ML18019A666
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-1876-1 Client Project/Site: RFP-CBA-022 (21 DAY TAT)
For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:
4/23/2013 3:18:23 PM Ivan Vania Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
TestAmerica Job ID: 160-1876-1 Page 2 of 22 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
6 Definitions/Glossary.......................................
7 Method Summary.........................................
8 Sample Summary.........................................
9 Client Sample Results......................................
10 QC Sample Results........................................
17 QC Association Summary...................................
20 Tracer Carrier Summary....................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-1876-1 Project/Site: RFP-CBA-022 (21 DAY TAT)
Job ID: 160-1876-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (21 DAY TAT)
Report Number: 160-1876-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 03/26/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 18.0 °C.
TECHNETIUM-99 (ICPMS)
Samples L050178TUB00 (160-1876-1), L050178TUQ00 (160-1876-2), L050179TUB00 (160-1876-3), L050180TUB00 (160-1876-4),
L050181TUB00 (160-1876-5), L050182TUB00 (160-1876-6), L050183TUB00 (160-1876-7), L050188TUB00 (160-1876-8) and L050189TUB00 (160-1876-9) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 04/15/2013 and analyzed on 04/16/2013.
No difficulties were encountered during the Tc-99 analyses. All quality control parameters were within the acceptance limits.
PERCENT SOLIDS Samples L050178TUB00 (160-1876-1), L050178TUQ00 (160-1876-2), L050179TUB00 (160-1876-3), L050180TUB00 (160-1876-4),
L050181TUB00 (160-1876-5), L050182TUB00 (160-1876-6), L050183TUB00 (160-1876-7), L050188TUB00 (160-1876-8) and TestAmerica St. Louis Page 3 of 22 1
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-1876-1 Project/Site: RFP-CBA-022 (21 DAY TAT)
Job ID: 160-1876-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
L050189TUB00 (160-1876-9) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 03/28/2013.
No difficulties were encountered during the % solids analyses. All quality control parameters were within the acceptance limits.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L050178TUB00 (160-1876-1), L050178TUQ00 (160-1876-2), L050179TUB00 (160-1876-3), L050180TUB00 (160-1876-4),
L050181TUB00 (160-1876-5), L050182TUB00 (160-1876-6), L050183TUB00 (160-1876-7), L050188TUB00 (160-1876-8) and L050189TUB00 (160-1876-9) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 03/27/2013, prepared on 03/29/2013 and analyzed on 04/03/2013.
Preparation Batch 43097:
Insufficient sample was provided for the following sample to fit the 0.5L marinelli geometry: L050188TUB00 (160-1876-8). The sample was put into a tuna can geometry.
The reporting limit for Thorium-234 was not met due to limited sample weight available for analysis. Analytical results are reported with the MDC achieved. L050188TUB00 (160-1876-8)
Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of Bismuth-214.
Because the samples have not had 21-day ingrowth, the activity for Radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between Radium-226 and Bismuth-214 by the loss of Radon-222 during sample preparation. L050178TUB00 (160-1876-1), L050178TUQ00 (160-1876-2), L050179TUB00 (160-1876-3), L050180TUB00 (160-1876-4),
L050181TUB00 (160-1876-5), L050182TUB00 (160-1876-6), L050183TUB00 (160-1876-7), L050188TUB00 (160-1876-8),
L050189TUB00 (160-1876-9)
Cesium 137, Cobalt 60, Protactinium 231, Protactinium 234m and Uranium 235 exceeded the rpd limit for the duplicate of sample 160-1875-21; however, the RER was within QC limits for all nuclides.
Refer to the QC report for details. No other difficulties were encountered during the Gamma spec analyses. All other quality control parameters were within the acceptance limits.
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Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I
Page 1 ofl Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization., a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HOP.
Chain of Cutodv ID No.
F-032513-01 Pa!!e 1/1 Reauested Analvsis Laboratory Name:
Project Name:
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X I 0.5" - 1.0" L050180TUBOO 3/23/2013 16:40 s G
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X 1 O" - 0.5" L050181TUBOO 3/23/2013 16:45 s G i :Xl X
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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-1876-1 Login Number: 1876 Question Answer Comment Creator: Daniels, Brian List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
True Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
False Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Qualifiers Metals Qualifier Description J
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier Rad Qualifier Description U
Indicates the analyte was analyzed for but not detected.
