ML18096B006

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Test Rept A28173 for Project, Fuel Oil Spills,Crane & Filter.
ML18096B006
Person / Time
Site: Salem  PSEG icon.png
Issue date: 09/03/1992
From: FIORIGLIO C M
ANALYTIKEM, INC. (FORMERLY S-R ANALYTICAL, INC.)
To:
Shared Package
ML18096B004 List:
References
A28173, A28173-01, A28173-1, NUDOCS 9210020139
Download: ML18096B006 (21)
v • d • e


Text

4f f. *.{. ;; AnalytiKEM An American NuKEM Company TEST REPORT NO. A28173 September 3, 1992 Prepared for: PSE&G P.O. Boz 236 Hail Code N34 Hancocks Bridge, NJ 08038 Attention:

James Sterner AnalytiKEM Inc. 28 Springdale Road Cherry Hill, NJ El8003 6091751-1122 1-800-TRY-LAB1 Fax: 6091751-0824 Project: Fuel Oil Spills, Crane & Filter llevieved

& Approved b/

  • Name: Ca=

Title: QA/QC Manager TABLE OF CONTENTS 4na/ytihE"r1 Page I. List of Certifications 1 II. Definition of Terms 2 III. Sample Designations 3 IV. Methodology 4 v. Laboratory Chronicle 5 VI. Extraction Log 6 VII. Outlier Summary 7 VIII. Analytical Results 8 -11 IX. Quality Control Data 12 -18 I i Test Report A 28173 Page 1 I. Certification AnalytiKEM, Inc. Current Certifications/Regulatory Approvals 4.na/ytil'\E\.1 Tabulated below are the current laboratory certifications that are held by each AnalytiKEM Laboratory.

Analyses performed at multiple AnalytiKEM locations will be noted in the test report. Cherry Hill, NJ Rock Hill, SC !Houston Analytical, TX State Cert # State Cert # State Cert # !Arkansas

  • s. Carolina 46067 N. Dakota R-006 tonnecticut PH-0715 IN. Carolina 316 !Oklahoma 8403 Florida 880985G INew Jersey 79795 !Texas Water Commission
  • No certification numbers are issued for these states.

--.... ) ' .I Test Report A2 8173 Page 2 ' II. Definition of Terms 4nalytikEH DI J MS/MSD NA ND NR RPO RSD u mg/L CCC SPCC PQL TCLP ZHE TC ug Definition Deionized Water Compound was detected at levels below the practical quantitation limit. The level reported is approximate.

Matrix Spike/Matrix Spike Duplicate Analysis not applicable to the sample matrix. Not Detected Not Requested Relative Percent Difference Relative Standard Deviation Compound was analyzed for but not detected.

The preceding number is the practical quantitation limit for the compound.

Milligrams of constituent per liter of TCLP Leachate; equivalent to parts-per-million (ppm). Calibration Check Compound; used to verify the precision of a GC/MS calibration curve. System Performance Check Compound; used to verify the correct operation of a GC/MS instrument.

Practical Quantitation Limit; the minimum level at which compounds can be dependably quantitated.

Toxic Characteristic Leachate Procedure Zero Headspace Extraction Toxic Characteristic Micrograms

... .: Test Report No. A28l?J Page 3 *III. Sample Designations AnalytiKEM Designation A28173-l A28173-2 Client Designation HZS-92-08-01 HZS-92-08-02 Matrix Nonaqueous Nonaqueous 4nalytik.E'H Date Sampled 8/11/92 Note: Samples will be held for 30 days beyond the test report date unless otherwise requested.

... ' . Test Report A2 3173 Page 4 -IV. Methodology 4.na/yt:il(EH All analysis are performed in accordance with methodologies found in the following publications:

Federal Register, Vol. 55, No. 126, June 29, 1990. 40 CFR, Part 216, Appendix 2, Method 1311. Test Methods for Evaluating Solid Waste, USEPA, SW-846, Second Edition, 1982. Test Methods for Evaluating Solid Waste, USEPA, SW-846, Third Edition, 1982. Methods for Chemical Analysis of Water and Wastes, EPA-600/4-79-020, USEPA, March 1983.

