ML16294A196
Text
Appendix G-Sub-Area 3.1.16-3.1.18-COA
I GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843} 556-8171 - www.gel.com Certificate of Analysis Company:
Address:
MJW Corporation l 5 Ha7.clwnod Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
- 3. !. !6.R.I Sample ID:
385070007 Matrix:
Soil Collect Date:
2 l *OCT-15 Receive Date:
05-NOV-15 Collector:
Client Moisture:
- 18. l %,
Gravimetric Solids AST.MD 2216 % Moisture As Received" Moisture Rnd G:un.ma Spec Analysis 18 I Gammaspec. Ge1mma. So(id "Dry Weight Correc1ed" Actimu111-227 U
-0.0964
+f-0.260 Anlimony-125 U
-0 0282
+/-0.112 Bismuth-212 Ul 0 00
+/-0.914 Bismuth-214 Ccsium-137 Cobalt-60 Europium-154 l.cud-212 Lcad-214 Potassium-40 Prolactmium-231 Radium-226 Raduim-228 Thallmm-208 Ul u
u 06fi2 I 75 0.00
-0.0231 0.930 0.944 11 7 0.306 0 682 0.716 lJ 278 Tin-l 26 U
0.0837 R~1d Gas Flow Proportional Counting GFPC Gross ArB. solid Dry Weight Corrected" Al~a 1~7 Bela 21.7 Tile following Prer :Vlelhods were performed
~i~th~d****--- * ** *
- o~~~rifi1ion **** ***- *-* ******
- Diy Soil Prep DT)* Sot! Prep GL-RAD*A-021
+/-0.167
+/-0.161
+/-00414
+l-0 114
->*/-0 129
+l-0 22ll
+f-1 55
+/,O 558
+/-0 I C17
+l-0 295
+I-\\} 0785
+/-0.143
+/-3 55.
+f-1 59
- i:~~- f<J:l.l?~vi11g,\\n al_~:t_ical !"1.etho.J.s_ ~vc.r:c per._fl)r.IU.l!d.,...
Method Description 2
3 ASTM D 2216 (Mod1ticd)
DOE HASL 300, 4.5 2 3/Ga*O 1-R EPA 900.0fSW846 93 lo;sM 71 IOB Modified Surl"O~ate!fr:1ccr Recovery Tes I Le 0.494 0 230 O:W6 0 0948 1.23 0 564 0 139 0.0628 0.0756
() 11339 00968 0 0423 0.\\91 1)()791 (J,"163 00778 0.149 0 0585 0 702 11291
\\.12 0.525 0.139 0.0628
() 279 0 123 00696 0 0313 ll 193 0 0922 3.98 l 77 2.91 1 38 Analyst CXCI Report Date:
December 17. 2015 Project:
Client ID:
MJWCOOll5 MJWCOOI percent CXCI l lfl0il5 1319 1521842
+1-0264 pCilg RXF'2 12!03115 1303 1522383 2
+f-ll 112 pCi/g
+1-1 00 pC1/g
+/-0 177 pCi/g
+/-0215 0.100 pC1!g
+/-0 0459 p("i/g
+/-0.114 pC110\\
+/-0.152 pCi/g
+1-0.234 pC1/g
+f-1.84 pC1/g
+/.{) 57')
pC1/g
+1-0 177 pC'1lg
+/-0 309 pC1.'g
+/-0.0818 pCi/g
+f-0.144 pCJ/g
+/-4.64 4 00 pC1/g.
KXB2 12102115 11 l 6 1525757
+/-4.02 10.0 pC1/g Date Time Prep Batch 1111011.)
1319 1521842 Batch ID Recovery%
Acce1>table Limits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company:
Address:
MJW Corpomtion 15 Hazelwood Drive Suite I 12 Buffalo. New York 14228
Contact:
M~. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
3.1.16.R.I Sample ID:
385070007 Certificate of Analysis Report Date:
December 17. 2015 Project:
MJWCOO 115 Client ID:
MJWCOOI "I '.
, \\,
raram_etc.r -* _....... -*...... qu_a_l_i.fi!r:... *-. R.c.s.u.lt_. _ !'.11."-ert_l)_in~*
.. :\\IP..~~****... !~_c_....
. TP.J'........1~~.. ~!.n.i.ts.. I?.F.r\\na_lyst... P~~~-1-:~~1~_.Ba~~~-.. l\\'!~~-*
Surrogate!fracer Reco\\'ery Test Batch llJ Recowry%
Acceptable Limits Notes:
TPU and Counting Uncertainty are calculated at the 95% confidence level (-1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company:
Address:
MJW Corporation 15 Hazcl'\\\\."(lOd Drive Suite! 12 Buffalo. New York !4228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotop~s Client Sample ID:
3.1.16.R.l Sample JD:
. 385070007 Matrix:
Soil Collect Date:
2 l -OCT-15 Receive Date:
05-NOV-15 Collector:
Client Moisture:
l&.1%
Parameter Gra,*inietric Solids ASTM D 2216 % Moist11re "As Received
Moisture Rad Gamma Spec Analysis l&.1 Certificate of Analysis Project:
Clienl ID:
Report Date:
December 17, 20 I 5 MJWCOOl 15 MJWCOOl percent CXCI 11/10.'IS 13\\9 1521842 Gammaspec, Gamma, Solid "D1:i' Weig/11 Corrected" Actimum-227 U
-0.0964
+/-0 2fl0
() 49.J 0230
.;./.Q.264 pC1/g RXF2 12;03115 1303 1522383 2
t\\J1t1mony-125 l!
-002&2
+/-0 112 Bismuth-212 Ul O.UO
+1-0 914 Bi~mmh-214 0.682
+i-0.167 Cesrnm-!37 Cobalr-60 Europium-154 Lead-212 L~ad-214 Pnlassium-40 Protaclmmm-231 Radium-226 Radium-228 Thallium-208 UI v
u Tio-126 U
Rad Gas Flow Proportional Countiug l 75 0.00
-0.0232 (J 930 0.944 11 7 0.306
() 682 0716 0.278 0.0837 GFPC. Gross../:B. solid "D1:l' Weigh1 Corrected" Alphu 14 7 13eta 21.7 l_"hC. foll.o:w.ing [>rc.p.'.\\l.c.t.~.~ds.. w~r.c.P.~':!"o~'Tll:tl.
Methot!
Description Dry Soil Prep 0!)* So1r Prep GL-RAD-A-021
+/.Q.161
+/-00414
+/-0. l\\4
+/-0.1.29.
+/.() 220
+/-\\ 55
+1-0.558
+/-0 167
+/-0 295
+f-0 0785
+/-0.143
+/-355
+l-2.59 i:~~ _f~!J~_wint::.'.\\n!J!Y.t.i~!l_l_ ":'.~ct_h.o~s '~~.i:e_ p_er~o_rn:!e~...
Methot!
Oesl'.ription 2
3 ASTM D 2216 (Modified)
DOE l*IASL 300_ 4.5.2 3/Ga-01-R F.PA 900 OISW846 9310/SM 71 IOB Modified Test
() 206 l 23 0 13\\J 0.0756 IJ096H
()I'll 0 163 0.149 0 7(12 I 12 0.139 0279 0.0696 0.193 3 98 2 91 (I 0948 0.564 0.0628 0.0339 00423 00791
() 0778 (I 0685 0 291
() 525 0 0628 I) 123 00313 0.0922 1.77 t 38 Analyst C.XCI
+/-0. \\ \\2 pCt/g
+I-\\ 0(1 pC1/g
+/-\\) 177 pC1ig
+/-0.215 0 100 pCi/g
+!-0 0459 pCi/g
+/-0.114 pCilg
+/-0.152 pC1/g
- /-0.234 p(\\ig
+l-1.84 pCilg
+/-0 579 pCi!g
+/-0 177 pC1lg
+/.() 309 pC1/g
+1-ll 0818 pC1lg
+l-0 144 pCi!g
+/-4 64 4 uo p('ilg KXB2 12102115 \\ \\ 16 1525757
+/-402 JOO pCllg Date Time Prep Batch ll/l0115 1319 1521842 Batcb JD Recow:ry%
Acceptable Limits Su!"'rogatc{fraccr Recovery
~**..................
3
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171
- www.gel.com Company:
Address:
MJW Corporation 15 Hazelwood Drive Suik 112 Buffalo, New York !4228
Contact:
Ms. Laurie Lose}
Project:
Soil Radioisotopes Client Sample TD:
3.1.16.R.l Sample ID:
385070007 Parllmeter Surrogat"cffracer Re~overy Test Notes:
Certificate of Analysis TPC TPU and Counting Unce1tainty arc calculated at the 95% confidence l<?vcl { 1.96-sigma).
Report Date:
December l 7, 201 S Project:
MJWCOOl 15 Client ID:
MJWCOOl RL. ~'.n~ts....l.J.F.. A~1.~lysf..... _D_11_t_i:.}*.iIJ1~.ll.a.tch Mtd.
Batch ID Recovery%
Ai:ccptablc Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:
Addres~:
Contact:
MJW Technical Services 15 Hazt!lwood Drive Suite 112 Buffalo. Nev. York 14228 Ms. Laurie Lo~cy Project Soil Radioisotopes Client Sample JD:
3.1.16.R.2 Sample ID:
389296012 Matrix:
Soil Collect Date:
2 !-OCT-! 5 Receive Date:
14-JAN-16 Collector:
Client Moisture:
16.6%
P:1rametcr
...............9~:1Jifier,....... Resu It_..... Fncel'h!i.~~'.t.......... ~1,0C Gravimetric Solids ASTA,/ D 2216 % Moismre "A.1 Reaived
Moisture 16.6 Rad Gamma Spec A11a!ysi~
Gamma with Ingrowth "Dry Weight Corrected" Actmmm-227 u
0.186
+/-0317 I) 567 Antunony-125 Lil 0 00
+/-(), 128 0256 Bismuth-212 Ul 0.00
+/-0 641 Ill 131smuth* 214 0.635
+/-0 180 0 J.J6 Ccsium-137 2.48 t/-0 176 0074 Cobalt-60 l!
-0.0267
+/-0 0439 00788 Eurapium-154 lJ
-0 0256
+/-0.136 0226 Lcad-212 07().l.
+l*O 128 0 132 Lcad-214 I 07
+/-0.214 0 340 Potassium-40 12.l
+/. t.57 0.510 Protactmium-23 l u
0.349
+f-0 57l I IJ Rndium-226 0.635
+f-0 180 0 146 Rudiun:i-228 0.663
+f-0 302 0 2'1-2 Thallmm-208 0 248
'+1-0.0756 0.0777 Tm-126 u
0.0248
+/-0 173
- 0. 170 qammaspec, Gamma. Solid "D1:v Weight Cu1-rected" Aclinium-227 u
- -0.0361
+/-0.247 0449 Aimmony-125 lJ
-0.081
... /.(! 107 0.!86 Bismuth-212 lll 0.0\\J
~1-0 503 09&8 Bismuth-214 0.475
+l*O 125 (J 117 c~~ium-137 2 *II
+/-0 138 0063 C'obalt-60 u
0.0219
+f-0 0352 0.0715 Europmm-15.J u
-0.0751
~l-0 105
- 0. l&I Lcad-212
() 829
+/-0 108 0 0995 lcad-214 0.684
+/-0 134 l) 122 Potassium-40 12.5
+/-! 26 0452 Prolactmu1m-2J I l.'
-0 189
+/-0.462
() 816 Ra<lmm*226 (1475
+/-0. 125
() 117 Radium-228 0.8.42
+1-0 214 0.2\\5 Thalhum-208 0220
+/-0 0636 0 0533 Ttn-126 Ul 0()0
+/-() 145
() 140 Rml Glls Flow Proportional Counting GFPC Gross A*B, solid "D1:v Weight Corrl!cted" Alpha 8 99
+1-3.55 3.91 Beta 17 0
+1-2.71 z 56 Le 02.66
..-1-i) 329 (J,\\20
+/-0 139 (1.501
+/-0.717
() 0663
+!-0 \\88 0.0331
+/-0.278 o.o:m
- /..fl.0456 0.096
<-/.{), 137 P0626
'+1-0 140 0 164
+!-0 232
- 0. 193
+/-\\ &S 0.530
+f-0 5<j7 00663
+/-0 188 (l 104
+i-0 317
()IJ353
+/.() 0787 0.08ll9
+J-0 174
()213
+1-0 247 0 0877
+f-ll l !3 0463
- 1-0.947 0 0546
.. /.() 13!
110292
+/-0.139 0 0323
+/-l) 0366 0 0811
- l-0 110 oil4n
<-/-0. l27 0 057
+/-0. 145 0192
~:-1.66 (J.385
+/-0.472 0 0546
+/-0. 131 0.0977
+1.n 253
{) 0245
... /-ll.0662 0 0667
+1-0 14:'
l 56
+/-3.95 1.17
+t-~. 73 Project:
Client ID:
RL Report Daie:
MJWC00115 MJWCOOl February IO, 2016 Units DF Anlll;rst... DatcJi_m~. B.a.tch Mtd.
.percent CXCl 0!114'16 1208 1537312 pC'1/g
.RXF2 02105'16 0843 1537546 2
pC1/g.
pCilg.
pCi/g 0 100 pC1ig pC1/g pCi!g pCi!g pCi/g pC1tg pCitg pCl/g pClfg pC1/g pCi/g pCi/g RXF2 Oll18116 1123 1537545 3
pC'i!g pCilg pCilg 0100 pCtlg pCi!g pCilg.
pC1/g pC1/g pC11g pCilg pCi/g pCi/g' pC1ig pCi/g 4 00 pC1/g KXB2 (1*1126/16 1152 !539462 4
\\0 0 pCi/g
GEL LABO RA TORlES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company; Address:
MJW Technical Services 15 1-lazelwood DriH!
Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project
. Soil Radioisotopes Client Sample ID:
- 3. l.16.R.2 Sample ID; 389296012 Certificate of Analysis Report Date:
February 10.2016 Project:
MJWCOO 115 Client ID:
MJWCOOI
~...............
Parameter
. _Ri:st~~~-...... U.11.~.l'.r.~ain.ty__.... ~:l[)C'...... L~.............. i:r.i;_...... ll~ __ ~~ni.t~... O.l'... _AJ)_~ily~t. Date Tl me Batch Mttl.
- r..11~. f()!l.owi_ag r.r.e.e_ ~t.~.t~o£s. '~e_r':.P~:rfo.r.111.~d....... "... -* '
'.\\let hod Description Dry Soil Prep Dry Soil Prep GL-RALl-A-021 1.'~c.. f<!.!~o~i_nll.'.\\nal1ti~a.1.. :VIe_tl.1<1d~. '"~r.~J?.l'.l;f().r~.l!d....... _.
Mel bod Description 2
3 4
ASTM D 2216 (Modified)
DOE HASL 300, 4 5.23/Ga-01-R DOE HAS!. 300, 4.5 2 3!Gn-IJ 1-R EPA 900.0iSW846 93Hl!SM 7\\ \\OB Mnd1ficd Test Analyst CXC1 Sm*rogate(fraeer RecoYcry Notes:
Dnte OllW\\o TPU and Counting Uncertainty are calculated at the 95% con fide nee level ('l.96-sigma).
