ML18010A299

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Final Status Survey Final Report Volume 3, Chapter 6, Survey Area Release Record for Land Survey Area 10, Analytical Report, 160-3234-2
ML18010A299
Person / Time
Site: 07000036
Issue date: 09/20/2013
From:
Testamerica Labs, Westinghouse
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML18010A247 List: ... further results
References
HEM-17-72 160-3234-2
Download: ML18010A299 (19)
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3234-2 Client Project/Site: RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

9/3/2013 5:24:07 PM Ivan Vania, Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-3234-2 Page 2 of 19 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

5 Receipt Checklists.........................................

7 Definitions/Glossary.......................................

8 Method Summary.........................................

9 Sample Summary.........................................

10 Client Sample Results......................................

11 QC Sample Results........................................

18 QC Association Summary...................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3234-2 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-3234-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)

Report Number: 160-3234-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 08/03/2013; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 4 coolers at receipt time were 0.8º C, 2.2º C, 23.7º C and 25.1º C.

TECHNETIUM-99 (ICPMS)

Samples L100801BRS00 (160-3234-1), L100802BES00 (160-3234-2), L100803BES00 (160-3234-3), L100804BRS00 (160-3234-4),

L100805BES00 (160-3234-5), L100806BES00 (160-3234-6), L100807BRQ00 (160-3234-7), L100807BRS00 (160-3234-8),

L100808BES00 (160-3234-9), L100809BES00 (160-3234-10), L100810BES00 (160-3234-11), L100811BRS00 (160-3234-12),

L100812BES00 (160-3234-13), L100813BES00 (160-3234-14) and L100814BRS00 (160-3234-15) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 08/07/2013 and analyzed on 08/09/2013.

No difficulties were encountered during the Tc-99 analysis. All quality control parameters were within the acceptance limits.

PERCENT SOLIDS Samples L100801BRS00 (160-3234-1), L100802BES00 (160-3234-2), L100803BES00 (160-3234-3), L100804BRS00 (160-3234-4),

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3234-2 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-3234-2 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

L100805BES00 (160-3234-5), L100806BES00 (160-3234-6), L100807BRQ00 (160-3234-7), L100807BRS00 (160-3234-8),

L100808BES00 (160-3234-9), L100809BES00 (160-3234-10), L100810BES00 (160-3234-11), L100811BRS00 (160-3234-12),

L100812BES00 (160-3234-13), L100813BES00 (160-3234-14) and L100814BRS00 (160-3234-15) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 08/05/2013.

No difficulties were encountered during the % solids analysis. All quality control parameters were within the acceptance limits.

CESIUM-137 & OTHER GAMMA EMITTERS (GS)

Samples L100801BRS00 (160-3234-1), L100802BES00 (160-3234-2), L100803BES00 (160-3234-3), L100804BRS00 (160-3234-4),

L100805BES00 (160-3234-5), L100806BES00 (160-3234-6), L100807BRQ00 (160-3234-7), L100807BRS00 (160-3234-8),

L100808BES00 (160-3234-9), L100809BES00 (160-3234-10), L100810BES00 (160-3234-11), L100811BRS00 (160-3234-12),

L100812BES00 (160-3234-13), L100813BES00 (160-3234-14) and L100814BRS00 (160-3234-15) were analyzed for Cesium-137 &

Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 08/06/2013, prepared on 08/08/2013 and analyzed on 08/08/2013, 08/09/2013 and 08/12/2013.

Preparation Batch 65532:

Lead-214 analyzed by gamma spectroscopy was detected above the MDC in the method blank. Variations in Compton backgrounds and statistical analyses allow for small area counts in the ROIs of this nuclide. Other Uranium decay chain products are not present in the blank to support Lead-214 identification. The data is reported. (160-3234-1 DU), (LCS 160-65532/2-A), (MB 160-65532/1-A),

L100801BRS00 (160-3234-1), L100802BES00 (160-3234-2), L100803BES00 (160-3234-3), L100804BRS00 (160-3234-4),

L100805BES00 (160-3234-5), L100806BES00 (160-3234-6), L100807BRQ00 (160-3234-7), L100807BRS00 (160-3234-8),

L100808BES00 (160-3234-9), L100809BES00 (160-3234-10), L100810BES00 (160-3234-11), L100811BRS00 (160-3234-12),

L100812BES00 (160-3234-13), L100813BES00 (160-3234-14), L100814BRS00 (160-3234-15)

No other difficulties were encountered during the Gamma spec analysis. All other quality control parameters were within the acceptance limits.

