ML16293A888

Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey Conducted in 2014, Rev. 0, Appendix F, Part 1 of 8

ML16293A888
Person / Time
Site:	West Valley Demonstration Project, P00M-032
Issue date:	08/22/2016
From:	MJW Technical Services
To:	Office of Nuclear Material Safety and Safeguards, State of NY, Energy Research & Development Authority, Office of Nuclear Reactor Regulation
Shared Package
ML16293A155	List: ML16293A130 ML16293A131 ML16293A132 ML16293A133 ML16293A134 ML16293A135 ML16293A136 ML16293A137 ML16293A139 ML16293A140 ML16293A141 ML16293A142 ML16293A143 ML16293A178 ML16293A179 ML16293A180 ML16293A181 ML16293A182 ML16293A183 ML16293A184 ML16293A185 ML16293A186 ML16293A187 ML16293A278 ML16293A279 ML16293A281 ML16293A282 ML16293A364 ML16293A365 ML16293A366 ML16293A367 ML16293A368 ML16293A389 ML16293A391 ML16293A392 ML16293A393 ML16293A394 ML16293A674 ML16293A675 ML16293A676 ML16293A677 ML16293A678 ML16293A808 ML16293A809 ML16293A810 ML16293A811 ML16293A812 ML16293A843 ML16293A844 ML16293A846 ... further results
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Text

Appendix F -

Analytical Results by Area

Analytical Results by Area (Area 1)

• Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty GAS Units Lab Qua MDL CRDL CDilution 1% MoistL 1.1.C1 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.598 0.511 14952-40-0 PCl/G U 0.703 1.00 32 1.1.C1 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 12.6 3.93 12587-46-1 PCl/G 3.89 4.00 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.143 0.176 14234-35-6 PCl/G U 0.346 1.00 32 1.1.C1 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 711 OB Modified 25.5 3.89 12587-47-2 PCl/G 3.57 10.0 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.236 0.678 14913-49-6 PCl/G U 1.33 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.740 0.216 14733-03-0 PCl/G 0.200 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 3.64 0.256 10045-97-3 PCl/G 0.108 0.100 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.011 0.0535 10198-40-0 PCl/G U 0.112 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0401 0.155 15585-10-1 PCl/G U 0.316 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.615 0.142 15092-94-1 PCl/G 0.155 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.910 0.196 15067-28-4 PCl/G 0.403 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 10.4 1.92 13966-00-2 PCl/G 0.958 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.936 0.826 14331-85-2 PCl/G U 1.27 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.740 0.216 13982-63-3 PCl/G 0.200 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.777 0.275 15262-20-1 PCl/G 0.308 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.121 0.102 14913-50-9 PCl/G 0.0968 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0572 0.174 PCl/G U 0.191 1.00 32 1.1.C2 SAMPLE 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.039 0.193 14952-40-0 PCl/G U 0.355 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.189 0.366 14952-40-0 PCl/G U 0.420 1.00 17.8 1.1.C2 SAMPLE 1/11/2016 388092 ALPHA R EPA 900.0/SW846 931 O/SM 711 OB Modified 9.22 1.49 12587-46-1 PCl/G 1.62 4.00 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0086 0.072 14234-35-6 PCl/G U 0.134 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00955 0.0883 14234-35-6 PCl/G U 0.168 1.00 17.8 1.1.C2 SAMPLE 1/11/2016 388092 BETA R EPA 900.0/SW846 9310/SM 71108 Modified 14.3 1.24 12587-47-2 PCl/G 1.28 10.0 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.409 14913-49-6 PCl/G UI 0.824 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 1.04 14913-49-6 PCl/G UI 1.31 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.599 0.112 14733-03-0 PCl/G 0.0966 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.814 0.159 14733-03-0 PCl/G 0.119 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.182 0.0431 10045-97-3 PCl/G 0.0264 0.100 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.150 0.0613 10045-97-3 PCl/G 0.0615 0.100 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00744 0.0317 10198-40-0 PCl/G U 0.0575 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00777 0.0336 10198~40-0 PCl/G U 0.0701 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0456 0.0908 15585-10-1 PCl/G U 0.180 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00312 0.113 15585-10-1 PCl/G U 0.220 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.522 0.104 15092-94-1 PCl/G . 0.106 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.646 0.119 15092-94-1 PCl/G 0.0981 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.878 0.146 15067-28-4 PCl/G 0.106 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.946 0.168 15067-28-4 PCl/G 0.296 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 9.80 1.00 13966-00-2 PCl/G 0.601 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 9.18 1.34 13966-00-2 PCl/G 0.726 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.561 14331-85-2 PCl/G U 0.599 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.454 14331-85-2 PCl/G UI 0.626 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.599 0.112 13982-63-3 PCl/G 0.0966 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.814 0.159 13982-63-3 PCl/G 0.119 1.00 17.8

Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty CAS Units Lab Qua MDL CRDL C Dilution I% MoistL 1.1.C2 SAMPLE 12/29/2015 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.663 0.230 15262-20-1 PCl/G 0.169 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.685 0.271 15262-20-1 PCl/G 0.223 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.248 0.0628 14913-50-9 PCl/G 0.0465 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.191 0.0609 14913-50-9 PCl/G 0.0636 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0313 0.0955 PCl/G U 0.130 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0805 PCl/G UI 0.0794 1.00 17.8 1.1.C2 DUP 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0874 0.193 14952-40-0 PCl/G U 0.347 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.128 0.273 14952-40-0 PCl/G U 0.542 1.00 0 1.1.C2 DUP 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.015 0.0715 14234-35-6 PCl/G U 0.128 1.00 17.8 1.1.C2 DUP ' 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0514 0.109 '14234-35-6 PCl/G U 0.214 1.00 0 1.1.C2 DUP 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.574 14913-49-6 PCl/G UI 0.899 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.454 0.581 14913-49-6 PCl/G U 1.21 1.00 0 1.1.C2 DUP 12/29/2015 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.670 0.114 14733-03-0 PCl/G *0.0968 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.776 0.187 14733-03-0 PCl/G 0.148 1.00 0 1.1.C2 DUP 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.174 0.0601 10045-97-3 PCl/G 0.0528 0.100 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.153 0.0583 10045-97-3 PCl/G 0.075 0.100* 1.00 0 1.1.C2 DUP 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00795 0.0282 10198-40-0 PCl/G U 0.0531 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0129 0.041 10198-40-0 PCl/G U 0.0868 1.00 0 1.1.C2 DUP 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R *0.00279 0.0924 15585-10-1 PCl/G U 0:178 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.113 0.154 15585-10-1 PCl/G U 0.300 1.00 0 1.1.C2 DUP 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.621 0.0829 15092-94-1 PCl/G 0.0771 1.00 17 .8 1.1.C2 DUP 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.677. 0.136 15092-94-1 PCl/G 0.139 1.00 0 1.1.C2 DUP 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.749 0.119 15067-28-4 PCl/G 0.214 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.11 0.206 15067-28-4 PCl/G 0.362 1.00 0 1.1.C2 DUP 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 10.9 1.05 13966-00-2 PCl/G 0.538 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 9.98 1.34 13966-00-2 PCl/G 0.805 1.00 0 1.1.C2 DUP 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0317 0.440 14331-85-2 PCl/G U 0.713 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.633 14331-85-2 PCl/G UI 1.12 1.00 0 1.1.C2 DUP 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.670 0.114 13982-63-3 PCl/G 0.0968 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.776 0.187 13982-63-3 PCl/G 0.148 1.00 0 1.1.C2 DUP 12/29/2015 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.603 0.199 15262-20-1 PCl/G 0.223 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.667 0.195 15262-20-1 PCl/G 0.242 1.00 0 1.1.C2 DUP 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.178 0.0528 14913-50-9 PCl/G 0.0524 1.00 17 .8 1.1.C2 DUP 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.195 0.0797 14913-50-9 PCl/G 0.0705 1.00 0 1.1.C2 DUP 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0721 PCl/G UI 0.101 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.145 PCl/G UI 0.181 1.00 0 1.1.R5 SAMPLE 1/11 /2016 387904 Actinium-227 R EPA901.1 6.50 33.0 14952-40-0 PCl/L U 57.3 1.00 100 1.1.R5 SAMPLE 1/5/2016 387904 ALPHA R EPA 900.0/SW846 9310 -2.57 1.15 12587-46-1 PCl/L U 4.15 5.00 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Antimony-125 R EPA901.1 -4.3 11.5 14234-35-6 PCl/L U 20.2 1.00 100 1.1.R5 SAMPLE 1/5/2016 387904 BETA R EPA 900.0/SW846 9310 -1.44 2.11 12587-47-2 PCl/L U 4.42 5.00 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Bismuth-212 R EPA901.1 42.3 67.1 14913-49-6 PCl/L U 112 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Bismuth-214 R EPA901.1 0.00 14.9 14733-03-0 PCl/L UI 18.0 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Cesium-137 R EPA901.1 0.00 4.73 10045-97-3 PCl/L UI 9.28 10.0 1.00 100

