ML18010A307

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Final Status Survey Final Report Volume 3, Chapter 6, Survey Area Release Record for Land Survey Area 10, Analytical Report, 160-4124-1
ML18010A307
Person / Time
Site: 07000036
Issue date: 10/21/2013
From:
Testamerica Labs, Westinghouse
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML18010A247 List: ... further results
References
HEM-17-72 160-4124-1
Download: ML18010A307 (32)
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-4124-1 Client Project/Site: RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

10/21/2013 9:39:34 AM Ivan Vania, Project Manager I (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-4124-1 Page 2 of 32 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

6 Receipt Checklists.........................................

7 Definitions/Glossary.......................................

8 Method Summary.........................................

9 Sample Summary.........................................

10 Client Sample Results......................................

11 QC Sample Results........................................

20 QC Association Summary...................................

29 Surrogate Summary.......................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-4124-1 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-4124-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)

Report Number: 160-4124-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 10/15/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 5.0 C.

VOLATILE ORGANIC COMPOUNDS BY GC/MS Samples 6703-03-L10-09-0013-SO (160-4124-1), 6703-03-L10-09-0014-SO (160-4124-2), 6703-03-L10-09-0015-SO (160-4124-3),

6703-03-L10-09-0016-SO (160-4124-4), 6703-03-L10-09-0017-SO (160-4124-5) and 6703-03-L10-09-0018-SO (160-4124-6) were analyzed for Volatile Organic Compounds by GC/MS in accordance with EPA SW-846 Method 8260C. The samples were prepared and analyzed on 10/16/2013.

Batch 79538:

The continuing calibration verification (CCV) for n-Butanol associated with batch 79538 recovered above the upper control limit. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. (CCVIS 160-79538/3)

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-4124-1 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-4124-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

The laboratory control sample (LCS) for batch 79538 recovered outside control limits for the following analytes:1,4-Dioxane. This was not a requested analyte, and thus does not adversely affect the data.

Insufficient sample volume was available to perform batch matrix spike/matrix spike duplicate (MS/MSD) associated with batch 79538.

The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch. (LCS 160-79123/2-A), (LCSD 160-79123/3-A)

The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for preparation batch 79538 recovered outside control limits for the following analytes: 1,4-Dioxane. This was not requested analyte, and thus does not adversely affect the data.

(LCS 160-79123/2-A), (LCSD 160-79123/3-A)

No difficulties were encountered during the Volatiles analysis. All quality control parameters were within the acceptance limits.

VOLATILE ORGANIC COMPOUNDS (GC/MS)

Sample 6703-03-L10-09-0022-TB (160-4124-10) was analyzed for Volatile Organic Compounds (GC/MS) in accordance with EPA SW-846 Method 8260C. The samples were analyzed on 10/16/2013.

Batch 79367:

The continuing calibration verification (CCV) for Freon-114 and Bromomethane associated with batch 79367 recovered above the upper control limit. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.

(CCVIS 160-79367/3)

The laboratory control sample (LCS) and / or the laboratory control sample duplicate (LCSD) for batch 79367 recovered outside control limits for Freon-114, and Iodomethane. These analytes were not target compounds of interest. Therefore, this excursion does not affect the reported data. (LCS 160-79367/4), (LCSD 160-79367/5)

The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for preparation batch 79367 recovered outside control limits for Acetone. The LCS/LCSD spike recoveries for this analyte were within QC limits. (LCS 160-79367/4), (LCSD 160-79367/5)

Insufficient sample volume was available to perform batch matrix spike/matrix spike duplicate (MS/MSD) associated with batch 79367.

The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch. (LCS 160-79367/4), (LCSD 160-79367/5)

No other difficulties were encountered during the VOA analysis. All other quality control parameters were within the acceptance limits.

SEMIVOLATILE ORGANIC COMPOUNDS (GC/MS)

Samples 6703-03-L10-09-0019-SO (160-4124-7), 6703-03-L10-09-0020-SO (160-4124-8) and 6703-03-L10-09-0021-SO (160-4124-9) were analyzed for Semivolatile Organic Compounds (GC/MS) in accordance with EPA SW-846 Method 8270D. The samples were prepared and analyzed on 10/16/2013.

No difficulties were encountered during the Semi-VOA analysis. All quality control parameters were within the acceptance limits.

TOTAL METALS (ICP)

Samples 6703-03-L10-09-0019-SO (160-4124-7), 6703-03-L10-09-0020-SO (160-4124-8) and 6703-03-L10-09-0021-SO (160-4124-9) were analyzed for total metals (ICP) in accordance with EPA SW-846 Method 6010C. The samples were prepared and analyzed on 10/18/2013.

Preparation Batch 79708, Analytical Batch 76757:

Due to a sequencing error, there are 11 samples between CCV/CCB's instead of 10. All QC is within acceptable limits, results will be reported with this NCM. (160-4124-7 MS), (160-4124-7 MSD), (160-4124-7 SD), (LCS 160-79708/2-A), (MB 160-79708/1-A),

6703-03-L10-09-0019-SO (160-4124-7), 6703-03-L10-09-0020-SO (160-4124-8), 6703-03-L10-09-0021-SO (160-4124-9)

Preparation Batch 79708, Analytical Batch 76757:

The following sample(s) was diluted due to high concentrations of iron which interferes with arsenic: (160-4124-7 MS), (160-4124-7 TestAmerica St. Louis Page 4 of 32 1

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-4124-1 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-4124-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

MSD), (160-4124-7 SD), 6703-03-L10-09-0019-SO (160-4124-7), 6703-03-L10-09-0020-SO (160-4124-8), 6703-03-L10-09-0021-SO (160-4124-9). Elevated reporting limits (RLs) are provided.

No difficulties were encountered during the metals analysis. All quality control parameters were within the acceptance limits.

PERCENT SOLIDS Samples 6703-03-L10-09-0013-SO (160-4124-1), 6703-03-L10-09-0014-SO (160-4124-2), 6703-03-L10-09-0015-SO (160-4124-3),

6703-03-L10-09-0016-SO (160-4124-4), 6703-03-L10-09-0017-SO (160-4124-5), 6703-03-L10-09-0018-SO (160-4124-6),

6703-03-L10-09-0019-SO (160-4124-7), 6703-03-L10-09-0020-SO (160-4124-8) and 6703-03-L10-09-0021-SO (160-4124-9) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 10/16/2013.

No difficulties were encountered during the % solids analysis. All quality control parameters were within the acceptance limits.

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10 11 12 Hematite Procedure HDP-PR-QA-006, Chain of Custody Decommissioning Revision: 3 Page 1 of!

Project Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization., a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain ofCutodv ID No.

093013-04 Pa!!e 1/1 Reauested Analysis Laboratorv Name:

Project Name:

TA-MO Westinghouse Electric Company Contact Person:

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Quality Record

Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-4124-1 Login Number: 4124 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Qualifiers GC/MS VOA Qualifier Description RPD of the LCS and LCSD exceeds the control limits Qualifier J

Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method Method Description Laboratory Protocol SW846 8260C Volatile Organic Compounds by GC/MS TAL SL SW846 8260C Volatile Organic Compounds (GC/MS)

TAL SL SW846 8270D Semivolatile Organic Compounds (GC/MS)

TAL SL SW846 6010C Metals (ICP)

TAL SL EPA Moisture Percent Moisture TAL SL Protocol

References:

EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 32 1

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Sample Summary TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-4124-1 6703-03-L10-09-0013-SO Solid 10/14/13 14:15 10/15/13 17:55 160-4124-2 6703-03-L10-09-0014-SO Solid 10/14/13 14:20 10/15/13 17:55 160-4124-3 6703-03-L10-09-0015-SO Solid 10/14/13 14:25 10/15/13 17:55 160-4124-4 6703-03-L10-09-0016-SO Solid 10/14/13 14:30 10/15/13 17:55 160-4124-5 6703-03-L10-09-0017-SO Solid 10/14/13 14:35 10/15/13 17:55 160-4124-6 6703-03-L10-09-0018-SO Solid 10/14/13 14:40 10/15/13 17:55 160-4124-7 6703-03-L10-09-0019-SO Solid 10/14/13 14:45 10/15/13 17:55 160-4124-8 6703-03-L10-09-0020-SO Solid 10/14/13 14:50 10/15/13 17:55 160-4124-9 6703-03-L10-09-0021-SO Solid 10/14/13 14:55 10/15/13 17:55 160-4124-10 6703-03-L10-09-0022-TB Water 10/14/13 14:00 10/15/13 17:55 TestAmerica St. Louis Page 10 of 32 1

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Client Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4124-1 Client Sample ID: 6703-03-L10-09-0013-SO Matrix: Solid Date Collected: 10/14/13 14:15 Percent Solids: 82.3 Date Received: 10/15/13 17:55 Method: 8260C - Volatile Organic Compounds by GC/MS RL MDL Acetone ND 19 6.0 ug/Kg

10/16/13 10:40 10/16/13 18:07 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier 4.7 0.23 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Benzene ND 4.7 0.23 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Bromodichloromethane ND 4.7 0.34 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Bromoform ND 9.3 1.0 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Methyl bromide ND 120 15 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

n-Butanol ND 19 1.8 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

2-Butanone ND 4.7 0.64 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Carbon disulfide ND 4.7 0.47 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Carbon tetrachloride ND 4.7 0.35 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Chlorobenzene ND 4.7 0.38 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Chlorodibromomethane ND 9.3 0.48 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Chloroethane ND 4.7 0.35 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Chloroform ND 9.3 0.61 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Chloromethane ND 9.3 1.4 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

