ML16294A197
Text
{{#Wiki_filter:Appendix G-Sub-Area 3.1.19-3.1.24-COA
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Anal;ysis Report Date: December4, 2015 Company: Address:
Contact:
Project: OOO**OOOO*>oo*" HOOO 0 Client Sample ID: Sample JD: Matrix: Collect Date; Receive Date: Collector: Moisture: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Soil Radioisotopes 3.1.19.R.1 385070013 Soil 20-0CT*IS 13:40 05-NOV-IS Client 19.9% Parameter Gravimetric Solids ........9t1~[-~~er..... ~e.sult Uncert_ainty ASTM D 2216 % Moisture "As Received" Mohture 19 9 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Actimum-227 "Dry Weight Corrected" l! -0 U.0374 +/-0 244 Antimony-125 u -0.0461 +1-0 0992 Cesium-137 I 07 -t-1-0 ll)9 . Cobclt-60 Europium-154 Protactmium-231 Radium-226 Radrnm-22& u u u Tin-126 L' Rad Gas Flow Proportional Counting -OOUR\\2 2.92E-05 0.773 () 779 1.02 0.115 GFPC, Gross AIB, solid "Dry Weight Co1Tected" M* lU BMa [~9 !h.e f.o.l!C>\\\\'i.n~. P_r~p )l,1_cth~~~- \\Y.':'r.~.P_~~_fo,r~i:i~1=. Method Description +/-0.0401 +/-0.l l l +/-0.559 +/-0.132 ~1-0.211 +/-0.139 +f-3.51 +J-2 73 or;: So1f Prep... _................... I)!)."so1iPrcii"CiC-"i'1:iiD;A;Oi! *-*.... Tl~e ~ollow ing Analrti.:~~ l\\'.fe:t.~1i::ds ~e~*e ~e~_fi:>~~-e-~_:... M?.1h~tL............. ..... 1?.esi::riptlqn........................ ASTM D 2216 (Modified} ~ DOE HASL J00,4 5 2 3fGa-Ol-R 3 EPA 900 O!SW846 93 lO/SM 71 lOB Modified Notes: Project: MJWCOOl 15 Client ID: MJWCOOI MDC RL percent CXCI I L/l0/15 1319 1521842 0.468 pC1lg RXF2 12103115 t305 I 522383 0 177 pCi/g I) 0739 () 100 pC1/g 0.0765 pC1/g 0211 pCi/g 0 S91 pCi/g 0.111 pCi/g () 263 pCi/g 0.133 pCi/g 3.83 4()0 pCi!g KXB2 12/02115 1120 1525757 3 13 IO.U. pCi/g Analyst Date Time Prep Batch
- cxc1-...........
l )110115 .. f3.1Cj'....... f5if842-**-......... -..... ****-......... ............. _. Ani:i.l.YS.!.C.:<:>1.rupcnts. Counting Uncertainty is calculated at the 95% confidence level (l.96-sigma). 2 3
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.geLcom Company: Address: MJW Corporntion I 5 lfozelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.l.19.R.l Sample TD: 385070013 Matrix: So.il Collect Date: 20-0CT-l 5 Receive Date: 05-NOV-15 Collector: Client Moisture: 19.9% Certificate of Analysis Report Date: December 17. 2015 Project: MJWCOO 115 Client ID: MJWCOO I Parameter . _91~ali lier.. Result.. l'.ilcerl:iin~.~-...... MDC Le .... IPL....... RL. L!nits... _DF_ Analrst.. Date Time Balch ~ltd. Gral*imetric Solids ASTM D 22 I 6 % },,[oisture "As Rr:ceived" Moisture 19.9 Rad Gamma Spec Analysis Gammuspec. Gamma. So/icl "Dry Weight Corrected" Aclmium-227 l! -0 00&74 +1-0 244 Anrnnony-125 U -0.0461 +i-U 09'}2 Brnmulh-212 Ul o 00 >-/-0 746 IJismuth-214 o 779 +/-0 132 Cesium-137 Cobalt-(}(} Etiropium-154 Lcad*2 l2 l.cncl-214 Potassium-40 Prota1:tmium-23 I Radium-226 Radium-228 Thalhutn-208 ll u lJ I Tin-126 Ul Rad Gas Flow Proportional Counting 1.07 -0.00812 2 92E-05 1 ][J 0 970 12 9 0.00 0.779 1.02 0.325 0 00 GFPC. Gross A;B, solid "Dry Weight Corrected Alpha 14.7 Beta 19 9
- !".h..c fo_ll_O~li.ng_ P_rcp.. ~Je.tl~l)~S.\\l:~!f:! P':!.~.fl)_ri:n.f:!_d_.....
- \\<fethocl Dc~criptio11 Dry Soil Prep Dry Soil Prep GL-RAD-A-021
+f-0.109 +1-0()4()1 +f-0.111 <-i-0 127. +/60202 +/-1.41 "'-/-0.559 +/-0 132 +/-11277 +1-0 0871 +/-0.139 +/-3 57 +/-2.73 1:he. (~11!>.'"..i.n_g ~!l_a.t;r-t~~--~~~t_!J~~-s w~_rc pcr.form_ed..... --**-* Method Description ASTM D 2216 (Modified) 2 DOE 1-IASL 30(). 4 5 2 J!Ga-0 \\-R 3 EPA 900 OISW846 9310/SM.711013 Modified Surrog:itcffraccr Recovery Test perccnl. CXCl 11110!15 1319 1521842 OA6S o.:m +1-0.244 pCilg RAF2 12103/15 1305 \\522383 2 0.177 00815 +1-0 101 pC'i/g 1.21 0 561! +/-0.994 pC1/g 0l11 0 0499 +/*O 147 pC1fg 0.0739 (J 0336 H-0140 (} 100 pCilg 0 0765 0 033 +/-0,0402 pC1/g 0.211 0.0\\114 +/-(I 111 pCi/g 0.11 l 0 0522 +1-0.161 pCi!g 0.137 0 0635 +/-0.21 'J pC'i/g 0.5.81 (!:238 +/-I 81 pCi/g ll.891 0416 +/-0 586 p('1/g IJ.\\11 0 0499 +/-0 147 pCi/g ll263 0.\\17 +1-0.317 pCi/g U.0669 0 0304 +1-00913 pC!lg 0 133 0 0634 +r-0 141 pC1/g 383 1.68 +1-4 57 4.00 p('1!g KXB2 12i02/l 5 1120 1525757 3 313 1.48 +l-3 9() HJ 0 pC1/g Analyst C"XC! Oatc 11110!15 Time Prep Batch 1319 1521842 Batch ID Rcconry% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 * (843) 556-8171 -www.gel.com Company: Address:
- MJW Corporation 15 Hazelwood Drive Suite l 12 Buffalo. Nev.* York 14228
Contact:
Ms. I.auric Losey Project: Soil Rndioiso!opcs Client Sample ID:
- 3. l.19.R.1 Sample ID:
385070013 Surragatcffraccr Recovery Tc.st Notes: Certificate of Analysis Report Date: December 17, 2015 Project MJWCOOl 15 Client ID: MJWCOO l i.c ...1J'.F _.. __.)3-:L..... ~!f!it~... f?.F __ AJ111ly~t _._!)ate_ :_fin,ie _Batch.. ~i_t~.. Batch ID Rcco,*ery% Acceptable Limits TPU and Counting Uncertainty are calculated at the 95% confidence level (\\.96-sigma}.
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.19.R. I Sample JO: 385070013 Matrix: Soil Collect Date: 20-0CT-15 Receive Date:
- 05-NOV-l 5 Collector:
Client Moisture: 19.9% Certificate of Analysis Project: Client ID:
- Repon Date:
December 17. 2015 MJWCOOl15 MJWCOOl l'aramctcr .... 9_u_l{l_i_~C.~...... _l_l~~IJl.t.......l'.!l.ccr.~l!i!!!'I'...... MDC' J,c* TPl' RL l'.nits DF Anah*st Date Time Batch Mtd. Gravimetric Solids ASTM D 22!6 % Moisture "As Receired" Moisture ! 9 9 Rad Gamma Spec Analysis Gammaspec. Gamma, Solid "D1:r Weight Corrected" Acttnium-227 U -0 ()0874 +/-0.244 Antimotl}' 125 U -0.0461 +l-0.0992 Bismuth-212 lJI 0 00 +/-0 746 Bismuth-214
- 0. 77~
- +/-0 132 Ccsium-13 7 1.07
+/-0 l09 Cobalt-60 ll -0 00812 +/-0 040 I Europium-154 ll
- 2. 92E-05
+1-0 111 Lead-212
- 1. tQ
+r-0.127 J.cad"2 I 4 O 970 +i-0 202 Potassnnn-40 Prot.actinium-23 I Radmm-226 Rad1um-22K Thal11um*208 Ul 129 0.00 0779 I 02 0 325 Tin-f26 UI 000 Rad Gas Flow Proportional Counting GFPC. Gros.~ A.B, solid "Di}' Weight Cm-reeled" Alpha 14 7 Betn 199 T~c.__f~_H!J.Wi_n_g_!.'r.c.l! ~'.l_l!~_~fld_s_1v.crc _pc~fo_rr11c_(~.. Method Description +/-1.41 +/-0 55'9 +/-0 132 +/.() 277 +/-0 0871 +/-0.139 +1-3.57 +/-2 73 0468 0 177 121 0 Ill 0 0739 0.0765 0 21 l 0 Ill 0.137 0.581 0 89! ()Ill 0 263 00661} 0133 3.83 3 13 0.219 () 0815 0 560 0 049') 0.033{i () 033 0 0914 00522 0 0635 0 238 0416 U.0499 0.117 00304 00634 1.68 !.\\8 +f-0 244 +/-0 10 I +/-0.994 +1-0 147 +/-0 140 +/.Q.0402 +/-0.111 +/-0.161 +/-0.219 +/-1.81 +/-0.586 +i-0.147 +/-0 317 +/-0.0913 +/-0 141 +/-4 57 +J.J. 9ll Analyst Date percent CXCl 11/10115 1319 15218*12 pCil£ RXF2 12/()3/15 l:i05 1522383 pC1/g pCi/g pCi!g 0 100 pC1/g pCr/g pCilg pCilg pC'l!g pCi/g pCilg pCi/g pC1/g pC1lg pC1/g 4.00 pCilg KXB2 12f02fl5 1120 1525757 10.0 pCi/g Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-02 ! CXC I I l/!0115 1319 1521842
- r~.e..!o_ll~~\\'iJl~.i\\lla!~*ti~~l.l\\'l_i:.t~.o~.~-'Y.crc: pc..rfl!rll!~?................. _...... _
Method Description ASTM D 2216 {Modified) 2 DOE llASL 300, 4 5.2 31Ga*01-R 3 F.PA 9ll0,0!SW846 93 l O!SM 71 IOD Modifi~d Suuogatcffrace1* Recovery Test Batch [D Rec1>~*cry% Acceptable Limits 2
GEL LABO RA TORJES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company: Address: MJ\\V Corporation 15 l-laz.c!wood Drive Suire! 12 Buffalo. New York !4228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.19.R.1 Sample ID: 385070013 Surrog;iteffracer Recovery Test Notes: Certificate of Analysis Reporl Date: December I 7. 20 l 5 Project: MJWCOOl 15 C'lient JD: MJWCOOl Ml)C_.. Le TP.l:. .... R_l'... l*~!.t~.... D..F... ~~~:ilY~~-- -~~~~.Tl_i~e __ ll._:t_t~_l_1 ___ ~1t~:- B11tch ID Recovery% Acceptable Limils .TPU and Counting Uncertainty are calculated at the 95% confidence level (I.96-sigma).
