ML16294A195
Text
{{#Wiki_filter:*> Appendix G-Sub-Area 3.1.11-3.1.15-COA
GEL LABORATORIES LLC 204D Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company : MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.11.E. l Sample lD: 385070002 Matrix: Soil Collect Date: 21-0CT~ 15 13:35 Receive Date: 05-NOV-15 Collector: Client Moisture: 22.8'% Parameter Result Uncertainty Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moi~ture 22 8 Racl Gamma Spec Analysis Gammaspec, Gamma, Solid Actimum-227 "Dry Weight Corrected" A11t1mo11y-l 25 Cesium-137 Colw.lt-60 Europium-154* Prota~Lin:tum-23 l Radmm-226 Radium-228 ll 0 l67 +/-0.254 u 0.053 l ..-/.().104 ll u u 0 984 +l-0 0988 -0.0236 0.l45 0.476 0946 l.23 +l-0 0349 +/-0.JJI +/-0.571 +/-0 149 +f-0.325 Tin-126 U! 000 +/.() 126 Rad Gas Flow Proportional Counting GFPC, Gross A!B. solid "Dry Weight CotTected" Alpha \\3.S .. 1.. 3 32 lkta 21 0
- +2 81
}'~e.f.~11.l:J~i.~~.. :P!.epJ-:1.~~~~~~.*v~r~.P.".f.f(ll_11~~~:.................. Melhod Descriptfon oiy* s*c;i1 rrer................. *... or;*sc;1rr*icil cir:.~1~,;;:o:A:-02 i.. *..
- T.~.e.f.o.1.19"".i.n!?..0n.alr.ti.c~! M.~Uto?s_."\\:~r~ ~e~f.o.rt1l~~'.... _
M~tho.g......................J=?!':~~r.iptjqn.................... /ISTM D 2216 (Modified) 2 DOE HASL 300. 4.523fGa-O1-R 3 Ef'A 900.0ISW846 93!01SM 71 IOB Modified Notes: Project: MJW(OO! 15 Client ID: MJWCOOI MDC RL Units percent CXCl 11110'15 1319 1521842 (J 482 pC1/g RXF2 \\2/03/15 0846 1522383 2 0 llJ7 pC1lg ll 0738 0100 pCrlg 0060 pCi!g () 255 pCi!g 0 840 pCilg 0123 pCi!g 0 26(> pCi/g 0.135 pCi/g J 46 4.00 p('1/g KXB2 12i02/15 1112 1525757 3 3.25 10.U pCi/g Analyst Date cxC:;i*.. *.... * *-i'iiioiis Time Prep Batch .. i3f9... **-*i52i 842'"............ - *- *******-**-**- .........,.............AiJ.?..LY~LC9-.lillT!f.ltl_tS.... _. Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma}.
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 Hazelwood Orive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Lose} Project: Soil Radioisotopes Client Sample ID:
- 3. l.11.E.1 Sample ID:
385070002 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-l 5 Collector: Client. Moisture: 22.8% Parameter Gravimetric Solids 1IST:'vl D 22 l 6 % llois1ure "As Received" Moi~turc 22 8 Rad Gamma Spc~ Allalysis Gammaspec, Gamma. Solid "Di:v Weigl1t Cor1*ected" Actmrnm-227 U 0.167 +/-0 254 Antimony-125 U 0.0531 +/-Q.104 Ilisnmth-212 Bismuth-214 Cesmm-137 Cobalt-60 . Europium-154 Lead-212 Lcad-214 Potassium-40 Prota.ctinium-231 Radium-226 Radium-228 Thallium-208 u Ul UT 1.53 0 946
- 0. 984
-0.0236 0 00 I 29 I 23 16 5 ouo ().~46 I 23 0364 Tin-126 UI o.oo Rad Gas Flow Proportional Counting GFPC. Gross AB. solid uD1:1' Weighi Corrected Alpllil 13.8 Beta The following Prep Methods were performed ~1~tl;~d*-........ *oc;~~*iptii;;:;... *.............................. D1y Soil Prep Dry Soil Prep GL-RAD-A-02 \\ T~c. fol.lowi11g_~lt~.1~:t.i~~l. ~l~th.ll~~-*'V.e.rc.P~l'.f.l>':".*~e~
- .\\'let hod Description ASTM 02216 (Modified) 2 DOE HASL 300, 4.52JiGa-O\\-R
+/-0.832 +(-0 149 +/-0.0988 +l-0 0349 +/-0.13\\ . <-/-0. \\29 +/-0. \\91 +/-!.34 +1-0 572 +/-0.149 +1-0 325 +/-0_0786 +/*O 126 +/-3 32 +/-U\\ J EPA 900 OiSWS46 9310/SM 71 IOB Modified Surrogatefrracer Recovery Test Report Date; December 17, 2015 Project: Client ID: MJWCOOl 15 MJ\\\\/COOI MDC Le TPL' RL Date Time Batch Mtd. p~rccnt CXCI 111!0/15 1319 \\521842 0.41>2 0 228 +/-0.266 pC1lg RXF2 l2i03115 0846 1522383 2 () !97 00925 +J-0 107 pC1/g 0 628 {) 279 +1-0.847 pC1/g iJ. 123 (}057 +/.0.168 pCilg 0 0738. 0.0343 +1-0.127 () 100 pC1lg 0.060 00261 +1-0.0J65 pCi/g 0 255 0 l \\7 +/-0 147 pCilg ()I 12 () 0531 +/-(} 165 pCilg 0 139 O Of>53 +/-0.216 pC1lg (1455 (l 189 4*/-1 9<i pC1/g 0 840 0.394 '1*/-0 582 pC11g l) 123 0 057 +l-0.168 pCilg 0 266 () 122 +f-iJ.381 pCr!g 0 0624 0 0288 +/-0 0&43 pCi!g l) 135 0064 +/-0.128 pC1/g 3.46 1.51 +l-4:B 400 pCi!g KXB2 12102/15 l l 12 1525757 3 3 2.5 1.54 +/-4.09 10 0 pCilg Analyst Date Time Prep Batch CXC! I tl!O/l.5 \\319 !521842 Batel! ID R~cover)'% Acceptable'.Limils
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.geLcom Company: Address:
Contact:
MJW Corporation 1.5 1-fazelwood Drive Suite I 12 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisoto:pc~ Client Sample 10: 3.1.11.E. l Sample ID: 385070002 Certificate of Anal,ysis
- Report Date:
December 17, 2015 Project: MJWCOOl 15 Client ID: MJWCOOl Parameter....... -.... _......9.u.1tli.rii:r._ ***-.. ~~s.u.it... ~;n~c;.J:tj!Jn.~....... :VIDC' Le ..... _JP_L ... ~.L.. _ l'ni~s DI' Anal}'s; Dat_c !i.l_lle.ll.~~4?~... ~~td. Surrogi1ti!ffracer Reco,*ery Test Batch lD l<cco\\*cry% Acceptable Limits Nutes: TPU and Counting Uncertainty are calculated at t11e 95% confidence level ( 1.96-sigma}.
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: Address:
Contact:
MJW Corporation 15 l!azelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: So.ii Radioisotopes Client Sample ID; 3.1.l l.E.1 Sample JD: 3&5070002 Matrix: Soil Collect Date: 21-0CT-I 5 Receive Date: 05-NOV-!5 Collector: Client Moisture: 22.8% .l'a.r.~.rr_i.eter_............. 9~.'.'!i_fic~~-- Res11I~...... r.o.c.cr.!ai.~.t~*......... i\\'IDC Le Gravimetric Solids ASTM D 22 J 6 *% A-Jois111re "As Received" Moisture
- 22. 8 Rad Gamma Spcc Analysis Gammaspec, Gamma, Sa/id "D1:;* Weigfu Corrected
Actinrnm-227 U 0.167 +/-0.254 Antimony-125 U 0.0531 +/-0 104 Bismuth-212 I.SJ +/-0.832 B15mulh-214 0 946 +/-0.149 0!$1Um-!J7 0.984 +/-0 0988 Cobalt-60 U -0.0236 +/-0.0349 Europium-154 l)I 000 +/-0131 Lead-212 1 Z9 -t-/-0 129 Lcad-214 1 2J +/-0 191 Potassium-40 Protactinium-231 Rildium-226 R~dium-228 Thall ium-208 Tm-126 !JI U! Rad Gas Fiuw Proportional Counting 16 5 (] 00 0.946 1 23 0.364 000 GFPC Gross A.B, solid "D1:J' Weight.Corrected" Alpha 13.8 Beta 21.0 I.h..e. foll.~~~ng P.i:ep !\\_:f~t~1~~s-n:~re pcrfo_r~~~-....... Met bod Description DI)* Soil Prep Dr;.* Soil Prep GL-RAD-A-021 +!-I 34 +/-0.572 +l-0 149 +/-0.315 +/-0 0786 +/-0 126 +/-3.32 +/-2 81 The following Analytical Methods were performed ~i~ii;~;i * ** **-
- --o~;;~.**ipii~~ * * * *-- *** * *--* **** ** ** *** * *
- ASTM D 2216 (Modified)
DOE I IASL 300. 4 S.2 3/Ga-01-R 3 EPA 9000'SW846 9310/SM 71 IOB Modified Surrogate/Tr~lccr Rceo~*ery Test 0.48~ O.l97 0628. 0 123 0.0738 0 060 0.255
- 0. 112 0.139
() 455 !1840 0123 0 266 00624 0.135 3.2:5 \\) 228 0:0925 0 279 0057 00343 00261 0l17 0 0531 1).0653 0 189 0.394 0 057 () 122 0 02&8 ow~4 1.51 1 54 Analrst CXCI Project: Client ID: TPt: Report Date: Dcccmber*l7, 2015 MJWCOOl 15 MJWCODI ~/-0.266 +/-D.107 +/.() 847 +/-0.168 +/-0.127 +/.() 0365 +/-0 147 +/*0.166 +1-0216 +/-1.96 +f-0 582 +1-0 108
- /-0.381
+/-1) 0843 +/-0 128 +/-4 33 +/-4 09 pcrccm pCi!g pCl/g pCilg pC1tg 0 100 pCi/g pClfg pC1/g pCi/g pCilg pCi/g pCi/g pCi!g. pC1/g pC1ig pC1lg 4 00 pCiig HJ 0 pC1/g Date Time l 1110/15 1319 CXCI 1 l/lllll5 1319 1521842 RXF2 12103115 (l84ri* 1522383 2 KXB2 12102115 1112 1525757 3 Prep Batch 1521842 Batch ID Rt>eovery% Acceptable Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 1422&
Contact:
Ms. Laurie Losey Project: Soi! Radioisotopes Client Sample ID: 3.1.11.E. I Sample ID: 385070002 P:i 1:n.TI1 etc r........ _... ____ 9.IJ _;i_li_li~.r-_ -*.. _ .~es~_l_t Surrogatcfl'raccr Recovery Test Certificate. of Analysis Report Date: December 17. 2015 Project: MJWCOO I 15 Client ID: MJWCODI .. l'n~~rla_ifll.Y....... _i\\I~~~...... Le........... 1~!.'!'......... R.-.J,... l!nit~ DF.A.n:1Iy_s~... _.))i1ti;. T.i.llle B_atcl1 Mtd. Batch ID Rccorcry% Acceptable Limils Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level (l.96-sigma).
GELLABORATOruESLLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact Ms. Laurie Losey Project: Soi! Radioisotopes Client Sample ID:
- 3. l.1 I.E.2 Sample ID:
389296007 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 22.&% -~~~a~1.e~~r............... 9u11)_i~~r.. Re_s!1_1t_.... _ l)!cert.~h1f\\:......... J\\:1.DC Le Gravimetric Solids AST:\\.! D 22 I 6 % Moiswre "As Recei**ed" Moisture 22.8 Rad Gamma Spec Analysis Gamma with fngrowrft "D1:i* Weight C'on*ectc:d" Aotimurn-127 U -0.00461 Antimony-125 B1smutl1-2 I 2 Bi~muth-214 Cesium-137 Cobah-60 Europi111n-154 Lcad-212
- Lead-214 Porassium-40 Prornctinmm-231 Radmm-226 Radium-228 Timll mrn-208 Tin-126 lJ u
u LI! lll -01)71)9 1 07 1.18 I 35 ll.00937 O.CJS62 I 25 I 17 15 4 000 I 18 1.23 0.424 0 00 +/.()JOU +/-0.134 +/-0 710 ... l-0 2UO ... /.!J.136 +/-0 0501 +/-0.145 +/-0 134 +/-0 174 +/-1.72 +l-0 763 +/-0200 +/-0.388 +l-0 0832 +/.!l.0899 Gammaspec. Gamma. Sa/id Dry Weii?ht Correc1ed Ac1mrnm*227 l!
- 0. 127
+/-0 443 Antimony-125 lJ -0.0984
- t-/-0 l6n llismuth-212 lJ 0 37\\
+/.() 956 llismulh-214 IJ \\!18 +/-0 235 Ce~ium-137 144 +1-0.183 Cobalt-60 U -0 0486 +/-0.0489 Europium-154 U -0.0346 +/-0. l 7.J. Lead-2 !2 I 41 <-/-0 181 Lead-214 0.988
- /-0.2;i0 Pota>sium-40 Protactinium-23 I Radmm-226 Radmm-228
'rballium-20& Tin-126 \\J Rad Gas Flow Propo11ional Counting 14 7 0.00 0.918 1 78 0 316 0 0695 GFPC. Grass A;B, solid "D1:1' We/gJ11 Corrected" Alpha 12.4 BelD 23.l +/-2 43 +l-l 16 +/-0.235 +/-0 417 +l-0.121 +/-0.156 -t-f-3 64 +l-3.J.4 0 5.60 0.232 I CIS ll 157 0 0821 0 ()994 0 3()1 0.113 0 171 0.931 (1.960 0 263 0 107 0472 I) 07t4 0.037! 0 043--1 (l 133 () 053 00798 0 404 0446 !) 157 0.0714 0266 0.0755 0.112 0805 019! 1 93 U.220 (1.115 00725 0.349 0 163 0.221 l 42 I 20 0220 () 537 0 11:5 0 233 393 418 0.116 (J 0342 0.0537 0 375 0.131 0 866 0.0972 ll 051.}3 ()0239 u 141 0.0759 ()JOO (} 585 11543 () 0972 0.'..:36 [)051 ll lll. I 67 1.99 Project: Client TD: Report Date: MJWC00115 MJWCOOl l'cbrual)* I 0, 2016 .. n.c..... _RL. Y.11its DF.. A_1111lys.t. _Uat_c Frn.c.J3a_t~l1.. :\\ltd * +1-0.300 +/-0 138 t-l-ll 718 +/-0.223 +/.() 174 +/.O 0503
- +1.0 150
"-f-0216 +f-0 208 +/-2 20 -t-/.fJ.787 +/-0.223 +1-0.433 +/-0.0906 .. /-0.0937 +/-0.447 +/-0.172 +l-0 971 +/-0.246 +/-0.216 +/-0.0537 +/-0.175 +/-0.21(1
- '1-0.2(13
+/-2.74 +/-1.20 "'-l*0.246 -rf-0 469 +/-0 123 .,./-0.157 +/-4 37 +1-4 78 0 \\00 0.100 perccnL pC1/g pC1/g pC1/g pCitg pC1/g pC1ig pC1!g pci;g pC1/g pCi/g pC"tlg pC1.lg pCi/g pCr/g pCilg p('1!g pCi/g pC1/g pC1/g pCilg pC1!g pCifg pCi/g pCi/g pC1/g pC1tg pC1/g pCilg pC1/g pCtlg 4 Oil pC1/g lOll pCi/g CXC! 01114116 120S 1537312 RXF2 02i05/I& 0744 1537546 RXF2 01/l8/16 1004 1537545 KXB2 01126116 1 !50 1539462 4
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drh*c Suite !12 Buffalo, New York l4228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample l D: 3.1.11.E.2 Sample JD: 389296007 Parameter ~rhc_f.ollo~\\:i~g_Pre_p ~!~!~'.ld.~_\\\\:ei-e.11.crfor.mcd -* -**..... Method Dc~criplion Dry Soll Prep Dry Soil Prep GL-R.AD-A-021 Jl1c JO..l!.O..'l\\'.i_l})J_r\\'.'a.lyti_c~.1.'\\'.lc_t~.n.~s.~\\:C.re P£'.'.f()~Tl_l~.~..... '.\\lcthml Description I ASTM D 2216 (Modified) 2 3 4 DOE l*IASL 300, 4 5 2 3!Ga-O I *R DOE HASL 300, 4 5 2.3/Ga-01-R EPA 'JOO OiSW846 9310/SM 71 IOB Modifkd Surrogateffraccr Recover)' Test Notes: Certificate of Analysis Report Date: Fehrual)' I 0, 20 l 6 Project: l'vUWCOO I LS Client ID: MJWCOO l !\\IDC i,c ..... TP..l.'.......... ~.L... _\\n_its... 9.Y... :'.\\naly_s1...... l>!1t~ T_ime.. IJ.atc~. ~*ltll_. Analyst Date Time Prep Batch CXCI 01114116 1208 1537312 Batch IIJ Recovery% Acceptable Limils TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: Address:
Contact:
Project: MJW Corporation 15 Hazelwood Drive Suite l 12 Buffalo. New York 14228 .Ms. Laurie Losey Soil Radioisotopes Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Moisture:
- 3. L.12.E.1 385070003 Soil 21-0CT-15 10:25 05-NOV-15 Client 22.6%
Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received Moisture 22 6 Rad Gamma Spec Analysis .Gammaspec, Gamma, Solid "Dry Weight Corrected" Actimum-227 U iJ 0126 +/-0 297 Antimony-125 lJ -0107 +/-0.111 Ccs1um-l37 Cobalt-60 Europitim-154 Protuctinium-231 Radium-226 Rad1um-228 u .u LI Tm-126 lll Rad Gas Flow Proportional Counting !OS -0 0284 0 0371 0.666 I 06 141 0.00 GFPC', Gross A/B, solid "D!Y Weight Corrected" Alpha l6 3 Bm M4 +1-0 120 +l-0 [1415 +1-0.134 +/-0.642 +/-0.187 +!-0 282 +J-0 133 +/-3 'JS +/-3.40 T~~ foU.?~!11~.~~-~P..~1.~t~~d~.\\Ve.re perf.~r.rn_ed:_........ 0 53R 0.189 O.On6 0072 0251 0.997 0 145 0259 0.157 3.95 "01 RL 0 lOO 400 100 Project: Client ID: Units percent pC1lg pC1!g pCi/g pC1/g pC1/g pCilg pC1/g pC1/g pC1/g pCi!g pC1lg. MJWCOOJ 15 MJWCOO! CXCI 11110/15 1319 1521842 RXF2 !2i03/l5 0846 1522383 KXB2 12102115 1112 1525757 Method Description Analyst Date Time Prep Batch or:;:*.sotfiir.eP _..... -* ****-..... ****b"ry* S-Oii"Prep-*nL:RAD~~.(-t)2'1 *.....
- ***cxc1 * ** **** * ***** frfioTis - * * *f3*1**i
... 1.5}t"842"..... *-*. ***-** -*-*.. .. The..f.ol!o\\'>' l.~¥-~~.1.a.l)~ic~l.. 1\\1.~t~~~-s.v.-.e.r~y~rr.~~lll.e.d:............................... J'y1~th~9.. -****.............,.. J;?_e_~cript.(CJ.n........ I ASTM D 2216 (Modtficd} 2 DOF. HASL 300, 4 5 2.3/Ga-Ol-R 3
- EPA 900.0iSW846 9JIOISM 71 lOB Modified Notes:*
Counting Uncertainty is calculated at the 95% confidence level ( l.96-sigma). 2 3
GELLABORATOruESLLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gef.com Company: Address:
Contact:
MJ\\V Corporation 15 Hazelwood Drin! Suite 112 Buffalo. New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.l.12.E.1 Samp[e ID: 385070003 Matrix: Soil Collect Date: 2 l-OCT-15 Receive Date: OS*NOV-15 Collector: Client Moist11re: 22.6% Certificate of Analysis Project: Client ID: Rcpo11 Oate: December 17, 2015 MJWCOOl 15 MJWCOOl Parameter ............. Q.u~~-ifi~1:. Result J:n.cl!r:tainty... )\\.1D( Le ... Et:..... RL.... ~'ni!S_. P..F.. :~11.~l~*st ___ [)JjtC !im.~ _B_a!~h.. ~l.t~. Gravimetric Solids ASTM D 2216 %.\\.foi:slm'e "As Rec<?ived" Moisture 22 6 percent CXCJ 1 l/10/1.5 Bl l) 1521842 Rad Gamma Spec Anal)'Sis Gammaspec, Gamma, Solid "D1:v 11-"<!iglll Corr<?Cll!d" Act!mum-227 ll 0.0126 +1-0297 {) 538 0.256 +/-0 297 pC1/g R..'i:F2 12103/\\ 5 0846 1522383 2 Antimony-125 u -0 IU7 +/-0 111 0 189 0 0889 +/-0 \\21 pCt/g Bismlllh-212 UI 000 +/-0 968 1 27 () 598 +/.J 17 pC1!g Bismuth-214 I 06 +1-0.187 () 145 0.0678 +/-0 208 pC1/g Ccsiwn-137 1.05 +/-0 120 0.0736 110342 +/-0.151 O.IOO pCi/g Coball-60 u -0 0284 ..,.() 0415 0()72 (1.0321 -.-/-0.0435 pCi!g Europium-154 u 0.0371 +i-0 134 0.251 0.115 +l-0.135 pC1!g l.ead-212 !..35 H-0 140 0 l \\7 (I 0559 +/-0.175 pC1/g L~ad-214 14(} +/.O 182 0 329 0.161 +/-0.212 pCJ/g Polassmm-40 \\8 3 +/-1.45 0.h80 li.3()2 +/-2 IJ pCi/g Protuctimum-231 Ul 0.00 +/-0.642 0 997 0474 +/-0 ()59 pCifg Radrnm-226 1.06 +/-0 187 0 145 lJ.0678 +i-0.. 208 pC1lg Radium-228 1.41 +/.Q 282 ll.259 0.119 +/-0.319 pC1tg Thalliurn-208 0.407 ... /.().07\\ () 0677 (Ul3!.5 +/-O.ll791 pCi/g Tm-126 Ul 0.00 ..-/-0.133 0 1.57 00756 t/.(J 135 pC1lg Rad Gas Flow Propol'tional Counting GFPC. Gross A B, solid "DrJ' Weight Corrected Alpha 16 3 +1.3 98 3.95 169 +1-511 4.00 pC1/g. KXB2 12i02/15 1112 1525757 3 Beta 26 4 +1-3 40 4 01 I 'JI +l-5.01 100 pCilg
- 1:~c_f,o]!o,\\~i1_1g_P_r:f.'.P._!\\I~~~~~-8 w~r~
__ per.ro_rm.ed......... -*. !\\-Ictlrnd Description Analyst Date Time Prep Balch OO>*M**** "'" Dry Soil Prep Dry Soil Prep GJ.-RAD-A-021 CXCl l \\ll0/15 1319 15218~2 T_h_e._follcnying_r.'\\n_al~:t\\c~.1.'.\\Ie.th_l)~S-~~.r.'.!Jll!rf.nrm~d
- Viet bod Description ASTM [)2216(Mod1fi~)
2 DOE HASL 300. 4.5 2 3.iGa-01-R 3 El'A 900UISW846 9310JSM 71 JOB l\\fod1fied Su rrogatcffracer Recu"*ery Test Balch ID Recovery% Acceptable Limits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite l 12 Buffalo. New York 14.22&
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID:
- 3. !.12.E.l Sample TD:
385070003 Surrogateffracer Recovery Test Notes: Certificate of Analysis Report Date: December 17. 2015
- Project:
MJWCOOl 15
- Client ID:
MJWCOOI Batch ID Recovery% Acceptable Limits TPU and Counting Uncertainty are calculated at the 95% confidence level ( l.96-sigma}.
