ML18010A313

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Final Status Survey Final Report Volume 3, Chapter 6, Survey Area Release Record for Land Survey Area 10, Analytical Report, 160-5313-2
ML18010A313
Person / Time
Site: 07000036
Issue date: 02/23/2014
From: Swanson M, Vania I
TestAmerica Labs - St. Louis, Westinghouse
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML18010A247 List: ... further results
References
HEM-17-72 160-5313-2
Download: ML18010A313 (19)
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Text

ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-5313-2 Client Project/Site: RFP-CBA-022 (28 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

2/23/2014 10:53:00 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

TestAmerica Job ID: 160-5313-2 Page 2 of 19 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

4 Receipt Checklists.........................................

6 Definitions/Glossary.......................................

7 Method Summary.........................................

8 Sample Summary.........................................

9 Client Sample Results......................................

10 QC Sample Results........................................

18 QC Association Summary...................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-5313-2 Project/Site: RFP-CBA-022 (28 DAY TAT)

Job ID: 160-5313-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (28 DAY TAT)

Report Number: 160-5313-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 01/27/2014; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 17.0 C.

RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)

Samples L101017BRS00 (160-5313-1), L101018BES00 (160-5313-2), L101019BSS00 (160-5313-3), L101020BRS00 (160-5313-4),

L101021BRS00 (160-5313-5), L101023BRS00 (160-5313-6), L101025BRS00 (160-5313-7), L101026BES00 (160-5313-8),

L101027BSS00 (160-5313-9), L101028BRQ00 (160-5313-10), L101028BRS00 (160-5313-11), L101029BSS00 (160-5313-12),

L101030BRS00 (160-5313-13), L101031BES00 (160-5313-14), L101032BUB00 (160-5313-15) and L101033BUB00 (160-5313-16) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 01/28/2014, prepared on 01/30/2014 and analyzed on 02/20/2014.

No difficulties were encountered during the Radium 226 analysis. All other quality control parameters were within the acceptance limits.

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Page 1 ofl Hematite Decommissioning Project !Revision: 3 I

I Westingl,ouse Non-Proprietny Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutody ID No. I F-012714-01 Page 1/2 Project Name:

Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number:

314-810-3382 Sampler Name Scott Jenkins Sample ID L1010 l 7BRSOO Ll01018BESOO L101019BSSOO L101020BRSOO L10102 lBRSOO L101023BRSOO L101025BRSOO Ll O 1026BESOO Ll01027BSSOO Ll O 1028BRQOO Ll O 1028BRSOO L101029BSSOO Relinquished by:

Company Name: u) £:.L Received by:

Company Name:

Relinquished by:

Company Name:

Date Time

!Matrix 1/25/2014 8:401 S

1/25/2014 8:451 S

1/25/2014 8:501 S

1/25/2014 9:001 S

1/25/2014 9:201 S

1/25/2014 14:301 S

1/25/2014 10:001 s 1/25/2014 10:051 S

1/25/2014 10:151 S

1/25/2014 10:251 S

1/25/2014 10:251 S

1/25/2014 10:40 r

Date/Time Company Name:

--.i4-Laboratory Name:

TA-MO Laboratory Address:

13715 Rider Trail North

~ =-------------------

  • g PhoneNo.

=

8 314-298-8566

'I§ Laboratory Contact Person:

~ foe Walker Phone No.

708-870-8453 Ium Around Time Rush (7 days)

Remarks 1 LSA-10-10 Sys. Samples 1 LSA-10-10 Sys. Samples 1 LSA-10-10 Sys. Samples 1 LSA-10-10 Sys. Samples 1 LSA-10-10 Sys. Samples 1 LSA-10-10 Sys. Samples 1 LSA-10-10 Sys. Samples 1 LSA-10-10 Sys_ Samples 1 LSA-10-10 Sys. Samples 1 LSA-10-10 QC Sample I LSA-10-10 Sys. Samples 1 LSA-10-10 Sys. Samples Cooler Temperature:

Cooler ID: !Shipper and Number:

127-Date/Time

!Comments: Please analyze samples for Tc-99 on a 7 day TAT.

qate!yime t(v11rif l 'O'l;)

Please analyze samples for gamma spec after a 21 day in growth period.

