Text

Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey Conducted in 2014, Rev. 0, Appendix F, Part 4 of 8
	ML16293A905
Person / Time
Site:	West Valley Demonstration Project, P00M-032
Issue date:	08/22/2016
From:	; MJW Technical Services
To:	; Office of Nuclear Material Safety and Safeguards, State of NY, Energy Research & Development Authority, Office of Nuclear Reactor Regulation
Shared Package
ML16293A155	List: ML16293A130; ML16293A131; ML16293A132; ML16293A133; ML16293A134; ML16293A135; ML16293A136; ML16293A137; ML16293A139; ML16293A140; ML16293A141; ML16293A142; ML16293A143; ML16293A178; ML16293A179; ML16293A180; ML16293A181; ML16293A182; ML16293A183; ML16293A184; ML16293A185; ML16293A186; ML16293A187; ML16293A278; ML16293A279; ML16293A281; ML16293A282; ML16293A364; ML16293A365; ML16293A366; ML16293A367; ML16293A368; ML16293A389; ML16293A391; ML16293A392; ML16293A393; ML16293A394; ML16293A674; ML16293A675; ML16293A676; ML16293A677; ML16293A678; ML16293A808; ML16293A809; ML16293A810; ML16293A811; ML16293A812; ML16293A843; ML16293A844; ML16293A846; ... further results
References
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Analytical Results by Area (Background)

Sample No. TYpe BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE BGA1.1.1 SAMPLE Analyzed SDG 1/4/2016 388119 1/20/2016 388119 1/11/2016 388119 1/12/2016 388119

-1/4/2016 388119 1/20/2016 388119 1/11/2016 388119 1/4/2016 388119 1/20/2016 388119 1/4/2016 388119 1/20/2016 388119 1/19/2016 388119 1/4/2016 388119 1/20/2016 388119 1/4/2016 388119 1/20/2016 388119 1/12/2016 388119 1/12/2016 388119 1/12/2016 388119 1/4/2016 388119 1/20/2016 388119 1/20/2016 388119 1/4/2016 388119 1/20/2016 388119 1/4/2016 388119 1/20/2016 388119 1/12/2016 388119 1/12/2016 388119 1/12/2016 388119 1/14/2016 388119 1/4/2016 388119 1/20/2016 388119 1/4/2016 388119 1/20/2016 388119 1/4/2016 388119 1/20/2016 388119 1/4/2016 388119 1/20/2016 388119 1/7/2016 388119 1/19/2016 388119 1/4/2016 388119 1/20/2016 388119 1/12/2016 388119 Parameter Actinium-227 Actinium-227 ALPHA Americium-241 Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Curium-242 Curium-243/244 Curium-245/246 Europium-154 Europium-154 lodine-129 Lead-212 Lead-212 Lead-214 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Strontium-90 Technetium-99 Thallium-208 Thallium-208 Thorium-228

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

R EPA EERF C-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R ASTM C 1476-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified DOE EML HASL-300, Tc-02-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Th-01-RC Modified Result 0.00

-0.15 23.8

-0.00264 0.0231

-0.00342 24.9 0.860 0.00 0.784 0.956

-0.335 0.167 0.120

-0.0105 0.012 0.00 0.0298 0.0569 0.0356 0.00899 0.00 1.40 1.28 1.10 1.36 0.0614 0.0173 0.0288

-5.07 14.9 14.2 0.00 0.00 0.784 0.956 1.00 1.23

-0.842

-0.214 0.392 0.374 1.01 Uncertainty GAS Units 0.173 14952-40-0 PCl/G PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G 0.247 4.96 0.0397 0.0671 0.0904 3.46 0.631 0.782 0.134 0.166 0.796 0.0417 0.0534 0.0323 0.040 0.0289 0.0526 0.067 0.111 0.117 0.921 0.0952 0.141 0.128 0.208 0.230 0.0668 0.0655 6.92 1.08 1.51 0.532 0.695 0.134 0.166 0.218 0.287 0.757 1.64 0.0606 0.0803 0.607 14952-40-0 12587-46-1 14596-10-2 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 14762-75-5 PCl/G U

10045-97-3 PCl/G 10045-97-3 PCl/G 10198-40-0 PCl/G U

10198-40-0 PCl/G U

OER-100-93 PCl/G PCl/G PCl/G 15585-10-1 PCl/G U

15585-10-1 PCl/G U

15046-84-1 PCl/G UI 15092-94-1 PCl/G 15092-94-1 PCl/G 15067-28-4 PCl/G 15067-28-4 PCl/G 13994-20-2 PCl/G U

13981-16-3 PCl/G U

OER-100-70 PCl/G U

14119-32-5 PCl/G U

13966-00-2 PCl/G 13966-00-2 PCl/G 14331-85-2 PCl/G UI 14331-85-2 PCl/G UI 13982-63-3 PCl/G 13982-63-3 PCl/G 15262-20-1 PCl/G 15262-20-1 PCl/G 10098-97-2 PCl/G U

14133-76-7 PCl/G U

14913-50-9 PCl/G 14913-50-9 PCl/G 14274-82-9 PCl/G MDL

. CRDL C Dilution % MoistL 0.339 1.00 22.9 0.450 1.00 22.9 3.49 4.00 0.0927 1.00 0.125 0.170 3.81 10.0 0.659 1.46 0.0993 0.129 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.37 2.00 1.00 22.9 0.0456 0.100 1.00 22.9 0.0683 0.100 1.00 22.9 0.0489 1.00 22.9 0.0814 1.00 22.9 0.043 1.00 1.00 22.9 0.0797 1.00 1.00 22.9 0.0725. 1.00 1.00 22.9 0.185 1.00 22.9 0.227 1.00 22.9 0.525 1.00 1.00 22.9 0.0765 1.00 22.9 0.120 1.00 22.9 0.235 1.00 22.9 0.368 1.00 22.9 0.388 1.00 1.00 22.9 0.129 1.00 1.00 22.9 0.112 1.00 1.00 22.9 12.2 15.0 1.00 22.9 0.437 1.00 22.9 0.743 1.00 22.9 0.596 1.00 22.9 0.927 1.00 22.9 0.0993 1.00 22.9 0.129 1.00 22.9 0.218 1.00 22.9 0.261 1.00 22.9 1.66 2.00 1.00 22.9 2.88 5.00 1.00 22.9 0.0466 1.00 22.9 0.0698 1.00 22.9 0.483 1.00 1.00 22.9

Sample No. Type BGA1.1.1 SAMPLE BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 BGA1.1.1 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MS MS MS DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP BGA1.1.1 DUP Analyzed 1/12/2016 1/12/2016 1/12/2016 1/4/2016 1/20/2016 1/11/2016 1/12/2016 1/12/2016 1/12/2016 1/12/2016 1/20/2016 1/20/2016 1/12/2016 1/5/2016 1/20/2016 1/5/2016 1/20/2016 1/5/2016 1/20/2016 1/5/2016 1/20/2016 1/20/2016 1/5/2016 1/20/2016 1/5/2016 1/20/2016 1/5/2016 1/20/2016 1/20/2016 1/5/2016 1/5/2016 1/20/2016 1/5/2016 1/20/2016 1/5/2016 1/20/2016 1/5/2016 1/20/2016 1/5/2016 1/20/2016 1/5/2016 1/20/2016 SDG 388119 "388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 38.8119 1/19/2016 388092 Parameter Thorium-229 Thorium-230 Thorium-232 Tin-126 Tin-126 Tritium Uranium-232 Uranium-233/234 Uranium-235/236 Uranium-238 Carbon-14 lodine-129 Tritium*

Actinium-227 Actinium-227 Antimony-125 Antimony-125 Bismuth-212 Bfsmuth-212 Bismuth-214 Bismuth-214 Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 lodine-129 Lead-210 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Technetium-99

Background

Fraction Method R

DOE EML HASL-300, Th-01-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 906.0 Modified R

DOE EML HASL-300, U-02-RC Modified R

EPA EERF C-01 Modified R

R R

R DOE EML HASL-300,1-01 Modified EPA 906.0 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA EERF C-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Tc-02-RC Modified Result 0.143 1.36 0.887 0.00 0.00 0.104

-0.00902 0.855 0.136 0.863 97.6 79.7 103 0.191 0.129 0.00

-0.0387 0.00 ci.oo 0.905 1.15 0.0673 0.0764 0.191 0.0167

-0.0268 0.0389

-0.127 0.042 3.06 1.28 1.34 0.979 1.10 15.4 14.5 0.00 0.458 0.905 1.15 1.37 1.05

-1.03 Uncertainty CAS 0.280 15594-54-4 0.675 14269-63-7 0.549 0.0645 0.116 2.36 0.0623 7440-29-1 10028-17-8 14158-29-3 Units PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G Lab Qu MDL CRDL 0.389 1.00 0.388 1.00 0.242 1.00 UI 0.0681 UI 0.174 u

4.09 6.00 u

0.152 1.00 0.246 13968-55-3/1391 PCl/G 0.123 1.00 0.104 15117-96-1/139:PCl/G 0.246 7440-61-1 PCl/G 1.79 3.30 9.58 0.269 0.299 0.0895 0.0983 0.878 0.807 0.177 0.203 0.802 0.0702 0.0737 0.0338 0.0429 0.101 0.125 0.239 5.61 0.131 0.134 0.166 0.197 1.26 1.48 0.483 0.704 0.177 0.203 0.253 0.365 1.70 14762-75-5 15046-84-1 10028-17-8 14952-40-0 14952-40-0 14234-35-6 14234-35-6 14913-49-6 14913-49-6 14733-03-0 14733-03-0 14762-75-5 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15046-84-1 14255-04-0 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14133-76-7 PCl/G U

PCl/G U

PCl/G UI PCl/G U

PCl/G UI PCl/G UI PCl/G PCl/G PCl/G U

PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G.

