Text

Revised Final Status Survey (FSS) Report - Phase 2, RR 6100 Isocs Reports Part 1 of 2
	ML19295G791
Person / Time
Site:	Zion File:ZionSolutions icon.png
Issue date:	04/18/2016
From:	; ZionSolutions
To:	; Office of Nuclear Material Safety and Safeguards
Shared Package
ML19295G627	List: ML19295G587; ML19295G611; ML19295G612; ML19295G617; ML19295G621; ML19295G625; ML19295G670; ML19295G674; ML19295G699; ML19295G702; ML19295G705; ML19295G726; ML19295G728; ML19295G734; ML19295G738; ML19295G742; ML19295G747; ML19295G751; ML19295G758; ML19295G764; ML19295G768; ML19295G788; ML19295G791; ML19295G795; ML19295G816; ML19295G818; ML19295G820; ML19295G822; ML19295G826; ML19295G828; ML19295G831; ML19295G837; ML19295G841; ML19295G843; ML19295G846; ML19295G850; ML19295G853; ML19295G855; ML19295G857; ML19295G859; ML19295G863; ML19295G866; ML19295G870; ZS-2019-0090, Revised Final Status Survey (FSS) Report - Phase 2, Release Record - Waste Water Treatment Facility Survey Unit 09100;
References
	ZS-2019-0090
	Download: ML19295G791 (249)
	v • d • e

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****         r:;AM~1A     :S ,..' E C T R U M         A N A L Y S __ S                        *****
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.lename: 545 2 iport Generated On 4/1 8/2 016 1:49:25 PM 1mple Title B306100AFRWC001GD tmple Description TB 560 1mple Identification 1mpl e Type 1mpl e Geometry iak Locate Threshold 3 .00 iak Locate Range (in channels ) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mpl e Size 1.000E+OOO SQM 1mple Taken On

quisition Started 4/ 1 8/ 2 016 1: 39: 2 4 PM

.ve Time 600.0 seconds ial Time 600.6 seconds !ad Time 0.10 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBWALL Da.\~ \\o.\,~o.~~J 'OJ Q~~ 12- !5-1~ O{glO [84]

1ak Analysis Report 4 / 1 8/2 01 6 1: 4 9: 25 P} Page 2

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Detector Name: 545 2 Sample Title: B306 1 00AFRWC001GD Peak Analysis Performed on: 4/18/2016 1: 4 9: 25 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid {keV) {keV ) Area Uncert. Counts 1 307- 316 310.71 77.33 0 .61 6.09E+OOO 36. 2 9 1.37E+002 2 1400- 1 413 1407. 22 351.77 1. 13 5.15E+001 21. 83 2 .45E+001 3 2429- 2441 2434.79 608.88 1. 23 3.72E+001 19.19 2 .08E+001 4 58 2 7- 5850 5840.50 1460.39 0 .93 l.82E+00 2 2 8.71 6.00E+OOO

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted sing l et

rors quoted at 2 .000 sigma

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1terference Corrected Act i ty Report 4 / 1 8/2016 9: 2 5 PM Page 3

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Sample Title: B306l00AFRWC001GD Nuclide Library Used: C:\GENIE2K\CAMFILES\ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energj' Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K-40 1. 000 1460.82* 10.66 1. 2 4086E+006 2 . 2 3417E+005 Bi-211 0. 9 99 35 1. 07* 1 3.02 l.4 22 44E + 005 6.44957E+004

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold =             0. 3 0 Errors quoted at 2 .000 s igma

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Nuclide Wt mean Wt mean Nuclide Id Activity Activit y Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 l.2 40 862E+006 2 . 2 34170E+005 Bi -2 11 0.999 1.4 22 436E+005 6.449567E+004

      ? = Nuclide i s part of an undetermined solution X  = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2. 00 0 sigma
 **********     U N I   D E N T I     F I  E D      P E A K S       **********

Peak Locate Performed on: 4/18/ 2 01 6 1:49:25 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second Z; Uncertainty Type Nu c li d e 1 77.33 1.0146E-00 2 596. 1 7 To l. Pb214-XR Pb2 14 -XR Eu-155 Pb212-XR Pb2 1 2 -XR 3 608.88 6.1932E- 00 2 5 1 .64 Tol. Zr-97 Sb-125 Sb-125 Cs- 1 34 Bi -2 14 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 s i gma [87]

4/18/ 2 01( 1: 49: 25 PM Page 5 tclide MDA Report

N U C L I D E M D A R E P O R T *****

Detector Name: 545 2 Sample Geometry: Sample Title: B306l00AFRWC001GD Nuclide Library Used: C:\GENIE2K\CAMFILES\ Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( i: ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) K-40 1460. 82

10.66 1.284E+005 1. 2 8E+005 1 .241E+006 5.496E+004

+                                                                                   7. 2 90E+004 Cr-5 1       32 0.08     9.91   1.552E+005       1.55E+005 2 .129E+004 Mn-54        834.85    99.98    1.704E+004       1.70E+004 -4.993E+003       7.775E+00 3 Co-58        810.76    99.45    1.364E+004       1.36E+004 6.131E+003        6.080E+00 3 Co-:-6 0   117 3 . 23  99.85    1.883E+004       1.30E+004 8.559E+003        8.536E+003 1 332 .49   99.98    1. 2 98E+004                 -2 .016E+004    5.555E+003 Nb-94        702.65    99.81    1. 5 96E+004     1.46E+004 2 .502E+003       7.291E+003 871. 0 9  99.89    1.456E+004                   -5 .736E+00 3   6.5 2 3E+003 Sn-11 3      255.13      2. 1 1 7.532E+005       2 .18E+004 3 .544E+004      3.570E+005 391.7 0   64.97    2 .177E+004                    1.021E+004    1.009E+004 Cs- 134      475.36      1. 48  9.006E+005       l .60E+004 -5.671E+004      4.119E+005 563.25      8.34   1 .892E+005                    1. 163E +005  8.721E+004 569.33    1 5.37   9.359E + 004                 -8.553E+003     4. 27 6E+004 604.7 2   97.62    2 .157E+004                  -6.920E+003     1 .013E+004 795.86    85.46    1.603E+004                     3 .557E+003   7.166E+003 801.95      8.69   1.669E+005                   - 4.770E+00 4   7.503E+004 1038.6 1      0.99   l.544E+006                     1 .8 3 1E+005 6.883E+005 1167.97       1. 79  1.002E+006                   -3.810E+005     4.523E+005 1365.19       3.0 2  4.660E+005                   -3.078E+005     2 .017E+005 Cs-137       66 1. 66  85.10    1.585E+004       1.59E+004 -3 .221E+00 3     7.141E+00 3 Eu-1 52      12 1 .78  28.67    6.657E+004       5.42E+004 5.999E+00 4       3 . 2 16E+004 244.70      7.61   2 .036E+005                  -1.062E+005     9.649E+004 295.94      0.45   3.623E+006                     2 .528E+005   1.7 1 2E+006 344.28    26 .60   5.417E+004                   -4.163E+004     2 . 52 8E+004 367.79      0.86   1. 7 53E+00 6                -8.468E+005     8.189E+005 411.1 2     2 . 24 6.082E+005                   -1.607E+0 0 5   2 .806E+005 443.96      2 .83  4 . 699E+005                 - 3 .784E+005   2 .156E+005 488.68      0.42   3.322E+006                     1.663E+006    1 .524E+006 563.99      0.49   3.086E+006                     1.858E+005    l .417E+006 586. 2 6    0.46   3.887E+006                     5 .673E+005   1.807E+006 678.62      0.47   3.321E+006                     2 .166E+006   1.517E+006 688.67      0.86   1.650E+006                     1.249E+005    7.458E+005 7 1 9.35    0.28   5.559E+006                     1.326E+006    2 .531E+006 778.90    12 .96   1 .25 7E+005                 -6.620E+004     5.731E+004 81 0 .45    0.32   4. 22 4E+006                   1.899E+006    1 .883E+006 867.37      4.26   3 .408E+005                    2 . 29 7E+004 1 .52 6E+005 919.33      0.43   3 .301E+006                  - 3 . 63 3E+006 1.468E+006 964.08    1 4.65   1.471E+005                     9 . 62 1E+004 6.812E+004 1085.87     10 . 2 4 1 . 401E+005                 - 1. 2 1 6E+005 6.179E+004 1089.74       1. 73  8. 3 06E+005                 - 4.740E+005    3.664E+005 1112.07     13.69    1 . 3 1 9E+005                 8.597E+004    5.972E+004 1 2 12.95     1. 43  1.155E+006                   - 4.917E+004    5.150E+005

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4/18/ 2 01 1:49: 25 PM Page 6 1c.lide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) Eu-1 52 1249.94 0. 1 9 8.670E+006 5.42E+004 5.069E+006 3.857E+006 1299.14 1. 63 9.170E+005 4.324E+005 4.018E+005 1408.01 2 1. 07 6.125E+004 3.715E+004 2 .606E+004 1457.64 0.50 9.959E+006 2.650E+007 4.784E+006 1528.10 0.28 3.978E+006 -6.623E+004 1.631E+006 Eu-154 123.07 40.40 4.706E+004 4.71E+004 3.273E+004 2 .273E+004 247.93 6.89 2 .082E+005 -2.230E+005 9.819E+004 591.76 4.95 3 . 1 69E+005 1.769E+005 l.457E+005 692.42 1. 78 7.875E+005 3 .519E+005 3.554E+005 723.30 20.06 8.871E+004 -5.714E+003 4.089E+004 756.80 4.52 3.017E+005 1.016E+005 1. 351E+005 873.18 12.08 1. 2 89E+005 7.940E+004 5.816E+004 996.29 10.48 1.401E+005 -6.595E+004 6. 2 33E+004 1004.76 18.01 9.550E+004 2.530E+004 4.323E+004 1274.43 34.80 5. 2 09E+004 1.321E+004 2 .342E+004 1596.48 1. 80 6.021E+005 2 .562E+005 2 .433E+005 Eu-155 45.30 1. 31 9.038E+005 7.44E+004 6.551E+005 4. 2 76E+005 60.01 1. 22 1.338E+006 -1.087E+006 6.431E+005 86.55 30.70 7.436E+004 5.630E+004 3 .614E+004 105.31 2 1.10 9.810E+004 7.190E+004 4.754E+004 Tl -2 08 583.19 85.00 2.031E+004 2 .03E+004 -1.240E+004 9.417E+003

+      Bi-21 1     351. 07*  13.02    8.220E+004     8.22E+004    1 .422E+005     3.736E+004 Pb-- 2 11    404.85     3.78   3.606E+005     3.61E+005  -4.305E+005       1 .665E+005 42 7.09    1. 76  7. 32 9E+005              - 2 .544E+004     3.359E+005 8 32 .01   3.52   5.120E+005                  3 .759E+005     2.349E+005 Bi-212         39.86    1. 06  9.709E+005     2 .67E+005 -1.977E+005       4.555E+005 727.33     6.67   2.675E+005                  2 .296E+005     1. 233E+005 785.37     1.10   1. 539E+006                 8.4 2 9E+005    7.041E+005 1620.50      1. 4 7 7.909E+005                  2 . 82.'.2E+004 3.242E+005 Pb-212       115.18     0.60   3.124E+006     4.53E+004    5.516E+005      1.508E+006 23 8.63  43.60    4.535E+004                  3.382E+004      2.176E+004 300.09     3.30   4.046E+005                -9.180E+005       1.887E+005 Pb212-XR       74.8 2 10.28    2 .387E+005    l. 35E+005   2.740E+005      1. 1 63E+005 77.11  17.10    1.351E+005                  1.190E+005      6.567E+004 87.35    3.97   5.702E+005                  2 .789E+005     2 .771E+005 89.78    1. 46  1.521E+006                -1. 2 77E+006     7.389E+005 Bi-2 14      609.32   45.49    4.778E+004     4.78E+004    7.894E+004      2 . 2 48E+004 768.36     4.89   2 .999E+005               -5.132E+004       1.354E+005 806.18     1. 2 6 1.111E+006                  5.072E+005      4.974E+005 934.06     3.11   5.4 22 E+005                3.689E+005      2.458E+005 1120. 2 9  14.92    1. 2 32E+005                1.997E+004      5.587E+004 1155.21      1. 63  9.257E+005                -4.4 2 9E+003     4.096E+005 1 238.1 2    5.83   3.164E+005                  9.707E+004      1.428E+005 1280.98      1. 43  1. 2 67E+006                9.743E+005      5 .699E+005 1377.67      3.99   4.322E+005                  1 . 2 93E+005   1.922E+005 1385.31      0.79   1. 732E+006               - 1.810E+006      7.456E+005 1401.52      1. 33  9.295E+005                -2.2 68E+005      3.925E+005 1407.99      2.39   5.391E+005                  3 . 2 69E+005   2.293E+005 1509. 2 1    2.13   6.064E+005                -1.218E+004       2.561E+005 1661. 2 7    1. 05  9.842E+005                  3.754E+005      3.905E+005

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1c}ide MDA Report 4/18/ 2 0H 1:49:25 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Bi-214 1 729.59 2.88 4. 2 03E+005 4.78E+004 1.959E+005 1.723E+005 1 764.49 15.30 1.384E+005 1.332E+005 6.199E+004 1847.43 2.03 6.538E+005 -9.916E+004 2 .712E+005

 >                 2 118.51      1.16   O.OOOE+OOO                     O.OOOE+OOO O.OOOE+OOO Pb-214        2 41.99     7.25   2 .611E+005   5 . 3 8E+004     1.717E+005 1. 2 50E+005 295.22    1 8.42  8.924E+004                    - 2 . 2 64E+004 4. 22 0E+004 351. 93   35.60   5.380E+004                      7.185E+004 2 .553E+004 7 85.96     1. 06 1 .582E+006                     8.642E+005 7.228E+005 Pb2 14 -XR      74.82     5.80  4. 2 31E+005   2 . 3 8E+0 05    4.857E+005 2.061E+005 77.11     9.70  2 . 3 81E+005                   2 .098E+005 1.158E+005 87.35     2.24  1.011E+006                      4.943E+005 4.911E+005 89.78     0.82  2 .709E+006                   -2 . 2 73E+006 1.316E+006 Ra-226        186. 2 1    3.64  4.684E+005     4.68E+005        2.591E+005 2 .244E+005 Ac-228        129.07     2.42   7.566E+005     7.84E+004        1.881E+005 3 .649E+005 2 09. 2 5  3.89   4.009E+005                   -3.793E+005 1.908E+005 2 70. 2 4  3.46   4.647E+005                   -1.605E+004 2 . 2 01E+005 328.00     2 .95  5. 3 07E+005                 -6.239E+0 0 3 2 .494E+005 338.32    11. 2 7 1.403E+005                      9.472E+00 3 6.591E+004 409.46     1. 92  6.578E+005                   -5.423E+005 3.015E+005 463.00     4.40   3. 406E+005                     7.939E+004 1.576E+005 794.95     4.25   3.036E+005                   - 4.771E+005 1.347E+005 91 1. 20  25.80   7.840E+004                      3.440E+004 3.619E+004 964.77     4.99   4.283E+005                     2 .666E+005 1 .982E+005 968.97    15.80   1.331E+005                     1.035E+005 6. 1 50E+004 1 588. 2 0    3.22   3.350E+005                   -7 .027E+004 1.353E+005 Pa -23 1       27.36    10.30   7.074E+004    7.07E+004        4.196E+004 3 . 22 8E+004 283.69      1. 70  9.735E+005                     4.887E+005 4.611E+005 30 0.0 7    2 .47  5.405E+005                   -1. 22 6E+006 2 .521E+005 302.65      2.2 0  6.182E+005                     4.055E+005 2 .886E+005 330. 0 6    1. 40  1.049E+006                   - 6.997E+005 4.911E+005 Th- 23 4       92.38     2 .13  1.009E+006    1 .01E+006       4.910E+005 4.898E+005 92.8 0    2 .10  1.020E+006                     5.649E+005 4.948E+005 112.8 1     0.2 1  9.036E+00 6                    4.136E+006 4.366E+006 U-235        143.76     10.96   1.555E+005    2 .99E+004     -1.295E+004 7.472E+004 1 63.33     5.08   3. 2 70E+005                 -7.552E+004 1.568E+005 1 85.7 1   57.20   2.993E+004                     1.991E+004 1.434E+004 2 02. 11    1. 08  1.499E+006                   -7.465E+005 7.155E+005 2 05.31     5.01   3.370E+005                     1.344E+005 l.611E+005 Am-24 1        59.54    35.90   4.516E+004    4.52E+004      -3 .589E+00 4 2 .170E+004
     + = Nucl ide identified during the nuclide identification

Energy line found in the spectrum

     >     Calculated MDA is z ero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @     Half-life too short to be able to perform the decay correction

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"**************************    *************************" ****************
' ***        GAMM A       S P E C T R U M         A N A L Y S 1- S                *****
  ***********************************************************************

.l ename: 54 52 iport Generated On 5/2/2 01 6 2 :47: 3 4 PM tmple Title B3 0 6100AFRWC002GD tmple Description TB #2 PEDESTAL WALL tmple Identification tmple Type tmple Geometry iak Locate Thr e shold 3 . 00 iak Locate Range (in channels) 85 - 81 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10.000 keV tmple Si ze 1.000E+OOO SQM tmple Taken On

quisition Started 5/ 2 /2016 2:37:32 PM

.ve Time 600. 0 seconds ial Time 6 00 .7 seconds iad Time 0.1 1 % Energy Calibration Used Done On 1/13/2 01 5 Efficiency Calibration Used Done On 4/14/2 01 6 Efficiency ID TBWALL p* P 1)"\o. \l"\1<\o.\eJ '°J

                                                                      ~JJ,5"- /8' t)/,I~

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iak Analysis Report 5 / 2 / 2 0 16 2 :4 7 :34 PM Page 2

' ************ * * **********************************************************

'*** P E A K A N A L Y S I S R E P O R T ***** ' ************************************************************************ Detector Name: 5452 Sample Title: B306100AFRWC002GD Peak Analysis Performed on: 5/2/2016 2 : 4 7: 33 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) ( keV ) Area Uncert. Counts 1 113- 1 2 3 117.45 28.95 0 .9 0 5.26E+001 32 . 0 7 6.84E+001 2 152- 159 155.04 38.37 0 .6 4 1 .32E+OOO 22 .87 6.37E+001 3 296- 305 301.19 74.95 0 .6 1 4.53E+001 43.94 1 .94E+002 4 2428- 2 441 2 435.37 609.02 1.11 5.83E+001 2 1. 70 2.07E+00 1 5 5827- 5848 5837.78 1 459.71 2. 0 2 1.87E+002 2 8.71 5.28E+OOO First peak in a multiplet region

=   Other peak in a multiplet region
=   Fitted singlet

rors quoted at 2 .000 sigma

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1terference Corrected Activ -Y Report 5/ 2 / 2 01 6 2: : 34 PM Page 3

- - - - * ********************************* * **********

"*** N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title: B306100AFRWC002GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTI FIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM ) Uncertainty K-40 0.998 1460. 82

10.66 1. 272 69E+006 2. 24767E+005 Th-231 0.875 25.64* 14.10 8.75985E+004 5.73474E+004 84.21* 6.60 1.61142E+005 1.60908E+005 89.95 1. 00

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuc l ide confidence index threshold=            0.30 Errors quoted at 2 .000 sigma

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1terference Corrected Activ -Y Report 5/2/2016 2; . : 3 4 PM Pag e 4

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 0.998 1.272689E+006 2.247668E+005 X Pa- 23 1 0.377 Th-231 0.875 9.588715E+004 5.401920E+004

     ?    Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2. 000 sigma
 **********      U N I D E N T I F I E D          P E A K S       **********

Peak Locate Performed on: 5/2/2016 2 :47:33 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second % Uncertainty Type Nuclide 2 38.37 2 .1923E-00 3 1738.61 Tol. Eu-155 Bi-21 2 4 609.0 2 9.7131E-00 2 37.24 Tol. Zr-97 Sb-125 Sb-125 Cs-134 Bi -2 14 M First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [94]

iclide MDA Report 5/2 / 2 0 1 6 2 :47:34 PM Page 5 "******************************************************************************

- - - N U C L I D E MD A R E P O R T *****

"****************************************************************************** Detector Name: 545 2 Sample Geometry: Sample Title: B306100AFRWC00 2GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM)

+      K-40       1460.82*    10.66 1.172E+005        1.17E+00 5 1. 2 73E+00 6      4.940E+004 Cr-5 1       320.08      9.9 1 1.497E+005      1 .50E+005 6.485E+004         7.019E+004 Mn-54        834.85    99.98 1. 52 5E+004      1.53E+004 -4.121E+00 2        6.883E+00 3 Co-58        810.76    99.45 1.604E+004        1.60E+004 1.825E+00 3         7.283E+003 Co-60      1173. 23    99.85 1.685E+004        1.34E+004 1.296E+004          7.545E+003 1 332 .49   99.98 1.343E+004                        3 .765E+003   5.782E+003 Nb-94        702.65    99.81 1.576E+004        1.51E+004 - 8.004E+002        7.194E+003 871.09    99.89 1. 5 07E+004                      8.551E+003    6.778E+00 3 Sn- 1 13     255. 1 3   2. 1 1 7. 3 71E+005    2 . 2 1E+004 1.151E+005       3.489E+005 391. 70   64.97 2 . 2 13E+004                     4.809E+00 3   1.028E+004 Cs- 134       475.36     1. 48   9.418E+005     1.97E+004 5.638E+004          4. 32 5E+005 563.25     8.34 1.911E+005                        1.167E+005    8.813E+004 569.33    15.37 9.690E+004                      -5 .773E+004    4.442E+004 604.72    97.62 2 .576E+004                     - 2 .513E+003   1. 22 3E+004 795.86    85.46 1.974E+004                      - 7.860E+001    9.017E+003 801. 95    8.69 1.583E+005                      -1.056E+005     7.074E+004 1038.61      0.99 1 .765E+006                     - 4.876E+00 4  7.991E+005 1167.97      1. 79 8.300E+005                     -2 .684E+005   3.661E+005 1365.19      3.0 2 4.938E+005                    -2 .664E+005    2 .156E+005 Cs-137        661.66    85.10 1.799E+004        1.80E+004 -4.641E+00 3       8.208E+003 Eu -152       121.78    28.67    6.9 1 7E+004   5.75E+004 -5.025E+00 3       3.346E+004 2 44.70    7 .61 2 .243E+005                      8.713E+003   l.068E+005 2 95.94     0.45 3 .790E+006                       1.332E+006   1.795E+006 344. 2 8  26.60 5.751E+004                      - 1 .266E+00 4  2 .694E+004 367.79      0.86 1.692E+006                     -2 .971E+005    7.882E+005 411. 1 2   2 . 2 4 7.150E+005                  -2 . 2 91E+005  3 . 3 39E+005 443.96     2 .83 5.454E+005                       1. 3 55E+005 2 .534E+005 488.68     0.42 4.007E+006                        1 .711E+006  1.867E+006 563.99      0.49 3.119E+006                     -l.635E+006     1.434E+006 586. 2 6    0.46 4.037E+006                        2 .326E+006  1.882E+006 678.62      0.47 3.240E+006                       2 .069E+006   1. 4 77E+006 688. 67     0.86 1.746E+006                       1.024E+006    7.940E+005 719.35      0. 2 8 6.042E+006                      4.804E+005   2 .772E+006 778.90    12.96 l.122E+005                         6.877E+004   5.054E+004 810.45      0.32 4.969E+006                        6.075E+005   2.256E+006 867.37      4.26 3.809E+005                     - 4.614E+004    1.727E+005 919.33      0.43 3.431E+006                       3 .2 2 9E+006 l.534E+006 964.08    14.65 1.350E+005                        6.774E+004    6.207E+004 1085.87     10.2 4 1.665E+005                     -2.242E+004     7.502E+004 1089.74       1. 73 9.550E+005                    -4.246E+005     4. 2 86E+005 1112.07     13.69 1. 33 8E+00 5                   -1.560E+005     6.068E+004 1212.95       1. 43 1. 35 9E+00 6                   5.760E+005    6. 1 69E+005

[95]

iclide MDA Report 5/2/ 2 016 2 :47:34 PM Page 6 Nucli de Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( i) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) Eu- 1 52 1249.94 0.19 7.326E+006 5.75E+004 6.185E+005 3 .185E+006 1299.14 1. 63 7. 2 97E+005 - 5.069E+005 3 .082E+005 1408.01 21.07 6.579E+004 4.390E+004 2 .833E+004 1457.64 0.50 9.911E+006 2.360E+007 4 . 760E+006 1 528 .10 0. 2 8 3 .736E+006 -3.444E+006 1.510E+006 Eu-154 12 3 .07 40.40 5 .001E+004 4.94E +004 1.323E+004 2 .421E+004 247.93 6.89 2 .283E+005 -3 .283E+003 1.082E+005 591. 76 4.95 2 .927E+005 -4.529E+004 1.336E+005 692.4 2 1. 78 7.875E+005 - 5.301E+005 3.554E+00 5 723.30 2 0.06 8.695E+004 - 4.348E+004 4.001E+004 756.80 4.5 2 3 . 5 57E+005 -4.832E+004 l .622E+005 873.18 12.08 1. 2 06E+005 4. 2 80E+004 5.400E+004 996.29 10 .48 1.457E+005 -4.082E+004 6.511E+004 1 004.76 18.01 8.020E+004 4. 7 60E+004 3.558E+004 1274.43 34.80 4.941E+004 3 .177E+004 2.209E+004 1596.48 1. 80 6.411E+005 -3.263E+005 2 .628E+005 Eu-155 45.30 1. 3 1 1. 2 38E+006 7.69E+004 4. 27 9E+005 5.946E+005 60.01 1.2 2 1.463E+006 - 2 .971E+003 7.057E+005 86.55 30.70 7.686E+004 5.3 75E+004 3.739E+004 1 05.31 21.10 1.017E+005 -2 .838E+004 4.936E+004 Tl-208 583.19 85.00 2 . 2 88E+004 2 . 2 9E+004 2 .657E+004 1.070E+004 Bi-211 351. 07 13.02 1 .487E+005 1. 4 9E+005 1.176E+005 7 . 061E+004 Pb-211 404.85 3.78 4.111E+005 4.11E+005 - 1 .329E+005 1.917E+005 42 7.09 1. 76 8.532E+005 1.861E+005 3.961E+005 8 32. 0 1 3.52 4.326E+005 4.030E+003 1.952E+005 Bi-212 39.86 1. 06 1.537E+006 2.48E+005 - 1.200E+006 7. 3 84E+005 727.33 6.67 2 .484E+005 -7.590E+004 1.137E+005 785.37 1.10 1.427E+006 -1.325E+006 6.477E+005 1 620.50 1. 4 7 6 .3 2 6E+005 2 .107E+005 2 .451E+005 Pb-2 1 2 115.18 0.60 3.587E+006 4.86E+004 1.562E+006 1 .740E+006 238.63 43 . 60 4.855E+004 7.407E+004 2.336E+004 300.09 3.30 4.737E+005 -2 .487E+005 2.233E+005 Pb212-XR 74.82 10. 2 8 2 .464E+005 1 .42E+005 3 .581E+005 1 . 201E+005 77.11 17.10 1 .417E+005 -1.481E+004 6.901E+004 87.35 3 . 97 5 .983E+005 6.802E+005 2 .911E+005 89.78 1. 4 6 1.552E+006 -3 .458E+005 7.540E+005 Bi-21 4 609.32 45.49 5.549E+004 5.55E+ 004 8.024E+00 4 2 . 633E+004 768.36 4.89 3.511E+005 1.574E+005 1.609E+005 806. 1 8 1. 26 1.169E+006 2 .932E+005 5.264E+005 934. 0 6 3.11 5.792E+00 5 2.363E+0 0 5 2 .643E+005 11 2 0. 2 9 14.92 1. 2 67E+005 5.213E+0 0 3 5.759E+004 11 55.21 1. 63 1.058E+006 2 .960E+005 4.759E+005 1238.12 5.83 2 .430E+005 -4.6 1 2E+004 1 .061E+005 128 0 .98 1. 43 1 .133E+006 -9.373E+004 5.026E+005 1 377.67 3.99 4.143E+005 2 .484E+005 1.833E+005 1385.31 0.79 1.410E+006 -2.367E+006 5.849E+005 14 01.52 1. 33 1.004E+006 -9.338E+004 4.300E+005 1407.99 2.39 5.790E+005 3.864E+005 2 .493E+005 1509.21 2 .13 6.553E+005 1 .770E+005 2. 805E+005 1661. 2 7 1.05 9.842E+005 3.754E+005 3.905E+005 [96]

5/2/2016 2:47:34 PM Page 7 iclide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM) Bi-2 1 4 1729.59 2 .88 3.013E+005 5.55E+004 8.397E+004 l. 1 2 8E+005 1764.49 1 5.30 8.881E+004 - 6.676E+004 3 .7 1 9E+004 1847.43 2 .03 5.402E+005 -1.319E+005 2 .144E+005 211 8.51 1.16 O.OOOE+OOO O.OOOE+OOO O.OOOE+OOO

  >                                                                            1.368E+005 Pb-214       241.99      7.25   2 .848E+005   5.51E+004    4.066E+005 295.22    18.42    8.965E+004               -3.434E+004     4. 2 41E+004 35 1. 93  35.60    5.508E+004                 6.433E+004    2 .6 1 7E+004 785.96      1. 06  1.544E+006                 6.301E+005    7.036E+005 Pb214-XR       74.82     5.80   4.367E+005    2 .50E+005   6.347E+005    2 .1 2 9E+005

77. 11 9.70 2 .499E+005 - 2 .611E+004 1.217E+005 87.35 2.24 1.060E+006 1. 2 06E+006 5.160E+005 89.78 0. 82 2 .763E+006 -6.157E+005 1.342E+006 Ra-226 186. 2 1 3.64 4.659E+005 4.66E+005 -1.480E+004 2 .232E+005 Ac-228 129.07 2.4 2 8.431E+005 7.30E+004 -2.163E+005 4.082E+005 209.25 3.89 4.288E+005 -1. 2 03E+005 2 .047E+005 270. 2 4 3. 4 6 4.196E+005 -1.233E+005 1.975E+005 328.00 2.95 5.060E+005 1.618E+005 2.371E+005 338.32 11. 27 1.591E+005 4.180E+004 7.529E+004 409.46 1. 92 8.427E+005 2.963E+005 3.940E+005 463.00 4.40 3.583E+005 4.090E+005 1.664E+005 794.95 4 . 25 4.107E+005 3.552E+004 l.882E+005 91 1. 2 0 25.80 7.303E+0 04 4 . 0 96E+004 3.351E+004 964. 77 4.99 3.966E+005 3.125E+005 1 .823E+005 968.97 15.80 1. 2 68E+005 1.033E+005 5.834E+004 1 588.20 3.22 3.567E+005 -3.902E+004 1.462E+005 Pa-23 1 27.36* 10.30 1. 1 35E+005 l.14E+005 l.199E+005 5.368E+004 283.69 1. 70 8.463E+005 - 1.926E+005 3.975E+005 300.07 2 .47 6.329E+005 - 3.323E+005 2 .983E+005 302.65 2 . 20 6.834E+005 2.310E+004 3.212E+005 330.06 1. 40 1.043E+006 -7.515E+005 4.876E+005 Th-234 92.38 2.13 1.048E+006 1.05E+006 3.489E+005 5.089E+005 92.80 2 .10 1.063E+006 6.193E+005 5.163E+005 1 12.81 0.21 1.053E+007 -6.587E+005 5.113E+006 U- 235 143.76 10.96 1.659E+005 2 .91E+004 -7.878E+004 7.993E+004 163.33 5.08 3 .395E+005 -2.558E+004 1.630E+005 185.71 57.20 2 .912E+004 -7.005E+003 1.394E+004 202.11 1. 08 1.533E+006 3.503E+004 7.323E+005 2 05.31 5.0 1 3.128E+005 -1.340E+005 1.490E+005 Am-241 59.54 35.90 4.905E+004 4.91E+004 -2 .960E+00 2 2 .364E+004

     + = Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
     > == Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ = Half-life too short to be abl e to perform the decay correction

[97]

************************** *************************'                                              * ~: **** ** * * ** * ***
****        G A M MA           S I:- E C T R U M                       A N A L Y S I S                                *****
************************************************************************
.lename: 5452

!port Generated On 4/14/ 2 016 3:08:08 PM tmple Title B306100AFRFC003GD tmple Description U-1 STS TB FLOOR 56 3 tmple Identification tmple Type tmple Geometry !ak Locate Threshold 3 .00 !ak Locate Range (in channels ) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Si ze 1 .000E+OOO SQM tmple Taken On

quisition Started 4/14/ 2 016 2 :58:05 PM

.ve Time 600.0 seconds !al Time 601.0 seconds 1 C: ,. iad Time 0 * ..L V 0 Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TB FLOOR lM

                ~~ r   ~~'-'      \t.,.~   s~-..e     "'fb    Arc.l,..~'ll\lt  '3 -"-e.-rc.,e- ' ~ cl~
               ~.O     "'>-Sc:c.s AS     \1:k)' C:..0\\'11-..~ C!L \              -L         ~         I
                     \                                                         """'-~ 1ZI'\. c..,.\\'1!.t::.T 1)0.~tt. '~ o.\\da\eJ b/

0~ J,,/ /8' t) e,;a [98]

iak Analysis Report 4/14/ 2 0 16 3 : 08: 08 H. Page 2

*************************************************************************
****              P E A K      A N A L Y S I S           R E P O R T                 *****
**************************************************************** ~'********

Detector Name: 545 2 Sample Title: B306100AFRFC003GD Peak Analysis Performed on: 4/14/2016 3:08: 07 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 284 - 306 300.47 74.77 0.84 2 .25E+002 89.18 4.55E+002 2 947 - 96 1 954.64 2 38.51 1. 35 6.69E+001 41. 2 8 1. 2 4E+002 3 1401- 1412 1406.8 1 351. 67 0.55 7.53E+001 2 7. 22 4. 3 7E+001 4 2325- 2335 233 0.6 1 58 2 .81 0.30 4.17E+00 1 2 0.7 3 2.73E+001 5 24 25- 2444 2 435.38 609.02 1.14 1.09E+00 2 2 9.19 2 .96E+001 6 3634- 3648 3 640.4 2 910.4 2 0.86 4.35E+001 16.87 9.49E+OOO 7 5828- 585 2 5840.01 1 460. 2 7 2 . 17 3.79E+00 2 41. 41 1. 22 E+001 8 7049- 7062 7055.8 2 1764. 0 3 0.78 3.70E+001 12.17 O.OOE+OOO

= First peak in a multiplet region
= Other peak i n a multiplet region Fitted singlet

rors quoted at 2. 000 sigma

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1terference Corrected Acti ty Report 4/14/ 2 01 6 8 :0 8 PM Page 3

- - - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****
      - * **********************************************

Sample Title: B306100AFRFC003GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K-40 1. 000 1460.82* 10 .66 7.00378E+005 9.77803E+004 Tl-2 08 1. 000 58 3 .19* 85.00 5.96712E+003 3.05316E+003 Pb-212 0.873 11 5.18 0 .60 23 8.63* 43.60 1 . 11 080E+004 7.08997E+003 30 0 . 0 9 3.3 0 Bi- 2 14 0. 32 9 609.32* 45.49 2 .99515E+004 8.76409E+003 768.36 4.89 8 0 6. 1 8 1. 26 934. 0 6 3. 11 1 120. 2 9 14.92 1 155.21 1. 63 1238.12 5.83 128 0. 98 1. 43 1377.67 3.99 1385. 3 1 0 .79 1401.52 1. 33 1407.99 2 .39 1509.21 2 .13 1661.27 1. 05 17 2 9.59 2 .88 1764.49* 15.3 0 5.36646E+004 1.81608E+004 1847.43 2 .03 2 118.5 1 1. 16 Pb- 2 1 4 0 . 491 2 41.99* 7. 25 6.67917E+004 4. 2 6052E+004 2 95. 22 1 8. 42 351.93* 35.60 1. 92 583E+004 7.61612E+0 0 3 785.96 1. 06

       * = Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :           10.0 0 0 keV Nuclide confidence index threshold                     0.30 Errors quoted at 2 . 000 s i gma

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1t erference Corrected Acti cy Report 4/14/2016 8:08 PM Page 4

- - - - ***********************i*******************
    - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 7.003775E+005 9.778033E+004 Tl-208 1. 000 5.967122E+003 3.053155E+003 X Bi-211 0.999 Pb-2 1 2 0.873 7.905 1 51E+003 7. 1 97705E+003 Bi-2 1 4 0.329 3.443078E+004 7.893060E+003 Pb-2 1 4 0.491 l. 92 5832E+004 7.615745E+003

      ?    Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2.000 sigma
 **********       U N I D E N T I F I E D          P E A K S      * *** , .*****

Peak Locate Performed on: 4/14/ 2 016 3: 0 8: 07 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. ( keV) Counts per Second ~ Uncertainty Type Nuclide 1 74.77 3.7479E-001 39.66 Tol. Pb214-ZR Ba-133 Pb212-XR Pb212-XR Pb2 14 -XR 6 910. 42 7.25 2 4E -00 2 38.77 Tol. Eu-1 52 Ac-228 M First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 s i gma [101]

1clide MDA Report 4/14/ 2 01( 3 :08:08 PM Page 5

- - - - * **************
    - N U C L I D E M D A R E P O R T *****
      - ************************************************************************

Detector Name: 54 52 Sample Geometry: Sample Title: B306100AFRFC003GD Nuclide Library Used: C:\GENI E2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) K-40 1460.8 2

10.66 4.796E+004 4.80E+004 7.004E+005 2 .148E+004

+                                                                                   2 .385E+004 Cr-51        320.08       9.91   5.005E+004      5.00E+004 1. 790E+004 Mn-54        834.85     99.98    5.459E+003      5.46E+00 3 -2 . 27 4E+00 3  2 .531E+003 Co-58        810.76     99.45    5.406E+003      5.41E+00 3 2 .782E+00 3     2 .507E+003 Co-60      1173. 23     99.85    6.415E+003      4.49E+00 3 1.398E+003       2 .970E+003 133 2 .49    99.98    4.487E+00 3                 -2 .539E+003    l .991E+003 Nb-94        702.65     99.81    5. 32 9E+00 3   4.71E+00 3 1.040E+002       2 .483E+003 871. 09    99.89    4.711E+00 3                   4.678E+003    2 .152E+003 Sn-113       255.13       2 . 11 2 .568E+005     7.84E+ 00 3 -5.842E+004     1. 2 35E+005 391. 7 0   64.97    7.8 3 7E+003                  2 .403E+003   3.716E+003 Cs- 1 34     475.36       1. 48  3. 2 16E+005    6.34E+003 1. 2 15E+005      l. 5 08E+005 563 . 25     8 . 34 5.631E+004                  - 7.076E+003    2.622E+004 569.33     15.37    3. 2 74E+004                -5.858E+002     1.531E+004 604.72     97.6 2   7.730E+00 3                 -2 . 2 67E+003  3.693E+003 795.86     85.46    6.335E+00 3                 -5 .156E+002    2.941E+003 8 01. 95     8.69   5.888E+004                  -3.370E+004     2.720E+004 1038.61        0 .99  5.158E+005                  -2 .32 9E+005   2.354E+005 1167.97        1. 79  3.539E+005                  - 1.707E+005    1.637E+005 1 3 65. 1 9    3.0 2  1.182E+005                  - 4.565E+004    5.060E+004 Cs-137       661.66     85.10    4.913E+003      4.9 1E+00 3 -1.940E+00 3    2.Z50E+003 Eu-152       1 2 1. 78  2 8.67   2.016E+004      1 .93E+004 -2 .038E+004     9.809E+003 2 44.70      7.61   7.169E+004                  -2 .741E+004    3.454E+004 2 95.94      0.45   1. 2 64E+006                  1.697E+006    6.071E+005 3 44. 2 8  26.60    1.926E+004                  - 3 .033E+002   9.173E+003 3 67. 7 9    0.86   5.615E+005                    2 .055E+005   2 .661E+005 411.12       2 .24  2.167E+005                  -1. 2 02E+005   1.0 2 3E+005 443.96       2 .83  1.806E+005                    6.236E+004    8.534E+004 488.68       0.42   1.149E+006                    5.696E+005    5.388E+005 563.99       0.49   9.713E+005                  -2 .890E+005    4.527E+005 586.26       0.46   1 .463E+006                   1.094E+006    6.957E+005 678.62       0.47   9.944E+005                  - 1. 746E+005   4.594E+005 688.67       0.86   6.480E+005                    3.092E+005    3.031E+005 719.35       0. 2 8 1.915E+00 6                 -2.584E+005     8.919E+005 778.90     12.96    4.132E+004                  -8.377E+00 3    1 .918E+004 810.45       0.32   1. 67 5E+00 6                 3. 2 95E+005  7.764E+005 867.37       4.26   1.154E+005                  -1.163E+005     5. 2 94E+004 919.33       0.43   1.310E+00 6                   7.8 2 1E+005  6.059E+005 964.08     14.65    4.564E+004                    3 . 2 16E+003 2 .136E+004 1085.87      10.24    5.579E+004                    2 .442E+004   2 .567E+004 1089.74        1. 73  2 .790E+00 5                -2 .629E+005    1. 2 63E+005 11 1 2 .07   13.69    3 .955E+004                 -4.856E+004     1.809E+004 1 2 12.95      1. 43  4.103E+00 5                 -3 .800E+005    1.883E+00 5

