ML18010A281

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Final Status Survey Final Report Volume 3, Chapter 6, Survey Area Release Record for Land Survey Area 10, Analytical Report: 160-5228-1
ML18010A281
Person / Time
Site: 07000036
(SNM-0033)
Issue date: 12/13/2017
From: Swanson M, Vania I
TestAmerica Labs - St. Louis, Westinghouse
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML18010A247 List: ... further results
References
160-5228-1, HEM-17-72
Download: ML18010A281 (30)
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Text

ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-5228-1 Client Project/Site: RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

1/27/2014 2:38:36 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-5228-1 Page 2 of 30 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

5 Receipt Checklists.........................................

9 Definitions/Glossary.......................................

10 Method Summary.........................................

11 Sample Summary.........................................

12 Client Sample Results......................................

13 QC Sample Results........................................

23 QC Association Summary...................................

26 Tracer Carrier Summary....................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-5228-1 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-5228-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)

Report Number: 160-5228-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 01/20/2014; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 18.0º C and 18.0º C.

TECHNETIUM-99 (ICPMS)

Samples L100525BUB00 (160-5228-1), L100526BUB00 (160-5228-2), L100527BUB00 (160-5228-3), L100528BUB00 (160-5228-4),

L100501BES00 (160-5228-5), L100502BEQ00 (160-5228-6), L100502BES00 (160-5228-7), L100503BES00 (160-5228-8),

L100504BES00 (160-5228-9), L100505BES00 (160-5228-10), L100506BES00 (160-5228-11), L100507BES00 (160-5228-12),

L100508BES00 (160-5228-13), L100509BSS00 (160-5228-14), L100510BSS00 (160-5228-15), L100511BSS00 (160-5228-16),

L100512BSS00 (160-5228-17), L100513BSS00 (160-5228-18), L100514BSS00 (160-5228-19), L100515BSS00 (160-5228-20),

L100516BSS00 (160-5228-21), L100517BSS00 (160-5228-22), L100518BSS00 (160-5228-23), L100519BSS00 (160-5228-24),

L100520BSS00 (160-5228-25), L100521BSS00 (160-5228-26), L100522BSS00 (160-5228-27), L100523BSS00 (160-5228-28) and L100524BSS00 (160-5228-29) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 01/23/2014 and analyzed on 01/24/2014.

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-5228-1 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-5228-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

No difficulties were encountered during the Tc-99 analysis. All quality control parameters were within the acceptance limits.

PERCENT SOLIDS Samples L100525BUB00 (160-5228-1), L100526BUB00 (160-5228-2), L100527BUB00 (160-5228-3), L100528BUB00 (160-5228-4),

L100501BES00 (160-5228-5), L100502BEQ00 (160-5228-6), L100502BES00 (160-5228-7), L100503BES00 (160-5228-8),

L100504BES00 (160-5228-9), L100505BES00 (160-5228-10), L100506BES00 (160-5228-11), L100507BES00 (160-5228-12),

L100508BES00 (160-5228-13), L100509BSS00 (160-5228-14), L100510BSS00 (160-5228-15), L100511BSS00 (160-5228-16),

L100512BSS00 (160-5228-17), L100513BSS00 (160-5228-18), L100514BSS00 (160-5228-19), L100515BSS00 (160-5228-20),

L100516BSS00 (160-5228-21), L100517BSS00 (160-5228-22), L100518BSS00 (160-5228-23), L100519BSS00 (160-5228-24),

L100520BSS00 (160-5228-25), L100521BSS00 (160-5228-26), L100522BSS00 (160-5228-27), L100523BSS00 (160-5228-28) and L100524BSS00 (160-5228-29) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 01/21/2014.

No difficulties were encountered during the % solids analysis. All quality control parameters were within the acceptance limits.

TestAmerica St. Louis Page 4 of 30 1

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!Procedure HDP-PR-QA-006, Chain of Custody Page 1 ofl Hematite Decommissioning Project §"evision: 3 I

I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed Coe to HDP.

Chain ofCutody ID No. I F-011914-02 Pa2e Project Name:

Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number; 314-810-3382 Sampler Name Scott Jenkins 1/1

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Turn Around Time Rush (7 days)

Remarks 1 ILSA-10-05 Bias Samples 1 ILSA-10-05 Bias Samples 1 ILSA-10-05 Bias Samples 1 ILSA-10-05 Bias Samples Cooler Temperature:

AmhiP.nt Cooler ID: I Shipper and Number:

_OJ 20-=1l4 Comments: Please analyze samples on a 7 day TAT for Tc-99.

Please analyze samples for gamma spec after a 21 day ingrowth period.

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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning I>roject Revision: 3 I

Page 1 ofl Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time 1he container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify 1hat the sample is correctly identified before 1he sample is released for use or analysis and send the completed CoC to HDP.

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X X 1 LSA-10-05 Sidewall Samples Relinquished b'("" _;_..!:,,,- ~ Date/Tim~ ~"l: /'J/J. Date/Time Total Cooler Temperature: 9,.0" \\ "NT .A. o,_4 0 ')<; Amhient ./t ~~ Company-Name: \\A),..... < l<'.;ompany~ Cooler ID: Shipper and Number: r....L.----" I Jl/'1/ o.ciss, \\ 0 1 ?.OJH /04 Received by: Date/Time Relin~ishe<P')'iJ,,,. Date/Time Comments: Please analyze samples on a 7 TAT for Tc-99. 1/-J.,,,z, * ~,.. , a,....._;,,.1-~i~ Please analyze samples for gamma spec after a 21 day ingrowth Company Name: .Company Name: period. /">'(°"'A.~'(',.,<:::) c\\ <; Relinquished by: Date/Time Re~ Date0e VerifiedBy: tv-c-J~..S Lu~ L &-.v,- t/2.;; ti/ Company Name: Colllf.fl-Y Name: cin L.

