ML18010A309

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Final Status Survey Final Report Volume 3, Chapter 6, Survey Area Release Record for Land Survey Area 10, Analytical Report, 160-4779-2
ML18010A309
Person / Time
Site: 07000036
Issue date: 01/14/2014
From:
TestAmerica Labs - St. Louis, Westinghouse
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML18010A247 List: ... further results
References
HEM-17-72 160-4779-2
Download: ML18010A309 (18)
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-4779-2 Client Project/Site: RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

1/14/2014 9:35:14 AM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-4779-2 Page 2 of 18 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

4 Receipt Checklists.........................................

6 Definitions/Glossary.......................................

7 Method Summary.........................................

8 Sample Summary.........................................

9 Client Sample Results......................................

10 QC Sample Results........................................

17 QC Association Summary...................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-4779-2 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-4779-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)

Report Number: 160-4779-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 12/05/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 18.0 C.

RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)

Samples L101001BRS00 (160-4779-1), L101002BES00 (160-4779-2), L101003BRS00 (160-4779-3), L101005BRS00 (160-4779-4),

L101006BES00 (160-4779-5), L101007BRS00 (160-4779-6), L101008BES00 (160-4779-7), L101009BSS00 (160-4779-8),

L101010BRS00 (160-4779-9), L101011BSQ00 (160-4779-10), L101011BSS00 (160-4779-11), L101012BRS00 (160-4779-12),

L101013BSS00 (160-4779-13), L101014BRS00 (160-4779-14) and L101015BES00 (160-4779-15) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 12/18/2013, prepared on 12/20/2013 and analyzed on 01/11/2014.

No other difficulties were encountered during the Radium 226 analysis. All other quality control parameters were within the acceptance limits.

TestAmerica St. Louis Page 3 of 18 1

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I

Page 1 ofl Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the Coe. The Laboratory/End User must verify tha1 the sample is correctly identified before the sample is released for use or analysis and send the completed Coe to EDP.

Chain of Cutod:v ID No.

F-120513-01 Pa2e 1/2 Requested Analysis Laboratorv Name:

Project Name:

TA-MO

'!:)

N Westinghouse Electric Company N

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I Contact Person:

Laboratory Address:

Gerald Rood

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13715 Rider Trail North

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i Phone Number:

  • e Phone No.

314-810-3382 8 314-298-8566 s

Sampler Name

-a Laboratory Contact Person:

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§ Scott Jenkins

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s Joe Walker

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Phone No-ci o.

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OJ 708-870-8453

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Turn Around Time Q

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Sample ID Date Time Matrix 0

0 Remarks u

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I LIO l 00 lBRSOO 12/4/2013 10:15 s C

X X

1 LSA-10-10 Sys. Samples LIO 1002BESOO 12/4/2013 10:20 s

C..

X X

1 LSA-10-10 Sys. Samples LIOI003BRSOO 12/4/2013 10:45 s

C X

X 1 LSA-10-10 Sys. Samples LI01005BRSOO 12/4/2013 11:00 s C

X X

I LSA-10-10 Sys. Samples L 101006BESOO 12/4/2013 11 :05 s

C X

X 1 LSA-10-10 Sys. Samples LIO I 007BRSOO 12/4/2013 13:55 s

C X

X 1 LSA-10-10 Sys. Samples LI01008BESOO 12/4/2013 14:00 s C

X X

1 LSA-10-10 Sys. Samples LIO 1009BSSOO 12/4/2013 14:10 s C

X X

1 LSA-10-10 Sys. Samples Ll01010BRSOO 12/4/2013 14:25 s

C X

X 1 LSA-10-10 Sys. Samples LI01011BSQOO 12/4/2013 14:45 s

C X

X 1 LSA-10-10 QC Sample Ll01011BSSOO 12/4/2013 14:45 s

C X

X 1 LSA-10-10 Sys. Samples LI01012BRSOO 12/4/2013 14:55 s

C X

X I LSA-10-10 Sys. Samples Relinquished b?

r-Date/Time Ref~by: /?£}_

Date/Time Total Cooler Temperature:

r-2:1 A.,Q

{1/s ff:;e; l'i 4 nP.DTP.f>S: ('_

Company Namet..c) Et _

,2.-s-0/ Company Name:,

Cooler ID: Shipper and Number:

1<<5 n~foad.5 1?0-<i.O?

