Thorium 234 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.233 0.144 0.143 U

0.0931 Uranium 235 pCi/g 08/28/13 10:52 08/28/13 23:51 1

2.54 3.19 3.08 8.29 Protactinium 234m pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.0972 0.177 0.134 1.12 Thorium 232 Tl-208 0.377 0.0477 0.0617 0.0311 pCi/g 08/28/13 10:52 08/28/13 23:51 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-11 Client Sample ID: L050310PES00 Matrix: Solid Date Collected: 08/21/13 09:19 Percent Solids: 81.2 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00069 0.000021 mg/Kg

08/23/13 14:01 08/27/13 16:24 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0626 U

(2+/-)

0.0732 (2+/-)

1 08/27/13 16:24 08/23/13 14:01 pCi/g 0.235 1.37 RL MDC

-0.0652 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:24 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 89 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.15 (2+/-)

0.169 (2+/-)

1 08/29/13 08:19 08/28/13 10:52 pCi/g 0.102 RL MDC 0.122 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 08:19 1

0.113 0.0669 0.0669 U

-0.00426 Americium 241 pCi/g 08/28/13 10:52 08/29/13 08:19 1

0.382 0.449 0.421 1.51 Bismuth 212 pCi/g 08/28/13 10:52 08/29/13 08:19 1

0.0725 0.129 0.0953 0.831 Bismuth 214 pCi/g 08/28/13 10:52 08/29/13 08:19 1

0.0845 0.152 0.0792 1.00 Lead 212 pCi/g 08/28/13 10:52 08/29/13 08:19 1

0.0741 0.134 0.0907 0.954 Lead 214 pCi/g 08/28/13 10:52 08/29/13 08:19 1

0.370 2.41 1.20 20.4 Potassium 40 pCi/g 08/28/13 10:52 08/29/13 08:19 1

1.27 0.190 0.187 U

0.293 Protactinium 231 pCi/g 08/28/13 10:52 08/29/13 08:19 1

0.0725 1.00 0.129 0.0953 0.831 Radium 226 TestAmerica St. Louis Page 20 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-11 Client Sample ID: L050310PES00 Matrix: Solid Date Collected: 08/21/13 09:19 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 0.748 U

(2+/-)

0.374 (2+/-)

1 08/29/13 08:19 08/28/13 10:52 pCi/g 1.05 1.00 RL MDC 0.365 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 08:19 1

0.195 0.167 0.164 0.290 Uranium 235 pCi/g 08/28/13 10:52 08/29/13 08:19 1

4.56 2.80 2.79 U

2.40 Protactinium 234m pCi/g 08/28/13 10:52 08/29/13 08:19 1

0.102 0.169 0.122 1.15 Thorium 232 Tl-208 0.379 0.0519 0.0651 0.0411 pCi/g 08/28/13 10:52 08/29/13 08:19 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-12 Client Sample ID: L050311PRS00 Matrix: Solid Date Collected: 08/21/13 09:42 Percent Solids: 81.7 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00075 0.000023 mg/Kg

08/23/13 14:01 08/27/13 16:28 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0691 U

(2+/-)

0.0397 (2+/-)

1 08/27/13 16:28 08/23/13 14:01 pCi/g 0.258 1.51 RL MDC

-0.0316 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:28 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 81 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.22 (2+/-)

0.189 (2+/-)

1 08/28/13 23:51 08/28/13 10:52 pCi/g 0.138 RL MDC 0.148 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.108 0.580 0.580 U

-0.0435 Americium 241 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.439 0.526 0.503 1.59 Bismuth 212 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.0842 0.148 0.117 0.940 Bismuth 214 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.0570 0.152 0.0805 1.20 Lead 212 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.0817 0.132 0.0933 0.969 Lead 214 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.389 2.53 1.39 21.9 Potassium 40 pCi/g 08/28/13 10:52 08/28/13 23:51 1

1.36 0.285 0.283 U

0.366 Protactinium 231 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.0842 1.00 0.148 0.117 0.940 Radium 226 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.971 1.00 0.802 0.792 1.32 Thorium 234 pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.264 0.157 0.157 U

0.101 Uranium 235 pCi/g 08/28/13 10:52 08/28/13 23:51 1

5.30 2.96 2.96 U

-0.316 Protactinium 234m pCi/g 08/28/13 10:52 08/28/13 23:51 1

0.138 0.189 0.148 1.22 Thorium 232 Tl-208 0.395 0.0498 0.0629 0.0349 pCi/g 08/28/13 10:52 08/28/13 23:51 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-13 Client Sample ID: L050312PES00 Matrix: Solid Date Collected: 08/21/13 10:47 Percent Solids: 81.4 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00073 0.000022 mg/Kg

08/23/13 14:01 08/27/13 16:32 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0820 U

(2+/-)

0.0315 (2+/-)

1 08/27/13 16:32 08/23/13 14:01 pCi/g 0.249 1.46 RL MDC

-0.0253 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:32 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 84 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.20 (2+/-)

0.198 (2+/-)

1 08/29/13 08:15 08/28/13 10:52 pCi/g 0.145 RL MDC 0.155 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 08:15 1

0.106 0.0632 0.0632 U

0.0195 Americium 241 pCi/g 08/28/13 10:52 08/29/13 08:15 1

0.322 0.444 0.416 1.50 Bismuth 212 pCi/g 08/28/13 10:52 08/29/13 08:15 1

0.0805 0.160 0.119 1.03 Bismuth 214 pCi/g 08/28/13 10:52 08/29/13 08:15 1

0.0637 0.169 0.0823 1.14 Lead 212 pCi/g 08/28/13 10:52 08/29/13 08:15 1

0.0755 0.139 0.0903 1.02 Lead 214 pCi/g 08/28/13 10:52 08/29/13 08:15 1

0.167 2.56 1.38 21.1 Potassium 40 pCi/g 08/28/13 10:52 08/29/13 08:15 1

1.32 0.808 0.804 U

-0.704 Protactinium 231 pCi/g 08/28/13 10:52 08/29/13 08:15 1

0.0805 1.00 0.160 0.119 1.03 Radium 226 pCi/g 08/28/13 10:52 08/29/13 08:15 1

0.838 1.00 0.647 0.633 1.26 Thorium 234 pCi/g 08/28/13 10:52 08/29/13 08:15 1

0.237 0.137 0.136 U

0.153 Uranium 235 pCi/g 08/28/13 10:52 08/29/13 08:15 1

6.29 3.71 3.70 U

1.95 Protactinium 234m pCi/g 08/28/13 10:52 08/29/13 08:15 1

0.145 0.198 0.155 1.20 Thorium 232 Tl-208 0.384 0.0579 0.0703 0.0430 pCi/g 08/28/13 10:52 08/29/13 08:15 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-14 Client Sample ID: L050313PRS00 Matrix: Solid Date Collected: 08/21/13 11:21 Percent Solids: 85.5 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00070 0.000021 mg/Kg

08/23/13 14:01 08/27/13 16:36 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0419 U

(2+/-)

0.0524 (2+/-)

1 08/27/13 16:36 08/23/13 14:01 pCi/g 0.239 1.40 RL MDC

-0.0433 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:36 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 83 TestAmerica St. Louis Page 22 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-14 Client Sample ID: L050313PRS00 Matrix: Solid Date Collected: 08/21/13 11:21 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.14 (2+/-)

0.174 (2+/-)

1 08/29/13 03:09 08/28/13 10:52 pCi/g 0.158 RL MDC 0.134 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 03:09 1

0.112 0.0812 0.0812 U

-0.00399 Americium 241 pCi/g 08/28/13 10:52 08/29/13 03:09 1

0.553 0.415 0.403 1.05 Bismuth 212 pCi/g 08/28/13 10:52 08/29/13 03:09 1

0.0792 0.138 0.110 0.858 Bismuth 214 pCi/g 08/28/13 10:52 08/29/13 03:09 1

0.0690 0.153 0.0840 1.19 Lead 212 pCi/g 08/28/13 10:52 08/29/13 03:09 1

0.0749 0.128 0.0976 0.861 Lead 214 pCi/g 08/28/13 10:52 08/29/13 03:09 1

0.414 2.54 1.41 21.8 Potassium 40 pCi/g 08/28/13 10:52 08/29/13 03:09 1

1.20 0.210 0.206 U

0.410 Protactinium 231 pCi/g 08/28/13 10:52 08/29/13 03:09 1

0.0792 1.00 0.138 0.110 0.858 Radium 226 pCi/g 08/28/13 10:52 08/29/13 03:09 1

0.893 1.00 0.348 0.338 U

0.837 Thorium 234 pCi/g 08/28/13 10:52 08/29/13 03:09 1

0.227 0.172 0.170 0.231 Uranium 235 pCi/g 08/28/13 10:52 08/29/13 03:09 1

8.15 1.72 1.72 U

0.141 Protactinium 234m pCi/g 08/28/13 10:52 08/29/13 03:09 1

0.158 0.174 0.134 1.14 Thorium 232 Tl-208 0.337 0.0464 0.0568 0.0341 pCi/g 08/28/13 10:52 08/29/13 03:09 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-15 Client Sample ID: L050314PES00 Matrix: Solid Date Collected: 08/21/13 11:38 Percent Solids: 83.0 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00073 0.000022 mg/Kg

08/23/13 14:01 08/27/13 16:40 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0712 U

(2+/-)

0.0878 (2+/-)

1 08/27/13 16:40 08/23/13 14:01 pCi/g 0.250 1.46 RL MDC

-0.0717 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:40 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 82 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.11 (2+/-)

0.197 (2+/-)

