ML18019A685
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3585-1 Client Project/Site: RFP-CBA-022 (7 DAY TAT)
For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:
9/9/2013 4:47:39 PM Ivan Vania, Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-3585-1 Page 2 of 27 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
7 Definitions/Glossary.......................................
8 Method Summary.........................................
9 Sample Summary.........................................
10 Client Sample Results......................................
11 QC Sample Results........................................
21 QC Association Summary...................................
24 Tracer Carrier Summary....................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3585-1 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3585-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)
Report Number: 160-3585-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 08/30/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 20.0 C.
TECHNETIUM-99 (ICPMS)
Samples L0501100TUB0 (160-3585-1), L0501101TUB0 (160-3585-2), L0501102TUB0 (160-3585-3), L0501103TUB0 (160-3585-4),
L0501104TUB0 (160-3585-5), L0501105TUB0 (160-3585-6), L0501106TUB0 (160-3585-7), L0501107TUB0 (160-3585-8),
L0501108TUB0 (160-3585-9), L050198TUB00 (160-3585-10), L050199TUB00 (160-3585-11), L050146TSS00 (160-3585-12) and L050147TRS00 (160-3585-13) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 09/03/2013 and analyzed on 09/04/2013.
No difficulties were encountered during the Tc-99 analysis. All quality control parameters were within the acceptance limits.
PERCENT SOLIDS Samples L0501100TUB0 (160-3585-1), L0501101TUB0 (160-3585-2), L0501102TUB0 (160-3585-3), L0501103TUB0 (160-3585-4),
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3585-1 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3585-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
L0501104TUB0 (160-3585-5), L0501105TUB0 (160-3585-6), L0501106TUB0 (160-3585-7), L0501107TUB0 (160-3585-8),
L0501108TUB0 (160-3585-9), L050198TUB00 (160-3585-10), L050199TUB00 (160-3585-11), L050146TSS00 (160-3585-12) and L050147TRS00 (160-3585-13) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 09/03/2013.
No difficulties were encountered during the % solids analysis. All quality control parameters were within the acceptance limits.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L0501100TUB0 (160-3585-1), L0501101TUB0 (160-3585-2), L0501102TUB0 (160-3585-3), L0501103TUB0 (160-3585-4),
L0501104TUB0 (160-3585-5), L0501105TUB0 (160-3585-6), L0501106TUB0 (160-3585-7), L0501107TUB0 (160-3585-8),
L0501108TUB0 (160-3585-9), L050198TUB00 (160-3585-10), L050199TUB00 (160-3585-11), L050146TSS00 (160-3585-12) and L050147TRS00 (160-3585-13) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 09/03/2013, and prepared and analyzed on 09/05/2013.
Preparation Batch 70772:
Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of bismuth-214.
Because the samples have not had a 21-day ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. (160-3585-13 DU), (LCS 160-70772/2-A), (MB 160-70772/1-A), L0501100TUB0 (160-3585-1), L0501101TUB0 (160-3585-2), L0501102TUB0 (160-3585-3), L0501103TUB0 (160-3585-4), L0501104TUB0 (160-3585-5), L0501105TUB0 (160-3585-6),
L0501106TUB0 (160-3585-7), L0501107TUB0 (160-3585-8), L0501108TUB0 (160-3585-9), L050146TSS00 (160-3585-12),
L050147TRS00 (160-3585-13), L050198TUB00 (160-3585-10), L050199TUB00 (160-3585-11)
The reporting limit for thorium-234 was not met due to insufficient sample weight available for analysis. Analytical results are reported with the MDC achieved. L0501101TUB0 (160-3585-2), L0501103TUB0 (160-3585-4), L0501108TUB0 (160-3585-9), L050199TUB00 (160-3585-11)
No other difficulties were encountered during the Gamma spec analysis. All other quality control parameters were within the acceptance limits.
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,Procedure BDP-PR-QA-006, Chain of Custody Pagel ofl Hematite Decommissioning Project !Revision: 3 I
I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to BDP.
Chain of Cutod ID No_
F-083013-01 Pae 1/1 Project Name:
Westinghouse Electric Company Contact Person:
Gerald Rood
-~
Phone Number:
314-810-3382
. ' \\ *;:.
Sampler Name
<<l JeffHo:ffman; Scott Jenkins 8
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L0501100TUBO 8/29/2013 13:15 s
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L050I 102TUBO 8/29/2013 13:45 s
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L0501103TUBO 8/29/2013 14:00 s
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L0501104TUBO 8/29/2013 13:00 s
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LOSO l 105TUBO 8/29/2013 13:15 s
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L0501106TUBO 8/29/2013 13:25 s
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L050 l 107TUBO 8/29/2013 13:40 s
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7,(.~e Relinquished J:,y: ---
Date/Time
&/30/!3 Company Name:,, t;L.-
Date/Time
[pi°?J n*, 10 Relinquished by:
Date/Time Received by:
Date/Time Company Name:
Company Name:
Laboratorv Name:
TA-MO
,Laboratory Address:
13715 Rider Trail North
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"' *.s Phone No.
"' 314-298-8566 0 u
-a Laboratory Contact Person:
0 Joe Walker E-<
Phone No.
708-870-8453 Turn Around Time Rush (7 days)
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Shipper and Number:
Comments: Please re-analyze samples after 21-day ingrowth period.
