ML18010A293

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Final Status Survey Final Report Volume 3, Chapter 6, Survey Area Release Record for Land Survey Area 10, Analytical Report: 160-4745-1
ML18010A293
Person / Time
Site: 07000036
Issue date: 01/13/2014
From: Swanson M, Vania I
TestAmerica Labs - St. Louis, Westinghouse
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML18010A247 List: ... further results
References
HEM-17-72 160-4745-1
Download: ML18010A293 (18)
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-4745-1 Client Project/Site: RFP-CBA-022 (21 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

1/13/2014 4:43:29 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

TestAmerica Job ID: 160-4745-1 Page 2 of 18 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

4 Receipt Checklists.........................................

6 Definitions/Glossary.......................................

7 Method Summary.........................................

8 Sample Summary.........................................

9 Client Sample Results......................................

10 QC Sample Results........................................

17 QC Association Summary...................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-4745-1 Project/Site: RFP-CBA-022 (21 DAY TAT)

Job ID: 160-4745-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (21 DAY TAT)

Report Number: 160-4745-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 12/03/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 20.0 C.

RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)

Samples L100701BUB00 (160-4745-1), L100702BES00 (160-4745-2), L100703BSS00 (160-4745-3), L100704BRQ00 (160-4745-4),

L100704BRS00 (160-4745-5), L100705BES00 (160-4745-6), L100706BRS00 (160-4745-7), L100707BES00 (160-4745-8),

L100708BES00 (160-4745-9), L100709BRS00 (160-4745-10), L100710BES00 (160-4745-11), L100711BRS00 (160-4745-12),

L100712BES00 (160-4745-13), L100713BRS00 (160-4745-14) and L100714BES00 (160-4745-15) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 12/17/2013, prepared on 12/19/2013 and analyzed on 01/10/2014.

No other difficulties were encountered during the Radium 226 analysis. All other quality control parameters were within the acceptance limits.

TestAmerica St. Louis Page 3 of 18 1

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revisioi:i: 3 I

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Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain ofCutody ID No.

F-120213-01 Pa!!e 1/2 Reauested Analysis Laboratorv Name:

Project Name:

Co TA-MO Westinghouse Electric Company N

c--;

ro Contact Person:

~

Laboratory Address:

Gerald Rood

<8 1371 5 Rider Trail North l'.,

2 i::

Phone Number:

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  • .;; Phone No.

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314-810-3382

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0 314-298-8566 u

t Sampler Name ro

,; Laboratory Contact Person:

-0 15 Scott Jenkins

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a f-- Joe Walker

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Phone No.

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0 CC) ro Q) 708-870-8453 0

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0 ro Remarks u

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~ f-0 Ll00701BUBOO 11/20/2013 9:45 s C

X X

I L<..A. 10'07 E,~

L 100702BES00 11/26/2013 16:00 s C

X X

1 L.$1:>.

10-07 Svs..

L 100703BSSOO 11/27/2013 14:30 s C

X X

1 I <A to-()7 Svs L100704BRQOO 11/27/2013 14:50 s C

X X

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[0,01 (') (_

LI 00704BRS00 11/27/2013 14:50 s C

X X 1

L C.. h.

, r,-ol Jy_j L100705BESOO 11/26/2013 15:50 s C

X X

1

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L 100706BRSOO I 1/27/2013 14:10 s C

X X

1 LI 00707BES00 11/27/2013 14:15 s C

X X

1 LI 00708BESOO 11/27/2013 10:00 s C

X X

1 LI 00709BRSOO 11/26/2013 15:30 s C

X X

I LI 0071 OBESOO 11/26/2013 15:35 s C

X X

I

.* y LI0071 IBRSOO 11/27/2013 10:20 s C

X X

1 LSA

[() '0} Sv.s Relinquished bye_:-

Date/Time Receiv~

y:../1/J_

Date/Time Total Cooler Temperature:

,.2_,,3... 1.3 i;.7,,,..,.__' :.£.,,.,

  • --., 1 (7:',~ 1ooS Vi Amhie,nt Company Namtt) £L-

~ ;e;cany ~~ck Cooler ID: Shipper and Number:

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Received by:

Date/Time

~~he~£ Date/Time Comments: Please analyze samples for Tc-99 on a 7 TAT.

(~*\\~.}tJ Please analyze samples for Gamma Spec after a 2 I day ingrowth Company Name:

, Company Name:

period.