Page 7 of 30 1 2 3 4 5 6 7 8 9 10 11 12 Procedure 8DP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I Pagel ofl Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP. Chain of Cutodv ID No. F-011914-01 Paee 2/3 ..,.. i\\,. .. ReanestedAnal"vsis-Laboratorv Name: Project Name: [~

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L100516BSSOO 1/17/2014 11:00 s C . ? X X 1 LSA-10-05 Sidewall Samples L1005 l 7BSSOO 1/16/2014 15:35 s C X X, 1 LSA-10-05 Sidewall Samples Ll00518BSSOO 1/16/2014 15:10 s C ~ - X 1 LSA-10-05 Sidewall Samples L1005 l 9BSSOO 1/17/2014 14:55 s C X X 1 LSA-10-05 Sidewall Samples L100520BSSOO 1/17/2014 14:45 s C c.. rx X (. 1 LSA-10-05 Sidewall Samples L100521BSSOO 1/16/2014 14:15 s C X X 1 LSA-10-05 Sidewall Samples Ll 00522BSSOO 1/16/2014 14:20 s C X X 1 LSA-10-05 Sidewall Samples Ll 00523BSSOO 1/16/2014 14:35 s C,...., .::X X l LSA-10-05 Sidewall Samples Relinquished r =- J-Date/Tim'-\\ ~by: r1/J~..- Date/Time Total Cooler Temperature: 9-0"' \\ \\'1...,0 \\'-7 ?"i Aml-.ie,nt Company Name: \\.l)f/1 - \\',{ 5' Company Name: Cooler ID: Shipper and Number: I I>/ Cvoss.--c,a&-5 \\ le 0120-0,/0tl Received by: Date/Time ~!n~~~~~- Date/Time Comments: Please analyze samples on a 7 TAT for Tc-99. 0 ~ Please analyze samples for gamma spec after a 21 day ingrowth Company Name: Company ~~e: \\"'(JJ \\(? period. C'<'c:::%"'o 4 W~l~r Relinquished by: Date/Time Rec~ D/t/Iime C:.)>,..,~;- ~ l 2.P{'( Verified By: Company Name: Company Name: {; rt:t C ~

Page 8 of 30 1 2 3 4 5 6 7 8 9 10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I Page 1 ofl Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP. Chain of Cutodv ID No. F-011914-01 Pa!!e 3/3 R).()Jlci;ted.~alvsrs. Laboratorv Name: Project Name: r'cc-

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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-5228-1 Login Number: 5228 Question Answer Comment Creator: Daniels, Brian J List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter. True The cooler's custody seal, if present, is intact. N/A Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or tampered with. False Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is <6mm (1/4"). True Multiphasic samples are not present. True Samples do not require splitting or compositing. N/A Residual Chlorine Checked. TestAmerica St. Louis Page 9 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Definitions/Glossary TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Qualifiers Metals Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Qualifier Rad Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica St. Louis Page 10 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Method Summary TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL Protocol

References:

EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 11 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Sample Summary TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Lab Sample ID Client Sample ID Received Collected Matrix 160-5228-1 L100525BUB00 Solid 01/19/14 12:50 01/20/14 18:30 160-5228-2 L100526BUB00 Solid 01/19/14 13:00 01/20/14 18:30 160-5228-3 L100527BUB00 Solid 01/19/14 13:10 01/20/14 18:30 160-5228-4 L100528BUB00 Solid 01/19/14 13:15 01/20/14 18:30 160-5228-5 L100501BES00 Solid 01/16/14 08:55 01/20/14 18:30 160-5228-6 L100502BEQ00 Solid 01/16/14 09:15 01/20/14 18:30 160-5228-7 L100502BES00 Solid 01/16/14 09:15 01/20/14 18:30 160-5228-8 L100503BES00 Solid 01/14/14 11:05 01/20/14 18:30 160-5228-9 L100504BES00 Solid 01/14/14 14:20 01/20/14 18:30 160-5228-10 L100505BES00 Solid 01/14/14 10:50 01/20/14 18:30 160-5228-11 L100506BES00 Solid 01/14/14 14:00 01/20/14 18:30 160-5228-12 L100507BES00 Solid 01/14/14 14:15 01/20/14 18:30 160-5228-13 L100508BES00 Solid 01/14/14 10:35 01/20/14 18:30 160-5228-14 L100509BSS00 Solid 01/17/14 14:30 01/20/14 18:30 160-5228-15 L100510BSS00 Solid 01/17/14 11:10 01/20/14 18:30 160-5228-16 L100511BSS00 Solid 01/17/14 10:45 01/20/14 18:30 160-5228-17 L100512BSS00 Solid 01/17/14 10:50 01/20/14 18:30 160-5228-18 L100513BSS00 Solid 01/17/14 14:20 01/20/14 18:30 160-5228-19 L100514BSS00 Solid 01/17/14 13:50 01/20/14 18:30 160-5228-20 L100515BSS00 Solid 01/17/14 14:10 01/20/14 18:30 160-5228-21 L100516BSS00 Solid 01/17/14 11:00 01/20/14 18:30 160-5228-22 L100517BSS00 Solid 01/16/14 15:35 01/20/14 18:30 160-5228-23 L100518BSS00 Solid 01/16/14 15:10 01/20/14 18:30 160-5228-24 L100519BSS00 Solid 01/17/14 14:55 01/20/14 18:30 160-5228-25 L100520BSS00 Solid 01/17/14 14:45 01/20/14 18:30 160-5228-26 L100521BSS00 Solid 01/16/14 14:15 01/20/14 18:30 160-5228-27 L100522BSS00 Solid 01/16/14 14:20 01/20/14 18:30 160-5228-28 L100523BSS00 Solid 01/16/14 14:35 01/20/14 18:30 160-5228-29 L100524BSS00 Solid 01/16/14 15:00 01/20/14 18:30 TestAmerica St. Louis Page 12 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Client Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Lab Sample ID: 160-5228-1 Client Sample ID: L100525BUB00 Matrix: Solid Date Collected: 01/19/14 12:50 Percent Solids: 81.0 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000067 0.000020 mg/Kg