V eri.fied By:
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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Page 1 of 1 Hematite Decommissioning Project !Revision: 3 I
I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006*1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign 1he CoC. The Labonrtory/End User must verify that 1he sample is correctly identified before 1he sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutody ID No. I F-083013-02 Page Project Name:
Westinghouse Electric Company Contact Person:
Gerald Rood Phone Number:
314-81{)-3_3 82 Sampler Name Thomas Yardy Sample JD L050146TSSOO L050147TRS00 Relinquished by;,
Company Namelc.) pl.,
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Compan~:
Relinquished by:
Company Name:
Date Time 8/30/2013 8:10 8/30/2013 8:30 Date/Time g/y;/13 Date/Time
<:g/-;;0//3 J )~,o Date/Time 1/1
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Date/Time 12.4>
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Date/Time g,30(\\~
Date/Time Total Laboratory Name:
TA-MO Laboratory Address:
13715 Rider Trail North t ct---------------------i
- .s Phone No.
C 8 314-298-8566 "El Laboratory Contact Person:
~ Joe Walker Phone No.
708-870-8_453 Rush Turn Around Tune (7 days)
Remarks DS'-D3 0YD3 Cooler Temperature:
Cooler ID: I Shipper and Number:
Comments: Please re-analyze samples after 21-day ingrowth period.
Verified By: c
Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3585-1 Login Number: 3585 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
False Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Qualifiers Metals Qualifier Description J
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier Rad Qualifier Description U
Indicates the analyte was analyzed for but not detected.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 27 1
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Sample Summary TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-3585-1 L0501100TUB0 Solid 08/29/13 13:15 08/30/13 18:00 160-3585-2 L0501101TUB0 Solid 08/29/13 13:30 08/30/13 18:00 160-3585-3 L0501102TUB0 Solid 08/29/13 13:45 08/30/13 18:00 160-3585-4 L0501103TUB0 Solid 08/29/13 14:00 08/30/13 18:00 160-3585-5 L0501104TUB0 Solid 08/29/13 13:00 08/30/13 18:00 160-3585-6 L0501105TUB0 Solid 08/29/13 13:15 08/30/13 18:00 160-3585-7 L0501106TUB0 Solid 08/29/13 13:25 08/30/13 18:00 160-3585-8 L0501107TUB0 Solid 08/29/13 13:40 08/30/13 18:00 160-3585-9 L0501108TUB0 Solid 08/29/13 18:00 08/30/13 18:00 160-3585-10 L050198TUB00 Solid 08/29/13 11:20 08/30/13 18:00 160-3585-11 L050199TUB00 Solid 08/29/13 13:00 08/30/13 18:00 160-3585-12 L050146TSS00 Solid 08/30/13 08:10 08/30/13 18:00 160-3585-13 L050147TRS00 Solid 08/30/13 08:30 08/30/13 18:00 TestAmerica St. Louis Page 10 of 27 1
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Client Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-1 Client Sample ID: L0501100TUB0 Matrix: Solid Date Collected: 08/29/13 13:15 Percent Solids: 96.8 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000058 0.000017 mg/Kg
09/03/13 10:58 09/04/13 17:48 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.217 (2+/-)
0.0621 (2+/-)
1 09/04/13 17:48 09/03/13 10:58 pCi/g 0.199 1.16 RL MDC 0.0509 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 17:48 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.301 (2+/-)
0.0760 (2+/-)
1 09/05/13 22:28 09/05/13 11:17 pCi/g 0.0577 RL MDC 0.0696 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0641 0.0371 0.0371 U
0.00962 Americium 241 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.395 0.276 0.272 0.426 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0354 0.0720 0.0611 0.367 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0459 0.0634 0.0468 0.331 Lead 212 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0625 0.0792 0.0705 0.347 Lead 214 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.288 1.09 0.809 7.08 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.689 0.333 0.330 U
0.354 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0354 1.00 0.0720 0.0611 0.367 Radium 226 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.496 1.00 0.367 0.355 0.877 Thorium 234 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.152 0.0946 0.0940 U
0.101 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 22:28 1
5.23 2.86 2.86 U
0.165 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0577 0.0760 0.0696 0.301 Thorium 232 Tl-208 0.0929 0.0280 0.0296 0.0266 pCi/g 09/05/13 11:17 09/05/13 22:28 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3585-2 Client Sample ID: L0501101TUB0 Matrix: Solid Date Collected: 08/29/13 13:30 Percent Solids: 92.2 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000081 0.000062 0.000019 mg/Kg
09/03/13 10:58 09/04/13 17:59 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.39 (2+/-)
0.231 (2+/-)
1 09/04/13 17:59 09/03/13 10:58 pCi/g 0.214 1.25 RL MDC 0.155 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 17:59 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 TestAmerica St. Louis Page 11 of 27 1
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Client Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-2 Client Sample ID: L0501101TUB0 Matrix: Solid Date Collected: 08/29/13 13:30 Date Received: 08/30/13 18:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.740 (2+/-)
0.233 (2+/-)
1 09/05/13 21:08 09/05/13 11:17 pCi/g 0.335 RL MDC 0.220 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 21:08 1