Verified By:

C--V'-t-:-S w~f d.J-r

~

(j\\J uJ

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Page 1 ofl Hematite Decommissioning Project !Revision: :3 I

I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutody ID No. I F-012714-01 Page 2/2 Project Name:

Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number:

314-810-3382 Sampler Name Scott Jenkins Sample ID Ll O 1030BRSOO Ll 0103 lBESOO Ll01032BUBOO Ll01033BUBOO Received bv:

Company Name:

Relinquished by:

Company Name:

Date Time 1/25/2014 11:00 1/25/2014 8:30 1/25/2014 14:00 1/25/2014 14:10 Date/fime Date/Time Matrix s

s s

s Compan.lc-~e:

Date/fime

\\"'i ~~30 Date/fime v,i11qJP Dfte/fjme i/ 1---,, {,y 1.,bU)

Laboratory Name:

TA-MO Laboratory Address:

13715 Rider Trail North

  • ~-------------------

".§ PhoneNo.

8 314-298-8566

~ Laboratory Contact Person:

~ Joe Walker Phone No.

708-870-8453 Turn Around Time Rush (7 days)

Remarks LSA-10-10 Sys. Samples 1 ILSA-10-10 Sys. Samples LSA-10-10 Bias Samples 1 ILSA-10-10 Bias Samples Cooler Temperature:

Ambient Cooler ID: I Shipper and Number:

27-02 Comments: Please analyze samples for Tc-99 on a 7 day TAT.

Please analyze samples for gamma spec after a 21 day in growth period.

Verified By: C,.0,-,-h~

~~ I J...t.-,,---

~

Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-5313-2 Login Number: 5313 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

False Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

Thermal preservation not required.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Qualifiers Rad Qualifier Description U

Result is less than the sample detection limit.

Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 19 1

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Sample Summary TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-5313-1 L101017BRS00 Solid 01/25/14 08:40 01/27/14 18:00 160-5313-2 L101018BES00 Solid 01/25/14 08:45 01/27/14 18:00 160-5313-3 L101019BSS00 Solid 01/25/14 08:50 01/27/14 18:00 160-5313-4 L101020BRS00 Solid 01/25/14 09:00 01/27/14 18:00 160-5313-5 L101021BRS00 Solid 01/25/14 09:20 01/27/14 18:00 160-5313-6 L101023BRS00 Solid 01/25/14 14:30 01/27/14 18:00 160-5313-7 L101025BRS00 Solid 01/25/14 10:00 01/27/14 18:00 160-5313-8 L101026BES00 Solid 01/25/14 10:05 01/27/14 18:00 160-5313-9 L101027BSS00 Solid 01/25/14 10:15 01/27/14 18:00 160-5313-10 L101028BRQ00 Solid 01/25/14 10:25 01/27/14 18:00 160-5313-11 L101028BRS00 Solid 01/25/14 10:25 01/27/14 18:00 160-5313-12 L101029BSS00 Solid 01/25/14 10:40 01/27/14 18:00 160-5313-13 L101030BRS00 Solid 01/25/14 11:00 01/27/14 18:00 160-5313-14 L101031BES00 Solid 01/25/14 08:30 01/27/14 18:00 160-5313-15 L101032BUB00 Solid 01/25/14 14:00 01/27/14 18:00 160-5313-16 L101033BUB00 Solid 01/25/14 14:10 01/27/14 18:00 TestAmerica St. Louis Page 9 of 19 1

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Client Sample Results TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Lab Sample ID: 160-5313-1 Client Sample ID: L101017BRS00 Matrix: Solid Date Collected: 01/25/14 08:40 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.21 (2+/-)

0.211 (2+/-)

1 02/20/14 01:37 01/30/14 10:30 pCi/g 0.118 RL MDC 0.171 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 01:37 1

0.502 0.574 0.549 1.61 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 01:37 1

0.0895 0.190 0.139 1.25 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 01:37 1

0.0838 0.176 0.0907 1.17 Lead 212 pCi/g 01/30/14 10:30 02/20/14 01:37 1

0.0873 0.186 0.117 1.39 Lead 214 pCi/g 01/30/14 10:30 02/20/14 01:37 1

0.418 2.19 1.33 17.0 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 01:37 1

1.58 0.968 0.964 U

-0.830 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 01:37 1

0.0895 1.00 0.190 0.139 1.25 Radium 226 pCi/g 01/30/14 10:30 02/20/14 01:37 1

0.118 0.211 0.171 1.21 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 01:37 1

1.06 0.876 0.857 1.71 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 01:37 1