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com
- Certificate of Analysis Company:
Address: MJW Tt::chnical Services 15 Hazelwood Drive Suite I !2 Buffalo. Ne"v York. 1,1228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample JD;
- 3. L 19.R.2 Sample ID:
389296014 Matrix: Soil Collect Date: 20-0CT-l 5 Receive Date: 14-JAN-I 6 Collector: Client Moisture: 2"1% Parameter ...... Q~ali!fo.r:... Hcsult __ J'.1_1ser_1~in_tv.. MDC Le Grm*imctric Solids ASH-! D 2216 % Moisture "As Rf!ceiwd" Moisture 21.0 Rad G:1mm11 Spec Analysis Gamma with Ingrowth '1D1y Weight Corrected" i\\ctinmm-227 u 0 0926 +J.()307 0 597 027M Antimony-125 u 0.060
- r/-0 138 0 266 0 122 Bismuth-212 Ul 0 ()()
+I-I 19 l.78 U.827 Bismuth-214 0722 +!-0 197 0 175 !i.0794 Cesium-137 146 +/-0 l52 0.0917 !) 0411 Cobalt-60 u -0.0033 +/-0 0361 0.0752 00299 Europium-154 t: 0 0518 . +/-0.163 0.339 0.149 Lead-212 0.818 -~/-0231 0.157 0074 l.ead-214 I 22 +/-0207 () 391 (l 189 Pota>smm-40 13.7 +/-1.74 0.721 0 285 Protactrnium-231 u -0.00463 +/-0.664 I 16 0537 Radium-226 0722 +/-0197 0 175 00794 Radium-228 1.19 ... 1.0 267 0 344 0 \\52 Thal11um-208 OJJS +/-0 105 00929 0 0422 Tin-126 L'l [)[)() +/-0 134 ll 2()0 ll.0945 Gammaspec. Gamma, Solid "Dry Weight Corrected" /\\ctinium-:Z27 u -0.116 +*l-027\\l 0,498 0.233 Antimony-125 u -0 00536 +l-0119 0.214 0099 Bismuth-212 l!I 0.00 +/-0 8 ]() 129
- O 599 Bismuth-214 0.849
+1-0161 0 124 0.056 Ccsmm-137 I 51 +/.() 129 0 ()771 0 035 Coball"-60 L~ (l.0135 +i-0 035 0.0755 0 !l321 E~roptum-154 L' -0 !08 +J-0 104 0 166 () 0679 Lcail-212 1.17 +1-0 131 0 126 () 0594 Lead-214 0.%7 +/-0 IB6 () 160 0 0747 Potassrum-40 14Jl
- 1-l 58
() 7ltl 0.300 Protactimmn-231 ll! 0()0 +/-0912 (1923 0429 Radium-226 O.S49 +/-0.161 U.124 () 056 Radiurn-228 0 898 +J-0 347 0.286 0 !28 'lltallmm-208 0 222 ... ;.o 0855 00724 () 033 Tin-126 \\JI 0 00 +/-0.120 0 154 0.074 Rad Gas l<low Proportional ('ounting GFPC. Gross..i:e. solid "Dry TVeighr Corrected" Alpha 7 32 +f-3.21 J 70 147 Beta 17.8 +f-3.00 2.86 us JPt: t/-0 310 +/-0.140 +/-1.47 +/-0.206. +r.o 193 ~1-0 ()361 +/-0. \\65 +/-0.242 .;./.() 232 +1-2 (19 -r/-1) 664 +i-0.206 +/-0.3()9 +/-0 JOB +l-0.135 +/-0 285 N-0 I l'J +/-0.953 +/-0 176. +/-0 181 +/.() 035(> +/-0.) 16 +!-0.173 +/-0.205 +/-2 02 +1-0.966 +/-0 \\76 +/-037! +f.() 0875 ..-/.(). 121 +/-3.51 +l-3.95 Report Date: February 10, 2016 Project: Client !D: MJWCOOJ IS MJWCOOI percent CXCl Ol/!4116 1208 1537312 pC1/g RXF2 O'.!ill5116 0856 1537546 2 p<.'1ig p('i/g pCilg 0 100 pCl!g pCLlg pCi/g pCilg pCiig pC1/g pC1lg pCifg pCt!g pCifg pC1/g pC1/g RXFZ O 1!!8116 1124 1537545 3 pC1/g pCi!g pC11g 0 100 pC1/g pC1lg pC1lg pC1lg pC1lg pCi/g pCi/g pt't/g pCiig pCilg pC'i!g. 400. pC1/g KX132 01126116 1215 1~39462 4 10 0 pC1lg
Company: Address: GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-6171 -www.gef.com ~JW Technical Services 15 llrrzclwood Ori ve Suite 112 Certificate of Analysis Buffalo. New York 14228 Report Date: February I 0, 2016
Contact:
(\\fa Laurie Losey Project: Soil Radioisotopes Client Sample ID;
- 3. l.19.R.2 Sample ID; 3892960!4 Project:
MJWCOOI15 ClientlD: MJWCOOl . L~.. _........ -** :rPl' RL l'nils DF Anah*st Date Time Batch Mtd. The foH()'~ing Pr.ep.Me_thod_s.'v.ere_p(!r!or_med..... *-******.. -*-........... *-*-**** ---*-.
- 'Vlcthod Description Analyst Dry S01l Prep Dry Sotl Prep GL-RAD-A-021
!h.~ follo~i1_1g ;\\[]!llY._l_ic_al ~J.~tl1ods '~c.r.e_per.f.1.>~llled............. _.... Method . Description 2 3 4 ASTM D 2216 (Modified) DOE HASL 300. 4.5.2 3iGa*Ol*R DOE !IASL 300, 4.5.23/Ga-01-R EPA 900.0ISW846 93J01SM 71 IOB Modified Surrogateffracer RccO\\'Cry Test Notes: C'XC'l Date Ol/14ito TPU and Counting Uncertainty are calculated at the 9~% confidence level (I.%~sigma). Time Prep Batch 1208 1537312 Butch ID Reco\\*cry% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8i71 - www.gel.com Certificate of Analysis Report Date: December 4, 20 ! 5 Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes .. ~. Client Sample ID: 3.1.20.R.l Project: Sample m: 385070014 Client ID: MJWCOOIJS MJWCOOJ Matrix: Soil Collect Da1e: 20-0CT-15 10:00 Receive Date: 05-NOV-15 Collector: Client Moisture: 17.1% Param~ter............... Qu~li~er__ Resul~... !Jn~erlai.nty...... MDC RL Units Gravimetric Solids ASTM D 2216 '%Moisture "As Received" M01sturc 171 percent Rad Gamma Spec Analysis Garnmaspec, Gamma. Solid "Dry Weight Corrected" Actmrnm-227 u -0.0414 +/-0 268 0.502 pCi!g Antmrnny-l 25 u 0.0855 +/-0.0966 O I% pC1/g Cestum-137 0.414 +/-0 089 0 0777 0.100 pC1lg C'obalt-60 lJ O.OlM +/-0.0362 0.(}78 pCi/g Europmm-154 u 0.0284 i'/-0.128 0 256. pC1/g Protactmium-231 l! I) 326 +1-(H507 I) 92l pC1/g Radium-226 0 8J3 +/-0. 172 0 143 p(i!g Rfldimn-228 I 03 +/-0.249 0234 pC1/g. Tm-126 u ll 157 +{.() 123 0162 pCilg Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dt)' Weight Corrected Alplm 15 I +1-34lJ 3.10 4 0() pCi/g. Beta 2!6 +/-2 76 3.03 10 ll pCi/g }h!;!_f()l!ow_in.&.P.rep. Nf.C.t.l~<?d~.\\~~r.e.. re.r.f.oti~.ed._:.....
- Method Description Dry SO"!i"Prep*.. -...... - --.. ****- bf): 'SOl(PiCP Ci1.-RA"D~~,-~Oif"....
Analyst Date
- ******exec* **** -*** ** *Yi1ioi1s
!.h..c ~ol_l°..~V..i~~. ~-~":!~~ic.a.l __ ~e!h~~s. \\V~r~.. P..~~~()r,~1~d.'.. DF Analyst Date Tiine Batch Method CXCl 11110/15 1319 1521842 RXF2 12103115 1305 1522383 2 KXB2 12/02115 112(). i525757 3 - Time ... 6i9... Prep Batch 1521842"............................... *********- . M.et.h_o~!.. __.... _........... P~!>.c~*ip_t.i.9!1.. ASTM 02216(Mod1ficdJ ............. _.................. A'.1-a.l_y§~--~on11Jle.nt§ 2 DOE HASL 300. 4 5.2.3.'G~-01-R 3 EPA 9000/SW846 9310.iSM 71 l()B Moo1fied Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - WW\\'1.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.20.R. I Sam!?le 10: 385070014 Matnx: Soil Collect Date: 20-0CT-15 Receive Date: 05-NOV-15 Collector: Client l\\.foisturc: (7. [0/o Project: ClientlD: Report Date: December 17. 2015 MJWCOOl 15 MJWCOOJ Parameter
- - _ 9_u_~li~~~~-
... Re~u~t.. _ _.l'nccrl11i1_1ry_.... Mf>.C.. ~c........ TP.l_!.... _____ RL __ yn_i~~..-!?.!.'... *~.1:1~.lp~. ___ fJ.J!.l': __ Ti.'!lc jlatch.. ~ltd.. Gra\\*imetric Solids AST/14 D 1;! I 6 %.Hofstwe .,Is Received" Mmsturc 17 I percent CXCI l \\110.115 1319 1521S42 Rad Gamma Spec Analysis Gammaspec, Gamma. Solid "DI)' Weight Corrected" Actimum-227 ll
- 00414
+/-0 268 0.502 0 235 +!-0 269 pC1!g RXF2 12103/15 1305 1522383 .2 Anlimony-125 u 0 0&55 +/-0.0966 0.1911 0 0903 +/-0.104 pCi/g !31smuth-212 lJ[ OOll +/-() 844 I 24 0 569 +/-I.OS pC1/g Bismuth-214 fl.833 +/-0 172 (J.143 () (1653 +/-0.186 pCilg Cesium-137 ll414 +/-0 089 0.0777 I) 0353 +1-0.0953
- 0. !00 pCi!g Cobalt-60 u
()()164 +/-0.0362. 0 078 0.0334 +/-0 037 pCt!g Europium-I 54 u 0.0284 +/-0 128 0 256 0.113 -+1-0.\\29 pCi/g Lcad-212 I 02 +/-0.137 (1.128 0.0607 +/-0 161 pCi/g Lcad-214 I 00 +/-0 211 0.326 u 157 "-/-0 227 pCi!g Pmassiuin-40 12 5 +/-1.39 (l.685 0.287 +/-1 78 pCt/g Prorncunium-231 u 0.326 +/-0 607 0 921 0429 +/-0.6\\1 pCt'g Radium-226 !J.833 +1-0.172 () 143 0 0653 +/-0.186 pCi.lg Radium-228 1.03 +/-0 249 0.23-1 [) 102 +1-0.293 p(\\lg Thallium"208 0.309 +/-0.0722. 0.0634 0.o2.&5 +/-1).0768 pC1/g Tm-126 U! (){}() +/-0.123 0 162 0.0776 +/-0.124 pCtl(l. Rad Gas Flow Proportional Counting OFPC. Gross AB. solid "Di:p Weig/rt Corrected" Alpha 15 l +-1-3 49 3 \\0 I 30 +/-4 57 400 pCilg KXB2 12102.ll5 1120 1525757 3 Beta 216 +/-2.76 3 03 I 43 +/-409 10.0 pC!lg T~c fo!l1m_i_11g_Prcp ~C.!h!Jlls. \\\\'l!".t! per.!<<>.~.~cd.... .Ylctlrnd Dcstription Analyst Date Time Prep Batch Dry Soil Prep Dry Sl11I Prep GL-RAD-A-021 CXC'I 11110!15 1319 1521842 The followiug Analytical Methods were performed ~.f~iii~x*****---*******-ocsci:il>'tioii.... * * **** * ** * *** * *** * * ****-- ASTMD 2216 (Modified) 2 DOE I !ASL 300, 4 5.2 3/Ga-Ol-R 3 EPA 900.0/SW846 93 !0fSM 71 lOB Modifie\\l SurrogatcJT1*acer Recovery Test Batch ID Rcco1*ery% Acccpt~blc Limits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company:. Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID;
- 3. l.20.R. l Sample ID:
385070014 Certificate of Analysis Report Date: December 17, 2015 Project: M.TWCOO t 15 Client ID: MJWCOOI Parameter Result.....,t:_n~~f!:ti.11fy....... !\\:~i:l,~. L~............ '.fl~L _..... R1-:.... r.~~.rs... D_F,~_11aly~t.... ~~t~ _Time. B.at~~.. _:vl_td. Surrogateffracer Rccm*ery Test Batch ID Recovery% Acceptable Limib Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level (!.%-sigma).