1 08/29/13 08:18 08/28/13 10:52 pCi/g 0.113 RL MDC 0.161 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 08:18 1

0.120 0.0715 0.0715 U

-0.0242 Americium 241 pCi/g 08/28/13 10:52 08/29/13 08:18 1

0.539 0.428 0.414 1.04 Bismuth 212 pCi/g 08/28/13 10:52 08/29/13 08:18 1

0.0831 0.137 0.111 0.785 Bismuth 214 pCi/g 08/28/13 10:52 08/29/13 08:18 1

0.0705 0.160 0.0859 1.04 Lead 212 pCi/g 08/28/13 10:52 08/29/13 08:18 1

0.111 0.140 0.110 0.832 Lead 214 pCi/g 08/28/13 10:52 08/29/13 08:18 1

0.200 2.37 1.42 18.6 Potassium 40 pCi/g 08/28/13 10:52 08/29/13 08:18 1

1.28 0.365 0.359 U

0.605 Protactinium 231 pCi/g 08/28/13 10:52 08/29/13 08:18 1

0.0831 1.00 0.137 0.111 0.785 Radium 226 TestAmerica St. Louis Page 23 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-15 Client Sample ID: L050314PES00 Matrix: Solid Date Collected: 08/21/13 11:38 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.57 (2+/-)

0.852 (2+/-)

1 08/29/13 08:18 08/28/13 10:52 pCi/g 1.01 1.00 RL MDC 0.836 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 08:18 1

0.209 0.136 0.135 U

0.138 Uranium 235 pCi/g 08/28/13 10:52 08/29/13 08:18 1

5.01 1.20 1.20 U

0.000 Protactinium 234m pCi/g 08/28/13 10:52 08/29/13 08:18 1

0.113 0.197 0.161 1.11 Thorium 232 Tl-208 0.269 0.0519 0.0590 0.0435 pCi/g 08/28/13 10:52 08/29/13 08:18 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-16 Client Sample ID: L050315PRS00 Matrix: Solid Date Collected: 08/21/13 13:40 Percent Solids: 82.3 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00076 0.000023 mg/Kg

08/23/13 14:01 08/27/13 16:44 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0502 U

(2+/-)

0.0482 (2+/-)

1 08/27/13 16:44 08/23/13 14:01 pCi/g 0.259 1.51 RL MDC

-0.0387 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:44 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 81 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.158 (2+/-)

1 08/29/13 08:20 08/28/13 10:52 pCi/g 0.111 RL MDC 0.113 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 08:20 1

0.0932 0.0551 0.0551 U

0.00258 Americium 241 pCi/g 08/28/13 10:52 08/29/13 08:20 1

0.392 0.427 0.411 1.12 Bismuth 212 pCi/g 08/28/13 10:52 08/29/13 08:20 1

0.0539 0.114 0.0834 0.742 Bismuth 214 pCi/g 08/28/13 10:52 08/29/13 08:20 1

0.0566 0.169 0.0752 1.17 Lead 212 pCi/g 08/28/13 10:52 08/29/13 08:20 1

0.0688 0.126 0.0837 0.910 Lead 214 pCi/g 08/28/13 10:52 08/29/13 08:20 1

0.385 2.28 1.19 19.1 Potassium 40 pCi/g 08/28/13 10:52 08/29/13 08:20 1

1.10 0.668 0.665 U

-0.543 Protactinium 231 pCi/g 08/28/13 10:52 08/29/13 08:20 1

0.0539 1.00 0.114 0.0834 0.742 Radium 226 pCi/g 08/28/13 10:52 08/29/13 08:20 1

0.920 1.00 0.745 0.727 1.54 Thorium 234 pCi/g 08/28/13 10:52 08/29/13 08:20 1

0.223 0.0937 0.0933 U

0.0913 Uranium 235 pCi/g 08/28/13 10:52 08/29/13 08:20 1

4.78 2.34 2.28 5.23 Protactinium 234m pCi/g 08/28/13 10:52 08/29/13 08:20 1

0.111 0.158 0.113 1.09 Thorium 232 Tl-208 0.325 0.0447 0.0560 0.0340 pCi/g 08/28/13 10:52 08/29/13 08:20 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-17 Client Sample ID: L050316PES00 Matrix: Solid Date Collected: 08/21/13 13:55 Percent Solids: 81.7 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00068 0.000020 mg/Kg

08/23/13 14:01 08/27/13 16:55 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0254 U

(2+/-)

0.0700 (2+/-)

1 08/27/13 16:55 08/23/13 14:01 pCi/g 0.231 1.35 RL MDC

-0.0632 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:55 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.44 (2+/-)

0.236 (2+/-)

1 08/29/13 10:11 08/28/13 10:52 pCi/g 0.101 RL MDC 0.191 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 10:11 1

0.109 0.0633 0.0633 U

0.00284 Americium 241 pCi/g 08/28/13 10:52 08/29/13 10:11 1

0.438 0.452 0.439 1.09 Bismuth 212 pCi/g 08/28/13 10:52 08/29/13 10:11 1

0.0825 0.149 0.120 0.911 Bismuth 214 pCi/g 08/28/13 10:52 08/29/13 10:11 1

0.0675 0.157 0.0843 1.23 Lead 212 pCi/g 08/28/13 10:52 08/29/13 10:11 1

0.0751 0.128 0.0899 0.946 Lead 214 pCi/g 08/28/13 10:52 08/29/13 10:11 1

0.358 2.35 1.32 20.1 Potassium 40 pCi/g 08/28/13 10:52 08/29/13 10:11 1

1.25 0.233 0.225 U

0.618 Protactinium 231 pCi/g 08/28/13 10:52 08/29/13 10:11 1

0.0825 1.00 0.149 0.120 0.911 Radium 226 pCi/g 08/28/13 10:52 08/29/13 10:11 1

0.798 1.00 0.615 0.601 1.36 Thorium 234 pCi/g 08/28/13 10:52 08/29/13 10:11 1

0.293 0.176 0.176 U

0.0944 Uranium 235 pCi/g 08/28/13 10:52 08/29/13 10:11 1

4.80 2.73 2.73 U

0.895 Protactinium 234m pCi/g 08/28/13 10:52 08/29/13 10:11 1

0.101 0.236 0.191 1.44 Thorium 232 Tl-208 0.386 0.0461 0.0594 0.0352 pCi/g 08/28/13 10:52 08/29/13 10:11 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-18 Client Sample ID: L050317PRS00 Matrix: Solid Date Collected: 08/21/13 15:15 Percent Solids: 82.7 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00071 0.000021 mg/Kg

08/23/13 14:01 08/27/13 16:59 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0574 U

(2+/-)

0.0223 (2+/-)

1 08/27/13 16:59 08/23/13 14:01 pCi/g 0.244 1.43 RL MDC

-0.0181 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 16:59 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 85 TestAmerica St. Louis Page 25 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-18 Client Sample ID: L050317PRS00 Matrix: Solid Date Collected: 08/21/13 15:15 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.23 (2+/-)

0.189 (2+/-)

1 08/29/13 10:13 08/28/13 10:52 pCi/g 0.130 RL MDC 0.146 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 10:13 1

0.106 0.0633 0.0633 U

0.0205 Americium 241 pCi/g 08/28/13 10:52 08/29/13 10:13 1

0.469 0.597 0.571 1.78 Bismuth 212 pCi/g 08/28/13 10:52 08/29/13 10:13 1

0.0615 0.147 0.107 1.04 Bismuth 214 pCi/g 08/28/13 10:52 08/29/13 10:13 1

0.0679 0.209 0.0866 1.26 Lead 212 pCi/g 08/28/13 10:52 08/29/13 10:13 1

0.0817 0.163 0.110 1.09 Lead 214 pCi/g 08/28/13 10:52 08/29/13 10:13 1

0.436 2.58 1.39 22.5 Potassium 40 pCi/g 08/28/13 10:52 08/29/13 10:13 1

0.970 0.392 0.371 1.03 Protactinium 231 pCi/g 08/28/13 10:52 08/29/13 10:13 1

0.0615 1.00 0.147 0.107 1.04 Radium 226 pCi/g 08/28/13 10:52 08/29/13 10:13 1

0.903 1.00 0.752 0.734 1.65 Thorium 234 pCi/g 08/28/13 10:52 08/29/13 10:13 1

0.274 0.139 0.139 U

0.105 Uranium 235 pCi/g 08/28/13 10:52 08/29/13 10:13 1

6.25 3.74 3.73 U

2.40 Protactinium 234m pCi/g 08/28/13 10:52 08/29/13 10:13 1

0.130 0.189 0.146 1.23 Thorium 232 Tl-208 0.361 0.0539 0.0643 0.0449 pCi/g 08/28/13 10:52 08/29/13 10:13 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-19 Client Sample ID: L050318PES00 Matrix: Solid Date Collected: 08/21/13 15:21 Percent Solids: 81.4 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00070 0.000021 mg/Kg

08/23/13 14:01 08/27/13 17:03 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0489 U

(2+/-)

0.0192 (2+/-)

1 08/27/13 17:03 08/23/13 14:01 pCi/g 0.241 1.41 RL MDC

-0.0160 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 17:03 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.19 (2+/-)

0.195 (2+/-)

1 08/29/13 10:12 08/28/13 10:52 pCi/g 0.123 RL MDC 0.153 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 10:12 1