0.296 0.178 0.177 U

0.189 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 01:37 1

0.131 0.0781 0.0781 U

0.0219 Americium 241 pCi/g 01/30/14 10:30 02/20/14 01:37 1

6.79 3.75 3.75 U

0.0119 Protactinium 234m Lab Sample ID: 160-5313-2 Client Sample ID: L101018BES00 Matrix: Solid Date Collected: 01/25/14 08:45 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.30 (2+/-)

0.182 (2+/-)

1 02/20/14 01:38 01/30/14 10:30 pCi/g 0.137 RL MDC 0.126 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 01:38 1

0.512 0.573 0.552 1.46 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 01:38 1

0.0756 0.201 0.129 1.48 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 01:38 1

0.0651 0.202 0.0870 1.41 Lead 212 pCi/g 01/30/14 10:30 02/20/14 01:38 1

0.0801 0.194 0.102 1.59 Lead 214 pCi/g 01/30/14 10:30 02/20/14 01:38 1

0.445 2.26 1.24 18.4 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 01:38 1

1.24 0.393 0.386 U

0.698 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 01:38 1

0.0756 1.00 0.201 0.129 1.48 Radium 226 pCi/g 01/30/14 10:30 02/20/14 01:38 1

0.137 0.182 0.126 1.30 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 01:38 1

0.936 0.353 0.343 U

0.817 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 01:38 1

0.269 0.162 0.161 U

0.152 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 01:38 1

0.112 0.0665 0.0665 U

-0.0114 Americium 241 pCi/g 01/30/14 10:30 02/20/14 01:38 1

5.98 3.36 3.36 U

0.826 Protactinium 234m Lab Sample ID: 160-5313-3 Client Sample ID: L101019BSS00 Matrix: Solid Date Collected: 01/25/14 08:50 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.05 (2+/-)

0.184 (2+/-)

1 02/20/14 02:34 01/30/14 10:30 pCi/g 0.122 RL MDC 0.149 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.405 0.457 0.437 1.30 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.0804 0.180 0.133 1.17 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.0901 0.164 0.0916 1.05 Lead 212 TestAmerica St. Louis Page 10 of 19 1

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Client Sample Results TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Lab Sample ID: 160-5313-3 Client Sample ID: L101019BSS00 Matrix: Solid Date Collected: 01/25/14 08:50 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.25 (2+/-)

0.175 (2+/-)

1 02/20/14 02:34 01/30/14 10:30 pCi/g 0.0874 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.467 2.21 1.39 16.8 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 02:34 1

1.49 0.212 0.210 U

0.257 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.0804 1.00 0.180 0.133 1.17 Radium 226 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.122 0.184 0.149 1.05 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 02:34 1

1.12 0.936 0.919 1.70 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.269 0.190 0.189 U

0.160 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.0898 0.0552 0.0549 U

0.0522 Americium 241 pCi/g 01/30/14 10:30 02/20/14 02:34 1

7.77 4.16 4.15 U

1.61 Protactinium 234m Lab Sample ID: 160-5313-4 Client Sample ID: L101020BRS00 Matrix: Solid Date Collected: 01/25/14 09:00 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.00 (2+/-)

0.164 (2+/-)

1 02/20/14 02:34 01/30/14 10:30 pCi/g 0.106 RL MDC 0.128 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.453 0.543 0.525 1.35 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.0603 0.148 0.0984 1.07 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.0574 0.143 0.0669 0.977 Lead 212 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.0647 0.143 0.0776 1.16 Lead 214 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.281 2.14 1.07 18.1 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 02:34 1

1.03 0.256 0.252 U

0.428 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.0603 1.00 0.148 0.0984 1.07 Radium 226 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.106 0.164 0.128 1.00 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.810 0.645 0.628 1.42 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.208 0.124 0.123 U

0.135 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 02:34 1

0.0905 0.0537 0.0537 U

-0.00650 Americium 241 pCi/g 01/30/14 10:30 02/20/14 02:34 1

4.48 2.76 2.74 U

2.93 Protactinium 234m Lab Sample ID: 160-5313-5 Client Sample ID: L101021BRS00 Matrix: Solid Date Collected: 01/25/14 09:20 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.30 (2+/-)

0.257 (2+/-)

1 02/20/14 17:22 01/30/14 10:30 pCi/g 0.161 RL MDC 0.220 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 17:22 1

1.12 0.710 0.706 U

0.728 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 17:22 1

0.206 0.260 0.231 1.14 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 17:22 1