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Relinquished by:

Date/Time

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/U Date/Time r:>-o>43 Verified By:

Company Name:

C~anyName:

C rf;"".*ro r* ~CG.d<

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision: 3 1

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Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain ofCutodv ID No.

F-120213-01 Pa2e 2/2 Requested Analysis Laboratorv Name:

Project Name:

G' TA-MO Westinghouse Electric Company N

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Contact Person:

i::::::

Laboratory Address:

Gerald Rood

<8 13715 Rider Trail North

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Scott Jenkins 8

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Phone No.

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708-870-8453

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Remarks u

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0 L1007I2BESOO 11/27/2013 10:25 s C

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/1"'1-0/ Svs Ll00713BRSOO 11/27/2013 10:50 s C

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L1007I4BESOO 11/27/2013 11:00 s C

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Date/Time Total Cooler Temperature:

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Date/Time

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1£ompanyN~

period.

V "CT ".,-c~-;{t:,:

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Date/Time

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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-4745-1 Login Number: 4745 Question Answer Comment Creator: Daniels, Brian J List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Qualifiers Rad Qualifier Description U

Indicates the analyte was analyzed for but not detected.

Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 18 1

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Sample Summary TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-4745-1 L100701BUB00 Solid 11/20/13 09:45 12/03/13 18:10 160-4745-2 L100702BES00 Solid 11/26/13 16:00 12/03/13 18:10 160-4745-3 L100703BSS00 Solid 11/27/13 14:30 12/03/13 18:10 160-4745-4 L100704BRQ00 Solid 11/27/13 14:50 12/03/13 18:10 160-4745-5 L100704BRS00 Solid 11/27/13 14:50 12/03/13 18:10 160-4745-6 L100705BES00 Solid 11/26/13 15:50 12/03/13 18:10 160-4745-7 L100706BRS00 Solid 11/27/13 14:10 12/03/13 18:10 160-4745-8 L100707BES00 Solid 11/27/13 14:15 12/03/13 18:10 160-4745-9 L100708BES00 Solid 11/27/13 10:00 12/03/13 18:10 160-4745-10 L100709BRS00 Solid 11/26/13 15:30 12/03/13 18:10 160-4745-11 L100710BES00 Solid 11/26/13 15:35 12/03/13 18:10 160-4745-12 L100711BRS00 Solid 11/27/13 10:20 12/03/13 18:10 160-4745-13 L100712BES00 Solid 11/27/13 10:25 12/03/13 18:10 160-4745-14 L100713BRS00 Solid 11/27/13 10:50 12/03/13 18:10 160-4745-15 L100714BES00 Solid 11/27/13 11:00 12/03/13 18:10 TestAmerica St. Louis Page 9 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-4745-1 Client Sample ID: L100701BUB00 Matrix: Solid Date Collected: 11/20/13 09:45 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.20 (2+/-)

0.206 (2+/-)

1 01/10/14 12:44 12/19/13 12:55 pCi/g 0.0955 RL MDC 0.166 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 12:44 1

0.470 0.589 0.559 1.79 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 12:44 1

0.0893 0.201 0.141 1.39 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 12:44 1

0.0821 0.184 0.0932 1.22 Lead 212 pCi/g 12/19/13 12:55 01/10/14 12:44 1

0.100 0.196 0.125 1.46 Lead 214 pCi/g 12/19/13 12:55 01/10/14 12:44 1

0.317 2.48 1.42 19.9 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 12:44 1

1.51 0.358 0.350 U

0.666 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 12:44 1

0.0893 1.00 0.201 0.141 1.39 Radium 226 pCi/g 12/19/13 12:55 01/10/14 12:44 1

0.0955 0.206 0.166 1.20 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 12:44 1

1.96 1.17 1.11 3.35 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 12:44 1

0.568 3.32 0.767 31.8 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 12:44 1

0.248 0.779 0.779 U

-0.00577 Americium 241 pCi/g 12/19/13 12:55 01/10/14 12:44 1

8.50 1.57 1.57 U

0.000 Protactinium 234m Lab Sample ID: 160-4745-2 Client Sample ID: L100702BES00 Matrix: Solid Date Collected: 11/26/13 16:00 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.198 (2+/-)

1 01/10/14 12:45 12/19/13 12:55 pCi/g 0.187 RL MDC 0.164 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 12:45 1

0.539 0.451 0.431 1.28 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 12:45 1

0.0883 0.179 0.133 1.15 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 12:45 1

