ML18010A300

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Final Status Survey Final Report Volume 3, Chapter 6, Survey Area Release Record for Land Survey Area 10, Analytical Report, 160-3235-1
ML18010A300
Person / Time
Site: 07000036
Issue date: 08/13/2013
From:
Testamerica Labs, Westinghouse
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML18010A247 List: ... further results
References
HEM-17-72 160-3235-1
Download: ML18010A300 (27)
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Text

ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3235-1 Client Project/Site: RFP-CBA-022 (21 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

8/13/2013 4:30:50 PM Ivan Vania, Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

TestAmerica Job ID: 160-3235-1 Page 2 of 27 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

5 Receipt Checklists.........................................

7 Definitions/Glossary.......................................

8 Method Summary.........................................

9 Sample Summary.........................................

10 Client Sample Results......................................

11 QC Sample Results........................................

21 QC Association Summary...................................

24 Tracer Carrier Summary....................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3235-1 Project/Site: RFP-CBA-022 (21 DAY TAT)

Job ID: 160-3235-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (21 DAY TAT)

Report Number: 160-3235-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 08/03/2013; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 4 coolers at receipt time were 0.8º C, 2.2º C, 23.7º C and 25.1º C. Several of the samples were received on ice with a temperature of <

2C. For this job, there are only rad analyses requested. Samples for rad analysis do not require cold preservation.

TECHNETIUM-99 (ICPMS)

Samples L100816BUB00 (160-3235-1), L100817BUB00 (160-3235-2), L100818BUB00 (160-3235-3), L100819BUB00 (160-3235-4),

L100820BUB00 (160-3235-5), L100821BUB00 (160-3235-6), L100822BUB00 (160-3235-7), L100823BUB00 (160-3235-8),

L100824BUB00 (160-3235-9), L100825BUB00 (160-3235-10), L100826BUB00 (160-3235-11), L100827BUB00 (160-3235-12) and L100828BUB00 (160-3235-13) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 08/06/2013 and analyzed on 08/09/2013 and 08/12/2013.

No difficulties were encountered during the Tc-99 analysis. All quality control parameters were within the acceptance limits.

PERCENT SOLIDS TestAmerica St. Louis Page 3 of 27 1

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3235-1 Project/Site: RFP-CBA-022 (21 DAY TAT)

Job ID: 160-3235-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

Samples L100816BUB00 (160-3235-1), L100817BUB00 (160-3235-2), L100818BUB00 (160-3235-3), L100819BUB00 (160-3235-4),

L100820BUB00 (160-3235-5), L100821BUB00 (160-3235-6), L100822BUB00 (160-3235-7), L100823BUB00 (160-3235-8),

L100824BUB00 (160-3235-9), L100825BUB00 (160-3235-10), L100826BUB00 (160-3235-11), L100827BUB00 (160-3235-12) and L100828BUB00 (160-3235-13) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 08/05/2013.

No difficulties were encountered during the % solids analysis. All quality control parameters were within the acceptance limits.

CESIUM-137 & OTHER GAMMA EMITTERS (GS)

Samples L100816BUB00 (160-3235-1), L100817BUB00 (160-3235-2), L100818BUB00 (160-3235-3), L100819BUB00 (160-3235-4),

L100820BUB00 (160-3235-5), L100821BUB00 (160-3235-6), L100822BUB00 (160-3235-7), L100823BUB00 (160-3235-8),

L100824BUB00 (160-3235-9), L100825BUB00 (160-3235-10), L100826BUB00 (160-3235-11), L100827BUB00 (160-3235-12) and L100828BUB00 (160-3235-13) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 08/06/2013, and prepared and analyzed on 08/08/2013.

Preparation Batch 65535:

Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of Bismuth-214.

Because the samples have not had a 21-day ingrowth, the activity for Radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between Radium-226 and Bismuth-214 by the loss of Radon-222 during sample preparation. (160-3235-1 DU), (MB 160-65535/1-A), L100816BUB00 (160-3235-1), L100817BUB00 (160-3235-2), L100818BUB00 (160-3235-3), L100819BUB00 (160-3235-4), L100820BUB00 (160-3235-5), L100821BUB00 (160-3235-6), L100822BUB00 (160-3235-7),

L100823BUB00 (160-3235-8), L100824BUB00 (160-3235-9), L100825BUB00 (160-3235-10), L100826BUB00 (160-3235-11),

L100827BUB00 (160-3235-12), L100828BUB00 (160-3235-13)

No other other difficulties were encountered during the Gamma spec analysis. All other quality control parameters were within the acceptance limits.

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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 3

]

Page l of 11 Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAJN OF CUSTODY Instructions: Each time the container is transferred to ano1her organization, a person from each oq~anization should sign 1he CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain ofCutody ID No.l F-080213-01 Page Project Name:

Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number:

314-810-3382 Sampler Name Scott Jenkins Sample ID Date Time 1/2 I I *

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TA-MO Laboratory Address:

13715 Rider Trail North Phone No.

314-298-8566 Laboratory Contact Person:

Joe Walker Phone No.

708-870-8453 Rush Turn A.round Time (7 days)

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L100822BUBOO 8/1/2013 10:08 Ll00823BUBOO 8/1/2013 10:18 L100824BUBOO 8/1/2013 10:28 1Ll 00825BUBOO 8/1/2013 10:38 ILI 00826BUBOO 8/1/2013 10:48 IL 100827BUBOO 8/1/2013 10:58 Date/Time Relinquishe~: ~..._.:-

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.4 De2Tees C Cooler ID: !Shipper and Number:

080'.l-Ol Comments: Please re-analyze samples after 21-day ingrowth period.