0.151 0.221 0.154 1.22 Lead 212 pCi/g 01/30/14 10:30 02/20/14 17:22 1

0.190 0.227 0.191 1.17 Lead 214 pCi/g 01/30/14 10:30 02/20/14 17:22 1

0.805 2.79 2.02 18.8 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 17:22 1

2.76 0.457 0.452 U

0.598 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 17:22 1

0.206 1.00 0.260 0.231 1.14 Radium 226 TestAmerica St. Louis Page 11 of 19 1

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Client Sample Results TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Lab Sample ID: 160-5313-5 Client Sample ID: L101021BRS00 Matrix: Solid Date Collected: 01/25/14 09:20 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 1.30 (2+/-)

0.257 (2+/-)

1 02/20/14 17:22 01/30/14 10:30 pCi/g 0.161 RL MDC 0.220 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 17:22 1

2.59 0.721 0.713 U

1.03 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 17:22 1

0.504 0.313 0.312 U

0.191 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 17:22 1

0.275 0.163 0.163 U

-0.0491 Americium 241 pCi/g 01/30/14 10:30 02/20/14 17:22 1

8.92 4.29 4.28 U

2.08 Protactinium 234m Lab Sample ID: 160-5313-6 Client Sample ID: L101023BRS00 Matrix: Solid Date Collected: 01/25/14 14:30 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.21 (2+/-)

0.505 (2+/-)

1 02/20/14 17:21 01/30/14 10:30 pCi/g 0.693 RL MDC 0.490 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 17:21 1

2.59 1.49 1.49 U

0.698 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.201 0.363 0.336 1.32 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.243 0.298 0.248 1.29 Lead 212 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.236 0.340 0.304 1.46 Lead 214 pCi/g 01/30/14 10:30 02/20/14 17:21 1

1.81 3.66 3.28 15.9 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 17:21 1

3.89 1.84 1.83 U

1.60 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.201 1.00 0.363 0.336 1.32 Radium 226 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.693 0.505 0.490 1.21 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 17:21 1

4.30 2.49 2.48 U

1.39 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.892 0.153 0.153 U

0.0985 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.402 0.238 0.238 U

0.114 Americium 241 pCi/g 01/30/14 10:30 02/20/14 17:21 1

27.0 14.6 14.6 U

3.43 Protactinium 234m Lab Sample ID: 160-5313-7 Client Sample ID: L101025BRS00 Matrix: Solid Date Collected: 01/25/14 10:00 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.927 (2+/-)

0.195 (2+/-)

1 02/20/14 17:21 01/30/14 10:30 pCi/g 0.140 RL MDC 0.170 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.461 0.578 0.552 1.64 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.102 0.189 0.146 1.16 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.0730 0.157 0.0848 1.02 Lead 212 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.0887 0.175 0.114 1.28 Lead 214 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.487 2.22 1.40 16.9 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 17:21 1

1.47 0.269 0.263 U

0.497 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.102 1.00 0.189 0.146 1.16 Radium 226 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.140 0.195 0.170 0.927 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 17:21 1

1.01 0.801 0.783 1.60 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.286 0.112 0.112 U

0.0642 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 17:21 1

0.122 0.0723 0.0723 U

0.000765 Americium 241 TestAmerica St. Louis Page 12 of 19 1

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Client Sample Results TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Lab Sample ID: 160-5313-7 Client Sample ID: L101025BRS00 Matrix: Solid Date Collected: 01/25/14 10:00 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Protactinium 234m 1.46 U

(2+/-)

4.05 (2+/-)

1 02/20/14 17:21 01/30/14 10:30 pCi/g 7.15 RL MDC 4.04 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Lab Sample ID: 160-5313-8 Client Sample ID: L101026BES00 Matrix: Solid Date Collected: 01/25/14 10:05 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.03 (2+/-)

0.164 (2+/-)

1 02/20/14 17:19 01/30/14 10:30 pCi/g 0.0875 RL MDC 0.126 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.414 0.526 0.497 1.63 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.0764 0.143 0.103 0.959 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.0557 0.156 0.0695 1.08 Lead 212 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.0689 0.143 0.0929 1.05 Lead 214 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.348 2.24 1.11 19.0 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 17:19 1

1.20 0.728 0.726 U

-0.541 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.0764 1.00 0.143 0.103 0.959 Radium 226 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.0875 0.164 0.126 1.03 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.837 0.707 0.685 1.66 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.224 0.137 0.136 U