U PCl/G PCl/G PCl/G PCl/G PCl/G U

0.0842 1.00 0.107 1.00 1.40 2.00 1.57 1.00 9.54 6.00 0.461 0.556 0.178 0.179 1.33 1.48 0.127 0.141 1.37 2.00 0.065 0.100 0.0693 0.100 0.0729 0.0758 0.220 0.201 0.564 1.00 10.4 0.108 0.114 0.126 0.136 0.467 0.588 0.985 1.04 0.127 0.141 0.226 0.286 3.04 5.00 Dilution % Moistl 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9 22.9

Sample.No. Type BGA1.1.1 DUP BGA1.1.1 DUP BGA1.1.1 DUP BGA1.1.1 DUP BGA1.1.1 DUP BGA1.1.1 DUP BGA 1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA 1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA 1.1.2 SAMPLE BGA 1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA 1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA 1.1.2 SAMPLE BGA 1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA 1.1.2 SAMPLE BGA1.1.2 SAMPLE BGA1.1.3 SAMPLE BGA 1.1.3 SAMPLE BGA1.1.3 SAMPLE BGA1.1.3 SAMPLE BGA 1.1.3 SAMPLE Analyzed 1/19/2016 1/5/2016 1/20/2016 1/5/2016 1/20/2016 1/12/2016 1/4/2016 1/20/2016 1/11/2016 1/4/2016 1/20/2016 1/11/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/11/2016 1/4/2016 1/20/2016 SDG 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 Parameter Technetium-99 Thallium-208 Thallium-208 Tin-126 Tin-126 Tritium Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212*

Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125

Background Fraction Method R

DOE EML HASL-300, Tc-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 906.0 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result

-1.03 0.332 0.445 0.00 0.00

-0.262

-0.0853 0.104 15.8 0.0408 0.0805 23.0 1.25 0.00 0.769 1.06 0.00 0.00

-0.0108 0.0278

-0.0256 0.073 1.40 1.39 1.15 1.36 14.6 13.4 0.00 0.00 0.769 1.06 1.23 1.25 0.372 0.380 0.00 0.00 0.0748 0.151 16.5 0.0429

-0.0191 Uncertainty GAS 1.70 14133-76-7 0.0625 14913-50-9 0.0796 0.117 0.120 2.36 0.176 0.253 3.99 0.059 0.0929 3.30 0.490 0.765 0.117 0.200 0.0378 0.0435 0.0262 0.0434 0.0807 0.131 0.0923 0.136 0.120 0.175 0.965 1.45 0.425 0.614 0.117 0.200 0.204 0.390 0.0487 0.0818 0.093 0.156 0.235 0.320 3.71 0.0809 0.106 14913-50-9 10028-17-8 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 Units Lab Qu PCl/G U

PCl/G PCl/G PCliG UI PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

CRDL C Dilution % MoistL 3.04 5.00 1.00 22.9 0.0625 0.0738 0.155 0.131 4.12 6.00 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 0.309 1.00 22.6 0.495 1.00 22.6 3.93 4.00 1.00 22.6 0.112 1.00 22.6 0.188 1.00 22.6 3.77 10.0 1.00 22.6 0.641 1.00 22.6 1.39 1.00 22.6 0.083 1.00 22.6 0.136 1.00 22.6 0.0434 0.100 1.00 22.6 0.0915 0.100 1.00 22.6 0.0462 1.00 22.6 0.0918 1.00 22.6 0.143 1.00 22.6 0.271 1.00 22.6 0.0697 1.00 22.6 0.104 1.00 22.6 0.089 1.00 22.6 0.162 1.00 22.6 0.415 1.00 22.6 0.575 1.00 22.6 0.589 1.00 22.6 0.769 1.00 22.6 0.083 1.00 22.6 0.136 1.00 22.6 0.164 1.00 22.6 0.278 1.00 22.6 0.045 1.00 22.6 0.0811 1.00 22.6 0.0983 1.00 22.6 0.110 1.00 22.6 0.426 1.00 22.6 0.624 1.00 22.6 3.41 4.00 1.00 22.6 0.154 1.00 22.6 0.194 1.00 22.6

Sample No. Type Analyzed

SDG BGA1.1.3 SAMPLE 1/11/2016 388119 BGA1.1.3 SAMPLE 1/4/2016 388119 BGA 1.1.3 SAMPLE 1/20/2016 388119 BGA1.1.3 SAMPLE 1/4/2016 388119 BGA1.1.3 SAMPLE 1/20/2016 388119 BGA1.1.3 SAMPLE 1/4/2016 388119 BGA1.1.3 SAMPLE 1/20/2016 388119 BGA 1.1.3 SAMPLE 1 /4/2016 388119 BGA1.1.3 SAMPLE 1/20/2016 388119 BGA1.1.3 SAMPLE 1/4/2016 388119

.BGA1.1.3 SAMPLE 1/20/2016 388119 BGA1.1.3 SAMPLE 1/4/2016 388119 BGA1.1.3 SAMPLE 1/20/2016 388119 BGA1.1.3 SAMPLE 11412016 38e119 BGA1.1.3 SAMPLE 1/20/2016 388119 BGA1.1.3 SAMPLE 1/4/2016 388119 BGA1.1.3 SAMPLE 1/20/2016 388119 BGA 1.1.3 SAMPLE 1/4/2016 388119 BGA1.1.3 SAMPLE 1/20/2016 388119 BGA 1.1.3 SAMPLE 1/4/2016 388119 BGA1.1.3 SAMPLE 1/20/2016 388119 BGA1.1.3 SAMPLE 1/4/2016 388119 BGA1.1.3 SAMPLE 1/20/2016 388119 BGA1.1.3 SAMPLE 1/4/2016 388119 BGA1.1.3 SAMPLE 1/20/2016 388119 BGA1.1.3 SAMPLE 1/4/2016 388119 BGA1.1.3 SAMPLE 1/20/2016 388119 BGA1.1.4 SAMPLE 1/4/2016 388119 BGA1.1.4 SAMPLE 1/20/2016 388119 BGA1.1.4 SAMPLE 1/11/2016 388119 BGA1.1.4 SAMPLE 1/12/2016 388119 BGA1.1.4 SAMPLE 1/4/2016 388119 BGA1.1.4 SAMPLE 1/20/2016 388119 BGA1.1.4 SAMPLE 1/11/2016 388119 BGA1.1.4 SAMPLE 1/4/2016 388119 BGA1.1.4 SAMPLE 1/20/2016 388119 BGA1.1.4 SAMPLE 1/4/2016 388119 BGA1.1.4 SAMPLE 1/20/2016 388119 BGA1.1.4 SAMPLE 1/19/2016 388119 BGA1.1.4 SAMPLE 1/4/2016 388119 BGA1.1.4 SAMPLE 1/20/2016 388119 BGA1.1.4 SAMPLE 1/4/2016 388119' BGA1.1.4 SAMPLE 1/20/2016 388119 Parameter BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Americium-241 Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60

Background

Fraction Method R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA EERF C-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 28.9 1.84 0.00 0.844

'1.18 0.0159 0.017 0.00

-0.0234 0.0175

-0.0454 1.63 1.46 1.15 1.44 13.6 14.7 0.00 0.00 0.844

1. 18 1.42 1.36 0.479 0.427 0.00 0.00

-0.0553 0.0889 10.7 0.0135

-0.0116

-0.0245 22.5 1.04 1.33 0.911 1.07

-0.0544 0.134 0.175

-0.00101 0.021 Uncertainty CAS 3.25 12587-47-2 0.712 14913-49-6 0.877 0.140 0.196 0.0356 0.0446 0.0384 0.0491 0.0999 0.155 0.112 0.153 0.155 0.223

1. 19 1.64 0.701 0.659.

0.140 0.196 0.261 0.404 0.0749 0.0988 0.109 0.154 0.191 0.295 3.19 0.0507 0.0691 0.103 2.85 0.545 0.849 0.122 0.162 0.757 0.0444 0.0599 0.0251 0.0391 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14596-10-2 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 14762-75-5 10045-97-3 10045-97-3 10198-40-0 10198-40-0 Units Lab Qu MDL CRDL PCl/G 3.42 10.0 PCl/G 0.852 PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

1.42 0.128 0.129 0.0661 0.100 0.0808 0.100 0.0636 0.0913 0.187 0.290 0.0948 0.128 0.124 0.400 0.547 0.638 0.763 1.32 0.128 0.129 0.237 0.267 0.0617 0.0815 0.141 0.181 0.341 0.499 PCl/G 3.95 4.00 PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G PCl/G PCl/G U

PCl/G U

0.0854 1.00 0.121 0.182 3.21 0.632 0.903 0.0868 0.132 10.0 1.29 2.00 0.0488 0.100 0.0849 0.100 0.0477 0.0817 Dilution % Moistl 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00*

22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 22.6 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3

Sample No.* Type

BGA 1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA 1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA 1.1.4 SAMPLE BGA 1.1.4 SAMPLE BGA1.1.4

. SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.4 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE

Analyzed 1/12/2016 1/12/2016 1/12/2016 1/4/2016 1/20/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/12/2016 1/12/2016 1/12/2016 1/14/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/7/2016 1/19/2016 1/4/2016 1/20/2016 1/12/2016 1/12/2016 1/12/2016 1/12/2016 1/4/2016 1/20/2016 1/11/2016 1/12/2016 1/12/2016 1/12/2016 1/12/2016 1/4/2016 1/20/2016 1/11/2016 SDG 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 BGA1.1.5 SAMPLE 1/12/2016 388119 BGA1.1.5 SAMPLE 1/4/2016 388119 BGA1.1.5 SAMPLE 1/20/2016 388119 Parameter Curium-242 Curium-243/244 Curium-245/246 Europium-154 Europium-154 lodine-129 Lead-212 Lead-212 Lead-214 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Strontium-90 Technetium-99 Thallium-208 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232 Tin-126 Tin-126 Tritium Uranium-232 Uranium-233/234 Uranium-235/236 Uranium-238 Actinium-227 Actinium-227 ALPHA Americium-241 Antimony-125 Antimony-125

Background

Fraction Method R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300,1-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

ASTM C 1476-00 Modified R

DOE EML HASL-300, Pu-11-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE, HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 905.0 Modified/DOE RP501 Rev. 1 Modified R

DOE EML HASL-300, Tc-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300, Th-01-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 906.0 Modified R

DOE EML HASL-300, U-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.00

-0.00844 0.0106 0.0224 0.0778 0.0342 1.32 1.41 1.17 1.29 0.0027 0.0447

-0.00927

-6.99 14.7 13.1 0.00 0.00 0.911 1.07 1.41 1.35

-0.228

-0.814 0.349 0.348 1.28 0.227 1.21 0.929.

0.00 0.00 0.101 0.0496 0.847 0.0502 0.730 0.0103 0.139 15.9 0.00962

-0.0414 0.0346 Uncertainty CAS.

Units Lab Qu MDL CRDL C Dilution % MoistL 0.0389 OER-100-93 PCl/G 0.0579 1.00 1.00 20.3 0.0373 0.0589 0.0896 0.132 0.644 0.0983 0.136 0.128 0.194 0.200 0.0611 0.0419 5.82 1.06 1.43 0.413 0.655.

0.122 0.162 0.222 0.340 0.549 1.80 0.0564 0.0917 0.653 0.336 0.623 0.548 0.0793 0.135 2.30 0.0715 0.220 0.0636 0.203 0.190 0.339 3.56 0.0535 0.0774 0.122 15585-10-1 15585-10-1 15046-84-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13994-20-2 13981-16-3 PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G OER-100-70 PCl/G U

14119-32-5 PCl/G U

13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 10098-97-2 14133-76-7 14913-50-9 14913-50-9 14274-82-9 15594-54-4 14269-63-7 7440-29-1 10028-17-8 14158-29-3 PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G 13968-55-3/1391 PCl/G 15117-96-1/1391 PCl/G 7440-61-1 PCl/G 14952-40-0 14952-40-0 12587-46-1 14596-10-2 14234-35-6 14234-35-6 PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

0.0974 1.00 0.113 1.00 0.171 0.268 1.17 1.00 0.0807 0.106 0.0984 0.354 0.445 1.00 0.0833 1.00 0.106 1.00 10.4 15.0 0.356 0.619 0.732 0.880 0.0868 0.132 0.165 0.293 1.14 2.00 3.21 5.00 0.0425 0.0701 0.517 1.00 0.492 1.00 0.455 1.00 0.411 1.00 0.0803 0.124 3.98 6.00 0.0863 1.00 0.105 1.00 0.079 1.00 0.0869 1.00 0.355 0.659 3.41 4.00 0.102 1.00 0.141 0.232 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 1.00 20.3 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 20.3 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8

Sample No. Type BGA 1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA 1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA 1.1.5 SAMPLE BGA 1.1.5 SAMPLE BGA 1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA 1.1.5 SAMPLE

. BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA 1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA 1.1.5 SAMPLE BGA 1.1.5 SAMPLE BGA 1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA 1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA 1.1.5 SAMPLE BGA 1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE Analyzed 1/11/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/19/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/12/2016 1/12/2016 1/12/2016 1/4/2016 1/20/2016 1/20/2016 1/4/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/12/2016 1/12/2016 1/12/2016 1/14/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/4/2016 1/20/2016 1/6/2016 1/19/2016 1/4/2016 1/20/2016 1/12/2016 1/12/2016 1/12/2016 1/12/2016 1/4/2016 SDG 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 388119 BGA1.1.5 SAMPLE 1/20/2016 388119 Parameter BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Curium-242 Curium-243/244 Curium-245/246 Europium-154 Europium-154 lodine-129 Lead-21 O Lead-212 Lead-212 Lead-214 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Strpntium-90 Technetium-99 Thallium-208 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232 Tin-126 Tin-126

Background

Fraction Method R

EPA 900.0/SW846 9310/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA EERF C-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300,1-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

. DOE HASL 300, 4.5.2.3/Ga-01~R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

ASTM C 1476-00 Modified R

DOE EML HASL-300, Pu-11-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 905.0 Modified/DOE RP501 Rev. 1 Modified R

DOE EML HASL-300, Tc-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300, Th-01-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 27.1 0.00 0.00 0.974 1.02

-0.512 0.138 0.147 0.00687

-0.0204.