01/23/14 16:53 01/24/14 18:55 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.00484 U (2+/-) 0.0163 (2+/-) 1 01/24/14 18:55 01/23/14 16:53 pCi/g 0.231 1.35 RL MDC -0.0149 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 18:55 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 91 Lab Sample ID: 160-5228-2 Client Sample ID: L100526BUB00 Matrix: Solid Date Collected: 01/19/14 13:00 Percent Solids: 76.0 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000071 0.000021 mg/Kg

01/23/14 16:53 01/24/14 19:06 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0129 U (2+/-) 0.0247 (2+/-) 1 01/24/14 19:06 01/23/14 16:53 pCi/g 0.244 1.43 RL MDC 0.0225 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 19:06 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 92 Lab Sample ID: 160-5228-3 Client Sample ID: L100527BUB00 Matrix: Solid Date Collected: 01/19/14 13:10 Percent Solids: 80.4 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000068 0.000020 mg/Kg

01/23/14 16:53 01/24/14 19:18 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.283 (2+/-) 0.0304 (2+/-) 1 01/24/14 19:18 01/23/14 16:53 pCi/g 0.232 1.36 RL MDC 0.00949 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 19:18 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 91 TestAmerica St. Louis Page 13 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Client Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Lab Sample ID: 160-5228-4 Client Sample ID: L100528BUB00 Matrix: Solid Date Collected: 01/19/14 13:15 Percent Solids: 71.7 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000078 0.000023 mg/Kg

01/23/14 16:53 01/24/14 19:22 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0137 U (2+/-) 0.0749 (2+/-) 1 01/24/14 19:22 01/23/14 16:53 pCi/g 0.268 1.57 RL MDC -0.0664 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 19:22 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 89 Lab Sample ID: 160-5228-5 Client Sample ID: L100501BES00 Matrix: Solid Date Collected: 01/16/14 08:55 Percent Solids: 72.4 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000077 0.000023 mg/Kg

01/23/14 16:53 01/24/14 19:26 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0242 U (2+/-) 0.0637 (2+/-) 1 01/24/14 19:26 01/23/14 16:53 pCi/g 0.263 1.54 RL MDC -0.0571 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 19:26 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 90 Lab Sample ID: 160-5228-6 Client Sample ID: L100502BEQ00 Matrix: Solid Date Collected: 01/16/14 09:15 Percent Solids: 70.9 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000087 0.000026 mg/Kg

01/23/14 16:53 01/24/14 19:29 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.00268 U (2+/-) 0.0557 (2+/-) 1 01/24/14 19:29 01/23/14 16:53 pCi/g 0.298 1.74 RL MDC -0.0453 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 19:29 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 81 Lab Sample ID: 160-5228-7 Client Sample ID: L100502BES00 Matrix: Solid Date Collected: 01/16/14 09:15 Percent Solids: 70.5 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000082 0.000025 mg/Kg

01/23/14 16:53 01/24/14 19:33 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier TestAmerica St. Louis Page 14 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Client Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Lab Sample ID: 160-5228-7 Client Sample ID: L100502BES00 Matrix: Solid Date Collected: 01/16/14 09:15 Percent Solids: 70.5 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0144 U (2+/-) 0.0456 (2+/-) 1 01/24/14 19:33 01/23/14 16:53 pCi/g 0.282 1.65 RL MDC 0.0391 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 19:33 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 86 Lab Sample ID: 160-5228-8 Client Sample ID: L100503BES00 Matrix: Solid Date Collected: 01/14/14 11:05 Percent Solids: 83.1 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00012 0.000067 0.000020 mg/Kg

01/23/14 16:53 01/24/14 19:37 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.99 (2+/-) 0.260 (2+/-) 1 01/24/14 19:37 01/23/14 16:53 pCi/g 0.229 1.34 RL MDC 0.147 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 19:37 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 90 Lab Sample ID: 160-5228-9 Client Sample ID: L100504BES00 Matrix: Solid Date Collected: 01/14/14 14:20 Percent Solids: 81.3 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000067 0.000020 mg/Kg

01/23/14 16:53 01/24/14 19:41 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.247 (2+/-) 0.0380 (2+/-) 1 01/24/14 19:41 01/23/14 16:53 pCi/g 0.228 1.33 RL MDC 0.0268 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 19:41 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 93 Lab Sample ID: 160-5228-10 Client Sample ID: L100505BES00 Matrix: Solid Date Collected: 01/14/14 10:50 Percent Solids: 82.4 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000068 0.000020 mg/Kg

01/23/14 16:53 01/24/14 19:45 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier TestAmerica St. Louis Page 15 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Client Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Lab Sample ID: 160-5228-10 Client Sample ID: L100505BES00 Matrix: Solid Date Collected: 01/14/14 10:50 Percent Solids: 82.4 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0474 U (2+/-) 0.0334 (2+/-) 1 01/24/14 19:45 01/23/14 16:53 pCi/g 0.234 1.37 RL MDC -0.0291 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 19:45 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 88 Lab Sample ID: 160-5228-11 Client Sample ID: L100506BES00 Matrix: Solid Date Collected: 01/14/14 14:00 Percent Solids: 78.7 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000073 0.000022 mg/Kg