r*

Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method , *Result Uncertainty GAS Units Lab Qua MDL CRDL C Dilution I% Maish 1-1 RS SAMPLE 1/11/2016 387904 Cobalt-60 R EPA901.1 1.92 3.80 10198-40-0 PCl/L u 7.60 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Europium-154 R EPA901.1 -1.34 9.76 15585-10-1 PCl/L u 18.1 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Lead-212 R EPA901.1 6.21 12.8 15092-94-1 PCl/L u 14.9 1.00 100 1.1.RS SAMPLE 1/11 /2016 387904 Lead-214 R EPA901.1 0.00 15.6 15067-28-4 PCl/L UI 19.4 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Potassium-40 R EPA901.1 -17 50.7 13966-00 PCl/L u 89.9 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Protactinium-231 R EPA901.1 11.0 60.1 14331-85-2 PCl/L U 104 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Radium-228 R EPA901.1 -2.9 18.7 15262-20-1 PCl/L U 31.4 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Thallium-208 R EPA901.1 0.00 7.58 14913-50-9 PCl/L UI 5.45 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Tin-126 R EPA901.1 1.19 13.6 PCl/L U 15.6 1.00 100 1.2.C1 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0837 0.370 14952-40-0 PCl/G U 0.680 1.00 24 1.2.C1 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 7.52 3.29 12587-46-1 PCl/G 3.92 4.00 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0215 0.151 14234-35-6 PCl/G U 0.281 1.00 24 1.2.C1 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 931 O/SM 711 OB Modified 24.5 3.81 12587-47-2 PCl/G 3.69 10.0 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.529 0.674 14913-49-6 PCl/G U 1.36 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.909 0.223 14733-03-0 PCl/G 0.201 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 2.52 0.198 10045-97-3 PCl/G 0.102 0.100 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0114 0.0405 10198-40-0 PCl/G U 0.0856 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0436 0.133 15585-10-1 PCl/G U 0.245 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.621 0.130 15092-94-1 PCl/G 0.153 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.926 0.244 15067-28-4 PCl/G 0.205 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 11.7 1.50 13966-00-2 PCl/G 0.645 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.537 0.730 14331-85-2 PCl/G U 1.32 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.909 0.223 13982-63-3 PCl/G 0.201 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.595 0.287 15262-20-1 PCl/G 0.350 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.246 0.090 14913-50-9 PCl/G 0.0946 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0136 0.166 PCl/G U 0.262 1.00 24 1.2.C2 SAMPLE 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.035 0.176 14952-40-0 PCl/G U 0.343 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.017 0.253 14952-40-0 PCl/G U 0.495 1.00 15.8 1.2.C2 SAMPLE 1/11/2016 388092 ALPHA R EPA 900.0/SW846 9310/SM 711DB Modified 6.53 1.68 12587-46-1 PCl/G 2.29 4.00 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.033 0.0658 14234-35-6 PCl/G U 0.128 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0944 14234-35-6 PCl/G

• UI 0.200 1.00 15.8 1.2.C2 SAMPLE 1/11/2016 388092 BETA R EPA 900.0/SW846 9310/SM 711DB Modified 17.0 1.45 12587-47-2 PCl/G 1.69 10.0 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.523 14913-49-6 PCl/G U 0.852 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.557 0.587 14913-49-6 PCl/G U 1.22 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.605 0.126 14733-03-0 PCl/G 0.0912 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.730 0.170 14733-03-0 PCl/G 0.131 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.139 0.0437 10045-97-3 PCl/G 0.051 0.100 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.143 0.0636 10045-97-3 PCl/G 0.0815 0.100 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0124 0.030 10198-40-0 PCl/G U 0.0606 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00831 0.0387 10198-40-0 PCl/G U 0.0741 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0494 0.128 15585-10-1 PCl/G U 0.180 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0202 0.147 15585-10-1 PCl/G U 0.276 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.715 0.132 15092-94-1 PCl/G 0.0806 1.00 15.8

Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result *Uncertainty CAS Units Lab Qua MDL CRDL C Dilution I% Moist(

1.2.C2 SAMPLE 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.892 0.126 15092-94-1 PCl/G 0.117 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.812 0.114 15067-28-4 PCl/G 0.200 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.03 0.209 15067-28-4 PCl/G 0.131 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 13.0 1.06 13966-00-2 PCl/G 0.348 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 14.7 1.52 13966-00-2 PCl/G 0.670 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.388 14331-85-2 PCl/G U 0.530 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.189 0.521 14331-85-2 PCl/G U 0.843 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.605 0.126 13982-63-3 PCl/G 0.0912 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.730 0.170 13982-63-3 PCl/G 0.131 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Radium-228 R DOE HASL 300, 4:5.2.3/Ga-01-R 0.456 0.233 15262-20-1 PCl/G 0.159 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.932 0.262 15262-20-1 PCl/G 0.295 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.226 0.0531 14913-50-9 PCl/G 0.0445 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.185 0.080 14913-50-9 PCl/G 0.0679 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.107 PCl/G UI 0.129 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0471 0.140 PCl/G U 0.161 1.00 15.8 1.3.C1 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0109 0.316 14952-40-0 PCl/G U 0.586 1.00 39.2 1.3.C1 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 7.84 3.45 12587-46-1 PCl/G 3.97 4.00 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.152 14234-35-6 PCl/G UI 0.314 1.00 39.2 1.3.C1 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 25.6 3.77 12587-47-2 PCl/G 3.05 10.0 1.00* 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 1.08 14913-49-6 PCl/G UI 2.21 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.802 0.242 14733-03-0 PCl/G 0.194 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.406 0.144 10045-97-3 PCl/G 0.109 0.100 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0075 0.0663 10198-40-0 PCl/G U 0.136 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.165 0.187 15585-10-1 PCl/G U 0.429 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Lead-210 R DOE HASL 300, 4.5.2.3/Ga-01-R 3.71 0.987 14255-04-0 PCl/G 0.993 4.00 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.879 0.137 15092-94-1 PCl/G 0.156 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.930 0.237 15067-28-4 PCl/G 0.222 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Potassium-40 R. DOE HASL 300, 4.5.2.3/Ga-01-R 14.3 2.24 13966-00-2 PCl/G 0.904 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.752 14331-85-2 PCl/G UI 1.33 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.802 0.242 13982-63-3 PCl/G 0.194 1.00 39.2 1".3.C1 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.03 0.402 15262-20-1 PCl/G 0.434 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.369 0.107 14913-50-9 PCl/G 0.104 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0942 PCl/G UI 0.106 1.00 39.2 1.3.C2 SAMPLE 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0784 0.231 14952-40-0 PCl/G U 0.413 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 . Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.166 0.311 14952-40-0 PCl/G U 0.595 1.00 21.6 1.3.C2 SAMPLE 1/11/2016 388092 ALPHA R EPA 900.0/SW84!) 9310/SM 7110B Modified 11.1 2.15 12587-46-1 PCl/G 2.78 4.00 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0254 0.0997 14234-35-6 PCl/G U 0.166 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0396 0.116 14234-35-6 PCl/G U 0.203 1.00 21.6 1.3.C2 SAMPLE 1/11/2016 388092 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 21.2 1.80 12587-47-2 PCl/G 2.19 10.0 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.39 0.700 14913-49-6 PCl/G 0.852 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 1.07 14913-49-6 PCl/G UI 1.59 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Bismuth-214 R DOE HAS.L 300, 4.5.2.3/Ga-01-R 0.678 0.122 14733-03-0 PCl/G 0.114 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.170 14733-03-0 PCl/G 0.152 1.00 21.6

Area 1.

• Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty CAS Units Lab Qua MDL CRDL CDilution I% MoistL 1.3.C2 SAMPLE 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.405 0.0678 10045-97-3 PCl/G 0.0658 0.100 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.482 0.0947 10045-97-3 PCl/G 0.0637 0.100 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0136 0.0426 10198-40-0 PCl/G U 0.0739 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0129 0.0444 10198-40-0 PCl/G U 0.0907 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0175 0.121 15585-10-1 PCl/G U 0.217 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0122 0.138 15585-10-1 PCl/G U 0.268 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.06 0.104 15092-94-1 PCl/G 0.0882 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.07 0.138 15092-94-1 PCl/G 0.126 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.776 0.142 15067-28-4 PCl/G 0.129 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.31 0.211 15067-28-4 PCl/G 0.388 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 15.2 1.34 13966-00-2 PCl/G 0.547 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 14.2 1.72 13966-00-2 PCl/G 0.877 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.728 14331-85-2 PCl/G U 0.769 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.623 14331-85-2 PCl/G UI 1.05 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.678 0.122 13982-63-3 PCl/G 0.114 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.170 13982-63-3 PCl/G 0.152 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.03 0.216 15262-20-1 PCl/G 0.215 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.02 0.272 15262-20-1 PCl/G 0.309 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.286 0.0695 14913-50-9 PCl/G 0.0568 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.360 0.0938 14913-50-9 PCl/G 0.0771 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.113 PCl/G U 0.111 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.130 PCl/G UI 0.209 1.00 21.6 1.3.C5 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.181 0.293 14952-40-0 PCl/G U 0.568 1.00 39.7 1.3.C5 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 931 O/SM 711 OB Modified. 9.43 3.61 12587-46-1 PCl/G 3.99 4.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Americium-241 R DOE EML HASL-300, Am-05-RC Modified 0.0173 0.0593 14596-10-2 PCl/G U 0.110 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Antimony-1:~5 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0603 0.109 14234-35-6 PCl/G U 0.213 1.00 39. 7 1.3.C5 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 27.0 3.46 12587-47-2 PCl/G 2.52 10.0 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.39 0.906 14913-49-6 PCl/G 1.12 1.00 39. 7 1.3.C5 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.803 0.169 14733-03-0 PCl/G 0.156 1.00 39.7 1.3.C5 SAMPLE 12/4/2015 385101 Carbon-14 .R EPA EERF C-01 Modified -0.459 *a.768 14762-75-5 PCl/G U 1.32 2.00 1.00 39. 7 1.3.C5 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.481 0.110 10045-97-3 PCl/G 0.0796 0.100 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00427 0.0412 10198-40-0 PCl/G U 0.0788 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 3B5101 Curium-242 R DOE EML HASL-300, Am-05-RC Modified -0.00457 0.0394 OER-100-93 PCliG U 0.0913 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Curium-243/244 R DOE EML HASL-300, Am-05-RC Modified -0.0119 0.0359 PCl/G U 0.101 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Curium-245/246 R DOE EML HASL-300, Am-05-RC Modified 0.0382 0.0654 PCl/G 0.0573 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0118 0.149 15585-10-1 PCl/G U 0.277 1.00 39.7 1.3.C5 SAMPLE 12/2/2015 385101 lodine-129 R DOE EML HASL-300,1-01 Modified 0.130 0.576 15046-84-1 PCl/G U 0.928 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.928 0.127 15092-94-1 PCl/G 0.112 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.188 15067-28-4 PCl/G 0.384 1.00 39.7 1.3.C5 SAMPLE 11/23/2015 385101 Neptunium-237 R ASTM C 1476-00 Modified -0.146 0.252 13994-20-2 PCl/G U 0.714 1.00 1.00 39.7 1.3.C5 SAMPLE 11/23/2015 385101 Plutonium-238 R DOE EML HASL-300, Pu-11-RC Modified -0.0042 0.0363 13981-16-3 PCl/G U 0.084 1.00 1.00 39.7 1.3.C5 SAMPLE 11/23/2015 385101 Plutonium-239/240 R DOE EML HASL-300, Pu-11-RC Modified 0.0147 0.0734 OER-100-70 PCl/G U 0.147 1.00 1.00 39.7 1.3.C5 SAMPLE 11/25/2015 385101 Plutonium-241 R DOE EML HASL-300, Pu-11-RC Modified -1.82 5.80 14119-32-5 PCl/G U 10.1 15.0 1.00 39.7