1,2-Dibromo-3-Chloropropane ND 4.7 0.65 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

1,2-Dibromoethane ND 4.7 0.36 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

1,1-Dichloroethane ND 4.7 0.81 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

1,2-Dichloroethane ND 4.7 0.56 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

cis-1,2-Dichloroethene ND 4.7 0.88 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

trans-1,2-Dichloroethene ND 4.7 1.5 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

1,1-Dichloroethene ND 9.3 0.89 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

1,2-Dichloroethene, Total ND 4.7 0.35 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

1,2-Dichloropropane ND 4.7 0.56 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

cis-1,3-Dichloropropene ND 4.7 0.33 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

trans-1,3-Dichloropropene ND 4.7 0.28 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Ethylbenzene ND 19 1.6 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

2-Hexanone ND 4.7 1.5 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Methylene Chloride ND 19 0.68 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

4-Methyl-2-pentanone ND 4.7 0.33 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Styrene ND 4.7 0.37 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

1,1,2,2-Tetrachloroethane ND 4.7 0.30 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Tetrachloroethene ND 4.7 0.65 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Toluene ND 4.7 0.40 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

1,2,4-Trichlorobenzene ND 4.7 0.40 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

1,1,1-Trichloroethane ND 4.7 0.53 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

1,1,2-Trichloroethane ND 4.7 0.36 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Trichloroethene ND 4.7 0.73 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Vinyl acetate ND 4.7 0.40 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Vinyl chloride ND 9.3 0.79 ug/Kg 10/16/13 10:40 10/16/13 18:07 1

Xylenes, Total ND 4-Bromofluorobenzene (Surr) 101 63 - 150 10/16/13 10:40 10/16/13 18:07 1

Surrogate Dil Fac Analyzed Prepared Qualifier Limits

%Recovery 1,2-Dichloroethane-d4 (Surr) 107 10/16/13 10:40 10/16/13 18:07 1

72 - 127 Toluene-d8 (Surr) 97 10/16/13 10:40 10/16/13 18:07 1

80 - 120 Dibromofluoromethane (Surr) 107 10/16/13 10:40 10/16/13 18:07 1

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Client Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4124-2 Client Sample ID: 6703-03-L10-09-0014-SO Matrix: Solid Date Collected: 10/14/13 14:20 Percent Solids: 80.0 Date Received: 10/15/13 17:55 Method: 8260C - Volatile Organic Compounds by GC/MS RL MDL Acetone ND 20 6.6 ug/Kg

10/16/13 10:40 10/16/13 18:32 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier 5.1 0.25 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Benzene ND 5.1 0.25 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Bromodichloromethane ND 5.1 0.37 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Bromoform ND 10 1.1 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Methyl bromide ND 130 17 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

n-Butanol ND 20 1.9 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

2-Butanone ND 5.1 0.70 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Carbon disulfide ND 5.1 0.52 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Carbon tetrachloride ND 5.1 0.39 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Chlorobenzene ND 5.1 0.42 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Chlorodibromomethane ND 10 0.53 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Chloroethane ND 5.1 0.39 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Chloroform ND 10 0.66 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Chloromethane ND 10 1.5 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

1,2-Dibromo-3-Chloropropane ND 5.1 0.71 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

1,2-Dibromoethane ND 5.1 0.40 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

1,1-Dichloroethane ND 5.1 0.88 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

1,2-Dichloroethane ND 5.1 0.61 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

cis-1,2-Dichloroethene 2.2 J

5.1 0.95 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

trans-1,2-Dichloroethene ND 5.1 1.6 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

1,1-Dichloroethene ND 10 0.97 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

1,2-Dichloroethene, Total 2.2 J

5.1 0.39 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

1,2-Dichloropropane ND 5.1 0.61 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

cis-1,3-Dichloropropene ND 5.1 0.35 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

trans-1,3-Dichloropropene ND 5.1 0.30 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Ethylbenzene ND 20 1.8 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

2-Hexanone ND 5.1 1.6 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Methylene Chloride ND 20 0.74 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

4-Methyl-2-pentanone ND 5.1 0.35 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Styrene ND 5.1 0.41 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

1,1,2,2-Tetrachloroethane ND 5.1 0.32 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Tetrachloroethene 1.8 J

5.1 0.71 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Toluene ND 5.1 0.44 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

1,2,4-Trichlorobenzene ND 5.1 0.44 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

1,1,1-Trichloroethane ND 5.1 0.58 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

1,1,2-Trichloroethane ND 5.1 0.40 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Trichloroethene 3.1 J

5.1 0.79 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Vinyl acetate ND 5.1 0.44 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Vinyl chloride ND 10 0.86 ug/Kg 10/16/13 10:40 10/16/13 18:32 1

Xylenes, Total ND 4-Bromofluorobenzene (Surr) 100 63 - 150 10/16/13 10:40 10/16/13 18:32 1

Surrogate Dil Fac Analyzed Prepared Qualifier Limits

%Recovery 1,2-Dichloroethane-d4 (Surr) 106 10/16/13 10:40 10/16/13 18:32 1

72 - 127 Toluene-d8 (Surr) 94 10/16/13 10:40 10/16/13 18:32 1

80 - 120 Dibromofluoromethane (Surr) 105 10/16/13 10:40 10/16/13 18:32 1

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Client Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4124-3 Client Sample ID: 6703-03-L10-09-0015-SO Matrix: Solid Date Collected: 10/14/13 14:25 Percent Solids: 88.3 Date Received: 10/15/13 17:55 Method: 8260C - Volatile Organic Compounds by GC/MS RL MDL Acetone ND 18 5.7 ug/Kg

10/16/13 10:40 10/16/13 18:57 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier 4.4 0.22 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Benzene ND 4.4 0.22 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Bromodichloromethane ND 4.4 0.32 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Bromoform ND 8.8 0.96 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Methyl bromide ND 110 14 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

n-Butanol ND 18 1.7 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

2-Butanone ND 4.4 0.60 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Carbon disulfide ND 4.4 0.45 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Carbon tetrachloride ND 4.4 0.33 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Chlorobenzene ND 4.4 0.36 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Chlorodibromomethane ND 8.8 0.46 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Chloroethane ND 4.4 0.33 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Chloroform ND 8.8 0.57 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Chloromethane ND 8.8 1.3 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

1,2-Dibromo-3-Chloropropane ND 4.4 0.61 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

1,2-Dibromoethane ND 4.4 0.34 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

1,1-Dichloroethane ND 4.4 0.76 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

1,2-Dichloroethane ND 4.4 0.53 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

cis-1,2-Dichloroethene ND 4.4 0.82 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

trans-1,2-Dichloroethene ND 4.4 1.4 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

1,1-Dichloroethene ND 8.8 0.84 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

1,2-Dichloroethene, Total ND 4.4 0.33 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

1,2-Dichloropropane ND 4.4 0.53 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

cis-1,3-Dichloropropene ND 4.4 0.31 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

trans-1,3-Dichloropropene ND 4.4 0.26 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Ethylbenzene ND 18 1.6 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

2-Hexanone ND 4.4 1.4 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Methylene Chloride ND 18 0.64 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

4-Methyl-2-pentanone ND 4.4 0.31 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Styrene ND 4.4 0.35 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

1,1,2,2-Tetrachloroethane ND 4.4 0.28 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Tetrachloroethene ND 4.4 0.61 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Toluene ND 4.4 0.38 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

1,2,4-Trichlorobenzene ND 4.4 0.38 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

1,1,1-Trichloroethane ND 4.4 0.50 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

1,1,2-Trichloroethane ND 4.4 0.34 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Trichloroethene ND 4.4 0.68 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Vinyl acetate ND 4.4 0.38 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Vinyl chloride ND 8.8 0.74 ug/Kg 10/16/13 10:40 10/16/13 18:57 1

Xylenes, Total ND 4-Bromofluorobenzene (Surr) 100 63 - 150 10/16/13 10:40 10/16/13 18:57 1

Surrogate Dil Fac Analyzed Prepared Qualifier Limits

%Recovery 1,2-Dichloroethane-d4 (Surr) 107 10/16/13 10:40 10/16/13 18:57 1

72 - 127 Toluene-d8 (Surr) 102 10/16/13 10:40 10/16/13 18:57 1

80 - 120 Dibromofluoromethane (Surr) 106 10/16/13 10:40 10/16/13 18:57 1

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Client Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4124-4 Client Sample ID: 6703-03-L10-09-0016-SO Matrix: Solid Date Collected: 10/14/13 14:30 Percent Solids: 84.0 Date Received: 10/15/13 17:55 Method: 8260C - Volatile Organic Compounds by GC/MS RL MDL Acetone ND 18 5.9 ug/Kg

10/16/13 10:40 10/16/13 19:22 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier 4.6 0.23 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Benzene ND 4.6 0.23 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Bromodichloromethane ND 4.6 0.34 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Bromoform ND 9.1 1.0 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Methyl bromide ND 110 15 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

n-Butanol ND 18 1.8 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

2-Butanone ND 4.6 0.63 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Carbon disulfide ND 4.6 0.47 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Carbon tetrachloride ND 4.6 0.35 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Chlorobenzene ND 4.6 0.37 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Chlorodibromomethane ND 9.1 0.48 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Chloroethane ND 4.6 0.35 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Chloroform ND 9.1 0.59 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Chloromethane ND 9.1 1.3 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

1,2-Dibromo-3-Chloropropane ND 4.6 0.64 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

1,2-Dibromoethane ND 4.6 0.36 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

1,1-Dichloroethane ND 4.6 0.80 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

1,2-Dichloroethane ND 4.6 0.55 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

cis-1,2-Dichloroethene ND 4.6 0.86 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

trans-1,2-Dichloroethene ND 4.6 1.5 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