01/23/14 16:53 01/24/14 19:49 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0441 U (2+/-) 0.0603 (2+/-) 1 01/24/14 19:49 01/23/14 16:53 pCi/g 0.250 1.46 RL MDC 0.0522 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 19:49 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 87 Lab Sample ID: 160-5228-12 Client Sample ID: L100507BES00 Matrix: Solid Date Collected: 01/14/14 14:15 Percent Solids: 77.4 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000071 0.000021 mg/Kg

01/23/14 16:53 01/24/14 19:53 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0174 U (2+/-) 0.0516 (2+/-) 1 01/24/14 19:53 01/23/14 16:53 pCi/g 0.242 1.41 RL MDC -0.0471 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 19:53 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 91 Lab Sample ID: 160-5228-13 Client Sample ID: L100508BES00 Matrix: Solid Date Collected: 01/14/14 10:35 Percent Solids: 76.0 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000073 0.000022 mg/Kg

01/23/14 16:53 01/24/14 20:04 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier TestAmerica St. Louis Page 16 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Client Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Lab Sample ID: 160-5228-13 Client Sample ID: L100508BES00 Matrix: Solid Date Collected: 01/14/14 10:35 Percent Solids: 76.0 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0135 U (2+/-) 0.0294 (2+/-) 1 01/24/14 20:04 01/23/14 16:53 pCi/g 0.249 1.45 RL MDC -0.0267 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 20:04 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 91 Lab Sample ID: 160-5228-14 Client Sample ID: L100509BSS00 Matrix: Solid Date Collected: 01/17/14 14:30 Percent Solids: 81.0 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000069 0.000021 mg/Kg

01/23/14 16:53 01/24/14 20:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0249 U (2+/-) 0.0405 (2+/-) 1 01/24/14 20:08 01/23/14 16:53 pCi/g 0.235 1.37 RL MDC -0.0362 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 20:08 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 90 Lab Sample ID: 160-5228-15 Client Sample ID: L100510BSS00 Matrix: Solid Date Collected: 01/17/14 11:10 Percent Solids: 80.8 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000032 J 0.000066 0.000020 mg/Kg

01/23/14 16:53 01/24/14 20:12 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.546 (2+/-) 0.0924 (2+/-) 1 01/24/14 20:12 01/23/14 16:53 pCi/g 0.227 1.33 RL MDC 0.0697 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 20:12 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 93 Lab Sample ID: 160-5228-16 Client Sample ID: L100511BSS00 Matrix: Solid Date Collected: 01/17/14 10:45 Percent Solids: 86.2 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000064 0.000019 mg/Kg

01/23/14 16:53 01/24/14 20:16 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier TestAmerica St. Louis Page 17 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Client Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Lab Sample ID: 160-5228-16 Client Sample ID: L100511BSS00 Matrix: Solid Date Collected: 01/17/14 10:45 Percent Solids: 86.2 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.274 (2+/-) 0.0497 (2+/-) 1 01/24/14 20:16 01/23/14 16:53 pCi/g 0.219 1.28 RL MDC 0.0372 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 20:16 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 90 Lab Sample ID: 160-5228-17 Client Sample ID: L100512BSS00 Matrix: Solid Date Collected: 01/17/14 10:50 Percent Solids: 82.2 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000067 0.000020 mg/Kg

01/23/14 16:53 01/24/14 20:20 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0533 U (2+/-) 0.0615 (2+/-) 1 01/24/14 20:20 01/23/14 16:53 pCi/g 0.229 1.34 RL MDC -0.0555 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 20:20 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 91 Lab Sample ID: 160-5228-18 Client Sample ID: L100513BSS00 Matrix: Solid Date Collected: 01/17/14 14:20 Percent Solids: 80.5 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000067 0.000020 mg/Kg

01/23/14 16:53 01/24/14 20:24 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0210 U (2+/-) 0.0449 (2+/-) 1 01/24/14 20:24 01/23/14 16:53 pCi/g 0.231 1.35 RL MDC -0.0415 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 20:24 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 92 Lab Sample ID: 160-5228-19 Client Sample ID: L100514BSS00 Matrix: Solid Date Collected: 01/17/14 13:50 Percent Solids: 80.8 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000067 0.000020 mg/Kg

01/23/14 16:53 01/24/14 20:27 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier TestAmerica St. Louis Page 18 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Client Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Lab Sample ID: 160-5228-19 Client Sample ID: L100514BSS00 Matrix: Solid Date Collected: 01/17/14 13:50 Percent Solids: 80.8 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0573 U (2+/-) 0.0225 (2+/-) 1 01/24/14 20:27 01/23/14 16:53 pCi/g 0.228 1.33 RL MDC 0.0202 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 20:27 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 93 Lab Sample ID: 160-5228-20 Client Sample ID: L100515BSS00 Matrix: Solid Date Collected: 01/17/14 14:10 Percent Solids: 79.6 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000069 0.000021 mg/Kg

01/23/14 16:53 01/24/14 20:31 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0559 U (2+/-) 0.0176 (2+/-) 1 01/24/14 20:31 01/23/14 16:53 pCi/g 0.236 1.38 RL MDC -0.0151 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:53 01/24/14 20:31 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 91 Lab Sample ID: 160-5228-21 Client Sample ID: L100516BSS00 Matrix: Solid Date Collected: 01/17/14 11:00 Percent Solids: 79.6 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000068 0.000021 mg/Kg

01/23/14 16:58 01/24/14 20:51 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.000468 U (2+/-) 0.0115 (2+/-) 1 01/24/14 20:51 01/23/14 16:58 pCi/g 0.234 1.37 RL MDC 0.0105 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:58 01/24/14 20:51 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 92 Lab Sample ID: 160-5228-22 Client Sample ID: L100517BSS00 Matrix: Solid Date Collected: 01/16/14 15:35 Percent Solids: 82.0 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000069 0.000021 mg/Kg