Received by:

Daterfime

~~d~y2/,.

DatelTime Comments: Please analyze the samples for Tc-99 on a 7 day 1,:'? i,;C; TAT. Please analyze the samples for gamma spec after a 21 day Company Name:

tompany Name:f

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ingrowth period.

/? h>,e.-e;:,v- -

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Relinquished by:

DatelTime Received by:

lvv, Date/Time

\\'l,{*\\.'3 Verified By:

Company Name:

Company Name: 1 Pr

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 I

Page 1 of 1 Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each tirne the container is transferred to another organization, a person frorn each organization should sign the Coe. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutodv ID No.

F-120513-01 Pa~e 2/2 Reauested Analvsis Laboratorv Name:

Project Name:

TA-MO

N I

o:j Contact Person:

~ Ji-Laboratory Address:

Gerald Rood

. c8 13715 Rider Trail North

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Phone Number:

IS Phone No.

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314-810-3382 0

314-298-8566 u

Sampler Name o:j

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-0 Scott Jenkins 8

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~ Joe Walker

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Phone No.

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Remarks 0

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L101013BSSOO 12/4/2013 15:05 s C

X X I LSA-10-10 Sys. Samples L101014BRSOO 12/4/2013 15:15 s

C X

X 1 LSA-10-10 Sys. Samples L101015BESOO 12/4/2013 9:45 s

C X

X 1 LSA-10-10 Sys. Samples Relinquished by{"'"~

Date/Time ~nh~

Date/Time Total Cooler Temperature:

15 4 nporpp<, C r~

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,1:'"',(:;'77 Company Name; I l 2..-&-R>-

lftompan~d:

Cooler ID: Shipper and Number:

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Received by:

Date/Time l~q~~by;a_d,,,,

D0/Tim.e Comments: Please analyze the samples for Tc-99 on a 7 day Company Name:

,1 to~anyName~.?

,i,,.,1~i TAT. Please analyze the samples for gamma spec after a 21 day Cl ~~V"'a ingrowth period.

Relinquished by:

Date/Time Received by: ~

Date/Time J'l* t;-\\3 Verified By:

Company Name:

CompanyName: i'ft

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  • Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-4779-2 Login Number: 4779 Question Answer Comment Creator: Daniels, Brian J List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

False Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Qualifiers Rad Qualifier Description U

Indicates the analyte was analyzed for but not detected.

Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 18 1

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Sample Summary TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-4779-1 L101001BRS00 Solid 12/04/13 10:15 12/05/13 18:00 160-4779-2 L101002BES00 Solid 12/04/13 10:20 12/05/13 18:00 160-4779-3 L101003BRS00 Solid 12/04/13 10:45 12/05/13 18:00 160-4779-4 L101005BRS00 Solid 12/04/13 11:00 12/05/13 18:00 160-4779-5 L101006BES00 Solid 12/04/13 11:05 12/05/13 18:00 160-4779-6 L101007BRS00 Solid 12/04/13 13:55 12/05/13 18:00 160-4779-7 L101008BES00 Solid 12/04/13 14:00 12/05/13 18:00 160-4779-8 L101009BSS00 Solid 12/04/13 14:10 12/05/13 18:00 160-4779-9 L101010BRS00 Solid 12/04/13 14:25 12/05/13 18:00 160-4779-10 L101011BSQ00 Solid 12/04/13 14:45 12/05/13 18:00 160-4779-11 L101011BSS00 Solid 12/04/13 14:45 12/05/13 18:00 160-4779-12 L101012BRS00 Solid 12/04/13 14:55 12/05/13 18:00 160-4779-13 L101013BSS00 Solid 12/04/13 15:05 12/05/13 18:00 160-4779-14 L101014BRS00 Solid 12/04/13 15:15 12/05/13 18:00 160-4779-15 L101015BES00 Solid 12/04/13 09:45 12/05/13 18:00 TestAmerica St. Louis Page 9 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4779-1 Client Sample ID: L101001BRS00 Matrix: Solid Date Collected: 12/04/13 10:15 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.15 (2+/-)

0.171 (2+/-)

