ML16294A195
Text
{{#Wiki_filter:*> Appendix G-Sub-Area 3.1.11- 3.1.15- COA
GEL LABORATORIES LLC 204D Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company : MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.11.E. l Project: MJW(OO! 15 Sample lD: 385070002 Client ID: MJWCOOI Matrix: Soil Collect Date: 21-0CT~ 15 13:35 Receive Date: 05-NOV-15 Collector: Client Moisture: 22.8'% Parameter Result Uncertainty MDC RL Units Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moi~ture 22 8 percent CXCl 11110'15 1319 1521842 Racl Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Actimum-227 ll 0 l67 +/-0.254 (J 482 pC1/g RXF2 \2/03/15 0846 1522383 2 A11t1mo11y- l 25 u 0.053 l ..-/.().104 0 llJ7 pC1lg Cesium-137 0 984 +l-0 0988 ll 0738 0100 pCrlg Colw.lt-60 ll -0.0236 +l-0 0349 0060 pCi!g Europium-154* u 0.l45 +/-0.JJI () 255 pCi!g Prota~Lin:tum-23 l u 0.476 +/-0.571 0 840 pCilg Radmm-226 0946 +/-0 149 0123 pCi!g Radium-228 l.23 +f-0.325 0 26(> pCi/g Tin-126 U! 000 +/.() 126 0.135 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross A!B. solid "Dry Weight CotTected" Alpha \3.S ..1..3 32 J 46 4.00 p('1/g KXB2 12i02/15 1112 1525757 3 lkta 21 0 *+2 81 3.25 10.U pCi/g
}'~e .f.~11.l:J~i.~~. :P!.epJ-:1.~~~~~~.*v~r~ .P.".f.f(ll_11~~~: ................. . *******-**-*** ******-*
Melhod Descriptfon Analyst Date Time Prep Batch oiy* s*c;i1 rrer... . . . .. .. .. .. * ... or;*sc;1rr*icil cir:.~1~,;;:o:A:-02 i . *.
- cxC:;i* . * .... * *-i'iiioiis ..i3f9 ... **-*i52i 842'" ............ - *- *******-**-**-
T.~.e .f.o.1.19"".i.n!?..0n.alr.ti.c~! M.~Uto?s_ ."\:~r~ ~e~f.o.rt1l~~'. ... _ M~tho.g ...... ... . . . ....... .J=?!':~~r.iptjqn .. .. .. .. . .. . . .. . . . .. ......... ,. .. . . .. . . . .. .AiJ.?..LY~LC9-.lillT!f.ltl_tS. ... _.
/ISTM D 2216 (Modified) 2 DOE HASL 300. 4.523fGa-O1-R 3 Ef'A 900.0ISW846 93!01SM 71 IOB Modified Notes:
Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma}.
GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Orive Suite 112 Buffalo, New York 14228 Report Date; December 17, 2015
Contact:
Ms. Laurie Lose} Project: Soil Radioisotopes Client Sample ID: 3. l.11.E.1 Project: MJWCOOl 15 Sample ID: 385070002 Client ID: MJ\\/COOI Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV- l 5 Collector: Client. Moisture: 22.8% Parameter MDC Le TPL' RL Date Time Batch Mtd. Gravimetric Solids 1IST:'vl D 22 l 6 % llois1ure "As Received" Moi~turc 22 8 p~rccnt CXCI 111!0/15 1319 \521842 Rad Gamma Spc~ Allalysis Gammaspec, Gamma. Solid "Di:v Weigl1t Cor1*ected" Actmrnm-227 U 0.167 +/-0 254 0.41>2 0 228 +/-0.266 pC1lg RXF2 l2i03 115 0846 1522383 2 Antimony-125 U 0.0531 +/-Q.104 () !97 00925 +J-0 107 pC1/g Ilisnmth-212 1.53 +/-0.832 0 628 {) 279 +1-0.847 pC1/g Bismuth-214 0 946 +(-0 149 iJ. 123 (}057 +/.0.168 pCilg Cesmm-137 0. 984 +/-0.0988 0 0738. 0.0343 +1-0.127 () 100 pC1lg Cobalt-60 u -0.0236 +l-0 0349 0.060 00261 +1-0.0J65 pCi/g .Europium-154 Ul 0 00 +/-0.13\ 0 255 0 l \7 +/-0 147 pCilg Lead-212 I 29 . <-/-0. \29 ()I 12 () 0531 +/-(} 165 pCilg Lcad-214 I 23 +/-0. \91 0 139 OOf>53 +/-0.216 pC1lg Potassium-40 16 5 +/-!.34 (1455 (l 189 4*/-1 9':".*~e~ .... ***-*.. ***-***** ************ ...
- .\'let hod Description ASTM 02216 (Modified) 2 DOE HASL 300, 4.52JiGa-O\-R J EPA 900 OiSWS46 9310/SM 71 IOB Modified Surrogatefrracer Recovery Test Batel! ID R~cover)'% Acceptable'.Limils
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.geLcom Certificate of Anal,ysis Company: MJW Corporation Address: 1.5 1-fazelwood Drive Suite I 12 Buffalo, New York 14228 *Report Date: December 17, 2015
Contact:
Ms. Laurie Losey Project: Soil Radioisoto:pc~ Client Sample 10: 3.1.11.E. l Project: MJWCOOl 15 Sample ID: 385070002 Client ID: MJWCOOl Parameter ....... -.... _......9.u.1tli.rii:r._ ***- .. ~~s.u.it ... ~;n~c;.J:tj!Jn.~ ....... :VIDC' Le ..... _JP_L ...~.L.. _l'ni~s DI' Anal}'s; Dat_c !i.l_lle .ll.~~4?~ ... ~~td. Surrogi1ti!ffracer Reco,*ery Test Batch lD l<cco\*cry% Acceptable Limits Nutes: TPU and Counting Uncertainty are calculated at t11e 95% confidence level ( 1.96-sigma}.
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 l!azelwood Drive Suite 112 Buffalo, New York 14228 Report Date: Dcccmber*l7, 2015
Contact:
Ms. Laurie Losey Project: So.ii Radioisotopes Client Sample ID; 3.1.l l.E.1 Project: MJWCOOl 15 Sample JD: 3&5070002 Client ID: MJWCODI Matrix: Soil Collect Date: 21-0CT- I 5 Receive Date: 05-NOV-!5 Collector: Client Moisture: 22.8% .l'a.r.~.rr_i.eter_ . . ...........9~.'.'!i_fic~~-- Res11I~ ...... r.o.c.cr.!ai.~.t~* ......... i\'IDC Le TPt: -*** Gravimetric Solids ASTM D 22 J6 *% A-Jois111re "As Received" Moisture 22. 8 pcrccm CXCI 1l/lllll5 1319 1521842 Rad Gamma Spcc Analysis Gammaspec, Gamma, Sa/id "D1:;* Weigfu Corrected Actinrnm-227 U 0.167 +/-0.254 0.48~ \) 228 ~/-0.266 pCi!g RXF2 12103115 (l84ri* 1522383 2 Antimony-125 U 0.0531 +/-0 104 O.l97 0:0925 +/-D.107 pCl/g Bismuth-212 I.SJ +/-0.832 0628. 0 279 +/.() 847 pCilg B15mulh-214 0 946 +/-0.149 0 123 0057 +/-0.168 pC1tg 0!$1Um-!J7 0.984 +/-0 0988 0.0738 00343 +/-0.127 0 100 pCi/g Cobalt-60 U -0.0236 +/-0.0349 0 060 00261 +/.() 0365 pClfg Europium-154 l)I 000 +/-0131 0.255 0l17 +/-0 147 pC1/g Lead-212 1 Z9 -t-/-0 129 0. 112 0 0531 +/*0.166 pCi/g Lcad-214 1 2J +/-0 191 0.139 1).0653 +1-0216 pCilg Potassium-40 16 5 +!-I 34 () 455 0 189 +/-1.96 pCi/g Protactinium-231 !JI (] 00 +/-0.572 !1840 0.394 +f-0 582 pCi/g Rildium-226 0.946 +l-0 149 0123 0 057 +1-0 108 pCi!g. R~dium-228 1 23 +/-0.315 0 266 () 122 */-0.381 pC1/g Thall ium-208 0.364 +/-0 0786 00624 0 02&8 +/-1) 0843 pC1ig Tm-126 U! 000 +/-0 126 0.135 ow~4 +/-0 128 pC1lg Rad Gas Fiuw Proportional Counting GFPC Gross A.B, solid "D1:J' Weight.Corrected" Alpha 13.8 +/-3.32 1.51 +/-4 33 4 00 pCiig KXB2 12102115 1112 1525757 3 Beta 21.0 +/-2 81 3.2:5 1 54 +/-4 09 HJ 0 pC1/g I.h..e. foll.~~~ng P.i:ep !\_:f~t~1~~s- n:~re pcrfo_r~~~- ...... . Met bod Description Analrst Date Time Prep Batch DI)* Soil Prep Dr;.* Soil Prep GL-RAD-A-021 CXCI l 1110/15 1319 1521842 The following Analytical Methods were performed
~i~ii;~;i * * **- ***--o~;;~.**ipii~~ ****--** * *--* **** * ** *** * *
- ASTM D 2216 (Modified)
DOE I IASL 300. 4 S.2 3/Ga-01-R 3 EPA 9000'SW846 9310/SM 71 IOB Modified Surrogate/Tr~lccr Rceo~*ery Test Batch ID Rt>eovery% Acceptable Limits
GEL LA BORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate. of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo. New York 1422& Report Date: December 17. 2015
Contact:
Ms. Laurie Losey Project: Soi! Radioisotopes Client Sample ID: 3.1.11.E. I Project: MJWCOO I 15 Sample ID: 385070002 Client ID: MJWCODI P:i 1:n.TI1 etc r . . .. . .. _. .. ____ 9.IJ_;i_li_li~.r- _-* .. _.~es~_l_t .. l'n~~rla_ifll.Y ....... _i\I~~~ ...... Le ........... 1~!.'!' .........R.-.J,... l!nit~ DF .A.n:1Iy_s~... _.))i1ti;. T.i.llle B_atcl1 Mtd. Surrogatcfl'raccr Recovery Test Batch ID Rccorcry% Acceptable Limils Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level (l .96-sigma).
GELLABORATOruESLLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Technical Services Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Report Date: l'cbrual)* I 0, 2016 Contact Ms. Laurie Losey Project: Soi! Radioisotopes Client Sample ID: 3. l .1 I .E.2 Project: MJWC00115 Sample ID: 389296007 Client TD: MJWCOOl Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 22.&% -~~~a~1.e~~r............... 9u11)_i~~r .. Re_s!1_1t_ .... _l)!cert.~h1f\: .........J\:1.DC Le .. n.c ..... _RL. Y.11its DF.. A_1111lys.t. _Uat_c Frn.c.J3a_t~l1 .. :\ltd* Gravimetric Solids AST:\.! D 22 I6 % Moiswre "As Recei**ed" Moisture 22.8 perccnL CXC! 01114116 120S 1537312 Rad Gamma Spec Analysis Gamma with fngrowrft "D1:i* Weight C'on*ectc:d" Aotimurn-127 U -0.00461 +/.()JOU 0 5.60 0 263 +1-0.300 pC1/g RXF2 02i05/I& 0744 1537546 Antimony-125 lJ -01)71)9 +/-0.134 0.232 0 107 +/-0 138 pC1/g B1smutl1-2 I2 1 07 +/-0 710 I CIS 0472 t-l-ll 718 pC1/g Bi~muth-214 1.18 ...l-0 2UO ll 157 I) 07t4 +/-0.223 pCitg Cesium-137 I 35 .../.!J.136 0 0821 0.037! +/.() 174 0 \00 pC1/g Cobah-60 u ll.00937 +/-0 0501 0 ()994 0 043--1 +/.O 0503 pC1ig Europi111n-154 u O.CJS62 +/-0.145 0 3()1 (l 133 *+1.0 150 pC1!g Lcad-212
- I 25 +/-0 134 0.113 () 053 "-f-0216 pci;g Lead-214 I 17 +/-0 174 0 171 00798 +f-0 208 pC1/g Porassium-40 15 4 +/-1.72 0.931 0 404 +/-2 20 pCi/g Prornctinmm-231 LI! 000 +l-0 763 (1.960 0446 -t-/.fJ.787 pC"tlg Radmm-226 I 18 +/-0200 !) 157 0.0714 +/-0.223 pC1.lg Radium-228 1.23 +/-0.388 0266 0.116 +1-0.433 pCi/g Timll mrn-208 0.424 +l-0 0832 0.0755 (J 0342 +/-0.0906 pCr/g Tin-126 lll 0 00 +/.!l.0899 0.112 0.0537 .. /-0.0937 pCilg Gammaspec. Gamma. Sa/id Dry Weii?ht Correc1ed
Ac1mrnm*227 l! 0. 127 +/-0 443 0805 0 375 +/-0.447 p('1!g RXF2 01/l8/16 1004 1537545 Antimony-125 lJ -0.0984 *t-/-0 l6n 019! 0.131 +/-0.172 pCi/g llismuth-212 lJ 0 37\ +/.() 956 1 93 0 866 +l-0 971 pC1/g llismulh-214 IJ \!18 +/-0 235 U.220 0.0972 +/-0.246 pC1/g Ce~ium-137 144 +1-0.183 (1.115 ll 051.}3 +/-0.216 0.100 pCilg Cobalt-60 U -0 0486 +/-0.0489 00725 ()0239 +/-0.0537 pC1!g Europium-154 U -0.0346 +/-0. l 7.J. 0.349 u 141 +/-0.175 pCifg Lead-2 !2 I 41 <-/-0 181 0 163 0.0759 +/-0.21(1 pCi/g Lead-214 0.988 */-0.2;i0 0.221 ()JOO *'1-0.2(13 pCi/g Pota>sium-40 14 7 +/-2 43 l 42 (} 585 +/-2.74 pC1/g Protactinium-23 I 0.00 +l-l 16 I 20 11543 +/-1.20 pC1tg Radmm-226 0.918 +/-0.235 0220 () 0972 "'-l*0.246 pC1/g Radmm-228 1 78 +/-0 417 () 537 0.'..:36 -rf-0 469 pCilg
'rballium-20& 0 316 +l-0.121 0 11:5 [)051 +/-0 123 pC1/g Tin-126 \J 0 0695 +/-0.156 0 233 ll lll. .,./-0.157 pCtlg Rad Gas Flow Propo11ional Counting GFPC. Grass A;B, solid "D1:1' We/gJ11 Corrected" Alpha 12.4 -t-f-3 64 393 I 67 +/-4 37 4 Oil pC1/g KXB2 01126116 1 !50 1539462 4 BelD 23.l +l-3 .J.4 418 1.99 +1-4 78 lOll pCi/g
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Technical Services Address: 15 Hazelwood Drh*c Suite !12 Buffalo, New York l4228 Report Date: Fehrual)' I0, 20 l 6
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample l D: 3 .1.11.E.2 Project: l'vUWCOO I LS Sample JD: 389296007 Client ID: MJWCOO l Parameter !\IDC i,c ..... TP..l.'. ......... ~.L... _\n_its... 9.Y... :'.\naly_s1...... l>!1t~ T_ime .. IJ.atc~. ~*ltll_.
~rhc_f.ollo~\:i~g_Pre_p ~!~!~'.ld.~_\\:ei-e.11.crfor.mcd -* -** ..... ... *******-** ........ **************-** ..... .................. .
Method Dc~criplion Analyst Date Time Prep Batch Dry Soll Prep Dry Soil Prep GL-R.AD-A-021 CXCI 01114116 1208 1537312 Jl1c JO..l!.O..'l\'.i_l})J_r\'.'a.lyti_c~.1.'\'.lc_t~.n.~s.~\:C.re P£'.'.f()~Tl_l~.~ ..... '.\lcthml Description I ASTM D 2216 (Modified) 2 DOE l*IASL 300, 4 5 2 3!Ga-O I*R 3 DOE HASL 300, 4 5 2.3/Ga-01-R 4 EPA 'JOO OiSW846 9310/SM 71 IOB Modifkd Surrogateffraccr Recover)' Test Batch IIJ Recovery% Acceptable Limils Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite l 12 Buffalo. New York 14228
Contact:
.Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3. L.12.E.1 Project: MJWCOOJ 15 Sample ID: 385070003 Client ID: MJWCOO! Matrix: Soil Collect Date: 21-0CT-15 10:25 Receive Date: 05-NOV-15 Collector: Client Moisture: 22.6% Parameter.............. --*-* .......... *-** Qualifier Result
.... **-****Uncertainty MDC RL Units Gravimetric Solids ASTM D 2216 % Moisture As Received
Moisture 22 6 percent CXCI 11110/15 1319 1521842 Rad Gamma Spec Analysis .Gammaspec, Gamma, Solid "Dry Weight Corrected" Actimum-227 U iJ 0126 +/-0 297 0 53R pC1lg RXF2 !2i03/l5 0846 1522383 2 Antimony-125 lJ -0107 +/-0.111 0.189 pC1!g Ccs1um-l37 !OS +1-0 120 O.On6 0 lOO pCi/g Cobalt-60 u -0 0284 +l-0 [1415 0072 pC1/g Europitim-154 .u 0 0371 +1-0.134 0251 pC1/g Protuctinium-231 LI 0.666 +/-0.642 0.997 pCilg Radium-226 I 06 +/-0.187 0 145 pC1/g Rad1um-228 141 +!-0 282 0259 pC1/g Tm-126 . lll 0.00 +J-0 133 0.157 pC1/g Rad Gas Flow Proportional Counting GFPC', Gross A/B, solid "D!Y Weight Corrected" Alpha l6 3 +/-3 'JS 3.95 400 pCi!g KXB2 12102115 1112 1525757 3 Bm M4 +/-3.40 "01 100 pC1lg. T~~ foU.?~!11~ .~~-~P. .~1.~t~~d~ .\Ve.re perf.~r.rn_ed:_ ....... . Method Description Analyst Date Time Prep Batch or:;:*.sotfiir.eP _..... -* ****- . ... ****b"ry* S-Oii"Prep-*nL:RAD~~.(-t)2'1 *..... * ***cxc1 ** **** * ***** frfioTis - * * *f3*1**i ...1.5}t"842" ..... *-*. ***-** -*-* ..
. The. .f.ol!o\'>' l.~¥-~~.1.a.l)~ic~l.. 1\1.~t~~~-s.v.-.e.r~y~rr.~~lll.e.d:.............................. .
J'y1~th~9 .. -**** . ... .. ... .. , . J;?_e_~cript.(CJ.n .... .... . .................... I ASTM D 2216 (Modtficd} 2 DOF. HASL 300, 4 5 2.3/Ga-Ol-R 3
- EPA 900.0iSW846 9JIOISM 71 lOB Modified Notes:*
Counting Uncertainty is calculated at the 95% confidence level ( l.96-sigma).
GELLABORATOruESLLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gef.com Certificate of Analysis Company: MJ\V Corporation Address: 15 Hazelwood Drin! Suite 112 Buffalo. New York 14228 Rcpo11 Oate: December 17, 2015
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.l.12.E.1 Project: MJWCOOl 15 Samp[e ID: 385070003 Client ID: MJWCOOl Matrix: Soil Collect Date: 2 l-OCT-15 Receive Date: OS*NOV-15 Collector: Client Moist11re: 22.6% Parameter . . . ...... ... . Q.u~~-ifi~1:. Result J:n.cl!r:tainty ... )\.1D( Le ... Et: ..... RL .... ~'ni!S_. P..F.. :~11.~l~*st___[)JjtC !im.~ _B_a!~h .. ~l.t~. Gravimetric Solids ASTM D 2216 % .\.foi:slm'e "As Rec<?ived" Moisture 22 6 percent CXCJ 1l/10/1.5 Bl l) 1521842 Rad Gamma Spec Anal)'Sis Gammaspec, Gamma, Solid "D1:v 11-"<!iglll Corr<?Cll!d" Act!mum-227 ll 0.0126 +1-0297 {) 538 0.256 +/-0 297 pC1/g R..'i:F2 12103/\ 5 0846 1522383 2 Antimony-125 u -0 IU7 +/-0 111 0 189 0 0889 +/-0 \21 pCt/g Bismlllh-212 UI 000 +/-0 968 1 27 () 598 +/.J 17 pC1!g Bismuth-214 I 06 +1-0.187 () 145 0.0678 +/-0 208 pC1/g Ccsiwn-137 1.05 +/-0 120 0.0736 110342 +/-0.151 O.IOO pCi/g Coball-60 u -0 0284 ..,.() 0415 0()72 (1.0321 -.-/-0.0435 pCi!g Europium-154 u 0.0371 +i-0 134 0.251 0.115 +l-0.135 pC1!g l.ead-212 !..35 H-0 140 0 l \7 (I 0559 +/-0.175 pC1/g L~ad-214 14(} +/.O 182 0 329 0.161 +/-0.212 pCJ/g Polassmm-40 \8 3 +/-1.45 0.h80 li.3()2 +/-2 IJ pCi/g Protuctimum-231 Ul 0.00 +/-0.642 0 997 0474 +/-0 ()59 pCifg Radrnm-226 1.06 +/-0 187 0 145 lJ.0678 +i-0 ..208 pC1lg Radium-228 1.41 +/.Q 282 ll.259 0.119 +/-0.319 pC1tg Thalliurn-208 0.407 ... /.().07\ () 0677 (Ul3!.5 +/-O.ll791 pCi/g Tm-126 Ul 0.00 ..-/-0.133 0 1.57 00756 t/.(J 135 pC1lg Rad Gas Flow Propol'tional Counting GFPC. Gross A B, solid "DrJ' Weight Corrected Alpha 16 3 +1.3 98 3.95 169 +1-511 4.00 pC1/g. KXB2 12i02/15 1112 1525757 3 Beta 26 4 +1-3 40 4 01 I 'JI +l-5.01 100 pCilg
*1:~c_f,o]!o,\~i1_1g_P_r:f.'.P._!\I~~~~~-8 w~r~__ per.ro_rm.ed......... -* . !\-Ictlrnd Description Analyst Date Time Prep Balch OO>*M**** "'"
Dry Soil Prep Dry Soil Prep GJ.-RAD-A-021 CXCl l \ll0/15 1319 15218~2 T_h_e._follcnying_r.'\n_al~:t\c~.1.'.\Ie.th_l)~S-~~.r.'.!Jll!rf.nrm~d
- Viet bod Description ASTM [)2216(Mod1fi~)
2 DOE HASL 300. 4.5 2 3.iGa-01-R 3 El'A 900UISW846 9310JSM 71 JOB l\fod1fied Su rrogatcffracer Recu"*ery Test Balch ID Recovery% Acceptable Limits
GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite l 12 Buffalo. New York 14.22& Report Date: December 17. 2015 *
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3. !.12.E.l Project: MJWCOOl 15 Sample TD: 385070003 *Client ID: MJWCOOI Surrogateffracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( l .96-sigma}.