01/23/14 16:58 01/24/14 21:02 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier TestAmerica St. Louis Page 19 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Client Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Lab Sample ID: 160-5228-22 Client Sample ID: L100517BSS00 Matrix: Solid Date Collected: 01/16/14 15:35 Percent Solids: 82.0 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0387 U (2+/-) 0.0762 (2+/-) 1 01/24/14 21:02 01/23/14 16:58 pCi/g 0.235 1.37 RL MDC 0.0681 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:58 01/24/14 21:02 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 89 Lab Sample ID: 160-5228-23 Client Sample ID: L100518BSS00 Matrix: Solid Date Collected: 01/16/14 15:10 Percent Solids: 71.4 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000081 0.000024 mg/Kg

01/23/14 16:58 01/24/14 21:06 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.00446 U (2+/-) 0.0203 (2+/-) 1 01/24/14 21:06 01/23/14 16:58 pCi/g 0.278 1.63 RL MDC -0.0176 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:58 01/24/14 21:06 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 87 Lab Sample ID: 160-5228-24 Client Sample ID: L100519BSS00 Matrix: Solid Date Collected: 01/17/14 14:55 Percent Solids: 71.8 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000079 0.000024 mg/Kg

01/23/14 16:58 01/24/14 21:10 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0556 U (2+/-) 0.0607 (2+/-) 1 01/24/14 21:10 01/23/14 16:58 pCi/g 0.270 1.58 RL MDC -0.0538 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:58 01/24/14 21:10 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 89 Lab Sample ID: 160-5228-25 Client Sample ID: L100520BSS00 Matrix: Solid Date Collected: 01/17/14 14:45 Percent Solids: 74.4 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000075 0.000022 mg/Kg

01/23/14 16:58 01/24/14 21:14 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier TestAmerica St. Louis Page 20 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Client Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Lab Sample ID: 160-5228-25 Client Sample ID: L100520BSS00 Matrix: Solid Date Collected: 01/17/14 14:45 Percent Solids: 74.4 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0546 U (2+/-) 0.0166 (2+/-) 1 01/24/14 21:14 01/23/14 16:58 pCi/g 0.256 1.50 RL MDC -0.0141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:58 01/24/14 21:14 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 90 Lab Sample ID: 160-5228-26 Client Sample ID: L100521BSS00 Matrix: Solid Date Collected: 01/16/14 14:15 Percent Solids: 70.3 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000082 0.000024 mg/Kg

01/23/14 16:58 01/24/14 21:18 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0472 U (2+/-) 0.00651 (2+/-) 1 01/24/14 21:18 01/23/14 16:58 pCi/g 0.279 1.63 RL MDC -0.00362 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:58 01/24/14 21:18 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 87 Lab Sample ID: 160-5228-27 Client Sample ID: L100522BSS00 Matrix: Solid Date Collected: 01/16/14 14:20 Percent Solids: 73.7 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000078 0.000023 mg/Kg

01/23/14 16:58 01/24/14 21:22 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.110 U (2+/-) 0.143 (2+/-) 1 01/24/14 21:22 01/23/14 16:58 pCi/g 0.266 1.55 RL MDC 0.125 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:58 01/24/14 21:22 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 88 Lab Sample ID: 160-5228-28 Client Sample ID: L100523BSS00 Matrix: Solid Date Collected: 01/16/14 14:35 Percent Solids: 75.4 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000074 0.000022 mg/Kg

01/23/14 16:58 01/24/14 21:25 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier TestAmerica St. Louis Page 21 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Client Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Lab Sample ID: 160-5228-28 Client Sample ID: L100523BSS00 Matrix: Solid Date Collected: 01/16/14 14:35 Percent Solids: 75.4 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0593 U (2+/-) 0.0512 (2+/-) 1 01/24/14 21:25 01/23/14 16:58 pCi/g 0.254 1.49 RL MDC 0.0452 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:58 01/24/14 21:25 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 89 Lab Sample ID: 160-5228-29 Client Sample ID: L100524BSS00 Matrix: Solid Date Collected: 01/16/14 15:00 Percent Solids: 73.5 Date Received: 01/20/14 18:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000077 0.000023 mg/Kg

01/23/14 16:58 01/24/14 21:37 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 -0.0477 U (2+/-) 0.142 (2+/-) 1 01/24/14 21:37 01/23/14 16:58 pCi/g 0.264 1.54 RL MDC -0.126 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert. Uncert. Re 30 - 110 Carrier 01/23/14 16:58 01/24/14 21:37 1 Dil Fac Analyzed Prepared Qualifier Limits %Yield 89 TestAmerica St. Louis Page 22 of 30 1 2 3 4 5 6 7 8 9 10 11 12

QC Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-101018/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 101151 Prep Batch: 101018 RL MDL Technetium 99 ND 0.000052 0.000016 mg/Kg 01/23/14 16:53 01/24/14 18:47 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-101018/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 101151 Prep Batch: 101018 Technetium 99 0.00239 0.00246 mg/Kg 103 80 - 120 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits Client Sample ID: L100525BUB00 Lab Sample ID: 160-5228-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 101151 Prep Batch: 101018 Technetium 99 ND 0.00294 0.00307 mg/Kg 104 75 - 125

Analyte MS MS D Unit Result Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: L100525BUB00 Lab Sample ID: 160-5228-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 101151 Prep Batch: 101018 Technetium 99 ND 0.00297 0.00311 mg/Kg 105 75 - 125 1 30