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843} 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 Hazelwood Drive Suite ll2 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample JD: 3.1.20.R.1 Sample ID: 3850700 l 4 Matrix: Soil Collect Date: 20-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 17.!% P.ar_aI!l_e~cr...... **-*-*. _9_1111_lificr_..... Result *.. r11_c_~rt.:1.in.tv_. Gravimetric Solids ASHf D 2216 % Moisture "As Received" Mo11;1urc
- 17. 1 Rutl Gamma Spec Analysis Gammaspec, Gamm(/, Solid "DI'.\\' Weight Correcled" Actinium-227 U
-00414 +/-0 268 Anltmony-l 2.5 lJ 0 0855 +/-0 0966 l31smuth-212 Ul 0.00 +/-0.844 Btsmuth-214 Cesmm-137 Cobal!-60 Europium-154 Lead-212 l.cad-214 Potassium-40 Protacllnium-231 Radmm-226 Radium-228 u v u 0.833 0414 (l".()\\64 0.0284 1 02 I 0(1 12 5 0326 0.833 l 03 +!-0 172 +/-0 089 +/-0.0362 +/-0.128 +/-0.137 +/-0.211 +!-\\ 39 +/-0607 +1-0 172 +1-0 249 Tlrnllium-208 0.309 +/-0.0722 Tm-126 Ul 0.00 +/-0.123 Rad Gas Flow Propmiional Counting GFPC. Gross A.B, solid "Dry Weight CorrecJed" Alph~ 15 I +/-3.49 Beta 21.6 +/-2.76 !l~e f.~~~:".i'~-~ ~r~.P. -~~11~o~S... '~:e~e _P.~!"forrnc~.- Methot.I Description Dn* Soil Prep DJ)' Soll Prep GL-RAD-A-021 Tl1~ f!Jlll):'!il_l~,\\nal~*~ica_I_ ~~t~llJ.~:~. ~~c~_c. _p_erforrne_d_
- \\lcthod Description ASTM D 2216 (Modifi~d)
DOE HASL 300, 4 5.2 3/Ga-01-R 2 3 EPA 900.0tSW846 9310.'SM 71 IOB Modified Surrogatc!fracer Recovery Test ~IDC 0.502 () 1% 1.24 () 143 0.0777 0078 {) 25(> tl 128 I) 326 (l.b85 ri921 ll.143
- 0.234 0 OC>J4 ll.162 3 10 3 03 Le 0.235 (l 1)9()3
(} 569 G.06D 0 0353 0.0334 0.113 0.0607
- 0. 157 0187 (J.429 00653 (J !02
{10285 0.0776 l 30 1.43 Analyst CXCl Report Date; December 17. 2015 Project: Client ID: MJWCOOJ !5 MJWCOOI TPl: RL per~cnl CXCI 11110115 1319 1521842 +{-() 269 pC1/g RXF2 12.103115 1305 1522383 2 +/-0.104 pC1lg +/-l.08 pCi/g +/-0.18.6 pCilg +/-0.0953 0 100 pCilg +/-ll.037 pCi/g +/-ll 129 pCi/g +/-0 161 pCi/g +/-0 227 pC'1/g +/-\\.78 pC'1/g +/-o.611 pCi/g +/-0 186 pCilg H-0.293 pCilg +/-0 0768 pCifg +l-0 124 pCi/g +J-4.57 4.00 pC'1/g KXB2 l2i02/15 1120 !525757 3 +/-4 09 ]{) 0 pCi!g Date Time Prep Batch 11/10115 1319 1521842 Batch TD Recovery% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company: Address: MJW C{lrporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey Prqject: Soil Radioisotopes Client Sample ID: 3.1.20.R. ! Sample ID: 385070014 Sul'rogate!fracer Recovery Test Notes: Certificate of Analysis ~me Le TPU TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma). Report Date:
- December 17. 2015 Project:
MJWCOOl 15 Client fD: MJWCOOJ RL.... ~'11.its_.. ~f..;\\11al~:sr_ .~a.~e.}'in~~._B.at.i:I~.. ~~t<i-. Batch JD Recovery% Acl'cpfable Liniits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 ~ www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228
Contact:
Ms. Laurie Losey ....... ~.r?.i.~ct: ..... *-- ~?ll __ ~~~ioisot?P_()_S..... Client Sample ID: 3.1.21.R.l Sample iD: 385070015 Matrix: Soil Collect Date: 20-0CT-l 5 14:30 Receive Date: Collector: Moisture: 05-NOV-!5 Client 19.5% Parameter.......... -*....... Qualifier Result .l1-~~~ert~int_y Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 19.5 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Con*ected" Actmium-227 l! 0 181 +/-0.316 Antimony-125 lJ -0.0507 Cesmm-137 0.824 Cobalt-60 U -0 00202 Europium-154 U 0 0258 Promcumum-231 U 0 232* Radium-22(> 0.649 Radirnn-228 0.857 Tin-126 U 0 139 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid Dry Weight Con-ected" Alpha $.73 Beta 23 0 +/-0 I !3 "+/-0.112 +/-0.038 . +/-0.163 +l-0.665 f/-0.195 +1-0403 +1-0127 +/-2.97 +1-3.05 ~li_e.f?ll?..W._i~~.. Pr_~P..~~eth~~.s.~V.~.r.~ p~rron.1:ed..:........ Method Description o~:*sail Pier*** -- ***-**** **- ***Di)* *sori°i'reiiCiCR:A:o-X~O:ii ***
- _T~.e f(.ll_~o:¥i_n~.'..\\n~t.?.ti.~~l.l'vfet_ho.ds were perfo_r1~.~~:.
Mt:th9~........................ P..e~!'.r.iptio.n....... I ASTM D 2216 (Modified) 2 DOE HASL 300, 4.5 2 3iGa*Ol*R 3 EPA 900.0/SW846 9310/SM 711013 Modified Project: Client ID: MJWC00\\15 MJWCOOI MDC RL Units DF Analyst Date Time Batch Method Of>O I 0 206 0.086 0.0739 0.272 1.09 0 161 0 270 0.171 365 J.31 0 100 4.00 IO.O Analyst (;)((:"1. -..... percent CXCI I l/10/J5 13!9 1521842 pCtig RXF2 !2i03/l5 1321 1522383 2 pC1/g pC1ig pC1tg pC1/g pCi/g pC1/g pCilg pCi/g pC1/g KXB2 1210211 S 1123 1525757 3 pCi/g Date Time Prep Batch 11110/!5
- y319-*** -15:ii842...... ***-**-*-**....... -*** -*....
. -**.. A.na~y~.\\(pn1rn~!J.I§.... **--*-***... Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
Company: Address: GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 -www.gel.com MJW Corpora1ion 15 Hazel\\l:ood Drive Suite 112 Certificate of Analysis Buffalo. New York 14228 Report Date: December 17. 2015
Contact:
Ms. Laurie Losey . Project: Soil Radioisotopes Client Sample ID: 3.1.21.R.1 Sample ID: 385070015 Matrix: Soil Collect Date: 20-0CT-l 5 Receive Date: 05-NOV -15 Collector: Client Moisture: 19.5%
- rar:tmctcr Result Le Project:
Client ID: MJWC00ll5 MJWC001 RL l'nits Dale Time Batcb Mtd. 9~~1.lifi~.~... Vncc.rt:1i1)~..... :\\-WC.............,..,....... IPI.............. *******************. .P..*~.'\\.~jjlyst................. Gravimetric Solids ASIM D 2216 % Moistw*e "As Receiwd" Moisture 19 5 Rad Gamma Spec Analysis Gamma.vpec. Gamma, Solid Di:r Weigh/ Correctl!d" Actinmrn-227 u 0.181 +1-0.316 Anlimony-125 u -0 0507 +1-0 113 Bismuth-212 lJ 0.427 +/-0.688 Bismuth-214 0 649 +/-0. 195 Ccs1um-l37 0.824 +f-0.112 Cobalt-60 u -() 00202 +1-0 038 Europrurn-154 u 0.0258 +/-0.163 Lea<i-212. \\.33 +-1-'J 146 Lcad-214 0.942 +/-0 189 l'olassium-40 13.0 +/-1 41 l'rotactmium-231 u 0 232 +/-0.665 Rµdium-226 0.649 +/-U.195 Radium-228 0 857 t-/-0 408 Thalltum-208 0 257. +/-Q.0(l92 Tfn-126 Lil 0.00 +/-0 127 Rad Gas Flow Proportional Counting GFl'C, Gross A,B, solid "DI'.\\! Weight Corrected" Alpha 8.73 +-1-2 97 Beta 23.0 +/-3 05 Th..~ ~ul1o\\l*ing:.. f..~cll ~J.e.~lt~ds ~~e.r~ pc~~IJ.~~i.e_d.. l\\*lethod
- Description D.ry Soil Prep Diy Soil Prep GL-RAD-A-021
!_hc_~0Ho,~*i.11g_A.na.ly_tic~.l-~*!~.t_b_(_)_~s. u:i:re p~r_f~:r111c5l.... Method Description I ASTM D 2216 (Modified) DOE HASL 300. 4.5.2 3/Ga-01-R 2 3 HPA 900.(J/SW846 93l01S1'17110B Modified Surrogaten'racer Recovery Test percent CXC! 11/10115 !319 1521842 0.601 0 284 +/-0,327 pC"tlg RXF2 12103fl5 \\321 1522383 2 0206 0 ()954 +/-ll. 115 pC1fg 1.33 0.618 +/-0 715 pCifg 0 16\\ 00742 +/-0.202 pC1!g 0086 0 0394 /-0 130 0.100 pCi!g 0 0739 0.0315 +/-0 0381 p('i/g 0.272 (J 121 +l-0 163 pCi/g 0.125 00591 +J-0.182 pCi/g 0.164 0()768 +/-0.204' pCi/g 0 449 {1170 +/-I 79
- pCi/g 1 (!<)
0.515 +/-0 675 pCi/g 0 'hi ll0742 +/-Cl 202 pCs!g 0270 0 120 +/-0424 pCi/g G.0679 0 0307 +/-0 0724 pCilg
- o. 171 G.0821
+/.(l !29 pCifg 3 65 1.59 +/-141 400 pC1/g KX.B2 12roi11s 1123 1525757 3 3.31 155 +1-4 40 10 [) pC1/g Analyst Date. Time Prep Batch CXCl 1 \\1101!5 131'l 1521842 Batch ID Recovery% Ac~eptable Limits. --1
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -WW\\V.gel.com Company: Address: M.TW Corporation I 5 Hazelwood Drive Suite l 12 Buffalo. New York 14228
Contact:
Ms. Laurie'Losey Project: Soil Radioisotopes Client Sample ID: 3.1.2 J.R. l Sample lD: 3&5070015 Ce11ificate of Analysis Report Date: December 17. 2015 Project: MJWCOOl !5 C'lient ID: MJWCOO l l'arameter. _....... _..... 9u.~1Jfi~r. Result ...l: 11cei:tain.tv_ . ~!D<::......l:*c..... _. TPl'..... ~l~.. l.!.nit_s..... _DF.. !'\\".llh~.t-. _,i?.?.t~.~.iJl1l!. _:tl.atc~.. :\\:It~~. Surrogatcffraccr Recovery Test Batch ID Recovery% Acceptable Limits Nutes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma). \\
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843} 556-8171 - www.gel.com Certificate of Analysis Company: Address: MJ\\V Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample JD: 3.1.21.R. l Sample ID: 3850700 l5 Matrix: Soil Collect Date: 20-0CT-15 Receive Date: 05-NOV-l S Collector: Client Moisture: 19.5% Parameter Gravimetrie Solids ASTM D 22./6 % Moisture "As Received" Mmsturc Rad Gamma Spec Analysis ('} 5 Gammaspec, Gamma, Solid "Dry Weigh! Corrected" Actinium-227 U 0.181 +1-0 31(> Antmtony-125 U -0 0507 +/-0 I 13 Bismuth-212 lJ 0.427
- +/-0,688 B1smuth*2 l 4 0 649
+/'.0.195 Ccsium-137 Cob~ll-60 Europ1t1m-l 54 Lead-212 Lcad-214 Potassium-40 Protactinium-231 Radium-226 Hadium-228 lJ u LI 0 824 .Q 00202 0.02:58 l 33 ().942 13.0 0 232 0.649 0 857 +/-0.112 +/-0 038 +l-0 163 +f*O 146 +1*0 189 +/-1 41 +/-G.665 +/-0.195 +/-0 4()8 1l1al hum-208 0 257 +J-Q. 0692 Tin-126 lJI 0.00 +/-0 127 Rad Gas Flow Proportional Counting GFPC. Gross A.-'B, solid "D1:v 1feighl Cnl"l"ected" Alpha
- 8. 73
+/-2 97 Beta 23.0 +1*3 OS }'~-~ f11ll~m:i11g.. P.rep ~~e.~~-°-~s _,v~r..~ per:~o.'.mC!.d... Method Description Le 0.601 u 284 . 0 206 0 0954 1 33 0.618 () 161 0 0742 0 086 0.0394. 0 0739 (I 0315 o.:m o 121 0.125 () 0591 0.164 0 0768 0 449 0 170 1 09 0.515' 0!61 00742 {) 270 0 12() 0.0679 0.0307 0.171 0.0821 3 65 l.59 3 31 1 5.5 Analyst Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI
- rh_c_foll.o\\vi.ng.~.na.lr..t!~a.!.. l\\!e_t_~~ds.'.".*.cr.e.r.erfo~lll~.~.. -.