0.245 0.152 0.152 U
0.0522 Americium 241 pCi/g 09/05/13 11:17 09/05/13 21:08 1
1.31 0.812 0.809 U
0.734 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 21:08 1
0.171 0.224 0.202 0.923 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 21:08 1
0.175 0.259 0.154 0.966 Lead 212 pCi/g 09/05/13 11:17 09/05/13 21:08 1
0.190 0.208 0.171 0.895 Lead 214 pCi/g 09/05/13 11:17 09/05/13 21:08 1
1.03 2.95 2.18 19.4 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 21:08 1
2.57 1.49 1.49 U
-0.499 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 21:08 1
0.171 1.00 0.224 0.202 0.923 Radium 226 pCi/g 09/05/13 11:17 09/05/13 21:08 1
2.59 1.00 1.17 1.14 U
2.43 Thorium 234 pCi/g 09/05/13 11:17 09/05/13 21:08 1
0.637 0.377 0.377 U
0.221 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 21:08 1
11.5 7.26 7.26 U
3.13 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 21:08 1
0.335 0.233 0.220 0.740 Thorium 232 Tl-208 0.393 0.105 0.113 0.0893 pCi/g 09/05/13 11:17 09/05/13 21:08 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3585-3 Client Sample ID: L0501102TUB0 Matrix: Solid Date Collected: 08/29/13 13:45 Percent Solids: 91.6 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000058 0.000017 mg/Kg
09/03/13 10:58 09/04/13 18:03 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0498 U
(2+/-)
0.0319 (2+/-)
1 09/04/13 18:03 09/03/13 10:58 pCi/g 0.197 1.15 RL MDC 0.0301 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 18:03 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 95 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.404 (2+/-)
0.0941 (2+/-)
1 09/05/13 22:27 09/05/13 11:17 pCi/g 0.0487 RL MDC 0.0846 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 22:27 1
0.0774 0.0452 0.0452 U
0.00588 Americium 241 pCi/g 09/05/13 11:17 09/05/13 22:27 1
0.521 0.282 0.282 U
0.00251 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 22:27 1
0.0450 0.0754 0.0660 0.351 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 22:27 1
0.0574 0.0661 0.0583 0.240 Lead 212 pCi/g 09/05/13 11:17 09/05/13 22:27 1
0.0459 0.0556 0.0468 0.288 Lead 214 pCi/g 09/05/13 11:17 09/05/13 22:27 1
0.335 1.17 0.906 7.30 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 22:27 1
0.783 0.197 0.197 U
0.104 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 22:27 1
0.0450 1.00 0.0754 0.0660 0.351 Radium 226 TestAmerica St. Louis Page 12 of 27 1
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Client Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-3 Client Sample ID: L0501102TUB0 Matrix: Solid Date Collected: 08/29/13 13:45 Date Received: 08/30/13 18:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 0.874 (2+/-)
0.576 (2+/-)
1 09/05/13 22:27 09/05/13 11:17 pCi/g 0.684 1.00 RL MDC 0.569 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 22:27 1
0.163 0.0943 0.0938 U
0.102 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 22:27 1
4.69 2.53 2.53 U
0.482 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 22:27 1
0.0487 0.0941 0.0846 0.404 Thorium 232 Tl-208 0.105 0.0289 0.0309 0.0248 pCi/g 09/05/13 11:17 09/05/13 22:27 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3585-4 Client Sample ID: L0501103TUB0 Matrix: Solid Date Collected: 08/29/13 14:00 Percent Solids: 96.2 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0027 0.000058 0.000017 mg/Kg
09/03/13 10:58 09/04/13 18:07 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 46.8 (2+/-)
4.77 (2+/-)
1 09/04/13 18:07 09/03/13 10:58 pCi/g 0.197 1.15 RL MDC 0.555 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 18:07 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.273 U
(2+/-)
0.274 (2+/-)
1 09/05/13 21:34 09/05/13 11:17 pCi/g 0.561 RL MDC 0.273 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 21:34 1
0.329 0.191 0.191 U
0.0544 Americium 241 pCi/g 09/05/13 11:17 09/05/13 21:34 1
1.99 1.08 1.08 U
0.246 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 21:34 1
0.319 0.268 0.263 0.495 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 21:34 1
0.198 0.155 0.146 0.392 Lead 212 pCi/g 09/05/13 11:17 09/05/13 21:34 1
0.191 0.234 0.223 0.696 Lead 214 pCi/g 09/05/13 11:17 09/05/13 21:34 1
2.05 1.53 1.50 2.81 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 21:34 1
2.97 0.714 0.714 U
0.116 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 21:34 1
0.319 1.00 0.268 0.263 0.495 Radium 226 pCi/g 09/05/13 11:17 09/05/13 21:34 1
2.74 1.00 1.13 1.09 2.75 Thorium 234 pCi/g 09/05/13 11:17 09/05/13 21:34 1
0.497 0.393 0.381 0.929 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 21:34 1
21.7 11.6 11.6 U
-2.23 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 21:34 1
0.561 0.274 0.273 U
0.273 Thorium 232 Other Detected Radionuclide None pCi/g 09/05/13 11:17 09/05/13 21:34 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-5 Client Sample ID: L0501104TUB0 Matrix: Solid Date Collected: 08/29/13 13:00 Percent Solids: 93.2 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00099 0.000058 0.000017 mg/Kg
09/03/13 10:58 09/04/13 18:11 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 16.9 (2+/-)
1.73 (2+/-)
1 09/04/13 18:11 09/03/13 10:58 pCi/g 0.199 1.16 RL MDC 0.341 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 18:11 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.315 (2+/-)
0.0633 (2+/-)
1 09/05/13 22:28 09/05/13 11:17 pCi/g 0.0355 RL MDC 0.0546 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0509 0.0304 0.0304 U
0.0132 Americium 241 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.250 0.156 0.155 U