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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 3 I

Page 1 ofll Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person (rom each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain ofCutody ID No.J F-080213-01 Project Name:

Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number:

314-810-3382 Sampler Name Scott Jenkins Page 2/2 8

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Laborato!Y Name:

TA-MO Laboratory Address:

I3715 Rider Trail North

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8 314-298-8566 iii Laboratory Contact Person:

~ Joe Walker Phone No.

708-870-8453 Rush Turn Around Time (7 days)

Remarks 1{'; ~s:.c\\ -- I="<, Ia_~£$u L~A 1oocf I

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Dateffime Date/Time Total ICooler Temperature:

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0803-01 Comments: Please re-analyze san1ples after 21-day ingrowth period.

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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3235-1 Login Number: 3235 Question Answer Comment Creator: Vania, Ivan H List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

True Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

Where required True Cooler Temperature is acceptable.

See NCM True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Qualifiers Metals Qualifier Description J

Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier Rad Qualifier Description U

Indicates the analyte was analyzed for but not detected.

Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 27 1

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Sample Summary TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-3235-1 L100816BUB00 Solid 08/01/13 09:08 08/03/13 16:01 160-3235-2 L100817BUB00 Solid 08/01/13 09:18 08/03/13 16:01 160-3235-3 L100818BUB00 Solid 08/01/13 09:28 08/03/13 16:01 160-3235-4 L100819BUB00 Solid 08/01/13 09:38 08/03/13 16:01 160-3235-5 L100820BUB00 Solid 08/01/13 09:48 08/03/13 16:01 160-3235-6 L100821BUB00 Solid 08/01/13 09:58 08/03/13 16:01 160-3235-7 L100822BUB00 Solid 08/01/13 10:08 08/03/13 16:01 160-3235-8 L100823BUB00 Solid 08/01/13 10:18 08/03/13 16:01 160-3235-9 L100824BUB00 Solid 08/01/13 10:28 08/03/13 16:01 160-3235-10 L100825BUB00 Solid 08/01/13 10:38 08/03/13 16:01 160-3235-11 L100826BUB00 Solid 08/01/13 10:48 08/03/13 16:01 160-3235-12 L100827BUB00 Solid 08/01/13 10:58 08/03/13 16:01 160-3235-13 L100828BUB00 Solid 08/01/13 15:32 08/03/13 16:01 TestAmerica St. Louis Page 10 of 27 1

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Client Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-1 Client Sample ID: L100816BUB00 Matrix: Solid Date Collected: 08/01/13 09:08 Percent Solids: 90.7 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000035 J

0.00054 0.000016 mg/Kg

08/06/13 09:27 08/12/13 12:06 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.598 (2+/-)

0.0680 (2+/-)

1 08/12/13 12:06 08/06/13 09:27 pCi/g 0.184 1.07 RL MDC 0.0433 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/12/13 12:06 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 103 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.490 (2+/-)

0.117 (2+/-)

1 08/08/13 21:20 08/08/13 11:06 pCi/g 0.159 RL MDC 0.106 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 21:20 1

0.109 0.0657 0.0657 U

-0.0316 Americium 241 pCi/g 08/08/13 11:06 08/08/13 21:20 1

0.196 0.320 0.301 1.03 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 21:20 1

0.0694 0.118 0.100 0.605 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 21:20 1

0.0523 0.123 0.0682 0.792 Lead 212 pCi/g 08/08/13 11:06 08/08/13 21:20 1

0.0675 0.115 0.0877 0.710 Lead 214 pCi/g 08/08/13 11:06 08/08/13 21:20 1

0.423 1.82 1.19 13.5 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 21:20 1

6.02 3.61 3.61 U

0.491 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 21:20 1

1.25 0.756 0.753 U

-0.550 Protactinium 231 pCi/g 08/08/13 11:06 08/08/13 21:20 1

0.0694 0.118 0.100 0.605 Radium 226 pCi/g 08/08/13 11:06 08/08/13 21:20 1

0.954 0.498 0.432 2.37 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 21:20 1

0.245 0.217 0.200 0.831 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 21:20 1

0.159 0.117 0.106 0.490 Thorium 232 Tl-208 0.253 0.0442 0.0514 0.0313 pCi/g 08/08/13 11:06 08/08/13 21:20 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3235-2 Client Sample ID: L100817BUB00 Matrix: Solid Date Collected: 08/01/13 09:18 Percent Solids: 91.0 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000025 J

0.00077 0.000023 mg/Kg

08/06/13 09:27 08/09/13 19:52 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.431 (2+/-)

0.277 (2+/-)

1 08/09/13 19:52 08/06/13 09:27 pCi/g 0.265 1.55 RL MDC 0.192 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 19:52 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 71 TestAmerica St. Louis Page 11 of 27 1

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Client Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-2 Client Sample ID: L100817BUB00 Matrix: Solid Date Collected: 08/01/13 09:18 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.552 (2+/-)

0.0911 (2+/-)

1 08/08/13 17:25 08/08/13 11:06 pCi/g 0.0681 RL MDC 0.0716 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 17:25 1

0.0795 0.0475 0.0475 U

-0.0163 Americium 241 pCi/g 08/08/13 11:06 08/08/13 17:25 1

0.220 0.224 0.215 0.601 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 17:25 1

0.0503 0.0890 0.0700 0.529 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 17:25 1

0.0583 0.0815 0.0508 0.492 Lead 212 pCi/g 08/08/13 11:06 08/08/13 17:25 1

0.0499 0.0839 0.0588 0.575 Lead 214 pCi/g 08/08/13 11:06 08/08/13 17:25 1

0.271 1.33 0.762 10.7 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 17:25 1

3.18 2.14 2.11 3.63 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 17:25 1

0.767 0.158 0.156 U

0.216 Protactinium 231 pCi/g 08/08/13 11:06 08/08/13 17:25 1

0.0503 0.0890 0.0700 0.529 Radium 226 pCi/g 08/08/13 11:06 08/08/13 17:25 1

0.654 0.575 0.546 1.71 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 17:25 1