1,1-Dichloroethene ND 9.1 0.88 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

1,2-Dichloroethene, Total ND 4.6 0.35 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

1,2-Dichloropropane ND 4.6 0.55 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

cis-1,3-Dichloropropene ND 4.6 0.32 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

trans-1,3-Dichloropropene ND 4.6 0.27 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Ethylbenzene ND 18 1.6 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

2-Hexanone ND 4.6 1.4 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Methylene Chloride ND 18 0.67 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

4-Methyl-2-pentanone ND 4.6 0.32 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Styrene ND 4.6 0.37 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

1,1,2,2-Tetrachloroethane ND 4.6 0.29 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Tetrachloroethene 0.92 J

4.6 0.64 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Toluene ND 4.6 0.39 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

1,2,4-Trichlorobenzene ND 4.6 0.39 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

1,1,1-Trichloroethane ND 4.6 0.52 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

1,1,2-Trichloroethane ND 4.6 0.36 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Trichloroethene ND 4.6 0.71 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Vinyl acetate ND 4.6 0.39 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Vinyl chloride ND 9.1 0.78 ug/Kg 10/16/13 10:40 10/16/13 19:22 1

Xylenes, Total ND 4-Bromofluorobenzene (Surr) 99 63 - 150 10/16/13 10:40 10/16/13 19:22 1

Surrogate Dil Fac Analyzed Prepared Qualifier Limits

%Recovery 1,2-Dichloroethane-d4 (Surr) 108 10/16/13 10:40 10/16/13 19:22 1

72 - 127 Toluene-d8 (Surr) 97 10/16/13 10:40 10/16/13 19:22 1

80 - 120 Dibromofluoromethane (Surr) 109 10/16/13 10:40 10/16/13 19:22 1

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Client Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4124-5 Client Sample ID: 6703-03-L10-09-0017-SO Matrix: Solid Date Collected: 10/14/13 14:35 Percent Solids: 87.0 Date Received: 10/15/13 17:55 Method: 8260C - Volatile Organic Compounds by GC/MS RL MDL Acetone 13 J

21 6.8 ug/Kg

10/16/13 10:40 10/16/13 19:47 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier 5.2 0.26 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Benzene ND 5.2 0.26 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Bromodichloromethane ND 5.2 0.39 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Bromoform ND 10 1.2 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Methyl bromide ND 130 17 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

n-Butanol ND 21 2.0 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

2-Butanone ND 5.2 0.72 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Carbon disulfide ND 5.2 0.53 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Carbon tetrachloride ND 5.2 0.40 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Chlorobenzene ND 5.2 0.43 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Chlorodibromomethane ND 10 0.55 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Chloroethane ND 5.2 0.40 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Chloroform ND 10 0.68 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Chloromethane ND 10 1.5 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

1,2-Dibromo-3-Chloropropane ND 5.2 0.73 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

1,2-Dibromoethane ND 5.2 0.41 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

1,1-Dichloroethane ND 5.2 0.91 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

1,2-Dichloroethane ND 5.2 0.63 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

cis-1,2-Dichloroethene ND 5.2 0.99 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

trans-1,2-Dichloroethene ND 5.2 1.7 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

1,1-Dichloroethene ND 10 1.0 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

1,2-Dichloroethene, Total ND 5.2 0.40 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

1,2-Dichloropropane ND 5.2 0.63 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

cis-1,3-Dichloropropene ND 5.2 0.37 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

trans-1,3-Dichloropropene ND 5.2 0.31 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Ethylbenzene ND 21 1.9 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

2-Hexanone ND 5.2 1.7 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Methylene Chloride ND 21 0.77 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

4-Methyl-2-pentanone ND 5.2 0.37 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Styrene ND 5.2 0.42 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

1,1,2,2-Tetrachloroethane ND 5.2 0.34 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Tetrachloroethene ND 5.2 0.73 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Toluene ND 5.2 0.45 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

1,2,4-Trichlorobenzene ND 5.2 0.45 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

1,1,1-Trichloroethane ND 5.2 0.60 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

1,1,2-Trichloroethane ND 5.2 0.41 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Trichloroethene ND 5.2 0.82 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Vinyl acetate ND 5.2 0.45 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Vinyl chloride ND 10 0.89 ug/Kg 10/16/13 10:40 10/16/13 19:47 1

Xylenes, Total ND 4-Bromofluorobenzene (Surr) 99 63 - 150 10/16/13 10:40 10/16/13 19:47 1

Surrogate Dil Fac Analyzed Prepared Qualifier Limits

%Recovery 1,2-Dichloroethane-d4 (Surr) 107 10/16/13 10:40 10/16/13 19:47 1

72 - 127 Toluene-d8 (Surr) 95 10/16/13 10:40 10/16/13 19:47 1

80 - 120 Dibromofluoromethane (Surr) 105 10/16/13 10:40 10/16/13 19:47 1

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Client Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4124-6 Client Sample ID: 6703-03-L10-09-0018-SO Matrix: Solid Date Collected: 10/14/13 14:40 Percent Solids: 89.3 Date Received: 10/15/13 17:55 Method: 8260C - Volatile Organic Compounds by GC/MS RL MDL Acetone ND 19 6.2 ug/Kg

10/16/13 10:40 10/16/13 20:12 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier 4.8 0.24 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Benzene ND 4.8 0.24 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Bromodichloromethane ND 4.8 0.36 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Bromoform ND 9.6 1.1 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Methyl bromide ND 120 16 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

n-Butanol ND 19 1.8 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

2-Butanone ND 4.8 0.66 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Carbon disulfide ND 4.8 0.49 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Carbon tetrachloride ND 4.8 0.37 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Chlorobenzene ND 4.8 0.39 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Chlorodibromomethane ND 9.6 0.50 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Chloroethane ND 4.8 0.37 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Chloroform ND 9.6 0.63 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Chloromethane ND 9.6 1.4 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

1,2-Dibromo-3-Chloropropane ND 4.8 0.67 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

1,2-Dibromoethane ND 4.8 0.38 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

1,1-Dichloroethane ND 4.8 0.84 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

1,2-Dichloroethane ND 4.8 0.58 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

cis-1,2-Dichloroethene ND 4.8 0.90 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

trans-1,2-Dichloroethene ND 4.8 1.5 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

1,1-Dichloroethene ND 9.6 0.92 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

1,2-Dichloroethene, Total ND 4.8 0.37 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

1,2-Dichloropropane ND 4.8 0.58 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

cis-1,3-Dichloropropene ND 4.8 0.34 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

trans-1,3-Dichloropropene ND 4.8 0.29 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Ethylbenzene ND 19 1.7 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

2-Hexanone ND 4.8 1.5 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Methylene Chloride ND 19 0.70 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

4-Methyl-2-pentanone ND 4.8 0.34 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Styrene ND 4.8 0.38 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

1,1,2,2-Tetrachloroethane ND 4.8 0.31 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Tetrachloroethene 0.48 J

4.8 0.67 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Toluene ND 4.8 0.41 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

1,2,4-Trichlorobenzene ND 4.8 0.41 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

1,1,1-Trichloroethane ND 4.8 0.55 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

1,1,2-Trichloroethane ND 4.8 0.38 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Trichloroethene ND 4.8 0.75 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Vinyl acetate ND 4.8 0.41 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Vinyl chloride ND 9.6 0.82 ug/Kg 10/16/13 10:40 10/16/13 20:12 1

Xylenes, Total ND 4-Bromofluorobenzene (Surr) 97 63 - 150 10/16/13 10:40 10/16/13 20:12 1

Surrogate Dil Fac Analyzed Prepared Qualifier Limits

%Recovery 1,2-Dichloroethane-d4 (Surr) 110 10/16/13 10:40 10/16/13 20:12 1

72 - 127 Toluene-d8 (Surr) 95 10/16/13 10:40 10/16/13 20:12 1

80 - 120 Dibromofluoromethane (Surr) 105 10/16/13 10:40 10/16/13 20:12 1

70 - 126 TestAmerica St. Louis Page 16 of 32 1

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Client Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4124-7 Client Sample ID: 6703-03-L10-09-0019-SO Matrix: Solid Date Collected: 10/14/13 14:45 Percent Solids: 87.0 Date Received: 10/15/13 17:55 Method: 8270D - Semivolatile Organic Compounds (GC/MS)

RL MDL Acenaphthene ND 380 38 ug/Kg

10/16/13 10:27 10/16/13 16:51 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Acenaphthylene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Anthracene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Benzo(a)anthracene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Benzo(b)fluoranthene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Benzo(k)fluoranthene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Benzo(g,h,i) perylene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Benzo(a)pyrene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Chrysene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Dibenz(a,h)anthracene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Fluoranthene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Fluorene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Indeno(1,2,3-cd)pyrene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Naphthalene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Phenanthrene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 16:51 1

Pyrene ND 2-Fluorophenol (Surr) 59 53 - 97 10/16/13 10:27 10/16/13 16:51 1

Surrogate Dil Fac Analyzed Prepared Qualifier Limits

%Recovery 2,4,6-Tribromophenol (Surr) 49 10/16/13 10:27 10/16/13 16:51 1

46 - 111 Nitrobenzene-d5 (Surr) 66 10/16/13 10:27 10/16/13 16:51 1

55 - 98 Phenol-d5 (Surr) 59 10/16/13 10:27 10/16/13 16:51 1

54 - 101 Terphenyl-d14 (Surr) 77 10/16/13 10:27 10/16/13 16:51 1

58 - 123 2-Fluorobiphenyl (Surr) 64 10/16/13 10:27 10/16/13 16:51 1

56 - 97 Method: 6010C - Metals (ICP)