0.00 0.0365 0.00 0.120

-0.0712 0.0755 2.26 1.33 1.33 0.987 1.29 0.00 0.0457 0.0012

-4.61 14.8 12.6 0.00 0.00 0.974 1.02 1.10 1.47

-0.319

-0.48 0.376 0.348 0.998 0.143 0.632 1.45 0.00 0.00 Uncertainty CAS 3.05 12587-47-2 0.634 14913-49-6 1.03 0.142 0.224 0.792 0.0683 0.0731 0.045 0.0402 0.0404 0.0626 0.0427 0.156 0.147 0.352 0.726 0.0985 0.158 0.144 0.201 0.147 0.0678 0.0553 6.11 1.39 1.60 0.585 0.695 0.142 0.224 0.362 0.344 0.841 2.20 0.0762 0.0995 0.610 0.281 0.511 0.691 0.065 0.157 14913-49-6 14733-03-0 14733-03-0 14762-75-5 10045-97-3 10045-97-3 10198-40-0 10198-40-0 OER-100-93 15585-10-1 15585-10-1 15046-84-1 14255-04-0 15092-94-1" 15092-94-1.

15067-28-4 15067-28-4 13994-20-2 13981-16-3 OER-100-70 14119-32-5 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 10098-97-2 14133-76-7 14913-50-9 14913-50-9 14274-82-9 15594-54-4 14269-63-7 7440-29-1 Units Lab Qu MDL CRDL PCl/G 3.11 10.0 PCl/G UI 1.24 PCl/G UI 1.57 PCl/G 0.130 PCl/G 0.141 PCl/G U

PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G 1.37 2.00 0.0821 0.100 0.0901 0.100 0.0864 0.0738 0.0602 1.00 0.0548 1.00 0.0635 1.00 0.271 0.268 0.767 1.00 0.596 4.00 PCl/G 0.0763 PCl/G 0.140 PCl/G 0.108 PCl/G 0.187 PCl/G 0.218 1.00 PCl/G 0.0991 1.00 PCl/G U

PCl/G U

0.121 1.00 10.8 15.0 PCl/G 0.659 PCl/G 0.754 PCl/G UI 0.691 PCl/G UI 1.34 PCl/G 0.130 PCl/G 0.141 PCl/G 0.301 PCl/G 0.289 PCl/G U

PCl/G U

1.72 2.00 3.87 5.00 PCl/G 0.0638 PCl/G 0.0845 PCl/G 0.524 1.00 PCl/G 0.389 1.00 PCl/G 0.568 1.00 PCl/G 0.242 1.00 PCl/G UI PCl/G UI 0.0656 0.146 Dilution % Moisti 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00

23.8 1.00

. 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00 23.8 1.00

- 23.8 1.00 23.8

Sample No. Type BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.1.5 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA 1.2.1 SAMPLE BGA 1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA 1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA 1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA1.2.1 SAMPLE BGA 1.2.1 SAMPLE Analyzed SDG 1/11/2016 388119 1/12/2016 388119 1/12/2016 388119 1/12/2016 388119 1/12/2016 388119 1/4/2016 388119 1/20/2016 388119 1/11/2016 388119 1/4/2016 388119 1/20/2016 388119 1/11/2016 388119 1/4/2016' 388119 1/20/2016 388119 1/4/2016 388119 1/20/2016 388119 1/4/2016 388119 1/20/2016 388119 1/4/2016 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 BGA 1.2.1 SAMPLE 42389 388119 388119 388119 388119 388119 388119 388119 BGA1.2.2 SAMPLE 42373 BGA1.2.2 SAMPLE 42389 BGA1.2.2 SAMPLE 42380 BGA1.2.2 SAMPLE 42373 BGA1.2.2 SAMPLE 42389 BGA1.2.2 SAMPLE 42380 Parameter*

Tritium Uranium-232 Uranium-233/234 Uranium-235/236 Uranium-238 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA

Background

Fraction Method R

EPA 906.0 Modified R

DOE EML HASL-300, U-02-RC Modified R

DOE EML HASL-300, U-02-RC Modified

-R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R.

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified Result 1.29 0.013 0.644 0.0212

. 0.670 0.0242

-0.137 19.7 0.0359 0.0241 23.8 0.726 0.00 0.758 0.987 0.228 0.206 0.00185 0.00495 0.00

-0.0883 1.01 0.892 1.02 0.901 13.8 12.7 0.00 0.0225 0.758 0.987 0.891 o.722 0.287 0.265 0.00 0.00 0.041 0.199 17.1

-0.0116

-0.0697 21.5 Uncertainty GAS.

Units Lab Qu MDL CRDL C Dilution % MoistL 2.38 10028-17-8 PCl/G U

4.05 6.00 1.00 23.8 0.0487 14158-29-3 PCl/G U

0.0818 1.00 1.00 23.8 0.235 13968-55-3/1391 PCl/G 0.117 1.00 1.00 23.8 0.0595 0.238 0.188 0.289 4.53 0.0799 0.114 3.42 0.653 1.06 0.102 0.171 0.071 0.0839 0.0276 0.0479 0.0963 0.125 0.0906 0.128 0.127 0.214 1.16 1.53 0.407 0.647 0.102 0.171 0.201 0.376 0.0617 0.0727 0.0911 0.140 0.209 0.317 3.52 0.080 0.120 2.70 15117-96-1/1391 PCl/G 7440-61-1 PCl/G 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G UI PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G 0.0635 1.00 0.101 1.00 0.338 0.514 3.23 4.00 0.128 0.211 3.91 10.0 0.631 0.968 1.00 23.8 1.00 23.8 1.00 25.3 1.00 25.3 1.00 25.3 1.00 25.3 1.00 25.3 1.00 25.3 1.00 25.3 1.00 25.3 0.0887 1.00 25.3 0.129 1.00 25.3 0.0449 0.100 1.00 25.3 0.0956 0.100 1.00 25.3 0.0513 1.00 25.3 0.0939 1.00 25.3 0.163 1.00 25.3 0.213 1.00 25.3 0.077 1.00 25.3 0.121 1.00 25.3 0.210 1.00 25.3 0.141 1.00 25.3 0.470 1.00 25.3 0.550 1.00 25.3 0.681 1.00 25.3 1.14 1.00 25.3 0.0887 1.00 25.3 0.129 1.00 25.3 0.160 1.00 25.3 o.360 f.oo 25.3 0.0438 1.00 25.3 0.0728 1.00 25.3 0.110 1.00 25.3 0.177 0.398 0.619 3.36 4.00 0.144 0.207 2.80 10.0 1.00 1.00 1.00 1.00 1.00 1.00 1.00 25.3 18.8 18.8 18.8 18.8 18.8 18.8

Sample No. Type BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA 1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.2.2 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA 1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA 1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE BGA1.3.1 SAMPLE Analyzed SDG 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42380 388119 42373 388119 42389 388119 42380 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 Parameter 8ismuth-212 8ismuth-212 8ismuth-214 8ismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA 8ismuth-212 8ismuth-212 8ismuth-214 8ismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4:5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 1.51 0.00 0.915 0.934 0.185 0.178 0.0141

-0.0237 0.0841

-0.0872 1.12 1.32 1.21 1.24 12.7 12.8 0.00 0.00 0.915 0.934 1.15 1.10 0.302 0.360 0.00 0.00 0.104

-0.205 11.8 0.0505

-0.0316 21.8 1.32 0.00 0.791 1.02 0.328 0.354 0.000158

-0.0406

-0.0688 0.0171 1.03 Uncertainty CAS 0.591 14913-49-6 0.897 14913-49-6 0.136 14733-03-0 0.202 0.0502 0.092 0.0331 0.0465 0.119 0.152 0.0982 0.153 0.148 0.205 1.19 1.71 0.498 0.677 0.136 0.202 0.270 0.344 0.066 0.095 0.112 0.169 0.193 0.293 3.23 0.0785 0.110 2.94 0.565 0.819 0.115 0.177 0.0532 0.0766 0.0319 0.0557 0.090 0.114 0.0913 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 Units Lab Qu MDL CRDL PCl/G 0.731 PCl/G UI 1.50 PCl/G 0.108 PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

PCl/G 0.178 0.0548 0.100 0.0999 0.100 0.0657 0.0861 0.235 0.274 0.083 0.134 0.269 0.168 0.423 0.841 0.624 1.38 0.108 0.178 0.231 0.289 0.0547 0.0783 0.105 0.196 0.360 0.518 3.61 4.00 PCl/G U

0.144 PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G 0.196 3.45 10.0 0.663 1.51 0.0959 0.144 0.0538 0.100 0.0703 0.100 0.0588 0.095 0.152 0.233 0.0813 Dilution % Moistt 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.. 8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 18.8 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6

pample No. Type Analyzed SDG BGA1.3.1 SAMPLE 42389 388119 BGA 1.3.1 SAMPLE 42373 388119 BGA 1.3. 1 SAMPLE 42389 388119 BGA1.3.1 SAMPLE 42373 388119 BGA1.3.1 SAMPLE 42389 388119 BGA 1.3.1 SAMPLE 42373 388119 BGA1.3.1 SAMPLE 42389 388119 BGA1.3.1 SAMPLE 42373 388119

. BGA1.3.1 SAMPLE 42389 388119 BGA 1.3. 1 SAMPLE 42373 388119 BGA1.3.1 SAMPLE 42389 388119 BGA 1.3.1 SAMPLE 42373 388119 BGA 1.3.1 SAMPLE 42389 388119 BGA 1.3.1 SAMPLE 42373 388119 BGA 1.3.1 SAMPLE 42389 388119 BGA 1.3.2 SAMPLE 42373 388119 BGA 1.3.2 SAMPLE 42389 388119 BGA1.3.2 SAMPLE 42380 388119 BGA1.3.2 SAMPLE 42373 388119 BGA1.3.2 SAMPLE 42389 388119 BGA1.3.2 SAMPLE 42380 388119 BGA1.3.2 SAMPLE.

