ML18010A298
| ML18010A298 | |
| Person / Time | |
|---|---|
| Site: | 07000036 (SNM-0033) |
| Issue date: | 08/13/2013 |
| From: | Swanson M Testamerica Labs, Westinghouse |
| To: | Office of Nuclear Material Safety and Safeguards |
| Shared Package | |
| ML18010A247 | List:
|
| References | |
| HEM-17-72 160-3234-1 | |
| Download: ML18010A298 (29) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3234-1 Client Project/Site: RFP-CBA-022 (7 DAY TAT)
Revision: 1 For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:
8/13/2013 5:15:07 PM Ivan Vania, Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-3234-1 Page 2 of 29 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
7 Definitions/Glossary.......................................
8 Method Summary.........................................
9 Sample Summary.........................................
10 Client Sample Results......................................
11 QC Sample Results........................................
23 QC Association Summary...................................
26 Tracer Carrier Summary....................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3234-1 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3234-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)
Report Number: 160-3234-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 08/03/2013; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 4 coolers at receipt time were 0.8º C, 2.2º C, 23.7º C and 25.1º C. Several of the samples were received on ice with a temperature of <
2C. For this job, there are only rad analyses requested. Samples for rad analysis do not require cold preservation.
TECHNETIUM-99 (ICPMS)
Samples L100801BRS00 (160-3234-1), L100802BES00 (160-3234-2), L100803BES00 (160-3234-3), L100804BRS00 (160-3234-4),
L100805BES00 (160-3234-5), L100806BES00 (160-3234-6), L100807BRQ00 (160-3234-7), L100807BRS00 (160-3234-8),
L100808BES00 (160-3234-9), L100809BES00 (160-3234-10), L100810BES00 (160-3234-11), L100811BRS00 (160-3234-12),
L100812BES00 (160-3234-13), L100813BES00 (160-3234-14) and L100814BRS00 (160-3234-15) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 08/07/2013 and analyzed on 08/09/2013.
No difficulties were encountered during the Tc-99 analysis. All quality control parameters were within the acceptance limits.
PERCENT SOLIDS TestAmerica St. Louis Page 3 of 29 1
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3234-1 Project/Site: RFP-CBA-022 (7 DAY TAT)
Job ID: 160-3234-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
Samples L100801BRS00 (160-3234-1), L100802BES00 (160-3234-2), L100803BES00 (160-3234-3), L100804BRS00 (160-3234-4),
L100805BES00 (160-3234-5), L100806BES00 (160-3234-6), L100807BRQ00 (160-3234-7), L100807BRS00 (160-3234-8),
L100808BES00 (160-3234-9), L100809BES00 (160-3234-10), L100810BES00 (160-3234-11), L100811BRS00 (160-3234-12),
L100812BES00 (160-3234-13), L100813BES00 (160-3234-14) and L100814BRS00 (160-3234-15) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 08/05/2013.
No difficulties were encountered during the % solids analysis. All quality control parameters were within the acceptance limits.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L100801BRS00 (160-3234-1), L100802BES00 (160-3234-2), L100803BES00 (160-3234-3), L100804BRS00 (160-3234-4),
L100805BES00 (160-3234-5), L100806BES00 (160-3234-6), L100807BRQ00 (160-3234-7), L100807BRS00 (160-3234-8),
L100808BES00 (160-3234-9), L100809BES00 (160-3234-10), L100810BES00 (160-3234-11), L100811BRS00 (160-3234-12),
L100812BES00 (160-3234-13), L100813BES00 (160-3234-14) and L100814BRS00 (160-3234-15) were analyzed for Cesium-137 &
Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 08/06/2013, prepared on 08/08/2013 and analyzed on 08/08/2013, 08/09/2013 and 08/12/2013.
Preparation Batch 65524:
Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of Bismuth-214.
Because the samples have not had a 21-day ingrowth, the activity for Radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between Radium-226 and Bismuth-214 by the loss of Radon-222 during sample preparation.
Lead-214 analyzed by gamma spectroscopy was detected above the MDC in the method blank. Variations in Compton backgrounds and statistical analyses allow for small area counts in the ROIs of this nuclide. Other Uranium decay chain products are not present in the blank to support Lead-214 identification. The data is reported. (160-3234-1 DU), (LCS 160-65524/2-A), (MB 160-65524/1-A),
L100801BRS00 (160-3234-1), L100802BES00 (160-3234-2), L100803BES00 (160-3234-3), L100804BRS00 (160-3234-4),
L100805BES00 (160-3234-5), L100806BES00 (160-3234-6), L100807BRQ00 (160-3234-7), L100807BRS00 (160-3234-8),
L100808BES00 (160-3234-9), L100809BES00 (160-3234-10), L100810BES00 (160-3234-11), L100811BRS00 (160-3234-12),
L100812BES00 (160-3234-13), L100813BES00 (160-3234-14), L100814BRS00 (160-3234-15)
No other difficulties were encountered during the Gamma spec analysis. All other quality control parameters were within the acceptance limits.
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10 11 12 Procedure HDP0 PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 3 l
Page 1 oflj Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HOP.
Chain of Cutody ID No. I F-080213-02 Pae:e Project Name:
Westinghouse Electric Company Contact Person:
Gerald Rood Phone Number:
314-810-3382 Sampler Name Scott Jenkins Sample ID Date Time 1/2
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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 1
Page l of 1 Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutody ID No. I F-080213-02 Pa!!e 2/2
. -. *. :R, ~ ested AnalySi} ': ;*< :
- Laboratorv Name:
Project Name:
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Laboratory Address:
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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3234-1 Login Number: 3234 Question Answer Comment Creator: Vania, Ivan H List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
True Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
True Samples were received on ice.
Where requried True Cooler Temperature is acceptable.