RL MDL Arsenic 7.2 1.1 0.71 mg/Kg

10/18/13 09:31 10/18/13 13:39 2

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Lab Sample ID: 160-4124-8 Client Sample ID: 6703-03-L10-09-0020-SO Matrix: Solid Date Collected: 10/14/13 14:50 Percent Solids: 86.8 Date Received: 10/15/13 17:55 Method: 8270D - Semivolatile Organic Compounds (GC/MS)

RL MDL Acenaphthene ND 380 38 ug/Kg

10/16/13 10:27 10/16/13 17:22 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Acenaphthylene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Anthracene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Benzo(a)anthracene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Benzo(b)fluoranthene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Benzo(k)fluoranthene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Benzo(g,h,i) perylene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Benzo(a)pyrene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Chrysene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Dibenz(a,h)anthracene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Fluoranthene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Fluorene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Indeno(1,2,3-cd)pyrene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Naphthalene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:22 1

Phenanthrene ND TestAmerica St. Louis Page 17 of 32 1

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Client Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4124-8 Client Sample ID: 6703-03-L10-09-0020-SO Matrix: Solid Date Collected: 10/14/13 14:50 Percent Solids: 86.8 Date Received: 10/15/13 17:55 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)

RL MDL Pyrene ND 380 38 ug/Kg

10/16/13 10:27 10/16/13 17:22 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier 2-Fluorophenol (Surr) 64 53 - 97 10/16/13 10:27 10/16/13 17:22 1

Surrogate Dil Fac Analyzed Prepared Qualifier Limits

%Recovery 2,4,6-Tribromophenol (Surr) 62 10/16/13 10:27 10/16/13 17:22 1

46 - 111 Nitrobenzene-d5 (Surr) 74 10/16/13 10:27 10/16/13 17:22 1

55 - 98 Phenol-d5 (Surr) 65 10/16/13 10:27 10/16/13 17:22 1

54 - 101 Terphenyl-d14 (Surr) 79 10/16/13 10:27 10/16/13 17:22 1

58 - 123 2-Fluorobiphenyl (Surr) 72 10/16/13 10:27 10/16/13 17:22 1

56 - 97 Method: 6010C - Metals (ICP)

RL MDL Arsenic 6.1 1.1 0.69 mg/Kg

10/18/13 09:31 10/18/13 13:59 2

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Lab Sample ID: 160-4124-9 Client Sample ID: 6703-03-L10-09-0021-SO Matrix: Solid Date Collected: 10/14/13 14:55 Percent Solids: 87.0 Date Received: 10/15/13 17:55 Method: 8270D - Semivolatile Organic Compounds (GC/MS)

RL MDL Acenaphthene ND 380 38 ug/Kg

10/16/13 10:27 10/16/13 17:54 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Acenaphthylene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Anthracene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Benzo(a)anthracene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Benzo(b)fluoranthene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Benzo(k)fluoranthene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Benzo(g,h,i) perylene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Benzo(a)pyrene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Chrysene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Dibenz(a,h)anthracene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Fluoranthene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Fluorene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Indeno(1,2,3-cd)pyrene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Naphthalene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Phenanthrene ND 380 38 ug/Kg 10/16/13 10:27 10/16/13 17:54 1

Pyrene ND 2-Fluorophenol (Surr) 62 53 - 97 10/16/13 10:27 10/16/13 17:54 1

Surrogate Dil Fac Analyzed Prepared Qualifier Limits

%Recovery 2,4,6-Tribromophenol (Surr) 61 10/16/13 10:27 10/16/13 17:54 1

46 - 111 Nitrobenzene-d5 (Surr) 70 10/16/13 10:27 10/16/13 17:54 1

55 - 98 Phenol-d5 (Surr) 63 10/16/13 10:27 10/16/13 17:54 1

54 - 101 Terphenyl-d14 (Surr) 99 10/16/13 10:27 10/16/13 17:54 1

58 - 123 2-Fluorobiphenyl (Surr) 69 10/16/13 10:27 10/16/13 17:54 1

56 - 97 Method: 6010C - Metals (ICP)

RL MDL Arsenic 8.5 1.0 0.65 mg/Kg

10/18/13 09:31 10/18/13 14:03 2

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier TestAmerica St. Louis Page 18 of 32 1

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Client Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4124-10 Client Sample ID: 6703-03-L10-09-0022-TB Matrix: Water Date Collected: 10/14/13 14:00 Date Received: 10/15/13 17:55 Method: 8260C - Volatile Organic Compounds (GC/MS)

RL MDL 1,1,1-Trichloroethane ND 1.0 0.070 ug/L 10/16/13 18:41 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier 1.0 0.10 ug/L 10/16/13 18:41 1

1,1,2,2-Tetrachloroethane ND 1.0 0.15 ug/L 10/16/13 18:41 1

1,1,2-Trichloroethane ND 1.0 0.080 ug/L 10/16/13 18:41 1

1,1-Dichloroethene ND 1.0 0.070 ug/L 10/16/13 18:41 1

1,1-Dichloroethane ND 1.0 0.080 ug/L 10/16/13 18:41 1

1,2,4-Trichlorobenzene ND 1.0 0.41 ug/L 10/16/13 18:41 1

1,2-Dibromo-3-Chloropropane ND 1.0 0.10 ug/L 10/16/13 18:41 1

1,2-Dichloroethane ND 2.0 0.15 ug/L 10/16/13 18:41 1

1,2-Dichloroethene, Total ND 1.0 0.10 ug/L 10/16/13 18:41 1

1,2-Dichloropropane ND 5.0 0.52 ug/L 10/16/13 18:41 1

2-Butanone ND 5.0 0.22 ug/L 10/16/13 18:41 1

2-Hexanone ND 5.0 0.12 ug/L 10/16/13 18:41 1

4-Methyl-2-pentanone ND 2.0 0.34 ug/L 10/16/13 18:41 1

Acetone ND 1.0 0.060 ug/L 10/16/13 18:41 1

Benzene ND 1.0 0.17 ug/L 10/16/13 18:41 1

Bromoform ND 2.0 0.25 ug/L 10/16/13 18:41 1

Methyl bromide ND 1.0 0.050 ug/L 10/16/13 18:41 1

Carbon disulfide ND 1.0 0.13 ug/L 10/16/13 18:41 1

Carbon tetrachloride ND 1.0 0.15 ug/L 10/16/13 18:41 1

Chlorobenzene ND 1.0 0.13 ug/L 10/16/13 18:41 1

Chlorodibromomethane ND 2.0 0.10 ug/L 10/16/13 18:41 1

Chloroethane ND 1.0 0.10 ug/L 10/16/13 18:41 1

Chloroform ND 2.0 0.080 ug/L 10/16/13 18:41 1

Chloromethane ND 1.0 0.090 ug/L 10/16/13 18:41 1

cis-1,2-Dichloroethene ND 1.0 0.070 ug/L 10/16/13 18:41 1

cis-1,3-Dichloropropene ND 1.0 0.090 ug/L 10/16/13 18:41 1

Bromodichloromethane ND 1.0 0.090 ug/L 10/16/13 18:41 1

Ethylbenzene ND 1.0 0.13 ug/L 10/16/13 18:41 1

1,2-Dibromoethane ND 1.0 0.27 ug/L 10/16/13 18:41 1

Methylene Chloride ND 50 12 ug/L 10/16/13 18:41 1

n-Butanol ND 1.0 0.070 ug/L 10/16/13 18:41 1

Styrene ND 1.0 0.18 ug/L 10/16/13 18:41 1

Tetrachloroethene ND 1.0 0.070 ug/L 10/16/13 18:41 1

Toluene ND 1.0 0.080 ug/L 10/16/13 18:41 1

trans-1,2-Dichloroethene ND 1.0 0.080 ug/L 10/16/13 18:41 1

trans-1,3-Dichloropropene ND 1.0 0.25 ug/L 10/16/13 18:41 1

Trichloroethene ND 2.0 0.18 ug/L 10/16/13 18:41 1

Vinyl acetate ND 2.0 0.080 ug/L 10/16/13 18:41 1

Vinyl chloride ND 3.0 0.20 ug/L 10/16/13 18:41 1

Xylenes, Total ND 1,2-Dichloroethane-d4 (Surr) 101 75 - 129 10/16/13 18:41 1

Surrogate Dil Fac Analyzed Prepared Qualifier Limits

%Recovery 4-Bromofluorobenzene (Surr) 108 10/16/13 18:41 1

81 - 130 Dibromofluoromethane (Surr) 111 10/16/13 18:41 1

81 - 124 Toluene-d8 (Surr) 108 10/16/13 18:41 1

87 - 128 TestAmerica St. Louis Page 19 of 32 1

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QC Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 8260C - Volatile Organic Compounds (GC/MS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-79367/2 Matrix: Water Prep Type: Total/NA Analysis Batch: 79367 RL MDL 1,1,1-Trichloroethane ND 1.0 0.070 ug/L 10/16/13 11:17 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier ND 0.10 1.0 ug/L 10/16/13 11:17 1