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company; Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York !4228 Contact Ms. Laurie Losey Project: Soil Radioisotopes Client Sample TD:
- 3. LI 2.E. !
Sample ID: 385070003 Matrix: So fl Collect Date: 21-0CT-15 Receive Date: 05-NOY-15 Collector: Client Moisture: 22.6% Parameter Gravimetric Solids ASTJf D 2216 % Moisture "As Rrtcdved" Moisture 22.6 Rm.I Gamma Spec Analysis. Gammaspec. Gamma. Solid "Dry Weight Corrected" Actinium-227 !J 0 0!26 +/.O 297 Aniimony-125 U -0 I 07 "'-/*O 111 Bismuth-212 UI 0.00
- +/-0.968 Bisnrnth-214 Cesium-137 Cobalt-60 Europmm-154 Lead-212 l.ead-214 POUIS~lllm-40 Protactmium-231 Radium-226 Radium-228
-Thallium-208
- lm-126 u
u Ul Lil Ratl Gas Flow Proportiunol Counting 1.06 I OS -0 0284 0 0371 1.35 I 40 18 3 ll.00 l.06 141 0407 o.on GFPC. Gross A*B. solid "Dry Weight Correc/ed" Alp\\la 16 3 B~ ~A +/-ll.187 +/.(l 120 +/-0 0415 +/-0.134 +/-0.140 +f-0 182 +/-1 45 +/-0642 +/-0. 187 +(.() 282 +/-[) 071 +/-0 133 +/-3.98 +-/-3.40 J'h~f()l_~~~v,i,1~1; !'.r~P ~-i,c_t~_o_~S. ~v,e.~e..P..e~.fn_r.~1~.d....... l\\-tcthod Description Dry Soil Pr~p DJ}' Soil Prep GL-RAD*A-021 I~.e..~IJIJ.0.1~'.ill~.t'\\'!:ll)'tic!,ll ~c!.h.t_l~S .c.rc __ p_crf()J'.111.e.d..... Method Dc~cription ASTM D 2216 l Mod1ticd) 2 DOE HASL 300, 4 S2JiGn-01-R 3 EPA 900.0fSW846 9310/SM 7l 10B Modified Surrogatefl"raccr Recovery Test Project: Client rD: Repoct Date: December l 7, 2015 MJWCOOl 15 MJWCOOJ M.!?~~-..... Le ..... TJ>~'.... _RL.. l1nits DF Anjjlyst.. _D_a~~-I!'-1.!~.. B_:t_!~l.!.. ~~!t~.. percent CXCl 11110115 1319 1521842 0 538 0 256 +1-0 297 pCi/g RJff2 12103115 0846 1522383 2 0 189 0 088'> +l-0 l2i pC11g I 27 0598 +1-1.17 pC'i!g 0 145 0 0678 +/-0 208 pCifg 0.0736 0.0342
- 1-0. 151 0.100 pCilg 0.072 0 0321
+f.().0435 pCllg 0251 0.115 +l-0 135 pCt!g IJ! l7 OOWJ +/-0. 173 pCi/g 0.329 0.161 +/-0 212 pCi!g 0680 l) 302 +/-2 13 pCi!g 0997 0.474 +/-0 659 pC1/g () 145 () 0(>78 +/-0 208 pCilg 0.259 () 119 +/-0 319 pCi/g 0.0577 (I 0315 +l-0Jl791 pCi/g 0 157 0 0756 +/-0. 135 pCilg
- ' 95 169
+-1-5. l I .i. 00 pCi/g KXB2 12102115 1112 1525757 3 4.01 1.91 +l-5 0 I !0.0 pCl/g !)ate Tinic Prep Batel! CXCl 11/10115 1319 1521842 Balch ID Recovery% Acceptable Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 - www.get.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Contact Ms. Laurie Losey Project: So.ii Radioisotopes Client Sample ID: 3.1.12.E.1 Sample lD: 385070003 Certificate of Analysis ~...............,......... - *-*. -.. -** *-* **-*............... -........ ***-. Report Date: December 17. 2015 Project: MJWCOOl 15 Client ID: MJWCOOJ . ~a.ralll~!.e~................. _9.l!a!if!c.i: _ ***-* l~c_s~_ll __. J *n~cr~aint~:... _i'r1J:)<;::_.... ~c. .. _._F'.~' -*. _. _ -~~ ___ _l~n~ts.. _ I:>.F... :~.~'.l_lyst. ___ 1)at_c __ !_i_~£- _B~f..c~.
- \\~_t_d.*.
Surrogatcffraccr Recovery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at t~e 95% confidence level ( !.96-sigma).
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 * (843) 556-8171 - www.gel.com Company: Address: MJW Technical Services 15 Hazel\\*ood Drive Suite 11'2
- Buffalo. New York 14228
Contact:
Ms. Lnurie Losey Project: Soil Radioisotopes Client Sample JD:
- 3. l.12.E.2 Sample ID:
389296008 Matrix: Soil Collect Date: 21~ocT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 22.7% Parameter .... Qu.~1_li.~C..r. Result Gra\\*imetric Solids ASTM D 2216 % Moisture "As Received" Moisture 221 R:id Gamma Spec Analysis Gamma wirh /11growth "Dry We(r;ht Correctl!d" Actmium-227 L' .Q 0241 Antimony-125 u -0 0245 Bismuth-212 lll 0.00 Bismuth-214 I 17 Cesn*m-137 I 4J Coball-60 lJ -0.0119 Europium-154 L' -0.0941 Lcad-212 l 32 Lead-214 \\.15 Potassium-40 .16.3 Protactimum-231 u 0214 Radium-226 1 11 Radium-228 t.27 Thall iuin-208 0.371 Tin-126 u 0 U343 Certificate of Analysis t'_11 c.c.rt.:1.i.n.ty..... !\\IDC Le +/-0 308 0.549 0260 +/-0.114 {) 203 U.095 +/-0.809 135 0.637 +/-0 153 0 127 0 OSR4 +/-0 117 0.0674 0 031 +!-0 039 () 0668 0.0293 +/-0 131) {) 222 0.()998 +/-0. l 32 0.110 0.0518 +/-0.2IO 0 324 {1158 +/-1.34 () 641 0 2!l0 +f-0.606 1.02 0.482 +I-() 153 () 127 00584 +1-0 300 0 261 O ll'J +/-0 0751 0(174 0.03.:15 +J-0 159 0.194 ()0936 Tl'li +/-0 JOS +/-0 114 .;./.1 31 +/-0.181 +/-0 164 +/-0.0394 +/-0 137 +/-0 169 +1-0230 +/-1 95 +/-0615 +/.{l 181 +l-0 362 +/-0.0&12 +/-0 160 Report Date: February 10, 2016 Pmject: Client ID: MJWCOOI 15 MJ\\VCOOl RL l'nits percent C'XC1 01114116 1208 1537312 pCi/g RXF2 021()511() 0745 153754.6 2 pC1lg pC1lg pCi.'g u 100 pCilg pC1lg pCi/g pC1lg pCtlg pC1/g pCilg pC1lg pCi/g pCiJg pC1/g Gammaspec. Gamma. Solid Dry Weighc Con*ecrl!d". Acunium-227 u
- O 203
+1-0.260 0°16[ 0 214 +/-0.278 pCiig RXF2 01118116 11:40 1537545 3 Antmiony-125 u ()0615 +/-0.116 0223 1).11)3 +/.() 11~ pC1/g B1smu1h-212 Ul (l.00 +/-0.843 146 ().676 +1-0 997 pCi/g Bismulh-214 1.00 f-l-0 174 0.147 '()l)n68 +/-0 193 pCi/g Cesium-137 I 35 +/.() 141 1)0947 0 0435 +1-U.177 0 JI}() pCtlg Cobalt-60 u -0 0423 +1-00438 0070 0.0289 t/-0.0479 p('i/g Europmm-154 u O.JO! +/-0 143 0.300 0.134 +i-IJ 150 pCi/g l.eod-212 1.28 +f-0.131 O. Hl8 () 0508 +/-0.217 pC1/g l.eud-214 1.21 ol-/-0 182 0 355 () !72 +/.t) 216 pCilg Potassiuin-40 16 5 +/-] 65 (! 750 0315 ol-i-2.20 pC!/g Prolactinium-23 l Ul 000 +/-U.805 {) 936 fl 435 +/-0816 pCi!g Radmm-226 I 00 +/-0.174 0.147 011668 +/-0.193 pCilg Radmm-228 142 +/-U 2CJ4 0208 00874 +/-0 368 pC'i/g Thalhum-208 0.466 +/-0 0933 fJ.0706 0 031& +1-0.!0l pCtfg Tin-\\26 Ul 000
- 1-0.0929 0.106 0 0503
+/-ll.0949 pCi/g Rad Gas Flow Proportional Counting GFPC. Gross A:B. solid "Dr.Y JJ.'eighi Con*ected" Alpha 13.2 ..-J-.3.11 3.89 1.65 <*/-4 51 4.UO pCi/g KXB2 01 i26116 I J 56 1539462 4 Beta 26 2 +/-3 18 287 1 33 +f-5 03 10 {) pCilg
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843} 556-8171 -www.gel.com Certificate of*Analysis C'ompany; Address: MJW Technical Services IS Hw.clwood Drive Suite 112 Buffalo. New York t-1228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.l.12.E.2 Sample ID: 389296008 Report Date: fcbruary I 0, 2016 Project: MJWCOOl 15 Client ID: MJWCOO I _I_'ar~111~_e_t_~.r....... ___ ***-. *-* _.Qu_:ili_li<<:r_ ***-.. ~c~_u!.t....... lJn.~cr1:1~11t.-...... Mf)C'....... L~.......... T.f>L. -* _.. ~!,.. Y.n.i.ts_... l?F _ ,~nnl~:.~.t.. .IJ.~~e '(imc __ B_~tc_ll.... ~*!t~, 'f.he __ follnwi!ll:l J>rcp ~~ct.~~tls ~H~r.e _ _pe_r_f!Jf.!'.ICl~.... -*..... *********-**......