Qualifier F
Duplicate RPD exceeds the control limit Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 22 1
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Sample Summary TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-1876-1 L050178TUB00 Solid 03/23/13 16:30 03/26/13 15:15 160-1876-2 L050178TUQ00 Solid 03/23/13 16:30 03/26/13 15:15 160-1876-3 L050179TUB00 Solid 03/23/13 16:35 03/26/13 15:15 160-1876-4 L050180TUB00 Solid 03/23/13 16:40 03/26/13 15:15 160-1876-5 L050181TUB00 Solid 03/23/13 16:45 03/26/13 15:15 160-1876-6 L050182TUB00 Solid 03/23/13 16:50 03/26/13 15:15 160-1876-7 L050183TUB00 Solid 03/23/13 16:55 03/26/13 15:15 160-1876-8 L050188TUB00 Solid 03/23/13 10:10 03/26/13 15:15 160-1876-9 L050189TUB00 Solid 03/23/13 10:20 03/26/13 15:15 TestAmerica St. Louis Page 9 of 22 1
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Client Sample Results TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Lab Sample ID: 160-1876-1 Client Sample ID: L050178TUB00 Matrix: Solid Date Collected: 03/23/13 16:30 Percent Solids: 82.5 Date Received: 03/26/13 15:15 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00029 J
0.00066 0.000020 mg/Kg
04/15/13 09:45 04/16/13 20:56 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 4.96 (2+/-)
0.666 (2+/-)
1 04/16/13 20:56 04/15/13 09:45 pCi/g 0.227 1.32 RL MDC 0.407 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/15/13 09:45 04/16/13 20:56 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.781 (2+/-)
0.132 (2+/-)
1 04/03/13 11:11 03/29/13 11:26 pCi/g 0.0658 RL MDC 0.106 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/29/13 11:26 04/03/13 11:11 1
0.0895 10.2 10.2 U
-0.00828 Americium 241 pCi/g 03/29/13 11:26 04/03/13 11:11 1
0.354 0.416 0.398 1.14 Bismuth 212 pCi/g 03/29/13 11:26 04/03/13 11:11 1
0.0603 0.130 0.0981 0.821 Bismuth 214 pCi/g 03/29/13 11:26 04/03/13 11:11 1
0.0454 0.106 0.0591 0.684 Lead 212 pCi/g 03/29/13 11:26 04/03/13 11:11 1
0.0743 0.122 0.0800 0.883 Lead 214 pCi/g 03/29/13 11:26 04/03/13 11:11 1
0.147 1.73 1.04 13.5 Potassium 40 pCi/g 03/29/13 11:26 04/03/13 11:11 1
3.65 2.23 2.22 U
1.75 Protactinium 234m pCi/g 03/29/13 11:26 04/03/13 11:11 1
0.920 0.238 0.233 U
0.463 Protactinium 231 pCi/g 03/29/13 11:26 04/03/13 11:11 1
0.0603 1.00 0.130 0.0981 0.821 Radium 226 pCi/g 03/29/13 11:26 04/03/13 11:11 1
0.748 1.00 0.570 0.560 0.972 Thorium 234 pCi/g 03/29/13 11:26 04/03/13 11:11 1
0.201 0.131 0.131 U
0.0860 Uranium 235 pCi/g 03/29/13 11:26 04/03/13 11:11 1
0.0658 0.132 0.106 0.781 Thorium 232 Tl-208 0.240 0.0425 0.0492 0.0352 pCi/g 03/29/13 11:26 04/03/13 11:11 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-1876-2 Client Sample ID: L050178TUQ00 Matrix: Solid Date Collected: 03/23/13 16:30 Percent Solids: 82.6 Date Received: 03/26/13 15:15 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00023 J
0.00065 0.000019 mg/Kg
04/15/13 09:45 04/16/13 21:03 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.90 (2+/-)
0.475 (2+/-)
1 04/16/13 21:03 04/15/13 09:45 pCi/g 0.222 1.29 RL MDC 0.260 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/15/13 09:45 04/16/13 21:03 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 93 TestAmerica St. Louis Page 10 of 22 1
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Client Sample Results TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Lab Sample ID: 160-1876-2 Client Sample ID: L050178TUQ00 Matrix: Solid Date Collected: 03/23/13 16:30 Date Received: 03/26/13 15:15 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.818 (2+/-)
0.143 (2+/-)
1 04/03/13 11:12 03/29/13 11:26 pCi/g 0.0901 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/29/13 11:26 04/03/13 11:12 1
0.0936 0.121 0.121 U
-0.00498 Americium 241 pCi/g 03/29/13 11:26 04/03/13 11:12 1
0.319 0.397 0.377 1.20 Bismuth 212 pCi/g 03/29/13 11:26 04/03/13 11:12 1
0.0551 0.126 0.0886 0.867 Bismuth 214 pCi/g 03/29/13 11:26 04/03/13 11:12 1
0.0533 0.115 0.0594 0.758 Lead 212 pCi/g 03/29/13 11:26 04/03/13 11:12 1
0.0792 0.136 0.0891 0.980 Lead 214 pCi/g 03/29/13 11:26 04/03/13 11:12 1