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 3 I

Page 1 ofll Westinghouse Non-Proprietary (lass 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HOP.

Chain of Cutody ID No. I F-080213-02 Paee Project Name:

Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number:

314-810-3_..3.82 Sampler Name Scott Jenkins 1/2 1:.

Reqii~sted An:~ly,siS,

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Laboratory Address:

'8 13715 Rider Trail North

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!Comments: Please re-analyze samples after a 21 day ingrowth period.

Date/Time Verified By:

_C_

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,Procedure HDP,PR-QA-006, Chain of Custody Hematite Decommissioning Project 'Revision: 3 I

Page 1 of 11 Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization., a person from each organization should sign the CoC. The Laboratozy/End User must verify that the sample is correctly identified before the sample is released for use ot analysis and send the completed CoC to HDP.

Chain of Cutody ID No. I F-080213-02 Page 2/2 Project Name:

Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number:

314-_1!10-338_2 Sampler Name Scott Jenkins Sample ID Date Time Matrix Laboratorv Name:

TA-MO Laboratory Address:

13715 Rider Trail North Phone No.

314-298-8566 Laboratory Contact Person:

Joe Walker Phone No.

708-870-8453 Rush Tum Around ]'ime (7 days) 8/1/2013

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Date/Time I Comments: Please re-analyze samples after a 21 day ingrowth period.

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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3234-2 Login Number: 3234 Question Answer Comment Creator: Vania, Ivan H List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

True Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

Where requried True Cooler Temperature is acceptable.

See NCM True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

True Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Qualifiers Rad Qualifier Description U

Indicates the analyte was analyzed for but not detected.

Qualifier F

Duplicate RPD exceeds the control limit Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 19 1

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Sample Summary TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-3234-1 L100801BRS00 Solid 08/01/13 15:14 08/03/13 16:01 160-3234-2 L100802BES00 Solid 08/01/13 15:23 08/03/13 16:01 160-3234-3 L100803BES00 Solid 08/01/13 15:54 08/03/13 16:01 160-3234-4 L100804BRS00 Solid 08/01/13 16:02 08/03/13 16:01 160-3234-5 L100805BES00 Solid 08/01/13 16:08 08/03/13 16:01 160-3234-6 L100806BES00 Solid 08/01/13 16:16 08/03/13 16:01 160-3234-7 L100807BRQ00 Solid 08/01/13 17:40 08/03/13 16:01 160-3234-8 L100807BRS00 Solid 08/01/13 17:40 08/03/13 16:01 160-3234-9 L100808BES00 Solid 08/01/13 17:45 08/03/13 16:01 160-3234-10 L100809BES00 Solid 08/01/13 16:35 08/03/13 16:01 160-3234-11 L100810BES00 Solid 08/01/13 16:48 08/03/13 16:01 160-3234-12 L100811BRS00 Solid 08/01/13 18:15 08/03/13 16:01 160-3234-13 L100812BES00 Solid 08/01/13 18:09 08/03/13 16:01 160-3234-14 L100813BES00 Solid 08/01/13 17:01 08/03/13 16:01 160-3234-15 L100814BRS00 Solid 08/01/13 18:00 08/03/13 16:01 TestAmerica St. Louis Page 10 of 19 1

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Client Sample Results TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3234-1 Client Sample ID: L100801BRS00 Matrix: Solid Date Collected: 08/01/13 15:14 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.952 (2+/-)

0.161 (2+/-)

1 09/02/13 20:53 08/08/13 10:41 pCi/g 0.0912 RL MDC 0.128 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 09/02/13 20:53 1