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1clide MDA Report 4/14/ 2 011 3 :08:08 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( %) {pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Eu- 1 52 1249.94 0.19 3.038E+006 1 . 93E+004 -7.456E+005 1. 390£+00 6 1 2 99.14 1. 63 3.561£+005 2 .570E+005 1.627£+00 5 1408.01 2 1. 07 2 . 2 00E+004 -5.483E+00 3 9.761E+00 3 1457.64 0 . 50 3 .776E+006 1.589E+007 1.835E+00 6 1 52 8.10 0.28 1.141E+006 -5.394E+004 4.732E+005 Eu- 1 54 1 23 .07 40.40 1.472E+004 1 . 47E+004 6.010E+002 7.168E+003 2 47.93 6.89 7.646E+004 -3 .578E+004 3 .678E+004 591.76 4.95 9.894E+004 - 1.008E+005 4.612E+004 692.42 1. 78 2 .971E+00 5 - 1.934E+005 1 .384E+005 723.30 20.06 2 .731E+004 -1.972E+004 1.274E+004 756.8 0 4.5 2 1.223E+005 1.888E+004 5.696E+004 873. 1 8 12 .08 3.993E+004 -2 .126E+004 1.8 2 8E+004 996. 2 9 10.48 4.830E+004 1. 25 2E+004 2 . 2 07E+004 1004.76 18.01 2 .535E+004 - 8.574£+003 1.146£+004 1 27 4.43 3 4.80 l.523E+004 -1.556E+004 6.904E+00 3 1 59 6 .48 1. 80 2 .404E+00 5 8.700£+00 3 1.045E+00 5 Eu-15 5 45.30 1. 31 2 .872E+005 2 . 2 3E+004 1.585E+005 1.377E+00 5 60.01 1.22 4.131E+005 1.560E+005 2 .002E+00 5 86.55 3 0.70 2. 232E+004 2 .894E+004 1.091E+004 10 5.31 21.10 3. 003E+004 6.708E+003 1.465E+004

+     Tl-2 0 8     583 , 19* 85.00    4.206E+00 3    4. 2 1E+00 3   5.967E+003    l.9 1 0E+003 Bi-2 11      351.07*   13.02    2 .603E+004    2.60E +004 5 . 2 66E+004     1. 207E+004 Pb-211       4 0 4.85    3.78   1.384E+005     1. 38E+005 9.934E+004        6.565E +004 427. 0 9    1. 76  2 .630E+005                   1.479E+005    1. 2 37E+005 832. 0 1    3.52   1 .508E+005                   5.260E+003    6.978E+004 Bi- 212        39.86     1. 06  3.494£+005     8.58E+004      1.002E+005    1.674E+005 727.33      6.67   8.584£+004                    6.509E+004    4.015£+004 785.37      1.10   4.799£+005                    9.339£+004    2.2 2 5E+005 1 62 0 .50    1. 47  2 .879E+005                   8.920E+004    1. 2 46E+005
+     Pb- 2 12     115.18      0 . 60 1.023E+006     l.08E+004 1.010E+006         4.988E+005 2 38.63*  43 . 60  1.081E+004                    1 .111E+004   5.180E+003 300.09      3.30   1 .52 4E+005                -2 .716E+005    7.280E+004 Pb21 2 -XR     74.82   10 . 28  7.179E+004     4.05E+004 1.411E+004         3 .515E+004 77.11   17. 10   4.047E+004                  -2 . 3 31E+002  1.978E+004 87.35     3.97   1.714£+005                    1. 775E+005   8. 3 77E+004 89.78     1.46   4.488E+005                  -2.621E+003     2.191E+005
+     Bi- 21 4     609.32*   45.49    9.907E+003     3.92E+003 2.995E+004         4.583E+003 768.36      4.89   1. 2 04E+005                -3.804E+004     5. 62 9E+004 8 0 6.18    1. 2 6 4.169E+005                    4.946E+003    1.930E+005 934.06      3.11   1.770E+005                    1. 2 31E+00 5 8. 1 71E+004 1120. 2 9   14.92    5.082E+004                    3.763E+004    2 . 3 86E+004 1155.21       1. 63  3.753E+005                  - 5.617E+005    1. 73 3E+00 5 1238.12       5.83   1 . 2 13E+005                 8.838E+004    5.649E+004 1280.98       1. 43  3.808E+005                    2 .564E+005   1.731E+005 1377.67       3.99   1.098E+005                    1. 2 94E+004  4.842E+004 1385.31       0. 79  5.136E+005                  -8. 2 82E+004   2 . 2 42E+005 1 401.52      1.33   3 .476E+005                 -1.472E+005     1.542E+005 1407.99       2 .39  1.936E+005                  -4.8 2 5E+004   8.591E+004 1509. 2 1     2.13   1.841E+005                    1. 22 8E+00 5 7.924E+004 1 661. 2 7    1. 05  3.065E+005                    1.4 2 9E+00 5 1. 2 56E+00 5

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lClide MDA Report 4/14 /2 01 3 :08:08 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM)

+     Bi-2 14     1729.59       2.88   1.623E+005     3 .92E+003      1.219E+005    7.087E+004 1764.49*     15.30   3 .925E+003                    5.366E+004    O.OOOE+OOO 1847.43       2.0 3  1 .583E+005                  -8.416E+00 3    6. 3 95E+004
  >               2118.51       1.16   O.OOOE+OOO                     O.OOOE+OOO    O.OOOE+OOO
+     Pb- 2 14      2 41.99*    7.25   6.500E+004     9.52E+00 3      6.679E+004    3.115E+004 2 95. 22   18.42   3.113E+004                     3.495E+004    1.496E+004 351.93*    35.60   9. 52 0E+003                   1. 926E+004   4.414E+003 785.96      1. 06  5.033E+005                     l.207E+005    2 . 33 5E+005 Pb214-XR        74.82     5.80   1. 272E+005    7.13E+004       2 .501E+004   6. 22 9E+004 77.11     9.70   7.134E+004                   -4.109E+002     3.488E+004 87.35     2 . 24 3.038E+005                     3 .145E+005   1 .485E+005 89.78     0 .8 2 7.991E+005                   - 4.667E+003    3.902E+005 Ra-226        186. 2 1    3.64   1. 4 61E+005   1. 4 6E+005   -7.441E+003     7.068E+004 Ac-228        1 2 9.07    2.42   2 .598E+005    2 . 72 E+004    1.8 2 8E+005  1. 2 67E+00 5 2 09. 2 5   3.89   1 . 422E+005                   4.464E+004    6 .877E+004 2 70. 2 4   3.46   1.588E+005                     6.189E+004    7.633E+004 328.00      2.95   l.640E+005                     2 . 940E+003  7.798E+004 338. 32    11. 27  5.034E+004                     7.360E+003    2 .410E+004 409.46      1. 92  2.651E+00 5                    l.051E+005    1. 2 55E+005 463.00      4.40   1.155E+005                     l.612E+003    5.447E+004 794.95      4. 2 5 l.273E+005                     l.554E+004    5.911E+004 911. 2 0   25.80   2 .720E+004                    2 .511E+004   1. 279E+004 964.77      4.99   1 .375£+005                    l .636E+005   6.445E+004 968.97     15.80   4. 2 98E+004                   3 .616E+004   2 .013E+004 1588.20       3.22   l .645E+005                    l.027E+005    7 .3 54E+004 Pa- 23 1        27.36    10.30   2 .155E+004    2 .16E+004      l.198E+004    1.003E+004 283.69      1. 70  2 .888E+005                  - 8.146E+004    1. 38 0E+00 5 300.07      2. 47  2 .036E+005                  - 3.629E+005    9.7 2 5E+004 302.65      2 . 20 2 . 2 69E+005                  2.463E+00 4   l.083E+005 330.06      1. 40  3.545E+005                     3.673E+004    l.688E+005 Th - 2 3 4      92.38     2 .13  3.022E+005     3 .02E+ 00 5  - 8.686E+004    l.475E+00 5 92.80     2 . 10 3.047E+005                   - 9.958E+004    l.487 E+00 5 112.81      0. 2 1 2 .854E+006                  -l.752E+006     1.390E+00 6 U-235         143.76     10.96   5. 2 00E+004   9 . 24 E+00 3 -l.086E+004     2 .528E+004 163.33      5.08   l.153E+005                   -3 .421E+004    5.601E+004 1 85.7 1   57. 2 0 9. 238 E+003                   l. 33 5E+003  4.469E+003 2 0 2 . 11  1. 08  5. 25 0E+005                   3. 2 52E+005  2 .542E+005 2 05.31     5.0 1  l.1 2 0E+00 5                  4. 3 29E+004  5.4 2 1E+004 Am- 2 41        59.54    35.90   l.373E+004     l.37E+004     -3 . 9 60E+00 3 6 .653E+003
     + = Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ = Half-life too short to be able to perform the decay correction

[104]

******~'******************~     *************************' w****************
****         G A MMA      S 1-' E C T R U M       A N A L Y S I S                    *****
********************~***************************************************

.lename: 545 2 iport Generated On 4/18/2016 3:12:11 PM 1mple Title B306100AFRWC004GD 1mple Description TB 560 tmple Identification 1mple Type 1mple Geometry !ak Locate Threshold 3 .00 iak Locate Range (in channels) 85 - 8192 !ak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmpl e Si ze 1.000E+OOO SQM tmple Taken On

quisition Started 4/18/2016 3 :0 2 :09 PM

.ve Time 600.0 seconds !al Time 600.6 seconds iad Time 0. 09 s;; Energy Calibration Used Don e On 1/13 /2 015 Efficiency Calibration Used Done On 4/14 /2 016 Efficiency ID TBWALL 1)C\il\ \\o.\,c'\akJ by Q~~ I c)- 5J 18

                                                                    ~ ~ /0

[105]

iak Ana~ysis Report 4/18/2016 3:12:11 PM Page 2

- - - - * *
    - P E A K A N A L Y S I S R E P O R T *****

Detector Name: 545 2 Sample Title: B306100AFRWC004GD Peak Analysis Performed on: 4/18/2016 3:1 2 : 1 0 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8 1 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV ) Area Uncert. Counts 1 297- 3 08 301.83 75.11 0.51 5.80E+001 45.00 1 .78E+002 2 368- 376 371. 4 7 9 2 .54 0. 3 8 2 . 2 0E+001 2 5.94 6.70E+001 3 5828 - 5851 5839.98 1460. 26 2 .01 1 .53E+00 2 2 4.74 O.OOE+OOO First peak in a multiplet region Other peak in a multiplet region Fitted singlet

rors quoted at 2 . 000 s igma

[106]

1terference Corrected Acti ty Report 4 /18/ 2 016 ~ . :2: 11 PM Page 3

- - - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title: B306100AFRWC004GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence ( keV) ( 'o ) (pCi/SQM ) Uncertainty K-40 0.999 1 460.82* 10.66 1.04309E+006 l .91441E+005 Cd-109 0.968 88.03* 3.70 1.40078E+005 l .67541E+005 Th227-XR 0.375 85.43 1. 34 88.47* 2 .18 2.37747E+005 2 .84603E+005 Ac228-XR 0.391 89.96 1. 90 93.35* 3.10 1.67190E+005 2 .04370E+005

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuclide confidence index threshold =               0.30 Errors quoted at 2 .000 sigma

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1terference Corrected Acti ty Report 4/ 1 8/2016 L2: 11 PM Page 4 "*********************************************************************** "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** "*********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 0.999 l.043087E+006 l.914407E+005

  ?   Cd-109       0.968        l.400778E+005        l.675406E+005
  ?   Th227-XR     0.375        2.377467E+005        2 .8460 2 7E+005
  ?   Ac228-XR     0.391        l.671896E+005        2 .043697E+00 5
      ?    Nuclide i s part of an undetermined solution X    Nuclide rejected by the interference analysis
      @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .000 sigma
 **********     U N I D E N T I F I E D         p E A K      s   **********

Peak Locate Performed on: 4/ 1 8/2 0 1 6 3:1 2 :10 PM Peak Locate from Channel: 85 Peak Locate To Channel: 81 92 Peak Energy Peak Si ze in Peak CPS Peak Tol. No. (keV) Counts per Second % Uncertainty Type Nuclide 1 75.11 9.66 1 7E-002 77.62 Tol. Pb2 1 4-XR Ba- 1 33 Pb212-XR Pb212-XR Pb2 1 4-XR M = First peak in a multiplet region rn = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000 s i gma [108]

tclide MDA Report 4/18/ 2 011., 3: 12 :11 PM Page 5

- - - N U C L I D E MD A R E P O R T *****

Detector Name: 545 2 Sample Geometry : Sample Title: B306100AFRWC004GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL . NLB Nucli de Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV ) ( ~) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM )

+      K-40       1460.8 2

1 0 .66 1.845E+004 1.84E+004 1.043E+006 O.OOOE+OOO Cr-51 320.08 9.91 1.351E+00 5 1.35E+005 5.795E+004 6. 2 88E+004 Mn-54 834.85 99.98 1.427E+004 1.43E+004 1.049E+003 6. 3 91E+003 Co-58 810.76 99.45 1.513E+004 1.51E+004 -5.638E+002 6.828E+003 Co-60 1173.23 99.85 1.559E+004 1.43E+004 8.186E+002 6.915E+00 3 133 2 .49 99.98 1.429E+004 8.616E+002 6.211E+00 3 Nb - 94 70 2 .65 99.81 1.476E+004 1.38E+004 1.006E+004 6.691E+00 3 87 1. 09 99.89 1.375E+004 2 .077E+003 6. 11 9E+00 3 Sn- 11 3 255.13 2 .11 7.564E+005 2 .50E+004 l.791E+005 3.586E+00 5 391.70 64.97 2.500E+004 1.543E+004 l.171E+004 Cs - 13 4 475.36 1. 48 9. 006E +005 1. 66E+004 5.731E+005 4.119E+005 563.25 8 .34 1.565E+005 -9.693E+004 7.083E+ 0 04 569.33 15.37 8.531E+004 7.454E+002 3.862E+004 604.72 97.6 2 2 .132E+004 7.168E+003 l.OOOE+004 795.86 85.46 1 .662E+004 9.916E+003 7.459E+00 3 801. 95 8.69 1. 35 9E+005 -l.551E+005 5.954E+004 1 038.61 0 .99 1.418E+006 3 .856E+005 6. 2 56E+005 1 167.97 1. 79 7.697E+005 1 .015E+005 3 . 3 60E+005 1 365.19 3.02 3.676E+005 -1. 3 32E+005 l.524E+005 Cs- 1 37 661. 66 85.10 l.885E+004 1.89E+004 5. 3 41E+002 8.641E+003 Eu-1 52 1 2 1. 78 2 8.67 5.897E+004 5.7 1E+004 2.128E+004 2 .837E+004 244.70 7.6 1 2.121E+005 6.868E+004 l .007E+005 295.94 0.45 3.657E+006 2 .858E+006 l.729E+00 6 344. 2 8 2 6.60 5.715E+004 - l.732E+004 2 .676E+004 367.79 0.86 1.602E+006 2 .134E+004 7.4 3 1E+005 411 . 1 2 2.24 6.586E+005 1.908E+005 3 .057E+005 443.96 2.83 4.750E+005 4.0 3 6E+005 2 .182E+005 488.68 0.42 3.429E+006 -l. 2 13E+005 l.578E+006 563.99 0. 4 9 2.735E+006 -8.553E+005 1. 2 42E+006 586. 2 6 0.46 3.634E+006 l.711E+006 l.680E+006 678.62 0.47 2.797E+006 -l.730E+004 1.255E+006 688.67 0.86 1.723E+006 6.461E+005 7.822E+005 719.35 0. 2 8 5.771E+006 -l. 25 8E+005 2.637E+006 778.90 12.96 l.007E+005 - 3.518E+004 4.480E+004 8 1 0.45 0.32 4.830E+006 1.246E+0 0 6 2 . 1 87E+00 6 867.37 4.26 3.346E+005 -l.517E+005 l.496E+005 919.33 0. 43 3.431E+006 9.630E+005 1. 5 34E+006 964. 0 8 14.65 l.081E+005 -l.378E+005 4.862E+004 1085.87 10.2 4 1.187E+005 3.363E+004 5.111E+004 1089.74 1. 73 7.702E+005 -3 .049E+005 3.362E+005 111 2 .07 13.69 1 . 1 76E+005 -6.570E+004 5.255E+004 121 2 .95 1. 43 l. 2 20E+006 -6.348E+005 5.476E+00 5

[109]

tclide MDA Report 4/18/201\., 3:12:11 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM) Eu-15 2 1 2 49.94 0.19 8.311E+006 5.71E+004 2 .386E+006 3 .677E+006 12 99. 1 4 1. 63 9.170E+005 -2 .464E+003 4.018E+005 1408.01 21.07 7.392E+004 3 . 7 50E+004 3. 2 39E+004 1457.64 0.50 8.912E+006 2 .324E+007 4. 2 60E+006 1 52 8.10 0. 2 8 3 .473E+006 -2 .517E+006 1. 378E+00 6 Eu-154 123.07 40.40 4.125E+004 4.13E+004 -3 .200E+004 1 . 983E+004 247.93 6.89 2 .283E+00 5 2 .803E+004 1.082E+005 591.76 4.95 2 .661E+005 1.825E+005 1. 2 03E+005 692.42 1. 78 7.875E+005 -2 .348E+004 3.554E+005 723.30 2 0.06 7.750E+004 -1.168E+004 3.528E+004 756.80 4.52 2 .850E+005 -1.910E+00 5 1. 2 68E+005 873.18 12 .08 1.042E+005 -7.543E+004 4.582E+004 996. 2 9 10.48 1.510E+005 5.713E+00 3 6.776E+004 1004.76 18.01 8.187E+004 1. 2 44E+004 3.642E+004 1274.43 34.80 4.454E+004 1.331E+004 1.965E+004 1596.48 1. 80 6.774E+005 -2 .668E+005 2 .809E+005 Eu-155 45.30 1. 3 1 8.915E+005 6.84E+004 5.961E+005 4.215E+005 60.01 1. 22 1.254E+006 4.484E+004 6.012E+005 86.55 30.70 6.841E+004 4.610E+004 3.317E+004 1 05.31 21.10 8.3 57 E+004 -2 .900E+004 4.027E+004 Tl-208 583.19 85.00 2.014E+004 2 .01E+004 2.388E+004 9. 3 31E+003 Bi-211 351. 07 1 3.02 1.463E+005 1.46E+005 7.141E+004 6.9 43E+004 Pb-211 404.85 3.78 3.961E+00 5 3 .82E+005 1.614E+005 1.842E+005 4 27 .09 1. 76 8. 2 49E+005 8.468E+004 3 .819E+005 8 32 .01 3.52 3.822E+005 4.745E+004 1.700E+005 Bi -2 1 2 39.86 1. 06 1.017E+006 2 .31E+005 9.572E+005 4.783E+005 727.33 6.67 2 .306E+00 5 5.99 1E+004 1.049E+005 785. 3 7 1.10 1.259E+00 6 5.515E+005 5 . 6 38E+005 1620.50 1. 4 7 9.553E+005 1.017E+005 4.064E+005 Pb-212 115.18 0.60 3.043E+006 4.36E+004 1.120E+006 1.468E+006 238.63 43.60 4.3 60E+004 2.692E+004 2 .088Et004 300.09 3.30 4.485E+005 -5.566E+005 2 .106E+005 Pb 212 - XR 74.8 2 10.28 2 .265E+005 1.30E+005 3 . 3 18E+005 1.101E+005 77.11 17.10 1.300E+005 4.743E+00 3 6.313E+004 87.35 3.97 5. 3 49E+005 7.639E+005 2 .594E+005 89.78 1. 46 1.326E+006 -1.388E+006 6.413E+005 Bi -2 14 609.3 2 45.49 4.778E+004 4.78E+004 5.200E+004 2.248E+004 768.36 4.89 3 .266E+005 1.983E+005 1.487E+005 806. 1 8 1. 26 l.130E+006 5.309E+005 5.073E+005 934.06 3.11 4.937E+005 -8. 2 62E+00 3 2.216E+005 1120.29 14.92 1.410E+005 l .011E+005 6.477E+004 1155.21 1. 63 8.618E+005 -3.346E+005 3.776E+005 1238.12 5.83 3.114E+005 -2.234E+005 1.403E+005 1280.98 1. 43 1.156E+006 1.037E+006 5.144E+005 1377.67 3.99 3.316E+005 - 3.083E+004 1.4 2 0E+005 1385.31 0.79 1.673E+006 - 6.130E+005 7.163E+005 1401. 52 1. 33 1. 2 27E+006 3.581E+005 5.411E+005 1407.99 2.39 6.506E+005 3.300E+005 2 .851E+005 1509. 2 1 2 .13 5.227E+005 -2.524E+005 2 .143E+005 1661. 2 7 1. 05 1.191E+006 - 7. 1 32E+005 4.940E+005 [110]

1cli.de MDA Report 4/18/ 2 0H, 3:12: 1 1 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) Bi -2 14 1729.59 2 .88 4.441E+005 4.78E+004 2 . 2 39E+005 1.842E+00 5 1764.49 15.30 1.409E+005 1.041E+005 6.321E+004 1847.43 2 .03 5.812E+005 2.473E+005 2 .348E+00 5

 >                  2118.51        1.16 O.OOOE+OOO                      O.OOOE+OOO     O.OOOE+OOO Pb-214        241.99       7.25 2.611E+005      5.38E+004       2.926E+005     1.250E+005 295.22     18.4 2 8.883E+004                      6.424E+004     4. 2 00E+004 351.93     35.60 5.380E+004                      2.985E+004      2 .553E+004 785.96       1. 06 1.332E+006                     6.010E+005     5.979E+005 Pb214-XR        74.82      5.80 4.014E+005      2 . 2 9E+005    5.882E+005     1.952E+005 77.11      9.70 2 .292E+005                    8.361E+003      1.113E+005 87.35      2.24 9.480E+005                     1.354E+006      4.598E+005 89.78      0 .82 2 .36 1E +006                -2 .471E+006     1.142E+006 Ra-226         1 86.2 1     3.64 4.263E+005      4. 2 6E+005    8.371E+004     2 .034E+005 Ac-2 2 8       1 2 9. 07    2 .42 7.610E+005     7.62E+004      2 . 2 05E+005  3.671E+005 209.25       3.89 4.023E+005                    -9.643E+004     1.915E+005 270.24       3. 46 3.914E+005                    2 .046E+005    1.834E+005 328.00       2.95 4.665E+005                   -3.573E+004      2 .173E+005 338.32     11. 27 1.419E+005                     6.370E+003     6.671E+004 409.46       1. 92 8.082E+005                    5.060E+005     3.767E+005 463.00       4.4 0 3.018E+005                    1. 27 9E+005   1.382E+005 794.95       4.25 3.340E+005                     9.770E+004     1. 4 99E+005 91 1. 20   25.8 0 7.6 1 5E+ 0 04               - 6.668E+003     3.507E+004 964.77       4.99 3.122E+005                   - 6.230E+005     1.401E+005 968.97     15.80 1.070E+005                      7.254E+004     4.843E+004 1 588.2 0      3.22 4.627E+005                     3.088E+005     1 .992E+005 Pa-23 1          27.36    10.30 6.807E+004      6 . 81E+004     3.555E+004     3.095E+004 2 83.69      1. 70 7.743E+005                    1.230E+005     3.615E+005 300.07       2 .47 5.992E+005                  - 7.436E+005     2.814E+005 302.65       2 . 2 0 6.637E+005                  5.887E+005     3 .114E+005 330.06      1. 40 9.787E+005                     4.319E+005     4.557E+005 Th-234           92 . 3 8  2 . 1 3 8.636E+005   8.6 4E+00 5   - 1 .234E+005    4.169E+005 92.80     2 . 1 0 8.713E+005                   2.653E+005     4. 2 05E+005 112.81        0. 2 1 8.432E+006                 -4.115E+006      4.064E+006 U-235         143.76      10.96 1.544E+005      2 .74E+004      2.513E+004     7.4 1 8E+004 1 63.33      5.08 3 .193E+005                     8.806E+003     1. 52 9E+005 1 85.71     57. 2 0 2 .735E+004                 -2 . 2 91E+00 3  1.306E+004 2 02.11      1. 08 1. 2 74E+006                 -1. 1 62E+006    6.027E+005 205.3 1      5.01 3 .039E+005                     5.902E+004     1.445E+005 Am-24 1         59.54     35.90 4.077E+004      4.08E+004     -2.446E+004      1.950E+004
     + = Nuclide identified during the nuclide identification
      * = Energy line found in the spectrum
     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @     Half-life too short to be able to perform the decay correction

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**************************     *************************            I- ***************
****         G A MM A    S P E C T R U M          A N A L Y S 1. S                *****
************************************************************************
.lename: C:\GENIE2K\CAMFILES\00001407.CNF iport Generated On                 5/ 3 /2016        6:53:0 2 AM tmple Title                        B306100AFRWC005GD tmple Description                  TB WALL tmple Identification tmple  Type tmple  Geometry iak Locate Threshold                 3.00 iak Locate Range (in channel s )        85 -     8 1 92

!ak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Size 1. OOOE+OOO SQM tmple Taken On

quisition Started 5/2/20 1 6 3:3 1 : 32 PM

.ve Time 600.0 seconds ial Time 600.5 seconds iad Time 0 . 09 % En ergy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBWALL DJa~o.\ida+ed Joy

                                                                        ~
                                                                        /~~o- It t1 /,I()

[112]

iak Analysis Report 5/3/2 01 6 6:53:02 AM Page 2

"************************************************************* ***********
"***               P E A K        A N A L Y S I S          R E P O R T                 *****

"************************************************************************ Detector Name: 5452 Sample Title: B306100AFRWC005GD Peak Analysis Performed on: 5/3/2 01 6 6:53: 0 1 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV ) Area Uncert. Counts 1 296- 306 3 00. 2 0 74.70 0.34 3 . 5 5E+001 48.77 2 .34E+002 2 946- 959 953 . 33 238. 1 9 0.4 2 4. 3 9E+001 28.17 5.61E+001 3 1400- 1413 1406.67 351. 64 0.35 4.lOE+OOl 22.33 3.00E+OOl 4 2 42 6- 2 440 2 433.90 608.65 1. 46 7.llE+OOl 2 1. 88 1.69E+001 5 58 2 6- 5848 58 3 7.65 1459.68 1. 82 1.51E+002 26.92 8.05E+000

= First peak in a multiplet region Other peak in a multiplet region
= Fitted singlet

rors quoted at 2.000 s igma

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1terference Corrected Acti* .y Report 5 / 3 / 2 01 6 6 3:02 AM Page 3 "*********************************************************************** "*** N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

- - - - * ***********************************************

Sample Title: B306100AFRWC005GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K-40 0.998 1460.8 2

10.66 1.02889E+006 2 .04078E+005 Pb-212 0.87 2 115.18 0.60 2 38.63* 43.60 2 .97822E+004 1.96939E+004 3 00.09 3.30 Pb-214 0. 4 92 2 41. 99* 7. 2 5 1 .79079E+005 1.18350E+005 2 95. 22 18.42 351.93* 35 .60 4.13939E+004 2 .35007E+004 785.96 1. 06

      * = Energy l ine found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuclide confidence index threshold=                0.30 Errors quoted at 2 . 000 sigma

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tterference Corrected Acti * -Y Report 5/3/20 1 6 6 3:02 AM Page 4 "*********************************************************************** "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0 .998 1 .0 2 8893E+006 2 .040784E+005 X Bi-21 1 0.999 Pb-212 0 .872 2.289805E+004 2 .006629E+004 Pb-214 0 . 4 92 4.139387E+004 2 .350013E+004

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysi s
      @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at          2 .000 sigma
 ******* **     U N I D E N T I F I E D             P E A K S     **********

Peak Locate Performed on: 5/3/2 01 6 6:53: 0 1 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . ( keV) Counts per Second *nty Type Nuclide 1 74.7 0 5.9190E- 0 02 Tol. Pb214-XR Ba-133 Pb212-XR Pb212-XR Pb214-XR 4 608.65 l . 1852E-001 Tol. Zr-97 Sb-125 Sb-125 M = Fir s t pea k in a multiplet region m = Other peak in a multiplet region

F = Fitted singlet Errors quoted at 2 . 000 sigma [115]

1clide MDA Report 5/3/20 1 6 6:53:02 AM Page 5

- - - N U C L I D E M D A R E P O R T **** '~

Detector Name: 545 2 Sample Geometry: Sample Title: B306100AFRWC005GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) (%) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM)

+      K-40       1460.82* 1 0 .66       1.417E+005     1.42E+005 1.029E+006        6.163E+004 Cr-51        320.08        9.91   1.552E+005     1 .55E+005 8.577E+004       7.290E+004 Mn- 54       834.85     99.98     1.595E+004     1 .59E+004 1.751E+003       7.231E+00 3 Co-58        810.76     99. 4 5   1.648E+004     1.65E+004 -8.591E+003       7.501E+00 3 Co-60      117 3 . 23   99.85     1.456E+004     1 .43E+004 - 1.351E+003     6.402E+00 3 1 332 .49    99.98     1.4 2 9E+004                 1.034E+004    6.211E+00 3 Nb-94        702.65     99.8 1    1 .411E+004    1. 40E+004 -2 .017E+004     6.369E+003 871.09     99.89     1.403E+004                 -3 .541E+003    6. 2 56E+003 Sn-113       2 55.13      2 .11   7.905E+00 5    2 .18E+004 -3 .900E+004     3.756E+005 3 91.70    64.97     2 .177E+004                -1.303E+004     1.009E+004 Cs-134       4 75.36      1. 48   8.792E+005     1.80E+004 -5.646E+005       4.012E+005 563.25       8.34    1.836E+OOS                   7. 2 08E+004  8.438E+004
                    .569. 33   15.37     9.581E+004                   4.458E+004    4.387E+004 6 0 4.72   97. 62   2.503E+004                  -1.926E+00 3   1 . 1 86E+004 795.86     85.46    1.799E+004                  - 5.796E+003    8.145E+003 801.95       8.69   1.852E+005                    1 .111E+005   8.420E+004 10 38.61       0 .99  1.631E+006                    8.175E+005   7.319E+005 11 67.97       1. 79  8.857E+005                    5.367E+00 5  3 .940E+005 1365.19        3.0 2  4.035E+OOS                 -8.572E+004     1. 704E+005 Cs-137        661. 66    85.10    1 .885E+004    1.89E+004 1 .379E+004       8.641E+00 3 Eu-15 2      121.78      2 8.67   6.668E+004     5.4 2E+004 6.749E+004       3 .222E+004 2 44.70       7.61   2.335E+00 5                   1.951E+004   1.114E+005 2 95.94       0.45   3.934E+00 6                   3.863E+005   1.867E+006 3 44. 2 8  26 .60    5.417E+004                 -5.582E+00 4    2 . 52 8E+004 3 67.79       0 .86  l.812E+006                    3.004E+005   8.485E+005 411.12        2 .2 4 6.848E+005                 - 1.080E+005    3.189E+005 443.96       2 .83   4.800E+005                 - 1 .961E+005   2 . 2 07E+005 488.68       0.42    3.249E+006                 -2 .127E+006    1.488E+00 6 563.99       0.49    3.184E+006                   2 . 3 44E+006 1.466E+006 586.26       0.46    3.948E+006                    9 .859E+005  1.837E+006 67 8. 62     0.47    3. 1 99E+006                 1.145E+006    1.456E+006 688.67       0.86    1.625E+006                    6.812E+004   7.333E+005 719.35       0. 2 8  5. 2 61E+006               -2 .536E+005    2 .382E+006 778.9 0    12.96     1.208E+005                 - 4.927E+004    5.487E+004 81 0 .45     0 .32   4.969E+006                 -6.109E+006     2.256E+00 6 867.37       4.26    3 .153E+005                -2 .611E+005    1.399E+005 919.33       0.43    3 .793E+006                  2 .388E+006   1.715E+006 964.08     14.65     1.307E+005                   1.156E+005    5.992E+004 1085.87      10.24     1.583E+005                   1. 2 05E+005  7.088E+004 1089.74        1. 73   9.040E+005                 -9.033E+004     4.031E+00 5 1 112.07     13.69     1.108E+005                 -2.319E+005     4.915E+004 1212.95        1. 43   1.085E+006                 -8.033E+005     4.803E+OOS

[116]

tclide MDA Report 5/3/2016 6:53:02 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity De c . Leve l Name (keV) (% ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) Eu- 1 52 1249.94 0.19 9.658E+006 5.42E+004 2 .663E+006 4.351E+006 1299.14 1. 63 8.161E+005 -2 .771E+005 3.514E+005 1408.01 21. 07 7.941E+004 2 .288E+004 3.5 1 4E+004 1457.64 0.50 9.095E+006 2 .300E+007 4.352E+006 1528.10 0.28 3.978E+006 -1.921E+006 1.631E+006 Eu-154 123.07 40.40 4. 5 55E+004 4.56E+004 -3.389E+004 2 .198E+004 247.93 6.89 2 .404E+005 -4. 22 9E+004 1.143E+005 591.76 4.95 2 . 6 61E+005 1 . 8 64E+005 1. 2 03E+005 692.42 1. 78 8.576E+005 -1. 1 67E+005 3 . 9 04E+005 723.30 2 0.06 8.143E+004 7.114E+004 3 . 72 5E+004 756.80 4. 52 3 .123E+005 1.181E+005 1 .404E+00 5 873. 1 8 12.08 1 .115E+005 - 1. 2 07E+005 4.949E+004 996. 2 9 10.48 1.536E+005 8.569E+003 6.905E+004 1004.76 18.01 9.121E+004 9.346E+004 4.109E+004 1274.43 34.80 4.941E+004 2 . 23 7E+004 2 .209E+004 1 596.48 1. 80 6.411E+005 -4.727E+005 2.628E+005 Eu-155 45.30 1. 31 9.119E+005 7.05E+004 1.943E+005 4.317E+005 60.01 1. 22 1.271E+006 -5.124E+005 6.095E+005 86.55 30.7 0 7.048E+004 3.330E+004 3 .421E+004 10 5.31 2 1. 1 0 9.160E+004 - 9.047E+002 4.428E+004 Tl-208 583.19 85.0 0 2.272E+004 2 . 2 7E+004 2 .076E+004 1.062E+004 Bi-21 1 351.07* 1 3.0 2 9.055E+004 9.06E+004 1 .132E+005 4.154E+004 Pb-2 1 1 404.85 3.78 4.199E+005 4. 2 0E+005 -5.025E+004 1.961E+005 427.09 1. 76 8.738E+005 - 4.198E+005 4.064E+005 832.01 3.5 2 4.586E+005 - 4.462E+004 2 .082E+005 Bi-212 39.86 1. 06 1 . 0 39E+006 2.37E+005 -1.854E+005 4.893E+005 727.33 6.67 2 . 3 67E+005 -1. 2 53E+005 l.079E+005 785.37 1.10 1.446E+006 -3 .902E+005 6.574E+005 1620.50 1. 47 6.326E+005 2 .107E+005 2 .451E+005

+     Pb-2 1 2     115.18       0.60   3.191E+006     2.96E+004      1. 3 90E+006  1. 542E+006 238.63*    43.60    2 .955E+004                   2.978E+004    1. 3 86E+004 30 0 . 0 9   3.30   5.0 2 3E+005                -6.990E+005     2 .375E+005 Pb212-XR       74.8 2   10. 2 8  2 .565E+005    1 .4 1E+005    6.383E+005    1 .252E+005

77. 11 17. 1 0 l.414E+005 -4.580E+003 6.886E+004 87.35 3.97 5.472E+005 5.712E+005 2 .656E+005 89.78 1. 46 1.463E+006 9.906E+00 5 7.099E+005 Bi -2 14 60 9. 32 45.49 5.436E+004 5.44E+004 8.750E+00 4 2 .577E+004 768.36 4.89 3.882E+005 4. 3 79E+005 1 .795E+005 8 0 6.18 1. 2 6 1. 25 9E+006 -6.191E+005 5.715E+005 934. 0 6 3.1 1 5.021E+005 l.524E+005 2 . 25 8E+005 1120.29 14 . 92 1 . 484E+005 6.762E+004 6.843E+004 1155. 21 1. 63 9.459E+005 - 1.064E+006 4.197E+005 1 23 8.12 5.83 3.662E+005 -1.482E+005 1.677E+005 1280.98 1. 43 1.180E+006 -1.640E+005 5. 2 60E+005 1377.67 3.99 4.891E+005 3 .941E+005 2 . 2 07E+005 1385. 3 1 0.79 1.842E+006 -4.133E+005 8.009E+005 1401.52 1. 33 1. 2 55E+006 4.789E+005 5.551E+005 1407.99 2 .39 6.989E+005 2 .014E+005 3.092E+005 1509.21 2 .13 6. 3 14E+005 1.044E+005 2 .686E+005 1661.27 1. 05 1.059E+006 4.504E+005 4.278E+005

[117]

1clide MDA Report 5/3/2016 6: 53 :0 2 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi -2 1 4 1729.59 2 .88 4.875E+005 5 .44E+004 2 .799E+005 2 .059E+005 1764.49 15.30 1 .632E+005 1.918E+005 7.438E+004 1847.43 2 .03 6.538E+005 - 2 .988E+005 2 .712E+005

 >                2 118.51      1. 16 O.OOOE+OOO                      O.OOOE+OOO     O.OOOE+OOO

+ Pb-214 2 41.99* 7.25 1.777E+005 3 . 3 1E+004 1 .791E+005 8.333E+004 2 95. 22 18.4 2 9.556E+004 3.366E+004 4.536E+004 351.93* 35.60 3.312E+004 4.139E+004 1. 519E+004 785.96 1. 06 1 .544E+006 8.740E+005 7.036E+005 Pb214-XR 74.82 5.80 4.547E+005 2 .49E+005 1.131E+006 2 . 2 18E+005 77.11 9.70 2 .494E+005 -8.073E+003 1. 2 14E+005 87.35 2 .24 9.698E+005 l.012E+006 4.707E+005 89.78 0.82 2 .605E+006 1.764E+006 1. 2 64E+006 Ra-226 186.21 3.64 4. 62 1E+005 4.62E+005 - 2.524E+004 2 .213E+005 Ac- 22 8 129.07 2.42 7.300E+005 8.41E+004 7.312E+004 3 .516E+005 209.25 3. 89 4.192E+005 2 .959E+005 2 .000E+005 270.24 3. 46 4.586E+005 5.450E+004 2 .170E+005 328.00 2.95 5.185E+005 3.415E+004 2 .433E+005 338.32 11.27 1.435E+005 4.588E+004 6.750E+004 409.46 1. 92 7.963E+005 -3.239E+005 3.708E+005 463.00 4.40 3.988E+005 3. 1 94E+005 1.867E+005 794.95 4.25 3.562E+005 -1.4 50E+005 1.610E+005 911. 20 25.80 8.409E+004 5.130E+004 3.904E+004 964.77 4.99 3.839E+00 5 3.988E+005 1.760E+005 968.97 1 5.80 1.159E+005 1. 2 1 3E+005 5. 2 91E+004 1588. 2 0 3.22 4.923E+005 1 .793E+005 2 .14 0E+005 Pa- 23 1 27.36 10.30 7.331E+004 7.33E+004 5.811E+004 3.357E+004 283.69 1. 70 9.302E+005 3.036E+005 4.394E+005 300.07 2 .47 6.710E+005 -9.339E+005 3.173E+005 302.65 2 . 2 0 7. 2 10E+005 -3.129E+005 3.400E+005 330.06 1. 40 1.063E+006 5.917E+005 4.978E+005 Th-234 92.38 2 .13 9.496E+005 9.50E+005 - 5.964E+005 4.598E+005 92.80 2 .10 9.763E+005 - 4.611E+005 4.730E+005 112.81 0.21 9.005E+006 -3.971E+006 4.350E+006 U- 235 143.76 10.96 1.645E+005 2 .93E+0 0 4 6.716E+004 7.926E+004 163.33 5.08 3.499E+005 -1.350E+005 1.683E+005 185.71 57. 2 0 2.929E+004 -5.067E+003 1.402E+004 2 02.11 1. 08 1.607E+006 -7.958E+005 7.691E+005 2 05.31 5.01 3.460E+005 1.676E+005 1.656E+005 Am-241 59.54 35 .90 4.308E+004 4.31E+004 4.159E+00 3 2 .066E+004

    +  = Nuclide identified during the nuclide identification
    *  = Energy line found in the spectrum
    >  = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @  = Half-life too short to be abl e to perform the decay correction

[118]

"*************************   *************************             *****************
"***        G A MMA      S P E C T R U M          A N A L Y S I S               *****
"********************~**************************************************

.lename: 5452 iport Generated On 4/18 /2 01 6 2 :50:44 PM tmple Title B306100AFRWC006GD tmple Description TB 560 tmple Identification tmple Type tmple Geometry iak Locate Threshold 3 .00 iak Locate Range (in channel s ) 85 - 81 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10.000 keV tmple Si ze 1.000E+OOO SQM tmpl e Taken On

quisition Started 4/ 1 8/2016 2 :40:4 3 PM

.ve Time 600.0 seconds ial Time 600.5 seconds iad Time 0.07 % Energy Calibration Used Done On 1 /13/2015 Efficiency CalibLa t ion Used Done On 4/14/2016 Efficiency ID TBWALL L)c1.\o. \\~\, c\0-\eJ k, G'~ 7

                                                                     /J ..5-IS
                                                                      ~"

[119]

iak Analysis Report 4/18/ 2 01 6 2 : 50: 4 4 Pl\ Page 2

- - - P E A K A N A L Y S I S R E P O R T *****

Detector Name: 545 2 Sample Title: B306100AFRWC006GD Peak Analysis Performed on: 4/18/2016 2:5 0 :44 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV ) Area Uncert. Counts 1 945 - 959 954.9 7 238.60 0.76 4.17E+001 28.75 5.63E+001 2 1401- 1414 1407.0 2 351. 73 0.85 4.75E+001 2 1. 2 0 2 .35E+001 3 1584 - 1593 1588.35 397.10 0.76 8.03E-001 13.07 1.82E+001 4 2430 - 2441 2 435. 2 1 608.98 0.96 4.56E+001 18.09 1.44E+001 5 5831 - 5851 5840.09 1460. 2 9 1. 64 1.50E+00 2 2 7.37 1 .llE+OO l First peak in a multiplet region Other peak in a multiplet region

= Fitted singlet

rors quoted at 2 .000 sigma

[120]

1terf erence Corrected Act. ~ ty Report 4/ 1 8/ 2 016 50: 4 4 PM Page 3

- - - - * *************************
    - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****
      - * ****************************************************

Sample Title: B306100AFRWC006GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activit y Name Confidence (keV) ( %) (pCi/SQM ) Uncertainty K-40 1. 000 1460.8 2

10.66 1 .02 1 84E+006 2 .06614E+005 Sn-11 3 0. 900 2 55.1 3 2 .11 391.7 0
64.97 4. 72 794E+002 7.69958E+003 Pb-212 0.87 2 115.18 0.60 23 8.63* 43.60 2 .83124E+004 2 .00315E+004 300.09 3.3 0 Pb-214 0. 4 92 2 41. 99* 7. 2 5 1 .7024~E+005 1. 2 0388E+005 2 95. 22 18.42 351.93* 35.60 4.795 03E+ 00 4 2 . 2 7426E+004 785.96 1. 06

      * = Energy line found in the spectrum.
      @=Energy line not used for Weighted Mean Activit?