0.146 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0304 0.0658 0.0501 0.411 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0342 0.0480 0.0330 0.270 Lead 212 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0405 0.0701 0.0538 0.432 Lead 214 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.205 0.770 0.526 5.49 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.466 0.178 0.177 U
0.0795 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0304 1.00 0.0658 0.0501 0.411 Radium 226 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.504 1.00 0.427 0.416 0.912 Thorium 234 pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.103 0.0813 0.0789 0.190 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 22:28 1
2.75 1.61 1.60 U
1.61 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 22:28 1
0.0355 0.0633 0.0546 0.315 Thorium 232 Tl-208 0.115 0.0186 0.0221 0.0114 pCi/g 09/05/13 11:17 09/05/13 22:28 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3585-6 Client Sample ID: L0501105TUB0 Matrix: Solid Date Collected: 08/29/13 13:15 Percent Solids: 64.5 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0034 0.000091 0.000027 mg/Kg
09/03/13 10:58 09/04/13 18:23 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 58.4 (2+/-)
6.49 (2+/-)
1 09/04/13 18:23 09/03/13 10:58 pCi/g 0.311 1.82 RL MDC 1.22 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 18:23 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 85 TestAmerica St. Louis Page 14 of 27 1
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Client Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-6 Client Sample ID: L0501105TUB0 Matrix: Solid Date Collected: 08/29/13 13:15 Date Received: 08/30/13 18:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.671 (2+/-)
0.132 (2+/-)
1 09/05/13 22:25 09/05/13 11:17 pCi/g 0.101 RL MDC 0.113 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 22:25 1
0.104 0.0616 0.0616 U
0.000192 Americium 241 pCi/g 09/05/13 11:17 09/05/13 22:25 1
0.243 0.333 0.317 0.979 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 22:25 1
0.0626 0.108 0.0856 0.629 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 22:25 1
0.0561 0.0990 0.0597 0.611 Lead 212 pCi/g 09/05/13 11:17 09/05/13 22:25 1
0.0647 0.113 0.0767 0.798 Lead 214 pCi/g 09/05/13 11:17 09/05/13 22:25 1
0.325 2.11 1.13 17.4 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 22:25 1
1.03 0.139 0.137 U
0.170 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 22:25 1
0.0626 1.00 0.108 0.0856 0.629 Radium 226 pCi/g 09/05/13 11:17 09/05/13 22:25 1
0.791 1.00 0.353 0.326 1.29 Thorium 234 pCi/g 09/05/13 11:17 09/05/13 22:25 1
0.198 0.165 0.161 0.365 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 22:25 1
4.96 2.75 2.75 U
0.715 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 22:25 1
0.101 0.132 0.113 0.671 Thorium 232 Tl-208 0.204 0.0353 0.0412 0.0277 pCi/g 09/05/13 11:17 09/05/13 22:25 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3585-7 Client Sample ID: L0501106TUB0 Matrix: Solid Date Collected: 08/29/13 13:25 Percent Solids: 95.4 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000087 0.000059 0.000018 mg/Kg
09/03/13 10:58 09/04/13 18:26 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.49 (2+/-)
0.208 (2+/-)
1 09/04/13 18:26 09/03/13 10:58 pCi/g 0.202 1.18 RL MDC 0.124 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 18:26 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.577 (2+/-)
0.166 (2+/-)
1 09/05/13 23:02 09/05/13 11:17 pCi/g 0.189 RL MDC 0.155 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 23:02 1
0.115 0.0685 0.0685 U
0.0193 Americium 241 pCi/g 09/05/13 11:17 09/05/13 23:02 1
0.375 0.528 0.499 1.66 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 23:02 1
0.0922 0.152 0.130 0.761 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 23:02 1
0.0663 0.136 0.0800 0.846 Lead 212 pCi/g 09/05/13 11:17 09/05/13 23:02 1
0.0817 0.133 0.105 0.788 Lead 214 pCi/g 09/05/13 11:17 09/05/13 23:02 1
0.436 2.23 1.47 16.4 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 23:02 1
1.55 0.292 0.288 U
0.462 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 23:02 1
0.0922 1.00 0.152 0.130 0.761 Radium 226 TestAmerica St. Louis Page 15 of 27 1
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Client Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-7 Client Sample ID: L0501106TUB0 Matrix: Solid Date Collected: 08/29/13 13:25 Date Received: 08/30/13 18:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 1.24 (2+/-)
0.405 (2+/-)
1 09/05/13 23:02 09/05/13 11:17 pCi/g 0.998 1.00 RL MDC 0.384 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 23:02 1
0.222 0.157 0.155 0.227 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 23:02 1
7.18 3.96 3.96 U
0.353 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 23:02 1
0.189 0.166 0.155 0.577 Thorium 232 Tl-208 0.331 0.0540 0.0640 0.0353 pCi/g 09/05/13 11:17 09/05/13 23:02 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3585-8 Client Sample ID: L0501107TUB0 Matrix: Solid Date Collected: 08/29/13 13:40 Percent Solids: 98.7 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000040 J
0.000055 0.000017 mg/Kg
09/03/13 10:58 09/04/13 18:30 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.682 (2+/-)
0.129 (2+/-)
1 09/04/13 18:30 09/03/13 10:58 pCi/g 0.190 1.11 RL MDC 0.100 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 18:30 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.152 (2+/-)