0.373 0.379 0.363 1.08 Bismuth 212 pCi/g 08/08/13 10:41 09/02/13 20:53 1

0.0683 0.142 0.0991 0.973 Bismuth 214 pCi/g 08/08/13 10:41 09/02/13 20:53 1

0.0618 0.147 0.0703 0.999 Lead 212 pCi/g 08/08/13 10:41 09/02/13 20:53 1

0.0755 0.149 0.0882 1.15 Lead 214 pCi/g 08/08/13 10:41 09/02/13 20:53 1

0.342 1.95 1.04 16.2 Potassium 40 pCi/g 08/08/13 10:41 09/02/13 20:53 1

1.14 0.224 0.220 U

0.419 Protactinium 231 pCi/g 08/08/13 10:41 09/02/13 20:53 1

0.0683 1.00 0.142 0.0991 0.973 Radium 226 pCi/g 08/08/13 10:41 09/02/13 20:53 1

0.0912 0.161 0.128 0.952 Thorium 232 pCi/g 08/08/13 10:41 09/02/13 20:53 1

1.13 0.838 0.560 5.97 Thorium 234 pCi/g 08/08/13 10:41 09/02/13 20:53 1

0.281 0.308 0.264 1.55 Uranium 235 pCi/g 08/08/13 10:41 09/02/13 20:53 1

0.124 0.0743 0.0743 U

0.0254 Americium 241 pCi/g 08/08/13 10:41 09/02/13 20:53 1

3.26 4.32 4.02 15.7 Protactinium 234m Lab Sample ID: 160-3234-2 Client Sample ID: L100802BES00 Matrix: Solid Date Collected: 08/01/13 15:23 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.01 (2+/-)

0.175 (2+/-)

1 08/30/13 04:02 08/08/13 10:41 pCi/g 0.157 RL MDC 0.142 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 04:02 1

0.438 0.464 0.447 1.17 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 04:02 1

0.0765 0.160 0.117 1.05 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 04:02 1

0.0655 0.156 0.0784 1.04 Lead 212 pCi/g 08/08/13 10:41 08/30/13 04:02 1

0.0858 0.157 0.106 1.11 Lead 214 pCi/g 08/08/13 10:41 08/30/13 04:02 1

0.160 2.18 1.24 17.6 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 04:02 1

1.18 0.267 0.261 U

0.525 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 04:02 1

0.0765 1.00 0.160 0.117 1.05 Radium 226 pCi/g 08/08/13 10:41 08/30/13 04:02 1

0.157 0.175 0.142 1.01 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 04:02 1

0.822 0.638 0.617 1.58 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 04:02 1

0.253 0.148 0.147 U

0.165 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 04:02 1

0.106 0.0623 0.0623 U

0.00525 Americium 241 pCi/g 08/08/13 10:41 08/30/13 04:02 1

6.07 3.66 3.65 U

2.60 Protactinium 234m Lab Sample ID: 160-3234-3 Client Sample ID: L100803BES00 Matrix: Solid Date Collected: 08/01/13 15:54 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.05 (2+/-)

0.173 (2+/-)

1 08/30/13 04:01 08/08/13 10:41 pCi/g 0.113 RL MDC 0.136 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 04:01 1

0.490 0.396 0.381 1.05 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 04:01 1

0.0882 0.161 0.125 0.978 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 04:01 1

0.0703 0.144 0.0779 0.939 Lead 212 TestAmerica St. Louis Page 11 of 19 1

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Client Sample Results TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3234-3 Client Sample ID: L100803BES00 Matrix: Solid Date Collected: 08/01/13 15:54 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.11 (2+/-)

0.149 (2+/-)

1 08/30/13 04:01 08/08/13 10:41 pCi/g 0.0747 RL MDC 0.0938 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 04:01 1

0.171 2.22 1.28 17.7 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 04:01 1

1.36 0.409 0.402 U

0.732 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 04:01 1

0.0882 1.00 0.161 0.125 0.978 Radium 226 pCi/g 08/08/13 10:41 08/30/13 04:01 1

0.113 0.173 0.136 1.05 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 04:01 1

0.928 0.751 0.728 1.79 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 04:01 1

0.229 0.189 0.185 0.373 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 04:01 1

0.118 0.0702 0.0702 U

0.00538 Americium 241 pCi/g 08/08/13 10:41 08/30/13 04:01 1

5.86 3.62 3.59 U

4.07 Protactinium 234m Lab Sample ID: 160-3234-4 Client Sample ID: L100804BRS00 Matrix: Solid Date Collected: 08/01/13 16:02 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.799 (2+/-)

0.161 (2+/-)

1 08/30/13 04:03 08/08/13 10:41 pCi/g 0.0980 RL MDC 0.139 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 04:03 1

0.396 0.403 0.391 0.922 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 04:03 1

0.0528 0.132 0.0878 0.943 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 04:03 1

0.0522 0.132 0.0632 0.900 Lead 212 pCi/g 08/08/13 10:41 08/30/13 04:03 1

0.0611 0.138 0.0881 1.03 Lead 214 pCi/g 08/08/13 10:41 08/30/13 04:03 1

0.284 1.89 0.995 15.7 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 04:03 1