Time 1208 Prep natch 1537311 llatch ID Rcco,*ery%
Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: Dec em her 4, 2015 Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample lD: 3. LI 6.R.6 Sample ID:
385070008 Matrix:
Water Collect Date:
2 l*OCT-15 14: I 5
. Receive Date:
05-NOV-15 Collector:
Client Project:
Client ID:
MJWCOOl !5 MJWCOOJ Parameter
. _.C??~l!f~~!..... _.Result Unc~rtaint:L.... Ivl.g~~... -.... __ RL Rad Gamma Spec Analysis Gammaspec, Gamma, Liquid (Standard List) "As Received" Actimum-227 ll 23 {1
+/-29 6 55.3 Antimony-125 U
-8.67
+/-l I 0 18 0 Ccsium-137 U
0 378
+/-4 01 7.52
.\\[).0 Cobalt-60 lJ 0318
+/-4.94 952 Europmm-154 ll I 81
- l-l2 7 2~ l'I Protactim11m-23 I U
24 2
+1-51.3 94.5 Radium-228 U
-22 7
+/-22.3 28.6 Tm-1~6 U
-68
+/-144 Hill Rad Gas Flow -Proportional Counfo1g GFPC. Gross A/B, liquid As Received" Alpha ll
-0.489
+/-) 76 3.75 5.00 Beta U
-2 58
+/-2 47 4 94 5 00 T_he_ ~0_1l()\\'.'i.11i; ~Il~l_Y_ti_c~l.. Me~~.~?:.. w~rc P.~~f~.~IIJe<l.:...................
M.~~~~~........................... P~~~~m.~i9_q....... _ ******-*...
I EPA 901.l 2
EPA 900.0tswg.169310 Notes:
Counting Uncertainty is calculated at the 95'% confidence level ( 1.96-sigma).
Units p(1il.
pC1!1.
pCi!L pC1/\\.
pC1/L pC1!L pCi/L pC1/L pC11L pCi/L MJHI 11117115 0657 l5219l5 JXB7 l210211S 1303 1525771
........ A.!1al_yst.<;9111!:rJe.!.l.~........... _.......
2
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company:
Address:
MJW Corporalion 15 Hazelwood Drive Suite !12 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sarnple ID:
3.1.16.R.6 Sample ID:
385070008 Matdx; Water Collect Date:
21-0CT-15 Receive Date:
05-NOV-15
...... ~<.?!Je~~o.r;_............. (l.i.~_l_l!._.. _... _.......,........... ****-....................
Rrstl Gamma Spec A11alysis Gammaspec. Gamma. I.iquid (Standard List) '~1s Received" Actmium-227 u
23.6
+1-29.6 55.3 26.2 Anumony-125 ti
-&.67
+1-11 0 18 0 836 Bismu!h-212 u
31 4
+f.54 8 HIS 49 3 Bismu!h-214.
u
-12 8
+1-10.9 16 5 7 68 Ccsium-137 lJ 0.378
+/-4.tll 7.52 3.44 Cobolt-60 Li
- 0. 318
+/-494 9 52 426 Eumpium-154 lJ l-81
+/-12 7 250 II I l.ead-212 UI 0.00
+ i-rn.9 12.5 5 95 Lcad-214 u
-! 37
+/-11 5 169 7.96 Po!llSsium-40 ll
-279
+/-56.9
!01 45 7 Protaclinium-23 l tJ 242
+l-51 3 94 5 44.5 Radiwn-228 lJ
-22 7
+/-22.3 28 (i 129 Thallrnm-208 UL 0.00
+1-5"92 6.62 J.02 Tm-126 u
-6.8
+l-!4.4 if1.0 7 66 Rad Gas Flow Pro11ortional Counting GFPC. Gras::; A-B. liquid "As Receiwd" Alpha u
-0 489
+/-l.76 3 75 I 56 Beta u
-2.58
+1-247 494 2.27
~h.c f?.!l~lv_i_ng_ ~~.nal_yl_icl:l.!~"~c.:1.ho~s..,\\'.C.1"~. F~!.~!'r.."!e~........
Method Descriptinn TPl'
+/-31.7
+1-11 7
+J-56 7
+/~!2.i /-4 01
+*1-4.94
+/-\\2 7
+/*11 0
+/-11.5
+/-58.3
+/-52.7
+/-24 7
+!-6 OJ
+1-14 8
+/-\\.76
+/-2 47 EPA90l.\\
2 EPA 900 O/SW846 9310 Snrrogatc/Tracer Recovery Test Notes:
TPU and Counting Uncertainty are calculated at the 95%1 confidence level (I.96*sigma}.
Report Date:
December L 7. 2015 Project:
Client ID:
l'v!JWCOO 115 MJWCOOI RL Vuits pCilL MJHI 11117/15 0657 1.521915 pCi1L pC1IL pC11L
. 10.0 pCllL pCi/L pC1IL pC1/L pCiiJ.
- pCiil pCi!L pCi/L pCi/1.
pC1IL 5 00 pC1/L JXB7 12/02115 1~03 1525771 2
5 OU pC'1/I.
Batch !D Rc.covery% Acceptnblt> Lilllit.~*
- GEL LABO RA TORIES LLC 2040 Savage Road Charlest~.rn SC 29407 - (843) 556-8171 -www.gel.com Company:
MJ W Corporatio.n Address:
15 Ha7.Clwood Drive Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
- 3. LI 6.R.6 Sample ID:
385070008 Matrix:
Water Collect Date:
21-0CT-15 Receive Date:
05-NOV-l 5 Col!~c~qr:_....... -*... C.1 iel)t..
Result Rad Gamma Spee Analysis Certificate of Analysis MD~'....... :r:-~..... TP_r.
Gammaspec, Gamma. liquid (Srandard lisl) "As ReceNed" Actmmm-227 u
23.6
+1-29.6 55.3 262
+1-.ll.7 AntimoRy-I 25 u
-8.67
+/-11 0 18.0 8 36
+i-11.7 Bisrnuth-212 u
31.4
+/-54 8 lll8
,i93
+1-56.7 Bismulh-214 l.l
-12 8
+/.JO 9 16.5 7.6S
+l-12.4 Ccsium-137 u
0.378
+l-4 Ol 7 52 344
+/-4.01 Cobali-60 u
0.318
+/-4 94 9 52 4.26
- H-4 94 Europium-154 u
I 81
+/-12 7 25 0 11.l
... 1-12 7 Lcad-212 Ul 000
+/-109 12 5 5.95
+/-11.0 Lead-2 l 4 I.I
-l 37
+l-11.5 16 9 7.96
+/- l 1.5 Pota;;sium-40 u
-27 9
+1-56.9
\\01 45 7
+l-58 3 Prmactm1um-23 l u
24.2
+!-51 3 94.5 44.S
+/-52 7 Radium-228 ll
-22.7
+/-22 3 28.6 12.9
+/-24.7 T1ialli11m-208 UJ 0 00
+/-5.92 o.62 3 02
+f.(J 01 Tin-126 u
-68
+l-14 4 16 0 7 66
+/.14 8 Rad Ga5 Flow Proportional Counting GFPC. Gross A,B, liquid "As Received" Alpha u
-0.489
+/-1 76 3 75 l 56
+/-1.76 Bela u
-2.58
+1-2.47 4.94 2.27
+/-2 47 T.~~. ~oll1?~.i.11g. AIJ.~!~:t.icai ~etli.c:i.':'s. \\\\:ere JlJ!.rf~.i::rn.cd.
Method Description EPA90l I 2
Ef'A 900 O/SW846 CJJIO Surrogatefl'racer Recovery Tes!
Notes:
TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
Project:
Client ID:
Report Date:
December 17; 2015 MJWCOOll5 MJWCOOI pC'ifL MJHI I lll7/J5 0(157 1521915 pC1/L pCiil..
pCi/L 10.0 pC111.
pCi.11..
pCi/L pC1.IL pC1/L pC1/L pCi!L pCJil..
pC1iL pCiiL 5.00 pCi/L JXB7 12/02115 1303 1525771 2
5.00 pC11L
'Batch ID Recovery% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate ofAnalysis Repo11 Date: December 4, 2015 Company :
MJW Corporation Address:
15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Cot1tact:
Ms. Laurie Losey Project:
Soil Radioisotopes 0
- OM..
000 0
0 0
Client Sample JD: 3.1.17.R. l Sample ID:
385070009 Matrix:
Soil CollectDate:
20-0CT-15 10:40 Receive Date:
05-NOV-15 Collector:
Client Moisture:
21 %
Project:
Client ID:
MJWCOOl lS MJ\\VCOOl Parameter
........ Qu_al.. i~e.'....... ~~s~.l~.... U!1cert~in_ty.... *---~1.1?\\....... ~
Unit~
Gravimetric Solids ASTM D 2216 % Moisture "As Received" M ois1ure
- 21. O percent CXCI I lflOll5 13\\'I 1521842 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 U
-0 0672
+/-() 346 Antimony- !25 U
0 0605
+/-0. !57 Ccsrnrn-137 0.935
+l-0 133 C'obal!-60 U
-2 82£-05
+/-0.0516 Europmm-154 U
-0 I \\2
.,./-0 235 Protactmium-231 U
0 403 t/-0 712
- Radium-226 l 05
+/-0 !97 Rad1w11-22B I 04
+/-0.329 Tin-126 u
O.U48 t
.,.,.o.154 IJ.631 pC1/g 0.272 pCi/g 00906 0 100 pCilg 0.103 pC1/g 0.336 pC1lg 1 23 pCi/g 0 163 pCtig 0 324 pOlg 0.220 pC1/g RXF2 l2i03fl5 1303 1522383 2
Rad Gas Flow Proportional Counting GFPC', Gross AiB, solid "Diy Weight Corrected" Alpha 1 l S
+1-2 94 O.cta 24.4
+/-2.64 3..\\6 4.00 pCilg 3 11 10.0 pCi/g KXB2 121021\\5 1128 1525757 3
Th~. foH_~~ill.~. ?.£er_M_et~<?.~~.~e.~e_p~rf~~r!1e1.: __
Method Description Dry Suii" rrc*p*-* --**--
-...... br;;*soi1'PrCP"GL~i~A"t5~i't~t)it°'-...
Analyst Date
- .......... c-xti ** ***-**... 1'ilfoii5 Time Prep Batch
- -- -1"3°"i9- -****
- 1sii842. * * * **-* * * * * * ****- *- ** * ***
Tbe following Analytical Methods were performed:
-~1~t~.94.: __.. **:*~: *.... ::: **:**J~es~~til:ii*~~-.:.. *::*:.. *.~.. :.*.*-.:.*::.: *:.*:.*_....
ASTM D 221 (> (Modified) 2 DOE HASL 300.4.5 2.3iGa-01-R J
EPA 900 O.iSW846 9310/SM 71 lOB Mo<ltfted Notes:
Counting Uncertainty is calculated at the 95% confidence level ( l.96-sigma).
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:
Address:
Contact:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffa!o.NcwYork 14228 Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
3.1.17.R.l Saml?te ID:.
385070009 Matrix:
Soil Collect Date:
20-0CT-l 5 Receive Date:
05-NOV-15 Collector:
Client Moisture:
21 %1 Paramet.c!:_......
............ 911~.lijj~~--...
Res~~-'...... r_!!_cer,tai'!t.Y.
Gravimetric Solids AST<\\-[ D 2216 % Moisture ",1s Received" Moisture 21 0 Rad Gamma Spec Analysis Gammaspec. (iµmma. Solid Actimum-227 "DJ}' Weight Corrected" u
-0.0672
+/-0 346 Anumony-125 u
0.0605
+f-0. 157 B1smuth*2 l 2 U!
0.00
+/-ll.727 Bismuth-2 l 4 1.05
+l-0 l 97 Ccsium-137 0.93S
'"l-0 \\J3 CobalH10 Europmm-*154 Lead-212 U
-2.82E-05 u
-0.112 I 04
+/-0.05.16
+/-0.235
+/.() 154 Lead-214 l.19
+/-0.231 Potassrnm-40 Protactinium-231 u
\\3 0 0.403 1.05
+/-L65
+/-0 712
+1-0 197 Radium-228 I 04
+J-0 329 Thallmm-208 Tm-\\26 u
Rad Gas Flow Proportional Cuunting 0426 0.04&1 CFPC. Gross A.-B, solid "Dl'.l' Weight Cori*ected" Alpha 11 8 llib N4
!~e _fol~().\\V.\\~g f:r._eP. _~l~h.ods.,v_er.:e p~~forme.d......
- \\'.lethod Description Dry Soil Prep Dry SOii l'rcp GL-RAD*A-021 Th_c.li)l![)\\!ii:tg A 11al~*_1i~,~-1._ry1_et~_[)d.s. wer:"... r~rf'!~*.111~d_
'.\\>1ethod Description ASTM 02216 (Modified) 2 DOE l!ASL JOO, 4.5.2 3/Ga-01-R
+!-0.0914
+/-0.154
+/-2 94
+/-2.64 3
El'A 900.0/SW846 9310/SM 71 !OB Modilied
~me l,c 0 631
(} 295 0.272 0.126 l SR o 729
- 0. \\63
() 0738 0.0906 0 0408 (1 103 IU.1443 0.336 0 149
. 0.142 Oll666 0406 l) 196 0 '102 0 380 I 23 0.57\\
0.163 0.073&
0.324 (1.143 0.0781 0 035
() 220 0 106 3.46 1.56 3.Jl l.50 Aiudy~t Project:
Client ID:
.Trr.....
RL Report Date:
December ! 7. 2015 MJWCOO!l5 MJWCOOI percent CXC!
\\lf\\()/15 JJ\\9 1521842
+/-0 3.+8
+1-0 160
+/.0.92\\
+l-0 218
+1-0 157
+l-0 0516
+/-0.240
+f-0.181
.,./-0.254
+i-1.98
+1-0 741
+l-0 21&
+/-0 366
+f-0 (}99
- -/-0. l 55
+/-3.80
+1-4.35 Date 0 !llO 400 lll.O pC1/g pCi.tg pC1/g pCi/g pCtfg pCi!g pC1lg pCi!g pCi/g pC1/g pCilg pCi/g pC1/g pCi/g pCilg pC1/g pCilg Time RXF2 12103/15 1303 U22383 KXB2 12102/15 1128 1525757 Prep Batch CXC\\
11110/15 1319 152\\842 2
3 Surro:zateffracer Reeovcry Test Batch ID R.ecovery%
Acceptable J,imils
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample rD:
3.1.17.R.I Sample ID:
385070009 Certificate of Analysis Pararncte.r_...... *****-** **-****.. 911.?li~er_........ 1.l~s11_1t _ **- rnc_cr::t_ai11tv MDC Le Surrogatdfracer Reconiry Test Notes:
TPU and Counting lJncertainty are calculated at the 95% confidence level (1.96-sigma).
Report Date:
December 17. 2015 Project:
MJWCOOl 15 Client fD:
MJWCOO I Batch JD Recovery%
Acceptable Limit~
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample JD:
- 3. l.17.R. I Sample ID:
385070009 Matrix:
Soi!
Collect Date:
20-0CT-15 Receive Date:
05-NOV -15 Collector:
Client
~foisture:
21%
Certificate of Analysis Project:
Client JD:
Report Dale:
Dt:cember 17, 2015 MJWCOOl 15 MJWCOO\\
Paramelcr
........... gu!i.liti~.i:...... Re5uJ.t......l.'11c.crta.in.~Y.......... :\\WC' Le
... JYr_...... g~.. y_~it~.. _f)F --~\\nti.I.>:st... Date _Ti.'!le.J:latcl1... ~l_td..
Gra,*imetric Solids ASTJf D 2216 % 1\\1oistiwe "As Recei\\*ed" Moisture 2\\.0 Had Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry Weight Corrected" Actmiuni-227 u
-0 0672 Antimony-125 u
(l 0605 Bismuth-212 Lii 0.00 Bismuth-214 I.OS Ccsmm-137 0 935 Cobalt-60 u
-2.82E-OS Europium-154 I.I
-0 112 Lcad-212
! 04 L~ad-214 l.19 PolaS$ium-40 13.0 P.rotactimum-23 l u
0 403 Radium-226 1.05 Radium-228 I 04 Thallium-208 0 426.