0.0473 (2+/-)
1 09/05/13 23:04 09/05/13 11:17 pCi/g 0.0558 RL MDC 0.0447 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0495 0.0291 0.0291 U
0.00153 Americium 241 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.237 0.150 0.149 U
0.159 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0308 0.0698 0.0504 0.464 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0292 0.0295 0.0240 0.133 Lead 212 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0330 0.0724 0.0500 0.504 Lead 214 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.185 0.783 0.499 5.90 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.393 0.208 0.207 U
0.177 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0308 1.00 0.0698 0.0504 0.464 Radium 226 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.381 1.00 0.300 0.290 0.731 Thorium 234 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.117 0.0672 0.0669 U
0.0672 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 23:04 1
2.29 14.1 14.1 U
-0.351 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0558 0.0473 0.0447 0.152 Thorium 232 Tl-208 0.0572 0.0159 0.0170 0.0147 pCi/g 09/05/13 11:17 09/05/13 23:04 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-9 Client Sample ID: L0501108TUB0 Matrix: Solid Date Collected: 08/29/13 18:00 Percent Solids: 95.2 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0019 0.000058 0.000017 mg/Kg
09/03/13 10:58 09/04/13 18:34 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 32.5 (2+/-)
3.32 (2+/-)
1 09/04/13 18:34 09/03/13 10:58 pCi/g 0.198 1.16 RL MDC 0.513 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 18:34 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.176 U
(2+/-)
0.170 (2+/-)
1 09/05/13 23:41 09/05/13 11:17 pCi/g 0.280 RL MDC 0.169 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 23:41 1
0.139 0.0817 0.0817 U
0.0239 Americium 241 pCi/g 09/05/13 11:17 09/05/13 23:41 1
0.907 0.523 0.522 U
0.235 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 23:41 1
0.207 0.186 0.181 0.411 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 23:41 1
0.137 0.107 0.103 0.235 Lead 212 pCi/g 09/05/13 11:17 09/05/13 23:41 1
0.167 0.166 0.153 0.599 Lead 214 pCi/g 09/05/13 11:17 09/05/13 23:41 1
1.28 0.603 0.603 U
0.0987 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 23:41 1
1.84 0.534 0.533 U
0.168 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 23:41 1
0.207 1.00 0.186 0.181 0.411 Radium 226 pCi/g 09/05/13 11:17 09/05/13 23:41 1
1.38 1.00 0.999 0.985 1.56 Thorium 234 pCi/g 09/05/13 11:17 09/05/13 23:41 1
0.343 0.238 0.237 U
0.293 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 23:41 1
9.03 5.26 5.25 U
2.86 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 23:41 1
0.280 0.170 0.169 U
0.176 Thorium 232 Other Detected Radionuclide None pCi/g 09/05/13 11:17 09/05/13 23:41 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3585-10 Client Sample ID: L050198TUB00 Matrix: Solid Date Collected: 08/29/13 11:20 Percent Solids: 85.3 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00022 0.000068 0.000020 mg/Kg
09/03/13 10:58 09/04/13 18:38 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.71 (2+/-)
0.465 (2+/-)
1 09/04/13 18:38 09/03/13 10:58 pCi/g 0.232 1.36 RL MDC 0.217 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 18:38 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 TestAmerica St. Louis Page 17 of 27 1
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Client Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-10 Client Sample ID: L050198TUB00 Matrix: Solid Date Collected: 08/29/13 11:20 Date Received: 08/30/13 18:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.916 (2+/-)
0.152 (2+/-)
1 09/05/13 23:04 09/05/13 11:17 pCi/g 0.105 RL MDC 0.120 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0878 0.249 0.249 U
-0.00622 Americium 241 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.321 0.339 0.325 0.918 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0471 0.107 0.0801 0.678 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0533 0.118 0.0628 0.774 Lead 212 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0722 0.106 0.0767 0.709 Lead 214 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.235 2.16 1.15 17.8 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 23:04 1
1.07 0.653 0.651 U
-0.518 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0471 1.00 0.107 0.0801 0.678 Radium 226 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.656 1.00 0.262 0.252 0.692 Thorium 234 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.180 0.116 0.116 U
0.104 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 23:04 1
5.75 1.81 1.80 U
1.82 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.105 0.152 0.120 0.916 Thorium 232 Tl-208 0.295 0.0410 0.0512 0.0289 pCi/g 09/05/13 11:17 09/05/13 23:04 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3585-11 Client Sample ID: L050199TUB00 Matrix: Solid Date Collected: 08/29/13 13:00 Percent Solids: 92.9 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00010 0.000061 0.000018 mg/Kg
09/03/13 10:58 09/04/13 18:42 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.78 (2+/-)
0.301 (2+/-)
1 09/04/13 18:42 09/03/13 10:58 pCi/g 0.209 1.22 RL MDC 0.210 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 18:42 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.944 (2+/-)
0.230 (2+/-)
1 09/05/13 21:37 09/05/13 11:17 pCi/g 0.126 RL MDC 0.208 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 21:37 1