0.168 0.133 0.126 0.418 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 17:25 1

0.0681 0.0911 0.0716 0.552 Thorium 232 Tl-208 0.185 0.0290 0.0348 0.0221 pCi/g 08/08/13 11:06 08/08/13 17:25 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3235-3 Client Sample ID: L100818BUB00 Matrix: Solid Date Collected: 08/01/13 09:28 Percent Solids: 84.9 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000035 J

0.00091 0.000027 mg/Kg

08/06/13 09:27 08/09/13 19:56 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.599 (2+/-)

0.169 (2+/-)

1 08/09/13 19:56 08/06/13 09:27 pCi/g 0.312 1.82 RL MDC 0.0937 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 19:56 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 64 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.15 (2+/-)

0.186 (2+/-)

1 08/08/13 17:27 08/08/13 11:06 pCi/g 0.0973 RL MDC 0.144 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.0941 0.0986 0.0985 U

-0.0205 Americium 241 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.418 0.500 0.474 1.55 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.0676 0.119 0.0932 0.712 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.0565 0.151 0.0714 1.03 Lead 212 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.0652 0.120 0.0849 0.822 Lead 214 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.138 2.04 1.12 16.6 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 17:27 1

5.47 3.13 3.13 U

0.800 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.975 0.237 0.232 U

0.448 Protactinium 231 TestAmerica St. Louis Page 12 of 27 1

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Client Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-3 Client Sample ID: L100818BUB00 Matrix: Solid Date Collected: 08/01/13 09:28 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Radium 226 0.712 (2+/-)

0.119 (2+/-)

1 08/08/13 17:27 08/08/13 11:06 pCi/g 0.0676 RL MDC 0.0932 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.943 0.821 0.784 2.34 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.179 0.158 0.149 0.522 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.0973 0.186 0.144 1.15 Thorium 232 Tl-208 0.307 0.0472 0.0569 0.0357 pCi/g 08/08/13 11:06 08/08/13 17:27 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3235-4 Client Sample ID: L100819BUB00 Matrix: Solid Date Collected: 08/01/13 09:38 Percent Solids: 83.0 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00094 0.000028 mg/Kg

08/06/13 09:27 08/09/13 20:00 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.231 U

(2+/-)

0.263 (2+/-)

1 08/09/13 20:00 08/06/13 09:27 pCi/g 0.321 1.87 RL MDC 0.169 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 20:00 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 65 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.11 (2+/-)

0.179 (2+/-)

1 08/08/13 17:27 08/08/13 11:06 pCi/g 0.0923 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.128 0.0763 0.0763 U

0.0246 Americium 241 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.589 0.424 0.415 0.845 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.0888 0.155 0.127 0.858 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.0762 0.167 0.0881 1.10 Lead 212 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.0939 0.133 0.0979 0.868 Lead 214 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.193 2.20 1.34 17.1 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 17:27 1

5.81 3.89 3.87 U

4.03 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 17:27 1

1.41 0.287 0.284 U

0.341 Protactinium 231 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.0888 0.155 0.127 0.858 Radium 226 pCi/g 08/08/13 11:06 08/08/13 17:27 1

1.17 0.559 0.498 2.42 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.252 0.222 0.209 0.727 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 17:27 1

0.0923 0.179 0.138 1.11 Thorium 232 Tl-208 0.397 0.0566 0.0700 0.0364 pCi/g 08/08/13 11:06 08/08/13 17:27 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 13 of 27 1

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Client Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-5 Client Sample ID: L100820BUB00 Matrix: Solid Date Collected: 08/01/13 09:48 Percent Solids: 77.5 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00096 0.000029 mg/Kg

08/06/13 09:27 08/09/13 20:04 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.276 U

(2+/-)

0.0441 (2+/-)

1 08/09/13 20:04 08/06/13 09:27 pCi/g 0.329 1.92 RL MDC 0.0152 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 20:04 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 67 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.924 (2+/-)

0.152 (2+/-)

1 08/08/13 17:28 08/08/13 11:06 pCi/g 0.101 RL MDC 0.120 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 17:28 1

0.0882 0.0528 0.0528 U

0.0210 Americium 241 pCi/g 08/08/13 11:06 08/08/13 17:28 1

0.320 0.354 0.337 1.03 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 17:28 1

0.0539 0.114 0.0846 0.740 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 17:28 1

0.0503 0.147 0.0669 1.01 Lead 212 pCi/g 08/08/13 11:06 08/08/13 17:28 1

0.0613 0.115 0.0748 0.844 Lead 214 pCi/g 08/08/13 11:06 08/08/13 17:28 1

0.288 2.24 1.11 19.0 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 17:28 1

4.79 2.76 2.76 U

0.861 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 17:28 1

0.955 0.251 0.246 U

0.455 Protactinium 231 pCi/g 08/08/13 11:06 08/08/13 17:28 1

0.0539 0.114 0.0846 0.740 Radium 226 pCi/g 08/08/13 11:06 08/08/13 17:28 1

0.752 0.582 0.567 1.25 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 17:28 1

0.209 0.109 0.108 U

0.0906 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 17:28 1

0.101 0.152 0.120 0.924 Thorium 232 Tl-208 0.319 0.0445 0.0555 0.0344 pCi/g 08/08/13 11:06 08/08/13 17:28 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3235-6 Client Sample ID: L100821BUB00 Matrix: Solid Date Collected: 08/01/13 09:58 Percent Solids: 80.4 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00085 0.000026 mg/Kg

08/06/13 09:27 08/09/13 20:08 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.222 U

(2+/-)

0.212 (2+/-)

1 08/09/13 20:08 08/06/13 09:27 pCi/g 0.292 1.70 RL MDC 0.152 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 20:08 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 73 TestAmerica St. Louis Page 14 of 27 1