0.968 0.303 0.298 U

0.523 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 04:03 1

0.0528 1.00 0.132 0.0878 0.943 Radium 226 pCi/g 08/08/13 10:41 08/30/13 04:03 1

0.0980 0.161 0.139 0.799 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 04:03 1

0.800 0.623 0.612 1.12 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 04:03 1

0.215 0.128 0.128 U

0.109 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 04:03 1

0.0861 0.0512 0.0512 U

0.0102 Americium 241 pCi/g 08/08/13 10:41 08/30/13 04:03 1

4.52 2.12 2.11 U

1.69 Protactinium 234m Lab Sample ID: 160-3234-5 Client Sample ID: L100805BES00 Matrix: Solid Date Collected: 08/01/13 16:08 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.869 (2+/-)

0.135 (2+/-)

1 08/30/13 08:34 08/08/13 10:41 pCi/g 0.101 RL MDC 0.101 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 08:34 1

0.334 0.380 0.365 0.997 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 08:34 1

0.0670 0.144 0.0998 0.993 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 08:34 1

0.0709 0.124 0.0655 0.812 Lead 212 pCi/g 08/08/13 10:41 08/30/13 08:34 1

0.0653 0.144 0.0847 1.12 Lead 214 pCi/g 08/08/13 10:41 08/30/13 08:34 1

0.251 2.01 0.982 17.1 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 08:34 1

0.947 0.254 0.251 U

0.368 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 08:34 1

0.0670 1.00 0.144 0.0998 0.993 Radium 226 TestAmerica St. Louis Page 12 of 19 1

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Client Sample Results TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3234-5 Client Sample ID: L100805BES00 Matrix: Solid Date Collected: 08/01/13 16:08 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 0.869 (2+/-)

0.135 (2+/-)

1 08/30/13 08:34 08/08/13 10:41 pCi/g 0.101 RL MDC 0.101 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 08:34 1

0.806 0.651 0.638 1.24 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 08:34 1

0.182 0.118 0.117 U

0.129 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 08:34 1

0.0982 0.0586 0.0586 U

-0.0134 Americium 241 pCi/g 08/08/13 10:41 08/30/13 08:34 1

3.88 1.96 1.93 U

3.44 Protactinium 234m Lab Sample ID: 160-3234-6 Client Sample ID: L100806BES00 Matrix: Solid Date Collected: 08/01/13 16:16 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.829 (2+/-)

0.136 (2+/-)

1 08/30/13 08:31 08/08/13 10:41 pCi/g 0.104 RL MDC 0.107 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 08:31 1

0.340 0.426 0.403 1.34 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 08:31 1

0.0614 0.151 0.104 1.05 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 08:31 1

0.0550 0.120 0.0640 0.789 Lead 212 pCi/g 08/08/13 10:41 08/30/13 08:31 1

0.0796 0.133 0.0809 1.01 Lead 214 pCi/g 08/08/13 10:41 08/30/13 08:31 1

0.138 1.77 1.03 14.1 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 08:31 1

1.11 0.164 0.162 U

0.241 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 08:31 1

0.0614 1.00 0.151 0.104 1.05 Radium 226 pCi/g 08/08/13 10:41 08/30/13 08:31 1

0.104 0.136 0.107 0.829 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 08:31 1

0.786 0.640 0.625 1.31 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 08:31 1

0.214 0.127 0.127 U

0.0289 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 08:31 1

0.0845 0.0505 0.0504 U

0.0244 Americium 241 pCi/g 08/08/13 10:41 08/30/13 08:31 1

4.90 2.79 2.79 U

-0.734 Protactinium 234m Lab Sample ID: 160-3234-7 Client Sample ID: L100807BRQ00 Matrix: Solid Date Collected: 08/01/13 17:40 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.817 (2+/-)

0.139 (2+/-)

1 08/30/13 08:32 08/08/13 10:41 pCi/g 0.0976 RL MDC 0.111 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 08:32 1

0.456 0.513 0.497 1.20 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 08:32 1

0.0783 0.151 0.118 0.907 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 08:32 1

0.0629 0.113 0.0676 0.704 Lead 212 pCi/g 08/08/13 10:41 08/30/13 08:32 1

0.0654 0.140 0.0939 1.00 Lead 214 pCi/g 08/08/13 10:41 08/30/13 08:32 1

0.169 1.82 1.13 14.0 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 08:32 1