0.178 0.104 0.104 U
0.00979 Americium 241 pCi/g 09/05/13 11:17 09/05/13 21:37 1
1.11 0.702 0.697 U
0.760 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 21:37 1
0.180 0.179 0.164 0.692 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 21:37 1
0.142 0.175 0.136 0.851 Lead 212 pCi/g 09/05/13 11:17 09/05/13 21:37 1
0.190 0.159 0.139 0.743 Lead 214 pCi/g 09/05/13 11:17 09/05/13 21:37 1
0.944 2.65 1.87 18.2 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 21:37 1
2.19 0.725 0.723 U
0.424 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 21:37 1
0.180 1.00 0.179 0.164 0.692 Radium 226 TestAmerica St. Louis Page 18 of 27 1
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Client Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-11 Client Sample ID: L050199TUB00 Matrix: Solid Date Collected: 08/29/13 13:00 Date Received: 08/30/13 18:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 0.678 U
(2+/-)
0.562 (2+/-)
1 09/05/13 21:37 09/05/13 11:17 pCi/g 1.45 1.00 RL MDC 0.558 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 21:37 1
0.355 0.290 0.284 0.587 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 21:37 1
10.4 5.69 5.69 U
0.551 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 21:37 1
0.126 0.230 0.208 0.944 Thorium 232 Tl-208 0.318 0.0959 0.101 0.0963 pCi/g 09/05/13 11:17 09/05/13 21:37 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3585-12 Client Sample ID: L050146TSS00 Matrix: Solid Date Collected: 08/30/13 08:10 Percent Solids: 94.7 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000055 0.000016 mg/Kg
09/03/13 10:58 09/04/13 18:46 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.114 U
(2+/-)
0.0736 (2+/-)
1 09/04/13 18:46 09/03/13 10:58 pCi/g 0.188 1.10 RL MDC 0.0694 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 18:46 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 95 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.150 (2+/-)
0.0530 (2+/-)
1 09/05/13 23:05 09/05/13 11:17 pCi/g 0.105 RL MDC 0.0508 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 23:05 1
0.0621 0.0199 0.0199 U
0.000 Americium 241 pCi/g 09/05/13 11:17 09/05/13 23:05 1
0.282 0.162 0.162 U
0.0703 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 23:05 1
0.0372 0.0738 0.0596 0.418 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 23:05 1
0.0368 0.0359 0.0303 0.149 Lead 212 pCi/g 09/05/13 11:17 09/05/13 23:05 1
0.0423 0.0714 0.0547 0.441 Lead 214 pCi/g 09/05/13 11:17 09/05/13 23:05 1
0.200 1.06 0.713 7.63 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 23:05 1
0.550 0.169 0.167 U
0.190 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 23:05 1
0.0372 1.00 0.0738 0.0596 0.418 Radium 226 pCi/g 09/05/13 11:17 09/05/13 23:05 1
0.531 1.00 0.247 0.239 0.615 Thorium 234 pCi/g 09/05/13 11:17 09/05/13 23:05 1
0.145 0.0927 0.0922 U
0.0933 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 23:05 1
2.92 1.82 1.81 U
1.57 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 23:05 1
0.105 0.0530 0.0508 0.150 Thorium 232 Tl-208 0.0770 0.0205 0.0220 0.0175 pCi/g 09/05/13 11:17 09/05/13 23:05 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3585-13 Client Sample ID: L050147TRS00 Matrix: Solid Date Collected: 08/30/13 08:30 Percent Solids: 93.1 Date Received: 08/30/13 18:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000058 0.000017 mg/Kg
09/03/13 10:58 09/04/13 18:50 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0918 U
(2+/-)
0.0568 (2+/-)
1 09/04/13 18:50 09/03/13 10:58 pCi/g 0.199 1.16 RL MDC 0.0519 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 09/03/13 10:58 09/04/13 18:50 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 93 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.173 (2+/-)
0.0430 (2+/-)
1 09/05/13 23:04 09/05/13 11:17 pCi/g 0.0355 RL MDC 0.0391 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0447 0.0262 0.0262 U
0.00113 Americium 241 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.136 0.144 0.140 0.310 Bismuth 212 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0333 0.0613 0.0492 0.352 Bismuth 214 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0271 0.0320 0.0246 0.158 Lead 212 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0299 0.0605 0.0448 0.391 Lead 214 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.136 0.890 0.542 6.90 Potassium 40 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.495 0.0873 0.0867 U
0.0938 Protactinium 231 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0333 1.00 0.0613 0.0492 0.352 Radium 226 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.423 1.00 0.346 0.339 0.679 Thorium 234 pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.100 0.0635 0.0634 U
0.0383 Uranium 235 pCi/g 09/05/13 11:17 09/05/13 23:04 1
2.50 1.42 1.42 U
0.690 Protactinium 234m pCi/g 09/05/13 11:17 09/05/13 23:04 1
0.0355 0.0430 0.0391 0.173 Thorium 232 Tl-208 0.0446 0.0141 0.0148 0.0143 pCi/g 09/05/13 11:17 09/05/13 23:04 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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QC Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-70119/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70773 Prep Batch: 70119 RL MDL Technetium 99 ND 0.000051 0.000015 mg/Kg 09/03/13 10:58 09/04/13 17:40 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-70119/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70773 Prep Batch: 70119 Technetium 99 0.00240 0.00251 mg/Kg 105 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: L0501100TUB0 Lab Sample ID: 160-3585-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 70773 Prep Batch: 70119 Technetium 99 ND 0.00274 0.00243 mg/Kg 88 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: L0501100TUB0 Lab Sample ID: 160-3585-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 70773 Prep Batch: 70119 Technetium 99 ND 0.00272 0.00231 mg/Kg 85 75 - 125 5
