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{{#Wiki_filter:Appendix F -Analytical Results by
{{#Wiki_filter:Appendix F -
Analytical Results by Area
 
Analytical Results by Area (Area 1)
*

Latest revision as of 22:48, 4 February 2020

Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey Conducted in 2014, Rev. 0, Appendix F, Part 1 of 8
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Text

Appendix F -

Analytical Results by Area

Analytical Results by Area (Area 1)

  • Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty GAS Units Lab Qua MDL CRDL CDilution 1% MoistL 1.1.C1 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.598 0.511 14952-40-0 PCl/G U 0.703 1.00 32 1.1.C1 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 12.6 3.93 12587-46-1 PCl/G 3.89 4.00 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.143 0.176 14234-35-6 PCl/G U 0.346 1.00 32 1.1.C1 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 711 OB Modified 25.5 3.89 12587-47-2 PCl/G 3.57 10.0 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.236 0.678 14913-49-6 PCl/G U 1.33 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.740 0.216 14733-03-0 PCl/G 0.200 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 3.64 0.256 10045-97-3 PCl/G 0.108 0.100 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.011 0.0535 10198-40-0 PCl/G U 0.112 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0401 0.155 15585-10-1 PCl/G U 0.316 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.615 0.142 15092-94-1 PCl/G 0.155 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.910 0.196 15067-28-4 PCl/G 0.403 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 10.4 1.92 13966-00-2 PCl/G 0.958 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.936 0.826 14331-85-2 PCl/G U 1.27 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.740 0.216 13982-63-3 PCl/G 0.200 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.777 0.275 15262-20-1 PCl/G 0.308 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.121 0.102 14913-50-9 PCl/G 0.0968 1.00 32 1.1.C1 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0572 0.174 PCl/G U 0.191 1.00 32 1.1.C2 SAMPLE 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.039 0.193 14952-40-0 PCl/G U 0.355 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.189 0.366 14952-40-0 PCl/G U 0.420 1.00 17.8 1.1.C2 SAMPLE 1/11/2016 388092 ALPHA R EPA 900.0/SW846 931 O/SM 711 OB Modified 9.22 1.49 12587-46-1 PCl/G 1.62 4.00 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0086 0.072 14234-35-6 PCl/G U 0.134 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00955 0.0883 14234-35-6 PCl/G U 0.168 1.00 17.8 1.1.C2 SAMPLE 1/11/2016 388092 BETA R EPA 900.0/SW846 9310/SM 71108 Modified 14.3 1.24 12587-47-2 PCl/G 1.28 10.0 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.409 14913-49-6 PCl/G UI 0.824 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 1.04 14913-49-6 PCl/G UI 1.31 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.599 0.112 14733-03-0 PCl/G 0.0966 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.814 0.159 14733-03-0 PCl/G 0.119 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.182 0.0431 10045-97-3 PCl/G 0.0264 0.100 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.150 0.0613 10045-97-3 PCl/G 0.0615 0.100 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00744 0.0317 10198-40-0 PCl/G U 0.0575 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00777 0.0336 10198~40-0 PCl/G U 0.0701 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0456 0.0908 15585-10-1 PCl/G U 0.180 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00312 0.113 15585-10-1 PCl/G U 0.220 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.522 0.104 15092-94-1 PCl/G . 0.106 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.646 0.119 15092-94-1 PCl/G 0.0981 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.878 0.146 15067-28-4 PCl/G 0.106 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.946 0.168 15067-28-4 PCl/G 0.296 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 9.80 1.00 13966-00-2 PCl/G 0.601 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 9.18 1.34 13966-00-2 PCl/G 0.726 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.561 14331-85-2 PCl/G U 0.599 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.454 14331-85-2 PCl/G UI 0.626 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.599 0.112 13982-63-3 PCl/G 0.0966 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.814 0.159 13982-63-3 PCl/G 0.119 1.00 17.8

Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty CAS Units Lab Qua MDL CRDL C Dilution I% MoistL 1.1.C2 SAMPLE 12/29/2015 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.663 0.230 15262-20-1 PCl/G 0.169 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.685 0.271 15262-20-1 PCl/G 0.223 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.248 0.0628 14913-50-9 PCl/G 0.0465 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.191 0.0609 14913-50-9 PCl/G 0.0636 1.00 17.8 1.1.C2 SAMPLE 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0313 0.0955 PCl/G U 0.130 1.00 17.8 1.1.C2 SAMPLE 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0805 PCl/G UI 0.0794 1.00 17.8 1.1.C2 DUP 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0874 0.193 14952-40-0 PCl/G U 0.347 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.128 0.273 14952-40-0 PCl/G U 0.542 1.00 0 1.1.C2 DUP 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.015 0.0715 14234-35-6 PCl/G U 0.128 1.00 17.8 1.1.C2 DUP ' 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0514 0.109 '14234-35-6 PCl/G U 0.214 1.00 0 1.1.C2 DUP 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.574 14913-49-6 PCl/G UI 0.899 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.454 0.581 14913-49-6 PCl/G U 1.21 1.00 0 1.1.C2 DUP 12/29/2015 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.670 0.114 14733-03-0 PCl/G *0.0968 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.776 0.187 14733-03-0 PCl/G 0.148 1.00 0 1.1.C2 DUP 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.174 0.0601 10045-97-3 PCl/G 0.0528 0.100 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.153 0.0583 10045-97-3 PCl/G 0.075 0.100* 1.00 0 1.1.C2 DUP 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00795 0.0282 10198-40-0 PCl/G U 0.0531 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0129 0.041 10198-40-0 PCl/G U 0.0868 1.00 0 1.1.C2 DUP 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R *0.00279 0.0924 15585-10-1 PCl/G U 0:178 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.113 0.154 15585-10-1 PCl/G U 0.300 1.00 0 1.1.C2 DUP 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.621 0.0829 15092-94-1 PCl/G 0.0771 1.00 17 .8 1.1.C2 DUP 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.677. 0.136 15092-94-1 PCl/G 0.139 1.00 0 1.1.C2 DUP 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.749 0.119 15067-28-4 PCl/G 0.214 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.11 0.206 15067-28-4 PCl/G 0.362 1.00 0 1.1.C2 DUP 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 10.9 1.05 13966-00-2 PCl/G 0.538 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 9.98 1.34 13966-00-2 PCl/G 0.805 1.00 0 1.1.C2 DUP 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0317 0.440 14331-85-2 PCl/G U 0.713 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.633 14331-85-2 PCl/G UI 1.12 1.00 0 1.1.C2 DUP 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.670 0.114 13982-63-3 PCl/G 0.0968 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.776 0.187 13982-63-3 PCl/G 0.148 1.00 0 1.1.C2 DUP 12/29/2015 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.603 0.199 15262-20-1 PCl/G 0.223 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.667 0.195 15262-20-1 PCl/G 0.242 1.00 0 1.1.C2 DUP 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.178 0.0528 14913-50-9 PCl/G 0.0524 1.00 17 .8 1.1.C2 DUP 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.195 0.0797 14913-50-9 PCl/G 0.0705 1.00 0 1.1.C2 DUP 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0721 PCl/G UI 0.101 1.00 17.8 1.1.C2 DUP 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.145 PCl/G UI 0.181 1.00 0 1.1.R5 SAMPLE 1/11 /2016 387904 Actinium-227 R EPA901.1 6.50 33.0 14952-40-0 PCl/L U 57.3 1.00 100 1.1.R5 SAMPLE 1/5/2016 387904 ALPHA R EPA 900.0/SW846 9310 -2.57 1.15 12587-46-1 PCl/L U 4.15 5.00 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Antimony-125 R EPA901.1 -4.3 11.5 14234-35-6 PCl/L U 20.2 1.00 100 1.1.R5 SAMPLE 1/5/2016 387904 BETA R EPA 900.0/SW846 9310 -1.44 2.11 12587-47-2 PCl/L U 4.42 5.00 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Bismuth-212 R EPA901.1 42.3 67.1 14913-49-6 PCl/L U 112 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Bismuth-214 R EPA901.1 0.00 14.9 14733-03-0 PCl/L UI 18.0 1.00 100 1.1.R5 SAMPLE 1/11/2016 387904 Cesium-137 R EPA901.1 0.00 4.73 10045-97-3 PCl/L UI 9.28 10.0 1.00 100