1,1,2,2-Tetrachloroethane ND 0.15 1.0 ug/L 10/16/13 11:17 1

1,1,2-Trichloroethane ND 0.080 1.0 ug/L 10/16/13 11:17 1

1,1-Dichloroethene ND 0.070 1.0 ug/L 10/16/13 11:17 1

1,1-Dichloroethane ND 0.080 1.0 ug/L 10/16/13 11:17 1

1,2,4-Trichlorobenzene ND 0.41 1.0 ug/L 10/16/13 11:17 1

1,2-Dibromo-3-Chloropropane ND 0.10 1.0 ug/L 10/16/13 11:17 1

1,2-Dichloroethane ND 0.15 2.0 ug/L 10/16/13 11:17 1

1,2-Dichloroethene, Total ND 0.10 1.0 ug/L 10/16/13 11:17 1

1,2-Dichloropropane ND 0.52 5.0 ug/L 10/16/13 11:17 1

2-Butanone ND 0.22 5.0 ug/L 10/16/13 11:17 1

2-Hexanone ND 0.12 5.0 ug/L 10/16/13 11:17 1

4-Methyl-2-pentanone ND 0.34 2.0 ug/L 10/16/13 11:17 1

Acetone ND 0.060 1.0 ug/L 10/16/13 11:17 1

Benzene ND 0.17 1.0 ug/L 10/16/13 11:17 1

Bromoform ND 0.25 2.0 ug/L 10/16/13 11:17 1

Methyl bromide ND 0.050 1.0 ug/L 10/16/13 11:17 1

Carbon disulfide ND 0.13 1.0 ug/L 10/16/13 11:17 1

Carbon tetrachloride ND 0.15 1.0 ug/L 10/16/13 11:17 1

Chlorobenzene ND 0.13 1.0 ug/L 10/16/13 11:17 1

Chlorodibromomethane ND 0.10 2.0 ug/L 10/16/13 11:17 1

Chloroethane ND 0.10 1.0 ug/L 10/16/13 11:17 1

Chloroform ND 0.080 2.0 ug/L 10/16/13 11:17 1

Chloromethane ND 0.090 1.0 ug/L 10/16/13 11:17 1

cis-1,2-Dichloroethene ND 0.070 1.0 ug/L 10/16/13 11:17 1

cis-1,3-Dichloropropene ND 0.090 1.0 ug/L 10/16/13 11:17 1

Bromodichloromethane ND 0.090 1.0 ug/L 10/16/13 11:17 1

Ethylbenzene ND 0.13 1.0 ug/L 10/16/13 11:17 1

1,2-Dibromoethane ND 0.27 1.0 ug/L 10/16/13 11:17 1

Methylene Chloride ND 12 50 ug/L 10/16/13 11:17 1

n-Butanol ND 0.070 1.0 ug/L 10/16/13 11:17 1

Styrene ND 0.18 1.0 ug/L 10/16/13 11:17 1

Tetrachloroethene ND 0.070 1.0 ug/L 10/16/13 11:17 1

Toluene ND 0.080 1.0 ug/L 10/16/13 11:17 1

trans-1,2-Dichloroethene ND 0.080 1.0 ug/L 10/16/13 11:17 1

trans-1,3-Dichloropropene ND 0.25 1.0 ug/L 10/16/13 11:17 1

Trichloroethene ND 0.18 2.0 ug/L 10/16/13 11:17 1

Vinyl acetate ND 0.080 2.0 ug/L 10/16/13 11:17 1

Vinyl chloride ND 0.20 3.0 ug/L 10/16/13 11:17 1

Xylenes, Total 1,2-Dichloroethane-d4 (Surr) 103 75 - 129 10/16/13 11:17 1

MB MB Surrogate Dil Fac Prepared Analyzed Qualifier Limits

%Recovery 112 10/16/13 11:17 1

4-Bromofluorobenzene (Surr) 81 - 130 111 10/16/13 11:17 1

Dibromofluoromethane (Surr) 81 - 124 109 10/16/13 11:17 1

Toluene-d8 (Surr) 87 - 128 TestAmerica St. Louis Page 20 of 32 1

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QC Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-79367/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 79367 1,1,1-Trichloroethane 10.0 10.0 ug/L 100 85 - 116 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits 1,1,2,2-Tetrachloroethane 10.0 9.46 ug/L 95 80 - 120 1,1,2-Trichloroethane 10.0 9.59 ug/L 96 80 - 120 1,1-Dichloroethene 10.0 9.58 ug/L 96 80 - 120 1,1-Dichloroethane 10.0 10.3 ug/L 103 80 - 120 1,2,4-Trichlorobenzene 10.0 9.84 ug/L 98 75 - 121 1,2-Dibromo-3-Chloropropane 10.0 8.71 ug/L 87 73 - 123 1,2-Dichloroethane 10.0 9.84 ug/L 98 80 - 115 1,2-Dichloroethene, Total 20.0 19.6 ug/L 98 80 - 120 1,2-Dichloropropane 10.0 9.97 ug/L 100 80 - 120 2-Butanone 10.0 9.48 ug/L 95 67 - 127 2-Hexanone 10.0 8.89 ug/L 89 70 - 123 4-Methyl-2-pentanone 10.0 7.88 ug/L 79 75 - 126 Acetone 10.0 8.77 ug/L 88 69 - 129 Benzene 10.0 9.96 ug/L 100 80 - 120 Bromoform 10.0 9.86 ug/L 99 80 - 120 Methyl bromide 10.0 11.6 ug/L 116 70 - 124 Carbon disulfide 10.0 10.1 ug/L 101 80 - 121 Carbon tetrachloride 10.0 10.2 ug/L 102 83 - 125 Chlorobenzene 10.0 9.84 ug/L 98 80 - 120 Chlorodibromomethane 10.0 9.53 ug/L 95 80 - 120 Chloroethane 10.0 9.64 ug/L 96 73 - 119 Chloroform 10.0 9.72 ug/L 97 80 - 120 Chloromethane 10.0 10.3 ug/L 103 72 - 124 cis-1,2-Dichloroethene 10.0 9.77 ug/L 98 80 - 120 cis-1,3-Dichloropropene 10.0 9.99 ug/L 100 80 - 120 Bromodichloromethane 10.0 10.0 ug/L 100 80 - 120 Ethylbenzene 10.0 10.2 ug/L 102 80 - 120 1,2-Dibromoethane 10.0 9.10 ug/L 91 80 - 120 Methylene Chloride 10.0 9.29 ug/L 93 80 - 120 n-Butanol 250 212 ug/L 85 62 - 128 Styrene 10.0 9.78 ug/L 98 81 - 133 Tetrachloroethene 10.0 9.79 ug/L 98 83 - 123 Toluene 10.0 9.99 ug/L 100 80 - 120 trans-1,2-Dichloroethene 10.0 9.85 ug/L 98 80 - 120 trans-1,3-Dichloropropene 10.0 10.0 ug/L 100 82 - 124 Trichloroethene 10.0 9.56 ug/L 96 80 - 120 Vinyl acetate 10.0 9.78 ug/L 98 63 - 140 Vinyl chloride 10.0 9.85 ug/L 99 77 - 122 1,2-Dichloroethane-d4 (Surr) 75 - 129 Surrogate 98 LCS LCS Qualifier Limits

%Recovery 97 4-Bromofluorobenzene (Surr) 81 - 130 107 Dibromofluoromethane (Surr) 81 - 124 98 Toluene-d8 (Surr) 87 - 128 TestAmerica St. Louis Page 21 of 32 1

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QC Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 160-79367/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 79367 1,1,1-Trichloroethane 10.0 10.0 ug/L 100 85 - 116 0

20 Analyte LCSD LCSD D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Limit RPD RPD 1,1,2,2-Tetrachloroethane 10.0 10.3 ug/L 103 80 - 120 8

20 1,1,2-Trichloroethane 10.0 10.1 ug/L 101 80 - 120 5

20 1,1-Dichloroethene 10.0 9.56 ug/L 96 80 - 120 0

20 1,1-Dichloroethane 10.0 10.1 ug/L 101 80 - 120 2

20 1,2,4-Trichlorobenzene 10.0 10.1 ug/L 101 75 - 121 2

20 1,2-Dibromo-3-Chloropropane 10.0 10.0 ug/L 100 73 - 123 14 20 1,2-Dichloroethane 10.0 10.3 ug/L 103 80 - 115 5

20 1,2-Dichloroethene, Total 20.0 19.3 ug/L 97 80 - 120 2

20 1,2-Dichloropropane 10.0 10.3 ug/L 103 80 - 120 3

20 2-Butanone 10.0 10.5 ug/L 105 67 - 127 10 20 2-Hexanone 10.0 10.7 ug/L 107 70 - 123 18 20 4-Methyl-2-pentanone 10.0 9.00 ug/L 90 75 - 126 13 20 Acetone 10.0 11.1 ug/L 111 69 - 129 23 20 Benzene 10.0 9.96 ug/L 100 80 - 120 0

20 Bromoform 10.0 10.4 ug/L 104 80 - 120 5

20 Methyl bromide 10.0 11.5 ug/L 115 70 - 124 1

20 Carbon disulfide 10.0 9.95 ug/L 99 80 - 121 2

20 Carbon tetrachloride 10.0 10.1 ug/L 101 83 - 125 0

20 Chlorobenzene 10.0 9.83 ug/L 98 80 - 120 0

20 Chlorodibromomethane 10.0 10.2 ug/L 102 80 - 120 7

20 Chloroethane 10.0 9.38 ug/L 94 73 - 119 3

20 Chloroform 10.0 9.91 ug/L 99 80 - 120 2

20 Chloromethane 10.0 10.1 ug/L 101 72 - 124 2

20 cis-1,2-Dichloroethene 10.0 9.71 ug/L 97 80 - 120 1

20 cis-1,3-Dichloropropene 10.0 10.4 ug/L 104 80 - 120 4

20 Bromodichloromethane 10.0 10.3 ug/L 103 80 - 120 3

20 Ethylbenzene 10.0 10.1 ug/L 101 80 - 120 2

20 1,2-Dibromoethane 10.0 9.69 ug/L 97 80 - 120 6

20 Methylene Chloride 10.0 9.54 ug/L 95 80 - 120 3

20 n-Butanol 250 243 ug/L 97 62 - 128 14 20 Styrene 10.0 10.0 ug/L 100 81 - 133 3