0.115 0.0679 0.0679 U

-0.00657 Americium 241 pCi/g 08/28/13 10:52 08/29/13 10:12 1

0.478 0.579 0.554 1.61 Bismuth 212 pCi/g 08/28/13 10:52 08/29/13 10:12 1

0.0841 0.149 0.118 0.869 Bismuth 214 pCi/g 08/28/13 10:52 08/29/13 10:12 1

0.0781 0.165 0.0874 1.08 Lead 212 pCi/g 08/28/13 10:52 08/29/13 10:12 1

0.0826 0.148 0.111 0.942 Lead 214 pCi/g 08/28/13 10:52 08/29/13 10:12 1

0.189 2.61 1.47 21.1 Potassium 40 pCi/g 08/28/13 10:52 08/29/13 10:12 1

1.46 0.269 0.264 U

0.456 Protactinium 231 pCi/g 08/28/13 10:52 08/29/13 10:12 1

0.0841 1.00 0.149 0.118 0.869 Radium 226 TestAmerica St. Louis Page 26 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-19 Client Sample ID: L050318PES00 Matrix: Solid Date Collected: 08/21/13 15:21 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.40 (2+/-)

0.784 (2+/-)

1 08/29/13 10:12 08/28/13 10:52 pCi/g 0.977 1.00 RL MDC 0.770 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 10:12 1

0.219 0.158 0.158 U

0.128 Uranium 235 pCi/g 08/28/13 10:52 08/29/13 10:12 1

6.55 3.61 3.61 U

0.146 Protactinium 234m pCi/g 08/28/13 10:52 08/29/13 10:12 1

0.123 0.195 0.153 1.19 Thorium 232 Tl-208 0.364 0.0587 0.0698 0.0455 pCi/g 08/28/13 10:52 08/29/13 10:12 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-20 Client Sample ID: L050319PRS00 Matrix: Solid Date Collected: 08/21/13 16:42 Percent Solids: 84.2 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00065 0.000020 mg/Kg

08/23/13 14:01 08/27/13 17:07 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0560 U

(2+/-)

0.0825 (2+/-)

1 08/27/13 17:07 08/23/13 14:01 pCi/g 0.224 1.31 RL MDC

-0.0748 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:01 08/27/13 17:07 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.989 (2+/-)

0.156 (2+/-)

1 08/29/13 10:14 08/28/13 10:52 pCi/g 0.147 RL MDC 0.124 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 10:52 08/29/13 10:14 1

0.0979 0.0583 0.0582 U

0.0142 Americium 241 pCi/g 08/28/13 10:52 08/29/13 10:14 1

0.477 0.533 0.515 1.42 Bismuth 212 pCi/g 08/28/13 10:52 08/29/13 10:14 1

0.0815 0.132 0.105 0.828 Bismuth 214 pCi/g 08/28/13 10:52 08/29/13 10:14 1

0.0902 0.139 0.0850 1.02 Lead 212 pCi/g 08/28/13 10:52 08/29/13 10:14 1

0.0769 0.123 0.0887 0.879 Lead 214 pCi/g 08/28/13 10:52 08/29/13 10:14 1

0.343 2.45 1.30 21.6 Potassium 40 pCi/g 08/28/13 10:52 08/29/13 10:14 1

1.28 0.312 0.306 U

0.602 Protactinium 231 pCi/g 08/28/13 10:52 08/29/13 10:14 1

0.0815 1.00 0.132 0.105 0.828 Radium 226 pCi/g 08/28/13 10:52 08/29/13 10:14 1

0.950 1.00 0.265 0.254 U

0.753 Thorium 234 pCi/g 08/28/13 10:52 08/29/13 10:14 1

0.211 0.128 0.128 U

0.0985 Uranium 235 pCi/g 08/28/13 10:52 08/29/13 10:14 1

5.44 3.50 3.50 U

1.85 Protactinium 234m pCi/g 08/28/13 10:52 08/29/13 10:14 1

0.147 0.156 0.124 0.989 Thorium 232 Tl-208 0.376 0.0511 0.0628 0.0379 pCi/g 08/28/13 10:52 08/29/13 10:14 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-21 Client Sample ID: L050320PES00 Matrix: Solid Date Collected: 08/21/13 16:50 Percent Solids: 83.8 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00068 0.000020 mg/Kg

08/23/13 14:05 08/27/13 17:19 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0576 U

(2+/-)

0.0689 (2+/-)

1 08/27/13 17:19 08/23/13 14:05 pCi/g 0.231 1.35 RL MDC

-0.0603 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 17:19 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 88 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.927 (2+/-)

0.226 (2+/-)

1 08/28/13 19:12 08/28/13 13:20 pCi/g 0.143 RL MDC 0.205 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 19:12 1

0.204 0.120 0.120 U

0.0154 Americium 241 pCi/g 08/28/13 13:20 08/28/13 19:12 1

0.382 0.532 0.511 1.42 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 19:12 1

0.107 0.155 0.138 0.683 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 19:12 1

0.115 0.169 0.126 0.868 Lead 212 pCi/g 08/28/13 13:20 08/28/13 19:12 1

0.115 0.161 0.145 0.689 Lead 214 pCi/g 08/28/13 13:20 08/28/13 19:12 1

0.660 2.55 1.74 18.2 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 19:12 1

1.82 0.602 0.601 U

0.317 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 19:12 1

0.107 1.00 0.155 0.138 0.683 Radium 226 pCi/g 08/28/13 13:20 08/28/13 19:12 1

1.82 1.00 0.608 0.603 U

0.759 Thorium 234 pCi/g 08/28/13 13:20 08/28/13 19:12 1

0.363 0.214 0.213 U

0.213 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 19:12 1

8.51 4.95 4.94 U

2.53 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 19:12 1

0.143 0.226 0.205 0.927 Thorium 232 Tl-208 0.239 0.0583 0.0633 0.0626 pCi/g 08/28/13 13:20 08/28/13 19:12 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-22 Client Sample ID: L050321PRS00 Matrix: Solid Date Collected: 08/21/13 16:19 Percent Solids: 83.0 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00070 0.000021 mg/Kg

08/23/13 14:05 08/27/13 17:30 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.00286 U

(2+/-)

0.0870 (2+/-)

1 08/27/13 17:30 08/23/13 14:05 pCi/g 0.238 1.39 RL MDC 0.0748 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 17:30 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 86 TestAmerica St. Louis Page 28 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-22 Client Sample ID: L050321PRS00 Matrix: Solid Date Collected: 08/21/13 16:19 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.19 (2+/-)

0.182 (2+/-)

1 08/28/13 20:18 08/28/13 13:20 pCi/g 0.139 RL MDC 0.142 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 20:18 1

0.102 0.0605 0.0605 U

0.0206 Americium 241 pCi/g 08/28/13 13:20 08/28/13 20:18 1

0.681 0.541 0.541 U

0.000 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 20:18 1

0.0854 0.130 0.110 0.720 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 20:18 1

0.0722 0.140 0.0867 1.03 Lead 212 pCi/g 08/28/13 13:20 08/28/13 20:18 1

0.0906 0.124 0.0943 0.835 Lead 214 pCi/g 08/28/13 13:20 08/28/13 20:18 1

0.201 2.27 1.41 18.4 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 20:18 1

1.32 0.290 0.286 U

0.467 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 20:18 1

0.0854 1.00 0.130 0.110 0.720 Radium 226 pCi/g 08/28/13 13:20 08/28/13 20:18 1

0.778 1.00 0.558 0.546 1.18 Thorium 234 pCi/g 08/28/13 13:20 08/28/13 20:18 1

0.245 0.148 0.148 U

0.110 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 20:18 1

4.73 2.40 2.40 U

0.000 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 20:18 1

0.139 0.182 0.142 1.19 Thorium 232 Tl-208 0.340 0.0529 0.0623 0.0393 pCi/g 08/28/13 13:20 08/28/13 20:18 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-23 Client Sample ID: L050322PES00 Matrix: Solid Date Collected: 08/21/13 16:24 Percent Solids: 82.2 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00069 0.000021 mg/Kg

08/23/13 14:05 08/27/13 17:42 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.000943 U

(2+/-)

0.0682 (2+/-)

1 08/27/13 17:42 08/23/13 14:05 pCi/g 0.236 1.38 RL MDC 0.0605 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 17:42 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 89 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.33 (2+/-)

0.255 (2+/-)

1 08/28/13 20:21 08/28/13 13:20 pCi/g 0.0964 RL MDC 0.216 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 20:21 1

0.113 0.0662 0.0662 U

0.000403 Americium 241 pCi/g 08/28/13 13:20 08/28/13 20:21 1

0.297 0.529 0.489 1.95 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 20:21 1

0.104 0.129 0.110 0.660 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 20:21 1

0.0849 0.168 0.0949 1.07 Lead 212 pCi/g 08/28/13 13:20 08/28/13 20:21 1

0.101 0.138 0.108 0.825 Lead 214 pCi/g 08/28/13 13:20 08/28/13 20:21 1

0.384 2.44 1.54 18.5 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 20:21 1

1.49 0.253 0.249 U

0.394 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 20:21 1

0.104 1.00 0.129 0.110 0.660 Radium 226 TestAmerica St. Louis Page 29 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-23 Client Sample ID: L050322PES00 Matrix: Solid Date Collected: 08/21/13 16:24 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.21 (2+/-)

0.444 (2+/-)

1 08/28/13 20:21 08/28/13 13:20 pCi/g 1.09 1.00 RL MDC 0.425 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 20:21 1

0.291 0.174 0.174 U

0.0873 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 20:21 1

6.39 3.62 3.61 U

1.24 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 20:21 1

0.0964 0.255 0.216 1.33 Thorium 232 Tl-208 0.419 0.0642 0.0775 0.0389 pCi/g 08/28/13 13:20 08/28/13 20:21 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-24 Client Sample ID: L050323PUB00 Matrix: Solid Date Collected: 08/19/13 16:35 Percent Solids: 84.6 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00067 0.000020 mg/Kg