- 'vi et hod Description Anal~*st Dry Sml Prep Dry Soil Prep OL-RAD-A-(l2l CXC l T.!.1.~. f.ollo~vi11g i:':.n~ly_ti_c111. ~1.E!i~_O.d..s.Yl'el_'~J_le~ftJ.r:*n.:e.~...............
Method Description 2 3 .\\ ASTM D 2216 (Modified) DOElIASL 300. 4 5.2 3/Ga-01-R DOE llASL 300. 4 5.2JiQa,{IJ-R EPA 900.0ISW846 9310/SM 711 OB.Modified. Surmgnteffracer Recovery Test Notes: D:ite Time Prep Batch ()l/14/16 l208 [537312 Batch ID Recovery% Acceptable Limils TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Reporl Date: December4, 2015 MJW Corporation Company; Address; 15 Hazelwood Drive Suite 112
Contact:
Buffalo, New York 14228 Ms. Laurie Losey Project: Client Sample ID: Sample TD: ~.?ii r.za~i()_i_~ot°.p~s. 3.l.13.R.1 3&5070004 Matrix: Collect Date: Receive Date: Collector: Moisture: Soil 21-0CT-15 10:55 05-NOV-15 Client 20.5% Parameter........... __...... Qu_~l_ifle.r....... ~~-t_i_I_t_.. l!ncertainty Gravimetric Solids ASTM D 2216 % Moisture "As Received"
- \\lo1 sture 20 5 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Con-ected" Actmium-227 U
0 121 ""/-0.266 Antlmony-125 Cesium-137 Col>alt-60 Europmm-154 Protactinium-231 Radium-226 Radmrn-228 u u u u Tin-126 U .Rad Gas Flow Proportional Counting -0.0425 0 966 0.0291 0.0314 a 90s 0.964 0 679 0 112 Of PC, Gross A/B, solid "Dry Weight Corrected" Alplla
- 8. \\7 B~
IU
- n~e. fol_lo~~i-~~.. i;>r~r. lv_let~~-~.S._\\~~1~e _pe_rfo1111e.d_:
+/-0 111 +/-0.126 +/.O 0422 +/-0.136. +1-0.859 +/-0 208 +l-0 385 +/-0 124 +1-2 26 +/-2.09 Method Description Df)*SOii r*rcp*,**..... *-.... --. "Ill)* 'sOif Prep**oL=R.ftj).A'-021'....,... _Th.~.~?~ l_~l\\vi~t;. f\\_nal_y_ti_ca_!_ ~e_t~?~S. ~~'.:. P..~.r~°.rin.~.~'.. Me_llt9.~......... _........... pe~criptic;i,ri.__... ASTM D 2216 (Modified) DOE HASL 300, 4 5 2 3/Ga-01-R EPA 900 OISW846 93 IO/SM 71 JOB Modified MDC 0 537 (1.201 0.107 0 0935 o.273 ()%8 0.146 0.302 (l \\J5 2.68 2.47 RL 0.100 40() !OJ) Project: Client ID: Units percent pCi/g pC1/g pC'l/g pC1lg pC1/g pC1/g pCi!g pCi/g pC!/g MJWCOOll5 MJWCOOI C'XCI 11/10115 1319 1521342 RXF2 12i03!15 0&47 15223g3 KXB2. 12i02/l5 1114 1525757 Analyst Date Time Prep Batch ... CXCT ... *-.. **1t.iit}.ij5**....... ****-i3fl~***-******152'i84i... *-*******......,......... 2 J . A.i1!llyst~mmni;:r.1t.~....... Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96*sigma).
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 1-lazclwood Dri\\'c Suite 112 Buffalo, New York !4228
Contact:
Ms. Laurie Lose,;' Project: Soil Radioisotopes C licnt Sample lD: 3.1.13.R. ! Sample ID: 385070004 Matrix: Soi! Collect Date: 21-0CT*l5 Receive Date: 05-NOV-15 Collector; Client Moisture: 20.5% P11rametcr G1*1ivimctric Solids ASTJf D 2216 % Moistzmr "As Received" Moisture 20.5 Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry Weight C~orrected" Actmium-227 lJ 0.121 +/-0266 Antm1011y-i 25 l) -0.0425 +f-0.1 l I 13ismulh-212 l.86 +1-0.689 Bi~muth-214 0.964 +/-U.208' Cesium-137 0.966 +/-0.126 Cobalt-60 U (l 0291 +t-0 0422 Europium-154 U 0.()314 +/-O. l36 Lcad-2 ll
- 1 04
+/.Q 16 l Lead-214 0.786 -t-1-0 218 PoUl5s1um-40 Protactinium-231 Radrnm-226 Radmm-22& Thallmm-208 Ul 109 0.00 0.9M ll.679 0.385 Tin-126 Ul 0 00 Rad Gas Flow Proportional Counting GFPC. Gross AiB, solid "D1y 1-Veight Corrected" Alplia 8 17 Beta 16 3 !_11.~..f~!!<:l'vin.g J.'rep M.etl1i:i~~-'~e.r:e.. pc~~o.rn.1c.d. Method Description Ory Soil Prep 0[)* Soil l'r"P GL-RAD-A-021 ".f~~.e.f<>.1.lo~~i!lg,\\_11~ly!l~~l.. ~l~t.~o.~s- "'.(!l'C perf()r.!.11_e~ Method Description ASTM 022l6(Modified) DOE llAS1, JOO. 4.5.2 3/Ga-Ol-R +J-1 55 +1-0 859 +l-D.208 +/-0385 +1-0.077 +!-0 124 +/-2.26 +f-2.09 2 3 EPA 900_0ISW846 93IOISM 71 lOB Modified Surro1!:ale/Tracer Recovery Test MD("... Le 0.537 0 251 0201 0.0921 1.07 0 47g 0.146 0.0658 (1107 0 0493 0.0935 (}0404 0.273 0 119 0.137 0 {)647 0.!59 110736 0 407 0 140 0.968 0.449 0.146 0 0558 0 302 0 134 0 0737 00332 (l 135 00638 2 6g I l'l 2-47 I 18 Analyst CXC! Repml Date: December l 7, 2015 Project: Client ID: MJ\\VCOOl !5 MJWCOO! Jl1.ll....... _R,1~... X_ni.ts..... DF A!?a)y~~... f.>al~ !J.~~.!l.a.tch Mid. p;;rcent . ('XCI 111101\\5 1319 1521842 +/-IJ272 pCi/g R..XF2 12/03115 0847 15223K3 2 +/-0.113 pCrlg +/-0.713. pCi/g +/-0-224 pC11g +/-U.149 0 100 pCilg +/-0 0442 pCl!g +J-() 137 pCi/g +/-0.182 pCl!g +/-0 228 pC1lg +/-I.Bl pCifg +/-0 383 pCi!g
- 1-/-1)224 pCi/g
+l*O 396 pC1/g +/-0 0841 pC1!g +/.() 125 pCi!g +/-2.78 4 00 pC1/g KXB2 12!02/15 I I 14 1525757 3 +1-3 23 10.0 pC1/g Date Time Prep Batch I l/!0115 1319 1521842 Batch 10 H.ecovery% Acceptable Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company: Address: MJ\\V Corporation l5 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.13.R.1 Sample JD: 385070004 Certificate of Anal;ysis Report Date: December 17. 2015 Project: MJWCOOI15 Client ID: MJWCOOJ J>ar_a.n1_c_t~.r..... _....... Qllal!ficr... _ _l~e~-~t. _ V11~ertiii11ty MDC Le ..... __.. IPY.. -*..... }~~..... ~!.~.~t.!'.. _ I)_~-- ~-~~~l.Y-.s.t.... !?.a.t_e_ !}.~~l'... !l~.~~h..... :\\1.td'.. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite J 12 Bufla!o. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.13.R. l Sample ID: 385070004 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 20.5% Certificate of Analysis Project: Client rD: Report Date: December 17, 2015 M1WC00115 MJWCOOI P~r:i.~c~e~..... .. *- _.. _....9.~a!i_fle_~****.. Res_u_l_I_. ___ I_l).c_cr.tain,tv Ml.>.C:.. 1.c.... _. ___ Tl'V.... RL l"nits. D.l'.. ~\\na,lyst.... _l)n,!_~ __ l_'im..~. !3!1~c-~.. ~~~* Grnvi1i1ctric Solids ASTM D 2216 % Moiswre *~*1s Received" Moisture 2l>.5 Rad Gamma Spec Analysis Gamma~7Jec, Gamma, Solid "Dry Weigh! Correcti!d" Actmium-227 u 0.121 Antirnony-125 u -0.0425 Bismuth-212 1.86 Bismuth-214 0.964 Ccsium-137 0.966 Cobalt-60 lJ 00291 Europmm-154 u 00314 Lcad-212 1 04 Lcnd-214 0786 Pota5~ium-4() 109 !'mtactiniurn-231 .Ul 0()0 Radium-226 0.964-Radium-228 0.679 Th.allium-208 0.385 Tm-126 lJl 0.UO Rnd Gas Flow Proportional Counting GFPC', Gl'oss A. B.. mlid "DrJ' Weigln Corrected" Alpha S.17 Beta 16 3 +/-0.266 +/-0 111 +/-0 68'J +/-0.208 +/-0.12.6* +1-0 0422 +/-[).136 +l-0 161 +l-0 218 +/-I 55 +/-0 859 +/.CJ.208 +/-0.38'5 +1-0.077 +/-0.124 -i-/-226 +1*2.09
- r.Jtl.!.. ~o.!!C!.'!:i~t; J.'rc_p.~1el~(_l_d~-~~r,e __ pcrfo_r.~.C..~................. _
l\\!lethod Descriplioo [)ry Soil Pr!!p Diy Soil Prep GL-RAD*A-021 T~.C-~l)_H~_why~ r\\n_~_lytiC.jll :VI~t.l~t1.~s __,~ere !'l.!1'.f.oi::1~cd _
- Vlcthod Description I
2 3 ASTM D2216 (Modified) DOE HASL 300, 45.2.3/G<i-O1-R EPA 900.0ISW846 93!0/SM 7l IOB Modified Su.. rogateffracer Recovery Test (I.537 0.201 I 07 0.146 0 !07 0093~ IJ.273 0.137 0.159 0407 0.968 0.146 0 302 0 {1737 0 l35 2 68 2.47 ll251 0.0921 0479 0.0658 ()0493 (}0404 0.119 0 (1647 0 0736 0.140 0449 0.0658 () 134 0 0332 () 0638 I 19 l !R Analyst CXCI +1.0 272 +!-0 113 +/-0 713 +/-0 224 +/-0.149 +/-0.0442 +/-0 137 +r-0.182 +f-ll 228 +/-I 81 +/.I) 8R3 +/-0 224 +/-0 396 +/-0 0841 +1-tl 125 +/-2 78 +/-3.23 perce1tl pCi./g pCi/g pC1!g pCi/g 0.100 pC1lg pCi/g pCi/g pCi!g. pCifg pCi/g pCilg pCi/g pC1lg pCi!g pC1lg 4.00 pCi/g 10 0 pC1/g Date Time l l/10!!5 1319 CXCI 11/10!15 1319 1521842 RXF2 1210311.5 0847 1522383 2 KXB2 12/02115 l l 14 1525757 3 Prep Batch 1521842 Batch ID Recovery% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company: Address; Contact Project: MJ W Corporation 15 Hnzclwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Soil Radioisotopes Client Sample ID: 3.1.13.R. I Sample ID: 385070004 Surrogalerfracer Recovery Test Notes: Certificate of Analysis TPU and Counting Uncertainty are calculated at the 95'l-'o confidence level (l.96-sigma). Report Date: December 17, 2015 Project: MJWCOOJ 15 Client ID: MJWCOOI Bakh ID Recovery% Acceptable Umils