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company; MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo. New York !4228 Repoct Date: December l 7, 2015 Contact Ms. Laurie Losey Project: Soil Radioisotopes Client Sample TD: 3. LI 2.E. ! Project: MJWCOOl 15 Sample ID: 385070003 Client rD: MJWCOOJ Matrix: So fl Collect Date: 21-0CT-15 Receive Date: 05-NOY-15 Collector: Client Moisture: 22.6% Parameter M.!?~~- ..... Le ..... TJ>~' .... _RL .. l1nits DF Anjjlyst.. _D_a~~-I!'-1.!~ . B_:t_!~l.!.. ~~!t~ .. Gravimetric Solids ASTJf D 2216 % Moisture "As Rrtcdved" Moisture 22.6 percent CXCl 11110115 1319 1521842 Rm.I Gamma Spec Analysis . Gammaspec. Gamma. Solid "Dry Weight Corrected" Actinium-227 !J 0 0!26 +/.O 297 0 538 0 256 +1-0 297 pCi/g RJff2 12103115 0846 1522383 2 Aniimony-125 U -0 I07 "'-/*O 111 0 189 0 088'> +l-0 l2i pC11g Bismuth-212 UI 0.00 *+/-0.968 I 27 0598 +1-1.17 pC'i!g Bisnrnth-214 1.06 +/-ll.187 0 145 0 0678 +/-0 208 pCifg Cesium-137 I OS +/.(l 120 0.0736 0.0342 **1-0. 151 0.100 pCilg Cobalt-60 u -0 0284 +/-0 0415 0.072 0 0321 +f.().0435 pCllg Europmm-154 u 0 0371 +/-0.134 0251 0.115 +l-0 135 pCt!g Lead-212 1.35 +/-0.140 IJ! l7 OOWJ +/-0. 173 pCi/g l.ead-214 I 40 +f-0 182 0.329 0.161 +/-0 212 pCi!g POUIS~lllm-40 18 3 +/-1 45 0680 l) 302 +/-2 13 pCi!g Protactmium-231 Ul ll.00 +/-0642 0997 0.474 +/-0 659 pC1/g Radium-226 l.06 +/-0. 187 () 145 () 0(>78 +/-0 208 pCilg Radium-228 141 +(.() 282 0.259 () 119 +/-0 319 pCi/g -Thallium-208
- 0407 +/-[) 071 0.0577 (I 0315 +l-0Jl791 pCi/g lm-126 Lil o.on +/-0 133 0 157 0 0756 +/-0. 135 pCilg Ratl Gas Flow Proportiunol Counting GFPC. Gross A*B. solid "Dry Weight Correc/ed" Alp\la 16 3 +/-3.98 169 +-1-5. l I .i. 00 pCi/g KXB2 12102115 1112 1525757 3
*' 95 B~ ~A +-/-3.40 4.01 1.91 +l-5 0 I !0.0 pCl/g J'h~f()l_~~~v,i,1~1; !'.r~P ~-i,c_t~_o_~S. ~v,e.~e..P..e~.fn_r.~1~.d ...... .
l\-tcthod Description !)ate Tinic Prep Batel! Dry Soil Pr~p DJ}' Soil Prep GL-RAD*A-021 CXCl 11/10115 1319 1521842 I~.e. .~IJIJ.0.1~'.ill~.t'\'!:ll)'tic!,ll ~c!.h.t_l~S .c.rc__p_crf()J'.111.e.d. .... Method Dc~cription ASTM D 2216 l Mod1ticd) 2 DOE HASL 300, 4 S2JiGn-01-R 3 EPA 900.0fSW846 9310/SM 7l 10B Modified Surrogatefl"raccr Recovery Test Balch ID Recovery% Acceptable Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 - www.get.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Report Date: December 17. 2015 Contact Ms. Laurie Losey Project: So.ii Radioisotopes Client Sample ID: 3.1.12.E.1 Project: MJWCOOl 15 Sample lD: 385070003 Client ID: MJWCOOJ
. . . .. ... . . . . .. **-* -.................. **-*" -**. --*** .. . ... . .. . ...... ~. .
.~a.ralll~!.e~ .... ... . . ........ _9.l!a!if!c.i: _***-* l~c_s~_ll __ . J *n~cr~aint~: .. . _i'r1J:)<;::_ . .. . ~c. . . _._F'.~' -* ._. _-~~ ___ _l~n~ts. . _I:>.F. ..:~.~'.l_lyst. ___ 1)at_c __!_i_~£- _B~f..c~. :\~_t_d.*. Surrogatcffraccr Recovery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at t~e 95% confidence level ( ! .96-sigma).
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 * (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Technical Services Address: 15 Hazel\*ood Drive Suite 11'2
- Buffalo. New York 14228 Report Date: February 10, 2016
Contact:
Ms. Lnurie Losey Project: Soil Radioisotopes Client Sample JD: 3. l.12.E.2 Pmject: MJWCOOI 15 Sample ID: 389296008 Client ID: MJ\VCOOl Matrix: Soil Collect Date: 21~ocT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 22.7% Parameter ..... . . .. - ......... ******-** .. - . .... Qu.~1_li.~C..r. Result ... t'_11 c.c.rt.:1.i.n.ty ..... . .................Le
!\IDC -*** Tl'li RL l'nits Gra\*imetric Solids ASTM D 2216 % Moisture "As Received" Moisture 221 percent C'XC1 01114116 1208 1537312 R:id Gamma Spec Analysis Gamma wirh /11growth "Dry We(r;ht Correctl!d" Actmium-227 L' .Q 0241 +/-0 308 0.549 0260 +/-0 JOS pCi/g RXF2 021()511() 0745 153754.6 2 Antimony-125 u -0 0245 +/-0.114 {) 203 U.095 +/-0 114 pC1lg Bismuth-212 lll 0.00 +/-0.809 135 0.637 .;./.1 31 pC1lg Bismuth-214 I 17 +/-0 153 0 127 0 OSR4 +/-0.181 pCi.'g Cesn*m-137 I 4J +/-0 117 0.0674 0 031 +/-0 164 u 100 pCilg Coball-60 lJ -0.0119 +!-0 039 () 0668 0.0293 +/-0.0394 pC1lg Europium-154 L' -0.0941 +/-0 131) {) 222 0.()998 +/-0 137 pCi/g Lcad-212 l 32 +/-0. l 32 0.110 0.0518 +/-0 169 pC1lg Lead-214 \.15 +/-0.2IO 0 324 {1158 +1-0230 pCtlg Potassium-40 .16.3 +/-1.34 () 641 0 2!l0 +/-1 95 pC1/g Protactimum-231 u 0214 +f-0.606 1.02 0.482 +/-0615 pCilg Radium-226 1 11 +I-() 153 () 127 00584 +/.{l 181 pC1lg Radium-228 t .27 +1-0 300 0 261 O ll'J +l-0 362 pCi/g Thall iuin-208 0.371 +/-0 0751 0(174 0.03.:15 +/-0.0&12 pCiJg Tin-126 u 0 U343 +J-0 159 0.194 ()0936 +/-0 160 pC1/g Gammaspec. Gamma. Solid Dry Weighc Con*ecrl!d".
Acunium-227 u *O 203 +1-0.260 0°16[ 0 214 +/-0.278 pCiig RXF2 01118116 11:40 1537545 3 Antmiony-125 u ()0615 +/-0.116 0223 1).11)3 +/.() 11~ pC1/g B1smu1h-212 Ul (l.00 +/-0.843 146 ().676 +1-0 997 pCi/g Bismulh-214 1.00 f-l-0 174 0.147 '()l)n68 +/-0 193 pCi/g Cesium-137 I 35 +/.() 141 1)0947 0 0435 +1-U.177 0 JI}() pCtlg Cobalt-60 u -0 0423 +1-00438 0070 0.0289 t/-0.0479 p('i/g Europmm-154 u O.JO! +/-0 143 0.300 0.134 +i-IJ 150 pCi/g l.eod-212 1.28 +f-0.131 O. Hl8 () 0508 +/-0.217 pC1/g l.eud-214 1.21 ol-/-0 182 0 355 () !72 +/.t) 216 pCilg Potassiuin-40 16 5 +/-] 65 (! 750 0315 ol-i-2.20 pC!/g Prolactinium-23 l Ul 000 +/-U.805 {) 936 fl 435 +/-0816 pCi!g Radmm-226 I 00 +/-0.174 0.147 011668 +/-0.193 pCilg Radmm-228 142 +/-U 2CJ4 0208 00874 +/-0 368 pC'i/g Thalhum-208 0.466 +/-0 0933 fJ.0706 0 031& +1-0.!0l pCtfg Tin-\26 Ul 000 **1-0.0929 0.106 0 0503 +/-ll.0949 pCi/g Rad Gas Flow Proportional Counting GFPC. Gross A:B. solid "Dr.Y JJ.'eighi Con*ected" Alpha 13.2 ..-J-.3.11 3.89 1.65 <*/-4 51 4.UO pCi/g KXB2 01 i26116 I J56 1539462 4 Beta 26 2 +/-3 18 287 1 33 +f-5 03 10 {) pCilg
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843} 556-8171 -www.gel.com Certificate of*Analysis C'ompany; MJW Technical Services Address: IS Hw.clwood Drive Suite 112 Buffalo. New York t-1228 Report Date: fcbruary I 0, 2016
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.l.12.E.2 Project: MJWCOOl 15 Sample ID: 389296008 Client ID: MJWCOO I _I_'ar~111~_e_t_~.r ....... ___ ***-. *-* _.Qu_:ili_li<<:r_ ***- .. ~c~_u!.t ....... lJn.~cr1:1~11t.- ...... Mf)C' .......L~..... . .... T.f>L. -* _.. ~!,.. Y.n.i.ts_ ... l?F _,~nnl~:.~.t.. .IJ.~~e '(imc __ B_~tc_ll .... ~*!t~,
'f.he__follnwi!ll:l J>rcp ~~ct.~~tls ~H~r.e__pe_r_f!Jf.!'.ICl~ .... -* ..... *********-** ..... .