See NCM True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
True Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Qualifiers Metals Qualifier Description J
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier Rad Qualifier Description U
Indicates the analyte was analyzed for but not detected.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 29 1
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Sample Summary TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-3234-1 L100801BRS00 Solid 08/01/13 15:14 08/03/13 16:01 160-3234-2 L100802BES00 Solid 08/01/13 15:23 08/03/13 16:01 160-3234-3 L100803BES00 Solid 08/01/13 15:54 08/03/13 16:01 160-3234-4 L100804BRS00 Solid 08/01/13 16:02 08/03/13 16:01 160-3234-5 L100805BES00 Solid 08/01/13 16:08 08/03/13 16:01 160-3234-6 L100806BES00 Solid 08/01/13 16:16 08/03/13 16:01 160-3234-7 L100807BRQ00 Solid 08/01/13 17:40 08/03/13 16:01 160-3234-8 L100807BRS00 Solid 08/01/13 17:40 08/03/13 16:01 160-3234-9 L100808BES00 Solid 08/01/13 17:45 08/03/13 16:01 160-3234-10 L100809BES00 Solid 08/01/13 16:35 08/03/13 16:01 160-3234-11 L100810BES00 Solid 08/01/13 16:48 08/03/13 16:01 160-3234-12 L100811BRS00 Solid 08/01/13 18:15 08/03/13 16:01 160-3234-13 L100812BES00 Solid 08/01/13 18:09 08/03/13 16:01 160-3234-14 L100813BES00 Solid 08/01/13 17:01 08/03/13 16:01 160-3234-15 L100814BRS00 Solid 08/01/13 18:00 08/03/13 16:01 TestAmerica St. Louis Page 10 of 29 1
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-1 Client Sample ID: L100801BRS00 Matrix: Solid Date Collected: 08/01/13 15:14 Percent Solids: 83.7 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000035 J
0.00065 0.000020 mg/Kg
08/07/13 10:55 08/09/13 20:54 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.591 (2+/-)
0.0648 (2+/-)
1 08/09/13 20:54 08/07/13 10:55 pCi/g 0.223 1.30 RL MDC 0.0244 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 20:54 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.856 (2+/-)
0.162 (2+/-)
1 08/12/13 21:23 08/08/13 09:35 pCi/g 0.125 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/12/13 21:23 1
0.124 0.0743 0.0743 U
0.0267 Americium 241 pCi/g 08/08/13 09:35 08/12/13 21:23 1
0.398 0.455 0.435 1.28 Bismuth 212 pCi/g 08/08/13 09:35 08/12/13 21:23 1
0.0692 0.129 0.0961 0.829 Bismuth 214 pCi/g 08/08/13 09:35 08/12/13 21:23 1
0.0550 0.145 0.0655 0.998 Lead 212 pCi/g 08/08/13 09:35 08/12/13 21:23 1
0.0613 0.128 0.0831 0.932 Lead 214 pCi/g 08/08/13 09:35 08/12/13 21:23 1
0.294 1.86 1.03 15.2 Potassium 40 pCi/g 08/08/13 09:35 08/12/13 21:23 1
1.18 0.717 0.715 U
-0.555 Protactinium 231 pCi/g 08/08/13 09:35 08/12/13 21:23 1
0.0692 1.00 0.129 0.0961 0.829 Radium 226 pCi/g 08/08/13 09:35 08/12/13 21:23 1
0.927 1.00 0.756 0.464 5.71 Thorium 234 pCi/g 08/08/13 09:35 08/12/13 21:23 1
0.221 0.252 0.191 1.60 Uranium 235 pCi/g 08/08/13 09:35 08/12/13 21:23 1
3.99 4.54 4.41 10.5 Protactinium 234m pCi/g 08/08/13 09:35 08/12/13 21:23 1
0.125 0.162 0.137 0.856 Thorium 232 Tl-208 0.285 0.0417 0.0511 0.0341 pCi/g 08/08/13 09:35 08/12/13 21:23 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3234-2 Client Sample ID: L100802BES00 Matrix: Solid Date Collected: 08/01/13 15:23 Percent Solids: 82.8 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00066 0.000020 mg/Kg
08/07/13 10:55 08/09/13 21:06 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.295 (2+/-)
0.0584 (2+/-)
1 08/09/13 21:06 08/07/13 10:55 pCi/g 0.226 1.32 RL MDC 0.0459 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:06 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 TestAmerica St. Louis Page 11 of 29 1
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-2 Client Sample ID: L100802BES00 Matrix: Solid Date Collected: 08/01/13 15:23 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.07 (2+/-)
0.203 (2+/-)
1 08/08/13 20:21 08/08/13 09:35 pCi/g 0.155 RL MDC 0.171 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 20:21 1
0.118 0.0702 0.0702 U
-0.0177 Americium 241 pCi/g 08/08/13 09:35 08/08/13 20:21 1
0.349 0.523 0.488 1.82 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 20:21 1
0.0753 0.153 0.121 0.889 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 20:21 1
0.0743 0.159 0.0865 1.03 Lead 212 pCi/g 08/08/13 09:35 08/08/13 20:21 1
0.0819 0.134 0.107 0.782 Lead 214 pCi/g 08/08/13 09:35 08/08/13 20:21 1
0.339 2.29 1.41 17.6 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 20:21 1
1.61 0.980 0.976 U
-0.735 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 20:21 1
0.0753 1.00 0.153 0.121 0.889 Radium 226 pCi/g 08/08/13 09:35 08/08/13 20:21 1
0.891 1.00 0.674 0.657 1.42 Thorium 234 pCi/g 08/08/13 09:35 08/08/13 20:21 1
0.250 0.169 0.167 0.279 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 20:21 1
7.81 4.72 4.71 U
1.69 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 20:21 1
0.155 0.203 0.171 1.07 Thorium 232 Tl-208 0.338 0.0503 0.0613 0.0310 pCi/g 08/08/13 09:35 08/08/13 20:21 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3234-3 Client Sample ID: L100803BES00 Matrix: Solid Date Collected: 08/01/13 15:54 Percent Solids: 81.8 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00064 0.000019 mg/Kg
08/07/13 10:55 08/09/13 21:10 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.255 (2+/-)
0.0611 (2+/-)
1 08/09/13 21:10 08/07/13 10:55 pCi/g 0.220 1.29 RL MDC 0.0525 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:10 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 94 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.976 (2+/-)
0.153 (2+/-)
1 08/08/13 20:23 08/08/13 09:35 pCi/g 0.0887 RL MDC 0.116 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 20:23 1
0.107 0.0633 0.0633 U
0.00230 Americium 241 pCi/g 08/08/13 09:35 08/08/13 20:23 1
0.278 0.326 0.309 0.993 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 20:23 1