GEL LAB ORA TORIES LLC 2040 Savage Road Charleston SC 29407 - {843} 556-8171 - www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazel\\\\ood Drive Suite 112 Buffo!o, Ne*w York 14228
Contact:
Ms. Laurie Losey Project Soil Radioisotopes Client Sample ID: 3.1.13.R.2 Sample JD: 389296009 Matrix: Soil Collect Date: 2l~OCT-l5 Receive Date: 14-JAN-16 . Collector: Client Moisture: 22.4% Parameter .. 9!1~.1.i_lie~.... Rcs_u~t-... J)~ccl'_I~ in_ty_...... i\\1DC Gravimetric Solids ASTM D.:?216 % !vloisture "As Received" Moisture 22 4 Rad Gammn Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actmium-227 IJ 0172 Antimony-125 l! -IJ.000515 Bi~muth-2 l 2 1.52 l31~muth-2 I 4 0.785 Cesium-137 0.991 C'oball-60 lJ -0022 Europium-! 54 lJ 00246 Lend-212 1 JO Lcad-214 0 998 Potassium-40 12.0 Protaclmium-231 UI 0.00 Radium-226 () 785 Radmm-22_8 Ul 0 00 Thnllmm-208 02% Tm-126 u 0.0406 +J-0 331 +/-0 119 +/-0 645 +/-0 179 +1-0 123 +1-0 os ts +/-0 128 +/-0 140 +J-0 204 ... 1-1.1>3 +f-0 91)3 +/-() 179 +f-0 328 +/-0 074 +/.() 114 Gammaspec. Gamma. Solid "D1y Weight Corrected" Actinium-227 u () l l3 +/-0.345 Antmiony-125 lJ -O.ll00289 +1-0 143 Bismulh-212 UI 0.00 +1-1.21 Bismulh-214 0.618 +1-0 184 Ccsium-137 1.10 +l-0 142 Cobalt-60 UI 000 +f-00285 Europium-154 u -<Hl409 +/-0.139 Lcad-212 0 986 +/-0.148 Lcad-214 0 994 +/-0.280 Potassium-40 11.8 +l-1.65 Protactmium-23 l UI noo +/-0.622 Radium-226 0 618 +/-0.184 Radmm-218 Ill +/-(] 281 Thalltum-208 0.326 +!-0 HJ4 Tm-126 UI 0.00 +/-0 l'l2 Rad Gas Flow Proportional Counting Gr"PC. Gross.-1 B. solid "D1:i* Weigh1 Correc:ti!d" Alpha 11 9 +/-3.8! Beta 21 <) +/-2.90 U63l 0.216 0.792 () 171 0.0733 0.0944 0.236 () 137 0 173 0.917 I 05 0 l7l I) 650 (l.()756 0 213 11658 0264 I 65 0 170 0.0823 0.0&45 0258 0 l3R 0 376 0 818
- l. tO u 170 0271
<l.084 {) 263 399 2.5~ Le ll.297 +/-0.342 0.0987 +/-0.l t9 0.339 .. 1-0.666 0 0785 +/-0 193 0.0325 +l-0.153 0.0404 ~1-0 0527 0.0998 +/-0.129 00642 +1-0 173 (l 080.J +l-0 223 0.392 +/-193 0.485 +/-0922 0 0785 +/-() 193 0 307 +/-0 539 O U34 +/-0 0786
- 0. !02
+/-0 116 0 31<1 +/-0 349 0.123 +/-0.143 () 763 +l-1 42 (J.077 +1-0.191 00367 +1-0.168 0 0354 +/-0 0348 () 111 +/-[} 140 O.llM8 +/.JJ l 67 ll 182 +f-0 290 0 342 +/-I 95 0.510 .,./-0.63& 01177 +/-ll.\\91 0.117 +/-0 315 O.fl3S ... 1-0.107 ll.126 +/-0*193 I 65 -4*/-4.44 l 16 +l-4.31 Project: Client JD: Report Date: MJWCOOl 15 MJ\\VCOO I February IO, 2016 percent CXCl 01114116 1208 1537312 pC1/g RXF2 02i05/l6 0747 1537546 2 pC1/g. pC'ilg pCi/g; 0.100 pCi!g. pC-1/g. pC11g pCi/g pC'i/g pC1lg pCi/g pC1lg. pCilg pCi/g pCi!g pCiig RXF2 01118/16 I 12\\ 1537545 pCi/g pC1/g pC'ilg O.IUO pC1/g pCilg pCiig pC1lg pC1!g pCi.'g pCi/g. pC1lg pCi/g pCilg. pC1lg 40() pCi.lg KXB2 Ol/26116 !152 1539462 4 10.0 pCilg
GEL LA BORA TORIES LLC 2040 Savage Road Charteston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Ilazelwuod Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: J.1.l 3.R.2 Sample ID: 389296009 l'ar~m~_1:e.~-........... Qtrnli_ffor.... _ ~.esul~..... l!!lm~J1.i11ty_.. ~me::. The.f ~H°.\\\\'.i_rtg_ f_r_c.J.l.~1.c!.~O_<~.~".~.r~. P.<<::r.f.o.rm_e4..............
- \\fotho<l Description Le Analyst Date Report Date:
February !O. 2016 Project: MJWCOO ! !5 Client ID: MJWCOO I Time Prep Batch Dry Soil Prep Dry Soil PrepGL-RAD-A-021 CXCI 0 l/l4f16 . 1208 1537312 1:bc.. fo.~Jo_\\fi_ng_1\\n_a!Y,ti~a~~lC!~()~~ \\~'.C.~ pe.r_fol_'Jl1Cd............ ___.. Method Description 1 3 4 ASTM D 2216 (!vh1dified) DOE HASL 300..4.5 2.3/Ga-01-R DOE HASL 300. 4 5 2.3/Ga-01-R EPA 900 OfSW846 9310/SM 71 IOB Modified Surrog:itcrrrncer Recovery Test Notes: TPV and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Batch ID Reco-n~ry% Acceptable Limits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-B171-www.gel.com Ce.rtificate of Analysis Report Date: December 4, 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisolopes Client Sample JD: 3.l.l4.R.J Sample 10: 385070005 Matrix: Soil Collect Date: 21-0CT-15 10:20 Receive Date: 05-NOV-15 Collector: Client Moisture: 18.3'% Paramct~r......... _....... _. 9ua!ifier. _ -~~-s~:l_t. _U11certaJn:t>-* Gravimetric Solids ASTM D 2216 % Moisture "As Received Moisture 18 3 Rad Gamma Spm:: Analysis Gammaspe~. Gamma, Solid "Dry Weight Corrected" Achnrui:n-227 U -0 143 +/-0.26& ll.nt1inon}*-125 U -0 126 +/.lJ 10 I Ces[um-137 I 3(! +/-0 128 Cob~lt-6U lJ -0 0090 I +/-0 0442 Europium-154 U 0 00656 . +/-0 118 Protactmium-231 UI 0 00 +J-0.71 R Radtum-226 0.770 +/-U 161 Radiurn-228 O.\\l8S +1-0.281
- Tm-12&
U! 000 +/-0.0927 Rad Gas Flow Proportional Counting GFPC. Gross A/B, solid "Dry Weight Corrected". Alpha 9 96 +1-3 08 Bel~
- 21) 0
+/-2 46 The _t?.Il~.~in~_.Pr.e.P.... M!?tlJ..CJ.~~-~~re.. e~r[o_rrne~.:........ _........... Method Description ofi sii*irri~ii * ** *** ** ** ** * -*** * * * **or; *siii1 1*~.;*r c;c:::R.:i\\o:,;,.:i:ii-i * ** Project: Client ID: MJWCOOl 15 lVUWCOOI IvIDC RL (J 482 0 173 0 oss 0.0833 0 232 0 81 I 0 124 02~4 ()0936 3 99 306 lJ lllO 4ll0 100 p~rcont pC1!g pCi/g pC.lg pCi/g pCiig pC1/g pC1rg pC1lg pCi!g pC1/g p('1/g CXCI 11/J0/15 1319 1521842 RXF2 l 2i03/l.5 0&47 1522383 KXB2 12/02115 I\\ 14 1525757 Analyst Date Time Prep Batch
- *c*xcr -******** - *iifi011:s*
1319
- fsii-842********- -****
.T..~-~-'..?_l!.o.v.ving J\\.n.a_IXti_~_a! ivlet'.1(}~s -\\~~r~ pe_rform_ed_:............................... Mt:t.hq~... _.............. P.c.~~rl.P_tio!, __....... .. -***-** b.l.l!!:IY_~t c;::0111!1.1~m.~. I ASTM D 22 \\6 (Modified) 2 DOE HASL 300. 4 5.23/Ga-Ol-R 3 EPA 900.0/SWll.\\6 93 IOiSM 71 IOB Modified Notes: Counting Uncertainty is calculated at the 95% confidence fevel ( 1.96-sigma). 2 3
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Bu!Tulo, New York l4228
Contact:
Ms. Laurie Losey Project: Sot! Radioisotopes Client Sample ID:
- 3. !.14.R. l Sample ID:
385070005 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 18.3% Parameter ........ _.9~1.l_lifi.e'........ -~~sult Cnccrta.int)' *-..... ~!D~ Griwimetric Solids ASTM D 22!6 % ivloisture "As Receil'ed" Moisture Had Gamma Spec Analysis 18.3 Gammaspec. Gamma, Solid "D1y Weight Con*ected" Actinium-227 U -0.143 +/.(l 268 Annmony-125 ll -0.126 +1-0 101 l3i~mu~1-212 !Jl 0.00 +1-0 555 Bismulh-214 0 770 +f-0.16! Cesium-137 I 36 +f-0, 128 Cobillt-60 u -0.00901 +1-0.0442 Europium-154 ll 0.00656 +l-0. 11 S Lcad-212 1.07 +/-0.112 Lead-214 0817 +/-ll.194 Potnssium-40 11 5 +/-! 34 Protactmmm-231 Radium-226 Radium-228 111alhum-208 Tm-126 lll Ul Rad Gas Flow Proportional Counting 0()() 0.770 0 988 0277 0.00 GFPC Gross ;[:B, solid "Dry 1-Veight Corrected" Alph<i 9 96 Bern 20.u
- r~~.!~l_h1_\\l:!~g.P._r~p-~l_e_t~'?-~~ _\\\\:er,cpi;1:rori,n_c~!._.. _. -*
