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{{#Wiki_filter:Appendix F -Analytical Results by Area Analytical Results by Area (Area 1)
{{#Wiki_filter:Appendix F -
Sample No. Type 1.1.C1 SAMPLE 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C1 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/29/2015 388092 1/18/2016 388092 1/11/2016 388092 12/29/2015 388092 1/18/2016 388092 1 /11/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 Parameter Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226
Analytical Results by Area
* Area 1 Fraction Method R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 711 OB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 931 O/SM 711 OB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 71108 Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R Result -0.598 12.6 0.143 25.5 0.236 0.740 3.64 0.011 0.0401 0.615 0.910 10.4 -0.936 0.740 0.777 0.121 0.0572 0.039 0.189 9.22 -0.0086 0.00955 14.3 0.00 0.00 0.599 0.814 0.182 0.150 -0.00744 0.00777 0.0456 -0.00312 0.522 0.646 0.878 0.946 9.80 9.18 0.00 0.00 0.599 0.814 Uncertainty GAS 0.511 14952-40-0 3.93 12587-46-1 0.176 3.89 0.678 0.216 0.256 0.0535 0.155 0.142 0.196 1.92 0.826 0.216 0.275 0.102 0.174 0.193 0.366 1.49 0.072 0.0883 1.24 0.409 1.04 0.112 0.159 0.0431 0.0613 0.0317 0.0336 0.0908 0.113 0.104 0.119 0.146 0.168 1.00 1.34 0.561 0.454 0.112 0.159 14234-35-6 12587-47-2 14913-49-6


14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 14952-40-0  
Analytical Results by Area (Area 1)
* Area 1 Sample No. Type  Analyzed  SDG    Parameter        Fraction Method                                  Result  Uncertainty GAS        Units Lab Qua MDL    CRDL CDilution 1% MoistL 1.1.C1    SAMPLE 12/3/2015  385101 Actinium-227    R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.598  0.511      14952-40-0 PCl/G U      0.703        1.00      32 1.1.C1    SAMPLE 12/2/2015  385101 ALPHA            R        EPA 900.0/SW846 9310/SM 7110B  Modified 12.6    3.93        12587-46-1 PCl/G        3.89  4.00  1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Antimony-125    R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.143    0.176      14234-35-6 PCl/G U      0.346        1.00      32 1.1.C1    SAMPLE 12/2/2015  385101 BETA            R        EPA 900.0/SW846 9310/SM 711 OB  Modified 25.5    3.89        12587-47-2 PCl/G        3.57  10.0  1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Bismuth-212      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.236    0.678      14913-49-6 PCl/G U      1.33        1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Bismuth-214      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.740    0.216      14733-03-0 PCl/G        0.200        1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Cesium-137      R        DOE HASL 300, 4.5.2.3/Ga-01-R            3.64    0.256      10045-97-3 PCl/G        0.108  0.100 1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Cobalt-60        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.011    0.0535      10198-40-0 PCl/G U      0.112        1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Europium-154    R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.0401  0.155      15585-10-1 PCl/G U      0.316        1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Lead-212        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.615    0.142      15092-94-1 PCl/G        0.155        1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Lead-214        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.910    0.196      15067-28-4 PCl/G        0.403        1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Potassium-40    R        DOE HASL 300, 4.5.2.3/Ga-01-R            10.4    1.92        13966-00-2 PCl/G        0.958        1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Protactinium-231 R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.936  0.826      14331-85-2 PCl/G U      1.27        1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Radium-226      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.740    0.216      13982-63-3 PCl/G        0.200        1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Radium-228      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.777    0.275      15262-20-1 PCl/G        0.308        1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Thallium-208    R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.121    0.102      14913-50-9 PCl/G        0.0968      1.00      32 1.1.C1    SAMPLE 12/3/2015  385101 Tin-126          R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.0572  0.174                  PCl/G U      0.191        1.00      32 1.1.C2    SAMPLE 12/29/2015 388092 Actinium-227    R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.039    0.193      14952-40-0 PCl/G U      0.355        1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Actinium-227    R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.189    0.366      14952-40-0 PCl/G U      0.420        1.00      17.8 1.1.C2    SAMPLE 1/11/2016  388092 ALPHA            R        EPA 900.0/SW846 931 O/SM 711 OB Modified 9.22    1.49        12587-46-1 PCl/G        1.62  4.00  1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Antimony-125    R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.0086  0.072      14234-35-6 PCl/G U      0.134        1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Antimony-125    R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00955  0.0883      14234-35-6 PCl/G U      0.168        1.00      17.8 1.1.C2    SAMPLE 1/11/2016  388092 BETA            R        EPA 900.0/SW846 9310/SM 71108  Modified 14.3    1.24        12587-47-2 PCl/G        1.28  10.0  1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Bismuth-212      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00    0.409      14913-49-6 PCl/G UI      0.824        1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Bismuth-212      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00    1.04        14913-49-6 PCl/G UI      1.31        1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Bismuth-214      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.599    0.112      14733-03-0 PCl/G        0.0966      1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Bismuth-214      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.814    0.159      14733-03-0 PCl/G        0.119        1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Cesium-137      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.182    0.0431      10045-97-3 PCl/G        0.0264 0.100 1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Cesium-137      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.150    0.0613      10045-97-3 PCl/G        0.0615 0.100 1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Cobalt-60        R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.00744 0.0317      10198-40-0 PCl/G U      0.0575      1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Cobalt-60        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00777  0.0336      10198~40-0 PCl/G U      0.0701      1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Europium-154    R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.0456  0.0908      15585-10-1 PCl/G U      0.180        1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Europium-154    R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.00312 0.113      15585-10-1 PCl/G U      0.220        1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Lead-212        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.522    0.104      15092-94-1 PCl/G      . 0.106        1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Lead-212        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.646    0.119      15092-94-1 PCl/G        0.0981      1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Lead-214        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.878    0.146      15067-28-4 PCl/G        0.106        1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Lead-214        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.946    0.168      15067-28-4 PCl/G        0.296        1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Potassium-40    R        DOE HASL 300, 4.5.2.3/Ga-01-R            9.80    1.00        13966-00-2 PCl/G        0.601        1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Potassium-40    R        DOE HASL 300, 4.5.2.3/Ga-01-R            9.18    1.34        13966-00-2 PCl/G        0.726        1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Protactinium-231 R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00    0.561      14331-85-2 PCl/G U      0.599        1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Protactinium-231 R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00    0.454      14331-85-2 PCl/G UI      0.626        1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Radium-226      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.599    0.112      13982-63-3 PCl/G        0.0966      1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Radium-226      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.814    0.159      13982-63-3 PCl/G        0.119        1.00      17.8


12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 Units Lab Qua MDL CRDL CDilution 1% MoistL PCl/G U 0.703 1.00 32 PCl/G 3.89 4.00 1.00 32 PCl/G U PCl/G PCl/G U PCl/G PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G U PCl/G PCl/G PCl/G PCl/G U PCl/G U PCl/G U PCl/G PCl/G U PCl/G U PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G U PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G UI PCl/G PCl/G 0.346 1.00 32 3.57 10.0 1.00 32 1.33 1.00 32 0.200 1.00 32 0.108 0.100 1.00 32 0.112 1.00 32 0.316 1.00 32 0.155 1.00 32 0.403 1.00 32 0.958 1.27 0.200 0.308 0.0968 0.191 0.355 1.00 32 1.00 32 1.00 32 1.00 32 1.00 32 1.00 32 1.00 17.8 0.420 1.00 17.8 1.62 4.00 1.00 17.8 0.134 1.00 17.8 0.168 1.00 17.8 1.28 10.0 1.00 17.8 0.824 1.00 17.8 1.31 1.00 17.8 0.0966 1.00 17.8 0.119 1.00 17.8 0.0264 0.100 1.00 17.8 0.0615 0.100 1.00 17.8 0.0575 1.00 17.8 0.0701 1.00 17.8 0.180 1.00 17.8 0.220 1.00 17.8 . 0.106 1.00 17.8 0.0981 1.00 17.8 0.106 1.00 17.8 0.296 1.00 17.8 0.601 1.00 17.8 0.726 1.00 17.8 0.599 1.00 17.8 0.626 1.00 17.8 0.0966 1.00 17.8 0.119 1.00 17.8
Area 1 Sample No. Type  Analyzed  SDG    Parameter        Fraction Method                        Result  Uncertainty CAS          Units Lab Qua MDL    CRDL C Dilution I% MoistL 1.1.C2    SAMPLE 12/29/2015 388092 Radium-228      R        DOE HASL 300, 4.5.2.3/Ga-01-0.663    0.230        15262-20-1  PCl/G        0.169        1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Radium-228      R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.685    0.271        15262-20-1  PCl/G        0.223        1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Thallium-208    R        DOE HASL 300, 4.5.2.3/Ga-01-0.248    0.0628      14913-50-9  PCl/G         0.0465        1.00     17.8 1.1.C2    SAMPLE 1/18/2016  388092 Thallium-208    R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.191    0.0609      14913-50-9  PCl/G         0.0636        1.00      17.8 1.1.C2    SAMPLE 12/29/2015 388092 Tin-126          R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.0313  0.0955                  PCl/G U       0.130        1.00      17.8 1.1.C2    SAMPLE 1/18/2016  388092 Tin-126          R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.00    0.0805                  PCl/G UI      0.0794        1.00      17.8 1.1.C2    DUP    12/29/2015 388092 Actinium-227    R        DOE HASL 300, 4.5.2.3/Ga-01-R  -0.0874  0.193        14952-40-0  PCl/G U      0.347        1.00      17.8 1.1.C2    DUP    1/18/2016  388092 Actinium-227    R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.128    0.273        14952-40-0  PCl/G U       0.542        1.00      0 1.1.C2    DUP    12/29/2015 388092 Antimony-125    R        DOE HASL 300, 4.5.2.3/Ga-01-R  -0.015  0.0715      14234-35-6  PCl/G U      0.128        1.00     17.8 1.1.C2    DUP '  1/18/2016  388092 Antimony-125    R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.0514  0.109      '14234-35-6  PCl/G U      0.214        1.00     0 1.1.C2    DUP    12/29/2015 388092 Bismuth-212      R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.00    0.574        14913-49-6  PCl/G UI      0.899        1.00     17.8 1.1.C2    DUP    1/18/2016  388092 Bismuth-212      R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.454    0.581        14913-49-6  PCl/G U      1.21          1.00     0 1.1.C2    DUP    12/29/2015 388092 Bismuth-214      R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.670    0.114        14733-03-0  PCl/G        *0.0968        1.00     17.8 1.1.C2    DUP    1/18/2016  388092 Bismuth-214      R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.776    0.187        14733-03-0 PCl/G        0.148        1.00     0 1.1.C2    DUP    12/29/2015 388092 Cesium-137      R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.174    0.0601      10045-97-3  PCl/G        0.0528 0.100  1.00     17.8 1.1.C2    DUP    1/18/2016  388092 Cesium-137      R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.153    0.0583      10045-97-3  PCl/G        0.075  0.100* 1.00     0 1.1.C2    DUP    12/29/2015 388092 Cobalt-60        R        DOE HASL 300, 4.5.2.3/Ga-01-R  -0.00795 0.0282      10198-40-0  PCl/G U      0.0531        1.00     17.8 1.1.C2     DUP    1/18/2016 388092 Cobalt-60        R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.0129  0.041        10198-40-0  PCl/G U      0.0868        1.00      0 1.1.C2    DUP    12/29/2015 388092 Europium-154    R        DOE HASL 300, 4.5.2.3/Ga-01-R *0.00279  0.0924      15585-10-1 PCl/G U      0:178        1.00      17.8 1.1.C2    DUP    1/18/2016 388092 Europium-154    R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.113    0.154        15585-10-1 PCl/G U      0.300        1.00      0 1.1.C2    DUP    12/29/2015 388092 Lead-212        R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.621    0.0829      15092-94-1 PCl/G        0.0771        1.00      17 .8 1.1.C2    DUP    1/18/2016 388092 Lead-212        R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.677. 0.136        15092-94-1 PCl/G        0.139        1.00      0 1.1.C2    DUP    12/29/2015 388092 Lead-214        R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.749    0.119        15067-28-4  PCl/G        0.214        1.00      17.8 1.1.C2    DUP    1/18/2016 388092 Lead-214        R        DOE HASL 300, 4.5.2.3/Ga-01-R  1.11    0.206        15067-28-4  PCl/G        0.362        1.00      0 1.1.C2    DUP    12/29/2015 388092 Potassium-40    R        DOE HASL 300, 4.5.2.3/Ga-01-R  10.9    1.05        13966-00-2  PCl/G        0.538        1.00      17.8 1.1.C2     DUP    1/18/2016  388092 Potassium-40    R        DOE HASL 300, 4.5.2.3/Ga-01-R  9.98    1.34        13966-00-2  PCl/G        0.805        1.00      0 1.1.C2     DUP    12/29/2015 388092 Protactinium-231 R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.0317  0.440        14331-85-2  PCl/G U      0.713        1.00      17.8 1.1.C2     DUP    1/18/2016  388092 Protactinium-231 R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.00    0.633        14331-85-2  PCl/G UI      1.12          1.00      0 1.1.C2     DUP    12/29/2015 388092 Radium-226      R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.670    0.114        13982-63-3  PCl/G        0.0968        1.00      17.8 1.1.C2     DUP    1/18/2016  388092 Radium-226      R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.776    0.187        13982-63-3  PCl/G        0.148        1.00      0 1.1.C2     DUP    12/29/2015 388092 Radium-228      R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.603    0.199        15262-20-1 PCl/G        0.223        1.00      17.8 1.1.C2     DUP    1/18/2016  388092 Radium-228      R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.667    0.195        15262-20-1 PCl/G        0.242        1.00      0 1.1.C2    DUP    12/29/2015 388092 Thallium-208    R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.178    0.0528      14913-50-9  PCl/G        0.0524        1.00      17 .8 1.1.C2    DUP   1/18/2016  388092 Thallium-208    R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.195    0.0797      14913-50-9  PCl/G        0.0705        1.00      0 1.1.C2    DUP    12/29/2015 388092 Tin-126          R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.00    0.0721                  PCl/G UI      0.101        1.00      17.8 1.1.C2    DUP    1/18/2016 388092 Tin-126          R        DOE HASL 300, 4.5.2.3/Ga-01-R  0.00    0.145                    PCl/G UI      0.181        1.00      0 1.1.R5    SAMPLE 1/11 /2016 387904 Actinium-227    R        EPA901.1                      6.50    33.0        14952-40-0  PCl/L U      57.3          1.00      100 1.1.R5    SAMPLE 1/5/2016  387904 ALPHA            R        EPA 900.0/SW846 9310          -2.57    1.15        12587-46-1  PCl/L U      4.15  5.00  1.00      100 1.1.R5    SAMPLE 1/11/2016  387904 Antimony-125    R        EPA901.1                      -4.3    11.5        14234-35-6  PCl/L U      20.2          1.00      100 1.1.R5    SAMPLE 1/5/2016  387904 BETA            R        EPA 900.0/SW846 9310          -1.44    2.11        12587-47-2  PCl/L U      4.42  5.00  1.00      100 1.1.R5    SAMPLE 1/11/2016  387904 Bismuth-212      R        EPA901.1                      42.3    67.1          14913-49-6 PCl/L U      112          1.00      100 1.1.R5    SAMPLE 1/11/2016  387904 Bismuth-214      R        EPA901.1                      0.00    14.9          14733-03-0 PCl/L UI      18.0          1.00      100 1.1.R5    SAMPLE 1/11/2016  387904 Cesium-137      R        EPA901.1                      0.00    4.73          10045-97-3 PCl/L UI      9.28  10.0  1.00      100
*-.... Sample No. Type Analyzed SDG 1.1.C2 SAMPLE 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.C2 1.1.R5 1.1.R5 1.1.R5 1.1.R5 1.1.R5 1.1.R5 1.1.R5 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE DUP DUP DUP DUP ' DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP SAMPLE SAMPLE SAMPLE SAMPLE 1/18/2016 388092 1 /11 /2016 387904 1 /5/2016 387904 1/11/2016 387904 1/5/2016 387904 SAMPLE 1/11/2016 387904 SAMPLE 1/11/2016 387904 SAMPLE 1/11/2016 387904 Parameter Radium-228
*-....


Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 Antimony-125 Antimony-125 Bismuth-212  
r*
Area 1 Sample No. Type  Analyzed  SDG    Parameter        Fraction Method ,                                *Result  Uncertainty GAS          Units  Lab Qua MDL    CRDL C Dilution I% Maish 1-1 RS    SAMPLE 1/11/2016  387904 Cobalt-60        R        EPA901.1                                  1.92    3.80        10198-40-0  PCl/L  u      7.60          1.00      100 1.1.RS    SAMPLE 1/11/2016  387904 Europium-154    R        EPA901.1                                  -1.34    9.76        15585-10-1  PCl/L  u      18.1          1.00      100 1.1.RS    SAMPLE 1/11/2016  387904 Lead-212        R        EPA901.1                                  6.21    12.8        15092-94-1  PCl/L  u      14.9          1.00      100 1.1.RS    SAMPLE 1/11 /2016 387904 Lead-214        R        EPA901.1                                  0.00    15.6        15067-28-4  PCl/L  UI      19.4          1.00      100 1.1.RS    SAMPLE 1/11/2016  387904 Potassium-40    R        EPA901.1                                  -17      50.7        13966-00 PCl/L  u      89.9          1.00      100 1.1.RS    SAMPLE 1/11/2016  387904 Protactinium-231 R        EPA901.1                                  11.0    60.1        14331-85-2  PCl/L  U      104          1.00      100 1.1.RS    SAMPLE 1/11/2016  387904 Radium-228       R        EPA901.1                                  -2.9    18.7        15262-20-1  PCl/L  U      31.4          1.00      100 1.1.RS    SAMPLE 1/11/2016  387904 Thallium-208     R        EPA901.1                                  0.00    7.58        14913-50-9  PCl/L  UI      5.45          1.00      100 1.1.RS    SAMPLE 1/11/2016  387904 Tin-126          R        EPA901.1                                  1.19    13.6                    PCl/L  U      15.6          1.00      100 1.2.C1    SAMPLE 12/3/2015  385101 Actinium-227    R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.0837  0.370      14952-40-0  PCl/G U        0.680        1.00      24 1.2.C1    SAMPLE 12/2/2015  385101 ALPHA            R        EPA 900.0/SW846 9310/SM 7110B  Modified  7.52    3.29        12587-46-1  PCl/G          3.92  4.00  1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Antimony-125    R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.0215  0.151      14234-35-6  PCl/G U        0.281        1.00      24 1.2.C1    SAMPLE 12/2/2015  385101 BETA            R        EPA 900.0/SW846 931 O/SM 711 OB Modified  24.5    3.81        12587-47-2  PCl/G          3.69  10.0  1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Bismuth-212      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.529    0.674      14913-49-6  PCl/G U        1.36          1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Bismuth-214      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.909    0.223      14733-03-0  PCl/G          0.201        1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Cesium-137      R        DOE HASL 300, 4.5.2.3/Ga-01-R            2.52    0.198      10045-97-3  PCl/G          0.102  0.100  1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Cobalt-60        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.0114  0.0405      10198-40-0  PCl/G U        0.0856        1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Europium-154    R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.0436  0.133      15585-10-1  PCl/G U        0.245        1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Lead-212        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.621    0.130      15092-94-1  PCl/G          0.153        1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Lead-214        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.926    0.244      15067-28-4  PCl/G          0.205        1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Potassium-40    R        DOE HASL 300, 4.5.2.3/Ga-01-R            11.7    1.50        13966-00-2  PCl/G          0.645        1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Protactinium-231 R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.537    0.730      14331-85-2  PCl/G U        1.32          1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Radium-226      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.909    0.223      13982-63-3  PCl/G          0.201        1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Radium-228      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.595    0.287      15262-20-1  PCl/G          0.350        1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Thallium-208     R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.246    0.090      14913-50-9  PCl/G          0.0946        1.00      24 1.2.C1    SAMPLE 12/3/2015  385101 Tin-126         R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.0136  0.166                    PCl/G U        0.262        1.00      24 1.2.C2    SAMPLE 12/29/2015 388092 Actinium-227     R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.035    0.176      14952-40-0  PCl/G U        0.343        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092 Actinium-227     R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.017    0.253      14952-40-0  PCl/G U        0.495        1.00      15.8 1.2.C2    SAMPLE 1/11/2016  388092 ALPHA            R        EPA 900.0/SW846 9310/SM 711DB  Modified  6.53    1.68        12587-46-1  PCl/G          2.29  4.00  1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092 Antimony-125     R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.033    0.0658      14234-35-6  PCl/G U        0.128        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092 Antimony-125     R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00    0.0944      14234-35-6  PCl/G
* UI      0.200        1.00      15.8 1.2.C2    SAMPLE 1/11/2016  388092 BETA            R        EPA 900.0/SW846 9310/SM 711DB  Modified  17.0    1.45        12587-47-2  PCl/G          1.69  10.0  1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092 Bismuth-212      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00    0.523      14913-49-6  PCl/G U        0.852        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092 Bismuth-212      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.557    0.587      14913-49-6  PCl/G U        1.22          1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092 Bismuth-214      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.605    0.126      14733-03-0  PCl/G          0.0912        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092 Bismuth-214      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.730    0.170      14733-03-0  PCl/G          0.131        1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092 Cesium-137      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.139    0.0437      10045-97-3  PCl/G          0.051  0.100  1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092 Cesium-137      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.143    0.0636      10045-97-3  PCl/G          0.0815 0.100  1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092 Cobalt-60        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.0124  0.030      10198-40-0  PCl/G U        0.0606        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092 Cobalt-60        R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.00831 0.0387      10198-40-0  PCl/G U        0.0741        1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092 Europium-154    R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.0494  0.128      15585-10-1  PCl/G U        0.180        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092 Europium-154    R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.0202  0.147      15585-10-1  PCl/G U        0.276        1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092 Lead-212         R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.715    0.132      15092-94-1  PCl/G          0.0806        1.00      15.8


Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Area 1 Fraction Method R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA901.1 R EPA 900.0/SW846 9310 R EPA901.1 R EPA 900.0/SW846 9310 R R R EPA901.1 EPA901.1 EPA901.1 Result 0.663 0.685 0.248 0.191 0.0313 0.00 -0.0874 0.128 -0.015 0.0514 0.00 0.454 0.670 0.776 0.174 0.153 -0.00795 0.0129 *0.00279 0.113 0.621 0.677. 0.749 1.11 10.9 9.98 0.0317 0.00 0.670 0.776 0.603 0.667 0.178 0.195 0.00 0.00 6.50 -2.57 -4.3 -1.44 42.3 0.00 0.00 Uncertainty CAS 0.230 15262-20-1 0.271 15262-20-1 0.0628 0.0609 0.0955 0.0805 0.193 0.273 0.0715 0.109 0.574 0.581 0.114 0.187 0.0601 0.0583 0.0282 0.041 0.0924 0.154 0.0829 0.136 0.119 0.206 1.05 1.34 0.440 0.633 0.114 0.187 0.199 0.195 0.0528 0.0797 0.0721 0.145 14913-50-9 14913-50-9 14952-40-0 14952-40-0 14234-35-6
Area 1 Sample No. Type  Analyzed  SDG      Parameter        Fraction Method                                 Result  *Uncertainty CAS        Units Lab Qua MDL    CRDL C Dilution I% Moist(
'14234-35-6 14913-49-6  
1.2.C2    SAMPLE 1/18/2016  388092  Lead-212        R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.892    0.126      15092-94-1 PCl/G        0.117        1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092  Lead-214        R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.812    0.114      15067-28-4 PCl/G        0.200        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092  Lead-214        R       DOE HASL 300, 4.5.2.3/Ga-01-R           1.03    0.209      15067-28-4 PCl/G        0.131        1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092  Potassium-40    R       DOE HASL 300, 4.5.2.3/Ga-01-R           13.0    1.06        13966-00-2 PCl/G        0.348        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092  Potassium-40    R       DOE HASL 300, 4.5.2.3/Ga-01-R           14.7    1.52        13966-00-2 PCl/G        0.670        1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092  Protactinium-231 R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.00    0.388      14331-85-2 PCl/G U      0.530        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092  Protactinium-231 R       DOE HASL 300, 4.5.2.3/Ga-01-R           -0.189  0.521      14331-85-2 PCl/G U      0.843        1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092  Radium-226      R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.605    0.126      13982-63-3 PCl/G        0.0912        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092  Radium-226      R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.730    0.170      13982-63-3 PCl/G        0.131        1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092  Radium-228      R       DOE HASL 300, 4:5.2.3/Ga-01-R           0.456    0.233      15262-20-1 PCl/G        0.159        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092  Radium-228      R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.932    0.262      15262-20-1 PCl/G        0.295        1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092  Thallium-208    R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.226    0.0531      14913-50-9 PCl/G        0.0445        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092  Thallium-208    R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.185    0.080      14913-50-9 PCl/G        0.0679        1.00      15.8 1.2.C2    SAMPLE 12/29/2015 388092  Tin-126          R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.00    0.107                  PCl/G UI      0.129        1.00      15.8 1.2.C2    SAMPLE 1/18/2016  388092  Tin-126          R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.0471  0.140                  PCl/G U      0.161        1.00      15.8 1.3.C1    SAMPLE 12/3/2015  385101  Actinium-227    R       DOE HASL 300, 4.5.2.3/Ga-01-R           -0.0109  0.316      14952-40-0 PCl/G U      0.586        1.00      39.2 1.3.C1    SAMPLE 12/2/2015  385101  ALPHA            R       EPA 900.0/SW846 9310/SM 7110B Modified  7.84    3.45        12587-46-1 PCl/G        3.97  4.00  1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Antimony-125    R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.00    0.152      14234-35-6 PCl/G UI      0.314        1.00      39.2 1.3.C1    SAMPLE 12/2/2015  385101  BETA            R        EPA 900.0/SW846 9310/SM 7110B Modified  25.6    3.77        12587-47-2 PCl/G        3.05  10.0  1.00*    39.2 1.3.C1    SAMPLE 12/3/2015  385101  Bismuth-212      R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.00    1.08        14913-49-6 PCl/G UI      2.21          1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Bismuth-214      R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.802    0.242      14733-03-0 PCl/G        0.194        1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Cesium-137      R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.406    0.144      10045-97-3 PCl/G        0.109  0.100  1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Cobalt-60        R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.0075  0.0663      10198-40-0 PCl/G U      0.136        1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Europium-154    R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.165    0.187      15585-10-1 PCl/G U      0.429        1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Lead-210        R       DOE HASL 300, 4.5.2.3/Ga-01-R           3.71    0.987      14255-04-0 PCl/G        0.993  4.00  1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Lead-212        R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.879    0.137      15092-94-1 PCl/G        0.156        1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Lead-214        R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.930    0.237      15067-28-4 PCl/G        0.222        1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Potassium-40    R.      DOE HASL 300, 4.5.2.3/Ga-01-R           14.3    2.24        13966-00-2 PCl/G        0.904        1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Protactinium-231 R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.00    0.752      14331-85-2 PCl/G UI      1.33          1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Radium-226      R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.802    0.242      13982-63-3 PCl/G        0.194        1.00      39.2 1".3.C1    SAMPLE 12/3/2015  385101  Radium-228      R       DOE HASL 300, 4.5.2.3/Ga-01-R           1.03    0.402      15262-20-1 PCl/G        0.434        1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Thallium-208    R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.369    0.107      14913-50-9 PCl/G        0.104        1.00      39.2 1.3.C1    SAMPLE 12/3/2015  385101  Tin-126          R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.00    0.0942                PCl/G UI      0.106        1.00      39.2 1.3.C2    SAMPLE 12/29/2015 388092  Actinium-227    R       DOE HASL 300, 4.5.2.3/Ga-01-R           -0.0784  0.231      14952-40-0 PCl/G U      0.413        1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 . Actinium-227    R       DOE HASL 300, 4.5.2.3/Ga-01-R           0.166    0.311      14952-40-0 PCl/G U      0.595        1.00      21.6 1.3.C2    SAMPLE 1/11/2016  388092  ALPHA            R       EPA 900.0/SW84!) 9310/SM 7110B Modified  11.1   2.15        12587-46-1 PCl/G        2.78  4.00  1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092  Antimony-125    R        DOE HASL 300, 4.5.2.3/Ga-01-R          0.0254  0.0997      14234-35-6 PCl/G U      0.166        1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092  Antimony-125    R        DOE HASL 300, 4.5.2.3/Ga-01-R          -0.0396  0.116      14234-35-6 PCl/G U      0.203        1.00      21.6 1.3.C2    SAMPLE 1/11/2016  388092  BETA            R        EPA 900.0/SW846 9310/SM 7110B Modified  21.2    1.80        12587-47-2 PCl/G        2.19  10.0   1.00     21.6 1.3.C2    SAMPLE 12/29/2015 388092  Bismuth-212      R        DOE HASL 300, 4.5.2.3/Ga-01-R            1.39    0.700      14913-49-6 PCl/G        0.852        1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092  Bismuth-212      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00    1.07        14913-49-6 PCl/G UI      1.59          1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092  Bismuth-214      R        DOE HAS.L 300, 4.5.2.3/Ga-01-R          0.678  0.122      14733-03-0 PCl/G        0.114        1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092  Bismuth-214      R        DOE HASL 300, 4.5.2.3/Ga-01-R            1.08    0.170      14733-03-0 PCl/G        0.152        1.00      21.6


14913-49-6 14733-03-0  
Area 1.
* Sample No. Type  Analyzed  SDG    Parameter          Fraction Method                                    Result    Uncertainty CAS        Units Lab Qua MDL    CRDL CDilution I% MoistL 1.3.C2    SAMPLE 12/29/2015 388092 Cesium-137        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.405    0.0678      10045-97-3 PCl/G        0.0658 0.100 1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 Cesium-137        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.482    0.0947      10045-97-3 PCl/G        0.0637 0.100 1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092 Cobalt-60          R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.0136    0.0426      10198-40-0 PCl/G U      0.0739      1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 Cobalt-60          R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.0129    0.0444      10198-40-0 PCl/G U      0.0907      1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092 Europium-154      R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.0175  0.121      15585-10-1 PCl/G U      0.217        1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 Europium-154      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.0122    0.138      15585-10-1 PCl/G U      0.268        1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092 Lead-212          R        DOE HASL 300, 4.5.2.3/Ga-01-R            1.06      0.104      15092-94-1 PCl/G        0.0882      1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 Lead-212          R        DOE HASL 300, 4.5.2.3/Ga-01-R            1.07      0.138      15092-94-1 PCl/G        0.126        1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092 Lead-214          R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.776    0.142      15067-28-4 PCl/G        0.129        1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 Lead-214          R        DOE HASL 300, 4.5.2.3/Ga-01-R            1.31      0.211      15067-28-4 PCl/G        0.388        1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092 Potassium-40      R        DOE HASL 300, 4.5.2.3/Ga-01-R            15.2      1.34        13966-00-2 PCl/G        0.547        1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 Potassium-40      R        DOE HASL 300, 4.5.2.3/Ga-01-R            14.2      1.72        13966-00-2 PCl/G        0.877        1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092 Protactinium-231  R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00      0.728      14331-85-2 PCl/G U      0.769        1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 Protactinium-231  R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00      0.623      14331-85-2 PCl/G UI      1.05        1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092 Radium-226        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.678    0.122      13982-63-3 PCl/G        0.114        1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 Radium-226        R        DOE HASL 300, 4.5.2.3/Ga-01-R            1.08      0.170      13982-63-3 PCl/G        0.152        1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092 Radium-228        R        DOE HASL 300, 4.5.2.3/Ga-01-R            1.03      0.216      15262-20-1 PCl/G        0.215        1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 Radium-228        R        DOE HASL 300, 4.5.2.3/Ga-01-R            1.02      0.272      15262-20-1 PCl/G        0.309        1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092 Thallium-208      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.286    0.0695      14913-50-9 PCl/G        0.0568      1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 Thallium-208      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.360    0.0938      14913-50-9 PCl/G        0.0771      1.00      21.6 1.3.C2    SAMPLE 12/29/2015 388092 Tin-126            R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00      0.113                  PCl/G U      0.111        1.00      21.6 1.3.C2    SAMPLE 1/18/2016  388092 Tin-126            R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.00      0.130                  PCl/G UI      0.209        1.00      21.6 1.3.C5    SAMPLE 12/3/2015  385101 Actinium-227      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.181    0.293      14952-40-0 PCl/G U      0.568        1.00      39.7 1.3.C5    SAMPLE 12/2/2015  385101 ALPHA              R        EPA 900.0/SW846 931 O/SM 711 OB Modified. 9.43      3.61        12587-46-1 PCl/G        3.99  4.00  1.00      39.7 1.3.C5    SAMPLE 11/24/2015 385101 Americium-241      R        DOE EML HASL-300, Am-05-RC Modified      0.0173    0.0593      14596-10-2 PCl/G U      0.110  1.00  1.00      39.7 1.3.C5    SAMPLE 12/3/2015  385101 Antimony-1:~5      R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.0603    0.109      14234-35-6 PCl/G U      0.213        1.00      39. 7 1.3.C5    SAMPLE 12/2/2015  385101 BETA              R        EPA 900.0/SW846 9310/SM 7110B Modified    27.0      3.46        12587-47-2 PCl/G        2.52  10.0  1.00      39.7 1.3.C5    SAMPLE 12/3/2015  385101 Bismuth-212        R        DOE HASL 300, 4.5.2.3/Ga-01-R            1.39      0.906      14913-49-6 PCl/G        1.12        1.00      39. 7 1.3.C5    SAMPLE 12/3/2015  385101 Bismuth-214        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.803    0.169      14733-03-0 PCl/G        0.156        1.00      39.7 1.3.C5    SAMPLE 12/4/2015  385101 Carbon-14        .R        EPA EERF C-01 Modified                    -0.459  *a.768      14762-75-5 PCl/G U      1.32  2.00  1.00      39. 7 1.3.C5    SAMPLE 12/3/2015  385101 Cesium-137        R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.481    0.110      10045-97-3 PCl/G        0.0796 0.100 1.00      39.7 1.3.C5    SAMPLE 12/3/2015  385101 Cobalt-60          R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.00427  0.0412      10198-40-0 PCl/G U      0.0788      1.00      39.7 1.3.C5    SAMPLE 11/24/2015 3B5101 Curium-242        R        DOE EML HASL-300, Am-05-RC Modified      -0.00457  0.0394      OER-100-93 PCliG U      0.0913 1.00  1.00      39.7 1.3.C5    SAMPLE 11/24/2015 385101 Curium-243/244    R        DOE EML HASL-300, Am-05-RC Modified      -0.0119  0.0359                PCl/G U      0.101  1.00  1.00      39.7 1.3.C5    SAMPLE 11/24/2015 385101 Curium-245/246    R        DOE EML HASL-300, Am-05-RC Modified      0.0382    0.0654                PCl/G        0.0573 1.00  1.00      39.7 1.3.C5    SAMPLE 12/3/2015  385101 Europium-154      R        DOE HASL 300, 4.5.2.3/Ga-01-R            -0.0118  0.149      15585-10-1 PCl/G U      0.277        1.00      39.7 1.3.C5    SAMPLE 12/2/2015  385101 lodine-129        R        DOE EML HASL-300,1-01 Modified            0.130    0.576      15046-84-1 PCl/G U      0.928  1.00  1.00      39.7 1.3.C5    SAMPLE 12/3/2015  385101 Lead-212          R        DOE HASL 300, 4.5.2.3/Ga-01-R            0.928    0.127      15092-94-1 PCl/G        0.112        1.00      39.7 1.3.C5    SAMPLE 12/3/2015  385101 Lead-214          R        DOE HASL 300, 4.5.2.3/Ga-01-R            1.08      0.188      15067-28-4 PCl/G        0.384        1.00      39.7 1.3.C5    SAMPLE 11/23/2015 385101 Neptunium-237      R        ASTM C 1476-00 Modified                  -0.146    0.252      13994-20-2 PCl/G U      0.714  1.00  1.00      39.7 1.3.C5    SAMPLE 11/23/2015 385101 Plutonium-238      R        DOE EML HASL-300, Pu-11-RC Modified      -0.0042  0.0363      13981-16-3 PCl/G U      0.084  1.00  1.00      39.7 1.3.C5    SAMPLE 11/23/2015 385101 Plutonium-239/240  R        DOE EML HASL-300, Pu-11-RC Modified      0.0147    0.0734      OER-100-70 PCl/G U      0.147  1.00  1.00      39.7 1.3.C5    SAMPLE 11/25/2015 385101 Plutonium-241      R        DOE EML HASL-300, Pu-11-RC Modified      -1.82    5.80        14119-32-5 PCl/G U      10.1  15.0  1.00      39.7
_J