0.0773 0.175 0.0895 1.16 Lead 212 pCi/g 12/19/13 12:55 01/10/14 12:45 1

0.107 0.164 0.106 1.21 Lead 214 pCi/g 12/19/13 12:55 01/10/14 12:45 1

0.524 2.30 1.42 17.7 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 12:45 1

1.57 0.336 0.328 U

0.670 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 12:45 1

0.0883 1.00 0.179 0.133 1.15 Radium 226 pCi/g 12/19/13 12:55 01/10/14 12:45 1

0.187 0.198 0.164 1.09 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 12:45 1

0.982 0.798 0.779 1.64 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 12:45 1

0.295 0.150 0.149 U

0.120 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 12:45 1

0.132 0.0788 0.0788 U

-0.0233 Americium 241 pCi/g 12/19/13 12:55 01/10/14 12:45 1

7.38 4.22 4.22 U

1.05 Protactinium 234m Lab Sample ID: 160-4745-3 Client Sample ID: L100703BSS00 Matrix: Solid Date Collected: 11/27/13 14:30 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.160 (2+/-)

1 01/10/14 12:46 12/19/13 12:55 pCi/g 0.0831 RL MDC 0.115 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 12:46 1

0.310 0.418 0.387 1.51 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 12:46 1

0.0643 0.151 0.102 1.08 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 12:46 1

0.0550 0.152 0.0705 1.04 Lead 212 TestAmerica St. Louis Page 10 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-4745-3 Client Sample ID: L100703BSS00 Matrix: Solid Date Collected: 11/27/13 14:30 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.23 (2+/-)

0.158 (2+/-)

1 01/10/14 12:46 12/19/13 12:55 pCi/g 0.0616 RL MDC 0.0929 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 12:46 1

0.376 2.21 1.16 18.4 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 12:46 1

1.02 0.221 0.217 U

0.368 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 12:46 1

0.0643 1.00 0.151 0.102 1.08 Radium 226 pCi/g 12/19/13 12:55 01/10/14 12:46 1

0.0831 0.160 0.115 1.09 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 12:46 1

0.833 0.652 0.631 1.56 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 12:46 1

0.184 0.146 0.145 0.204 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 12:46 1

0.109 0.0653 0.0652 U

-0.0152 Americium 241 pCi/g 12/19/13 12:55 01/10/14 12:46 1

5.37 2.67 2.63 U

4.52 Protactinium 234m Lab Sample ID: 160-4745-4 Client Sample ID: L100704BRQ00 Matrix: Solid Date Collected: 11/27/13 14:50 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.08 (2+/-)

0.195 (2+/-)

1 01/10/14 12:48 12/19/13 12:55 pCi/g 0.169 RL MDC 0.161 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 12:48 1

0.419 0.497 0.470 1.55 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 12:48 1

0.0784 0.178 0.130 1.16 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 12:48 1

0.0745 0.172 0.0895 1.13 Lead 212 pCi/g 12/19/13 12:55 01/10/14 12:48 1

0.104 0.195 0.134 1.36 Lead 214 pCi/g 12/19/13 12:55 01/10/14 12:48 1

0.602 2.51 1.56 19.2 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 12:48 1

1.44 0.475 0.467 U

0.832 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 12:48 1

0.0784 1.00 0.178 0.130 1.16 Radium 226 pCi/g 12/19/13 12:55 01/10/14 12:48 1

0.169 0.195 0.161 1.08 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 12:48 1

1.26 0.398 0.389 U

0.806 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 12:48 1

0.294 0.166 0.166 U

0.0729 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 12:48 1

0.127 0.0757 0.0757 U

0.0213 Americium 241 pCi/g 12/19/13 12:55 01/10/14 12:48 1

8.78 4.93 4.93 U

-0.153 Protactinium 234m Lab Sample ID: 160-4745-5 Client Sample ID: L100704BRS00 Matrix: Solid Date Collected: 11/27/13 14:50 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.11 (2+/-)

0.167 (2+/-)

1 01/10/14 14:40 12/19/13 12:55 pCi/g 0.117 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 14:40 1

0.427 0.469 0.452 1.17 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 14:40 1

0.0694 0.143 0.0923 1.05 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 14:40 1

0.0533 0.168 0.0716 1.17 Lead 212 pCi/g 12/19/13 12:55 01/10/14 14:40 1

0.0756 0.166 0.104 1.25 Lead 214 pCi/g 12/19/13 12:55 01/10/14 14:40 1

0.256 2.25 1.09 19.2 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 14:40 1