20 Tetrachloroethene 10.0 9.66 ug/L 97 83 - 123 1

20 Toluene 10.0 9.86 ug/L 99 80 - 120 1

20 trans-1,2-Dichloroethene 10.0 9.61 ug/L 96 80 - 120 2

20 trans-1,3-Dichloropropene 10.0 10.4 ug/L 104 82 - 124 4

20 Trichloroethene 10.0 9.28 ug/L 93 80 - 120 3

20 Vinyl acetate 10.0 10.6 ug/L 106 63 - 140 8

20 Vinyl chloride 10.0 9.51 ug/L 95 77 - 122 4

20 1,2-Dichloroethane-d4 (Surr) 75 - 129 Surrogate 104 LCSD LCSD Qualifier Limits

%Recovery 100 4-Bromofluorobenzene (Surr) 81 - 130 111 Dibromofluoromethane (Surr) 81 - 124 98 Toluene-d8 (Surr) 87 - 128 TestAmerica St. Louis Page 22 of 32 1

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QC Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 8260C - Volatile Organic Compounds by GC/MS Client Sample ID: Method Blank Lab Sample ID: MB 160-79123/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 79538 Prep Batch: 79123 RL MDL Acetone ND 20 6.5 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier ND 0.25 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Benzene ND 0.25 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Bromodichloromethane ND 0.37 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Bromoform ND 1.1 10 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Methyl bromide ND 16 130 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

n-Butanol ND 1.9 20 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

2-Butanone ND 0.69 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Carbon disulfide ND 0.51 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Carbon tetrachloride ND 0.38 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Chlorobenzene ND 0.41 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Chlorodibromomethane ND 0.52 10 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Chloroethane ND 0.38 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Chloroform ND 0.65 10 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Chloromethane ND 1.5 10 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

1,2-Dibromo-3-Chloropropane ND 0.70 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

1,2-Dibromoethane ND 0.39 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

1,1-Dichloroethane ND 0.87 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

1,2-Dichloroethane ND 0.60 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

cis-1,2-Dichloroethene ND 0.94 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

trans-1,2-Dichloroethene ND 1.6 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

1,1-Dichloroethene ND 0.96 10 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

1,2-Dichloroethene, Total ND 0.38 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

1,2-Dichloropropane ND 0.60 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

cis-1,3-Dichloropropene ND 0.35 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

trans-1,3-Dichloropropene ND 0.30 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Ethylbenzene ND 1.8 20 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

2-Hexanone ND 1.6 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Methylene Chloride ND 0.73 20 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

4-Methyl-2-pentanone ND 0.35 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Styrene ND 0.40 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

1,1,2,2-Tetrachloroethane ND 0.32 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Tetrachloroethene ND 0.70 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Toluene ND 0.43 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

1,2,4-Trichlorobenzene ND 0.43 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

1,1,1-Trichloroethane ND 0.57 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

1,1,2-Trichloroethane ND 0.39 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Trichloroethene ND 0.78 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Vinyl acetate ND 0.43 5.0 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Vinyl chloride ND 0.85 10 ug/Kg 10/16/13 10:40 10/16/13 13:07 1

Xylenes, Total 4-Bromofluorobenzene (Surr) 94 63 - 150 10/16/13 13:07 1

MB MB Surrogate 10/16/13 10:40 Dil Fac Prepared Analyzed Qualifier Limits

%Recovery 93 10/16/13 10:40 10/16/13 13:07 1

1,2-Dichloroethane-d4 (Surr) 72 - 127 95 10/16/13 10:40 10/16/13 13:07 1

Toluene-d8 (Surr) 80 - 120 96 10/16/13 10:40 10/16/13 13:07 1

Dibromofluoromethane (Surr) 70 - 126 TestAmerica St. Louis Page 23 of 32 1

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QC Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)

Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-79123/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 79538 Prep Batch: 79123 Acetone 50.0 46.6 ug/Kg 93 59 - 129 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Benzene 50.0 47.8 ug/Kg 96 80 - 120 Bromodichloromethane 50.0 49.1 ug/Kg 98 80 - 120 Bromoform 50.0 49.1 ug/Kg 98 84 - 126 Methyl bromide 50.0 46.9 ug/Kg 94 74 - 128 n-Butanol 1250 1550 ug/Kg 124 60 - 140 2-Butanone 50.0 50.9 ug/Kg 102 61 - 134 Carbon disulfide 50.0 49.9 ug/Kg 100 79 - 121 Carbon tetrachloride 50.0 50.5 ug/Kg 101 80 - 125 Chlorobenzene 50.0 48.7 ug/Kg 97 80 - 120 Chlorodibromomethane 50.0 50.9 ug/Kg 102 80 - 120 Chloroethane 50.0 49.2 ug/Kg 98 73 - 129 Chloroform 50.0 48.8 ug/Kg 98 80 - 120 Chloromethane 50.0 49.4 ug/Kg 99 70 - 129 1,2-Dibromo-3-Chloropropane 50.0 52.5 ug/Kg 105 75 - 129 1,2-Dibromoethane 50.0 50.2 ug/Kg 100 80 - 120 1,1-Dichloroethane 50.0 48.9 ug/Kg 98 80 - 120 1,2-Dichloroethane 50.0 48.6 ug/Kg 97 76 - 125 cis-1,2-Dichloroethene 50.0 50.4 ug/Kg 101 80 - 120 trans-1,2-Dichloroethene 50.0 52.3 ug/Kg 105 80 - 120 1,1-Dichloroethene 50.0 50.6 ug/Kg 101 80 - 120 1,2-Dichloroethene, Total 100 103 ug/Kg 103 80 - 120 1,2-Dichloropropane 50.0 47.4 ug/Kg 95 80 - 120 cis-1,3-Dichloropropene 50.0 49.7 ug/Kg 99 80 - 125 trans-1,3-Dichloropropene 50.0 49.7 ug/Kg 99 82 - 124 Ethylbenzene 50.0 48.5 ug/Kg 97 80 - 120 2-Hexanone 50.0 54.2 ug/Kg 108 71 - 127 Methylene Chloride 50.0 51.2 ug/Kg 102 80 - 120 4-Methyl-2-pentanone 50.0 49.1 ug/Kg 98 75 - 127 Styrene 50.0 50.6 ug/Kg 101 80 - 120 1,1,2,2-Tetrachloroethane 50.0 45.9 ug/Kg 92 78 - 121 Tetrachloroethene 50.0 48.0 ug/Kg 96 80 - 120 Toluene 50.0 49.2 ug/Kg 98 80 - 120 1,2,4-Trichlorobenzene 50.0 57.1 ug/Kg 114 75 - 124 1,1,1-Trichloroethane 50.0 48.9 ug/Kg 98 81 - 124 1,1,2-Trichloroethane 50.0 48.7 ug/Kg 97 80 - 120 Trichloroethene 50.0 46.9 ug/Kg 94 80 - 120 Vinyl acetate 50.0 53.1 ug/Kg 106 67 - 134 Vinyl chloride 50.0 50.2 ug/Kg 100 65 - 123 4-Bromofluorobenzene (Surr) 63 - 150 Surrogate 98 LCS LCS Qualifier Limits

%Recovery 96 1,2-Dichloroethane-d4 (Surr) 72 - 127 102 Toluene-d8 (Surr) 80 - 120 100 Dibromofluoromethane (Surr) 70 - 126 TestAmerica St. Louis Page 24 of 32 1

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QC Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)

Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 160-79123/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 79538 Prep Batch: 79123 Acetone 50.0 48.7 ug/Kg 97 59 - 129 4

20 Analyte LCSD LCSD D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Limit RPD RPD Benzene 50.0 47.9 ug/Kg 96 80 - 120 0

20 Bromodichloromethane 50.0 50.0 ug/Kg 100 80 - 120 2

20 Bromoform 50.0 49.0 ug/Kg 98 84 - 126 0

20 Methyl bromide 50.0 44.6 ug/Kg 89 74 - 128 5

20 n-Butanol 1250 1530 ug/Kg 122 60 - 140 1

20 2-Butanone 50.0 59.1 ug/Kg 118 61 - 134 15 20 Carbon disulfide 50.0 48.4 ug/Kg 97 79 - 121 3