1 01/11/14 02:36 12/20/13 15:39 pCi/g 0.117 RL MDC 0.125 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.406 0.489 0.462 1.54 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.0614 0.147 0.0964 1.07 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.0722 0.148 0.0724 1.00 Lead 212 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.0813 0.156 0.0913 1.22 Lead 214 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.346 2.35 1.14 20.1 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 02:36 1

1.08 0.253 0.248 U

0.455 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.0614 1.00 0.147 0.0964 1.07 Radium 226 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.117 0.171 0.125 1.15 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 02:36 1

1.04 0.319 0.307 U

0.812 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.235 0.168 0.167 U

0.134 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.101 0.0596 0.0596 U

0.000250 Americium 241 pCi/g 12/20/13 15:39 01/11/14 02:36 1

4.38 2.71 2.70 U

2.48 Protactinium 234m Lab Sample ID: 160-4779-2 Client Sample ID: L101002BES00 Matrix: Solid Date Collected: 12/04/13 10:20 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.991 (2+/-)

0.153 (2+/-)

1 01/11/14 02:34 12/20/13 15:39 pCi/g 0.125 RL MDC 0.115 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 02:34 1

0.376 0.473 0.444 1.58 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 02:34 1

0.0709 0.163 0.112 1.14 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 02:34 1

0.0603 0.149 0.0728 1.00 Lead 212 pCi/g 12/20/13 15:39 01/11/14 02:34 1

0.0691 0.162 0.0933 1.28 Lead 214 pCi/g 12/20/13 15:39 01/11/14 02:34 1

0.411 2.12 1.20 17.1 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 02:34 1

1.22 0.744 0.741 U

-0.624 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 02:34 1

0.0709 1.00 0.163 0.112 1.14 Radium 226 pCi/g 12/20/13 15:39 01/11/14 02:34 1

0.125 0.153 0.115 0.991 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 02:34 1

0.863 0.333 0.320 0.870 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 02:34 1

0.223 0.129 0.129 U

0.0667 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 02:34 1

0.0805 0.0808 0.0808 U

-0.00175 Americium 241 pCi/g 12/20/13 15:39 01/11/14 02:34 1

5.57 3.20 3.18 U

3.38 Protactinium 234m Lab Sample ID: 160-4779-3 Client Sample ID: L101003BRS00 Matrix: Solid Date Collected: 12/04/13 10:45 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.00 (2+/-)

0.187 (2+/-)

1 01/11/14 02:35 12/20/13 15:39 pCi/g 0.0949 RL MDC 0.157 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 02:35 1

0.398 0.498 0.478 1.35 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 02:35 1

0.0850 0.168 0.128 1.04 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 02:35 1

0.0727 0.135 0.0757 0.866 Lead 212 TestAmerica St. Louis Page 10 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4779-3 Client Sample ID: L101003BRS00 Matrix: Solid Date Collected: 12/04/13 10:45 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.14 (2+/-)

0.163 (2+/-)

1 01/11/14 02:35 12/20/13 15:39 pCi/g 0.0769 RL MDC 0.111 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 02:35 1

0.258 1.98 1.19 15.5 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 02:35 1

1.18 0.184 0.183 U

0.131 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 02:35 1

0.0850 1.00 0.168 0.128 1.04 Radium 226 pCi/g 12/20/13 15:39 01/11/14 02:35 1

0.0949 0.187 0.157 1.00 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 02:35 1

0.950 0.822 0.804 1.65 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 02:35 1

0.185 0.133 0.132 U

0.172 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 02:35 1

0.100 0.0593 0.0593 U

0.00189 Americium 241 pCi/g 12/20/13 15:39 01/11/14 02:35 1

6.05 3.36 3.36 U

0.165 Protactinium 234m Lab Sample ID: 160-4779-4 Client Sample ID: L101005BRS00 Matrix: Solid Date Collected: 12/04/13 11:00 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.808 (2+/-)

0.123 (2+/-)

1 01/11/14 02:36 12/20/13 15:39 pCi/g 0.0922 RL MDC 0.0910 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.313 0.274 0.258 0.870 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.0539 0.124 0.0848 0.874 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.0497 0.126 0.0595 0.860 Lead 212 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.0682 0.132 0.0822 0.992 Lead 214 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.386 1.62 0.924 13.0 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.843 0.196 0.192 U