1.17 0.304 0.298 U

0.544 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 14:40 1

0.0694 1.00 0.143 0.0923 1.05 Radium 226 TestAmerica St. Louis Page 11 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-4745-5 Client Sample ID: L100704BRS00 Matrix: Solid Date Collected: 11/27/13 14:50 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 1.11 (2+/-)

0.167 (2+/-)

1 01/10/14 14:40 12/19/13 12:55 pCi/g 0.117 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 14:40 1

0.778 0.317 0.303 0.907 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 14:40 1

0.196 0.154 0.152 0.220 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 14:40 1

0.108 0.0640 0.0640 U

-0.000114 Americium 241 pCi/g 12/19/13 12:55 01/10/14 14:40 1

4.83 3.19 3.16 U

3.67 Protactinium 234m Lab Sample ID: 160-4745-6 Client Sample ID: L100705BES00 Matrix: Solid Date Collected: 11/26/13 15:50 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.975 (2+/-)

0.190 (2+/-)

1 01/10/14 14:41 12/19/13 12:55 pCi/g 0.125 RL MDC 0.162 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 14:41 1

0.273 0.364 0.338 1.30 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 14:41 1

0.0951 0.140 0.0961 0.982 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 14:41 1

0.0729 0.151 0.0729 1.02 Lead 212 pCi/g 12/19/13 12:55 01/10/14 14:41 1

0.0769 0.171 0.102 1.33 Lead 214 pCi/g 12/19/13 12:55 01/10/14 14:41 1

0.331 2.44 1.15 21.0 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 14:41 1

1.06 0.287 0.281 U

0.553 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 14:41 1

0.0951 1.00 0.140 0.0961 0.982 Radium 226 pCi/g 12/19/13 12:55 01/10/14 14:41 1

0.125 0.190 0.162 0.975 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 14:41 1

0.936 0.813 0.785 2.03 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 14:41 1

0.217 0.148 0.139 0.496 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 14:41 1

0.100 0.0594 0.0594 U

-0.00733 Americium 241 pCi/g 12/19/13 12:55 01/10/14 14:41 1

4.52 3.17 3.08 7.33 Protactinium 234m Lab Sample ID: 160-4745-7 Client Sample ID: L100706BRS00 Matrix: Solid Date Collected: 11/27/13 14:10 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.26 (2+/-)

0.207 (2+/-)

1 01/10/14 14:36 12/19/13 12:55 pCi/g 0.0758 RL MDC 0.162 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 14:36 1

0.521 0.455 0.431 1.42 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 14:36 1

0.0891 0.192 0.136 1.31 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 14:36 1

0.0698 0.178 0.0876 1.20 Lead 212 pCi/g 12/19/13 12:55 01/10/14 14:36 1

0.0995 0.185 0.113 1.41 Lead 214 pCi/g 12/19/13 12:55 01/10/14 14:36 1

0.406 2.58 1.45 20.9 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 14:36 1

0.705 0.393 0.392 U

0.323 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 14:36 1

0.0891 1.00 0.192 0.136 1.31 Radium 226 pCi/g 12/19/13 12:55 01/10/14 14:36 1

0.0758 0.207 0.162 1.26 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 14:36 1

0.960 0.367 0.355 U

0.917 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 14:36 1

0.219 0.140 0.140 U

0.134 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 14:36 1

0.119 0.118 0.118 U

-0.0325 Americium 241 TestAmerica St. Louis Page 12 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-4745-7 Client Sample ID: L100706BRS00 Matrix: Solid Date Collected: 11/27/13 14:10 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Protactinium 234m 2.59 U

(2+/-)

3.97 (2+/-)

1 01/10/14 14:36 12/19/13 12:55 pCi/g 6.62 RL MDC 3.96 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Lab Sample ID: 160-4745-8 Client Sample ID: L100707BES00 Matrix: Solid Date Collected: 11/27/13 14:15 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.29 (2+/-)

0.288 (2+/-)

1 01/10/14 14:37 12/19/13 12:55 pCi/g 0.198 RL MDC 0.256 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 14:37 1

0.504 0.695 0.656 2.21 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 14:37 1

0.114 0.230 0.174 1.44 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 14:37 1

0.0906 0.188 0.103 1.22 Lead 212 pCi/g 12/19/13 12:55 01/10/14 14:37 1

0.112 0.203 0.137 1.44 Lead 214 pCi/g 12/19/13 12:55 01/10/14 14:37 1

0.366 2.59 1.60 19.9 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 14:37 1