Tm-126 l!
0.0481 Rad Gas Flow Pro11ortio11al Counting GFPC. Gross.. f'B, solid "Dry Weigfit C'on*ected" Alpho.
11.8 Bela 24 4
!~.~ _foll~~':i11g_Pr~p __ ~~!_ho~s.. '"._cre petf!J_r_i~~~.. _.
Method Description Dry Soil Prep Dry Sod Prep GL-RAD-A-02 l T~~- folll)_~V.}.~g_ ~.\\~~l:r.~!cal __ t\\1c!h.'?~~--:'e1'.~.P~rf?.rrn.~d
- \\*Icthod Description ASTM D 2216 (Modified l 2
DOF. HASLJ00.4.5 2 3.iGtt-01-R
+/-0.346 /-() 157
+l-0 727
+/-0.197
+/-0.133
+l-0 05\\6
+/-0.235
+l-0.IS*l
+f-0.231
+/-1.65
+/-0712
+{-0.197
+/.() 329
+/-0.0914
+/-0.154
+/-2 94
+1-2.64 3
EPA 900.0.'SWS46 9310.iSM 71 lOB Modified Su rrogatcffracel' Recovery Test 0.631
()272 l 58 0163
()0906
() 103 0.336 0.142 (l 4()1\\
0.902 I 23 0 163 0.324 0.0781
!) 220 3.46 3 11 0 295 0.126 0729 0.0738 ll.040R
() 0443 0.149 0 0666 01%
() 380 0 571 0.0738 0 143 tl 035 0 106 1.56 1.50 Analyst CXCI
+/.(} 348
+f-0 160
+/-0 921
+/-0 218
+/-0.157
+1-0 osic.
+/-0240
+/-0.181
+1-0 254
+/-] 9ti
+1-0 741
+/-0218
+/~0.366
+/-0.099
...,.() 155
+/-3 8(1
+l-4 35 Date ll/lll/15 P<!fCCnl C'XCl 11/10115 \\319 1521842 pCi/g RXF2 12i0J!l5 1303 1522383 2
pCilg pC1/g pCi/g 0.100 pCilg pC1!g pC1/g pCi/g pCVg pC1/g pCi/g pC11g pC1lg p('i!g pCi/g 4-.00 pCi!g KXB2 12i02/l 5 1128 1525757 3
10.0 pCl/g Time Prep Batch 1319 152 l 842 Batch ID Recovery% AcCC[Jtablc Limits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556--8171-www.gel.com Company:
Address:
MJW Corporation 15 Hazelwood Drh:e Suite 112 Bu!Talo, New York. 14228
Contact:
Ms. Laurie Lose}'
Project:
Soil Radioisotopes Client Sample ID:
- 3. I. I 7.R. I Sample ID:
385070009 Parameter Surrogaten*racer Recovery Test Notes:
Certificate of Analysis TPU and Counting Uncertainty are calculated at the 95% confidence level {1.96-sigma).
Report Date:
December 17. 2015 Project:
MJWCOOl 15 Client ID:
MJWCOO I Batch ID Recovery% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:
Address:
Contact:
MJW Corporation 15 Hazelwood Drive Suite 112 BulTalo. New York 14228 Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample JD:
3.Ll7.R.2 Sample !D:
388092017 Matrix:
Soil Collect Date:
20-0CT-15 Receive Date:
23-DEC-15 Collector:
Client Moisture:
20.6%
Parameter Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weigh! Corrected" Actm1im1-227 U
0.0259
+1-\\J 34'1 Ant1mon7-125 U
0 0466
+f-0 127 Bismuth-212 ur ooo
+1-1.12 Bismuth-214 O 81.\\
+/-0 20ll Ce~ium-137 0 742
+/-0 107 Cobalt-60 U
-000171
+/-0.0366 Europium-154 Leali-212 Lcod-214 Potassium-40 Pro!acrnuum-23 \\
Radium-226 Radium-228 Thalhum-208 Tm-126 u
U!
ll[
{) 122 1.04 1.05 140
()00 0.814 1.12 0 293 000
+/-0 136
+l-0 132
+/-0 2\\5
+1-1 68
+/-\\ 66
+1-0 20()
+f-0.309
+/-0.0\\15
+/-0 139 T!1~ foll.mv.i11g.P..~.e_p ;'v!~th.od.S. ~"'.~re. v.c.r~~r~~~ _........... *.-
Method Description Dry Soll Prep Dry Soil PrcpGL-RAD-A-021 The.f.~lll)w.i!lg A1l.l1.IJ!i~alJ\\1._e.t.~1si.d..s.~l*e.rc J.1~.r!.1:1-:in~<l Method Descriptiofl DOE 1-JASL 300. 4.5 2 3/Ga-01-R Project:
Client ID:
Report Date:
MJWCOOl 15
.MJWCOO!
Jammry 20. 2016 MDC L.c __.
..... TPl'.
RL
() 6\\3 0 290
+/.() 348 pC1lg MJHI 01/18/16 0723 1534020 0 246 0.115
+/-0.129 pCiig*
1.27 0.583
+/-1.18 pCi/g 0.162 I) 0742
+/-0.211
µCi/g 0.0879
() 0402
+/-0.122 0 \\00 pC1!g
() 072 u 0302
+/-0 0366 pCi/g
()293 0.131
+l*O 148 pC1!g 0.\\30 00616
+/-0 157 pCilg 0.17(1 1).0823
+1-0232 pCifg
,0 570 0.228
+1-2.0(i pCi!g
! ()8 0.507
. +/-! 70 pCi/g
() 162 00742
+/-n.211 pCi/g 0 293 0 [31
+/-0 344 pCilg ll.0779 00356
+/.0.098 pC1/g 0.165
() ()79
+/-U MO pCifg
- o
- * * -**-" H**O Analysl Date Time Prep Batch I.YT!
12124/15 070J 1533924 Batch ID Recm.-cry%
Acceptable Limits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-B 171 - www.gel.com Company:
Address:
MJ W Corporation 15 Hazelwood Drive Sulte J 12
.Buffalo. New York 14228 Contaqt:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample JD:
3.1.17.R.2 Sample JD:
388092017 Certificate of Analysis Report Date:
PrQject:
MJWCOOl 15 Client ID:
MJWCOO I Jnnunry 20, 20*16 Parameter
.. 91:1.~~~ficr........ !l~~~~-t.... JLn1:~r-~ain~y....... Ml)C: ***-*...l~i.:......... 1J>_I:_...... ~L. *-- t:nil.S... _l)F __ ~n-~ly~t....D.at~_Ti~t: J:l:it_~ll.)I_l_d..
Surrogatcftraccr Recovery Test Batch ID Recovery%
Acceptable Limits Notes:
TPU and Counting Uncertainty are calculated at the 95% confidence level { 1.96-sigina).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843} 556-8171 - www.gel.com Certificate of Analysis Company:
Address:
MJW Corporation 15 !-lazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
3.!.17.R.2 Sample ID:
388092007 Matrix:
Soil Collect Date:
20-0CT-15 Receive Date:
23-DEC-15 Collector:
Client Moisture:
20.6%
Parameter Result l'ncertainh*
Gravimetric Solids AS1M D 2216 % Moisture "As Received" Mmsmre
.2(16 Rnd Alpha Spec Al)alysi.5 ASP Plutonium isotopic. Solid "Dry Weight Corrected" Plu\\omum-238 (J 0518
+/-0 0673 Plutonmm-239i24(l 003!
+/-0.0549
..ISP l.l*anium Isotopic, Solid "Di)' JYeight CoJ-rected" llrumurn-232 u
-00392
+/-0 0409 U mnium-2331234 0759
+1-0 245 1 lranium-2351236 0.0296:
+/-00681 t:ramum-238 0.841
+/-0 256 Alp/1aspe,c Sp237, Solid "D1J' Weight Cotrecled" Ncpluamm-2:n u
00424
""/-11.274 Afphaspec 171229 ~ 228.130.232 Solid "Dry ll'eight Correcled" Thonurn-228 I 26
+/-0 642 Thorium-229 u
-0 0682
+/.[) 158 TI1onrnn-2JO I 03
+l-0.55'i Thonum-232 0.848
+/-0 SO I Am24l, Cm Solid "D1:r Weight C'orl'i!Cted" Americium-241 u
0 0173
+/.() 0477 Curmm-242 0.00
+/-() 0385 Curium-2431244 0.0205
- l-0 ()47 Cunum-2451246 0.0155
+/-0.0436 Liquid Si:int Pu24 l, Solid "Dry* Weight Corrected" l'lutomum-24 l ll
-6.03
+/-7 26 Rad Gamma Spec Analysis Gamma I 129. Solid "Dry Weight Corrected" loomc-129 lJ 0.0563
+1-0 400 Gammaspec. Gamma, Solid "Dry Weight Cm*i*ected" Actmmm-227 ll
- 0.0339
+/-0 182 Antunony-!25
\\]
0.0422
+/-0.0675 Bismurh-212
{)
0.00
+/-0.624 Bismuth-214 0.746
+f-0.123 Ce~mrn-137 0773
+i-0 0773 Cobalt*60 u
-0.000218
+f-00238 Europium-154
\\J
-0 ()157
+/-1)()955
_Lcad-212 I OS
+/-U.0862 Lcad-214
{) 841
+/.() 122 MDC Le 0 0957 0.0274
+/-0.0677 0()832 (1.0212
+/.() 055 0.142 0 0464
+/-0.041 Cl 128 0 0349
+l-0 280 CUOS
()0247
+/-0.0683 0.119 00302
+/-0.297 0.560
() 167
+/-0 274 0449 0.109
+/-0 698 0468 0 128
+/-0 159 0 393 0090
+/-0600 0.212 00()
+1-0.532 00827 00211
+1-0.047.S
()()573 (l 00
+/.() 0386 (107..\\5 0 0171
+l-0-0471 0.0465 (l 00
+/*0.0436 12.9 6.26
+/-7.26 I tl6 0.360
+1-0 4Cll 0336 0 160
+/-0 182 I) 129 0 ()606
+1-0.0702
() 8J2 0 392
+/-0 972 00981 0.046
+/-0.138 0.045 0 02()7
+/-0 0999 O.lW>l (l.0202
+/.() 0238 0 172 0.[!78:?
+/.() (1957 00739 0 ll353
+,'-0 127 u 0942 0.0445
+/.() 142 Report Date:
January 20, 2016 Project:
Client ID:
MJWC00115 rvlJWCOOI percent LYT1 12124/15 0703 1533555 I Otl pCiig MXS:? 01/12116 !021 1534070 2
I 0\\l 1JC1lg 1.00 pC11g MXS2 01/12116 \\015 1534063 3
100 pC1/g I 00 pCi/g I 00 pCl/g I 00 pCiig MXS2 011121!(1 1032 1534069 4
1.00 pCiig MXS2 Olfl2/l6 l031 1534062 5
1.00 pC!lg I 00 pC1lg I OU pCi!g
! 00 pC1/g MXS2 01/12/16 1103 1534067 6
l.00 pCllg
!.00 pCifg 1 00 pC'1lg 1.5.0 pC1!g MXS2 01/14/16 1749 1534073 7
1 00 pCtlg MJHI 01115116 0849 1535059 8
pCilg MJH I 12129115 115(>
I 53356:?
9 pC1/g pCilg pC1/g O. !UO p('1!g.
pC1lg pCilg pC1.1g pC1/g
GEL LABORATORIES LLC 2040 SaY<!ge Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, Nc:w York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
3.1.17.R.2 Sample ID:
388092007 Parameter Rad Gamnm Spec Analysis
. Gammaspec. Gamma, Solid "Dry 11-'eighl Corrected" Potassium-40 12.5 Pro1acu11iu111-231 tll O 00 Radiwn-226 0 746 Rudium-228 Thalliwn-20~
0965 ll.330
+f-1.09
+/-0.411
+/-0 123
+/-0 17'>
+/-0.0473 Tm-126 LI 0.00
+1-0 0766 Rad Gas Flow Proportional Counting GFPC. Gross ;J B. solid "D1:i* Weight Corrected" Alpha 10 2
+f-3 8 I Beta 17 9
+/-3.27 Gl'PC. Sr90,.wlid "Dry Weigh1 Corrected" S1ronm11n-90 U
-0.298
+f-0.841 Rad Liquid Scintillation Analysis LSC Tr ilium Dist. Solid "D1:i* Weight Correc1ed" Tntium IJ I 27
+/-2 46 Liquid Sdm CJ.I. Solid "Dry Weight Corrected" Curbon-!4 U
-0182
+/-0.783 Liquid Sein/ Tr:99. Solid "Dry Weig/11 COl*rected" Teclmetium-99 U
0.241
+/-1 64
- p1~.. rol~olV.i~g ~-r.~.P ~f ~t.h?.d.s. \\~ ~r.~. r~r:fnrm.cd,...
Method Dcsci-iption Dry Soil Prep Dry So11 l'rcpGL-RAD-A-()21 OA75 0.209 0 710 0.340 0 0981" 0 04/i 0.182
() 0832 0.0465
{) 0217 0086
!)0413 3.82 1.48 2 92 1.28 I 70 0 745 4 19 2.02 1 34 OMO 2.&4 I 36 Analyst LYTI
. _:rrr
+1-1.55
+1-0.449
+/-0 138
+l-0 232
+/-0.0547
+/.Cl.0791
+f.4,)(}
+/-4.08
+/-0 841
+/.n 7S3
+/-1 64 Date Report Date:
January 20, 2016 Project:
Client ID:
MJWCOOJJ5 MJWCOOJ pCi!g pC1/g pC'1/g pC1fg pCLlg pCifg 4.00 pCi/g 10.0 pC1/g 200 pCifg 6.00 pC1/g 200 pC1/g 5 00 pCJJg Time JXB7 01112116 0319 1534760 I 0 KSDl 01/061.16 1654 1534788 11 TXJl IJl!JOl\\6 2115 1534918 12 TXJI 01/16116 1233 1534935 13 MYM 01119116 0642 1534638 14 1
Prl!p Batch 12124113 0703 1533555
!~~ _f?._llo~~~i.11g.J\\n:tl~tka.l_~~t_!ICJ_ds ncr~_r.i:r~(lrmcd... __. __.............................,.... *--*-**-*......,. _..... **-*****
Method llcsc:ription 2
4 5
6 7
8 9
10 II 12 13 ASTM D 2216 (Modified)
DOE EML HASL-300. Pu-11-RC Modified DOE EML HASL-300, lJ-02-RC Modi lied ASTM c 1476-00 Modified DOE EML HASL-300, Th-01-RC Modified I:JOE EML UASL-300. Am-05-RC Modtficd DOE EMI. HASL-300. Pu-11-RC Modified DOE El\\IL HASL-300,!-01 Modified DOE HASL300.4 5 2 3iGa-01-R EPA 9000JSWR~693IO!SM111UB Modified EPA 905 0 Modified/DOE RP501 Rev 1 ~od1t'icd EPA 906.0 Modi tied EPA EERFC-0 I Modified
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company:
Address:
1\\-IJW Co!Jloration 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
3.1.l 7.R.2 Certificate of Anal;ysis Report Dale:
January 20. 2016 Project:
Sample JD:
388092007 Client ID:
MJWCOOIJS MJWCOOl Parameter
. Q'!a!ifi~!:... __ _l~~~_u_lt....J:n.ci;r~:i_in_ty...... ~Ill..<"........l.~c........... Il'.r........ RL 14 DOE EML 11 ASI.-300, Tc-02*RC Modified Surrogatcffraccr Recovciy Plntonium-242 Tracer Uran:ium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Aclinium-227 Tracer Americium-:?.43 Tracer Plutoninin-242 Tracer Strontiulll Cmrier Tec!melium-99m Tracer Notes:
Test ASP Plutonium Isotopic. Solid "Dry Weight Correclecl" ASP Uranium Isotopic, Solid "Dry Weigl1t Corrected" l\\SP Uranium Isotopic. Solid "Dry Weight Corrected" Alphaspec Np237. Solid "Dry Wdght Corrected" Alphaspce Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241. Cm Solid "Dry \\\\!eight Corrected" Liquid Sc.:int Pu24 I. Solid "Dry Weight Corrected" GFPC, Sr90. solid "Dry Weight Corrected" Liquid Sein! Tc99, Solid "Dry Weight C-0rrectcd" TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).