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Client Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-6 Client Sample ID: L100821BUB00 Matrix: Solid Date Collected: 08/01/13 09:58 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.15 (2+/-)

0.208 (2+/-)

1 08/08/13 18:00 08/08/13 11:06 pCi/g 0.128 RL MDC 0.172 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 18:00 1

0.0783 0.0456 0.0456 U

-0.00238 Americium 241 pCi/g 08/08/13 11:06 08/08/13 18:00 1

0.262 0.514 0.465 2.10 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 18:00 1

0.0864 0.142 0.120 0.729 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 18:00 1

0.0659 0.155 0.0829 1.01 Lead 212 pCi/g 08/08/13 11:06 08/08/13 18:00 1

0.0925 0.146 0.118 0.837 Lead 214 pCi/g 08/08/13 11:06 08/08/13 18:00 1

0.502 2.22 1.42 16.7 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 18:00 1

7.63 4.23 4.23 U

0.0572 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 18:00 1

1.47 0.241 0.237 U

0.382 Protactinium 231 pCi/g 08/08/13 11:06 08/08/13 18:00 1

0.0864 0.142 0.120 0.729 Radium 226 pCi/g 08/08/13 11:06 08/08/13 18:00 1

0.902 0.730 0.707 1.74 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 18:00 1

0.232 0.146 0.146 U

0.108 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 18:00 1

0.128 0.208 0.172 1.15 Thorium 232 Tl-208 0.363 0.0529 0.0650 0.0343 pCi/g 08/08/13 11:06 08/08/13 18:00 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3235-7 Client Sample ID: L100822BUB00 Matrix: Solid Date Collected: 08/01/13 10:08 Percent Solids: 82.0 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000025 J

0.00076 0.000023 mg/Kg

08/06/13 09:27 08/09/13 20:12 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.431 (2+/-)

0.215 (2+/-)

1 08/09/13 20:12 08/06/13 09:27 pCi/g 0.260 1.52 RL MDC 0.168 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 20:12 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 80 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.08 (2+/-)

0.171 (2+/-)

1 08/08/13 18:04 08/08/13 11:06 pCi/g 0.101 RL MDC 0.131 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 18:04 1

0.102 0.0607 0.0607 U

0.0139 Americium 241 pCi/g 08/08/13 11:06 08/08/13 18:04 1

0.248 0.356 0.326 1.37 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 18:04 1

0.0604 0.107 0.0825 0.657 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 18:04 1

0.0497 0.152 0.0672 1.06 Lead 212 pCi/g 08/08/13 11:06 08/08/13 18:04 1

0.0628 0.121 0.0844 0.837 Lead 214 pCi/g 08/08/13 11:06 08/08/13 18:04 1

0.270 2.06 1.03 17.4 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 18:04 1

4.26 2.55 2.55 U

1.68 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 18:04 1

1.08 0.212 0.205 U

0.473 Protactinium 231 TestAmerica St. Louis Page 15 of 27 1

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Client Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-7 Client Sample ID: L100822BUB00 Matrix: Solid Date Collected: 08/01/13 10:08 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Radium 226 0.657 (2+/-)

0.107 (2+/-)

1 08/08/13 18:04 08/08/13 11:06 pCi/g 0.0604 RL MDC 0.0825 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 18:04 1

0.748 0.303 0.286 0.952 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 18:04 1

0.223 0.129 0.128 U

0.146 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 18:04 1

0.101 0.171 0.131 1.08 Thorium 232 Tl-208 0.308 0.0394 0.0508 0.0297 pCi/g 08/08/13 11:06 08/08/13 18:04 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3235-8 Client Sample ID: L100823BUB00 Matrix: Solid Date Collected: 08/01/13 10:18 Percent Solids: 71.7 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00091 0.000027 mg/Kg

08/06/13 09:27 08/09/13 20:15 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.429 (2+/-)

0.139 (2+/-)

1 08/09/13 20:15 08/06/13 09:27 pCi/g 0.312 1.82 RL MDC 0.0978 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 20:15 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 76 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.983 (2+/-)

0.146 (2+/-)

1 08/08/13 18:05 08/08/13 11:06 pCi/g 0.0834 RL MDC 0.107 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 18:05 1

0.0981 0.0584 0.0584 U

-0.00793 Americium 241 pCi/g 08/08/13 11:06 08/08/13 18:05 1

0.319 0.396 0.376 1.20 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 18:05 1

0.0673 0.110 0.0858 0.657 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 18:05 1

0.0758 0.147 0.0848 0.925 Lead 212 pCi/g 08/08/13 11:06 08/08/13 18:05 1

0.0723 0.107 0.0740 0.744 Lead 214 pCi/g 08/08/13 11:06 08/08/13 18:05 1

0.319 2.15 1.05 18.3 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 18:05 1

4.13 2.44 2.40 4.36 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 18:05 1

0.969 0.184 0.181 U

0.304 Protactinium 231 pCi/g 08/08/13 11:06 08/08/13 18:05 1

0.0673 0.110 0.0858 0.657 Radium 226 pCi/g 08/08/13 11:06 08/08/13 18:05 1

0.832 0.706 0.690 1.43 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 18:05 1

0.217 0.121 0.120 U

0.123 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 18:05 1

0.0834 0.146 0.107 0.983 Thorium 232 Tl-208 0.309 0.0422 0.0530 0.0325 pCi/g 08/08/13 11:06 08/08/13 18:05 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 16 of 27 1

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Client Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-9 Client Sample ID: L100824BUB00 Matrix: Solid Date Collected: 08/01/13 10:28 Percent Solids: 83.0 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00090 0.000027 mg/Kg

08/06/13 09:27 08/09/13 20:19 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.326 (2+/-)

0.210 (2+/-)

1 08/09/13 20:19 08/06/13 09:27 pCi/g 0.307 1.79 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 20:19 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 67 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.04 (2+/-)