Energy Tolerance : 1 0.000 keV Nuclide confidence index threshold = 0.3 0 Errors quoted at 2 .000 sigma [121]

tterference Corrected Act: ty Report 4/18/ 2 01 6 >0: 4 4 PM Page 4

- - - - * *****************************************************

"*** I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nucl ide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 1 .0 2 1842E+006 2 . 0 66142E+005 Sn-11 3 0.900 4.7 2 7943E+002 7.699580E+003 X Bi- 2 1 1 0.999 Pb- 212 0.872 2 .033793E+004 2 .037507E+004 Pb- 2 14 0. 492 4.795032E+004 2 . 2 74184E+004

     ? = Nuclide is part of an undetermined solution V

L\. Nuclide rejected b y the interference analysi s

     @      Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at        2 . 000 sigma
 **********       U N I D E N T I F I E D           P E A K S         **********

Peak Locate PPrfnrmerl on: 4/18/ 2 01 6 2 :50:44 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV) Counts per Second 9-; Uncertainty Type Nuclide 4 608.98 7.5944E-00 2 39.7 0 Tol. Zr-97 Sb-125 Sb-125 Cs - 134 Bi -2 14 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [122]

1clide MDA Report 4/18 /2 01l 2 :50:44 PM Page 5

- - - N U C L I D E M DA R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample Title: B306100AFRWC006GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Acti1.7ity Dec. Level Name ( keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) (pCi/SQM)

+      K-40       1460.82*     10.66 l.556E+005       1.56E+005 1.022E+006        6.857E+004 Cr-51         320.08      9.91 1.402E+005      1.40E+005 1.848E+004        6.541E+004 Mn-54         834.85    99.98 1.617E+004       1.62E+004 8. 3 00E+003      7. 3 43E+00 3 Co-58        810.76     99.45 1.337E+004       1.34E+004 -4.954E+00 2      5.947E+00 3 Co-60      11 73. 2 3   99.85 1.383E+004       1.15E+004 -2 . 2 10E+003    6.0 3 6E+00 3 1332.49      99.98 1.149E+004                   -3 . 2 74E+003  4.811E+00 3 Nb-94        702.65     99.81 1.576E+004       1. 23E+004    4. 3 49E+003  7.194E+003 871. 09    99.89 1. 2 27E+004                 - 7.479E+003    5.379E+003

+ Sn-11 3 255.13 2 .11 6. 2 74E+005 1.41E+004 - 7.358E+005 2 .941E+005 391.70* 64. 97 1.414E+004 4.728E+002 6.273E+003 Cs-134 475.36 1. 48 1.073E+006 1.57E+004 1 .813E+005 4.980E+005 563.25 8.34 l.911E+005 9.444E+004 8.813E+004 569.33 15.37 9.690E+004 -4.969E+004 4.442E+004 604.72 97. 62 2 . 27 8E+004 -1.114E+004 1.074E+004 795.86 85.46 1.573E+004 -1.572E+002 7.015E+003 801. 95 8.69 1.523E+005 -8. 22 4E+004 6.773E+004 1038.61 0.99 1.315E+006 6.555E+004 5.741E+005 1167.97 1. 79 7.697E+005 -3.4 3 0E+005 3.360E+005 1365.19 3.02 5.071E+005 - 3.0 5 6E+005 2 . 22 2E+005 Cs-137 661.66 85.10 2 .065E+004 2 .07E+004 1. 2 47E+004 9.542E+00 3 Eu-1 52 1 2 1.78 2 8.67 6. 2 03E+004 5 .22E+004 3. 2 85E+004 2 .989E+004 2 44.70 7.6 1 2 .121E+005 -6.661E+004 1. 0 07E+005 2 95.94 0.45 3 .871E+006 2 .974E+006 1.836E+006 3 44. 2 8 2 6.60 5.222E+004 -2 .432E+004 2.430E+004 3 67.79 0.86 1.812E+006 7.514E+005 8.485E+005 411.1 2 2.24 6.745E+005 - 1.451E+002 3.137E+005 443.96 2.83 4.997E+005 3 .116E+005 2 .305E+005 488.68 0.42 3 .633E+006 1.990E+006 1 .680E+006 563.99 0.49 3 .247E+006 2 .111E+006 1.498E+006 586. 2 6 0.46 3 .948E+006 3 .194E+006 1.837E+00 6 678. 62 0.47 3 .157E+006 -1.173E+006 1.435E+00 6 688.67 0.86 1.770E+006 -5 . 55 6E+005 8.056E+005 7 1 9.35 0.28 5.630E+006 -2 .743E+006 2 . 5 66E+006 778.90 12.96 1. 2 08E+005 4.081E+004 5 .487E+004 810.45 0.32 4. 2 24E+006 1.020E+006 l.883E+006 867.37 4.26 3.017E+005 -5 .905E+004 1. 33 1E+005 919.33 0.43 3.020E+006 1.757E+005 l. 32 8E+006 964.08 14.65 1.432E+005 5.330E+004 6 .617E+004 1085.87 10. 2 4 1.638E+005 9.141E+00 3 7. 3 66E+004 1 089.74 1. 73 8.496E+00 5 -5.908E+005 3 .759E+005 1112.07 1 3 .69 1 .357E+00 5 1. 22 6E+004 6 .162E+004 1212.95 1. 43 1. 22 0E+00 6 -2 .308E+004 5 .476E+00 5 [123]

1clide MDA Report 4/18/201L 2 :50:44 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM) Eu-152 1249.94 0. 1 9 9.013E+006 5 . 2 2E+004 4.757E+006 4.028E+006 1299.14 1. 63 9.170E+005 2.464E+003 4.018E+005 1408.01 2 1. 07 7.941E+004 6.754E+004 3.514E+004 1457.64 0.50 9.121E+006 2 .439E+007 4.365E+006 1528. 1 0 0. 2 8 3 .978E+006 1.854E+006 1.631E+006 Eu-154 123. 07 40.40 4.292E+004 3.90E+004 1.932E+004 2.066E+004 247.93 6.89 2 .082E+005 - 7.224E+004 9.819E+004 59 1. 76 4.95 3 . 3 61E+005 1.287E+005 1.553E+005 692.42 1. 78 8.686E+005 6.382E+004 3.959E+005 7 23 .30 2 0.06 8.606E+004 - 5.286E+004 3.956E+004 756.80 4.52 3.419E+005 8.097E+003 1.552E+005 873. 1 8 12.08 1.161E+005 2 .992E+004 5. 1 79E+004 996.29 10.48 1 .4 2 9E+005 3 .098E+004 6.373E+004 1 004.76 18.01 7.115E+004 5.340E+004 3.106E+004 1274.43 34.80 3.898E+004 4.845E+002 l.687E+004 1 596.48 1. 80 5.597E+005 - 1. 494E+005 2 .221E+005 Eu- 1 55 45.30 1. 31 9.038E+005 7.41E+004 7.767E+005 4.276E+005 6 0 .0 1 1. 22 1.341E+006 -3 .052E+005 6.447E+005 86.55 30.70 7.410E+004 4.022E+004 3.601E+004 10 5.3 1 2 1. 10 8.474E+004 8.534E+001 4.086E+004 Tl-2 0 8 583.19 85 . 00 2 . 1 15E+004 2 .11E+004 1 . 603E+003 9.836E+003 Bi- 2 11 351. 07* 13.02 8. 0 64E+004 8.06E+004 1 .311E+005 3.658E+0 04 Pb-211 40 4.85 3.78 4.052E+005 4.05E+005 3.450E+005 1.888E+005 427.09 1. 76 8. 3 92E+005 -1.603E+005 3.891E+005 832.01 3.52 4.392E+005 7.401E+003 1.985E+005 Bi-212 39. 86 1. 06 8.916E+005 2.65E+005 1.880E+005 4.158E+005 727.33 6.67 2 .648E+005 l.874E+005 1. 22 0E+005 785.37 1.10 l.303E+006 1.041E+006 5.859E+005 1620.5 0 1. 47 7.909E+005 7.900E+004 3.242E+005

+     Pb-2 1 2     115.18       0.60   3.095E+006     3.05E+004      9.978E+005    1.494E+006 238.63*    43.60    3.049E+004                    2.831E+004    1.433E+004 300.09       3.30   4.834E+005                  -4.858E+005     2 . 2 81E+005 Pb2 12-XR      74.8 2   10. 2 8  2 .382E+005    l.38E+ 00 5    4.447E+005    1 . 160E+005 77.11    17.10    1.375E+005                    8.827E+004    6.691E+004 87.35      3 . 97 5.702E+005                    1 .603E+005   2 .771E+005 89.78      1. 46  1.465E+006                    2 . 25 0E+005 7. 1 09E+005 Bi -2 14     609.3 2    45.49    4.830E+004     4.83E+004      4 .314E+004   2 . 2 74E+004 768.36       4.89   3.350E+005                    9.468E+004    l.5 2 9E+005 806.18       1. 26  l . 1 50E+006                 9.155E+00 5   5 . 170E+005 934.06       3.1 1  5.498E+005                    2.860E+005    2 .496E+005 1120. 2 9    1 4.92   1.333E+005                    4.737E+004    6.089E+004 1155.21        1. 63  1.058E+006                    3 .620E+005   4.759E+005 1238.12        5.83   3.446E+005                    2.479E+005    1.569E+005 1280.98        1. 43  1.005E+006                    4.147E+005    4 . 387E+005 1377.67        3.99   4. 2 33E+005                  7.089E+004    1.878E+005 1385.3 1       0.79   1.732E+006                  - 9.214E+005    7.456E+005 1401.52        1. 33  1 . 137E+006                  2 . 23 4E+005 4.965E+005 1407.99        2.39   6.989E+005                    5.944E+005    3.092E+005 1 509.21       2 .13  5.523E+005                    2 .785E+005   2.291E+005 1661.27        1. 05  1.127E+006                    5.094E+004    4.621E+005

[124]

1clide MDA Report 4/18/20ll 2 :50:44 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi- 2 1 4 1 729.59 2 .88 3.947E+005 4.83E+004 1.679E+005 1.595E+005 1764.49 15.30 1.136E+005 5. 1 96E+004 4.959E+004 1847.43 2 .0 3 5.812E+005 2 .473E+005 2 .348E+005

 >                 2 118.5 1      1.16    O.OOOE+OOO                  O.OOOE+OOO O.OOOE+OOO

+ Pb- 2 14 2 41.99* 7.25 1 .834E+005 2 .95E+004 l.702E+005 8.616E+004 2 95. 22 18.4 2 9. 2 46E+004 1.949E+004 4.381E+004 3 51.93* 35.60 2 .949E+004 4.795E+004 1.338E+004 785.96 1. 06 1. 3 09E+006 4.360E+005 5.863E+005 Pb2 1 4-XR 74.82 5.80 4.222E+005 2 .42E+005 7.882E+005 2 .056E+005 77.11 9.70 2 .425E+005 1.556E+005 1 .179E+005 87.35 2.24 1.011E+006 2 .841E+005 4.911E+005 89.78 0 .8 2 2 .609E+006 4.006E+005 1. 2 66E+006 Ra- 226 186. 2 1 3.64 4.478E+005 4.48E+005 1. 4 71E+005 2.142E+005 Ac- 22 8 1 2 9.07 2 .42 6.991E+005 8.13E+004 2.400E+005 3.362E+005 2 09. 2 5 3 .89 3.965E+005 2 .438E+005 1.886E+005 2 70. 2 4 3 .46 4.502E+005 -3.550E+005 2 .128E+00 5 328. 00 2 .95 4.932E+005 3.746E+005 2.307E+005 338.32 11. 27 1.427E+005 5.900E+004 6.711E+004 409.46 1. 92 7.404E+005 -8.949E+005 3.428E+005 463. 00 4.40 3.375E+005 -6.939E+004 1.561E+005 794.95 4.25 3.100E+005 -2.546E+005 1.379E+005 91 1. 20 25.80 8.130E+004 6.334E+004 3.764E+004 964.77 4.99 4. 2 45E+005 1 .386E+005 1.963E+005 968.97 15.80 1. 2 94E+005 5.771E+004 5.963E+004 1588.20 3. 22 4.308E+005 -7.719E+004 1.833E+005 Pa -23 1 27.36 10.30 6.334E+004 6.33E+004 1.676E+004 2 .858E+004 283.69 1. 70 8.060E+005 2.913E+005 3.773E+005 3 00 . 0 7 2 .47 6.459E+005 -6.490E+005 3.047E+005 302.65 2 . 20 6.911E+005 9.472E+004 3.250E+005 330.06 1. 40 1.043E+006 -3.557E+005 4 .876E+005 Th-234 92.38 2. 1 3 9.807E+005 9.81E+005 -7.644E+004 4.754E+005 92.80 2 .10 1.000E+006 4.544E+005 4.850E+005 112.8 1 0. 2 1 8.764E+006 6.833E+006 4. 2 30E+006 U-235 1 43.76 1 0.96 1 .548E+005 2.92E+004 5.645E+004 7.436E+004 163.33 5.08 3 .132E+005 -1.028E+005 1 .499E+005 185.71 57.20 2 . 92 0E+004 3.288E+004 1 .398E+004 202. 1 1 1. 08 1.389E+006 - 8.197E+004 6.602E+005 2 05.3 1 5.0 1 2 .912E+005 -1.935E+005 1.382E+005 Am-24 1 59.54 35.90 4.548E+004 4.55E+004 -1.158E+004 2 .186E+004

    + = Nuclide identified during the nuclide identification

Energy line found in the spectrum

    >     Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @     Half-li fe too short to be able to perform the decay correction

[125]

*************************~ **************************                 ****************
****        G A MMA      S .I:' E C T R U M         A N A L Y S I S                *****

.lename: C:\GENIE2K\CAMFILES\00001336.CNF iport Generated On 4/14/2016 4:01:07 PM 1mple Title B306100AFRWC07GD 1mple Description U-1 STS TB PEDESTAL WALL 1mple Identification 1mpl e Type 1mpl e Geometry iak Locate Threshold 3. 00 iak Locate Range (in channels) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 1. 000 FWHM 1mple Size l.OOOE+OOO SQM 1mple Taken On

quisition Started 4/14/ 2 016 1: 4 8: 4 9 PM

.ve Time 600.0 seconds ial Time 600.4 seconds iad Time 0. 07 5ci Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBWALL l)~dt 'to.\,~ce\ed ky

IJ.-6'-J'l

                                                                        ~ /,Id

[126]

iak Analysis Report 4/14 /2 016 4: 01: 07 PI Page 2

- - - P E A K A N A L Y S I S R E P O R T *****
      - *******************************************************************

Detector Name: 5452 Sample Title: B306100AFRWC07GD Peak Analysis Performed on: 4/14 /2 01 6 4:01:06 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV) Area Uncert. Counts 1 296- 308 3 00 .79 74.85 0.33 4.73E+001 46.88 1 .90E+00 2 2 5825- 5850 5838. 2 7 1459.84 1. 54 1.58E+00 2 31. 05 1.94E+001 = First peak in a multiplet region = Other peak in a multiplet region = Fitted sing l et ~rors quoted at 2 .000 sigma [127]

1terference Corrected Act: ty Report 4/14 /2 01 6 ) 1:07 PM Page 3

"*** N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Ti t le: B306100AFRWC07GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K- 40 0. 950 1460.82* 10.66 1.07 3 97E+006 2 .31293E+005

       * = Energy line found in the spectrum.
       @=Energy line not used for Weighted Mean Activity Energy Tolerance :      1.000 FWHM Nuclide confidence index threshold          0.30 Errors quoted at 2.000 sigma

[128]

1terference Corrected Act: ty Report 4/ 1 4/ 2 016 )1:07 PM Page 4

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      - * *********************************************************

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0.950 1.073970E+006 2.312934E+005

     ? = Nuclide is part of an undetermined solution X  = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Error s quoted at       2 .000 s i gma
 **********        U N I D E N T I F I E D         P E A K       s  **** ,: ** ***

Peak Locate Performed on: 4/14/2016 4:01:06 PM Peak Locat e From Channel: 85 Pea k Locate To Channel: 8192 Peak En ergy Peak Si ze in Peak CPS Peak Tol. No . ( keV) Counts per Second % Uncertainty Type Nuclide 1 74.8 5 7 .887 1E-00 2 99. 0 7 Tol. Pb212-XR Pb214-XR M = First peak in a multiplet region m Other peak in a multiplet region F Fitted singlet Errors quot ed at 2 . 000 s igma [129]

1cl ide MDA Report 4/14/ 2 01 4:01:07 PM Page 5

- - - N U C L I D E M D A R E P O R T *****
      - * **

Detector Name: 545 2 Sample Geometry: Sample Title: B306100AFRWC07GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) K-40 1460.8 2

10 .66 2. 2 34E+005 2 . 2 3E+005 1.074E+00 6 1.025E+005

+                                                                                     6.184E+004 Cr-5 1       32 0.08       9.91   l.330E+005      l. 3 3E+005 - l.280E+005 Mn-54        83 4.85     99.98    l.375E+004      l .3 7E+004 9.914E+00 3      6.130E+00 3 Co- 5 8      810.76      99.45    l.130E+004      1 . 13E+004 -8.048E+00 3     4.910E+00 3 Co-60      1173. 23      99.85    l.744E+004      l . 15E+004 1. 2 91E+004     7.841E+00 3 1332.49       99.98    l. 1 49E+004                   6. 2 04E+003  4.811E+00 3 Nb-94        70 2 .65    99.81    l.455E+004      l .35E+004 l.0 1 3E+003      6.585E+00 3 871. 09     99.89    l.347E+004                     2 .403E+003   5.978E+00 3 Sn-1 1 3     255.13        2 .11  7.468E+005      2 .06E+004 -1.919E+005       3.538E+005 39 1 .70    64 . 97  2 .064E+004                  -8.483E+003     9.5 2 7E+003 Cs-13 4      475.36        1. 48  9.812E+005      1.93E+004 -4.111E+005        4.522E+005 563.25        8.3 4  l. 609E+005                  -l.251E+005     7.308E+004 569.33      15.37    9.015E+004                     4.324E+004    4.104E+004 604.72      97. 62   l.932E+004                     4.090E+003    9.004E+003 795.86      85.46    l.974E+004                     2 .042E+004   9.017E+003 801. 95       8.69   l.696E+005                     6.822E+004    7.641E+004 10 3 8.61       0 .99  l .385E+006                    4.370E+005    6.089E+005 1 167.97        1. 79  9.706E+005                     3 .079E+005   4. 3 65E+005 1365.19         3 .0 2 3 . 2 67E+005                  l.390E+005    l. 32 0E+005 Cs- 1 37     661.66      85. 1 0  l . 3 33E+004   l.33E+004 -3. 54 1E+003      5.882E+003 Eu-152       121.78      28.67    6. 2 40E+004    4.98E+004 -5.553E+003        3.008E+004 244.70        7.61   2 .121E+005                    l.578E+00 3   l.007E+005 295.94        0 .45  3 .465E+006                  -9.608E+005     l.633E+006 344. 2 8    2 6.60   4.977E+004                   -7. 2 03E+004   2 .307E+004 367.79        0 .86  1 .641E+006                    l. 33 4E+006  7.628E+005 41 1. 12      2.24   6 .141E+005                  - 4.0 6 0E+005  2.835E+005 443.96        2.83   4.900E+005                     9 .1 7 1E+004 2.256E+005 488.68        0.42   2 .935E+006                  - 3 . 3 73E+005 1.330E+006 563.99        0.49   2 .735E+006                  -7 . 3 91E+005  l . 2 42E+006 586. 26       0 . 46 3.794E+006                   -1. 2 1 0E+005  1 .760E+006 678. 62       0.47   2 .937E+006                    7.115E+004    l.326E+006 688. 67       0.86   1.493E+006                   - 8.122E+005    6 .671E+005 719.35        0. 2 8 4.688E+006                     2 .758E+005   2 .095E+006 778.90      12.96    l.157E+005                     2 .771E+004   5. 23 1E+004 810.45        0. 32  3 .789E+006                  -l.172E+004     l.666E+006 867.37        4.26   3 . 2 83E+005                -1. 732E+005    l.464E+005 919.33        0.43   2 .946E+006                  - 1.009E+006    1. 2 91E+006 96 4 . 0 8  14.65    l. 2 78E+005                 -2 .542E+004    5.844E+004 1085.87       10.24    l.105E+005                   -9. 099E+004    4.702E+004 1089.74         1. 73  6.553E+005                   -4 . 927E+004   2 .788E+005 11 1 2 .07    13.69    l.131E+005                   -l.823E+004     5.031E+004 12 1 2 .95      1. 43  l.132E+00 6                  -2 .948E+005    5.037E+005

[130]

1clide MDA Report 4/14/ 2 01 4:01:07 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) {pCi/SQM ) (pCi/SQM ) Eu-15 2 1249.94 0.1 9 9.812E+006 4.98E+004 1.025E+007 4.428E+006 1 2 99.14 1. 63 8.682E+005 -1.920E+005 3.774E+005 1408.01 2 1 .07 7.392E+004 3.308E+004 3.239E+004 1457.64 0.50 9.623E+006 2 .446E+007 4.616E+006 1 528.10 0. 2 8 3.978E+006 1.854E+006 l .631E+006 Eu-154 123.07 40.40 4.373E+004 4 .3 7E+004 5 . 2 59E+00 3 2 .107E+004 2 47.93 6.89 2 .185E+005 -1.049E+005 1.033E+005 591.76 4.95 2 .779E+005 3.862E+003 1. 262E+005 692.42 1. 78 7.875E+005 5. 0 35E+005 3.554E+005 723.30 2 0.06 6.537E+004 - 1 . 1 56E+004 2 . 922 E+004 756.80 4.52 3.174E+005 9.750E+003 1 .430E+005 873.18 12.08 1.067E+005 -1.420E+005 4.707E+004 996. 2 9 10.48 1.250E+005 -1. 32 1E+005 5.479E+004 1004.76 18.01 8.973E+004 4.756E+004 4.035E+004 1274.43 34.80 4.848E+004 3. 107E+004 2. 162E+004 1 596.48 1. 80 4.596E+005 - 2 .348E+00 5 1.720E+005 Eu-155 45.30 1. 31 8.956E+005 6.97E+004 9.506E+005 4. 2 35E+005 60.0 1 1. 22 1.345E+006 4.582E+005 6.462E+005 86.55 3 0.70 6.974E+004 8.919E+004 3 . 3 83E+004 105.31 2 1.10 8.752E+004 5.847E+004 4. 22 5E+004 Tl-2 0 8 583.19 85.00 2 .082E+004 2.08E+004 2 .313E+004 9.670E+003 Bi-2 11 351.07 13.02 1.384E+005 l.38E+005 1.486E+005 6.546E+004 Pb-2 11 404.85 3.78 3.772E+005 3.77E+005 -1.898E.+005 1 .7 48E+005 427.09 1. 76 8.805E+005 2.763E+005 4. 0 98E+005 832.01 3.52 4.118E+005 5 .873E+004 1.848E+005 Bi-21 2 39.86 1. 06 1.011E+006 2 . 2 1E+005 4.357E+005 4.755E+005 727.33 6.67 2. 2 12E+005 6.570E+004 l.001E+005 785.37 1.10 1.346E+006 - 2 .047E+004 6.072E+005 1620.50 1. 4 7 6.905E+005 -5.425E+005 2 .740E+005 Pb-212 115.18 0.60 3.038E+006 4.40E+004 7.272E+005 1.465E+006 23 8.63 43.60 4 .3 95E+004 3.788E+004 2 .106E+004 300.09 3.30 4.432E+005 1. 2 86E+005 2 .080E+005 Pb212-XR 74.82 10. 2 8 2 . 23 6E+005 l. 2 4E+005 4.196E+005 1.087E+005 77.1 1 17. 1 0 1.242E+005 -2 .622E+004 6.023E+004 87.35 3.97 5.386E+005 3 .483E+005 2 .613E+005 89.78 1. 46 1.390E+006 7.544E+004 6.733E+005 Bi -2 1 4 609. 32 45.49 4.310E+004 4.3 1E+004 4.563E+004 2 .014E+004 768.36 4.89 3.350E+005 3.3 00E+004 1.529E+005 806.18 1. 2 6 9.599E+005 2 . 72 6E+005 4. 22 1E+005 934. 0 6 3.11 4.392E+005 -1.410E+005 l.943E+005 1 120.29 14.92 1 . 1 79E+005 3.964E+004 5.319E+004 1155.21 1. 63 1.058E+006 - 2 .340E+005 4.759E+005 1 238.12 5.83 3.401E+005 1.617E+005 1.546E+005 1 280.98 1. 43 1.133E+006 -1.179E+004 5.026E+005 1 377.67 3.99 4.408E+005 2 .758E+005 1.966E+005 1 385.3 1 0.79 1.788E+006 -4.651E+005 7.737E+005 1 401.5 2 1. 33 1 .039E+006 6.936E+005 4.4 7 6E+005 1407.99 2.39 6.506E+005 2 .911E+005 2.851E+005 1509.21 2.13 5.523E+005 -2 . 3 93E+004 2 . 2 91E+005 1661.27 1. 05 8.081E+005 -2 . 62 8E+005 3.0 2 5E+005 [131]

iclide MDA Report 4/14/201 4:01:07 PM Page 7 Nuclide Energy Yi eld Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) (pCi/SQM) Bi-214 1729.59 2 .88 3.013E+005 4.31E+004 - 3.265E+005 l. 1 2 8E+005 1764.49 15.30 1.590E+00 5 1.355E+005 7. 22 9E+004 1847.43 2 .03 4.950E+005 1.648E+005 l.917E+005 2118.51 1.16 O.OOOE+OOO O.OOOE+OOO O.OOOE+OOO

Pb-2 14 241.99 7. 2 5 2 .537E+005 5.04E+004 9.848E+004 l.213E+005 2 95. 22 18.42 8.675E+004 1.833E+004 4.096E+004 351.93 35.60 5.044E+004 5 .208E+004 2 .386E+004 785.96 1. 06 1.463E+006 1 . 3 35E+005 6.633E+005 Pb2 1 4-XR 74.82 5.80 3.964E+005 2 .19E+0 0 5 7.437E+005 1. 927E+005 77.11 9.70 2 .189E+005 -4. 62 1E+004 1.062E+005 87.35 2.24 9.545E+005 6.172E+005 4.631E+005 89.78 0.82 2 .475E+006 1 .343E+005 l .199E+006 Ra-226 186.21 3.64 4.304E+005 4.30E+005 -3.134E+004 2.054E+005 Ac- 22 8 129.07 2.42 6.783E+005 7.14E+004 -1.485E+005 3. 2 57E+005 209. 2 5 3.89 4.137E+005 - 2 .168E+004 l .972E+005 27 0. 2 4 3 . 46 4.439E+005 2.419E+004 2.096E+005 32 8.00 2.95 4.489E+005 5.113E+004 2 .085E+005 338.32 11. 27 1 .311E+005 3.424E+004 6.133E+004 409.46 1. 92 7.404E+005 1.888E+005 3 .428E+005 463.00 4.40 3.313E+005 2 .348E+003 1 .530E+005 794.95 4 . 25 3.870E+005 1.574E+005 1.764E+005 911. 2 0 25.80 7. 1 42E+004 2 . 0 57E+004 3.270E+004 964.77 4.99 3.924E+005 1.900E+005 1.802E+005 968.97 15.80 1.255E+005 3.250E+004 5.769E+004 1588. 2 0 3. 22 3.114E+005 1.188E+005 l. 23 6E+005 Pa-2 31 27.36 10. 3 0 7.497E+004 7.50E+004 2 .257E+004 3.440E+004 283.69 1. 70 7.904E+005 - 7.363E+005 3.695E+005 300.07 2 .47 5.922E+005 1.718E+005 2 .779E+005 302.65 2 . 20 5 .872E+005 8.562E+004 2 .731E+005 330. 0 6 1. 40 9.099E+005 - 3.141E+005 4. 2 13E+005 Th-23 4 92.38 2.13 9.129E+005 9.13E+005 -5.630E+005 4.415E+005 92.8 0 2 . 10 9.246E+005 -2 .597E+005 4.471E+005 112.81 0 .2 1 8. 2 27E+006 -1.680E+006 3.961E+006 U-235 1 43.76 10 .96 1.395E+005 2.76E+004 2 .315E+004 6.676E+004 1 63.33 5. 0 8 3.069E+005 1.721E+005 l .467E+005 185.7 1 57. 2 0 2 .761E+004 - 8.020E+003 1.319E+004 202. 11 1. 08 1.394E+006 -2 .548E+004 6.628E+005 205.3 1 5.0 1 3.172E+005 4. 3 95E+004 1.512E+005 Am- 2 41 59.5 4 35.90 4.527E+004 4 . 53E+004 8.849E+003 2 .175E+004

     +  =  Nuclide identified during the nuclide identification
     *  =  Energy line found in the spectrum
     >  =  Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ =   Half-life too short to be able to perform the decay correction

[132]

*************************     ************************* '       *****************
****        GAMM A        S P E C T R U M         A N A L Y S I S              *****
************************************************************************

.l ename: E:\4 -2 6-17\TB 56 0 SP08.CNF iport Generat ed On 4/27/2 01 7 11:34:35 AM tmpl e Title B306100AFRFC008GD tmpl e Description TURBINE BUILDING tmple Identification SP08 tmple Type tmple Geometry TB FLOOR iak Locate Threshold 3. 00 iak Locate Range (in channels ) 85 - 8 1 92 iak Area Range (in channels) 85 - 8 1 92 lentification Energy Tolerance 10.000 keV tmple Size 1.000E+OOO SQ M tmple Taken On 2/4/2 0 16 8:47:00 AM

quisition Started 2/4/2 01 6 8:47:19 AM

.ve Time 600.0 seconds ial Time 600. 3 s e conds iad Time 0 .05 % Energy Calibration Used Done On 1/27/2015 Efficiency Calibration Used Done On 4/24/2017 Efficiency ID TBFLOOR

1) o.\ ~ 1o.\\do.\ed O\f 0~'4- I

                                                              /,2-5-J'o
                                                               ~ (p/O

[133]

iak Analysis Report 4 /2 7/ 2 017 11:34:35 A Page 2

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Detector Name: 5456 Sample Title: B306100AFRFC008GD Peak Analysis Performed on: 4/ 27/2 017 11:34: 3 5 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroi d ( keV) (keV ) Area Uncert. Counts 1 5826- 5851 5840.56 1 459 .4 5 1.8 1 1.69E+002 2 8.01 6.50E+OOO

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 .000 sigma

[134]

1terf erence Corrected Act. ... ty Report 4/27/2017 1 34:35 AM Page 3

- - - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

'****************************************************************** * **** Sample Title: B306100AFRFC008GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL . NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQ M) Uncertainty K-40 0.997 1460.82* 10 .66 1 .14839E+006 2 .1538 1E+0 05

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold=             0.30 Errors quoted at 2 .000 sigma

[135]

1terference Corrected Act _ i ty Report 4/ 2 7 /2 017 1 3 4 :35 AM Page 4

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-*********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 0.997 1.148392£+0 0 6 2.153807£+005

     ? = Nuclide i s part of an undetermined solution X = Nuclide rejected by the interference analysi s
     @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2 . 000 s igma
 **********     U N I D E N T I F I E D          P E A K S        **********

Peak Locate Performed on: 4/ 27/2017 11:34:35 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV) Counts per Second % Uncertainty Type Nuclide Al l peaks were identified. [136]

1clide MDA Report 4/27/ 2 01 1 1:34:35 AM Page 5

- - - N U C L I D E M D A R E P O R T *****

Detector Name: 5456 Sample Geometry: TB FLOOR Sample Title: B306100AFRFC008GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV} ( %} (pCi/SQ M) (pCi/SQ M} (pCi/SQ M} (pCi/SQ M)

+      K-40       1460.82*     10.66     1.364E+005     1.36E+005 1.148E+006          5.895E+004 Cr-51        32 0.08      9.91    1.460E+005     1.46E+005 - 6.017E+004        6.832E+004 Mn-54        834.85     99.98     1.348E+004     1.35E+004 - 2.541E+003        5.995E+00 3 Co-58        810.76     99.45     1.390E+004     1.39E+004 4.876E+003          6. 2 11E+003 Co-60      117 3 . 23   99.85     1.491E+004     1.30E+004 1.135E+003          6.578E+003 1 332 .49    99.98     1. 2 98E+004                - 1. 2 97E+004   5.555E+003 Nb-94        702.65     99.81     1. 4 96E+004   1. 2 9E+004 -5.392E+002       6.794E+003 871. 09    99.89    1.289E+004                     4.907E+003     5.686E+003 Sn-113       255.13       2.11    6.721E+005     2 .06E+004 -4.634E+005        3. 1 64E+005 391. 70    64.97    2 .064E+004                  -8.611E+003      9.527E+003 Cs-134       475.36       1. 48   9.518E+005     1.69E+004 6.112E+005          4.375E+005 563 . 2 5    8 . 34  l . 737E+005                -5 . 069E+004    7.944E+004 569.33     15.37     9.904E+004                    2 .774E+003    4.549E+004 604.72     97. 62   2 .513E+004                    2 .1 1 1E+004 1.191E+004 7 95. 8 6  85.46    1.690E+004                     1 . 3 46E+004 7.601E+00 3 801.95       8.69   1.427E+005                   -1.042E+005      6. 2 94E+004 1038.61        0.99   1.631E+006                     1. 2 86E+006  7. 3 19E+005 1167.97        1. 79  8.104E+005                   -6.008E+005     3.564E+005 1365.19        3.0 2  4.660E+005                     4.054E+004    2.017E+005 Cs-137        661.66     85.10    1.906E+004      l.91E+004 l.305E+004         8.746E+00 3 Eu- 1 52      121.78     2 8.67   6. 3 14E+004    5.07E+004 - 8.558E+003       3.045E+004 244.70       7.61   2 .138E+005                    8.094E+004    1.016E+005 295.94       0.45   3.839E+006                     1.672E+006    1.8 2 0E+006 344. 2 8   2 6.60   5.261E+004                  -1.083E+004      2.450E+004 367.79       0.86   1 .615E+006                 -2 .048E+005     7.497E+005 411.12       2 . 24 6.255E+005                  -4.631E+005      2.892E+005 443.96      2 .83   4.850E+005                  -2 .081E+005     2.232E+005 488.68       0.42   3.358E+006                    2 .840E+006    1 .542E+006 563.99       0.49   3.053E+006                     6 . 1 95E+005 1.401E+006 586.26        0.46   3.978E+006                    1.441E+006     1.852E+006 678.62       0.47   3.199E+006                    1.164E+006     1.456E+006 688.67      0.86    1.815E+006                    6.8 3 4E+005   8.283E+005 719.35       0. 2 8  5.024E+006                  - 1 .167E+006    2 .263E+006 778.90      12.96    1.192E+005                    4.7 2 1E+004   5.403E+004 810.45       0.32    4.305E+006                    6. 1 54E+005   1 .924E+006 867.37       4.26    3.086E+005                  -7 . 3 82E+004   1.365E+005 919.33       0.43    3.020E+006                    1.170E+006     l.328E+006 964.08     14.65     1.307E+005                    9.558E+004     5.992E+004 1085.87      10.24     1.464E+005                    2 .873E+004    6.497E+004 1089.74        1. 73   7.909E+005                  - l.987E+005     3.466E+005 1112.07      13.69     1.197E+005                  - 1.939E+005     5.363E+004 1212.95        1. 43   1 . 1 32E+006                 1.527E+005     5.037E+005

[137]

1clide MDA Report 4 /27/ 201 11:34:35 AM Page 6 Nuclide Energy Yield Line MDA Nuc l ide MDA Activity Dec. Level Name (keV ) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Eu-15 2 1249.94 0.19 7.933E+006 5.07E+004 2 .700E+005 3 .489E+00 6 1299.14 1. 63 6.981E+005 -1. 36 1E+005 2.924E+005 1408.01 21. 07 5.071E+004 -6 . 2 48E+004 2.079E+004 1457.64 0.50 9.375E+006 2 .584E+007 4.492E+006 1528.10 0.28 4.415E+006 -2 .605E+006 l.849E+006 Eu-154 123.07 40.40 4.478E+004 3.65E+004 l.882E+004 2 .159E+004 247.93 6.89 2 .145E+005 -4 .181E+004 l .013E+005 591. 76 4.95 2 .927E+005 4.025E+004 1.336E+005 692.42 1. 78 8.116E+005 1.841E+005 3.674E+005 723.30 2 0.06 7.005E+004 -1.419E+003 3.156E+004 756.80 4.52 2.608E+005 - l.1 2 9E+004 1 . 147E+005 873. 1 8 1 2 .08 1.067E+005 2 .107E+004 4.707E+004 996. 2 9 10.48 1.484E+005 1. 2 85E+004 6 .645E+004 1004.76 18.01 7.306E+004 -7.196E+004 3 . 2 02E+004 1274.43 34.80 3.648E+004 -3 .020E+004 1.562E+004 1596.48 1. 80 6.021E+005 -5.728E+005 2 .433E+00 5 Eu-155 45.3 0 1. 31 8.123E+005 6.68E+004 7.423E+004 3.816E+005 60.01 1. 2 2 1.260E+006 1.031E+005 6 . 038E+005 86.55 3 0 .70 6.683E+004 4.912E+004 3. 23 7E+004 105.31 21.10 8.919E+004 2 . 67 4E+004 4.308E+004

      'l'l-2 0 8   583.19   85.00    2.2 42E+004   2.24E+004    1 .82 0E+004   l ,047E+004 Bi-211       351. 07  13.02    1.621E+005    1.62E+005    1 . 770 E+00 5 7.7 3 0E+004 Pb-211       404.85     3. 7 8 3.868E+005    3.87E+005  -8.703E+004      1 .796E+005 427 .09    1. 76  7.649E+005               -1.691E+005      3 .5 1 9E+005 832 .01    3.52   3.898E+005               -1.131E+005      1.738E+0 0 5 Bi-2 12       39.86     1. 06  9.806E+005    2 .11E+005 -1.084E+005      4.600E+005 727.33     6.67   2 .112E+005                3 .396E+004    9.516E+004 785.37     1.10   1. 303E+006                1 .441E+005    5.859E+005 1 620.50     1. 47  7.428E+005               -4.389E+004      3 .001E+005 Pb-212       11 5.18    0.60   3 .002E+006   4.59E+004    3.638E+005     1. 447E+006 23 8.63  43.60    4.592E+004                 l.167E+004     2 . 2 04E+004 300.09     3.30   4.536E+005               -5.0 3 8E+005    2 .132E+005 Pb212-XR      74.82   10.28    2 .519E+005   l.40E+005    5. 2 01E+005   1 . 2 28E+005 77.11   17.10    1.404E+005                 9.702E+00 4    6.834E+004 87.35     3.97   5.122E+005                 1. 205E+005    2 .480E+005 89.78     1. 4 6 1.365E+006               -9.318E+005      6.604E+005 Bi-2 14      609.3 2  45.49    5.789E+004    5.79E+004    8.308E+004     2 .753E+004 768.36     4.89   3.091E+005               -2 . 2 97E+005   1.399E+005 806.18     1. 2 6 1.006E+006                 1 .924E+005    4.449E+005 934.06     3.11   5.573E+005                 3 .063E+005    2 .534E+00 5 1120. 2 9  14.92    1. 455E+005                1. 27 1E+005   6.699E+004 1155. 2 1    1. 63  9.657E+005               -5.905E+004      4. 2 96E+005 1 23 8.12    5.83   3.446E+005                 3.483E+005     1 .569E+005 1 28 0.98    1. 43  1.005E+006                 4.980E+005     4.387E+005 1377.67      3.99   4.736E+005                 4. 2 58E+004   2 .130E+00 5 1385.31      0.79   1.788E+006                 6.476E+005     7.737E+005 1401.52      1. 33  1.106E+006                 1.868E+005     4.808E+005 1 407.99     2.39   4.463E+005               - 5.499E+005     1.829E+005 1509. 2 1    2. 1 3 5.801E+005                 1. 21 8E+005   2.429E+005 1661. 2 7    1. 0 5 1 .127E+006              -4.504E+005      4.621E+005

[138]