08/23/13 14:05 08/27/13 17:46 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.00439 U

(2+/-)

0.0201 (2+/-)

1 08/27/13 17:46 08/23/13 14:05 pCi/g 0.231 1.35 RL MDC 0.0177 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 17:46 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 88 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.30 (2+/-)

0.213 (2+/-)

1 08/28/13 21:13 08/28/13 13:20 pCi/g 0.0620 RL MDC 0.172 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.102 0.0601 0.0601 U

0.00160 Americium 241 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.417 0.471 0.454 1.29 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.0738 0.129 0.105 0.769 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.0629 0.187 0.0823 1.11 Lead 212 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.0813 0.132 0.0899 0.883 Lead 214 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.448 2.31 1.33 19.6 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 21:13 1

1.31 0.800 0.796 U

-0.628 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.0738 1.00 0.129 0.105 0.769 Radium 226 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.893 1.00 0.733 0.719 1.41 Thorium 234 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.278 0.137 0.137 U

0.0424 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 21:13 1

6.05 3.35 3.35 U

-0.0587 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.0620 0.213 0.172 1.30 Thorium 232 Tl-208 0.336 0.0515 0.0610 0.0384 pCi/g 08/28/13 13:20 08/28/13 21:13 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-25 Client Sample ID: L050324PUB00 Matrix: Solid Date Collected: 08/19/13 16:45 Percent Solids: 84.5 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00068 0.000020 mg/Kg

08/23/13 14:05 08/27/13 17:49 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0325 U

(2+/-)

0.0453 (2+/-)

1 08/27/13 17:49 08/23/13 14:05 pCi/g 0.232 1.36 RL MDC

-0.0393 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 17:49 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.187 (2+/-)

1 08/28/13 20:19 08/28/13 13:20 pCi/g 0.0853 RL MDC 0.153 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 20:19 1

0.104 0.0624 0.0624 U

0.0252 Americium 241 pCi/g 08/28/13 13:20 08/28/13 20:19 1

0.379 0.424 0.407 1.22 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 20:19 1

0.0643 0.131 0.102 0.835 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 20:19 1

0.0645 0.144 0.0818 1.10 Lead 212 pCi/g 08/28/13 13:20 08/28/13 20:19 1

0.0893 0.120 0.0852 0.875 Lead 214 pCi/g 08/28/13 13:20 08/28/13 20:19 1

0.399 2.68 1.45 23.4 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 20:19 1

1.21 0.227 0.225 U

0.307 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 20:19 1

0.0643 1.00 0.131 0.102 0.835 Radium 226 pCi/g 08/28/13 13:20 08/28/13 20:19 1

0.859 1.00 0.660 0.646 1.38 Thorium 234 pCi/g 08/28/13 13:20 08/28/13 20:19 1

0.245 0.137 0.137 U

0.0720 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 20:19 1

5.88 3.71 3.71 U

1.31 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 20:19 1

0.0853 0.187 0.153 1.12 Thorium 232 Tl-208 0.381 0.0524 0.0641 0.0373 pCi/g 08/28/13 13:20 08/28/13 20:19 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-26 Client Sample ID: L050325PUB00 Matrix: Solid Date Collected: 08/19/13 16:55 Percent Solids: 82.7 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00073 0.000022 mg/Kg

08/23/13 14:05 08/27/13 17:53 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0358 U

(2+/-)

0.0339 (2+/-)

1 08/27/13 17:53 08/23/13 14:05 pCi/g 0.249 1.45 RL MDC

-0.0278 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 17:53 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 83 TestAmerica St. Louis Page 31 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-26 Client Sample ID: L050325PUB00 Matrix: Solid Date Collected: 08/19/13 16:55 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.08 (2+/-)

0.184 (2+/-)

1 08/28/13 20:20 08/28/13 13:20 pCi/g 0.101 RL MDC 0.152 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 20:20 1

0.115 0.236 0.236 U

-0.0219 Americium 241 pCi/g 08/28/13 13:20 08/28/13 20:20 1

0.520 0.385 0.376 0.858 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 20:20 1

0.0799 0.137 0.113 0.789 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 20:20 1

0.0639 0.154 0.0853 1.20 Lead 212 pCi/g 08/28/13 13:20 08/28/13 20:20 1

0.0829 0.132 0.103 0.856 Lead 214 pCi/g 08/28/13 13:20 08/28/13 20:20 1

0.311 2.76 1.49 24.1 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 20:20 1

1.35 0.826 0.823 U

-0.697 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 20:20 1

0.0799 1.00 0.137 0.113 0.789 Radium 226 pCi/g 08/28/13 13:20 08/28/13 20:20 1

1.08 1.00 0.365 0.357 U

0.803 Thorium 234 pCi/g 08/28/13 13:20 08/28/13 20:20 1

0.274 0.145 0.145 U

0.0944 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 20:20 1

6.60 3.80 3.80 U

1.17 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 20:20 1

0.101 0.184 0.152 1.08 Thorium 232 Tl-208 0.402 0.0506 0.0640 0.0311 pCi/g 08/28/13 13:20 08/28/13 20:20 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-27 Client Sample ID: L050326PUB00 Matrix: Solid Date Collected: 08/20/13 14:55 Percent Solids: 97.8 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00057 0.000017 mg/Kg

08/23/13 14:05 08/27/13 17:57 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.121 U

(2+/-)

0.189 (2+/-)

1 08/27/13 17:57 08/23/13 14:05 pCi/g 0.196 1.14 RL MDC 0.169 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 17:57 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.314 (2+/-)

0.0675 (2+/-)

1 08/28/13 21:12 08/28/13 13:20 pCi/g 0.0605 RL MDC 0.0595 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.149 0.0893 0.0893 U

-0.00857 Americium 241 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.343 0.229 0.226 0.363 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0519 0.0774 0.0650 0.404 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0548 0.0495 0.0406 0.219 Lead 212 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0472 0.0760 0.0581 0.472 Lead 214 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.176 0.808 0.548 5.80 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.700 0.355 0.353 U

0.337 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0519 1.00 0.0774 0.0650 0.404 Radium 226 TestAmerica St. Louis Page 32 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-27 Client Sample ID: L050326PUB00 Matrix: Solid Date Collected: 08/20/13 14:55 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 36.3 (2+/-)

4.22 (2+/-)

1 08/28/13 21:12 08/28/13 13:20 pCi/g 1.73 1.00 RL MDC 1.83 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.399 0.776 0.343 6.84 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 21:12 1

2.17 6.48 4.85 42.5 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0605 0.0675 0.0595 0.314 Thorium 232 Tl-208 0.111 0.0272 0.0296 0.0253 pCi/g 08/28/13 13:20 08/28/13 21:12 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-28 Client Sample ID: L050327PUB00 Matrix: Solid Date Collected: 08/21/13 09:15 Percent Solids: 87.1 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00067 0.000020 mg/Kg

08/23/13 14:05 08/27/13 18:01 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.00115 U

(2+/-)

0.0384 (2+/-)

1 08/27/13 18:01 08/23/13 14:05 pCi/g 0.230 1.34 RL MDC

-0.0328 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 18:01 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 85 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.05 (2+/-)

0.193 (2+/-)

1 08/28/13 21:12 08/28/13 13:20 pCi/g 0.127 RL MDC 0.164 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.144 0.0868 0.0867 U

0.0504 Americium 241 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.611 0.427 0.420 0.791 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0750 0.141 0.115 0.837 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0676 0.139 0.0838 1.03 Lead 212 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0911 0.145 0.115 0.908 Lead 214 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.337 2.50 1.49 20.8 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 21:12 1

1.30 0.296 0.292 U

0.510 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0750 1.00 0.141 0.115 0.837 Radium 226 pCi/g 08/28/13 13:20 08/28/13 21:12 1

1.46 1.00 2.42 1.48 19.7 Thorium 234 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.334 0.497 0.307 4.03 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 21:12 1

1.70 5.55 4.92 26.7 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.127 0.193 0.164 1.05 Thorium 232 Tl-208 0.353 0.0588 0.0681 0.0451 pCi/g 08/28/13 13:20 08/28/13 21:12 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-29 Client Sample ID: L050328PUB00 Matrix: Solid Date Collected: 08/21/13 09:45 Percent Solids: 84.9 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00068 0.000020 mg/Kg

08/23/13 14:05 08/27/13 18:05 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0446 U

(2+/-)

0.0125 (2+/-)

1 08/27/13 18:05 08/23/13 14:05 pCi/g 0.232 1.36 RL MDC

-0.0101 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 18:05 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.10 (2+/-)

0.174 (2+/-)

1 08/28/13 21:12 08/28/13 13:20 pCi/g 0.106 RL MDC 0.133 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.204 0.124 0.124 U

0.0775 Americium 241 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.393 0.493 0.462 1.66 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0778 0.119 0.0974 0.656 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0698 0.155 0.0773 1.04 Lead 212 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0683 0.129 0.0920 0.870 Lead 214 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.336 2.58 1.28 21.8 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 21:12 1

1.27 0.418 0.411 U

0.701 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.0778 1.00 0.119 0.0974 0.656 Radium 226 pCi/g 08/28/13 13:20 08/28/13 21:12 1

1.95 1.00 4.40 2.05 37.2 Thorium 234 pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.378 0.849 0.381 7.46 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 21:12 1

4.06 7.50 6.30 40.3 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 21:12 1

