ML16293A888

Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey Conducted in 2014, Rev. 0, Appendix F, Part 1 of 8

ML16293A888
Person / Time
Site:	West Valley Demonstration Project, P00M-032
Issue date:	08/22/2016
From:	MJW Technical Services
To:	Office of Nuclear Material Safety and Safeguards, State of NY, Energy Research & Development Authority, Office of Nuclear Reactor Regulation
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Appendix F -Analytical Results by Area Analytical Results by Area (Area 1)

Sample No. Type 1.1.C1 SAMPLE 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/29/2015 388092 1/18/2016 388092 1/11/2016 388092 12/29/2015 388092 1/18/2016 388092 1 /11/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 Parameter Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226

• Area 1 Fraction Method R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 711 OB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 931 O/SM 711 OB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 71108 Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R Result -0.598 12.6 0.143 25.5 0.236 0.740 3.64 0.011 0.0401 0.615 0.910 10.4 -0.936 0.740 0.777 0.121 0.0572 0.039 0.189 9.22 -0.0086 0.00955 14.3 0.00 0.00 0.599 0.814 0.182 0.150 -0.00744 0.00777 0.0456 -0.00312 0.522 0.646 0.878 0.946 9.80 9.18 0.00 0.00 0.599 0.814 Uncertainty GAS 0.511 14952-40-0 3.93 12587-46-1 0.176 3.89 0.678 0.216 0.256 0.0535 0.155 0.142 0.196 1.92 0.826 0.216 0.275 0.102 0.174 0.193 0.366 1.49 0.072 0.0883 1.24 0.409 1.04 0.112 0.159 0.0431 0.0613 0.0317 0.0336 0.0908 0.113 0.104 0.119 0.146 0.168 1.00 1.34 0.561 0.454 0.112 0.159 14234-35-6 12587-47-2 14913-49-6

14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 14952-40-0

12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 Units Lab Qua MDL CRDL CDilution 1% MoistL PCl/G U 0.703 1.00 32 PCl/G 3.89 4.00 1.00 32 PCl/G U PCl/G PCl/G U PCl/G PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G U PCl/G PCl/G PCl/G PCl/G U PCl/G U PCl/G U PCl/G PCl/G U PCl/G U PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G U PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G UI PCl/G PCl/G 0.346 1.00 32 3.57 10.0 1.00 32 1.33 1.00 32 0.200 1.00 32 0.108 0.100 1.00 32 0.112 1.00 32 0.316 1.00 32 0.155 1.00 32 0.403 1.00 32 0.958 1.27 0.200 0.308 0.0968 0.191 0.355 1.00 32 1.00 32 1.00 32 1.00 32 1.00 32 1.00 32 1.00 17.8 0.420 1.00 17.8 1.62 4.00 1.00 17.8 0.134 1.00 17.8 0.168 1.00 17.8 1.28 10.0 1.00 17.8 0.824 1.00 17.8 1.31 1.00 17.8 0.0966 1.00 17.8 0.119 1.00 17.8 0.0264 0.100 1.00 17.8 0.0615 0.100 1.00 17.8 0.0575 1.00 17.8 0.0701 1.00 17.8 0.180 1.00 17.8 0.220 1.00 17.8 . 0.106 1.00 17.8 0.0981 1.00 17.8 0.106 1.00 17.8 0.296 1.00 17.8 0.601 1.00 17.8 0.726 1.00 17.8 0.599 1.00 17.8 0.626 1.00 17.8 0.0966 1.00 17.8 0.119 1.00 17.8

• -.... Sample No. Type Analyzed SDG 1.1.C2 SAMPLE 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.R5 1.1.R5 1.1.R5 1.1.R5 1.1.R5 1.1.R5 1.1.R5 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE DUP DUP DUP DUP ' DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP SAMPLE SAMPLE SAMPLE SAMPLE 1/18/2016 388092 1 /11 /2016 387904 1 /5/2016 387904 1/11/2016 387904 1/5/2016 387904 SAMPLE 1/11/2016 387904 SAMPLE 1/11/2016 387904 SAMPLE 1/11/2016 387904 Parameter Radium-228

Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 Antimony-125 Antimony-125 Bismuth-212

Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Area 1 Fraction Method R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA901.1 R EPA 900.0/SW846 9310 R EPA901.1 R EPA 900.0/SW846 9310 R R R EPA901.1 EPA901.1 EPA901.1 Result 0.663 0.685 0.248 0.191 0.0313 0.00 -0.0874 0.128 -0.015 0.0514 0.00 0.454 0.670 0.776 0.174 0.153 -0.00795 0.0129 *0.00279 0.113 0.621 0.677. 0.749 1.11 10.9 9.98 0.0317 0.00 0.670 0.776 0.603 0.667 0.178 0.195 0.00 0.00 6.50 -2.57 -4.3 -1.44 42.3 0.00 0.00 Uncertainty CAS 0.230 15262-20-1 0.271 15262-20-1 0.0628 0.0609 0.0955 0.0805 0.193 0.273 0.0715 0.109 0.574 0.581 0.114 0.187 0.0601 0.0583 0.0282 0.041 0.0924 0.154 0.0829 0.136 0.119 0.206 1.05 1.34 0.440 0.633 0.114 0.187 0.199 0.195 0.0528 0.0797 0.0721 0.145 14913-50-9 14913-50-9 14952-40-0 14952-40-0 14234-35-6

'14234-35-6 14913-49-6

14913-49-6 14733-03-0

14733-03-0

10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 33.0 14952-40-0 1.15 12587-46-1 11.5 14234-35-6 2.11 12587-47-2 67.1 14.9 4.73 14913-49-6 14733-03-0 10045-97-3 Units Lab Qua MDL CRDL C Dilution I% MoistL PCl/G 0.169 1.00 17.8 PCl/G 0.223 1.00 17.8 PCl/G PCl/G PCl/G U PCl/G UI PCl/G U PCl/G U PCl/G U PCl/G U PCl/G UI PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G U PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/L U PCl/L U PCl/L U PCl/L U PCl/L U PCl/L UI PCl/L UI 0.0465 1.00 17.8 0.0636 1.00 17.8 0.130 1.00 17.8 0.0794 1.00 17.8 0.347 1.00 17.8 0.542 1.00 0 0.128 1.00 17.8 0.214 1.00 0 0.899 1.00 17.8 1.21 1.00 0 *0.0968 1.00 17.8 0.148 1.00 0 0.0528 0.100 1.00 17.8 0.075 0.100* 1.00 0 0.0531 1.00 17.8 0.0868 1.00 0 0:178 1.00 17.8 0.300 1.00 0 0.0771 1.00 17 .8 0.139 1.00 0 0.214 1.00 17.8 0.362 1.00 0 0.538 1.00 17.8 0.805 1.00 0 0.713 1.00 17.8 1.12 1.00 0 0.0968 1.00 17.8 0.148 1.00 0 0.223 1.00 17.8 0.242 1.00 0 0.0524 1.00 17 .8 0.0705 1.00 0 0.101 1.00 17.8 0.181 1.00 0 57.3 4.15 5.00 20.2 4.42 5.00 112 18.0 9.28 10.0 1.00 1.00 1.00 100 100 100 1.00 100 1.00 100 1.00 100 1.00 100 r* Sample No. Type 1-1 RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE Analyzed SDG 1/11/2016 387904 1/11/2016 387904 1/11/2016 387904 1 /11 /2016 387904 1/11/2016 387904 1/11/2016 387904 1/11/2016 387904 1/11/2016 387904 1/11/2016 387904 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/29/2015 388092 1/18/2016 388092 1/11/2016 388092 12/29/2015 388092 1/18/2016 388092 1/11/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 Parameter Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-228 Thallium-208 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Area 1 Fraction Method , R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 931 O/SM 711 OB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 711DB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 711DB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R

• Result 1.92 -1.34 6.21 0.00 -17 11.0 -2.9 0.00 1.19 -0.0837 7.52 0.0215 24.5 0.529 0.909 2.52 0.0114 -0.0436 0.621 0.926 11.7 0.537 0.909 0.595 0.246 -0.0136 0.035 0.017 6.53 0.033 0.00 17.0 0.00 0.557 0.605 0.730 0.139 0.143 0.0124 -0.00831 0.0494 -0.0202 0.715 Uncertainty GAS 3.80 10198-40-0 9.76 12.8 15.6 50.7 60.1 18.7 7.58 13.6 0.370 3.29 0.151 3.81 0.674 0.223 0.198 0.0405 0.133 0.130 0.244 1.50 0.730 0.223 0.287 0.090 0.166 0.176 0.253 1.68 0.0658 0.0944 1.45 0.523 0.587 0.126 0.170 0.0437 0.0636 0.030 0.0387 0.128 0.147 0.132 15585-10-1 15092-94-1 15067-28-4 13966-00-2