1clide MDA Report 4/27/20~ 11 :34:35 AM Page 7 Nuclide Energy Yield Line MDA Nucl ide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Bi -2 14 1729.59 2.88 5.966E+005 5.79E+004 2 . 2 78E+005 2 .604E+005 1764.49 1 5.30 1.732E+00 5 2 .185E+005 7.938E+004 1847.43 2 . 0 3 5 .812E+005 2 .473E+005 2.348E+005

  >                2118.51        1. 1 6 0.000E+OOO                  O.OOOE+OOO     O.OOOE+OOO Pb-2 1 4       2 41. 99     7.25 2 .596E+005     6.05E+004     8.691E+004     1. 2 43E+005 295. 22    18.42 9.441E+004                     9.020E+004     4.479E+004 351. 93   35.60 6.050E+004                      8.422E+004     2 .888E+004 785.96      1. 06 1.285E+006                  -1.911E+005      5.745E+005 Pb214-XR         7 4 .82   5.80 4.465E+005       2 .48E+005    9.218E+005     2 .177E+005 77.11      9.70 2 .476E+005                   1.710E+005     1.205E+005 87.35     2 . 2 4 9.077E+005                  2 .135E+005    4.395E+005 89.78     0.82 2.430E+006                   -1.659E+006      1.176E+006 Ra-226         186.21      3.64 4 . 122E+005     4.12E+005     3.069E+005     1.963E+005 Ac-228         1 2 9.07    2.42 7.116E+005       6.72E+004     4.048E+004     3 .424E+00 5 2 09. 2 5   3.89 3.906E+00 5                    1.160E+005     1 . 857E+005 270. 2 4    3. 46 4.668E+005                    4.463E+005     2 .211E+005 328.00      2.95 5.060E+005                     2.011E+005     2 .371E+005 338.32    1 1. 27 1.387E+005                  -7.431E+003      6.511E+004 409.46      1. 92 7.595E+005                    3 .773E+005   3.524E+005 463.00      4.40 3.583E+005                     1 .506E+004   1.664E+005 794.95      4.25 3. 2 82E+005                   1 .835E+005   1. 4 70E +005 911.2 0   25.80 6.719E+004                      4 . 979E+004  3.059E+004 964.77      4.99 3.796E+005                     2.067E+005    1 .738E+005 968.97    15 . 80 1.100E+005                    3.433E+004    4.996E+004 1588.20       3. 22 4.308E+005                    O.OOOE+O OO   1.833E+005 Pa-231          2 7.36   10.30 9.399E+004        9.40E+004  -2.375E+004      4.388E+004 283.69       1. 70 8.705E+005                    6.506E+005    4.095E+005 300.07       2 .47 6.061E+005                 -6.731E+005      2 .848E+005 302.65       2 . 2 0 6.756E+005                 1 .159E+005    3 . 1 73E+005 330.06       1. 40 1 .056E+006                -1.802E+00 5     4.945E+005 Th- 23 4         92.38      2 .1 3 9.341E+005    9.34E+005     3.192E+005     4.520E+005 92.80      2 .10 9.505E+005                   4.746E+005     4.600E+005 112.81       0. 2 1 8.141E+006                  2 .972E+006    3 .918E+006 U-235          143.76     1 0 .96 1.656E+005     2 .60E+004    2 .089E+004    7.976E+004 163.33       5.08 3.193E+005                    3.280E+004     1.529E+005 185.71     57.20 2 .601E+004                    8.106E+003     1. 2 39E+004 2 02 .11    1. 08     1.420E+006              - 4.872E+005     6.757E+005 2 05.31     5.01 2.994E+005                   - 8.933E+004     1.423E+005 Am-24 1          59.54    35.90 4. 2 71E+004     4. 2 7E+004   1 .845E+004    2 .046E+004
    + = Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @    Hal f- life too short to be able to perform the decay correction

[139]

*************************'       *************************         *****************
****          G A M MA       S P E C T R U M        A N A L Y S I S                  *****
************************************************************************
.lename: 5452

!port Generated On 4/18/2016 2 :10:58 PM tmple Title B306100AFRWC009GD tmple Description TB 560 tmple Identification tmple Type tmple Geometry !ak Locate Threshold 3 .00 !ak Locate Range (in channels ) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Size 1.000E+OOO SQM tmple Taken On

qui s ition Started 4/18/2016 2 :00:56 PM

.ve Time 600.0 seconds ial Time 600.5 seconds iad Time 0 . 08 % Energy Calibration Used Done On 1 /13/2015 Efficiency Calibration Used Done On 4/14/2016 Ef f icienc: ID 1 TBWALL 1)<<\~ ~o.\;do...\ t'd 'Dy 0~ I ~-5--lB' 06'/D [140]

iak Analysis Report 4/18/ 2 016 2: 10: 58 P' Page 2

- - - P E A K A N A L Y S I S R E P O R T *****

' ************************************************************************ Detector Name: 5452 Sample Title: B306l00AFRWC009GD Peak Analysis Performed on: 4/18 /2 016 2:10:57 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 442 - 450 446.08 111. 22 0.61 -3.76E+OOO 24.69 7.18E+001 2 951- 961 955.48 238.72 0. 2 8 l.96E+001 22.35 4.34E+001 3 5829- 5850 5840. 2 9 1460. 3 4 1. 46 1.16E+002 23.29 5.35E+OOO

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2.000 sigma

[141]

1terference Corrected Act_ ty Report 4/18/ 2 016 10 :58 PM Page 3

- - - - ~*********************************************************
    - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title: B306100AFRWC009GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQM ) Uncertainty K-40 1. 000 1460.82* 10.66 7.88496E+005 1 .72907E+005 Pb-212 0.894 115.18* 0.60 -1.49195E+005 9.80 92 1E+005 238.63* 43.60 l.33002E+004 1.5 32 15E+004 300.09 3.30

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold =        0. 3 0 Errors quoted at 2 .000 sigma

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1terference Corrected Act~ .ty Report 4/18 /2 01 6 1 0:58 PM Page 4 "***********************************************************************

- - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 7.884957E+005 1.729071E+005 Pb-212 0.894 1. 33 0024E+004 1.532148E+004

     ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .000 sigma
 **********    U N I D E N T I F I E D          P E A K S     **********

Peak Locate Performed on: 4/18/2016 2 :10:57 PM Peak Locate From Channel: 85 Peak Locate To rhann~l

8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertaint 1, Type Nuclide All peaks were identified. [143]

tclide MDA Report 4/ 1 8/20h 2 :10:58 PM Page 5

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    - N U C L I D E MD A R E P O R T *****
      - * ******************************************************

Detector Name: 545 2 Sample Geometry: Sample Title: B306100AFRWC009GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (t) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM )

+      K-40       1 460.8 2

10.66 1.186E+D05 1.19E+005 7.885E+005 5.007E+004 Cr-51 320.08 9.91 1.469E+005 l.47E+005 6.987E+004 6.879E+004 Mn-54 834.85 99.98 1.572E+004 1.57E+004 1.314E+004 7.117E+003 Co-58 810.76 99.45 1.559E+D04 l.56E+004 1.022E+004 7.059E+003 Co-60 1173.~3 99.85 1.559E+004 1. 2 0E+004 -4.317E+00 3 6.9 1 5E+00 3 1332.49 99.98 1. 2 01E+D04 2 .774E+003 5.071E+003 Nb-94 70 2 .65 99.81 1.32DE+004 1.32E+004 - 4.871E+00 3 5.914E+003 871. 09 99.89 l.375E+D04 -1.183E+004 6.119E+003 Sn-11 3 255.13 2.11 7. 27 2E+005 2 . 2 8E+004 3.911E+004 3.440E+005 391. 70 64.97 2 .284E+004 -1.469E+004 1.063E+004 Cs-13 4 475.36 1. 48 9.617E+005 1.66E+004 -4.059E+005 4.425E+005 563 . 25 8 . 34 1.653E+005 1.722E+004 7.526E+004 569.33 1 5.37 8.777E+D04 -3.382E+004 3 .985E+004 604.72 97.62 2 .054E+D04 l.245E+004 9.616E+003 795.86 85.46 1. 662E+004 - 8.785E+003 7.459E+00 3 801.95 8.69 1.669E+005 1.347E+005 7.503E+004 1038.61 0 .99 1 .9 1 3E+006 l.496E+006 8.730E+00 5 1167.97 1. 79 7.904E+D05 -8.761E+004 3 .463E+005 1 365.19 3.0 2 4. 2 02E+005 8.793E+004 1.787E+005 Cs-137 661.66 85.10 1.821E+004 l.82E+004 l .315E+004 8.319E+003 Eu-1 52 121.78 2 8.67 5.845E+004 5.49E+004 -2 .476E+004 2 .810E+004 2 44.70 7.61 2 .001E+005 8. 1 9 0E+004 9 . 473E+004 2 95.94 0.45 3 .606E+006 1.335E+006 1.703E+006 3 44. 2 8 26.60 5.493E+004 3.737E +00 3 2.566E+004 3 67.79 0.86 1.602E+006 l.386E+006 7.4 3 1E+005 41 1.1 2 2.24 6.198E+005 1 .915E+005 2 .8 6 4E+005 443.96 2.83 4.800E+005 2 .610E+005 2 . 2 07E+005 488.68 0.42 3.173E+006 9.498E+005 1.450E+006 563.99 0.49 2 .809E+D06 - 6.378E+005 1. 2 79E+006 586.26 0.46 4.037E+00 6 4.132E+006 1.882E+006 678.62 0.47 2 .891E+00 6 l.855E+006 1. 3 03E+006 688.67 0.86 1. 54 7E+006 -4.694E+005 6.943E+005 719.35 0.28 5.486E+006 -1.866E+006 2 .494E+006 778.90 1 2 .96 1.085E+005 1.437E+004 4.870E+004 810.45 0.32 4.900E+D06 4.360E+006 2 . 222E+006 867. 3 7 4.26 3 . 3 46E+005 9.637E+004 1 . 496E+005 919. 33 0.43 3 .093E+006 -3.538E+006 1.365E+006 964.08 14.65 1. 322E+D05 l.197E+005 6.064E+004 1085.87 10. 2 4 1. 2 99E+005 -5.789E+004 5.671E+004 1089.74 1. 73 8.306E+005 -4.350E+005 3.664E+005 111 2. 07 1 3 .69 1.154E+005 -4. 3 65E+004 5. 1 44E+004 1212.95 1. 43 1.1 77 E+00 6 7.968E+005 5. 26 1E+00 5

[144]

1clide MDA Report 4/18 /2 01 l 2 :10:58 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM) Eu-1 52 1249.94 0.19 7.534E+00 6 5 .49E+004 2 .375E+005 3 . 2 89E+006 1299.14 1. 63 6. 2 90E+005 7.0 3 1E+004 2 .578E+005 1408.01 2 1. 07 7.580E+004 6.079E+004 3.333E+004 1457.64 0.50 8.077E+006 1.891E+007 3.843E+006 1528.10 0. 2 8 5.161E+006 -3.312E+005 2.222E+006 Eu-1 5 4 123.07 40.40 4.172E+004 4.17E+004 2.211E+004 2.007E+004 247.93 6.89 2 .134E+005 -1.123E+005 1.008E+005 591.76 4.95 3 .102E+005 1.004E+005 1.423E+005 69 2 .42 1. 78 7.996E+005 5.125E+005 3.614E+005 723.30 2 0.06 7.750E+004 - 7.799E+004 3.528E+004 756.80 4.5 2 2 .850E+005 -9.373E+004 1.268E+005 873.18 12 .08 1.139E+005 -7.638E+004 5 .065E+004 996.29 10.48 1.343E+005 1.143E+005 5 .943E+004 1004.76 18.01 7.848E+004 -4.055E+004 3 .473E+004 1274.4 3 3 4.80 4.350E+004 -2 .035E+004 1.913E+004 1596.48 1. 80 6.021E+005 -1.050E+005 2 .433E+005 Eu- 1 55 45.30 1. 31 9.965E+005 6.55E+004 7.444E+005 4.740E+005 60.01 1. 22 1 .182E+006 - 8.113E+005 5.650E+005 86.55 30.70 6.548E+004 5.333E+004 3.170E+004 105.31 21.10 8. 2 04E+004 2 .632E+004 3.951E+004 Tl- 2 0 8 583.19 85.00 2 .147E+004 2 .15E+004 9.081E+00 3 9.998E+003 Bi-211 35 1. 07 13.0 2 l .487E+005 1.49E+005 2. 053 E+005 7.061E+004 Pb- 2 11 404.85 3.78 3.538E+005 3.54E+00 5 2.659E+004 1. 63 0E+005 427.09 1. 76 8.601E+005 -2 .069E+005 3 . 99 6E+005 832.01 3.5 2 4.890E+005 4.151E+005 2 .234E+005 Bi -2 12 39.. 86 1. 06 1. 2 22E+006 2.34E+005 5.113E+005 5.812E+005 727.33 6.67 2 .337E+005 9.662E+003 1.064E+005 785.37 1.10 1.346E+006 - 2.908E+005 6.072E+005 1 620.50 1. 4 7 6.905E+005 2.633E+005 2 .740E+005

+     Pb-2 1 2     115.18*     0.60   1.740E+006     2 .47E+004  -l.492E+005    8.163E+005 238.63*   43.60    2 .475E+004                  l.330E+00 4  l.146E+004 300. 0 9    3.30   4.688E+005                 - 2 .230E+005  2 . 2 08E+005 Pb212 - XR    74.8 2   10.28    2 .170E+005    1. 2 0E+005   3 .653E+005  1 .0 5 4E+005

77. 1 1 17.10 1.202E+005 5.460E+004 5.8 2 5E+004 87.35 3.97 4.962E+005 - 5.870E+004 2.401E+00 5 89.78 1. 46 1 . 2 88E+006 - 4.496E+005 6. 22 4E+00 5 Bi -2 1 4 609.32 45.49 4.592E+004 4.59E+004 5.0 2 8E+004 2 .155E+004 768.36 4.89 3.308E+005 2 .674E+005 1.508E+005 806.18 1. 26 1.169E+006 -2 .558E+004 5. 2 64E+005 934.06 3.11 4.673E+005 2 .991E+005 2 .084E+005 11 2 0. 2 9 14.92 1.410E+005 1.239E+005 6.477E+004 11 55. 2 1 1. 63 9. 2 57E+005 - 2 .165E+005 4.096E+005 1238.1 2 5.83 3.114E+005 l.883E+005 1.403E+005 1280 . 98 1. 43 1.309E+006 l.120E+006 5.906E+005 1 377.67 3.99 3.544E+005 -2 .416E+005 1. 5 3 4E+005 1385.31 0.79 1.673E+006 1 .067E+006 7.163E+005 1401. 52 1. 33 9.678E+005 -8.064E+005 4.117E+005 1407.99 2.39 6.671E+005 5.350E+005 2 .934E+005 1509. 2 1 2 .13 5.801E+005 -1.828E+005 2 . 42 9E+005 1 661. 2 7 1. 05 1 .127E+006 -l.078E+006 4. 62 1E+005

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tclide MDA Report 4/ 1 8/ 2 0 1 E 2: 1 0:58 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( \, ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) Bi-214 1729.59 2 .88 5.630E+005 4.59E+004 1.579E+005 2 .436E+00 5 1764.49 1 5.3 0 1.611E+005 1.503E+005 7.334E+004 1847.43 2 .03 4.950E+005 -2 .550E+005 1.917E+005

  >              2118.51        1.16   O.OOOE+OOO                      O.OOOE+OOO    O.OOOE+OOO Pb-214      241.99       7.25   2.349E+005     5. 2 9E+004      2 . 2 19E+004 1.119E+005 295.22     18.42    8.590E+004                    -2 .574E+004    4.053E+004 351. 93    35.60    5. 2 93E+004                    2 .1 72 E+004 2.510E+004 785.96       1. 06  1.355E+006                    -4.158E+005     6.093E+005 Pb214-XR      74.82      5.80   3 .847E+005    2 .12E+005       6.474E+005    1.869E+005 77.11      9.70   2. 119E+005                     9.625E+004    1.027E+005 87.35      2.24   8.794E+005                    -1.040E+005     4.255E+005 89.78      0.82   2.294E+006                    -8.005E+005     1.108E+006 Ra-226      1 86.2 1     3.64   4.492E+005     4.49E+005        1.731E+005    2 . 1 48E+005 Ac-228      129.07       2.42   6.815E+005     8.41E+004      - 2 .393E+005   3.274E+ 0 05 209. 2 5     3.89   4.023E+005                    - 2 .646E+004   1 .915E+005 270. 2 4     3.46   4.439E+005                      5.749E+004    2 .096E+005 328.00       2. 95  4.997E+005                    -5. 2 96E+004   2 .339E+005 338. 32    11. 27   1.311E+005                    -3.761E+004     6.133E+004 409.46       1. 92  7.273E+005                      4.653E+004    3.363E+005 463.00       4.40   3.345E+005                      2.459E+005    1.545E+005 794.95       4. 2 5 3.508E+005                      5.556E+003    1.583E+005 911.20     2 5 . 80 8.409E+004                      9.946E+004    3.904E+004 964.77       4.99   3.796E+005                      2.499E+005    1.738E+005 968.97     15.80    1.115E+005                      5.361E+003    5.071E+004 1588.20        3.22   3.567E+005                      1.103E+004    1.462E+005 Pa-2 31       27.36    10.30    8.771E+004     8.77E+004        7.830E+004    4.077E+004 283.69       1. 70  8.414E+005                    -3 .924E+005    3 .950E+005 300.07       2.47   6. 2 63E+005                  -2 .980E+0 0 5  2 .950E+005 302.65       2.20   6.637E+005                      3.640E+005    3 .114E+005 330.06       1. 40  1.049E+006                    -1.679E+005     4.911E+005 Th-234        92.38      2 .13  8.476E+005     8. 4 8E+005      5.562E+005    4.089E+005 92.8 0     2 .10  8.533E+005                      7 . 914E+004  4.115E+005 112.81       0 . 21 8.015E+006                      2 .187E+005   3 .855E+006 U-235       143.76     10 .96   1.451E+005     2 .85E+004     -4.014E+004     6.951E+004 163.33       5.08   3. 1 05E+005                    l.889E+005    1 .485E+00 5 1 85.71    57.2 0   2 .846E+004                     l.058E+00 4   1.361E+004 2 02.11      1. 08  1. 509E+006                   - 2 .684E+005   7. 2 03E+005 2 0 5.31     5.0 1  3 . 2 15E+005                 -1. 3 33E+005   1.533E+005 Am-241        59.54    35.90    4.029E+004     4.03E+004      -8.673E+003     1.9 2 6E+004
     + = Nuclide identified during the nuclide identification

Energy line found in the spectrum

     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ =  Half-life    too short to be able to perform the decay correction

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' *******~****************    '*************************        *****************
' ***        GAMM A       S P E C T R U M         A N A L Y S I S                     *****

' ************************ * ********************************************** .lename: 54 52 iport Generated On 4/18 /2 01 6 1:24:07 PM tmple Title B306100AFRWC010GD tmple Description TB 560 tmple Identification 1mple Type tmple Geometry iak Locate Threshold 3. 00 iak Locate Range (in channels) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mple Size 1.000E+OOO SQM tmple Taken On

quisition Started 4/18/2016 1:14:06 PM

.ve Time 600.0 seconds ial Time 600.6 seconds !ad Time 0.11 % Energy Calibration Used Done On 1 / 13 / 2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBWALL

1) o.\.tA. ~o_\i. c\a. \eJ by Ci)~

                                                                    /)-5-)i cJ/i,50

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iak Analysis Report 4/ 1 8 / 201 6 1:2 4 :07 P1- Page 2

"************************************************************************

- - - P E A K A N A L Y S I S R E P O R T *****
      - * **********

Detector Name: 5452 Sample Title: B306100AFRWC0l0GD Peak Analysis Performed on: 4/18/2016 1: 2 4:0 7 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start en d centroid (keV) (keV ) Area Uncert. Counts 1 285 - 3 07 301.39 75.00 0.65 1.70E+002 73.72 3 .06E+002 2 948 - 960 955.85 238.82 0.68 5.32E+001 2 6.15 4.48E+001 3 1127- 11 3 6 113 1 .30 282.73 0.77 8.03E+OOO 15.01 2 .lOE+OOl 4 1176- 1187 118 1. 17 295.21 0.69 2 .74E+001 17.54 1.96E+001 5 2430- 2 44 2 2 434.81 608.88 0. 32 4. 1 4E+001 17.57 1. 3 6E+001 6 5829- 5851 5839.80 1460. 22 1.18 1 .86E+002 31. 66 1.68E+001 First peak in a multiplet region

= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 . 000 sigma

[148]

1terference Corrected Act:,. ~ ty Report 4/ 1 8/ 2 01 6 .... 24: 08 PM Page 3 ' *********************************************************************** ' *** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** '*********************************************************************** Sample Titl e : B306100AFRWC0l0GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQM ) Uncertainty K-40 0.999 1460.82* 10.66 1 .26935E+00 6 2.42341E+005 ...f ,., l'-

Hg 203 Pb-2 1 2 0.900 0.975 279.20* 115.18

01. 56 0.60 3.17303E+003 5.95007E1003 f ""'",,

2 38. 63

43.60 3.61328E+004 1.86845E+004 3 00.09* 3.30 2.73152E+005 1.80456E+005

       * = Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :        10.000 keV Nuclide confidence index threshold=                0.3 0 Errors quoted at 2 .000 s igma

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1t~rfer~nce Corrected Act~ Lty Report 4/18/ 2 016 .1.. . 24: 08 PM Page 4 "***********************************************************************

- - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

****************** *****************************************************

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 0.999 1.269355E+006 2.423413E+005 II~ 203 QI ggg 3.1730341!:+003 5. 950870E:4tltl~' ,,1,/a Pb-212 0.975 3.864686E+004 1.858511E+004

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at          2 .000 sigma
 **********        U N I D E N T I F I E D            P E A K S       **********

Peak Locate Performed on: 4/18/2016 1: 2 4:07 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. g_ No . (keV) Counts per Second a Uncertainty Type Nucl ide 1 75. 00 2 .8324E-00 1 @ Tol. Pb214- XR Ba-133 Pb2 1 2-XR Pb21 2 -XR Pb214-XR 5 6 0 8.88 6.9053E- 00 2 Tol. Zr-97 Sb-125 Sb-125

M = First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [150]

1clide MDA Report 4/18/2 0 h , 1:24:08 PM Page 5

- - - N U C L I D E MD A R E P O R T *****

Detector Name: 545 2 Sample Geometry: Sample Title: B306100AFRWC010GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM )

+      K-40       1460.82*     10.66 1.984E+005       1.98E+005 1.269E+00 6         8.997E+004 Cr-51        32 0 .08      9.91 1 .552E+005    1.55E+005 1. 2 05E+004        7. 2 90E+004 Mn-54        834.85      99.98   1.661E+004    1.66E+004 9 . 53 7E+003       7.562E+003 Co-58        810.76      99.45 1. 3 09E+004    1. 31E+004 -1.163E+004        5.8 1 0E+003 Co-60      1173.23      99.85 1.744E+004       1. 4 7E+004 3 .652E+003       7.841E+00 3 1 332 . 4 9  99.98 1.469E+004                    -4.383E+003      6.414E+00 3 Nb-94        702.65     99.81 1.652E+004       1.46E+004 -2 .034E+003        7.573E+00 3 871. 09    99.89 1.456E+004                      7.430E+003     6.523E+00 3 Sn-113       255.13       2 .11 7.404E+00 5    2 .39E+004 2 .169E+005        3.506E+005 391. 70    64.97 2 .386E+004                     1.350E+004     1.114E+004 Cs-134       475.36       1. 48 1.055E+006     1.57E+004 - 1.922E+005        4.892E+005 563.25       8.34 1.797E+005                   -5. 2 08£+004    8. 2 44E+004 569.33     15.37 1.001E+005                    -1.120E+004      4.601E+004 604.72     97.62 2.106E+004                    -1.976E+004      9.876E+003 795.86     85.46 1.573E+004                    -7.703E+003     7.015E+003 8 01. 95     8.69 1.641E+005                     5.467E+004    7. 3 63E+004 1 0 38.61      0 .99 l.573E+006                  - 5.771E+005    7. 0 31E+005 1167.97        1. 79 8.300E+005                  -4.4 28 E+005   3.661E+005 1365.19        3.0 2 4. 3 61E+005               -1. 4 62 E+005   1. 8 67E+005 Cs-137        661 . 66   85.10 1 .754E+004      1.75E+004 1.0 52 E+003       7.984E+003 Eu-15 2       12 1. 7 8  28 .67  6.610E+004     5.71E+004 1.981E+004         3 .193E+004 2 44.7 0     7.61 2.342E+005                     1.763E+004    1.118E+00 5 2 95.94      0.45 3.588E+006                     1.420E+006    1.695E+00 6 344. 2 8    2 6.60 5.7 1 5E+004                -5 .498E+004     2 .676E+004 367.79        0 .86 1.667E+006                    4. 2 67E+005  7.756E+005 4 11 .12     2.24  6.024E+005                 -1.57 1 E+005    2.776E+005 443.96       2.83 5. 32 1E+005                   2 . 2 88E+005 2.467E+005 488.68       0.42 2 .976E+006                 -2 .824E+006     1.351E+006 563.99        0.49 3 . 0 53E+006               -2 .861E+006     1.401E+006 586. 2 6      0.46 4. 3 48E+006                   5.470E+006    2 .037E+006 678.62        0.47 3.439E+006                     1 . 3 08E+006 1.576E+006 688.67       0.86 1.815E+006                   -8.199E+005      8. 2 83E+005 7 1 9. 3 5   0.28 5. 33 7E+006                 -5.362E+006      2 .420E+006 778.9 0    1 2 .96 1. 475E+005                    9.803E+004    6.821E+004 810.45       0.32 4.056E+006                   - 3.332E+006     1.800E+006 867.37       4. 2 6 3.468E+005                 -5.678E+004      1. 55 7E+005 919.33       0.43 3.020E+006                   -8.784E+004      1. 32 8E+006 964.08     14.65 1.392E+005                      3.1 5 8E+004   6.415E+004 1085.87      10. 2 4 1. 4 64E+005                  1. 93 0E+004   6.497E+004 1089.74        1. 73 7.909E+005                  -1.716E+005      3.466E+005 1112.07      13.69 1. 239E+005                   -1.111E+005      5.574E+004 1 212.95       1. 43 1.359E+006                    5.470E+005     6.169E+005

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4/18/ 2 0ll 1: 2 4:08 PM Page 6 1cli,de J.v!DA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Eu-1 52 1249.94 0.19 9.013E+006 5.71E+00 4 l. 465E+006 4.0 2 8E+006 1 2 99.14 1. 63 9.629E+005 - 3 .792E+005 4. 2 48E+005 1 4 0 8.01 2 1. 07 7.392E+004 1.083E+004 3 . 2 39E+004 1 457.64 0.50 1.033E+007 3 .161E+007 4.969E+006 1528.10 0. 2 8 4.987E+006 4.415E+004 2.135E+006 Eu-1 5 4 1 23 .07 40.40 4.656E+004 4.66E +004 1.848E+004 2.249E+004 2 47.93 6.89 2 .422E+005 1.911E+004 l.152E+005 591.76 4.95 2 .854E+005 -1.961E+005 l. 2 99E+005 692.42 1. 78 9.115E+005 -8. 1 94E+005 4.174E+005 723.30 20. 0 6 8. 1 43E+004 2 .848E+004 3 .725E+004 756.80 4.5 2 3.419E+005 6.248E+004 l.552E+005 873.18 1 2 .08 1. 2 48E+ 0 05 1.706E+004 5.611E+004 996.29 10.48 1.658E+005 4.999E+004 7.5 1 8E+004 1004.76 18.01 1.060E+005 -1.855E+004 4.849E+004 1274.4 3 34.80 4.753E+004 1 .828E+0 0 3 2 .114E+004 1596.48 1. 80 7.115E+005 -2 .241E+005 2 .980E+005 Eu-155 45.30 1. 3 1 8.359E+005 7.58E+004 2 .511E+005 3.937E+005 60.01 1. 22 1. 3 38E+006 -5.472E+005 6.431E+005 86.55 30.70 7.584E+004 5.334E+004 3.688E+004 10 5.31 2 1.10 9.506E+004 3.489E+004 4.601E+004 Tl-208 583.19 85.00 2 . 4 0 5 E-1. 0 0 4 '"> A"P * "f\A L... .'":tUD i~ VU":t 1. 9 58E+004 1.129E+004 Bi-211 351.07 1 3.02 l .538E+005 1 .54E+005 2.572E+005 7.319E+004 Pb-2 11 404 .85 3.78 3.772E+005 3.77E+005 - 2.847E+005 1.748E+005 4 27. 0 9 1. 76 7.955E+005 3.4 5 1E+002 3.673E+005 8 32 . 0 1 3.52 4.392E+005 - 4.513E+005 1.985E+005 Bi -2 1 2 39.86 1. 0 6 9.825E+005 2.37E+005 -6 .554E+005 4.6 1 3E+005 727.33 6 . 67 2 .367E+005 1.542E+005 1.079E+005 785.37 1. 10 1 .427E+006 5.930E+005 6.477E+005 1 620.50 1. 4 7 6.905E+005 2 .633E+005 2 .740E+005

+       Pb- 2 12       115.18       0.60   3.197E+006            2 . 61E+004             6.315E+00 4   1.545E+006 2 38.63*   43.60    2.606E+004                                    3.613E+004    1. 2 11E+004 300. 09 ~-   3.30   2.579E+00 5                                   2 .73~E+005   1.155E+005 Pb212-XR          74.82    10. 2 8  2.478E+00 5           1 .40E+005              2 .802E+00 4  1. 2 08E+005

77. 11 17.10 1.398E+005 -1.699E+004 6.8 0 4E+004 87.35 3.97 5.844E+005 4.659E+005 2 .842E+005 89.78 1.4 6 1.498E+006 -1.611E+005 7. 2 75E+005 Bi- 2 1 4 609. 32 45.49 4.646E+004 4. 65 E+004 5.786E+004 2 . 1 82E+004 768.36 4.89 3.627E+005 - 3.333E+004 1.667E+005 806.18 1. 2 6 1.091E+006 2 .138E+004 4.874E+005 934.06 3.1 1 5.0 2 1E+005 -7.887E+004 2 . 25 8E+00 5 1120. 2 9 14.92 1. 3 00E+005 4.458E+004 5 . 92 6E+004 1155. 2 1 1. 63 1.022E+006 -5 . 2 16E+005 4.579E+005 1 23 8.12 5.83 2 .960E+005 2 .045E+005 1 . 32 6E+005 1280.98 1. 43 1.133E+006 -3 .064E+005 5 .026E+005 1377.67 3.99 3.857E+005 - 2 .788E+005 l.690E+005 1385.31 0.79 2 .3 08E+006 -2 .222E+005 1.034E+006 1401.52 1. 33 1.198E+006 6.603E+005 5.266E+005 1407.99 2.39 6.5 0 6E+005 9.529E+004 2 .851E+005 1509. 2 1 2.13 7.421E+005 3.699E+005 3 . 23 9E+005 1661. 2 7 1. 05 9.842E+005 3.754E+005 3.905E+005

[152]

tclide MDA Report 4/18 /2 0 lt, 1:24:08 PM Page 7 Nucl ide Energ~' Yield Line MDA Nuc l ide MDA Activity Dec. Level Name (keV ) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi-2 14 1729.59 2 .88 4.664E+005 4.65E+004 - 9. 32 9E+00 3 1 .953E+005 1764.49 15.30 1. 2 80E+005 7.784E+004 5.681E+004 1 847.43 2.03 4.436E+005 l .23 6E+005 1.660E+00 5

  >              2 11 8.51      1.16   O.OOOE+OOO                    O.OOOE+OOO    O.OOOE+OOO Pb- 2 1 4    2 41. 99    7. 2 5  2 .718E+005   5 .61E+004 -2 .602E+005       1.304E+005 295.22    1 8.42    8.504E+004                   3 . 3 48E+004  4.010E+004 351. 93   3 5.6 0   5.613E+004                    6 .927E+004   2 .670E+004 785.96      1. 06   1.463E+006                   1.103E+005     6 .633E+00 5 Pb214-XR       74 . 82   5.80    4. 3 92E+005  2 .46E+005 4.967E+004         2 .141E+00 5 77.11     9.70    2 .465E+005                 -2 .995E+004    1. 2 00E+005 87.35     2 . 24 1 .036E+006                   8. 2 57E+005   5.037E+005 89.78     0.8 2  2 .668E+006                  -2 .868E+005    1. 2 95E+006 Ra-226       186.21      3.64    4.916E+00 5   4.92E+005 3.301E+005          2 . 3 60E+005 Ac-228       129.07      2 .42  7.419E+005     7. 2 2E+004 -1.685E+004      3. 576E+005 209. 2 5    3.89   4.459E+005                    2 .979E+00 5   2 .133E+005 270. 2 4    3.46   4.565E+005                    l.503E+005     2 .159E+005 328.00      2 .95  5. 2 16E+005                  1.452E+005    2 .449E+005 338.32    11.27    1.458E+005                    3 .077E+004    6.867E+004 4 0 9.46    1. 92  7.140E+005                  - 1.8 2 9E+005  3 . 2 96E+005 4 63.00     4.40   3.583E+005                    2 .159E+005   1 . 664E+005 794.95      4. 2 5 3.222E+005                    8.069E+004    1.440E+005 911. 20   25.80    7.223E+004                    6.402E+004    3.311E+004 964.77      4.99   4.007E+005                  -1.122E+004     l.844E+005 968.97    15.80    1 .306E+005                   6.704E+004    6.0 2 6E+004 1 588.2 0      3. 22  3.958E+005                    2 .138E+005   1.658E+005 Pa-23 1       27.36    10.30    6.897E+004     6.90E+004 5.042E+004         3.140E+004 283.69       1. 70  8.846E+005                    3.178E+005    4.166E+005 300.07       2 .47  6.459E+005                    4.380E+004    3.047E+005 302.65       2 . 20 7.355E+005                    3.406E+005    3.472E+005 330.06       1. 40  1.015E+006                  -5.645E+005     4.737E+005 Th- 23 4      92.38      2 .13  9.807E+005    9.81E+005 -4.141E+005         4.754E+005 92.8 0    2 .10   9.849E+005                  -2 .790E+005    4.773E+005 112.81       0. 2 1 9. 2 39E+006                  5. 2 48E+006  4.467E+006 U-235       1 43.76    10.9 6   1.573E+005    3.09E+004 -5.522E+004         7.562E+004 1 63.33     5.08    3.436E+005                  -6.713E+004     1.651E+005 185.7 1    57.20    3.086E+004                    4.621E+003    1.481E+004 2 02 . 11   1. 08   1.552E+006                    4.789E+005    7.416E+005 2 05.3 1    5.01    3 .401E+005                 -l.390E+005     1. 62 6E+005 Am- 2 41       59.54    35.90    4. 3 97E+004  4.40E+004 -5.351E+004         2 . 1 10E+004
    +    Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    >    Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Half-life too short to be able to perform the decay correction

[153]

"************************* ~************************* * *****************

- - - G A MMA S P E C T R U M A N A L Y S I S *****

"************ *********************************************************** .lename: 54 5 2 iport Generated On 4/19/2016 8:27:53 AM 1mple Title B306100AFRFC011GD tmple Description TB 580 1mpl e Identification tmple Type tmple Geometry !ak Locate Threshold 3 .00 !ak Locate Range (in channels ) 85 - 8 1 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10.000 keV 1mple Size 1.000E+OOO SQMl ,,, , tmple Taken On

quisition Started 4/19/2016 8:17:50 AM

.ve Time 600.0 seconds !al Time 601.3 seconds iad Time 0. 2 1 9_; Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/20 1 6 Efficiency ID TBFLOOR

                                                                \)o.+~ ~o.\\q~~ec\ 'by
                                                                 ~4
                                                                  /p-6,-/~

01/~ [154]

ia k Analysi s Report 4/19/2016 8 : 2 7 : 5 3 AJ.v1 Page 2

************************************************ * ************************
"***               P E A K       A N A L Y S I S          R E P O R T                       *****
"************************************************************************

Detector Name: 5452 Sample Title: B306100AFRFC011GD Peak Analysis Performed on: 4/19/2016 8:27:52 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 12 2 115.79 28.54 0.69 5.22E+001 2 0.93 2.18E+001 2 296- 306 301. 23 74.96 0.97 6.96E+001 40.08 1.38E+002 3 455- 462 458.83 114.41 0. 2 5 -1.46E+OOO 21. 39 5.75E+0 01 4 949- 959 954.66 238.52 0.88 3 .02E+001 2 1 .74 3 .68E+001 5 1 402- 1413 1407.44 351. 8 3 1. 25 3 .36E+001 18.13 1 .94E+001 6 2430- 2440 2435.90 609. 1 5 1. 24 3 .79E+001 15.13 8. 1 3E+OOO 7 5829- 5850 5839.7 2 1460. 2 0 1. 84 l.40E+002 2 4.47 2 .57E+OOO First peak in a multiplet region

= Other peak in a multiplet region
, _

Fitted sing l et

rors quoted at 2 .000 sigma

[155]

1terference Corrected Act_ ity Report 4/19/2016 0; 2 7:53 AM Page 3

'*** N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title: B306100AFRFC011GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB

 . . . ... . . . .. . . . . . . . . . IDENTIFIED NUCLIDES            . . ............... .. .