Method Description ASTM D2216 (Modified) 2 DOE !!ASL 300. 4.5.2 3/Ga-0\\-R 3 EPA 900.0!SW846 9310/SM 71 lOB Modified Surrogate!rracer Recovery Test Project: Client JD: Report Date: December 17, 2015 MJWCOOll5 MJWCOOl TPC...... ~-.1,*.... l'11its....DF Analyst l)a.te_.~l}_i_nc Batch Mtd. +/-0.327 +/-0 115 +/-0 715 +/-0 202 +1-0 130 +/-0.0381 +/-0 163 +/-C).182 +/*ll.204 +l-1.19 +f-0 675 +/-0 202 +/.() 424 +/-0.0724 +/-0 129
- rl-3 41
+1-4.40 Date percent pC1/g pCi/g pCi/g pCtlg O 100 pCilg pCilg pCitg rC'if~ pCiig
- pC1/g pCi/g pCtfg pCifg pCi/g pC1lg 4 00 pCilg 10.0 pCtfg Time CXCI 111\\0f\\5 1319 1521842 RXF2 12103115 1321 1522383 2
KXB2 12i02/15 1123 1525757 3 Prep Balch l 1110!15 1319 1521842 B:iteh II) Rcco\\*ery% 1\\cccptablc Limits
GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171-www.gel.com Company: Address:
Contact:
MJ\\V Corporation 15 Hazelwood Drive Suite l 12 Buffalo. New York 14228 Ms. Laurie Losey Project: Soil Radioiso1opes Client Sample ID: 3.l.21.R.I Sample ID: 385070015 Certificate of Analysis Report Date: December 17. 2015 Project: MJWC00! 15 Client ID: .MJWCOO I Parameter .... t:Jn.~uri~.r.... Result l'nccrtain.~v..... ~!l.C.:....... Le TPl~ R.~*. l,!n~ts.. [)F_ An:1_lyst. D_a~.. !i111e ~at~l.1_ --~-~~~ Surrogalc{fraccr Recovery Te~l Batch lD Recovery% Acceptuble Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: Address:
Contact:
Project: MJW Technical.Services 15 l lnzclwood Drive Suite l 12 Buffalo, New York 14228 Ms. Lamie Losey Soil Radioisotopes Client Sample ID: 3.1.21.R.2 389303001 Soil 20-0CT-15 14-JAN-16 Client 20.5% Sample ID: Matrix: Collect Date: Receive Date: Collector: Moisture: raramet~.r..... *-*........... 9.':1;tli1:ier..... Result _ l!_n(!e.rt:i.i11.t.Y. . ND..C Gravimetric Solids ASTM D 2216 % Moiswre "As Received" Moisture 20 5 Rad Gamma Spec Analysis Gamma with lngrow1h "Dry Weighr CorrecNd" Actmium-227 u -0 128 +/-0 236 () 430 Anumony-125 u -0 127 /-0 111 () 181 B 1smu1h-2 I 2 lll (1.00 +/-U.887 I 50 Bismulh-214 0 733 T/-0 167 ll.145 Ccsium-137 I 24 +/-0 122 0.0765 CobalL-60 u -!J.(J3S +/-0.0351 0.0529 Europium-154 u 0 0486. +/-0.139 0.259 Lcad-212 1.07 <*/-ll l !6 o.rnn Lead-214 0.9()8 +/-{! 14& 0.153 Po1ass1t1m-40 12.3 +/-14*1 0.6&1 Protacumum-231 1.05 .,./-0 787 0.841 Radium-226 0 733 +/-0 167 0.145 Rodium-228 0 835 +/-0.307 0.224 llialhum-108 0 309 +/-0.0688 0.0771 Tm-126 UI 0.00 +l-0 131 OllJ Gammaspec. Gamma. Solid "D1:1* Weight Carrected" Acnrnum-227 u -00269 +/-0.308 I} 569 Antimony-125 lJ 0 0419 +/-() 135 (l 254 Bismuth-212 UI 0 00 +/.() 938 1.39 Bismuth-2\\4 0.824 +/-0 185 0.166 Ccsimn-131 l.02 +/-0 153 0.!00 C<Jbalt-60 u -0.026 +/-0 0503 0 [)'}28 Europmm-154 u
- O 0303
+/.() 129 0.251 Lead-212 0917 +/-0 134 0 136 Lcad-214 0 875 +/-0.182 0.342 Potass1 um-40 11 8 +/-I f.7 0 71)\\ Protaclinium-231 L; 0202 +l-0(18tl 1.14 Radium-226 () 824 +/-0.185 0 166 Radium-228 0769 +/-0.313 0.333 Thallmm-208 0 3211 +/-0.0958 () 0754 Tin-126 u 0.0757 +/-0 192 I} 232 Rad Gas Flow Pruportional Co1mtini: GFPC Gross.4.-B, solid "Dry Weigh/ Corrected" Alpha 13.3 +/-4 lll 3.78 Beta 24 l t-/-3.57 3.40 Le 0.199 0.082.5 0699 006:"1 OOH5 0.0206 0.114 0 0469 0 WI! I (} 2&3 (/J89 ()0659 00964 {) 0353 ().0543 0265 0117 ne.3o 00745 0.0454 0.0389 () 105 OOM 0 164 0271 {) 53l 0 0745 () 146 0.0334 0.111 I 52 I 55 Project: Client ID: Report Date:
- February IO, 2016 MJWCOOl 15 MJWCOOI
......TP.l'..... _ ~~... ~'.n~_ts_ *-I>.~. l\\na_lyst_ !lat.c. _Jim_e_.. B..at1:_h.. M_td. percent CXCI 01/14/16 1202 1537321 +/-0244 pC1/g RXl'2 02/05116 0641 I 537551 2 -<-/-0.126 pCLlg +t-1 25 pC1/g +/-0 178 p('i/g +/-0 157 0 HIO pC1/g +/-00391 pCilg +/-0.141 pCilg +l-t\\.185 pC1.lg +/-0.172 pCi.lg +1-1.81 p('1!g +/.[) 815 pC1!g +/-0.178 pCilg +1-0 333 pC1/g +/-0.0737 pC1lg +J-0 131 pC1/g +1-0.309 pCi!g RXF2 01/18!16 0935 153754& 3 +/-0 136 pCi/g +/-1 01 pC1/g +/-0.197 pCilg +!-0 174 0 100 pCiig /-().0518 pC1lg +/-0 130 pC1/g +/-0.155 pC'ilg +/-0 194 pC'1/g
- 1-2 05 pC1!g
+/-0.688 pCi/g +1-0.197 pCilg +/-0.327 pCilg +/-0.0996 pCilg +/-0 J<J3 pC11g
- l-4 77 400 pCi!g JXB7 Ol/26!16 1140 1539464 4
"-/-..\\ 94 100 pC*ig
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-817"! -Ww\\v.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.21.R.2 Sample ID: 389303001 Certificate of Analysis P:irarJ)etcr __________..... qu:_il_cfler......... Res._ult_..... _l)cerll!_i!J_tv __... _ l\\.1-J?..C ________ l_~c ___....... TP.V. T.~e_ful_l(Jl~i_ng__P~".P :V!c_th1>.~.l_s_'"-~1'.~. pe_rfo.r.1*1e(J __ Method Description An11lyst nate Report Date: February IO. 2016 Project: MJWCOO I ! 5 Client ID: MJWCOO ! Time Prep Batch Dry Sod Prep Dry Soil Prep GL-RAD-A-021 CXCI 01114116 \\202 1537321 Th_e foll1l\\v,in_g__;\\n_alytic:a.I ~-'~~l~()-~5-.l':*e_re __ p_e_r_fo_r1ne_d __.. _.... ____.. ___. _______............... _. _____.... ____. ___..... _.. Mel bud Description 2 3 4 ASTivl D 2216 (Modified) DOE HASL 300. 4 5 2 3/Ga-01-R DOE HASL 300.. 4 5.2 3/Ga-01-R EPA 900.0iSW846 93 JOISM 711013 Modified Surrogateffracer Recovery Test Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.. 96-sigma). Butch ID Rcco,'ery% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Dale: Decem her 4, 2015 Company: Address: MJW Corporation l 5 Hazelwood Drive Suite l 12 Buffalo, New York 1422&
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.22.R.1 Sample ID: 385070016 Matrix: Soil Collect Date: 20-0CT-15 14:45 Receive Date: Collector: Moisture: 05-NOV-15 Client 19% Project: Client ID: MJWC00115 MJWCOOJ Parameter . _....... 9.~~!i_~_er_. _.. R_e~11_lt Uncert.a._i11ty.*...... _ ~!I?S.......... ~ ___.... *-**.'!.nl~s....... J?f. __ A._n_aixs.!... J?ate. Ti_in_e.. ~~~~h_ -~-eth?.~. Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 19 0 Rad Gamma Spec Analysis Gammaspec. Gamma, Solid Actmium-227 Antimony-125 Ccsrnm-137 Cobalt-60 Europium-154
- Protacumum-231 Radium-226 Radium-228 "Dry Weight Corrected" u
-005! +/-0.245 u 0.0519 +/-0 0931 l 15 +/.() 121 u -0 (10936 +/-0.0338 u Ul -0.0211 0 00 0 875 +/-0.110 +/-0 795 +/-0.143 Tin-126 U 0.927 0 [(17 +/-0.258 +/-0.109 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "D1y Weight Con-ccted" 0.455 0 181 0.0595 0.0641 0 180 0.872 0 117 0.245 (J 133 Alpha
- 14. 9
+/-320 2.53 !3eta 25 4 +/-3.09 3.20 percenl CXCI ll/JO!IS l3l9 !521842 pCilg RXF2 12103/15 1306 l 52.23S3 pC'1lg 0 100 pCi/g pCi/g pCi/g pCi/g pCifg p('i/g pC1lg 4 00 pCi/g KXB2 12102115 1123 1525757 . I()() pCi/g _1:1i_c f.o.H_".'Y.i~-~--Pr~p M_~th.o_d_~ ~c~'.e_ p~rr.c:i~~~~:...... Method Description Aualyst Date Time Prep Batch 2 3 nry-*soif rrc*p * *** * * * * * *......... *o*~~ *s*o1*crr*e*p*at~RAb~A~O:i f
- * *** *- ** c_;xcr*.... * *** *** *
- 11lt'o:1TS ***-* ** -- - i"3Hi" *......
- T5"2'i8~2 -*
- _T~!'. f?l_!_o\\vi_n.~. ~n~l~_tic~l. rvt.e~~~~s ~:e.~e_p~i!,o.'.111~9_:. -**... *-**-***-... *-*....................... *-.... **-****.. *-**.. -**** __ *******-**-... *-**...... -*.............
. tv.l~~ho.L....... -............ Pesc:i:i.P.~i_on _____. -*........... ....... A-1.1(!!1st.. C<:imnw11IL ___... -***-............. I ASTM D 2216 (.Modified)
- 2.
DOE HASL 300, 4.523iGa-n1-R 3 EPA 900 O/SW846 9310/SM 71 IOB Moddicd Notes: Counting Uncertainty is calculaled at the 95% confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 566-8171 -www.gel.com Certificate of Analysis Company: Address; MJ \\\\' Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.l.22.R.I Sample ID:
- 385070016 Matrix:
Soil
- Cotlect Date:
20-0CT-l 5 Receive Date: 05-NOV-15 Co[Jector: Client Moisture: 19% Parameter . 9_u~Ji-~~r.... Result..... r.11cc..r~.ai!1~X........ :\\11)~'. Le Gravimetric Solids ASTM D 2216 ~*"ii Moisture "A.v Received" Mo1slure 19.ll Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry Weight Corrected" Actinium-217 lJ -U.051 +/-(l.245 Antimon~*-125 u 0 05 l 9 +f-0 093 l Bismuth-2 \\2 UJ 0 00 +/.() 763 Bisrnuth-2 l 4 Cestum-\\37 Cobalt-60 Europmm*\\54 Lcad-212 Lead-214 Pota~sium-40 Protactmmm-231 Radium-226 Radmm-228 11mlhurn-208 Tin-126 u LI Ul LI I Rml Gns !'low l'roportimml Counting 01!75 1.15 -0.00936 -0.0211 1.02 0971 11.4 0.00 0.875 0.927 0.293 000 GFPC, Gross AB.* ~olid "Dry Weight Corrected" Alpha 14.9 Beta 25.4
- q1e fol!o\\~!.ll.&.~re_p_'.\\'f_et~o':1~.. ~.er.:c 11_c~fo!'t11e1I _
- \\fothod Description DI}' Sod Prep Dry Sod Prep GL-RAD-A-021
+/.() 143 +/-(} 121 +/-0.03.38 +l-0 110 +/-0.113 +/-0.194 +/-1 35 +/-0 795 .,,.() 143 +1-0 258 +l-0.0704 +/-0.109 +1*3 2() +f-3 09 0.455 0.181 I 13 0.117. () 0595 0.0641 0.180 0 llJ3 0 12'-) II 61& () 872 0.117 D 245 b 059 () 133 2.53 3 20 T~-~ fol~_o,v~ng __ ~~l!!r!Li:_a_l_ ~!.et~o~~ *'".c-~e P.c.rf~ft!l.C<l_........ -****....... _........ Method Desc1*iption ASTM D 2216 (Modified) 2 DOE 1-!ASL 300, 4 5 2.3/Ga-0.1-R 3 EPA 'f00.0/SW846 93 lOiSM 71 IOB Modified Surrogatcffracer.Recovery Test 0214 0.084 () 524 0 0535 00268 0.0274 00771 0 0485 0 0597 0 263 0 409 () 0535 () 110 0.0268 0 0638 1.04 150 Analyst CXCl Report Date: December 17, 2015 Project: Client JD: MJWC00115 MJWCOOI .. JP~_: __ +l*O 246 +l-0 0961 +1-1 no +1-0.161 +l-0 155 +/-0 0341 +1-0.1 IO +l-0 158
- f/-0212
+/-I 69 +1-0 842 +/.Q.161 +i-0.292 +/-U 0745 +/-() 11() !*l-129 +/-I 68 Date 11/10.!!5 !J.l 00 400 10.0 percent CXCI 11/10/15 !319 1521842 pCi!g RXF2 12/03/15 l 306 152238_3 2 pCi!g pC'1/g pCi/g pC1/g pC1lg pCi/g pCi/g pCitg pC1/g pCi/g pC1/g pC1!g pCi.lg pCi/g pCi/g KXB2 1.2102115 1123 I 525757 3 pC1/g Time Prep Batch 1319 1521842 Batch ID Recon:ry% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 - www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Su1te 112 Buffalo. New York 14228 Contact
- Ms. Laurie Losey Project:
$oil Radioisotopes Client Sample ID: 3.1.22.R.l SampldD: 385070016 P:inimcler Surrugutefrraccr Rcco\\*cry Test Notes: Certificate of Analysis* Report Date: December 17. 2015 Project: MJWC00115 Client ID: MJWCOOI Batch ID Reco\\"ery%. Acceptable.Limit.~ TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).
