ML18010A301

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Final Status Survey Final Report Volume 3, Chapter 6, Survey Area Release Record for Land Survey Area 10, Analytical Report, 160-3235-2
ML18010A301
Person / Time
Site: 07000036
Issue date: 09/03/2013
From:
Testamerica Labs, Westinghouse
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML18010A247 List: ... further results
References
HEM-17-72 160-3235-2
Download: ML18010A301 (18)
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3235-2 Client Project/Site: RFP-CBA-022 (21 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

9/3/2013 5:37:36 PM Ivan Vania, Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

TestAmerica Job ID: 160-3235-2 Page 2 of 18 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

5 Receipt Checklists.........................................

7 Definitions/Glossary.......................................

8 Method Summary.........................................

9 Sample Summary.........................................

10 Client Sample Results......................................

11 QC Sample Results........................................

17 QC Association Summary...................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3235-2 Project/Site: RFP-CBA-022 (21 DAY TAT)

Job ID: 160-3235-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (21 DAY TAT)

Report Number: 160-3235-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 08/03/2013; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 4 coolers at receipt time were 0.8º C, 2.2º C, 23.7º C and 25.1º C.

TECHNETIUM-99 (ICPMS)

Samples L100816BUB00 (160-3235-1), L100817BUB00 (160-3235-2), L100818BUB00 (160-3235-3), L100819BUB00 (160-3235-4),

L100820BUB00 (160-3235-5), L100821BUB00 (160-3235-6), L100822BUB00 (160-3235-7), L100823BUB00 (160-3235-8),

L100824BUB00 (160-3235-9), L100825BUB00 (160-3235-10), L100826BUB00 (160-3235-11), L100827BUB00 (160-3235-12) and L100828BUB00 (160-3235-13) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 08/06/2013 and analyzed on 08/09/2013 and 08/12/2013.

No difficulties were encountered during the Tc-99 analysis. All quality control parameters were within the acceptance limits.

PERCENT SOLIDS Samples L100816BUB00 (160-3235-1), L100817BUB00 (160-3235-2), L100818BUB00 (160-3235-3), L100819BUB00 (160-3235-4),

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3235-2 Project/Site: RFP-CBA-022 (21 DAY TAT)

Job ID: 160-3235-2 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

L100820BUB00 (160-3235-5), L100821BUB00 (160-3235-6), L100822BUB00 (160-3235-7), L100823BUB00 (160-3235-8),

L100824BUB00 (160-3235-9), L100825BUB00 (160-3235-10), L100826BUB00 (160-3235-11), L100827BUB00 (160-3235-12) and L100828BUB00 (160-3235-13) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 08/05/2013.

No difficulties were encountered during the % solids analysis. All quality control parameters were within the acceptance limits.

CESIUM-137 & OTHER GAMMA EMITTERS (GS)

Samples L100816BUB00 (160-3235-1), L100817BUB00 (160-3235-2), L100818BUB00 (160-3235-3), L100819BUB00 (160-3235-4),

L100820BUB00 (160-3235-5), L100821BUB00 (160-3235-6), L100822BUB00 (160-3235-7), L100823BUB00 (160-3235-8),

L100824BUB00 (160-3235-9), L100825BUB00 (160-3235-10), L100826BUB00 (160-3235-11), L100827BUB00 (160-3235-12) and L100828BUB00 (160-3235-13) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 08/06/2013, and prepared and analyzed on 08/08/2013.

Preparation Batch 65539:

Bismuth-214/Radium-226 analyzed by gamma spectroscopy was detected above the MDC but below the CRDL in the method blank. The data is reported. (160-3235-1 DU), (LCS 160-65539/2-A), (MB 160-65539/1-A), L100816BUB00 (160-3235-1), L100817BUB00 (160-3235-2), L100818BUB00 (160-3235-3), L100819BUB00 (160-3235-4), L100820BUB00 (160-3235-5), L100821BUB00 (160-3235-6),

L100822BUB00 (160-3235-7), L100823BUB00 (160-3235-8), L100824BUB00 (160-3235-9), L100825BUB00 (160-3235-10),

L100826BUB00 (160-3235-11), L100827BUB00 (160-3235-12), L100828BUB00 (160-3235-13)

No other difficulties were encountered during the Gamma spec analysis. All other quality control parameters were within the acceptance limits.