0.116 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.104 0.0620 0.0620 U

-0.0118 Americium 241 pCi/g 01/30/14 10:30 02/20/14 17:19 1

4.86 2.26 2.26 U

1.48 Protactinium 234m Lab Sample ID: 160-5313-9 Client Sample ID: L101027BSS00 Matrix: Solid Date Collected: 01/25/14 10:15 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.05 (2+/-)

0.175 (2+/-)

1 02/20/14 17:18 01/30/14 10:30 pCi/g 0.133 RL MDC 0.139 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.345 0.434 0.408 1.42 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.0684 0.158 0.108 1.11 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.0758 0.143 0.0735 0.951 Lead 212 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.0811 0.153 0.0983 1.13 Lead 214 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.228 2.23 1.09 19.0 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 17:18 1

1.16 0.186 0.183 U

0.274 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.0684 1.00 0.158 0.108 1.11 Radium 226 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.133 0.175 0.139 1.05 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.887 0.770 0.743 1.92 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.249 0.140 0.139 U

0.121 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.105 0.0629 0.0628 U

-0.0302 Americium 241 pCi/g 01/30/14 10:30 02/20/14 17:18 1

4.55 2.85 2.83 U

2.88 Protactinium 234m TestAmerica St. Louis Page 13 of 19 1

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Client Sample Results TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Lab Sample ID: 160-5313-10 Client Sample ID: L101028BRQ00 Matrix: Solid Date Collected: 01/25/14 10:25 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.07 (2+/-)

0.181 (2+/-)

1 02/20/14 17:18 01/30/14 10:30 pCi/g 0.0968 RL MDC 0.145 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.382 0.423 0.405 1.18 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.0820 0.174 0.124 1.18 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.0578 0.160 0.0754 1.09 Lead 212 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.0823 0.154 0.109 1.05 Lead 214 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.218 2.36 1.25 19.6 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 17:18 1

1.34 0.820 0.817 U

-0.677 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.0820 1.00 0.174 0.124 1.18 Radium 226 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.0968 0.181 0.145 1.07 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.931 0.766 0.744 1.73 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.253 0.151 0.150 U

0.115 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 17:18 1

0.108 0.0643 0.0643 U

-0.0206 Americium 241 pCi/g 01/30/14 10:30 02/20/14 17:18 1

5.67 2.89 2.89 U

1.48 Protactinium 234m Lab Sample ID: 160-5313-11 Client Sample ID: L101028BRS00 Matrix: Solid Date Collected: 01/25/14 10:25 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.06 (2+/-)

0.221 (2+/-)

1 02/20/14 17:19 01/30/14 10:30 pCi/g 0.170 RL MDC 0.192 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.406 0.536 0.509 1.61 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.105 0.183 0.144 1.09 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.0833 0.161 0.0891 1.04 Lead 212 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.0804 0.171 0.118 1.20 Lead 214 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.465 2.51 1.50 19.7 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 17:19 1

1.41 0.252 0.249 U

0.364 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.105 1.00 0.183 0.144 1.09 Radium 226 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.170 0.221 0.192 1.06 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 17:19 1

1.07 0.960 0.923 2.53 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.281 0.192 0.191 U

0.156 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 17:19 1

0.117 0.0693 0.0693 U

0.00672 Americium 241 pCi/g 01/30/14 10:30 02/20/14 17:19 1

8.94 3.06 3.06 U

0.000 Protactinium 234m Lab Sample ID: 160-5313-12 Client Sample ID: L101029BSS00 Matrix: Solid Date Collected: 01/25/14 10:40 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.955 (2+/-)

0.164 (2+/-)

1 02/20/14 18:03 01/30/14 10:30 pCi/g 0.166 RL MDC 0.132 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 18:03 1

0.568 0.672 0.647 1.74 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 18:03 1

0.0757 0.176 0.133 1.11 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 18:03 1

0.0764 0.157 0.0864 1.01 Lead 212 TestAmerica St. Louis Page 14 of 19 1

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Client Sample Results TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Lab Sample ID: 160-5313-12 Client Sample ID: L101029BSS00 Matrix: Solid Date Collected: 01/25/14 10:40 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.20 (2+/-)

0.176 (2+/-)

1 02/20/14 18:03 01/30/14 10:30 pCi/g 0.0897 RL MDC 0.124 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 18:03 1

0.533 2.43 1.51 18.6 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 18:03 1