0.353 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.0539 1.00 0.124 0.0848 0.874 Radium 226 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.0922 0.123 0.0910 0.808 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.710 0.568 0.551 1.34 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.141 0.0885 0.0870 0.155 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 02:36 1

0.0914 0.0549 0.0548 U

-0.0241 Americium 241 pCi/g 12/20/13 15:39 01/11/14 02:36 1

3.45 19.4 19.4 U

-0.485 Protactinium 234m Lab Sample ID: 160-4779-5 Client Sample ID: L101006BES00 Matrix: Solid Date Collected: 12/04/13 11:05 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.704 (2+/-)

0.142 (2+/-)

1 01/11/14 03:14 12/20/13 15:39 pCi/g 0.0786 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.217 0.282 0.266 0.898 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.0460 0.101 0.0703 0.693 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.0398 0.0974 0.0490 0.650 Lead 212 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.0492 0.110 0.0707 0.805 Lead 214 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.261 1.21 0.716 9.53 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.891 0.139 0.137 U

0.235 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.0460 1.00 0.101 0.0703 0.693 Radium 226 TestAmerica St. Louis Page 11 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4779-5 Client Sample ID: L101006BES00 Matrix: Solid Date Collected: 12/04/13 11:05 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 0.704 (2+/-)

0.142 (2+/-)

1 01/11/14 03:14 12/20/13 15:39 pCi/g 0.0786 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.644 0.233 0.223 U

0.638 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.171 0.102 0.102 U

0.0513 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.0761 0.0461 0.0460 U

0.0304 Americium 241 pCi/g 12/20/13 15:39 01/11/14 03:14 1

3.50 1.99 1.99 U

0.965 Protactinium 234m Lab Sample ID: 160-4779-6 Client Sample ID: L101007BRS00 Matrix: Solid Date Collected: 12/04/13 13:55 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.00 (2+/-)

0.182 (2+/-)

1 01/11/14 03:15 12/20/13 15:39 pCi/g 0.121 RL MDC 0.150 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.347 0.329 0.305 1.17 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.0649 0.154 0.103 1.11 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.0756 0.150 0.0750 1.00 Lead 212 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.0808 0.157 0.0919 1.22 Lead 214 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.411 2.29 1.17 19.3 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 03:15 1

1.13 0.200 0.197 U

0.298 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.0649 1.00 0.154 0.103 1.11 Radium 226 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.121 0.182 0.150 1.00 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.874 0.711 0.694 1.48 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.159 0.103 0.101 0.166 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.102 0.0616 0.0615 U

0.0288 Americium 241 pCi/g 12/20/13 15:39 01/11/14 03:15 1

5.22 3.16 3.12 U

5.06 Protactinium 234m Lab Sample ID: 160-4779-7 Client Sample ID: L101008BES00 Matrix: Solid Date Collected: 12/04/13 14:00 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.14 (2+/-)

0.168 (2+/-)

1 01/11/14 03:13 12/20/13 15:39 pCi/g 0.0886 RL MDC 0.122 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:13 1

0.467 0.514 0.494 1.37 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 03:13 1

0.0619 0.163 0.109 1.17 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 03:13 1

0.0514 0.157 0.0727 1.08 Lead 212 pCi/g 12/20/13 15:39 01/11/14 03:13 1

0.0818 0.157 0.0954 1.20 Lead 214 pCi/g 12/20/13 15:39 01/11/14 03:13 1

0.347 2.27 1.24 18.6 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 03:13 1

0.669 1.00 1.00 U

0.105 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 03:13 1

0.0619 1.00 0.163 0.109 1.17 Radium 226 pCi/g 12/20/13 15:39 01/11/14 03:13 1

0.0886 0.168 0.122 1.14 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 03:13 1

0.816 0.319 0.304 0.906 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 03:13 1

0.245 0.146 0.146 U

0.0672 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 03:13 1

0.0715 0.0415 0.0415 U

0.000123 Americium 241 TestAmerica St. Louis Page 12 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4779-7 Client Sample ID: L101008BES00 Matrix: Solid Date Collected: 12/04/13 14:00 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Protactinium 234m 1.91 U

(2+/-)

2.75 (2+/-)