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I

Page 1 ofl Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sarnple is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutodv ID No.

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nR<n.n1 Comments: Please re-analyze samples after 21-day ingrowth period.

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Page 1 of l Hematite Decommissioning Project !Revision: 3 J

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,Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each tim_e the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User rnust verify that the sample is correctly identified

before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutody ID No. I F-080213-01 Project Name:

Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number:

314-810-3382 Sampler Name Scott Jenkins Sample ID Ll00828BUBOO Date 8/1/2013 P~e 2/2 Tirne

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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3235-2 Login Number: 3235 Question Answer Comment Creator: Vania, Ivan H List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

True Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

Where required True Cooler Temperature is acceptable.

See NCM True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-3235-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Qualifiers Rad Qualifier Description U

Indicates the analyte was analyzed for but not detected.

Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-3235-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 18 1

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Sample Summary TestAmerica Job ID: 160-3235-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-3235-1 L100816BUB00 Solid 08/01/13 09:08 08/03/13 16:01 160-3235-2 L100817BUB00 Solid 08/01/13 09:18 08/03/13 16:01 160-3235-3 L100818BUB00 Solid 08/01/13 09:28 08/03/13 16:01 160-3235-4 L100819BUB00 Solid 08/01/13 09:38 08/03/13 16:01 160-3235-5 L100820BUB00 Solid 08/01/13 09:48 08/03/13 16:01 160-3235-6 L100821BUB00 Solid 08/01/13 09:58 08/03/13 16:01 160-3235-7 L100822BUB00 Solid 08/01/13 10:08 08/03/13 16:01 160-3235-8 L100823BUB00 Solid 08/01/13 10:18 08/03/13 16:01 160-3235-9 L100824BUB00 Solid 08/01/13 10:28 08/03/13 16:01 160-3235-10 L100825BUB00 Solid 08/01/13 10:38 08/03/13 16:01 160-3235-11 L100826BUB00 Solid 08/01/13 10:48 08/03/13 16:01 160-3235-12 L100827BUB00 Solid 08/01/13 10:58 08/03/13 16:01 160-3235-13 L100828BUB00 Solid 08/01/13 15:32 08/03/13 16:01 TestAmerica St. Louis Page 10 of 18 1

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Client Sample Results TestAmerica Job ID: 160-3235-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-1 Client Sample ID: L100816BUB00 Matrix: Solid Date Collected: 08/01/13 09:08 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.756 (2+/-)

0.120 (2+/-)

1 08/29/13 11:53 08/08/13 11:47 pCi/g 0.0938 RL MDC 0.0923 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 11:53 1

0.380 0.381 0.373 0.747 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 11:53 1

0.0530 0.116 0.0837 0.774 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 11:53 1

0.0481 0.116 0.0579 0.776 Lead 212 pCi/g 08/08/13 11:47 08/29/13 11:53 1

0.0555 0.117 0.0708 0.891 Lead 214 pCi/g 08/08/13 11:47 08/29/13 11:53 1

0.258 1.67 0.900 13.7 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 11:53 1

1.01 0.296 0.287 U

0.644 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 11:53 1

0.0530 1.00 0.116 0.0837 0.774 Radium 226 pCi/g 08/08/13 11:47 08/29/13 11:53 1

0.0938 0.120 0.0923 0.756 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 11:53 1

0.792 0.730 0.682 2.50 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 11:53 1

0.214 0.176 0.157 0.773 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 11:53 1

0.0878 0.0526 0.0526 U

0.0194 Americium 241 pCi/g 08/08/13 11:47 08/29/13 11:53 1

3.77 2.30 2.23 5.83 Protactinium 234m Lab Sample ID: 160-3235-2 Client Sample ID: L100817BUB00 Matrix: Solid Date Collected: 08/01/13 09:18 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.663 (2+/-)

0.112 (2+/-)

1 08/29/13 11:54 08/08/13 11:47 pCi/g 0.0783 RL MDC 0.0890 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.351 0.242 0.237 0.455 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.0526 0.103 0.0734 0.690 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.0569 0.0883 0.0519 0.552 Lead 212 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.0571 0.103 0.0644 0.775 Lead 214 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.234 1.34 0.754 10.8 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.771 0.183 0.179 U