-14331-85-2 15262-20-1 14913-50-9 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1

15585-10-1 15092-94-1 Units Lab Qua MDL CRDL C Dilution I% Maish PCl/L PCl/L PCl/L PCl/L PCl/L u 7.60 1.00 100 u 18.1 1.00 100 u 14.9 1.00 100 UI 19.4 1.00 100 u 89.9 1.00 100 PCl/L U PCl/L U PCl/L UI PCl/L U PCl/G U PCl/G PCl/G U PCl/G PCl/G U PCl/G PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G U PCl/G PCl/G PCl/G PCl/G U PCl/G U PCl/G U PCl/G PCl/G U PCl/G

• UI PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G U PCl/G U PCl/G U PCl/G 104 1.00 100 31.4 1.00 100 5.45 1.00 100 15.6 1.00 100 0.680 1.00 24 3.92 4.00 1.00 24 0.281 1.00 24 3.69 10.0 1.00 24 1.36 1.00 24 0.201 1.00 24 0.102 0.100 1.00 24 0.0856 1.00 24 0.245 1.00 24 0.153 0.205 0.645 1.32 0.201 0.350 0.0946 0.262 0.343 0.495 2.29 4.00 0.128 0.200 1.69 10.0 0.852 1.22 0.0912 0.131 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 1.00 1.00 1.00 0.051 0.100 1.00 15.8 15.8 15.8 15.8 15.8 0.0815 0.100 1.00 15.8 0.0606 1.00 15.8 0.0741 1.00 15.8 0.180 1.00 15.8 0.276 1.00 15.8 0.0806 1.00 15.8 Sample No. Type 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1".3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 1.3.C2 1.3.C2 SAMPLE SAMPLE SAMPLE Analyzed SDG 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/29/2015 388092 1/18/2016 388092 1/11/2016 388092 12/29/2015 388092 1 /18/2016 388092 1/11/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 Parameter Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-210 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 . Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212

Bismuth-214 Bismuth-214 Area 1 Fraction Method R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4:5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R. DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW84!)

9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R R R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HAS.L 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.892 0.812 1.03 13.0 14.7 0.00 -0.189 0.605 0.730 0.456 0.932 0.226 0.185 0.00 0.0471 -0.0109 7.84 0.00 25.6 0.00 0.802 0.406 0.0075 0.165 3.71 0.879 0.930 14.3 0.00 0.802 1.03 0.369 0.00 -0.0784 0.166 11.1 0.0254 -0.0396 21.2 1.39 0.00 0.678 1.08 *Uncertainty CAS 0.126 15092-94-1 0.114 0.209 1.06 1.52 0.388 0.521 0.126 0.170 0.233 0.262 0.0531 0.080 0.107 0.140 0.316 3.45 0.152 3.77 1.08 0.242 0.144 0.0663 0.187 0.987 0.137 0.237 2.24 0.752 0.242 0.402 0.107 0.0942 0.231 0.311 2.15 0.0997 0.116 1.80 0.700 1.07 0.122 0.170 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2

14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 14255-04-0 15092-94-1 15067-28-4

13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6

14733-03-0 14733-03-0 Units Lab Qua MDL PCl/G 0.117 PCl/G 0.200 PCl/G 0.131 PCl/G 0.348 PCl/G 0.670 PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G U PCl/G U PCl/G PCl/G UI PCl/G PCl/G UI PCl/G PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G UI PCl/G U PCl/G U PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G UI PCl/G PCl/G 0.530 0.843 0.0912 0.131 0.159 0.295 0.0445 0.0679 0.129 0.161 0.586 3.97 0.314 3.05 2.21 0.194 0.109 0.136 0.429 0.993 0.156 0.222 0.904 1.33 0.194 0.434 0.104 0.106 0.413 0.595 2.78 0.166 0.203 2.19 0.852 1.59 0.114 0.152 CRDL C Dilution I% Moist( 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8