1 01/11/14 03:13 12/20/13 15:39 pCi/g 4.58 RL MDC 2.75 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Lab Sample ID: 160-4779-8 Client Sample ID: L101009BSS00 Matrix: Solid Date Collected: 12/04/13 14:10 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.05 (2+/-)

0.175 (2+/-)

1 01/11/14 03:14 12/20/13 15:39 pCi/g 0.161 RL MDC 0.139 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.279 0.552 0.498 2.30 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.0848 0.167 0.127 1.04 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.0895 0.158 0.0900 1.00 Lead 212 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.0735 0.177 0.120 1.24 Lead 214 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.517 2.27 1.42 17.3 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 03:14 1

1.03 0.385 0.378 U

0.679 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.0848 1.00 0.167 0.127 1.04 Radium 226 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.161 0.175 0.139 1.05 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.997 0.796 0.783 1.38 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.188 0.107 0.106 U

0.159 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 03:14 1

0.123 0.0733 0.0733 U

0.0211 Americium 241 pCi/g 12/20/13 15:39 01/11/14 03:14 1

7.39 4.17 4.17 U

0.652 Protactinium 234m Lab Sample ID: 160-4779-9 Client Sample ID: L101010BRS00 Matrix: Solid Date Collected: 12/04/13 14:25 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.17 (2+/-)

0.187 (2+/-)

1 01/11/14 03:15 12/20/13 15:39 pCi/g 0.106 RL MDC 0.145 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.344 0.398 0.378 1.21 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.0806 0.162 0.116 1.09 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.0631 0.161 0.0753 1.10 Lead 212 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.0641 0.153 0.0892 1.19 Lead 214 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.379 2.42 1.23 20.4 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 03:15 1

1.09 0.658 0.656 U

-0.460 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.0806 1.00 0.162 0.116 1.09 Radium 226 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.106 0.187 0.145 1.17 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.848 0.664 0.643 1.61 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.237 0.132 0.131 U

0.153 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 03:15 1

0.0941 0.0567 0.0566 U

0.0319 Americium 241 pCi/g 12/20/13 15:39 01/11/14 03:15 1

5.23 3.09 3.08 U

2.17 Protactinium 234m TestAmerica St. Louis Page 13 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4779-10 Client Sample ID: L101011BSQ00 Matrix: Solid Date Collected: 12/04/13 14:45 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.28 (2+/-)

0.223 (2+/-)

1 01/11/14 03:53 12/20/13 15:39 pCi/g 0.128 RL MDC 0.181 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:53 1

0.675 0.500 0.488 1.07 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 03:53 1

0.0784 0.194 0.143 1.26 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 03:53 1

0.0851 0.174 0.0967 1.12 Lead 212 pCi/g 12/20/13 15:39 01/11/14 03:53 1

0.121 0.206 0.157 1.27 Lead 214 pCi/g 12/20/13 15:39 01/11/14 03:53 1

0.530 2.56 1.61 19.5 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 03:53 1

1.53 0.930 0.927 U

-0.744 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 03:53 1

0.0784 1.00 0.194 0.143 1.26 Radium 226 pCi/g 12/20/13 15:39 01/11/14 03:53 1

0.128 0.223 0.181 1.28 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 03:53 1

1.09 0.438 0.418 1.26 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 03:53 1

0.300 0.182 0.182 U

0.139 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 03:53 1

0.136 0.0807 0.0806 U

0.0178 Americium 241 pCi/g 12/20/13 15:39 01/11/14 03:53 1

7.34 4.56 4.53 U

4.83 Protactinium 234m Lab Sample ID: 160-4779-11 Client Sample ID: L101011BSS00 Matrix: Solid Date Collected: 12/04/13 14:45 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.938 (2+/-)

0.162 (2+/-)

1 01/11/14 03:49 12/20/13 15:39 pCi/g 0.104 RL MDC 0.131 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.389 0.461 0.442 1.29 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0730 0.162 0.112 1.13 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0591 0.164 0.0752 1.13 Lead 212 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0761 0.163 0.0920 1.30 Lead 214 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.354 2.24 1.16 18.7 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 03:49 1

1.28 0.190 0.185 U

0.373 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0730 1.00 0.162 0.112 1.13 Radium 226 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.104 0.162 0.131 0.938 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.962 0.802 0.782 1.71 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.173 0.123 0.122 U