Analyte MSD MSD D Unit Result Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Limit RPD RPD Client Sample ID: Method Blank Lab Sample ID: MB 160-101020/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 101151 Prep Batch: 101020 RL MDL Technetium 99 ND 0.000052 0.000016 mg/Kg 01/23/14 16:58 01/24/14 20:35 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-101020/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 101151 Prep Batch: 101020 Technetium 99 0.00241 0.00252 mg/Kg 105 80 - 120 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits Client Sample ID: L100516BSS00 Lab Sample ID: 160-5228-21 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 101151 Prep Batch: 101020 Technetium 99 ND 0.00303 0.00320 mg/Kg 106 75 - 125

Analyte MS MS D Unit Result Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: L100516BSS00 Lab Sample ID: 160-5228-21 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 101151 Prep Batch: 101020 Technetium 99 ND 0.00302 0.00321 mg/Kg 106 75 - 125 0 30

Analyte MSD MSD D Unit Result Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Limit RPD RPD TestAmerica St. Louis Page 23 of 30 1 2 3 4 5 6 7 8 9 10 11 12

QC Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-101018/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 101152 Prep Batch: 101018 Technetium 99 Analyte U 1 01/24/14 18:47 01/23/14 16:53 pCi/g 0.178 MDC 1.04 RL 0.0535 -0.0514 (2+/-) (2+/-) MB -0.01724 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert. Count Uncert. Total Carrier Re 30 - 110 01/23/14 16:53 01/24/14 18:47 1 Dil Fac Prepared Analyzed Qualifier Limits %Yield 96 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-101018/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 101152 Prep Batch: 101018 Technetium 99 Analyte 120 80 103 42.12 40.9 4.23 1.04 0.177 RL MDC (2+/-) LCS LCS pCi/g Unit Result Qual %Rec Added Spike Limits %Rec. Uncert. Total Re Carrier 30 - 110 LCS Qualifier Limits %Yield 96 LCS Client Sample ID: L100525BUB00 Lab Sample ID: 160-5228-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 101152 Prep Batch: 101018 Technetium 99 Analyte 125 75 104 52.57 50.4 -0.00484 U 5.27 1.34 0.229 RL MDC (2+/-) MS MS pCi/g Unit Result Qual %Rec Added Spike Result Sample Sample Qual Limits %Rec. Uncert. Total Re Carrier 30 - 110 MS Qualifier Limits %Yield 92 MS Client Sample ID: L100525BUB00 Lab Sample ID: 160-5228-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 101152 Prep Batch: 101018 Technetium 99 Analyte 1 0.07 125 75 105 53.31 50.8 -0.00484 U 5.45 1.35 0.232 RL MDC (2+/-) MSD MSD pCi/g Unit Result Qual %Rec Limit Added Spike Result Sample Sample Qual Limits %Rec. Uncert. Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits %Yield 91 MSD Client Sample ID: Method Blank Lab Sample ID: MB 160-101020/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 101152 Prep Batch: 101020 Technetium 99 Analyte U 1 01/24/14 20:35 01/23/14 16:58 pCi/g 0.180 MDC 1.05 RL 0.0221 -0.0207 (2+/-) (2+/-) MB -0.03826 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert. Count Uncert. Total TestAmerica St. Louis Page 24 of 30 1 2 3 4 5 6 7 8 9 10 11 12

QC Sample Results TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued) Client Sample ID: Method Blank Lab Sample ID: MB 160-101020/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 101152 Prep Batch: 101020 Carrier Re 30 - 110 01/23/14 16:58 01/24/14 20:35 1 Dil Fac Prepared Analyzed Qualifier Limits %Yield 95 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-101020/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 101152 Prep Batch: 101020 Technetium 99 Analyte 120 80 105 43.18 41.3 4.19 1.06 0.181 RL MDC (2+/-) LCS LCS pCi/g Unit Result Qual %Rec Added Spike Limits %Rec. Uncert. Total Re Carrier 30 - 110 LCS Qualifier Limits %Yield 95 LCS Client Sample ID: L100516BSS00 Lab Sample ID: 160-5228-21 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 101152 Prep Batch: 101020 Technetium 99 Analyte 125 75 106 54.73 51.8 0.000468 U 5.66 1.34 0.230 RL MDC (2+/-) MS MS pCi/g Unit Result Qual %Rec Added Spike Result Sample Sample Qual Limits %Rec. Uncert. Total Re Carrier 30 - 110 MS Qualifier Limits %Yield 94 MS Client Sample ID: L100516BSS00 Lab Sample ID: 160-5228-21 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 101152 Prep Batch: 101020 Technetium 99 Analyte 1 0.01 125 75 106 54.91 51.6 0.000468 U 6.52 1.39 0.238 RL MDC (2+/-) MSD MSD pCi/g Unit Result Qual %Rec Limit Added Spike Result Sample Sample Qual Limits %Rec. Uncert. Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits %Yield 91 MSD TestAmerica St. Louis Page 25 of 30 1 2 3 4 5 6 7 8 9 10 11 12