0.0533 0.109 0.0795 0.712 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 20:23 1
0.0533 0.150 0.0677 1.04 Lead 212 pCi/g 08/08/13 09:35 08/08/13 20:23 1
0.0590 0.111 0.0733 0.797 Lead 214 pCi/g 08/08/13 09:35 08/08/13 20:23 1
0.270 2.13 1.05 18.1 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 20:23 1
1.06 0.226 0.221 U
0.403 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 20:23 1
0.0533 1.00 0.109 0.0795 0.712 Radium 226 TestAmerica St. Louis Page 12 of 29 1
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-3 Client Sample ID: L100803BES00 Matrix: Solid Date Collected: 08/01/13 15:54 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 2.32 (2+/-)
0.696 (2+/-)
1 08/08/13 20:23 08/08/13 09:35 pCi/g 0.792 1.00 RL MDC 0.652 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 20:23 1
0.162 0.153 0.148 0.391 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 20:23 1
7.14 2.98 2.98 U
0.000 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 20:23 1
0.0887 0.153 0.116 0.976 Thorium 232 Tl-208 0.328 0.0436 0.0553 0.0316 pCi/g 08/08/13 09:35 08/08/13 20:23 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3234-4 Client Sample ID: L100804BRS00 Matrix: Solid Date Collected: 08/01/13 16:02 Percent Solids: 84.1 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00065 0.000020 mg/Kg
08/07/13 10:55 08/09/13 21:14 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.168 U
(2+/-)
0.0749 (2+/-)
1 08/09/13 21:14 08/07/13 10:55 pCi/g 0.224 1.31 RL MDC 0.0663 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:14 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.741 (2+/-)
0.138 (2+/-)
1 08/08/13 20:24 08/08/13 09:35 pCi/g 0.0897 RL MDC 0.115 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 20:24 1
0.0922 0.0553 0.0553 U
0.0223 Americium 241 pCi/g 08/08/13 09:35 08/08/13 20:24 1
0.300 0.386 0.364 1.24 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 20:24 1
0.0574 0.106 0.0810 0.662 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 20:24 1
0.0697 0.121 0.0651 0.791 Lead 212 pCi/g 08/08/13 09:35 08/08/13 20:24 1
0.0624 0.113 0.0831 0.734 Lead 214 pCi/g 08/08/13 09:35 08/08/13 20:24 1
0.266 1.91 0.970 16.0 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 20:24 1
0.997 0.216 0.213 U
0.363 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 20:24 1
0.0574 1.00 0.106 0.0810 0.662 Radium 226 pCi/g 08/08/13 09:35 08/08/13 20:24 1
0.732 1.00 0.622 0.602 1.52 Thorium 234 pCi/g 08/08/13 09:35 08/08/13 20:24 1
0.222 0.124 0.124 U
0.106 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 20:24 1
4.18 2.30 2.29 U
1.52 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 20:24 1
0.0897 0.138 0.115 0.741 Thorium 232 Tl-208 0.239 0.0434 0.0500 0.0374 pCi/g 08/08/13 09:35 08/08/13 20:24 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 13 of 29 1
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-5 Client Sample ID: L100805BES00 Matrix: Solid Date Collected: 08/01/13 16:08 Percent Solids: 81.6 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00067 0.000020 mg/Kg
08/07/13 10:55 08/09/13 21:25 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.278 (2+/-)
0.0713 (2+/-)
1 08/09/13 21:25 08/07/13 10:55 pCi/g 0.231 1.35 RL MDC 0.0592 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:25 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.863 (2+/-)
0.139 (2+/-)
1 08/08/13 20:25 08/08/13 09:35 pCi/g 0.103 RL MDC 0.107 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 20:25 1
0.0888 0.0530 0.0530 U
0.0237 Americium 241 pCi/g 08/08/13 09:35 08/08/13 20:25 1
0.242 0.323 0.304 1.07 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 20:25 1
0.0593 0.112 0.0869 0.683 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 20:25 1
0.0542 0.134 0.0670 0.896 Lead 212 pCi/g 08/08/13 09:35 08/08/13 20:25 1
0.0674 0.110 0.0829 0.690 Lead 214 pCi/g 08/08/13 09:35 08/08/13 20:25 1
0.298 2.03 1.14 16.5 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 20:25 1
0.748 0.478 0.460 1.19 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 20:25 1
0.0593 1.00 0.112 0.0869 0.683 Radium 226 pCi/g 08/08/13 09:35 08/08/13 20:25 1
0.738 1.00 0.300 0.288 0.793 Thorium 234 pCi/g 08/08/13 09:35 08/08/13 20:25 1
0.222 0.133 0.133 U
0.109 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 20:25 1
5.00 2.83 2.83 U
0.629 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 20:25 1
0.103 0.139 0.107 0.863 Thorium 232 Tl-208 0.321 0.0454 0.0563 0.0309 pCi/g 08/08/13 09:35 08/08/13 20:25 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3234-6 Client Sample ID: L100806BES00 Matrix: Solid Date Collected: 08/01/13 16:16 Percent Solids: 86.4 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00065 0.000019 mg/Kg
08/07/13 10:55 08/09/13 21:29 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.188 U
(2+/-)
0.132 (2+/-)
1 08/09/13 21:29 08/07/13 10:55 pCi/g 0.221 1.29 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:29 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 TestAmerica St. Louis Page 14 of 29 1
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-6 Client Sample ID: L100806BES00 Matrix: Solid Date Collected: 08/01/13 16:16 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.814 (2+/-)
0.146 (2+/-)
1 08/08/13 20:26 08/08/13 09:35 pCi/g 0.0686 RL MDC 0.120 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 20:26 1
0.0816 0.0479 0.0479 U
-0.000761 Americium 241 pCi/g 08/08/13 09:35 08/08/13 20:26 1
0.337 0.338 0.329 0.729 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 20:26 1
0.0596 0.109 0.0879 0.623 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 20:26 1
0.0542 0.126 0.0682 0.823 Lead 212 pCi/g 08/08/13 09:35 08/08/13 20:26 1
0.0816 0.0987 0.0766 0.599 Lead 214 pCi/g 08/08/13 09:35 08/08/13 20:26 1
0.163 1.81 1.11 14.0 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 20:26 1