14733-03-0  
Area 1 Sample No. Type  Analyzed  SDG    P_arameter        Fraction Method                                        Result      Uncertainty CAS            Units .Lab Qua MDL    CRDL C Dilution I% Moistt 1.3.C5    SAMPLE 12/3/2015  385101  Potassium-40      R        DOE HASL 300, 4.5.2.3/Ga-01-R                14.2        1.66        13966-00-2      PCl/G          0.807          1.00      39.7 1.3.C5    SAMPLE 12/3/2015  385101  Protactinium-231  R        DOE HASL 300, 4.5.2.3/Ga-01-R                0.0888      0.620      14331-85-2      PCl/G u        1.03          1.00      39.7 1.3.C5    SAMPLE 12/3/2015  385101  Radium-226        R        DOE HASL 300, 4.5.2.3/Ga-01-R                0.803      0.169      13982-63-3      PCl/G          0.156          1.00      39.7 1.3.C5    SAMPLE 12/3/2015  385101  Radium-228        R        DOE HASL 300, 4.5.2.3/Ga-01-R                0.665      0.382      15262-20-1      PCl/G          0.300          1.00      39.7 1.3.C5    SAMPLE 12/2/2015  385101  Strontium-90      R        EPA 905.0 Modified/DOE RP501 Rev. 1 Modified  -0.321      0.889      10098-97-2      PCl/G u        1.76    2.00  1.00      39.7 1.3.C5    SAMPLE 11/29/2015 385101  Technetium-99    R        DOE EML HASL-300, Tc-02-RC Modified          1.57        2.00        14133-76-7      PCl/G u        3.38    5.00  1.00      39.7 1.3.C5    SAMPLE 12/3/2015  385101  Thallium-208      R        DOE HASL 300, 4.5.2.3/Ga-01-R                0.354      0.0817      14913-50-9      PCl/G          0.0704        1.00      39.7 1.3.C5    SAMPLE 11/24/2015 385101  Thorium-228      R        DOE EML HASL-300, Th-01-RC Modified          1.40        0.595      14274-82-9      PCl/G          0.449  1.00  1.00      39.7 1.3.C5    SAMPLE 11/24/2015 385101  Thorium-229      R        DOE EML HASL-300, Th-01-RC Modified          -0.0406    0.122      15594-54-4      PCl/G U        0.344  1.00  1.00      39.7 1.3.C5    SAMPLE 11/24/2015 385101  Thorium-230      R        DOE EML HASL-300, Th-01-RC Modified          0.803      0.444      14269-63-7      PCl/G          0.343  1.00  1.00      39.7 1.3.C5    SAMPLE 11/24/2015 385101  Thorium-232      R        DOE EML HASL-300, Th-01-RC Modified          0.616      0.381      7440-29-1      PCl/G          0.168  1.00  1.00      39.7 1.3.C5    SAMPLE 12/3/2015  385101" Tin-126          R        DOE HASL 300, 4.5.2.3/Ga-01-R                0.00        0.163                      PCl/G UI      0.130          1.00      39.7 1.3.CS    SAMPLE 12/2/2015  385101  Tritium          R        EPA 906.0 Modified                          2.71      . 2.71        10028-17-8      PCl/G          4.45    6.00  1.00      39.7 1.3.C5    SAMPLE 11/24/2015 385101  Uranium-232      R        DOE EML HASL-300, U-02-RC Modified          0.0644      0.127      14158-29-3      PCl/G U        0.225  1.00  1.00      39.7 1.3.C5    SAMPLE 11/24/2015 385101  Uranium-233/234  R        DOE EML HASL-300, U-02-RC Modified          0.656      0.320      13968-55-3/1391 PCl/G          0.261  1.00  1.00      39.7 1.3.C5    SAMPLE 11/24/2015 385101  Uranium-235/236  R        DOE EML HASL-300, U-02-RC Modified          0.0709      0.121      15117-96-1/139: PCl/G          0.106  1.00  1.00      39.7 1.3.C5    SAMPLE 11/24/2015 385101  Uranium-238      R        DOE EML HASL-300, U-02-RC Modified          0.954      0.367      7440-61-1      PCl/G          0.106  1.00  1.00      39.7 1.3.C6    SAMPLE 12/3/2015  385101  Actinium-227      R        DOE HASL 300, 4.5.2.3/Ga-01-R                -0.478      0.464      14952-40-0      PCl/G u        0.775          1.00      23.6
. 1.3.C6    SAMPLE 12/3/2015  385101  ALPHA.            R      . EPA 900.0/SW846 9310/SM 7110B Modified      7.80        3.22        12587-46-1 . PCl/G          3.91    4.oo  1.00      23.6 1.3.C6    SAMPLE 11/24/2015 385101  Americium-241    R        DOE EML HASL-300, Am-05-RC Modified          0.0315      0.062      14596-10-2      PCl/G          0.0859  1.00  1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Antimony-125      R        DOE HASL 300, 4.5.2.3/Ga-01-R                0.0263      0.202      14234-35-6      PCl/G U        0.369          1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  BETA              R        EPA 900.0/SW846 931 O/SM 711 OB Modified      18.3      2.99        12587-47-2      PCl/G          2.69    10.0  1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Bismuth-212      R        DOE HASL 300, 4.5.2.3/Ga-01-R                0.725      1.19        14913-49-6      PCl/G U        2.35          1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Bismuth-214      R        DOE HASL 300, 4.5.2.3/Ga-01-R                1.08      0.289      14733-03-0     PCl/G          0.255          1.00      23.6 1.3.C6    SAMPLE 12/4/2015  385101  Carbon-14        R        EPA EERF C-01 Modified                      -0.833      0.891      14762-75-5      PCl/G U        1.55    2.00  1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Cesium-137        R        DOE HASL 300, 4.5.2.3/Ga-01-R                0.357      0.122      10045-97-3      PCl/G          0.178  0.100  1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Cobalt-60        R        DOE HASL 300, 4.5.2.3/Ga-01-R                -0.0195    0.0816      10198-40-0      PCl/G U        0.153          1.00      23.6 1.3.C6    SAMPLE 11/24/2015 385101  Curium-242        R        DOE EML HASL-300, Am-05-RC Modified          0.00      0.0412      OER-100-93      PCl/G          0.061.3 1.00  1.00      23.6 1.3.C6    SAMPLE 11/24/2015 385101  Curium-243/244    R        DOE EML HASL-300, Am-05-RC Modified          0.00921    0.0512                      PCl/G U        0.0981  1.00  1.00      23.6.
1.3.C6    SAMPLE 11/24/2015 385101  Curium-245/246    R        DOE EML HASL-300, Am-05-RC Modified          0.0361    0.0709                      PCl/G          0.0983  1.00  1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Europium-154      R        DOE HASL 300, 4.5.2.3/Ga-01-R                -0.00356  0.241      15585-10-1      PCl/G U        0.468          1.00      23.6 1.3.C6    SAMPLE 12/2/2015  385101  lodine-129        R        DOE EML HASL-300,1-01 Modified                0.214      0.383      15046-84-1      PCl/G U        0.769  1.00  1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Lead-212          R        DOE HASL 300, 4.5.2.3/Ga-01-R                1.34      0.197      15092-94-1      PCl/G          0.181          1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Lead-214          R        DOE HASL 300, 4.5.2.3/Ga-01-R                1.09      0.363      15067-28-4      PCl/G          0.580          1.00      23.6 1.3.C6    SAMPLE 11/23/2015 385101  Neptunium-237    R        ASTM C 1476-00 Modified                      -0.0342    0.236      13994-20-2      PCl/G U        0.575  1.00  1.00      23.6 1.3.C6    SAMPLE 11/23/2015 385101  Plutonium-238    R        DOE EML HASL-300, Pu-11-RC Modified          0.00979    0.0544      13981-16-3      PCl/G U        0.104  1.00  1.00      23.6 1.3.C6    SAMPLE 11/23/2015 385101  Plutonium-239/240 R        DOE EML HASL-300, Pu-11-RC Modified          0.00677    0.0799      OER-100-70      PCl/G U        0.168  1.00  1.00      23.6 1.3.C6    SAMPLE 11/25/2015 385101  Plutonium-241    R        DOE EML HASL-300, Pu-11-RC Modified          -2.07      6.40        14119-32-5      PCl/G U        11.2    15.0  1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Potassium-40      R        DOE HASL 300, 4.5.2.3/Ga-01-R                13.9      2.27        13966-00-2      PCl/G          1.05          1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Protactinium-231  R        DOE HASL 300, 4.5.2.3/Ga-01-R                0.801      0.980      14331-85-2      PCl/G U        1.81          1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Radium-226        R        DOE HASL 300, 4.5.2.3/Ga-01-R                1.08      0.289      13982-63-3      PCl/G          0.255          1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101  Radium-228        R        DOE HASL 300, 4.5.2.3/Ga-01-R                0.892      0.403      15262-20-1      PCl/G          0.526          1.00      23.6 1.3.C6    SAMPLE 12/2/2015  385101  Strontium-90      R        EPA 905.0 Modified/DOE RP501 Rev. 1 Modified  -0.122    0.659      10098-97-2      PCl/G U        1.34    2.00  1.00      23.6