1.22 0.252 0.249 U

0.348 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 08:32 1

0.0783 1.00 0.151 0.118 0.907 Radium 226 pCi/g 08/08/13 10:41 08/30/13 08:32 1

0.0976 0.139 0.111 0.817 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 08:32 1

0.757 0.283 0.274 U

0.671 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 08:32 1

0.257 0.144 0.143 U

0.132 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 08:32 1

0.0995 0.0587 0.0587 U

0.00291 Americium 241 TestAmerica St. Louis Page 13 of 19 1

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Client Sample Results TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3234-7 Client Sample ID: L100807BRQ00 Matrix: Solid Date Collected: 08/01/13 17:40 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Protactinium 234m 1.31 U

(2+/-)

2.82 (2+/-)

1 08/30/13 08:32 08/08/13 10:41 pCi/g 4.87 RL MDC 2.81 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Lab Sample ID: 160-3234-8 Client Sample ID: L100807BRS00 Matrix: Solid Date Collected: 08/01/13 17:40 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.770 (2+/-)

0.125 (2+/-)

1 08/30/13 08:33 08/08/13 10:41 pCi/g 0.0715 RL MDC 0.0967 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 08:33 1

0.323 0.363 0.347 1.00 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 08:33 1

0.0591 0.132 0.0909 0.923 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 08:33 1

0.0478 0.111 0.0546 0.749 Lead 212 pCi/g 08/08/13 10:41 08/30/13 08:33 1

0.0590 0.132 0.0850 0.976 Lead 214 pCi/g 08/08/13 10:41 08/30/13 08:33 1

0.299 1.55 0.853 12.7 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 08:33 1

0.875 0.209 0.205 U

0.357 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 08:33 1

0.0591 1.00 0.132 0.0909 0.923 Radium 226 pCi/g 08/08/13 10:41 08/30/13 08:33 1

0.0715 0.125 0.0967 0.770 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 08:33 1

0.606 0.430 0.424 0.658 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 08:33 1

0.182 0.104 0.104 U

0.0499 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 08:33 1

0.0776 0.0461 0.0461 U

-0.00656 Americium 241 pCi/g 08/08/13 10:41 08/30/13 08:33 1

3.07 1.79 1.79 U

0.908 Protactinium 234m Lab Sample ID: 160-3234-9 Client Sample ID: L100808BES00 Matrix: Solid Date Collected: 08/01/13 17:45 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.01 (2+/-)

0.151 (2+/-)

1 08/30/13 09:56 08/08/13 10:41 pCi/g 0.0755 RL MDC 0.110 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.370 0.491 0.466 1.51 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.0614 0.148 0.0972 1.08 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.0505 0.160 0.0677 1.12 Lead 212 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.0709 0.144 0.0897 1.08 Lead 214 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.309 2.05 1.02 17.3 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.871 0.455 0.449 U

0.670 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.0614 1.00 0.148 0.0972 1.08 Radium 226 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.0755 0.151 0.110 1.01 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.797 0.321 0.311 U

0.737 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.231 0.0702 0.0701 U

0.0388 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.106 0.0630 0.0630 U

-0.00229 Americium 241 pCi/g 08/08/13 10:41 08/30/13 09:56 1

4.93 2.83 2.83 U

0.546 Protactinium 234m TestAmerica St. Louis Page 14 of 19 1

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Client Sample Results TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3234-10 Client Sample ID: L100809BES00 Matrix: Solid Date Collected: 08/01/13 16:35 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.842 (2+/-)

0.150 (2+/-)

1 08/30/13 09:57 08/08/13 10:41 pCi/g 0.102 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 09:57 1

0.334 0.396 0.379 1.13 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 09:57 1

0.0663 0.134 0.0965 0.896 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 09:57 1

0.0657 0.118 0.0633 0.773 Lead 212 pCi/g 08/08/13 10:41 08/30/13 09:57 1

0.0676 0.140 0.0863 1.06 Lead 214 pCi/g 08/08/13 10:41 08/30/13 09:57 1

0.266 1.84 0.954 15.4 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 09:57 1

1.01 0.175 0.172 U

0.304 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 09:57 1

0.0663 1.00 0.134 0.0965 0.896 Radium 226 pCi/g 08/08/13 10:41 08/30/13 09:57 1

0.102 0.150 0.123 0.842 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 09:57 1

0.789 0.634 0.623 1.12 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 09:57 1