0.295 1.80 0.962 15.1 Potassium 40 pCi/g 03/29/13 11:26 04/03/13 11:12 1
4.63 2.74 2.74 U
1.44 Protactinium 234m pCi/g 03/29/13 11:26 04/03/13 11:12 1
1.04 0.258 0.253 U
0.459 Protactinium 231 pCi/g 03/29/13 11:26 04/03/13 11:12 1
0.0551 1.00 0.126 0.0886 0.867 Radium 226 pCi/g 03/29/13 11:26 04/03/13 11:12 1
0.698 1.00 0.521 0.510 1.02 Thorium 234 pCi/g 03/29/13 11:26 04/03/13 11:12 1
0.221 0.121 0.120 U
0.147 Uranium 235 pCi/g 03/29/13 11:26 04/03/13 11:12 1
0.0901 0.143 0.117 0.818 Thorium 232 Tl-208 0.238 0.0409 0.0476 0.0313 pCi/g 03/29/13 11:26 04/03/13 11:12 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-1876-3 Client Sample ID: L050179TUB00 Matrix: Solid Date Collected: 03/23/13 16:35 Percent Solids: 83.2 Date Received: 03/26/13 15:15 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00012 J
0.00066 0.000020 mg/Kg
04/15/13 09:45 04/16/13 21:10 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.06 (2+/-)
0.261 (2+/-)
1 04/16/13 21:10 04/15/13 09:45 pCi/g 0.227 1.32 RL MDC 0.140 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/15/13 09:45 04/16/13 21:10 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.917 (2+/-)
0.147 (2+/-)
1 04/03/13 11:13 03/29/13 11:26 pCi/g 0.0970 RL MDC 0.113 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/29/13 11:26 04/03/13 11:13 1
0.101 0.0601 0.0601 U
-0.00923 Americium 241 pCi/g 03/29/13 11:26 04/03/13 11:13 1
0.422 0.472 0.454 1.24 Bismuth 212 pCi/g 03/29/13 11:26 04/03/13 11:13 1
0.0695 0.139 0.102 0.916 Bismuth 214 pCi/g 03/29/13 11:26 04/03/13 11:13 1
0.0604 0.140 0.0693 0.944 Lead 212 pCi/g 03/29/13 11:26 04/03/13 11:13 1
0.0671 0.154 0.0997 1.13 Lead 214 pCi/g 03/29/13 11:26 04/03/13 11:13 1
0.239 2.06 1.07 17.2 Potassium 40 pCi/g 03/29/13 11:26 04/03/13 11:13 1
4.94 2.99 2.98 U
2.21 Protactinium 234m pCi/g 03/29/13 11:26 04/03/13 11:13 1
1.03 0.229 0.221 U
0.538 Protactinium 231 TestAmerica St. Louis Page 11 of 22 1
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Client Sample Results TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Lab Sample ID: 160-1876-3 Client Sample ID: L050179TUB00 Matrix: Solid Date Collected: 03/23/13 16:35 Date Received: 03/26/13 15:15 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Radium 226 0.916 (2+/-)
0.139 (2+/-)
1 04/03/13 11:13 03/29/13 11:26 pCi/g 0.0695 1.00 RL MDC 0.102 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/29/13 11:26 04/03/13 11:13 1
0.820 1.00 0.635 0.625 1.06 Thorium 234 pCi/g 03/29/13 11:26 04/03/13 11:13 1
0.209 0.163 0.162 U
0.169 Uranium 235 pCi/g 03/29/13 11:26 04/03/13 11:13 1
0.0970 0.147 0.113 0.917 Thorium 232 Tl-208 0.308 0.0402 0.0514 0.0279 pCi/g 03/29/13 11:26 04/03/13 11:13 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-1876-4 Client Sample ID: L050180TUB00 Matrix: Solid Date Collected: 03/23/13 16:40 Percent Solids: 80.7 Date Received: 03/26/13 15:15 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000027 J
0.00066 0.000020 mg/Kg
04/15/13 09:45 04/16/13 21:18 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.461 (2+/-)
0.202 (2+/-)
1 04/16/13 21:18 04/15/13 09:45 pCi/g 0.224 1.31 RL MDC 0.186 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/15/13 09:45 04/16/13 21:18 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 95 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.05 (2+/-)
0.178 (2+/-)
1 04/03/13 20:02 03/29/13 11:26 pCi/g 0.0948 RL MDC 0.143 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/29/13 11:26 04/03/13 20:02 1
0.0950 0.172 0.172 U
-0.00664 Americium 241 pCi/g 03/29/13 11:26 04/03/13 20:02 1
0.286 0.392 0.358 1.54 Bismuth 212 pCi/g 03/29/13 11:26 04/03/13 20:02 1
0.0560 0.137 0.0931 0.981 Bismuth 214 pCi/g 03/29/13 11:26 04/03/13 20:02 1
0.0524 0.141 0.0645 0.969 Lead 212 pCi/g 03/29/13 11:26 04/03/13 20:02 1
0.0620 0.141 0.0848 1.08 Lead 214 pCi/g 03/29/13 11:26 04/03/13 20:02 1
0.356 2.11 1.07 18.0 Potassium 40 pCi/g 03/29/13 11:26 04/03/13 20:02 1
4.91 2.76 2.76 U
0.0557 Protactinium 234m pCi/g 03/29/13 11:26 04/03/13 20:02 1