0.369 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.0526 1.00 0.103 0.0734 0.690 Radium 226 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.0783 0.112 0.0890 0.663 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.734 0.643 0.619 1.66 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.168 0.132 0.125 0.407 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.0837 0.0500 0.0500 U

-0.0138 Americium 241 pCi/g 08/08/13 11:47 08/29/13 11:54 1

3.59 2.35 2.33 U

3.51 Protactinium 234m Lab Sample ID: 160-3235-3 Client Sample ID: L100818BUB00 Matrix: Solid Date Collected: 08/01/13 09:28 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.986 (2+/-)

0.155 (2+/-)

1 08/29/13 11:54 08/08/13 11:47 pCi/g 0.108 RL MDC 0.118 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.440 0.349 0.335 0.940 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.0792 0.160 0.118 1.04 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.0572 0.150 0.0714 1.02 Lead 212 TestAmerica St. Louis Page 11 of 18 1

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Client Sample Results TestAmerica Job ID: 160-3235-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-3 Client Sample ID: L100818BUB00 Matrix: Solid Date Collected: 08/01/13 09:28 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.14 (2+/-)

0.158 (2+/-)

1 08/29/13 11:54 08/08/13 11:47 pCi/g 0.0788 RL MDC 0.105 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.138 2.04 1.12 16.7 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 11:54 1

1.07 0.313 0.308 U

0.512 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.0792 1.00 0.160 0.118 1.04 Radium 226 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.108 0.155 0.118 0.986 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.941 0.854 0.806 2.71 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.203 0.165 0.157 0.510 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 11:54 1

0.0857 0.0730 0.0729 U

-0.0324 Americium 241 pCi/g 08/08/13 11:47 08/29/13 11:54 1

5.43 3.23 3.23 U

1.94 Protactinium 234m Lab Sample ID: 160-3235-4 Client Sample ID: L100819BUB00 Matrix: Solid Date Collected: 08/01/13 09:38 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.39 (2+/-)

0.251 (2+/-)

1 08/29/13 11:55 08/08/13 11:47 pCi/g 0.115 RL MDC 0.207 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 11:55 1

0.357 0.470 0.444 1.49 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 11:55 1

0.108 0.170 0.125 1.11 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 11:55 1

0.0766 0.176 0.0904 1.17 Lead 212 pCi/g 08/08/13 11:47 08/29/13 11:55 1

0.0993 0.175 0.113 1.28 Lead 214 pCi/g 08/08/13 11:47 08/29/13 11:55 1

0.193 2.30 1.38 18.0 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 11:55 1

1.44 0.298 0.292 U

0.539 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 11:55 1

0.108 1.00 0.170 0.125 1.11 Radium 226 pCi/g 08/08/13 11:47 08/29/13 11:55 1

0.115 0.251 0.207 1.39 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 11:55 1

1.16 1.03 0.986 2.94 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 11:55 1

0.326 0.210 0.206 0.388 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 11:55 1

0.136 0.0808 0.0808 U

0.0162 Americium 241 pCi/g 08/08/13 11:47 08/29/13 11:55 1

7.83 4.52 4.52 U

1.42 Protactinium 234m Lab Sample ID: 160-3235-5 Client Sample ID: L100820BUB00 Matrix: Solid Date Collected: 08/01/13 09:48 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.10 (2+/-)

0.188 (2+/-)

1 08/29/13 11:56 08/08/13 11:47 pCi/g 0.165 RL MDC 0.151 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 11:56 1

0.533 0.434 0.417 1.14 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 11:56 1

0.0930 0.189 0.145 1.16 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 11:56 1

0.0694 0.160 0.0837 1.05 Lead 212 pCi/g 08/08/13 11:47 08/29/13 11:56 1

0.0818 0.172 0.111 1.27 Lead 214 pCi/g 08/08/13 11:47 08/29/13 11:56 1

0.318 2.22 1.35 17.2 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 11:56 1

0.962 0.569 0.569 U

0.278 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 11:56 1

0.0930 1.00 0.189 0.145 1.16 Radium 226 TestAmerica St. Louis Page 12 of 18 1

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Client Sample Results TestAmerica Job ID: 160-3235-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-5 Client Sample ID: L100820BUB00 Matrix: Solid Date Collected: 08/01/13 09:48 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 1.10 (2+/-)