1.32 0.783 0.782 U

0.386 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 14:37 1

0.114 1.00 0.230 0.174 1.44 Radium 226 pCi/g 12/19/13 12:55 01/10/14 14:37 1

0.198 0.288 0.256 1.29 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 14:37 1

1.03 0.399 0.388 U

0.899 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 14:37 1

0.352 0.199 0.198 U

0.138 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 14:37 1

0.152 0.0927 0.0924 U

-0.0719 Americium 241 pCi/g 12/19/13 12:55 01/10/14 14:37 1

8.47 4.70 4.70 U

0.246 Protactinium 234m Lab Sample ID: 160-4745-9 Client Sample ID: L100708BES00 Matrix: Solid Date Collected: 11/27/13 10:00 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.14 (2+/-)

0.188 (2+/-)

1 01/10/14 16:26 12/19/13 12:55 pCi/g 0.0783 RL MDC 0.148 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 16:26 1

0.540 0.373 0.366 0.709 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 16:26 1

0.0994 0.151 0.108 1.01 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 16:26 1

0.0665 0.173 0.0813 1.18 Lead 212 pCi/g 12/19/13 12:55 01/10/14 16:26 1

0.0826 0.175 0.104 1.36 Lead 214 pCi/g 12/19/13 12:55 01/10/14 16:26 1

0.380 2.41 1.26 20.1 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 16:26 1

1.34 0.263 0.259 U

0.452 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 16:26 1

0.0994 1.00 0.151 0.108 1.01 Radium 226 pCi/g 12/19/13 12:55 01/10/14 16:26 1

0.0783 0.188 0.148 1.14 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 16:26 1

1.01 0.866 0.843 1.88 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 16:26 1

0.278 0.169 0.168 U

0.125 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 16:26 1

0.118 0.0701 0.0701 U

-0.0133 Americium 241 pCi/g 12/19/13 12:55 01/10/14 16:26 1

6.54 18.1 18.1 U

-0.541 Protactinium 234m TestAmerica St. Louis Page 13 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-4745-10 Client Sample ID: L100709BRS00 Matrix: Solid Date Collected: 11/26/13 15:30 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.32 (2+/-)

0.198 (2+/-)

1 01/10/14 16:27 12/19/13 12:55 pCi/g 0.0804 RL MDC 0.145 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 16:27 1

0.410 0.506 0.478 1.60 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 16:27 1

0.0788 0.169 0.117 1.18 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 16:27 1

0.0897 0.169 0.0873 1.12 Lead 212 pCi/g 12/19/13 12:55 01/10/14 16:27 1

0.0839 0.181 0.117 1.32 Lead 214 pCi/g 12/19/13 12:55 01/10/14 16:27 1

0.407 2.53 1.30 21.2 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 16:27 1

1.34 0.191 0.189 U

0.217 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 16:27 1

0.0788 1.00 0.169 0.117 1.18 Radium 226 pCi/g 12/19/13 12:55 01/10/14 16:27 1

0.0804 0.198 0.145 1.32 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 16:27 1

1.04 0.840 0.829 1.30 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 16:27 1

0.292 0.0315 0.0315 U

-0.00449 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 16:27 1

0.0887 0.0523 0.0523 U

0.00888 Americium 241 pCi/g 12/19/13 12:55 01/10/14 16:27 1

6.16 3.41 3.41 U

0.997 Protactinium 234m Lab Sample ID: 160-4745-11 Client Sample ID: L100710BES00 Matrix: Solid Date Collected: 11/26/13 15:35 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.17 (2+/-)

0.179 (2+/-)

1 01/10/14 16:28 12/19/13 12:55 pCi/g 0.111 RL MDC 0.134 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 16:28 1

0.373 0.436 0.413 1.33 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 16:28 1

0.0869 0.188 0.132 1.28 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 16:28 1

0.0604 0.167 0.0787 1.14 Lead 212 pCi/g 12/19/13 12:55 01/10/14 16:28 1

0.0837 0.175 0.109 1.33 Lead 214 pCi/g 12/19/13 12:55 01/10/14 16:28 1

0.265 2.34 1.27 19.2 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 16:28 1

1.33 0.814 0.811 U

-0.668 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 16:28 1

0.0869 1.00 0.188 0.132 1.28 Radium 226 pCi/g 12/19/13 12:55 01/10/14 16:28 1

0.111 0.179 0.134 1.17 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 16:28 1

1.04 0.649 0.639 1.06 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 16:28 1