Method Dcscriplion +/-0.71 B +/-0.161 +/-(l.281 +/.II 0893 +i-0 0927 +/-3.08 +/-2.46 Ory Soil Prep Dry Soil l'tep GL-RAD-A-OJ I The following Analytical :\\fothods were performl'd -~~th~ii *** * ** *** ** .n~~~-~ip.iian* *.... ** ***** - -** * -- 2 3 ASTM 02216 (Modified) DOE I IASL 300, 4.5.2 3iGa-01-R EPA. 900.0!SW846 93 IOiSM 71 lOB Modified Surrogatefl'raccr Recovery Test 0.482 0.173 1 14 () \\24 0.0S.5 0.USJJ 0 232 0 IUI 0 137 () 7~13 {) 811 ().124 0244 0.0735 0()936 3.9\\l 306 0 228 0.0796 0 523 () 056 0 0392 0.0364 0 10:?. 0.0478 0 0639 (IJl9 O.J"I& 0.056 0 108 0.0338 () 0449 1 so 147 Analyst CXCl +1-0 277 +1-0 117 +/-0.613 +l-0.173 +/-0.172 +/-0.04*14 <-1-0 118 +/-0.173 +l-0 207 +/-! 74 +l-0149 +/-0 173 +/.() 3 lfl -t/-0.0924 +/-0.094& +1-370 +/.) 86 Date Report Date: December 17, 2015 Project: Client ID: MJWC'00115 MJWCOOI percent CXCI pC'i/g RXF2 pCLig pCllg pCi/g 010(1 pCi/g pCi/g pCi/g pC1/g pCLlg pC!/g. pCi/g pC1/g pC1/g pC1/g pC1/g l\\110115 1319 1521842 .12103115 0847 1522383 2 4.00 pC1/g KXB2 12102115 1114 1525757 3 !O.O pC1lg Time Prcf1 Batch 11110.115 1319 1521842 Ilatcb ID Recovery% Acceptable Umits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company: Address:
Contact:
MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 M~. Laurie Losey Project: Soil Radioisotopes Client Sample fD:
- 3. !.[ 4.R.I Sample ID:
385Q_70005 Surrogatcffnu:er Reco\\*ery Test Notes: Certificate of Analysis TPU and Counting Uncertainty are calculated at the 95%1 confidence level ( 1.96-sigma}. Report Date: December 17, 2015 Project: MJWCOO l 15 Client ID: MJWC001 Batcb lD Recovery% Acceptable Limils
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -{843) 556-8171 -www.gel.com. Certificate of Analysis Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes. ClientSampleID: 3.I.14.R.l Sample ID: 385070005 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 18.3% .~ar:im.~t~r.................. _q~~lif.i:~.r... .~csult . l!ti~-~.r.ta.i*\\.tv...... i\\:IJ>~. Gravimetric Solids ASTJf D 2216 % Moisture ".-fs Recefred" Moisture 183 Rad Gamma Spec Analysis Gammaspec. Ganmw. Sofid "D1:v Weight Corrected" Actinium-22 7 ll -0.143 +/-0.268 0 482 Antimolly-12:5 u -0.126 +l-0 IOI 0 173 Bismuth-212 UI 000 +l-0.555 1.14 Bismuth-214 0770 +/-0.161 0 124 Cesium-137 1.36 +/-0 128 0.08:5 Cobalt-60 u -0.00901 +/-0.0442 0 !1833 Europium-154 lJ 0.00656 +/-0.118 0.232 Lcad-212. 1.07 +/-0I12 0.101 Lcad-214 0.817 +/-0.194 0.137 Pub~siurn-40 11 5 +/-134 0 743 Protactmium-231 U! 0.00 +/-0 718 0 811 Radium-226 0 770 +/-0 161 () 124 Radium-228 () 988
- 1'/-0281 0.244 Thalhum-208 0 277
+/.(] 0893 0:0735
- ['in-J2C1 l!I O.ClO
+/-0 0927 0 093t\\ Rad Gas Flow Proportional Counting GFPC Gross A.'B, solid "Dry if'eight Corrected" Alpha \\l.96 +/-3.08 3 99 Beta 20.0 +/-246 3.06 'fhc followil1g Prep Melhods were performed
- Vi~th~d ______....... "*u*e~c~ii;ii~~....... -.............. *..
- Dry Soil Prep Dry Soil Prep GL-RAD-A-02 l
!~.I! r~.1.101~~~g.. \\na,l)'~_ic:t~ ~e~h.o~s.w~~i: p~rr~.r~1c.d.. ' Method Description ASTM]) 2216 {Modified) 2 DOE HASL 300, 4.5.2.3/Ga:ot-R 3 EPA 90U.0/SW846 9310/SM 71 IOB Modified Surrngatcffracer.Recovery Test Project: Client TD: Report Dale: December 17. 2015 MJWCOOJ !5 MJWCOOI ..Le......... :rrt.! __........ l!-L..... l:n.i!S... l!f. :.\\11.:ilyst. _,J):it.~_!i~.c.. B.atch --~ltd. () 228 (J 0796 0 523 0056 00392 0 0364 0 \\02 0 0478 0 0639 OJ\\9 OJ78 0.056 0 108 () 0338 0 0449 1.80 147 Analyst CXC! +1-0 277 +1-0.117 +1-0 613 +/-0. 173 +1-0 172 +1-0.0444 +/-0.118 +/-O.l7J +/-0 207 +r-1 74 +/-0 749
- /-0 173
+/-0.310 +/-0.0924 +l-0 0948 +/-170 +/-3 86 Dute 1 )/10115 percent CXCI 1 tll0/15 1319 1521842 pCiig RXF2 12/03/15 0847 1522383 2 pCrJg pCi/g pC1!g 0 !00 pC1/g pC1/g pCi!g pCi/g: pCifg pCi!g pCt!g pCi!g pCi/g: pC1/g pCilg 4 00 pCilg KXB2 12102115 1114 1525757 3 10.0 pCi/g Time Prep Batch 1319 1521842 Batch ID Rcconry% Acceptable Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Sui1e 112 Bu!Talo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample TD:
- 3. l. l 4.R.1 Sample ID:
385070005 Certificate of Analysis Report Date: December 17. 2015 Project: MJWCOO 115 Client ID: MJWCOO I l'a~'.'!11~.t~.r.... ***-.......... guaH!icr.
- Result Snccrt:iinty
- \\-JDC Le TPC RL Uuit~ OF Analvst Date Time Batch Mttl.
...... *--****-* ****-- *- ******--* **---****-- ******-***....... -.. *-*-****........ -*........... ~-*....... ~....... -**... -**........ Surrogateffracer Recovery Test Batch JD RcCnl'cry% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 - www.gel.com Certificate of Analysis Company; Address: MJW Technical Service~ l5 Hazelwood Drive Suite 112 Buffalo, New Yorl< 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.14.R.2 Sample ID: 389296010 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 19.4% Paraniet~r................ qu_a_li~cr..... ~e.sul!.... r11.i!~r~:Ji!!ll' Gravinietric Solids ASTM D 2216 % Jfoisture "As Recefred" Moisture 19.4 Rad Gamma S1icc Analysis Gamma wit/: lngrowrh Dry Weigfll Corr~c:ted" Actmium-227 u -0 172 . +/-0 211 Antimony-125 LT ll 0178
- r/-0.0897 Aismulh-212 UJ 0 00
+/-0.621 Bismuth-214 O.S69 +/-0.144 Cesium-137 1 27 +/-Q.0964 Cobalt-60 u () 110241 +/-0 030 Europium-154 u .() ()386 +f-0.0904 Le~d-212 0.794 +/-0.!04 Lead-214 0.915 +/-0 142 Potassmm-40 11.9 +1-1 17 Protactmium-231 u 0.342 +l-0 443 Radium-226 0869 .,./-0.144 Radium-228 1.02 +l-0 11!0
- niallium-208 0203
+l-0 Oo5l Tin-126 lJ I 000 +/-0 lJ84 Gammaspec. Gamma. Solid "Dry Weight Correcred" Actinium-227 ll -0(}627 +/-0 280 Antimony-125 lJ -00142 +/-0 117 Bismuth-212 1.77 f /.(1 7()0 Bismuth-214 0144 +/-U 173 Ccsium-137 137 +/-0 141 Cobalt-60 ll ll.0227 -t-/*ll 0403 Europium-154 u -00087 +/-0 139 l.ead-212 () 942 +l-0 158 Le~d-214 0 764 +l-0 187 Potassiwn-40 II 4 +/-] 41, Prolactinium-23 I U! ()00 +/-0.706 Radmm-226 (1.744 +/-0 173 Radmm-228 0.952 +/-0 265 Thilllimn-208 0.100 +/-0.079 Tin-126 UI 000 +/.() 0993 Rad Gas Flow Proportional Counting GFPC Gross A:B. solid "Dry Weigh/ C'on*ected" Alpha 9 16 +/.J 18 Bela 19 6 ..-/-2 47 .. MQ~ -----* -'~<<:'. (I 3(J5 0 174 0.160 IJ.1)759 0 063 0.305 0.104 () 0486 O.U564 00263 0 0568 0.0254 0.160 00719 0 0986 0.0475 () 234 0114 ll.428 0185 () 775 0.370 0 1Cl4 00486 0 172 0.0779 0 0563 ().0264 () 126 0061 0.518 0.242 0.213 00982 () 864 0.379 0 129 0.0576 0.0746 0.0335 0 OBS6 0.038! 0269 0.118 (j_m 0.0574 0 148 0 0681 0.591 0234 0 953 0.443 0129 (1.0576 \\1258 0.112 0 0639 0.0285 0.175 () 0841 3 99 I 75 2.2t/ 1.06 Project: Client lD: .TPr Report Date: MJ\\VCOOl 15 MJWCOOl February lO, 2016 ~!,:..... l'.uits.. _DF_ An:1lys~.. _ D:i.te.. Tim_e_ B,a~~~----~*1. td: perccnl CXCI 01114116 120g 15373!2 +/.(l.226 pC,/g RXF2 ()2I05fl6 0842 1537546 2 +1-0 0901 pC1lg +/.l) 643 pCi/g +/.():161 pCilg +/-!l.140 0 100 pCilg +/.() (}30 pC!lg +/-0.0921 pC1/g +/.{) 121 pC1/g +/.() 159 pCi/g +/*l.60 pC'ilg +1-Q 475* pCilg +i-0 161 pCi/g +/-0.228 pCl/g +/-00672 pC'ilg +/.{) 0858 pC'ilg +/-0.282 pC1fg RXF2 Ol/181115 112*1 1537.545 3 +/-0 117 pC1/g +t-0 781 pC1/g +/.() 184 pC1/g +i-0.180 0 100 pC1lg +/.(I 0417 pCi/g +1-ll 140 pCifg +/-1) 179 pCi!& +/-0.198. pCilg +I-I 77 pC!lg +/-ll 720 pC1/g +/-fl 184 pCi.lg +/-0 302 pCilg +/.() 0&01 pC1lg +/.() 112 pC1'g +/-3.62 4 00 pCi/g. KX02 ()1126/t(i 1155 1539462 4 +/-3 70 100 pC1/g
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8.171 -www.gel.com Company: Address:
Contact:
MJ\\1.' Technical Services 15 Hazelwood Drive Suite ll2 Buffalo, New York !4228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.14.R.2 Sample ID: 389296010 Certificate of Analysis Report Date: February !O, 2016 Project: MJWCOOl 15 Client ID: MJWCOO I .P.~.r~.~e.tc.r.......... -. -. -- - g~~l~.fie.i:._ -**. __ l_~~s11_*1..... -r ~.~~f_tain~y. !.l.11~.folln~Jng_ P!,t:.P..~'!Cthl)d_S. \\~e~I:.r.crfor.m.ctl..