42373 388119 BGA1.3.2 SAMPLE 42389 388119 BGA1:3.2 SAMPLE 42373 388119 BGA 1.3.2 SAMPLE 42389 388119 BGA1.3.2 SAMPLE 42373 388119 BGA 1.3.2 SAMPLE 42389 388119 BGA1.3.2 SAMPLE 42373 388119 BGA1.3.2 SAMPLE 42389 388119 BGA1.3.2 SAMPLE 42373 388119 BGA1.3.2 SAMPLE 42389 388119 BGA 1.3.2 SAMPLE 42373 388119 BGA 1.3.2 SAMPLE 42389 388119 BGA 1.3.2 SAMPLE 42373 388119 BGA1.3.2 SAMPLE 42389 388119 BGA 1.3.2 SAMPLE 42373 388119 BGA1.3.2 SAMPLE 42389 388119 BGA1.3.2 SAMPLE 42373 388119 BGA1.3.2 SAMPLE 42389 388119 BGA1.3.2 SAMPLE 42373 388119 BGA1.3.2 SAMPLE 42389 388119 BGA1.3.2 SAMPLE 42373 388119 BGA1.3.2 SAMPLE 42389 388119 Parameter Lead-212 Lead-214 Lead-214 Potassium-40

Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.964 1.04 1.10 12.3 13.2 0.00 0.352 0.791 1.02 1.04 0.953 0.265 0.258 0.00 0.00

-0.0251 0.0671 16.5 0.00835

-0.0362 21.8 1.22 0.810 0.837 1.01 0.284 0.299

-0.0051

-0.00414 0.0753 0.00 1.19 1.27 1.12 1"15 14.6 14.6 0.00 0.00 0.837 1.01 1.12 1.29 Uncertainty CAS 0.126 15092-94-1 0.128 0.190 1.01 1.62 0.557 0.882 0.115 0.177 0.209 0.287 0.0647 0.0895 0.0852 0.102 0.216 0.372 3.79 0.0791 0.148 2.81 0.706 0.901 0.137 0.252 0.0735 0.137 0.0285 0.0597 0.107 0.132 0.0991 0.172 0.160 0.302 1.29 2.22 0.478 0.953 0.137 0.252 0.269 0.421 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 Units Lab Qu MDL CRDL C Dilution % Moistt PCl/G

0. 115 1.00 42.6 PCl/G 0.236 1.00 42.6 PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G 0.162 0.422 0.683 0.615 1.02 0.0959 0.144 0.177 0.272 0.0506 0.0752 0.077 0.130 0.389 0.683 3.43 4.00 0.141 0.274 3.15 10.0 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 42.6 1.00 22.8 1.00 22.8 1.00 22.8 1.00 22.8 1.00 22.8 1.00 22.8 0.739 1.00 22.8 1.93 1.00 22.8 0.115

1.00 22.8 0.229 1.00 22.8 0.0611

0. 100 1.00 22.8 0.136 0.100 1.00 22.8 0.0522 1.00 22.8

0. 122 1.00 22.8 0.170 1.00 22.8 0.387 1.00 22.8 0.0829 1.00 22.8 0.165 1.00 22.8 0.259 1.00 22.8 0.202 1.00 22.8 0.537 1.00 22.8 1.15 1.00 22.8 0.696 1.00 22.8 1.19 1.00 22.8 0.115 1.00 22.8 0.229 1.00 22.8 0.229 1.00 22.8 0.396 1.00 22.8

Sample No. Type BGA1.3.2 SAMPLE BGA1.3.2 SAMPLE BGA1.3.2 SAMPLE BGA1.3.2 SAMPLE BGA 1.4.1 SAMPLE BGA 1.4.1 SAMPLE BGA 1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA 1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA 1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA1.4.1 SAMPLE BGA 1.4.1 SAMPLE BGA 1.4.1 SAMPLE BGA 1.4.2 SAMPLE BGA1.4.2 SAMPLE BGA1.4.2 SAMPLE BGA1.4.2 SAMPLE BGA1.4.2 SAMPLE BGA1.4.2 SAMPLE BGA1.4.2 SAMPLE Analyzed SDG 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119

. 42380 388119 42373 388119 42389 388119

. 42380 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 38811 9 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 38811 9 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42380 38811 9 42373 388119 42389 388119 42380 388119 42373 388119 Parameter Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154

Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.322 0.425 0.00 0.00

-0.0795 0.0553 -

10.8 0.00677

-0.0409 20.0 0.562 0.00 0.749 0.965 0.260 0.232 0.00557 0.0271

-0.0608

-0.0468 1.03 0.986 0.986 1.05 11.4 12.8 0.00 0.191 0.749 0.965 0.729 1.15 0.226 0.301 0.00 0.0994

-0.0875 0.042 13.6

-0.0107

-0.00353 20.0 0.00 Uncertainty CAS 0.0541 14913-50-9 0.119 14913-50-9 0.106 0.145 0.184 0.311 3.17 0.0659 0.122 2.79 0.471 0.992 0.132 0.191 0.0542 0.0868 0.0266 0.0479 6.0935 0.154 0.0865 0.154 0.124 0.206 1.01 1.60 0.524 0.683 0.132 0.191 0.190 0.297 0.0523 0.0957 0.0881 0.141 0.181 0.260 3.55 0.0647 0.0985

' 2.67 0.634 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 Units Lab Qu MDL CRDL PCl/G 0.0545 PCl/G 0.0976 PCl/G UI 0.110 PCl/G UI 0.173 PCl/G U

0.334 PCl/G U

0.591 PCl/G 3.92 4.00 PCl/G U

0.122 0.220 PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G u

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G U

3.35 10.0 0.700 1.54 0.0953 0.164 0.0569 0.100 0.0891 0.100 0.051 0.103 0.158 0.283 0.0754 0.128 0.0995 0.382 0.467 0.834 0.616 1.19 0.0953 0.164 0.175 0.316 0.0517 0.0847 0.0983 0.263 0.289 0.490 PCl/G 3.94 4.00 PCl/G U

0.117 PCl/G U

0.179 PCl/G 3.04 10.0 PCl/G UI 0.850 Dilution % Moist(

1.00 22.8 1.00 22.8 1.00 22.8 1.00 22.8 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2

. 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 33.2 1.00 22 1.00 22 1.00 22 1.00 22 1.00 22 1.00 22 1.00 22

Sample No. Type Analyzed SDG BGA1.4.2 SAMPLE 42389 388119 BGA1.4.2 SAMPLE 42373 388119 BGA1.4.2 SAMPLE 42389 388119 BGA1.4.2 SAMPLE 42373 388119 BGA1.4.2 SAMPLE 42389 388119 BGA1.4.2 SAMPLE 42373 388119 BGA1.4.2 SAMPLE 42389 388119 BGA1.4.2 SAMPLE

. 42373 388119 BGA1.4.2 SAMPLE 42389 388119 BGA 1.4.2 SAMPLE 42373 388119 BGA1.4.2 SAMPLE 42389 388119 BGA1.4.2 SAMPLE 42373 388119 BGA1.4.2 SAMPLE 42389 388119 BGA 1.4.2 SAMPLE 42373 388119 BGA1.4.2 SAMPLE 42389 388119 BGA 1.4.2 SAMPLE 42373 388119 BGA1.4.2 SAMPLE 42389 388119 BGA 1.4.2 SAMPLE 42373 388119 BGA 1.4.2 SAMPLE 42389 388119 BGA1.4.2 SAMPLE 42373 388119 BGA1.4.2 SAMPLE 42389 388119 BGA1.4.2 SAMPLE 42373 388119 BGA1.4.2 SAMPLE 42389 388119 BGA1.4.2 SAMPLE 42373 388119 BGA 1.4.2 SAMPLE 42389 388119 BGA1.5.1 SAMPLE 42373 388119 BGA 1.5.1 SAMPLE 42389 388119 BGA1.5.1 SAMPLE 42380 388119 BGA 1.5.1 SAMPLE 42373 388119 BGA1.5.1 SAMPLE 42389 388119 BGA1.5.1 SAMPLE 42380 388119 BGA1.5.1 SAMPLE 42373 388119 BGA1.5.1 SAMPLE 42389 388119 BGA1.5.1 SAMPLE 42373 388119 BGA1.5.1 SAMPLE 42389 388119 BGA1.5.1 SAMPLE 42373 388119 BGA1.5.1 SAMPLE 42389 388119 BGA1.5.1 SAMPLE 42373 388119 BGA1.5.1 SAMPLE 42389 388119 BGA 1.5.1 SAMPLE BGA1.5.1 SAMPLE BGA1.5.1 SAMPLE BGA1.5.1 SAMPLE 42373 388119 42389 388119 42373 388119 42389 38811 9 Parameter Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.00 0.654 0.889 0.188 0.215 0.00729

-0.0209 0.00

-0.00916 1.02 1.18 0.968 0.950 11.9 11.7 0.00 0.00 0.654 0.889 0.784 0.945 0.274 0.313

. 0.00 0.00 0.0237

-0.25 13.2 0.0439 0.00 30.3 0.00 0.00 0.959 1.10 0.337 0.391 0.00312

-0.0127 0.00

-0.134 1.16 1.09 Uncertainty CAS.

0.598 14913-49-6 0.130 14733-03-0 0.169 14733-03-0 0.0539 0.0782 0.0276 0.0343 0.0769 0.091 0.088 0.123 0.123 0.175 0.981 1.37 0.472 0.646 0.130 0.169 0.199 0.227 0.0594 0.0725 0.0816 0.122 0.279 0.269 3.60 0.113 0.289 3.31 0.914 0.847 0.160 0.198 0.0867 0.0852 0.0437 0.0439 0.138 0.184 0.127 0.121 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 Uriits

. Lab Qu MDL CRDL c Dilution % Moistl PCl/G UI 1.16 1.00 22 PCl/G 0.0828 1.00 22 PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G UI PCl/G U

PCl/G PCl/G

-PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G UI PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G UI PCl/G U

PCl/G PCl/G 0.137 1.00 22

0. 0457 0.100 1.00 22 0.0609 0.100 1.00 22 0.0525 1.00 22 0.0482 1.00 22 0.162 1.00 22 0.180 1.00 22 0.0697 1.00 22 0.100 1.00 22 0.0908 1.00 22 0.143 1.00 22 0.367 1.00 22 0.571 1.00 22 0.584 1.00 22 0.803 1.00 22 0.0828 1.00 22 0.137 1.00 22 0.167 1.00 22 0.212 1.00 22 0.0434 1.00 22 0.0624 1.00 22 0:0309 1.00 22 0.124 1.00 22 0.517 0.456 3.89 4.00 0.209 0.192 3.56 10.0 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.33 1.00 27.6 1.43 1.00 27.6 0.141 1.00 27.6 0.146 1.00 27.6 0.0828 0.100 1.00 27.6 0.0851 0.100 1.00 27.6 0.084 1.00 27.6 0.0823 1.00 27.6 0.295 0.254 0.116 0.126 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6

Sample No. Type BGA1.5.1 SAMPLE BGA1.5.1 SAMPLE BGA1.5.1 SAMPLE BGA1.5.1 SAMPLE BGA1.5.1 SAMPLE BGA1.5.1 SAMPLE BGA1.5.1 SAMPLE BGA1.5.1 SAMPLE BGA1.5.1 SAMPLE BGA1.5.1 SAMPLE.

BGA1.5.1 SAMPLE BGA 1.5.1 SAMPLE BGA 1.5.1 SAMPLE BGA 1.5.1 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPL.E BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA 1.5.2 SAMPLE BGA 1.5.2 SAMPLE BGA 1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA1.5.2 SAMPLE Analyzed SDG 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42380 388119 42373 388119 42389 388119 42380 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 Parameter Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R f3.

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R

. R DOE HASL 300, 4.5.Z.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result.