1.12 0.264 0.259 U
0.450 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 20:26 1
0.0596 1.00 0.109 0.0879 0.623 Radium 226 pCi/g 08/08/13 09:35 08/08/13 20:26 1
0.784 1.00 0.316 0.304 0.835 Thorium 234 pCi/g 08/08/13 09:35 08/08/13 20:26 1
0.236 0.140 0.140 U
0.138 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 20:26 1
5.78 3.19 3.19 U
-0.0317 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 20:26 1
0.0686 0.146 0.120 0.814 Thorium 232 Tl-208 0.269 0.0442 0.0523 0.0319 pCi/g 08/08/13 09:35 08/08/13 20:26 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3234-7 Client Sample ID: L100807BRQ00 Matrix: Solid Date Collected: 08/01/13 17:40 Percent Solids: 80.5 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00069 0.000021 mg/Kg
08/07/13 10:55 08/09/13 21:33 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.276 (2+/-)
0.0375 (2+/-)
1 08/09/13 21:33 08/07/13 10:55 pCi/g 0.237 1.38 RL MDC 0.0225 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:33 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.772 (2+/-)
0.127 (2+/-)
1 08/08/13 20:27 08/08/13 09:35 pCi/g 0.0477 RL MDC 0.0993 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 20:27 1
0.0800 0.0260 0.0260 U
0.000 Americium 241 pCi/g 08/08/13 09:35 08/08/13 20:27 1
0.265 0.332 0.312 1.08 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 20:27 1
0.0565 0.101 0.0790 0.605 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 20:27 1
0.0476 0.125 0.0605 0.842 Lead 212 pCi/g 08/08/13 09:35 08/08/13 20:27 1
0.0516 0.104 0.0742 0.703 Lead 214 pCi/g 08/08/13 09:35 08/08/13 20:27 1
0.286 1.63 0.918 13.2 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 20:27 1
0.853 0.291 0.288 U
0.416 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 20:27 1
0.0565 1.00 0.101 0.0790 0.605 Radium 226 TestAmerica St. Louis Page 15 of 29 1
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-7 Client Sample ID: L100807BRQ00 Matrix: Solid Date Collected: 08/01/13 17:40 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 1.14 (2+/-)
0.597 (2+/-)
1 08/08/13 20:27 08/08/13 09:35 pCi/g 0.745 1.00 RL MDC 0.585 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 20:27 1
0.193 0.0896 0.0895 U
0.0427 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 20:27 1
4.35 2.68 2.66 U
3.54 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 20:27 1
0.0477 0.127 0.0993 0.772 Thorium 232 Tl-208 0.293 0.0345 0.0460 0.0170 pCi/g 08/08/13 09:35 08/08/13 20:27 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3234-8 Client Sample ID: L100807BRS00 Matrix: Solid Date Collected: 08/01/13 17:40 Percent Solids: 74.6 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00074 0.000022 mg/Kg
08/07/13 10:55 08/09/13 21:37 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.194 U
(2+/-)
0.136 (2+/-)
1 08/09/13 21:37 08/07/13 10:55 pCi/g 0.252 1.47 RL MDC 0.121 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:37 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.764 (2+/-)
0.118 (2+/-)
1 08/08/13 21:22 08/08/13 09:35 pCi/g 0.0793 RL MDC 0.0884 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 21:22 1
0.0804 0.0481 0.0480 U
0.0157 Americium 241 pCi/g 08/08/13 09:35 08/08/13 21:22 1
0.163 0.245 0.225 0.937 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 21:22 1
0.0487 0.0926 0.0709 0.573 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 21:22 1
0.0451 0.106 0.0528 0.713 Lead 212 pCi/g 08/08/13 09:35 08/08/13 21:22 1
0.0541 0.0929 0.0692 0.596 Lead 214 pCi/g 08/08/13 09:35 08/08/13 21:22 1
0.229 1.57 0.824 13.0 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 21:22 1
0.842 0.147 0.145 U
0.246 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 21:22 1
0.0487 1.00 0.0926 0.0709 0.573 Radium 226 pCi/g 08/08/13 09:35 08/08/13 21:22 1
0.623 1.00 0.468 0.462 0.717 Thorium 234 pCi/g 08/08/13 09:35 08/08/13 21:22 1
0.152 0.125 0.124 0.155 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 21:22 1
3.41 2.21 2.21 U
0.731 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 21:22 1
0.0793 0.118 0.0884 0.764 Thorium 232 Tl-208 0.258 0.0326 0.0422 0.0223 pCi/g 08/08/13 09:35 08/08/13 21:22 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-9 Client Sample ID: L100808BES00 Matrix: Solid Date Collected: 08/01/13 17:45 Percent Solids: 78.0 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00070 0.000021 mg/Kg
08/07/13 10:55 08/09/13 21:41 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0296 U
(2+/-)
0.0865 (2+/-)
1 08/09/13 21:41 08/07/13 10:55 pCi/g 0.241 1.41 RL MDC 0.0793 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:41 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.04 (2+/-)
0.171 (2+/-)
1 08/08/13 22:11 08/08/13 09:35 pCi/g 0.111 RL MDC 0.134 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.115 0.0681 0.0681 U
0.00444 Americium 241 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.564 0.379 0.374 0.589 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.0616 0.131 0.104 0.775 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.0683 0.158 0.0809 1.05 Lead 212 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.0839 0.118 0.0873 0.765 Lead 214 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.293 2.28 1.33 18.1 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 22:11 1
1.31 0.259 0.254 U
0.451 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.0616 1.00 0.131 0.104 0.775 Radium 226 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.878 1.00 0.341 0.331 U
0.795 Thorium 234 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.276 0.100 0.100 U
0.0326 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 22:11 1
5.28 3.12 3.12 U