1.05 0.276 0.272 U
0.430 Protactinium 231 pCi/g 03/29/13 11:26 04/03/13 20:02 1
0.0560 1.00 0.137 0.0931 0.981 Radium 226 pCi/g 03/29/13 11:26 04/03/13 20:02 1
0.745 1.00 0.600 0.580 1.44 Thorium 234 pCi/g 03/29/13 11:26 04/03/13 20:02 1
0.162 0.0978 0.0967 U
0.146 Uranium 235 pCi/g 03/29/13 11:26 04/03/13 20:02 1
0.0948 0.178 0.143 1.05 Thorium 232 Tl-208 0.292 0.0453 0.0544 0.0351 pCi/g 03/29/13 11:26 04/03/13 20:02 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Lab Sample ID: 160-1876-5 Client Sample ID: L050181TUB00 Matrix: Solid Date Collected: 03/23/13 16:45 Percent Solids: 82.8 Date Received: 03/26/13 15:15 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000057 J
0.00065 0.000019 mg/Kg
04/15/13 09:45 04/16/13 21:25 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.974 (2+/-)
0.154 (2+/-)
1 04/16/13 21:25 04/15/13 09:45 pCi/g 0.222 1.30 RL MDC 0.111 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/15/13 09:45 04/16/13 21:25 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 93 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.677 (2+/-)
0.136 (2+/-)
1 04/03/13 20:01 03/29/13 11:26 pCi/g 0.0514 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.0825 0.0485 0.0485 U
0.00816 Americium 241 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.420 0.288 0.284 0.469 Bismuth 212 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.0678 0.129 0.0987 0.792 Bismuth 214 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.0538 0.108 0.0610 0.693 Lead 212 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.0641 0.123 0.0793 0.905 Lead 214 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.141 1.71 1.02 13.5 Potassium 40 pCi/g 03/29/13 11:26 04/03/13 20:01 1
4.32 2.58 2.57 U
1.64 Protactinium 234m pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.921 0.170 0.167 U
0.315 Protactinium 231 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.0678 1.00 0.129 0.0987 0.792 Radium 226 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.673 1.00 0.268 0.255 0.763 Thorium 234 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.217 0.126 0.125 U
0.108 Uranium 235 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.0514 0.136 0.117 0.677 Thorium 232 Tl-208 0.266 0.0368 0.0460 0.0228 pCi/g 03/29/13 11:26 04/03/13 20:01 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-1876-6 Client Sample ID: L050182TUB00 Matrix: Solid Date Collected: 03/23/13 16:50 Percent Solids: 79.1 Date Received: 03/26/13 15:15 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00060 J
0.00068 0.000020 mg/Kg
04/15/13 09:45 04/16/13 21:33 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 10.2 (2+/-)
1.06 (2+/-)
1 04/16/13 21:33 04/15/13 09:45 pCi/g 0.232 1.35 RL MDC 0.275 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/15/13 09:45 04/16/13 21:33 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 93 TestAmerica St. Louis Page 13 of 22 1
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Client Sample Results TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Lab Sample ID: 160-1876-6 Client Sample ID: L050182TUB00 Matrix: Solid Date Collected: 03/23/13 16:50 Date Received: 03/26/13 15:15 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.05 (2+/-)
0.161 (2+/-)
1 04/03/13 20:01 03/29/13 11:26 pCi/g 0.114 RL MDC 0.120 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.110 0.0659 0.0659 U
-0.0229 Americium 241 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.356 0.386 0.367 1.12 Bismuth 212 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.0674 0.140 0.0990 0.957 Bismuth 214 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.0607 0.161 0.0750 1.10 Lead 212 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.0707 0.154 0.0924 1.19 Lead 214 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.419 2.38 1.24 19.9 Potassium 40 pCi/g 03/29/13 11:26 04/03/13 20:01 1
5.16 3.19 3.13 5.98 Protactinium 234m pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.820 0.496 0.495 U