.* ** Test Report A2BLiJ Page S e V. Laboratory Chronicle Date Sampled Receipt/Refrigeration TCLP Extractions Zero Headspace Extraction TC Extraction Sample Preparations Semi volatiles Pesticides Metals: General Mercury Analyses Volatiles Semi volatiles Pesticides Metals General Mercury I 8/11/92 8/12/92 8/13/92 8/13/92 8/21/92 8/21/92 8/18/92 8/21/92 8/19 & 8/20/92 8/28/92 8/23/92 8/20/92 8/21/92 Laboratory Manager Review & Approval (Signature) (Printed Name) (Date) J\na/ytil\El1 II NOTE: If fractions are reextracted and reanalyzed because the initial endeavors failed to meet the required quality control criteria, the dates of reextraction and/or reanalysis will be entered in column II additionally.

Test R 6 eport

  • A28173 Page VI. Extraction Log Sample Designation A28173-l A28173-l A28173-2 A28173-2 Zero Headspace Extraction, (g) 25 25 J\na/ytil(E'H TGLP Extraction Fluid Extraction, (g) Volume (ml) 100 100 1 1 1 1 500 2,000 500 2,000
  • .. Test Report No. A2Sl?J Page 7 -Ana/y£ik.

E 'H VII. OUtlier SYmmary: Toxicity Characteristic Leachate Procedure CTCLP) No Compounds were reported above the Regulatory Limits for the following samples: A28173-l A28173-2 HZS-92-08-01 HZS-92-08-02

  • .. *VIII. .. Test Report No. A 28173 e Page 8 -Analytical Results TCLP Organic Analyses 4.nd/yr-ik.

E'H AnalytiKEH A28173-l Client Designation:

HZS-92-08-01 EPA Method Sample Regulatory Number Parameter Blank Result Level Volatile Organics 0043 Vinyl Chloride 0.011 u 0.063 u 0.2 0029 1,1-0ichloroethylene 0.010 u 0.051 u 0.7 0022 Chloroform 0.010 u 0.051 u 6.0 0028 1,2-0ichloroethane 0.010 u '0.053 u 0.5 0035 2-Butanone (MEI<) 0.022 u 0.046 u 200 0019 Carbon Tetrachloride 0.010 u 0.052 u 0.5 0040 Trichloroethylene 0.010 u 0.051 u 0.5 0018 Benzene 0.010 u 0.052 u 0.5 0039 Tetrachloroethylene 0.010 u 0.051 u 0.7 0021 Chlorobenzene 0.011 u 0.051 u 100 Semivolatile Organics 0038 Pyridine 0.071 u 0.071 u 5.0 0027 1,4-0ichlorobenzene 0.016 u 0.016 u 7.5 0023 o-Cresol 0.019 u 0.019 u 200 0024,0025 m,p-Cresol 0.019 u 0.019 u 200 0034 Hexachloroethane 0.023 u 0.023 u 3.0 0036 Nitrobenzene 0.013 u 0.013 u 2.0 0033 Hexachlorobutadiene 0.013 u 0.013 u 0.5 0042 2,4,6-Trichlorophenol 0.018 u 0.018 u 2.0 0041 2,4,5-Trichlorophenol 0.081 u 0.081 u 400 0030 2,4-Dinitrotoluene 0.030 u 0.030 u 0.13 0032 Hexachlorobenzene 0.025 u 0.025 u 0.13 D037 Pentachlorophenol 0.056 u 0.056 u 100 Pesticides 0020 Chlordane 0.0088 u 0.0088 u 0.03 0012 Endrin 0.0022 u 0.0022 u 0.02 0031 Heptachlor 0.0019 u 0.0019 u 0.008 0031 Heptachlor Epoxide 0.0010 u 0.0010 u 0.008 0013 Lindane 0.12 u 0.12 u 0.4 0014 Methoxychlor 0.14 u 0.14 u 10 0015 Toxaphene 0.44 u 0.44 u 0.5 Units (mg/l) (mg/l) (mg/l) Note: All results are corrected for spike recoveries.

Note: The TCLP Herbicides analyses were subcontracted to Laboratory Resources, Inc. Please see the attached copy of their report .

  • *-* Test Report No. A2Bl?J Page 9 e VIII. Analytical Results (Cont'd) TCLP Metals AnalytiKEM Designation:

A28173-l Client Designation:

HZS-92-08-01 EPA Method Number Parameter Blank 0004 Arsenic 0.54 u 0005 Barium 2.2 u 0006 Cadmium 0.11 u 0007 Chromium 0.52 u 0008 Lead 0.56 u 0009 Mercury 0.017 u 0010 0.50 u DOll Silver 0.44 u Units (mg/1) Sample , Result 0. 54 u 0.077 J 0.11 u 0.52 u 0.56 u 0.017 u 0.50 u 0.44 u (mg/1) Note: All results are corrected for spike recoveries.