0.106 0.174 0.133 1.10 Thorium 232 Tl-208 0.351 0.0550 0.0660 0.0435 pCi/g 08/28/13 13:20 08/28/13 21:12 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-30 Client Sample ID: L050329PUB00 Matrix: Solid Date Collected: 08/21/13 10:50 Percent Solids: 83.9 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00071 0.000021 mg/Kg

08/23/13 14:05 08/27/13 18:09 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.0692 U

(2+/-)

0.0631 (2+/-)

1 08/27/13 18:09 08/23/13 14:05 pCi/g 0.242 1.41 RL MDC

-0.0527 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 18:09 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 84 TestAmerica St. Louis Page 34 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-30 Client Sample ID: L050329PUB00 Matrix: Solid Date Collected: 08/21/13 10:50 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.214 (2+/-)

1 08/28/13 21:13 08/28/13 13:20 pCi/g 0.141 RL MDC 0.185 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.209 0.233 0.233 U

-0.0123 Americium 241 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.465 0.626 0.590 2.13 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.0804 0.141 0.112 0.870 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.0849 0.152 0.0906 1.13 Lead 212 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.0882 0.134 0.106 0.849 Lead 214 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.412 2.85 1.55 24.7 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 21:13 1

1.56 0.366 0.359 U

0.751 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.0804 1.00 0.141 0.112 0.870 Radium 226 pCi/g 08/28/13 13:20 08/28/13 21:13 1

2.43 1.00 5.25 1.60 51.2 Thorium 234 pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.524 1.33 0.534 12.6 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 21:13 1

4.70 10.3 8.35 62.9 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 21:13 1

0.141 0.214 0.185 1.12 Thorium 232 Tl-208 0.349 0.0550 0.0646 0.0427 pCi/g 08/28/13 13:20 08/28/13 21:13 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-31 Client Sample ID: L050330PUB00 Matrix: Solid Date Collected: 08/21/13 11:10 Percent Solids: 85.8 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00068 0.000020 mg/Kg

08/23/13 14:05 08/27/13 18:13 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0440 U

(2+/-)

0.124 (2+/-)

1 08/27/13 18:13 08/23/13 14:05 pCi/g 0.233 1.36 RL MDC 0.107 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 18:13 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 86 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.05 (2+/-)

0.170 (2+/-)

1 08/28/13 22:02 08/28/13 13:20 pCi/g 0.0999 RL MDC 0.132 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 22:02 1

0.231 0.139 0.139 U

-0.0181 Americium 241 pCi/g 08/28/13 13:20 08/28/13 22:02 1

0.391 0.385 0.368 1.10 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 22:02 1

0.0891 0.144 0.117 0.817 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 22:02 1

0.0707 0.159 0.0770 1.07 Lead 212 pCi/g 08/28/13 13:20 08/28/13 22:02 1

0.0861 0.135 0.103 0.843 Lead 214 pCi/g 08/28/13 13:20 08/28/13 22:02 1

0.422 2.41 1.22 20.3 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 22:02 1

1.35 0.221 0.217 U

0.396 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 22:02 1

0.0891 1.00 0.144 0.117 0.817 Radium 226 TestAmerica St. Louis Page 35 of 50 1

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-31 Client Sample ID: L050330PUB00 Matrix: Solid Date Collected: 08/21/13 11:10 Date Received: 08/22/13 16:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 53.3 (2+/-)

5.92 (2+/-)

1 08/28/13 22:02 08/28/13 13:20 pCi/g 1.77 1.00 RL MDC 1.99 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 22:02 1

0.330 0.408 0.284 2.88 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 22:02 1

2.78 9.56 6.92 65.3 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 22:02 1

0.0999 0.170 0.132 1.05 Thorium 232 Tl-208 0.384 0.0558 0.0686 0.0447 pCi/g 08/28/13 13:20 08/28/13 22:02 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3482-32 Client Sample ID: L050331PUB00 Matrix: Solid Date Collected: 08/21/13 11:20 Percent Solids: 85.0 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00068 0.000020 mg/Kg

08/23/13 14:05 08/27/13 18:17 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0418 U

(2+/-)

0.0464 (2+/-)

1 08/27/13 18:17 08/23/13 14:05 pCi/g 0.234 1.36 RL MDC 0.0400 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 18:17 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.07 (2+/-)

0.178 (2+/-)

1 08/29/13 21:25 08/28/13 13:20 pCi/g 0.0645 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/29/13 21:25 1

0.232 0.140 0.140 U

0.0558 Americium 241 pCi/g 08/28/13 13:20 08/29/13 21:25 1

0.600 0.428 0.418 0.890 Bismuth 212 pCi/g 08/28/13 13:20 08/29/13 21:25 1

0.0774 0.147 0.110 0.930 Bismuth 214 pCi/g 08/28/13 13:20 08/29/13 21:25 1

0.0740 0.157 0.0826 1.03 Lead 212 pCi/g 08/28/13 13:20 08/29/13 21:25 1

0.102 0.142 0.102 0.955 Lead 214 pCi/g 08/28/13 13:20 08/29/13 21:25 1

0.171 2.47 1.37 20.2 Potassium 40 pCi/g 08/28/13 13:20 08/29/13 21:25 1

1.40 0.306 0.304 U

0.337 Protactinium 231 pCi/g 08/28/13 13:20 08/29/13 21:25 1

0.0774 1.00 0.147 0.110 0.930 Radium 226 pCi/g 08/28/13 13:20 08/29/13 21:25 1

2.06 1.00 6.67 2.33 59.8 Thorium 234 pCi/g 08/28/13 13:20 08/29/13 21:25 1

0.336 0.439 0.311 3.05 Uranium 235 pCi/g 08/28/13 13:20 08/29/13 21:25 1

4.01 11.3 8.54 73.7 Protactinium 234m pCi/g 08/28/13 13:20 08/29/13 21:25 1

0.0645 0.178 0.141 1.07 Thorium 232 Tl-208 0.334 0.0569 0.0666 0.0478 pCi/g 08/28/13 13:20 08/29/13 21:25 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3482-33 Client Sample ID: L050332PUB00 Matrix: Solid Date Collected: 08/21/13 13:40 Percent Solids: 83.7 Date Received: 08/22/13 16:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00071 0.000021 mg/Kg

08/23/13 14:05 08/27/13 18:28 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99

-0.000968 U

(2+/-)

0.0849 (2+/-)

1 08/27/13 18:28 08/23/13 14:05 pCi/g 0.242 1.41 RL MDC

-0.0716 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/23/13 14:05 08/27/13 18:28 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 84 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.950 (2+/-)

0.205 (2+/-)

1 08/28/13 22:03 08/28/13 13:20 pCi/g 0.136 RL MDC 0.183 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/28/13 13:20 08/28/13 22:03 1

0.109 0.0814 0.0814 U

-0.000906 Americium 241 pCi/g 08/28/13 13:20 08/28/13 22:03 1

0.644 0.444 0.437 0.796 Bismuth 212 pCi/g 08/28/13 13:20 08/28/13 22:03 1

0.0650 0.133 0.105 0.830 Bismuth 214 pCi/g 08/28/13 13:20 08/28/13 22:03 1

0.0776 0.154 0.0910 1.16 Lead 212 pCi/g 08/28/13 13:20 08/28/13 22:03 1

0.0788 0.125 0.0891 0.904 Lead 214 pCi/g 08/28/13 13:20 08/28/13 22:03 1

0.192 2.39 1.44 19.8 Potassium 40 pCi/g 08/28/13 13:20 08/28/13 22:03 1

0.919 0.402 0.396 U

0.652 Protactinium 231 pCi/g 08/28/13 13:20 08/28/13 22:03 1

0.0650 1.00 0.133 0.105 0.830 Radium 226 pCi/g 08/28/13 13:20 08/28/13 22:03 1

0.987 1.00 0.852 0.813 2.62 Thorium 234 pCi/g 08/28/13 13:20 08/28/13 22:03 1

0.206 0.143 0.141 0.253 Uranium 235 pCi/g 08/28/13 13:20 08/28/13 22:03 1

5.73 3.41 3.40 U

2.15 Protactinium 234m pCi/g 08/28/13 13:20 08/28/13 22:03 1

0.136 0.205 0.183 0.950 Thorium 232 Tl-208 0.429 0.0648 0.0770 0.0471 pCi/g 08/28/13 13:20 08/28/13 22:03 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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QC Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-68378/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68378 RL MDL Technetium 99 ND 0.00053 0.000016 mg/Kg 08/23/13 14:01 08/27/13 15:22 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-68378/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68378 Technetium 99 0.00247 0.00244 mg/Kg 99 80 - 120 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Client Sample ID: L050301PRS00 Lab Sample ID: 160-3482-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68378 Technetium 99 ND 0.00321 0.00285 mg/Kg 89 75 - 125

Analyte MS MS D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Client Sample ID: L050301PRS00 Lab Sample ID: 160-3482-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68378 Technetium 99 ND 0.00324 0.00300 mg/Kg 93 75 - 125 5

30

Analyte MSD MSD D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Limit RPD RPD Client Sample ID: Method Blank Lab Sample ID: MB 160-68379/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68379 RL MDL Technetium 99 ND 0.00053 0.000016 mg/Kg 08/23/13 14:05 08/27/13 17:11 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-68379/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68379 Technetium 99 0.00241 0.00242 mg/Kg 100 80 - 120 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Client Sample ID: L050320PES00 Lab Sample ID: 160-3482-21 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68379 Technetium 99 ND 0.00313 0.00289 mg/Kg 92 75 - 125