- \\fothlld Description Dry Soil Prep Dry Soil Prep GL-RAD*A-021
'f.hcJoll~w.i11g. Ana..fY.t.i.cal M.cthutls.~\\'.c.i.-11*ptrfo~*nied...
- Vkilwd Description 2
3 4 ASTM D2216(Motli!lcd) oot HASL 300. *l.5 2 3/Ga-01-R DOE HASL 300, 4.5 2.3iGa-01-R EPA 900 OISW846 931 OISM 71 lOB Modified Surrogakffracer Recovery Test Notes: Analyst CXCI Date Time Prep B:itch 01114/lf> 1208 1537312 Balch lD Rcccwcr)'% Acceptable Limits TPU and Counting Unce11ainly are calculated at the 95% confidence level ( J. 96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of AnaJysis Report Date: December 4, 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York t4228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.15.R.l Sample ID: 3&5070006 Matrix: Soil Collect Date: 21-0CT-15 14:40 Receive Date: OS~NOV-15 Collector: Cl.ient Moisture: 21.9% Parameter Qualifier Gravimetric Solids ASTM D 2216 % Moisture "As Received" Europlllm-154
- Protactinium-23 I Radium-226 Radium-228 u
u u UI Tin-126 U Rad Gas Flow Proportional Counting 21.9
- 0. 121 I 28 00155 0 00314 0,00 0932 01)06 0.0586 GFPC, Gross A/B. solid "Dry Weight Corrected"
~pha 13 I Beta 21 7 +/-0.151 +/-0.914 +/-0.230 +J-0 363 +J-0. 189 +1-3 19 +1-2.71 !!1.e.:f?.l.lo~*i~~-~.r~pJvfeth(JdS -""~E~ p~_rf.or.1n_e<l.:...................... Method Description o~: *s*oj1 rrcp**** * **..,... * * ****-** - **nr}~son--*Prep *01~-RAD~)\\-Oz"f * * *** **-* * * ~he ~?l_l_C?.:~i_n?. A11~l:yti~_a.l __ fl.J~t.h?.d_5..Y'c.reye.r.f.?.li1.1ed:_... ~-~-t!.~C?Q....... _ J?~sc.r.ip\\i.QJ1.................. ASTM D 2216 (Modifi~d) 2 DOE HASL 300, 4 5 2.3iGa-Ol-R 3 EPA 9000ISW846 9310/SM 71 IOB Modified MDC RL 0.605 0.246 00961 0 100 "(I 099& 0 291 1 23 0.190 0.340 0 238 3 76 4 00 3 36 10.0 Project: Client !D: percent pCi!g pCi/g pC1/g pC1!g pCrlg pC1/g pC1fg pCilg pCi!g pCi!g pCiig MJWCOOI !5 MJWCOOl CXCI 11/1011:5 1319 1521842 RXF2 12iOJ/15 1303 1522383 KXB2 12i02/l5 1116 !525757 Analyst Dale Time Prep Batch
- *.. c:,*xci...........
- 1"iith1i5- *****..... *1:119** *..... 15:.frs4i.... *-..... * -
................ A!J.a.1.Yst C (}llJAl~!ltS. Notes: Counting Uncertainty is calculated at'the 95% confidence level ( 1.96-sigma). 2 3
Company: Address: GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com MJW Corporation 15 Hazelwood Drive Suite l !2 Certificate of Analysis Buffalo, New York 14228 Report Date: December 17. 2015
Contact:
Ms. Laurie Losey Project: Soil RadioisoLopes Client Sample ID: 3.1.15.R.I Sample ID: 385070006 Matrix: Soil Colfect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 21.9% .P.~E~!11_et~r.... *-... -*...9~~1.i~er..... ~c_s!t_l_l_.. -* (11c4:!.l'.lll..i~.. lv Gra\\'imetric Solids ASTM D 2116 % !idoiswre "As Received" Moisture 21 9 Rad Gamnia Spec Analysis Gammaspec, Gamma. Solid "D1j* Weight Corn~cled" Actmium-227. U -0 178 +-1-0 348 Anumony-l 25 UI 0 00 +/-0.202 Bismuth-212 UI 0.00 +/-1 ll B1smuth*214 (J.932 +/-0 230 Cesium-137 I 28 +/*ll 158 Cobalt-60 U 0 0155 +/-0.0487 Europmm-I 54 U 0 00314 +/-0 151 Lead-212 1 10 +/-0.154 lead-214 1.16 +/-0.224 Potassium-40 15.0 +/-1.69 l'rolactm1um-23 l Radium-226 Rmlium-228 Thallium-208 l1l (I{){) !l.932 0 906 0 295 Tin-126 U 0 058(i Rae.I Gas Flow PrQporticmal Counting GFPC. Gross AB. solid "Dry lf'eight Corrected'.' Alpha 13.1 Beta 21 7 +/-0.914 +/-0 230 +i-0 363 +/.() 0794 +!-0 189 +/-3 19 +/-2.71 Th..I! ~oll.~wi1_1g_!'.r_ep ~lctho,~s.'\\'l'..Z:c.. pcrfor111.~~-....................... Method Description Dry Soil Prep Dty Soil Prep GL*RAD-A-021 MDC 0 ()05 0246 I 55 (J 190 00961 \\J.0998 () 29\\ n 144 0.17] IJ 731 1.23 0.190 0 340 0 0849 () 238 3.76 3 36 ~r_!J_e fol_l?.'Yi'!~ An_~ly_l_ic~~ J_\\'~j!t~IJdS '.".e.~e r.i:r~'or~.e~.................... _........ Method Description J 2 3 ASTM D 2116 (Modtricd) bOE HASL 300. 4.5.2.3/Ga-O\\-R EPA 900 OiSW846 9310iSM 71 IOB Modified Le t\\283 0.114 071!! 1)(1877 0.043R 0.0431 0.127 00681 00798 () 297 ll.574 U.O!S77 0.152 00385 0 114 l.70 1.62 Analyst CXCI Project: Client ID: MJWCOOl 15 MJWCOOJ percent CXCI +/-0.358 pC1/g RXF2 +/-0.210 pCi/g +1-125 pC1/g +/-0 243 pCi/g .,./-0.192 0 !00 pC1/g +/.(! 0492 pCt/g +/-0.151 pC1/g +/-0.181 pC1lg +1*0245 pC1/g +/-2.12 pC1tg +/-0.')72 pC1/g +/-0.243 pCt!g +/.() 387 pCilg +l-0 ()834 pCtlg +l-0.190 pCi/g +/-4 06 400 pCi/g KXB2 +/-404 10.0 pCi/g Date Time Prep Batch 11/10!15 1319 1521842 \\ 1110!\\5 1319 1521842 12i03!15 1303 1522383 12i02115 1116 1525757 2 3 Su nogateffraccr Recovery Tcsl Batch lD RccO\\'crr% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - 1Nwv1.gel.com Company: Address:
Contact:
MJW Corporation 15 Hazelwood Drive Suite l 12 Buffalo. New York 14228 Ms. Laurie Losey Project; Soil Radioisotopes Client Sample ID: 3.1. 15.R. r Sample ID: 385070006 Pnr.am.~~~r........................ Q.u_a~if1cr...... !lesull Surrogutcffracer Recovery Test Notes: Certificate of Analysis Report Date: l)ecember 17. 2015 Project: MJWCOOI15 Client ID: .MJWCOO I _l)1m.~a.i.nt~:.... ~ID<;......Ice........ __. WL......... __ Rf: __ X1_1i_t_~ __ ~F ;\\11a~ys_~.... Da~e. Ti.l?.e -~:ttc_l1 __ !VI.t~.-. Batch ID Recovery% Acceptable Limits TPU and Counting Uncertainty are calculated at 1he 95% confidence level ( 1.96-sigirta).
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Corporation l 5 Huzeh,*ood Drive Suite 112 Bu/Talo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.15.R. I Sample 10: 385070006 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 21.9% Paran1eter Grnvimetric Soliils A STM D 2216 % Mois111re "As Recefred" Mornture 21 9 Rad Gamma Spec Analysis Certificate of Analysis l'ncerlaintv MlJC Le Gammaspec, Gamma. Solid "Dry Weight ('orrecl;~d Report Date: December 17. 2015 Project: MJWCOOl 15 Client ID: MJWCOO! percent CXC"l 11/Hl/15 1319 !521842 i\\ctimum-227 U -0 178 +/-0 34S. 0 605 0.283 +/.0.358 pC1/g RXF2 12103115 1303 1522383 2 i\\ntimony-125 UI 0.00 +1-ll 202 Blsmuth-2!2 lll () 00 +/-1 l l Basnrnth-214 Ccsiurn-13 7 Cabalt-60 Europium-l 54 Lcad-212 Lcad-214 Pota.~ium-40 Protactimum-231 Radmm-226 Radmm-228. Thallium-208 u u Lil Tin-126 ll Rad Gns l'low Proportional Counting 0.932 l 28 0 0155 0.003 \\4 1.10. 1.16 IS.0 000 0.932 0.906 0.195 0.05&6 c;FPC, Gross A/B. solid "D1:1' Weig/if Corrected"* Alpha 13.1 Bela 21 7 +/-0.230 +J-0 l5S +/-0 0487 +l-0 15! +/-0 154 +/-0 224 +J-1 69 +/-0914 +/-0.230 <*/-0.363 .,./-0.(l794 +!-0 189 +/-3 l9 +/-2.71 0.246 155 0 190 00961 00998 () 291 0 144 [) 173 0 731 123 0.190 0340 O.OS49 023~ 3 76 3 36 lJ11'...~l!l.~c.1wi11g r,rep :vl_e~h.~.~~.ll*~i:eJi.ci:-1:0.".1.11~.~.......... '*** ".................