Units DF An:1lvst Date Time Batcb Mtd.
. -* -*****............ --.. ~-......... *-**..... *-.. -*........ *-.........
Batch lD Rccover,y<Yo Acceptable Limits 1534070 1534063 1534063 1534069 1534062 1534067 1534073 1534788 1534638 75.4 65.4 B6.1 93 85.1 91.4 75.4 60 95.9
{15%*125%)
{15%-125%)
( 15%-125%)
(15%-125%)
(15%-125%)
(15%-125%)
(15%-125%)
(25%*125%)
(_ 15%-l 25%}
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company :
MJW Corporation Address :
15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie* Losey Project:
Soil Radioisotopes Parameter Client Sample ID: 3.!. !7.R.5 Sample ID:
385070010 Matrix:
Soi!
Collect Date:
20-0CT-I 5 10:45 Receive Date:
Collector; i\\foisturc:
05-NOV-15 Client 21%
Grav.imetric Solids*
ASTM D 2216 <!-*(,Moisture "As Received" Moisture 21.0 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected"
- Plutomum-238 l!
0 0726
+f-0 09\\9 Plutomum-:?391240 lJ 0.0437
+/-O. liJ5 ASP Uranium Isotopic, Solid Dry Weight Corrected" llramum-232
\\J 0.0135
+/-00953 llrnnium-233i234 I 05
- +l-0.329 Ummum-2351236 lJ 0 0456
+/-0 0897 l!rnmum-238 0 956
+i-0.312 Alphaspec Np237, Solid Dry Weight Con-ected" Neptunimn-237 U
-0 0887
+J-0.206 Alphaspec 111229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 l.05
+/-0.517 Thanum-229 U
0 Gl44
+/-0 151 Thonum-230
- 0. 924
+/-0.439 111or111rn-232 1 33
+/-0.522 Arn241, Cm Solid "Dry Weight Corrected" Amencmm-241 lJ
-0.0175
+f-0.0406 Cunum-242 lJ 0.00
+/-0.0421 Curmm-2431244 ll 0 0\\44
+/-0.0647 Curium-2451246 lJ 0 0417
- /-0 0715 Liquid Sc:int Pu24 l, Solid "Dry Weight Corrected
Plutomum-241 L'
-3.38
+f-64\\1 Rad Gamma Spec Analysis Gamma I 129, Solid "Dry Weight Corrected" lodmc-129 ll
-0.067
+/-0.270 Gammaspec. Gamma, Solid "Dry Weight Co(rected" Aclinmm-221 U
-0 0434
+/.() 269 Anumony-12:"
U
-tl.0629
+/-0. J l(J Cc~ium-137 I 00
+/-0.114 Cobalt-60 IJ 0 (){)885
+1-0 0356 Europium- !54 U
-0 0-1-S9
+/-0. \\37 Protacimmm-131 Ul 0 00
+/-0.773 0 I \\4 0.190 0 196 0.14.'l
() 124 00715 06()9 0.50!
0 314 0 154 0.154 0 120 u 0627 0 126 00626 114 I) 491 0 4S'l
() 199 0 0654 00759
() 255 0 968
\\.00 1.00
\\ 00 1.00 1.00 1.00 l (10 l 00
\\ 0()
1.00 1.00 1.0()
](1(1 t.00 I 00 15 ll I.OU 0 100 Project:
Client m:
percent pCi!g pCi/g pcifg pci/g pci!g pc1/g pCi!g pC1!g p('ifg pClfg pC!lg_
pCilg pCilg pC!lg pCi!g pC.1/g pCi!g pC1/g p{,'.tlg j1Ci/g pCi!g pCilg pCt!g Report Date: December 4. 2015 MJWC00\\15 MJWCOOI CXCl 11110!15 l 3 ! 9 1521842 HAKB 11123115 1501 1522577 2
HAKll I 1/2.4/I5 085 l l 522580 3
llAKB 11i23/15 1706 1522576 4
HAKB 11124115 1014 15'22579 HAKB l li24/15 1042 1522571 6
!IA KB l !i25/l 5 0930 1522578 7
MJHI 12i02/15 1342 1522374 8
RXF2 12!03115 1304 152231B 9
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis.
Report Date: December 4, 2015 Company:
MJW Corporation Address:
15 Hazelwood Drive Suite 112
Contact:
Buffalo, New York 14228 Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample JD: 3.1.17.R.5 Sample ID:
385070010 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Radtum-226 0 800
+/-0.174 Radium-228 0.968
+/-0.302 Tin-126 U1 0.00
+/-0 134 Rad Gas Flow Proportional Counting GFPC, Gross A!B, solld "Dzy Weight Comcted" Alpha 15 2
... /-2.8.+
13eta 25 2
+/-2.55 GFPC, Sr90, solid "Dry Weight Corrected" Sttomium-90
- U
-0.358
+l-0 742 Rad Liquid Scintillation Analysis LSC, Tritium Dist. Solid Ory Weight Corrected" Tritmm U
1.90
+/-1 91 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 U
0 232
+/-0.868 Liquid Scint Tc99, Solid "Dry Weight Corrected" Tcchnctium-99 U
1 12
+/-l 58 0.126 0 294 D 137 2 57 2.84 l.53
- 3. 14 1.48 Hi?
1~!~~_f9}l()~V.i.ng}'!~.I'..~.e!~I.()~~-w_e~e r.e.r.fo1:1ned.: ****-............................
Method Description "Dry.Soll Prep
................ 'br).'g(,jj Pr~p Gl-RAD:A:o21..
4.00 10 0 2 ()0 6.00 200 5 00 Analyst c*xc:.~i'.
Project:
Client ID:
pC1lg pCilg pCilg pClfg.
pC'1/g*
pCi!g pCilg pC1/g pC1lg MJWCOOl 15 MJWCOOI KXB2 12102115 KSDI 12i02/15 TXJI 12102115 TXJJ l 2i03!15 MYMl 1 \\129115 Date Time Prep Batch 1128 1525757 1.641 !525755 1324 1522724 1940 1522716 1017 1522715
- *1 *ilioiTs* * ** ** * *i"JW*** * ** *i"s.21842......... -..... ** *.......
IO 11 12 13 14
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey
......... *-p~~jec_t: _
......... ~?i.t.. R.:ad!?.!~°.~opc*s***... _..............
Client Sample ID: 3.1.17.R.5 Sample 10:
385070010
- --~..... *-** *-** ***-**-*- -*************** *--**** -* ****-** -***......... ****************
Project:
Client ID:
MJWCOOI 15 MJWCOO!
_The folt.o'.".'.in.~ ~'-~.alx~t~~~.~~~~?_<l.s v;~~~_perfo~~~=.....
M~t~.9.d... _............. _........ Q~~~ript.ign............
An!!b'~t C:9!l)fll.e.n\\~...........
I
/\\STMD2216(Modificd) 2 3
4 5
6 7
8 9
10 11 12 13 14 ODE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1476-00 Mod1!ied POE EML HASL-300. Th-01-RC Modified DOE EML l-IASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE.EML f*!ASL-300.l~Ol Modified DOE BASL 300. 4 5.2.3/Ga-01-R Er A 'JOO O/S W84& 931 OiSM 711 OB Modi tied f:PA 905.0 ModifiediDOE RP501 Rev. 1 Madtf1cd EPA 906 0 Modified EPA EERF C-Ol Modi lied DOE EML HASL-300. Tc-02-RC Modified
~.urr.~~ate/)'r!l~:r~~c.ov_e.~Y.
1'1\\1ton1um-242 Tracer Test......................... -* -**.... *******-*-*****-*.....
ASP Plutonium lso1op1c. Solid "D1y Weight Corrected" Urunium-2;32 Tracer Uranium-2351236 Tracer Amcricium-243 Tracer Acurnum-227 Tracer Americium-243 Tracer Plutomum-242 Tracer Strontium Carrier Teclmctium-99m Tracer ASP Uranium fsot<Jpic. Sohd "Dry Weight Corrected" ASP Uranium lsotop1c*. Solid "Dry Weight Corrected" Alphnspec Np237. Sohd "Dry Weight Corrected" Alphaspec;: Th229 + 228.230.232 Sohd "Dry Wei1:ht Corrected" Am24 I, Cm Sohd Dry Weight CorrCC1ed" Liquid Scmt Pu24 I. Solid "Dry Wetghl Corrected" GFPC, Sr90, solid Dry Weight Corrected
l.1qmd Sci~t Tc99, Solid "Dry Weight Corrected" Notes:
Counting Uncertainty is calculated at the 95% confidence levei ( 1.96-sigma}.
Result 72 9 57.5 63 8 70.5 88.?
68 8 72 9 86.7 94 2 (15%-125%)
115%-125%)
(15%-125%)
(15%-125%)
(15%-125%)
{15%-125%)
[15%-125%)
(25%-125%)
(15%-125%)
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company:
Address:
Contact:
M.JW Corporation 15 Hazelwood Drive Suite l 12 13uffalo, New York I 422S Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
- 3. l.17.R.5 Sample JD:
3850700 lO Matrix:
Soil Collect Date:
20-0CT -15 Receive Date:
05-NOV-15 Collector:
Client Moisture:
21%
}~~r~n,ie_t~~--.......... __ 9u_alili~r..... _Rc~t1It.... V.11<:ert_1tii:ttY Gravimell*ic Solids ASTM D 1216 % Moisltlre "As Received" Moisture 21 0 Rad Alpha Spec Analysis ASP Pluronium Isotopic. Solid HDIJ* Weight Corrected" Plutonium-238 0 0726
+/-0 O<J 19 Plutonium-239/240 U
0 0437
+/-0 105 1tSP Uranium Isotopic. SoUd "DI}' Weighr COl'l'er:wd" Uramum-232 U
0 0135
+/-0.0953 l/ramum-233/234 I 05
+/-0.329 tlranium-235/236 0.0456
+/-0.0897 l)rantui:n-238
- 0. 956
+/-0 312 Afphaspec ;\\'p237, Solid "D1:1* Weight Corrected" Ncptuoium-237 lJ
-0 0887
+/-0 206 Alphaspec 771229
- 228.230,232 Solid. "Dry Weight Corrected" Tiiorium-228 1 05
+f-0. 517 Thorium-229
. lJ 0.0144
- +f-0.151 Thonum-230
- 0. 924
+/-0 439 Thonum-232 I 33 Am24l._Cm Solid "DIJ-* JVeight C'orrected
Amencium-241 U
-0.0 !75 Curium-242 (J.00 Cunum-243i244 ll U 0144 Curmm-2451246 0 0417 f.iquid Seim ?11241. Solid "D1J' Weight Correc1eir f'lutonium-241 U
-3 38 Rad Garn ma Spe~ Analysis Gamma fl 29. Solid "D1y 1J!eig/Jt C'orrecled" lodinc-129 U
-0 067
+/-0.522
+/-0.0406
+"/-0.0421
+1-0.0647
+/-0.0715
- ~/-6.49
+/-0 270 Gammasper:. Gamma, Solid "Dry J-Ve{ghl Cortecl~d" Actimum-227 U
-0.0434
+1-0.269 An111J1ony-125 U
-0.0629
+/-0 ! 10 Bisrnuth-212 UJ 0 00 /-1.09 Bismuth-21 4 Ccsium-137 Cobalt-60 Europilim-154 Lcad-212 Lcad-214 ll u
0.800
! 00 0.00885
-0.0489 1.10 1.04
+/-0 174
+/-0.114
+l-0.0356
+f-0 137
- 1*/-0 \\33
+/-0 183
- -.me Le 0.114 00262 I} !90 0.064!
0.196 0.0641
() 143 (l.())28 0.124
() 0233 00775 (l.00 (1609 0166 0.501 0 171 0314 0080 0 154 (1.00 0 154 0 00 0120 0 0327.
0.0627 0 00
() 126 00362 0.0626 0 I]\\)
1\\.4 5.53 0 491 0.2Hl
() 489 0 228 0.199 00916 0.860 0.379 (l 126 O.ll5M 0.0654
{) 029 0 0759 (J.0322 0.25.5 0.112 0 105 0.049 0341 11165 TPl!
+/-0.0926
+/-0 105
+/-0 0954
+/-0400
- /-0.0902 t/-0.375
... /.() 2()6
+/-0 542
+f-0.15\\
+f-<J.461
+/.() 560
-r/-0 0407
+/-0.0422
+/-0.0647
+/-0.0718
"'"/-6 49
+/-tl.272
+/-0 270
+l-0 11*1
+1-UJ9
~1-0. \\86
+1-0. 141
+/-0 0358
+/-0 139
- +f-0 I 64
- ~/-0 204 Report Dale:
December 17. 2015 Project:
Client ID:
MJWC00! 15 MJWCOOJ
. -~--- __ l}_l_l_its.. DI_'_. f.\\niily_~t... ~atc_}'h11c.':3-:..i!~_b __.. ~Ud, percent I OU pCiig 1\\)0 pCi/g l.00 pcilg I 00 pcilg 1.00 pciig l.00 pci/g l.Oll pCilg 1.00 pC'1lg I()(!
pCilg 1.(1()
pCi/g l.UO pCi/g 100 pCi/g I 00 pC1lg 1.00 pC1/g J.00 pCi/g 15.0 pCiig 1.00 pCi!g.
pCl/g pCllg pC1/g pC1.lg 0 HJO pCt/g pCJ/g pCilg pCu'g pC1/g CXC"l 11/I0/15 1319 1521842 HAK!l l li23il5 1501 1522577 2
HAKB l 11241!5 0851 1522580 3
HAKB 111231!5 1706 1522576 4
HAKB 11i24/15 1014 1522579 5
llAKB 11/24ll5 1042 1522571 6
HAKl"l I li25115 0930 1522578 7
MJHl l2i021!5 1342 1522374 8
RXF2 12i'03/15 1304 I 522383 9
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company:
Address:
MJW Corporation IS Haz.elwood Drive Suite 112 13ufTa!o, New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
3.1.l 7.R.5 Sample lD:
385070010 Certificate of Analysis Project:
Client ID:
Report Date:
December 17, 2015
!VUWCOOl !5 MJWCOOl
. Parameter
.... Q.~:i.lif!C.!'.......
~~s~lt...... Ync~"!a.i!ltY..... ~1Df....... Li:.........
Tl'~!.. _ _ RL. J~~1i.t$ _ J?F. 1\\Jt.~~rs.~.. _D_a,t.e.Time Batch Mtcl.
Rail Gamma Spec Anulysis Gammaspec. Gamma. Solid "Dry Weigh! Corrected
Potassium-4 O 0.9 Protacuniwn-231 UJ 0 00 Rudium-226 0.&00 Radium-228 0 968 Thallium-208 0.352 Tm-126 U!