0.176 (2+/-)

1 08/08/13 18:06 08/08/13 11:06 pCi/g 0.106 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 18:06 1

0.103 0.145 0.145 U

-0.00271 Americium 241 pCi/g 08/08/13 11:06 08/08/13 18:06 1

0.361 0.479 0.450 1.59 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 18:06 1

0.0706 0.127 0.100 0.755 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 18:06 1

0.0577 0.144 0.0735 0.954 Lead 212 pCi/g 08/08/13 11:06 08/08/13 18:06 1

0.0799 0.132 0.0967 0.868 Lead 214 pCi/g 08/08/13 11:06 08/08/13 18:06 1

0.295 2.35 1.31 19.1 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 18:06 1

4.44 2.54 2.54 U

1.04 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 18:06 1

1.14 0.219 0.215 U

0.386 Protactinium 231 pCi/g 08/08/13 11:06 08/08/13 18:06 1

0.0706 0.127 0.100 0.755 Radium 226 pCi/g 08/08/13 11:06 08/08/13 18:06 1

0.855 0.703 0.669 2.06 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 18:06 1

0.205 0.167 0.161 0.446 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 18:06 1

0.106 0.176 0.141 1.04 Thorium 232 Tl-208 0.345 0.0473 0.0594 0.0336 pCi/g 08/08/13 11:06 08/08/13 18:06 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3235-10 Client Sample ID: L100825BUB00 Matrix: Solid Date Collected: 08/01/13 10:38 Percent Solids: 81.9 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.0011 0.000033 mg/Kg

08/06/13 09:27 08/09/13 20:23 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.379 (2+/-)

0.339 (2+/-)

1 08/09/13 20:23 08/06/13 09:27 pCi/g 0.373 2.18 RL MDC 0.186 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 20:23 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 56 TestAmerica St. Louis Page 17 of 27 1

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Client Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-10 Client Sample ID: L100825BUB00 Matrix: Solid Date Collected: 08/01/13 10:38 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.01 (2+/-)

0.180 (2+/-)

1 08/08/13 18:07 08/08/13 11:06 pCi/g 0.147 RL MDC 0.147 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 18:07 1

0.115 0.0682 0.0682 U

-0.000490 Americium 241 pCi/g 08/08/13 11:06 08/08/13 18:07 1

0.379 0.501 0.478 1.45 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 18:07 1

0.0798 0.127 0.106 0.677 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 18:07 1

0.0666 0.141 0.0769 0.916 Lead 212 pCi/g 08/08/13 11:06 08/08/13 18:07 1

0.0690 0.119 0.0925 0.725 Lead 214 pCi/g 08/08/13 11:06 08/08/13 18:07 1

0.177 2.27 1.32 18.0 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 18:07 1

8.38 1.83 1.83 U

0.000 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 18:07 1

1.18 0.189 0.187 U

0.275 Protactinium 231 pCi/g 08/08/13 11:06 08/08/13 18:07 1

0.0798 0.127 0.106 0.677 Radium 226 pCi/g 08/08/13 11:06 08/08/13 18:07 1

0.892 0.719 0.698 1.65 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 18:07 1

0.215 0.184 0.182 0.323 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 18:07 1

0.147 0.180 0.147 1.01 Thorium 232 Tl-208 0.271 0.0451 0.0531 0.0361 pCi/g 08/08/13 11:06 08/08/13 18:07 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3235-11 Client Sample ID: L100826BUB00 Matrix: Solid Date Collected: 08/01/13 10:48 Percent Solids: 82.8 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00073 0.000022 mg/Kg

08/06/13 09:27 08/09/13 20:27 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.100 U

(2+/-)

0.0595 (2+/-)

1 08/09/13 20:27 08/06/13 09:27 pCi/g 0.250 1.46 RL MDC 0.0486 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 20:27 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 83 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.08 (2+/-)

0.157 (2+/-)

1 08/08/13 18:08 08/08/13 11:06 pCi/g 0.101 RL MDC 0.112 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 18:08 1

0.0965 0.0570 0.0570 U

0.000792 Americium 241 pCi/g 08/08/13 11:06 08/08/13 18:08 1

0.337 0.338 0.325 0.906 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 18:08 1

0.0681 0.117 0.0909 0.715 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 18:08 1

0.0538 0.151 0.0700 1.03 Lead 212 pCi/g 08/08/13 11:06 08/08/13 18:08 1

0.0637 0.120 0.0783 0.881 Lead 214 pCi/g 08/08/13 11:06 08/08/13 18:08 1

0.320 2.29 1.16 19.3 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 18:08 1

4.94 2.65 2.61 U

4.09 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 18:08 1

0.768 0.295 0.291 U

0.469 Protactinium 231 TestAmerica St. Louis Page 18 of 27 1

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Client Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-11 Client Sample ID: L100826BUB00 Matrix: Solid Date Collected: 08/01/13 10:48 Date Received: 08/03/13 16:01 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Radium 226 0.715 (2+/-)

0.117 (2+/-)

1 08/08/13 18:08 08/08/13 11:06 pCi/g 0.0681 RL MDC 0.0909 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 18:08 1

0.833 0.666 0.647 1.53 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 18:08 1

0.208 0.159 0.158 U

0.129 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 18:08 1

0.101 0.157 0.112 1.08 Thorium 232 Tl-208 0.358 0.0471 0.0600 0.0344 pCi/g 08/08/13 11:06 08/08/13 18:08 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3235-12 Client Sample ID: L100827BUB00 Matrix: Solid Date Collected: 08/01/13 10:58 Percent Solids: 80.4 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00088 0.000026 mg/Kg

08/06/13 09:27 08/09/13 20:39 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.251 U

(2+/-)

0.169 (2+/-)