0.188 (2+/-)

1 08/29/13 11:56 08/08/13 11:47 pCi/g 0.165 RL MDC 0.151 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 11:56 1

1.07 0.877 0.862 1.56 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 11:56 1

0.182 0.155 0.153 0.247 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 11:56 1

0.0879 0.0619 0.0616 U

0.0573 Americium 241 pCi/g 08/08/13 11:47 08/29/13 11:56 1

7.35 3.97 3.93 U

5.29 Protactinium 234m Lab Sample ID: 160-3235-6 Client Sample ID: L100821BUB00 Matrix: Solid Date Collected: 08/01/13 09:58 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.165 (2+/-)

1 08/29/13 22:27 08/08/13 11:47 pCi/g 0.128 RL MDC 0.119 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 22:27 1

0.288 0.360 0.335 1.27 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 22:27 1

0.0652 0.141 0.0990 0.964 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 22:27 1

0.0601 0.140 0.0691 0.942 Lead 212 pCi/g 08/08/13 11:47 08/29/13 22:27 1

0.0773 0.152 0.0922 1.17 Lead 214 pCi/g 08/08/13 11:47 08/29/13 22:27 1

0.345 2.17 1.12 18.1 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 22:27 1

1.06 0.639 0.637 U

-0.454 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 22:27 1

0.0652 1.00 0.141 0.0990 0.964 Radium 226 pCi/g 08/08/13 11:47 08/29/13 22:27 1

0.128 0.165 0.119 1.12 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 22:27 1

0.892 0.720 0.704 1.45 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 22:27 1

0.226 0.149 0.148 U

0.144 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 22:27 1

0.102 0.0607 0.0607 U

-0.00660 Americium 241 pCi/g 08/08/13 11:47 08/29/13 22:27 1

5.09 2.75 2.75 U

1.16 Protactinium 234m Lab Sample ID: 160-3235-7 Client Sample ID: L100822BUB00 Matrix: Solid Date Collected: 08/01/13 10:08 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.10 (2+/-)

0.213 (2+/-)

1 08/29/13 22:29 08/08/13 11:47 pCi/g 0.143 RL MDC 0.181 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 22:29 1

0.329 0.431 0.408 1.34 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 22:29 1

0.0914 0.155 0.112 1.03 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 22:29 1

0.0729 0.146 0.0790 0.946 Lead 212 pCi/g 08/08/13 11:47 08/29/13 22:29 1

0.0919 0.150 0.101 1.07 Lead 214 pCi/g 08/08/13 11:47 08/29/13 22:29 1

0.411 1.99 1.24 15.2 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 22:29 1

0.862 0.472 0.456 1.11 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 22:29 1

0.0914 1.00 0.155 0.112 1.03 Radium 226 pCi/g 08/08/13 11:47 08/29/13 22:29 1

0.143 0.213 0.181 1.10 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 22:29 1

0.919 0.795 0.763 2.15 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 22:29 1

0.216 0.137 0.135 U

0.193 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 22:29 1

0.111 0.0660 0.0660 U

-0.0145 Americium 241 TestAmerica St. Louis Page 13 of 18 1

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Client Sample Results TestAmerica Job ID: 160-3235-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-7 Client Sample ID: L100822BUB00 Matrix: Solid Date Collected: 08/01/13 10:08 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Protactinium 234m 0.989 U

(2+/-)

3.65 (2+/-)

1 08/29/13 22:29 08/08/13 11:47 pCi/g 6.39 RL MDC 3.65 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Lab Sample ID: 160-3235-8 Client Sample ID: L100823BUB00 Matrix: Solid Date Collected: 08/01/13 10:18 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.861 (2+/-)

0.199 (2+/-)

1 08/29/13 23:18 08/08/13 11:47 pCi/g 0.164 RL MDC 0.179 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 23:18 1

0.371 0.488 0.464 1.46 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 23:18 1

0.0790 0.170 0.128 1.07 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 23:18 1