0.00 Rad Gas Flow Proportional Counting GFPC. Gross ti '8, solid "Dry Weight Corrected" Alpha 15.2 Beta 25 2 GFPC. S1'90. solid "D1:v Weighr Correcff!d" Sironttum-90 U
-0.358 Rad Liquitl Scintillation Analysis LSC frilium Dist, Solid "D1:1' Weight (orrected" Tnlium 190 Liquid Seim(' 14, Solid "Di:1* Weight Correcled" Carban-14 U
0.232 liquid Sein/ Tc99. Solid "D1y Wdg/1t Cm*rected" Technctmm-99
- U 1.12
+l-1.52
- /-0 773
+/-0.174
+/-Q 302
- 1/-!l 073
+/-0 134
+/-2 84
+1-2.55
+1-0.742
+/-I 91
+l-0.868
+/-1 58
~r_h.~.. f~lln'IY.in_g.f!.llP Mc~~~~.s. '~~r.f.l Jl~!"fo.r111cd._........... -*-*..
Method Description 0.732 (l 968 0.126.
0 294 0.0627 0 137 2.57 2.84 1.53 3.14 1.48 2 67 0 308
+/-193 0.451
+/-0 806 0.11564
+/-0 186 0 \\3l
""'*0.334 0.028
+/-fl 07R7 0.064S
+/-0.136 l.IJ t-f-412 4.0U 136
""/-4.38 lll.O
() 670
+/-0 742 200 I j7
+/-I 91 6.00 0 725
+/-0.868 200 1 28
+/-1 58 5 ()0 Aualyst Date pCi/g pCi!g pCilg pCt!g pCt!g pCilg pCi!g pC1/g pCi!g pCilg pCt/g, pCi!g Time KXB2 12/02/15 1128 1525757 10 KSD1 12102115 1641 1525755 11 TXJl l2i02!15 1324 152272.f 12 TXJI 12/G3115 1940 1.522716 13 MYM 11129115 lO 17 1522715 14 J'
Prep Batch Dry Soil Prep DI)' Soil PrcpGL-RAD*A-021 CXCl I l/!Ofl5 1319
~~ll.~011~,~-i-~g.:~!.ll~~i.c~l)~~et~(Jil~ w~r~pe.".f.<!.r[tlC~.:.............................................................................
- 1.. 1 ethou Description 1
ASTM D 2216 (Modified) 2 3
4 5
6 7
8 9
10 JI 12 13 DOE EML HASL-300, Pu-l 1-RC Moililied DOE EMLHASL-300, U-02-RC Mndtfied ASTM C 1476-00 Modified DOE EML HASL-300, *ni-01-RC Modified OOE EML HASl.-300. Am-OS-RC Modified DOE EML HASL-300. Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE UASL 300, 4.5.2.3!Ga-01-R EPA 900 OiSW846 93JOiSM 71 IOB Modified EPA 905.0 Mod1fiedtDOE RP501 Rev I Modified EPA 9.06.0 Modified EPA EERF C-01 Modified
!521842
GEL LABORATORIES LLC 2040 Savage Road Charles~on SC 29407 - {843) 556-8171 - www.gel.com Company:
Address:
Contact:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
3.1.17.R.5 Sample ID; 385070010 Certificate of Analysis Parameter
.......... 9..ll3-!i~"i~r.......... I?.e_s_nlt..... F 11c~.r.ta!11.t:Y....
TPl" 14 DOE EML l-IASL-300. Tc-02-RC Madilied Surrogatc!fraccr Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Amcricium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technctium-99m Tracer Notes:
ASP Plutonium Isotopic. Solid "Dry Weight Corrected"
. ASP Uranium Isotopic. Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Coriected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspcc Th.229 + 228,230,232 Solirl Dry Weight Corrected" Am241. Cm Solid "DI)' Weight Corrected" Liquid Scint Pu24 l, Solid Dry Weight Corrected" GFPC, Sr90. solid "Dry Weight Corrected" Liquid Scint Tc99. Solid 1101}* Weight Correctt::d" TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigrna).
PrCiject:
Client lD:
Report Dme:
December 17. 2015 MJWC00115 MJWCOOl Date Time Bal"ch :\\ltd.
Batch rn Recovery%
Accep!nble Limits 1522577 72.9 (15%-125%)
1522580 57.5 (15%-125%)
15225&0 63.8
( 15%-125~(,)
1522576 70.5 (15%-125%}
1522579 88.9 (15%-125%)
1522571 68.8 (15%-125%1) 1522578 72.9
{!5%-125%)
1525755
&6.7 (25%-125%)
1522715 94.2 (15%-125%}
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.get.com Certificate of Analysis Company:
Address:
Contact:
MJW Corporation 15 Hazelwood Drive Suite 1 !2
!:luffalo. New York !4228 Ms. Laurie Los~y Project:
Soil Radioi~otopes Client Sample JD:
3.1.17.R.5 Sample JD:
385070010 Matrix:
Soil Collect Date:
20-0CT-15 Receive Date:
05-NOV-15 Collectol':
Client Moisture:
21%
P_ar.~i:i1e.!~~--...... *-.. ______ 9u.~!i~c.r..... Result
.. Vni;.~t_llinn:
Gravimetric Solid~
ASTM D 2216 % Moistwe "As Received" tvloisture 21 0 Rad Alpha Spec Analysi~
ASP Pl11to11i11m lsotapic. Solid "Dry Weight Corrected" Pluioniurn-23&
0 0726
+/-0 0919 Phnoniuni-239/240 u
0.0.\\37
+f-0 105 ASP Ur,111i11m Isotopic. Solid "D1:v Wei;;hr Corrected" lJramum-232 U
0.0!35
+f-0.0953 llramum-233!234
- 1 05
+/-0.329 Uranium-2351236 0.0456
+/-0 0897 llrnnium-23.8 0 956
+/-0 312 Alphaspec Np237. Solid "Di:v Weight Corrected
NcplLmium-237 LI
-0 08$7
+/.Q 206
.-l!phaspec T/1229 ~ 228,230,232 So/id "D1:i* Weight Corrected" Thorium-228 I 05
+f.(l.517
- nmnum-229
\\J 0.0144
+/-0 151 Timnum-230 "lliorium-232 0.924 I 33 tlm241, Cm Solid "Dry IYeiglu Corrected" Amencium-241 U
-0O175 Curium-242 Cunum-2431244 u
0 00 00144
+J-0 439
+/-0.522
+l-0.0406
+/-0.0421
+l-0 0647 Curium-245.1246 0 0417
+1-0 0715 liquid Sci11I P1124l, Solid "D1y Weight Col'rected" Phuonmm-241 U
-3. 38
+1-6.49 Rad Gammu Spec Analysis Gamma l l 2.9. Solid "Dry IVC?ight Corrected" Jodmc-129 U
- O 067
+/-0 27()
Gammaspec', Gamma. Solid "D1y Weight Corrected" Actinium-227 lJ
-0 0434
+/-0.269 Antimony-125 U
-0.062'!
+/-0 110 Llismuth-2 I 2 Ll!
0 lltl
+/. 1 09 Llisrnuth-214 0 80!)
+/-0 17*1 Cl'sium-137 1.(10
+/-0 114 Cobalt-60 U
O 00885
+!-0 0356 Europium-15.\\
U
-0 0489
+/-0.. 137 Lcad-212 I 10
+1-0 133 Lcad-214 1.04
+/-0 183
.M°-~*** *-- __ Le 0.114 0 0262
+/-0.0926 0 190 0.0641
+/-0 105 0.196 0 064 l
+J-0 0954 0 143 0.0328
+1-0400 0.124 011233
+/-0 0902 0 0775
()00
+/-0 375 0.609 ll.166
+/-0.206 0.501 0 \\71
+1-0.542 0.314 0.080
+/-0 151 0.154
(}.[)()
+/-0.461 0 154 oon
+/-0 560 0.120 0 0327
+/-0.0407 0.0627 0 00
+1-0.0422 0.126
() 0362
+1-00647 00626 O.llG
+/-0.07\\8 114 5..53
+/-6 49 0 491 0 2IO
+/-0 272 0.\\89 0.228
+f-0.270 0 19'l 0 0916
.. 1.0 I \\4
() 860 0 379
+/-1.09
() 126 0.0564
+/-0.186
() 0654 0.029
+/-0 141
(!0759 0 0322
+/-0 0358 0255 u 112
+l-0 139
() lll5 0049
.,/-0.164 0 341 0 165
-t/-0.204 Project:
Client ID:
Report Date:
December 17. 2015 MJWCOOJIS MJWCOOl perc~nl CXCI 11/10!15 1319 1521842 1.00 pCi/g flAKll 11/23115 150\\
1522577 2
l 00 pC1/g
\\.00 pc1.lg HAKB 11/24/15 0851 1522580 3
1 Oll pc1.lg 1.00 pci/g I UO pci/g I 00 pCi/g HAKB 11123/15 1706 1522575 4
I 00 pCi/g HAKB \\ 1124/15 1014 1522579 5
I 0(1 pC1/g I 00 pe1lg 1.00 pC1/g 1.00 pCi/g HAKB 11124/15 1042 1522571 (1
1.00 pCi/g 1.00 pCi/g I 00
- pCilg 15 0 pC1lg HA Ki3 11125! l 5 0930 1522578 7
I 00 pC1/g MJlll 12102/15 1342 1522374 pCilg R.XF2 12i03/!5 1304
\\522383 9
pC1lg pCi./g pC1/g 0.100 pC1lg pC1/g pCi!g pCrlg pCilg
Company:
Address:
GEL LABORATORIES LLC 2040 Savage Road Charlesto11 SC 29407 - (843) 556-8171 -www.gel.com MJW Corporation 15 Hazelwood Drive Suite I !2 Certificate of Analysis Buffalo, "Ne.w York 142.28 Report Date:
Dccc!llbcr 17. 2015
Contact:
!'.1s. Laurie. Losey Project:
Soil Radioisotopes Client Sample ID:
Sample ID:
3.1.17.R.5 385070010 Parameter 9..?.alifier.... __ R,_cs.u_l_l_....l:I1ct:rt51i_n_~,:....... ~IQ.C........ !'.s:......
!tad Gamma Spee Analysis Gammaspec. Gamma. Solid "Dry IVeiglrt Corre.cted" Potassmm-40 13 9 Protactmium-23 l Radium-226 Radium-228 Tha!hum-208 Tin-126 Ul Ul Rad Gas Flow Proportional Ccunting 0.UO 0 800
()%8 0.352 0 00 GFPC. Gross AB. solid "Dry JVeight Corrected" Alph~
15 2 Lktu 25 2 GFPC. Sr9D. solid "DIJ' Weight Corrected" Strontmm-9(1 LI
-0.358 Rad Liquid Scintillation Analysis LSC. Tritium Dist, Solid "Dry Weight Corrected" Tritium I.90 Liquid Sein/Cl.f, Solid "Dry Weight Corrected" Curbon-14 U
ll.232 Liquid Sci1Jt Tc.99. Solid "D1:1' Weight CoTl'ected" Tcchneuum-99 U
I 12 1.:~c..f ollo~~~~g _P.rep.. ~~~~~ods_ 'v.i:r_c_p~r.~orm_c_d Method Description
+1-1 52 0 732 0 308
+/-0 773 D.968 0451
+/-() 174 I) 126 00564
+/.. <J.302 0.29.+
{) 131
+/-0.073 O.ll(127 0 018
+/-0 134 0 137 ll.OM.5
....,_2 84 2 57 I 13
+/-2 55 284 I 36
~1-o.n2 l.53 o.&10
+(.. ] 91 3.14 I 37
+/-0.868 l 4S 0 725
+/-1 58 267 1.28 Analysl
+/-1.93
+/-0.!\\06
+i-0.18(>
+1-0 334 i*/-(1.()787
+J-0136
+/...J.12
+1-4.38
+1-li 742
+f-1 91
+l-0 868
+/-[ 58 Project:
ClienllD:
MJWCOOl15 MJWC001 pC1/g.
pCi/g pCi!g pCilg pC11g pC1/g 4.00 pCi.lg KXB2 100 pC1lg 2.00 pCi/g KSDI 6.00 pC1/g
- TXJI 2 00 pCilg TXJ!
500 pCi/g MYM I
12102;15 1128 1525757 12102115 1641 1525755 t2J02/l5 1324 1522724 12/03!15 ! 940 1522716 I !/29/!5 I017 15227!5 Date Time Prep Balch Dry Soil Prep Dry Siu\\ Prep GL-RAD-A-021 1:h.e _fo_l_l~'~i Dl{ __ Ana!)'.1 ~~-~.1-~1_c_~~ o~s-~v,e:~ ('~ r~o.i:ll.1_cd.
Method Description I
2 3
4 5
6 7
8 9
](l II 12 13 ASTM D 2216 (Modified)
DOE EM!. HASL-300, Pu-I I-RC Modified DOE EML HASL-300. U-02-RC Modified ASTM C 1476-00 Modified DOE EML HASL-3()0, Th-01-RC 1'fod1ficd DOE EML HASL-300. Am-ll5-RC Moclifi~d DOE EML HASL-300, Pu-\\ l-RC Modllicd DOE EML HASL-300J-01 Mod1ficd DOE HASL 300,45 2 3/Ga-01-R EPA 900.0/S\\\\.'846 93 IO/SM 71 lOB Modified EPA 905.0 ModifiedlDOE RP50! Rev. I Modified EPA '106 ()Modified EPA EERF C-01 Modil1cd CXCI 11110115.
1319 1521842
]()
II 12 13 14
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite 112
.Buffalo, New York 14228
Contact:
Ms. Luurie Losey Project:
Soil Radiobotopes Client Sample ID:
3.1.!7.R.5 Sample ID:
385070010 Certificate of Analysis
\\4 DOE EML l-IASL-300, Tc-02-RC' Modified Surrogatcffr:icer RecO\\*cry Plutonium-242 Tracer lJrnnium-232 Tracer l.lranium-2351236 Tracer Americium-243 Tracer Actiniurn-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Te*chnetium-99m Tracer Notes:
Test ASP Plutonium Isotopic, Solid "Dry *Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspcc Np237. Solid DI)' Weight Corrected" A!phaspec Th229 + 228.230,232 Solid "Dry Weight Corrected" Am24 l. Cm Solid "Dry Weight Corrected" Liquid Scint Pu24 L Solid "Dry Weight Corrected" GFPC Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99. Solid "Dry Welght Correcred" TPU and Counting Uncertainty are calculated at the 95% confidence level ( l.96-sigma).