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQMl) Uncertainty K-40 0.999 1460.8 2

10.66 9.57354E+005 l.86380E+005 Pb-21 2 0.895 115.18* 0.60 - 5.83073E+004 8.51950E+005 2 38.63* 43.60 2 .05117E+004 l.51118E+004 300.09 3.30 Pb-214 0. 4 92 2 41.99* 7.25 1 . 2333 6E+005 9.08241E+004 2 95. 22 18.42 351.93* 35.60 3.39524E+004 1.91003E+004 785.96 1. 06 Th-231 0.877 25.64* 14.10 8.79164E+004 4.094 2 1E+004 84.21* 6.60 2 .50334E+005 1 .55563E+005 89.95 1. 00

        * = Energy line found in the spectrum.
        @=Energy line not used for Weighted Mean Activity Energy Tolerance :                   10.000 keV Nuclide confidence index threshold =                       0.30 Errors quoted at 2 .000 s igma

[156]

1terference Corrected Act~ _ty Report 4/ 1 9/2 01 6 c... 27: 53 AM Page 4

- - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQMl ) Uncertainty K-40 0.999 9.573543E+005 1.863797E+ 0 05 X Co-57 0.744 X Bi-211 0.999 Pb-21 2 0.895 1 .48651 4E+004 1 .543482E+004 Pb-214 0. 4 92 3.395236E+004 1.909983E+004 X Pa-231 0.376 Th-231 0.877 9.843777E+004 3.959380E+004

     ?     Nuclide is part of an undetermined solution X     Nuclide rejected by the interference analysis
     @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2 . 000 s igma
 **********     U N I D E N T I F I E D            p E A K     s  **********

Peak Locate Performed on: 4/19/2016 8: 27 :52 AM Peak. Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV) Counts per Second % Uncertainty Type Nuclide 6 609.15 6.3116E- 00 2 39.95 Tol. Zr-97 Sb-125 Sb-125 Cs-134 Bi-214 M = First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [157]

1clide MDA Report 4 / 1 9/ 2 01 1 8: 2 7:53 AM Page 5

- - - N U C L I D E M D A R E P O R T *****

"****************************************************************************** Detector Name: 545 2 Sample Geometry: Sample Title: B306l00AFRFC0 l 1GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQMl) (pCi/SQMl) (pCi/SQMl) (pCi/SQMl)

+      K-40       1 460.8 2

10.66 8.666E+004 8.67E+004 9.574E+005 3.411E+004 Cr-51 320.08 9.91 1.450E+005 1.45E+00 5 l.082E+005 6.784E+004 Mn-54 834.85 99.98 l.477E+004 1.48E+004 7.733E+00 2 6.642E+00 3 Co-58 810.76 99.45 l .337E+004 l.34E+004 -1 . 089E+004 5.947E+00 3 Co-60 1173.23 99.85 l.654E+004 l.43E+004 -9.2 44E+00 3 7.393E+00 3 1332. 4 9 99.98 1.429E+004 1.034E+004 6. 2 11E+003 Nb-94 70 2 .65 99.81 l.517E+004 1.38E+004 -7.996E+00 3 6.897E+003 871. 09 99.89 1.375E+004 8.035E+00 3 6.119E+00 3 Sn-113 255. 1 3 2 .11 6.793E+00 5 2 . 1 6E+004 4 .2 48E+005 3.200E+005 391.70 64.97 2 .159E+004 6 .037E+003 l.OOOE+004 Cs- 1 3 4 475.36 1. 48 9. 2 15E+005 1.75E+004 -2 . 72 8E+005 4.224E +005 563.25 8.3 4 l.874E+005 5.379E+0 0 3 8.628E+004 569.33 15.3 7 8.655E+004 4. 2 12E+004 3.924E+004 604.72 97. 62 2 .041E+004 - 1 .501E+00 3 9.550E+003 795.86 85. 4 6 1.746E+004 - 1.122E+003 7.877E+00 3 80 1 .95 8.69 1.523E+00 5 9.423E+004 6.773E+004 1038.61 0.99 1.385E+00 6 - 2 .365E+005 6.089E+005 1167.97 1. 79 1.018E+006 l .083E+006 4.601E+005 1365. 1 9 3 . 02 4. 3 61E+00 5 1. 2 89E+005 1.867E+005 Cs -137 661.66 85. 1 0 1.927E+004 1 .93E+004 1.1 2 7E+004 8.849E+003 Eu-1 5 2 121.78 28.67 5.463E+004 5.46E+004 - 1.843E+004 2 .619E+004 244.70 7 . 61 2 .146E+005 1 . 2 18E+005 1.020E+005 295.94 0.45 3.657E+006 2 . 3 93E+006 1.729E+006 344.28 26.60 5.715E+004 4.185E+00 4 2 .676E+004 367.79 0.86 1.654E+006 3.682E+005 7.692E+005 411.12 2.24 6. 1 41E+005 8.988E+004 2 .835E+005 443.96 2.83 4.997E+005 -1.502E+005 2 . 3 05E+005 488.68 0.42 2 .763E+006 -2 .421E+006 1. 2 45E+006 563.99 0.49 3 . 11 9E+006 9.635E+005 l.434E+006 586. 2 6 0.46 3.634E+006 1.3 3 4E+006 1.680E+006 678.62 0.47 2 .542E+006 - 3.4 2 6E+005 1.128E+006 688.67 0.86 1.599E+006 6.162E+005 7. 2 05E+005 719.35 0. 2 8 5.183E+006 2 . 2 65E+006 2 .343E+006 778.90 12.96 9.437E+004 -3 .344E+0 0 4 4.163E+004 810.45 0.32 4. 22 4E+006 -8.440E+004 1 .883E+006 867.37 4.26 3.283E+005 7.032E+004 1.464E+005 919.33 0.43 3.677E+006 7.401E+005 1.656E+006 964.08 14.65 1. 2 92E+005 1 . 007E+005 5.918E+004 1 085.87 10. 2 4 1.611E+005 - 3 .844E+004 7. 22 9E+004 1 089.74 1. 7 3 9.873E+005 -1. 3 16E+005 4.448E+00 5 1 112.07 13.69 1.154E+005 -4.430E+004 5.144E+004 1212.95 1. 43 1.282E+006 1.154E+005 5.783E+005

[158]

1clide MDA Report 4/19/ 2 0 1L 8: 2 7:53 AM Page 6 Nuclide Energy Yiel d Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQMl) (pCi/SQMl ) (pCi/SQMl ) (pCi/SQMl) Eu- 1 52 1249.94 0.19 8.125E+006 5.46E+004 -1.488E+006 3.584E+006 1299.14 1. 63 8.930E+005 -4.817E+005 3.898E+005 1408.01 2 1. 07 6.579E+004 2 .702E+004 2 .833E+004 1457.64 0.50 8.615E+006 2 .093E+007 4. 1 12E+00 6 1528.10 0. 2 8 2.460E+006 5. 2 98E+005 8.716E+005 Eu-154 123.07 40.40 3.952E+004 3 .95E+0 0 4 -1. 32 5E+002 1.896E+004 247.93 6.89 2.145E+005 -1.940E+005 l.013E+005 591. 76 4.95 2 .580E+005 7.080E+004 1.162E+005 692.4 2 1. 78 7.996E+005 -2 .737E+005 3 .614E+005 723.30 2 0.06 6.892E+004 -9.186E+003 3.099E+004 756.80 4. 52 3.225E+005 2 .832E+005 1.455E+005 873. 1 8 12.08 1.067E+005 5 .864E+003 4.707E+004 996. 2 9 10 .48 1 . 5 36E+005 4.760E+004 6.905E+004 100 4.76 18.01 7.848E+004 4.831E+004 3.473E+004 1 274.43 34.80 4. 2 42E+004 9. 632 E+003 1.859E+004 1596.48 1. 80 7.744E+005 2 . 2 71E+005 3.294E+005 Eu-155 45.30 1. 31 1.006E+006 6.63E+004 8.612E+005 4.787E+005 60.01 1. 22 1. 201E+006 8.428E+003 5.742E+005 86.55 3 0.70 6.633E+004 6.989E+004 3. 2 12E+004 105.31 2 1.10 8.137E+004 -3 .682E+00 3 3.916E+004 Tl-208 583.19 85.00 2.014E +004 2.01E+004 1 .517E+004 9.331E +003 Bi-211 351.07* 13.0 2 7.078E+004 7.08E+004 9.283E+004 3.165E+004 Pb-211 404.85 3.78 3.503E+005 3.50E+005 -1.818E+005 1.613E+005 42 7.09 1. 76 8.532E+005 2 .8 3 4E+005 3 .961E+005 832 .01 3.5 2 4. 1 89E+005 -2 .227E+005 1.883E+005 Bi -2 12 39.86 1. 06 1.138E+006 1.90E+005 - 5.566E+005 5.388E+005 727.33 6.67 1.896E+005 - 1 .774E+004 8.435E+004 785.37 1.10 1.346E+006 - 2 . 26 5E+005 6 .072E+005 1 620.50 1. 47 8.777E+005 4.740E+005 3.676E+005 + Pb-2 1 2 11 5.18* 0.60 1.518E+006 2.28E+004 -5 .831E+004 7.051E+005 23 8.63* 43.60 2 . 2 75E+004 2 .0 5 1E+004 1.046E+004 30 0 . 0 9 3.30 4.511E+005 -1.685E+005 2 .119E+005 Pb2 1 2-XR 74.8 2 10. 2 8 2 .162E+005 1. 2 3E+005 4.125E+005 1.050E+005

77. 11 17.10 1. 22 8E+005 - 1.374E+004 5.953E+004 87.35 3.97 5.161E+005 5.415E+005 2 .499E+005 89.78 1. 46 1.365E+006 - 1.877E+004 6.604E+005 Bi-2 14 609. 32 45.49 4.453E+004 4.45E+004 3.928E+004 2 . 085E+004 768.36 4.89 3 . 1 36E+005 2 . 2 42E+005 1.422E+005 806.18 1. 2 6 1 .070E+006 -5. 1 78E+005 4.771E+005 934.06 3.1 1 4.673E+005 -2 .802E+004 2 .084E+005 1 120. 2 9 14.92 1. 316E+005 -5. 3 07E+00 3 6.008E+004 11 55. 2 1 1. 63 8.618E+005 - 3.699E+005 3.776E+005 1238.12 5.83 3.213E+00 5 1.248E+005 1.452E+005 128 0 .98 1. 43 1.005E+006 4.412E+005 4.387E+005 1377.67 3.99 3. 316E+005 - 3 .083E+004 1 .420E+005 1385.31 0.79 1. 2 54E+006 -1. 3 85E+006 5 .065E+005 1401.52 1. 33 1.137E+006 1. 2 01E+005 4.965E+005 1407.99 2 .39 5.790E+005 2 . 37 8E+005 2 .493E+005 1509. 2 1 2 .13 6.782E+005 4. 52 5E+005 2 .920E+005 1661. 2 7 1. 05 9.0 1 7E+005 3.003E+005 3 .493E+005

[159]

1clide MDA Report 4/19/201L 8:27:53 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQMl ) (pCi/SQMl) (pCi/SQMl) (pCi/SQMl) Bi -2 14 1729.59 2 .88 4.875E+005 4.45E+004 7. 27 7E+004 2 .059E+00 5 1764.49 15.30 1. 2 25E+005 1.013E+005 5.404E+004 1847.43 2 . 03 6.188E+00 5 2 .885E+005 2 .536E+00 5 2 118.51 1. 16 O.OOOE+OOO O.OOOE+OOO O.OOOE+OOO

  >                                                                              6.289E+004

+ Pb-2 14 241.99* 7.25 1 . 3 68E+005 2 .59E+004 1. 2 33E+00 5 295. 22 18.4 2 8.759E+004 2.016E+004 4.138E+004 351.93* 35.60 2.589E+004 3.395E+004 1.158E+004 785.96 1. 06 1.442E+006 -4.171E+005 6.529E+005 Pb214-XR 74.82 5.80 3.832E+005 2 .17E+005 7.310E+005 l .860E+005 77.11 9.70 2.165E+005 -2 .422E+004 1.050E+005 87.35 2 .24 9.146E+005 9.597E+005 4.430E+005 89.78 0 .82 2.430E+006 -3.343E+004 1.176E+006 Ra-226 186.21 3.64 4.035E+005 4.04E+005 -9.467E+003 1.920E+005 Ac-22 8 129.07 2.42 6.750E+005 7.69E+004 2 .618E+005 3.241E+005 209. 2 5 3.89 3 .876E+005 2. 103E+005 1.842E+005 270.24 3. 4 6 4 .264E+005 2 .115E+005 2 .009E+005 328.00 2.95 5.154E+005 1.856E+005 2 .418E+005 338.32 11.27 1. 23 1E+005 -7 .416E+004 5 .731E+004 40 9.46 1. 92 7.072E+005 l .845E+005 3 . 2 62E+005 463. 00 4. 4 0 3.313E+005 2 .437E+005 1.530E+005 794.95 4.25 3.616E+005 5.452E+004 1.637E+005 911.20 25.80 7.691E+004 3.612E+004 3 .545E+004 964.77 4.99 3 .796E+005 4. 72 5E+005 1.738E+005 968.97 15.80 l.229E+005 3 .716E+004 5.637E+004 1588.20 3 . 22 4.471E+005 8. 26 4E+004 1.914E+005 Pa- 23 1 2 7.36

10.30 6.361E+004 6.36E+004 1. 2 04E+005 2 .869E+004 283.69 1. 70 8.657E+005 2 .095E+005 4.072E+005 300. 0 7 2 .47 6.026E+005 -2 . 2 51E+005 2 .831E+005 302.65 2 . 20 6.516E+005 -5 .683E+00 4 3 .053E+005 330. 0 6 1. 40 l.036E+006 2 .177E+005 4.842E+005 Th-234 92.38 2 .1 3 9.070E+005 9.0 7E+005 9.787E+005 4. 3 84E+005 92.80 2 .10 9.105E+005 9.450E+005 4.400E+005 112.8 1 0.21 7.999E+006 2 .930E+006 3.846E+006 U- 235 1 43.76 10.96 l. 383E+005 2.57E+004 2.660E+004 6.615E+004 1 63.33 5.08 3 .158E+005 - 4.898E+003 1 .512E+005 1 85.71 57. 2 0 2 .574E+004 -6.782E+003 l .225E+004 2 02.11 1. 08 l . 3 62E+006 - 5.843E+005 6.470E+005 205.31 5.0 1 3. 073E+005 8.551E+004 1.462E+005 Am- 2 41 59.54 35.90 4.094E+004 4.09E+004 4. 2 96E+003 1.957E+004

     +     Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @  = Half-life too short to be able to perform the deca~1 correction

[160]

- - - - ************************* ~****************
    - G A MMA S r E C T R U M A N A L Y S I S *****

.lename: 54 52 iport Generated On 4/ 1 4/ 2 016 2 :26:37 PM 1mple Title B306100AFRFC0l 2G D 1mple Description U-1 STS TB FLOOR 560 1mpl e Identification 1mpl e T~ pe 1 1mple Geometry iak Locate Threshold 3.00 iak Locate Range (in channels ) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 1. 000 FWHM 1mple Si ze 1. OOOE+OOO SQM 1mple Taken On

quisition Started 4/14/ 2 016 2 : 1 6: 35 PM

.ve Time 600.0 seconds ial Time 600.4 seconds iad Time 0 . 07 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBFLOOR D o.h,. \to.\1de1teJ loy

                                                                   ~4
                                                                    ,.,_,_,~

0110 [161]

!ak Analysis Report 4/14/2016 2 :26:37 P Page 2

- - - P E A K A N A L Y S I S R E P O R T *****

'************************************************************************ Detector Name: 545 2 Sample Title: B3061 0 0AFRFC012GD Peak Analysis Performed on: 4/14/2016 2:26:36 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid ( keV) (keV) Area Uncert. Counts 1 1400- 1414 1406.51 351.60 1. 26 5.46E+001 23.96 3.04E+001 2 5825- 5850 5839.53 1460. 1 5 1. 62 1.40E+00 2 3 0 .63 2 . 2 4E+001

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 . 000 sigma

[162]

1terference Corrected Act j_ :y Report 4/14/ 2 016 <. 6:37 PM Pag e 3

- - - - r***************
    - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Ti tle: B306l00AFRFC0l2GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zi o n Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yie ld Activity Activity Name Confidence (keV) ( t, ) (pCi/SQM) Uncertainty K-40 0. 976 1460.82* 1 0.66 9.51387E+005 2 . 2 4590E+005 Bi -2 11 0. 985 351.07* 13.02 l.50792E+005 7.04854E+004

       * = Energy line found in the spectrum.
       @ = Ene rg y line not used for Weighted Mean Activity Energy Tolerance :        1.000 FWHM Nuclide confidence index threshold =             0.3 0 Errors quoted at 2 .000 sigma

[163]

1terference Corrected Acti ty Report 4/14/2016 '. 6: 37 PM Page 4

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Nucl ide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0 .976 9.513867E+005 2.245902E+005 Bi-211 0 .985 1 .507923E+005 7.048536E+004

     ?  =  Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysi s
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2 .000 sigma
 **********     U N I D E N T I F I E D         P E A K S     **********

Peak Locate Performed on: 4/14/20 1 6 2:26:36 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Si z e in Peak CPS Peak Tol. No . (keV) Counts per Second ~ Uncertainty Type Nuclide Al l peaks were i dentified. [164]

1clide MDA Report 4/14/ 2 01 2 : 2 6:37 PM Page 5

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Detector Name: 5452 Sample Geometry: Sample Title: B306 1 00AFRFC0l2GD Nuclide Library Us ed: C:\GENIE2K\CAMFILES\Zi o n Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM) 1460.8 2

10.66 2 .371E+005 2 .37E+005 9.514E+005 1.093E+005

+      K-40

7. 2 90E+004 Cr-51 32 0.08 9.91 1.552E+005 1.55E+005 -8.048E+004 Mn-54 834.85 99.98 1.452E+004 1.45E+004 - 4.892E+003 6.518E+00 3 Co-58 810.76 99 . 45 1.489E+004 1.49E+004 -3 .951E+003 6.709E+00 3 Co-60 1 173. 23 99.85 1.8 2 9E+004 1.39E+004 1.525E+004 8. 2 65E+003 1332.49 99.98 1 .387E+004 -5.120E+003 6.000E+003 Nb-94 702.65 99.81 1.652E+004 1 .58E+0 0 4 5.695E+003 7.573E+00 3 87 1. 09 99.89 1.581E+004 -9 . 7 2 0E+003 7.145E+003 Sn-113 255.13 2 .11 7.532E+005 2 .45E+004 5. 2 63E+005 3.570E+005 391. 70 64. 97 2 .452E+004 1.302E+004 1.147E+004 Cs-134 475.36 1. 4 8 9.812E+005 1. 97E+004 2 .193E+005 4.522E+0 0 5 563.25 8.34 1 .816E+005 1.122E+004 8. 3 42E+004 569.33 15.37 1 .042E+005 7.518E+004 4.806E+004 604.7 2 97. 62 2 . 2 31E+004 9.440E+003 1.050E+004 795.86 85.46 1.974E+004 8.489E+003 9.017E+003 801. 95 8.69 1.8 2 7E+005 -8.690E+004 8. 2 95E+004 1 038.61 0.99 1.451E+006 1 .234E+006 6.419E+005 11 67.97 1. 79 1.063E+006 4.981E+005 4.8 2 5E+005 1365.19 3 . 02 4.035E+005 2.317E+005 1 .704E+005 Cs-137 661. 66 85.10 1. 947E+004 1. 95E+004 1.4 2 9E+004 8.951E+003 Eu-152 121.78 2 8.67 6.313E+004 6.03E+004 4.082E+00 4 3 .045E+004 244.7 0 7.61 2.171E+005 -1.999E+005 1.032E+005 295.94 0.45 4.012E+006 2 .632E+006 1.906E+006 344. 2 8 26.6 0 6.031E+004 -4.006E+00 4 2 .834E+004 367.79 0.86 1. 5 75E+006 5.095E+005 7 . 2 97E+005 411. 12 2.24 6.141E+005 - 7.522E+005 2 .835E+005 443.96 2.83 5.366E+005 3.825E+005 2 .490E+005 488.68 0.42 3.4 2 9E+006 2 .373E+006 1.578E+006 563.99 0.49 3.086E+006 -8.822E+005 1.417E+006 586.26 0.46 3 .666E+006 5.007E+004 1.696E+006 678.62 0.47 2 .891E+006 1.772E+006 1.303E+006 688.67 0.86 1.985E+006 1. 696E+006 9 . 135E+005 719.35 0.28 5.486E+006 -5.137E+004 2 .494E+006 778.90 12.96 1.225E+005 -4.468E+004 5.5 6 9E+004 810.45 0.32 4.830E+006 -1.694E+006 2 .1 8 7E+006 867. 3 7 4.26 3.586E+005 -4.844E+005 1.615E+005 919. 33 0.43 3.557E+006 -6.845E+005 1.596E+006 964.08 14.65 1.278E+005 5.832E+004 5.844E+004 1085.87 10.24 1.147E+005 -2.052E+005 4.911E+004 1089.74 1. 73 8.682E+005 3.114E+005 3.852E+005 1112.07 1 3 .69 1.430E+005 -2.076E+005 6.525E+004 121 2 .95 1. 43 1.132E+006 - 2.161E+005 5.037E+005

[165]

1clide MDA Report 4/14/ 2 01 2 : 2 6:37 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) Eu-1 52 1249.94 0.19 7.110E+006 6.03E+004 -2 .903E+005 3 .077E+006 1299.14 1. 63 7.885E+005 -4.590E+005 3 . 3 76E+005 1408.01 21. 07 7.392E+004 -l.187E+004 3 . 2 39E+004 1457.64 0.50 9. 2 74E+006 2 .382E+007 4.442E+006 1528. 10 0. 2 8 4.415E+006 3.385E+00 5 1.849E+006 Eu-154 123.07 40.40 4.443E+004 4.44E+004 -3.409E+00 3 2 .142E+004 247.93 6.89 2 . 3 12E+005 4.656E+004 1.097E+005 591. 76 4.95 3.033E+005 9.782E+004 1. 389E+005 692.42 1. 78 9.522E+005 6.079E+005 4.377E+005 723.30 2 0.06 9.043E+004 7.895E+004 4.175E+004 756.80 4.52 3.017E+005 - 2 . 99 9E+005 l .351E+005 873.18 12 .08 1.403E+005 -2 . 2 55E+004 6.389E+004 996. 2 9 10.48 1. 343E+005 5.498E+004 5.943E+004 1004.76 18.01 8.0 2 0E+004 2 .754E+004 3.558E+004 1 274.4 3 3 4.80 5.1 22 E+004 2 . 3 74E+004 2 . 2 99E+004 1 596. 4 8 1. 80 8.318E+005 5.550E+005 3 . 5 81E+005 Eu-155 45.30 1. 31 9.357E+00 5 7 . 3 9E +00 4 5.519E+005 4.436E+005 60.01 1. 22 1. 2 97E+00 6 -7.924E+004 6. 22 5E+005 86.55 30.70 7.392E+004 3.211E+004 3 .592E+004 10 5.31 21.10 9.129E+004 - 4.458E+003 4.413E+004 Tl- 2 08 583.19 85.00 1.979E+004 l.98E+004 5.038E+002 9. 1 57E+003

+     Bi-211       351.07*  13 . 02  9.315E+004      9.32E+004 1.508E+005           4. 2 84E+004 Pb- 211      40 4.85    3 .78  3.836E+005      3.84E+005 -1.075E+005          1 .7808+005 427. 0 9   1. 76  7.955E+005                       l.949E+005    3 .673E+005 832. 0 1   3.52   3 .898E+005                    - 6.148E+004    1.738E+005 Bi-212        39.86     1. 06  l.028E+006      2 .65E+0 0 5 -2.368E+005       4.838E+005 727.33     6.67   2 .648E+005                      1.817E+005    1. 22 0E+005 785.37     1.10   l.503E+006                       6.543E+005    6.858E+005 1 620.50     1. 4 7 7.428E+005                       5.047E+004    3.001E+005 Pb-21 2      115. 1 8   0.60   3 .014E+006     4 . 41E+004 - 1.313E+006       l.453E+006 238.63   43.60    4.407E+004                       4.999E+004    2 .112E+004 30 0 .09   3.30   4.953E+005                     - l .489E+005   2 .340E+005 Pb212-XR      74.82   10. 2 8  2 .414E+005     l .3 4E+00 5 4. 5 05E+005      l.176E+005

77. 11 1 7.10 l.340E+005 7.889E+004 6.5 1 3E+004 87.35 3.97 5.784E+005 4.680E+005 2 .8 1 2E+005 89.78 1. 46 1. 4 97E+006 -4.473E+005 7. 2 65E+005 Bi -2 14 609.32 45.49 5. 1 06E+004 5.1 1E+004 6.093E+004 2 .412E+004 768.36 4.89 3 . 1 3 6E+005 -l.891E+004 l.422E+005 806.18 1.26 l. 2 06E+006 7.805E+005 5 .449E+005 934.06 3.1 1 5.720E+005 3 .159E+005 2 .607E+005 1120. 2 9 14.92 l.645E+005 6 . 32 3E+004 7.651E+004 1155. 2 1 1. 63 l.143E+006 3 . 1 62E+005 5.181E+005 1238.12 5.83 3.164E+005 l.041E+005 1.428E+005 1 280.98 1. 43 1 .156E+006 -7. 2 16E+005 5. 144E+005 1377.67 3.99 3.544E+005 -l .007E+004 l.534E+005 1385.31 0.79 1.673E+006 -9 .778E+005 7.163E+00 5 1401.52 1. 33 l.168E+006 -2 .456E+005 5.118E+005 1407.99 2 .39 6.. 506E+005 -l.045E+005 2.851E+005 1509.2 1 2 .13 5.523E+005 2 .785E+005 2.291E+005 166 1. 27 1. 05 l. 2 51E+006 1. 689E+005 5.239E+005

[166]

1clide MDA Report 4/14/201 2 : 2 6:37 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( !;,) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Bi-2 1 4 1729.59 2 .88 4.44 1E+005 5.11E+004 2 . 23 9E+005 l.842E+005 1 764.49 15.30 1.732E+005 2 .185E+005 7.938E+004 1847.43 2 .03 5.812E+005 -5.495E+004 2 .348E+005

 >                2118.51       1. 16    O.OOOE+OOO                     O.OOOE+OOO     O.OOOE+OOO Pb-214       241.99      7.25     2.604E+005     5.42E+004      1. 5 14E+005    1.246E+005 2 95.22   18.4 2     9.707E+004                     6. 2 90E+004   4.612E+004 351. 93   35.6 0     5.423E+004                    2 .349E+004     2 .575E+004 785.96      1. 06    1.582E+006                    l.043E+006      7.228E+005 Pb214-XR       74.82     5.80     4. 2 78E+005   2.3 6E+005     7.985E+005      2 . 084E+005

77. 11 9.70 2 . 3 62E+005 1.391E+005 1.148E+005 87.35 2 .24 1. 025E+006 8. 2 94E+005 4.984E+005 89.78 0.82 2 .665E+006 - 7.965E+005 l. 2 94E+006 Ra-226 186. 2 1 3 .64 4.734E+005 4.73E+005 2 .310E+005 2.269E+005 Ac-228 12 9.07 2 .4 2 7 . 639E+005 8. 2 0E+004 1.658E+005 3.685E+005 2 0 9.25 3 .89 4.165E+005 1.963E+005 l.986E+005 270.24 3 . 46 5 .167E+005 1.858E+005 2 .460E+005 328.00 2 .95 5.060E+005 l.582E+005 2.371E+005 338.32 11. 27 1.489E+005 l.923E+004 7.0 2 0E+004 409.46 1. 92 7 . 468E+005 -6.792E+005 3.460E+005 463.00 4.40 3.611E+005 1 .407E+005 l .678E+005 794.95 4. 2 5 3.919E+005 8.505E+004 1 .788E+005 911.20 25.80 8.201E+004 2 .858E+004 3.800E+004 964.77 4.99 3.796E+005 2 .586E+005 l.738E+005 968.97 15.80 l.145E+005 - 2 . 804E+003 5 . 2 1 9E+004 1 588. 2 0 3.2 2 5.063E+005 3 .800E+005 2.2 1 0E+005 Pa-231 27.36 10.3 0 6.133E+004 6.13E+004 l.787E+004 2.758E+004 2 83.69 1. 70 9.032E+005 -3 .093E+005 4.2 5 9E+005 3 00 . 0 7 2.47 6.617E+005 - 1 .989E+005 3. 1 2 7E+005 30::2. 65 2.20 6.516E+005 - 5.734E+005 3. 053E+005 330.06 1. 40 9.933E+005 -6.269E+005 4.630E+005 Th-234 92.38 2.13 9.779E+005 9.78E+0 05 8. 2 87E+003 4.740E+005 92.8 0 2.10 9 . 877E+005 1.649E+005 4.787E+005 112.81 0.2 1 9.177E+006 8.146E+006 4.4 3 6E+006 U-235 143.76 10.96 l . 604E+005 3.02E+004 3 .348E+004 7.720E+004 163.33 5.08 3.193E+005 8.785E+004 l.529E+005 1 85.71 57. 2 0 3 .024E+004 2 .085E+004 l.450E+004 2 02 .11 1. 08 l.460E+006 -1.558E+005 6.959E+005 205.31 5.01 3. 1 3 9E+005 -8.633E+004 1.495E+005 Am-241 59.54 35.90 4.240E+004 4. 24 E+004 -1.855E+004 2.032E+004

    +     Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ Half-l ife too short to be able to perform the decay correction

[167]

*************************1    *************************         ' ****************
****         G A MMA      S P E C T R U M       A N A L Y S I S                *****
******************************* * ****************************************
.lename: 54 52 iport Generated On                 4/18/2016      1:0 2 :59 PM tmple  Title                        B306100AFRFC013GD tmple  Description                  TB 560 tmple  Identification tmple  Type tmple  Geometry iak Locate Threshold                 3 .00

!ak Locate Range (in channels) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Si ze 1.000E+OOO SQM tmpl e Taken On

quisition Started 4/18/2016 12:5 2 :57 PM

.ve Time 600.0 seconds !al Time 601.l seconds iad Time 0.18 % Energy Calibration Used Done On 1/1 3/ 2015 Efficiency Calibration Used Done On 4/14 /2 016 Efficiency ID TBFLOOR Ua.ttA. 'Jo.li'da1eo/ by G)~~ IJ-C.~li 0'110 [168]

iak Analysis Report 4/18/ 2 016 1: 0 2 :59 P1 Page 2

- - - P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample Title: B306 10 0AFRFC 0 13GD Peak Analysis Performed on: 4/18/2016 1 :0 2 :59 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV) Area Uncert. Counts 1 1 13- 119 115.84 28.55 0.47 1.83E+001 1 7.49 2.27E+001 2 2 93- 306 301.51 75.03 0.7 1 1.39E+00 2 53.83 2.12E+00 2 3 1129- 11 39 1134.01 2 83.40 0.41 1.22E+001 18.24 2.88E+001 4 1 401- 14 1 3 1406.83 3 51.68 0. 99 4.43E+001 2 2.28 2.97E+00 1 5 232 6- 2336 2 331. 1 9 58 2 .96 1. 0 6 1.93E+001 14.44 1.38E+001 6 2 42 9- 2444 2 435.84 609.14 1. 22 6.62E+001 19.53 9.76E+OOO 7 5830- 585 1 5841.30 1460.59 0.65 1.68E+002 2 8.17 8.19E+OOO

=  First peak in a mul tiplet region
=  Other peak in a mul tiplet region
=  Fitted singlet

rors quoted at 2. 000 sigma

[169]

1terference Corrected Acti ty Report 4/18/ 2 01 6 l , 2: 59 PM Page 3

- - - - * ***************************************
    - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title: B306100AFRFC013GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( i;;) (pCi/SQM ) Uncertainty K-40 1. 000 1460.82* 10.66 1.14418E+006 2.16272E+005 31.83 fva II~ 203 0.972 279.20* 81. 56 4.8:20801!:+003 7. 25476E t GOY. t.F ,1.0 s~t/- Tl-208 1. 000 583. 1 9* 85.00 1.05050E+004 7.97879E+00 3 Bi-211 0.999 351. 0 7* 1 3.02 1 .22277E+00 5 6.45974E+004 ~,i.,f../1# Th- 23 1 0.878 25.64* 1 4.10 3 .07689E+004 3.03250E+004

84. 2 1

6.60 4.99454E+005 2 . 2 6070E+005 89.95 1. 00

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :        10.000 keV Nuclide confidence index threshold=                 0.3 0 Errors quoted at 2 .000 sigma

[170]

1terference Corrected Act i ty Report 4/ 1 8/20 1 6 1 .,2 : 59 PM Page 4 '***** ****************************************************************** ' *** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** ' *********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 1.144184E+006 2.162718E+005 II~ 203 0.972 4.820804E1003 7.254764E1003 Tl-208 1. 000 1.050497E+004 7.978790E+00 3 Bi-211 0.999 1 .222770E+005 6.459741E+004 X Pa-231 0.515 Th-231 0.878 3.9 0 5311E+004 3 .005580E+004

       ? = Nuclide i s part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at         2 . 000 sigma
  ********'**       U N I D E N T I F I E D          P E A K S      *********

Peak Loca t e Performed on: 4/18/2016 1:02:59 PM Peak Locate From Channel: 85 Peak Locate To Channel: 81 92 Peak Energy Peak Size in Peak CPS Peak Tol.

No . ( keV) Counts per Second ~~ Uncertainty Type Nu clide 6 609.14 1.1041E-001 2 9.49 Sum M = First peak in a multiplet region m Other peak in a multiplet region F Fitted singlet Errors quoted at 2 .000 s igma [171]

iclide MDA Report 4/18/20ll 1 :0 2 :59 PM Page 5 "****************************************************************************** "*** N U C L I D E M D A R E P O R T *****

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Detector Name: 5452 Sample Geometry: Sample Title: B306100AFRFC013GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Leve l Name ( keV) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM )

+      K-40       1460.82*    10 .66    1 .426E+00 5    1.43E+005 l.144E+006           6.207E+004 Cr-51        32 0.08      9.91   1.638E+00 5     1.64E+005 1. 2 03E+005         7.722E+004 Mn-54        834.85    99.98     1.805E+004      1.81E+004 2 .976E+003          8.284E+00 3 Co-58        810.76    99.45     1.536E+004      1 .54E+004 -1.912E+004         6.944E+00 3 Co-60      1173. 2 3   99.85     1.654E+004      1. 2 0E+004 -7.433E+00 2       7. 393 E+00 3 1332.49     99.98     1.201E+004                   - 7.841E+00 3     5.071E+00 3 Nb- 94       702.65    99.81     1.496E+004      1.50E+004 -6 .240E+002         6.794E+00 3 871. 0 9  99.89     1 .532E+004                  -3 .755E+002      6.903E+003 Sn- 1 13     255.13      2 .11   7.105E+005      2 .35E+004 -2 .526E+004        3.356E+005 391. 70   64.97     2 . 3 53E+004                  4.151E+003      1.097E+004 Cs- 1 34     475 . 36    1. 48   1.055E+006      1.97E+004 -6. 2 57E+005        4.892E+005 563.25      8. 3 4  1.836E+005                   -1.103E+004       8.438E+004 569.33    15.37     9.798E+004                     6.162E+004      4.496E+004 604.72    97.62     2 .302E+004                  - 5.436E+00 3    1 .085E+004 795.86    85.46    1.974E+004                      9.490E+003      9.017E+003 801. 95     8.69   1.776E+005                    -6.4 8 7E+004    8.040E+004 1038.61       0 .99  1.315E+006                      3.046E+005     5.741E+005 1167.97       1. 79  1.077E+006                      5.591E+005     4.898E+005 1365. 1 9     3.02   4.361E+005                      l.207E+005     l.867E+005 Cs-137        661. 66   85. 1 0  2.282E+004       2.28E+004 2 .643E+004         1.063E+004 Eu-1 52       121.78    2 8.67   6.458E+004       5.82E+004 -1.311E+004         3 .117E+004 244.7 0     7.61   2.250E+005                   -1.919E+005       1.072E+005 295.94      0 .45  4.221E+006                      3 .130E+006    2 .011E+006 344.28    2 6.60   5.822E+004                   - 1.152E+004      2 .730E+004 367.79      0 .86  1.801E+006                      7.114E+00 3    8 . 426E+005 411.1 2     2.24   7.296E+005                      5.566E+004     3 .412E+005 443.96      2 .83  5.044E+005                      3.575E+003     2 . 32 9E+005 488.68      0.42   3 .464E+006                  -1.011E+006       1.595E+006 563.99       0.49   3 .086E+006                    2 .842E+005     1.417E+006 586. 2 6     0.46   3 .887E+006                    1.585E+004      1.807E+006 678. 62    0.47    3.071E+006                     1.687E+006      1.392E+006 688.67     0.86    1. 62 5E+006                   7.1 1 5E+004    7.333E+005 719.35      0.28    5.701E+006                   - 3.404E+005      2 .602E+006 778.90    12.96     l .289E+005                    3.309E+004      5.888E+004 8 10 .45    0.32    4.830E+006                   - 5.610E+006      2 .187E+006 867.37      4.26    3.468E+005                     4.744E+0 0 4    1.557E+005 919.33      0.43    3.906E+006                   -5.656E+0 0 5     1.771E+006 964.08    14.65     1. 2 16E+00 5                -5.660E+0 0 4     5.536E+004 1085.87     10.24     1.495E+005                   -2.992E+004       6.649E+004 1089.74       1. 73   8.496E+005                   -2.891E+005       3.759E+005 1 112.07    13.69     1. 3 00E+005                 -1.092E+005       5.875E+004 1212.95       1. 43   1.155E+006                     5.650E+00 5     5.150E+005

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tclide MDA Report 4/18/ 2 01 t 1:02:59 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (% ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM) Eu- 1 52 1249.94 0.19 9.658E+00 6 5 .82E+004 - 2 .405E+006 4.351E+006 1299.14 1.6 3 7.885E+00 5 -7 . 33 1E+004 3.376E+005 1408.01 21. 07 7.392E+004 1.098E+004 3.239E+004 1457.64 0.50 9.696E+006 2 .771E+007 4.653E+006 1528.10 0.28 4.615E+006 2 .649E+006 1. 94 9E+006 Eu-154 1 23 .07 40.40 4.530E+004 4.53E+004 - 2 .778E+004 2 .185E+004 2 47.93 6.89 2 .386E+005 1.859E+005 l.134E+005 591.76 4.95 3 . 23 4E+005 -1.847E+004 l.489E+005 692.42 1. 78 8. 2 33E+005 7.382E+005 3 .733E+005 723.30 20.06 8. 2 38E+004 4.486E+004 3 .772E+004 756.80 4.52 3 . 3 72E+005 -2 .033E+004 1.529E+005 873. 1 8 1 2 .08 1.403E+005 1.349E+005 6.389E+004 996.29 10.48 1.6 1 0E+005 5.584E+004 7. 2 79E+004 1 004.76 18.01 9.688E+004 1 .794E+004 4. 3 92E+004 1274.43 3 4.80 4.848E+004 -8.720E+003 2 .162E+004 1 596.48 1. 80 6.774E+005 -2. 668E+005 2 .809E+00 5 Eu- 1 55 45.30 1. 31 9.608E+00 5 7.55E+004 -3.582E+005 4.559E+005 60.01 1. 22 l.469E+00 6 2 .636E+005 7 .083E+005 86.55 30.70 7.554E+004 5.070E+004 3 .672E+004 1 05.31 2 1. 10 9. 1 85E+004 -3.979E+004 4.441E+004

+     Tl-208       583.19*    85.00    1.177E+004     l.18E+004 1.050E+004          5.145E+003
+-    Bi-21 1      351.07*    13. 0 2  8.863E+004     8.86E+004 1. 22 3E+005        4.058E+004 Pb- 211      404.85       3 .78  4. 2 56E+005   4. 2 6E+005 1.117E+004        1.990E+005 427.09       1. 76  9.070E+005                     4.610E+005    4. 23 0E+005 83 2 . 0 1   3 . 52 4.771E+005                   - 1.058E+005    2 .175E+005 Bi -2 12       3 9.86     1. 06  1.128E+006     2 .43E+0 0 5 3 .583E+005      5. 33 7E+005 727.33       6.67   2 .426E+005                    7.704E+004    l.109E+005 785.37       1.10   l. 52 1E+006                   4. 2 60E+005  6.950E+005 1620.50        1. 4 7 7.909E+005                     1. 3 7 )E+005 3. 2 42E+005 Pb-212       1 15.18      0.60   3 . 2 95E+006  4.47E+004 1.8 2 9E+006        l .594E+006 238.63     43.60    4.466E+004                     5.109E+004    2 .141E+004 300.09       3.30   4.906E+005                   - l.063E+006    2 .317E+005 Pb212-XR       74.82    10. 2 8  2.512E+005     1. 3 9E+005 6.416E+005        l. 2 25E+005

77. 11 17.10 1.386E+005 -1.677E+0 0 4 6.742E+004 87.35 3 .97 5.835E+005 5.922E+005 2 .836E+00 5 89.78 1. 46 1.526E+006 -9.377E+005 7.410E+005 Bi-214 609.32 45.49 5 .008E+004 5 . 01 E+00 4 6.196E+004 2 . 3 63E+004 768.36 4.89 3 . 2 66E+005 -3.511E+005 l.487E+005 806.18 1. 2 6 l. 2 76E+006 4. 1 82E+005 5.801E+005 934.06 3 . 11 5.498E+005 2.843E+005 2 .496E+00 5 1 12 0 . 2 9 1 4.92 l.333E+005 4.760E+004 6.089E+004 1 155. 2 1 1. 63 1.143E+006 4.921E+003 5 .181E+005 12 3 8. 1 2 5.83 3 . 62 0E+005 1.425E+005 1.656E+005 1280.98 1. 43 1.1 5 6E+006 - 9.075E+005 5.144E+005 1377.67 3.99 4.322E+005 2 .615E+005 1 . 922 E+005 1385.31 0.79 1.895E+006 - 2. 5 97E+005 8. 2 72E+005 1 40 1. 52 1. 33 1. 1 37E+006 8.537E+005 4.965E+005 1407.99 2 .39 6.506E+005 9.660E+004 2 .851E+005 1509.21 2 .13 4.181E+005 1 . 3 92E+005 1 .620E+005 1661.27 1. 05 9.017E+005 -8.446E+005 3 .493E+005

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tclide MDA Report 4/18/ 2 01- 1:0 2 :59 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM) (pCi/SQM) Bi-2 14 1729.59 2 .88 4. 2 03E+005 5.01E+004 1.959E+005 1.723E+005 1764.49 15.30 1. 4 79E+005 1.545E+005 6.676E+004 1847.43 2 .0 3 6.867E+005 - 3.892E+005 2 .876E+005

  >              2 118.51       1.1 6   O.OOOE+OOO                   O.OOOE+OOO   O.OOOE+OOO Pb- 2 1 4    2 41.99      7.25    2 .669E+005   5.61E+004      1.436E+005 1. 2 79E+005 2 95. 22   1 8.42    1.022E+005                   4.243E+004 4.867E+004 351. 93   35.60      5.613E+004                   8.361E+004 2 .670E+004 78 5 .96     1. 06   1 .601E+006                  1.052E+006 7.323E+005 Pb214-XR       74.8 2     5.80    4.452E+005    2 .44E+005     1.137E+006 2 .171E+005

77. 1 1 9.70 2 .443E+005 -2 .956E+004 1.188E+005 87.35 2 . 24 1.034E+006 1 .050E+006 5.027E+005 89.78 0.82 2 .717E+006 -l.670E+006 l. 319E+006 Ra-2 2 6 1 86.21 3.64 4.928E+005 4.93E+005 2 .187E+005 2.3 66E+005 Ac-228 129.07 2 .4 2 7.739E+005 7.22 E+004 4.161E+005 3 .7 3 5E+005 209.25 3 .89 4.485E+005 1.666E+005 2 .146E+005 270.24 3. 46 4.728E+005 -2 .549E+005 2 . 2 41E+005 328.00 2 .95 4.965E+005 9.934E+004 2.323E+005 338. 32 11.27 1.481E+005 9.977E+004 6.982E+004 409.46 1. 92 8.483E+00 5 6.635E+004 3.968E+005 463.00 4.40 3.375E+005 - 1.586E+005 1.561E+005 794 . 95 4.25 4.014E+005 1 .959E+005 1.836E+005 91 1. 2 0 25.80 7.223E+004 - 7.226E+004 3.311E+004 964.77 4.99 3.663E+005 -4.861E+004 1.672E+005 968.97 15.80 1.306E+005 1.337E+005 6.026E+004 1 588.20 3 . 22 4. 62 7E+005 1.265E+005 1.992E+005 Pa-231 27.36* 10.3 0 6.405E+004 6.41E+004 4. 2 12E+004 2.891E+004 283.69* 1. 70 5.773E+005 2.313E+005 2.630E+005 300.07 2 .47 6.554E+005 -1.421E+006 3.095E+005 302.65 2 . 20 6.987E+005 -4.054E+005 3.288E+005 330. 0 6 1. 40 9.860E+005 -8.271E+005 4.593E+005 Th-234 92.38 2 .13 1.014E+006 1.01E+006 -1.701E+005 4.9 1 9E+005 92 . 80 2 .10 1.028E+006 3.538E+005 4.989E+005 112.81 0.2 1 9.277E+006 3.115E+006 4.485E+006 U-235 1 43.76 10.96 1.632E+005 3.12E+004 6.748E+004 7.858E+004 1 63.33 5.08 3.236E+005 -2.563E+005 1.551E+005 185.71 57. 2 0 3.117E+004 9.474E+00 3 1.496E+004 202. 11 1. 08 1.629E+006 7.746E+005 7.803E+005 2 05.31 5.0 1 3 .460E+005 - 2 .987E+005 1.656E+005 Am-241 59.54 35.90 4.964E+004 4.96E+004 2 .438E+004 2 .392E+004

    + = Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    >= Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been c alculated
    @ = Half-life too short to be able to perfo rm the decay correction

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"************************' -************************** *****************
****        G A MMA      S P E C T R U M          A N A L Y S I S                 *****

- - - - * ************************* * ******************** * ********

.lename: 5452 !port Generated On 4/19/2016 9:17:53 AM tmple Title B306100AFRFC014GD tmple Description TB 580 tmple Identification tmple Type tmple Geometry !ak Locate Threshold 3.00 !ak Locate Range (in channels ) 85 - 8 1 92 iak Area Range (in channels) 85 - 8 1 92 lentification Energy Tolerance 10.000 keV tmple Size 1 .000E+OOO SQM tmple Taken On

quisition Started 4/19/2016 9: 0 7:51 AM

.ve Time 60 0 . 0 seconds ial Time 60 0 .7 seconds iad Time 0. 12 ~ Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBFLOOR l) cA\~ io.\\da}eJ by

                                                                   ~c4
                                                                   /J - tl, - /t 0 '{,JO

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iak Analysis Report 4/19/ 2 01 6 9:17:53 A. Page 2

- - - - * ********************* * *************************************
    - P E A K A N A L Y S I S R E P O R T *****
      - * ***********************************************************

Detector Name: 5452 Sample Title: B3061 00AFRFC014GD Peak Analysis Performed on: 4/19/2016 9: 1 7:5 3 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV) Area Uncert. Counts 1 297- 309 301. 4 6 75.02 0.61 7.50E+001 3 8.48 1.11E+002 2 14 01- 1414 1407. 2 7 351.79 0.69 5.05E+001 2 0.96 2 .15E+001 3 2429- 2 441 2 435. 2 3 6 0 8.99 1.14 4.43E+001 16.75 9.75E+OOO 4 5831- 5 849 5839.99 1 460.26 0.87 9.98E+001 2 4.84 1.62E+001

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 . 000 sigma

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1terference Corrected Acti Lt y Report 4/ 1 9/20 1 6 :; 1 7:53 AM Page 3

- - - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title: B306100AFRFC014GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K-40 1. 000 1460.82* 10 .66 6.80229E+005 1. 7 934 7E+005 Bi -2 11 0. 999 351. 07* 1 3.02 1.39532E+005 6.2 0 892E+004

       *=Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold             0.3 0 Errors quoted at 2.000 sigma

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1terference Corrected Acti _ty Report 4/19/2016 S .L7: 53 AM Page 4 "*********************************************************************** "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** "*********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 6.802293E+005 1. 793470E+005 Bi-211 0.999 1.395324E+005 6.208922E+004

     ?     Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2.000 sigma
 **********      U N I D E N T I F I E D         P E A K S      **********

Peak Locate Performed on: 4/19/2016 9:17:53 AM Peak Locate From Channel: 85 Peak Locate To rh~nnPl

8192 Pea k Energy Peak Si z e in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide 1 75.02 1. 2502E- 001 51. 3 0 Tol. Pb214-XR Ba-133 Pb212-XR Pb212-XR Pb214-XR 3 608.99 7 .3 750E-00 2 3 7.84 Tol. Zr-97 Sb-125 Sb-125 Cs-134 Bi -2 14 M = First peak in a multiplet region m Other peak in a multiplet region F Fitted singlet Errors quoted at 2 .000 sigma [178]

1clide MDA Report 4/19/20lt, 9:17:53 AM Page 5 "****************************************************************************** "*** N U C L I D E M D A R E P O R T *****

Detector Name: 545 2 Sample Geometry: Sample Title: B306100AFRFC014GD Nuclide Librar 11 Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( ~) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM)

+      K-40       1460.8 2

10.66 1.840E+005 1.84E+005 6.802E+005 8. 2 77E+004 Cr-51 320.08 9.91 1.232E+005 1. 2 3E+005 -6.845E+004 5.693E+004 Mn-54 834.85 99.98 1.171E+004 1.17E+004 -4.121E+003 5. 11 3E+003 Co-58 810.76 99.45 1. 28 1E+004 1. 28E+004 -9.537E+001 5.670E+003 Co-60 117 3 . 23 99.85 1.130E+004 1.13E+004 1.687E+003 4.772E+003 1 33 2 .49 99.98 1.343E+004 8.961E+003 5.782E+003 Nb-94 70 2 .65 99.8 1 1.195E+004 1. 2 0E+004 - 1.385E+003 5.289E+003 871. 09 99.89 1. 2 59E+004 2.181E+003 5.535E+003 Sn-11 3 255.13 2.11 6.539E+005 1.90E+004 -8.600E+004 3 .073E+005 391.70 64.97 1.901E+004 - 2 .055E+003 8.715E+003 Cs- 1 3 4 475.36 1. 48 9.111E+005 l.69E+004 3.991E+005 4.172E+005 563. 2 5 8.34 1.394E+005 l .276E+004 6. 2 32E+004 569.33 1 5.37 8.655E+004 -1.510E+004 3.924E+004 604.72 97.62 2 .041E+004 -1.671E+004 9.550E+00 3 795.86 85.46 1.690E+004 3.022E+003 7.601E+00 3 801. 95 8.69 1.359E+005 - 1.751E+005 5.954E+004 1038.61 0.99 1.161E+006 - 4.627E+004 4.972E+005 1167.97 1. 79 6.549E+005 - 1. 2 05E+006 2 .786E+005 1365.19 3.02 4.5 1 3E+005 -3 . 3 59E+005 l .943E+005 Cs - 1 37 661. 66 85.10 1.731E+004 1.73E+004 -9.836E+00 3 7.869E+00 3 Eu - 1 52 121.78 28.67 4.830E+004 4.7 2 E+004 -9.812E+00 3 2 .303E+004 244.70 7.6 1 1 .815E+005 -6 .003E+004 8.542E+004 295.94 0.45 3. 2 61E+00 6 8.462E+005 1.531E+006 344.28 2 6.60 4.718E+004 -3.343E+004 2 .178E+004 367.79 0.86 1.403E+006 4.322E+005 6 . 43 6E+005 411.12 2.24 6.255E+005 -1. 2 60E+005 2 .892E+005 443.96 2.83 4.595E+005 1 .537E+005 2 .104E+005 488.68 0.42 3.429E+006 2.556E+006 1 .578E+006 563.99 0.49 2.369E+006 1.278E+006 1 .059E+006 586. 2 6 0.46 3.567E+006 l.027E+006 1.647E+006 678. 62 0.47 2 .375E+006 1. 2 49E+005 1.044E+006 688.67 0.86 1 .574E+006 9. 2 19E+005 7.076E+005 719.35 0. 2 8 5. 2 61E+006 2.194E+005 2 .382E+006 778.90 12 .96 1. 04 7E+005 -3.182E+004 4.679E+004 810.45 0. 32 3.969E+006 -1.561E+005 1.756E+006 867.37 4. 2 6 3. 2 83E+005 3.018E+005 1.464E+005 919.33 0.43 3.617E+006 3.633E+006 1. 62 7E+006 964.08 1 4.65 1 .117E+005 9.903E+004 5.039E+004 1085.87 10.24 1.263E+005 - 5.566E+004 5.491E+004 1089.74 1. 73 8.682E+005 2 .981E+005 3 .8 52 E+005 1112.07 13.69 9.556E+004 -2 . 2 32E+005 4.154E+004 1212.95 1. 43 1.109E+006 -2 .803E+004 4.921E+005

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4/19/20 h 9:17:5 3 AM Page 6 1clide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activit y Dec. Level Name ( keV} ( %} (pCi/SQM} (pCi/SQM ) (pCi/SQM ) (pCi/SQM) Eu-152 1 249.94 0.19 6.886E+006 4.72E+004 - 8.836E+004 2 .965E+006 1299.14 1. 6 3 7.598E+005 1.361E+00 5 3. 2 32E+005 14 0 8.01 21. 07 6.579E+004 1.240E+004 2 .833E+004 1457.64 0.50 7.959E+006 1.765E+007 3 .784E+006 1528.10 0. 2 8 2 .852E+006 -2. 164E+006 l.067E+006 Eu - 1 54 123.07 40.40 3 .432E+004 3.43E+004 -1.440E+004 1.636E+004 247.93 6.89 2 .029E+005 -7.441E+004 9.552E+004 591.76 4.95 2 .495E+005 5.664E+004 l. 1 2 0E+005 692.42 1. 78 7.751E+005 -1.844E+005 3 .492E+005 723.30 2 0.06 7. 2 27E+004 -2.692E+003 3. 2 67E+004 756.80 4.5 2 2 .850E+005 -6.970E+004 1. 2 68E+005 873.18 12 .08 1 . 1 15E+005 4.598E+004 4.949E+004 996. 2 9 10.48 1.250E+005 -1.915E+004 5.479E+004 1 004.76 18 . 01 8.351E+004 -5.155E+004 3.724E+004 1274.4 3 3 4.80 3 .775E+004 -1.453E+003 1.625E+004 1 596.48 1. 80 6.02 1E+005 2 .562E+005 2 .433E+005 Eu-155 45.30 1. 31 6.965E+005 5.36E+004 -2 .016E+005 3 . 2 37E+005 60.01 1. 22 9.394E+005 2 .432E+003 4.434E+005 86.55 30.70 5.359E+004 4.486E+004 2 .575E+004 105.31 21.10 6.841E+004 -1.065E+004 3. 2 68E+004 Tl -2 08 583.19 85.00 1 .925E+004 1 .93E+004 9.961E+003 8.888E+003

+     Bi-2 11      351.07*   13 . 02  7 . 743E+004   7 , 74E+004 1 . 395E+005    3 . 498E+004 Pb-211       404.85      3.78   3 .432E+005    3. 2 3E+005 - 4.856E +004   1.578E+005 427.09      1. 76  7.491E+005                 - 5.844E+005    3.440E+005 832.01      3.5 2  3.229E+005                 - 5.843E+004    1.404E+0 05 Bi -2 1 2      39.86     1. 06  7.357E+005     1.90E+005 -3.134E+005       3.376E+005 727.33      6.67   1 .896E+005                -1.809E+005     8.435E+004 785.37      1.10   1.427E+006                   4.604E+005    6.477E+005 1620.5 0      1. 4 7 4.891E+005                 -7.900E+004     1.733E+005 Pb- 212      115.18      0.60   2 .516E+006    3.67E+004 1.676E+006        1.204E+006 238.63    43.60    3 . 670E+004                 1.689E+004    1.743E+004 3 00.09     3.30   3.928E+005                 - 5.902E+005    1 .828E+005 Pb212-XR       74.82   10. 2 8  1 .957E+005    1.06E+005 4.4 3 8E+0 0 5    9.471E+004 77.11   17.10    1 .059E+005                -4.391E+0 0 4   5.105E+004 87.35     3.97   4. 2 40E+005                 4.673E+0 0 5  2 .039E+00 5 89.78     1. 46  1.156E+006                   4.328E+0 0 5  5.558E+005 Bi-214       609.32    45.49    4.161E+004     4.16E+004 4.644E+0 0 4      1.939E+004 7 68.36     4 . 89 2 .755E+005                  1.587E+005    l. 2 31E+005 806. 1 8    1. 2 6 9.361E+005                   4.446E+005    4. 1 02E+005 934. 0 6    3 .11  5.0 2 1E+005                 3.917E+005    2 . 25 8E+005 112 0 . 2 9 14.92    1. 2 84E+005                 6.262E+004    5.843E+004 1155. 2 1     1. 63  9.459E+005                 -7.696E+0 0 5   4.197E+005 1238.1 2      5.83   2 .558E+005                -7.788E+0 0 4   1 . 1 2 5E+005 1280.98       1. 43  9.771E+005                   5.893E+004    4. 2 48E+005 1377.67       3.99   3.756E+005                   3 .964E+004   1.6 3 9E+005 1385.31       0 .79  1.732E+006                   6.154E+005    7.456E+005 1401. 52      1. 33  1.106E+006                   6.670E+004    4.808E+005 1407.99       2.39   5.790E+005                   1.092E+005    2 .493E+005 1509. 2 1     2 . 13 6.314E+005                   3 .8 2 9E+005 2 .686E+005 1661. 2 7     1. 0 5 1.059E+00 6                -1.314E+005     4. 2 78E+005

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1clide MDA Report 4/19/ 2 011_ 9:17:53 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) (pCi/SQM) Bi -2 14 1729.59 2 .88 3 .013E+005 4.16E+004 8. 3 97E+004 1.128E+005 1764.49 15.3 0 1.359E+005 8.427E+004 6.073E+004 1847.43 2 .03 5.40 2E +005 -8.654E+004 2 .144E+005

 >                 2118.51      1.16   O.OOOE+OOO                    O.OOOE+OOO     O.OOOE+OOO Pb- 2 14     241.99      7.25   2.223E+005     5. 02E+004     1.4 1 8E+00 5  1.056E+00 5 295.22    18.42    8.106E+004                    4.858E+004     3.811E+004 351.93    35.60    5.021E+004                    5 .777E+004    2.374E+004 785.96      1. 06  1.463E+006                    1.488E+005     6.633E+005 Pb2 1 4-XR      74.82    5.80    3 .468E+005    1.87E+005      7.866E+005     1.679E+005 77.11     9.70  1.866E+005                   -7.741E+004      9.000E+004

87. 3 5 2 . 24 7.515E+005 8.282E+005 3 .614E+005 89.78 0.82 2 .057E+006 7.706E+005 9.895E+00 5 Ra-226 1 86. 2 1 3. 64 3.533E+005 3 .53E+005 9.915E+004 1.669E+005 Ac-228 129.07 2 .4 2 5.853E+005 7.99E+004 -1.359E+005 2 .793E+005 209.25 3.89 3.547E+005 - 6.923E+004 1.677E+005 27 0 .24 3.46 3.840E+005 - 3.822E+005 1. 7 97E+00 5 328. 00 2.95 4.489E+005 2 .778E+005 2 .085E+005 338.32 11. 2 7 1. 2 85E+005 4.668E+004 6.002E+ 0 04 409.46 1. 92 6.795E+005 -3 .983E+005 3.123E+005 463. 00 4.40 3.053E+005 6.673E+004 1.399E+005 794.95 4.25 3.453E+005 -7.357E+004 1.556E+005 911. 2 0 25.80 7 . 986E+004 1.134E+005 3 .693E+0 0 4 964.77 4.99 3. 2 80E + 005 1.979E+005 1.480E+005 968.97 15.80 1.054E+005 6.387E+004 4.764E+004 1588.2 0 3 . 22 3.567E+005 - 5.768E+00 4 1.462E+005 Pa- 23 1 2 7.36 10.30 7.318E+004 7. 32E+004 5.195E+004 3 . 3 47E+004 28 3 .69 1. 70 8.008E+005 3.681E+005 3 .747E+005 300. 07 2 .47 5.248E+005 -7.884E+005 2 .442E+005 302.65 2 . 20 5.687E+005 -5.458E+005 2. 638E+005 330. 0 6 1. 40 9.019E+005 -5.836E+004 4 . 1 73E+005 Th-2 34 92.38 2 .13 7. 2 19E+005 7. 2 2E+005 -7.783E+004 3.459E+005 92.8 0 2 .10 7.302E+005 7.974E+004 3.498E+005 112.8 1 0 .21 6.937E+006 -8.164E+00 5 3.315E+006 U-235 1 43.76 10 .96 1 .295E+005 2 . 22 E+004 3 . 3 73E+004 6. 17 4E+004 1 63.33 5.08 2 .628E+005 -3 . 3 41E+004 1. 2 47E+005 1 85.71 57. 2 0 2 . 2 24E+004 7. 2 47E+00 3 l.050E+004 20 2 .11 1. 08 1.184E+006 3 .034E+005 5.580E+005 205.31 5.01 2 . 5 99E+005 -8 .288E+004 1. 2 25E+005 Am- 2 41 59.54 35.90 3 .129E+004 3. 1 3E+004 6 .503E+00 3 1. 4 7 5E+004

    +      Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    >= Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Hal f- life too short to be abl e to perform the decay correction

[181]

*************************'   *************************           '****************
****        G A MMA      S P E C T R U M        A N A L Y S I S                   *****
************************************************************************

.l ename: 5452 iport Generated On 4/18 /2 016 2 : 22 :3 5 PM tmple Title B306100AFQWC009GD tmple Description TB 560 ' 1mple Identification 1mple Type tmple Geometry iak Locate Thre shold 3. 00 iak Locate Range (in channels) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mple Si ze 1.000E+OOO SQM 1mple Taken On

quisition Started 4/18/ 2 016 2 :1 2 : 33 PM

.ve Time 600.0 seconds ial Time 600.5 seconds iad Time 0.08 % Energy Calibration Used Done On 1/1 3 /2015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBWALL

                                                                      -P~t6. \Ja\,c\o.\cJ. by o~~

1:,-6,-IYi 0 '116 [182]

iak Analysis Report 4/ 1 8 /2 016 2 : 22 : 35 Pi. Page 2

- - - - * ***********************************************************
    - P E A K A N A L Y S I S R E P O R T *****

"************************************************************ * *********** Detector Name: 5452 Sample Title: B306100AFQWC009GD Peak Analysis Performed on: 4/18/2016 2 : 22 :3 4 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV) Area Uncert. Counts 1 1 1 74- 1183 1178.69 294.58 0.49 1.97E+001 17.82 2 .63E+001 2 1401- 1412 1407.05 351.73 0.67 4.05E+001 2 0 .47 2.5 5E+001 3 2 428- 2 443 2436.61 609.33 1. 29 6.89E+001 19.97 1.0lE+OOl 4 5828- 5851 5841.46 1460.63 1. 31 1 .24E+00 2 2 4.45 6.19E+OOO First peak in a multiplet region Other peak in a multiplet region Fitted singlet

rors quoted at 2 .000 sigma

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iterference Corrected Act1 _ty Report 4/18/ 2 016 22:35 PM Page 3

- - - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****
      - * ********************************

Sample Title: B306100AFQWC009GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( gc:) (pCi/SQM ) Uncertaint~, K-40 1. 000 1460.82* 10.66 8.44191E+ 005 l.82121E+005 Bi-21 1 0.999 351.07* 13. 0 2 1.11729E+005 5.93298E+004 Pb-21 4 0.778 2 41. 99 7. 2 5 2 95. 22

18.42 3.51481E+004 3.23072E+004 351. 93* 35.60 4. 0 86 2 8E+004 2 . 1 6862E+004 785.96 1. 06

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuclide confidence index threshold=               0. 3 0 Errors quoted at 2. 000 sigma

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1terference Corrected Acti ty Report 4/ 1 8/ 2 01 6 :2: 35 PM Page 4

- - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 8.441911E+005 1.821208E+005 Bi-211 0.999 l .562543E+004 l.063903E+005 Pb-214 0.778 3.514812E+004 3.230688E+004

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2 . 000 sigma
 **********     U N I D E N T I      F I  E D    P E A K s        **********

Peak Locate Performed on: 4/18/ 2 01 6 2: 22 :34 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Si ze in Peak CPS Peak Tol. No. ( keV) Counts per Second % Uncertainty Type Nuclide 3 609.33 1.1478E-001 29.0 0 Tol. Zr-97 Sb-125 Sb- 1 25 Cs - 1 34 Bi - 21 4 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted s i nglet Errors quoted at 2 .000 s i gma [185]

~elide MDA Report 4/ 1 8/ 2 0 1 2:22:35 PM Page 5 "******************* * ********** * ************ * ********************************** "*** N U C L I D E MD A R E P O R T ***** "****************************************************************************** Detector Name: 545 2 Sample Geometry: Sample Title: B306l00AFQWC009GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) 1460.8 2

10 .66 1.321E+005 l.32E+005 8.442E+005 5.680E+004

+      K-40 6.879E+004 Cr-51        32 0. 0 8    9.9 1  1.469E+005     1. 4 7E+005 8.623E+004 Mn-54        83 4.85    99.98    1.375E+004     1.37E+004 8.779E+003          6.130E+003 Co-58        810.76     99.45    1. 2 23E+004   1. 2 2E+004 2.331E+003        5.379E+003 Co-60      117 3 . 23   99.85    1.525E+004     1.53E+004 - 1.250E+004        6.749E+003 1 33 2 .49   99.98    1.584E+004                    8.145E+003     6.990E+003 Nb-94        702.65     99.81    1.296E+004     9.77E+00 3 8.685E+002         5.794E+003 871. 0 9   99.89    9.768E+003                  -1.416E+004      4.125E+003 Sn-113       2 55. 1 3    2 .11  6.576E+005     1.94E+004 2.188E+004          3.092E+005 391. 7 0   64.97    1.943E+004                    5.4 22 E+003   8. 92 5E+003 Cs- 1 34     475.36       1. 48  8.683E+005     1.80E+004 4.261E+005          3.958E+0 0 5 563.25       8.34   l.757E+005                  -3.346E+004      8.045E+004 569.33     15.37    8.777E+004                  -3.382E+0 0 4    3.985E+004 604.72     97. 62   2.33 6E+004                 -1.140E+004      1.103E+004 795.86     85.46    1.799E+004                    1.949E+004     8.145E+003 801. 95      8.69   1. 4 91E+005                -7.153E+004      6.617E+004 1038.61        0 .99  1.451E+006                    9. 1 00E+004   6.4 1 9E+005 1167.97        1. 79  1.002E+006                    2 . 2 1 9E+005 4.523E+005 1 365.19       3.0 2  4.035E+005                  -8.919E+004      1.704E+005 Cs-137       661. 66    85.10    1 .585E+004    1.59E+004 - 1. 746E+004       7.141E+003 Eu - 152     121.78     2 8 . 67 6.001E+004     5.34E+004 1.502E+004          2 .888E+004 244.7 0      7.61   1.938E+005                  -2.609E+005      9.158E+004 295.94       0.45   3 .790E+006                 -3.198E+005      l .795E+006 344.28     2 6.60   5.340E+004                    2 . 3 74E+004  2 .489E+004 367.79       0.86   1 .628E+006                 -1.999E+006      7.563E+005 411 .12      2.24   6.478E+005                  - 1.508E+005     3.003E+005 443.96       2.83   4.900E+005                  - 6.679E+005     2 . 2 56E+005 488.68       0.42   3.096E+006                    5.912E+005     1.411E+006 563.99       0.49   2.951E+006                  -2 .466E+005     1.350E+006 586.26       0 . 46 3. 2 49E+006                  9.354E+005     1.488E+006 678.62       0.47   2 .937E+006                 - 1.075E+006     1 .326E+006 688.67       0 . 86 1 .650E+006                   1.098E+006     7.458E+005 719.35       0.28   5.771E+006                    3 .111E+006    2 .637E+006 778.90     12.96    1.085E+005                  -5 . 2 98E+004   4.870E+004 81 0 .45     0. 32  3.598E+006                    l.899E+005     1.571E+006 867.37       4. 2 6 2. 2 86E+005                - 2. 618E+005    9.654E+004 919.33       0.43   3.850E+006                    1.0 2 1E+006   1.743E+006 964. 0 8   1 4.65   1.117E+005                    6.262E+004     5.039E+004 1085.87      10. 2 4  1. 52 5E+005                -1.523E+004      6.799E+004 1089.74        1. 73  9.040E+005                    6.209E+005     4.03 1E+00 5 1 112.07     13.69    1.108E+005                  -6.076E+004      4.915E+004 1212.95        1. 43  1 .155E+006                   4.501E+005     5.150E+005

[186]

4/18/ 2 01l 2 : 22 :35 PM Page 6 1clide MDA Report Nuclid e Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Eu- 1 52 1249.94 0.19 7.110E+006 5 . 3 4E+004 -2.468E+006 3.077E+006 1299.14 1. 63 7.885E+005 -1.843E+006 3.376E+005 1408.01 21. 07 7.941E+004 4.120E+004 3 .514E+004 1457.64 0.50 8.336E+006 1.885E+00 7 3 .973E+006 1528.10 0.28 4.203E+006 - 1.954E+00 6 1 .743E+006 Eu-154 123.07 40.40 4.200E+004 4. 2 0E+004 1. 3 80E+004 2 .021E+004 247.93 6.89 2 .155E+005 -1. 2 08E+005 1.018E+005 591. 76 4.95 2 .362E+005 -2.134E+005 1.053E+00 5 692.42 1. 78 7.875E+005 2.878E+005 3 .554E+00 5 723.30 20.06 8.695E+004 7.101E+004 4.001E+004 756.80 4.52 3.324E+005 2.479E+005 1.505E+005 873.18 1 2 .08 9.621E+004 1. 509E+004 4.183E+004 996. 2 9 10.48 1.250E+005 -9.081E+004 5.479E+004 1004.76 18.01 8.668E+004 6.088E+004 3 .882E+004 1274.43 34.80 4.557E+004 -2 .907E+00 3 2 .016E+004 1596.48 1. 80 5.597E+005 - 3.949E+005 2 . 22 1E+005 Eu-155 45.30 1. 31 8.491E+005 6.35E+004 5.432E+005 4.003E+005 60.01 1. 22 1.082E+006 2 .568E+004 5 . 1 48E+005 86.55 3 0.70 6.355E+004 4.934E+004 3 .074E+004 105.31 2 1. 10 8.031E+004 -1.760E+004 3 .864E+004 Tl-208 583.19 85.00 1 .813E+004 1.81E+004 1. 22 2E+004 8. 32 7E+003

+     Bi-211       351.07*    13.02    8. 0 34E+004   8.03E+004 1.117E+005         3.643E+004 Pb-211       404.85       3.78   3 .707E+005    3.66E+005 -2 .187E+005       1.715E+005 427.09       1. 76  7.804E+005                    5.194E+005    3.597E+005 83 2 .01     3.5 2  3 .664E+005                 -4. 2 07E+005   1.621E+005 Bi-21 2       3 9.86      1. 06  8.589E+005     2.43E+00 5 -3 .940E+005      3.995E+005 727.33       6.67   2 .4 2 6E+005               -5 .055E+004    1.109E+005 785.37       1.10   1 . 2 59E+006               - 1. 1 55E+006  5.638E+005 1620.50        1. 4 7 8. 3 56E+005                  3 . 2 92E+004 3.466E+005 Pb- 2 1 2    115.18       0.60   2 .781E+006    4.05E+004 8.822E+005         1 . 3 37E+006 238.63     43 .60   4.050E+004                    5.729E+00 4   1 .933E+004 30 0 . 0 9   3.30   4.713E+005                  -1. 22 1E+005   2 . 22 0E+005 Pb21 2 -XR    74.8 2    10. 2 8  2 .132E+005    1 . 1 6E+005 3 .613E+005     1. 0 35E+005

77. 11 17. 1 0 1. 1 65E+005 2. 1 88E+004 5.638E+004 87.35 3.97 4.850E+00 5 2. 2 08E+005 2.345E+005 89.78 1. 4 6 1.238E+00 6 -3.745E+005 5.971E+005 Bi -2 14 609.32 45.49 5.155E+004 5.15E+004 9.010E+004 2 .436E+004 768.36 4.89 3 .266E+005 l .935E+005 1.487E+005 806.18 1. 2 6 9. 11 6E+005 1 .818E+005 3.980E+005 934.06 3.11 5.186E+005 -1.448E+005 2 .340E+005 1120.29 14 .92 1. 2 67E+005 3.609E+004 5.759E+004 1 155.21 1. 63 8.837E+005 - 2 .953E+005 3.886E+005 1238.12 5.83 3.064E+005 9.456E+004 1.378E+005 1280.98 1. 43 1.133E+006 -8.340E+005 5.0 2 6E+005 1 377.67 3.99 3.652E+005 -2.290E+004 1.587E+005 1385.31 0.79 1.612E+006 -1.525E+006 6.858E+005 140 1 .5 2 1. 33 1.335E+006 - 2.337E+005 5.953E+005 1 407.99 2 .39 6.989E+005 3.626E+005 3 .092E+005 1 509. 21 2 .1 3 5.227E+005 2.437E+005 2 .143E+005 1661. 27 1. 05 1 .251E+006 6.757E+005 5. 23 9E+005

[187]

!Slide MDA Report 4/18/201 l 2 : 22 : 35 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi -2 14 1729.59 2 .88 4. 2 03E+005 5.15E+004 - l.100E+005 l.723E+00 5 1764.49 15.30 1. 3 84E+005 4.338E+004 6.199E+004 1847.43 2 .03 6.188E+005 2 .885E+005 2 .536E+OOS 2118.51 1.16 O.OOOE+OOO O. OOOE+OOO O.OOOE+OOO

  >
+      Pb- 2 14      241.99     7. 2 5 2 .421E+005    2.94E+004 2 .064E+005       1.155E+00 5 295. 22

18.42 5.021E+004 3 .515E+004 2 . 2 69E+004 351.93* 35 .60 2 .938E+004 4.086E+004 1.332E+004 785.96 1. 06 l.399E+006 5.818E+OOS 6.315E+005 Pb214-XR 74.82 5.80 3 .779E+005 2 .05E+00 5 6.403E+OOS l.835E+005 77.11 9.70 2 .053E+005 3.857E+004 9.939E+004 87.35 2 . 24 8.596E+005 3.914E+005 4.156E+OOS 89.78 0.82 2 . 2 04E+006 -6.669E+005 l.063E+006 Ra- 2 26 186.21 3.64 4.331E+005 4. 3 3E+005 9.412E+004 2 .068E+005 Ac-228 129.07 2.42 6.684E+005 7 .8 4E+004 2 .082E+005 3.208E+005 209. 2 5 3.89 4.0 23 E+005 4. 2 06E+00 5 l.915E+005 270. 2 4 3.46 4. 2 42E+005 1.424E+004 l.998E+005 328.00 2 .95 4.867E+005 9.419E+004 2.274E+005 338.32 11. 27 1. 2 76E+005 2 . 12 0E+004 5.958E+004 409.46 1. 92 7.532E+005 4.050E+005 3.492E+005 463.00 4.40 3.120E+005 -5.942E+004 l.433E+005 794.95 4. 2 5 3.562E+005 3.042E+005 l.610E+005 911. 2 0 25.80 7.840E+004 l. 2 51E+004 3.619E+004 964.77 4.99 3.176E+005 9.505E+004 1.4 2 8E+00 5 968.97 15.80 1.054E+005 2 .031E+004 4.764E+004 1588.20 3. 22 3.768E+005 -2 .360E+005 1.563E+005 Pa- 23 1 27.36 10.30 6 . 133E+004 6.13E+004 3.971E+003 2 .758E+004 2 83.69 1. 70 8.008E+00 5 -2 .972E+005 3 .747E+005 300.07 2 .47 6. 2 96E+00 5 -1.632E+005 2 .966E+005 30 2 .65 2 . 20 6.597E+005 -2 .079E+005 3.094E+005 330.06 1. 40 1.015E+006 3.607E+005 4.737E+005 Th- 23 4 92.38 2 .13 8. 2 64E+005 8. 2 6E+005 -5.060E+005 3.982E+005 92.80 2 .10 8.332E+005 -5 .925E+005 4.014E+005 112.81 0. 2 1 7.907E+006 1.077E+005 3.801E+006 U- 2 35 143.76 10.96 l.447E+005 2 .78E+004 -2 .409E+004 6.932E+004 163.33 5.08 3 .078E+005 6.074E+004 l.472E+005 185.71 57.20 2 .779E+004 8. 63 1E+003 l.327E+004 2 02.11 1. 08 l.420E+006 -7.821E+005 6.757E+005 205.31 5.0 1 3.117E+005 -5.512E+004 l.484E+005 Am-241 59.54 35.90 3.596E+004 3 .60E+004 -1.974E+004 l.709E+004

     +      Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
     > = Calculated MDA is zero due to z ero counts in the region, or the r egion is outside the spectrum, or MDA has not been calculated
     @ =    Half-life   too short to be able to perform the decay correction

[188]

"**** * *******************    ~********************** *

i *****************

"***          GAMM A      S .I! E C T R U M         A N A L Y ~ I S               *****
"***********************************************************************
.lename : E:\Zion Nuclear\Inspector Shots\B306100ASJWC15GD.CNF iport Generated On                   1/31/2 01 7       1:35: 2 9 PM tmple  Title                         B3061008SJWC15GD tmple  Description                   Clean/Dirty Oil Tank Room tmple   Identification                East Wall 1mpl e  Type tmpl e  Geometry                      3 meter iak Locate Threshold                    3. 00 iak Locate Range (in channels )             85 -   8 1 92 iak Area Range (in channels )               85 -   8 1 92 lentification Energy Tolerance            10.000 keV tmple Size                              1.000E+OOO SQ MET tmple Taken On

quisition Started 1 2 / 22/2 015 2 :34:58 PM

.ve Time 600.0 seconds ial Time 600.5 seconds iad Time 0 .09 % Energy Calibration Used Done On 1/27/2015 Efficiency Calibration Used Done On 1/31/2017 Efficiency ID CRIBHOUSE 3M u~,o. ~ohAa\.e~ lov Q~ ( tz-eo~1y; O'bOO [189]

iak Analysis Report 1 /3 1 /20 1 7 1 :35: 2 9 f Page 2

********************************************** * **************************
"***             P E A K        A N A L Y S I S               R E P O R T                *****
******************************** * ****************************************

Detector Name: 5456 Sample Title: B306 100 8S JWC 15GD Peak Analysis Performed on: 1 /31/2017 1:35: 2 9 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) (keV ) Area Uncert. Counts 1 2 97 - 308 301.80 75.18 0.69 8.39E+001 60.43 3.26E+002 2 5 27- 533 5 2 9.95 13 2 . 2 6 0. 33 4. 2 3E+OOO 24.87 7.78E+001 3 1404- 1415 14 0 9.38 352 . 22 0.7 3 5. 3 0E+001 23.92 3.60E+001 4 2433- 2448 2439.06 609.67 0.41 5.68E+001 21. 42 1.92E+001 5 5838- 5859 5847.73 1461. 2 4 1. 56 1.59E+00 2 25.22 O.OOE+OOO First peak in a multiplet region Other peak in a multiplet region

=  Fitted singlet

rors quoted at 2 . 000 sigma

[190]

1terference Corrected Act . ~ty Report 1/31/2017 35 : 29 PM Page 3 "*********************************************************************** "*** N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

- - - - * ********************************* * **********************

Sampl e Title: B306l008SJWC15GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQ M) Uncertainty K-40 1. 000 1 460.82* 10.66 l.07 62 7E+006 1. 94616E+005 Tc-99m 0.897 1 40.51* 89.00 l.15 52 2E+003 6.79272E+003 Bi- 2 1 1 0.998 3 51.07* 13.02 1. 46183E+005 7.00631E+004

       * = Energy line found in the spectrum .
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :         10.000 keV Nuclide confidence index thre shold =         0. 3 0 Errors quoted at 2 .000 sigma

[191]

1terference Corrected Act . ~ty Report 1/3 1 /2017 35: 2 9 PM Page 4 "*************** * ******************************************************* "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** "*********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 1. 000 1. 076268E+006 1 .946164E+005 Tc-99m 0.897 l . 1 55223E+003 6.792718E+003 Bi-211 0.998 1.461826E+005 7.006305E+004

        ? = Nuclide is part of an undetermined solution X     Nuclide rejected by the interference analysis
       @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2 .000 sigma
 ** * *******      U N I D E N T I F I E D           P E A K S       **********

Peak Locate Performed on: 1/31/2 017 1:35: 2 9 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second % Uncertainty Type Nucl ide 1 75.18 1 .3985E- 001 72 . 02 Tol. Pb214-XR Ba- 1 33 Pb2 1 2-XR Pb212-XR Pb21 4 -XR 4 6 09.67 9.4594E-00 2 37.7 4 To l . Zr-97 Sb-125 Sb-125 Cs-134 Bi- 2 14 M = First peak in a multiplet region m = Other peak in a multiplet region F Fitted singlet Errors quoted at 2 . 000 sigma [192]

1clide MDA Report 1 /3 1/ 2 01 1:35: 29 PM Page 5

- - - - * ***************************************************************

"*** N U C L I D E MD A R E P O R T ***** "****************************************************************************** Detector Name: 5456 Sample Geometry: 3 meter Sample Title: B3061008SJWC15GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name {keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) + K-40 1460.82* 10.66 1.832E+004 1.83E+004 1.076E+006 O.OOOE+OOO Cr-51 32 0.08 9.91 1.712E+005 1.71E+005 1.384E+004 8.092E+004 Mn-54 834.85 99.98 l. 3 97E+004 1.40E+004 -3 .572E+003 6.243E+003 Co-58 810.76 99.45 1.531E+004 1. 53E+004 -1. 41 2E+003 6.919E+003 Co-60 1173. 2 3 99.85 1.649E+004 1.46E+004 4.863E+003 7.370E+003 1332.49 99.98 1.461E+004 7.1 3 4E+003 6.379E+003 Nb-94 702.65 99.81 1.358E+004 1. 3 6E+004 -3.550E+003 6.107E+003 871. 09 99.89 l.601E+004 - 2 .631E+003 7. 2 47E+003 Sn-113 255.13 2 .11 8.505E+005 2.31E+004 1. 209E+005 4.055E+00 5 391. 7 0 64.97 2 . 3 13E+004 -8.282E+003 1.077E+004 Cs-134 475.36 1. 48 1.077E+006 1.79E+004 1.604E+005 5 .001E+005 563.25 8.34 1.917E+005 1.4 6 0E+005 8.852E+004 569.33 15.37 1.139E+005 5.2 3 6E+004 5. 2 96E+004 604.72 97.6 2 1.788E+004 -1.813E+004 8. 2 92E+003 795.86 85.46 2.058E+004 9.618E+003 9.443E+003 801. 95 8.69 1.717E+005 -3.468E+005 7.746E+004 1038.61 0.99 l.348E+006 3.540E+005 5.906E+005 1 167.97 1. 79 9.006E+005 6.252E+005 4.016E+005 1365 .1 9 3.02 3.837E+005 -2.405E+005 1.607E+005 Cs-137 661. 6 6 85.10 1.695E+004 1.69E+004 1.132E+004 7.694E+003 Eu-152 121. 78 28.67 7.323E+004 5.84E+004 4.239E+004 3 .550E+004 244.70 7.61 2 .614E+005 7.329E+004 1.253E+005 295.94 0.45 4.429E+006 2 .860E+006 2 .115E+006 344.28 2 6.60 6.574E+004 - 8.012E+003 3.106E+004 367.79 0.86 2 .097E+006 -2 .139E+005 9.908E+005 411.12 2 . 24 7.462E+005 8.393E+004 3 .496E+005 443.96 2 .8 3 6.010E+005 3.577E+005 2 .812E+005 488.68 0.4 2 3.583E+006 -8.1 1 6E+005 1.655E+006 563.99 0.49 3.227E+006 3 . 92 6E+005 1 .489E+006 586. 2 6 0.46 3.770E+006 1.909E+006 1.749E+006 678. 62 0.47 3.050E+006 2 .889E+005 1.383E+006 688.67 0.86 1.931E+006 -3 . 1 44E+004 8.869E+005 719.35 0. 2 8 5. 2 30E+006 -5 .454E+004 2.368E+006 778.90 12.96 1. 2 36E+005 -5 .708E+004 5. 626E+004 810.45 0. 32 4.742E+006 1.256E+006 2 .143E+006 867.37 4. 26 3.520E+005 1.615E+005 1.583E+005 919.33 0.43 3.843E+006 2 .058E+006 1.740E+006 964.08 14.65 1.362E+005 - 2 .588E+004 6.266E+004 1085.87 10. 2 4 1.429E+005 5 . 2 43E+004 6.324E+004 1089.74 1. 73 8.090E+005 4.540E+005 3 .557E+00 5 1112.07 1 3 .69 1.057E+005 -2.989E+004 4.663E+004 1 212 .95 1. 43 1 .007E+006 -4.944E+005 4.412E+005 [193]