Analytik.E

'H Regulatory Level 5.0 100 1. 0 5.0 5.0 0.2 1.0 5.0 (mg/l)

Test Report Page 10 e 'VIII. Analytical Results (Cont'd) TCLP Organic Analyses Analyt!KEM Designation:

A28173-2 Client Designation:

HZS-92-08-02 EPA Number Parameter Volatile Organics 0043 0029 0022 0028' 0035 0019 0040 0018 0039 0021 Vinyl Chloride 1,1-0ichloroethylene Chloroform 1,2-0ichloroethane 2-Butanone (MEI<) Carbon Tetrachloride Trichloroethylene Benzene Tetrachloroethylene Chlorobenzene Semivolatile Organics 0038 0027 0023 0024,0025 0034 0036 0033 0042 0041 0030 0032 0037 Pesticides 0020 0012 0031 0031 0013 0014 0015 Units Pyridine 1,4-0ichlorobenzene o-Cresol m,p-Cresol Hexachloroethane Nitrobenzene Hexachlorobutadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2,4-0initrotoluene Hexachlorobenzene Pentachlorophenol Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Method Blank 0. 011 u 0.010 u 0.010 u 0.010 u 0.022 u 0.010 u 0.010 u 0.010 u 0.010 u 0.011 u 0 .071 u 0.016 u 0.019 u 0.019 u 0.023 u 0.013 u 0.013 u 0.018 u 0.081 u 0.030 u 0.025 u 0.056 u 0.0088 u 0.0022 u 0.0019 u 0.0010 u 0.12 u 0.14 u 0.44 u (mg/l) Sample Result 0.063 u 0.051 u 0.051 u 0.053 u 0.046 u 0.052 u 0.051 u 0.052 u 0.051 u 0.051 u 0.071 u 0.016 u 0.019 u 0.019 u 0.023 u 0.013 u 0. 013 u 0.018 u 0.081 u 0.030 u 0.025 u 0.056 u 0.0088 u 0.0022 u 0.0019 u 0.0010 u 0.12 u 0.14 u 0.44 u (mg/l) Note: All results are corrected for spike recoveries.

,4flalyt:ik.E H Regulatory Level 0.2 0. 7 6.0 0.5 200 0.5 0.5 0.5 0.7 100 5.0 7.5 200 200 3.0 2.0 0.5 2.0 400 0.13 0.13 100 0.03 0.02 0.008 0.008 0.4 10 0.5 (mg/l) Note: The TCLP Herbicides analyses were subcontracted to Laboratory Resources, Inc. Please see the attached copy of their report.

-r Test Report A28L73 Page 11 e "lIII. Analytical Results (Cont'd) TGLP Metals 4na/ytikE H AnalytiKEH Designation:

A28173-2 Client Designation:

HZS-92-08-02 EPA Method Sample Regulatory Number Parameter Blank Result Level 0004 Arsenic 0.54 u 0.54 u 5.0 0005 Barium 2.2 u 0.97 J 100 0006 Cadmium 0.11 u 0.11 u 1. 0 0007 Chromium 0.52 u 0.52 u 5.0 0008 Lead 0.56 u 0.56 u 5.0 0009 Mercury 0.017 u 0.017 u 0.2 0010 Selenium 0. 50 u 0.50 u 1.0 0011 Silver 0.44 u 0.44 u 5.0 Units (mg/l) (mg/l) (mg/l) Note: All results are corrected for spike recoveries.

T .-' . Test Report A23L7J Page 12 W IX. Quality Control Data TCLP Procedure Volatile Organics Aqueous Matrix Spike Recovery Data Parameter Vinyl Chloride 1,1-Dichloroethene Chloroform 1,2-Dichloroethane 2-Butanone (MEI<) Carbon Tetrachloride Trichloroethene Benzene Tetrachloroethene Chlorobenzene Units Sample Spiked A27863-6 Alnount of Spike 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 (ug) Recovery MS 92 98 97 97 46 98 98 100 100 94 (%) 4.na/ytik.E l1

l. ., . Test Report A281 Page 13 e IX. Quality Control Data (Cont'd) TCLP Procedure Volatile Organics Aqueous Surrogate Recovery Data Sample l,2-Dichloroethane-d 4 Designation (0.25 ug Added) Method Blank 1 104 Method Blank 2 112 A27863-6 Spike 95 A28173-1 102 A28173-2 99 Units (%) 4.na/ytik.I:

H Surrogate Recovery Toluene-d 8 4-Bromofluorobenzene (0.25 ug Added) (0.25 ug Added) 96 102 99 98 95 100 96 104 103 105 (%) (%)

Test Report A 2317 J ,, Page 14 e IX. Quality Control Data (Cont'd) TCLP Procedure Semivolatile Organics Aqueous Matrix Spike Recovery Data Sample Spiked A28073-l Alnount Recovery Parameter of Spike MS Pyridine 100 14 1,4-Dichlorobenzene 100 61 o-Cresol 200 53 m,p-Cresol 400 54 Hexachloroethane 100 43 Nitrobenzene 100 77 Hexachlorobutadiene 100 77 2,4,6-Trichlorophenol 200 56 2,4,5-Trichlorophenol 200 62 2,4-Dinitrotoluene 100 33 Hexachlorobenzene 100 40 Pentachlorophenol 200 90 Units (ug) (%)

., Test Report Page 15 A2817 3 , IX. Quality Control Data (Cont'd) TCLP Procedure Semivolatile Organics Aqueous Surrogate Recovery Data Sample *2-Fluorophenol Designation (200 ug Added) Method Blank 76 A28073-l Spike 37 A28173-l 91 A28173-2 94 Units (%) Sample Nitrobenzene-d 5 Designation (100 ug Added) Method Blank 86 A28073-l Spike 39 A28173-l 108 A28173-2 102 Units (%) Surrogate Recovery Phenol-d 5 2,4,6-Tribromophenol (200 ug Added) (200 ug Added) 68 106 34 122 108 122 85 109 (%) (%) Surrogate Recovery 2-Fluorobiphenyl Terphenyl-d 14 ClOO ug Added) (100 ug Added) 49 127 60 75 98 76 93 81 (%) (%)

Test Report A28t7J Page 16 e IX. Quality Control Data (Cont'd) TCLP Procedure Pesticides Aqueous Matrix Spike Recovery Data Sample Spiked A28173-l Amount Recovery Parameter of Spike ..l1L gamma-BHC (Lindane) 0.2 34 Heptachlor 0.2 43 Heptachlor Epoxide 0.2 79 Endrin 0.5 93 Methoxychlor 2.0 70 alpha-Chlordane 0.2 78 gamma-Chlordane 0.2 90 Toxaphene

4.0 113 Units (ug) (%) ; Spike performed on sample A28173-2.

,* . Test Report Page 17 e IX. Quality Control Data (Cont'd) TCLP Procedure Pesticides Aqueous Surrogate Recovery Data Sample Designation Method Blank A28173-l Spike (Pest.) A28173-2 Spike (Tox.) A28173-l A28173-2 Units Surrogate Recovery Dibutylchlorendate (1. 0 ug Added) 98 66 39 62 84 (%)

,._.-', -** Test Report A2817J Page 18 e IX. Quality Control Data (Cont'd) TCLP Procedure Metals Aqueous Matrix Spike Recovery Data Sample Spiked A28174-1 Amount Recovery Parameter of Spike Arsenic 100 92 Barium 300 90 Cadmium 300 90 Chromium 300 96 Lead 300 89 Mercury 20 117 Selenium 100 101 Silver 300 90 Units (ug) (%) Spike performed on sample A28173-1.

28 Springdale Road Cherry Hill, New Jersey 08003 (609)751-1122

  • (215)923-2068 rax:

751-0824 Client /15..l. l l, SAMPLE DESIGNATION DATE

'i/11/11....

HZ<i-9J-6f"-02..

thtHL , -1. Field Measurements:

Data Sheets: Y N Filtered:

Y Not Required Relinquished By: ( \*:: r Chain-of-Custody Projed:f"ucL o.*L 'ip1l

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Contact -%-i.-1-i.' i' i' i I I c: MATRIX 1; tf/§G 11 /; /; Ii I ./ 454 South Anderson Ro;:id OTC Rock Hill, South Carolina 2!:1730 (803) 329-9690 Fax: (803) 329-9689 f-k'Df'u . I -PARAMETERS

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  • Field Conditions/Comments:

_________________________

_ Ill. Special Instructions:

___________________________

_ (Detection Limits, Data Package, etc.) Time/Date:

Time/Date:

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