1.04 1.18 11.7 12.5 0.413 0.00 0.959 1.10 0.801 1.01 0.314 0.267 0.00 0.00 0.018 0.179 11.4 0.00

-0.00353 20.7 0.00 0.00 0.740 0.895 0.220 0.241 0.0138

-0.0111 0.00543

-0.0451 1.00 1.12 1.04 1.12 12.7 12.8 0.317 0.00 0.740 0.895 0.00 1.01 0.358 Uncertainty CAS 0.180 15067-28-4 0.175 15067-28-4 1.43 13966-00-2 1.46 0.587 0.828 0.160 0.198 0.349 0.299 0.0879 0.0959 0.0903 0.0914 0.229 0.275 3.40 0.0897 0.102 2.90 0.533 0.924 0.150 0.179 0.0693 0.079 0.030 0.0361 0.107 0.111 0.102 0.121 0.164 0.156 1.11 1.21 0.551 0.650 0.150 0.179 0.218 0.257 0.0662 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 Units Lab Qu MD.L CRDL:

PCl/G 0.318 PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

0.152 0.676 0.692 1.08 0.916 0.141 0.146 0.274 0.300 0.0738 0.0704 0.0929 0.128 0.413 0.518 PCl/G 4.05 4.00 PCl/G UI 0.149 PCl/G U

0.186 3.22 1.02 0.913 0.109 0.127 10.0 PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G UI PCl/G PCl/G 0.0563 0.100 0.078 0.100 0.061 0.0657 0.201 0.199 0.0894 0.109 0.268 0.136 0.572 0.659 0.762 0.907 0.109 0.127 0.425 0.273 0.0556 Dilution % Moistl 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 27.6 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2

Sample No. Type BGA1.5.2 SAMPLE BGA 1.5.2 SAMPLE BGA1.5.2 SAMPLE BGA 1.5.2 MSD BGA1.5.2 MSD BGA1.5.2 MS BGA1.5.2 MS BGA1.5.2 DUP.

BGA1.5.2 DUP BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE BGA2.1.1 SAMPLE Analyzed SDG 42389 388119 42373 388119 42389 388119 42380 388119 42380 388119 42383 388119 42383 388119 42380 388119 42380 388119 42373 388119 42389 388119 42380 388119 42381 388119 42373 388119 42389 388119 42380 388119 42373 388119 42389 388119 42373 388119 42389 388119 42388 388119 42373 388119 42389 388119 42373 388119 42389 388119 42381 388119 42381 388119 42381 388119 42373 388119 42389 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42381 388119 42381 388119 42381 388119 42383 388119 42373 388119 42389 388119 42373 388119 42389 388119 Parameter Thallium-208 Tin-126 Tin-126 ALPHA BETA ALPHA BETA ALPHA BETA Actinium-227 Actinium-227 ALPHA Americium-241 Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Curium-242 Curium-243/244 Curium-245/246 Europium-154 Europium-154 lodine-129 Lead-212 Lead-212 Lead-214 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA EERF C-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE. HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300,1-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

ASTM C 1476-00 Modified R

DOE EML HASL-300, Pu-11-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R

Result 0.309 0.00 0.00 114 117 75.5 120 10.8 24.2

-0.0573 0.114 9.23

-0.0317

-0.0159 0.107 15.0 0.00 0.00 0.550 0.688

-0.12 0.646 0.769 Uncertainty OAS 0.085 14913-50-9 0.0913 0.117 16.0 17.9 13.5 18.9 3.35 3.42 0.237 0.379 3.11 0.0399 0.0898 0.138 2.62 0.651 0.762 0.116 0.199 1.00 0.0907 0.127

-0.00335

. 0.0336 12587-46-1 12587-47-2 12587-46-1 12587-47-2 12587-46-1 12587-47-2 14952-40-0 14952-40-0 12587-46-1 14596-10-2 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 14762-75-5 10045-97-3 10045-97-3 10198-40-0 10198-40-0 OER-100-93

-0.0248 0.0464 0.0136 0.00457 0.0287

-0.0293

-0.0558

-0.0504 0.513 0.692 0.618 0.819

-0.0585

-0.0073 0.0195

-9.13 6.95 6.78 0.00 0.104 0.051 0.0477 0.066 0.090 0.150 0.472 0.0947 0.128 0.144 0.193 0.264 0.0323 0.0536 6.96 1.01 1.27 0.793 0.747 15585-10-1 15585-10-1 15046-84-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13994-20-2 13981-16-3 OER-100-70 14119-32-5 13966-00-2 13966-00-2 14331-85-2 14331-85-2 Units Lab Qu MDL

CRDL C Dilution % Moistt PCl/G 0.0664 1.00 21.2 PCl/G UI PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G U

PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G UI PCl/G U

0.125 0.164 6.42 4.00 4.17 10.0 6.49 4.00 3.93 10.0 3.98 4.00 4.00 10.0 0.423 0.685 3.78 4.00 0.133 1.00 0.158 0.272 3.19 10.0 0.950 1.61 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 21.2 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 0.108 1.00 39.4 0.200 1.00 39.4 1.72 2.00 1.00 39.4 0.0647 0.100 1.00 39.4 0.0823 0.100 1.00 39.4 0.0642 1.00 39.4 0.0807 1.00 39.4 0.0858 1.00 1.00 39.4 0.0996 1.00 1.00 39.4 0.105 1.00 1.00 39.4 0.167 0.269 0.928 1.00 0.108 0.140 0.249 0.393 0.666 1.00 0.0843 1.00 0.0929 1.00 12.5 15.0 0.562 0.930 0.732 1.28 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4 1.00 39.4

Sample No.

Type BGA2.1.1 SAMPLE BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1.1 BGA2.1."1 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 BGA2.1.2 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE BGA2.1.2 SAMPLE BGA2.1.2 SAMPLE BGA2.1.2 SAMPLE BGA2.1.2 SAMPLE BGA2.1.2 SAMPLE BGA2.1.2 SAMPLE Analyzed SDG 42373 388119 42389 388119 42373 388119 42389 388119 42375 388119 42388 388119 42373 388119 42389 388119 42381 388119 42381 388119 42381 388119 42381 388119 42373 388119 42389 388119 42381 388119 42381 388119 42381 388119 42381 388119 42381 388119 42373 388119 42389 388119 42380 388119 42373 388119 42389 388119 42380 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 Parameter Radium-226 Radium-226 Radium-228 Radium-228 Strontium-9D Technetium-99 Thallium-208 Thallium-2D8 Thorium-228 Thorium-229 Thorium-23D Thorium-232 Tin-126 Tin-126 Tritium Uranium-232 Uranium-233/234 Uranium-235/236 Uranium-238 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-6D Cobalt-6D Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-4D Potassium-4D Protactinium-231 Protactinium-231

Background

Fraction Method R

DOE HASL 3DD, 4.5.2.3/Ga-D1-R R

EPA 9D5.D Modified/DOE RP5D1 Rev. 1 Modified R

DOE EML HASL-3DD, Tc-D2-RC Modified R

DOE HASL 3DO, 4.5.2.3/Ga-D1-R R

DOE HASL 30D, 4.5.2.3/Ga-D1-R R

DOE EML HASL-3DO, Th-D1-RC Modified R

DOE EML HASL-3DO; Th-D1-RC Modified R

DOE EML HASL-3DD, Th-D1-RC Modified R,

DOE EML HASL-30D, Th-D1-RC Modified R

DOE HASL 30D, 4.5.2.3/Ga-01-R R

DOE HASL 3DD, 4.5.2.3/Ga-01-R R

EPA 906.0 Modified R

DOE EML HASL-30D, U-D2-RC Modified R

DOE EML HASL-3DD, U-D2-RC Modified R

DOE EML HASL-30D, U-D2-RC Modified.

R DOE HASL 3DD, 4.5.2.3/Ga-D1-R R

DOE HASL 3DO, 4.5.2.3/Ga-D1-R R

EPA 9DD.D/SW846 931 O/SM 711 OB Modified R

DOE HASL 3DO, 4.5.2.3/Ga-D1-R R

DOE HASL 30D, 4.5.2.3/Ga-D1-R R

EPA 9DD.D/SW846 9310/SM 71108 Modified R

DOE HASL 30D, 4.5.2.3/Ga-D1-R R

DOE HASL 3DD, 4.5.2.3/Ga-D1-R R

DOE HASL 3DD, 4.5.2.3/Ga-01-R R

DOE HASL 3DD, 4.5.2.3/Ga-D1-R R

DOE HASL 3DD, 4.5.2.3/Ga-01-R R

R R

R DOE HASL 3DD, 4.5.2.3/Ga-D1-R DOE HASL 3DD, 4.5.2.3/Ga-D1-R DOE HASL 3DD, 4.5.2.3/Ga-D1-R DOE HASL 3DD, 4.5.2.3/Ga-D1-R DOE HASL 3DD, 4.5.2.3/Ga-D1-R DOE HASL 3DD, 4.5.2.3/Ga-D1-R Result 0.550 0.688 0.00 0.00

-0.638

-0.715 0.158 0.181 0.584 0.00 0.733 1.20 O.DD D.D534 D.867 D.0228 D.775 D.D495 -

D.690 D.D855 D.D727 6.21

-D.D23 D.D49 16.9 O.DD 1.11 D.622 D.697 D.D421 D.D238 D.DDD729

-D.D115

-D.D571 D.D429 D.814 D.8D2 0.799 D.9D8 7.51 8.3D O.DD D.295 Uncertainty GAS Units Lab Qu MDL CRDL D.116 13982-63-3 PCl/G D.108 D.199 13982-63-3" PCl/G 0.20D D.270 D.248 D.832 2.78 D.D635 D.115 D.535 D.203 D.599 D.711 D.D987 D.128 3.D5 D.114 D.411 0.169 D.374 0.169 0.2D3 2.78 D.0617 D.D737 2.73 D.394 0.73D D.D988 0.165 O.D4D4 D.0366 D.0259 D.D345 D.177 D.D913 D.D842 0.1D6 0.130 0.141 D.844 1.10 D.407 D.576 15262-2D-1 15262-20-1 1 DD98-97-2 14133-76-7 14913-5D-9 14913-50-9 14274-82-9 15594-54-4 14269-63-7 7440-29-1 10028-17-8 14158-29-3 PCl/G UI PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G U

13968-55-3/1391 PCl/G 15117-96-1 /139: PCl/G U

7440-61-1 PCl/G 14952-40-0 14952-4D-D 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-D 1 D045-97-3 1 DD45-97-3 10198-4D-D 10198-4D-D 15585-1D-1 15585-1 D-1 15D92-94-1 15092-94-1 15D67-28-4 15D67-28-4 13966-DD-2 13966-0D-2 14331-85-2 14331-85-2 PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G U

0.454 D.546 1.76 4.91 D.0621 D.D92 2.DD 5.0D 0.498 1.DD D.3D3 1.DD D.615 1.DD D.301 1.DD D.112 D.21D 5.24 6.00 D.227 1.0D D.368 1.00 D.314 1.0D D.263 1.DD D.327 D.4D5 3.75 D.1D8 D.151 4.DD 3.25 10.0 0.782 D.748 D.D855 D.121 D.D501 D.1 DO D.0753 0.1 OD D.D511 0.0643 0.148 0.199 O.D75 D.D79 D.218 D.1D5 D.4D2 D.105 0.737 0.789 Dilution % Moistl 1.DD 39.4 1.DD 39.4 1.00 39.4 1.0D 39.4 1.0D 39.4 1.DO 39.4 1.DD 39.4 1.00 39.4 1.0D 39.4 1.DD 39.4 1.DD 39.4 1.DO 39.4 1.DO 39.4 1.DO 39.4 1.0D 39.4 1.DD 39.4 1.00 39.4 1.0D 39.4 1 :oo 39.4 1.00 29 1.DD 29 1.DD 29 1.DD 29 1.00 29 1.00 29 1.0D 29 1.0D 29 1.DD 29 1.DO 29 1.DD 29 1.0D 29 1."DD 29 1.DD 29 1.DD 29 1.DD 29 1.DD 29 1.DD 29 1.DD 1.DD 1.0D 1.00 1.DO 1.00 29 29 29 29 29 29