- \\1ctt1od Descri11tion Dry Soil Prep Dry Sad Prep GL-RAD-A-021
!_li_e.~(111()"'.i.~.g.'\\n.?!Y.tii:.a..1. ~.l~~~Y.~S.. 'v.er.e J>_er.f.oi_:11:1e~. ~lcthod Description ASTM D 2216 (Modifo:d) 2 DOE HASL 300. 4 5 2. 3/Gn-0 l -R 3 EPA 9GO.O/SW846 93 JO!SM 71 IOB Modified Surrogatefl'racer Recovery Test 0.114 +/-0 210 pCi/g 0 71S +/-! 2~ pC1/g 0 0877 +/-0.243 pC1lg 0 0438 +/-0 192 0.100 pC1/g 0.0431 +/.!) 0492 pC1/g 0.127 +1-0.1 s l pC1/g 00681 +J-0 lSI pCr/g 00798 +(-0 245 pC1/g () 297 +l-2 12 pCi/g 0..574 +f-0.'>72 pCi.lg 0.0877 +f-0.243 pC1/g 0 152 +/-0.387 pC1/g 0 03S5 +/-0.0834 pCi!g () 114 +/-0*190 pCilg 1.70 +/-4.06 4.00 p('rlg KXB2 12i02fl5 1116 1525757 3 l 62 +1-4.04 100 pCi/g Analyst Date Time Prell Batch CXCl 11110115 1319 1521842 Batch 10 Recovery% Acceptuble Limits
GEL LAB.ORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171
- w.vw.gel.com Company:
Address:
Contact:
Project: MJW Corporation 15 Hazelwood Drh*c Suile 112 Buffalo, New York 14228 Ms. Laurie Losey Soil Radioisotopes Client Sample ID: 3.1.15.R. I Sample ID: 385070006 Notes: Certificate of Analysis Reporl Date: December 17.2015 Project: MJWCOOl 15 Client ID: MJWCOOI . ~*\\:....... __ Tl'.L. ***--. }_~!,.... _l~_11_it~.. -~F. An:i_ly~t... J?.a.~e. :r_-~1.ne__ -~:J~.<:l_i_.. ~ltd,=. Batch H) Reco\\*ery% Acceptable Limits TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigrna).
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843} 556-8'\\71 - www.gel.com Company: Address:* MJW Technical Ser.-ices 15 Ha:telwood Drive Suite 112 Buffalo, New York 1422.8
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample m:
- 3. !.15.R.2 Sample ID:
389296011 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 22.1% . ~~rarn_et~r. _ ****-**.. _... _ q1~.~li.fi.c.r. Gravimetric Solids ,-lSTJf D 2216 % Moi.~ture "As Received" M(nsturc 22.1 Rad Gamma Spec An;1lysis Gwnma with lngrowlh "Dry Weight Corrected" A~tmium-227 u -0.053 Anlimony-125 ll 00738 Bismuth-212 2.07 Bismuth-214 0.833 Cesium-137 1.72 Cob.alt-60 lJ O.U252 Europmm-154 u -U.024 Lead-212 1.18 Lcad-214 I 2(! Po1ass1um-40 15 3 Prota~lmmm-231 UI 0.00 Radium-226 0 &33 Radmm-228 I 14 Tlmllium-208 0 J87 Tm-126 Lil 0.00 Certificate of Analysis .Il~.t:. +/-1) 283 lJ 489 0 231 +1-0 284 +/-0.121 0.231 () ]()9 +/-0.126 +/-0.966 0 966 0.435 +t-0.985 +lo 116 () 143 0.0655 -~/-U 189 +/-0 140 009[) 00411> +1-<i 196 +/-0.0471 0 0908 00396 +1-0 0485 +/-0.150 0.244 0.!06 +/-0.150 -r/-0 129 0.118 O.ll563 +f-0 162 ...,.() 185 0.33& 0 164 +1-ll 212 +/-1 71 IJ 730 () 308 +l-2 16 +/-0996 () 9117 0427 +/-1.09 +/-() \\7() 0 143 0.0655 +/-() 189 +/.() 287 0282 0.126 +f-0 318 +/-0.080 0.0742 0.034 +/-0.0862 0l12 () 124 () 0595 +/.O.l 14 Gammaspec, Gamma. Solid "Dry Weight Corrected" Actmium-227 lJ -00408 +/-0 357 () 663 0.310 +1-0 353 Ant11110ny-125 u 0.0275 +/-0.152 0 281 0 !3lJ +/-0 152 Bismulh-212 Ul 0.00 "-/-0.857 I 67 0773 +/-I 16 Bismulh-214 o s2g +/-01% O.lbO OlJ7\\7 +/-0.210 Cesium-137 1.68 +/.().183 .() 1()8 [I 0493 +l-0 23~ Cobalt-60 u 0 00658 +/-0.055! 0.111 00479 +f-0 0552 r::uroprnm-154 v 0.0103 +/-0.135 0.275 0 117 +/-0.135 Lead-212 120 +/.().151 (I 147 0.069\\ '+/-0. \\85 Lead-214 0 944 <*/-0.267 0204 0.[)948 +/-0 279 Potass i um-40 13 3 +l-1.65 () 617 () 234 +1-2.!JI) Protacumum-23.\\ lJI 0.00 +/-0 8&8 1.54 0727 +-1-1.0(> Radium-226 0.818 +/-0.196 O.lfiO 0.0717 +/-0.2!0
- Radmm-228 I U7
+/-0 376 {) 377 () 168 +/-0 405 Timllmm-208 0.301 +/.()0966 0 0881 0.(139R +/-0.100 Tm-126 UI 000 +/-0 188 ().2iJ2 U U91i ... /-0.189 Rad Gas Flow Proportional Counting GFPC. Grass A:S. solid "Dry JVeight Con*ected" Alpha 18 s
- l-4 07 3.95 1.72.
+/-5 49 Beta 23 7 +/-2 89 282 I 31 +1-4 5(> Rep.or! Dute: Pcqruary I 0, 2016 Project: Client ID: MJWC'OOl 15 MJWCOOI percent CXCl 01114116 1208 1537312 pC1!g RXF2 02105116 0842 1537546 2 pCi/g pC1/g pCi/g 0.100 pCi/g pC!lg pCi/g pCi/g pC!lg pC'1/g pCi/g pC1/g pCilg pCilg pCi/g pC1!g RXF2 01/18!16 1122 1537.545 3 pC1!g pCi!g pC1/g 0.100 pCi!g pCi/g pC!lg pCt/g pC1lg pC1ig p('t1£. pCt/g pCiJg pC1/g pC1/g 4.(1() pC1/g KXB2 Ol/26116 1152 1539462 4 100 pCi/g
Company:. Address: GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com MJW Technical Scrvkcs 15 Hazelwood Drive Suite 112 Certificate of Analysis Buffalo. New York 14228 Report Date: February 10. 2016
Contact:
Ms. Laurie Losey Project: Soil Rndioisotop(!s Client Sample ID: 3.1.15.R.2 Sample ID: 389296011 Parameter The.fo.ll~."'}.ng_f.'r.cJ!.~1.e.~ho<!~~-e.i:~.J!l:~fl)_r~ne~. Method Description Dry Soil Prep Cncert~intv Th.c. r.011~,'t.i.ng,\\~a..1yti~<:1l_i\\-f.e.1110..d.~ ~\\*.e.re. p~rf1n::n1.e~...
- \\*le thud Description 4
.ASTM D 2216 I Modifa:d) DOE HASL300.4.5 2.3/Ga-01-R DOI:: HASL 300. 4 5 2 3/Ga-01-R EPA 900.0iSW846 93 !Q.1SM 71 I013 Modified Surrogatcffracer Recovery Test Notes: Project: MJWC'OO ll5 Client JD: MJWCOOl Le TPl' Time C'XC' I Ol/14116 1208 Prep Batch 1537312 Dnte Time B:itch Mtd. Batch ID Recovery% Acceptable Limits TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843).556-8171 -www.gel.com Certificate of Analysis Rep011 Date: December 4, 2015 Company: Address:
Contact:
Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Moisture: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 1422& Ms. Laurie Losey Soil Radioisotopes 3.1.16.R.I 385070007 Soil 21-0CT-15 14:10 05-NOV-15 Client 18.1% Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Mmsturc 18.! Rad Gamma Spec.Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 U -0 0964 +i-0 260 Antimony-125 U -0.0282 -t/-0 112 Ccsium-137 I 75 +/-0 161 Cobalt-60 ll 0.0436 +/-0.0414 Europium-154 Protaclinmn1*23 I Radiwn-226 R.adiw11-228 u lJ Tm*126 U Rad Gas Flow Proportional Counting -0 0232 0 306 0 682 0.716 () 0837 GFPC. Gross AfB, solid "Dry Weight Corrce<ted" Alpha* 14-7 Beta 21-7 +1-0 114 -t-/-0558 +1-0167 +1-0.295 +1*0 143 +1-3 55 +/-2.59 0 494 0206 00756 00968 n.19! 1.12 0 139 0.279 0 193 3.9S 2.91 ll 100 4.00 100 Pmject Client JD: percent pC1/g pCi/J;? pCi/g pCi!g pC1/g: pCilg pCi/g pC1/g pC1rg Ih.~ fo.l!()~V.i.n~.P:~~P ~',~et.~?~s_ ~_ere_r.erforin~d.:_ ***--* __..... _ -* MJWCOOll5
- ...-uwcoo1 CXCl l l/10115
\\319 1521842 RXF2 12/03/1; 1303 I 522383 KXB2 12!02il5 1116 1525757 Method Description Analyst Date Time or;;*s-c;,Trre.i>>.... ****-* * * **.. * ***5iY*s1i11 fiiei> dC:R'AB~;\\:-02t * - *- *****- * **** ***** * *** ** -*txc1* -* *... * * -fihohs* -
- f:fr9 *
- Prep Batch 1521842 Th~. f~l~()~Y.i~¥_~~-~Ixti~a:1_ ~~~?.ds_\\v.er-~ P.~~o.r1ned_:..........................
_rv1~~h.P.~. _....... ********-.... _ _pe~c:r~.P.tion........................ . -*...A.!1-~h'1>.t(Qf.\\lll)_~n.~s.. _ ASTM D 22!6 (Modified) 2 DOE HASL 300. 4.5.2 3/Ga-Ol-R 3 EPA 900 0 1SW846 9310/SM 71 IOB Modified Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma). 2 3}}