r*

Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method , *Result Uncertainty GAS Units Lab Qua MDL CRDL C Dilution I% Maish 1-1 RS SAMPLE 1/11/2016 387904 Cobalt-60 R EPA901.1 1.92 3.80 10198-40-0 PCl/L u 7.60 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Europium-154 R EPA901.1 -1.34 9.76 15585-10-1 PCl/L u 18.1 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Lead-212 R EPA901.1 6.21 12.8 15092-94-1 PCl/L u 14.9 1.00 100 1.1.RS SAMPLE 1/11 /2016 387904 Lead-214 R EPA901.1 0.00 15.6 15067-28-4 PCl/L UI 19.4 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Potassium-40 R EPA901.1 -17 50.7 13966-00 PCl/L u 89.9 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Protactinium-231 R EPA901.1 11.0 60.1 14331-85-2 PCl/L U 104 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Radium-228 R EPA901.1 -2.9 18.7 15262-20-1 PCl/L U 31.4 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Thallium-208 R EPA901.1 0.00 7.58 14913-50-9 PCl/L UI 5.45 1.00 100 1.1.RS SAMPLE 1/11/2016 387904 Tin-126 R EPA901.1 1.19 13.6 PCl/L U 15.6 1.00 100 1.2.C1 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0837 0.370 14952-40-0 PCl/G U 0.680 1.00 24 1.2.C1 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 7.52 3.29 12587-46-1 PCl/G 3.92 4.00 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0215 0.151 14234-35-6 PCl/G U 0.281 1.00 24 1.2.C1 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 931 O/SM 711 OB Modified 24.5 3.81 12587-47-2 PCl/G 3.69 10.0 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.529 0.674 14913-49-6 PCl/G U 1.36 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.909 0.223 14733-03-0 PCl/G 0.201 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 2.52 0.198 10045-97-3 PCl/G 0.102 0.100 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0114 0.0405 10198-40-0 PCl/G U 0.0856 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0436 0.133 15585-10-1 PCl/G U 0.245 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.621 0.130 15092-94-1 PCl/G 0.153 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.926 0.244 15067-28-4 PCl/G 0.205 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 11.7 1.50 13966-00-2 PCl/G 0.645 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.537 0.730 14331-85-2 PCl/G U 1.32 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.909 0.223 13982-63-3 PCl/G 0.201 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.595 0.287 15262-20-1 PCl/G 0.350 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.246 0.090 14913-50-9 PCl/G 0.0946 1.00 24 1.2.C1 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0136 0.166 PCl/G U 0.262 1.00 24 1.2.C2 SAMPLE 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.035 0.176 14952-40-0 PCl/G U 0.343 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.017 0.253 14952-40-0 PCl/G U 0.495 1.00 15.8 1.2.C2 SAMPLE 1/11/2016 388092 ALPHA R EPA 900.0/SW846 9310/SM 711DB Modified 6.53 1.68 12587-46-1 PCl/G 2.29 4.00 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.033 0.0658 14234-35-6 PCl/G U 0.128 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0944 14234-35-6 PCl/G

  • UI 0.200 1.00 15.8 1.2.C2 SAMPLE 1/11/2016 388092 BETA R EPA 900.0/SW846 9310/SM 711DB Modified 17.0 1.45 12587-47-2 PCl/G 1.69 10.0 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.523 14913-49-6 PCl/G U 0.852 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.557 0.587 14913-49-6 PCl/G U 1.22 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.605 0.126 14733-03-0 PCl/G 0.0912 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.730 0.170 14733-03-0 PCl/G 0.131 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.139 0.0437 10045-97-3 PCl/G 0.051 0.100 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.143 0.0636 10045-97-3 PCl/G 0.0815 0.100 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0124 0.030 10198-40-0 PCl/G U 0.0606 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00831 0.0387 10198-40-0 PCl/G U 0.0741 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0494 0.128 15585-10-1 PCl/G U 0.180 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0202 0.147 15585-10-1 PCl/G U 0.276 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.715 0.132 15092-94-1 PCl/G 0.0806 1.00 15.8

Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result *Uncertainty CAS Units Lab Qua MDL CRDL C Dilution I% Moist(