0.355 Protactinium 231 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.0674 1.00 0.140 0.0990 0.957 Radium 226 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.985 1.00 0.384 0.371 U
0.943 Thorium 234 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.245 0.0680 0.0677 U
0.0567 Uranium 235 pCi/g 03/29/13 11:26 04/03/13 20:01 1
0.114 0.161 0.120 1.05 Thorium 232 Tl-208 0.332 0.0472 0.0584 0.0372 pCi/g 03/29/13 11:26 04/03/13 20:01 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-1876-7 Client Sample ID: L050183TUB00 Matrix: Solid Date Collected: 03/23/13 16:55 Percent Solids: 79.5 Date Received: 03/26/13 15:15 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00096 0.00067 0.000020 mg/Kg
04/15/13 09:45 04/16/13 21:40 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 16.5 (2+/-)
1.79 (2+/-)
1 04/16/13 21:40 04/15/13 09:45 pCi/g 0.228 1.33 RL MDC 0.760 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/15/13 09:45 04/16/13 21:40 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 95 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.04 (2+/-)
0.153 (2+/-)
1 04/03/13 21:00 03/29/13 11:26 pCi/g 0.117 RL MDC 0.110 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/29/13 11:26 04/03/13 21:00 1
0.109 0.0643 0.0643 U
0.00408 Americium 241 pCi/g 03/29/13 11:26 04/03/13 21:00 1
0.482 0.526 0.513 1.12 Bismuth 212 pCi/g 03/29/13 11:26 04/03/13 21:00 1
0.0619 0.147 0.103 1.01 Bismuth 214 pCi/g 03/29/13 11:26 04/03/13 21:00 1
0.0647 0.160 0.0771 1.09 Lead 212 pCi/g 03/29/13 11:26 04/03/13 21:00 1
0.0858 0.154 0.103 1.11 Lead 214 pCi/g 03/29/13 11:26 04/03/13 21:00 1
0.264 2.34 1.20 19.6 Potassium 40 pCi/g 03/29/13 11:26 04/03/13 21:00 1
5.18 3.29 3.29 U
0.000 Protactinium 234m pCi/g 03/29/13 11:26 04/03/13 21:00 1
1.06 0.301 0.298 U
0.391 Protactinium 231 TestAmerica St. Louis Page 14 of 22 1
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Client Sample Results TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Lab Sample ID: 160-1876-7 Client Sample ID: L050183TUB00 Matrix: Solid Date Collected: 03/23/13 16:55 Date Received: 03/26/13 15:15 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Radium 226 1.01 (2+/-)
0.147 (2+/-)
1 04/03/13 21:00 03/29/13 11:26 pCi/g 0.0619 1.00 RL MDC 0.103 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/29/13 11:26 04/03/13 21:00 1
0.901 1.00 0.697 0.679 1.49 Thorium 234 pCi/g 03/29/13 11:26 04/03/13 21:00 1
0.229 0.143 0.142 U
0.175 Uranium 235 pCi/g 03/29/13 11:26 04/03/13 21:00 1
0.117 0.153 0.110 1.04 Thorium 232 Tl-208 0.362 0.0511 0.0634 0.0382 pCi/g 03/29/13 11:26 04/03/13 21:00 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-1876-8 Client Sample ID: L050188TUB00 Matrix: Solid Date Collected: 03/23/13 10:10 Percent Solids: 73.7 Date Received: 03/26/13 15:15 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000049 J
0.00074 0.000022 mg/Kg
04/15/13 09:45 04/16/13 21:47 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.839 (2+/-)
0.214 (2+/-)
1 04/16/13 21:47 04/15/13 09:45 pCi/g 0.252 1.47 RL MDC 0.180 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/15/13 09:45 04/16/13 21:47 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.34 (2+/-)
0.247 (2+/-)
1 04/03/13 20:00 03/29/13 11:26 pCi/g 0.162 RL MDC 0.205 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/29/13 11:26 04/03/13 20:00 1
0.209 0.149 0.148 U
0.133 Americium 241 pCi/g 03/29/13 11:26 04/03/13 20:00 1
0.582 0.658 0.633 1.71 Bismuth 212 pCi/g 03/29/13 11:26 04/03/13 20:00 1
0.143 0.217 0.182 1.14 Bismuth 214 pCi/g 03/29/13 11:26 04/03/13 20:00 1
0.129 0.260 0.128 1.05 Lead 212 pCi/g 03/29/13 11:26 04/03/13 20:00 1
0.134 0.210 0.148 1.13 Lead 214 pCi/g 03/29/13 11:26 04/03/13 20:00 1
0.943 2.23 1.56 15.6 Potassium 40 pCi/g 03/29/13 11:26 04/03/13 20:00 1
7.84 4.90 4.89 U
3.27 Protactinium 234m pCi/g 03/29/13 11:26 04/03/13 20:00 1
1.91 0.615 0.605 U
0.679 Protactinium 231 pCi/g 03/29/13 11:26 04/03/13 20:00 1
0.143 1.00 0.217 0.182 1.14 Radium 226 pCi/g 03/29/13 11:26 04/03/13 20:00 1
1.84 1.00 1.43 1.42 U
1.82 Thorium 234 pCi/g 03/29/13 11:26 04/03/13 20:00 1