- 'vi et hod Description Anal~*st D:ite Time Prep Batch Dry Sml Prep Dry Soil Prep OL-RAD-A-(l2l CXC l ()l/14/16 l208 [537312 T.!.1.~. f.ollo~vi11g i:':.n~ly_ti_c111. ~1.E!i~_O.d..s.Yl'el_'~J_le~ftJ.r:*n.:e.~ .............. .
Method Description ASTM D 2216 (Modified) 2 DOElIASL 300. 4 5.2 3/Ga-01-R 3 DOE llASL 300. 4 5.2JiQa,{IJ-R .\ EPA 900.0ISW846 9310/SM 711 OB.Modified . Surmgnteffracer Recovery Test Batch ID Recovery% Acceptable Limils Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Reporl Date: December4, 2015 Company; MJW Corporation Address; 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project:
~.?ii r.za~i()_i_~ot°.p~s.
Client Sample ID: 3.l.13.R.1 Project: MJWCOOll5 Sample TD: 3&5070004 Client ID: MJWCOOI Matrix: Soil Collect Date: 21-0CT-15 10:55 Receive Date: 05-NOV-15 Collector: Client Moisture: 20.5% Parameter ........... __ ...... Qu_~l_ifle.r. ...... ~~-t_i_I_t_ .. l!ncertainty MDC RL Units Gravimetric Solids ASTM D 2216 % Moisture "As Received"
- \lo1 sture 20 5 percent C'XCI 11/10115 1319 1521342 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Con-ected" Actmium-227 U 0 121 ""/-0.266 0 537 pCi/g RXF2 12i03!15 0&47 15223g3 2 Antlmony-125 u -0.0425 +/-0 111 (1.201 pC1/g Cesium-137 0 966 +/-0.126 0.107 0.100 pC'l/g Col>alt-60 u 0.0291 +/.O 0422 0 0935 pC1lg Europmm-154 u 0.0314 +/-0.136 . o.273 pC1/g Protactinium-231 u a 90s +1-0.859 ()%8 pC1/g Radium-226 0.964 +/-0 208 0.146 pCi!g Radmrn-228 0 679 +l-0 385 0.302 pCi/g Tin-126 U 0 112 +/-0 124 (l \J5 pC!/g
.Rad Gas Flow Proportional Counting Of PC, Gross A/B, solid "Dry Weight Corrected" Alplla 8. \7 +1-2 26 2.68 40() KXB2. 12i02/l5 1114 1525757 J B~ IU +/-2.09 2.47 !OJ)
- n~e. fol_lo~~i-~~ . i;>r~r. lv_let~~-~.S._\~~1~e _pe_rfo1111e.d_:
Method Description Analyst Date Time Prep Batch Df)*SOii r*rcp* ,** .... .*- .... -- . "Ill)* 'sOifPrep**oL=R.ftj).A'-021' .... ,... ...CXCT ... *- .. **1t.iit}.ij5** ....... ****-i3fl~***-******152'i84i ... *-******* ......, ....... . _Th.~.~?~ l_~l\vi~t;. f\_nal_y_ti_ca_!_ ~e_t~?~S. ~~'.:. P..~.r~°.rin.~.~'. . .. ..............-... . ................ .,.......... -............................. . Me_llt9.~ . . . . . . ._........... pe~criptic;i,ri.__ ... .. . .A.i1!llyst~mmni;:r.1t.~ ..... .. ASTM D 2216 (Modified) DOE HASL 300, 4 5 2 3/Ga-01-R EPA 900 OISW846 93 IO/SM 71 JOB Modified Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96*sigma).
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 1-lazclwood Dri\'c Suite 112 Buffalo, New York !4228 Repml Date: December l 7, 2015
Contact:
Ms. Laurie Lose,;' Project: Soil Radioisotopes C licnt Sample lD: 3.1.13 .R. ! Project: MJ\VCOOl !5 Sample ID: 385070004 Client ID: MJWCOO! Matrix: Soi! Collect Date: 21-0CT*l5 Receive Date: 05-NOV-15 Collector; Client Moisture: 20.5% P11rametcr MD("... Le Jl1.ll....... _R,1~... X_ni.ts.....DF A!?a)y~~... f.>al~ !J.~~ .!l.a.tch Mid. G1*1ivimctric Solids ASTJf D 2216 % Moistzmr "As Received" Moisture 20.5 p;;rcent . ('XCI 111101\5 1319 1521842 Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry Weight C~orrected" Actmium-227 lJ 0.121 +/-0266 0.537 0 251 +/-IJ272 pCi/g R..XF2 12/03115 0847 15223K3 2 Antm1011y- i 25 l) -0.0425 +f-0.1 l I 0201 0.0921 +/-0.113 pCrlg 13ismulh-212 l.86 +1-0.689 1.07 0 47g +/-0.713. pCi/g Bi~muth-214 0.964 +/-U.208' 0.146 0.0658 +/-0-224 pC11g Cesium-137 0.966 +/-0.126 (1107 0 0493 +/-U.149 0 100 pCilg Cobalt-60 U (l 0291 +t-0 0422 0.0935 (}0404 +/-0 0442 pCl!g Europium-154 U 0.()314 +/-O. l36 0.273 0 119 +J-() 137 pCi/g Lcad-2 ll
- 1 04 +/.Q 16 l 0.137 0 {)647 +/-0.182 pCl!g Lead-214 0.786 -t-1-0 218 0.!59 110736 +/-0 228 pC1lg PoUl5s1um-40 109 +J-1 55 0 407 0 140 +/-I.Bl pCifg Protactinium-231 Ul 0.00 +1-0 859 0.968 0.449 +/-0 383 pCi!g Radrnm-226 0.9M +l-D.208 0.146 0 0558 *1-/-1)224 pCi/g Radmm-22& ll.679 +/-0385 0 302 0 134 +l*O 396 pC1/g Thallmm-208 0.385 +1-0.077 0 0737 00332 +/-0 0841 pC1!g Tin-126 Ul 0 00 +!-0 124 (l 135 00638 +/.() 125 pCi!g Rad Gas Flow Proportional Counting GFPC. Gross AiB, solid "D1y 1-Veight Corrected" Alplia 8 17 +/-2.26 2 6g I l'l +/-2.78 4 00 pC1/g KXB2 12!02/15 I I 14 1525757 3 Beta 16 3 +f-2.09 2-47 I 18 +1-3 23 10.0 pC1/g
!_11.~..f~!!<:l'vin.g J.'rep M.etl1i:i~~-'~e.r:e .. pc~~o.rn.1c.d.
Method Description Analyst Date Time Prep Batch Ory Soil Prep 0[)* Soil l'r"P GL-RAD-A-021 CXC! I l/!0115 1319 1521842 ".f~~.e .f<>.1.lo~~i!lg ,\_11~ly!l~~l..~l~t.~o.~s- "'.(!l'C perf()r.!.11_e~ Method Description ASTM 022l6(Modified) 2 DOE llAS1, JOO. 4.5.2 3/Ga-Ol-R 3 EPA 900_0ISW846 93IOISM 71 lOB Modified Surro1!:ale/Tracer Recovery Test Batch 10 H.ecovery% Acceptable Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Anal;ysis Company: MJ\V Corporation Address: l5 Hazelwood Drive Suite 112 Buffalo, New York 14228 Report Date: December 17. 2015
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.13.R.1 Project: MJWCOOI15 Sample JD: 385070004 Client ID: MJWCOOJ J>ar_a.n1_c_t~.r. .... _ . . .... . Qllal!ficr... _ _l~e~-~t. _ V11~ertiii11ty MDC Le ..... __ ..IPY.. -* ..... }~~ ..... ~!.~.~t.!'.. _I)_~-- ~-~~~l.Y-.s.t .... !?.a.t_e_ !}.~~l'. .. !l~.~~h.....:\1.td'.. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite J 12 Bufla!o. New York 14228 Report Date: December 17, 2015
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.13.R. l Project: M1WC00115 Sample ID: 385070004 Client rD: MJWCOOI Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 20.5% P~r:i.~c~e~ . .... .. *- _.. _....9.~a!i_fle_~**** .. Res_u_l_I_. ___ I_l).c_cr.tain,tv Ml.>.C: .. 1.c . ... _. ___ Tl'V .... RL l"nits . D.l' ..~\na,lyst.... _l)n,!_~ __l_'im..~. !3!1~c-~ .. ~~~* Grnvi1i1ctric Solids ASTM D 2216 % Moiswre *~*1s Received" Moisture 2l>.5 perce1tl CXCI 11/10!15 1319 1521842 Rad Gamma Spec Analysis Gamma~7Jec, Gamma, Solid "Dry Weigh! Correcti!d" Actmium-227 u 0.121 +/-0.266 (I.537 ll251 +1.0 272 pCi./g RXF2 1210311.5 0847 1522383 2 Antirnony-125 u -0.0425 +/-0 111 0.201 0.0921 +!-0 113 pCi/g Bismuth-212 1.86 +/-0 68'J I 07 0479 +/-0 713 pC1!g Bismuth-214 0.964 +/-0.208 0.146 0.0658 +/-0 224 pCi/g Ccsium-137 0.966 +/-0.12.6* 0 !07 ()0493 +/-0.149 0.100 pC1lg Cobalt-60 lJ 00291 +1-0 0422 0093~ (}0404 +/-0.0442 pCi/g Europmm-154 u 00314 +/-[).136 IJ.273 0.119 +/-0 137 pCi/g Lcad-212 1 04 +l-0 161 0.137 0 (1647 +r-0.182 pCi!g. Lcnd-214 0786 +l-0 218 0.159 0 0736 +f-ll 228 pCifg Pota5~ium-4() 109 +/-I 55 0407 0.140 +/-I 81 pCi/g
!'mtactiniurn-231 .Ul 0()0 +/-0 859 0.968 0449 +/.I) 8R3 pCilg Radium-226 0.964- +/.CJ.208 0.146 0.0658 +/-0 224 pCi/g Radium-228 0.679 +/-0.38'5 0 302 () 134 +/-0 396 pC1lg Th.allium-208 0.385 +1-0.077 0 {1737 0 0332 +/-0 0841 pCi!g Tm-126 lJl 0.UO +/-0.124 0 l35 () 0638 +1-tl 125 pC1lg Rnd Gas Flow Proportional Counting GFPC', Gl'oss A. B..mlid "DrJ' Weigln Corrected" Alpha S.17 -i-/-226 2 68 I 19 +/-2 78 4.00 pCi/g KXB2 12/02115 l l 14 1525757 3 Beta 16 3 +1*2.09 2.47 l !R +/-3.23 10 0 pC1/g
- r.Jtl.!. ~o.!!C!.'!:i~t; J.'rc_p .~1el~(_l_d~-~~r,e_ pcrfo_r.~.C..~................. _
l\!lethod Descriplioo Analyst Date Time Prep Batch [)ry Soil Pr!!p Diy Soil Prep GL-RAD*A-021 CXCI l l/10!!5 1319 1521842 T~.C-~l)_H~_why~ r\n_~_lytiC.jll :VI~t.l~t1.~s__,~ere !'l.!1'.f.oi::1~cd _
- Vlcthod Description I ASTM D2216 (Modified) 2 DOE HASL 300, 45.2.3/G<i-O1-R 3 EPA 900.0ISW846 93!0/SM 7l IOB Modified Su .. rogateffracer Recovery Test Batch ID Recovery% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJ W Corporation Address; 15 Hnzclwood Drive Suite 112 Buffalo, New York 14228 Report Date: December 17, 2015 Contact Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.13.R. I Project: MJWCOOJ 15 Sample ID: 385070004 Client ID: MJWCOOI Surrogalerfracer Recovery Test Bakh ID Recovery% Acceptable Umils Notes: TPU and Counting Uncertainty are calculated at the 95'l-'o confidence level (l.96-sigma).