GELLABORATO~ESLLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Bumi.lo. New"fork 14-228
Contact:
Ms. La.uiie Losey Project: Soil Ri1dioisotopes Client Sample TD: 3.1.22.R.I Sample ID: 385070016 Matrix: Soil Collect Date: 20-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 19% Certificate of Analysis Report Date: December 17. 2015 Project: MJWCOOl 15 Client ID: MJWCOOI . ~!!-ram.pt~r.................... _9.u:i.J_i_fi~~-. *****-.~e.sult : ~'f1cer.!a_in.!1:.. MDC .. !:-'.~.,............ I~IL.........1~.. __ Ln_i_~... !!It_ ;\\n_alr.st.... l_>~.t~ J:!~c.. ~.a t~!t.. ;'.vi.I(}: Gtavimetric Solids ASTM D 12 J 6 ~-"1 fvloisrure .*Is Received" Moisture 19.0 R:1d Gamma Spec Analysis Gammaspec, Gamma, Solid "D1:i-* Weight Con*ected Acumum-227 u -0051 Antimolly-125 u 0.0519 llismuth-212 Lil lJ 00 Bismudi-214 0 875 Cesium-137 1.15 Cobalt-60 lJ -0 00936 Europmm-154 lJ -00211 LcBd-212 I 02 Lcad-214 0.971 Polassium-40 114 Protitctmmm-23 \\ U! 000 Radium-226 0 875 Radium-228 0.927 Thallium-20g 0293 Tin-126 Ul 0 ()() Rml Gas Flow Proportional Counting GFPC. Gross Ai8, solid Dry Weight Corrected" Alpha 14.9 Beta 254 The following Prep :\\<lethods were performed ~1e-11;~x**-**-** ****-n~scY"ij)lion*** ** -**- ****** ***** Dry Soil Prep Dry Soil Prep GL-RAD-A-021 Th c __ f ()1.~o,_~i ll~ ~-Ii ~1 lr..t!~.a I_.M~~~l)-~~-'.v_e.~~ p_cr.f o~ !fl.~~.. Method Des*cription ASTM D2216lModificd) 2 'DOE HASL 300, 4.5 2 3/Ga-01-R +/-0.245 +l-0 0931 +f-0 763 +l-0 143 +/-0.121 ' +/-0 0338 +/-0 110 -+/-0 123 +/-0 194 +/. J.35 +/-0 795 +/-0.143 +t--0 258 +l-11.0704 +1-0.109 +/-3.20 +/-3 09 3 EPA 900 OfSW84fi 9310/SM 71 !0l3 Modified Surrogate!Tm~cr Recovery Test ix:rccnt CXC'l t!/10115 1319 1521842 0.455 0214 +/-0.246 pCilg R.'\\1'2 12i03/15 1306 1522383 2 0 181 0.084 +/-0.0961 pC1/g 113 () 524 +/-1.00 pCi!g 0l17 00535 +/-0161 pCi/g 0.0595 0 0268 +I-{) I 55 0 100 pC1!g 00641 0 0274 +/-0.0341 pCi!g 0.180 00771 +/-0 110 pCtlg 0.103 0 0485 +/-0.1.58 pCi/g 0 1-29 0 0597 +l-0.212 pCt/~ 0.(ilS () 263 +I-I 69 pC1lg 0.872 0.409 +/-0.842 pCilg 0.117 0 0535 +/*O 161 pCilg 0245 0.110 +1-0 292 pCrlg 0059 1.10268 +i-0 0745 pCi/g () 133 (I 063B +/-0 110 pCi/g 2 53. l 04 +/-4 29 4 00 pCilg KXB2 1210211 S 1123 152575! 3 320 15() +!-4 (18 !0.0 pCi/g AnHly!il Date Time Prep Batch CXCI 11/1 O!l5 1.119 1521842 J3atcli ID Recovery% Acceptable Limits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.geLcom Company: Address: MJW Corporation l 5 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact Ms. Laurie Losey Project: Soil Radioiso.topes Client Sample JD: 3.1.22.R. l Sample ID: 385070016 Certificate of Analysis Report Date: December 17. 2015 Project: MJWCOOl 15 Client JD: MJWCOOI Pal'i*11.J.~_tcr._....................9.?.~_li_~~r.... _. l_l~u!.t..... El!~_c_rJ:_iintv _;_\\U~.c.......f.._c ____.... __.HI.. _...... Ill_. _ l_T_i:ii_ts_._.:i?l'.*:':.n_alysl_... !J.a.t~.. Ii.m.~. ~'!~~"-. ~i~f:!- Surrogatcn*r:icer Recovery Test Bntch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence !eve! ( t.96-sigma}.
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171-' w..vw.geLcom Certificate of Analysis Company: Address:
Contact:
MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, Ne\\\\' York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample JD; 3.1.22.R.2 Sample ID: 389303002 Matrix: Soil Collect Date: 20-0CT -15 Receive Date: 14-JAN-!6 Collector: Client Moisture: 19.4% Parameter.... -**-.. Q1.1_a_li~e..r.~ ... ~~s.~*!.t..... _En..ecr.tai_n_tv _... _)'.1.D(~ Gravimetric Solids ASTM D 1216 % Mqisture As Received" Moisture 19 4 Rad G:1mm11 Spec Analysis Gamma wiih Jngrowth "Dl'y Weight Co1-rec1ed" Actinmm-227 11 0.133 +/-0.371 o r,93 Antm1ony-I 25 u .[)(1714 +/-0.1.14 0.277 lfa,muth-212 lJ 0.475 +/-1.08 1.83 Bismmh-214 0821 +/-0 239 0.195 Cesium-137 l 37 +/-0 178 0 )\\) Cobalt-60 lJ 0 0299 +l-0 0619 0.140 Europium-15.\\ i; -0 0619 +l-0 148 0 285 Lead-212 0891. +/-(} 182 0 l72 J.cad-214 () 774 +/-0.230 0.224 .Potassium-40 11.8 +/-1 97 1.21 Protactimum-231 lll 0.00 +1-0720 144 Radmm-226 0.821 +1-023') IJ 195 Rudium-228 1 02 T/-0449 0319 Tha!hum-208 0.359 +/-0.119 0.0914 Tm-126 UI 0.00 +/-0 168 0.186 Gammaspec. Gamma. Solid "Dry Weight Corrected" i\\ctirnum-227 u (l 0982 +1-0 337 0 637 Antimony-125 u . -0.0112 +/-0 123 () 233 Oismnth-212 UI I) 00 +1-0 771 I 49 13i~muth-214 0529 +/-0 192 0.170 Cer.iurn-137 l 27 +J-0 155 0.IOl Cobalt-60 u -0.04 +/-0.052 0.0861 Europmm-15*1 lT -0 0655 +/-0.162 0289 Lead-212 0&32 +f*O 174 11169 Lcad-214 0.815 +/-0223 0.195 Potassium-40 12.9 +t-1 59 0.593 Protacumum-231 U-() 505 +/-1 05 1.26 Radium-226. 0.529 +/-0 192 (1 170 Radium-228 I 14 +/-0.354 0.265 Th~lhum-203 0 284 ~/-0 0985 0.0937 Tm-126 UI 0.00
- +O 143 02(){)
Rad Gas Flow Propor1iomtl Countin~ GFPC. Gross AB. solid "Dry /Veight Corrected" Alpha 16 8 +1-4.32 3 86 Bew 30.S +1-3.49 2 56 Le .. :rrr .0.321 +/-0 376 0.115 +l-ll.157 0 821 +/-1.10 0.0857 +/-0.248 00488 +/-0.209 00587 +/-0 06JJ 0 112 +l-ll 151 () 0807 +l-0 196 0 103 +/-0.231) 0.494 +/c2 22 ()668 +1-0 827 0 0857 +/-(l 248 () 130 +l-0 466 G.0398 +/-0.122 0.0884 +/-0 168 0299 +J-0.341 O.I07 +/-0. I 23 0688 ... 1.1 13 00774 +/-0 197 011461 +1-0 190 0 0361 +/-0 0551 0 126 +l-0 165 IJ.0803 +l-0191 0.IJ909 +f-0 236 0.228 +/-I IJ3 0.593 . +1-1 05 0 0774 .../.0.197
- u. t 14
+/-0.390 ll 043 "':/-0 102 (J.0957 +/-O.l4S I 59 +/-5 47 1.15 +i-5 50 Report Date: Februfll)' LO. 2016 Project: Client ID: MJWC00115 MJWC'OOI percent CXC! 01114/16 !202 1537321 pC11g RXl'2 02i05116 0715 !537551 2 pC1/~ pCi/g pC1lg 0.100 pC1lg pCilg pCilg pC1lg pC'ilg pC1lg pCi/g pCi/g pCilg pCi/g pCi/g pC1/g RXF2 011!8/16 0935 1537548 3 pCilg pClfg pC1fg 0100 pCt/g pC1/g pCifg pC1!g pCi-'g pCilg pC'ilg pC11g pC1!g pC1/g pC1!g 4.00 pC1!g KXB2 01120/16 1225 1539462 10.(l pC1/g
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843} 556-8171 -WWW.gel.com Company: Address: /l.U\\V Technical Services 15 Hazelwood Drive Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisolopes Client Sample ID:
- 3. l.22.R.2 Sample ID:
389303002 Certificate of Analysis Parameter.................Qua.li~er..... ~c~u.lt_... l!n."crtain.~v MJ?C...... L.c........... Tf.~:.. Th~ fol!o\\\\'.i~g !'r~p j\\1et~o~s. \\~*ere.Pc.rf<irm~d.... Methnd"' Description Date Project Client ID: Report Date: Fcbi:uary lO, 2016 MJWCOOl 15 MJ\\\\'COOI .. RL.. _.l.ini~s.. D.~. A.~!llyst Date_Ti~!.. Batch.. :"1.td. Time Dry Soi\\ Prep Dry Soil Prep GL*RAD*A-021 Analyst CXC' I 0 lll4fl6 1202 Prep Batch 1537321 T.l.1c f1i.llol,vi~g i\\_n_a!~*tic,:il. ~-li;~.ho~s-~!e_r.~_p.cr..f().r111e_d_. Method Description -* ** 1. ****** I ASTM D 2216 (Mod1f1ed) 2 DOE HASL 300, 4 5.2 3/Ga-0\\-R 3 DOE BASL 300. 4..5.2 JiGa-01-R EPA 900 OiSW846 9310iSM 71 IOB Modified Surrogateffr:iccr Rcco,*ery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level { 1.96-sigma)_
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: Address:
Contact:
Project: Client Sample ID: Sample1D: Matrix: Collect Date: Receive Date: Collector: Moisture: MJW Corporatioll 15 Hazelwood Drive Suite !12 Buffalo, New York Ms. Laurie Losey Soil Radioisotopes 3.1.23.R. I 385070017 Soil 20-0CT*IS 15:10 05-NOV-15 Client 21.9% 14228 Project: Client ID: MJWCOOl 15 MJWCOOl Pm:~rne~~1:.......... *-*. Qualifier ResuH ~nce'.ia~nt.Y....... IY1DS'........... R..~ *-.......... 1JT1it~ ... f:)F. f\\naly~t.. Date Time Batch Method Gravimetric Solids ASTM D 2216 % Moisture "As Received" Mmslurc Rad Gamma Spec Analysis Garnmaspec, Gamma, Solid Actmium-227 Anlimony-125 Ccsium-137 Cobait-60 Europium-154 Protactimum-23 l Radmm-226 Radium-228 21.9 "Dry Weight Cotrected" U -U 0379 +l-0 295 u 0.000438 +/-().130 1.39. +/-0.155 u 0.0434 +l-0 0402 u u 0201 0.407 0 855 0.797 +/.() 168 +f-0612 +/-0.1&9 +/-0.383 Tin-126 Ul 0.00 +/-0.01(}<) Rad Gas Flow Proportional Counting GFPC, Gross A!B, solid "Dry Weight CotTected" {) 556 () 250 {) 116 0 104 0 373 l 'IS () 175 OJ55 0.136 Alpha 12.4 +/-3.09 2.55 Beta
- 22. 8
+/-3 44 4 23 Th.efo.I_l~\\Y.i~~-:P..~~p fv~(!t~.c:cts.. :-v(!r.~.P~rf.oi:rr.t.~!1'._............. _........................... 0 100 4.00 JO 0 Method Description Analyst o~ *s0ir'riei1-.. *............. bf):.. sor1-rreri.di...~R:Ao-A-ii:fr..... - .... * *...... <:.'xi'..' r ***
- The.f.ol.1.o~vi.°:~-~.~_:11.Y.!i~~l-~~th.~~s.~er~.. P.:.r!.°.i:z1C.d.=......... _......... ---*
percent pC1/g pCi/g pC!lg pCi/g pCilg pCi/g p('i/g pCilg pCilg pCilg 'pCi/g Date CXCl 11/10/15 1319 1521842 RXF2 12/03115 !30(\\ 15-22383 KXB2 12/02/!5 1123 1525757 Time Prep Batch .. i tiiO'iE *-.... *13i 9*...... i52.i842... MeU_ip~ _................ Pc:~<:r.i.t~J}'?.1.1....... _..........