Project:
Client JD:
Report Date:
December l 7. 2015 MJWCOOl J5 MJWCOOl Batch ID Recovery% Acceptable Limits
[522577 72.9 (l5%-\\25%)
1522580 57.5 (15%-125%)
1522580 63.8 (15%-125%)
1522576 70.5 (15%-125%}
1522579 SB.9 (15%-125%}
1522571 68.8 (15%-125%)
1522578 72.9 (15%-125%)
1525755 86.7 (25%-125%)
1522715 94.2 (15%-125%}
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :
MJW Corporation Address:
15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Cliem Sample JD: 3.1.17.R.6 Sample ID:*
385070011 Matrix:
Soil Collect Date; 20-0CT-15 10:55 Receive Date:
05-NOV-l 5 Collector:
Client Moisture:
20.5%,
Parameter Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 20.5 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plll!onium-238 U
-0 00502
+/-0 0433 Plutonium-2391240 U
-0 0301
+/-0.0486 ASP Uranium (sotopic, Solid "Dry Weight Corrected" l!ranium-232 U
0 0643
+/-0 0953 Uraniurn-2331234 I 2()
+1-0 361 Urarnum-23?/236 0.110
+l-0.12.l Uramum-238 0 767
.;./.() 289 Alphaspec Np237. Solid "Dry Weight CmTccted" Neptumum-237 U
-0.181
+/-0.189 Alphaspec Th229 + 228,230,232 Solid "Dr)r Weight Corrected" Thonum-228 l 41
. +1-0 530 ThorJum-229 U
-0.0111
+/-0.0957 Thorium-230 0 773
+/-0.385 Thorium-232 1.08
+/-0 452 Am241. Cm Solid "Dry Weight Corrected" Amcricium-241 U
-0 00355
+*1-0 030(>
Cunum-242 U
0 00
+/-0.0341 Curium-243/244 U
0.000584
+/-0.0433 Cmium-245/Z46 X
0 185
+/-0. l \\5 Liquid Scint Pu241, Solid "Dry Weight Corrected
Plutonium-241 lJ
-3 4
+/-7.0S R,ad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Conected" lodine-129 U
-0 0593
+1-0 280 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actimum-227 l) 0.0212
+l-0.279 Antimony-125 U
-0.00335
+f-0 116 Ccsium-137 0 661
+-1-0 111 Cobalt-60 U
-0 015
+l-0 0369 F-uropium-154 lJ
-0 0303
+/-0.122 Protactinmm-23 J lJ 0 806
+/-0..524
() lllO
() 155 0.139
() 13 l O.OBH (l 0822 (1.656 0.336
() 222 0.221 0 255 0.0708 0.0508 0.0963 0.0507
(!554 0 529
() 187 0 0858 0 0681 0.229 I 09 l 00 1 00 i 00 1.00 I 00
! IJO j 00 l 00 LOO.
1.00 l 00 I 00 I 00 l uo 1 00 15 ()
1 !10 0 100 Project:
Client ID:
percent pC1/g pC1lg pc1tg.
pc1lg pcifg pc1lg pCitg pCilg
µC1lg pCi/g pCl/g pC!lg pCi/g pC!lg pC1/g p('i/g pCi!g pCilg pCi.1g pCi/g pC1!g pC1/g pC1/g Report Date: December 4, 2015 MJWCOOl 15 MJWCOOJ
. exp 1uw11s n1'1 1521842 HAKB 11123115 1501 1522577 2
HAKB I 1124115 085 l 1522580 3
HAKB 11123!15 1707 1522576 4
HAKB lli24115 1014 1522579 5
!-IAKB 11/24115
!042 1522571 HAKB ll/25/15 1031 1522578 7
MJHl 12i02/l 5 1343 1522374 8
RXF2 12:03/15 1304 1522383 9
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - \\"JWW.gel.com Certificate of Analysis Report Date: December 4, 2015 Company :
MJW Corporation Address:
15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey
. P.r~je~-~:-...
.......... s_o_i_~ ~~di?.~~~topes...
Client Sample ID:. 3.1.I 7.R.6 Sample ID:
385070011 Rad Gamma Spec Analysis Gammaspec, Gamma. Solid "Dry Weight Corrected" Radmm-226 0.634
+/-0_ 133 Radium-228 UI 0 00
~t-0 275 Tin-126 U
0 114
+/-0 i30 Rad Gas Flow Propo1tional Counting GFPC. Gross A/B, solid "Dry Weight Corrected
Alph~
12.0
+/-lll Beta
.22.6
+1-2.41 GFPC, Sr90, solid "Dry Weight Com~cted
.-0.244
+/-0.623 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "D1y Weight Conected" Tnti111n U
-0.0268
+/-I 65 Liquid Scint Cl4, Solid "Dry Weight Co!'rected" Carbon-14 U
-0.435
+/-0.836 Liquid Scint Tc99, Solid "DI)' Weight Corrected" Techneuum-IJ9 U
1.73
+/-1.69 T~()ll?_,~ir.i~ ?..r~p.~Ie,!l!_~~s ~e.T:C.. P.erf.o!.!!!~~: __.........................
Method Description oiY*soii"hep-**- -** -*** * * *-* ***** ** *o~: sO"ii"Prcr aL:k."ii.o:koii-****-*
0 118 0.55ll 0.159 3.98 2.8+
1.31 3 19 I 45 2.82 Project:
Client ID:
pCi/g pCilg pC1!g 4.00 pCi/g 1011 pCl/g 2 llO pC1/£!
600 pC1/g 2.00 pC1/g 5.00 pCilg MJWC00115 MJWCOOI KXB2 12i02/l 5 1128 KSDI 12i02115. 1655 TXJI 12/02/15 1411 TXJI 12103/\\5 2053 MYMI 11129115 1044 152.5757 1525755 1522724 1522716 1522715 Analyst Date Time Prep Batch
- * **** *"C.'xC.'i....... * * ** * **11no115*** *....... i319* *
- rsi"i 842.
JO II 12 13 14
Company:
Address:
Contact:
Project Client Sample lD:
Sample JD:
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis MJW Corporation 15 Hazelwood Drive Suite! 12 Buffalo, New York 14228 Ms. Laurie Losey Soil Radioisotopes 3.l.17.R.6 385070011 Project:
Client ID:
Report Date: December 4, 2015 MJWCOOIIS MJWCOO\\
0 0 --
00 0000 'H..
H 000 0
o'
"'... **-***** O **-** 0 00 -* ** '
- 0
~--.
0 '*
0 rv!etho_d,_........
2 J
4 5
6 7
ll 9
10 IJ 12 13
.. _l?.~~r.\\ll1Jor.i............................
ASTM D 2216 (Modified)
DOE EMI. HASL-300. Pu-1 !-RC Modified DOE EML HASL-300. U-02-RC Mod1ticd ASTM C 1476-00 Modified DOE EMI. HASL-300, Th-0!-RC Modified DOE EMl HASL-300. Am-05-RC Modrfietl POE EMl HASL-300. Pu-11-RC Modified DO£ EML HASL-300,1-0J Modified DOE l!ASL3(l0, 4.5.2.JiG:i-O\\-R EPA 900.0/SWS46 9'.>°IO/SM 71 JOB Modified EPA 905.0 lvfodificd/DOE RP50 I Rev I Modified EPA 906 0 ~lodificd EPA EERF C'-Ol Modified 14 DOE EML HASL-300, *rc.02-RC Modified
~~~~a.t:=IT!ac.er.~~~.'>.Y~r.Y Test P!ulonium-242 Tracer Umnium-232 Tracer UraniLll11*2351236 Tracer Americium-243 Tracer
/\\c!m1um-227 Tracer Amcricium-243 Tracer Plulomum-242 Tracer Stromium Carrier Teclmct1um-99m Tracer ASP Plulonium Isotopic, Solid Dry Wei[!,hl Corrected" ASP Uran mm Isotopic, Solid "Dry Weight Corrected" ASP Unmmm lso1op1c, Solid Dry Weight Corrected" Alphaspcc Np237, Solid "Dry Weight C<Jrrected" Alphaspcc tht.29+ 228)30.232 Solid "Dry Weight Corrected" Am24L Cm Solid "Dry Weight Corrected" Liquid Scmt Pu241, Solid "Dry Weight Corrected" GFPC. Sr'IO. solid "Dry Weight Corrected" Liqrnd Scmt Tc99. Solid "Dry Weight Corrected
Notes:
Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
- ....... An~J.Y.~t~9n:irn~ms........
Resuh Non1inal.. R:ec?.v_~ry 0
(<>
67.4 52 9 673 918 98.9 769 67.4 88.9 956 Ac~.~pt~.b.le. !:.iir.i~ts
( 15%*125%)
(15%-125%)
(15%-125%)
(15%-125%)
(15%-125%)
[15%-125%)
(15%-125%)
(25%-125%)
(l:i%-!25%)
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite l 12 Buffale>. New York 14228
Contact:
Ms. Laurie Losey Project:*
Soil Radioisotopes Client Sample ID:
3.1.17.R.6 Sample ID:
385070011 Matrix:
Soi!
Collect Date:
20-0CT-15 Receive Date:
05-NOV-15 Collector:
Client Moisture:
20.5%
Gravimetric Solids
. AS1:i.1 D 2216 % ;\\,loi:m1re "As Received" Moisture 20.5 Rad Alpha Spec Analysis ASP P/uloniwn isotopic, Solid "D1y Weight Co1-rec1ed" Plutonmm-238 U
-0.00502 "f"/-0.0433 Plutonmm-239i240 U
-0.030f
+/-0 0486 ASP l.~*anium Isotopic, Solid "Dry Weight Corrected" Urantum-232 0 0643
+/-0.0953 Urmiium-2331234 I 20
+/-0.361 Uranium-2351236 0 l 10
+ /-0 121 Uramum-238 0.767
+/-0.289 A/phaspec Np237. Solid "Dry Weight Coi*rected
Ncpl~nium-237 U
-0.181
+i-0 189 Alphaspec Th229,. 228,230,232 Solid "D1:11 Weight Corrected" lnonum-228 I 41
+/-0.530 Thonum-229 V
-0.0lI1
+/.() 0957 Thonui11-230 0 773
+/-0.385 Thonum-2J2 l O~
+1-0 452 Am241, Cm Sa/id "l)ry Weight Corrected" Amcricium-24!
U
-0 00355 Cunum-242 0 00 Curium-2431244 U
0.000584 Curium-2451246 X
0.1 &6 Liquid Seim ?11241. Solid "Dry Weight Corrected
Plutomum-241 U
-3.4 Rad Gamma Spec Analysis Gamma I J 29. Solid "Dry 'fVeight Corrected" lo<linc-\\29 U
-0 0593
+J.(J..030(,
+i-0 0341 t/-0.043J
+/-0.115
+/-7.0S
+/-0 280 Gammaspec, Gamma, Solid '.'Dry Weight Corri;cred
- Actinium-227 lJ 0.0212
+/-0.279 Antimony-125 U
-00ll335
+/-0 116 Bismuth-212 Ul 0 00
+1-0 669 Bismuth-214 Ce~ium-137 Cobalt-60 u
Europmm-154 LT Lead-212 Lc~d-214 0634 0 66\\
-0 015
-0 0303 1.13 I 05
+/-0 13.}
+1-0 111
+/-0.0369
+/-0.122
+/-0 130
+/-0.194 MDC Le TPl' 0.100 (I 0188
+l-0.(1435 0.!55 0 046
+/-0.()487 0 139 0 038
<*/-0.0%4 0.13!
0.0246
+/-0 446 00824 00(}
+l-0 123 Oll822 000
+/-0 335 0 656 0 215
... 1.0 190 0 336 0.0964
+/-0.569 0 222 0.0415
+l-0 0959 I) 221 0.11414
+/-0 400 0 255 0.0584
+/.().478 0.0708 0 0133
+/-0 0306 0 050&
0.00
+l-0 0342 n 0963 0 0262
+1-(l 0434 ll.0507 0.00
+/-0.118 12 4 6 03
+/-7.08 0554 0 215
+/.(J.281 0.529 0 24R
+/-0.279
(} 187 0.0861
+/.{] t 16 l.JO 0601
+/-0.90&
0 118 0.053
+/-0.143 00858 0 0394
+/.() 123 00681 00285
+/-0 0375 0229 0.0993
- r/.{) 123 0 112 0.0526
+/-0.161 0.342 0 \\66
+/-0.212 Project:
Client ID:
Ri;:port Date:
December 17.2015 MJWCOOI [5 MJWCOOl pcrcc11t CXCl 11110115 1319 1521842 l.00 pCt/g HAKB 11/2.ll\\5 1501 1522577 2
l.00 pCt/g I OQ pc1/g
!IAKB ll/241150851 1522580 I 00 pcr/g 1 00 pci/g 1.()0 pci/g 1.0(1 pCilg HAKB 11123115 1707 1522576 4
I 00 pCilg HAKB \\1124115 !014 1522579 5
I 00 pC1/g I 00 pC'1/g I GO p.Cilg I 00 pCilg HAKB 11124/15 Hl42 1522571 6
\\.00 pCi/g l.00 pCi/g I 00 pCi/g 15.0 pC1!g l-IAKB 11125115 1031
! 522578 7
l 00 pCr/g MJHI 12i02fl5 1343 !522374 8
pC1/g RXFl
!2/03/\\5 130-l 1522383 9
p('1.lg pCtlg pCi/g 0 100 pC1/g pCi.'g pCi/g pCilg pC1/g
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite ll2 13uffalo, New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
3.1.17.R.6 Sample ID:
3850700 l l Parameter Rau Gamma Spec Analysis Gamrnaspec. Gamma. Solid "D1y Weight Conec1ed"
[ __
Potassium-40 13 6 Protactinium-231 r~adium-226 Radium-228 Thallium-208 UI UI Tm-126 Ul Rad Gas Flow Proporlional Counting 0 00 0.634 000 0.258 0.00 GFPC. Gross A*-B, solid "Dl".I' ll'eight CoJ'l'ected" Alpha 120 Beta 22 6 GFPC. Sr90, solid "Dr,1-* Weight Correc1ed" Strnntium-90 U
-0.244 Rad Liquid Scintillation Analysis LSC, Tritium DJsr. Solid "D1*y lfeight Corrected
Tntium U
-0.0268 l.iquid Sein! CJ 4. Solid "Dry Weight Corrected" Carbon-14 U
-0 435 Liquid Scinl Tc99, Solid "D1:1* Weight Corrected" Technctium-99 1 73 Th~--f~l!~~-i~g-~r~11 ::0:1".~h.!l..<.1.s _,'.*i.:.i:c p(?rfor111c_<I.
Method Description
-* Dry Soil Prep Dry Soil Prep GL-RAL>-A-021
+/-1 48
+l-0 524
-;./-0. 133
... /-0.275
+/-0:0808
+/-0.130
+/-3.12
+/-2 41
+/-0 623
+/-1.65
+/-0.836
+/-1 69
~*:~~- £o.1_1.£?.'".i.ng_~na Jytica._I ~le!~I)~~- w,c~! _r._cr.~11rmc~......... -*.
- \\1ethod Description 2
4 s
6 7
8 9
lO 11 12 13 ASTM D2216{Mod1fied)
DOE EM!. HASL-300, l'u-11-RC Modified DOE EML HASL-300, U-02-RC Modified
,\\SU.IC' t 476-00 Modified DOE EML HAS L-300, Th-0 I-RC Modified DOE f:ML l*!ASL-300, Am-05-RC Modified DOE F.ML HASL-300, Pu-1 I-RC Modified DOE EML HASL-300,1-01 Modified DOE HAS L 300, 4 5.2.3/Ga-O 1-R EPA 900.01SW8.\\(, 93 lOiS;'v! 71 !OB M11dified EPfl 905.0 Modified/DOE R!'501 Rev l Modified EPA 906.0 Mod1lied EPA EERF C-0\\ Modilie<l 0 719 1 09 0 11g 0 550 00782 0 159 3.98 2.84 1 31 3.19 1.45 2 82 Project:
Client lD:
Report Date:
December 17, 2015 MJWC00115 MJWCOOl
...... R!~....i.;_nit~.. J?.J1. i\\:Jl~ly~.t.... "f:>.~_tc.. 1.'.i!Jlc. Batch Mtd.