1.84 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.111 0.171 0.134 1.04 Thorium 232 Tl-208 0.300 0.0571 0.0650 0.0449 pCi/g 08/08/13 09:35 08/08/13 22:11 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3234-10 Client Sample ID: L100809BES00 Matrix: Solid Date Collected: 08/01/13 16:35 Percent Solids: 88.6 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000041 J
0.00064 0.000019 mg/Kg
08/07/13 10:55 08/09/13 21:45 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.695 (2+/-)
0.166 (2+/-)
1 08/09/13 21:45 08/07/13 10:55 pCi/g 0.218 1.27 RL MDC 0.133 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:45 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 TestAmerica St. Louis Page 17 of 29 1
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-10 Client Sample ID: L100809BES00 Matrix: Solid Date Collected: 08/01/13 16:35 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.911 (2+/-)
0.135 (2+/-)
1 08/08/13 22:08 08/08/13 09:35 pCi/g 0.102 RL MDC 0.0981 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 22:08 1
0.0702 0.0420 0.0420 U
0.0190 Americium 241 pCi/g 08/08/13 09:35 08/08/13 22:08 1
0.269 0.315 0.298 0.972 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 22:08 1
0.0576 0.109 0.0837 0.666 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 22:08 1
0.0487 0.123 0.0604 0.829 Lead 212 pCi/g 08/08/13 09:35 08/08/13 22:08 1
0.0586 0.0963 0.0673 0.662 Lead 214 pCi/g 08/08/13 09:35 08/08/13 22:08 1
0.318 1.80 0.965 14.8 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 22:08 1
0.893 0.284 0.281 U
0.356 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 22:08 1
0.0576 1.00 0.109 0.0837 0.666 Radium 226 pCi/g 08/08/13 09:35 08/08/13 22:08 1
0.782 1.00 0.666 0.649 1.42 Thorium 234 pCi/g 08/08/13 09:35 08/08/13 22:08 1
0.154 0.103 0.101 0.195 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 22:08 1
4.52 2.82 2.80 U
2.78 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 22:08 1
0.102 0.135 0.0981 0.911 Thorium 232 Tl-208 0.250 0.0353 0.0438 0.0260 pCi/g 08/08/13 09:35 08/08/13 22:08 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3234-11 Client Sample ID: L100810BES00 Matrix: Solid Date Collected: 08/01/13 16:48 Percent Solids: 86.4 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00063 0.000019 mg/Kg
08/07/13 10:55 08/09/13 21:48 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.266 (2+/-)
0.0909 (2+/-)
1 08/09/13 21:48 08/07/13 10:55 pCi/g 0.215 1.25 RL MDC 0.0798 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:48 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.780 (2+/-)
0.133 (2+/-)
1 08/08/13 22:09 08/08/13 09:35 pCi/g 0.0851 RL MDC 0.107 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 22:09 1
0.0800 0.0473 0.0473 U
-0.000887 Americium 241 pCi/g 08/08/13 09:35 08/08/13 22:09 1
0.365 0.406 0.397 0.788 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 22:09 1
0.0771 0.0824 0.0673 0.457 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 22:09 1
0.0645 0.105 0.0592 0.675 Lead 212 pCi/g 08/08/13 09:35 08/08/13 22:09 1
0.0601 0.0910 0.0712 0.545 Lead 214 pCi/g 08/08/13 09:35 08/08/13 22:09 1
0.250 1.56 0.847 12.8 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 22:09 1
0.724 0.181 0.181 U
0.0973 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 22:09 1
0.0771 1.00 0.0824 0.0673 0.457 Radium 226 TestAmerica St. Louis Page 18 of 29 1
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-11 Client Sample ID: L100810BES00 Matrix: Solid Date Collected: 08/01/13 16:48 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 1.34 (2+/-)
0.585 (2+/-)
1 08/08/13 22:09 08/08/13 09:35 pCi/g 0.710 1.00 RL MDC 0.568 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 22:09 1
0.161 0.0469 0.0468 U
0.0268 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 22:09 1
2.48 2.66 2.61 5.02 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 22:09 1
0.0851 0.133 0.107 0.780 Thorium 232 Tl-208 0.243 0.0355 0.0435 0.0266 pCi/g 08/08/13 09:35 08/08/13 22:09 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3234-12 Client Sample ID: L100811BRS00 Matrix: Solid Date Collected: 08/01/13 18:15 Percent Solids: 83.5 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00065 0.000020 mg/Kg
08/07/13 10:55 08/09/13 21:52 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0301 U
(2+/-)
0.0738 (2+/-)
1 08/09/13 21:52 08/07/13 10:55 pCi/g 0.223 1.30 RL MDC 0.0676 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:52 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.796 (2+/-)
0.155 (2+/-)
1 08/08/13 22:11 08/08/13 09:35 pCi/g 0.122 RL MDC 0.132 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.0793 0.0478 0.0477 U
0.0352 Americium 241 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.426 0.466 0.454 1.03 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.0707 0.123 0.0992 0.705 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.0571 0.129 0.0697 0.837 Lead 212 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.0660 0.117 0.0806 0.820 Lead 214 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.306 1.77 1.12 13.4 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 22:11 1
1.01 0.304 0.300 U
0.418 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.0707 1.00 0.123 0.0992 0.705 Radium 226 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.808 1.00 0.278 0.270 U
0.657 Thorium 234 pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.230 0.134 0.134 U
-0.00434 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 22:11 1
5.34 3.06 3.05 U
1.04 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 22:11 1
0.122 0.155 0.132 0.796 Thorium 232 Tl-208 0.277 0.0473 0.0554 0.0353 pCi/g 08/08/13 09:35 08/08/13 22:11 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 19 of 29 1
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-13 Client Sample ID: L100812BES00 Matrix: Solid Date Collected: 08/01/13 18:09 Percent Solids: 76.6 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00072 0.000022 mg/Kg