20 Carbon tetrachloride 50.0 48.7 ug/Kg 97 80 - 125 4

20 Chlorobenzene 50.0 48.2 ug/Kg 96 80 - 120 1

20 Chlorodibromomethane 50.0 49.8 ug/Kg 100 80 - 120 2

20 Chloroethane 50.0 48.1 ug/Kg 96 73 - 129 2

20 Chloroform 50.0 48.6 ug/Kg 97 80 - 120 0

20 Chloromethane 50.0 48.9 ug/Kg 98 70 - 129 1

20 1,2-Dibromo-3-Chloropropane 50.0 52.8 ug/Kg 106 75 - 129 1

20 1,2-Dibromoethane 50.0 49.9 ug/Kg 100 80 - 120 1

20 1,1-Dichloroethane 50.0 48.9 ug/Kg 98 80 - 120 0

20 1,2-Dichloroethane 50.0 48.4 ug/Kg 97 76 - 125 0

20 cis-1,2-Dichloroethene 50.0 51.0 ug/Kg 102 80 - 120 1

20 trans-1,2-Dichloroethene 50.0 51.6 ug/Kg 103 80 - 120 1

20 1,1-Dichloroethene 50.0 49.8 ug/Kg 100 80 - 120 1

20 1,2-Dichloroethene, Total 100 103 ug/Kg 103 80 - 120 0

20 1,2-Dichloropropane 50.0 49.8 ug/Kg 100 80 - 120 5

20 cis-1,3-Dichloropropene 50.0 51.3 ug/Kg 103 80 - 125 3

20 trans-1,3-Dichloropropene 50.0 49.0 ug/Kg 98 82 - 124 2

20 Ethylbenzene 50.0 48.3 ug/Kg 97 80 - 120 0

20 2-Hexanone 50.0 55.4 ug/Kg 111 71 - 127 2

20 Methylene Chloride 50.0 50.7 ug/Kg 101 80 - 120 1

20 4-Methyl-2-pentanone 50.0 48.1 ug/Kg 96 75 - 127 2

20 Styrene 50.0 50.3 ug/Kg 101 80 - 120 1

20 1,1,2,2-Tetrachloroethane 50.0 46.5 ug/Kg 93 78 - 121 1

20 Tetrachloroethene 50.0 48.9 ug/Kg 98 80 - 120 2

20 Toluene 50.0 49.7 ug/Kg 99 80 - 120 1

20 1,2,4-Trichlorobenzene 50.0 54.6 ug/Kg 109 75 - 124 4

20 1,1,1-Trichloroethane 50.0 47.7 ug/Kg 95 81 - 124 2

20 1,1,2-Trichloroethane 50.0 50.0 ug/Kg 100 80 - 120 3

20 Trichloroethene 50.0 46.9 ug/Kg 94 80 - 120 0

20 Vinyl acetate 50.0 50.9 ug/Kg 102 67 - 134 4

20 Vinyl chloride 50.0 49.1 ug/Kg 98 65 - 123 2

20 4-Bromofluorobenzene (Surr) 63 - 150 Surrogate 103 LCSD LCSD Qualifier Limits

%Recovery 98 1,2-Dichloroethane-d4 (Surr) 72 - 127 102 Toluene-d8 (Surr) 80 - 120 101 Dibromofluoromethane (Surr) 70 - 126 TestAmerica St. Louis Page 25 of 32 1

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QC Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 8270D - Semivolatile Organic Compounds (GC/MS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-79122/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 79507 Prep Batch: 79122 RL MDL Acenaphthene ND 330 33 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Acenaphthylene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Anthracene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Benzo(a)anthracene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Benzo(b)fluoranthene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Benzo(k)fluoranthene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Benzo(g,h,i) perylene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Benzo(a)pyrene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Chrysene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Dibenz(a,h)anthracene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Fluoranthene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Fluorene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Indeno(1,2,3-cd)pyrene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Naphthalene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Phenanthrene ND 33 330 ug/Kg 10/16/13 10:27 10/16/13 15:16 1

Pyrene 2-Fluorophenol (Surr) 82 53 - 97 10/16/13 15:16 1

MB MB Surrogate 10/16/13 10:27 Dil Fac Prepared Analyzed Qualifier Limits

%Recovery 71 10/16/13 10:27 10/16/13 15:16 1

2,4,6-Tribromophenol (Surr) 46 - 111 89 10/16/13 10:27 10/16/13 15:16 1

Nitrobenzene-d5 (Surr) 55 - 98 83 10/16/13 10:27 10/16/13 15:16 1

Phenol-d5 (Surr) 54 - 101 96 10/16/13 10:27 10/16/13 15:16 1

Terphenyl-d14 (Surr) 58 - 123 88 10/16/13 10:27 10/16/13 15:16 1

2-Fluorobiphenyl (Surr) 56 - 97 Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-79122/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 79507 Prep Batch: 79122 Acenaphthene 3330 2660 ug/Kg 80 63 - 95 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Acenaphthylene 3330 2700 ug/Kg 81 62 - 98 Anthracene 3330 2760 ug/Kg 83 63 - 100 Benzo(a)anthracene 3330 3000 ug/Kg 90 74 - 114 Benzo(b)fluoranthene 3330 2770 ug/Kg 83 68 - 109 Benzo(k)fluoranthene 3330 2880 ug/Kg 86 69 - 111 Benzo(g,h,i) perylene 3330 2670 ug/Kg 80 67 - 121 Benzo(a)pyrene 3330 2740 ug/Kg 82 63 - 103 Chrysene 3330 2630 ug/Kg 79 66 - 100 Dibenz(a,h)anthracene 3330 2710 ug/Kg 81 67 - 114 Fluoranthene 3330 2690 ug/Kg 81 63 - 101 Fluorene 3330 2540 ug/Kg 76 62 - 96 Indeno(1,2,3-cd)pyrene 3330 2760 ug/Kg 83 65 - 120 Naphthalene 3330 2520 ug/Kg 76 60 - 90 Phenanthrene 3330 2780 ug/Kg 84 63 - 99 Pyrene 3330 2850 ug/Kg 85 64 - 102 TestAmerica St. Louis Page 26 of 32 1

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QC Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-79122/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 79507 Prep Batch: 79122 2-Fluorophenol (Surr) 53 - 97 Surrogate 73 LCS LCS Qualifier Limits

%Recovery 69 2,4,6-Tribromophenol (Surr) 46 - 111 81 Nitrobenzene-d5 (Surr) 55 - 98 75 Phenol-d5 (Surr) 54 - 101 76 Terphenyl-d14 (Surr) 58 - 123 81 2-Fluorobiphenyl (Surr) 56 - 97 Client Sample ID: Matrix Spike Lab Sample ID: 160-4123-B-4-B MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 79507 Prep Batch: 79122 Acenaphthene ND 4220 3250 ug/Kg 77 57 - 94

Analyte MS MS D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Acenaphthylene ND 4220 3320 ug/Kg 79 57 - 97

Anthracene ND 4220 3560 ug/Kg 84 58 - 99

Benzo(a)anthracene ND 4220 3940 ug/Kg 94 68 - 114

Benzo(b)fluoranthene ND 4220 3570 ug/Kg 85 63 - 107

Benzo(k)fluoranthene ND 4220 3790 ug/Kg 90 65 - 108

Benzo(g,h,i) perylene ND 4220 3630 ug/Kg 86 54 - 127

Benzo(a)pyrene ND 4220 3570 ug/Kg 85 61 - 102

Chrysene ND 4220 3460 ug/Kg 82 61 - 100

Dibenz(a,h)anthracene ND 4220 3690 ug/Kg 87 59 - 118

Fluoranthene ND 4220 3600 ug/Kg 85 58 - 103

Fluorene ND 4220 3240 ug/Kg 77 58 - 97

Indeno(1,2,3-cd)pyrene ND 4220 3780 ug/Kg 90 56 - 123

Naphthalene ND 4220 2740 ug/Kg 65 52 - 86

Phenanthrene ND 4220 3620 ug/Kg 86 60 - 98

Pyrene ND 4220 3620 ug/Kg 86 53 - 106

2-Fluorophenol (Surr) 53 - 97 Surrogate 65 MS MS Qualifier Limits

%Recovery 73 2,4,6-Tribromophenol (Surr) 46 - 111 74 Nitrobenzene-d5 (Surr) 55 - 98 67 Phenol-d5 (Surr) 54 - 101 91 Terphenyl-d14 (Surr) 58 - 123 78 2-Fluorobiphenyl (Surr) 56 - 97 Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-4123-B-4-C MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 79507 Prep Batch: 79122 Acenaphthene ND 4190 3290 ug/Kg 78 57 - 94 1

30

Analyte MSD MSD D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Limit RPD RPD Acenaphthylene ND 4190 3340 ug/Kg 80 57 - 97 1

30

Anthracene ND 4190 3550 ug/Kg 85 58 - 99 0

30

Benzo(a)anthracene ND 4190 3910 ug/Kg 93 68 - 114 1

30

Benzo(b)fluoranthene ND 4190 3590 ug/Kg 86 63 - 107 1

30

Benzo(k)fluoranthene ND 4190 3670 ug/Kg 88 65 - 108 3

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QC Sample Results TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-4123-B-4-C MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 79507 Prep Batch: 79122 Benzo(g,h,i) perylene ND 4190 3680 ug/Kg 88 54 - 127 1

30

Analyte MSD MSD D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Limit RPD RPD Benzo(a)pyrene ND 4190 3550 ug/Kg 85 61 - 102 1

30

Chrysene ND 4190 3450 ug/Kg 82 61 - 100 1

30

Dibenz(a,h)anthracene ND 4190 3760 ug/Kg 90 59 - 118 2

30

Fluoranthene ND 4190 3510 ug/Kg 84 58 - 103 3

30

Fluorene ND 4190 3230 ug/Kg 77 58 - 97 0

30

Indeno(1,2,3-cd)pyrene ND 4190 3850 ug/Kg 92 56 - 123 2

30

Naphthalene ND 4190 2840 ug/Kg 68 52 - 86 3

30

Phenanthrene ND 4190 3590 ug/Kg 86 60 - 98 1

30

Pyrene ND 4190 3630 ug/Kg 87 53 - 106 0

30

2-Fluorophenol (Surr) 53 - 97 Surrogate 68 MSD MSD Qualifier Limits

%Recovery 70 2,4,6-Tribromophenol (Surr) 46 - 111 77 Nitrobenzene-d5 (Surr) 55 - 98 72 Phenol-d5 (Surr) 54 - 101 77 Terphenyl-d14 (Surr) 58 - 123 80 2-Fluorobiphenyl (Surr) 56 - 97 Method: 6010C - Metals (ICP)