0.445 0.214 0.213 U
0.0711 Uranium 235 pCi/g 03/29/13 11:26 04/03/13 20:00 1
0.162 0.247 0.205 1.34 Thorium 232 Tl-208 0.388 0.0691 0.0800 0.0592 pCi/g 03/29/13 11:26 04/03/13 20:00 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Lab Sample ID: 160-1876-9 Client Sample ID: L050189TUB00 Matrix: Solid Date Collected: 03/23/13 10:20 Percent Solids: 79.7 Date Received: 03/26/13 15:15 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000020 J
0.00065 0.000020 mg/Kg
04/15/13 09:45 04/16/13 21:55 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.334 (2+/-)
0.118 (2+/-)
1 04/16/13 21:55 04/15/13 09:45 pCi/g 0.223 1.30 RL MDC 0.109 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/15/13 09:45 04/16/13 21:55 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 96 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.844 (2+/-)
0.149 (2+/-)
1 04/03/13 11:14 03/29/13 11:26 pCi/g 0.116 RL MDC 0.124 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/29/13 11:26 04/03/13 11:14 1
0.107 0.177 0.177 U
-0.0931 Americium 241 pCi/g 03/29/13 11:26 04/03/13 11:14 1
0.419 0.476 0.461 1.21 Bismuth 212 pCi/g 03/29/13 11:26 04/03/13 11:14 1
0.0771 0.128 0.106 0.741 Bismuth 214 pCi/g 03/29/13 11:26 04/03/13 11:14 1
0.0621 0.117 0.0725 0.858 Lead 212 pCi/g 03/29/13 11:26 04/03/13 11:14 1
0.0767 0.134 0.101 0.906 Lead 214 pCi/g 03/29/13 11:26 04/03/13 11:14 1
0.379 2.58 1.39 22.6 Potassium 40 pCi/g 03/29/13 11:26 04/03/13 11:14 1
5.93 2.90 2.90 U
0.810 Protactinium 234m pCi/g 03/29/13 11:26 04/03/13 11:14 1
1.15 0.318 0.313 U
0.588 Protactinium 231 pCi/g 03/29/13 11:26 04/03/13 11:14 1
0.0771 1.00 0.128 0.106 0.741 Radium 226 pCi/g 03/29/13 11:26 04/03/13 11:14 1
0.893 1.00 0.707 0.697 1.19 Thorium 234 pCi/g 03/29/13 11:26 04/03/13 11:14 1
0.268 0.161 0.161 U
0.0753 Uranium 235 pCi/g 03/29/13 11:26 04/03/13 11:14 1
0.116 0.149 0.124 0.844 Thorium 232 Tl-208 0.278 0.0507 0.0575 0.0411 pCi/g 03/29/13 11:26 04/03/13 11:14 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 16 of 22 1
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QC Sample Results TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-45835/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 46398 Prep Batch: 45835 RL MDL Technetium 99 ND 0.00052 0.000016 mg/Kg 04/15/13 09:45 04/16/13 20:04 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-45835/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 46398 Prep Batch: 45835 Technetium 99 0.0119 0.0119 mg/Kg 100 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: Matrix Spike Lab Sample ID: 160-1875-A-21-F MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 46398 Prep Batch: 45835 Technetium 99 0.000068 J
0.0163 0.0148 mg/Kg 90 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-1875-A-21-G MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 46398 Prep Batch: 45835 Technetium 99 0.000068 J
0.0163 0.0150 mg/Kg 91 75 - 125 1
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-45835/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 46399 Prep Batch: 45835 Technetium 99 Analyte U
1 04/16/13 20:04 04/15/13 09:45 pCi/g 0.177 MDC 1.03 RL 0.0682
-0.0662 (2+/-)
(2+/-)
MB
-0.05489 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 04/15/13 09:45 04/16/13 20:04 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 97 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-45835/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 46399 Prep Batch: 45835 Technetium 99 Analyte 120 80 100 204.5 205 19.9 1.02 0.175 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 98 LCS TestAmerica St. Louis Page 17 of 22 1
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QC Sample Results TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: Matrix Spike Lab Sample ID: 160-1875-A-21-F MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 46399 Prep Batch: 45835 Technetium 99 Analyte 125 75 90 253.4 279 1.17 26.4 1.39 0.239 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 90 MS Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-1875-A-21-G MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 46399 Prep Batch: 45835 Technetium 99 Analyte 30 1