* _......... _.......... _....... ___....... ___ Ari_a.!.Y'!.L~<;>rµn1~J1ts..
ASTh1 D 2216 (Modified) 2 DOE [*!ASL 300. 4.5.2.J/Ga-01-R 3 EPA 900.0iSW846 93 IOiSM 711013 Modified Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigrna). 3
Company: Address; GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com MJ\\V Corporation 15 Hazelwood Drive Suite 112 Certificate of Analysis Buffalo, New York !4228 Report Date: December 17. 2015
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample JD:
- 3. 1.23.R. l Sample ID:
385070017 Matrix: Soil Collect Date: 20-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 21.9% Gr:wimetric Solids AST,\\,/ D 1116 % Moisture "As Received" Moisture 21 9 Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "D1y Weig/rt Corrected" Actmium-227 (.\\ -0.0379 +1-0 2CJ5 Anti.mony-125 l,' 0000438 +1-0.130 Bismuth-212 1.73 -t-/-134 Bismuth-214 0.855 +/-0 189 Ces1um-!J7 1.39 +/-0 155 C'ob:ilt-60 lJ 0.0434 +/-(l.0*102 Europium-154 UI 0.00 +1-0.168. Lead-212 1.11 +/-0 130 Lcad-214 1.16 +/-0 236 Potassmm-40 14.1 +/-1 82 Protacrimum-231 u 0.407 +/-0 672 Radium-226 0 855 +/-IJ 189 Rudium-228 0.797 +/.() 383 Thallium-208 0 J6! +/-0.104 Tin-126 Ul o.oo +/-00769 Rad Gas lllow Proporliona! Counting GFPC. Gross AfB. solid "Dl'.I' IViJight Corrected 0 55(> 0261 +i-0 296 0250 0 116 +/-0.130 l 05 0.457
- 1/-1.35 0 175 0.0786
+t-0 202 0 116 0.0528 +/-0 192 0.104 0 0436 +1-0 0449 0.373 0 163 f/-0.192 0.120 0 0563 +/-0 178 0 180 00837 +1-0 257 I 06 0447 +/-2 22 l 18 0.553 +/-0 703 0 175 (l.0786 +1-0 202 OJ55 0 155 +f-0 397 0.0873 00392 +1-0.108 0 136 00659 +/-0.131 Project: Client ID: iV!JWCOOl 15 MJWCOOI ~rccm CXCI pC1/g RXl'2 pC1/g pCilg pCilg 0.100 pCllg pC1lg pCi!g pCi!g-pCilg pC1/g pCi!g pCi!g pCilg pCi/g. pC1/g 11/10/15 1319 1521842 1 ~{1)3/15 1306 1522383 2 Alpha 12 4 +l-3 09 +/-3..\\4 . 2 55 423 I 02 2.01 +1-3.91 +/-4 71 4 Oil pC!/g, KXB2 12102115 1123 1525757
- 3 Bctu 228
}'he fo.flo_~\\:~~g f.'.re.r M.c.t.h.o~s ~vc.r.~.. P.~r:fll.t.:.ll'I~~........ Method Description Dry Soi) Prep Dry Soil Prep Gl.-RAD-A-021 }'Iii: ~i,>llo~vi.Jlg.~n..:i~ytic.a.1.~11!1.~e>.~~ '.".t!~e pez:~or111ct1.. Method Description ASTM D 2216 (Modified) DOE HASL 300. 4 S 2.31Gu-01-R 3 EPA 900.0/SW84ii 9310/SM 71 WB Modified Surrogat~ffraccr Recovery Test A.nalysl CXCI Date 11110115 10 0 pCilg Time Prep Batch 13l9 1521842 Batch ID Recovery% Acceptable Limits
GEL LAB ORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID:
- 3. I.23.R.I Sample ID:
385070017 Certificate of Analxsis Report Date: December 17, 2015 Project: MJWCOO 1 l 5 Client JD: MJWCOOl xi1r.ll:!11etc~............. _Qua_li_~er..... !t.c~1:1lt.... _. l:n_c(!rt.:tin.ty..... ;\\1J>.C... Le TPl'......*. ~~~... l!nif_s_ I>Y _r-\\_nalyst. p:1t~_J:i1ne. ~atc)1.~It.~.. Surrogatcfl'racer Recovery Test Bnlch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95%, confidence level ( 1.96-sigma).
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Address: MJW Corporation I 5-Bazel wood Drive Suite 112 BulTa!o. New York 14228
Contact:
Ms. Laurie [.,o~ey Project: Soil Radfoisutopes Client Sample ID: 3.1.23.R.l Sample ID: 385070017 Matrix: Soil Collect Date: 20-0CT-l 5 Receive Date: 05-NOV-15 Collector: Client Moisture: 21.9% Par.am._c~er........ *-*-*-.. _ gul}l_Uier..,R_cs_u_l~.... _l_'.*~_cer:tain_ly...... -~;!~(;... _. _!,-~ Gravimetric Solids AST.'vl D 2216 % Mois//lre "A.~ Received" Mmsturc 21.9 Rad Gamma Spec Analysis Gammaspec. Gamma, Solid "Dry Weight Correc1ed" Actmium-227 u -00379 +/-0.295 Antimony-125 u 0.000438 +/.() \\31J Bismuth-212 I 73 +f-1 34 Bismuth-214 o*sss +l-ll. l89 Ccsium-137 I 39. +/-0.155 Cobalt-60 u 0 0434 +l-0.0402 Europmm-154 UI 0.00 +f-0 168 Lead-212 I *II +f-U.130 Leud-214 l 16 +j.I) 236 Putassium-40 141 +/-1.82 Prot;ictmrnm-231 u 0.407 -+/-0.672 Radium-226 () 855 +/-0.189 Radium-228 0797 +/-0.383 Thalhum-208 0361 +/-0 104 Tm-126 U! 000 +/-0.0769 Rad Gas Flow Pi:-011ortional Counting GFPC'. Gross A*B, 9olid "Dry Weight Corrected" Alpha 12 4 +/-3.[)9 Beta 22.8 +1-l4il }he f~.ll~~!_i1~g_ P..r:l!P... ~le_th_o_~s-~v~r_e_r.1'..~f<ir~cd_.. Method Descript1ou Dry Soil Prep Dry Soil Prep GL*RAD-A-021 Th.c. fo_l~o~~ i_D.g _A_nalyt_i~a 1.. '.\\'.l!,_l~~d.~. w~_r_e.P..C.1:'~~'.-~.~d........... _.. M.cthod Description 2 3 ASTM [)2216 {Modified) DOE HASL 300, 4 5 2J!Ga-OJ-R EPA 900.0!S\\V846 93 !01SM 711 Ofl Modified Surrogatefr:racer Recovery Test 0.556 0 261 0.250 0.1 lo l ()5 0 457 om o.n786 o I 16 !J.Cl528 0.!04 0.0436 0 373 0 163 0.120. 0.0563 0 180 0 083.7 I.(){, ()4-1.7 1 18 Cl.553 o.m 0078() () 355 II. !55 0.0873 () 0392 (} 136 0 0659 2.55 1 02 4.23 201 An.ilyst CXCl TPV +1-0.2% +f-0 13() +I-I 35 +/-0.202 +l-0 192 T/-0.0449 +/.l).!92 +/-0 l7S +1-0257 +/-2 22 +f-0.703 +1-0 202 +/-0 397 +/-(l.108 +f-0 lJ l +l-3 91 +/-4.71 Report Date: December 17. 2015 Project: CHent ID: MJWCOOl 15 MJWCOO! percent CX(l 11110/15 !319 1521842 pC!lg RXF2 I 2i03/l 5 1306 1522383 2 pCi/g pCi/g. pC'i!g 0.100 pCi!g pCi.lg pCi/g . pC1rg p('1/g pCifg pCifg pCi/g pC1!g pCi/g pC1/g 400 pCilg KXB2 12!02/15 1123 1525757 3 HJ.() pCi/g Date Time Prep B:1tch 11/101\\5 1319 1521842 Batch ID Recovery% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 - www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14223
Contact:
Ms. Laurie toscy Project: Soil Radioisotopes Client Sample 1.D: 3.1.23.R.l Sample ID: 385070017 Tc!'t Certificate of Analxsis Report Date: December 17. 2015 Project: MJWCOOl 15 Client.ID: MJWCOOJ MDC Le T.l'.L.......... )ll,._ ~!IJ.i.ts.... P.J<.J\\~al>.:s.t.. l)a.t~.. Ti111c. }latc!1.. ~It_~*. Batch ID Recovery% Acceptable Limits Surrogate/Triu~cr Recovery ~ *****............................ -....... Notes: TPU and Counting Uncertainty are calct1lated at the 95% coufidence level ( l.96~sigma}.
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
- Company:
Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.23.R.2 Sample ID: 389303003 Matrix: Soil Collect Date: 20-0CT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 20.6% Paramcte.r......................... QuaU~cr Result Gravimcl'ric Solids ASTivf D 2216. % Jfoi.m1re "As Received N!o1sturc 20 6 Rad Gammn S11ec Analysis Gamma with lngrowt/1 "Dry Weight Corrected" Aclmrnm-227 u 0.0473 Antimony-125 u 0.0162 Bimnuth-212 Ul 0.00 B1sm11th-214 () 875 Cesium-137 1.64 Cobalt-60 u 0.0050 I Europium-154 u .00201 Lead-212 I 03 Lcad-214 095!! Potas~ iu rn-40 13.7 Prolacttnmm-23 l VI 00(} Radium-226 (l 875 Ra<lium-228 0.911 Thallium-20S
- 0.290 Tin-126 u
0.0186 Certificate of Analysis Le +1-0.305 tJ583 0272 +/-0.306 +1-0118 I) 222 0 I02 +/-0.118 +/-0793 1.35 0.617 +/-0.936 +/-0 17.5 0 ISi 0.0828 +/-0 191 +/-0 161 I) 0903 0(1408 +/-0.215 +t-01)408 0.086 0.0353 +/-0 0409 +/-lJ !3(1 U.265 () 113 +/-U J3(> +/-0.136 (} 131 00615 +/-0.160 +/-0.241 0.356 0.172 +/-0 254 +/-! 69 0.677 11269 +/-2.D5 +/-0.851 I 18 () 553 +/-0.866 +/-0 175 () 181 O.OB28 +/-0 191 +/,.{) 288 0277 () 120 +/-0.31 s +/-0 0749 (l 0767 0 0344 +/-110791 +/-0 15& 0211 0 llJl +/-0 157 Gamma~pec. Gamma. Solid "Dry lf/eig/11 Corrected" Actmmm*227 lJ -0 00968 +l-0 302 () 562 0264 +/-0.302 Anunu~ny-125 u -0 0441 +/-0 115 0 204 (}0934 +/-0 117 Bismuth-212 l!I 000
- l-0 929 l 26 u 580
+/-I 01 Bismuth-214 0.727 +/-0 161 0.144 0.0655 +!*0.172 Ccsium-137 1.79 .,.,_{) 152 () 0824 0 0374 +1-0.208 Cobalt-60 u 0 0229 +/-0 0394 0 0864 OOJn +/-()()408 Europium-154 u -00362 +/-0.119 0.222 ll.0949 +/-0 120 Lcad-212 0 821 +1-0 18! 0.157 0.0748 +/-() 194 Lcad-21*1 0.785 +/-0 19.J 0.324 0 157 +/-0 205 Potassium-40 124 +/-1.i2 0 760 0.321 +/-! 78 Protucunium-231 u 0.394 +1-0.87() 1 07 0 50(1 +/-0 874 Radium-226 0727 +/-0 161
- 0. \\44 0 0655
+/-0.172 Radium-228 l 00 .,./-0.279 1)222 0.094& +/-0.315 Tha!lium-208 0 283 +i-0.Ul)23 U.0789 0.03(> +1-0.0952 tin-126 UI o on +/-0 j ](l ll 098\\ 0 0457 +f-ll.117 Rad G11s flow Proportional Counting GFPC. Gross A:B, solid "D1:1' Weight Corrected" Alpha 144 +/-4 45 3 9\\ I.SI +f-5 22 Bel!! 24 2 +f-3 26 2 30 I 01 +/-4 71 Repot1 Date: February I 0, 2016 Project: Client ID: MJWC00\\15 MJWCOOl percent C'XCl 01114116 IW2 1537321 p('ilg RXF2 02/05116 0716 153755! 2 pC1lg pC1!g
- pCr/g o lllO pC'iig pCi/g pCi/g pC1/g pCiig pCilg pCi!g pC1/g pCt/g pO/g pC11g pC1ig R..XF2 01118116 0936 1537548 3
pC1/g pC1lg pC1ig 0 1()() pCi/g pCilg pC1/g pC1lg pCi/g pC'1/g pCi!g pCi/g pCilg pCi/g pC1lg 4.00 pCi!g JXl37 0!/26/16 !140 1539464 4 IU.O pC1/g
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843} 556-8171 -www.gel.com Company: Address:
Contact:
MJW Tcch11ical Services 15 Hazelwood Drive Suite ! !2 Buffalo. New York 14228 Ms. Laurie Losey Project Soil Radioisotopes Client Sample ID: 3.1.23.R.2 Sample ID: 389303003 Certificate of Analysis Parameter ..... 91:1.al_iner..... ~cs.11It..... J111~ertai11tv MDC' Le The _f ()l_l_~~vi11.g.~_r_ep_ ~~e.t.~_()d.~ '.t*er.e_p[!rf.oTIJll'.~.................... Mei hod Description A11alyst Date Report Date: February 10, 2016 Project: MJWCOOl 15 Client ID:
- YIJ\\VC001 Time Prep Batch Dry Sml Prep Dry Soil Prep GL-RAD-A-021 CXC'I 01114116 1202 1537321 l_~hc.. f P.l_~(}'.~J.llR.A.!,I~ lyt_ic'.11. '.\\1 ~th~.d~ wi:.r~.P.~.r_f()rf!l.Cd........