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-70119/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70774 Prep Batch: 70119 Technetium 99 Analyte U
1 09/04/13 17:40 09/03/13 10:58 pCi/g 0.176 MDC 1.03 RL 0.0488 0.0476 (2+/-)
(2+/-)
MB 0.04020 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 09/03/13 10:58 09/04/13 17:40 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 98 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-70119/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70774 Prep Batch: 70119 Technetium 99 Analyte 120 80 105 43.03 41.1 4.54 1.03 0.176 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 97 LCS TestAmerica St. Louis Page 21 of 27 1
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QC Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: L0501100TUB0 Lab Sample ID: 160-3585-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 70774 Prep Batch: 70119 Technetium 99 Analyte 125 75 88 41.57 47.0 0.217 4.46 1.17 0.201 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 89 MS Client Sample ID: L0501100TUB0 Lab Sample ID: 160-3585-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 70774 Prep Batch: 70119 Technetium 99 Analyte 1
0.23 125 75 85 39.61 46.6 0.217 4.11 1.16 0.199 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 89 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-70772/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 71113 Prep Batch: 70772 Actinium 228 Analyte U
1 09/06/13 14:30 09/05/13 11:17 pCi/g 0.0552 MDC RL 0.0290 0.0290 (2+/-)
(2+/-)
MB 0.003480 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
09/06/13 14:30 09/05/13 11:17 pCi/g 0.0194 0.0114 0.0114 U
0.006637 Americium 241 1
09/06/13 14:30 09/05/13 11:17 pCi/g 0.153 0.0849 0.0848 U
0.03470 Bismuth 212 1
09/06/13 14:30 09/05/13 11:17 pCi/g 0.0393 0.638 0.638 U
-0.01595 Bismuth 214 1
09/06/13 14:30 09/05/13 11:17 pCi/g 0.0246 0.0124 0.0124 U
0.001568 Lead 212 1
09/06/13 14:30 09/05/13 11:17 pCi/g 0.0338 0.0370 0.0370 U
-0.006096 Lead 214 1
09/06/13 14:30 09/05/13 11:17 pCi/g 0.236 0.0978 0.0978 U
-0.001517 Potassium 40 1
09/06/13 14:30 09/05/13 11:17 pCi/g 0.292 0.0168 0.0168 U
-0.007554 Protactinium 231 1
09/06/13 14:30 09/05/13 11:17 pCi/g 0.0393 1.00 0.638 0.638 U
-0.01595 Radium 226 1
09/06/13 14:30 09/05/13 11:17 pCi/g 0.264 1.00 0.371 0.371 U
-0.07750 Thorium 234 1
09/06/13 14:30 09/05/13 11:17 pCi/g 0.0589 0.0175 0.0175 U
0.004401 Uranium 235 1
09/06/13 14:30 09/05/13 11:17 pCi/g 2.12 0.616 0.616 U
0.2023 Protactinium 234m 1
09/06/13 14:30 09/05/13 11:17 pCi/g 0.0552 0.0290 0.0290 U
0.003480 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 09/05/13 11:17 09/06/13 14:30 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 22 of 27 1
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QC Sample Results TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-70772/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70831 Prep Batch: 70772 Americium 241 Analyte 116 87 98 95.30 97.7 9.92 0.566 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 31.6 31.37 3.29 0.200 0.173 pCi/g 99 87 - 120 Cobalt 60 24.7 24.21 2.45 0.109 pCi/g 98 87 - 115 Client Sample ID: L050147TRS00 Lab Sample ID: 160-3585-13 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 70831 Prep Batch: 70772 Actinium 228 Analyte 1
0.63 0.1118 0.173 0.0550 0.0883 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241 0.00113 U
0.000243 2
U 0.0322 0.0553 pCi/g 0.02 1
Bismuth 212 0.310 0.2572 0.166 0.176 pCi/g 0.17 1
Bismuth 214 0.352 0.3548 0.0670 0.0291 pCi/g 0.02 1
Lead 212 0.158 0.1699 0.0379 0.0348 pCi/g 0.17 1
Lead 214 0.391 0.3820 0.0651 0.0438 pCi/g 0.07 1
Potassium 40 6.90 6.839 1.02 0.307 pCi/g 0.03 1
Protactinium 231 0.0938 U
0.2685 U
0.184 0.666 pCi/g 0.64 1
Radium 226 0.352 0.3548 0.0670 1.00 0.0291 pCi/g 0.02 1
Thorium 234 0.679 0.5246 U
0.238 1.00 0.562 pCi/g 0.26 1
Uranium 235 0.0383 U
0.08916 U
0.0858 0.128 pCi/g 0.34 1
Protactinium 234m 0.690 U
1.117 U
1.50 4.00 pCi/g 0.15 1
Thorium 232 0.173 0.1118 0.0550 0.0883 pCi/g 0.63 1
TestAmerica St. Louis Page 23 of 27 1
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QC Association Summary TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Metals Prep Batch: 70119 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3585-1 L0501100TUB0 Total/NA Solid None 160-3585-1 MS L0501100TUB0 Total/NA Solid None 160-3585-1 MSD L0501100TUB0 Total/NA Solid None 160-3585-2 L0501101TUB0 Total/NA Solid None 160-3585-3 L0501102TUB0 Total/NA Solid None 160-3585-4 L0501103TUB0 Total/NA Solid None 160-3585-5 L0501104TUB0 Total/NA Solid None 160-3585-6 L0501105TUB0 Total/NA Solid None 160-3585-7 L0501106TUB0 Total/NA Solid None 160-3585-8 L0501107TUB0 Total/NA Solid None 160-3585-9 L0501108TUB0 Total/NA Solid None 160-3585-10 L050198TUB00 Total/NA Solid None 160-3585-11 L050199TUB00 Total/NA Solid None 160-3585-12 L050146TSS00 Total/NA Solid None 160-3585-13 L050147TRS00 Total/NA Solid None LCS 160-70119/2-A Lab Control Sample Total/NA Solid None MB 160-70119/1-A Method Blank Total/NA Analysis Batch: 70773 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 70119 