1.2.C2 SAMPLE 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.892 0.126 15092-94-1 PCl/G 0.117 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.812 0.114 15067-28-4 PCl/G 0.200 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.03 0.209 15067-28-4 PCl/G 0.131 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 13.0 1.06 13966-00-2 PCl/G 0.348 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 14.7 1.52 13966-00-2 PCl/G 0.670 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.388 14331-85-2 PCl/G U 0.530 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.189 0.521 14331-85-2 PCl/G U 0.843 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.605 0.126 13982-63-3 PCl/G 0.0912 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.730 0.170 13982-63-3 PCl/G 0.131 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Radium-228 R DOE HASL 300, 4:5.2.3/Ga-01-R 0.456 0.233 15262-20-1 PCl/G 0.159 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.932 0.262 15262-20-1 PCl/G 0.295 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.226 0.0531 14913-50-9 PCl/G 0.0445 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.185 0.080 14913-50-9 PCl/G 0.0679 1.00 15.8 1.2.C2 SAMPLE 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.107 PCl/G UI 0.129 1.00 15.8 1.2.C2 SAMPLE 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0471 0.140 PCl/G U 0.161 1.00 15.8 1.3.C1 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0109 0.316 14952-40-0 PCl/G U 0.586 1.00 39.2 1.3.C1 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 7.84 3.45 12587-46-1 PCl/G 3.97 4.00 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.152 14234-35-6 PCl/G UI 0.314 1.00 39.2 1.3.C1 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 25.6 3.77 12587-47-2 PCl/G 3.05 10.0 1.00* 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 1.08 14913-49-6 PCl/G UI 2.21 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.802 0.242 14733-03-0 PCl/G 0.194 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.406 0.144 10045-97-3 PCl/G 0.109 0.100 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0075 0.0663 10198-40-0 PCl/G U 0.136 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.165 0.187 15585-10-1 PCl/G U 0.429 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Lead-210 R DOE HASL 300, 4.5.2.3/Ga-01-R 3.71 0.987 14255-04-0 PCl/G 0.993 4.00 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.879 0.137 15092-94-1 PCl/G 0.156 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.930 0.237 15067-28-4 PCl/G 0.222 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Potassium-40 R. DOE HASL 300, 4.5.2.3/Ga-01-R 14.3 2.24 13966-00-2 PCl/G 0.904 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.752 14331-85-2 PCl/G UI 1.33 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.802 0.242 13982-63-3 PCl/G 0.194 1.00 39.2 1".3.C1 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.03 0.402 15262-20-1 PCl/G 0.434 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.369 0.107 14913-50-9 PCl/G 0.104 1.00 39.2 1.3.C1 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.0942 PCl/G UI 0.106 1.00 39.2 1.3.C2 SAMPLE 12/29/2015 388092 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0784 0.231 14952-40-0 PCl/G U 0.413 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 . Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.166 0.311 14952-40-0 PCl/G U 0.595 1.00 21.6 1.3.C2 SAMPLE 1/11/2016 388092 ALPHA R EPA 900.0/SW84!) 9310/SM 7110B Modified 11.1 2.15 12587-46-1 PCl/G 2.78 4.00 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0254 0.0997 14234-35-6 PCl/G U 0.166 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0396 0.116 14234-35-6 PCl/G U 0.203 1.00 21.6 1.3.C2 SAMPLE 1/11/2016 388092 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 21.2 1.80 12587-47-2 PCl/G 2.19 10.0 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.39 0.700 14913-49-6 PCl/G 0.852 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 1.07 14913-49-6 PCl/G UI 1.59 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Bismuth-214 R DOE HAS.L 300, 4.5.2.3/Ga-01-R 0.678 0.122 14733-03-0 PCl/G 0.114 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.170 14733-03-0 PCl/G 0.152 1.00 21.6

Area 1.

  • Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty CAS Units Lab Qua MDL CRDL CDilution I% MoistL 1.3.C2 SAMPLE 12/29/2015 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.405 0.0678 10045-97-3 PCl/G 0.0658 0.100 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.482 0.0947 10045-97-3 PCl/G 0.0637 0.100 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0136 0.0426 10198-40-0 PCl/G U 0.0739 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0129 0.0444 10198-40-0 PCl/G U 0.0907 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0175 0.121 15585-10-1 PCl/G U 0.217 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0122 0.138 15585-10-1 PCl/G U 0.268 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.06 0.104 15092-94-1 PCl/G 0.0882 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.07 0.138 15092-94-1 PCl/G 0.126 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.776 0.142 15067-28-4 PCl/G 0.129 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.31 0.211 15067-28-4 PCl/G 0.388 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 15.2 1.34 13966-00-2 PCl/G 0.547 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 14.2 1.72 13966-00-2 PCl/G 0.877 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.728 14331-85-2 PCl/G U 0.769 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.623 14331-85-2 PCl/G UI 1.05 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.678 0.122 13982-63-3 PCl/G 0.114 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.170 13982-63-3 PCl/G 0.152 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.03 0.216 15262-20-1 PCl/G 0.215 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.02 0.272 15262-20-1 PCl/G 0.309 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.286 0.0695 14913-50-9 PCl/G 0.0568 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.360 0.0938 14913-50-9 PCl/G 0.0771 1.00 21.6 1.3.C2 SAMPLE 12/29/2015 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.113 PCl/G U 0.111 1.00 21.6 1.3.C2 SAMPLE 1/18/2016 388092 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.130 PCl/G UI 0.209 1.00 21.6 1.3.C5 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.181 0.293 14952-40-0 PCl/G U 0.568 1.00 39.7 1.3.C5 SAMPLE 12/2/2015 385101 ALPHA R EPA 900.0/SW846 931 O/SM 711 OB Modified. 9.43 3.61 12587-46-1 PCl/G 3.99 4.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Americium-241 R DOE EML HASL-300, Am-05-RC Modified 0.0173 0.0593 14596-10-2 PCl/G U 0.110 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Antimony-1:~5 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0603 0.109 14234-35-6 PCl/G U 0.213 1.00 39. 7 1.3.C5 SAMPLE 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 27.0 3.46 12587-47-2 PCl/G 2.52 10.0 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.39 0.906 14913-49-6 PCl/G 1.12 1.00 39. 7 1.3.C5 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.803 0.169 14733-03-0 PCl/G 0.156 1.00 39.7 1.3.C5 SAMPLE 12/4/2015 385101 Carbon-14 .R EPA EERF C-01 Modified -0.459 *a.768 14762-75-5 PCl/G U 1.32 2.00 1.00 39. 7 1.3.C5 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.481 0.110 10045-97-3 PCl/G 0.0796 0.100 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00427 0.0412 10198-40-0 PCl/G U 0.0788 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 3B5101 Curium-242 R DOE EML HASL-300, Am-05-RC Modified -0.00457 0.0394 OER-100-93 PCliG U 0.0913 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Curium-243/244 R DOE EML HASL-300, Am-05-RC Modified -0.0119 0.0359 PCl/G U 0.101 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Curium-245/246 R DOE EML HASL-300, Am-05-RC Modified 0.0382 0.0654 PCl/G 0.0573 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0118 0.149 15585-10-1 PCl/G U 0.277 1.00 39.7 1.3.C5 SAMPLE 12/2/2015 385101 lodine-129 R DOE EML HASL-300,1-01 Modified 0.130 0.576 15046-84-1 PCl/G U 0.928 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.928 0.127 15092-94-1 PCl/G 0.112 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.188 15067-28-4 PCl/G 0.384 1.00 39.7 1.3.C5 SAMPLE 11/23/2015 385101 Neptunium-237 R ASTM C 1476-00 Modified -0.146 0.252 13994-20-2 PCl/G U 0.714 1.00 1.00 39.7 1.3.C5 SAMPLE 11/23/2015 385101 Plutonium-238 R DOE EML HASL-300, Pu-11-RC Modified -0.0042 0.0363 13981-16-3 PCl/G U 0.084 1.00 1.00 39.7 1.3.C5 SAMPLE 11/23/2015 385101 Plutonium-239/240 R DOE EML HASL-300, Pu-11-RC Modified 0.0147 0.0734 OER-100-70 PCl/G U 0.147 1.00 1.00 39.7 1.3.C5 SAMPLE 11/25/2015 385101 Plutonium-241 R DOE EML HASL-300, Pu-11-RC Modified -1.82 5.80 14119-32-5 PCl/G U 10.1 15.0 1.00 39.7