10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 33.0 14952-40-0 1.15 12587-46-1 11.5 14234-35-6 2.11 12587-47-2 67.1 14.9 4.73 14913-49-6 14733-03-0 10045-97-3 Units Lab Qua MDL CRDL C Dilution I% MoistL PCl/G 0.169 1.00 17.8 PCl/G 0.223 1.00 17.8 PCl/G PCl/G PCl/G U PCl/G UI PCl/G U PCl/G U PCl/G U PCl/G U PCl/G UI PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G U PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/L U PCl/L U PCl/L U PCl/L U PCl/L U PCl/L UI PCl/L UI 0.0465 1.00 17.8 0.0636 1.00 17.8 0.130 1.00 17.8 0.0794 1.00 17.8 0.347 1.00 17.8 0.542 1.00 0 0.128 1.00 17.8 0.214 1.00 0 0.899 1.00 17.8 1.21 1.00 0 *0.0968 1.00 17.8 0.148 1.00 0 0.0528 0.100 1.00 17.8 0.075 0.100* 1.00 0 0.0531 1.00 17.8 0.0868 1.00 0 0:178 1.00 17.8 0.300 1.00 0 0.0771 1.00 17 .8 0.139 1.00 0 0.214 1.00 17.8 0.362 1.00 0 0.538 1.00 17.8 0.805 1.00 0 0.713 1.00 17.8 1.12 1.00 0 0.0968 1.00 17.8 0.148 1.00 0 0.223 1.00 17.8 0.242 1.00 0 0.0524 1.00 17 .8 0.0705 1.00 0 0.101 1.00 17.8 0.181 1.00 0 57.3 4.15 5.00 20.2 4.42 5.00 112 18.0 9.28 10.0 1.00 1.00 1.00 100 100 100 1.00 100 1.00 100 1.00 100 1.00 100 r* Sample No. Type 1-1 RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.1.RS SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C1 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE Analyzed SDG 1/11/2016 387904 1/11/2016 387904 1/11/2016 387904 1 /11 /2016 387904 1/11/2016 387904 1/11/2016 387904 1/11/2016 387904 1/11/2016 387904 1/11/2016 387904 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/29/2015 388092 1/18/2016 388092 1/11/2016 388092 12/29/2015 388092 1/18/2016 388092 1/11/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 Parameter Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-228 Thallium-208 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Area 1 Fraction Method , R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R EPA901.1 R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 931 O/SM 711 OB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 711DB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 711DB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R
    -"
*Result 1.92 -1.34 6.21 0.00 -17 11.0 -2.9 0.00 1.19 -0.0837 7.52 0.0215 24.5 0.529 0.909 2.52 0.0114 -0.0436 0.621 0.926 11.7 0.537 0.909 0.595 0.246 -0.0136 0.035 0.017 6.53 0.033 0.00 17.0 0.00 0.557 0.605 0.730 0.139 0.143 0.0124 -0.00831 0.0494 -0.0202 0.715 Uncertainty GAS 3.80 10198-40-0 9.76 12.8 15.6 50.7 60.1 18.7 7.58 13.6 0.370 3.29 0.151 3.81 0.674 0.223 0.198 0.0405 0.133 0.130 0.244 1.50 0.730 0.223 0.287 0.090 0.166 0.176 0.253 1.68 0.0658 0.0944 1.45 0.523 0.587 0.126 0.170 0.0437 0.0636 0.030 0.0387 0.128 0.147 0.132 15585-10-1 15092-94-1 15067-28-4 13966-00-2
,-~"
-14331-85-2 15262-20-1 14913-50-9 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6 14733-03-0 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1
Area 1 Sample No. Type  Analyzed  SDG    Parameter      Fraction Method                                Result Uncertainty CAS            Units Lab Qua MDL    CRDL CDilution 1% MoistL 1.3.C6    SAMPLE 11/29/2015 385101 Technetium-99  R        DOE EML HASL-300, Tc-02-RC Modified    1.60  1.76        14133-76-7      PCl/G        2.95  5.00 1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101 Thallium-208    R        DOE HASL 300, 4.5.2.3/Ga-01-R          0.381  0.168      14913-50-9     PCl/G        0.131        1.00      23.6 1.3.C6    SAMPLE 11/24/2015 385101 Thorium-228    R        DOE EML HASL-300, Th-01-RC Modified    0.984  0.482      14274-82-9      PCl/G         0.395  1.00 1.00      23.6 1.3.C6    SAMPLE 11/24/2015 385101 Thorium-229    R        DOE EML HASL-300, Th-01-RC Modified    0.131  0.207      15594-54-4      PCl/G         0.287  1.00  1.00      23.6 1.3.C6    SAMPLE 11/24/2015 385101 Thorium-230    R        DOE EML HASL-300, Th-01-RC Modified    1.16  0.498      14269-63-7      PCl/G         0.286  1.00  1.00      23.6 1.3.C6    SAMPLE 11/24/2015 385101 Thorium-232    R        DOE EML HASL-300, Th-01-RC Modified    0.979  0.452      7440-29-1      PCl/G         0.155  1.00  1.00      23.6 1.3.C6    SAMPLE 12/3/2015  385101 Tin-126        R        DOE HASL 300, 4.5.2.3/Ga-01-R          0.00  0.185                      PCl/G UI      0.177        1.00      23.6 1.3.C6    SAMPLE 12/2/2015  385101 Tritium        R        EPA 906.0 Modified                    1.95  2.00        10028-17-8      PCl/G         3.30  6.00  1.00      23.6 1.3.C6    SAMPLE 11/24/2015 385101 Uranium-232    R        DOE EML HASL-300, U-02-RC Modified    0.0473 0.121      14158-29-3      PCl/G u      0.222  1.00  1.00     23.6 1.3.C6    SAMPLE 11/24/2015 385101 Uranium-233/234 R        DOE EML HASL-300, U-02-RC Modified    0.799  0.301      13968-55-3/1391 PCl/G        0.214  1.00 1.00      23.6 1.3.C6    SAMPLE 11/24/2015 385101 Uranium-235/236 R        DOE EML HASL-300, U-02-RC Modified    0.0469 0.0921      15117-96-1/1391 PCl/G        0.128  1.00 1.00     23.6 1.3.C6    SAMPLE 11/24/2015 385101 Uranium-238    R        DOE EML HASL-300, U-02-RC Modified    1.14  0.345      7440-61-1       PCl/G        0.0796 1.00 1.00     23.6 1.3.C6    MSD    12/3/2015  385101 ALPHA          R        EPA 900.0/SW846 9310/SM 7110B Modified 80.3  13.2        12587-46-1     %            5.73  4.00 1.00     23.6 1.3.C6    MSD    12/3/2015  385101 BETA            R        EPA 900.0/SW846 9310/SM 7110B Modified 97.1   17.4        12587-47-2      %            5.68  10.0 1.00     23.6 1.3.C6    MS    12/2/2015  385101 ALPHA          R        EPA 900.0/SW846 9310/SM 7110B Modified 96.6  16.0       12587-46-1      %            7.76  4.00 1.00     23.6 1.3.C6    MS    12/2/2015  385101 BETA            R        EPA 900.0/SW846 9310/SM 7110B Modified 99.17.4       12587-47-2     %            6.22  10.0 1.00     23.6 1.3.C6    DUP    12/3/2015  385101 ALPHA          R        EPA 900.0/SW846 9310/SM 7110B Modified 11.5  3.55        12587-46-1     PCl/G        3.63  4.00 1.00     23.6 1.3.C6    DUP    12/3/2015  385101 BETA            R        EPA 900.0/SW846 9310/SM 7110B Modified 23.2  2.99        12587-47-2     PCl/G         2.17   10.0 1.00     23.6}}
 
15585-10-1 15092-94-1 Units Lab Qua MDL CRDL C Dilution I% Maish PCl/L PCl/L PCl/L PCl/L PCl/L u 7.60 1.00 100 u 18.1 1.00 100 u 14.9 1.00 100 UI 19.4 1.00 100 u 89.9 1.00 100 PCl/L U PCl/L U PCl/L UI PCl/L U PCl/G U PCl/G PCl/G U PCl/G PCl/G U PCl/G PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G U PCl/G PCl/G PCl/G PCl/G U PCl/G U PCl/G U PCl/G PCl/G U PCl/G
* UI PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G U PCl/G U PCl/G U PCl/G 104 1.00 100 31.4 1.00 100 5.45 1.00 100 15.6 1.00 100 0.680 1.00 24 3.92 4.00 1.00 24 0.281 1.00 24 3.69 10.0 1.00 24 1.36 1.00 24 0.201 1.00 24 0.102 0.100 1.00 24 0.0856 1.00 24 0.245 1.00 24 0.153 0.205 0.645 1.32 0.201 0.350 0.0946 0.262 0.343 0.495 2.29 4.00 0.128 0.200 1.69 10.0 0.852 1.22 0.0912 0.131 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 1.00 1.00 1.00 0.051 0.100 1.00 15.8 15.8 15.8 15.8 15.8 0.0815 0.100 1.00 15.8 0.0606 1.00 15.8 0.0741 1.00 15.8 0.180 1.00 15.8 0.276 1.00 15.8 0.0806 1.00 15.8 Sample No. Type 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.2.C2 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1".3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C1 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 SAMPLE 1.3.C2 1.3.C2 1.3.C2 SAMPLE SAMPLE SAMPLE Analyzed SDG 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/29/2015 388092 1/18/2016 388092 1/11/2016 388092 12/29/2015 388092 1 /18/2016 388092 1/11/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 Parameter Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-210 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 . Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212
 
Bismuth-214 Bismuth-214 Area 1 Fraction Method R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4:5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R. DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW84!)
9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R R R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HAS.L 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.892 0.812 1.03 13.0 14.7 0.00 -0.189 0.605 0.730 0.456 0.932 0.226 0.185 0.00 0.0471 -0.0109 7.84 0.00 25.6 0.00 0.802 0.406 0.0075 0.165 3.71 0.879 0.930 14.3 0.00 0.802 1.03 0.369 0.00 -0.0784 0.166 11.1 0.0254 -0.0396 21.2 1.39 0.00 0.678 1.08 *Uncertainty CAS 0.126 15092-94-1 0.114 0.209 1.06 1.52 0.388 0.521 0.126 0.170 0.233 0.262 0.0531 0.080 0.107 0.140 0.316 3.45 0.152 3.77 1.08 0.242 0.144 0.0663 0.187 0.987 0.137 0.237 2.24 0.752 0.242 0.402 0.107 0.0942 0.231 0.311 2.15 0.0997 0.116 1.80 0.700 1.07 0.122 0.170 15067-28-4 15067-28-4 13966-00-2 13966-00-2 14331-85-2
 
14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 14255-04-0 15092-94-1 15067-28-4
 
13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14234-35-6 14234-35-6 12587-47-2 14913-49-6 14913-49-6
 
14733-03-0 14733-03-0 Units Lab Qua MDL PCl/G 0.117 PCl/G 0.200 PCl/G 0.131 PCl/G 0.348 PCl/G 0.670 PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G U PCl/G U PCl/G PCl/G UI PCl/G PCl/G UI PCl/G PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G UI PCl/G U PCl/G U PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G UI PCl/G PCl/G 0.530 0.843 0.0912 0.131 0.159 0.295 0.0445 0.0679 0.129 0.161 0.586 3.97 0.314 3.05 2.21 0.194 0.109 0.136 0.429 0.993 0.156 0.222 0.904 1.33 0.194 0.434 0.104 0.106 0.413 0.595 2.78 0.166 0.203 2.19 0.852 1.59 0.114 0.152 CRDL C Dilution I% Moist( 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8 1.00 15.8
 
1.00 39.2 4.00 1.00 39.2 1.00 39.2 10.0 1.00* 39.2 1.00 39.2 1.00 39.2 0.100 1.00 39.2 1.00 39.2 1.00 39.2 4.00 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 39.2 1.00 21.6 1.00 21.6 4.00 1.00 21.6 1.00 21.6 1.00 21.6 10.0 1.00 21.6 1.00 21.6 1.00 21.6 1.00 21.6 1.00 21.6 Sample No. Type Analyzed SDG 1.3.C2 SAMPLE 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1.3.C2 SAMPLE 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C2 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE 1/18/2016 388092 12/3/2015 385101 12/2/2015 385101 11/24/2015 385101 12/3/2015 385101 12/2/2015 385101 12/3/2015 385101 12/3/2015 385101 12/4/2015 385101 12/3/2015 385101 12/3/2015 385101 SAMPLE 11/24/2015 3B5101 SAMPLE 11/24/2015 385101 SAMPLE 11/24/2015 385101 SAMPLE 12/3/2015 385101 SAMPLE 12/2/2015 385101 SAMPLE 12/3/2015 385101 SAMPLE 12/3/2015 385101 SAMPLE 11/23/2015 385101 SAMPLE 11/23/2015 385101 SAMPLE 11/23/2015 385101 SAMPLE 11/25/2015 385101 Parameter Cesium-137
 
Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228
 
Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Americium-241 BETA Bismuth-212 Bismuth-214 Carbon-14 Cesium-137 Cobalt-60 Curium-242 Curium-243/244 Curium-245/246 Europium-154 lodine-129 Lead-212 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Area 1.
* Fraction Method R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 931 O/SM 711 OB Modified.
R DOE EML HASL-300, Am-05-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 9310/SM 7110B Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R . R EPA EERF C-01 Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R R R R R R R R
R R R DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R ASTM C 1476-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified Result 0.405 0.482 0.0136 0.0129 -0.0175 0.0122 1.06 1.07 0.776 1.31 15.2 14.2 0.00 0.00 0.678 1.08 1.03 1.02 0.286 0.360 0.00 0.00 0.181 9.43 0.0173 0.0603 27.0 1.39 0.803 -0.459 0.481 -0.00427
-0.00457
-0.0119 0.0382 -0.0118 0.130 0.928 1.08 -0.146 -0.0042 0.0147 -1.82 Uncertainty CAS Units Lab Qua MDL CRDL CDilution I% MoistL 0.0678 10045-97-3 PCl/G 0.0658 0.100 1.00 21.6 0.0947 0.0426 0.0444 0.121 0.138 0.104 0.138 0.142 0.211 1.34 1.72 0.728 0.623 0.122 0.170 0.216 0.272 0.0695 0.0938 0.113 0.130 0.293 3.61 0.0593 0.109 3.46 0.906 0.169 *a.768 0.110 0.0412 0.0394 0.0359 0.0654 0.149 0.576 0.127 0.188 0.252 0.0363 0.0734 5.80 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1
 
15092-94-1
 
15067-28-4 15067-28-4 13966-00-2
 
13966-00-2 14331-85-2
 
14331-85-2
 
13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14913-50-9 14952-40-0 12587-46-1
 