0.157 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.111 0.0668 0.0667 U

0.0290 Americium 241 pCi/g 12/20/13 15:39 01/11/14 03:49 1

5.29 2.89 2.89 U

0.185 Protactinium 234m Lab Sample ID: 160-4779-12 Client Sample ID: L101012BRS00 Matrix: Solid Date Collected: 12/04/13 14:55 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.05 (2+/-)

0.177 (2+/-)

1 01/11/14 03:49 12/20/13 15:39 pCi/g 0.0957 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.431 0.463 0.446 1.21 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0658 0.163 0.108 1.18 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0773 0.148 0.0745 0.987 Lead 212 TestAmerica St. Louis Page 14 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4779-12 Client Sample ID: L101012BRS00 Matrix: Solid Date Collected: 12/04/13 14:55 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.14 (2+/-)

0.155 (2+/-)

1 01/11/14 03:49 12/20/13 15:39 pCi/g 0.0751 RL MDC 0.0995 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.438 2.35 1.18 19.9 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 03:49 1

1.19 0.238 0.232 U

0.456 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0658 1.00 0.163 0.108 1.18 Radium 226 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0957 0.177 0.141 1.05 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.795 0.320 0.302 1.02 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.251 0.151 0.151 U

0.0617 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.101 0.0604 0.0604 U

-0.00931 Americium 241 pCi/g 12/20/13 15:39 01/11/14 03:49 1

6.49 1.95 1.94 U

0.372 Protactinium 234m Lab Sample ID: 160-4779-13 Client Sample ID: L101013BSS00 Matrix: Solid Date Collected: 12/04/13 15:05 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.16 (2+/-)

0.177 (2+/-)

1 01/11/14 03:48 12/20/13 15:39 pCi/g 0.121 RL MDC 0.132 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:48 1

0.478 0.521 0.500 1.38 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 03:48 1

0.0836 0.176 0.128 1.16 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 03:48 1

0.0709 0.158 0.0821 1.05 Lead 212 pCi/g 12/20/13 15:39 01/11/14 03:48 1

0.0721 0.159 0.105 1.14 Lead 214 pCi/g 12/20/13 15:39 01/11/14 03:48 1

0.292 2.46 1.36 20.0 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 03:48 1

1.28 0.779 0.776 U

-0.574 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 03:48 1

0.0836 1.00 0.176 0.128 1.16 Radium 226 pCi/g 12/20/13 15:39 01/11/14 03:48 1

0.121 0.177 0.132 1.16 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 03:48 1

0.814 0.632 0.604 1.78 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 03:48 1

0.187 0.139 0.139 U

0.160 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 03:48 1

0.109 0.0657 0.0656 U

0.0376 Americium 241 pCi/g 12/20/13 15:39 01/11/14 03:48 1

6.07 3.43 3.43 U

0.690 Protactinium 234m Lab Sample ID: 160-4779-14 Client Sample ID: L101014BRS00 Matrix: Solid Date Collected: 12/04/13 15:15 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.03 (2+/-)

0.175 (2+/-)

1 01/11/14 03:49 12/20/13 15:39 pCi/g 0.143 RL MDC 0.140 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.613 0.410 0.405 0.656 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0809 0.172 0.127 1.12 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0744 0.145 0.0795 0.940 Lead 212 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0826 0.158 0.100 1.18 Lead 214 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.395 2.16 1.29 16.9 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 03:49 1

1.33 0.223 0.217 U

0.486 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.0809 1.00 0.172 0.127 1.12 Radium 226 TestAmerica St. Louis Page 15 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-4779-14 Client Sample ID: L101014BRS00 Matrix: Solid Date Collected: 12/04/13 15:15 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 1.03 (2+/-)

0.175 (2+/-)

1 01/11/14 03:49 12/20/13 15:39 pCi/g 0.143 RL MDC 0.140 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.953 0.802 0.787 1.51 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.281 0.158 0.158 U

0.0722 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 03:49 1

0.111 0.0660 0.0660 U

0.0137 Americium 241 pCi/g 12/20/13 15:39 01/11/14 03:49 1

7.90 1.20 1.20 U

0.000 Protactinium 234m Lab Sample ID: 160-4779-15 Client Sample ID: L101015BES00 Matrix: Solid Date Collected: 12/04/13 09:45 Date Received: 12/05/13 18:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.23 (2+/-)