GEL LAB ORA TORIES LLC 2040 Savage Road Charleston SC 29407 - {843} 556-8171 - www.gel.com Certificate of Analysis Company: MJW Technical Services Address: 15 Hazel\\ood Drive Suite 112 Buffo!o, Ne*w York 14228 Report Date: February IO, 2016
Contact:
Ms. Laurie Losey Project Soil Radioisotopes Client Sample ID: 3.1.13.R.2 Project: MJWCOOl 15 Sample JD: 389296009 Client JD: MJ\VCOO I Matrix: Soil Collect Date: 2l~OCT-l5 Receive Date: 14-JAN-16
. Collector: Client Moisture: 22.4%
Parameter ..9!1~.1.i_lie~.. .. Rcs_u~t- ... J)~ccl'_I~ in_ty_ ...... i\1DC Le Gravimetric Solids ASTM D .:?216 % !vloisture "As Received" Moisture 22 4 percent CXCl 01114116 1208 1537312 Rad Gammn Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actmium-227 IJ 0172 +J-0 331 U63l ll.297 +/-0.342 pC1/g RXF2 02i05/l6 0747 1537546 2 Antimony-125 l! -IJ.000515 +/-0 119 0.216 0.0987 +/-0.l t9 pC1/g. Bi~muth-2 l 2 1.52 +/-0 645 0.792 0.339 .. 1-0.666 pC'ilg l31~muth-2 I4 0.785 +/-0 179 () 171 0 0785 +/-0 193 pCi/g; Cesium-137 0.991 +1-0 123 0.0733 0.0325 +l-0.153 0.100 pCi!g. C'oball-60 lJ -0022 +1-0 os ts 0.0944 0.0404 ~1-0 0527 pC-1/g. Europium-! 54 lJ 00246 +/-0 128 0.236 0.0998 +/-0.129 pC11g Lend-212 1 JO +/-0 140 () 137 00642 +1-0 173 pCi/g Lcad-214 0 998 +J-0 204 0 173 (l 080.J +l-0 223 pC'i/g Potassium-40 12.0 ...1-1.1>3 0.917 0.392 +/-193 pC1lg Protaclmium-231 UI 0.00 +f-0 91)3 I 05 0.485 +/-0922 pCi/g Radium-226 () 785 +/-() 179 0 l7l 0 0785 +/-() 193 pC1lg. Radmm-22_8 Ul 0 00 +f-0 328 I) 650 0 307 +/-0 539 pCilg Thnllmm-208 02% +/-0 074 (l.()756 OU34 +/-0 0786 pCi/g Tm-126 u 0.0406 +/.() 114 0 213 0. !02 +/-0 116 pCi!g Gammaspec. Gamma. Solid "D1y Weight Corrected" Actinium-227 u () l l3 +/-0.345 11658 0 31<1 +/-0 349 pCiig RXF2 01118/16 I 12\ 1537545 Antmiony-125 lJ -O.ll00289 +1-0 143 0264 0.123 +/-0.143 pCi/g Bismulh-212 UI 0.00 +1-1.21 I 65 () 763 +l-1 42 pC1/g Bismulh-214 0.618 +1-0 184 0 170 (J.077 +1-0.191 pC'ilg Ccsium-137 1.10 +l-0 142 0.0823 00367 +1-0.168 O.IUO pC1/g Cobalt-60 UI 000 +f-00285 0.0&45 0 0354 +/-0 0348 pCilg Europium-154 u -<Hl409 +/-0.139 0258 () 111 +/-[} 140 pCiig Lcad-212 0 986 +/-0.148 0 l3R O.llM8 +/.JJ l 67 pC1lg Lcad-214 0 994 +/-0.280 0 376 ll 182 +f-0 290 pC1!g Potassium-40 11.8 +l-1.65 0 818 0 342 +/-I 95 pCi.'g Protactmium-23 l UI noo +/-0.622 l. tO 0.510 .,./-0.63& pCi/g. Radium-226 0 618 +/-0.184 u 170 01177 +/-ll.\91 pC1lg Radmm-218 Ill +/-(] 281 0271 0.117 +/-0 315 pCi/g Thalltum-208 0.326 +!-0 HJ4 <l.084 O.fl3S ...1-0.107 pCilg. Tm-126 UI 0.00 +/-0 l'l2 {) 263 ll.126 +/-0*193 pC1lg Rad Gas Flow Proportional Counting Gr"PC. Gross .-1 B. solid "D1:i* Weigh1 Correc:ti!d" Alpha 11 9 +/-3.8! 399 I 65 -4*/-4.44 40() pCi.lg KXB2 Ol/26116 !152 1539462 4 Beta 21 <) +/-2.90 2.5~ l 16 +l-4.31 10.0 pCilg
GEL LA BORATORIES LLC 2040 Savage Road Charteston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Technical Services Address: 15 Ilazelwuod Drive Suite 112 Buffalo, New York 14228 Report Date: February !O. 2016
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: J.1.l 3.R.2 Project: MJWCOO ! !5 Sample ID: 389296009 Client ID: MJWCOO I l'ar~m~_1:e.~-. .......... Qtrnli_ffor.. .. _~.esul~ ..... l!!lm~J1.i11ty_ . . ~me::. Le The .f~H°.\\'.i_rtg_ f_r_c.J.l .~1.c!.~O_<~ .~".~.r~. P.<<::r.f.o.rm_e4. . . .. . . . ....
- \fotho<l Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil PrepGL-RAD-A-021 CXCI 0 l/l4f16 . 1208 1537312 1:bc ..fo.~Jo_\fi_ng_1\n_a!Y,ti~a~~lC!~()~~ \~'.C.~ pe.r_fol_'Jl1Cd ............ ___ ..
Method Description ASTM D 2216 (!vh1dified) 1 DOE HASL 300..4.5 2.3/Ga-01-R 3 DOE HASL 300. 4 5 2.3/Ga-01-R 4 EPA 900 OfSW846 9310/SM 71 IOB Modified Surrog:itcrrrncer Recovery Test Batch ID Reco-n~ry% Acceptable Limits Notes: TPV and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-B171-www.gel.com Ce.rtificate of Analysis Report Date: December 4, 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisolopes Client Sample JD: 3.l.l4.R.J Project: MJWCOOl 15 Sample 10: 385070005 Client ID: lVUWCOOI Matrix: Soil Collect Date: 21-0CT-15 10:20 Receive Date: 05-NOV-15 Collector: Client Moisture: 18.3'% Paramct~r ......... _ ....... _ . 9ua!ifier . _-~~-s~:l_t. _U11certaJn:t>-* IvIDC RL Gravimetric Solids ASTM D 2216 % Moisture "As Received Moisture 18 3 p~rcont CXCI 11/J0/15 1319 1521842 Rad Gamma Spm:: Analysis Gammaspe~. Gamma, Solid "Dry Weight Corrected" Achnrui:n-227 U -0 143 +/-0.26& (J 482 pC1!g RXF2 l 2i03/l .5 0&47 1522383 2 ll.nt1inon}*-125 U -0 126 +/.lJ 10 I 0 173 pCi/g Ces[um-137 I 3(! +/-0 128 0 oss lJ lllO pC.lg Cob~lt-6U lJ -0 0090 I +/-0 0442 0.0833 pCi/g Europium-154 U 0 00656 . +/-0 118 0 232 pCiig Protactmium-231 UI 0 00 +J-0.71 R 0 81 I pC1/g Radtum-226 0.770 +/-U 161 0 124 pC1rg Radiurn-228 O.\l8S +1-0.281
- 02~4 pC1lg Tm-12& U! 000 +/-0.0927 ()0936 pCi!g Rad Gas Flow Proportional Counting GFPC. Gross A/B, solid "Dry Weight Corrected".
Alpha 9 96 +1-3 08 3 99 4ll0 pC1/g KXB2 12/02115 I\ 14 1525757 3 Bel~ 21) 0 +/-2 46 306 100 p('1/g The _t?.Il~.~in~_.Pr.e.P.. .M!?tlJ..CJ.~~-~~re..e~r[o_rrne~.:........ _.......... . .... . . .. . *-** **- ... -**-****-*-***- --** ***- ........ . Method Description Analyst Date Time Prep Batch ofi sii*irri~ii ** * * * ** ** *-*** ** * **or; *siii1 1*~.;*r c;c:::R.:i\o:,;,.:i:ii-i * * * *c*xcr -******** - *iifi011:s* 1319 *fsii-842********- -****
.T..~-~-'..?_l!.o.v.ving J\.n.a_IXti_~_a! ivlet'.1(}~s -\~~r~ pe_rform_ed_:. .. .... ... .. ... . ... ...... .... .. ... ............ **- .... ... ... .. . . . . . .... ... _..... ***********-* ..... .