1 /31/2 0 1 1:35:29 PM Page 6 1clide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Eu- 1 52 1249.94 0.19 7. 2 94E+006 5.84E+004 1.455E+006 3 .171E+006 1299. 1 4 1. 63 8.885E+005 4.702E+005 3 .879E+005 1408. 0 1 21. 0 7 5.843E+004 -3.061E+004 2 . 4 68E+004 1457.64 0.50 8.845E+006 -6. 2 32E+006 4. 22 9E+006 1528.10 0. 2 8 2 .440E+006 5.254E+005 8 .643E+005 Eu-15 4 123.07 40.40 4.969E+004 4.22E+004 -1.404E+004 2 .405E+004 247.93 6.89 2 .852E+005 2.136E+005 1. 3 67E+005 591. 76 4.95 2 .301E+005 -2 .734E+005 1.023E+005 692.42 1. 78 9.557E+005 1.636E+00 5 4.397E+005 723.30 20.06 7.805E+004 4.358E+004 3 .558E+004 756.80 4.52 3 . 2 09E+005 -2 .023E+004 1 .448E+005 873. 1 8 1 2 .08 1. 2 45E+005 -1.471E+004 5.599E+004 996. 2 9 10.48 1.454E+005 1. 568E+004 6.499E+004 1004.76 18.01 9.392E+004 4.442E+003 4. 2 45E+004 1274.43 34 . 80 4.222E+004 6.354E+003 1.850E+004 1596.48 1. 8 0 8.768E+005 6.345E+005 3 .812E+005 Eu-155 45. 3 0 1. 31 2 .081E+006 8. 2 1E+004 -3 . 2 79E+004 1.011E+00 6 60.01 1. 22 2 . 3 64E+006 1. 3 67E+006 l .151E+00 6 86.55 30.70 8. 2 08E+004 5.982E+004 4.000E+004 105.31 2 1.10 9.696E+004 -4.521E+004 4.697E+004 Tl -2 08 583. 1 9 85.00 2 .228E+004 2 . 2 3E+004 2 .461E+004 1.041E+004 + Bi -2 11 351. 0 7* 13.0 2 9.360E+004 9. 3 6E+004 1.462E+005 4. 3 07E+004 Pb-2 11 404.85 3 .78 4.946E+005 3.65E+005 -9.720E+003 2 . 33 5E+005 427.09 1. 76 9.542E+005 2 .578E+005 4.467E+005 832.01 3.52 3.652E+005 -2 .815E+005 1.616E+005 Bi- 212 39.86 1. 06 2 .800E+006 2.32E+005 1. 3 96E+006 1. 3 64E+006 727.33 6.67 2 .324E+005 1.338E+005 1 .058E+00 5 785.37 1.10 1.497E+006 1.022E+006 6.830E+005 1 620.5 0 1. 4 7 7.834E+005 3.652E+005 3 . 2 11E+005 Pb-21 2 115. 1 8 0.60 3.229E+006 4.70E+004 -2 .445E+006 1.561E+006 238.63 43.60 4.702E+004 1 .427E+004 2 .259E+004 300.09 3.30 5 .859E+005 -3 . 444E+005 2 .793E+005 Pb2 1 2-XR 74.8 2 10.28 3 .170E+005 1.78E+005 4.707E+005 1.552E+005 77.11 17.10 1.780E+005 -2 .718E+004 8.704E+004 87.35 3.97 6.217E+005 1 .682E+005 3 .028E+005 89.78 1. 46 1. 598E+006 -9.644E+005 7.774E+005 Bi-214 609. 32 45.49 5.096E+004 5.10E+004 7.4 3 7E+004 2 .408E+004 768. 3 6 4.89 3 .4 1 6E+00 5 -7.052E+004 1 . 562E+005 8 0 6.18 1. 2 6 1. 219E+006 -2 .886E+004 5.519E+005 934. 0 6 3.11 4.754E+005 1.476E+004 2 .125E+005 1 1 2 0. 2 9 14.92 1.436E+005 1.905E+005 6.608E+004 1 155. 2 1 1. 63 1 .171E+006 6.641E+005 5.324E+005 1238. 1 2 5.83 3 .051E+005 1.050E+005 1. 3 72E+005 1 2 80.98 1. 43 1 .103E+006 6.598E+005 4.8 82E+005 1377.67 3.99 3 .629E+005 3.940E+004 1.578E+005 1385.31 0.79 1.831E+006 -1.466E+006 7.958E+005 140 1. 52 1. 33 1.190E+006 9.541E+005 5.232E+00 5 1407.99 2 .39 5.143E+005 -2.694E+005 2 .172E+00 5 1509.21 2 .13 6.727E+005 -1.892E+005 2 .896E+00 5 1661.27 1. 05 1 .179E+006 -3 .902E+005 4.891E+005 [194]

1clide MDA Report 1 /31/ 2 01 1: 35 : 2 9 PM Page 7 Nucl ide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Bi -2 14 1729.59 2 .88 3.905E+005 5.10E+004 1.661E+005 1.578E+00 5 1764.49 15.3 0 1.463E+005 1.528E+005 6.602E+004 1847.43 2 .03 6.460E+005 3 . 25 7E+005 2 .679E+005

 >                2118.51       1.16 O.OOOE+OOO                     O.OOOE+OOO       O.OOOE+OOO Pb- 2 14     24 1. 99    7.25 2.927E+005 5.94E+004           2 . 62 8E+005    1.407E+005 295.22    1 8.42 1 .066E+005                    8.006E+004       5. 0 86E+004 351.93    35.60 5.942E+004                      7.615E+004       2 .834E+004 785.96      1. 06 1.477E+006                  -6.464E+005        6.708E+005 Pb214-XR       74.8 2    5.80 5.618E+005 3 .14E+005          8. 3 43E+005    2 .750E+005 77.11     9.70 3 .138E+005                  -4.791E+004       1.534E+005 87.35     2.24 1. 1 02E+006                   2 .982E+005     5.367E+005 89.78     0.82 2 .846E+006                  -1.717E+006       1.384E+006 Ra-2 2 6      186.2 1    3 .64 4.884E+005 4.88E+005         - 1.487E+005      2.344E+005 Ac-228        129.07     2 .4 2 8.153E+005 7.45E+004       -1.692E+005        3.943E+005 2 09.25    3 .89 4.684E+005                     1.115E+004      2.245E+005 2 70.24    3 . 46 5.437E+005                    2 .720E+005     2.595E+005 328.00     2 .95 6.162E+005                     1.031E+005      2.922E+005 338.32   11. 2 7 1. 691E+00 5                   7.820E+004      8.031E+004 409.46     1. 92 8.677E+005                  -9 .840E+005       4.065E+005 463.00     4. 40 3 .762E+005                    3 .360E+004     1.754E+005 794.95      4.25 4.091E+005                   - 6.8 2 3E+004     1. 87 5E+005 911.20   25.80 7.447E+004                       3.000E+004      3.424E+004 964.77     4.99 4.080E+005                      1 . 562E+005    1.881E+005 968.97    15.8 0 1.157E+00 5                  - 1.783E+004       5.281E+004 1588.2 0     3.22 4.100E+005                   - 6.472E+004       1.731E+005 Pa- 23 1       27.36   10 .3 0 3.375E+005 3 . 3 8E+005     -1. 3 84E+00 5     1.651E+005 283.69      1. 7 0 1.042E+006                 -9.329E+00 5       4.952E+005 300.07      2 .47 7.828E+005                  -4.601E+005        3.732E+005 302 . 65    2 . 20 8 . 523E+ 0 05                8 . 7 1 7E+004  4.056E+005 330.06      1. 40 l.361E+006                    1 .033E+006      6.467E+005 Th-234         92.38     2 .13 l.071E+006 1. 0 7E+006         4.423E+005      5. 2 08E+005 92.80     2 .10 1.088E+006                    7. 2 99E+005     5. 2 89E+005 11 2.81     0.21 9.0 2 0E+006                 -1.691E+006        4.357E+006 U-2 35       1 43.76   10.96 1.823E+005 3 .13E+004           1.806E+005       8.813E+004 163.33      5.08 3 .526E+005                    1.435E+005       1.695E+005 185.71    57. 2 0 3 .127E+004                 -1.822E+004        1.501E+004 202.11      1. 08 1.633E+006                  -9.212E+005        7.819E+005 205.31      5.01 3.680E+005                   -1. 62 5E+005      1.765E+005 Am-24 1        59.54   35.90 8.079E+004 8. 0 8E+004          6.940E+004       3.933E+004
    +     Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @     Half-life too short to be able to perform the decay correction

[195]

"************************       '********************* * ***      *****************
****          GAMM A       S t' E C T R U M         A N A L Y ::, I S                  *****
*************** * **************** * ***************************************
.lename: E: \ Zion Nuclear \ Inspector Shots\B306100ASJWC16GD.CNF
!port Generated On                    1/31 /2 017     2 :05:44 PM tmple  Title                          B3061008SJWC16GD tmple  Description                    Clean/Dirty 5"ii Tank Room tmple  Identification                 North Wall tmple  Type tmpl e Geometry                       3 meter iak Locate Threshold                    3 . 00

!ak Locate Range (in channels) 85 - 81 92 !ak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10 . 000 keV tmpl e Size 1.000E+OOO SQ MET tmple Taken On

quisition Started 12/ 22 /2015 2:52:47 PM

.ve Time 600.0 seconds !al Time 600.3 seconds !ad Time 0 . 05 % Energy Calibration Used Done On 1/27/2015 Efficiency Calibration Used Done On 1/31/2017 Efficiency ID CRIBHOUSE 3M

                                                                  \ ) o:\C\ \lo.\ ic\o..\ec\ 'oy Q~4
                                                                    ,~-{,,~/'l 6150

[196]

iak Analysis Report 1 /31/2017 2 :05:44 f Page 2

*************************************************************************
****             P E A K      A N A L Y S I S           R E P O R T              *****
********************************* * ***************************************

Detector Name: 5456 Sample Title: B30610 0 8SJWC16GD Peak Analysis Performed on: 1 /31 /2 017 2:05:4 3 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area Uncert. Counts 1 2 431- 2447 2440.63 610 .06 1. 48 6.05E+001 21.19 1.65E+001 2 3875 - 3884 3879.34 969.6 2 0.37 1. 2 0E+001 9.73 5.00E+OOO 3 5839- 5859 5849.31 1461.64 1. 31 1.44E+00 2 27.19 1.08E+001

=  First peak in a mul tiplet region
=  Other peak in a mul tiplet region
= Fitted singlet

rors quoted at 2 .000 sigma

[197]

1terference Corrected Act ity Report 1/31/2017 05:44 PM Page 3 "***********************************************************************

- - - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title: B3061008SJWC16GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQ M) Uncertainty K-40 0.999 1460.8 2

10.66 9.76374E+005 2 .0 2 688E+00 5

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold =       0.30 Errors quoted at 2 .000 sigma

[198]

1terference Corrected Act ity Report 1 / 3 1 /2017 05: 44 PM Page 4

- - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****
      - * *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 0.999 9.763741E+005 2 .026880E+005

      ?  = Nuclide is part of an undetermined solution X   = Nuclide rejected by the interference analysis
      @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at        2. 000 sigma
 **********       U N I D E N T I F I E D        P E A K S          **********

Peak Locate Performed on: 1 /31/2017 2:05:43 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak To l. No. (keV) Counts per Second % Uncertainty Type Nuclide 1 61 0 .06 1.00 83E- 001 3 5. 0 3 Tol. Zr-97 Sb- 125 Sb- 1 25 Cs- 1 34 Bi-2 14 2 969.62 2 .0000E-00 2 8 1.1 2 To l . Eu-152 Ac-228 Ac-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 s igma [199]

1cl i de MDA Report 1/31/ 2 0 ] 2 :05 : 44 PM Page 5

- - - N U C L I D E MD A R E P O R T *****

Detector Name: 5456 Sample Geometry: 3 meter Sample Title: B3061008SJWC16GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) (%) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M)

+       K-40       1460. 82

10.66 1.603E+005 1.60E+005 9.764E+005 7.101E+004 Cr-5 1 32 0.08 9.91 1.479E+005 1.48E+005 -4.877E+004 6.927E+004 Mn-54 834.85 99.98 1.448E+004 1.45E+004 5.936E+003 6.498E+003 Co-58 810.76 99.45 1.531E+004 1. 53E+004 1 .072E+004 6.919E+003 Co-60 1173. 2 3 99.85 1.486E+004 1. 34E+004 -2 .910E+00 3 6.557E+003 13 32 .49 99.98 1.336E+004 4.443E+003 5.750E+003 Nb-94 70 2 .65 99.81 1.264E+004 1. 2 6E+004 -9. 1 92E+003 5.636E+003 871. 09 99.89 1.504E+004 4.870E+002 6.763E+003 Sn-113 255.13 2 .11 6.611E+005 2 . 1 9E+004 -1. 93 4E+005 3.108E+005 391. 70 64.97 2.189E+004 -3.910E+003 l.0 1 6E+004 Cs- 134 475.36 1. 48 9 . 2 76E+005 1.68E+004 6.145E+005 4. 25 6E+005 563. 2 5 8. 3 4 l.578E+005 - 1.010E+005 7.153E+004 569.33 15. 3 7 8.603E+004 -l. 3 71E+004 3 .900E+004 604.72 97. 62 l.833E+004 -8.061E+003 8.515E+00 3 795.86 85.46 l.684E+004 -9.569E+002 7.571E+003 801. 95 8.69 1.517E+005 2 .600E+004 6.747E+004 1038.61 0.99 l.510E+006 1 .016E+006 6.718E+005 1167.97 1. 79 8. 27 4E+005 -l.710E+005 3.650E+005 1365.19 3.02 4.632E+005 3.224E+005 2.004E+005 Cs-137 661.66 85.10 l.871E+004 l .87E+004 4.669E+003 8.5 7 6E+00 3 Eu- 15 2 121. 78 2 8.67 6.037E+004 5. 0 1E+004 -2 .464E+004 2 .907E+004 244.70 7.61 l. 932E +005 -7.276E+002 9.123E+004 2 95.94 0.45 3.508E+006 1.156E+006 1.654E+006 344. 2 8 2 6.60 5.011E+004 -l.610E+004 2 . 32 5E+004 367.79 0.86 l .502E+006 -3.942E+005 6.935E+005 411.12 2 . 24 6.064E+005 1 . 1 71E+005 2 .797E+005 443.96 2 .8 3 4.881E+005 -1.093E+005 2 . 2 48E+005 488.68 0.4 2 3.042E+006 1. 3 66E+005 l .385E+006 563.99 0.49 2.604E+006 -l. 62 7E+006 l.177E+006 586. 2 6 0.46 4. 23 9E+006 3. 517E+006 l.984E+006 678. 62 0.47 2.629E+006 -l.376E+006 l.172E+006 688.67 0.86 l. 2 39E+006 -2 . 2 39E+006 5.410E+005 719.35 0. 2 8 4.298E+006 9.550E+005 l.902E+006 778.90 1 2 .96 l.062E+005 6.029E+004 4.755E+004 810.45 0.32 4.670E+006 l.430E+006 2 .107E+006 867.37 4.26 3.746E+005 -4.751E+004 1. 696E+005 919. 33 0.43 3.899E+006 1.545E+006 1 .768E+006 964.08 14.65 1. 2 90E+005 4. 2 71E+004 5.908E+004 1085.87 10.24 1.429E+005 5. 3 19E+004 6.324E+004 1089.74 1. 73 7.683E+005 l.577E+004 3 . 3 54E+005 111 2 .07 13.69 l.032E+005 -4.024E+004 4. 5 39E+004 1 212 .95 1. 43 1. 2 57E+0 0 6 7.572E+005 5 . 6 62E+005

[200]

lClide MDA Report 1 /31/201 2 :05:44 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Eu-15 2 1 249.94 0.19 8.275E+006 5.01E+004 4.984E+006 3.661E+006 1299.14 1. 63 7.846E+005 -2 .614E+005 3.359E+005 1408.01 21. 07 8. 22 8E +004 7.380E+004 3.660E+004 1 457.64 0.50 8.819E+006 -3.784E+006 4.2 1 6E+006 1528.10 0. 2 8 3 .156E+006 -1.363E+006 1.222E+006 Eu-154 123.07 40.40 4. 21 8E+004 4 . 11E+004 -3.678E+004 2.029E+004 247.93 6.89 1 .905E+005 -1. 752E+005 8.930E+004 59 1. 76 4.95 2 .604E+005 1.7 5 0E+005 1. 17 5E+005 692.42 1. 78 7.448E+005 2 . 2 00E+005 3.343E+00 5 723.30 2 0.06 5 .993E+004 -7.0 2 8E+004 2.652E+004 756.8 0 4. 52 2 .595E+005 - 2 .890E+004 1.141E+005 873.18 12 .08 1 . 22 4E+005 -9.130E+004 5.495E+004 996. 2 9 10.48 1.632E+005 4.732E+004 7.386E+004 1004.76 18.01 8.336E+004 9.488E+00 3 3 .717E+004 1274.4 3 34.80 4.112E+004 - 6.142E+004 1.795E+004 1596.48 1. 80 6.712E+005 6.742E+004 2 .784E+005 Eu-155 45.3 0 1. 3 1 9.704E+005 7.18E+004 6.4 3 7E+004 4. 5 61E+005

60. 0 1 1. 22 1.603E+006 2 .0 5 1E+005 7.704E+005 86.55 3 0.70 7.185E+004 l.014E+005 3 .488E+004 1 05.3 1 2 1.10 8. 32 5E+004 -3 . 1 2 0E+004 4.011E+004 Tl-208 58 3 . 1 9 85.00 2 .376E+004 2 . 3 8E+004 3.7 3 9E+004 1.114E+004 Bi-211 351. 0 7 13.0 2 1.387E+005 1. 3 9E+005 1. 3 10E+005 6.564E+004 Pb-211 404.85 3.78 3.595E+005 3 .60E+005 -7.613E+004 1. 660E+005 427. 0 9 1. 76 8.572E+005 -2 .161E+00 5 3 .982E+005 832. 01 3.52 4. 0 34E+005 6.990E+004 1.807E+005 Bi -2 1 2 39.86 1. 06 1. 1 44E+006 2 .07E+005 -l.550E+005 5.358E+005 727. 33 6.67 2. 0 66E+005 -8.127E+004 9.291E+004 785.37 1.10 1 .231E+ 0 06 4.042E+005 5.500E+005 1 620.50 1. 47 6.266E+ 0 05 2 .087E+005 2 .427E+005 Pb- 212 115.18 0.60 3.095E+006 4.09E+004 8.455E+005 1. 494E+006 2 38.63 43.60 4.091E+004 2 .911E+004 1.953E+004 300.09 3.30 4.492E+005 -8. 2 17E+005 2 .110E+005 Pb2 12-XR 74.82 10. 2 8 2 .618E+005 1. 4 7E+005 4.479E+005 1. 2 76E+005 77.11 17.10 1.469E+005 8.826E+004 7.150E+004 87.35 3.97 5.427E+005 4.952E+005 2 .633E+005 89.78 1. 46 1. 374E+006 -1.132E+006 6 .653E+005 Bi-21 4 609.32 45.49 5.096E+004 5. 1 0E+004 6.028E+004 2 .408E+004 768.36 4.89 3 .077E+005 5.091E+004 1.393E+005 806.18 1. 2 6 l.107E+006 -2.301E+005 4.956E+005 934.06 3.11 5.256E+005 2.5 92 E+005 2 .376E+005 1120.29 14.92 1.376E+005 3.070E+004 6.307E+004 1155.2 1 1. 63 1.171E+006 4.797E+005 5. 32 4E+005 1238.12 5.83 3. 2 95E+005 1. 041E+005 1.494E+005 1280.98 1. 43 1 . 1 27E+006 4.022E+005 5.002E+005 1377.67 3.99 4. 2 95E+005 1.703E+005 1. 911E+005 1385.31 0.79 1. 4 72E+006 -1.028E+006 6.164E+00 5 1401.52 1. 33 1.246E+006 3 .843E+005 5.5 1 5E+005 1 407.99 2.39 7. 2 42E+005 6.495E+005 3. 22 1E+005 1 509. 2 1 2.13 6.262E+005 1.852E+005 2.664E+005 1 661. 2 7 1. 05 1 .048E+006 4.460E+005 4.236E+005

[201]

1clide MDA Report 1/31/ 2 0~ 2 :05:44 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (% ) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Bi -21 4 1729.59 2 .88 4.8 2 3E+005 5.10E+004 2 .769E+005 2 . 0 37E+005 1764.49 15.30 1. 1 83E+005 4.831E+004 5 . 2 02E+004 1 84 7.43 2 . 03 5.742E+0 0 5 2 .443E+005 2 . 32 0E+005

 >                2 11 8.51          1. 1 6 O.OOOE+OOO                    O.OOOE+OOO   O.OOOE+OOO Pb-2 1 4     2 41. 99         7.25   2 .468E+005     5 .17E+004    1.876E+005   1 .178E+005 2 95. 22        18.42   8.607E+004                    6.642E+004   4.061E+004 351. 93         35.60   5.171E+004                    7. 1 07E+004 2 .449E+004 785.96           1. 06  1. 32 7E+006                - 6.515E+004   5.954E+005 Pb214-XR         74.8 2       5.80   4.640E+005      2.59E+00 5    7.939E+005   2 . 2 62E+005 77.11         9.70   2 .590E+005                   1.556E+005   l. 2 60E+005 87.35        2 . 24 9.619E+005                    8.776E+005   4.667E+005 89.78         0 .82  2 .447E+006                 -2 .016E+006   1.185E+006 Ra-22 6      186. 2 1         3.64   4. 25 6E+005    4. 2 6E+005   2 .850E+005  2 .030E+005 Ac-22 8      129. 07          2.42   7.345E+005      6.96E+004     5.714E+004   3.538E+005 209. 2 5         3.89   4.111E+005                    2 .799E+005  1.958E+005 2 70. 2 4        3.46   4.074E+005                  -8.436E+004    1.913E+005 328.00           2.95   4.832E+005                  -1.555E+005    2 .257E+005 338.32          11.2 7  1.417E+005                    3.903E+004   6.664E+004 409.46           1. 92  7.185E+005                    2 .513E+005  3 .319E+005 463. 00          4.40   3.596E+005                    3.063E+005   1.671E+005 794.95           4.25   3.384E+005                    1.388E+005   l .522E+005 911. 2 0        25 .80  6.963E+004                    2 .855E+004  3 .182E+004 964.77           4.99   4.040E+005                    7. 2 13E+004 1.861E+00 5 968.97          15.80   1.157E+005                    6.455E+004   5 . 2 81E+004 1588.20            3.22   3.734E+005                  -1.103E+004    1.549E+005 Pa- 2 3 1       27.36        10.30   1.162E+005      1.16E+005     1.084E+004   5.440E+004 283.69           1 . 70 8.031E+005                  -1.475E+005    3.758E+005 300.07           2.47   6.001E +005                 -l.098E+006    2 .818E+005 302.65           2. 2 0 6.921E+005                    2 .849E+005  3. 2 55E+005
                    '°\""'lf"I
                    .:>.:>U. UO f"lr

1. 4 0 l.042E+006 1 .161E+005 4.874E+005 Th- 234 92.38 2.13 9. 2 08E+005 9 .2 1E+005 -2 .028E+004 4.455E+005 92 .80 2 .10 9.416E+005 5.174E+005 4.556E+005 112.81 0. 2 1 8.398E+006 l.303E+006 4.046E+006 U- 235 143.76 10 . 96 1.559E+005 2 .78E+004 3 .943E+004 7.494E+004 163.33 5.08 3.119E+005 1.0 9 4E+005 1.492E+005 185.7 1 57. 2 0 2.776E+004 2.411E+004 1 .3 25E+004 2 02.11 1. 08 1.441E+006 -1.874E+005 6.862E+005 2 05. 3 1 5.01 3.163E+005 -4.865E+004 1.507E+005 Am-241 59.54 35.90 5.466E+004 5.47E+004 2 .000E+00 3 2 . 62 7E+004

     +     Nuclide identified during the nuclide identification

Energy line found in the spectrum

     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ = Half-l ife too short to b e able to perform the decay correction

[202]

*** * ******************** j     *************************            ~*****************
****          G A M MA      S l:? E C T R U M        A N A L Y S I S                              *****
****************************************************************** * *****
.lename: E: \ Zion Nucl ear \Turbine Building\B306100AFJWC017GD.CNF iport Generated On                     1/31/2017       11: 40 : 12 AM -    '{'e - '('I:>.\(\ V'CfN"'!' 1 ""~,:.*,*~"

1mple Title B306100AFJWC017GD tmple Description VALVE PIT ---. tmple Identification tmple Type tmple Geometry SQ M !ak Locate Threshold 3 . 00 !ak Locate Range (in channels ) 85 - 81 92 iak Area Range (in channels ) 85 - 81 92 lentification Energy Tolerance 10.000 keV tmple Size 1. OOOE+OOO 1 tmpl e Taken On

quisition Started 3/3/2 01 6 1 : 32 :14 PM

.ve Time 600.0 seconds ial Time 600.4 seconds !ad Time 0 . 06 % Energy Calibration Used Done On 1 /2 7 /2 015 Efficiency Calibration Used Done On 4/11 /2 016 Efficiency ID TB VALVE PIT

1) 0.. \ " ~o.\ \d a.~~ 'Q1 9~~~

1=2-, - ,i

                                                                       , , 10

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ia k Analysis Report 1 /3 1 / 2 017 11:40:12 Page 2

******************************* * **** * ************************************
****             P E A K        A N A L Y S I S             R E P O R T                *****
*************************************************************************

Detector Name: 5456 Sample Title: B306 1 00AFJWC017GD Peak Analysis Performed on: 1/31/2017 11:4 0 :12 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI RO I Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV ) Area Uncert. Counts 1 5830- 5853 5842.83 1 460.02 1.08 1. 3 9E+00 2 2 6. 32 8.57E+O OO

= First peak in a multiplet region Other peak in a multiplet region Fitted singlet

rors quoted at 2 .000 sigma

[204]

1terference Corrected Act ity Report 1/3 1 / 2 017 : 40:1 2 AM Page 3

- - - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Titl e : B306100AFJWC017GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/1 ) Uncertainty K-40 0.999 1460.82* 10.66 3.82069E+006 7.93761E+005

Energy line found in the spectrum.

      @=Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold =       0. 3 0 Errors quoted at 2 .000 s igma

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1terference Corrected Act ity Report 1/31/ 2 017 ;40:1 2 AM Page 4

- - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

' *********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/1 ) Uncertainty K-40 0.999 3.820690E+006 7.9376 1 0E+005

      ?    Nuclide is part of an undetermined solution X  = Nuclide rejected by the interference analysis
      @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at    2 .000 sigma
  **********    U N I D E N T I F I E D        P E A K S        **********

Peak Locate Performed on: 1 / 3 1/2017 11:40:12 AM Peak Locate From Channel: 85 Peak Locate To Channel: 81 92 Peak Energy Peak Size in Peak CPS Peak To1 . No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified. [206]

lClide MDA Report 1/31/ 2 0 11:40:1 2 AM Page 5 "****************************************************************************** "*** N U C L I D E MD A R E P O R T ***** "****************************************************************************** Detector Name: 5456 Sample Geometry: SQM Sample Title: B306100AFJWC0l7GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/1 ) (pCi/1 ) (pCi/1 ) (pCi/1 )

+      K-40       1460.8 2

1 0 .66 5.975E+005 5.97E+005 3 .821E+006 2.617E+005 Cr-51 32 0.08 9.91 9.699E+005 9.70E+005 2 .937E+005 4.518E+005 Mn-54 834.85 99.98 6.833E+004 6.83E+004 -5.058E+004 3.054E+004 Co-58 810.76 99.45 7.460E+004 7.46E+004 2 . 2 84E+004 3.366E+004 Co-60 11 73 . 2 3 99.85 6.451E+004 5.57E+004 -l.798E+004 2.846E+004 13 32 .49 99.98 5.568E+004 -5.057E+003 2.397E+004 Nb-94 7 0 2 .65 99.8 1 8.592E+004 6.86E+004 3 .106E+004 3.938E+004 871. 09 99.89 6.864E+004 -6 .141E+003 3.068E+004 Sn-113 255.1 3 2 .11 4.909E+006 1 .28E+005 -1.071E+006 2.303E+006 391.7 0 64.97 1. 2 83E+005 -2 .067E+004 5.896E+004 Cs-134 475.36 1. 48 5. 3 85E+006 8 .2 5E+004 -3 .590E+005 2.461E+006 563.25 8.34 7.744E+005 -3 .532E+004 3.453E+005 569.33 15.37 3 .863E+005 -1.513E+005 1.704E+005 604.72 97.62 9.743E+004 -1. 36 4E+004 4.511E+004 795.86 85.46 8. 2 51E+004 4.917E+004 3.703E+004 8 01. 95 8.69 7.537E+005 - 1.044E+005 3.353E+005 10 38.6 1 0.99 4.417E+006 - 3 . 3 93E+006 1.832E+006 11 67 . 97 1. 79 3 .838E+006 5.973E+005 1.707E+006 1 36.5. 19 3.02 l.660E+006 -2 .144E+005 7.009E+005 Cs- 1 37 66 1. 66 85.10 l.108E+005 l.11E+005 8.058E+004 5.125E+004 Eu- 1 52 1 21. 78 28.67 5.994E+005 2 .68E+005 -1.385E+005 2 .880E+005 2 44.7 0 7.61 1. 508E+006 5.524E+004 7.124E+005 2 95.94 0.45 2.460E+007 1.079E+007 1.158E+007 344. 2 8 2 6.6 0 3.390E+005 l.401E+005 1.571E+005 367.79 0.86 1.008E+007 3.039E+006 4.654E+006 411.12 2.24 3.705E+006 -2.568E+005 1.702E+006 443.96 2.83 3.223E+006 -5.488E+005 1. 4 91E+006 488.68 0.4 2 1.806E+007 8.917E+006 8. 2 09E+006 563.99 0.49 l. 2 08E+007 -3 . 2 37E+006 5.330E+006 586. 2 6 0 . 46 l.950E+007 2 . 2 75E+006 8.986E+006 678.62 0.47 1.281E+007 l.877E+006 5.652E+006 688.67 0.86 7.368E+006 2 .179E+006 3.269E+006 7 1 9.35 0.28 2 .325E+007 5.385E+006 1.034E+007 778.90 12.96 6. 2 92E+005 -2.999E+0 0 5 2. 868E+005 810.45 0. 32 2 . 3 47E+007 4.377E+006 1 . 061E+007 867.37 4. 2 6 1 .548E+006 -l.599E+005 6.885E+005 919.33 0.43 l .456E+ 0 07 2 .067E+006 6.423E+006 964.08 14.65 6.120E+ 0 05 4.883E+005 2 .808E+005 1 085.87 10 . 2 4 5.613E+005 -5.077E+005 2 .440E+005 1089.74 1. 73 3 .686E+006 1.243E+006 1 .62 6E+006 1 11 2 .07 13.69 3.959E+00 5 -3.583£+005 1.704E+005 121 2 .95 1. 43 4.433E+006 2 .669E+006 1.949E+006

[207]

1clide MDA Report 1 /31 /2 0 . 11:40:12 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/1 ) (pCi/1 ) (pCi/1 ) (pCi/1 ) Eu-15 2 1249.94 0.19 2 .917E+007 2.68E+005 -1.572E+007 1.2 5 6E+007 1299.14 1. 63 3 . 63 0E+006 4.817E+005 1.578E+006 1408.01 2 1. 07 2 .677E+005 8.457E+004 1.153E+005 1457.64 0.50 3.509E+007 7.989E+007 1.676E+007 1528.10 0.28 1. 2 60E+007 - 9.181E+006 4.882E+006 Eu-154 123.07 40.40 4. 2 94E+005 1.79E+005 2 .006E+005 2 .064E+005 247.93 6.89 1.443E+006 -7.487E+005 6.754E+005 591.76 4.9 5 1.455E+006 8.042E+005 6.566E+005 692.42 1. 78 3.987E+006 1.112E+006 1.793E+006 7 23 . 3 0 2 0.06 3.828E+005 1.688E+005 1.736E+005 756.80 4.52 1. 4 70E+006 -9.606E+005 6.556E+005 873.18 12.08 5.678E+005 2 .043E+005 2 .538E+005 996. 2 9 10.48 5.421E+005 -4.385E+005 2 .356E+005 1004.76 18.01 2 .654E+005 7.009E+004 1.121E+005 1274.43 34.80 1.785E+005 -1.602E+005 7.822E+004 1596.48 1. 80 3.353E+006 -4.049E+005 1.451E+006 Eu- 1 55 45.30 1. 31 8.367E+006 7.11E+005 -4. 2 00E+006 3. 92 8E+006 60.01 1. 22 1. 32 0E+007 3.780E+006 6. 32 7E+006 86.55 30.70 7.109E+005 5.411E+005 3.445E+005 105.31 21.10 8.443E+005 -5.002E+005 4.063E+005 Tl- 2 08 583.19 85.00 1.172E+005 1.17E+005 7.605E+004 5 .445E+004 Bi-211 351. 07 13.0 2 9.564E+005 9.56E+005 1.215E+006 4.527E+005 Pb-211 404.85 3.78 2 .368E+006 1 .90E+006 4. 2 00E+005 1.095E+006 42 7.09 1. 76 4.626E+006 - 1.186E+006 2 .120E+006 832.01 3.52 1.904E+006 1.902E+005 8.489E+005 Bi -212 39.86 1. 06 1. 2 62E+007 1.12E+006 2 .881E+006 5.995E+006 727.33 6.67 1.119E+006 4. 27 9E+005 5.056E+005 785.37 1. 1 0 7.590E+006 5.797E+006 3.468E+006 1 620.50 1. 4 7 3.247E+006 1 .637E+006 1.347E+006 Pb-212 1 15.18 0.60 2.976E+007 3.22E+005 - 1. 2 45E+007 1 .432E+007 2 38.63 43.60 3. 2 24E+005 1 .886E+005 1.539E+005 3 00.09 3.30 3.157E+006 -1.322E+006 1.480E+006 Pb212-XR 74.82 10.28 2.426E+006 1.35E+006 3.934E+006 1.181E+006

77. 11 17.10 1.351E+006 -1.033E+005 6.559E+005 87.35 3.97 5.410E+006 1.101E+006 2 .621E+006 89.78 1. 46 l.386E+007 - 1 .804E+005 6.699E+006 Bi-2 1 4 609. 32 45.49 2.490E+005 2 .49E+005 2 .819E+005 1.168E+005 768.36 4.89 1.461E+006 -2 .001E+006 6.569E+005 806.18 1. 2 6 5.774E+006 -l.509E+004 2 .601E+006 934.06 3.11 2 .502E+006 1. 25 4E+006 l.133E+006 1120. 2 9 14.9 2 6.133E+005 6.778E+005 2 .814E+005 1155. 2 1 1. 63 4.114E+006 5.422E+005 1.825E+006 1238. 1 2 5.83 l.113E+006 6.098E+005 4.911E+005 1280.98 1.43 4.956E+006 3.223E+006 2 .210E+006 1377.67 3.99 l .497E+006 1.228E+005 6.508E+005 1385.31 0.79 6.597E+006 - 9.259E+005 2 .806E+006 1 401. 52 1. 33 4. 2 37E+006 5.437E+004 1.824E+006 1 407.99 2.39 2 . 3 56E+006 7.443E+005 1.015E+006 1509.21 2.13 2 .411E+006 2 .561E+005 l.018E+006 1661.27 1.05 3.115E+006 -6.511E+005 l.166E+006

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1clide MDA Report 1/31 /2 0 _ 11:40:12 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/1 ) (pCi/ 1 ) (pCi/1 ) (pCi /1 ) Bi- 214 1729.59 2 .88 l. 2 79E+006 2 .49E+00 5 -2 .861E+005 4.954E+005 1 764.49 15.30 5 .039E+005 1.863E+005 2.247E+005 1847.43 2 .03 1.848E+006 6.154E+005 7.159E+005

 >               2 118.5 1      1.16    O.OOOE+OOO                      O.OOOE+OOO      O.OOOE+OOO Pb- 2 14     241.99       7. 2 5  1.8 2 1E+006   3 .50E+005       1.114E+005      8.667E+005 295.22      18.4 2   6.144E+005                      4.941E+005      2 .895E+00 5 351.93      35.60    3.499E+005                      4.455E+005      1.656E+00 5 785.96       1. 06   7.501E+006                      3.825E+006      3 .410E+006 Pb214-XR       74.8 2     5.80    4.300E+006     2 . 3 8E+006     6.972E+006      2 .093E+006 77.11      9.70    2.381E+006                    - 1.822E+005      1.156E+006 87.35      2 . 24  9.588E+006                      1. 951E+006     4.645E+006 89.78      0 .8 2  2 .467E+007                   -3. 2 12E+005     1.193E+007 Ra-226       186. 2 1     3 .64   3.597E+006     3.60E+006        1.792E+006      1.713E+006 Ac-228       12 9.07      2 .42   7.438E+006     3.63E+005        3.976E+006      3 .583E+006 2 0 9. 2 5   3.89    3.411E+006                      3.085E+006      l.625E+006 270. 2 4     3.46    2 .976E+006                   -1.286E+006      1. 3 95E+006 328. 00      2 .95  3 .193E+006                    -1.197E+006      1.485E+006 338. 32     11.27     9 .072E+005                     2.271E+004      4. 2 43E+005 409.46       1. 92  4 . 2 68E+006                  -2.422E+006      1.958E+006 463. 00      4.40   2 .026E+006                      7.789E+005      9.353E+005 794.95        4. 25  1.659E+006                       9.886E+005     7.445E+005 911.20      2 5.80   3.631E+005                       2.245E+005     1.674E+005 964.77        4.99   1.855E+006                      1.777E+006      8.534E+005 968.97      15.8 0   5.553E+005                      1.402E+005      2 .543E+005 1588.20        3. 22  1.685E+006                    - 1.459E+006      7.168E+005 Pa-2 31       27.36     10. 3 0  1. 4 78E+006   1.48E+006      - 6.282E+005      7.066E+005 283.69        1. 70  5.411E+006                    -1. 22 6E+006     2. 515E+006 300.07        2.47   4.217E+006                    -1. 766E+0 0 6    1.977E+006 302.65        2.20   4. 2 77E+006                  - 3 .647E+0 0 6   1.990E+006 330.06        1.40   7.039E+006                      5.366E+006      3 . 2 84E+006 Th-234         92.38       2.1 3  9.059E+006     9.06E+006      -2 .177E+006      4. 3 73E+006 92.80       2.10   9. 2 39E+006                    3 . 92 2E+004   4.460E+006 112.81        0. 2 1 8.165E+007                    -l.034E+007       3.923E+007 U- 235       1 43.76     10.96    1.414E+006     2 . 2 6E+005   -1.096E+006       6.778E+005 163.33       5.08    2 .482E+006                     2 .522E+005     1.179E+006 185.71      57.20    2.264E+00 5                     l.039E+005      1.078E+005 202.11       1. 08   1.094E+007                    -7.844E+006       5.181E+006 205.31       5.01    2 .579E+006                     6.925E+005      1. 22 7E+006 Am-24 1        59.54     35.90    4.414E+005     4.41E+005      -5.514E+004       2 .114E+005
    + = Nuclid e identified during the nuclide identification
    * = Energy line found in the spectrum
    >= Calculated MDA is z ero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Half-life too short to be able to perform the decay correction

[209]

***************************    ************************* ~**************
****        GAMM A         SP~ CTR UM          AN ALYS ~ S                            *****
"***********************************************************************
.lename: E:\0000 1 678.CNF
!port Generated On                4 /26/2017       5:55:44 PM 1mple  Title                       U2B306100AFJWC018GD tmple Description                 U 2 TB SUMP PIT tmple Identification tmple Type 1mple  Geometry iak Locate Threshold                3. 00 iak Locate Range (in channels )        85 -   8192

!ak Area Range ( in channels ) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mpl e Si ze 1.000E+OOO SQ METER tmple Taken On 2/29/2016 1 2 :00:00 PM

quisition Started 3/7/2016 10:09:34 AM

.ve Time 600.0 seconds !al Time 600.9 seconds !ad Time 0.16 % Energy Calibration Used Done On 1/27/2015 Efficiency Calibration Used Done On 4/11/2016 Efficiency ID TB VALVE PI T 1).,.\~ \la.\,do..\cc\ l..o~

~~

12-lo - 11 I\IC) [210]

iak Analysis Report 4/ 2 6/ 2 0 17 5 : 55 :4 5 PM Page 2

********************************* * ***************************************
****                P E A K        A N A L Y S I S               R E P O R T                 *****
*************************************************************************

Detector Name: 5456 Sample Title: U2B306 1 00AFJWC018GD Peak Analysis Performed on: 4/26/2017 5:55:44 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 2 95- 306 300.58 74.88 1.13 1.08E+00 2 78.87 5.76E+002 2 440- 447 44 2 .96 110.5 0 0.57 2 .72E+OOO 46.4 1 2 .64E+002 3 1396- 1414 1405.28 3 51. 2 0 1. 96 2 .40E+002 50.95 1. 2 1E+002 4 2322- 23 40 232 9.88 58 2 .38 1. 33 9. 2 7E+001 3 0 .44 4.13E+001 5 2 424- 2445 2 434. 62 608.56 1. 75 2 .43E+002 44.35 6.60E+001 6 2 633 - 2 654 2 643.68 66 0 .8 2 1. 46 4.45E+002 53.78 7.41E+001 7 4943 - 4 954 4948.90 1236.8 0 0.42 2 .80E+001 16.25 1.50E+001 8 58 23- 5850 5837.11 1458.59 0.95 3.61E+00 2 43.51 2 .46E+001 9 704 2- 7062 7052.7 2 1762. 0 3 1. 0 2 7.70E+001 19.47 4.96E+000

= First peak in a mul tiplet region
= Other peak in a mul tiplet region
= Fitted singlet

rors quoted at 2 .000 sigma

[211]

1terference Corrected Activ / Report 4/ 2 6/ 2 017 5 -, : 45 PM Page 3

N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title: U2B306100AFJWC018GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQ M) Uncertainty K-40 0.992 1460.82* 10.66 9.90112E+006 1. 46963E+006 Cs-1 3 7 0.999 661.66* 85.10 1 .37278E+006 2 .33907E+005 Tl -2 08 0.999 583.19* 85.00 2 .82532E+005 9.878 2 8E+004 Bi -2 11 1. 000 3 51.07* 13.0 2 4.51247E+006 1.20299E+006 Bi-214 0.377 609. 32

45.49 1.38991E+006 3 .03750E+005 768.36 4.89 806.18 1. 2 6 934.06 3 .11 11 2 0. 2 9 14.9 2 1155. 2 1 1. 63 1238.12* 5.83 l _35582E+006 7.94171E+005 1280.98 1. 43 1377.67 3 .99 1385.31 0.79 14 01. 52 1. 33 1407.99 2 .39 1509. 2 1 2 .13 1661.27 1. 05 1729.59 2 .88 1764.49* 15.30 1.55102E+006 4.11126E+005 1847.43 2 .03 2 118.51 1.16 Pb-214 0. 3 09 2 41. 99 7. 2 5 2 95. 22 18.4 2 3 51.93* 35.60 1.650 3 6E+006 4.38970E+005 785.96 1. 06

      * = Energy line found in the spectrum.
      @=Energy line not used for Weighted Mean Activity Energy Tolerance :         10.000 keV Nuclide confidence index threshold =             0. 3 0 Errors quoted at 2 .000 sigma