0.0733 0.160 0.0831 1.05 Lead 212 pCi/g 08/08/13 11:47 08/29/13 23:18 1

0.0982 0.170 0.115 1.20 Lead 214 pCi/g 08/08/13 11:47 08/29/13 23:18 1

0.299 2.39 1.38 19.1 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 23:18 1

1.35 0.290 0.282 U

0.612 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 23:18 1

0.0790 1.00 0.170 0.128 1.07 Radium 226 pCi/g 08/08/13 11:47 08/29/13 23:18 1

0.164 0.199 0.179 0.861 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 23:18 1

0.943 0.748 0.731 1.52 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 23:18 1

0.236 0.165 0.164 U

0.203 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 23:18 1

0.117 0.0695 0.0695 U

0.0183 Americium 241 pCi/g 08/08/13 11:47 08/29/13 23:18 1

7.98 4.62 4.62 U

-1.42 Protactinium 234m Lab Sample ID: 160-3235-9 Client Sample ID: L100824BUB00 Matrix: Solid Date Collected: 08/01/13 10:28 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.179 (2+/-)

1 08/29/13 23:17 08/08/13 11:47 pCi/g 0.0946 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.344 0.416 0.396 1.22 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.0737 0.155 0.110 1.05 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.0605 0.159 0.0736 1.09 Lead 212 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.0640 0.145 0.0868 1.11 Lead 214 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.344 2.10 1.10 17.5 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 23:17 1

1.14 0.257 0.252 U

0.450 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.0737 1.00 0.155 0.110 1.05 Radium 226 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.0946 0.179 0.137 1.12 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.943 0.794 0.770 1.86 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.195 0.152 0.146 0.409 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.113 0.0673 0.0673 U

0.00707 Americium 241 pCi/g 08/08/13 11:47 08/29/13 23:17 1

4.79 3.02 3.00 U

3.17 Protactinium 234m TestAmerica St. Louis Page 14 of 18 1

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Client Sample Results TestAmerica Job ID: 160-3235-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-10 Client Sample ID: L100825BUB00 Matrix: Solid Date Collected: 08/01/13 10:38 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.00 (2+/-)

0.166 (2+/-)

1 08/29/13 23:16 08/08/13 11:47 pCi/g 0.0858 RL MDC 0.131 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.381 0.460 0.439 1.34 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.0746 0.153 0.110 1.02 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.0780 0.133 0.0712 0.864 Lead 212 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.0762 0.151 0.101 1.08 Lead 214 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.278 2.30 1.10 19.8 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 23:16 1

1.12 0.221 0.218 U

0.345 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.0746 1.00 0.153 0.110 1.02 Radium 226 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.0858 0.166 0.131 1.00 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.882 0.717 0.701 1.45 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.242 0.143 0.142 U

0.175 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.103 0.0619 0.0619 U

-0.0204 Americium 241 pCi/g 08/08/13 11:47 08/29/13 23:16 1

5.45 3.11 3.11 U

-0.294 Protactinium 234m Lab Sample ID: 160-3235-11 Client Sample ID: L100826BUB00 Matrix: Solid Date Collected: 08/01/13 10:48 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.15 (2+/-)

0.195 (2+/-)

1 08/29/13 23:16 08/08/13 11:47 pCi/g 0.0874 RL MDC 0.155 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.320 0.408 0.384 1.33 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.0822 0.158 0.118 1.01 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.0639 0.154 0.0773 1.03 Lead 212 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.0796 0.160 0.103 1.18 Lead 214 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.324 2.39 1.33 19.4 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 23:16 1

1.19 0.261 0.260 U

0.250 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.0822 1.00 0.158 0.118 1.01 Radium 226 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.0874 0.195 0.155 1.15 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.900 0.688 0.676 1.22 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.247 0.159 0.158 U

0.0895 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 23:16 1

0.105 0.194 0.194 U

-0.0127 Americium 241 pCi/g 08/08/13 11:47 08/29/13 23:16 1

5.21 3.04 3.04 U

1.50 Protactinium 234m Lab Sample ID: 160-3235-12 Client Sample ID: L100827BUB00 Matrix: Solid Date Collected: 08/01/13 10:58 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.02 (2+/-)

0.172 (2+/-)