0 305
+/-1.89 pCifg 0.513
+/-0.663 pC1/g 0053
+f-0.143 pC1/g 0.260
+f-0.451 pC1/g ll.0359
+!-() 0835 pCi/g 0.076
+/-0. \\3 \\
pC1!g I 83
+/-3 91 4 00 pC1/g KXB2 12i"02/15 1128 1525757 JO 137
+/-397 10.0 pCilg
() 562
+/-0.623 2.00 pC1/g KSDI 12;0211 s 1655 1525755 11 1.39 t/-1 65 6.00 pCtlg
- TXJl 12i02/15 141 ! 1522724. 12 (J 710
+i-0 &36 2.00 pCtlg TXJI 12/03/15 2053 15227.16. 13 l 36
+/-1 70 5.00 pC'ilg MYM 11/29/1 s 1()44 15227!5 14 1
.... *-*.......... *****-***.... *******.. **-*....... -*-******--*****..... **~ -...... -*-***-.......................... -.
Analyst Oi1te Time Prep Balch CXCI I \\11().'(5 l319 1521842
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite I 12 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
3.1.17.R.6 Sample ID:
3850700! !
Certificate of Analysis
-~~r~r.i:iet.er... __ *- *-.. _. _....Qu.a._li!ie_r...... R.es~lt ___ r!lce.rta_i!*-....... ;\\-~~C Le 14 DOE EML HASL-300, Tc-02-RC Modified Surrugntc!rracer Recovery Test Plutonium*242 Tracer Uraaium-232 Tracer Vranium-2351236 Tnrcer Americium-243 Tracer Aclinium-227 Tracer Americinm-243 Tracer Plutonium-242 Tracer Strontium Carrier Tcchnetium-99m Tracer Notes:
ASP Plutonium Isotopic. Solid "D*f). Weight Corrected" ASP Uranium Isotopic. Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Wcighl Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec: Th229 + 228.230,232 Solid "Dry Weigh! Correctedu Am24L Cm Solid "Dry Weight Corrected" Liquid Sc:inl Pu24 l, Solid "Dry Weight Corrected
GF?C. Sr90. solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" TPU and Counting Uncertainty are calculated at the 95% confidence level (I.96-sigma).
Project:
Client tD:
Reporl Date:
December 17, 2015 MJWC00115 MJWCOOI Batch ID Recovery%
1522577 67.4 15225&0 52.9 1522580 67.3
!522576 91.8 1522579 98.9 1522571 76.9 1522578 67.4 1515155 88.9 1522715 95.6 Acceptable Limits (15%-125%)
(15%-l25'lu}
(15%-125%)
( 15%-125%)
(15%-125%)
(15%-125%)
(15%-125%)
(25%-125%)
(15%-125%)
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:
Address:
MJW Corporation
! 5 Hazelwood Drive Suite 112 Buffalo. New York 14228 Contact Ms. Laurie Losey Project:
Soil Radioisotopes Client Sample ID:
- 3. l.17.R.6 Sample ID:
385070011 Matrix:
Soil Collect Date:
20-0CT-15 Receive Date:
05-NOV-15 Collector:
Client Moisture:
20.5%
Gravimetric Solids ASTM D 2216 % Moislwr: "1Js Received" Mmsmrc 205 Rad Alpha Spec Analysis
.-ISP Plutonium Isotopic. Solid DI}* Wr:ighl Corrected" 1'1\\1tonium-238 lJ
-0.00502
+/-0 0433 Plutonium-239/240 u
-0 0301
+J-0 0486 ASP Uranium Isotopic. Solid "Di)' Weight Corrected" Uranium-232 0.0643
+/-0 0953 llmnmm-233/234 l.20
+/-0.36 l Ummurn-235/236
() 110
+/..() 121 Urnmum-238 0767
+/-0.289 Alphaspec Np2J7. Solid "Dry Weight Corrected" Ncptunium-237 u
-0.181
+/-0 189 Alphaspec Tlr229 + 228,230.232 Sofid Dry Weight Co/'reclr!d" Tnonum-228 1.41
+/-0.530 Thonum-229 ll
-0.0111
+l-0 0957 Thonum-230 0173
+/-0 385 Thorium-232 I.OS
+/-0.452 Am24l, On Sa/id Dr}' Weight Correcl<?d" Americiurn-241 u
-0.00355
+/.Q.0306 Curium-242 000
+/-0 0341 Cunum-243i244 lJ 0.()00584
+/-0.0.+33 Cunum-245/246 x
G 186
+/.(l.115 Liquid Seim Pu241. Sofid "Dry Weighr Corrected" Plutornum-24 l u
-3.4
+/-7.08 Rad Gamma Spec Analysis Gamma J 119, Solid "D1y Weight Corrected" lodine-129 u
-U.0593
+l-0 280 Gammaspec, Gamma, Solid "DIJ' Wr;ight Correcled" Actmium-227 u
0 ()212
+f*0.279 Anumony-125 lJ
-0.0Q335
+/.() l 16 Bismuth-212 lJl 0.00
+/-0.669 Bismuth-214
<l.634
+/-0 133 Ccsium-137 0.661
+1-0 111 Cobalt-60 u
-0.015
+/-0 0369 Europmm-154 u
-0 0303
+f-0 122 Lead-212 I 13
+1-0 130 Lead-214 1.05
+/.0.194 Le 0 JOO 0 OJS8
+/-0 0435 0.155 0.046
+/.(l 0487 0139 0.038
+l-0.0964 0.131
().1}246
+/-0.446 00824 (J(l(J
+/-0.123
(!.0822 0 0(1
+l-0 335 0.656
() 215
+/-0.190 0 336 0.0964
+/-ll 569 02n
().(J-115
+/-0.0959 0 221 0 (1414
+/-Cl.400 n 255 00584
+/.() 478 0.0708 00133
+i-0.0306 0.0508 0.00
. +f*O 0342 0.0963 0.0262
+/-0.043*1 0.0507
() 00
~1-0.11&
12 4 6()3
+.f-7.08 0.5.54 0 215
+1-0 281 0529 0.248
+/-0.279 0 187 0 0861
+1-0.l 16 I.JO 0 601
+/-0.90R 0 118 0 053
+/-0 143 0 085& u 03'14
+1-0.123 0.06RI IJ !l.:!RS
+f-0 ll375 0 229 0 099.3
+/.0.123 0 112 0 0526
+/.Q 161 0 342 0 166
+f-0.212 Report Date:
December 17. 2015 Project:
Client ID; MJWCOOl 15 MJWCOOI percent CXCI l l/10/15 1319 1521842 I 00 pC1lg HAKB 11123/15 1501 1522577 1
\\ 00 pCiig l 00 pc1/g l!AKB 11124/15 0851 1522580 3
l 00 pci/g l.00 01c1/g 1 (){)
pc1/g I 00 pC1lg HAKFl 11123/15 1707 1522576 4
I 00 pC1/g I IAKfl !1124/15 1014 1522579 S
1.00 pCilg 1.00 pC1/g l 0(!
pCJ/g 1.00
_pCi!g HAKB 11/24/15 Hl42 1522571 6
\\ 00 pCJ/g I 00 pC1/g 1.00 pCJ/g 15.0 pCtlg
!IAKl3 l 112:5/15 1031 1522578 7
LOO pC11g MJHl 12/02llS 1343 1522374 R
pCitg RXF2 12/03115 1304 1522383 9
pC1/g pCi/g pC1!g
() 100 pCilg pCi/g pC1/g pCilg pCi/g
Company:
Address:
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com MJW Corporation I 5 Hazelwood Drive Suite 112 Certificate of Analysis Buffalo. New York 14228 Report Dale:
December 17, 2015
Contact:
Ms. Laurie Losey Project:
Soil Radioi~otopes Client Sample ID:
3.1.17.R.6 Sample ID:
385070011
-~a.r_~l!l.c.t~~- *-............ ***- __ g~_a).i_~~.'.-.. **- _l!~~~-ll-...... ~'.!1.c.i;~taintv Rad Gnmma Spec Analysis Gammaspec, Gamma. So{id "D1:i* Weip}U C01*rec/ed" Poiassium-.JO 13.6 Protactimum-231 Radium-226 Radium-228
- 'nlallmm-208 Tin-126 Ul UJ Ul Rlld Gas Flow Prop<>rtio11al Counting 0.00 0.634 000.
0.258 000 GPPC. Gross A.B. solid "Dry Weight Corrected" Alpl1a 12.0 Beta 226 GFPC. Sr9fJ. solid "D1:v IVeight Corrected
Stronuum-90 lJ
-0 244 Rad Liquid Scintillation Anal~*sis LSC, Trit/11111 Dist. Sofi'd "Dry 1-Veight Correcied" Tritium U
-0.0268 Li'quid Sein/ C/4, Solid "Dry ll'eighl Corrected
Carbon-14 ll
-0 435 Liquid Scint Tc99. Solid "Dry IVeight Correcl<?d" Technetium-99 I 73 Tli_~ follmyir.ig ~~.cl? ~~e~l~l)_dS..~l:~i:~ _pel'..f?.~~I!~ -~..
i\\-lcthod Dcscri11tion
+/-[ 4&
+/-0 524
+l-0133
+/-0.275
+/-0.0808
+l-0 130 i*/-3. 12
+/-2 41
+/-0 (>23
+/-I 65
+/-0 83(>
+/-1.69 MDC 0.719 0.305
+/-1.89 1.09 0 513
+!-0.663 0 118
() 053
+1-0 143 0550 0.260
+/-0.451 0.0782 0.0359
+/-ll.0835 0.159 0.076
+/-0 131 3.98 I 83
+/-3.91 2.84 1.37
+/-3.97 1 31 (l 562
+/..() 623 3.19 1.39
+/-*l.65 1.45 0.7!0
+/-0 836 2 82 I 36
+i-1.70 Date Project:
Client !D:
MJWCOOIIS MJWCOOI pC11g pCilg pC1/g pC1/g pCilg pCi/g 4.00 pC1lg KXB2 IO 0 pC1/g 2 00 pCl!g KSDJ 600 pC1/g TXJI 2 00 pCi!g TX.It s 00 pCi/g MYM I
Time Pn!p Batch Dry Soil Prep Dry Soil Pr~p GL-RAD-A-021 Analyst CXCI 11/1011.5 1319
\\521842 The following Analytical Methods were performed
~*f~ti~*od * **** * *-* * ** *ocs~-riPiiOn*--- **
- _
... -*....... *****~.
2 3
4 5
6" 7
8 9
10 11 12 13 ASTM D 2216 (Modificq)
DOE EML HASL-300, l'u-11-RC' Modi lied DOE EML HASL-300. U-02-RC Modified ASTM C 1476-00 Modified DOE EML HASL-300. Th-01-RC Modified DOE EML HASL-300. Am-OS-RC Modtlicd DOE EMt HASL-300. Pu-I I-RC Modified DOE El>IL HASl.-300,1-01 Modified DOE HASL 300. 4.5.2.31Ga-Ol-R EPA 900.0!SW846 93 toiSM 71 IOB Mod1licd EPA 905 0 Mod1flediDOE RP501 Rev 1 Modifkd EPA 906 0 Modified EPA EERF C-01 Modified 12/02/15 1 [28 1525757 12i02115 !655 1525755 12/02/15 1411 152272.J I 2i03/ 15 "205 3 1522716 11/29/1 s 1044 1522715 10
[1 11 13 14
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite 112 BuO'alo. New York 14228
Contact:
Ms. Laurie Losey Project:
Soil Radioisotope~
Client Sample ID:
3.1.17.R.6 Sample ID:
385070011 Certificate of Analysis Project:
Client JD:
Report Date:
December 17, 20 I 5 MJWCOOl 15 (v1JWC001 Parameter
............ 9~.:~l!~!.c1:........ ~e~_ul.~. _... ~'.!l.i;~r:!:ii~_t.,:........ M_IK........ Lf:.......... _. T..f r_....... R~.. Vnits D~*. ~~ll_l!_IY:S.! __ [ll,lt!.. '!'.in_i~. J3at.ch_
- \\J.~d._
14 DOE EML HASL-300. Tc-02-RC Modified Surrogaterrracer Rec1>very l'lutonium-242 Tracer Uranium-232 Tracer Uranium-2351236 Tracer Aniericium-243 Tracer Actinium-227 Tracer Ainericium-243 Tracer Plutonium*242 Tracer Strontium Carrier Technetium-99m Tracer Notes:
Test ASP Plutonium Isotopic. Solid "Dry Weight Corrected" ASP Uranium Isotopic. Solid "DI)* Weight Corrected" ASP Uranium Isotopic. Solid "Dry Weight Corrcckd" A!phaspcc Np237. Solid "Dry Weight Corrected" Alphaspec Th229 + 228.230.232 Solid "Dry Weight Corrected" Am24 l. Cm Solid Dry Weight Corrected" Liquid Scint Pu24l, Sulid "Dry Weight Com:cted" GFPC. Sr90, solid "Dry Weight Corrcclecl" Liquid Scint Tc99. Solid "Dry Weight Corrected" TPU and Couniing Uncertainty are calculated at the 95% confidence level ( 1.96-sig,ma).
Batch ID Recovery%,\\cccptable Limits 1522577 67.4 (15%-125%)
1522580 52.9
{t5~a-I25%)
15225!>0 67.3 (15%-125%)
1522576 CJ 1.8
{15%-125%)
1522579 98.9 (15%rl25%)
!522571 76.9 (15%-125%)
1522578 67.4 (15%*125%)
1525755 88.9 (25%-125%)
1522715 95.6 (15%-125%)
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 * (843) 556-8171 -www.gel.com Certificate of Analxsis Report Date: December 4, 2015 Company :
MJW Corporation Address :
15 Hazelwood Drive Suite l !2 Buffalo, New York 14228
Contact:
Ms. Laurie.Losey Project:
Soil Radioisotopes Client Sample ID: 3.1.18.R.1 Sample ID:
385070012 Matrix:
Soil Collect Date:
20-0CT-I 5 11 :20 Receive Date:
Collector:
Moisture:
05-NOV-15 Client 19.8%
Project:
Client ID:
MJWCOOJ 15 MJWCOOI
-~~r.~~11e~e..~*-*.. _............ - Qu_~J_i~::r....... !lesu_lr _L,li,ic~n.:~i_n_tY..... _l\\~P~'..-..... ~-- ___ *.. __ Units DF Analyst Date Time Batch Method Gravimetric Solids ASTM. D 2216 % Moisture As Received" Moisture 19.8 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Actmium-227 "Dry Weight Conected" lJ 0 103
+/-0 301 Antimony-125 LI 000129
+l-0.12!
Ce5a1m-137 1 12
+/.() 127 Cobalt-60 lJ ll.0364
+/-0.0372 Europmm-154 Protactmmm-23 l Radilllu-226 Radium-228 lJ u
0.00261 0.367 0.866 1 04 Tm-126 U
0224 Rad Gas Flow Proportioiial Counting GFPC. Gross AiB, solid "Dry Weight Corrected".
Alpha 7 56 Beta 23.5
+/-0.116
+/-0.587
+/-0 181
+/-0.279
+/-0.244
+/-2 42
+l-2 39 0 588 0.227 0.0633 0.0807 0229 1.11 0167 0306
_ll 251 3 21 2.63 0.100 4.00 100 percent pCUg pC1/g pCilg pC1/g pCifg pCilg pC1/g pCi/g pCilg.
pCitg pCE!g CXCI 1 lllllfl5 1319 1521842 RXD 12!0.3115 1305 1522383 KXB2 !2i021!5 1128 \\525757 1.11.~ f~llo.~vi_n~ ~~~P. _N_!etJ1o_d_s. ~l{~~_pe_r[<?r.t~~~:.. _............... _..........
Method Description Analyst Date Time Prep Batch DrySoifPre*p*--...... _...-...... '"i5i)--Soi"I Pr~r.-GL~RAD:A~(i'iC............ _........ _.. *cxc1'......... - -i"1rloi(5-....... _ '1':fi9- -.. 'j5~ff84'i""""- -*
!he_f~l-~?:vt~~g-~~~l~ti~~I- ~~~~~?.ds.. \\ve.r~ _perfoE!l1_e_d: __
fyl_c~@!-1.