1.43 0.444 0.440 U

0.505 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 18:03 1

0.0757 1.00 0.176 0.133 1.11 Radium 226 pCi/g 01/30/14 10:30 02/20/14 18:03 1

0.166 0.164 0.132 0.955 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 18:03 1

1.00 0.803 0.773 2.07 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 18:03 1

0.235 0.137 0.135 U

0.231 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 18:03 1

0.129 0.0763 0.0763 U

-0.00554 Americium 241 pCi/g 01/30/14 10:30 02/20/14 18:03 1

7.87 11.2 11.2 U

-1.33 Protactinium 234m Lab Sample ID: 160-5313-13 Client Sample ID: L101030BRS00 Matrix: Solid Date Collected: 01/25/14 11:00 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.172 (2+/-)

1 02/20/14 18:04 01/30/14 10:30 pCi/g 0.123 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.330 0.391 0.370 1.22 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.0700 0.167 0.110 1.20 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.0578 0.163 0.0729 1.13 Lead 212 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.0720 0.166 0.0993 1.28 Lead 214 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.295 2.03 1.05 16.9 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 18:04 1

1.06 0.269 0.265 U

0.448 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.0700 1.00 0.167 0.110 1.20 Radium 226 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.123 0.172 0.129 1.12 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.894 0.724 0.715 1.06 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.224 0.130 0.130 U

0.0938 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.0959 0.0569 0.0569 U

0.00639 Americium 241 pCi/g 01/30/14 10:30 02/20/14 18:04 1

5.37 3.18 3.17 U

1.62 Protactinium 234m Lab Sample ID: 160-5313-14 Client Sample ID: L101031BES00 Matrix: Solid Date Collected: 01/25/14 08:30 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.20 (2+/-)

0.185 (2+/-)

1 02/20/14 18:04 01/30/14 10:30 pCi/g 0.102 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.395 0.444 0.427 1.18 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.0619 0.150 0.0995 1.08 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.0778 0.151 0.0758 1.01 Lead 212 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.0796 0.183 0.112 1.39 Lead 214 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.445 2.42 1.22 20.4 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 18:04 1

1.15 0.249 0.245 U

0.400 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.0619 1.00 0.150 0.0995 1.08 Radium 226 TestAmerica St. Louis Page 15 of 19 1

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Client Sample Results TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Lab Sample ID: 160-5313-14 Client Sample ID: L101031BES00 Matrix: Solid Date Collected: 01/25/14 08:30 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 1.20 (2+/-)

0.185 (2+/-)

1 02/20/14 18:04 01/30/14 10:30 pCi/g 0.102 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 18:04 1

1.10 0.679 0.673 U

0.883 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.258 0.163 0.163 U

0.129 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 18:04 1

0.108 0.0647 0.0646 U

-0.0313 Americium 241 pCi/g 01/30/14 10:30 02/20/14 18:04 1

5.13 2.95 2.95 U

0.646 Protactinium 234m Lab Sample ID: 160-5313-15 Client Sample ID: L101032BUB00 Matrix: Solid Date Collected: 01/25/14 14:00 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.28 (2+/-)

0.210 (2+/-)

1 02/20/14 18:05 01/30/14 10:30 pCi/g 0.137 RL MDC 0.164 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 18:05 1

0.432 0.527 0.500 1.58 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 18:05 1

0.0695 0.172 0.120 1.19 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 18:05 1

0.0701 0.157 0.0799 1.05 Lead 212 pCi/g 01/30/14 10:30 02/20/14 18:05 1

0.0772 0.177 0.107 1.36 Lead 214 pCi/g 01/30/14 10:30 02/20/14 18:05 1

0.356 2.36 1.31 19.1 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 18:05 1

1.24 0.308 0.304 U

0.458 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 18:05 1

0.0695 1.00 0.172 0.120 1.19 Radium 226 pCi/g 01/30/14 10:30 02/20/14 18:05 1

0.137 0.210 0.164 1.28 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 18:05 1

0.808 0.576 0.563 1.18 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 18:05 1

0.261 0.167 0.166 U

0.170 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 18:05 1

0.107 0.0637 0.0637 U

0.0128 Americium 241 pCi/g 01/30/14 10:30 02/20/14 18:05 1

6.06 3.30 3.29 U

2.81 Protactinium 234m Lab Sample ID: 160-5313-16 Client Sample ID: L101033BUB00 Matrix: Solid Date Collected: 01/25/14 14:10 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.985 (2+/-)

0.186 (2+/-)