0.205 0.130 0.130 U

0.0915 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 09:57 1

0.0876 0.0523 0.0523 U

0.0159 Americium 241 pCi/g 08/08/13 10:41 08/30/13 09:57 1

4.29 2.50 2.50 U

0.977 Protactinium 234m Lab Sample ID: 160-3234-11 Client Sample ID: L100810BES00 Matrix: Solid Date Collected: 08/01/13 16:48 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.833 (2+/-)

0.146 (2+/-)

1 08/30/13 09:54 08/08/13 10:41 pCi/g 0.0994 RL MDC 0.118 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 09:54 1

0.227 0.288 0.270 0.944 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 09:54 1

0.0579 0.129 0.0933 0.854 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 09:54 1

0.0532 0.115 0.0617 0.749 Lead 212 pCi/g 08/08/13 10:41 08/30/13 09:54 1

0.0549 0.143 0.0908 1.06 Lead 214 pCi/g 08/08/13 10:41 08/30/13 09:54 1

0.135 1.73 1.00 13.8 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 09:54 1

1.03 0.224 0.221 U

0.338 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 09:54 1

0.0579 1.00 0.129 0.0933 0.854 Radium 226 pCi/g 08/08/13 10:41 08/30/13 09:54 1

0.0994 0.146 0.118 0.833 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 09:54 1

0.730 0.574 0.558 1.30 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 09:54 1

0.223 0.129 0.129 U

0.0951 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 09:54 1

0.0906 0.0534 0.0534 U

0.00361 Americium 241 pCi/g 08/08/13 10:41 08/30/13 09:54 1

4.33 2.80 2.80 U

0.000 Protactinium 234m Lab Sample ID: 160-3234-12 Client Sample ID: L100811BRS00 Matrix: Solid Date Collected: 08/01/13 18:15 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.808 (2+/-)

0.123 (2+/-)

1 08/30/13 09:56 08/08/13 10:41 pCi/g 0.0948 RL MDC 0.0915 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.383 0.451 0.434 1.19 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.0624 0.156 0.106 1.10 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.0543 0.123 0.0641 0.816 Lead 212 TestAmerica St. Louis Page 15 of 19 1

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Client Sample Results TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3234-12 Client Sample ID: L100811BRS00 Matrix: Solid Date Collected: 08/01/13 18:15 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.17 (2+/-)

0.154 (2+/-)

1 08/30/13 09:56 08/08/13 10:41 pCi/g 0.0758 RL MDC 0.0937 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.368 1.83 1.04 14.7 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 09:56 1

1.05 0.216 0.213 U

0.318 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.0624 1.00 0.156 0.106 1.10 Radium 226 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.0948 0.123 0.0915 0.808 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.801 0.644 0.630 1.28 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.151 0.103 0.103 U

0.0927 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 09:56 1

0.0856 0.0517 0.0516 U

0.0333 Americium 241 pCi/g 08/08/13 10:41 08/30/13 09:56 1

4.54 2.00 2.00 U

0.277 Protactinium 234m Lab Sample ID: 160-3234-13 Client Sample ID: L100812BES00 Matrix: Solid Date Collected: 08/01/13 18:09 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.995 (2+/-)

0.168 (2+/-)

1 08/30/13 09:55 08/08/13 10:41 pCi/g 0.0675 RL MDC 0.134 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 09:55 1

0.466 0.518 0.501 1.26 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 09:55 1

0.0874 0.165 0.127 1.02 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 09:55 1

0.0709 0.143 0.0789 0.925 Lead 212 pCi/g 08/08/13 10:41 08/30/13 09:55 1

0.0796 0.158 0.111 1.08 Lead 214 pCi/g 08/08/13 10:41 08/30/13 09:55 1

0.343 2.19 1.33 17.1 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 09:55 1

1.28 0.199 0.198 U

0.228 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 09:55 1

0.0874 1.00 0.165 0.127 1.02 Radium 226 pCi/g 08/08/13 10:41 08/30/13 09:55 1

0.0675 0.168 0.134 0.995 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 09:55 1

0.794 0.580 0.568 1.14 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 09:55 1

0.273 0.183 0.182 U

0.115 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 09:55 1

0.110 0.0656 0.0656 U

0.0194 Americium 241 pCi/g 08/08/13 10:41 08/30/13 09:55 1

5.66 3.23 3.23 U

1.12 Protactinium 234m Lab Sample ID: 160-3234-14 Client Sample ID: L100813BES00 Matrix: Solid Date Collected: 08/01/13 17:01 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.936 (2+/-)

0.167 (2+/-)