................ _P.es.~~iQtion_........................... _................... _........................ t\\n.?.-\\y;;t Co1p_!lJ.?TI-t$ __... -....................
ASTM D 2216 (Modified) 2 DOE !-IASL 300. 4.5.2 3!Gn-01-R J
EPA 900 OISW846 9310/SM 71 \\OB Modified Notes:
Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
2 3
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company:
Address:
MJW Corporntion 15 l*luzelwood Drive Suite 112 Buffalo. New York I 4228 Contact; Ms. Laurie Losey Project:
Soll Radioisotopes ClientSampleID:
3.1.18.~.1 Sample ID:
385070012 Matrix:
Soil Collect Date:
20.-0CT-15 Receive Date:
05-NOV-15 Collector:
Client Moisture:
19.8%
Gr11vimetric Solids 1fSTM D 2216 % Moisture "As Recr!ived" Moisture "t9.8 Rat! Gamma Spec Analysis Gammaspec: Gamma. Solid "Dry l*Veight Corrected" Adinium-227 u
- 0. \\03
+/-0.30!
Antimony-125 u
0 00129
+/-0.121 Bismulh-212 Ul 000
+/-0.661 Bismuth-214 0.8<>6
+f-0. tSI c~sium-137 I 12
+/-0.127 Cobalt-60 UI 0.00
+/-0 0372 Europinm-154 u
000261
+/-0.116 Lead-212 0773
+l-0 156 Lea~-214 0978
+1-0 184 Paiassium-40 11 &
+/-1.49 Protacnmum-231 u
0.367
+f-0 587 R.admm-226
() 866
+/-0 181 Radium-228 l 04
+1-0 279 Thall1um-:ws 0 29!
+l-0 107 Tin-126 UI 0 ()()
+/-0 244 Rad Gas Flow Proportional Counting GFPC. Gross AB. solid "Dry Weight Corrected" Alpha 7.56
+1-2 42 l.lctil 23 5
+i-2.39
'f.h..~. follo~v!~~- fr~_P.}:I eth?.~.s. '".er.i.:. pc~.f oxrn.~c.1...................... _......
Metlrnd Description Dry Soil Prep Dry Soil Prep GL-ll.AD-A-021 T~e. ~().l_lo_,v~g-'~~a.lyti~.a! i\\:l_c~.l.104s '"~.r.e.r..er.~ur.111cd.
Method Description ASTM D 2216 (Modified J DOE HASL 300. 4.52.3/Ga:lll-R 3
EPA 900.0iSW846 9310/SM 711013 Modified
() 588 0.227 133 0.167 0.0(133 o ri&o7 0 229 0.173 G.332 0717 11 l 0 167
().JQ(,
0.065 0 251 3 21 263 Report Dale_:
December 17, 2015 Project:
Client JD:
MJWCOOJ 15 MJWCOOJ percent CXCI l !/l0/15 1319 1521842 0277
+/-0 305 pC1/g RXF2 12/03115 1305 1521383
() 105
+/-0121 pC!lg 0.615
+/-() 852 pC1fg.
0.0765
+f-0 195 pCifg 0027S
+1-0 157 O.LOO pCilg 0 0346
+t-0 040S pCitg 0.0989
+/-0l16 pC1/g
() 0832
+1-0. \\68 pCi/g 0.160
+/.() 199 pCt/g
() 301
+f-1 ~2 pC1/g 0 521
+1-0 615 pCllg 0 0765
+l-0 195 pCilg 0.137
+!-0 300 pCi/g 0 029
+/-!l.110 pCilg 0.121
+/-0.245 pCi/g l 46
+/-2.84 4 0()
pC1/g KXB2 121{)2/15 1128 1525757 12&
+l-4.04 10 0 pCilg Analyst Date Time Prep Batch CXCl 11/10/!5 1319 1521842 Surrogatcrrraccr.Recovery Test Batch ID Recovery%
Acceptable Li111its 2
3
GEL LABORATORIES LLC
- 2040 Savage Road Charleston SC 29407 - (843} 556-8171 -www.gel.com Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laude Losey Project:
Soil Radioisotopes Client Sample ID:
- 3. 1.18.R. I Sample ID:
385070012 Surrognteffracer Rec11\\*ery Test Notes:
Certificate of Analysis Report Date:
December 17. 20 I 5 Project:
MJWC'OO I 15 Client JD:
MJWCOOl
'OO OOO>>*o O
OO*O.. OHOOH.. 00000 H
- Vll)C........ L~...
1:'.~l'...... R_L... l.!~its... ~~* j\\!la_lyst_. i)_at~.. *_ri~c.n11.~ch.... 1\\:lt.d..
Batch ID Recovery%
Acceptable Umils TPU and Counting Uncc11ainty are calculated at the 95'% confidence level ( 1.96-sigma).
_J
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 19407 - (843) 556-8171 -www.ge!.com Certificate of Analysis Company:
Address:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Lo~ey Project:
SoH Radioisotopes Client Sample TD:
3.1.18.R.l Sample ID:
385070012 Matrix:
Soil Collect Date:
20-0CT-!5 Receive Date:
05-NOV-15 Collector:
Client
. Moisture:
19.8%
Param.c_!C.~.. -................
9u.'.11~~~r........ ~~~~It...
l1ncertai11ty......... !\\-IDC::.
Gravimetric Solid~
AST,-\\.{ D 2216 % :\\foistitre "1(s Recdved" Moisture Rad Gumm a Spec Analysi.~
19 8 Gammaspec. Gamma, Solid "Dry lf'eight Corrected" Aclmium-227 U
0 103
+/-0 301 Anlimony-125 U
0.00129
+/-0 121 Bismuth-212 Ul 0 00
+/-0.661 Bismuth-214 0.866
+/-0.181 Ccsium-137 Collalt-60 Europium-154 Lead-212 Lead-214 Potassmm-40 Protactmium-231 Radium-226 Radium-228
-niallium-208 Tm-126 lJl LI u
VI Rat! Gas Flow Proportional ('ounting 1.12 000 000261 0.773 D 978 11.8 0 367 lJ.866 l.[)4 0 291 0.00 GFPC. Gross kB. solid "D1:r Weight Corrected"
~~
~
Beta 23 5
- _f_h.e_f~~!~~i.11~. _l'_r~p.J\\:~ ~.t.1~~£1~ -~.ere p_crfor.'!.'~~
Mctlwd Description Dry Soil Prep Dry Soil PrcpGL-RAD-A-021 T.h..eJo.llC}\\Vi_ni;_ i\\lll_l:.ly_t_i_cl11 i\\1.~_thotl~ -~V~T.~.. P~r~C?,rl_Tled.
M.ethocl Description ASTM D 2216 (Modified}
DOE HASL 300, 4 5 2 3/Ga-01-R
+/-0 127
+/-00372
+l-0 116
+l-0 156
+/-0.184
+/-I 4g
+/-ll.587
+i-0.181
+/-0 279
+/-0 107
+l-0 244
+/-2.42
+/-2 39 2
3 EPA 900.0iSW846 93 lOiSM 71 tOB Mod1fi~d 0 S&B 0227 I 33 0167 0.0633 00807 0.229 0 173
() 332 0.717 I II 0 167 0 306 0065 0.251 3.21 2.63 Project:
Client ID:
Report Date:
December 17. 2015 MJWC00115 MJWCOOl Le....... JJ'_L....... ~~.... Ill its. _Df _A_n.?!Ys~.. _
_D_!!-~':.. }'i~c Batch Mttl.
0.277 0.\\0.5 0.615 0.0765 0 0278 O.OWi 00989 00832 0 16()
0 JOI
() 521 0 0765 0.137 0 029 0.121 146 1.26 Analyst CXC!
percent CXCI I 1110!15 1319 1521842
+/.[) 31)5 pC1/g RXF2 12i03115 1305
\\522383 2
+/-0.121 pCi/g
.;./.Q.852 pC1/g
+/-0.195 pCi/g
+l-0 157 0 100 pCi/g
+/-0 0408 pCi/g
+/-0.t 16 pC1/g
+/-0168 pC!.lg
+1-0 199 pCl/g
+/-1.82 pCi/g
+/-0 615 pCiig
+/-01.95 pCi/g
+/-0.309 pC1/g
+/-0110*
pC1ig
+/-0.245 pC1/g
+l-2 84 4 00 pC1lg K..'XB2 12i02/l 5 1128 1525757 3
+/-4.04 10.0 pCi/g Date Time Prep Batch 1ll!Oil5 13 l 9 1521842 Surrogatcffracer Rcco\\'cry Test Ilatch ID Recovery%
Acceptable Limits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (84S) 556-8171 - www.gel.com Company:
Address:
Contact:
MJ W Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Ms. Cauric Losey Project:
Soil RadioL~otopes Client Sample ID:
3.1.1 S.R. l Sample JD:
3&5070012 Certificate of Analysis
.. r~-~!1.£n.e.~c~.......... __. _... _g~-~-l~~e_r..... _R~sult__ __ l;'!)c_e.!'.!l!i!lt"'. _. *- _i\\'.IDC Le Surl'ogateffracer Reco\\*ery Test Notes:
TPU and Counting Uncertainty arc calculated at the 95% confidence level (1.96-sigma}.
Report Date; December 17. :2015 Project:
MJWCOO l 15 Client 10:
MJWCOOI Batch ID Recm:ery%
Acccplnble Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:
Address:
Contact:
MJW Technical Services 15 Hazelwood Drhe Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project Soil Radioisotopes Client Sample ID:
3.1.18.R.2 Sample ID:
3119296013
.Matrix:
Soil Col!ecl Dale:
20-0CT-15 Receive Date:
14-JAN-16 Collector:
Client
~foisture:
13.6%
Paramete.r... ******-**.. _...... 91.1~.li.f.i.~r. _.... !le~':'_l_t****-** r_ncei:!ai_l_l~L..
Gravimetric Sofkls AST.\\.f D 2216 % Moistw*e "1ls Received" Moistun:
13.6 Rad Gammn S1tcc Analy~is Gamma with (ngrowth "Dry Weig/ii Corrected" Acunium-227 lJl 0.00
+/.() 314 An11mony-125 u
-0.0409
- /-0.135
- Bismuth-212 UJ 000
+/-0.807 Bismuth-2!4 0.799
+i-0.183 C<.'h1um-\\ 37 1.83
+!-0 !60 Cobalt-60 u
0019
+/-0 0421 Europium-154 u
-0.0126
+f-0.129 Lead-212 0985
+f-0.135 Lead-2\\-1.
0.923
+l-0 230 PotaSi\\IUm-40 111
+/-1.54 Protactinium-231 UI Qfl(l
+/-0 92*1 Radiurn-226 0 799
+/-0.183 Radium-228 1 05
+/.Q 301 Tliallium-208
() 333
+l-0.079\\l Tin-126 lJ 0.0199
+/-0.195 Gammaspec, Gamma. Solid "D1:1' Weight Correcred
Actinmm-227 lJ
- 0.253
+/-0.H4 Antimony-125 lJ 0 0375
+/-0.134 Bismuth-212 UJ o 00
+/-0 710 Bismmh-214 O 704
+/-0.181 Ccsium-137 Cobalt-60 Europium-154 l.ead-212 l.ead-214 Potas~ium-40 Protactmmm-231 Radtum-226 lJ u
u l 89
-0.0257 0 0103 0 948 0 685 12 I 0.385 0.704
+i-0172
+/-0 0502
+/-(1.140 r/-0 133
+/-0.205
+/-! 42
+/-0 787
+1-0 181 Radium-228 1 16
+/-0 349 Thull ium-208 0.248
- +1-0 0833 Tin-126 l!l
- 0. 00
+l-0 139 Rad Gas Flow Proportional Counting GFPC. Gross A*B. solid Dry Weight Corrl!cted" Alpha 11 5
+l-3 28 17 3
+1.. 2 52 IJ.634 0298
+1-0146 (124CI 0 I IQ
+/.(} !36 1.43 0659
+1-D 987 0.165
().(1752
+l-0 196 0.0837
() 0376
+l*O 228 0 0844 O.o354
+!-0 043 0.250
() 106
+/-0.129
[) 123 00577
+/-0 160
() l87
().0871
+/.() 244 0.661 02M
+/-1 81 I 23 0.577
+/-0 934 U.165 0.0752
+/-0.196 0 340 0.152
+/-0 341 0.ll783 tl.0353
+1-0.0853 0 193 0.0923
+!-0 195 0.569 0 267
+/-0355 0.257 0 120
+1-0 136 I 09 0492
+/-0712
() 163 00746
+/-0.190 0()81i8
() 0365
+(-0 230
{) 0877 0 0378
+/-0.0516 0270 0 I !S
+/-0 140 0 133 0 0628
+/*O 154
() 186 0 0369
+;.0212
() 593 0 237
+/-1 75 1 29 0(109
+/-0.811
() !63 IJ(l7'J(i
+/-0.190 0.304
{) 136
+/-0.383 0 01!8 0 0405
+/-0.0$57 0.!92 00922
+/-0.159 3 91 '
1.73
+f.-3 95 2 77 I 30
+l-J.54 Report Dllte:
February 10, 2016 Project:
Client ID:
MJWC'OOl 15 MJ\\VC001 percent CXCl 01114116 1208 1537312 pCi/g R.XF2 02105/16 0843 1537546 2
pC1/g pCi/g p("ilg 0 100 pC1/g pC1/g pCi/g pCiig pC'i/g pC1/g pCi/g pCi/g pC1/g pCilg pCi/g pCi/g RXF2 01/ll!/16 1123 1537545 pCi!g pCi/g pC1/g 0100 pCi.'g pCi/g p("i/g pCi/g pC1/g pC1tg pC1lg pC1/g pC1/g pCi/g pCilg 400 pC1/g KXB2 0 l/26ll.6 1153 1539462 4
IO I) pC1lg
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
- Certificate of Analysis Company:
Address:
MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, Ni:w Ymk 14228
Contact:
Ms. Laurie Lo5ey Project:
Soil Radioisotopes Client Sample 10:
3.1.18.R.2 Sample ID:
389296013
.1.'a.rll.~.e.te.r....... ***-....
....... 9ua.f.i.~er....
.1:lc.s.u~t..... ~*l)~~r.t~i"1.1.Y....... :\\IDC
- r~~.f.~!~o'".!l_lg_f'i:~.P.. ~J.~_1.!!I!~:~. .er~.P..C.!f.~.r.1ncd,........-. ***-*-....
!Vlcthod Description Le Am1\\yst Date Report Date:
February I 0. 2016 Project:
MJWC00! 15 Client ID:
MJWCOOI Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 01114115 1208 1537312
'J'.he.. f.0.1.l~~~*!!:l.g.i:~!!lllJ~i~a.1_~1!1~<!~~ lve:r.~.pe_i:-f(lrlll.~~........ _.
- \\kthotl Description
- ~***** **-***.... ***-*--* **- *-*** **-...... *****-**-*.... --
1 ASTM D 2216 (1'fod1fied) 2 DOE HASL 300. 4.52JlGn-01-R 3
DOE HAS l.3()(), 4 5 2 3/Ga-01-R 4
EPA 900.0/SW846 93 ll>!SM 71 lOB Modifkd Surrognteffraccr Reco,*cry Test Batch ID l~ecovery% Acceptable Limits Notes:
TPU and Counting Uncertainty are c::alculated at the 95<l*o confidence level ( 1.96-sigma).