0.176 (2+/-)

1 01/11/14 03:50 12/20/13 15:39 pCi/g 0.0881 RL MDC 0.124 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/20/13 15:39 01/11/14 03:50 1

0.355 0.434 0.407 1.47 Bismuth 212 pCi/g 12/20/13 15:39 01/11/14 03:50 1

0.0662 0.144 0.0935 1.06 Bismuth 214 pCi/g 12/20/13 15:39 01/11/14 03:50 1

0.0532 0.159 0.0708 1.10 Lead 212 pCi/g 12/20/13 15:39 01/11/14 03:50 1

0.0784 0.169 0.108 1.25 Lead 214 pCi/g 12/20/13 15:39 01/11/14 03:50 1

0.347 2.33 1.16 19.7 Potassium 40 pCi/g 12/20/13 15:39 01/11/14 03:50 1

1.10 0.194 0.190 U

0.358 Protactinium 231 pCi/g 12/20/13 15:39 01/11/14 03:50 1

0.0662 1.00 0.144 0.0935 1.06 Radium 226 pCi/g 12/20/13 15:39 01/11/14 03:50 1

0.0881 0.176 0.124 1.23 Thorium 232 pCi/g 12/20/13 15:39 01/11/14 03:50 1

0.879 0.740 0.716 1.79 Thorium 234 pCi/g 12/20/13 15:39 01/11/14 03:50 1

0.237 0.142 0.142 U

0.0629 Uranium 235 pCi/g 12/20/13 15:39 01/11/14 03:50 1

0.102 0.0612 0.0611 U

0.0288 Americium 241 pCi/g 12/20/13 15:39 01/11/14 03:50 1

5.02 2.94 2.94 U

1.84 Protactinium 234m TestAmerica St. Louis Page 16 of 18 1

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QC Sample Results TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-93852/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 97574 Prep Batch: 93852 Actinium 228 Analyte U

1 01/11/14 02:40 12/20/13 15:39 pCi/g 0.0746 MDC RL 0.0375 0.0375 (2+/-)

(2+/-)

MB 0.004657 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

01/11/14 02:40 12/20/13 15:39 pCi/g 0.276 0.0352 0.0352 U

0.0000 Bismuth 212 1

01/11/14 02:40 12/20/13 15:39 pCi/g 0.0495 0.0254 0.0254 U

0.004073 Bismuth 214 1

01/11/14 02:40 12/20/13 15:39 pCi/g 0.0281 0.0177 0.0177 U

-0.001058 Lead 212 1

01/11/14 02:40 12/20/13 15:39 pCi/g 0.0355 0.0160 0.0160 U

0.008294 Lead 214 1

01/11/14 02:40 12/20/13 15:39 pCi/g 0.290 3.96 3.96 U

-0.09901 Potassium 40 1

01/11/14 02:40 12/20/13 15:39 pCi/g 0.420 0.231 0.231 U

-0.05956 Protactinium 231 1

01/11/14 02:40 12/20/13 15:39 pCi/g 0.0495 1.00 0.0254 0.0254 U

0.004073 Radium 226 1

01/11/14 02:40 12/20/13 15:39 pCi/g 0.0746 0.0375 0.0375 U

0.004657 Thorium 232 1

01/11/14 02:40 12/20/13 15:39 pCi/g 0.317 0.737 0.737 U

-0.1341 Thorium 234 1

01/11/14 02:40 12/20/13 15:39 pCi/g 0.0693 0.0389 0.0388 U

0.01321 Uranium 235 1

01/11/14 02:40 12/20/13 15:39 pCi/g 0.0252 0.0139 0.0139 U

0.002359 Americium 241 1

01/11/14 02:40 12/20/13 15:39 pCi/g 1.56 0.944 0.944 U

0.09068 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-93852/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 97576 Prep Batch: 93852 Americium 241 Analyte 116 87 98 98.68 101 10.3 0.565 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 35.9 34.77 3.64 0.145 pCi/g 97 87 - 120 Cobalt 60 42.5 40.13 4.04 0.0874 pCi/g 94 87 - 115 Client Sample ID: L101001BRS00 Lab Sample ID: 160-4779-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 97574 Prep Batch: 93852 Actinium 228 Analyte 1