- Vlethod Description 2
3 ASTM D 2216 {Modified) DOE llASL 300. 4..5 2 3/Ga--01-R DOE HAS!. 300, 4 5.2.3iGa-01-R EPA 9000.IS\\\\!846 93IO!SM 71 IOB Modified S urrogateffraeer Rccnn:ry Test Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level (_l.96-sigma). Batch ID Recovery% Acceptable Limits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York l4228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes --***** NOo***>>OO 0 000 0 O>H*ooo-*-***-**** 000'** Client Sample ID: 3.1.24.R. l Sample ID: 385070018 Matrix: Soil Collect Date: 20-0CT-I 5 I 5:35 Receive Date: 05-l\\)OV-15 Collector: Client Moisture: 18% .r..~ra.111~~~r......... **--......... ___ Q_u.al_i~:r...... -~es_~_l_t_. U_~1~:r.t~i.Il_I).'.. Gravimetric Solids ASTM D 2216 % Moisture "As Received" Mo15ture 18.0 Rad Gamma Spec Analysis Garnmaspec. Gamma. Solid '1Dry Weight Con*ected" Actinium-227 \\J 0.200 +/-0 247 Ant1111ony-125 U -0.0283 +l-00879 ~csium-137 1.65 +f-0. \\20 C'ohah-60 +/-0.031 u 0 0239 Europium-154 +1-0. I IO
- U
-0 0407 Protactinium-231 +l-0.552 ll 0 155 0 939 Rudium-226 +/-Cl.133 Radium-228 +/-0 242 0.86S Tin-126 Li I 0 00 +/-0.134
- Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha 12 4
+/-3.69 13eta 21.2 +l-3.25 The following Prep Methods were pcrfonned: Ni-Cii1ocf *- ** ** * *** **** * **- -**o~~~~iiitio~*** *** ** * *** ***** * * * ***-****-*** ***** Ory 0Sai*11;*rcp........ *-....... Di}: So1Ci'rep-GL~RAb°;A-02 c ***... !~.~!~~ l_?':".~~!?-~.~a!f.~i ~a!.J',ll~t.h.?.~~- :--Y:~:. p~rfo11~1ed:_.......... Mc::~ho.t:L............ _ . I>~s._cript.i.011.......................... I ASTM D 2216 (Modified) 2 DOE HASL 300, 4 5 2 3/Ga-01-R 3 EPA 900 OISW846 93 IOiSM 71 IOB Modified Notes: MDC RL 0.480 (l.!6\\ ()0529 0 065\\ 0.194 0 ~g7 0.115 0.205 0 128 342 3 39 0 100 4 00 10.0 Analyst
- cxc*1***
Counting Unce11ainty is calculated at the 95% confidence level ( 1.96-sigma). Project Client ID: MJ\\VCOOI 15 MJWCOO! percenl pCi.lg pCi!g pC1lg pC1/g pC1/g pC1/g pC1lg pC!lg. pC1/g pCi!g pCilg Date
- **uhoiis- ****
CXCI 11/10115 1319 1521842 RXF2 12103/15 1306 1522383 KXl32 I 2i02!!5 1125-1525757 Time Prep Batch 13"f9". .. "152"t"84i -*......... -..... .... Amtl..Y.~t.~R.ITl!Il.ents......... 2 3
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www_gel.com
- Certificate of Analysis Company:
Address: MJ W Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.24.R. I. Sa mp le ID; 3 850700 J 8 Matrix: Soil Collect Date: 20-0CT- [ 5 Receive Date: 05-NOV-15 Collector: Client Moisture: 18% Report Dole: December 17, 2015 Project: MJWCOOl 15 Client ID: MJWCOO ! l'~r~~ct~r.................... q~al_ifi"I'.._.. _}~_~s':!l_t ___ _ l_;lll:crtainty_ _______ :\\~DC'_... -~c--....... TP..l'...... _ Rk_ __ X!!its. ___ I>.~. -*~-a~~~~-- Date.1:i_~~ -~-a_tc_h. _ Tylt~. Gr:ivimcfric Solids ASJ!\\1 D 2216 % Moisture "As Received" Moisture !S_O pcrcem CXC'I 11110115 \\319 1521842 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Acunium-227 Ll 0.200 +/-0.247 ll 480 0230 +/-0.264 pCifg R-'<F2 12103115 1306 1522383 2 Antimony-125 lT -0.0283 +/.() 0879 0 161 0.0759 +/-0.0888 pCi/g Bismuth-212 0 809 +/-0 648 0762 0 352 +/-0.653 pC1lg ll1smulh-214 0 939 +/-0 133 0 115 OJJ53S +f-0 156 pC'ilg Ccsmm-137 1.65 +/-0.120 00529 0 0243 /-0.18(> 0 !()() pCi/g Coba!t-60 u () 0239 +1:0 031 0.0651 0.0293 +/-0 0328 pCi/g Europiurn-154 u -0 0407 +1-0 110 0 194 0 0881 +/-0 11 \\ pC'i/g Leml-212 I 01 +/-0.121 009H4 0.047 -t-/-0.144 pCi/g Lead-214 I 12 +/-0.168 n.121 00572 +/-U.190 pC'1lg Potassmm-40 137 +/-125 0562 0250 +/-1.71 pCilg Protnctmium-231 L' 0.155 +/-U 55-2 (} 897 0428 +/-0 558 pCi/g R~diurn-226 0.939 +l-0.133 0.115 0.0538 +/-0 156 pC1lg Ri!dium-228 0.868 +l-0 242 0.205 ().0936 +1:0 259 pC1/g Thal!ium-208 0.218 +l-0 0745 0.063 1}02% +/-0 0768 pCi!g T[n-126 lll !JOO +/-0 134 (), 128 00613. +1-0 135 pCilg Rad GA.s Fl!lw Proportional Counting GFPC. Gross A-'B, solid Dry S-Veight Correcred" Alpha 12.4 +/-3.69 3 42 1 37 +1-4 39 4.00 pCi/g KXB2 l 2i02115 l 125 1525757 3 Beta 212 +/-3.25 3.39 I 56 +1-4.40 10.0 pC1/g Th..e. fol!_[l~'ill.~.P~ep __ ~le_t~_o~~-'-vere.rc.rform_e~... .Method Description Analyst Date Time Prep Bakh ""'*****"'"''''"''''° *'*' Dry Soil Prep Dry Sq1I PrcpGL-RAD-A-021 CXCI 11/!0/l 5 1319 !521842 Tb_~!f)l_lf)\\l'i!l!:\\_A11_~lytj~a!_]\\.*!i:!~()~S __,!cr~.l'.c!_"_f~.rlll'"'.~- Mctl!Od Description r\\STM D 2216 (Modtficd) 2 DOE HJ\\SL 300. 4.5 2 JfGa-01-R 3 EPA 900 OiSW846 9310iSM 71 IOB Modified Surrogateffracct' Recovery Test Batch ID Re<:overy% Acceptable Limits
GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn
- Company:
Address:
Contact:
MJW Corporation 15 Hazelwood Drive Suite 1 lZ Buffalo. New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID:
- 3. !.24.R. I Sample ID:
385070018 Certificate of Analysis RcpOJ1 Date: December 17, 2015 Project: MJWCOOI 15 Client ID: MJWCOOI Parameter............... 9.U.:Jlifier_..... R.c~11.1t_...... rn_c_t?rt_a.i1tl......... _,\\1(?('.'... _. -~-c *-......... TJ;'J:.... *-.. ~1:--.. ~'!!_its_... :0.F.. '.:~!1.ao/,s_~..D.Sl!e. _T!i_nc.. fl.l!.t<:l~----~ltd!. Surrogatcffracer Recovery Test Balch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95%> confidence level ( 1.96-sigma).
\\... GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:
- Address:
M.IW Corporation 15 Hazelwood Drive Suite 1 l2 Buffalct. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.24.R. I Sample ID: 385070018 Matrix: Soil Collect Date: 20-0CT-15 Receive Date: 05-NOV-I 5 Collector: Client Moisture: 18% Result l)'11:ert~i1J..l~............ ~IDC Parameter .......... qua_Ji~er Gravimetric S(llids AST:\\./ D 2216 % Moisture "As Received" Moisture Rad Gamma Spec Analysis lX.O Gammaspec, Gamma, Solid "Dry Weig/it Crm*ected" Aclmmm-227 u U.200 +J-0.247 Antimony-l 25 u -0.02&3 +/-0 ()879 Bismuth-212 0 809 +l-0 o48 BismuLh-214 0.939 +/-0 133 Cesium-137 1.65 +/-0.120 Ca\\Jalt-60 LI 00239 +/-O.o3 \\ ELJrapmm-154 u -00407 i*/-0.110 Lcad-212 l Ol +/-0.121 Lcad-214 1.12 +/-0.168 l'otass1um-40 13.7 +/-1.25 Protactmium-231 lJ 0 155 +/-0 552 Radium-226 0 939 +/-0 133 Radium-228 0868 +/-0 242 Thallium-208 0.218 +/-0.()745 Tm-126 Ul 000 +/-0 134 Rad Gas Flo;,.,' Proportional Counting GFPC. Gross :4."B. solid "D1:r Weight Corrected" Alpha 12.4 i*/-3.69 Bern 21.2 +/-3.25
- f.b~_.f.oll~~!~llg_]>_!:~!!_:\\~eth~ds_ \\\\:e_r~.!!.~.r:~o~m.cd.. -*****..