1 08/29/13 23:17 08/08/13 11:47 pCi/g 0.0896 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.312 0.343 0.321 1.16 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.0634 0.134 0.0946 0.917 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.0551 0.147 0.0676 1.01 Lead 212 TestAmerica St. Louis Page 15 of 18 1

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Client Sample Results TestAmerica Job ID: 160-3235-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-12 Client Sample ID: L100827BUB00 Matrix: Solid Date Collected: 08/01/13 10:58 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.10 (2+/-)

0.145 (2+/-)

1 08/29/13 23:17 08/08/13 11:47 pCi/g 0.0587 RL MDC 0.0892 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.298 2.23 1.10 18.9 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.988 0.220 0.213 U

0.485 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.0634 1.00 0.134 0.0946 0.917 Radium 226 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.0896 0.172 0.137 1.02 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.773 0.302 0.286 0.927 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.219 0.131 0.131 U

0.0870 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 23:17 1

0.0905 0.0545 0.0545 U

-0.0301 Americium 241 pCi/g 08/08/13 11:47 08/29/13 23:17 1

4.73 2.86 2.85 U

2.07 Protactinium 234m Lab Sample ID: 160-3235-13 Client Sample ID: L100828BUB00 Matrix: Solid Date Collected: 08/01/13 15:32 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.662 (2+/-)

0.128 (2+/-)

1 08/29/13 23:55 08/08/13 11:47 pCi/g 0.127 RL MDC 0.108 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:47 08/29/13 23:55 1

0.523 0.334 0.331 U

0.387 Bismuth 212 pCi/g 08/08/13 11:47 08/29/13 23:55 1

0.0633 0.128 0.101 0.768 Bismuth 214 pCi/g 08/08/13 11:47 08/29/13 23:55 1

0.0578 0.0924 0.0590 0.550 Lead 212 pCi/g 08/08/13 11:47 08/29/13 23:55 1

0.0690 0.123 0.0911 0.792 Lead 214 pCi/g 08/08/13 11:47 08/29/13 23:55 1

0.269 1.32 0.916 9.35 Potassium 40 pCi/g 08/08/13 11:47 08/29/13 23:55 1

1.14 0.233 0.230 U

0.316 Protactinium 231 pCi/g 08/08/13 11:47 08/29/13 23:55 1

0.0633 1.00 0.128 0.101 0.768 Radium 226 pCi/g 08/08/13 11:47 08/29/13 23:55 1

0.127 0.128 0.108 0.662 Thorium 232 pCi/g 08/08/13 11:47 08/29/13 23:55 1

0.689 0.528 0.517 1.00 Thorium 234 pCi/g 08/08/13 11:47 08/29/13 23:55 1

0.221 0.131 0.131 U

0.0654 Uranium 235 pCi/g 08/08/13 11:47 08/29/13 23:55 1

0.0769 0.0453 0.0453 U

0.00672 Americium 241 pCi/g 08/08/13 11:47 08/29/13 23:55 1

5.17 1.13 1.13 U

0.000 Protactinium 234m TestAmerica St. Louis Page 16 of 18 1

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QC Sample Results TestAmerica Job ID: 160-3235-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-65539/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 69584 Prep Batch: 65539 Actinium 228 Analyte U

1 08/29/13 22:27 08/08/13 11:47 pCi/g 0.0236 MDC RL 0.00642 0.00642 (2+/-)

(2+/-)

MB 0.0000 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

08/29/13 22:27 08/08/13 11:47 pCi/g 0.180 0.0949 0.0949 U

0.01127 Bismuth 212 1

08/29/13 22:27 08/08/13 11:47 pCi/g 0.0305 0.0220 0.0215 0.04139 Bismuth 214 1

08/29/13 22:27 08/08/13 11:47 pCi/g 0.0262 0.0363 0.0363 U

-0.006612 Lead 212 1

08/29/13 22:27 08/08/13 11:47 pCi/g 0.0327 0.0193 0.0191 U

0.02108 Lead 214 1

08/29/13 22:27 08/08/13 11:47 pCi/g 0.228 0.104 0.104 U

0.02211 Potassium 40 1

08/29/13 22:27 08/08/13 11:47 pCi/g 0.371 0.0880 0.0879 U

0.02261 Protactinium 231 1

08/29/13 22:27 08/08/13 11:47 pCi/g 0.0305 1.00 0.0220 0.0215 0.04139 Radium 226 1