1 02/20/14 18:06 01/30/14 10:30 pCi/g 0.133 RL MDC 0.157 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 01/30/14 10:30 02/20/14 18:06 1

0.474 0.508 0.490 1.28 Bismuth 212 pCi/g 01/30/14 10:30 02/20/14 18:06 1

0.0734 0.163 0.118 1.08 Bismuth 214 pCi/g 01/30/14 10:30 02/20/14 18:06 1

0.0760 0.147 0.0799 0.957 Lead 212 pCi/g 01/30/14 10:30 02/20/14 18:06 1

0.0832 0.158 0.101 1.16 Lead 214 pCi/g 01/30/14 10:30 02/20/14 18:06 1

0.276 2.14 1.25 16.9 Potassium 40 pCi/g 01/30/14 10:30 02/20/14 18:06 1

1.35 0.833 0.828 U

-0.814 Protactinium 231 pCi/g 01/30/14 10:30 02/20/14 18:06 1

0.0734 1.00 0.163 0.118 1.08 Radium 226 pCi/g 01/30/14 10:30 02/20/14 18:06 1

0.133 0.186 0.157 0.985 Thorium 232 pCi/g 01/30/14 10:30 02/20/14 18:06 1

1.07 0.922 0.903 1.77 Thorium 234 pCi/g 01/30/14 10:30 02/20/14 18:06 1

0.216 0.141 0.139 0.263 Uranium 235 pCi/g 01/30/14 10:30 02/20/14 18:06 1

0.117 0.0698 0.0698 U

0.0149 Americium 241 TestAmerica St. Louis Page 16 of 19 1

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Client Sample Results TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Lab Sample ID: 160-5313-16 Client Sample ID: L101033BUB00 Matrix: Solid Date Collected: 01/25/14 14:10 Date Received: 01/27/14 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Protactinium 234m 1.25 U

(2+/-)

2.62 (2+/-)

1 02/20/14 18:06 01/30/14 10:30 pCi/g 5.43 RL MDC 2.61 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

TestAmerica St. Louis Page 17 of 19 1

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QC Sample Results TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-102136/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 106633 Prep Batch: 102136 Actinium 228 Analyte U

1 02/20/14 01:36 01/30/14 10:30 pCi/g 0.0968 MDC RL 0.0124 0.0124 (2+/-)

(2+/-)

MB 0.0000 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

02/20/14 01:36 01/30/14 10:30 pCi/g 0.224 0.120 0.120 U

-0.02722 Bismuth 212 1

02/20/14 01:36 01/30/14 10:30 pCi/g 0.0446 0.0218 0.0218 U

0.001633 Bismuth 214 1

02/20/14 01:36 01/30/14 10:30 pCi/g 0.0267 0.0559 0.0559 U

-0.006662 Lead 212 1

02/20/14 01:36 01/30/14 10:30 pCi/g 0.0345 0.0132 0.0132 U

0.004932 Lead 214 1

02/20/14 01:36 01/30/14 10:30 pCi/g 0.198 2.23 2.23 U

-0.05577 Potassium 40 1

02/20/14 01:36 01/30/14 10:30 pCi/g 0.369 0.0650 0.0649 U

-0.009007 Protactinium 231 1

02/20/14 01:36 01/30/14 10:30 pCi/g 0.0446 1.00 0.0218 0.0218 U

0.001633 Radium 226 1

02/20/14 01:36 01/30/14 10:30 pCi/g 0.0968 0.0124 0.0124 U

0.0000 Thorium 232 1

02/20/14 01:36 01/30/14 10:30 pCi/g 0.244 0.160 0.160 U

-0.02623 Thorium 234 1

02/20/14 01:36 01/30/14 10:30 pCi/g 0.0685 0.0340 0.0339 U

0.01582 Uranium 235 1

02/20/14 01:36 01/30/14 10:30 pCi/g 0.0189 0.0120 0.0120 U

0.01192 Americium 241 1

02/20/14 01:36 01/30/14 10:30 pCi/g 2.45 1.10 1.10 U

0.4526 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-102136/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 106631 Prep Batch: 102136 Americium 241 Analyte 116 87 101 101.5 101 10.6 0.534 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 35.8 35.16 3.68 0.166 pCi/g 98 87 - 120 Cobalt 60 41.9 40.51 4.08 0.148 pCi/g 97 87 - 115 Client Sample ID: L101017BRS00 Lab Sample ID: 160-5313-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 106633 Prep Batch: 102136 Actinium 228 Analyte 1