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Area 1 Sample No. Type Analyzed SDG P_arameter Fraction Method Result Uncertainty CAS Units .Lab Qua MDL CRDL C Dilution I% Moistt 1.3.C5 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 14.2 1.66 13966-00-2 PCl/G 0.807 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0888 0.620 14331-85-2 PCl/G u 1.03 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.803 0.169 13982-63-3 PCl/G 0.156 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.665 0.382 15262-20-1 PCl/G 0.300 1.00 39.7 1.3.C5 SAMPLE 12/2/2015 385101 Strontium-90 R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified -0.321 0.889 10098-97-2 PCl/G u 1.76 2.00 1.00 39.7 1.3.C5 SAMPLE 11/29/2015 385101 Technetium-99 R DOE EML HASL-300, Tc-02-RC Modified 1.57 2.00 14133-76-7 PCl/G u 3.38 5.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.354 0.0817 14913-50-9 PCl/G 0.0704 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-228 R DOE EML HASL-300, Th-01-RC Modified 1.40 0.595 14274-82-9 PCl/G 0.449 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-229 R DOE EML HASL-300, Th-01-RC Modified -0.0406 0.122 15594-54-4 PCl/G U 0.344 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-230 R DOE EML HASL-300, Th-01-RC Modified 0.803 0.444 14269-63-7 PCl/G 0.343 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Thorium-232 R DOE EML HASL-300, Th-01-RC Modified 0.616 0.381 7440-29-1 PCl/G 0.168 1.00 1.00 39.7 1.3.C5 SAMPLE 12/3/2015 385101" Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.163 PCl/G UI 0.130 1.00 39.7 1.3.CS SAMPLE 12/2/2015 385101 Tritium R EPA 906.0 Modified 2.71 . 2.71 10028-17-8 PCl/G 4.45 6.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-232 R DOE EML HASL-300, U-02-RC Modified 0.0644 0.127 14158-29-3 PCl/G U 0.225 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-233/234 R DOE EML HASL-300, U-02-RC Modified 0.656 0.320 13968-55-3/1391 PCl/G 0.261 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-235/236 R DOE EML HASL-300, U-02-RC Modified 0.0709 0.121 15117-96-1/139: PCl/G 0.106 1.00 1.00 39.7 1.3.C5 SAMPLE 11/24/2015 385101 Uranium-238 R DOE EML HASL-300, U-02-RC Modified 0.954 0.367 7440-61-1 PCl/G 0.106 1.00 1.00 39.7 1.3.C6 SAMPLE 12/3/2015 385101 Actinium-227 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.478 0.464 14952-40-0 PCl/G u 0.775 1.00 23.6

. 1.3.C6 SAMPLE 12/3/2015 385101 ALPHA. R . EPA 900.0/SW846 9310/SM 7110B Modified 7.80 3.22 12587-46-1 . PCl/G 3.91 4.oo 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Americium-241 R DOE EML HASL-300, Am-05-RC Modified 0.0315 0.062 14596-10-2 PCl/G 0.0859 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Antimony-125 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.0263 0.202 14234-35-6 PCl/G U 0.369 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 BETA R EPA 900.0/SW846 931 O/SM 711 OB Modified 18.3 2.99 12587-47-2 PCl/G 2.69 10.0 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Bismuth-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.725 1.19 14913-49-6 PCl/G U 2.35 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Bismuth-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.289 14733-03-0 PCl/G 0.255 1.00 23.6 1.3.C6 SAMPLE 12/4/2015 385101 Carbon-14 R EPA EERF C-01 Modified -0.833 0.891 14762-75-5 PCl/G U 1.55 2.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Cesium-137 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.357 0.122 10045-97-3 PCl/G 0.178 0.100 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Cobalt-60 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.0195 0.0816 10198-40-0 PCl/G U 0.153 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Curium-242 R DOE EML HASL-300, Am-05-RC Modified 0.00 0.0412 OER-100-93 PCl/G 0.061.3 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Curium-243/244 R DOE EML HASL-300, Am-05-RC Modified 0.00921 0.0512 PCl/G U 0.0981 1.00 1.00 23.6.