Analyte MS MS D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Client Sample ID: L050320PES00 Lab Sample ID: 160-3482-21 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 68965 Prep Batch: 68379 Technetium 99 ND 0.00315 0.00291 mg/Kg 92 75 - 125 1

30

Analyte MSD MSD D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Limit RPD RPD TestAmerica St. Louis Page 38 of 50 1

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QC Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-68378/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68378 Technetium 99 Analyte U

1 08/27/13 15:22 08/23/13 14:01 pCi/g 0.180 MDC 1.05 RL 0.0171

-0.0157 (2+/-)

(2+/-)

MB

-0.04825 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Carrier Re 30 - 110 08/23/13 14:01 08/27/13 15:22 1

Dil Fac Prepared Analyzed Qualifier Limits

%Yield 95 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-68378/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68378 Technetium 99 Analyte 120 80 99 41.74 42.3 4.26 1.06 0.181 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 LCS Qualifier Limits

%Yield 95 LCS Client Sample ID: L050301PRS00 Lab Sample ID: 160-3482-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68378 Technetium 99 Analyte 125 75 89 48.77 54.9

-0.0398 U

5.20 1.37 0.235 RL MDC (2+/-)

MS MS pCi/g Unit Result Qual

%Rec Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 MS Qualifier Limits

%Yield 87 MS Client Sample ID: L050301PRS00 Lab Sample ID: 160-3482-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68378 Technetium 99 Analyte 1

0.25 125 75 93 51.40 55.4

-0.0398 U

5.43 1.39 0.237 RL MDC (2+/-)

MSD MSD pCi/g Unit Result Qual

%Rec Limit Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits

%Yield 87 MSD Client Sample ID: Method Blank Lab Sample ID: MB 160-68379/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68379 Technetium 99 Analyte U

1 08/27/13 17:11 08/23/13 14:05 pCi/g 0.180 MDC 1.05 RL 0.0206

-0.0191 (2+/-)

(2+/-)

MB

-0.04694 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total TestAmerica St. Louis Page 39 of 50 1

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QC Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)

Client Sample ID: Method Blank Lab Sample ID: MB 160-68379/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68379 Carrier Re 30 - 110 08/23/13 14:05 08/27/13 17:11 1

Dil Fac Prepared Analyzed Qualifier Limits

%Yield 95 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-68379/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68379 Technetium 99 Analyte 120 80 100 41.44 41.3 4.01 1.03 0.177 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 LCS Qualifier Limits

%Yield 96 LCS Client Sample ID: L050320PES00 Lab Sample ID: 160-3482-21 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68379 Technetium 99 Analyte 125 75 92 49.54 53.6

-0.0576 U

5.61 1.34 0.229 RL MDC (2+/-)

MS MS pCi/g Unit Result Qual

%Rec Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 MS Qualifier Limits

%Yield 88 MS Client Sample ID: L050320PES00 Lab Sample ID: 160-3482-21 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 68966 Prep Batch: 68379 Technetium 99 Analyte 1

0.03 125 75 92 49.87 53.9

-0.0576 U

5.41 1.35 0.231 RL MDC (2+/-)

MSD MSD pCi/g Unit Result Qual

%Rec Limit Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits

%Yield 88 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-69096/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 69583 Prep Batch: 69096 Actinium 228 Analyte U

1 08/29/13 23:56 08/28/13 10:52 pCi/g 0.0507 MDC RL 0.0290 0.0290 (2+/-)

(2+/-)

MB 0.01168 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

08/29/13 23:56 08/28/13 10:52 pCi/g 0.0215 0.0124 0.0124 U

0.004928 Americium 241 1

08/29/13 23:56 08/28/13 10:52 pCi/g 0.213 0.113 0.113 U

-0.01066 Bismuth 212 1

08/29/13 23:56 08/28/13 10:52 pCi/g 0.0377 0.0516 0.0515 U

-0.008760 Bismuth 214 TestAmerica St. Louis Page 40 of 50 1

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QC Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Method Blank Lab Sample ID: MB 160-69096/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 69583 Prep Batch: 69096 Lead 212 Analyte U

1 08/29/13 23:56 08/28/13 10:52 pCi/g 0.0208 MDC RL 0.0113 0.0113 (2+/-)

(2+/-)

MB 0.006093 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

08/29/13 23:56 08/28/13 10:52 pCi/g 0.0294 0.0144 0.0144 U

0.005683 Lead 214 1

08/29/13 23:56 08/28/13 10:52 pCi/g 0.260 0.185 0.185 U

-0.05724 Potassium 40 1

08/29/13 23:56 08/28/13 10:52 pCi/g 0.419 0.0585 0.0585 U

0.0000 Protactinium 231 1

08/29/13 23:56 08/28/13 10:52 pCi/g 0.0377 1.00 0.0516 0.0515 U

-0.008760 Radium 226 1

08/29/13 23:56 08/28/13 10:52 pCi/g 0.281 1.00 0.144 0.144 U

-0.001515 Thorium 234 1

08/29/13 23:56 08/28/13 10:52 pCi/g 0.0577 0.0280 0.0279 U

0.02322 Uranium 235 1

08/29/13 23:56 08/28/13 10:52 pCi/g 0.953 0.604 0.603 U

0.1541 Protactinium 234m 1

08/29/13 23:56 08/28/13 10:52 pCi/g 0.0507 0.0290 0.0290 U

0.01168 Thorium 232 Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 08/28/13 10:52 08/29/13 23:56 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-69096/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 69119 Prep Batch: 69096 Americium 241 Analyte 116 87 94 92.24 97.7 9.60 0.452 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 31.7 29.97 3.14 0.200 0.145 pCi/g 95 87 - 120 Cobalt 60 24.8 23.27 2.35 0.0776 pCi/g 94 87 - 115 Client Sample ID: L050318PES00 Lab Sample ID: 160-3482-19 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 69580 Prep Batch: 69096 Actinium 228 Analyte 1

0.16 1.123 1.19 0.184 0.132 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Americium 241

-0.00657 U

-0.00935 0

U 0.0584 0.0982 pCi/g 0.02 1

Bismuth 212 1.61 1.052 0.332 0.378 pCi/g 0.61 1

Bismuth 214 0.869 0.8151 0.128 0.0696 pCi/g 0.20 1

Lead 212 1.08 1.126 0.163 0.0551 pCi/g 0.15 1

Lead 214 0.942 0.9246 0.133 0.0664 pCi/g 0.06 1

Potassium 40 21.1 20.73 2.44 0.304 pCi/g 0.06 1

Protactinium 231 0.456 U

0.4082 U

0.228 1.22 pCi/g 0.1 1

Radium 226 0.869 0.8151 0.128 1.00 0.0696 pCi/g 0.20 1

Thorium 234 1.40 1.433 0.696 1.00 0.881 pCi/g 0.02 1

Uranium 235 0.128 U

0.1260 U

0.131 0.226 pCi/g 0.01 1

Protactinium 234m 0.146 U

1.947 U

3.19 4.61 pCi/g 0.26 1

Thorium 232 1.19 1.123 0.184 0.132 pCi/g 0.16 1

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QC Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Method Blank Lab Sample ID: MB 160-69129/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 69117 Prep Batch: 69129 Actinium 228 Analyte U

1 08/28/13 20:18 08/28/13 13:20 pCi/g 0.0472 MDC RL 0.0230 0.0229 (2+/-)

(2+/-)

MB 0.009657 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.0247 0.0143 0.0143 U

-0.005719 Americium 241 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.177 0.0914 0.0914 U

0.007249 Bismuth 212 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.0314 0.0180 0.0179 U

0.01404 Bismuth 214 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.0251 0.0349 0.0349 U

-0.006510 Lead 212 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.0339 0.0102 0.0102 U

0.001975 Lead 214 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.297 0.171 0.171 U

-0.02397 Potassium 40 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.326 0.179 0.178 U

0.02778 Protactinium 231 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.0314 1.00 0.0180 0.0179 U

0.01404 Radium 226 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.314 1.00 0.453 0.453 U

-0.07931 Thorium 234 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.0573 0.0339 0.0338 U

0.01905 Uranium 235 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.953 0.366 0.366 U

0.0000 Protactinium 234m 1

08/28/13 20:18 08/28/13 13:20 pCi/g 0.0472 0.0230 0.0229 U

0.009657 Thorium 232 Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 08/28/13 13:20 08/28/13 20:18 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-69129/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 69118 Prep Batch: 69129 Americium 241 Analyte 116 87 93 90.80 97.7 9.45 0.490 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 31.7 30.37 3.18 0.200 0.137 pCi/g 96 87 - 120 Cobalt 60 24.8 23.37 2.36 0.0980 pCi/g 94 87 - 115 Client Sample ID: L050331PUB00 Lab Sample ID: 160-3482-32 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 69583 Prep Batch: 69129 Actinium 228 Analyte 1

0.06 1.094 1.07 0.178 0.103 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Americium 241 0.0558 U

-0.08660 U

0.152 0.251 pCi/g 0.49 1

Bismuth 212 0.890 1.150 0.473 0.465 pCi/g 0.29 1

Bismuth 214 0.930 0.8241 0.138 0.0881 pCi/g 0.37 1

Lead 212 1.03 1.114 0.164 0.0683 pCi/g 0.26 1

Lead 214 0.955 1.014 0.147 0.0763 pCi/g 0.20 1

Potassium 40 20.2 19.38 2.32 0.378 pCi/g 0.16 1

Protactinium 231 0.337 U

0.5302 U

0.352 1.36 pCi/g 0.29 1

Radium 226 0.930 0.8241 0.138 1.00 0.0881 pCi/g 0.37 1

Thorium 234 59.8 63.13 6.96 1.00 1.90 pCi/g 0.24 1

Uranium 235 3.05 2.915 0.440 0.330 pCi/g 0.15 1

Protactinium 234m 73.7 62.73 9.51 3.35 pCi/g 0.53 1

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QC Sample Results TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: L050331PUB00 Lab Sample ID: 160-3482-32 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 69583 Prep Batch: 69129 Thorium 232 Analyte 1