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Area 1 Sample No. Type Analyzed SDG P_arameter Fraction Method Result Uncertainty CAS Units .Lab Qua MDL CRDL C Dilution I% Moistt 1.3.C5 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 14.2 1.66 13966-00-2 PCl/G 0.807 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0888 0.620 14331-85-2 PCl/G u 1.03 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.803 0.169 13982-63-3 PCl/G 0.156 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.665 0.382 15262-20-1 PCl/G 0.300 1.00 39.7 1.3.C5 SAMPLE 12/2/2015 385101 Strontium-90 R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified -0.321 0.889 10098-97-2 PCl/G u 1.76 2.00 1.00 39.7 1.3.C5 SAMPLE 11/29/2015 385101 Technetium-99 R DOE EML HASL-300, Tc-02-RC Modified 1.57 2.00 14133-76-7 PCl/G u 3.38 5.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.354 0.0817 14913-50-9 PCl/G 0.0704 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-228 R DOE EML HASL-300, Th-01-RC Modified 1.40 0.595 14274-82-9 PCl/G 0.449 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-229 R DOE EML HASL-300, Th-01-RC Modified -0.0406 0.122 15594-54-4 PCl/G U 0.344 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-230 R DOE EML HASL-300, Th-01-RC Modified 0.803 0.444 14269-63-7 PCl/G 0.343 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-232 R DOE EML HASL-300, Th-01-RC Modified 0.616 0.381 7440-29-1 PCl/G 0.168 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101" Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.163 PCl/G UI 0.130 1.00 39.7 1.3.CS SAMPLE 12/2/2015 385101 Tritium R EPA 906.0 Modified 2.71 . 2.71 10028-17-8 PCl/G 4.45 6.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-232 R DOE EML HASL-300, U-02-RC Modified 0.0644 0.127 14158-29-3 PCl/G U 0.225 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-233/234 R DOE EML HASL-300, U-02-RC Modified 0.656 0.320 13968-55-3/1391 PCl/G 0.261 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-235/236 R DOE EML HASL-300, U-02-RC Modified 0.0709 0.121 15117-96-1/139: PCl/G 0.106 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-238 R DOE EML HASL-300, U-02-RC Modified 0.954 0.367 7440-61-1 PCl/G 0.106 1.00 1.00 39.7 1.3.C6 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.478 0.464 14952-40-0 PCl/G u 0.775 1.00 23.6

. 1.3.C6 SAMPLE 12/3/2015 385101 ALPHA. R . EPA 900.0/SW846 9310/SM 7110B Modified 7.80 3.22 12587-46-1 . PCl/G 3.91 4.oo 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Americium-241 R DOE EML HASL-300, Am-05-RC Modified 0.0315 0.062 14596-10-2 PCl/G 0.0859 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0263 0.202 14234-35-6 PCl/G U 0.369 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 BETA R EPA 900.0/SW846 931 O/SM 711 OB Modified 18.3 2.99 12587-47-2 PCl/G 2.69 10.0 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.725 1.19 14913-49-6 PCl/G U 2.35 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.289 14733-03-0 PCl/G 0.255 1.00 23.6 1.3.C6 SAMPLE 12/4/2015 385101 Carbon-14 R EPA EERF C-01 Modified -0.833 0.891 14762-75-5 PCl/G U 1.55 2.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.357 0.122 10045-97-3 PCl/G 0.178 0.100 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0195 0.0816 10198-40-0 PCl/G U 0.153 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Curium-242 R DOE EML HASL-300, Am-05-RC Modified 0.00 0.0412 OER-100-93 PCl/G 0.061.3 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Curium-243/244 R DOE EML HASL-300, Am-05-RC Modified 0.00921 0.0512 PCl/G U 0.0981 1.00 1.00 23.6.