0.15 1.094 1.15 0.209 0.144 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.54 1.571 0.466 0.319 pCi/g 0.03 1

Bismuth 214 1.07 1.158 0.176 0.0741 pCi/g 0.26 1

Lead 212 1.00 1.118 0.170 0.0786 pCi/g 0.37 1

Lead 214 1.22 1.317 0.182 0.0950 pCi/g 0.30 1

Potassium 40 20.1 16.96 2.25 0.569 pCi/g 0.68 1

Protactinium 231 0.455 U

0.7831 U

0.365 1.40 pCi/g 0.53 1

Radium 226 1.07 1.158 0.176 1.00 0.0741 pCi/g 0.26 1

Thorium 232 1.15 1.094 0.209 0.144 pCi/g 0.15 1

Thorium 234 0.812 U

1.745 0.811 0.993 pCi/g 0.83 1

Uranium 235 0.134 U

0.09598 U

0.165 0.267 pCi/g 0.11 1

Americium 241 0.000250 U

-0.02177 U

0.0767 0.128 pCi/g 0.16 1

Protactinium 234m 2.48 U

0.09730 U

4.32 7.75 pCi/g 0.34 1

TestAmerica St. Louis Page 17 of 18 1

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QC Association Summary TestAmerica Job ID: 160-4779-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Rad Leach Batch: 92870 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-4779-1 L101001BRS00 Total/NA Solid Dry and Grind 160-4779-1 DU L101001BRS00 Total/NA Solid Dry and Grind 160-4779-2 L101002BES00 Total/NA Solid Dry and Grind 160-4779-3 L101003BRS00 Total/NA Solid Dry and Grind 160-4779-4 L101005BRS00 Total/NA Solid Dry and Grind 160-4779-5 L101006BES00 Total/NA Solid Dry and Grind 160-4779-6 L101007BRS00 Total/NA Solid Dry and Grind 160-4779-7 L101008BES00 Total/NA Solid Dry and Grind 160-4779-8 L101009BSS00 Total/NA Solid Dry and Grind 160-4779-9 L101010BRS00 Total/NA Solid Dry and Grind 160-4779-10 L101011BSQ00 Total/NA Solid Dry and Grind 160-4779-11 L101011BSS00 Total/NA Solid Dry and Grind 160-4779-12 L101012BRS00 Total/NA Solid Dry and Grind 160-4779-13 L101013BSS00 Total/NA Solid Dry and Grind 160-4779-14 L101014BRS00 Total/NA Solid Dry and Grind 160-4779-15 L101015BES00 Total/NA Prep Batch: 93852 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 92870 160-4779-1 L101001BRS00 Total/NA Solid Fill_Geo-21 92870 160-4779-1 DU L101001BRS00 Total/NA Solid Fill_Geo-21 92870 160-4779-2 L101002BES00 Total/NA Solid Fill_Geo-21 92870 160-4779-3 L101003BRS00 Total/NA Solid Fill_Geo-21 92870 160-4779-4 L101005BRS00 Total/NA Solid Fill_Geo-21 92870 160-4779-5 L101006BES00 Total/NA Solid Fill_Geo-21 92870 160-4779-6 L101007BRS00 Total/NA Solid Fill_Geo-21 92870 160-4779-7 L101008BES00 Total/NA Solid Fill_Geo-21 92870 160-4779-8 L101009BSS00 Total/NA Solid Fill_Geo-21 92870 160-4779-9 L101010BRS00 Total/NA Solid Fill_Geo-21 92870 160-4779-10 L101011BSQ00 Total/NA Solid Fill_Geo-21 92870 160-4779-11 L101011BSS00 Total/NA Solid Fill_Geo-21 92870 160-4779-12 L101012BRS00 Total/NA Solid Fill_Geo-21 92870 160-4779-13 L101013BSS00 Total/NA Solid Fill_Geo-21 92870 160-4779-14 L101014BRS00 Total/NA Solid Fill_Geo-21 92870 160-4779-15 L101015BES00 Total/NA Solid Fill_Geo-21 LCS 160-93852/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-93852/1-A Method Blank Total/NA TestAmerica St. Louis Page 18 of 18 1

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