0.06 1.094 1.07 0.178 0.103 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER TestAmerica St. Louis Page 43 of 50 1

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QC Association Summary TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Metals Prep Batch: 68378 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3482-1 L050301PRS00 Total/NA Solid None 160-3482-1 MS L050301PRS00 Total/NA Solid None 160-3482-1 MSD L050301PRS00 Total/NA Solid None 160-3482-2 L050302PES00 Total/NA Solid None 160-3482-3 L050303PRS00 Total/NA Solid None 160-3482-4 L050304PEQ00 Total/NA Solid None 160-3482-5 L050304PES00 Total/NA Solid None 160-3482-6 L050305PRS00 Total/NA Solid None 160-3482-7 L050306PES00 Total/NA Solid None 160-3482-8 L050307PRS00 Total/NA Solid None 160-3482-9 L050308PES00 Total/NA Solid None 160-3482-10 L050309PRS00 Total/NA Solid None 160-3482-11 L050310PES00 Total/NA Solid None 160-3482-12 L050311PRS00 Total/NA Solid None 160-3482-13 L050312PES00 Total/NA Solid None 160-3482-14 L050313PRS00 Total/NA Solid None 160-3482-15 L050314PES00 Total/NA Solid None 160-3482-16 L050315PRS00 Total/NA Solid None 160-3482-17 L050316PES00 Total/NA Solid None 160-3482-18 L050317PRS00 Total/NA Solid None 160-3482-19 L050318PES00 Total/NA Solid None 160-3482-20 L050319PRS00 Total/NA Solid None LCS 160-68378/2-A Lab Control Sample Total/NA Solid None MB 160-68378/1-A Method Blank Total/NA Prep Batch: 68379 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3482-21 L050320PES00 Total/NA Solid None 160-3482-21 MS L050320PES00 Total/NA Solid None 160-3482-21 MSD L050320PES00 Total/NA Solid None 160-3482-22 L050321PRS00 Total/NA Solid None 160-3482-23 L050322PES00 Total/NA Solid None 160-3482-24 L050323PUB00 Total/NA Solid None 160-3482-25 L050324PUB00 Total/NA Solid None 160-3482-26 L050325PUB00 Total/NA Solid None 160-3482-27 L050326PUB00 Total/NA Solid None 160-3482-28 L050327PUB00 Total/NA Solid None 160-3482-29 L050328PUB00 Total/NA Solid None 160-3482-30 L050329PUB00 Total/NA Solid None 160-3482-31 L050330PUB00 Total/NA Solid None 160-3482-32 L050331PUB00 Total/NA Solid None 160-3482-33 L050332PUB00 Total/NA Solid None LCS 160-68379/2-A Lab Control Sample Total/NA Solid None MB 160-68379/1-A Method Blank Total/NA Analysis Batch: 68965 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 68378 160-3482-1 L050301PRS00 Total/NA Solid 6020A 68378 160-3482-1 MS L050301PRS00 Total/NA Solid 6020A 68378 160-3482-1 MSD L050301PRS00 Total/NA Solid 6020A 68378 160-3482-2 L050302PES00 Total/NA TestAmerica St. Louis Page 44 of 50 1

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QC Association Summary TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Metals (Continued)

Analysis Batch: 68965 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 68378 160-3482-3 L050303PRS00 Total/NA Solid 6020A 68378 160-3482-4 L050304PEQ00 Total/NA Solid 6020A 68378 160-3482-5 L050304PES00 Total/NA Solid 6020A 68378 160-3482-6 L050305PRS00 Total/NA Solid 6020A 68378 160-3482-7 L050306PES00 Total/NA Solid 6020A 68378 160-3482-8 L050307PRS00 Total/NA Solid 6020A 68378 160-3482-9 L050308PES00 Total/NA Solid 6020A 68378 160-3482-10 L050309PRS00 Total/NA Solid 6020A 68378 160-3482-11 L050310PES00 Total/NA Solid 6020A 68378 160-3482-12 L050311PRS00 Total/NA Solid 6020A 68378 160-3482-13 L050312PES00 Total/NA Solid 6020A 68378 160-3482-14 L050313PRS00 Total/NA Solid 6020A 68378 160-3482-15 L050314PES00 Total/NA Solid 6020A 68378 160-3482-16 L050315PRS00 Total/NA Solid 6020A 68378 160-3482-17 L050316PES00 Total/NA Solid 6020A 68378 160-3482-18 L050317PRS00 Total/NA Solid 6020A 68378 160-3482-19 L050318PES00 Total/NA Solid 6020A 68378 160-3482-20 L050319PRS00 Total/NA Solid 6020A 68379 160-3482-21 L050320PES00 Total/NA Solid 6020A 68379 160-3482-21 MS L050320PES00 Total/NA Solid 6020A 68379 160-3482-21 MSD L050320PES00 Total/NA Solid 6020A 68379 160-3482-22 L050321PRS00 Total/NA Solid 6020A 68379 160-3482-23 L050322PES00 Total/NA Solid 6020A 68379 160-3482-24 L050323PUB00 Total/NA Solid 6020A 68379 160-3482-25 L050324PUB00 Total/NA Solid 6020A 68379 160-3482-26 L050325PUB00 Total/NA Solid 6020A 68379 160-3482-27 L050326PUB00 Total/NA Solid 6020A 68379 160-3482-28 L050327PUB00 Total/NA Solid 6020A 68379 160-3482-29 L050328PUB00 Total/NA Solid 6020A 68379 160-3482-30 L050329PUB00 Total/NA Solid 6020A 68379 160-3482-31 L050330PUB00 Total/NA Solid 6020A 68379 160-3482-32 L050331PUB00 Total/NA Solid 6020A 68379 160-3482-33 L050332PUB00 Total/NA Solid 6020A 68378 LCS 160-68378/2-A Lab Control Sample Total/NA Solid 6020A 68379 LCS 160-68379/2-A Lab Control Sample Total/NA Solid 6020A 68378 MB 160-68378/1-A Method Blank Total/NA Solid 6020A 68379 MB 160-68379/1-A Method Blank Total/NA General Chemistry Analysis Batch: 68400 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3482-1 L050301PRS00 Total/NA Solid Moisture 160-3482-1 DU L050301PRS00 Total/NA Solid Moisture 160-3482-2 L050302PES00 Total/NA Solid Moisture 160-3482-3 L050303PRS00 Total/NA Solid Moisture 160-3482-4 L050304PEQ00 Total/NA Solid Moisture 160-3482-5 L050304PES00 Total/NA Solid Moisture 160-3482-6 L050305PRS00 Total/NA Solid Moisture 160-3482-7 L050306PES00 Total/NA TestAmerica St. Louis Page 45 of 50 1

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QC Association Summary TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

General Chemistry (Continued)

Analysis Batch: 68400 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3482-8 L050307PRS00 Total/NA Solid Moisture 160-3482-9 L050308PES00 Total/NA Solid Moisture 160-3482-10 L050309PRS00 Total/NA Solid Moisture 160-3482-11 L050310PES00 Total/NA Solid Moisture 160-3482-12 L050311PRS00 Total/NA Solid Moisture 160-3482-13 L050312PES00 Total/NA Solid Moisture 160-3482-14 L050313PRS00 Total/NA Solid Moisture 160-3482-15 L050314PES00 Total/NA Solid Moisture 160-3482-16 L050315PRS00 Total/NA Solid Moisture 160-3482-17 L050316PES00 Total/NA Solid Moisture 160-3482-18 L050317PRS00 Total/NA Solid Moisture 160-3482-19 L050318PES00 Total/NA Solid Moisture 160-3482-20 L050319PRS00 Total/NA Solid Moisture 160-3482-21 L050320PES00 Total/NA Solid Moisture 160-3482-22 L050321PRS00 Total/NA Solid Moisture 160-3482-23 L050322PES00 Total/NA Solid Moisture 160-3482-24 L050323PUB00 Total/NA Solid Moisture 160-3482-25 L050324PUB00 Total/NA Solid Moisture 160-3482-26 L050325PUB00 Total/NA Solid Moisture 160-3482-27 L050326PUB00 Total/NA Solid Moisture 160-3482-28 L050327PUB00 Total/NA Solid Moisture 160-3482-29 L050328PUB00 Total/NA Solid Moisture 160-3482-30 L050329PUB00 Total/NA Solid Moisture 160-3482-31 L050330PUB00 Total/NA Solid Moisture 160-3482-32 L050331PUB00 Total/NA Solid Moisture 160-3482-33 L050332PUB00 Total/NA Solid Moisture 160-3482-33 DU L050332PUB00 Total/NA Rad Prep Batch: 68378 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3482-1 L050301PRS00 Total/NA Solid None 160-3482-1 MS L050301PRS00 Total/NA Solid None 160-3482-1 MSD L050301PRS00 Total/NA Solid None 160-3482-2 L050302PES00 Total/NA Solid None 160-3482-3 L050303PRS00 Total/NA Solid None 160-3482-4 L050304PEQ00 Total/NA Solid None 160-3482-5 L050304PES00 Total/NA Solid None 160-3482-6 L050305PRS00 Total/NA Solid None 160-3482-7 L050306PES00 Total/NA Solid None 160-3482-8 L050307PRS00 Total/NA Solid None 160-3482-9 L050308PES00 Total/NA Solid None 160-3482-10 L050309PRS00 Total/NA Solid None 160-3482-11 L050310PES00 Total/NA Solid None 160-3482-12 L050311PRS00 Total/NA Solid None 160-3482-13 L050312PES00 Total/NA Solid None 160-3482-14 L050313PRS00 Total/NA Solid None 160-3482-15 L050314PES00 Total/NA Solid None 160-3482-16 L050315PRS00 Total/NA TestAmerica St. Louis Page 46 of 50 1