1.00 39.2 4.00 1.00 39.2 1.00 39.2 10.0 1.00* 39.2 1.00 39.2 1.00 39.2 0.100 1.00 39.2 1.00 39.2 1.00 39.2 4.00 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 21.6 1.00 21.6 4.00 1.00 21.6 1.00 21.6 1.00 21.6 10.0 1.00 21.6 1.00 21.6 1.00 21.6 1.00 21.6 1.00 21.6 Sample No. Type Analyzed SDG 1.3.C2 SAMPLE 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1.3.C2 SAMPLE 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE 1/18/2016 388092 12/3/2015 385101 12/2/2015 385101 11/24/2015 385101 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/3/2015 385101 12/4/2015 385101 12/3/2015 385101 12/3/2015 385101 SAMPLE 11/24/2015 3B5101 SAMPLE 11/24/2015 385101 SAMPLE 11/24/2015 385101 SAMPLE 12/3/2015 385101 SAMPLE 12/2/2015 385101 SAMPLE 12/3/2015 385101 SAMPLE 12/3/2015 385101 SAMPLE 11/23/2015 385101 SAMPLE 11/23/2015 385101 SAMPLE 11/23/2015 385101 SAMPLE 11/25/2015 385101 Parameter Cesium-137

Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228

Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Americium-241 BETA Bismuth-212 Bismuth-214 Carbon-14 Cesium-137 Cobalt-60 Curium-242 Curium-243/244 Curium-245/246 Europium-154 lodine-129 Lead-212 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Area 1.

• Fraction Method R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 931 O/SM 711 OB Modified.

R DOE EML HASL-300, Am-05-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R . R EPA EERF C-01 Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R R R R R R R R

R R R DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R ASTM C 1476-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified Result 0.405 0.482 0.0136 0.0129 -0.0175 0.0122 1.06 1.07 0.776 1.31 15.2 14.2 0.00 0.00 0.678 1.08 1.03 1.02 0.286 0.360 0.00 0.00 0.181 9.43 0.0173 0.0603 27.0 1.39 0.803 -0.459 0.481 -0.00427

-0.00457

-0.0119 0.0382 -0.0118 0.130 0.928 1.08 -0.146 -0.0042 0.0147 -1.82 Uncertainty CAS Units Lab Qua MDL CRDL CDilution I% MoistL 0.0678 10045-97-3 PCl/G 0.0658 0.100 1.00 21.6 0.0947 0.0426 0.0444 0.121 0.138 0.104 0.138 0.142 0.211 1.34 1.72 0.728 0.623 0.122 0.170 0.216 0.272 0.0695 0.0938 0.113 0.130 0.293 3.61 0.0593 0.109 3.46 0.906 0.169 *a.768 0.110 0.0412 0.0394 0.0359 0.0654 0.149 0.576 0.127 0.188 0.252 0.0363 0.0734 5.80 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1