1.3.C6 SAMPLE 11/24/2015 385101 Curium-245/246 R DOE EML HASL-300, Am-05-RC Modified 0.0361 0.0709 PCl/G 0.0983 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Europium-154 R DOE HASL 300, 4.5.2.3/Ga-01-R -0.00356 0.241 15585-10-1 PCl/G U 0.468 1.00 23.6 1.3.C6 SAMPLE 12/2/2015 385101 lodine-129 R DOE EML HASL-300,1-01 Modified 0.214 0.383 15046-84-1 PCl/G U 0.769 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Lead-212 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.34 0.197 15092-94-1 PCl/G 0.181 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Lead-214 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.09 0.363 15067-28-4 PCl/G 0.580 1.00 23.6 1.3.C6 SAMPLE 11/23/2015 385101 Neptunium-237 R ASTM C 1476-00 Modified -0.0342 0.236 13994-20-2 PCl/G U 0.575 1.00 1.00 23.6 1.3.C6 SAMPLE 11/23/2015 385101 Plutonium-238 R DOE EML HASL-300, Pu-11-RC Modified 0.00979 0.0544 13981-16-3 PCl/G U 0.104 1.00 1.00 23.6 1.3.C6 SAMPLE 11/23/2015 385101 Plutonium-239/240 R DOE EML HASL-300, Pu-11-RC Modified 0.00677 0.0799 OER-100-70 PCl/G U 0.168 1.00 1.00 23.6 1.3.C6 SAMPLE 11/25/2015 385101 Plutonium-241 R DOE EML HASL-300, Pu-11-RC Modified -2.07 6.40 14119-32-5 PCl/G U 11.2 15.0 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Potassium-40 R DOE HASL 300, 4.5.2.3/Ga-01-R 13.9 2.27 13966-00-2 PCl/G 1.05 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Protactinium-231 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.801 0.980 14331-85-2 PCl/G U 1.81 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Radium-226 R DOE HASL 300, 4.5.2.3/Ga-01-R 1.08 0.289 13982-63-3 PCl/G 0.255 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Radium-228 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.892 0.403 15262-20-1 PCl/G 0.526 1.00 23.6 1.3.C6 SAMPLE 12/2/2015 385101 Strontium-90 R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified -0.122 0.659 10098-97-2 PCl/G U 1.34 2.00 1.00 23.6

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Area 1 Sample No. Type Analyzed SDG Parameter Fraction Method Result Uncertainty CAS Units Lab Qua MDL CRDL CDilution 1% MoistL 1.3.C6 SAMPLE 11/29/2015 385101 Technetium-99 R DOE EML HASL-300, Tc-02-RC Modified 1.60 1.76 14133-76-7 PCl/G 2.95 5.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Thallium-208 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.381 0.168 14913-50-9 PCl/G 0.131 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-228 R DOE EML HASL-300, Th-01-RC Modified 0.984 0.482 14274-82-9 PCl/G 0.395 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-229 R DOE EML HASL-300, Th-01-RC Modified 0.131 0.207 15594-54-4 PCl/G 0.287 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-230 R DOE EML HASL-300, Th-01-RC Modified 1.16 0.498 14269-63-7 PCl/G 0.286 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Thorium-232 R DOE EML HASL-300, Th-01-RC Modified 0.979 0.452 7440-29-1 PCl/G 0.155 1.00 1.00 23.6 1.3.C6 SAMPLE 12/3/2015 385101 Tin-126 R DOE HASL 300, 4.5.2.3/Ga-01-R 0.00 0.185 PCl/G UI 0.177 1.00 23.6 1.3.C6 SAMPLE 12/2/2015 385101 Tritium R EPA 906.0 Modified 1.95 2.00 10028-17-8 PCl/G 3.30 6.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-232 R DOE EML HASL-300, U-02-RC Modified 0.0473 0.121 14158-29-3 PCl/G u 0.222 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-233/234 R DOE EML HASL-300, U-02-RC Modified 0.799 0.301 13968-55-3/1391 PCl/G 0.214 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-235/236 R DOE EML HASL-300, U-02-RC Modified 0.0469 0.0921 15117-96-1/1391 PCl/G 0.128 1.00 1.00 23.6 1.3.C6 SAMPLE 11/24/2015 385101 Uranium-238 R DOE EML HASL-300, U-02-RC Modified 1.14 0.345 7440-61-1 PCl/G 0.0796 1.00 1.00 23.6 1.3.C6 MSD 12/3/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 80.3 13.2 12587-46-1  % 5.73 4.00 1.00 23.6 1.3.C6 MSD 12/3/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 97.1 17.4 12587-47-2  % 5.68 10.0 1.00 23.6 1.3.C6 MS 12/2/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 96.6 16.0 12587-46-1  % 7.76 4.00 1.00 23.6 1.3.C6 MS 12/2/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 99.8 17.4 12587-47-2  % 6.22 10.0 1.00 23.6 1.3.C6 DUP 12/3/2015 385101 ALPHA R EPA 900.0/SW846 9310/SM 7110B Modified 11.5 3.55 12587-46-1 PCl/G 3.63 4.00 1.00 23.6 1.3.C6 DUP 12/3/2015 385101 BETA R EPA 900.0/SW846 9310/SM 7110B Modified 23.2 2.99 12587-47-2 PCl/G 2.17 10.0 1.00 23.6

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