Mt:t.hq~ ... _.. .. .......... *- P.c.~~rl.P_tio!,__ ....... . _____ . -*** ... . . . ... *-*- .... -*- ... . . . -***-** b.l.l!!:IY_~t c;::0111!1.1~m.~. I ASTM D 22 \6 (Modified) 2 DOE HASL 300. 4 5.23/Ga-Ol-R 3 EPA 900.0/SWll.\6 93 IOiSM 71 IOB Modified Notes: Counting Uncertainty is calculated at the 95% confidence fevel ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Bu!Tulo, New York l4228 Report Date: December 17, 2015
Contact:
Ms. Laurie Losey Project: Sot! Radioisotopes Client Sample ID: 3. ! .14.R. l Project: MJWC'00115 Sample ID: 385070005 Client ID: MJWCOOI Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 18.3% Parameter ........ _.9~1.l_lifi.e'.. ...... -~~sult Cnccrta.int)' *- .....~!D~ Griwimetric Solids ASTM D 22!6 % ivloisture "As Receil'ed" Moisture 18.3 percent CXCI l\110115 1319 1521842 Had Gamma Spec Analysis Gammaspec. Gamma, Solid "D1y Weight Con*ected" Actinium-227 U -0.143 +/.(l 268 0.482 0 228 +1-0 277 pC'i/g RXF2 .12103115 0847 1522383 2 Annmony-125 ll -0.126 +1-0 101 0.173 0.0796 +1-0 117 pCLig l3i~mu~1-212 !Jl 0.00 +1-0 555 1 14 0 523 +/-0.613 pCllg Bismulh-214 0 770 +f-0.16! () \24 () 056 +l-0.173 pCi/g Cesium- 137 I 36 +f-0, 128 0.0S.5 0 0392 +/-0.172 010(1 pCi/g Cobillt-60 u -0.00901 +1-0.0442 0.USJJ 0.0364 +/-0.04*14 pCi/g Europium-154 ll 0.00656 +l-0. 11 S 0 232 0 10:?. <-1-0 118 pCi/g Lcad-212 1.07 +/-0.112 0 IUI 0.0478 +/-0.173 pC1/g Lead-214 0817 +/-ll.194 0 137 0 0639 +l-0 207 pCLlg Potnssium-40 11 5 +/-! 34 () 7~13 (IJl9 +/-! 74 pC!/g. Protactmmm-231 lll 0()() +/-0.71 B {) 811 O.J"I& +l-0149 pCi/g Radium-226 0.770 +/-0.161 ().124 0.056 +/-0 173 pC1/g Radium-228 0 988 +/-(l.281 0244 0 108 +/.() 3 lfl pC1/g 111alhum-208 0277 +/.II 0893 0.0735 0.0338 -t/-0.0924 pC1/g Tm-126 Ul 0.00 +i-0 0927 0()936 () 0449 +/-0.094& pC1/g Rad Gas Flow Proportional Counting GFPC Gross ;[:B, solid "Dry 1-Veight Corrected" Alph~. . .Le.. .... .. . :rrt.! __ ........l!-L. .... l:n.i!S. .. l!f. :.\11.:ilyst. _,J):it.~_!i~.c ..B.atch --~ltd. Gravimetric Solids ASTJf D 2216 % Moisture ".-fs Recefred" Moisture 183 percent CXCI 1 tll0/15 1319 1521842 Rad Gamma Spec Analysis Gammaspec. Ganmw. Sofid "D1:v Weight Corrected" Actinium-22 7 ll -0.143 +/-0.268 0 482 () 228 +1-0 277 pCiig RXF2 12/03/15 0847 1522383 2 Antimolly-12:5 u -0.126 +l-0 IOI 0 173 (J 0796 +1-0.117 pCrJg Bismuth-212 UI 000 +l-0.555 1.14 0 523 +1-0 613 pCi/g Bismuth-214 0770 +/-0.161 0 124 0056 +/-0. 173 pC1!g Cesium-137 1.36 +/-0 128 0.08:5 00392 +1-0 172 0 !00 pC1/g Cobalt-60 u -0.00901 +/-0.0442 0 !1833 0 0364 +1-0.0444 pC1/g Europium-154 lJ 0.00656 +/-0.118 0.232 0 \02 +/-0.118 pCi!g Lcad-212. 1.07 +/-0I12 0.101 0 0478 +/-O.l7J pCi/g: Lcad-214 0.817 +/-0.194 0.137 0 0639 +/-0 207 pCifg Pub~siurn-40 11 5 +/-134 0 743 OJ\9 +r-1 74 pCi!g Protactmium-231 U! 0.00 +/-0 718 0 811 OJ78 +/-0 749 pCt!g Radium-226 0 770 +/-0 161 () 124 0.056 */-0 173 pCi!g Radium-228 () 988 *1'/-0281 0.244 0 108 +/-0.310 pCi/g: Thalhum-208 0 277 +/.(] 0893 0:0735 () 0338 +/-0.0924 pC1/g
*['in-J2C1 l!I O.ClO +/-0 0927 0 093t\ 0 0449 +l-0 0948 pCilg Rad Gas Flow Proportional Counting GFPC Gross A.'B, solid "Dry if'eight Corrected" Alpha \l.96 +/-3.08 3 99 1.80 +/-170 4 00 pCilg KXB2 12102115 1114 1525757 3 Beta 20.0 +/-246 3.06 147 +/-3 86 10.0 pCi/g 'fhc followil1g Prep Melhods were performed
- Vi~th~d ______....... "*u*e~c~ii;ii~~ .......-...... ... ..... *.
- Analyst Dute Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-02 l CXC! 1)/10115 1319 1521842
!~.I! r~.1.101~~~g ..\na,l)'~_ic:t~ ~e~h.o~s .w~~i: p~rr~.r~1c.d.. ' Method Description ASTM]) 2216 {Modified) 2 DOE HASL 300, 4.5.2.3/Ga:ot-R 3 EPA 90U.0/SW846 9310/SM 71 IOB Modified Surrngatcffracer .Recovery Test Batch ID Rcconry% Acceptable Limits
GEL LA BORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Sui1e 112 Bu!Talo. New York 14228 Report Date: December 17. 2015
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample TD: 3. l. l 4.R.1 Project: MJWCOO 115 Sample ID: 385070005 Client ID: MJWCOO I _l'a~'.'!11~.t~.r.... ***-.. .. . .. . . .guaH!icr.
- Result Snccrt:iinty :\-JDC Le TPC
**---****-- RL Uuit~ OF Analvst.......
******-*** ....... - .. *-*-**** ........ -* ........... ~-* ~
Time -**Batch Date....... Mttl. Surrogateffracer Recovery Test Batch JD RcCnl'cry% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 - www.gel.com Certificate of Analysis Company; MJW Technical Service~ Address: l5 Hazelwood Drive Suite 112 Buffalo, New Yorl< 14228 Report Date: February lO, 2016
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.14.R.2 Project: MJ\VCOOl 15 Sample ID: 389296010 Client lD: MJWCOOl Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 19.4% Paraniet~r... ...... .. . . ... qu_a_li~cr .....~e.sul! .... r11.i!~r~:Ji!!ll' . .MQ~ -----* -'~<<:'. .TPr
********- .. ****** ..... . ~!,:..... l'.uits. . _DF_ An:1lys~ .. _D:i.te.. Tim_e_ B,a~~~----~*1. td:
Gravinietric Solids ASTM D 2216 % Jfoisture "As Recefred" Moisture 19.4 perccnl CXCI 01114116 120g 15373!2 Rad Gamma S1icc Analysis Gamma wit/: lngrowrh Dry Weigfll Corr~c:ted" Actmium-227 u -0 172 . +/-0 211 (I 3(J5 0 174 +/.(l.226 pC,/g RXF2 ()2I05fl6 0842 1537546 2 Antimony-125 LT ll 0178 *r/-0.0897 0.160 IJ.1)759 +1-0 0901 pC1lg Aismulh-212 UJ 0 00 +/-0.621 0 063 0.305 +/.l) 643 pCi/g Bismuth-214 O.S69 +/-0.144 0.104 () 0486 +/.():161 pCilg Cesium-137 1 27 +/-Q.0964 O.U564 00263 +/-!l.140 0 100 pCilg Cobalt-60 u () 110241 +/-0 030 0 0568 0.0254 +/.() (}30 pC!lg Europium-154 u .() ()386 +f-0.0904 0.160 00719 +/-0.0921 pC1/g Le~d-212 0.794 +/-0.!04 0 0986 0.0475 +/.{) 121 pC1/g Lead-214 0.915 +/-0 142 () 234 0114 +/.() 159 pCi/g Potassmm-40 11.9 +1-1 17 ll.428 0185 +/*l.60 pC'ilg Protactmium-231 u 0.342 +l-0 443 () 775 0.370 +1-Q 475* pCilg Radium-226 0869 .,./-0.144 0 1Cl4 00486 +i-0 161 pCi/g Radium-228 1.02 +l-0 11!0 0 172 0.0779 +/-0.228 pCl/g
- niallium-208 0203 +l-0 Oo5l 0 0563 ().0264 +/-00672 pC'ilg Tin-126 lJ I 000 +/-0 lJ84 () 126 0061 +/.{) 0858 pC'ilg Gammaspec. Gamma. Solid "Dry Weight Correcred" Actinium-227 ll -0(}627 +/-0 280 0.518 0.242 +/-0.282 pC1fg RXF2 Ol/181115 112*1 1537.545 3 Antimony-125 lJ -00142 +/-0 117 0.213 00982 +/-0 117 pC1/g Bismuth-212 1.77 f /.(1 7()0 () 864 0.379 +t-0 781 pC1/g Bismuth-214 0144 +/-U 173 0 129 0.0576 +/.() 184 pC1/g Ccsium-137 137 +/-0 141 0.0746 0.0335 +i-0.180 0 100 pC1lg Cobalt-60 ll ll.0227 -t-/*ll 0403 0 OBS6 0.038! +/.(I 0417 pCi/g Europium-154 u -00087 +/-0 139 0269 0.118 +1-ll 140 pCifg l.ead-212 () 942 +l-0 158 (j_m 0.0574 +/-1) 179 pCi!&
Le~d-214 0 764 +l-0 187 0 148 0 0681 +/-0.198. pCilg Potassiwn-40 II 4 +/-] 41, 0.591 0234 +I-I 77 pC!lg Prolactinium-23 I U! ()00 +/-0.706 0 953 0.443 +/-ll 720 pC1/g Radmm-226 (1.744 +/-0 173 0129 (1.0576 +/-fl 184 pCi.lg Radmm-228 0.952 +/-0 265 \1258 0.112 +/-0 302 pCilg Thilllimn-208 0.100 +/-0.079 0 0639 0.0285 +/.() 0&01 pC1lg Tin-126 UI 000 +/.() 0993 0.175 () 0841 +/.() 112 pC1'g Rad Gas Flow Proportional Counting GFPC Gross A:B. solid "Dry Weigh/ C'on*ected" Alpha 9 16 +/.J 18 3 99 I 75 +/-3.62 4 00 pCi/g. KX02 ()1126/t(i 1155 1539462 4 Bela 19 6 ..-/-2 47 2.2t/ 1.06 +/-3 70 100 pC1/g
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8.171 -www.gel.com Certificate of Analysis Company: MJ\1.' Technical Services Address: 15 Hazelwood Drive Suite ll2 Buffalo, New York !4228 Report Date: February !O, 2016
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.14.R.2 Project: MJWCOOl 15 Sample ID: 389296010 Client ID: MJWCOO I r .P.~.r~.~e.tc.r.......... -. - . -- - g~~l~.fie.i:._ -**. __ l_~~s11_*1 ..... - ~.~~f_tain~y.