08/29/13 22:27 08/08/13 11:47 pCi/g 0.0236 0.00642 0.00642 U

0.0000 Thorium 232 1

08/29/13 22:27 08/08/13 11:47 pCi/g 0.264 0.139 0.139 U

0.03733 Thorium 234 1

08/29/13 22:27 08/08/13 11:47 pCi/g 0.0553 0.0101 0.0101 U

-0.003096 Uranium 235 1

08/29/13 22:27 08/08/13 11:47 pCi/g 0.0193 0.0106 0.0106 U

0.001052 Americium 241 1

08/29/13 22:27 08/08/13 11:47 pCi/g 2.18 1.22 1.22 U

0.4596 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-65539/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70048 Prep Batch: 65539 Americium 241 Analyte 116 87 98 95.93 97.7 9.99 0.568 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 31.6 31.15 3.27 0.180 pCi/g 98 87 - 120 Cobalt 60 24.8 24.20 2.45 0.118 pCi/g 98 87 - 115 Client Sample ID: L100816BUB00 Lab Sample ID: 160-3235-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 69584 Prep Batch: 65539 Actinium 228 Analyte 1

0.07 0.7731 0.756 0.125 0.0924 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 0.747 0.7684 0.320 0.323 pCi/g 0.03 1

Bismuth 214 0.774 0.7738 0.118 0.0617 pCi/g 0

1 Lead 212 0.776 0.6301 0.101 0.0676 pCi/g 0.67 1

Lead 214 0.891 0.8622 0.124 0.0634 pCi/g 0.12 1

Potassium 40 13.7 14.03 1.70 0.309 pCi/g 0.08 1

Protactinium 231 0.644 U

0.2824 U

0.208 0.901 pCi/g 0.72 1

Radium 226 0.774 0.7738 0.118 1.00 0.0617 pCi/g 0

1 Thorium 232 0.756 0.7731 0.125 0.0924 pCi/g 0.07 1

Thorium 234 2.50 2.460 0.748 0.802 pCi/g 0.03 1

Uranium 235 0.773 0.5762 0.144 0.185 pCi/g 0.62 1

Americium 241 0.0194 U

0.01505 U

0.0512 0.0858 pCi/g 0.04 1

Protactinium 234m 5.83 3.516 U

2.65 3.69 pCi/g 0.47 1

TestAmerica St. Louis Page 17 of 18 1

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QC Association Summary TestAmerica Job ID: 160-3235-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Rad Leach Batch: 65001 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3235-1 L100816BUB00 Total/NA Solid Dry and Grind 160-3235-1 DU L100816BUB00 Total/NA Solid Dry and Grind 160-3235-2 L100817BUB00 Total/NA Solid Dry and Grind 160-3235-3 L100818BUB00 Total/NA Solid Dry and Grind 160-3235-4 L100819BUB00 Total/NA Solid Dry and Grind 160-3235-5 L100820BUB00 Total/NA Solid Dry and Grind 160-3235-6 L100821BUB00 Total/NA Solid Dry and Grind 160-3235-7 L100822BUB00 Total/NA Solid Dry and Grind 160-3235-8 L100823BUB00 Total/NA Solid Dry and Grind 160-3235-9 L100824BUB00 Total/NA Solid Dry and Grind 160-3235-10 L100825BUB00 Total/NA Solid Dry and Grind 160-3235-11 L100826BUB00 Total/NA Solid Dry and Grind 160-3235-12 L100827BUB00 Total/NA Solid Dry and Grind 160-3235-13 L100828BUB00 Total/NA Prep Batch: 65539 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 65001 160-3235-1 L100816BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-1 DU L100816BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-2 L100817BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-3 L100818BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-4 L100819BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-5 L100820BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-6 L100821BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-7 L100822BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-8 L100823BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-9 L100824BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-10 L100825BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-11 L100826BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-12 L100827BUB00 Total/NA Solid Fill_Geo-21 65001 160-3235-13 L100828BUB00 Total/NA Solid Fill_Geo-21 LCS 160-65539/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-65539/1-A Method Blank Total/NA TestAmerica St. Louis Page 18 of 18 1

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