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QC Association Summary TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Rad (Continued)

Prep Batch: 68378 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3482-17 L050316PES00 Total/NA Solid None 160-3482-18 L050317PRS00 Total/NA Solid None 160-3482-19 L050318PES00 Total/NA Solid None 160-3482-20 L050319PRS00 Total/NA Solid None LCS 160-68378/2-A Lab Control Sample Total/NA Solid None MB 160-68378/1-A Method Blank Total/NA Prep Batch: 68379 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3482-21 L050320PES00 Total/NA Solid None 160-3482-21 MS L050320PES00 Total/NA Solid None 160-3482-21 MSD L050320PES00 Total/NA Solid None 160-3482-22 L050321PRS00 Total/NA Solid None 160-3482-23 L050322PES00 Total/NA Solid None 160-3482-24 L050323PUB00 Total/NA Solid None 160-3482-25 L050324PUB00 Total/NA Solid None 160-3482-26 L050325PUB00 Total/NA Solid None 160-3482-27 L050326PUB00 Total/NA Solid None 160-3482-28 L050327PUB00 Total/NA Solid None 160-3482-29 L050328PUB00 Total/NA Solid None 160-3482-30 L050329PUB00 Total/NA Solid None 160-3482-31 L050330PUB00 Total/NA Solid None 160-3482-32 L050331PUB00 Total/NA Solid None 160-3482-33 L050332PUB00 Total/NA Solid None LCS 160-68379/2-A Lab Control Sample Total/NA Solid None MB 160-68379/1-A Method Blank Total/NA Leach Batch: 68380 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3482-1 L050301PRS00 Total/NA Solid Dry and Grind 160-3482-2 L050302PES00 Total/NA Solid Dry and Grind 160-3482-3 L050303PRS00 Total/NA Solid Dry and Grind 160-3482-4 L050304PEQ00 Total/NA Solid Dry and Grind 160-3482-5 L050304PES00 Total/NA Solid Dry and Grind 160-3482-6 L050305PRS00 Total/NA Solid Dry and Grind 160-3482-7 L050306PES00 Total/NA Solid Dry and Grind 160-3482-8 L050307PRS00 Total/NA Solid Dry and Grind 160-3482-9 L050308PES00 Total/NA Solid Dry and Grind 160-3482-10 L050309PRS00 Total/NA Solid Dry and Grind 160-3482-11 L050310PES00 Total/NA Solid Dry and Grind 160-3482-12 L050311PRS00 Total/NA Solid Dry and Grind 160-3482-13 L050312PES00 Total/NA Solid Dry and Grind 160-3482-14 L050313PRS00 Total/NA Solid Dry and Grind 160-3482-15 L050314PES00 Total/NA Solid Dry and Grind 160-3482-16 L050315PRS00 Total/NA Solid Dry and Grind 160-3482-17 L050316PES00 Total/NA Solid Dry and Grind 160-3482-18 L050317PRS00 Total/NA Solid Dry and Grind 160-3482-19 L050318PES00 Total/NA Solid Dry and Grind 160-3482-19 DU L050318PES00 Total/NA Solid Dry and Grind 160-3482-20 L050319PRS00 Total/NA Solid Dry and Grind 160-3482-21 L050320PES00 Total/NA TestAmerica St. Louis Page 47 of 50 1

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QC Association Summary TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Rad (Continued)

Leach Batch: 68380 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3482-22 L050321PRS00 Total/NA Solid Dry and Grind 160-3482-23 L050322PES00 Total/NA Solid Dry and Grind 160-3482-24 L050323PUB00 Total/NA Solid Dry and Grind 160-3482-25 L050324PUB00 Total/NA Solid Dry and Grind 160-3482-26 L050325PUB00 Total/NA Solid Dry and Grind 160-3482-27 L050326PUB00 Total/NA Solid Dry and Grind 160-3482-28 L050327PUB00 Total/NA Solid Dry and Grind 160-3482-29 L050328PUB00 Total/NA Solid Dry and Grind 160-3482-30 L050329PUB00 Total/NA Solid Dry and Grind 160-3482-31 L050330PUB00 Total/NA Solid Dry and Grind 160-3482-32 L050331PUB00 Total/NA Solid Dry and Grind 160-3482-32 DU L050331PUB00 Total/NA Solid Dry and Grind 160-3482-33 L050332PUB00 Total/NA Prep Batch: 69096 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 68380 160-3482-1 L050301PRS00 Total/NA Solid Fill_Geo-0 68380 160-3482-2 L050302PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-3 L050303PRS00 Total/NA Solid Fill_Geo-0 68380 160-3482-4 L050304PEQ00 Total/NA Solid Fill_Geo-0 68380 160-3482-5 L050304PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-6 L050305PRS00 Total/NA Solid Fill_Geo-0 68380 160-3482-7 L050306PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-8 L050307PRS00 Total/NA Solid Fill_Geo-0 68380 160-3482-9 L050308PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-10 L050309PRS00 Total/NA Solid Fill_Geo-0 68380 160-3482-11 L050310PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-12 L050311PRS00 Total/NA Solid Fill_Geo-0 68380 160-3482-13 L050312PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-14 L050313PRS00 Total/NA Solid Fill_Geo-0 68380 160-3482-15 L050314PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-16 L050315PRS00 Total/NA Solid Fill_Geo-0 68380 160-3482-17 L050316PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-18 L050317PRS00 Total/NA Solid Fill_Geo-0 68380 160-3482-19 L050318PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-19 DU L050318PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-20 L050319PRS00 Total/NA Solid Fill_Geo-0 LCS 160-69096/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-69096/1-A Method Blank Total/NA Prep Batch: 69129 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 68380 160-3482-21 L050320PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-22 L050321PRS00 Total/NA Solid Fill_Geo-0 68380 160-3482-23 L050322PES00 Total/NA Solid Fill_Geo-0 68380 160-3482-24 L050323PUB00 Total/NA Solid Fill_Geo-0 68380 160-3482-25 L050324PUB00 Total/NA Solid Fill_Geo-0 68380 160-3482-26 L050325PUB00 Total/NA Solid Fill_Geo-0 68380 160-3482-27 L050326PUB00 Total/NA Solid Fill_Geo-0 68380 160-3482-28 L050327PUB00 Total/NA Solid Fill_Geo-0 68380 160-3482-29 L050328PUB00 Total/NA TestAmerica St. Louis Page 48 of 50 1

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QC Association Summary TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Rad (Continued)

Prep Batch: 69129 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 68380 160-3482-30 L050329PUB00 Total/NA Solid Fill_Geo-0 68380 160-3482-31 L050330PUB00 Total/NA Solid Fill_Geo-0 68380 160-3482-32 L050331PUB00 Total/NA Solid Fill_Geo-0 68380 160-3482-32 DU L050331PUB00 Total/NA Solid Fill_Geo-0 68380 160-3482-33 L050332PUB00 Total/NA Solid Fill_Geo-0 LCS 160-69129/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-69129/1-A Method Blank Total/NA TestAmerica St. Louis Page 49 of 50 1

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Tracer/Carrier Summary TestAmerica Job ID: 160-3482-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)

Re 86 160-3482-1 Percent Yield (Acceptance Limits)

L050301PRS00 87 160-3482-1 MS L050301PRS00 87 160-3482-1 MSD L050301PRS00 87 160-3482-2 L050302PES00 88 160-3482-3 L050303PRS00 85 160-3482-4 L050304PEQ00 81 160-3482-5 L050304PES00 86 160-3482-6 L050305PRS00 87 160-3482-7 L050306PES00 82 160-3482-8 L050307PRS00 86 160-3482-9 L050308PES00 86 160-3482-10 L050309PRS00 89 160-3482-11 L050310PES00 81 160-3482-12 L050311PRS00 84 160-3482-13 L050312PES00 83 160-3482-14 L050313PRS00 82 160-3482-15 L050314PES00 81 160-3482-16 L050315PRS00 90 160-3482-17 L050316PES00 85 160-3482-18 L050317PRS00 87 160-3482-19 L050318PES00 91 160-3482-20 L050319PRS00 88 160-3482-21 L050320PES00 88 160-3482-21 MS L050320PES00 88 160-3482-21 MSD L050320PES00 86 160-3482-22 L050321PRS00 89 160-3482-23 L050322PES00 88 160-3482-24 L050323PUB00 87 160-3482-25 L050324PUB00 83 160-3482-26 L050325PUB00 90 160-3482-27 L050326PUB00 85 160-3482-28 L050327PUB00 87 160-3482-29 L050328PUB00 84 160-3482-30 L050329PUB00 86 160-3482-31 L050330PUB00 87 160-3482-32 L050331PUB00 84 160-3482-33 L050332PUB00 95 LCS 160-68378/2-A Lab Control Sample 96 LCS 160-68379/2-A Lab Control Sample 95 MB 160-68378/1-A Method Blank 95 MB 160-68379/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 50 of 50 1

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ML18019A702

Text

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References:

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