Sample No. rype Analyzed SDG BGA2.1.2 SAMPLE 42373 388119 BGA2.1.2 SAMPLE 42389 388119 BGA2.1.2 SAMPLE 42373 388119 BGA2. 1.2 SAMPLE 42389 388119 BGA2.1.2 SAMPLE 42373 388119 BGA2.1.2 SAMPLE 42389 388119 BGA2.1.2 SAMPLE 42373 388119 BGA2.1.2 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42380 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42380 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.3 SAMPLE 42373 388119 BGA2.1.3 SAMPLE 42389 388119 BGA2.1.4 SAMPLE 42373 388119 BGA2.1.4 SAMPLE 42389 388119 BGA2.1.4 SAMPLE 42380 388119 Parameter Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300,4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R _

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.i3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 71108 Modified Result 0.622 0.697 0.719 0.880 0.236 0.178 0.00 0.00

-0.00612 0.0587 12.0

-0.0248 0.0904 21.4 0.00 0.00 0.737 0.808

-0.00545

-0.0157 0.0184 0.0456 0.00608 0.0917 0.940 1.01 1.04 0.949 12.9 11.4 0.00 0.264 0.737 0.808 0.860 0.783 0.300 0.225 0.0496 0.00

-0.0441

-0.0202 19.7 Uncertainty GAS 0.0988 13982-63-3 0.165 0.195 0.266 0.0559 0.0626 0.0799 0.0828 0.188 0.247 3.16 0.0711 0.203 2.56 0.642 0.689 0.142 0.216 0.0263 0.0492 0.0299 0.0544 0.102 0.179 0.0898 0.121 0.143 0.185 1.06 1.66 0.526 0.603 0.142 0.216 0.210 0.296 0.0573 0.0966 0.118 0.083 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00~2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 0.260 14952-40-0 0.292 14952-40-0 3.82 12587-46-1 Units Lab Qu MDL CRDL C Dilution % MoistL PCl/G 0.0855 1.00 29 PCl/G 0.121 1.00 29 PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G U

PCl/G U

PCl/G 0.209 0.214 0.0392 0.0582 0.0968 0.0856 0.355 0.488 3.81 0.127 0.208 4.00 2.74 10.0 1.00 29 1.00 29 1.00 29 1.00 29 1.00 29 1.00 29 1.00 20.7 1.00 20.7 1.00 20.7 1.00 20.7 1.00 20.7 1.00 20.7 0.979 1.00 20.7 1.50 1.00 20.7 0.0964 1.00 20.7 0.148 1.00 20.7 0.0487 0.100 1.00 20.7 0.0896 0.100 1.00

20. 7 0.055 1.00 20.7 0.122 1.00 20.7 0.166 1.00 20.7 0.373 1.00 20.7 0.0733 1.00 20.7 0.0941 1.00

20. 7 0.0993 1.00 20.7 0.163 1.00 20.7 0.430 1.00 20.7 0.787 1.00 20.7 0.599 1.00 20.7 1.06 1.00 20.7 0.0964 1.00 20.7 0.148 1.00 20.7 0.180 1.00 20.7 0.440 1.00 20.7 0.044 1.00 20.7 0.0737 1.00 20.7 0.119 1.00 20.7 0.0788 1.00 20.7 0.453 0.536 2.43 4.00 1.00 22 1.00 22 1.00 22

Sample No. Type BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 BGA2.1.4 BGA2.1.4 BGA2.1.4 BGA2.1.4 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE Analyzed SDG 42381 388119 42373 388119 42389 388119 42380 388119 42373 388119 42389 388119 42373 388119 42389 388119 42388 388119 42373 388119 42389 388119 42373 388119 42389 388119 42381 388119 42381 388119 42381 388119 42373 388119 42389 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42381 388119 42381 388119 42381 388119 1/2015/2016 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42373 388119 42389 388119 42376 388119 42388 388119 42373 388119 42389 388119 42381 388119 42381 388119 42381 388119 42381 388119 Parameter Americium-241 Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Carbon-14

Cesium-137 Cesium-137 Cobalt-60 Cobalt~60 Curium-242 Curium-243/244 Curium-245/246 Europium-154 Europium-154 1oi:line-129 Lead-212 Lead-212 Lead-214 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Strontium-90 Technetium-99 Thallium-208 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232

Background

Fraction Method R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

EPA EERF C-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,1-01 M*odified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R ASTM C 1476-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified DOE EML HASL-300, Tc-02-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified Result 0.0274 0.0373

-0.0796 35.2 0.173 1.80 1.24 0.990

-0.537 0.0037 0.0611 0.021

-0.0108

-0.00469 0.00926 0.00 0.0938 0.0959

-0.146 1.36 1.53 1.10 1.46

-0.0358 0.00414 0.0357

-6.29 23.6 25.6 0.437 0.00 1.24 0.990 1.21 1.08

-0.758 2.01 0.405 0.355 1.06 0.218 0.820 1.03 Uncertainty CAS Units Lab Qu MDL CRDL 0.063 14596-10-2 0.0999 1.00 0.11 0 14234-35-6 u

0.207 PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

0.110 14234-35-6 u

0.185 3.16 12587-47-2 2.74 10.0 0.908 14913-49-6 u

1.54 1.06 14913-49-6 0.185 14733-03-0 0.189 14733-03-0 0.766 0.0503 0.0503 0.0446 0.0486 0.0405 0.0515 0.0416 0.143 0.149 0.331 0.123 0.140 0.210 0.205 0.158 0.0471 0.0514 6.10 2.02 1.94 0.609 0.857 0.185 0.189 0.378 0.369 0.512 2.78 0.0953 0.0809 0.649 0.346 0.565 0.608 14762-75-5 10045-97-3 10045-97-3 10198-40-0 10198-40-0 OER-100-93 15585-10-1 15585-10-1 15046-84-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 PCl/G PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G 13994-20-2 PCl/G U

13981-16-3 PCl/G U

OER-100-70 PCl/G 14119-32-5 PCl/G U

13966-00-2 PCl/G 13966-00-2 PCl/G 14331-85-2 PCl/G U

14331-85-2 PCl/G UI 13982-63-3 PCl/G 13982-63-3 PCl/G 15262-20-1 PCl/G 15262-20-1 10098-97-2 14133-76-7 14913-50-9 14913-50-9 14274-82-9 15594-54-4 14269-63-7 7440-29-1 PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G 1.16 0.153 0.140 1.33 2.00 0.0905 0.100 0.082 0.100 0.093 0.089 0.0938 1.00 0.0986 1.00 0.0619 1.00 0.297 0.301 0.621. 1.00 0.101 0.108 0.147 0.381 0.413 1.00 0.100 1.00 0.062 1.00 10.9 15.0 0.777 0.651 1.06 0.983 0.153 0.140 0.336 0.282 1.21 2.00 4.71 5.00 0.0723 0.0811 0.553 1.00 0.478 1.00 0.477 1.00 0.258 1.00 Dilution % Moisti 1.00 22 1.00 22 1.00 22 1.00 22 1.00 22 1.00 22 1.00 22 1.00 22 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22 22

Sample No. Type BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.4 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE BGA2.1.5

SAMPLE BGA2.1.5 SAMPLE BGA2.1.5 SAMPLE Analyzed SDG 42373 388119 42389 388119 42381'-388119 42381 388119 42381 388119 42381 388119 42381 388119 42374 388119 42389 388119 42380 388119 42382 388119 42374 388119 42389 388119 42380 388119 42374 388119 42389 388119 42374 388119 42389 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42382 388119 42382 388119 42382 388119 42374 388119 42389 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 BGA2.1.5 SAMPLE 42381 388119 BGA2.1.5 SAMPLE 42381 388119 BGA2.1.5 SAMPLE 42381 388119 BGA2.1.5 SAMPLE 1/2015/2016 388119 BGA2.1.5 SAMPLE 42374 388119 BGA2.1.5 SAMPLE 42389 388119 BGA2.1.5 SAMPLE 42374 388119 BGA2.1.5 SAMPLE 42389 388119 BGA2.1.5 SAMPLE 42374 388119 BGA2.1.5 SAMPLE 42389 388119 Parameter Tin-126 Tin-126 Tritium Uranium-232 Uranium-233/234 Uranium-235/236 Uranium-238 Actinium-227 Actinium-227 ALPHA Americium-241 Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Curiurri-242 Curium-243/244 Curium-245/246 Europium-154 Europium-154 lodine-129 Lead-212 Lead-212 Lead-214 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

EPA 906.0 Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA EERF C-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300; Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R ASTM C 1476-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.00 0.00 0.719 0.0136 1.01 0.0508 1.10

-0.0321 0.00 4.38 0.00764

-0.00271 0.0668 14.1 0.570 1.23 0.469 0.526

-0.485 0.850 0.865 0.0168

-0.019 0.00 0.0221 0.0168

-0.0534 0.00

-0.408 0.648 0.676 0.701 0.777

-0.0315 0.0599 0.0325

-4.32 6.75 6.88 0.161

-0.0165 0.469 0.526 Uncertainty GAS Units Lab Qu MDL CRDL C Dilution % MoistL 0.128 0.142 2.35 0.0511 0.261 0.0668 0.271 0.235 0.403 2.43 0.0424 0.109 0.106 2.54 0.625 0.578 0.170 0.153 1.02 0.122 0.110 0.0342 0.0344 0.0323 0.0507 0.0473 0.120 0.116 0.472 0.104 0.120 0.140 0.187 0.271 0.0706 0.0647 6.45 1.12 1.22 0.517 0.551 0.170 0.153 PCl/G UI 0.118 1.00 22 PCl/G UI 0.172 1.00 22 10028-17-8 14158-29-3 PCl/G U

PCl/G U

13968-55-3/1391 PCl/G 15117-96-1/1391 PCl/G 7440-61-1 PCl/G 14952-40-0 PCl/G U

14952-40-0 PCl/G UI 12587-46-1 PCl/G 14596-10-2 PCl/G U

14234-35-6 PCl/G U

12587-47-2 PCl/G 14913-49-6 PCl/G 14913-49-6 PCl/G 14733-03-0 PCl/G 14733-03-0 PCl/G 14762-75-5 PCl/G U

10045-97-3 PCl/G 10045-97-3 PCl/G 10198-40-0 PCl/G U

10198-40-0 PCl/G U

. OER-100-93 PCl/G 15585-10-1 15585-10-1 15046-84-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 PCl/G PCl/G PCl/G U

PCl/G UI PCl/G U

PCl/G PCl/G PCl/G PCl/G 13994-20-2 PCl/G U

13981-16-3 PCl/G OER-100-70 PCl/G 14119-32-5 PCl/G U

13966-00-2 PCl/G 13966-00-2 PCl/G 14331-85-2 PCl/G U

14331-85-2 PCl/G U

13982-63-3 PCl/G 13982-63-3 PCl/G 4.03 6.00 0.0859 1.00 0.111 1.00 0.0508 1.00 0.103 1.00 0.440 0.637 3.62 4.00 0.0814 1.00 0.177 0.213 3.31 10.0 0.735 0.873 0.138 0.153 1.76 2.00 0.0792 0.100 0.0589 0.100 0.0751 0.0665 0.048