08/07/13 10:55 08/09/13 21:56 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.0372 U
(2+/-)
0.0754 (2+/-)
1 08/09/13 21:56 08/07/13 10:55 pCi/g 0.246 1.44 RL MDC 0.0681 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 21:56 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.01 (2+/-)
0.157 (2+/-)
1 08/09/13 10:03 08/08/13 09:35 pCi/g 0.0742 RL MDC 0.119 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/09/13 10:03 1
0.0911 0.0541 0.0541 U
0.00986 Americium 241 pCi/g 08/08/13 09:35 08/09/13 10:03 1
0.418 0.292 0.286 0.554 Bismuth 212 pCi/g 08/08/13 09:35 08/09/13 10:03 1
0.0626 0.114 0.0877 0.709 Bismuth 214 pCi/g 08/08/13 09:35 08/09/13 10:03 1
0.0501 0.144 0.0667 0.989 Lead 212 pCi/g 08/08/13 09:35 08/09/13 10:03 1
0.0795 0.121 0.0846 0.834 Lead 214 pCi/g 08/08/13 09:35 08/09/13 10:03 1
0.333 1.88 1.01 15.5 Potassium 40 pCi/g 08/08/13 09:35 08/09/13 10:03 1
0.845 0.210 0.206 U
0.406 Protactinium 231 pCi/g 08/08/13 09:35 08/09/13 10:03 1
0.0626 1.00 0.114 0.0877 0.709 Radium 226 pCi/g 08/08/13 09:35 08/09/13 10:03 1
0.662 1.00 0.444 0.428 1.15 Thorium 234 pCi/g 08/08/13 09:35 08/09/13 10:03 1
0.216 0.132 0.132 U
0.121 Uranium 235 pCi/g 08/08/13 09:35 08/09/13 10:03 1
4.69 2.70 2.69 U
0.663 Protactinium 234m pCi/g 08/08/13 09:35 08/09/13 10:03 1
0.0742 0.157 0.119 1.01 Thorium 232 Tl-208 0.302 0.0422 0.0526 0.0315 pCi/g 08/08/13 09:35 08/09/13 10:03 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3234-14 Client Sample ID: L100813BES00 Matrix: Solid Date Collected: 08/01/13 17:01 Percent Solids: 86.8 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00064 0.000019 mg/Kg
08/07/13 10:55 08/09/13 22:00 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.250 (2+/-)
0.0601 (2+/-)
1 08/09/13 22:00 08/07/13 10:55 pCi/g 0.217 1.27 RL MDC 0.0490 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 22:00 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 TestAmerica St. Louis Page 20 of 29 1
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-14 Client Sample ID: L100813BES00 Matrix: Solid Date Collected: 08/01/13 17:01 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.883 (2+/-)
0.165 (2+/-)
1 08/08/13 22:43 08/08/13 09:35 pCi/g 0.0968 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 22:43 1
0.100 0.0589 0.0589 U
-0.00274 Americium 241 pCi/g 08/08/13 09:35 08/08/13 22:43 1
0.233 0.400 0.372 1.41 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 22:43 1
0.0465 0.109 0.0882 0.613 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 22:43 1
0.0657 0.122 0.0722 0.760 Lead 212 pCi/g 08/08/13 09:35 08/08/13 22:43 1
0.0724 0.107 0.0874 0.598 Lead 214 pCi/g 08/08/13 09:35 08/08/13 22:43 1
0.310 1.86 1.20 13.9 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 22:43 1
1.28 0.778 0.776 U
-0.592 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 22:43 1
0.0465 1.00 0.109 0.0882 0.613 Radium 226 pCi/g 08/08/13 09:35 08/08/13 22:43 1
0.877 1.00 0.667 0.661 U
0.846 Thorium 234 pCi/g 08/08/13 09:35 08/08/13 22:43 1
0.227 0.0551 0.0551 U
0.00379 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 22:43 1
6.17 3.37 3.37 U
-0.0531 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 22:43 1
0.0968 0.165 0.138 0.883 Thorium 232 Tl-208 0.317 0.0506 0.0604 0.0329 pCi/g 08/08/13 09:35 08/08/13 22:43 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-3234-15 Client Sample ID: L100814BRS00 Matrix: Solid Date Collected: 08/01/13 18:00 Percent Solids: 90.1 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000026 J
0.00064 0.000019 mg/Kg
08/07/13 10:55 08/09/13 22:12 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.444 (2+/-)
0.0949 (2+/-)
1 08/09/13 22:12 08/07/13 10:55 pCi/g 0.218 1.28 RL MDC 0.0721 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 08/07/13 10:55 08/09/13 22:12 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.658 (2+/-)
0.106 (2+/-)
1 08/08/13 22:44 08/08/13 09:35 pCi/g 0.0829 RL MDC 0.0816 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 22:44 1
0.0806 0.0479 0.0479 U
0.00952 Americium 241 pCi/g 08/08/13 09:35 08/08/13 22:44 1
0.280 0.297 0.289 0.660 Bismuth 212 pCi/g 08/08/13 09:35 08/08/13 22:44 1
0.0491 0.0861 0.0666 0.526 Bismuth 214 pCi/g 08/08/13 09:35 08/08/13 22:44 1
0.0467 0.0995 0.0537 0.647 Lead 212 pCi/g 08/08/13 09:35 08/08/13 22:44 1
0.0584 0.0976 0.0752 0.599 Lead 214 pCi/g 08/08/13 09:35 08/08/13 22:44 1
0.340 1.37 0.823 10.7 Potassium 40 pCi/g 08/08/13 09:35 08/08/13 22:44 1
0.827 0.311 0.309 U
0.383 Protactinium 231 pCi/g 08/08/13 09:35 08/08/13 22:44 1
0.0491 1.00 0.0861 0.0666 0.526 Radium 226 TestAmerica St. Louis Page 21 of 29 1
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Client Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-3234-15 Client Sample ID: L100814BRS00 Matrix: Solid Date Collected: 08/01/13 18:00 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 0.947 (2+/-)
0.579 (2+/-)
1 08/08/13 22:44 08/08/13 09:35 pCi/g 0.713 1.00 RL MDC 0.570 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 08/08/13 09:35 08/08/13 22:44 1
0.182 0.110 0.110 U
0.0719 Uranium 235 pCi/g 08/08/13 09:35 08/08/13 22:44 1
3.86 2.26 2.26 U
1.11 Protactinium 234m pCi/g 08/08/13 09:35 08/08/13 22:44 1
0.0829 0.106 0.0816 0.658 Thorium 232 Tl-208 0.203 0.0303 0.0369 0.0221 pCi/g 08/08/13 09:35 08/08/13 22:44 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 22 of 29 1
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QC Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-65318/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 65972 Prep Batch: 65318 RL MDL Technetium 99 ND 0.00055 0.000017 mg/Kg 08/07/13 10:55 08/09/13 20:46 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-65318/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 65972 Prep Batch: 65318 Technetium 99 0.00251 0.00240 mg/Kg 95 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: L100801BRS00 Lab Sample ID: 160-3234-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 65972 Prep Batch: 65318 Technetium 99 0.000035 J