0.15 1.154 1.21 0.192 0.129 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.61 1.222 0.452 0.438 pCi/g 0.38 1

Bismuth 214 1.25 1.273 0.180 0.0762 pCi/g 0.07 1

Lead 212 1.17 1.291 0.187 0.0623 pCi/g 0.35 1

Lead 214 1.39 1.425 0.191 0.0957 pCi/g 0.09 1

Potassium 40 17.0 18.87 2.31 0.229 pCi/g 0.42 1

Protactinium 231

-0.830 U

0.4877 U

0.257 1.27 pCi/g 1.08 1

Radium 226 1.25 1.273 0.180 1.00 0.0762 pCi/g 0.07 1

Thorium 232 1.21 1.154 0.192 0.129 pCi/g 0.15 1

Thorium 234 1.71 1.649 0.768 0.986 pCi/g 0.04 1

Uranium 235 0.189 U

0.1205 U

0.181 0.283 pCi/g 0.19 1

Americium 241 0.0219 U

-0.01777 U

0.0669 0.112 pCi/g 0.27 1

Protactinium 234m 0.0119 U

1.112 U

3.31 5.74 pCi/g 0.16 1

TestAmerica St. Louis Page 18 of 19 1

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QC Association Summary TestAmerica Job ID: 160-5313-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (28 DAY TAT)

Rad Leach Batch: 101600 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-5313-1 L101017BRS00 Total/NA Solid Dry and Grind 160-5313-1 DU L101017BRS00 Total/NA Solid Dry and Grind 160-5313-2 L101018BES00 Total/NA Solid Dry and Grind 160-5313-3 L101019BSS00 Total/NA Solid Dry and Grind 160-5313-4 L101020BRS00 Total/NA Solid Dry and Grind 160-5313-5 L101021BRS00 Total/NA Solid Dry and Grind 160-5313-6 L101023BRS00 Total/NA Solid Dry and Grind 160-5313-7 L101025BRS00 Total/NA Solid Dry and Grind 160-5313-8 L101026BES00 Total/NA Solid Dry and Grind 160-5313-9 L101027BSS00 Total/NA Solid Dry and Grind 160-5313-10 L101028BRQ00 Total/NA Solid Dry and Grind 160-5313-11 L101028BRS00 Total/NA Solid Dry and Grind 160-5313-12 L101029BSS00 Total/NA Solid Dry and Grind 160-5313-13 L101030BRS00 Total/NA Solid Dry and Grind 160-5313-14 L101031BES00 Total/NA Solid Dry and Grind 160-5313-15 L101032BUB00 Total/NA Solid Dry and Grind 160-5313-16 L101033BUB00 Total/NA Prep Batch: 102136 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 101600 160-5313-1 L101017BRS00 Total/NA Solid Fill_Geo-21 101600 160-5313-1 DU L101017BRS00 Total/NA Solid Fill_Geo-21 101600 160-5313-2 L101018BES00 Total/NA Solid Fill_Geo-21 101600 160-5313-3 L101019BSS00 Total/NA Solid Fill_Geo-21 101600 160-5313-4 L101020BRS00 Total/NA Solid Fill_Geo-21 101600 160-5313-5 L101021BRS00 Total/NA Solid Fill_Geo-21 101600 160-5313-6 L101023BRS00 Total/NA Solid Fill_Geo-21 101600 160-5313-7 L101025BRS00 Total/NA Solid Fill_Geo-21 101600 160-5313-8 L101026BES00 Total/NA Solid Fill_Geo-21 101600 160-5313-9 L101027BSS00 Total/NA Solid Fill_Geo-21 101600 160-5313-10 L101028BRQ00 Total/NA Solid Fill_Geo-21 101600 160-5313-11 L101028BRS00 Total/NA Solid Fill_Geo-21 101600 160-5313-12 L101029BSS00 Total/NA Solid Fill_Geo-21 101600 160-5313-13 L101030BRS00 Total/NA Solid Fill_Geo-21 101600 160-5313-14 L101031BES00 Total/NA Solid Fill_Geo-21 101600 160-5313-15 L101032BUB00 Total/NA Solid Fill_Geo-21 101600 160-5313-16 L101033BUB00 Total/NA Solid Fill_Geo-21 LCS 160-102136/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-102136/1-A Method Blank Total/NA TestAmerica St. Louis Page 19 of 19 1

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