1.3.C6 SAMPLE 11/24/2015 385101 Curium-245/246 R DOE EML HASL-300, Am-05-RC Modified 0.0361 0.0709 PCl/G 0.0983 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00356 0.241 15585-10-1 PCl/G U 0.468 1.00 23.6 1.3.C6 SAMPLE 12/2/2015 385101 lodine-129 R DOE EML HASL-300,1-01 Modified 0.214 0.383 15046-84-1 PCl/G U 0.769 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.34 0.197 15092-94-1 PCl/G 0.181 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.09 0.363 15067-28-4 PCl/G 0.580 1.00 23.6 1.3.C6 SAMPLE 11/23/2015 385101 Neptunium-237 R ASTM C 1476-00 Modified -0.0342 0.236 13994-20-2 PCl/G U 0.575 1.00 1.00 23.6 1.3.C6 SAMPLE 11/23/2015 385101 Plutonium-238 R DOE EML HASL-300, Pu-11-RC Modified 0.00979 0.0544 13981-16-3 PCl/G U 0.104 1.00 1.00 23.6 1.3.C6 SAMPLE 11/23/2015 385101 Plutonium-239/240 R DOE EML HASL-300, Pu-11-RC Modified 0.00677 0.0799 OER-100-70 PCl/G U 0.168 1.00 1.00 23.6 1.3.C6 SAMPLE 11/25/2015 385101 Plutonium-241 R DOE EML HASL-300, Pu-11-RC Modified -2.07 6.40 14119-32-5 PCl/G U 11.2 15.0 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 13.9 2.27 13966-00-2 PCl/G 1.05 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.801 0.980 14331-85-2 PCl/G U 1.81 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.289 13982-63-3 PCl/G 0.255 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.892 0.403 15262-20-1 PCl/G 0.526 1.00 23.6 1.3.C6 SAMPLE 12/2/2015 385101 Strontium-90 R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified -0.122 0.659 10098-97-2 PCl/G U 1.34 2.00 1.00 23.6

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Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty CAS Units Lab Qua MDL CRDL CDilution 1% MoistL 1.3.C6 SAMPLE 11/29/2015 385101 Technetium-99 R DOE EML HASL-300, Tc-02-RC Modified 1.60 1.76 14133-76-7 PCl/G 2.95 5.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.381 0.168 14913-50-9 PCl/G 0.131 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-228 R DOE EML HASL-300, Th-01-RC Modified 0.984 0.482 14274-82-9 PCl/G 0.395 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-229 R DOE EML HASL-300, Th-01-RC Modified 0.131 0.207 15594-54-4 PCl/G 0.287 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-230 R DOE EML HASL-300, Th-01-RC Modified 1.16 0.498 14269-63-7 PCl/G 0.286 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-232 R DOE EML HASL-300, Th-01-RC Modified 0.979 0.452 7440-29-1 PCl/G 0.155 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.185 PCl/G UI 0.177 1.00 23.6 1.3.C6 SAMPLE 12/2/2015 385101 Tritium R EPA 906.0 Modified 1.95 2.00 10028-17-8 PCl/G 3.30 6.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-232 R DOE EML HASL-300, U-02-RC Modified 0.0473 0.121 14158-29-3 PCl/G u 0.222 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-233/234 R DOE EML HASL-300, U-02-RC Modified 0.799 0.301 13968-55-3/1391 PCl/G 0.214 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-235/236 R DOE EML HASL-300, U-02-RC Modified 0.0469 0.0921 15117-96-1/1391 PCl/G 0.128 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-238 R DOE EML HASL-300, U-02-RC Modified 1.14 0.345 7440-61-1 PCl/G 0.0796 1.00 1.00 23.6 1.3.C6 MSD 12/3/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 80.3 13.2 12587-46-1  % 5.73 4.00 1.00 23.6 1.3.C6 MSD 12/3/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 97.1 17.4 12587-47-2  % 5.68 10.0 1.00 23.6 1.3.C6 MS 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 96.6 16.0 12587-46-1  % 7.76 4.00 1.00 23.6 1.3.C6 MS 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 99.8 17.4 12587-47-2  % 6.22 10.0 1.00 23.6 1.3.C6 DUP 12/3/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 11.5 3.55 12587-46-1 PCl/G 3.63 4.00 1.00 23.6 1.3.C6 DUP 12/3/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 23.2 2.99 12587-47-2 PCl/G 2.17 10.0 1.00 23.6