QC Association Summary TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Metals Prep Batch: 101018 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-5228-1 L100525BUB00 Total/NA Solid None 160-5228-1 MS L100525BUB00 Total/NA Solid None 160-5228-1 MSD L100525BUB00 Total/NA Solid None 160-5228-2 L100526BUB00 Total/NA Solid None 160-5228-3 L100527BUB00 Total/NA Solid None 160-5228-4 L100528BUB00 Total/NA Solid None 160-5228-5 L100501BES00 Total/NA Solid None 160-5228-6 L100502BEQ00 Total/NA Solid None 160-5228-7 L100502BES00 Total/NA Solid None 160-5228-8 L100503BES00 Total/NA Solid None 160-5228-9 L100504BES00 Total/NA Solid None 160-5228-10 L100505BES00 Total/NA Solid None 160-5228-11 L100506BES00 Total/NA Solid None 160-5228-12 L100507BES00 Total/NA Solid None 160-5228-13 L100508BES00 Total/NA Solid None 160-5228-14 L100509BSS00 Total/NA Solid None 160-5228-15 L100510BSS00 Total/NA Solid None 160-5228-16 L100511BSS00 Total/NA Solid None 160-5228-17 L100512BSS00 Total/NA Solid None 160-5228-18 L100513BSS00 Total/NA Solid None 160-5228-19 L100514BSS00 Total/NA Solid None 160-5228-20 L100515BSS00 Total/NA Solid None LCS 160-101018/2-A Lab Control Sample Total/NA Solid None MB 160-101018/1-A Method Blank Total/NA Prep Batch: 101020 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-5228-21 L100516BSS00 Total/NA Solid None 160-5228-21 MS L100516BSS00 Total/NA Solid None 160-5228-21 MSD L100516BSS00 Total/NA Solid None 160-5228-22 L100517BSS00 Total/NA Solid None 160-5228-23 L100518BSS00 Total/NA Solid None 160-5228-24 L100519BSS00 Total/NA Solid None 160-5228-25 L100520BSS00 Total/NA Solid None 160-5228-26 L100521BSS00 Total/NA Solid None 160-5228-27 L100522BSS00 Total/NA Solid None 160-5228-28 L100523BSS00 Total/NA Solid None 160-5228-29 L100524BSS00 Total/NA Solid None LCS 160-101020/2-A Lab Control Sample Total/NA Solid None MB 160-101020/1-A Method Blank Total/NA Analysis Batch: 101151 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 101018 160-5228-1 L100525BUB00 Total/NA Solid 6020A 101018 160-5228-1 MS L100525BUB00 Total/NA Solid 6020A 101018 160-5228-1 MSD L100525BUB00 Total/NA Solid 6020A 101018 160-5228-2 L100526BUB00 Total/NA Solid 6020A 101018 160-5228-3 L100527BUB00 Total/NA Solid 6020A 101018 160-5228-4 L100528BUB00 Total/NA Solid 6020A 101018 160-5228-5 L100501BES00 Total/NA Solid 6020A 101018 160-5228-6 L100502BEQ00 Total/NA TestAmerica St. Louis Page 26 of 30 1 2 3 4 5 6 7 8 9 10 11 12

QC Association Summary TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Metals (Continued) Analysis Batch: 101151 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 101018 160-5228-7 L100502BES00 Total/NA Solid 6020A 101018 160-5228-8 L100503BES00 Total/NA Solid 6020A 101018 160-5228-9 L100504BES00 Total/NA Solid 6020A 101018 160-5228-10 L100505BES00 Total/NA Solid 6020A 101018 160-5228-11 L100506BES00 Total/NA Solid 6020A 101018 160-5228-12 L100507BES00 Total/NA Solid 6020A 101018 160-5228-13 L100508BES00 Total/NA Solid 6020A 101018 160-5228-14 L100509BSS00 Total/NA Solid 6020A 101018 160-5228-15 L100510BSS00 Total/NA Solid 6020A 101018 160-5228-16 L100511BSS00 Total/NA Solid 6020A 101018 160-5228-17 L100512BSS00 Total/NA Solid 6020A 101018 160-5228-18 L100513BSS00 Total/NA Solid 6020A 101018 160-5228-19 L100514BSS00 Total/NA Solid 6020A 101018 160-5228-20 L100515BSS00 Total/NA Solid 6020A 101020 160-5228-21 L100516BSS00 Total/NA Solid 6020A 101020 160-5228-21 MS L100516BSS00 Total/NA Solid 6020A 101020 160-5228-21 MSD L100516BSS00 Total/NA Solid 6020A 101020 160-5228-22 L100517BSS00 Total/NA Solid 6020A 101020 160-5228-23 L100518BSS00 Total/NA Solid 6020A 101020 160-5228-24 L100519BSS00 Total/NA Solid 6020A 101020 160-5228-25 L100520BSS00 Total/NA Solid 6020A 101020 160-5228-26 L100521BSS00 Total/NA Solid 6020A 101020 160-5228-27 L100522BSS00 Total/NA Solid 6020A 101020 160-5228-28 L100523BSS00 Total/NA Solid 6020A 101020 160-5228-29 L100524BSS00 Total/NA Solid 6020A 101018 LCS 160-101018/2-A Lab Control Sample Total/NA Solid 6020A 101020 LCS 160-101020/2-A Lab Control Sample Total/NA Solid 6020A 101018 MB 160-101018/1-A Method Blank Total/NA Solid 6020A 101020 MB 160-101020/1-A Method Blank Total/NA General Chemistry Analysis Batch: 100283 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-5228-1 L100525BUB00 Total/NA Solid Moisture 160-5228-2 L100526BUB00 Total/NA Solid Moisture 160-5228-3 L100527BUB00 Total/NA Solid Moisture 160-5228-4 L100528BUB00 Total/NA Solid Moisture 160-5228-5 L100501BES00 Total/NA Solid Moisture 160-5228-6 L100502BEQ00 Total/NA Solid Moisture 160-5228-7 L100502BES00 Total/NA Solid Moisture 160-5228-8 L100503BES00 Total/NA Solid Moisture 160-5228-9 L100504BES00 Total/NA Solid Moisture 160-5228-10 L100505BES00 Total/NA Solid Moisture 160-5228-11 L100506BES00 Total/NA Solid Moisture 160-5228-12 L100507BES00 Total/NA Solid Moisture 160-5228-13 L100508BES00 Total/NA Solid Moisture 160-5228-14 L100509BSS00 Total/NA Solid Moisture 160-5228-15 L100510BSS00 Total/NA Solid Moisture 160-5228-16 L100511BSS00 Total/NA TestAmerica St. Louis Page 27 of 30 1 2 3 4 5 6 7 8 9 10 11 12