160-3585-1 L0501100TUB0 Total/NA Solid 6020A 70119 160-3585-1 MS L0501100TUB0 Total/NA Solid 6020A 70119 160-3585-1 MSD L0501100TUB0 Total/NA Solid 6020A 70119 160-3585-2 L0501101TUB0 Total/NA Solid 6020A 70119 160-3585-3 L0501102TUB0 Total/NA Solid 6020A 70119 160-3585-4 L0501103TUB0 Total/NA Solid 6020A 70119 160-3585-5 L0501104TUB0 Total/NA Solid 6020A 70119 160-3585-6 L0501105TUB0 Total/NA Solid 6020A 70119 160-3585-7 L0501106TUB0 Total/NA Solid 6020A 70119 160-3585-8 L0501107TUB0 Total/NA Solid 6020A 70119 160-3585-9 L0501108TUB0 Total/NA Solid 6020A 70119 160-3585-10 L050198TUB00 Total/NA Solid 6020A 70119 160-3585-11 L050199TUB00 Total/NA Solid 6020A 70119 160-3585-12 L050146TSS00 Total/NA Solid 6020A 70119 160-3585-13 L050147TRS00 Total/NA Solid 6020A 70119 LCS 160-70119/2-A Lab Control Sample Total/NA Solid 6020A 70119 MB 160-70119/1-A Method Blank Total/NA General Chemistry Analysis Batch: 70085 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3585-1 L0501100TUB0 Total/NA Solid Moisture 160-3585-2 L0501101TUB0 Total/NA Solid Moisture 160-3585-3 L0501102TUB0 Total/NA Solid Moisture 160-3585-4 L0501103TUB0 Total/NA Solid Moisture 160-3585-5 L0501104TUB0 Total/NA Solid Moisture 160-3585-6 L0501105TUB0 Total/NA Solid Moisture 160-3585-7 L0501106TUB0 Total/NA Solid Moisture 160-3585-8 L0501107TUB0 Total/NA TestAmerica St. Louis Page 24 of 27 1
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QC Association Summary TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
General Chemistry (Continued)
Analysis Batch: 70085 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3585-9 L0501108TUB0 Total/NA Solid Moisture 160-3585-10 L050198TUB00 Total/NA Solid Moisture 160-3585-11 L050199TUB00 Total/NA Solid Moisture 160-3585-12 L050146TSS00 Total/NA Solid Moisture 160-3585-13 L050147TRS00 Total/NA Solid Moisture 160-3585-13 DU L050147TRS00 Total/NA Rad Leach Batch: 70118 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3585-1 L0501100TUB0 Total/NA Solid Dry and Grind 160-3585-2 L0501101TUB0 Total/NA Solid Dry and Grind 160-3585-3 L0501102TUB0 Total/NA Solid Dry and Grind 160-3585-4 L0501103TUB0 Total/NA Solid Dry and Grind 160-3585-5 L0501104TUB0 Total/NA Solid Dry and Grind 160-3585-6 L0501105TUB0 Total/NA Solid Dry and Grind 160-3585-7 L0501106TUB0 Total/NA Solid Dry and Grind 160-3585-8 L0501107TUB0 Total/NA Solid Dry and Grind 160-3585-9 L0501108TUB0 Total/NA Solid Dry and Grind 160-3585-10 L050198TUB00 Total/NA Solid Dry and Grind 160-3585-11 L050199TUB00 Total/NA Solid Dry and Grind 160-3585-12 L050146TSS00 Total/NA Solid Dry and Grind 160-3585-13 L050147TRS00 Total/NA Solid Dry and Grind 160-3585-13 DU L050147TRS00 Total/NA Prep Batch: 70119 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3585-1 L0501100TUB0 Total/NA Solid None 160-3585-1 MS L0501100TUB0 Total/NA Solid None 160-3585-1 MSD L0501100TUB0 Total/NA Solid None 160-3585-2 L0501101TUB0 Total/NA Solid None 160-3585-3 L0501102TUB0 Total/NA Solid None 160-3585-4 L0501103TUB0 Total/NA Solid None 160-3585-5 L0501104TUB0 Total/NA Solid None 160-3585-6 L0501105TUB0 Total/NA Solid None 160-3585-7 L0501106TUB0 Total/NA Solid None 160-3585-8 L0501107TUB0 Total/NA Solid None 160-3585-9 L0501108TUB0 Total/NA Solid None 160-3585-10 L050198TUB00 Total/NA Solid None 160-3585-11 L050199TUB00 Total/NA Solid None 160-3585-12 L050146TSS00 Total/NA Solid None 160-3585-13 L050147TRS00 Total/NA Solid None LCS 160-70119/2-A Lab Control Sample Total/NA Solid None MB 160-70119/1-A Method Blank Total/NA Prep Batch: 70772 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 70118 160-3585-1 L0501100TUB0 Total/NA Solid Fill_Geo-0 70118 160-3585-2 L0501101TUB0 Total/NA TestAmerica St. Louis Page 25 of 27 1
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QC Association Summary TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Rad (Continued)
Prep Batch: 70772 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 70118 160-3585-3 L0501102TUB0 Total/NA Solid Fill_Geo-0 70118 160-3585-4 L0501103TUB0 Total/NA Solid Fill_Geo-0 70118 160-3585-5 L0501104TUB0 Total/NA Solid Fill_Geo-0 70118 160-3585-6 L0501105TUB0 Total/NA Solid Fill_Geo-0 70118 160-3585-7 L0501106TUB0 Total/NA Solid Fill_Geo-0 70118 160-3585-8 L0501107TUB0 Total/NA Solid Fill_Geo-0 70118 160-3585-9 L0501108TUB0 Total/NA Solid Fill_Geo-0 70118 160-3585-10 L050198TUB00 Total/NA Solid Fill_Geo-0 70118 160-3585-11 L050199TUB00 Total/NA Solid Fill_Geo-0 70118 160-3585-12 L050146TSS00 Total/NA Solid Fill_Geo-0 70118 160-3585-13 L050147TRS00 Total/NA Solid Fill_Geo-0 70118 160-3585-13 DU L050147TRS00 Total/NA Solid Fill_Geo-0 LCS 160-70772/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-70772/1-A Method Blank Total/NA TestAmerica St. Louis Page 26 of 27 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-3585-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 88 160-3585-1 Percent Yield (Acceptance Limits)
L0501100TUB0 89 160-3585-1 MS L0501100TUB0 89 160-3585-1 MSD L0501100TUB0 87 160-3585-2 L0501101TUB0 95 160-3585-3 L0501102TUB0 91 160-3585-4 L0501103TUB0 92 160-3585-5 L0501104TUB0 85 160-3585-6 L0501105TUB0 89 160-3585-7 L0501106TUB0 92 160-3585-8 L0501107TUB0 91 160-3585-9 L0501108TUB0 87 160-3585-10 L050198TUB00 88 160-3585-11 L050199TUB00 95 160-3585-12 L050146TSS00 93 160-3585-13 L050147TRS00 97 LCS 160-70119/2-A Lab Control Sample 98 MB 160-70119/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 27 of 27 1
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