1.00 0.0804 1.00 0.0504 1.00 0.211 0.316 0.670 1.00 0.100 0.123 0.153 0.171 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 22 22 22 22 22 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 0.629 1.00 1.00 40.7 0.0764 1.00 1.00 40.7 0.105 1.00 1.00 40.7 11.4 15.0 1.00 40.7 0.714 1.00 40.7 0.897 1.00 40.7 0.962 1.00 40.7 0.997 1.00 40.7 0.138 1.00 40.7 0.153 1.00 40.7

Sample No. Type BGA2.1.5 SAMPLE BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.5 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.1.6 BGA2.2.1 BGA2.2.1 BGA2.2.1 BGA2.2.1 BGA2.2.1 BGA2.2.1 BGA2.2.1 BGA2.2.1 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE DUP DUP SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 42374 388119 42389 388119 42375 388119 42388 388119 42374 388119 42389 388119 42381 388119 42381 388119 42381 388119 42381 388119 42374 388119 42389 388119 42381 388119 42381 388119 42381 388119 42381 388119 42381 388119 42375 388092 42375 388119 42380 388121 42375 388121 42380 388121 42375 388121 42380 388121 42380 388121 42380 388121 42380 388121 42380 388121 42380 388121 42380 388121 42380 388121 42380 388121 42380 388121 42380 388121 42380 388121 42374 388119 42389 388119 42380 388119 42374 388119 42389 388119 42380 388119 42374 388119 42389 388119 Parameter Radium-228 Radium-228 Strontium-90 Technetium-99 Thallium-208 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232

Tin-126 Tin-126 Tritium Uranium-232 Uranium-233/234 Uranium-235/236 Uranium-238 Strontium-90 Strontium-90 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-13_7 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 905.0 Modified/DOE RP501 Rev. 1 Modified R

DOE EML HASL-300, Tc-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300, Th-01-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 906.0 Modified R

DOE EML HASL-300, U-02-RC Modified R

EPA 905.0 Modified/DOE RP501 Rev. 1 Modified R

EPA901.1 R

EPA 900.0/SW846 9310 R

EPA901.1 R

EPA 900.0/SW846 9310 R

EPA901.1 R

R R

R EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA 901.1 DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.753 0.593

-0.686 0.839 0.210 0.225 0.517 0.0661 0.867 0.370 0.0453 0.0714

-0.806

-0.0535 0.591 0.0624 1.02 0.240 0.240

-11.7

-1.01 6.50

-2.69 43.0 0.00

-0.165

-1.18

-0.889 6.25 5.16 19.7

-15.1

-0.994 2.84

-0.907 0.281

-0.112 13.0

-0.0738

-0.0293 29.4 0.998 0.598 Uncertainty CAS Units Lab*Qu MDL CRDL 0.257 15262-20-1 PCl/G 0.279 0.244 0.293 0.653 2.33 0.0766 0.0615 0.497 0.248 0.565 0.423 0.0905 0.0922 3.02 0.122 15262-20-1 10098-97-2 14133-76-7 14913-50-9 14913-50-9 14274-82-9 15594-54-4 14269-63-7 7440-29-1 10028-17-8 14158-29-3 PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G u

u 1.41 3.98 0.0788 0.0782 2.00 5.00 0.600 1.00 u

0.417 1.00 0.260 1.00 0.528 1.00 u

0.149 u

0.172 u

5.28 6.00 0.273 13968-55-3/1391 PCl/G u

0.332 1.00 0.0934 1.00 0.0936 1.00 0.107 15117-96-1/139:PCl/G 0.356 7440-61-1 PCl/G 0.149 1.00 0.795 0.795 28.8 1.07 9.82 2.41 51.7 14.7 3.50 3.60 10.4 13.6 10.4 64.9 54.0 16.1 4.56 8.81 0.398 0.409 3.73 0.146 0.152 3.35 1.00 1.34 10098-97-2 10098-97-2 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 15262-20-1 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 PCl/G PCl/G PCl/L PCl/L PCl/L PCl/L PCl/L PCl/L PCl/L PCl/L u

1.43 2.00

u.

1.43 2.00 u

49.4 u

2.98 u

18.1 u

4.84 u

102 UI u

15.9 6.42 u

6.09 PCl/L U

PCl/L U

19.7 13.1 17.3 65.0 92.8 27.9 7.67 15.9 0.756 0.710 5.00 5.00 10.0 PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G U

3.89 4.00 0.259 0.270 3.64 10.0 1.49 1.89 Dilution % Moisti 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00 40.7 1.00

. 40.7 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 100 100 100 100 100 100 100 100 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7

Sample No. Type BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1 SAMPLE BGA2.2.1.

SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE Analyzed SDG 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 38811 9 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42380 388119 42374 388119 42389 388119 42380 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 Parameter Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Background*.

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 71108 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 71108 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.892 0.871 0.323 0.292 0.0312 0.0223 0.0121 0.0458 1.02 0.902 0.983 0.839 17.4 20.1 0.380 0.00 0.892 0.871 0.888 1.05 0.362 0.395 0.00 0.027 0.0141 0.247 13.9

-0.0256

-0.0877 17.4 1.24 0.00 0.750 1.13 0.192 0.181 0.0441 0.0148 0.0371

-0.108 1.25 1.18 0.904 Uncertainty GAS 0.217 14 733-03-0 0.248 0.120 0.114 0.0465 0.0647 0.216 0.198 0.156 0.195 0.250 0.252 2.13 2.44 0.777 0.946 0.217 0.248 0.362 0.326 0.103 0.115 0.136 0.159 0.380 0.309 3.30 0.135 0.124 2.86 1.36 0.774 o."214 0.222 0.0717 0.0803 0.0537 0.0527 0.240 0.185 0.165 0.175 0.266 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 Units Lab Qu MDL CRDL C Dilution % Moistt PCl/G 0.242 1.00 38.7 PCl/G 0.203 1.00 38.7 PCl/G 0.112 0.100 1.00

38. 7 PCl/G 0.102 0.100 1.00

38. 7 PCl/G U

0.107 PCl/G U

0.134 PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G 0.407 0.397 0.167 0.217 0.202 0.187 1.10 1.18 1.40 1.33 0.242 0.203 0.430 0.319 0.0953 0.117 0.249 0.253 0.693 0.600 3.07 4.00 0.250 0.206 3.53 10.0 1.36 1.45 0.183 0.170 0.103 0.100 0.0989 0.100 0.115 0.0945 0.449 0.263 0.156 0.169 0.214 1.00 38.7 1.00 38.7 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7 38.7 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3 37.3

Sample No. Type BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.2.2 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE BGA2.3.1 SAMPLE Analyzed SDG 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388119 42389 388119 42374 388121 42389 388121 42381 388121 42374 388121 42389 388121

.42381 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 Parameter Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110.B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

. DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 1.07 19.5 18.1 0.00 0.00 0.750 1.13 1.34 1.25 0.461 0.412 0.00 0.062 0.00108 0.0372 11.9 0.0187 0.0053 21.4 2.03 0.00 0.876 0.765 0.359 0.328

-0.0388 0.0242

-0.00175

-0.0709 0.984 0.885 1.09 0.896 12.8 12.4 0.00 0.338 0.876 0.765 0.799 0.556 0.260 0.295 Uncertainty GAS 0.220 15067-28-4 2.12 13966-00-2 1.79 0.760 0.706 0.214 0.222 0.421 0.360 0.104 0.0854 0.156 0.219 0.299 0.321 3.86 0.112 0.116 3.07 0.748 0.685 0.161 0.157 0.0772 0.0933 0.0387 0.0413 0.134 0.160 0.137 0.139 0.202 0.217 1.66 1.54 0.699 0.673 0.161 0.157 0.303 0.366 0.102 0.106 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85~2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 Units Lab Qu MDL PCl/G PCl/G 0.190 0.694 PCl/G 0.730 PCl/G UI 1.07 PCl/G UI 1.18 PCl/G 0.183 PCl/G 0.170 PCl/G 0.395 PCl/G 0.318 PCl/G 0.0941 PCl/G 0.083 PCl/G UI 0.230 PCl/G U

0.205 PCl/G U

0.564 PCl/G U

0.608 PCl/G PCl/G U

PCl/G U

PCl/G PCl/G 3.97 0.210 0.219 2.91 1.11 PCl/G UI 1.37 PCl/G 0.149 PCl/G 0.152 CRDL 4.00

(

10.b PCl/G 0.0565 0.100 PCl/G 0.0929 0.100 PCl/G U

PCl/G U

0.0589 0.0913 0.263 0.287 PCl/G 0.122 PCl/G 0.138 PCl/G 0.367 PCl/G 0.178 PCl/G 0.861 PCl/G 0.649 PCl/G UI 1.02 PCl/G U

1.20 PCl/G 0.149 PCl/G 0.152 PCl/G 0.292 PCl/G 0.357 PCl/G 0.0894 PCl/G 0.0872 Dilution % Moistl 1.00 37.3 1.00 37.3 1.00 37.3 1.00 37.3 1.00 37.3 1.00 37.3 1.00 37.3 1.00 37.3 1.00 37.3 1.00 37.3 1.00 37.3 1.00 37.3 1.00 37.3 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7 1.00 32.7

Sample No., Type Analyzed SDG BGA2.3.1 SAMPLE 42374 388121 BGA2.3.1 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42381 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42381 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE.

42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.3.2 SAMPLE 42374 388121 BGA2.3.2 SAMPLE 42389 388121 BGA2.4.1 SAMPLE 42374 388121 BGA2.4.1 SAMPLE 42389 388121 BGA2.4.1 SAMPLE 42381 388121 BGA2.4.1 SAMPLE 42374 388121 BGA2.4.1

. SAMPLE 42389 388121 BGA2.4.1 SAMPLE 42381 388121 BGA2.4.1 SAMPLE 42374 388121 BGA2.4.1 SAMPLE 42389 388121 BGA2.4.1 SAMPLE 42374 388121 Parameter Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.00 0.00

-0.00517

-0.0775 5.20

-0.00452 0.0243 17.3 0.00 0.835 0.735 0.918 0.287 0.217 0.0165

-0.00721

-0.0959

-0.0784 1.03 0.990 1.05 1.08 12.7 14.0 0.00 0.00 0.735 0.918 1.02 0.841 0.225 0.362 0.00 0.0595

-0.0778 0.00457 12.5 0.0537 0.0689 23.6 0.00 0.619 0.561 Uncertainty CAS 0.137 0.376 0.245 0.263 2.84 0.0846 0.0906 2.80 0.783 0.657 0.163 0.156 0.0663 0.0904 0.0366 0.0411 0.111 0.125 0.116 0.119 0.176 0.187 1.46 1.42 0.943 0.570 0.163 0.156 0.263 0.206 0.0914 0.0776 0.0994 0.0951 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 0.269 14952-40-0 0.297 14952-40-0 3.50 12587-46-1 0.121 14234-35-6 0.111 14234-35-6 3.45 12587-47-2

0. 702 14913-49-6 0.67 4 14913-49-6 0.228 14733-03-0 Units Lab Qu MDL CRDt C Dilution % MoistL PCl/G UI 0.197 1.00 32.7 PCl/G UI 0.215 1.00 32.7 PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G UI PCl/G U