1 08/30/13 10:37 08/08/13 10:41 pCi/g 0.0985 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.377 0.459 0.440 1.27 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.0731 0.156 0.113 1.04 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.0603 0.135 0.0700 0.891 Lead 212 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.0652 0.143 0.0884 1.09 Lead 214 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.260 1.87 1.10 14.8 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 10:37 1

1.00 0.220 0.213 U

0.504 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.0731 1.00 0.156 0.113 1.04 Radium 226 TestAmerica St. Louis Page 16 of 19 1

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Client Sample Results TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3234-14 Client Sample ID: L100813BES00 Matrix: Solid Date Collected: 08/01/13 17:01 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 0.936 (2+/-)

0.167 (2+/-)

1 08/30/13 10:37 08/08/13 10:41 pCi/g 0.0985 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.712 0.523 0.511 1.05 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.218 0.132 0.131 U

0.106 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.0947 0.233 0.233 U

-0.00372 Americium 241 pCi/g 08/08/13 10:41 08/30/13 10:37 1

5.05 2.88 2.88 U

0.850 Protactinium 234m Lab Sample ID: 160-3234-15 Client Sample ID: L100814BRS00 Matrix: Solid Date Collected: 08/01/13 18:00 Date Received: 08/03/13 16:01 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.741 (2+/-)

0.141 (2+/-)

1 08/30/13 10:37 08/08/13 10:41 pCi/g 0.0890 RL MDC 0.119 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.371 0.416 0.405 0.900 Bismuth 212 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.0701 0.145 0.112 0.895 Bismuth 214 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.0571 0.104 0.0629 0.641 Lead 212 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.0606 0.130 0.0878 0.922 Lead 214 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.165 1.49 0.986 10.9 Potassium 40 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.672 0.412 0.411 U

0.350 Protactinium 231 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.0701 1.00 0.145 0.112 0.895 Radium 226 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.0890 0.141 0.119 0.741 Thorium 232 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.763 0.601 0.594 0.886 Thorium 234 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.236 0.144 0.143 U

0.110 Uranium 235 pCi/g 08/08/13 10:41 08/30/13 10:37 1

0.0899 0.0530 0.0530 U

0.00366 Americium 241 pCi/g 08/08/13 10:41 08/30/13 10:37 1

5.05 2.84 2.84 U

0.728 Protactinium 234m TestAmerica St. Louis Page 17 of 19 1

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QC Sample Results TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-65532/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70078 Prep Batch: 65532 Actinium 228 Analyte U

1 09/02/13 23:30 08/08/13 10:41 pCi/g 0.0719 MDC RL 0.0124 0.0124 (2+/-)

(2+/-)

MB 0.0000 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

09/02/13 23:30 08/08/13 10:41 pCi/g 0.279 0.0390 0.0390 U

0.0000 Bismuth 212 1

09/02/13 23:30 08/08/13 10:41 pCi/g 0.0386 0.0189 0.0189 U

0.005983 Bismuth 214 1

09/02/13 23:30 08/08/13 10:41 pCi/g 0.0292 0.0181 0.0181 U

-0.001503 Lead 212 1

09/02/13 23:30 08/08/13 10:41 pCi/g 0.0270 0.0207 0.0202 0.03985 Lead 214 1

09/02/13 23:30 08/08/13 10:41 pCi/g 0.434 3.32 3.32 U

-0.08289 Potassium 40 1

09/02/13 23:30 08/08/13 10:41 pCi/g 0.381 0.0990 0.0989 U

0.03928 Protactinium 231 1

09/02/13 23:30 08/08/13 10:41 pCi/g 0.0386 1.00 0.0189 0.0189 U

0.005983 Radium 226 1

09/02/13 23:30 08/08/13 10:41 pCi/g 0.0719 0.0124 0.0124 U

0.0000 Thorium 232 1

09/02/13 23:30 08/08/13 10:41 pCi/g 0.261 0.193 0.193 U

-0.03141 Thorium 234 1

09/02/13 23:30 08/08/13 10:41 pCi/g 0.0616 0.0386 0.0384 U

0.03595 Uranium 235 1

09/02/13 23:30 08/08/13 10:41 pCi/g 0.0203 0.0102 0.0102 U

0.002361 Americium 241 1

09/02/13 23:30 08/08/13 10:41 pCi/g 1.85 0.957 0.956 U

0.2854 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-65532/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70040 Prep Batch: 65532 Americium 241 Analyte 116 87 96 93.54 97.7 9.73 0.484 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 31.6 30.72 3.21 0.129 pCi/g 97 87 - 120 Cobalt 60 24.8 23.73 2.40 0.0715 pCi/g 96 87 - 115 Client Sample ID: L100801BRS00 Lab Sample ID: 160-3234-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 70078 Prep Batch: 65532 Actinium 228 Analyte 1