QC Association Summary TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) General Chemistry (Continued) Analysis Batch: 100283 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-5228-17 L100512BSS00 Total/NA Solid Moisture 160-5228-18 L100513BSS00 Total/NA Solid Moisture 160-5228-19 L100514BSS00 Total/NA Solid Moisture 160-5228-20 L100515BSS00 Total/NA Solid Moisture 160-5228-21 L100516BSS00 Total/NA Solid Moisture 160-5228-22 L100517BSS00 Total/NA Solid Moisture 160-5228-23 L100518BSS00 Total/NA Solid Moisture 160-5228-24 L100519BSS00 Total/NA Solid Moisture 160-5228-25 L100520BSS00 Total/NA Solid Moisture 160-5228-26 L100521BSS00 Total/NA Solid Moisture 160-5228-27 L100522BSS00 Total/NA Solid Moisture 160-5228-28 L100523BSS00 Total/NA Solid Moisture 160-5228-29 L100524BSS00 Total/NA Solid Moisture 160-5228-29 DU L100524BSS00 Total/NA Rad Prep Batch: 101018 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-5228-1 L100525BUB00 Total/NA Solid None 160-5228-1 MS L100525BUB00 Total/NA Solid None 160-5228-1 MSD L100525BUB00 Total/NA Solid None 160-5228-2 L100526BUB00 Total/NA Solid None 160-5228-3 L100527BUB00 Total/NA Solid None 160-5228-4 L100528BUB00 Total/NA Solid None 160-5228-5 L100501BES00 Total/NA Solid None 160-5228-6 L100502BEQ00 Total/NA Solid None 160-5228-7 L100502BES00 Total/NA Solid None 160-5228-8 L100503BES00 Total/NA Solid None 160-5228-9 L100504BES00 Total/NA Solid None 160-5228-10 L100505BES00 Total/NA Solid None 160-5228-11 L100506BES00 Total/NA Solid None 160-5228-12 L100507BES00 Total/NA Solid None 160-5228-13 L100508BES00 Total/NA Solid None 160-5228-14 L100509BSS00 Total/NA Solid None 160-5228-15 L100510BSS00 Total/NA Solid None 160-5228-16 L100511BSS00 Total/NA Solid None 160-5228-17 L100512BSS00 Total/NA Solid None 160-5228-18 L100513BSS00 Total/NA Solid None 160-5228-19 L100514BSS00 Total/NA Solid None 160-5228-20 L100515BSS00 Total/NA Solid None LCS 160-101018/2-A Lab Control Sample Total/NA Solid None MB 160-101018/1-A Method Blank Total/NA Prep Batch: 101020 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-5228-21 L100516BSS00 Total/NA Solid None 160-5228-21 MS L100516BSS00 Total/NA Solid None 160-5228-21 MSD L100516BSS00 Total/NA Solid None 160-5228-22 L100517BSS00 Total/NA TestAmerica St. Louis Page 28 of 30 1 2 3 4 5 6 7 8 9 10 11 12

QC Association Summary TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Rad (Continued) Prep Batch: 101020 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-5228-23 L100518BSS00 Total/NA Solid None 160-5228-24 L100519BSS00 Total/NA Solid None 160-5228-25 L100520BSS00 Total/NA Solid None 160-5228-26 L100521BSS00 Total/NA Solid None 160-5228-27 L100522BSS00 Total/NA Solid None 160-5228-28 L100523BSS00 Total/NA Solid None 160-5228-29 L100524BSS00 Total/NA Solid None LCS 160-101020/2-A Lab Control Sample Total/NA Solid None MB 160-101020/1-A Method Blank Total/NA TestAmerica St. Louis Page 29 of 30 1 2 3 4 5 6 7 8 9 10 11 12

Tracer/Carrier Summary TestAmerica Job ID: 160-5228-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT) Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110) Re 91 160-5228-1 Percent Yield (Acceptance Limits) L100525BUB00 92 160-5228-1 MS L100525BUB00 91 160-5228-1 MSD L100525BUB00 92 160-5228-2 L100526BUB00 91 160-5228-3 L100527BUB00 89 160-5228-4 L100528BUB00 90 160-5228-5 L100501BES00 81 160-5228-6 L100502BEQ00 86 160-5228-7 L100502BES00 90 160-5228-8 L100503BES00 93 160-5228-9 L100504BES00 88 160-5228-10 L100505BES00 87 160-5228-11 L100506BES00 91 160-5228-12 L100507BES00 91 160-5228-13 L100508BES00 90 160-5228-14 L100509BSS00 93 160-5228-15 L100510BSS00 90 160-5228-16 L100511BSS00 91 160-5228-17 L100512BSS00 92 160-5228-18 L100513BSS00 93 160-5228-19 L100514BSS00 91 160-5228-20 L100515BSS00 92 160-5228-21 L100516BSS00 94 160-5228-21 MS L100516BSS00 91 160-5228-21 MSD L100516BSS00 89 160-5228-22 L100517BSS00 87 160-5228-23 L100518BSS00 89 160-5228-24 L100519BSS00 90 160-5228-25 L100520BSS00 87 160-5228-26 L100521BSS00 88 160-5228-27 L100522BSS00 89 160-5228-28 L100523BSS00 89 160-5228-29 L100524BSS00 96 LCS 160-101018/2-A Lab Control Sample 95 LCS 160-101020/2-A Lab Control Sample 96 MB 160-101018/1-A Method Blank 95 MB 160-101020/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 30 of 30 1 2 3 4 5 6 7 8 9 10 11 12}}

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