14596-10-2 14234-35-6 12587-47-2 14913-49-6 14733-03-0 14762-75-5 10045-97-3 10198-40-0 PCl/G PCl/G U PCl/G U PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U PCl/G UI PCl/G U PCl/G PCl/G U PCl/G U PCl/G PCl/G PCl/G PCl/G U PCl/G PCl/G U OER-100-93 PCliG U PCl/G U PCl/G 15585-10-1 PCl/G U 15046-84-1 PCl/G U 15092-94-1 PCl/G 15067-28-4 PCl/G 13994-20-2 PCl/G U 13981-16-3 PCl/G U OER-100-70 PCl/G U 14119-32-5 PCl/G U 0.0637 0.100 1.00 21.6 0.0739 1.00 21.6 0.0907 1.00 21.6 0.217 1.00 21.6 0.268 1.00 21.6 0.0882 1.00 21.6 0.126 1.00 21.6 0.129 1.00 21.6 0.388 1.00 21.6 0.547 1.00 21.6 0.877 1.00 21.6 0.769 1.00 21.6 1.05 1.00 21.6 0.114 1.00 21.6 0.152 1.00 21.6 0.215 1.00 21.6 0.309 1.00 21.6 0.0568 1.00 21.6 0.0771 1.00 21.6 0.111 1.00 21.6 0.209 1.00 21.6 0.568 1.00 39.7 3.99 4.00 1.00 39.7 0.110 1.00 1.00 39.7 0.213 1.00 39. 7 2.52 10.0 1.00 39.7 1.12 1.00 39. 7 0.156 1.00 39.7 1.32 2.00 1.00 39. 7 0.0796 0.100 1.00 39.7 0.0788 1.00 39.7 0.0913 1.00 1.00 39.7 0.101 1.00 1.00 39.7 0.0573 1.00 1.00 39.7 0.277 1.00 39.7 0.928 1.00 1.00 39.7 0.112 1.00 39.7 0.384 1.00 39.7 0.714 1.00 1.00 39.7 0.084 1.00 1.00 39.7 0.147 1.00 1.00 39.7 10.1 15.0 1.00 39.7 I _J Sample No. Type 1.3.C5 SAMPLE 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.CS 1.3.C5 1.3.C5 1.3.C5 1.3.C5 1.3.C6 . 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 1.3.C6 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/2/2015 385101 11/29/2015 385101 12/3/2015 385101 11/24/2015 385101 11/24/2015 385101 11/24/2015 385101 11/24/2015 385101 12/3/2015 385101" 12/2/2015 385101 11/24/2015 385101 11/24/2015 385101 11/24/2015 385101 11/24/2015 385101 12/3/2015 385101 12/3/2015 385101 11/24/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/4/2015 385101 12/3/2015 385101 12/3/2015 385101 11/24/2015 385101 11/24/2015 385101 11/24/2015 385101 12/3/2015 385101 12/2/2015 12/3/2015 12/3/2015 385101 385101 385101 11/23/2015 385101 11/23/2015 385101 11/23/2015 385101 11/25/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/3/2015 385101 12/2/2015 385101 P_arameter Potassium-40 Protactinium-231 Radium-226 Radium-228 Strontium-90 Technetium-99 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232 Tin-126 Tritium Uranium-232 Uranium-233/234
 
Uranium-235/236 Uranium-238 Actinium-227 ALPHA. Americium-241 Antimony-125 BETA Bismuth-212 Bismuth-214 Carbon-14 Cesium-137 Cobalt-60 Curium-242 Curium-243/244
 
Curium-245/246 Europium-154 lodine-129 Lead-212 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Protactinium-231 Radium-226 Radium-228 Strontium-90 Area 1 Fraction Method R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified R DOE EML HASL-300, Tc-02-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE EML HASL-300, Th-01-RC Modified R DOE EML HASL-300, Th-01-RC Modified R DOE EML HASL-300, Th-01-RC Modified R DOE EML HASL-300, Th-01-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 906.0 Modified R DOE EML HASL-300, U-02-RC Modified R DOE EML HASL-300, U-02-RC Modified R DOE EML HASL-300, U-02-RC Modified R DOE EML HASL-300, U-02-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R . EPA 900.0/SW846 9310/SM 7110B Modified R DOE EML HASL-300, Am-05-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 900.0/SW846 931 O/SM 711 OB Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA EERF C-01 Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE EML HASL-300, Am-05-RC Modified R DOE EML HASL-300, Am-05-RC Modified R DOE EML HASL-300, Am-05-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE EML HASL-300,1-01 Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R ASTM C 1476-00 Modified R DOE EML HASL-300, Pu-11-RC Modified R DOE EML HASL-300, Pu-11-RC Modified R DOE EML HASL-300, Pu-11-RC Modified R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R DOE HASL 300, 4.5.2.3/Ga-01-R R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Result 14.2 0.0888 0.803 0.665 -0.321 1.57 0.354 1.40 -0.0406 0.803 0.616 0.00 2.71 0.0644 0.656 0.0709 0.954 -0.478 7.80 0.0315 0.0263 18.3 0.725 1.08 -0.833 0.357 -0.0195 0.00 0.00921 0.0361 -0.00356 0.214 1.34 1.09 -0.0342 0.00979 0.00677 -2.07 13.9 0.801 1.08 0.892 -0.122 Uncertainty CAS Units .Lab Qua MDL CRDL C Dilution I% Moistt 1.66 13966-00-2 0.807 1.00 39.7 0.620 14331-85-2 PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G u 1.03 1.00 39.7 0.169 13982-63-3 0.382 15262-20-1 0.156 0.300 1.00 39.7 1.00 39.7 0.889 10098-97-2 u 1.76 2.00 5.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 39.7 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6. 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 23.6 2.00 14133-76-7 u 3.38 0.0817 0.595 0.122 0.444 0.381 0.163 . 2.71 0.127 0.320 0.121 0.367 0.464 3.22 0.062 0.202 2.99 1.19 0.289 0.891 0.122 0.0816 0.0412 0.0512 0.0709 0.241 0.383 0.197 0.363 0.236 0.0544 0.0799 6.40 2.27 0.980 0.289 0.403 0.659 14913-50-9 14274-82-9 15594-54-4 14269-63-7 7440-29-1 10028-17-8 14158-29-3 PCl/G U PCl/G PCl/G PCl/G UI PCl/G PCl/G U 13968-55-3/1391 PCl/G 15117-96-1/139:
PCl/G 7440-61-1 PCl/G 14952-40-0 PCl/G u 12587-46-1 . PCl/G 14596-10-2 PCl/G 14234-35-6
 
12587-47-2 14913-49-6 14733-03-0 14762-75-5 10045-97-3 PCl/G U PCl/G PCl/G U PCl/G PCl/G U PCl/G 10198-40-0 PCl/G U OER-100-93 PCl/G 15585-10-1 15046-84-1 15092-94-1 15067-28-4 PCl/G U PCl/G PCl/G U PCl/G U PCl/G PCl/G 13994-20-2 PCl/G U 13981-16-3 PCl/G U OER-100-70 PCl/G U 14119-32-5 PCl/G U 13966-00-2 14331-85-2
 
13982-63-3 15262-20-1 10098-97-2 PCl/G PCl/G U PCl/G PCl/G PCl/G U 0.0704 0.449 1.00 0.344 1.00 0.343 1.00 0.168 1.00 0.130 4.45 6.00 0.225 1.00 0.261 0.106 0.106 0.775 1.00 1.00 1.00 3.91 4.oo 0.0859 1.00 0.369 2.69 10.0 2.35 1.00 0.255 1.00 1.55 2.00 1.00 0.178 0.100 1.00 0.153 0.061.3 1.00 0.0981 1.00 0.0983 1.00 0.468 0.769 1.00 0.181 0.580 0.575 1.00 0.104 1.00 0.168 1.00 11.2 15.0 1.05 1.81 0.255 0.526 1.34 2.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 
-"
Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty CAS Units Lab Qua MDL CRDL CDilution 1% MoistL 1.3.C6 SAMPLE 11/29/2015 385101 Technetium-99 R DOE EML HASL-300, Tc-02-RC Modified 1.60 1.76 14133-76-7 PCl/G 2.95 5.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.381 0.168 14913-50-9 PCl/G 0.131 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-228 R DOE EML HASL-300, Th-01-RC Modified 0.984 0.482 14274-82-9 PCl/G 0.395 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-229 R DOE EML HASL-300, Th-01-RC Modified 0.131 0.207 15594-54-4 PCl/G 0.287 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-230 R DOE EML HASL-300, Th-01-RC Modified 1.16 0.498 14269-63-7 PCl/G 0.286 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-232 R DOE EML HASL-300, Th-01-RC Modified 0.979 0.452 7440-29-1 PCl/G 0.155 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.185 PCl/G UI 0.177 1.00 23.6 1.3.C6 SAMPLE 12/2/2015 385101 Tritium R EPA 906.0 Modified 1.95 2.00 10028-17-8 PCl/G 3.30 6.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-232 R DOE EML HASL-300, U-02-RC Modified 0.0473 0.121 14158-29-3 PCl/G u 0.222 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-233/234 R DOE EML HASL-300, U-02-RC Modified 0.799 0.301 13968-55-3/1391 PCl/G 0.214 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-235/236 R DOE EML HASL-300, U-02-RC Modified 0.0469 0.0921 15117-96-1/1391 PCl/G 0.128 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-238 R DOE EML HASL-300, U-02-RC Modified 1.14 0.345 7440-61-1 PCl/G 0.0796 1.00 1.00 23.6 1.3.C6 MSD 12/3/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 80.3 13.2 12587-46-1
% 5.73 4.00 1.00 23.6 1.3.C6 MSD 12/3/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 97.1 17.4 12587-47-2
% 5.68 10.0 1.00 23.6 1.3.C6 MS 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 96.6 16.0 12587-46-1
% 7.76 4.00 1.00 23.6 1.3.C6 MS 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 99.8 17.4 12587-47-2
% 6.22 10.0 1.00 23.6 1.3.C6 DUP 12/3/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 11.5 3.55 12587-46-1 PCl/G 3.63 4.00 1.00 23.6 1.3.C6 DUP 12/3/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 23.2 2.99 12587-47-2 PCl/G 2.17 10.0 1.00 23.6}}

Revision as of 12:59, 30 October 2019

Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey Conducted in 2014, Rev. 0, Appendix F, Part 1 of 8
ML16293A888
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Text

Appendix F -

Analytical Results by Area

Analytical Results by Area (Area 1)

  • Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty GAS Units Lab Qua MDL CRDL CDilution 1% MoistL 1.1.C1 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.598 0.511 14952-40-0 PCl/G U 0.703 1.00 32 1.1.C1 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 12.6 3.93 12587-46-1 PCl/G 3.89 4.00 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.143 0.176 14234-35-6 PCl/G U 0.346 1.00 32 1.1.C1 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 711 OB Modified 25.5 3.89 12587-47-2 PCl/G 3.57 10.0 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.236 0.678 14913-49-6 PCl/G U 1.33 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.740 0.216 14733-03-0 PCl/G 0.200 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 3.64 0.256 10045-97-3 PCl/G 0.108 0.100 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.011 0.0535 10198-40-0 PCl/G U 0.112 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0401 0.155 15585-10-1 PCl/G U 0.316 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.615 0.142 15092-94-1 PCl/G 0.155 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.910 0.196 15067-28-4 PCl/G 0.403 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 10.4 1.92 13966-00-2 PCl/G 0.958 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.936 0.826 14331-85-2 PCl/G U 1.27 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.740 0.216 13982-63-3 PCl/G 0.200 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.777 0.275 15262-20-1 PCl/G 0.308 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.121 0.102 14913-50-9 PCl/G 0.0968 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0572 0.174 PCl/G U 0.191 1.00 32 1.1.C2 SAMPLE 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.039 0.193 14952-40-0 PCl/G U 0.355 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.189 0.366 14952-40-0 PCl/G U 0.420 1.00 17.8 1.1.C2 SAMPLE 1/11/2016 388092 ALPHA R EPA 900.0/SW846 931 O/SM 711 OB Modified 9.22 1.49 12587-46-1 PCl/G 1.62 4.00 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0086 0.072 14234-35-6 PCl/G U 0.134 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00955 0.0883 14234-35-6 PCl/G U 0.168 1.00 17.8 1.1.C2 SAMPLE 1/11/2016 388092 BETA R EPA 900.0/SW846 9310/SM 71108 Modified 14.3 1.24 12587-47-2 PCl/G 1.28 10.0 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.409 14913-49-6 PCl/G UI 0.824 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 1.04 14913-49-6 PCl/G UI 1.31 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.599 0.112 14733-03-0 PCl/G 0.0966 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.814 0.159 14733-03-0 PCl/G 0.119 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.182 0.0431 10045-97-3 PCl/G 0.0264 0.100 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.150 0.0613 10045-97-3 PCl/G 0.0615 0.100 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00744 0.0317 10198-40-0 PCl/G U 0.0575 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00777 0.0336 10198~40-0 PCl/G U 0.0701 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0456 0.0908 15585-10-1 PCl/G U 0.180 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00312 0.113 15585-10-1 PCl/G U 0.220 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.522 0.104 15092-94-1 PCl/G . 0.106 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.646 0.119 15092-94-1 PCl/G 0.0981 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.878 0.146 15067-28-4 PCl/G 0.106 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.946 0.168 15067-28-4 PCl/G 0.296 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 9.80 1.00 13966-00-2 PCl/G 0.601 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 9.18 1.34 13966-00-2 PCl/G 0.726 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.561 14331-85-2 PCl/G U 0.599 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.454 14331-85-2 PCl/G UI 0.626 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.599 0.112 13982-63-3 PCl/G 0.0966 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.814 0.159 13982-63-3 PCl/G 0.119 1.00 17.8

Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty CAS Units Lab Qua MDL CRDL C Dilution I% MoistL 1.1.C2 SAMPLE 12/29/2015 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.663 0.230 15262-20-1 PCl/G 0.169 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.685 0.271 15262-20-1 PCl/G 0.223 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.248 0.0628 14913-50-9 PCl/G 0.0465 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.191 0.0609 14913-50-9 PCl/G 0.0636 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0313 0.0955 PCl/G U 0.130 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0805 PCl/G UI 0.0794 1.00 17.8 1.1.C2 DUP 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0874 0.193 14952-40-0 PCl/G U 0.347 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.128 0.273 14952-40-0 PCl/G U 0.542 1.00 0 1.1.C2 DUP 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.015 0.0715 14234-35-6 PCl/G U 0.128 1.00 17.8 1.1.C2 DUP ' 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0514 0.109 '14234-35-6 PCl/G U 0.214 1.00 0 1.1.C2 DUP 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.574 14913-49-6 PCl/G UI 0.899 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.454 0.581 14913-49-6 PCl/G U 1.21 1.00 0 1.1.C2 DUP 12/29/2015 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.670 0.114 14733-03-0 PCl/G *0.0968 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.776 0.187 14733-03-0 PCl/G 0.148 1.00 0 1.1.C2 DUP 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.174 0.0601 10045-97-3 PCl/G 0.0528 0.100 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.153 0.0583 10045-97-3 PCl/G 0.075 0.100* 1.00 0 1.1.C2 DUP 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00795 0.0282 10198-40-0 PCl/G U 0.0531 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0129 0.041 10198-40-0 PCl/G U 0.0868 1.00 0 1.1.C2 DUP 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R *0.00279 0.0924 15585-10-1 PCl/G U 0:178 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.113 0.154 15585-10-1 PCl/G U 0.300 1.00 0 1.1.C2 DUP 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.621 0.0829 15092-94-1 PCl/G 0.0771 1.00 17 .8 1.1.C2 DUP 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.677. 0.136 15092-94-1 PCl/G 0.139 1.00 0 1.1.C2 DUP 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.749 0.119 15067-28-4 PCl/G 0.214 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.11 0.206 15067-28-4 PCl/G 0.362 1.00 0 1.1.C2 DUP 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 10.9 1.05 13966-00-2 PCl/G 0.538 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 9.98 1.34 13966-00-2 PCl/G 0.805 1.00 0 1.1.C2 DUP 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0317 0.440 14331-85-2 PCl/G U 0.713 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.633 14331-85-2 PCl/G UI 1.12 1.00 0 1.1.C2 DUP 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.670 0.114 13982-63-3 PCl/G 0.0968 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.776 0.187 13982-63-3 PCl/G 0.148 1.00 0 1.1.C2 DUP 12/29/2015 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.603 0.199 15262-20-1 PCl/G 0.223 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.667 0.195 15262-20-1 PCl/G 0.242 1.00 0 1.1.C2 DUP 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.178 0.0528 14913-50-9 PCl/G 0.0524 1.00 17 .8 1.1.C2 DUP 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.195 0.0797 14913-50-9 PCl/G 0.0705 1.00 0 1.1.C2 DUP 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0721 PCl/G UI 0.101 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.145 PCl/G UI 0.181 1.00 0 1.1.R5 SAMPLE 1/11 /2016 387904 Actinium-227 R EPA901.1 6.50 33.0 14952-40-0 PCl/L U 57.3 1.00 100 1.1.R5 SAMPLE 1/5/2016 387904 ALPHA R EPA 900.0/SW846 9310 -2.57 1.15 12587-46-1 PCl/L U 4.15 5.00 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Antimony-125 R EPA901.1 -4.3 11.5 14234-35-6 PCl/L U 20.2 1.00 100 1.1.R5 SAMPLE 1/5/2016 387904 BETA R EPA 900.0/SW846 9310 -1.44 2.11 12587-47-2 PCl/L U 4.42 5.00 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Bismuth-212 R EPA901.1 42.3 67.1 14913-49-6 PCl/L U 112 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Bismuth-214 R EPA901.1 0.00 14.9 14733-03-0 PCl/L UI 18.0 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Cesium-137 R EPA901.1 0.00 4.73 10045-97-3 PCl/L UI 9.28 10.0 1.00 100

  • -....

r*

Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method , *Result Uncertainty GAS Units Lab Qua MDL CRDL C Dilution I% Maish 1-1 RS SAMPLE 1/11/2016 387904 Cobalt-60 R EPA901.1 1.92 3.80 10198-40-0 PCl/L u 7.60 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Europium-154 R EPA901.1 -1.34 9.76 15585-10-1 PCl/L u 18.1 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Lead-212 R EPA901.1 6.21 12.8 15092-94-1 PCl/L u 14.9 1.00 100 1.1.RS SAMPLE 1/11 /2016 387904 Lead-214 R EPA901.1 0.00 15.6 15067-28-4 PCl/L UI 19.4 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Potassium-40 R EPA901.1 -17 50.7 13966-00 PCl/L u 89.9 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Protactinium-231 R EPA901.1 11.0 60.1 14331-85-2 PCl/L U 104 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Radium-228 R EPA901.1 -2.9 18.7 15262-20-1 PCl/L U 31.4 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Thallium-208 R EPA901.1 0.00 7.58 14913-50-9 PCl/L UI 5.45 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Tin-126 R EPA901.1 1.19 13.6 PCl/L U 15.6 1.00 100 1.2.C1 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0837 0.370 14952-40-0 PCl/G U 0.680 1.00 24 1.2.C1 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 7.52 3.29 12587-46-1 PCl/G 3.92 4.00 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0215 0.151 14234-35-6 PCl/G U 0.281 1.00 24 1.2.C1 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 931 O/SM 711 OB Modified 24.5 3.81 12587-47-2 PCl/G 3.69 10.0 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.529 0.674 14913-49-6 PCl/G U 1.36 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.909 0.223 14733-03-0 PCl/G 0.201 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 2.52 0.198 10045-97-3 PCl/G 0.102 0.100 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0114 0.0405 10198-40-0 PCl/G U 0.0856 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0436 0.133 15585-10-1 PCl/G U 0.245 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.621 0.130 15092-94-1 PCl/G 0.153 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.926 0.244 15067-28-4 PCl/G 0.205 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 11.7 1.50 13966-00-2 PCl/G 0.645 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.537 0.730 14331-85-2 PCl/G U 1.32 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.909 0.223 13982-63-3 PCl/G 0.201 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.595 0.287 15262-20-1 PCl/G 0.350 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.246 0.090 14913-50-9 PCl/G 0.0946 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0136 0.166 PCl/G U 0.262 1.00 24 1.2.C2 SAMPLE 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.035 0.176 14952-40-0 PCl/G U 0.343 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.017 0.253 14952-40-0 PCl/G U 0.495 1.00 15.8 1.2.C2 SAMPLE 1/11/2016 388092 ALPHA R EPA 900.0/SW846 9310/SM 711DB Modified 6.53 1.68 12587-46-1 PCl/G 2.29 4.00 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.033 0.0658 14234-35-6 PCl/G U 0.128 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0944 14234-35-6 PCl/G

  • UI 0.200 1.00 15.8 1.2.C2 SAMPLE 1/11/2016 388092 BETA R EPA 900.0/SW846 9310/SM 711DB Modified 17.0 1.45 12587-47-2 PCl/G 1.69 10.0 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.523 14913-49-6 PCl/G U 0.852 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.557 0.587 14913-49-6 PCl/G U 1.22 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.605 0.126 14733-03-0 PCl/G 0.0912 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.730 0.170 14733-03-0 PCl/G 0.131 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.139 0.0437 10045-97-3 PCl/G 0.051 0.100 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.143 0.0636 10045-97-3 PCl/G 0.0815 0.100 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0124 0.030 10198-40-0 PCl/G U 0.0606 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00831 0.0387 10198-40-0 PCl/G U 0.0741 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0494 0.128 15585-10-1 PCl/G U 0.180 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0202 0.147 15585-10-1 PCl/G U 0.276 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.715 0.132 15092-94-1 PCl/G 0.0806 1.00 15.8

Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result *Uncertainty CAS Units Lab Qua MDL CRDL C Dilution I% Moist(

1.2.C2 SAMPLE 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.892 0.126 15092-94-1 PCl/G 0.117 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.812 0.114 15067-28-4 PCl/G 0.200 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.03 0.209 15067-28-4 PCl/G 0.131 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 13.0 1.06 13966-00-2 PCl/G 0.348 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 14.7 1.52 13966-00-2 PCl/G 0.670 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.388 14331-85-2 PCl/G U 0.530 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.189 0.521 14331-85-2 PCl/G U 0.843 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.605 0.126 13982-63-3 PCl/G 0.0912 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.730 0.170 13982-63-3 PCl/G 0.131 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Radium-228 R DOE HASL 300, 4:5.2.3/Ga-01-R 0.456 0.233 15262-20-1 PCl/G 0.159 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.932 0.262 15262-20-1 PCl/G 0.295 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.226 0.0531 14913-50-9 PCl/G 0.0445 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.185 0.080 14913-50-9 PCl/G 0.0679 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.107 PCl/G UI 0.129 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0471 0.140 PCl/G U 0.161 1.00 15.8 1.3.C1 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0109 0.316 14952-40-0 PCl/G U 0.586 1.00 39.2 1.3.C1 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 7.84 3.45 12587-46-1 PCl/G 3.97 4.00 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.152 14234-35-6 PCl/G UI 0.314 1.00 39.2 1.3.C1 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 25.6 3.77 12587-47-2 PCl/G 3.05 10.0 1.00* 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 1.08 14913-49-6 PCl/G UI 2.21 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.802 0.242 14733-03-0 PCl/G 0.194 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.406 0.144 10045-97-3 PCl/G 0.109 0.100 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0075 0.0663 10198-40-0 PCl/G U 0.136 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.165 0.187 15585-10-1 PCl/G U 0.429 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Lead-210 R DOE HASL 300, 4.5.2.3/Ga-01-R 3.71 0.987 14255-04-0 PCl/G 0.993 4.00 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.879 0.137 15092-94-1 PCl/G 0.156 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.930 0.237 15067-28-4 PCl/G 0.222 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Potassium-40 R. DOE HASL 300, 4.5.2.3/Ga-01-R 14.3 2.24 13966-00-2 PCl/G 0.904 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.752 14331-85-2 PCl/G UI 1.33 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.802 0.242 13982-63-3 PCl/G 0.194 1.00 39.2 1".3.C1 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.03 0.402 15262-20-1 PCl/G 0.434 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.369 0.107 14913-50-9 PCl/G 0.104 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0942 PCl/G UI 0.106 1.00 39.2 1.3.C2 SAMPLE 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0784 0.231 14952-40-0 PCl/G U 0.413 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 . Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.166 0.311 14952-40-0 PCl/G U 0.595 1.00 21.6 1.3.C2 SAMPLE 1/11/2016 388092 ALPHA R EPA 900.0/SW84!) 9310/SM 7110B Modified 11.1 2.15 12587-46-1 PCl/G 2.78 4.00 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0254 0.0997 14234-35-6 PCl/G U 0.166 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0396 0.116 14234-35-6 PCl/G U 0.203 1.00 21.6 1.3.C2 SAMPLE 1/11/2016 388092 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 21.2 1.80 12587-47-2 PCl/G 2.19 10.0 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.39 0.700 14913-49-6 PCl/G 0.852 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 1.07 14913-49-6 PCl/G UI 1.59 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Bismuth-214 R DOE HAS.L 300, 4.5.2.3/Ga-01-R 0.678 0.122 14733-03-0 PCl/G 0.114 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.170 14733-03-0 PCl/G 0.152 1.00 21.6

Area 1.

  • Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty CAS Units Lab Qua MDL CRDL CDilution I% MoistL 1.3.C2 SAMPLE 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.405 0.0678 10045-97-3 PCl/G 0.0658 0.100 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.482 0.0947 10045-97-3 PCl/G 0.0637 0.100 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0136 0.0426 10198-40-0 PCl/G U 0.0739 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0129 0.0444 10198-40-0 PCl/G U 0.0907 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0175 0.121 15585-10-1 PCl/G U 0.217 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0122 0.138 15585-10-1 PCl/G U 0.268 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.06 0.104 15092-94-1 PCl/G 0.0882 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.07 0.138 15092-94-1 PCl/G 0.126 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.776 0.142 15067-28-4 PCl/G 0.129 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.31 0.211 15067-28-4 PCl/G 0.388 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 15.2 1.34 13966-00-2 PCl/G 0.547 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 14.2 1.72 13966-00-2 PCl/G 0.877 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.728 14331-85-2 PCl/G U 0.769 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.623 14331-85-2 PCl/G UI 1.05 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.678 0.122 13982-63-3 PCl/G 0.114 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.170 13982-63-3 PCl/G 0.152 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.03 0.216 15262-20-1 PCl/G 0.215 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.02 0.272 15262-20-1 PCl/G 0.309 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.286 0.0695 14913-50-9 PCl/G 0.0568 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.360 0.0938 14913-50-9 PCl/G 0.0771 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.113 PCl/G U 0.111 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.130 PCl/G UI 0.209 1.00 21.6 1.3.C5 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.181 0.293 14952-40-0 PCl/G U 0.568 1.00 39.7 1.3.C5 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 931 O/SM 711 OB Modified. 9.43 3.61 12587-46-1 PCl/G 3.99 4.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Americium-241 R DOE EML HASL-300, Am-05-RC Modified 0.0173 0.0593 14596-10-2 PCl/G U 0.110 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Antimony-1:~5 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0603 0.109 14234-35-6 PCl/G U 0.213 1.00 39. 7 1.3.C5 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 27.0 3.46 12587-47-2 PCl/G 2.52 10.0 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.39 0.906 14913-49-6 PCl/G 1.12 1.00 39. 7 1.3.C5 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.803 0.169 14733-03-0 PCl/G 0.156 1.00 39.7 1.3.C5 SAMPLE 12/4/2015 385101 Carbon-14 .R EPA EERF C-01 Modified -0.459 *a.768 14762-75-5 PCl/G U 1.32 2.00 1.00 39. 7 1.3.C5 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.481 0.110 10045-97-3 PCl/G 0.0796 0.100 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00427 0.0412 10198-40-0 PCl/G U 0.0788 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 3B5101 Curium-242 R DOE EML HASL-300, Am-05-RC Modified -0.00457 0.0394 OER-100-93 PCliG U 0.0913 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Curium-243/244 R DOE EML HASL-300, Am-05-RC Modified -0.0119 0.0359 PCl/G U 0.101 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Curium-245/246 R DOE EML HASL-300, Am-05-RC Modified 0.0382 0.0654 PCl/G 0.0573 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0118 0.149 15585-10-1 PCl/G U 0.277 1.00 39.7 1.3.C5 SAMPLE 12/2/2015 385101 lodine-129 R DOE EML HASL-300,1-01 Modified 0.130 0.576 15046-84-1 PCl/G U 0.928 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.928 0.127 15092-94-1 PCl/G 0.112 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.188 15067-28-4 PCl/G 0.384 1.00 39.7 1.3.C5 SAMPLE 11/23/2015 385101 Neptunium-237 R ASTM C 1476-00 Modified -0.146 0.252 13994-20-2 PCl/G U 0.714 1.00 1.00 39.7 1.3.C5 SAMPLE 11/23/2015 385101 Plutonium-238 R DOE EML HASL-300, Pu-11-RC Modified -0.0042 0.0363 13981-16-3 PCl/G U 0.084 1.00 1.00 39.7 1.3.C5 SAMPLE 11/23/2015 385101 Plutonium-239/240 R DOE EML HASL-300, Pu-11-RC Modified 0.0147 0.0734 OER-100-70 PCl/G U 0.147 1.00 1.00 39.7 1.3.C5 SAMPLE 11/25/2015 385101 Plutonium-241 R DOE EML HASL-300, Pu-11-RC Modified -1.82 5.80 14119-32-5 PCl/G U 10.1 15.0 1.00 39.7

_J

Area 1 Sample No. Type Analyzed SDG P_arameter Fraction Method Result Uncertainty CAS Units .Lab Qua MDL CRDL C Dilution I% Moistt 1.3.C5 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 14.2 1.66 13966-00-2 PCl/G 0.807 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0888 0.620 14331-85-2 PCl/G u 1.03 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.803 0.169 13982-63-3 PCl/G 0.156 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.665 0.382 15262-20-1 PCl/G 0.300 1.00 39.7 1.3.C5 SAMPLE 12/2/2015 385101 Strontium-90 R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified -0.321 0.889 10098-97-2 PCl/G u 1.76 2.00 1.00 39.7 1.3.C5 SAMPLE 11/29/2015 385101 Technetium-99 R DOE EML HASL-300, Tc-02-RC Modified 1.57 2.00 14133-76-7 PCl/G u 3.38 5.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.354 0.0817 14913-50-9 PCl/G 0.0704 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-228 R DOE EML HASL-300, Th-01-RC Modified 1.40 0.595 14274-82-9 PCl/G 0.449 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-229 R DOE EML HASL-300, Th-01-RC Modified -0.0406 0.122 15594-54-4 PCl/G U 0.344 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-230 R DOE EML HASL-300, Th-01-RC Modified 0.803 0.444 14269-63-7 PCl/G 0.343 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-232 R DOE EML HASL-300, Th-01-RC Modified 0.616 0.381 7440-29-1 PCl/G 0.168 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101" Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.163 PCl/G UI 0.130 1.00 39.7 1.3.CS SAMPLE 12/2/2015 385101 Tritium R EPA 906.0 Modified 2.71 . 2.71 10028-17-8 PCl/G 4.45 6.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-232 R DOE EML HASL-300, U-02-RC Modified 0.0644 0.127 14158-29-3 PCl/G U 0.225 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-233/234 R DOE EML HASL-300, U-02-RC Modified 0.656 0.320 13968-55-3/1391 PCl/G 0.261 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-235/236 R DOE EML HASL-300, U-02-RC Modified 0.0709 0.121 15117-96-1/139: PCl/G 0.106 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-238 R DOE EML HASL-300, U-02-RC Modified 0.954 0.367 7440-61-1 PCl/G 0.106 1.00 1.00 39.7 1.3.C6 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.478 0.464 14952-40-0 PCl/G u 0.775 1.00 23.6

. 1.3.C6 SAMPLE 12/3/2015 385101 ALPHA. R . EPA 900.0/SW846 9310/SM 7110B Modified 7.80 3.22 12587-46-1 . PCl/G 3.91 4.oo 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Americium-241 R DOE EML HASL-300, Am-05-RC Modified 0.0315 0.062 14596-10-2 PCl/G 0.0859 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0263 0.202 14234-35-6 PCl/G U 0.369 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 BETA R EPA 900.0/SW846 931 O/SM 711 OB Modified 18.3 2.99 12587-47-2 PCl/G 2.69 10.0 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.725 1.19 14913-49-6 PCl/G U 2.35 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.289 14733-03-0 PCl/G 0.255 1.00 23.6 1.3.C6 SAMPLE 12/4/2015 385101 Carbon-14 R EPA EERF C-01 Modified -0.833 0.891 14762-75-5 PCl/G U 1.55 2.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.357 0.122 10045-97-3 PCl/G 0.178 0.100 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0195 0.0816 10198-40-0 PCl/G U 0.153 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Curium-242 R DOE EML HASL-300, Am-05-RC Modified 0.00 0.0412 OER-100-93 PCl/G 0.061.3 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Curium-243/244 R DOE EML HASL-300, Am-05-RC Modified 0.00921 0.0512 PCl/G U 0.0981 1.00 1.00 23.6.

1.3.C6 SAMPLE 11/24/2015 385101 Curium-245/246 R DOE EML HASL-300, Am-05-RC Modified 0.0361 0.0709 PCl/G 0.0983 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00356 0.241 15585-10-1 PCl/G U 0.468 1.00 23.6 1.3.C6 SAMPLE 12/2/2015 385101 lodine-129 R DOE EML HASL-300,1-01 Modified 0.214 0.383 15046-84-1 PCl/G U 0.769 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.34 0.197 15092-94-1 PCl/G 0.181 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.09 0.363 15067-28-4 PCl/G 0.580 1.00 23.6 1.3.C6 SAMPLE 11/23/2015 385101 Neptunium-237 R ASTM C 1476-00 Modified -0.0342 0.236 13994-20-2 PCl/G U 0.575 1.00 1.00 23.6 1.3.C6 SAMPLE 11/23/2015 385101 Plutonium-238 R DOE EML HASL-300, Pu-11-RC Modified 0.00979 0.0544 13981-16-3 PCl/G U 0.104 1.00 1.00 23.6 1.3.C6 SAMPLE 11/23/2015 385101 Plutonium-239/240 R DOE EML HASL-300, Pu-11-RC Modified 0.00677 0.0799 OER-100-70 PCl/G U 0.168 1.00 1.00 23.6 1.3.C6 SAMPLE 11/25/2015 385101 Plutonium-241 R DOE EML HASL-300, Pu-11-RC Modified -2.07 6.40 14119-32-5 PCl/G U 11.2 15.0 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 13.9 2.27 13966-00-2 PCl/G 1.05 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.801 0.980 14331-85-2 PCl/G U 1.81 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.289 13982-63-3 PCl/G 0.255 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.892 0.403 15262-20-1 PCl/G 0.526 1.00 23.6 1.3.C6 SAMPLE 12/2/2015 385101 Strontium-90 R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified -0.122 0.659 10098-97-2 PCl/G U 1.34 2.00 1.00 23.6

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Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty CAS Units Lab Qua MDL CRDL CDilution 1% MoistL 1.3.C6 SAMPLE 11/29/2015 385101 Technetium-99 R DOE EML HASL-300, Tc-02-RC Modified 1.60 1.76 14133-76-7 PCl/G 2.95 5.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.381 0.168 14913-50-9 PCl/G 0.131 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-228 R DOE EML HASL-300, Th-01-RC Modified 0.984 0.482 14274-82-9 PCl/G 0.395 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-229 R DOE EML HASL-300, Th-01-RC Modified 0.131 0.207 15594-54-4 PCl/G 0.287 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-230 R DOE EML HASL-300, Th-01-RC Modified 1.16 0.498 14269-63-7 PCl/G 0.286 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-232 R DOE EML HASL-300, Th-01-RC Modified 0.979 0.452 7440-29-1 PCl/G 0.155 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.185 PCl/G UI 0.177 1.00 23.6 1.3.C6 SAMPLE 12/2/2015 385101 Tritium R EPA 906.0 Modified 1.95 2.00 10028-17-8 PCl/G 3.30 6.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-232 R DOE EML HASL-300, U-02-RC Modified 0.0473 0.121 14158-29-3 PCl/G u 0.222 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-233/234 R DOE EML HASL-300, U-02-RC Modified 0.799 0.301 13968-55-3/1391 PCl/G 0.214 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-235/236 R DOE EML HASL-300, U-02-RC Modified 0.0469 0.0921 15117-96-1/1391 PCl/G 0.128 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-238 R DOE EML HASL-300, U-02-RC Modified 1.14 0.345 7440-61-1 PCl/G 0.0796 1.00 1.00 23.6 1.3.C6 MSD 12/3/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 80.3 13.2 12587-46-1  % 5.73 4.00 1.00 23.6 1.3.C6 MSD 12/3/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 97.1 17.4 12587-47-2  % 5.68 10.0 1.00 23.6 1.3.C6 MS 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 96.6 16.0 12587-46-1  % 7.76 4.00 1.00 23.6 1.3.C6 MS 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 99.8 17.4 12587-47-2  % 6.22 10.0 1.00 23.6 1.3.C6 DUP 12/3/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 11.5 3.55 12587-46-1 PCl/G 3.63 4.00 1.00 23.6 1.3.C6 DUP 12/3/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 23.2 2.99 12587-47-2 PCl/G 2.17 10.0 1.00 23.6