0.32 1.058 0.952 0.172 0.141 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.08 1.360 0.468 0.429 pCi/g 0.33 1

Bismuth 214 0.973 1.077 0.168 0.0835 pCi/g 0.34 1

Lead 212 0.999 1.020 0.152 0.0614 pCi/g 0.07 1

Lead 214 1.15 1.146 0.153 0.0899 pCi/g 0.01 1

Potassium 40 16.2 16.30 2.03 0.260 pCi/g 0.03 1

Protactinium 231 0.419 U

-0.5947 U F 0.773 1.27 pCi/g 1.02 1

Radium 226 0.973 1.077 0.168 1.00 0.0835 pCi/g 0.34 1

Thorium 232 0.952 1.058 0.172 0.141 pCi/g 0.32 1

Thorium 234 5.97 5.811 0.853 1.18 pCi/g 0.09 1

Uranium 235 1.55 1.797 0.291 0.239 pCi/g 0.41 1

Americium 241 0.0254 U

0.04114 U

0.0585 0.0970 pCi/g 0.12 1

Protactinium 234m 15.7 17.20 5.11 3.69 pCi/g 0.16 1

TestAmerica St. Louis Page 18 of 19 1

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QC Association Summary TestAmerica Job ID: 160-3234-2 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Rad Leach Batch: 64984 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3234-1 L100801BRS00 Total/NA Solid Dry and Grind 160-3234-1 DU L100801BRS00 Total/NA Solid Dry and Grind 160-3234-2 L100802BES00 Total/NA Solid Dry and Grind 160-3234-3 L100803BES00 Total/NA Solid Dry and Grind 160-3234-4 L100804BRS00 Total/NA Solid Dry and Grind 160-3234-5 L100805BES00 Total/NA Solid Dry and Grind 160-3234-6 L100806BES00 Total/NA Solid Dry and Grind 160-3234-7 L100807BRQ00 Total/NA Solid Dry and Grind 160-3234-8 L100807BRS00 Total/NA Solid Dry and Grind 160-3234-9 L100808BES00 Total/NA Solid Dry and Grind 160-3234-10 L100809BES00 Total/NA Solid Dry and Grind 160-3234-11 L100810BES00 Total/NA Solid Dry and Grind 160-3234-12 L100811BRS00 Total/NA Solid Dry and Grind 160-3234-13 L100812BES00 Total/NA Solid Dry and Grind 160-3234-14 L100813BES00 Total/NA Solid Dry and Grind 160-3234-15 L100814BRS00 Total/NA Prep Batch: 65532 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 64984 160-3234-1 L100801BRS00 Total/NA Solid Fill_Geo-21 64984 160-3234-1 DU L100801BRS00 Total/NA Solid Fill_Geo-21 64984 160-3234-2 L100802BES00 Total/NA Solid Fill_Geo-21 64984 160-3234-3 L100803BES00 Total/NA Solid Fill_Geo-21 64984 160-3234-4 L100804BRS00 Total/NA Solid Fill_Geo-21 64984 160-3234-5 L100805BES00 Total/NA Solid Fill_Geo-21 64984 160-3234-6 L100806BES00 Total/NA Solid Fill_Geo-21 64984 160-3234-7 L100807BRQ00 Total/NA Solid Fill_Geo-21 64984 160-3234-8 L100807BRS00 Total/NA Solid Fill_Geo-21 64984 160-3234-9 L100808BES00 Total/NA Solid Fill_Geo-21 64984 160-3234-10 L100809BES00 Total/NA Solid Fill_Geo-21 64984 160-3234-11 L100810BES00 Total/NA Solid Fill_Geo-21 64984 160-3234-12 L100811BRS00 Total/NA Solid Fill_Geo-21 64984 160-3234-13 L100812BES00 Total/NA Solid Fill_Geo-21 64984 160-3234-14 L100813BES00 Total/NA Solid Fill_Geo-21 64984 160-3234-15 L100814BRS00 Total/NA Solid Fill_Geo-21 LCS 160-65532/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-65532/1-A Method Blank Total/NA TestAmerica St. Louis Page 19 of 19 1

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