125 75 91 256.8 280 1.17 27.7 1.40 0.240 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RPD RPD Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 90 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-43097/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 43940 Prep Batch: 43097 Actinium 228 Analyte U
1 04/03/13 11:09 03/29/13 11:26 pCi/g 0.0278 MDC RL 0.0239 0.0239 (2+/-)
(2+/-)
MB 0.0000 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
04/03/13 11:09 03/29/13 11:26 pCi/g 0.0278 0.0157 0.0157 U
-0.003109 Americium 241 1
04/03/13 11:09 03/29/13 11:26 pCi/g 0.277 1.85 1.85 U
-0.04630 Bismuth 212 1
04/03/13 11:09 03/29/13 11:26 pCi/g 0.0446 0.0231 0.0231 U
0.004396 Bismuth 214 1
04/03/13 11:09 03/29/13 11:26 pCi/g 0.0321 0.0276 0.0276 U
-0.003906 Lead 212 1
04/03/13 11:09 03/29/13 11:26 pCi/g 0.0404 0.000635 0.000635 U
-0.0001653 Lead 214 1
04/03/13 11:09 03/29/13 11:26 pCi/g 0.211 3.44 3.44 U
-0.08589 Potassium 40 1
04/03/13 11:09 03/29/13 11:26 pCi/g 2.80 7.15 7.15 U
-0.4082 Protactinium 234m 1
04/03/13 11:09 03/29/13 11:26 pCi/g 0.389 0.219 0.219 U
-0.06214 Protactinium 231 1
04/03/13 11:09 03/29/13 11:26 pCi/g 0.0446 1.00 0.0231 0.0231 U
0.004396 Radium 226 1
04/03/13 11:09 03/29/13 11:26 pCi/g 0.353 1.00 0.0347 0.0346 U
0.02008 Thorium 234 1
04/03/13 11:09 03/29/13 11:26 pCi/g 0.0667 0.0350 0.0350 U
0.009306 Uranium 235 1
04/03/13 11:09 03/29/13 11:26 pCi/g 0.0278 0.0239 0.0239 U
0.0000 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 03/29/13 11:26 04/03/13 11:09 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 18 of 22 1
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QC Sample Results TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-43097/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 43941 Prep Batch: 43097 Americium 241 Analyte 116 87 97 95.23 97.8 9.91 0.490 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 31.9 31.27 3.27 0.130 pCi/g 98 87 - 120 Cobalt 60 26.1 25.11 2.53 0.0713 pCi/g 96 87 - 115 Client Sample ID: Duplicate Lab Sample ID: 160-1875-A-21-D DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 43943 Prep Batch: 43097 Actinium 228 Analyte 40 10 1.077 0.972 0.162 0.0543 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RPD RPD Americium 241 0.0232 U
0.02020 U
0.0608 0.102 pCi/g 14 40 Bismuth 212 0.979 1.081 0.382 0.332 pCi/g 10 40 Bismuth 214 0.963 0.9921 0.145 0.0604 pCi/g 3
40 Lead 212 1.01 0.9484 0.142 0.0608 pCi/g 7
40 Lead 214 1.11 1.037 0.137 0.0693 pCi/g 6
40 Potassium 40 21.2 19.08 2.28 0.327 pCi/g 10 40 Protactinium 234m 1.52 U
6.032 F
2.84 5.55 pCi/g 120 40 Protactinium 231 0.302 U
-0.5433 U F 0.633 1.03 pCi/g 702 40 Radium 226 0.963 0.9921 0.145 1.00 0.0604 pCi/g 3
40 Thorium 234 1.20 1.194 0.664 1.00 0.852 pCi/g 0.8 40 Uranium 235 0.208 0.01608 U F 0.131 0.223 pCi/g 171 40 Thorium 232 0.972 1.077 0.162 0.0543 pCi/g 10 40 TestAmerica St. Louis Page 19 of 22 1
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QC Association Summary TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Metals Prep Batch: 45835 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-1875-A-21-F MS Matrix Spike Total/NA Solid None 160-1875-A-21-G MSD Matrix Spike Duplicate Total/NA Solid None 160-1876-1 L050178TUB00 Total/NA Solid None 160-1876-2 L050178TUQ00 Total/NA Solid None 160-1876-3 L050179TUB00 Total/NA Solid None 160-1876-4 L050180TUB00 Total/NA Solid None 160-1876-5 L050181TUB00 Total/NA Solid None 160-1876-6 L050182TUB00 Total/NA Solid None 160-1876-7 L050183TUB00 Total/NA Solid None 160-1876-8 L050188TUB00 Total/NA Solid None 160-1876-9 L050189TUB00 Total/NA Solid None LCS 160-45835/2-A Lab Control Sample Total/NA Solid None MB 160-45835/1-A Method Blank Total/NA Analysis Batch: 46398 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 45835 160-1875-A-21-F MS Matrix Spike Total/NA Solid 6020A 45835 160-1875-A-21-G MSD Matrix Spike Duplicate Total/NA Solid 6020A 45835 