0.282 0.0970 0.0966 U

0.0885 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 16:28 1

0.100 0.0756 0.0754 U

0.0486 Americium 241 pCi/g 12/19/13 12:55 01/10/14 16:28 1

5.53 2.82 2.82 U

0.686 Protactinium 234m Lab Sample ID: 160-4745-12 Client Sample ID: L100711BRS00 Matrix: Solid Date Collected: 11/27/13 10:20 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.07 (2+/-)

0.193 (2+/-)

1 01/10/14 16:29 12/19/13 12:55 pCi/g 0.111 RL MDC 0.159 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 16:29 1

0.619 0.420 0.413 0.732 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 16:29 1

0.0682 0.159 0.113 1.07 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 16:29 1

0.0723 0.160 0.0815 1.06 Lead 212 TestAmerica St. Louis Page 14 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-4745-12 Client Sample ID: L100711BRS00 Matrix: Solid Date Collected: 11/27/13 10:20 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.32 (2+/-)

0.179 (2+/-)

1 01/10/14 16:29 12/19/13 12:55 pCi/g 0.0743 RL MDC 0.115 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 16:29 1

0.515 2.14 1.30 16.6 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 16:29 1

1.29 0.404 0.399 U

0.600 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 16:29 1

0.0682 1.00 0.159 0.113 1.07 Radium 226 pCi/g 12/19/13 12:55 01/10/14 16:29 1

0.111 0.193 0.159 1.07 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 16:29 1

0.801 0.321 0.311 U

0.744 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 16:29 1

0.212 0.132 0.131 U

0.125 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 16:29 1

0.117 0.0703 0.0702 U

-0.0228 Americium 241 pCi/g 12/19/13 12:55 01/10/14 16:29 1

6.06 3.35 3.31 U

5.11 Protactinium 234m Lab Sample ID: 160-4745-13 Client Sample ID: L100712BES00 Matrix: Solid Date Collected: 11/27/13 10:25 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.16 (2+/-)

0.197 (2+/-)

1 01/10/14 16:30 12/19/13 12:55 pCi/g 0.128 RL MDC 0.158 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 16:30 1

0.317 0.395 0.365 1.46 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 16:30 1

0.0711 0.156 0.103 1.13 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 16:30 1

0.0686 0.171 0.0808 1.17 Lead 212 pCi/g 12/19/13 12:55 01/10/14 16:30 1

0.0922 0.167 0.0996 1.29 Lead 214 pCi/g 12/19/13 12:55 01/10/14 16:30 1

0.405 2.42 1.27 20.1 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 16:30 1

1.24 0.239 0.236 U

0.342 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 16:30 1

0.0711 1.00 0.156 0.103 1.13 Radium 226 pCi/g 12/19/13 12:55 01/10/14 16:30 1

0.128 0.197 0.158 1.16 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 16:30 1

0.874 0.627 0.616 1.15 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 16:30 1

0.268 0.155 0.154 U

0.144 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 16:30 1

0.116 0.0685 0.0685 U

0.00108 Americium 241 pCi/g 12/19/13 12:55 01/10/14 16:30 1

5.60 3.13 3.13 U

0.703 Protactinium 234m Lab Sample ID: 160-4745-14 Client Sample ID: L100713BRS00 Matrix: Solid Date Collected: 11/27/13 10:50 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.15 (2+/-)

0.197 (2+/-)

1 01/10/14 16:32 12/19/13 12:55 pCi/g 0.176 RL MDC 0.158 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 16:32 1

0.612 0.656 0.642 1.29 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 16:32 1

0.0958 0.191 0.145 1.19 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 16:32 1

0.0781 0.175 0.0925 1.15 Lead 212 pCi/g 12/19/13 12:55 01/10/14 16:32 1

0.0872 0.172 0.122 1.16 Lead 214 pCi/g 12/19/13 12:55 01/10/14 16:32 1

0.496 2.36 1.49 17.9 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 16:32 1

1.46 0.339 0.334 U

0.524 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 16:32 1

0.0958 1.00 0.191 0.145 1.19 Radium 226 TestAmerica St. Louis Page 15 of 18 1

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Client Sample Results TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Lab Sample ID: 160-4745-14 Client Sample ID: L100713BRS00 Matrix: Solid Date Collected: 11/27/13 10:50 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 1.15 (2+/-)

0.197 (2+/-)

1 01/10/14 16:32 12/19/13 12:55 pCi/g 0.176 RL MDC 0.158 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 16:32 1