PCl/G 0.466 0.476 3.85 4.00 0.158 0.171 2.62 10.0 0.901 0.835 0.130 1.00 27.5 1.00 27.5 1.00 27.5 1.00 27.5 1.00 27.5 1.00 27.5 1.00 27.5 1.00 27.5 1.00 27.5 0.110 1.00 27.5 0.0767 0.100 1.00 27.5 0.0654 0.100 1.00 27.5 0.0796 1.00 27.5 0.0674 1.00 27.5 0.187 1.00 27.5 0.219 1.00 27.5 0.0935 1.00 27.5 0.107 1.00 27.5 0.329 1.00 27.5 0.144 1.00 27.5 0.644 1.00 27.5 0.651 1.00 27.5 0.930 1.00 27.5 1.00 1.00 27.5 0.130 1.00 27.5 0.110 1.00 27.5 0.301 1.00 27.5 0.177 1.00 27.5 0.0657 1.00 27.5 0.0586 1.00 27.5 0.123 1.00 27.5 0.144 1.00 27.5 0.495 1.00 36.4 0.539 1.00 36.4 3.90 4.00 1.00 36.4 0.244 1.00 36.4 0.220 1.00 36.4 4.02 10.0 1.00

. 36.4 1.53 1.00 36.4 1.39 1.00 36.4 0.223 1.00 36.4

Sample No. Type BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 SAMPLE BGA2.4.1 MSD BGA2.4.1 MSD BGA2.4.1 MS BGA2.4.1 MS BGA2.4.1 DUP BGA2.4.1 BGA2.4.2 BGA2.4.2 BGA2.4.2 BGA2.4.2 BGA2.4.2 BGA2.4.2 BGA2.4.2 BGA2.4.2 BGA2.4.2 BGA2.4.2 BGA2.4.2 BGA2.4.2 BGA2.4.2 BGA2.4.2 DUP SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42380 388121 42380 388121 42381 388121 42381 388121 42381 388121 42381 388121 42374 388121 42389 388121 42381 388121 42374 388121 42389 388121 42381 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 Parameter Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40.

Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 ALPHA BETA ALPHA BETA ALPHA BETA Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.851 0.293 0.279 0.00712

-0.00501

-0.0744 0.0601 0.776 0.835 0.912 0.835 13.0 11.8 0.00 0.00 0.561 0.851 0.716 0.664 0.208 0.275 0.00 0.00 103 113 97.5 112 11.5 18.0 0.000969 0.167 10.0 0.037 0.0192 20.1 0.00 0.00 0.671 0.516 0.291 0.255

-0.00111

-0.00105 Uncertainty CAS 0.159 14733-03-0 0.105 10045-97-3 0.103 0.0619 0.0478 0.163 0.161' 0.115 0.111 0.221 0.186 1.87 1.58 0.876 0.583 0.228 0.159 0.331 0.346 0.0856 0.085 0.0798 0.112 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 13.7 12587-46-1 16.1 12587-47-2 13.9 12587-46-1 15.8 3.38 2.87 0.269 0.247 3.36 0.101 0.091 2.90 0.827 0.628 0.168 0.144 0.0772 0.0656 0.0367 0.0322 12587-47-2 12587-46-1 12587-47-2 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 Units Lab Qu MDL CRDL PCl/G 0.130 PCl/G 0.102 0.100 PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

0.0909 0.100 0.126 0.0922 0.298 0.324 0.116 0.108 0.372 0.146 1.51 0.444 0.897 0.963 0.223 0.130 0.290

o.255 0.106 0.0737 0.0849 0.0927 4.48 4.00 5.29 10.0 7.51 4.00 5.57 10.0 3.94 4.00 3.28 10.0 0.511 0.478 3.88 4.00 0.198 0.177 2.83 10.0 1.37 1.02 0.149 0.123 0.0898 0.100 0.0605 0.100 0.0757 0.0629 Dilution % Moistl 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 36.4 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 36.4 31.9 31.9 31.9 31.9 31.9 31.9 31.9 31.9 31.9 31.9 31.9 31.9 31.9 31.9

Sample No. Type Analyzed SDG BGA2.4.2 SAMPLE 42374 388121 BGA2.4.2 SAMPLE 42389 388121 BGA2.4.2 SAMPLE 42374 388121 BGA2.4.2 SAMPLE 42389 388121 BGA2.4.2 SAMPLE 42374 388121 BGA2.4.2 SAMPLE 42389 388121 BGA2.4.2 SAMPLE 42374 388121 BGA2.4.2 SAMPLE 42389 388121 BGA2.4.2 SAMPLE 42374 388121 BGA2.4.2 SAMPLE 42389 388121 BGA2.4.2 SAMPLE 42374 388121 BGA2.4.2 SAMPLE 42389 388121 BGA2.4.2 SAMPLE 42374 388121 BGA2.4.2 SAMPLE 42389 388121 BGA2.4.2 SAMPLE 42374 388121 BGA2.4.2 SAMPLE 42389 388121 BGA2.4.2 SAMPLE 42374 388121 BGA2.4.2 SAMPLE 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 BGA2.4.2 DUP 42389 388121 BGA2.4.2 DUP 42374 388121 Parameter Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 Antimony-125 Antimony-125 Bismuth-212 Bismuth-212

Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228

Background

Fraction Method

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result

-0.0484

-0.0762 0.725 0.926 0.905 0.793 11.9 12.1 0.274 0.00 0.671 0.516 0.599 0.723 0.236 0.193 0.011 0.00

-0.0942

-0.236

-0.0194

-0.017 0.00 0.160 0.637 0.643 0.242 0.253 0.0189 0.0133 0.0473

-0.0462 0.814 0.921 0.742 0.855 13.3 11.0 0.00 0.00 0.637 0.643 0.832 Uncertainty GAS 0.120 15585-10-1 0.105 0.154 0.117 0.189 0.194 1.49 1.42 0.601 0.803 0.168 0.144 0.271 0.246 0.0736 0.0628 0.109 0.0836 0.253 0.230 0.0892 0.086 0.742 0.702 0.172 0.162 0.0599 0.0815 0.0333 0.0377 0.107 0.094 0.110 0.138 0.150 0.166 1.41 1.24 0.878 0.667 0.172 0.162 0.246 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 14234-35-6 14234-35-6 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 Units Lab.Qu MDL CRDL c Dilution % MoistL PCl/G U

0.227 1.00 31.9 PCl/G U

0.179 1.00 31.9 PCl/G 0.140 1.00 31.9 PCl/G 0.0967 1.00 31.9 PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G U

PCl/G U

PCl/G UI PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G 0.328 1.00 31.9 0.129 1.00 31.9 0.826 1.00 31.9 0.588 1.00 31.9 1.05 1.00 31.9 0.910 1.00 31.9 0.149 1.00 31.9 0.123 1.00 31.9 0.326 1.00 31.9 0.235 1.00 31.9 0.0718 1.00 31.9 0.0574 1.00 31.9 0.191 1.00 31.9 0.141 1.00 31.9 0.443 1.00 31.9 0.412 1.00 31.9 0.160 1.00 31.9 0.160 1.00 31.9 1.10 1.00 31.9 1.12 1.00 31.9 0.115 1.00 31.9 0.120 1.00 31.9 0.0402 0.100 1.00 31.9 0.0688 0.100 1.00 31.9 0.0726 1.00 31.9 0.0706 1.00 31.9 0.203 1.00 31.9 0.167 1.00 31.9 0.0934 1.00 31.9 0.105 1.00 31.9 0.129 1.00 31.9 0.143 1.00 31.9 0.658 1.00 31.9 0.580 1.00 31.9 0.787 1.00 31.9 0.800 1.00 31.9 0.115 1.00 31.9 0.120 1.00 31.9 0.250 1.00 31.9

Sample No. Type BGA2.4.2 DUP BGA2.4.2 DUP BGA2.4.2 DUP BGA2.4.2 DUP BGA2.4.2 DUP BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.S.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.1 SAMPLE BGA2.5.2 SAMPLE BGA2.5.2 SAMPLE BGA2.5.2 SAMPLE BGA2.5.2 SAMPLE BGA2.5.2 SAMPLE BGA2.5.2 SAMPLE

, Analyzed*

SDG 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42381 388121 42374 388121 "42389 388121 42381 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42381 388121 42374 388121 42389 388121 42381 388121 Parameter Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300,"4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified Result 0.677 0.243 0.229 0.00 0.00

-0.00301 0.150 8.75 0.00046 0.00 22.9 0.00 0.00 0.726 0.674 0.372 0.427

-0.0499 0.0092

-0.169 0.0872 0.875 0.980 1.01 0.988 13.8 15.5 0.557 0.520 0.726 0.674 0.941 0.989 0.312 0.333 0.0536 0.00

-0.186

-0.493 12.9 0.0366

-0.109 25.2 Uncertainty GAS 0.217 15262-20-1 0.070 0.0758 0.0791 0.136 0.316 0.286 3.18 0.124 0.171 2.90 0.882 0.796 0.178 0.176 0.122 0.0877 0.0474 0.0425 0.167 0.118 0.180 0.125 0.213 0.205 1.76 1.69 0.674 0.655 0.178 0.176 0.384 0.262 0.0932 0.0805 0.183 0.127 0.310 0.387 4.02 0.141 0.155 3.30 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6.

12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 Units Lab Qu MDL CRDL PCl/G 0.220 PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

0.0528 0.0609 0.106 0.140 0.590 0.555 PCl/G 3.99 4.00 PCl/G U

0.230 PCl/G UI 0.236 PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCliG U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G 2.84 1.75 1.56 0.166 0.155 10.0 0.0885 0.100 0.0836 0.100 0.073 0.0874 0.267 0.262 0.196 0.113 0.200 0.151 0.715 0.728 1.27 1.15 0.166 0.155 0.369 0.299 0.0858 0.082 0.252 0.142 0.542 0.597 3.92 4.00 0.230 0.269 2.97 10.0 Dilution % Moist(

1.00 31.9 1.00 31.9 1.00 31.9 1.00 31.9 1.00 31.9 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 i.oo 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 44.7 1.00 30.5 1.00 30.5 1.00 30.5 1.00 30.5 1.00 30.5 1.00 30.5

Sample No. Type BGA2.5.2 SAMPLE BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 BGA2.5.2 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 42374 388121 42389 388121 Parameter Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126

Background

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.00 0.848 0.849 0.876 0.114 0.134 0.00308 0.0205

-0.0672 0.0568 1.12 1.15 0.940 1.15 17.6 19.5 0.00 0.00 0.849 0.876 0.937 1.10 0.354 0.312 0.00 0.0749 Uncertainty GAS 0.811 14913-49-6 1.16 0.191 0.282 0.0534 0.0807 0.0518 0.0643 0.166 0.152 0.142 0.162 0.242 0.276 1.80 2.57 0.968 1.16 0.191 0.282 0.362 0.366 0.0785 0.137 0.156 0.204 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 Units PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G

pcJ/G PCl/G PCl/G Lab Qu MDL

. CRDL C Dilution % MoistL UI 1.67 1.00 30.5 u

1.99 1.00 30.5 u

u u

u UI UI UI u

0.179 1.00 30.5 0.192 1.00 0.0927 0.100 1.00 0.105 0.100 1.00 0.102 1.00 0.140 1.00 0.301 1.00 0.347 1.00 0.132 1.00 0.155 1.00 0.170 0.224 0.741 1.10 1.04 1.23 0.179 0.192 0.283 0.454 0.0832 0.106 0.215 0.222 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5 30.5

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