!.l.11~ .folln~Jng_ P!,t:.P. .~'!Cthl)d_S. \~e~I: .r.crfor.m.ctl ..
- \fothlld Description Analyst Date Time Prep B:itch Dry Soil Prep Dry Soil Prep GL-RAD*A-021 CXCI 01114/lf> 1208 1537312
'f.hcJoll~w.i11g. Ana..fY.t.i.cal M.cthutls.~\'.c.i.-11*ptrfo~*nied ...
- Vkilwd Description ASTM D2216(Motli!lcd) 2 oot HASL 300. *l.5 2 3/Ga-01-R 3 DOE HASL 300, 4.5 2.3iGa-01-R 4 EPA 900 OISW846 931 OISM 71 lOB Modified Surrogakffracer Recovery Test Balch lD Rcccwcr)'% Acceptable Limits Notes:
TPU and Counting Unce11ainly are calculated at the 95% confidence level ( J. 96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of AnaJysis Report Date: December 4, 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York t4228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.15.R.l Project: MJWCOOI !5 Sample ID: 3&5070006 Client !D: MJWCOOl Matrix: Soil Collect Date: 21-0CT-15 14:40 Receive Date: OS~NOV-15 Collector: Cl.ient Moisture: 21.9% Parameter Qualifier MDC RL Gravimetric Solids ASTM D 2216 % Moisture "As Received" 21.9 percent CXCI 11/1011:5 1319 1521842 0.605 pCi!g RXF2 12iOJ/15 1303 1522383 2 u 0. 121 0.246 pCi/g I 28 00961 0 100 pC1/g u 00155 "(I 099& pC1!g Europlllm-154
- u 0 00314 +/-0.151 0 291 pCrlg Protactinium-23 I UI 0,00 +/-0.914 1 23 pC1/g Radium-226 0932 +/-0.230 0.190 pC1fg Radium-228 01)06 +J-0 363 0.340 pCilg Tin-126 U 0.0586 +J-0. 189 0 238 pCi!g Rad Gas Flow Proportional Counting GFPC, Gross A/B. solid "Dry Weight Corrected"
~pha 13 I +1-3 19 3 76 4 00 pCi!g KXB2 12i02/l5 1116 !525757 3 Beta 21 7 +1-2.71 3 36 10.0 pCiig !!1.e.:f?.l.lo~*i~~-~.r~pJvfeth(JdS -""~E~ p~_rf.or.1n_e<l.: .... ................ . ........ ***-***
Analyst Method o~: Description
*s*oj1 rrcp**** * ** .. ,... * *****-** - **nr}~son--*Prep *01~-RAD~)\-Oz"f ** *** **-* * * * *..c:,*xci ...........
- Dale Time Prep Batch 1"iith1i5- ***** ..... *1:119** * .....15:.frs4i .... *- ..... * -
~he ~?l_l_C?.:~i_n?. A11~l:yti~_a.l__fl.J~t.h?.d_5..Y'c.reye.r.f.?.li1.1ed:_ . . ~-~-t!.~C?Q .. . .. . _J?~sc.r.ip\i.QJ1...... ... . . . ..... . . ............... A!J.a.1.Yst C(}llJAl~!ltS.
ASTM D 2216 (Modifi~d) 2 DOE HASL 300, 4 5 2.3iGa-Ol-R 3 EPA 9000ISW846 9310/SM 71 IOB Modified Notes: Counting Uncertainty is calculated at'the 95% confidence level ( 1.96-sigma).
GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite l !2 Buffalo, New York 14228 Report Date: December 17. 2015
Contact:
Ms. Laurie Losey Project: Soil RadioisoLopes Client Sample ID: 3.1.15.R.I Project: MJWCOOl 15 Sample ID: 385070006 Client ID: MJWCOOJ Matrix: Soil Colfect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 21.9% .P.~E~!11_et~r .. .. *- . .. -* ...9~~1.i~er .....~c_s!t_l_l_ .. -* (11c4:!.l'.lll..i~. lv MDC Le Gra\'imetric Solids ASTM D 2116 % !idoiswre "As Received" Moisture 21 9 percent CXCI \ 1110!\5 1319 1521842 Rad Gamnia Spec Analysis Gammaspec, Gamma. Solid "D1j* Weight Corn~cled" Actmium-227. U -0 178 +-1-0 348 0 ()05 t\283 +/-0.358 pC1/g RXF2 12i03!15 1303 1522383 2 Anumony-l 25 UI 0 00 +/-0.202 0246 0.114 +/-0.210 pCi/g Bismuth-212 UI 0.00 +/-1 ll I 55 071!! +1-125 pC1/g B1smuth*214 (J.932 +/-0 230 (J 190 1)(1877 +/-0 243 pCi/g Cesium-137 I 28 +/*ll 158 00961 0.043R .,./-0.192 0 !00 pC1/g Cobalt-60 U 0 0155 +/-0.0487 \J.0998 0.0431 +/.(! 0492 pCt/g Europmm- I 54 U 0 00314 +/-0 151 () 29\ 0.127 +/-0.151 pC1/g Lead-212 1 10 +/-0.154 n 144 00681 +/-0.181 pC1lg lead-214 1.16 +/-0.224 0.17] 00798 +1*0245 pC1/g Potassium-40 15.0 +/-1.69 IJ 731 () 297 +/-2.12 pC1tg l'rolactm1um-23 l l1l (I{){) +/-0.914 1.23 ll.574 +/-0.')72 pC1/g Radium-226 !l.932 +/-0 230 0.190 U.O!S77 +/-0.243 pCt!g Rmlium-228 0 906 +i-0 363 0 340 0.152 +/.() 387 pCilg Thallium-208 0 295 +/.() 0794 0 0849 00385 +l-0 ()834 pCtlg Tin-126 U 0 058(i +!-0 189 () 238 0 114 +l-0.190 pCi/g Rae.I Gas Flow PrQporticmal Counting GFPC. Gross AB. solid "Dry lf'eight Corrected'.' Alpha 13.1 +/-3 19 3.76 l.70 +/-4 06 400 pCi/g KXB2 12i02115 1116 1525757 3 Beta 21 7 +/-2.71 3 36 1.62 +/-404 10.0 pCi/g Th..I! ~oll.~wi1_1g_!'.r_ep ~lctho,~s.'\'l'..Z:c . pcrfor111.~~- ...................... . ..... ....... -.............. ,..... ..... ,...... __ , .. ............._, ..... . ... *' Method Description Analyst Date Time Prep Batch Dry Soil Prep Dty Soil Prep GL*RAD-A-021 CXCI 11/10!15 1319 1521842
~r_!J_e fol_l?.'Yi'!~ An_~ly_l_ic~~ J_\'~j!t~IJdS '.".e.~e r.i:r~'or~.e~...................._....... .
Method Description J ASTM D 2116 (Modtricd) 2 bOE HASL 300. 4.5.2.3/Ga-O\-R 3 EPA 900 OiSW846 9310iSM 71 IOB Modified Su nogateffraccr Recovery Tcsl Batch lD RccO\'crr% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - 1Nwv1.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite l 12 Buffalo. New York 14228 Report Date: l)ecember 17. 2015
Contact:
Ms. Laurie Losey Project; Soil Radioisotopes Client Sample ID: 3.1. 15.R. r Project: MJWCOOI15 Sample ID: 385070006 Client ID: .MJWCOO I Pnr.am.~~~r........................Q.u_a~if1cr ...... !lesull _l)1m.~a.i.nt~:. . ..~ID<;. .... .Ice........ __ .WL ......... __Rf:__ X1_1i_t_~ __ ~F ;\11a~ys_~ .... Da~e. Ti.l?.e -~:ttc_l1 __ !VI.t~.-. Surrogutcffracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at 1he 95% confidence level ( 1.96-sigirta).
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: l 5 Huzeh,*ood Drive Suite 112 Bu/Talo. New York 14228 Report Date: December 17. 2015
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.15.R. I Project: MJWCOOl 15 Sample 10: 385070006 Client ID: MJWCOO! Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 21.9% Paran1eter l'ncerlaintv MlJC Le Grnvimetric Soliils A STM D 2216 % Mois111re "As Recefred" Mornture 21 9 percent CXC"l 11/Hl/15 1319 !521842 Rad Gamma Spec Analysis Gammaspec, Gamma. Solid "Dry Weight ('orrecl;~d i\ctimum-227 U -0 178 +/-0 34S . 0 605 0.283 +/.0.358 pC1/g RXF2 12103115 1303 1522383 2 i\ntimony-125 UI 0.00 +1-ll 202 0.246 0.114 +/-0 210 pCi/g Blsmuth-2!2 lll () 00 +/-1 l l 155 0 71S +/-! 2~ pC1/g Basnrnth-214 0.932 +/-0.230 0 190 0 0877 +/-0.243 pC1lg Ccsiurn-13 7 l 28 +J-0 l5S 00961 0 0438 +/-0 192 0.100 pC1/g Cabalt-60 u 0 0155 +/-0 0487 00998 0.0431 +/.!) 0492 pC1/g Europium-l 54 u 0.003 \4 +l-0 15! () 291 0.127 +1-0.1 s l pC1/g Lcad-212 1.10. +/-0 154 0 144 00681 +J-0 lSI pCr/g Lcad-214 1.16 +/-0 224 [) 173 00798 +(-0 245 pC1/g Pota.~ium-40 IS.0 +J-1 69 0 731 () 297 +l-2 12 pCi/g Protactimum-231 Lil 000 +/-0914 123 0 ..574 +f-0.'>72 pCi.lg Radmm-226 0.932 +/-0.230 0.190 0.0877 +f-0.243 pC1/g Radmm-228. 0.906 <*/-0.363 0340 0 152 +/-0.387 pC1/g Thallium-208 0.195 .,./-0.(l794 O.OS49 0 03S5 +/-0.0834 pCi!g Tin-126 ll 0.05&6 +!-0 189 023~ () 114 +/-0*190 pCilg Rad Gns l'low Proportional Counting c;FPC, Gross A/B. solid "D1:1' Weig/if Corrected"* Alpha 13.1 +/-3 l9 3 76 1.70 +/-4.06 4.00 p('rlg KXB2 12i02fl5 1116 1525757 3 Bela 21 7 +/-2.71 3 36 l 62 +1-4.04 100 pCi/g lJ11'...~l!l.~c.1wi11g r,rep :vl_e~h.~.~~.ll*~i:eJi.ci:-1:0.".1.11~.~.......... '*** " ................ .