1.07 0.863 0.846 1.64 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 16:32 1

0.246 0.151 0.150 U

0.139 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 16:32 1

0.117 0.0692 0.0692 U

-0.00932 Americium 241 pCi/g 12/19/13 12:55 01/10/14 16:32 1

7.49 4.28 4.28 U

1.33 Protactinium 234m Lab Sample ID: 160-4745-15 Client Sample ID: L100714BES00 Matrix: Solid Date Collected: 11/27/13 11:00 Date Received: 12/03/13 18:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 2.01 (2+/-)

0.339 (2+/-)

1 01/10/14 17:03 12/19/13 12:55 pCi/g 0.172 RL MDC 0.270 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 12/19/13 12:55 01/10/14 17:03 1

0.686 0.847 0.792 2.88 Bismuth 212 pCi/g 12/19/13 12:55 01/10/14 17:03 1

0.123 0.291 0.194 2.08 Bismuth 214 pCi/g 12/19/13 12:55 01/10/14 17:03 1

0.112 0.308 0.140 2.12 Lead 212 pCi/g 12/19/13 12:55 01/10/14 17:03 1

0.133 0.302 0.188 2.27 Lead 214 pCi/g 12/19/13 12:55 01/10/14 17:03 1

0.477 3.91 1.96 33.1 Potassium 40 pCi/g 12/19/13 12:55 01/10/14 17:03 1

2.08 0.709 0.694 U

1.34 Protactinium 231 pCi/g 12/19/13 12:55 01/10/14 17:03 1

0.123 1.00 0.291 0.194 2.08 Radium 226 pCi/g 12/19/13 12:55 01/10/14 17:03 1

0.172 0.339 0.270 2.01 Thorium 232 pCi/g 12/19/13 12:55 01/10/14 17:03 1

1.96 1.55 1.51 3.14 Thorium 234 pCi/g 12/19/13 12:55 01/10/14 17:03 1

0.494 0.281 0.280 U

0.262 Uranium 235 pCi/g 12/19/13 12:55 01/10/14 17:03 1

0.230 0.137 0.137 U

-0.0194 Americium 241 pCi/g 12/19/13 12:55 01/10/14 17:03 1

9.95 13.7 13.7 U

-0.548 Protactinium 234m TestAmerica St. Louis Page 16 of 18 1

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QC Sample Results TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-93355/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 97314 Prep Batch: 93355 Actinium 228 Analyte U

1 01/10/14 12:42 12/19/13 12:55 pCi/g 0.0500 MDC RL 0.0194 0.0193 (2+/-)

(2+/-)

MB 0.01730 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

01/10/14 12:42 12/19/13 12:55 pCi/g 0.227 0.0219 0.0219 U

0.0000 Bismuth 212 1

01/10/14 12:42 12/19/13 12:55 pCi/g 0.0386 0.0177 0.0177 U

0.002622 Bismuth 214 1

01/10/14 12:42 12/19/13 12:55 pCi/g 0.0273 0.0160 0.0160 U

-0.0008681 Lead 212 1

01/10/14 12:42 12/19/13 12:55 pCi/g 0.0364 0.0672 0.0672 U

-0.01201 Lead 214 1

01/10/14 12:42 12/19/13 12:55 pCi/g 0.304 0.153 0.153 U

-0.007341 Potassium 40 1

01/10/14 12:42 12/19/13 12:55 pCi/g 0.323 0.0386 0.0386 U

0.01680 Protactinium 231 1

01/10/14 12:42 12/19/13 12:55 pCi/g 0.0386 1.00 0.0177 0.0177 U

0.002622 Radium 226 1

01/10/14 12:42 12/19/13 12:55 pCi/g 0.0500 0.0194 0.0193 U

0.01730 Thorium 232 1

01/10/14 12:42 12/19/13 12:55 pCi/g 0.259 0.171 0.171 U

-0.02474 Thorium 234 1

01/10/14 12:42 12/19/13 12:55 pCi/g 0.0639 0.0307 0.0307 U

0.01620 Uranium 235 1

01/10/14 12:42 12/19/13 12:55 pCi/g 0.0201 0.0113 0.0113 U

0.003283 Americium 241 1

01/10/14 12:42 12/19/13 12:55 pCi/g 3.40 24.1 24.1 U

-0.6016 Protactinium 234m Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-93355/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 97316 Prep Batch: 93355 Americium 241 Analyte 116 87 97 97.60 101 10.2 0.530 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 35.9 33.91 3.55 0.165 pCi/g 95 87 - 120 Cobalt 60 42.5 39.54 3.98 0.148 pCi/g 93 87 - 115 Client Sample ID: L100702BES00 Lab Sample ID: 160-4745-2 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 97307 Prep Batch: 93355 Actinium 228 Analyte 1