0.00306 0.00282 mg/Kg 91 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: L100801BRS00 Lab Sample ID: 160-3234-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 65972 Prep Batch: 65318 Technetium 99 0.000035 J
0.00300 0.00285 mg/Kg 94 75 - 125 1
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-65318/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 65973 Prep Batch: 65318 Technetium 99 Analyte U
1 08/09/13 20:46 08/07/13 10:55 pCi/g 0.188 MDC 1.10 RL 0.0662 0.0602 (2+/-)
(2+/-)
MB 0.002262 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 08/07/13 10:55 08/09/13 20:46 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 91 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-65318/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 65973 Prep Batch: 65318 Technetium 99 Analyte 120 80 95 41.01 43.0 4.09 1.07 0.184 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 93 LCS TestAmerica St. Louis Page 23 of 29 1
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QC Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: L100801BRS00 Lab Sample ID: 160-3234-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 65973 Prep Batch: 65318 Technetium 99 Analyte 125 75 91 48.26 52.4 0.591 4.86 1.31 0.224 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 91 MS Client Sample ID: L100801BRS00 Lab Sample ID: 160-3234-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 65973 Prep Batch: 65318 Technetium 99 Analyte 1
0.06 125 75 94 48.84 51.4 0.591 5.19 1.29 0.220 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 94 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-65524/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 65949 Prep Batch: 65524 Actinium 228 Analyte U
1 08/09/13 07:07 08/08/13 09:35 pCi/g 0.128 MDC RL 0.0212 0.0212 (2+/-)
(2+/-)
MB 0.01002 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
08/09/13 07:07 08/08/13 09:35 pCi/g 0.0261 0.0145 0.0145 U
0.002838 Americium 241 1
08/09/13 07:07 08/08/13 09:35 pCi/g 0.190 0.104 0.104 U
0.04701 Bismuth 212 1
08/09/13 07:07 08/08/13 09:35 pCi/g 0.0382 0.0273 0.0271 U
0.03108 Bismuth 214 1
08/09/13 07:07 08/08/13 09:35 pCi/g 0.0319 0.0337 0.0337 U
-0.003624 Lead 212 1
08/09/13 07:07 08/08/13 09:35 pCi/g 0.0339 0.0270 0.0266 0.04104 Lead 214 1
08/09/13 07:07 08/08/13 09:35 pCi/g 0.330 0.137 0.137 U
0.01743 Potassium 40 1
08/09/13 07:07 08/08/13 09:35 pCi/g 0.481 0.00216 0.00216 U
-0.0003607 Protactinium 231 1
08/09/13 07:07 08/08/13 09:35 pCi/g 0.0382 1.00 0.0273 0.0271 U
0.03108 Radium 226 1
08/09/13 07:07 08/08/13 09:35 pCi/g 0.313 1.00 0.0302 0.0301 U
0.02238 Thorium 234 1
08/09/13 07:07 08/08/13 09:35 pCi/g 0.0733 0.0422 0.0422 U
0.01884 Uranium 235 1
08/09/13 07:07 08/08/13 09:35 pCi/g 1.56 0.424 0.424 U
0.0000 Protactinium 234m 1
08/09/13 07:07 08/08/13 09:35 pCi/g 0.128 0.0212 0.0212 U
0.01002 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 08/08/13 09:35 08/09/13 07:07 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 24 of 29 1
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QC Sample Results TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-65524/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 65553 Prep Batch: 65524 Americium 241 Analyte 116 87 89 86.79 97.7 9.03 0.490 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 31.7 29.79 3.13 0.200 0.165 pCi/g 94 87 - 120 Cobalt 60 24.9 23.51 2.38 0.118 pCi/g 94 87 - 115 Client Sample ID: L100801BRS00 Lab Sample ID: 160-3234-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 66068 Prep Batch: 65524 Actinium 228 Analyte 1
0.17 0.9078 0.856 0.144 0.0993 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241 0.0267 U
0.02963 U
0.0597 0.0989 pCi/g 0.02 1
Bismuth 212 1.28 1.098 0.303 0.263 pCi/g 0.24 1
Bismuth 214 0.829 0.8260 0.113 0.0500 pCi/g 0.01 1
Lead 212 0.998 1.010 0.142 0.0459 pCi/g 0.04 1
Lead 214 0.932 0.9306 0.117 0.0621 pCi/g 0
1 Potassium 40 15.2 15.54 1.80 0.276 pCi/g 0.1 1
Protactinium 231
-0.555 U
0.3512 U
0.191 0.814 pCi/g 1.0 1
Radium 226 0.829 0.8260 0.113 1.00 0.0500 pCi/g 0.01 1
Thorium 234 5.71 5.822 0.745 1.00 0.875 pCi/g 0.08 1
Uranium 235 1.60 1.644 0.271 0.223 pCi/g 0.08 1
Protactinium 234m 10.5 14.88 4.21 3.26 pCi/g 0.50 1
Thorium 232 0.856 0.9078 0.144 0.0993 pCi/g 0.17 1
TestAmerica St. Louis Page 25 of 29 1
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QC Association Summary TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Metals Prep Batch: 65318 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3234-1 L100801BRS00 Total/NA Solid None 160-3234-1 MS L100801BRS00 Total/NA Solid None 160-3234-1 MSD L100801BRS00 Total/NA Solid None 160-3234-2 L100802BES00 Total/NA Solid None 160-3234-3 L100803BES00 Total/NA Solid None 160-3234-4 L100804BRS00 Total/NA Solid None 160-3234-5 L100805BES00 Total/NA Solid None 160-3234-6 L100806BES00 Total/NA Solid None 160-3234-7 L100807BRQ00 Total/NA Solid None 160-3234-8 L100807BRS00 Total/NA Solid None 160-3234-9 L100808BES00 Total/NA Solid None 160-3234-10 L100809BES00 Total/NA Solid None 160-3234-11 L100810BES00 Total/NA Solid None 160-3234-12 L100811BRS00 Total/NA Solid None 160-3234-13 L100812BES00 Total/NA Solid None 160-3234-14 L100813BES00 Total/NA Solid None 160-3234-15 L100814BRS00 Total/NA Solid None LCS 160-65318/2-A Lab Control Sample Total/NA Solid None MB 160-65318/1-A Method Blank Total/NA Analysis Batch: 65972 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 65318 160-3234-1 L100801BRS00 Total/NA Solid 6020A 65318 160-3234-1 MS L100801BRS00 Total/NA Solid 6020A 65318 160-3234-1 MSD L100801BRS00 Total/NA Solid 6020A 65318 160-3234-2 L100802BES00 Total/NA Solid 6020A 65318 160-3234-3 L100803BES00 Total/NA