1 08/09/13 20:39 08/06/13 09:27 pCi/g 0.301 1.76 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 20:39 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 71 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.03 (2+/-)

0.178 (2+/-)

1 08/08/13 19:34 08/08/13 11:06 pCi/g 0.110 RL MDC 0.144 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 19:34 1

0.100 0.0600 0.0599 U

0.0265 Americium 241 pCi/g 08/08/13 11:06 08/08/13 19:34 1

0.412 0.505 0.476 1.62 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 19:34 1

0.0813 0.146 0.118 0.827 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 19:34 1

0.0721 0.161 0.0839 1.07 Lead 212 pCi/g 08/08/13 11:06 08/08/13 19:34 1

0.0861 0.134 0.0979 0.887 Lead 214 pCi/g 08/08/13 11:06 08/08/13 19:34 1

0.308 2.36 1.38 18.7 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 19:34 1

6.71 4.24 4.23 U

1.45 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 19:34 1

1.33 0.269 0.264 U

0.427 Protactinium 231 pCi/g 08/08/13 11:06 08/08/13 19:34 1

0.0813 0.146 0.118 0.827 Radium 226 pCi/g 08/08/13 11:06 08/08/13 19:34 1

0.992 0.802 0.792 1.22 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 19:34 1

0.204 0.159 0.157 U

0.200 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 19:34 1

0.110 0.178 0.144 1.03 Thorium 232 Tl-208 0.350 0.0557 0.0665 0.0374 pCi/g 08/08/13 11:06 08/08/13 19:34 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-3235-13 Client Sample ID: L100828BUB00 Matrix: Solid Date Collected: 08/01/13 15:32 Percent Solids: 88.6 Date Received: 08/03/13 16:01 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000029 J

0.00097 0.000029 mg/Kg

08/06/13 09:27 08/09/13 20:43 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.504 (2+/-)

0.377 (2+/-)

1 08/09/13 20:43 08/06/13 09:27 pCi/g 0.331 1.93 RL MDC 0.214 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/06/13 09:27 08/09/13 20:43 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 58 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.570 (2+/-)

0.0908 (2+/-)

1 08/08/13 19:38 08/08/13 11:06 pCi/g 0.0541 RL MDC 0.0697 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 08/08/13 11:06 08/08/13 19:38 1

0.0636 0.0374 0.0374 U

-0.00326 Americium 241 pCi/g 08/08/13 11:06 08/08/13 19:38 1

0.243 0.315 0.300 0.940 Bismuth 212 pCi/g 08/08/13 11:06 08/08/13 19:38 1

0.0424 0.0779 0.0612 0.463 Bismuth 214 pCi/g 08/08/13 11:06 08/08/13 19:38 1

0.0421 0.0852 0.0474 0.547 Lead 212 pCi/g 08/08/13 11:06 08/08/13 19:38 1

0.0424 0.0845 0.0596 0.577 Lead 214 pCi/g 08/08/13 11:06 08/08/13 19:38 1

0.236 1.23 0.725 9.76 Potassium 40 pCi/g 08/08/13 11:06 08/08/13 19:38 1

3.30 1.75 1.73 U

2.38 Protactinium 234m pCi/g 08/08/13 11:06 08/08/13 19:38 1

0.817 0.183 0.180 U

0.309 Protactinium 231 pCi/g 08/08/13 11:06 08/08/13 19:38 1

0.0424 0.0779 0.0612 0.463 Radium 226 pCi/g 08/08/13 11:06 08/08/13 19:38 1

0.646 0.531 0.525 0.775 Thorium 234 pCi/g 08/08/13 11:06 08/08/13 19:38 1

0.148 0.100 0.0995 U

0.102 Uranium 235 pCi/g 08/08/13 11:06 08/08/13 19:38 1

0.0541 0.0908 0.0697 0.570 Thorium 232 Tl-208 0.172 0.0260 0.0315 0.0180 pCi/g 08/08/13 11:06 08/08/13 19:38 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 20 of 27 1

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QC Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-64842/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 65972 Prep Batch: 64842 RL MDL Technetium 99 ND 0.00069 0.000021 mg/Kg 08/06/13 09:27 08/09/13 19:25 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-64842/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 66038 Prep Batch: 64842 Technetium 99 0.00217 0.00243 mg/Kg 112 80 - 120 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Client Sample ID: L100816BUB00 Lab Sample ID: 160-3235-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 66038 Prep Batch: 64842 Technetium 99 0.000035 J

0.00256 0.00277 mg/Kg 107 75 - 125

Analyte MS MS D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Client Sample ID: L100816BUB00 Lab Sample ID: 160-3235-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 66038 Prep Batch: 64842 Technetium 99 0.000035 J

0.00253 0.00276 mg/Kg 108 75 - 125 0

30

Analyte MSD MSD D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-64842/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 65973 Prep Batch: 64842 Technetium 99 Analyte U

1 08/09/13 19:25 08/06/13 09:27 pCi/g 0.237 MDC 1.38 RL 0.0154

-0.0110 (2+/-)

(2+/-)

MB

-0.01066 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Carrier Re 30 - 110 08/06/13 09:27 08/09/13 19:25 1

Dil Fac Prepared Analyzed Qualifier Limits

%Yield 72 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-64842/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 66039 Prep Batch: 64842 Technetium 99 Analyte 120 80 112 41.67 37.1 3.70 0.927 0.159 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 LCS Qualifier Limits

%Yield 107 LCS TestAmerica St. Louis Page 21 of 27 1

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QC Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)

Client Sample ID: L100816BUB00 Lab Sample ID: 160-3235-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 66039 Prep Batch: 64842 Technetium 99 Analyte 125 75 107 47.42 43.7 0.598 4.32 1.09 0.187 RL MDC (2+/-)