15092-94-1

15067-28-4 15067-28-4 13966-00-2

13966-00-2 14331-85-2

14331-85-2

13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 12587-46-1

14596-10-2 14234-35-6 12587-47-2 14913-49-6 14733-03-0 14762-75-5 10045-97-3 10198-40-0 PCl/G PCl/G U PCl/G U PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G UI PCl/G U PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G U PCl/G PCl/G U OER-100-93 PCliG U PCl/G U PCl/G 15585-10-1 PCl/G U 15046-84-1 PCl/G U 15092-94-1 PCl/G 15067-28-4 PCl/G 13994-20-2 PCl/G U 13981-16-3 PCl/G U OER-100-70 PCl/G U 14119-32-5 PCl/G U 0.0637 0.100 1.00 21.6 0.0739 1.00 21.6 0.0907 1.00 21.6 0.217 1.00 21.6 0.268 1.00 21.6 0.0882 1.00 21.6 0.126 1.00 21.6 0.129 1.00 21.6 0.388 1.00 21.6 0.547 1.00 21.6 0.877 1.00 21.6 0.769 1.00 21.6 1.05 1.00 21.6 0.114 1.00 21.6 0.152 1.00 21.6 0.215 1.00 21.6 0.309 1.00 21.6 0.0568 1.00 21.6 0.0771 1.00 21.6 0.111 1.00 21.6 0.209 1.00 21.6 0.568 1.00 39.7 3.99 4.00 1.00 39.7 0.110 1.00 1.00 39.7 0.213 1.00 39. 7 2.52 10.0 1.00 39.7 1.12 1.00 39. 7 0.156 1.00 39.7 1.32 2.00 1.00 39. 7 0.0796 0.100 1.00 39.7 0.0788 1.00 39.7 0.0913 1.00 1.00 39.7 0.101 1.00 1.00 39.7 0.0573 1.00 1.00 39.7 0.277 1.00 39.7 0.928 1.00 1.00 39.7 0.112 1.00 39.7 0.384 1.00 39.7 0.714 1.00 1.00 39.7 0.084 1.00 1.00 39.7 0.147 1.00 1.00 39.7 10.1 15.0 1.00 39.7 I _J Sample No. Type 1.3.C5 SAMPLE 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.CS 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C6 . 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/2/2015 385101 11/29/2015 385101 12/3/2015 385101 11/24/2015 385101 11/24/2015 385101 11/24/2015 385101 11/24/2015 385101 12/3/2015 385101" 12/2/2015 385101 11/24/2015 385101 11/24/2015 385101 11/24/2015 385101 11/24/2015 385101 12/3/2015 385101 12/3/2015 385101 11/24/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/4/2015 385101 12/3/2015 385101 12/3/2015 385101 11/24/2015 385101 11/24/2015 385101 11/24/2015 385101 12/3/2015 385101 12/2/2015 12/3/2015 12/3/2015 385101 385101 385101 11/23/2015 385101 11/23/2015 385101 11/23/2015 385101 11/25/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/2/2015 385101 P_arameter Potassium-40 Protactinium-231 Radium-226 Radium-228 Strontium-90 Technetium-99 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232 Tin-126 Tritium Uranium-232 Uranium-233/234

Uranium-235/236 Uranium-238 Actinium-227 ALPHA. Americium-241 Antimony-125 BETA Bismuth-212 Bismuth-214 Carbon-14 Cesium-137 Cobalt-60 Curium-242 Curium-243/244

Curium-245/246 Europium-154 lodine-129 Lead-212 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Protactinium-231 Radium-226 Radium-228 Strontium-90 Area 1 Fraction Method R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified R DOE EML HASL-300, Tc-02-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE EML HASL-300, Th-01-RC Modified R DOE EML HASL-300, Th-01-RC Modified R DOE EML HASL-300, Th-01-RC Modified R DOE EML HASL-300, Th-01-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 906.0 Modified R DOE EML HASL-300, U-02-RC Modified R DOE EML HASL-300, U-02-RC Modified R DOE EML HASL-300, U-02-RC Modified R DOE EML HASL-300, U-02-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R . EPA 900.0/SW846 9310/SM 7110B Modified R DOE EML HASL-300, Am-05-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 931 O/SM 711 OB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA EERF C-01 Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE EML HASL-300, Am-05-RC Modified R DOE EML HASL-300, Am-05-RC Modified R DOE EML HASL-300, Am-05-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE EML HASL-300,1-01 Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R ASTM C 1476-00 Modified R DOE EML HASL-300, Pu-11-RC Modified R DOE EML HASL-300, Pu-11-RC Modified R DOE EML HASL-300, Pu-11-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Result 14.2 0.0888 0.803 0.665 -0.321 1.57 0.354 1.40 -0.0406 0.803 0.616 0.00 2.71 0.0644 0.656 0.0709 0.954 -0.478 7.80 0.0315 0.0263 18.3 0.725 1.08 -0.833 0.357 -0.0195 0.00 0.00921 0.0361 -0.00356 0.214 1.34 1.09 -0.0342 0.00979 0.00677 -2.07 13.9 0.801 1.08 0.892 -0.122 Uncertainty CAS Units .Lab Qua MDL CRDL C Dilution I% Moistt 1.66 13966-00-2 0.807 1.00 39.7 0.620 14331-85-2 PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G u 1.03 1.00 39.7 0.169 13982-63-3 0.382 15262-20-1 0.156 0.300 1.00 39.7 1.00 39.7 0.889 10098-97-2 u 1.76 2.00 5.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6. 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 2.00 14133-76-7 u 3.38 0.0817 0.595 0.122 0.444 0.381 0.163 . 2.71 0.127 0.320 0.121 0.367 0.464 3.22 0.062 0.202 2.99 1.19 0.289 0.891 0.122 0.0816 0.0412 0.0512 0.0709 0.241 0.383 0.197 0.363 0.236 0.0544 0.0799 6.40 2.27 0.980 0.289 0.403 0.659 14913-50-9 14274-82-9 15594-54-4 14269-63-7 7440-29-1 10028-17-8 14158-29-3 PCl/G U PCl/G PCl/G PCl/G UI PCl/G PCl/G U 13968-55-3/1391 PCl/G 15117-96-1/139:

PCl/G 7440-61-1 PCl/G 14952-40-0 PCl/G u 12587-46-1 . PCl/G 14596-10-2 PCl/G 14234-35-6

12587-47-2 14913-49-6 14733-03-0 14762-75-5 10045-97-3 PCl/G U PCl/G PCl/G U PCl/G PCl/G U PCl/G 10198-40-0 PCl/G U OER-100-93 PCl/G 15585-10-1 15046-84-1 15092-94-1 15067-28-4 PCl/G U PCl/G PCl/G U PCl/G U PCl/G PCl/G 13994-20-2 PCl/G U 13981-16-3 PCl/G U OER-100-70 PCl/G U 14119-32-5 PCl/G U 13966-00-2 14331-85-2

13982-63-3 15262-20-1 10098-97-2 PCl/G PCl/G U PCl/G PCl/G PCl/G U 0.0704 0.449 1.00 0.344 1.00 0.343 1.00 0.168 1.00 0.130 4.45 6.00 0.225 1.00 0.261 0.106 0.106 0.775 1.00 1.00 1.00 3.91 4.oo 0.0859 1.00 0.369 2.69 10.0 2.35 1.00 0.255 1.00 1.55 2.00 1.00 0.178 0.100 1.00 0.153 0.061.3 1.00 0.0981 1.00 0.0983 1.00 0.468 0.769 1.00 0.181 0.580 0.575 1.00 0.104 1.00 0.168 1.00 11.2 15.0 1.05 1.81 0.255 0.526 1.34 2.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00

-"

Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty CAS Units Lab Qua MDL CRDL CDilution 1% MoistL 1.3.C6 SAMPLE 11/29/2015 385101 Technetium-99 R DOE EML HASL-300, Tc-02-RC Modified 1.60 1.76 14133-76-7 PCl/G 2.95 5.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.381 0.168 14913-50-9 PCl/G 0.131 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-228 R DOE EML HASL-300, Th-01-RC Modified 0.984 0.482 14274-82-9 PCl/G 0.395 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-229 R DOE EML HASL-300, Th-01-RC Modified 0.131 0.207 15594-54-4 PCl/G 0.287 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-230 R DOE EML HASL-300, Th-01-RC Modified 1.16 0.498 14269-63-7 PCl/G 0.286 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-232 R DOE EML HASL-300, Th-01-RC Modified 0.979 0.452 7440-29-1 PCl/G 0.155 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.185 PCl/G UI 0.177 1.00 23.6 1.3.C6 SAMPLE 12/2/2015 385101 Tritium R EPA 906.0 Modified 1.95 2.00 10028-17-8 PCl/G 3.30 6.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-232 R DOE EML HASL-300, U-02-RC Modified 0.0473 0.121 14158-29-3 PCl/G u 0.222 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-233/234 R DOE EML HASL-300, U-02-RC Modified 0.799 0.301 13968-55-3/1391 PCl/G 0.214 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-235/236 R DOE EML HASL-300, U-02-RC Modified 0.0469 0.0921 15117-96-1/1391 PCl/G 0.128 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-238 R DOE EML HASL-300, U-02-RC Modified 1.14 0.345 7440-61-1 PCl/G 0.0796 1.00 1.00 23.6 1.3.C6 MSD 12/3/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 80.3 13.2 12587-46-1

% 5.73 4.00 1.00 23.6 1.3.C6 MSD 12/3/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 97.1 17.4 12587-47-2

% 5.68 10.0 1.00 23.6 1.3.C6 MS 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 96.6 16.0 12587-46-1

% 7.76 4.00 1.00 23.6 1.3.C6 MS 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 99.8 17.4 12587-47-2

% 6.22 10.0 1.00 23.6 1.3.C6 DUP 12/3/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 11.5 3.55 12587-46-1 PCl/G 3.63 4.00 1.00 23.6 1.3.C6 DUP 12/3/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 23.2 2.99 12587-47-2 PCl/G 2.17 10.0 1.00 23.6