Solid 6020A 65318 160-3234-4 L100804BRS00 Total/NA Solid 6020A 65318 160-3234-5 L100805BES00 Total/NA Solid 6020A 65318 160-3234-6 L100806BES00 Total/NA Solid 6020A 65318 160-3234-7 L100807BRQ00 Total/NA Solid 6020A 65318 160-3234-8 L100807BRS00 Total/NA Solid 6020A 65318 160-3234-9 L100808BES00 Total/NA Solid 6020A 65318 160-3234-10 L100809BES00 Total/NA Solid 6020A 65318 160-3234-11 L100810BES00 Total/NA Solid 6020A 65318 160-3234-12 L100811BRS00 Total/NA Solid 6020A 65318 160-3234-13 L100812BES00 Total/NA Solid 6020A 65318 160-3234-14 L100813BES00 Total/NA Solid 6020A 65318 160-3234-15 L100814BRS00 Total/NA Solid 6020A 65318 LCS 160-65318/2-A Lab Control Sample Total/NA Solid 6020A 65318 MB 160-65318/1-A Method Blank Total/NA General Chemistry Analysis Batch: 64712 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3234-1 L100801BRS00 Total/NA Solid Moisture 160-3234-1 DU L100801BRS00 Total/NA Solid Moisture 160-3234-2 L100802BES00 Total/NA Solid Moisture 160-3234-3 L100803BES00 Total/NA TestAmerica St. Louis Page 26 of 29 1
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QC Association Summary TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
General Chemistry (Continued)
Analysis Batch: 64712 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3234-4 L100804BRS00 Total/NA Solid Moisture 160-3234-5 L100805BES00 Total/NA Solid Moisture 160-3234-6 L100806BES00 Total/NA Solid Moisture 160-3234-7 L100807BRQ00 Total/NA Solid Moisture 160-3234-8 L100807BRS00 Total/NA Solid Moisture 160-3234-9 L100808BES00 Total/NA Solid Moisture 160-3234-10 L100809BES00 Total/NA Solid Moisture 160-3234-11 L100810BES00 Total/NA Solid Moisture 160-3234-12 L100811BRS00 Total/NA Solid Moisture 160-3234-13 L100812BES00 Total/NA Solid Moisture 160-3234-14 L100813BES00 Total/NA Solid Moisture 160-3234-15 L100814BRS00 Total/NA Rad Leach Batch: 64984 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3234-1 L100801BRS00 Total/NA Solid Dry and Grind 160-3234-1 DU L100801BRS00 Total/NA Solid Dry and Grind 160-3234-2 L100802BES00 Total/NA Solid Dry and Grind 160-3234-3 L100803BES00 Total/NA Solid Dry and Grind 160-3234-4 L100804BRS00 Total/NA Solid Dry and Grind 160-3234-5 L100805BES00 Total/NA Solid Dry and Grind 160-3234-6 L100806BES00 Total/NA Solid Dry and Grind 160-3234-7 L100807BRQ00 Total/NA Solid Dry and Grind 160-3234-8 L100807BRS00 Total/NA Solid Dry and Grind 160-3234-9 L100808BES00 Total/NA Solid Dry and Grind 160-3234-10 L100809BES00 Total/NA Solid Dry and Grind 160-3234-11 L100810BES00 Total/NA Solid Dry and Grind 160-3234-12 L100811BRS00 Total/NA Solid Dry and Grind 160-3234-13 L100812BES00 Total/NA Solid Dry and Grind 160-3234-14 L100813BES00 Total/NA Solid Dry and Grind 160-3234-15 L100814BRS00 Total/NA Prep Batch: 65318 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3234-1 L100801BRS00 Total/NA Solid None 160-3234-1 MS L100801BRS00 Total/NA Solid None 160-3234-1 MSD L100801BRS00 Total/NA Solid None 160-3234-2 L100802BES00 Total/NA Solid None 160-3234-3 L100803BES00 Total/NA Solid None 160-3234-4 L100804BRS00 Total/NA Solid None 160-3234-5 L100805BES00 Total/NA Solid None 160-3234-6 L100806BES00 Total/NA Solid None 160-3234-7 L100807BRQ00 Total/NA Solid None 160-3234-8 L100807BRS00 Total/NA Solid None 160-3234-9 L100808BES00 Total/NA Solid None 160-3234-10 L100809BES00 Total/NA Solid None 160-3234-11 L100810BES00 Total/NA Solid None 160-3234-12 L100811BRS00 Total/NA TestAmerica St. Louis Page 27 of 29 1
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QC Association Summary TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Rad (Continued)
Prep Batch: 65318 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3234-13 L100812BES00 Total/NA Solid None 160-3234-14 L100813BES00 Total/NA Solid None 160-3234-15 L100814BRS00 Total/NA Solid None LCS 160-65318/2-A Lab Control Sample Total/NA Solid None MB 160-65318/1-A Method Blank Total/NA Prep Batch: 65524 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 64984 160-3234-1 L100801BRS00 Total/NA Solid Fill_Geo-0 64984 160-3234-1 DU L100801BRS00 Total/NA Solid Fill_Geo-0 64984 160-3234-2 L100802BES00 Total/NA Solid Fill_Geo-0 64984 160-3234-3 L100803BES00 Total/NA Solid Fill_Geo-0 64984 160-3234-4 L100804BRS00 Total/NA Solid Fill_Geo-0 64984 160-3234-5 L100805BES00 Total/NA Solid Fill_Geo-0 64984 160-3234-6 L100806BES00 Total/NA Solid Fill_Geo-0 64984 160-3234-7 L100807BRQ00 Total/NA Solid Fill_Geo-0 64984 160-3234-8 L100807BRS00 Total/NA Solid Fill_Geo-0 64984 160-3234-9 L100808BES00 Total/NA Solid Fill_Geo-0 64984 160-3234-10 L100809BES00 Total/NA Solid Fill_Geo-0 64984 160-3234-11 L100810BES00 Total/NA Solid Fill_Geo-0 64984 160-3234-12 L100811BRS00 Total/NA Solid Fill_Geo-0 64984 160-3234-13 L100812BES00 Total/NA Solid Fill_Geo-0 64984 160-3234-14 L100813BES00 Total/NA Solid Fill_Geo-0 64984 160-3234-15 L100814BRS00 Total/NA Solid Fill_Geo-0 LCS 160-65524/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-65524/1-A Method Blank Total/NA TestAmerica St. Louis Page 28 of 29 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-3234-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 92 160-3234-1 Percent Yield (Acceptance Limits)
L100801BRS00 91 160-3234-1 MS L100801BRS00 94 160-3234-1 MSD L100801BRS00 91 160-3234-2 L100802BES00 94 160-3234-3 L100803BES00 91 160-3234-4 L100804BRS00 90 160-3234-5 L100805BES00 89 160-3234-6 L100806BES00 90 160-3234-7 L100807BRQ00 90 160-3234-8 L100807BRS00 92 160-3234-9 L100808BES00 89 160-3234-10 L100809BES00 92 160-3234-11 L100810BES00 92 160-3234-12 L100811BRS00 90 160-3234-13 L100812BES00 90 160-3234-14 L100813BES00 87 160-3234-15 L100814BRS00 93 LCS 160-65318/2-A Lab Control Sample 91 MB 160-65318/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 29 of 29 1
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