MS MS pCi/g Unit Result Qual

%Rec Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 MS Qualifier Limits

%Yield 101 MS Client Sample ID: L100816BUB00 Lab Sample ID: 160-3235-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 66039 Prep Batch: 64842 Technetium 99 Analyte 1

0.02 125 75 108 47.26 43.3 0.598 4.51 1.08 0.185 RL MDC (2+/-)

MSD MSD pCi/g Unit Result Qual

%Rec Limit Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits

%Yield 102 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-65535/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 65546 Prep Batch: 65535 Actinium 228 Analyte U

1 08/08/13 17:21 08/08/13 11:06 pCi/g 0.0952 MDC RL 0.0112 0.0112 (2+/-)

(2+/-)

MB 0.0000 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

08/08/13 17:21 08/08/13 11:06 pCi/g 0.0216 0.0124 0.0124 U

0.005859 Americium 241 1

08/08/13 17:21 08/08/13 11:06 pCi/g 0.236 0.121 0.121 U

-0.02242 Bismuth 212 1

08/08/13 17:21 08/08/13 11:06 pCi/g 0.0416 0.0307 0.0306 U

0.02985 Bismuth 214 1

08/08/13 17:21 08/08/13 11:06 pCi/g 0.0284 0.0152 0.0152 U

0.008848 Lead 212 1

08/08/13 17:21 08/08/13 11:06 pCi/g 0.0431 0.0358 0.0358 U

-0.004672 Lead 214 1

08/08/13 17:21 08/08/13 11:06 pCi/g 0.327 0.187 0.187 U

-0.02095 Potassium 40 1

08/08/13 17:21 08/08/13 11:06 pCi/g 1.56 0.424 0.424 U

0.0000 Protactinium 234m 1

08/08/13 17:21 08/08/13 11:06 pCi/g 0.478 0.0523 0.0522 U

0.02099 Protactinium 231 1

08/08/13 17:21 08/08/13 11:06 pCi/g 0.0416 0.0307 0.0306 U

0.02985 Radium 226 1

08/08/13 17:21 08/08/13 11:06 pCi/g 0.290 0.0929 0.0927 U

0.06171 Thorium 234 1

08/08/13 17:21 08/08/13 11:06 pCi/g 0.0501 0.0311 0.0310 U

0.02561 Uranium 235 1

08/08/13 17:21 08/08/13 11:06 pCi/g 0.0952 0.0112 0.0112 U

0.0000 Thorium 232 Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 08/08/13 11:06 08/08/13 17:21 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected TestAmerica St. Louis Page 22 of 27 1

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QC Sample Results TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-65535/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 65544 Prep Batch: 65535 Americium 241 Analyte 116 87 97 94.39 97.7 9.88 0.979 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 31.7 31.72 3.33 0.200 0.195 pCi/g 100 87 - 120 Cobalt 60 24.9 24.79 2.51 0.101 pCi/g 99 87 - 115 Client Sample ID: L100816BUB00 Lab Sample ID: 160-3235-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 65551 Prep Batch: 65535 Actinium 228 Analyte 1

1.07 0.7712 0.490 0.147 0.0729 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Americium 241

-0.0316 U

0.000249 9

U 0.0468 0.0793 pCi/g 0.28 1

Bismuth 212 1.03 0.5934 0.253 0.332 pCi/g 0.77 1

Bismuth 214 0.605 0.5857 0.0980 0.0542 pCi/g 0.09 1

Lead 212 0.792 0.6887 0.105 0.0514 pCi/g 0.45 1

Lead 214 0.710 0.6472 0.0923 0.0564 pCi/g 0.30 1

Potassium 40 13.5 13.64 1.67 0.274 pCi/g 0.05 1

Protactinium 234m 0.491 U

2.283 U

2.53 4.23 pCi/g 0.29 1

Protactinium 231

-0.550 U

0.2482 U

0.161 0.788 pCi/g 0.87 1

Radium 226 0.605 0.5857 0.0980 0.0542 pCi/g 0.09 1

Thorium 234 2.37 1.958 0.561 0.675 pCi/g 0.39 1

Uranium 235 0.831 0.6715 0.148 0.177 pCi/g 0.44 1

Thorium 232 0.490 0.7712 0.147 0.0729 pCi/g 1.07 1

TestAmerica St. Louis Page 23 of 27 1

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QC Association Summary TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Metals Prep Batch: 64842 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3235-1 L100816BUB00 Total/NA Solid None 160-3235-1 MS L100816BUB00 Total/NA Solid None 160-3235-1 MSD L100816BUB00 Total/NA Solid None 160-3235-2 L100817BUB00 Total/NA Solid None 160-3235-3 L100818BUB00 Total/NA Solid None 160-3235-4 L100819BUB00 Total/NA Solid None 160-3235-5 L100820BUB00 Total/NA Solid None 160-3235-6 L100821BUB00 Total/NA Solid None 160-3235-7 L100822BUB00 Total/NA Solid None 160-3235-8 L100823BUB00 Total/NA Solid None 160-3235-9 L100824BUB00 Total/NA Solid None 160-3235-10 L100825BUB00 Total/NA Solid None 160-3235-11 L100826BUB00 Total/NA Solid None 160-3235-12 L100827BUB00 Total/NA Solid None 160-3235-13 L100828BUB00 Total/NA Solid None LCS 160-64842/2-A Lab Control Sample Total/NA Solid None MB 160-64842/1-A Method Blank Total/NA Analysis Batch: 65972 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 64842 160-3235-2 L100817BUB00 Total/NA Solid 6020A 64842 160-3235-3 L100818BUB00 Total/NA Solid 6020A 64842 160-3235-4 L100819BUB00 Total/NA Solid 6020A 64842 160-3235-5 L100820BUB00 Total/NA Solid 6020A 64842 160-3235-6 L100821BUB00 Total/NA Solid 6020A 64842 160-3235-7 L100822BUB00 Total/NA Solid 6020A 64842 160-3235-8 L100823BUB00 Total/NA Solid 6020A 64842 160-3235-9 L100824BUB00 Total/NA Solid 6020A 64842 160-3235-10 L100825BUB00 Total/NA Solid 6020A 64842 160-3235-11 L100826BUB00 Total/NA Solid 6020A 64842 160-3235-12 L100827BUB00 Total/NA Solid 6020A 64842 160-3235-13 L100828BUB00 Total/NA Solid 6020A 64842 MB 160-64842/1-A Method Blank Total/NA Analysis Batch: 66038 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 64842 160-3235-1 L100816BUB00 Total/NA Solid 6020A 64842 160-3235-1 MS L100816BUB00 Total/NA Solid 6020A 64842 160-3235-1 MSD L100816BUB00 Total/NA Solid 6020A 64842 LCS 160-64842/2-A Lab Control Sample Total/NA General Chemistry Analysis Batch: 64712 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3235-1 L100816BUB00 Total/NA Solid Moisture 160-3235-2 L100817BUB00 Total/NA Solid Moisture 160-3235-3 L100818BUB00 Total/NA Solid Moisture 160-3235-4 L100819BUB00 Total/NA Solid Moisture 160-3235-5 L100820BUB00 Total/NA TestAmerica St. Louis Page 24 of 27 1