!\\'let bod Descri11tion Dry Sail Prep Dry Sml Prep GL-RAD-A-!J2 I '~he_ f.ol!()'.".i.'!~.J\\.11:1_l~t.ical. :\\'!~.~-~.?..~s.'.".'.cr~.11.e_r_f~.~ll~~tl. Method Description ASTM D2216[Modified) DOE HltSL 300,4 5.2 3/Ga-0 l*R 2 3 EPA 900 O!SW846 93 l'O/SM 71108 Modified Surrogatcffracer Recovery Test 0.480 0 \\6\\ 0 762 0.115 00529 0.0651 () 194 00984. 0.121 0562 0&97 0.115 0.205 0.063 0 128 3 42 3.39 Le........ :r.r..r 0.230 +1-0 264 0.0759 +/-0.0888 0.152 t/-0 653 0.0538
- rl-0.156 0.0243
+/-0.186 0.0293 +1-0.0328 0.llSRI +/.() 111 0.047 .../.Q. \\44 00572 ...,.fl.190 0250 +/-1.71 0428 +/.!) 558 0.0538 +/-{} 156 0.0936 +i-0 259. 0 0291> +/.() 0768 0.0613 +/-ll 135 I 37 +/-4 39 l 56 +/-4.40 Analyst Date Report Date: December 17. 2015 Project: Client ID: MJWC00115 MJ\\VCOOl per~cnt CXCI .11110/15 1319 1521842 pCilg RXF2 12103115 130(> 1522383 2 pC1/g pC1/g pCi/g 0 100 pCi/g. pCilg pC1/g pCilg pC1/g pCilg pCr/g pCi/g pCilg pC1!g pC1/g 4.00 pCifg KXB2 12102115 1!25 1525757 3 10 0 pC1tg Time Prep Batch CXC' I 1\\/10115 1319 1521842 Batch ID Recovery% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.get.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.24.R. l Sample TD: 385070018 Certificate of Analysis .Y~r..~!Jl~~~~............. *--. 9u~li.f.i~_r _____. ---~esult l'nccrtaintY.......... ;'VlQ(....... _Le......... JP_l' Surrogateffraccr Rccove1-y Test Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma). Report Date: December 17. 2015 Project: MJWCOOl-15 Client ID: MJWCOOI ... ~~-... l~'!i~*-*.!_)E _i:\\CJ:!:Irs.t. -~~t:1:. ~*!me __. B..~t.ch ___ ;\\-1td_. Bat1;h ID Reco.-cry% Acceptable Limits
Company: Address: GEL LABORATORIES LLC 2040 Savage Road Charfeston SC 29407 - (843) 556-8171 -www.gel.com MJW Technical Services 15 Hazelwood Drive Suite 112 Certificate of Analysis Buffalo. New York 14228 Report Date: February IO, 20 ! 6
Contact:
Ms. Laurie Losey Project: Soil Radioi~otope~ Client Sample JD: 3.1.24.R.2 Sample ID: 389303004 Matrix: Soil Collect Date: 20-0CT-15 Receive Date: 14-JAN-16 Collector: Client Moisture: 19.7% ranunctcr ' q~~li.f.i:l!.r. _. Result .. -~inc.~r,l:~i_l)~V... Grnvimetric Solids AST:W D 2216 % Moisliwe "As Received" Moisture 19.7 Rm! Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Correcred" A~tinium-227 lJ -0 0852 +1-0.315 Anlimony-l 25 LI 0.0205 +f-0.128 B1smu1h-212 u 0 402 +/.-0.772 Bismuth-214 0.857 +/-0.\\9& Cesium-137 1 56
- ./.() 170 Cobalt-60 II 0.1>153
+i-0 053 Europium-154 lJ -00163 +/-0 130 Lead-212 1.04 +/.() 144 Le~d-214 I 15 +/-0 213 Potassium-40 137 +/-1 64 Protnctmrnm-231 Lil ll.00 +f-0 607 Radmm-226 0 857 +/.() 198 Radium-228 I 24 .+-].!) 353 Thallium-208 !) 284 +1-0 lO\\I Tin-126 u 0.0515 +/-() 135 Gammaspec. Gamma. Solid "Dry Weight Correc1ed" Aclmium-227 []
- 0. 108
+l-0 363 Ant11m.my-125 u -0.0309 .;./.0.142 13ismuth-212 Ul {]()() -'-/*0.788 Bismulh-214 0.686 +/-0.211 Cesium-137 I 53 +/-0.168 Cobalt-60 l1 O.ll\\54 +/-0.0505 Europium-154 l! 0 0257 +/.(J 135 Lcad-212 0.939 +/-!l 144 Lcad-214 0.801 +/.() 258 Potassium-40 13.2 +/-1.56 'Prolacllmurn-231 l? -D.m\\37 +f-0.838 Radiurn-226 () 686 +/-0 211 Radium-228 0.732 +-1-0 30\\ Tliallium-208 0 322 +/.00872 Tin-126 Cl 0.00 .. i-0 213 Rad Gas Flow Ptoport(onal Countinr; GFPC. Gross A*B, solid Dry Weight Corrected" Alpha 11.5 tf-3.78 Bern 22.3 +J-3.36 MDC Le 0 579 0269 0.239 CJ l IO I 36 tl62ll 0 151 0.1167.5 0.096 0 0435 (I 108 0 fl46& 0.252 () !06 0.126 (I 0588 0 373 0.180 0 392 0 125 1.l6 () 542 0 151 0 0675 O.JJ9 () 150 0.0776 {) 0347 0 206 0()985 0.655 () 3()9 0257 0l19 144 0.659 0 162 0 0731 (I JOO 0 IJ.\\56 0.0934 0.0399 0.273 0.118 0.144 0.0679 ll.18(} o.og36 !) 740 () 303 1.33 0 628 0.161 0.0731 0 306 D.135 0,0821 0 037] () 215 0 Jl)2 ) 87 1.57 3 35 1.54 Project: Client ID: MJ\\.VCOOJ 15 MJWCOOJ ....... T.J>l; '... Rt l'nib DF Analvst Date Time Bah:h Mtd. perccm CXC\\ 01/\\4/16 1202 1537321 +1-0 3lS pCilg RXF2 02/05/16 0719 1537551 2 H-0 l28 pCifg +l-0 794 pC1/g +l-0 213 pCi!g
- /-0 22t) ll, \\()()
pCi/g +/-0.0534 pC1/g +/-0.130 pCt/g +/-0.171 pCi/g +/-ll 231> pCi!g +/-2 02 pCtlg +/-0 632 pCtlg +/-0 213 pCi/g +/-0.399 pCi/g +/-0. 112 pCitg +/-0.136 pC'i/g +/.() 366 pCitg RXF2 () 1/18116 0936 1537548 3 +J-0 142 pC1/g +1-0 949 pC'i!g t/-0.219 pCi/g +/-0.209 0.100 pCi!g +/-0.051 pC1/g . "!"/.l) \\36 pCi!g +/"O \\62 pCtlg +/-0266 pCi/g +!-1.95 pC1lg +/.() ~39 pCi/g +/-0 219 pC1/g +1-0.315 pCilg +l-0.0913 pC'1lg +l-0215 pCi/g +i-4 37 4.00 pC1/g JXB7 0\\/26/l 6 I I.JO 1539464 4 +i-4 56 JO.() pt'1!g
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Company: Address: MJW Technical Services l 5 Hazelwood Drive Suite 112 BufTalo, New York 14228
Contact:
Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.24.R.2 Sample ID: 389303004 Certificate of Analysis Repon Date: .February 10. 2016 Project: MJWCOOl 15 C[ient rD: MJWCOO 1
- \\-JDC Le Tl~.cJollo~~-!~gJ'.~.~ILfy!e~l!l_l.~~-~l"!:-r~. p_cr~or.111.cd_.............. **-... -*........................................ _.....
!\\llcthod De.~cripticm Analyst Date Dry Soil !'rep DI)* SoJ! Prep GL-RAD-A-021 CXC I 01/14/16 T_h_c..f.o.l_l~n~ing f\\i:ia.ly£.k1t! ;'vi cth_c1ds ~ci:-l! pe_rf.o~rn~d..... _. Method Dcscripticm 2 3 4 ASTM D22!6(Modificd) DOE HASL 300. 4.5.2.3!Gn-01-R DOE MASI. 300. 4.5.2.3iGn-O 1-R EPA 900 OtSW846 931Q.'SM 71 IOB Modified Surrogate!fraccr Recovery Test Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma). Time Prep Batch 1202 \\53732[ Batch ID Recovery% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: Address: MJW Corporation 15 Hazelwood Drive Suite l 12
Contact:
~uffalo, New York 14228 Ms. Laurie Losey Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Soil Radioisotopes 3.1.24.R.6 385070019 Water 20-0CT-15 l6:00 05-NOV-15 Client Para!n..~.t~-~ *-...... gu~li_~:!.. **-- -~esult. lJ.nc~_rt_ai ~t~* Rad Gamma Spec Analysis Gammaspec, Gamma, Liquid (Standard List) "As Received" Aclinium-227 U -10 6 +/.26 8 Antimony-125 U 0 696 ~*/-10.5 Cesmm-137 lJ Cobalt-60 ti Europium-154 lJ Proiacumum-231 U Radium-228 U Tm-126 U Rad Gas Flow Proportional Counting GPPC, Gross A/B, liquid "As Received" -1 85 +/-4.78 3 35 +/-4.73 -5.74 +!-11.7 27 I +/-51.0 -16.5 t/-20.6 4.94 tf-l 1A MDC 471 19.0 7.89 9.+7 19.6 94.5 29.9 194 RL 10.0 Alphn U -I 8 +/-1 22 3 5.8 5.0ll Beta lJ 0 222 +/-2.57 4 69 5 00 .:rhe f.~l_l?.~'.!?.~.-~~~-!)'.ti_c_~.1 ~l.et):o~~- ~er_e. p_er_for1_n~~: __.... *-* **-. _..... .Me!!l.~L .....!?.~~cr_iptic;i11. :.... _ **-............................. --*-*-******* EPA 90\\.l 2 EPA 900 OISWS46 9310 Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma). Project: Client JD: l\\UWCOO! 15 MJWCOOI Units __ [)_F A,:1ialyst. Date
- n~1~.!3.~t.~h. Method pC1/L pCi/I.
pC1/l.. µCr.IL pCi/L pC1/L pCi/L pC1fl. pC1/L pCi/L MJH 1 11117115 0657 1521915 JXB7 12/03/15 I 129 1525771 2
GELLABORATOmESLLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Company: Address: MJW Corporation l 5 Hazelwood Drive Suite I 12 Buffalo. New York 14228
Contact:
!'>fa, Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.1.24.R.6 Sample ID: 385070019 Matrix: Water Collect Date: 20-0CT-15 Receive Date: 05-NOV-15 Collector: Client Parameter Rad Gamma Spee Analysis Certificate of Analysis YID(' Le Gammaspec. Gamma.. Liquid fStcmdard Lisi) ':4s Re,*efred" Actmium-227 u -JO 6 +J-16 8 47 I 22 3 +/-27 3 Amimony-125 ll 0 (l9fi +!-10 5 19 0 8 88 +/-10 5 Bi~mulh-212 ll 44 I +1-63 5 Hl8 5{) ll +/-66 7 Btsmuth-214 Ul 0.00 +J-16 8 17.1 804 +l-17 5 Cesium-137 ti -1.85 +/-4.78 7 89 3.66 +/-4 85 Cobalt-60 u 3 35 +1-4 73 947 4 31 +/-4.98 Europmm-154 u -5 74 +/-11 7 19.(l 8.61 +1-12 0 Lead-212
- u.
Q 17 +/-9.46 l3 5 6 41) +/-9 87 Le~d-214 U! 0.00 +/-12 9 15 2 7 17 +f-13.9 Potassium-40 l! -46.l +/-57 9 399 40 7 +/-61.7 Protacunium-23 I u 27.1 +1-51 0 94.5 44 8 +l-52.8 Radmm-228 ll -16.5 +/-206 . 29 9 138 +/-22 1i Thallium-i08 UI 0.00 +f-1 38 670 3 08 +J-7.39 Tin-126 lJ 494 +/-l 1.4 19 4 9JO +/-11.4 Rad Gas Flow Propurtional Counting: GFPC. Gross A.'B. liquid "As Reccfred" Alpha lJ -1.8 +/-1.22 3 58 I 4(> +1-1.22 Beta ll 0 222 +/-2 57 4.69 2 13. +1-2 57 I.~1.!_!o~_lo~vi.111?; :\\~J!.IY'..i~a~ _i\\'le~~!!_d_s_\\V.~.r.e. _per.fo_r.m~~ _. Method Description EPA90l 1 2 GPA 900.0/SW846 9310 Snrro~atcffrlicer Reco\\*ery Test Notes: TPU and Counting Uncertainty are calculated at the 95% confidence !eve! ( 1.96-sigma). Report Date: December 17. 20 l 5 Project: MJWCOOJ 15 Client ID: MJWCOOI pCi/L MlHl 111!7il5 0657 1521915 pCi!L pC1IL pC1/L 100 pCilL pC1iL pC1fL pC1/L pCiiL p(1ll. pCVL pCift pC1/L pC1/L 5 00 pCilL JXB7 12/lB/ I 5 1129 152577 l 2 5 00 pC1/L Batch ID RecoYery% Acceptable Limits
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171-www.gel.com Company: Address:
Contact:
MJW Corporation 15 Hazelwood Drive Suite 112 B11fialo. New York 1422& !vis. Laurie Losey Project: Soil Radioisotopes Client Sample fD: 3.1.24.R.6 Sample ID: 385070019 Matrix: Water Collect Date: 20-0CT- ! 5 Receive Date: 05-NOV-l S Certificate of Analysis Project: Client lD: Report Date: December 17. 2015 MJWC00115 MJWCOOI .. C:<:JH.~~tc:r.:............ ~1\\e.nt_........ .... TI'.r.. _.... !<.!-:-...... ~*.II.~~~... P.~. A11.:~_lyst. pat~ Time __ Hat.~h. !Ylt_d: Parameter Le Rad Gamma Spec A11alysis Gamiiraspl?c. Gamma. Liquid 1S1andard Us!J "As Received" Actinium-227 li -IU.6 +/-26.8 471 2.2 3 +/-27 3 pC1/L M.llfl 11/17115 0657 l.52191S Anlimon) -125 u 0696 +/-I0.5 191) 8 SS +I-JO 5 pCilL Bismuth-2 \\2 lJ 44 I +/-63.5 108 50 ll +/-66.7 pCi!L Bismuth-214 l!I 0.00 +/-16.8 17 I 8 04 +/-17 5 pC1/L Cesrum-137 u -l.85 +l-4.78 7 89 3.66 +/-4 85 10 0 pCilL Cobalt-60 LI 3 35
- -/-4.73 947
.J.Jl +/-4.98 pC1/L Europmm-1.54 u -5.74 +/-l I 7 196 8.6\\ +/-12 0 pCilL Lcad-212 lJ 6 17 +/-9.46 13.5 6 49 +/-9.87 pCi!1. Lead-214 Ul o.on +/-12 9 15 2 7 17 +/-13.'} pCifL Potassmm-40 LI -46.1 +/-57 9 89.\\1 40 7 +i-61 7 pCriL Pro!acunium-231 u 27 I +/-51 0 94-.5 44.8 +/-52.8 p('i*l. Radium-228 u -!6.5 +/-20.6 29.9 13.8 +/-22 0 pC1'1. Thallium-208 U! 0.110 +1-7.38 li.70 3.08 +/-7.39 pCifL Tin-126 () 494 +/-1 i".4 19 4 9 30 +/-\\l 4 pC'i/L Rad Gas Flow Proportional Cou11ting GFf'C. Gross A.'8. liquid As Received" Alpha ll .-1.8 +/-1.22 3.58 J 46 +/-1.22 500 pCi!L Beta u 0222 +/-2.57
- 169 2 13
+1-2 57 5.00 pCliL JXB7 !2i03/15 1129 !525771 .2 T..h.~.. f.~.1~(1\\\\'ing :.\\!1.a..lyti_c_!!!. ~!~.t.b.~d_s. ~H~~'O p~_rror.!11.ccI.. Method Descriptio11 EPA 90! I 2 EPA 900 OiSWS46 9310 Surnigatcffrncer Recovery Test Hatch TD Rccoycry% Acccpt:thic: Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( l.96-sigma).}}