- \1ctt1od Descri11tion Analyst Date Time Prell Batch Dry Soil Prep Dry Sad Prep GL-RAD-A-021 CXCl 11110115 1319 1521842
!_li_e.~(111()"'.i.~.g .'\n.?!Y.tii:.a..1. ~.l~~~Y.~S.. 'v.er.e J>_er.f.oi_:11:1e~ .
~lcthod Description ASTM D 2216 (Modifo:d) 2 DOE HASL 300. 4 5 2. 3/Gn-0 l -R 3 EPA 9GO.O/SW846 93 JO!SM 71 IOB Modified Surrogatefl'racer Recovery Test Batch 10 Recovery% Acceptuble Limits
GEL LAB.ORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171
- w.vw.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drh*c Suile 112 Buffalo, New York 14228 Reporl Date: December 17.2015
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.15.R. I Project: MJWCOOl 15 Sample ID: 385070006 Client ID: MJWCOOI
. ~*\: ....... __ Tl'.L. ***--. }_~!,.. . _l~_11_it~.. -~F. An:i_ly~t ...J?.a.~e. :r_-~1.ne__ -~:J~.<:l_i_ .. ~ltd,=.
Batch H) Reco\*ery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigrna).
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843} 556-8'\71 - www.gel.com Certificate of Analysis Company: MJW Technical Ser.-ices Address:* 15 Ha:telwood Drive Suite 112 Buffalo, New York 1422.8 Rep.or! Dute: Pcqruary I 0, 2016
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample m: 3. !.15.R.2 Project: MJWC'OOl 15 Sample ID: 389296011 Client ID: MJWCOOI Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 22.1% . ~~rarn_et~r. _****-** .. _ ... _ q1~.~li.fi.c.r. .Il~.t:. Gravimetric Solids
,-lSTJf D 2216 % Moi.~ture "As Received" M(nsturc 22.1 percent CXCl 01114116 1208 1537312 Rad Gamma Spec An;1lysis Gwnma with lngrowlh "Dry Weight Corrected" A~tmium-227 u -0.053 +/-1) 283 lJ 489 0 231 +1-0 284 pC1!g RXF2 02105116 0842 1537546 2 Anlimony-125 ll 00738 +/-0.121 0.231 () ]()9 +/-0.126 pCi/g Bismuth-212 2.07 +/-0.966 0 966 0.435 +t-0.985 pC1/g Bismuth-214 0.833 +lo 116 () 143 0.0655 -~/-U 189 pCi/g Cesium-137 1.72 +/-0 140 009[) 00411> +1-<i 196 0.100 pCi/g Cob.alt-60 lJ O.U252 +/-0.0471 0 0908 00396 +1-0 0485 pC!lg Europmm-154 u -U.024 +/-0.150 0.244 0.!06 +/-0.150 pCi/g Lead-212 1.18 -r/-0 129 0.118 O.ll563 +f-0 162 pCi/g Lcad-214 I 2(! ...,.() 185 0.33& 0 164 +1-ll 212 pC!lg Po1ass1um-40 15 3 +/-1 71 IJ 730 () 308 +l-2 16 pC'1/g Prota~lmmm-231 UI 0.00 +/-0996 () 9117 0427 +/-1.09 pCi/g Radium-226 0 &33 +/-() \7() 0 143 0.0655 +/-() 189 pC1/g Radmm-228 I 14 +/.() 287 0282 0.126 +f-0 318 pCilg Tlmllium-208 0 J87 +/-0.080 0.0742 0.034 +/-0.0862 pCilg Tm-126 Lil 0.00 0l12 () 124 () 0595 +/.O.l 14 pCi/g Gammaspec, Gamma. Solid "Dry Weight Corrected" Actmium-227 lJ -00408 +/-0 357 () 663 0.310 +1-0 353 pC1!g RXF2 01/18!16 1122 1537.545 3 Ant11110ny-125 u 0.0275 +/-0.152 0 281 0 !3lJ +/-0 152 pC1!g Bismulh-212 Ul 0.00 "-/-0.857 I 67 0773 +/-I 16 pCi!g Bismulh-214 o s2g +/-01% O.lbO OlJ7\7 +/-0.210 pC1/g Cesium-137 1.68 +/.().183 .() 1()8 [I 0493 +l-0 23~ 0.100 pCi!g Cobalt-60 u 0 00658 +/-0.055! 0.111 00479 +f-0 0552 pCi/g r::uroprnm-154 v 0.0103 +/-0.135 0.275 0 117 +/-0.135 pC!lg Lead-212 120 +/.().151 (I 147 0.069\ '+/-0. \85 pCt/g Lead-214 0 944 <*/-0.267 0204 0.[)948 +/-0 279 pC1lg Potass i um-40 13 3 +l-1.65 () 617 () 234 +1-2.!JI) pC1ig Protacumum-23.\ lJI 0.00 +/-0 8&8 1.54 0727 +-1-1.0(> p('t1£.
Radium-226 0.818 +/-0.196 O.lfiO 0.0717 +/-0.2!0 pCt/g
*Radmm-228 I U7 +/-0 376 {) 377 () 168 +/-0 405 pCiJg Timllmm-208 0.301 +/.()0966 0 0881 0.(139R +/-0.100 pC1/g Tm-126 UI 000 +/-0 188 ().2iJ2 U U91i ... /-0.189 pC1/g Rad Gas Flow Proportional Counting GFPC. Grass A:S. solid "Dry JVeight Con*ected" Alpha 18 s ***l-4 07 3.95 1.72. +/-5 49 4.(1() pC1/g KXB2 Ol/26116 1152 1539462 4 Beta 23 7 +/-2 89 282 I 31 +1-4 5(> 100 pCi/g
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:. MJW Technical Scrvkcs Address: 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Report Date: February 10. 2016
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Ms. Laurie Losey Project: Soil Rndioisotop(!s Client Sample ID: 3.1.15.R.2 Project: MJWC'OO ll5 Sample ID: 389296011 Client JD: MJWCOOl Parameter Cncert~intv Le TPl' Dnte Time B:itch......... Mtd.. The.fo.ll~."'}.ng_f.'r.cJ!.~1.e.~ho<!~~-e.i:~.J!l:~fl)_r~ne~. Method Description Time Prep Batch Dry Soil Prep C'XC' I Ol/14116 1208 1537312 Th.c. r.011~,'t.i.ng ,\~a..1yti~<:1l_i\-f.e.1110..d.~ ~\*.e.re. p~rf1n::n1.e~ ...
- \*le thud Description
.ASTM D 2216 IModifa:d)
DOE HASL300.4.5 2.3/Ga-01-R DOI:: HASL 300. 4 5 2 3/Ga-01-R 4 EPA 900.0iSW846 93 !Q.1SM 71 I013 Modified Surrogatcffracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) .556-8171 -www.gel.com Certificate of Analysis Rep011 Date: December 4, 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 1422&
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Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.16.R.I Pmject MJWCOOll5 Sample ID: 385070007 Client JD: ;...-uwcoo1 Matrix: Soil Collect Date: 21-0CT-15 14:10 Receive Date: 05-NOV-15 Collector: Client Moisture: 18.1% Result Uncertainty .... -*** **- .. -* .... MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Mmsturc 18.! percent CXCl l l/10115 \319 1521842 Rad Gamma Spec.Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 U -0 0964 +i-0 260 0 494 pC1/g RXF2 12/03/1; 1303 I 522383 2 Antimony-125 U -0.0282 -t/-0 112 0206 pCi/J;? Ccsium-137 I 75 +/-0 161 00756 ll 100 pCi/g Cobalt-60 ll 0.0436 +/-0.0414 00968 pCi!g Europium- 154 u -0 0232 +1-0 114 n.19! pC1/g: Protaclinmn1*23 I lJ 0 306 -t-/-0558 1.12 pCilg Radiwn-226 0 682 +1-0167 0 139 pCi/g R.adiw11-228 0.716 +1-0.295 0.279 pC1/g Tm*126 U () 0837 +1*0 143 0 193 pC1rg Rad Gas Flow Proportional Counting GFPC. Gross AfB, solid "Dry Weight Corrce<ted" Alpha* 14- 7 +1-3 55 3.9S 4.00 KXB2 12!02il5 1116 1525757 3 Beta 21-7 +/-2.59 2.91 100 Ih.~ fo.l!()~V.i.n~ .P:~~P ~',~et.~?~s_ ~_ere_r.erforin~d.:_ ***--* __ ... . . _-* ....... _.. . . . ... *- _.. _ Method Description Analyst Date Time Prep Batch or;;*s-c;,Trre.i>> .... ****-* *** .. * ***5iY*s1i11 fiiei> dC:R'AB~;\:-02t * - *- *****- ***** ***** **** * -*txc1* -* * ... * * - fihohs* -
- f:fr9 *
- 1521842
.Th~. f~l~()~Y.i~¥_~~-~Ixti~a:1_ ~~~?.ds_\v.er-~ P.~~o.r1ned_: ........................ .. _rv1~~h.P.~. _.... ... ********- .... __pe~c:r~.P.tion... .... ....... .. .. ..... . . . ..................... _.. . . .... .. . -* .. .A.!1-~h'1>.t(Qf.\lll)_~n.~s .. _ ASTM D 22!6 (Modified) 2 DOE HASL 300. 4.5.2 3/Ga-Ol-R 3 EPA 900 0 1SW846 9310/SM 71 IOB Modified Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).}}