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QC Association Summary TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

General Chemistry (Continued)

Analysis Batch: 64712 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3235-6 L100821BUB00 Total/NA Solid Moisture 160-3235-7 L100822BUB00 Total/NA Solid Moisture 160-3235-8 L100823BUB00 Total/NA Solid Moisture 160-3235-9 L100824BUB00 Total/NA Solid Moisture 160-3235-10 L100825BUB00 Total/NA Solid Moisture 160-3235-11 L100826BUB00 Total/NA Solid Moisture 160-3235-12 L100827BUB00 Total/NA Solid Moisture 160-3235-13 L100828BUB00 Total/NA Solid Moisture 160-3235-13 DU L100828BUB00 Total/NA Rad Prep Batch: 64842 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3235-1 L100816BUB00 Total/NA Solid None 160-3235-1 MS L100816BUB00 Total/NA Solid None 160-3235-1 MSD L100816BUB00 Total/NA Solid None 160-3235-2 L100817BUB00 Total/NA Solid None 160-3235-3 L100818BUB00 Total/NA Solid None 160-3235-4 L100819BUB00 Total/NA Solid None 160-3235-5 L100820BUB00 Total/NA Solid None 160-3235-6 L100821BUB00 Total/NA Solid None 160-3235-7 L100822BUB00 Total/NA Solid None 160-3235-8 L100823BUB00 Total/NA Solid None 160-3235-9 L100824BUB00 Total/NA Solid None 160-3235-10 L100825BUB00 Total/NA Solid None 160-3235-11 L100826BUB00 Total/NA Solid None 160-3235-12 L100827BUB00 Total/NA Solid None 160-3235-13 L100828BUB00 Total/NA Solid None LCS 160-64842/2-A Lab Control Sample Total/NA Solid None MB 160-64842/1-A Method Blank Total/NA Leach Batch: 65001 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3235-1 L100816BUB00 Total/NA Solid Dry and Grind 160-3235-1 DU L100816BUB00 Total/NA Solid Dry and Grind 160-3235-2 L100817BUB00 Total/NA Solid Dry and Grind 160-3235-3 L100818BUB00 Total/NA Solid Dry and Grind 160-3235-4 L100819BUB00 Total/NA Solid Dry and Grind 160-3235-5 L100820BUB00 Total/NA Solid Dry and Grind 160-3235-6 L100821BUB00 Total/NA Solid Dry and Grind 160-3235-7 L100822BUB00 Total/NA Solid Dry and Grind 160-3235-8 L100823BUB00 Total/NA Solid Dry and Grind 160-3235-9 L100824BUB00 Total/NA Solid Dry and Grind 160-3235-10 L100825BUB00 Total/NA Solid Dry and Grind 160-3235-11 L100826BUB00 Total/NA Solid Dry and Grind 160-3235-12 L100827BUB00 Total/NA Solid Dry and Grind 160-3235-13 L100828BUB00 Total/NA TestAmerica St. Louis Page 25 of 27 1

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QC Association Summary TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Rad (Continued)

Prep Batch: 65535 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 65001 160-3235-1 L100816BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-1 DU L100816BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-2 L100817BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-3 L100818BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-4 L100819BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-5 L100820BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-6 L100821BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-7 L100822BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-8 L100823BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-9 L100824BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-10 L100825BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-11 L100826BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-12 L100827BUB00 Total/NA Solid Fill_Geo-0 65001 160-3235-13 L100828BUB00 Total/NA Solid Fill_Geo-0 LCS 160-65535/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-65535/1-A Method Blank Total/NA TestAmerica St. Louis Page 26 of 27 1

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Tracer/Carrier Summary TestAmerica Job ID: 160-3235-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)

Re 103 160-3235-1 Percent Yield (Acceptance Limits)

L100816BUB00 101 160-3235-1 MS L100816BUB00 102 160-3235-1 MSD L100816BUB00 71 160-3235-2 L100817BUB00 64 160-3235-3 L100818BUB00 65 160-3235-4 L100819BUB00 67 160-3235-5 L100820BUB00 73 160-3235-6 L100821BUB00 80 160-3235-7 L100822BUB00 76 160-3235-8 L100823BUB00 67 160-3235-9 L100824BUB00 56 160-3235-10 L100825BUB00 83 160-3235-11 L100826BUB00 71 160-3235-12 L100827BUB00 58 160-3235-13 L100828BUB00 107 LCS 160-64842/2-A Lab Control Sample 72 MB 160-64842/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 27 of 27 1

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