0.40 1.256 1.09 0.222 0.142 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.28 1.862 0.635 0.493 pCi/g 0.53 1

Bismuth 214 1.15 1.186 0.181 0.0793 pCi/g 0.11 1

Lead 212 1.16 1.231 0.185 0.0796 pCi/g 0.20 1

Lead 214 1.21 1.377 0.196 0.106 pCi/g 0.47 1

Potassium 40 17.7 20.08 2.55 0.344 pCi/g 0.49 1

Protactinium 231 0.670 U

1.223 0.500 0.872 pCi/g 0.66 1

Radium 226 1.15 1.186 0.181 1.00 0.0793 pCi/g 0.11 1

Thorium 232 1.09 1.256 0.222 0.142 pCi/g 0.40 1

Thorium 234 1.64 1.438 0.799 1.05 pCi/g 0.13 1

Uranium 235 0.120 U

0.08798 U

0.171 0.307 pCi/g 0.1 1

Americium 241

-0.0233 U

-0.01141 U

0.0799 0.134 pCi/g 0.08 1

Protactinium 234m 1.05 U

0.1095 U

4.72 8.44 pCi/g 0.11 1

TestAmerica St. Louis Page 17 of 18 1

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QC Association Summary TestAmerica Job ID: 160-4745-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (21 DAY TAT)

Rad Leach Batch: 92616 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-4745-1 L100701BUB00 Total/NA Solid Dry and Grind 160-4745-2 L100702BES00 Total/NA Solid Dry and Grind 160-4745-2 DU L100702BES00 Total/NA Solid Dry and Grind 160-4745-3 L100703BSS00 Total/NA Solid Dry and Grind 160-4745-4 L100704BRQ00 Total/NA Solid Dry and Grind 160-4745-5 L100704BRS00 Total/NA Solid Dry and Grind 160-4745-6 L100705BES00 Total/NA Solid Dry and Grind 160-4745-7 L100706BRS00 Total/NA Solid Dry and Grind 160-4745-8 L100707BES00 Total/NA Solid Dry and Grind 160-4745-9 L100708BES00 Total/NA Solid Dry and Grind 160-4745-10 L100709BRS00 Total/NA Solid Dry and Grind 160-4745-11 L100710BES00 Total/NA Solid Dry and Grind 160-4745-12 L100711BRS00 Total/NA Solid Dry and Grind 160-4745-13 L100712BES00 Total/NA Solid Dry and Grind 160-4745-14 L100713BRS00 Total/NA Solid Dry and Grind 160-4745-15 L100714BES00 Total/NA Prep Batch: 93355 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 92616 160-4745-1 L100701BUB00 Total/NA Solid Fill_Geo-21 92616 160-4745-2 L100702BES00 Total/NA Solid Fill_Geo-21 92616 160-4745-2 DU L100702BES00 Total/NA Solid Fill_Geo-21 92616 160-4745-3 L100703BSS00 Total/NA Solid Fill_Geo-21 92616 160-4745-4 L100704BRQ00 Total/NA Solid Fill_Geo-21 92616 160-4745-5 L100704BRS00 Total/NA Solid Fill_Geo-21 92616 160-4745-6 L100705BES00 Total/NA Solid Fill_Geo-21 92616 160-4745-7 L100706BRS00 Total/NA Solid Fill_Geo-21 92616 160-4745-8 L100707BES00 Total/NA Solid Fill_Geo-21 92616 160-4745-9 L100708BES00 Total/NA Solid Fill_Geo-21 92616 160-4745-10 L100709BRS00 Total/NA Solid Fill_Geo-21 92616 160-4745-11 L100710BES00 Total/NA Solid Fill_Geo-21 92616 160-4745-12 L100711BRS00 Total/NA Solid Fill_Geo-21 92616 160-4745-13 L100712BES00 Total/NA Solid Fill_Geo-21 92616 160-4745-14 L100713BRS00 Total/NA Solid Fill_Geo-21 92616 160-4745-15 L100714BES00 Total/NA Solid Fill_Geo-21 LCS 160-93355/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-93355/1-A Method Blank Total/NA TestAmerica St. Louis Page 18 of 18 1

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