160-1876-1 L050178TUB00 Total/NA Solid 6020A 45835 160-1876-2 L050178TUQ00 Total/NA Solid 6020A 45835 160-1876-3 L050179TUB00 Total/NA Solid 6020A 45835 160-1876-4 L050180TUB00 Total/NA Solid 6020A 45835 160-1876-5 L050181TUB00 Total/NA Solid 6020A 45835 160-1876-6 L050182TUB00 Total/NA Solid 6020A 45835 160-1876-7 L050183TUB00 Total/NA Solid 6020A 45835 160-1876-8 L050188TUB00 Total/NA Solid 6020A 45835 160-1876-9 L050189TUB00 Total/NA Solid 6020A 45835 LCS 160-45835/2-A Lab Control Sample Total/NA Solid 6020A 45835 MB 160-45835/1-A Method Blank Total/NA General Chemistry Analysis Batch: 42760 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-1876-1 L050178TUB00 Total/NA Solid Moisture 160-1876-2 L050178TUQ00 Total/NA Solid Moisture 160-1876-3 L050179TUB00 Total/NA Solid Moisture 160-1876-4 L050180TUB00 Total/NA Solid Moisture 160-1876-5 L050181TUB00 Total/NA Solid Moisture 160-1876-6 L050182TUB00 Total/NA Solid Moisture 160-1876-7 L050183TUB00 Total/NA Solid Moisture 160-1876-8 L050188TUB00 Total/NA Solid Moisture 160-1876-9 L050189TUB00 Total/NA Solid Moisture 160-1876-9 DU L050189TUB00 Total/NA Rad Leach Batch: 42314 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-1875-A-21-D DU Duplicate Total/NA TestAmerica St. Louis Page 20 of 22 1
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QC Association Summary TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Rad (Continued)
Leach Batch: 42343 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-1876-1 L050178TUB00 Total/NA Solid Dry and Grind 160-1876-2 L050178TUQ00 Total/NA Solid Dry and Grind 160-1876-3 L050179TUB00 Total/NA Solid Dry and Grind 160-1876-4 L050180TUB00 Total/NA Solid Dry and Grind 160-1876-5 L050181TUB00 Total/NA Solid Dry and Grind 160-1876-6 L050182TUB00 Total/NA Solid Dry and Grind 160-1876-7 L050183TUB00 Total/NA Solid Dry and Grind 160-1876-8 L050188TUB00 Total/NA Solid Dry and Grind 160-1876-9 L050189TUB00 Total/NA Prep Batch: 43097 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 42314 160-1875-A-21-D DU Duplicate Total/NA Solid Fill_Geo-0 42343 160-1876-1 L050178TUB00 Total/NA Solid Fill_Geo-0 42343 160-1876-2 L050178TUQ00 Total/NA Solid Fill_Geo-0 42343 160-1876-3 L050179TUB00 Total/NA Solid Fill_Geo-0 42343 160-1876-4 L050180TUB00 Total/NA Solid Fill_Geo-0 42343 160-1876-5 L050181TUB00 Total/NA Solid Fill_Geo-0 42343 160-1876-6 L050182TUB00 Total/NA Solid Fill_Geo-0 42343 160-1876-7 L050183TUB00 Total/NA Solid Fill_Geo-0 42343 160-1876-8 L050188TUB00 Total/NA Solid Fill_Geo-0 42343 160-1876-9 L050189TUB00 Total/NA Solid Fill_Geo-0 LCS 160-43097/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-43097/1-A Method Blank Total/NA Prep Batch: 45835 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-1875-A-21-F MS Matrix Spike Total/NA Solid None 160-1875-A-21-G MSD Matrix Spike Duplicate Total/NA Solid None 160-1876-1 L050178TUB00 Total/NA Solid None 160-1876-2 L050178TUQ00 Total/NA Solid None 160-1876-3 L050179TUB00 Total/NA Solid None 160-1876-4 L050180TUB00 Total/NA Solid None 160-1876-5 L050181TUB00 Total/NA Solid None 160-1876-6 L050182TUB00 Total/NA Solid None 160-1876-7 L050183TUB00 Total/NA Solid None 160-1876-8 L050188TUB00 Total/NA Solid None 160-1876-9 L050189TUB00 Total/NA Solid None LCS 160-45835/2-A Lab Control Sample Total/NA Solid None MB 160-45835/1-A Method Blank Total/NA TestAmerica St. Louis Page 21 of 22 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-1876-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 90 160-1875-A-21-F MS Percent Yield (Acceptance Limits)
Matrix Spike 90 160-1875-A-21-G MSD Matrix Spike Duplicate 92 160-1876-1 L050178TUB00 93 160-1876-2 L050178TUQ00 90 160-1876-3 L050179TUB00 95 160-1876-4 L050180TUB00 93 160-1876-5 L050181TUB00 93 160-1876-6 L050182TUB00 95 160-1876-7 L050183TUB00 91 160-1876-8 L050188TUB00 96 160-1876-9 L050189TUB00 98 LCS 160-45835/2-A Lab Control Sample 97 MB 160-45835/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 22 of 22 1
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