Client Sample ID: Method Blank Lab Sample ID: MB 160-79708/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 79757 Prep Batch: 79708 RL MDL Arsenic ND 0.49 0.31 mg/Kg 10/18/13 09:31 10/18/13 13:32 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-79708/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 79757 Prep Batch: 79708 Arsenic 90.8 95.2 mg/Kg 105 70 - 131 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Client Sample ID: 6703-03-L10-09-0019-SO Lab Sample ID: 160-4124-7 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 79757 Prep Batch: 79708 Arsenic 7.2 114 98.9 mg/Kg 80 75 - 125

Analyte MS MS D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Client Sample ID: 6703-03-L10-09-0019-SO Lab Sample ID: 160-4124-7 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 79757 Prep Batch: 79708 Arsenic 7.2 102 89.4 mg/Kg 80 75 - 125 10 30

Analyte MSD MSD D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Limit RPD RPD TestAmerica St. Louis Page 28 of 32 1

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QC Association Summary TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

GC/MS VOA Prep Batch: 79123 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035 160-4124-1 6703-03-L10-09-0013-SO Total/NA Solid 5035 160-4124-2 6703-03-L10-09-0014-SO Total/NA Solid 5035 160-4124-3 6703-03-L10-09-0015-SO Total/NA Solid 5035 160-4124-4 6703-03-L10-09-0016-SO Total/NA Solid 5035 160-4124-5 6703-03-L10-09-0017-SO Total/NA Solid 5035 160-4124-6 6703-03-L10-09-0018-SO Total/NA Solid 5035 LCS 160-79123/2-A Lab Control Sample Total/NA Solid 5035 LCSD 160-79123/3-A Lab Control Sample Dup Total/NA Solid 5035 MB 160-79123/1-A Method Blank Total/NA Analysis Batch: 79367 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 8260C 160-4124-10 6703-03-L10-09-0022-TB Total/NA Water 8260C LCS 160-79367/4 Lab Control Sample Total/NA Water 8260C LCSD 160-79367/5 Lab Control Sample Dup Total/NA Water 8260C MB 160-79367/2 Method Blank Total/NA Analysis Batch: 79538 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260C 79123 160-4124-1 6703-03-L10-09-0013-SO Total/NA Solid 8260C 79123 160-4124-2 6703-03-L10-09-0014-SO Total/NA Solid 8260C 79123 160-4124-3 6703-03-L10-09-0015-SO Total/NA Solid 8260C 79123 160-4124-4 6703-03-L10-09-0016-SO Total/NA Solid 8260C 79123 160-4124-5 6703-03-L10-09-0017-SO Total/NA Solid 8260C 79123 160-4124-6 6703-03-L10-09-0018-SO Total/NA Solid 8260C 79123 LCS 160-79123/2-A Lab Control Sample Total/NA Solid 8260C 79123 LCSD 160-79123/3-A Lab Control Sample Dup Total/NA Solid 8260C 79123 MB 160-79123/1-A Method Blank Total/NA GC/MS Semi VOA Prep Batch: 79122 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3550C 160-4123-B-4-B MS Matrix Spike Total/NA Solid 3550C 160-4123-B-4-C MSD Matrix Spike Duplicate Total/NA Solid 3550C 160-4124-7 6703-03-L10-09-0019-SO Total/NA Solid 3550C 160-4124-8 6703-03-L10-09-0020-SO Total/NA Solid 3550C 160-4124-9 6703-03-L10-09-0021-SO Total/NA Solid 3550C LCS 160-79122/2-A Lab Control Sample Total/NA Solid 3550C MB 160-79122/1-A Method Blank Total/NA Analysis Batch: 79507 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270D 79122 160-4123-B-4-B MS Matrix Spike Total/NA Solid 8270D 79122 160-4123-B-4-C MSD Matrix Spike Duplicate Total/NA Solid 8270D 79122 160-4124-7 6703-03-L10-09-0019-SO Total/NA Solid 8270D 79122 160-4124-8 6703-03-L10-09-0020-SO Total/NA Solid 8270D 79122 160-4124-9 6703-03-L10-09-0021-SO Total/NA Solid 8270D 79122 LCS 160-79122/2-A Lab Control Sample Total/NA Solid 8270D 79122 MB 160-79122/1-A Method Blank Total/NA TestAmerica St. Louis Page 29 of 32 1

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QC Association Summary TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Metals Prep Batch: 79708 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3050B 160-4124-7 6703-03-L10-09-0019-SO Total/NA Solid 3050B 160-4124-7 MS 6703-03-L10-09-0019-SO Total/NA Solid 3050B 160-4124-7 MSD 6703-03-L10-09-0019-SO Total/NA Solid 3050B 160-4124-8 6703-03-L10-09-0020-SO Total/NA Solid 3050B 160-4124-9 6703-03-L10-09-0021-SO Total/NA Solid 3050B LCS 160-79708/2-A Lab Control Sample Total/NA Solid 3050B MB 160-79708/1-A Method Blank Total/NA Analysis Batch: 79757 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010C 79708 160-4124-7 6703-03-L10-09-0019-SO Total/NA Solid 6010C 79708 160-4124-7 MS 6703-03-L10-09-0019-SO Total/NA Solid 6010C 79708 160-4124-7 MSD 6703-03-L10-09-0019-SO Total/NA Solid 6010C 79708 160-4124-8 6703-03-L10-09-0020-SO Total/NA Solid 6010C 79708 160-4124-9 6703-03-L10-09-0021-SO Total/NA Solid 6010C 79708 LCS 160-79708/2-A Lab Control Sample Total/NA Solid 6010C 79708 MB 160-79708/1-A Method Blank Total/NA General Chemistry Analysis Batch: 79097 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-4124-1 6703-03-L10-09-0013-SO Total/NA Solid Moisture 160-4124-2 6703-03-L10-09-0014-SO Total/NA Solid Moisture 160-4124-3 6703-03-L10-09-0015-SO Total/NA Solid Moisture 160-4124-4 6703-03-L10-09-0016-SO Total/NA Solid Moisture 160-4124-5 6703-03-L10-09-0017-SO Total/NA Solid Moisture 160-4124-6 6703-03-L10-09-0018-SO Total/NA Solid Moisture 160-4124-7 6703-03-L10-09-0019-SO Total/NA Solid Moisture 160-4124-8 6703-03-L10-09-0020-SO Total/NA Solid Moisture 160-4124-9 6703-03-L10-09-0021-SO Total/NA Solid Moisture 160-4124-9 DU 6703-03-L10-09-0021-SO Total/NA TestAmerica St. Louis Page 30 of 32 1

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Surrogate Summary TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 8260C - Volatile Organic Compounds (GC/MS)

Prep Type: Total/NA Matrix: Water Lab Sample ID Client Sample ID (75-129)

(81-130)

(81-124)

(87-128) 12DCE BFB DBFM TOL 101 108 111 108 160-4124-10 Percent Surrogate Recovery (Acceptance Limits) 6703-03-L10-09-0022-TB 98 97 107 98 LCS 160-79367/4 Lab Control Sample 104 100 111 98 LCSD 160-79367/5 Lab Control Sample Dup 103 112 111 109 MB 160-79367/2 Method Blank Surrogate Legend 12DCE = 1,2-Dichloroethane-d4 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane (Surr)

TOL = Toluene-d8 (Surr)

Method: 8260C - Volatile Organic Compounds by GC/MS Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (63-150)

(72-127)

(80-120)

(70-126)

BFB 12DCE TOL DBFM 101 107 97 107 160-4124-1 Percent Surrogate Recovery (Acceptance Limits) 6703-03-L10-09-0013-SO 100 106 94 105 160-4124-2 6703-03-L10-09-0014-SO 100 107 102 106 160-4124-3 6703-03-L10-09-0015-SO 99 108 97 109 160-4124-4 6703-03-L10-09-0016-SO 99 107 95 105 160-4124-5 6703-03-L10-09-0017-SO 97 110 95 105 160-4124-6 6703-03-L10-09-0018-SO 98 96 102 100 LCS 160-79123/2-A Lab Control Sample 103 98 102 101 LCSD 160-79123/3-A Lab Control Sample Dup 94 93 95 96 MB 160-79123/1-A Method Blank Surrogate Legend BFB = 4-Bromofluorobenzene (Surr) 12DCE = 1,2-Dichloroethane-d4 (Surr)

TOL = Toluene-d8 (Surr)

DBFM = Dibromofluoromethane (Surr)

Method: 8270D - Semivolatile Organic Compounds (GC/MS)

Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (53-97)

(46-111)

(55-98)

(54-101)

(58-123)

(56-97) 2FP TBP NBZ PHL TPH FBP 65 73 74 67 91 78 160-4123-B-4-B MS Percent Surrogate Recovery (Acceptance Limits)

Matrix Spike 68 70 77 77 72 80 160-4123-B-4-C MSD Matrix Spike Duplicate 59 49 66 77 59 64 160-4124-7 6703-03-L10-09-0019-SO 64 62 74 79 65 72 160-4124-8 6703-03-L10-09-0020-SO 62 61 70 99 63 69 160-4124-9 6703-03-L10-09-0021-SO 73 69 81 76 75 81 LCS 160-79122/2-A Lab Control Sample 82 71 89 96 83 88 MB 160-79122/1-A Method Blank Surrogate Legend 2FP = 2-Fluorophenol (Surr)

TBP = 2,4,6-Tribromophenol (Surr)

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Surrogate Summary TestAmerica Job ID: 160-4124-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

NBZ = Nitrobenzene-d5 (Surr)

PHL = Phenol-d5 (Surr)

TPH = Terphenyl-d14 (Surr)

FBP = 2-Fluorobiphenyl (Surr)

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