[212]

1terference Corrected Activ J Report 4 / 2 6/2017 5 *. : 45 PM Page 4

- - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 0.992 9.901119E+006 l.469630E+006 Cs-137 0.999 1.372778E+006 2.339068E+005 Tl -2 08 0.999 2.825 3 17E+005 9.878276E+004

  ?  Bi -2 11   1. 000      4.512468E+006        l .202994E+006 Bi-214     0.377       l.438936E+006        2.335058E+005
  ?  Pb-214     0.309       l.650360E+006        4.389701E+005
     ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at  2. 000 sigma

[213]

1terference Corrected Activ J Report 4/ 2 6/ 2 017 5 ; : 45 PM Page 5

 **********     U N I D E N T I F I E D       P E A K S        **********

Peak Locate Performed on: 4/26/2 017 5:55:44 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second % Uncertainty Type Nuclide 1 74.88 1.8038E-001 72.87 Tol. Pb214-XR Ba-133 Pb212-XR Pb2 1 2-XR Pb2 1 4-XR 2 110.50 4.53 1 9E - 00 3 1 7 0 6 . 65 Tol. Eu-155 Pb-212 Th-234 U235-XR M = First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [214]

1clide MDA Report 4/ 2 6/ 2 017 5:55:45 PM Page 6

- - - - * **************************************************************
    - N U C L I D E M DA R E P O R T *****

"****************************************************************************** Detector Name: 5 456 Sample Geometry: Sample Title: U2B306100AFJWC018GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) 1460.8 2

10.66 1.027E+006 l.03E+006 9.901E+006 4.765E+005

+      K-40 1 .085E+00 6 Cr-5 1       32 0.08      9.91   2 .249E+006      2 .25E+006 3 .7 5 8E+005 Mn-54        834.85     99.98    1.110E+005       l.11E+005 1. 2 65E+005       5.182E+004 Co-58        810.76     99.45    l.123E+005       1.12E+005 -4. 3 87E+004      5 . 22 4E+004 Co-60      1173. 2 3    99.85    1.480E+005       l.31E+005 l.160E+005         7.018E+004 1 33 2 .49   99.98    1.307E+005                      l.155E+005    6.145E+004 Nb-94        702.65     99.81    1.151E+005       1.15E+005 4.421E+004         5.397E+004 871. 09    99.89    1.150E+005                      3.354E+004    5.387E+004 Sn- 113      255.13       2 . 11 l . 1 04E+007    2 .52E+005 8.971E+006        5.362E+006 391. 70    64. 97   2 .517E+005                     4.675E+004    1. 2 05E+005 Cs-1 34      475.36       1. 48  l.011E+007       1.43E+005 -6.821E+006        4.820E+006 563.25       8. 3 4 1.576E+006                      1.657E+005    7.460E+005 569.33     15. 37   8 . 32 7E+005                 -5.099E+004     3 .935E+005 604.7 2    97. 62   2.33 1E+005                   - 9.038E+003    l. 12 9E+005 795.86     85.46    1.433E+005                    - 5. 2 64E+004  6.738E+004 801. 95      8.69   1. 2 87E+006                  -5. 3 19E+005   6.019E+005 1 038.61       0.99   9.003E+006                      3 .818E+005   4.123E+006 1167.97        1. 79  7.932E+006                      5.863E+006    3 .753E+006 1 365.19       3.02   2.445E+006                      1.779E+006    1 .093E+006
+      Cs-137       661. 66*   85. 10   1.776E+005       l.78E+005 1. 373E+006        8.464E+004 Eu -152      121. 78    2 8.67   l.201E+006       3.88E+00 5 -5.662E+005       5.887E+005 244.70       7.61   3.085E+006                    -1. 33 3E+006   1.501E+006 295.94       0.45   5.093E+007                      6.171E+007    2 .474E+007 344. 2 8   2 6.60   6.568E+005                      3.014E+005    3 .159E+005 367. 7 9     0 .86  l.893E+007                    - 9.000E+006    9.076E+00 6 411.12       2.24   7.291E+006                      3 .430E+005   3.494E+00 6 443.96       2 .83  5.655E+006                      2 . 3 42E+004 2.707E+00 6 488.68       0.42   3.133E+007                    -1.666E+006     l.485E+007 563.99       0.49   2.566E+007                    -l.750E+007     l.212E+007 586. 2 6     0.46   3.440E+007                    -1.772E+007     1.644E+007 678.62       0.47   2.260E+007                      1. 25 6E+007  1 .054E+007 688.67       0.86   1. 286E+007                   -5 .782E+00 5   6 .017E+006 719.35       0.28   4.155E+007                    -4.147E+007     l.949E+007 778.90     1 2 .96  8.843E+005                      3 .780E+005   4.143E+005 810.45       0.32   3.253E+007                      4.439E+006    1.514E+007 867.37       4.26   2.466E+006                      2 . 92 5E+004 l.148E+OO 6 919.33       0.43   2.215E+007                    - 1.201E+007    1.022E+007 964.08     14.65    9.435E+005                      1.019E+006    4 . 465E+00 5 1085.87      10. 2 4  1 .026E+006                   - 4.939E+005    4.761E+00 5 1089.74        1. 73  6.268E+006                      5.353E+006    2 .917E+00 6 1112.07      13.69    8.062E+005                    -2 .935E+006    3 .756E+00 5 1212.95        1. 43  7.601E+006                      4.606E+006    3 .533E+00 6

[215]

tclide MDA Report 4/26/2017 5:55:45 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Eu-15 2 1249.94 0.19 5.134E+007 3.88 E+00 5 4. 3 06E+007 2 . 3 64E+007 1299.14 1. 63 5.089E+00 6 -8. 3 28E+005 2 . 3 07E+006 1408.01 2 1. 07 3 .878E+00 5 3 . 2 45E+005 l.753E+005 1457.64 0.50 5.591E+007 2 . 2 40E+008 2 .717E+007 1528.10 0. 2 8 2 .524E+007 8. 6 65E+006 l.1 2 0E+007 Eu-154 123.07 40.40 8.356E+005 2 .74E+005 -5.92 6E+004 4.0 95E+005 247.93 6.89 3.205E+006 5. 22 4E+005 l. 55 6E+006 591. 7 6 4.95 2 .380E+006 -4.893E+005 l.119E+006 692.42 1. 78 6.266E+006 2 .760E+006 2.932E+006 723.30 2 0.06 6.284E+005 3 .804E+005 2.963E+005 756.80 4.52 2 .434E+006 -l.610E+006 l.137E+006 873.18 12.08 9.589E+005 2 .952E+005 4.493E+005 996. 2 9 10.48 l.053E+006 -1.008E+005 4.913E+005 1004.76 18.01 6.093E+005 3.197E+005 2 .840E+005 1 274.43 34.80 2 .742E+005 -l.594E+005 1. 26 0E+005 1596.48 1. 80 3 .143E+006 -9.078E+005 l. 3 46E+006 Eu-155 45.30 1. 31 1.577E+007 1.16E+006 -9.661E+006 7. 62 8E+006 60.01 1. 22 2 . 22 0E+007 -3.438E+006 l.082E+007 86.55 30.70 l.156E+006 - 3.774E+004 5 .67 2E +005 105.31 21.10 l.561E+006 7.540E+005 7.646E+005

+     Tl-208       583.19*  85.00    l. 2 64E+005    1. 2 6E+005    2 .825E+005   5.907E+004
+     Bi-211       351.07*  13.0 2   l. 3 03E+006    l. 3 0E+006    4.512E+006    6. 2 61E+005 Pb-211       404.85     3.78   4.223E+006      3 .10E+006   -4.768E+005     2.022E+006 427.09     1. 76  8.789E+006                     3.036E+006    4. 2 02E+006 832.01     3.52   3.104E+006                     l.059E+006    l.449E+006 Bi -212       39.86     1.06   l.850E+007      l.88E+006    -2.502E+006     8. 9 35E+006 727.33     6.67   l.878E+006                     7.700E+005    8.855E+005 785.37     1.10   l.115E+007                     l.154E+006    5.247E+006 1620.50      1. 4 7 4.594E+006                   -3.155E+005     2 .0 2 0E+006 Pb-212       115.18     0.60   5.797E+007      6.15E+00.5   -2.889E+007     2 .842E+007 238.63   43.60    6.153E+005                     9. 3 33E+005  3 .004E+005 300.09     3.30   6.067E+006                   -l.407E+007     2 .935E+006 Pb21 2-XR     74.82   10.28    3.938E+006      2 . 2 9E+006   7.969E+006    l.936E+006 77.11   17.10    2 .291E+006                  -1.077E+005     1.126E+006 87.35     3.97   8.931E+006                   -2 .498E+006    4.381E+006 89.78     1. 46  2 .414E+007                  -1.092E+006     l.184E+007
+     Bi- 2 14     609.32*  45.49    3.123E+005      3 .12E+005     l.390E+006    l.484E+005 768.36     4.89   2.713E+006                     l.085E+006    1. 28 3E+00 6 806.18     1. 2 6 8.619E+006                   - 8.476E+005    4.024E+00 6 934.06     3.11   3.736E+006                     3 .912E+006   l.750E+00 6 1120.29    14.92    l.010E+006                     l.227E+006    4.7 9 6E+00 5 1155.21      1. 63  7.081E+006                     1.176E+006    3.309E+00 6 1238.12*     5.83   l.113E+006                     1.356E+006    4.909E+00 5 1280.98      1. 43  6.437E+006                     2 .534E+006   2 .950E+00 6 1377.67      3.99   2.499E+006                     l.943E+006    1.152E+00 6 1385.31      0.79   9.939E+006                     4.806E+005    4.478E+00 6 1401.52      1. 33  6.401E+006                     3 .064E+006   2 . 906E+OO 6 1407.99      2 .39  3.410E+006                     2 .854E+006   1. 541E+00 6 1509.21      2 .13  3.463E+006                   -2 .689E+006    l.544E+00 6 1661.27      1. 05  4.591E+006                   - 2 .007E+006   l.904E+00 6

[216]

lClide MDA Report 4 /26/2 017 5:55:45 PM Page 8 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M)

+     Bi-2 14    1 729.59      2 .88  2 .447E+006      3 .1 2E+005   2 .023E+006 1.080E+006 1 764.49*    15. 3 0 3 .331E+005                    1.551E+006  1.393E+005 1 847.43      2 .03  3 .095E+006                    8.792E+004  1.339E+006 2 118.51      1.16   O.OOOE+OOO                     O.OOOE+OOO  O.OOOE+OOO
  >
+     Pb-214       2 41.99     7. 25  3.525E+006       4.77E+00 5    1.514E+006  1.718E+006 2 95. 22   18.42   1.240E+006                     1.781E+006  6 . 025E+005 351.93*    35.60   4.766E+005                     1.650E+006  2 . 2 90E+005 785.96      1.06   1.165E+007                     5.371E+006  5.487E+006 Pb214-XR       74. 82    5.80   6.979E+006       4.04E+006     1.413E+007  3.432E+006

77. 11 9.70 4.039E+006 -1.898E+005 1.985E+006

87. 35 2 . 24 1.583E+007 -4.428E+006 7.765E+006 89.78 0. 82 4. 2 98E+007 -1.944E+006 2 .108E+007 Ra-226 186. 21 3.64 7.222E+006 7.22E+006 8.433E+005 3 .525E+006 Ac-228 129.07 2 .42 1.363E+007 5.83E+005 9.740E+006 6 .678E+006 209. 2 5 3.89 6.444E+006 3.366E+006 3 . 1 41E+006 27 0 . 2 4 3.46 6.367E+006 9.498E+005 3 .090E+006 328.00 2 .95 6.089E+006 -1. 22 8E+006 2 .933E+006 338.32 11.27 1 .695E+006 1.651E+006 8.182E+005 409.46 1. 92 8.392E+006 - 4.859E+006 4.020E+006 463. 00 4.40 3 .514E+006 - 8.793E+005 1.679E+006 794.95 4. 2 5 2 .956E+006 5.133E+005 1.393E+006 911. 20 25.80 5.830E+005 7.963E+005 2 .773E+005 964.77 4.99 2 .755E+006 2.332E+006 1. 3 04E+006 968.97 15.80 8.180E+005 5.471E+004 3 .856E+005 1588.20 3 . 22 2 . 32 4E+006 9.522E+005 1.036E+006 Pa-2 31 27.36 10.30 2 .182E+006 2 .18E+006 - 6.332E+005 1.058E+006 283.69 1. 70 1.178E+007 3.257E+006 5 .700E+006 3 00 . 0 7 2 . 47 8 . 106E+006 -1.879E+007 3 .921E+006 3 02.65 2 . 20 8.975E+006 - 4.120E+006 4.340E+006 330. 0 6 l. 40 l .230E+007 -1 . 511E+007 5 . 914E+006 Th-2 3 4 92.38 2 . 13 1 .999E+007 2 .00E+007 1.580E+007 9.801E+006 92.80 2 . 10 2 .003E+007 -2 .446E+005 9.823E+006 112.81 0 . 21 1 . 954E+008 8.889E+007 9.575E+007 U-235 1 43.76 10 .96 2.743E+006 4.64E+005 -9.571E+005 1. 3 42E+006 163.33 5.08 5.402E+006 3 .100E+005 2 .639E+006 185.71 57. 2 0 4.637E+005 1.507E+005 2 .264E+005 2 02. 11 1. 08 2 .349E+007 -8.765E+006 1.146E+007 2 0 5 .31 5.01 4.967E+006 -2 .351E+005 2 .421E+006 Arn-24 1 59.54 35.90 7.482E+005 7.48E+ 0 05 1.379E+00 5 3 .648E+005

     + = Nuclide identified during the nuclide identification
     * = Energy l ine found in the spectrum
     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @    Half-life    too short to be able to perform the decay correction

[217]

**************************   *************************'        ****************
****         G A MMA     S P E C T R U M         A N A L Y S I S          *****
************************************************************************
.lename: C:\GENIE2K\CAMFILES\B306100AFJFC019GD.CNF iport Generated On                4/11/2016        8:56:35 AM tmple Title                       B306100AFJC019GD tmple Description                 TB ELEVATOR--stmP 1mpl e Identification tmple  Type 1mple  Geometry

!ak Locate Threshold 3.00 iak Locate Range (in channels ) 85 - 8192 !ak Area Range (in channels ) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mple Siz e 1.000E+OOO SQ METER tmple Taken On

quisition Started 3/3 0/ 2 016 1:08:28 PM

.ve Time 600.0 seconds !al Time 600.4 seconds !ad Time 0.06 'i:i Energy Calibration Used Done On 1/27/2015 Efficiency Calibration Used Done On 4/11/2016 Efficiency ID TB VALVE PIT [218]

iak Analysis Report 4/11/ 2 016 8:56:36 AI Page 2

*************************************************************************
****              P E A K        A N A L Y S I S            R E P O R T               *****
*************************************************************************

Detector Name: 5456 Sample Title: B306100AFJC019GD Peak Analysis Performed on: 4/11 /2 016 8:56:35 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 819 2 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV ) (keV) Area Uncert. Count s 1 2 431- 2 449 2 44 1. 57 610 . 3 0 0.60 6.79E+001 23 . 0 7 1.91E+001 2 5843- 5864 5853.48 14 62 .68 2 . 11 1.41E+00 2 2 5.53 5.62E+OOO

= First peak in a multipl et region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 . 000 sigma

[219]

1terference Corrected Acti ty Report 4/11/ 2 01 6 i6: 3 6 AM Page 3 ' ***********************************************************************

*** N UCLIDE I D E N T I F I C A T I O N R E P O R T *****

Sample Titl e : B306100AFJC019GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQ M) Uncertainty K-40 0.994 1460. 82

10.66 3 .87614E+006 7.76756E+005

       * = Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold =       0.30 Errors quoted at 2 .00 0 sigma

[220]

1terference Corrected Act: ty Report 4/11 /2 01 6 j6:36 AM Page 4

- - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

"*********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 0.994 3.876141E+006 7.767560E+005

      ?    Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2 .000 s igma
 **********      U N I D E N T I F I E D       P E A K s     **********

Peak Locate Performed on: 4/11/2016 8:56:35 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second % Uncertainty Type Nuclide 1 610. 3 0 1.1310E-001 34. 00 Tol. M First peak in a multiplet region m Other peak in a multiplet region F Fitted singlet Errors quoted at 2 .000 sigma [221]

1clide MDA Report 4/11/ 2 01 1 8:56:36 AM Page 5 "******************************************************************************

- - - N U C L I D E M D A R E P O R T *****

Detector Name: 5456 Sample Geometry: Sample Title: B306100AFJC0 1 9GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M)

+      K-40       1 46 0 .82* 10.66     4. 93 6E+005     4.94E+005 3 .876E+006         2 .097E +0 05 Cr - 51      32 0 .08     9.91   9.770E+005       9.77E+005 -5.123E+004         4.554E+005 Mn-54        834.85     99.98    7.083E+004       7.08E+004 3.123E+004          3.179E+004 Co-58        810.76     99.45    7.460E+004       7.46E+004 7.783E+00 3         3.366E+004 Co-6 0     1 17 3 . 23  99.85    7.288E+004       5.92E+004 -6 .861E+004        3. 2 64E+004 1332.49      99.98    5.924E+004                     - 1.8 2 9E+004  2 .575E+004 Nb-94        702.65     99.81    7.340E+004       7. 2 4E+004 8.980E+003        3.312E+004 871. 09    99.89    7. 2 37E+004                     1.750E+004    3.254E+004 Sn-113        255.13       2.11   5. 3 59E+006     1. 32E+005 -2 .618E+006       2 .528E+006 391.70     64.97    1. 32 2E+005                     4.215E+004    6 .094E+004 Cs-1 3 4      475.36       1. 48  5.879E+006       8.67E+004 9.847E+005          2 .707E+006 563. 2 5     8.34   8.180E+005                     - 2 .541E+005   3 .671E+005 569. 33    15.37    5.081E+005                       3.458E+005    2 . 3 13E+005 604. 72    97.62    9.571E+004                       3.504E+004    4. 42 5E+004 795.86     85.46    8.667E+004                       4.136E+004   3.911E+004 801 .95      8.69   7.537E+005                     -4.4 2 1E+005  3.353E+005 10 38.61        0.99   6.966E+006                       4.506E+006   3.106E+006 11 67.97        1. 79 4.275E+006                        1.045E+006   1 .926E+006 1 365 . 19      3.02  1.512E+006                     - 4.049E+005    6. 2 69E+005 Cs-137        661.66     85 . 10 9 . 2 03E+004     9 . 2 0E+004 -3.2 03E+004    4 o184E+004 Eu-152       121.78      2 8.67  5 .867E+005      2 .49E+005 -3.809E+005        2 .817E+005 2 44.70       7.61  1.501E+006                     -9.351E+005     7.087E+005 295.94        0.45  2.447E+007                     -1. 7 2 0E+006  1 .151E+007 344.28     2 6.60   3.085E+005                     -5.042E+005     1.418E+005 367.79        0.86  8.751E+006                     -6.585E+006     3 .989E+006 411.1 2      2 . 24 3.744E+006                     - 1 .385E+006   1. 72 1E+006 443.96       2 .8 3 2.889E+006                       4.830E+005    1. 32 4E+006 488.68       0.4 2  2.010E+007                       2 .255E+006   9. 232 E+006 563.99       0.49   1.459E+007                     -4.939E+005     6.585E+006 586. 2 6     0.46   2.166E+007                       2.370E+007    1.007E+007 678.62       0.47   1 .618E+007                    -1. 407E+007    7.335E+006 688.67       0.86   9. 2 71E+006                     4.052E+005    4. 2 21E+006 719.35       0. 2 8 2 .548E+007                      1.164E+007    1.146E+007 778.9 0    12 .96   4.003E+00 5                      5.650E+004    1. 72 3E+005 8 10 .45     0.32   2 .311E+007                      5.863E+006    1.043E+007 867.37       4.26   1.548E+006                       4.446E+005    6.885E+005 919.33       0.43   l.522E+007                     -1.154E+007     6.753E+006 964.08     14.65    4.749E+005                     -1.0 3 8E+005   2 .123E+005 1085.87       10. 2 4  7.033E+005                       5. 2 43E+00 5 3 .150E+005 1089.74         1. 73  3 .771E+006                    -2 .842E+006    1. 668E+OO 6 1 112.07      1 3.69   5.277E+005                       5.080E+004    2.364E+005 1212.95         1. 43  4.746E+006                       8.041E+005    2.106E+006

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4/11/201

8:56: 3 6 AM Page 6 1clide MDA Report Nucli de Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( 9s) (pCi/SQ M) (pCi/SQ M ) (pCi/SQ M) (pCi/SQ M)

Eu-152 1249.94 0.19 3.520E+007 2 .49E+005 -2 .152E+006 1.558E+007 1299.14 1. 63 3.630E+006 -3 . 29 9E+005 1.578E+006 1408.01 2 1.07 2 .493E+005 1.512E+005 1.060E+005 1457.64 0.50 3.318E+007 -8.417E+006 1.581E+007 1528.10 0. 2 8 9.743E+006 -3 .410E+006 3.452E+006 Eu-154 123.07 40.40 4.195E+005 1 .96E+005 2 .548E+004 2 .015E+005 247.93 6.89 1 .611E+006 -7. 32 1E+005 7.593E+005 591.76 4.95 1.477E+006 -1.760E+006 6.678E+005 692.42 1. 78 3.987E+006 -2 .225E+006 1.793E+006 723.30 2 0.06 3.661E+005 - 2 .806E+005 1.652E+005 756.80 4.5 2 1. 681E+006 3 .649E+005 7.611E+005 873.18 12.08 6.084E+005 2 .767E+005 2 .741E+005 996. 29 10.48 7.147E+005 3 .101E+005 3 . 22 0E+005 1004.76 18.01 4.027E+005 -2 .983E+005 1.807E+005 1274.43 3 4.80 1.959E+005 7.068E+004 8.694E+004 1596.48 1. 80 3 . 2 48E+006 1.068E+006 1.398E+006 Eu-15 5 45.30 1. 31 9.072E+006 7.45E+005 4.4 3 1E+006 4. 2 81E+006 60.01 1. 22 1.338E+007 1.641E+006 6.414E+006 86.55 30.70 7.447E+005 8.563E+005 3.615E+005 105.31 21.10 8.313E+005 - 5.157E+005 3.998E+005 Tl-2 08 583.19 85.00 1.181E+005 1.18E+005 8. 33 6E+004 5.491E+004 Bi-211 351. 07 13.0 2 9.690E+005 9.69E+005 1.178E+006 4.590E+005 Pb-211 404.85 3 .78 2 .432E+006 l.79E+006 l.915E+006 1.127E+006 427.09 1. 76 4.926E+006 2 .458E+006 2.270E+006 832.01 3.52 l.789E+006 -3.576E+005 7.916E+005 Bi -2 12 39.86 1. 06 9.316E+006 1.18E+006 -1.167E+006 4.342E+006 727. 33 6.67 1.184E+006 3 .531E+005 5.383E+005 785. 3 7 1.10 5.931E+006 2 .641E+006 2 .639E+006 1 620.50 1. 4 7 3.247E+006 - 7 .674E+005 l.347E+006 Pb-212 11 5.18 0 .60 3.320E+007 3.33E+005 1. 075E+007 l.604E+007 23 8.63 43.6 0 3.334E+005 3 .924E+005 1 .594E+005 300.09 3.30 3.157E+006 -1. 766E+006 1 .480E+006 Pb212-XR 74.82 10.28 2.487E+006 1. 3 6E+006 4.378E+006 1.211E+006

77. 11 17.10 1.363E+006 -2 .432E+005 6.619E+005 87.35 3.97 5.637E+006 1. 29 5E+006 2 .7 3 4E+006 89.78 1. 46 l.406E+007 - 4.417E+006 6.803E+006 Bi -2 14 609.32 45.49 2 .908E+005 2.91E+005 4.776E+005 1.377E+005 768.36 4.89 l.706E+006 - 3 .718E+004 7.793E+005 806.18 1. 26 5.585E+006 ~ . 2 78E+006 2 .507E+ 0 06 934.06 3.11 2 .574E+006 3 .855E+005 1.169E+006 1120.29 14.92 5.928E+005 6.951E+004 2 .712E+005 1155. 2 1 1. 63 4.447E+006 2 . 2 91E+006 1.992E+006 1 238.12 5.83 1 .302E+006 4.722E+00 5 5.854E+005 1 280.98 1. 43 4. 2 22E+006 1.003E+006 1.843E+006 1 377.67 3.99 1.540E+006 2.3 47E+005 6.721E+005 1385.31 0.79 8.553E+006 2 .637E+006 3.784E+006 1401.52 1. 33 3 .788E+006 4.567E+005 1.600E+006 1407.99 2 . 39 2 .194E+006 1.331E+006 9. 3 33E+005 1509.21 2 .1 3 2 .4 1 1E+006 -3 .807E+005 1.018E +0 06 1661.27 1. 05 3 .115E+006 8 . 68 1E+005 1.166E+006

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1clide MDA Report 4/11/ 2 01 8:56:36 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M ) (pCi/SQ M) Bi-2 14 1729.59 2.88 1 . 2 79E+006 2 .91E+00 5 - 6.854E+005 4. 95 4E+005 1764.49 15.30 4.941E+005 4.431E+005 2 .198E+005 1847.43 2 .03 2 .564E+006 3.633E+005 l.074E+006

 >               2 118.51       1.16   O.OOOE+OOO                   O.OOOE+OOO O.OOOE+OOO Pb- 2 14      2 41.99     7.25   2 .002E+006 3 .47E+005 2 .1 3 0E+006 9.571E+005 2 95.22   1 8.42   6.144E+005                   3.828E+005 2 .895E+005 351.93    35.60    3.468E+005                   2 .958E+005 1.641E+005 785.96      1. 0 6  6. 2 90E+006                 3 .634E+006 2 .805E+006 Pb214-XR       74.82      5.8 0  4.407E+006 2 .40E+006 7.759E+006 2 .146E+006 77.11     9.7 0  2.403E+006                 -4.287E+005 1.167E+006 87.35    2.24    9.991E+006                  2 . 2 96E+006 4.846E+006 89.78      0 .82  2 .504E+007                -7.864E+006 1. 2 11E+007 Ra-226       186. 2 1    3.64    3.508E+006 3.51E+006 5.870E+005 1.668E+006 Ac-228       129. 0 7    2.42    7.028E+006 3 . 33E+00 5 6.415E+005 3.378E+006 209.25      3.89    3.190E+006                 -1.119E+006 1.514E+006 2 7 0 .24   3.46    3.137E+006                 -9.065E+005 1.475E+006 32 8.00     2.95   3.522E+006                   1. 92 7E+006 1.649E+006 33 8. 32  11.27     8.322E+005                 -6.045E+004 3 .868E +005 409.46      1. 92   4.451E+006                -2 .470E+006 2 .050E+006 463. 00     4.40   1.824E+006                 - l.780E+006 8.344E+005 794.95      4.25   1. 743E+006                  1.499E+006 7.863E+005 911. 2 0  25 .80   3.333E+005                   1. 3 4 7E+005 1.525E+005 964.77      4.99   1 .395E+006                -1. 37 8E+006 6. 2 33E+005 968.97    15.80    4.407E+005                 -7. 12 9E+004 1.970E+005 1 5 88. 2 0   3. 22  1. 749E+006                -6.967E+004 7.486E+005 Pa-2 31        27.36   10. 3 0  l.095E+006 1.09E+006 2.515E+00 5 5.150E+005 283.69      1. 70  6.418E+006                 -1. 7 2 4E+006 3 .019E+006 300.07      2 .47  4. 2 17E+006               -2 . 3 59E+006 1.977E+006 3 02 .65    2 .20  4.374E+006                   6.140E+005 2 .039E+006 33 0 .06    1. 40  7.331E+006                   1.069E+006 3. 430E+006 Th- 23 4        92.38     2 .13  9.322E+006 9.32E+0 0 6 -1.617E+006 4.504E+006 92.80     2 .10  9.472E+006                   2 .767E+005 4.577E+006 112.81       0. 2 1 8.843E+007                   7.361E+006 4. 262 E+007 U-235        143.76     10.96    l.407E+006 2 . 2 6E+ 0 05 -7.299E+005 6.740E+005 163.33       5.08   2.658E+006                   5.777E+004 1. 2 67E+006 185.71     57.20    2.264E+005                   1. 32 6E+005 1.078E+005 2 02 .11    1. 08   1. 2 38E+007                 6.980E+005 5.899E+006 205.31      5.01    2 .551E+006                -4.973E+005 1. 2 13E+006 Am-24 1        59 . 54  35.90    4.451E+005 4.45E+ 00 5 - 7.960E+004 2 .13 2E+005
    + = Nuclid e identified during the nuclide identification
    * = Energy line found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Half-life too short to b e abl e to perform the decay correction

[224]

**************************~ ************************* ****************
"***         GAMM A       S P ~ C T R U M          ANALYS.1S                           *****
************************************************************************
.lename: C:\GENIE2K\CAMFILES\00001309.CNF
!port Generated On                 4/ 27/2 017        8:54: 0 8 AM Lmple  Title                       B306100AFJFC0,2.0GD   --

Lmple Description Lmpl e Identification 1mpl e Type tmple Geometry iak Locate Threshold 3.0 0 !ak Locate Range (in channels ) 85 - 8 1 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10.000 keV 1mple Si ze 1. 00 OE+O OO SQM 1mple Taken On 1 /7 /2 013 12:00:00 PM

quisition Started 4/7 /2 016 1:15:23 PM

.ve Time 660.0 seconds !al Time 660.6 seconds iad Time 0.09 % Energy Calibration Used Done On 1/13/20 1 5 Efficiency Calibration Used Done On 4/27/20 1 7 Efficiency ID UlEQDRN SUMP NEW l) at A \{ O. \ l dO. .\cJ 'o y' vJ4~ IJ~t ~lf I 110 [225]

ia k Analysis Report 4/27/2017 8:54:08 AM Page 2

- - - P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample Title: B306l00AFJFC0 2 0GD Peak Analysis Performed on: 4/27/2 017 8:54:08 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV ) Area Uncert. Counts 1 2 636- 2654 2 645.06 661.48 0.89 1. 3 9E+00 2 2 9.93 2 .54E+001 2 5829- 585 1 584 2 .06 1 460.78 1. 73 1.36E+00 2 2 6.14 8.79E+OOO

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2. 000 s igma

[226]

1terference Corrected Acti, y Report 4/27 /2 017 8 4:08 AM Page 3

- - - N U C L I D E I D E N T I F I C A T I O N REPORT *****

Sample Title: B3 06100AFJFC020GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQM) Uncertainty K-40 1. 000 1460.8 2* 10.66 5.00151E+006 1.05362E+006 Cs-137 1.000 661.66* 85.10 4. 2 0594E+005 1.03947E+005

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold          0. 3 0 Errors quoted at 2 .000 sigma

[227]

1terference Corrected Activ y Report 4 /27/2 017 8 1:08 AM Page 4 "***********************************************************************

- - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 5.001512E+006 1 .053624£+006 Cs-137 1. 000 4. 2 05941E+005 1.039465£+005

     ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .000 sigma
 **********    U N I D E N T I F I E D         P E A K S      **********

Peak Locate Performed on: 4/27/201 7 8:54:08 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified. [228]

iclide MDA Report 4/27/ 2 017 8: 5 4:08 AM Page 5

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Detector Name: 54 52 Sample Geometry: Sample Title: B306100AFJFC020GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) + K-40 1460.8 2

10.66 8.105E+005 8.11E+005 5.002E+006 3 .556E+005 Cr-51 32 0.08 9.91 4.747E+018 4.75E+018 -5.902E+017 2 . 2 14E+018 Mn-54 834.85 99.98 9.935E+005 9.93E+005 2 .643E+005 4.450E+005 Co-58 810.76 99.45 8.359E+009 8. 3 6E+009 3.697E+009 3 .778E+009 Co-60 1173.23 99.85 1.332E+005 l. 2 0E+005 5.812E+004 5.954E+004 133 2 .49 99.98 1. 2 01E+005 -9.651E+004 5.244E+004 Nb-94 70 2 .65 99.81 7.421E+004 6.62E +004 -4.035E+004 3.374E+004 871.09 99.89 6. 62 2E+004 3.827E+004 2.930E+004 Sn-11 3 255.13 2.11 4. 21 5E+009 1.46E+008 - 3.251E+008 1.999E+009 391.70 64.97 1.460E+008 1.336E+007 6.847E+007 Cs- 1 3 4 475.36 1. 48 1.565E+007 2 . 92 E+00 5 - 1.139E+006 7. 2 93E+006 563. 25 8.34 2 .396E+006 -l.101E+006 1.094E+006 569. 33 15.37 1.190E+006 - 6.534E+005 5.377E+005 604.7 2 97. 62 3 .234E+005 2.665E+005 1.523E+005 795.86 85.46 2 .915E+005 2 .065E+005 l.332E+005 8 01. 95 8.69 2 . 2 96E+006 -4.588E+004 1.024E+006 1038.6 1 0.99 2 .460E+007 2 .368E+007 l.102E+007 1167.97 1. 79 1.490E+007 -3.470E+005 6.689E+006 1365.19 3.02 7.854E+006 3.650E+006 3 . 429E+006

+ Cs-13 7 661.66* 85.10 1.005E+005 l.01E+005 4.206E+005 4.614E+004 Eu-152 121. 7 8 2 8.67 3.555E+005 3 .03E+005 -1.790E+005 l.713E+005 244.70 7.61 1.190E+006 -6.343E+005 5.677E+005 295.94 0.45 2 .006E+007 1.130E+007 9.510E+006 344.28 2 6.60 3.033E+005 7.972E+004 1 .421E+005 367.79 0.86 9.746E+006 2 .139E+006 4 . 566E+006 411.12 2 . 24 3 .659E+006 -2. 593E+005 1.703E+006 443.96 2 .8 3 3 .083E+006 1 .1 3 8E+006 1.436E+006 488.68 0.4 2 2 .019E+007 3.598E+006 9. 3 42E+006 563.99 0.49 1.617E+007 6.872E+005 7. 3 80E+006 586. 2 6 0. 46 2 . 3 27E+007 2.469E+007 1.086E+007 678.6 2 0.47 1.864E+007 -7.151E+006 8.495E+006 688.67 0.86 1.084E+007 -1. 2 44E+005 4.963E+006 719.35 0.28 2 .957E+007 -2 .922E+007 l. 3 34E+007 778.90 1 2 .96 5. 3 91E+005 -1. 3 12E+006 2 . 3 70E+005 810.45 0.32 2 .755E+007 1.133E+007 1. 2 43E+007 867.37 4.26 1.869E+006 -2 .713E+005 8.292E+005 919.33 0.43 1.714E+007 -1.621E+006 7.483E+006 964.08 14.65 8.629E+005 1. 2 67E+005 3 .987E+00 5 1085.87 10.24 9.355E+005 -3 .491E+005 4.172E+005 1089.74 1.73 5.761E+006 -1.131E+005 2 .580E+006 1 112.07 1 3 .69 6.8 2 1E+005 2 .501E+005 3 .027E+005 1212.95 1. 43 6.455E+006 8. 3 08E+005 2 .8 3 8E+006 [229]

4/27/2 0 17 8:54:08 AM Page 6 tclide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM } (pCi/SQM) (pCi/SQM ) (pCi/SQM) Eu-152 1249.94 0.19 5.420E+007 3.03E+005 3 .772E+007 2 .411E+007 1 299.14 1.63 5.292E+006 -l.743E+006 2 . 29 0E+006 1408.01 2 1.07 4.303E+005 -9.704E+004 1.862E+005 1 457.64 0.50 5 .598E+007 1.351E+008 2 .675E+007 1528.10 0.28 2 .032E+007 -5.393E+006 7.873E+006 Eu-154 123.07 40.40 2 .779E+005 2 .60E+005 8.360E+004 1.339E+005 247.93 6.89 1.357E+006 - 1.536E+005 6.449E+005 591.76 4.95 1.678E+006 -1.452E+005 7.599E+005 692.42 1. 78 5.848E+006 2 .441E+006 2 .680E+006 723.30 2 0.06 5.313E+005 1.762E+005 2 .435E+005 756.80 4. 52 2 .162E+006 -1. 3 04E+005 9.804E+005 87 3 .18 12.08 7.123E +005 1.136E+004 3 .152E+005 996.29 10.48 9.710E+005 - 2 .582E+005 4.340E+00 5 1004.76 18.01 5. 23 9E+005 5.041E+004 2 .318E+00 5 1 274.43 34.80 2 .603E+005 -3.152E+005 1 .121E.+ 005 1 596.48 1. 80 5.464E+006 -1. 3 08E+006 2 . 32 5E+006 Eu-155 45.30 1. 31 1.734E+007 6.67E+005 -6.107E+006 8. 23 1E+006 60.01 1. 22 2 .237E+007 3 .742E+006 1.072E+007 86.55 30.70 6.666E+005 4.542E+005 3.230E+005 105.31 21.10 7. 3 49E+005 -5 .894E+004 3.544E+005 Tl - 2 0 8 583. 1 9 85.00 1.092E+005 1. 0 9E+005 9.195E+004 5.108E+004 Bi -2 11 351. 07 1 3 .02 6.328E+005 6.33E+005 8.342E+005 2 .997E+005 Pb-21 1 404.85 3 .78 1.830E+006 1.83E+006 1.842E+005 8.521E+005 427.09 1. 76 4.302E+006 2.177E+006 2 .011E+006 832.01 3.52 1.870E+006 -6.651E+005 8. 2 95E+005 Bi-212 39.86 1. 06 1.246E+007 1. 2 6E+006 1.117E+006 5.890E+006 727.33 6.67 1. 2 61E+006 9.760E+005 5.793E+005 785.37 1.10 6. 2 41E+006 -1.524E+006 2.795E+006 1 620.5 0 1. 47 5.196E+006 4.623E+005 2.2 1 0E+006 Pb-212 115. 1 8 0.60 1.599E+007 1.91E+005 l.148E+007 7.723E+006 238.63 43.6 0 1.915E+005 2 .134E+005 9.172E+004 300.09 3.30 2 .076E+006 -1.725E+006 9.780E+0 0 5 Pb212-XR 74.82 10 . 28 1.704E+006 9.35E+005 2 . 1 36E+006 8.280E+005 77.11 17.1 0 9.345E+005 2 .757E+005 4.536E+005 87.35 3 .97 3.143E+006 1.841E+006 1.523E+006 89.78 1. 46 7.811E+006 -5 .594E+006 3.776E+006 Bi-214 609.32 45.49 2 .603E+005 2 .60E+00 5 3 .272E+005 1. 2 34E+005 768.36 4.89 1.699E+006 1.150E+006 7.773E+005 8 0 6.18 1. 2 6 5.533E+006 -8 .777E+005 2 .478E+006 934.06 3 .11 2 .420E+006 -1. 803E+006 1.082E+006 1120.29 14.92 7.049E+005 1. 639E+005 3 . 2 2 4E+005 1155.21 1. 63 5.738E+006 5.898E+005 2 .589E+006 1 238.12 5.83 1.649E+006 5.103E+005 7.430E+005 1 280.98 1. 43 5.762E+006 9.499E+005 2 .542E+006 1377.67 3 .99 2.013E+006 6.980E+005 8.788E+005 1385.31 0.79 8.647E+006 1.614E+006 3 .678E+006 1401.52 1. 33 3.756E+006 - 6.446E+006 1.490E+006 1407.99 2 .39 3.212E+006 - 7. 2 42E+005 1.390E+006 1509.21 2 .13 2 .828E+006 1. 3 18E+006 1.159E+006 1661 .27 1. 05 4.413E+006 -4.851E+006 1.652E+006 [230]

1clide MDA Report 4 /27/2017 8:54:08 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (% ) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Bi- 2 14 1729.59 2 .88 2 .557E+006 2 .60E+005 1. 3 81E+006 l.071E+006 1764.49 1 5 .30 7.464E+005 7.025E+005 3 . 33 6E+005 1847.43 2 .03 3 .789E+006 2 . 0 46E+006 1.587E+006

 >               2118.51       1.16 O.OOOE+OOO                    O.OOOE+OOO     O.OOOE+OOO Pb-214      241.99       7. 2 5 l.175E+006 2 .32E+005 l.125E+006           5.629E+005 295. 22   1 8.4 2 4.115E+005                    1.902E+005     1.950E+005 35 1. 93   35.60 2 . 32 1E+005                  2 .854E+005    1 . 099E+005 785.96       1. 06 6.501E+006                   1.687E+006     2 .912E+006 Pb214-XR      74.82     5.80 3.024E+006 1.65E+006 3 .791E+006              1.470E+006 77.11      9.70 1 .650E+006                   4.867E+005     8.007E+005 87.35     2.24 5.578E+006                     3 . 2 68E+006  2 .702E+006 89.78     0 .82 1.393E+007                  -9.974E+006      6.732E+006 Ra-226      186. 2 1    3.64 2.132E+006 2 .13E+006 4.004E+005             1 .023E+006 Ac-228      1 2 9.07    2.42 3.522E+006 3.57E+005 -2 . 2 68E+006          1.697E+006 2 09. 2 5   3.89 1.985E+006                    1.169E+006      9.499E+005 2 7 0.24    3.46 2 .036E+006                   1.056E+006     9.640E+005 328. 00     2.95 2 .077E+006                 - 1.979E+006     9.678E+005 338.32    11. 27 6. 2 96E+005                - 3 .443E+005    2 .959E+005 409.46      1. 92 3 .629E+006                  8.126E+005     1.690E+006 463.00      4. 40 1.724E+006                 - 6.990E+005     8.033E+005 794.95      4.25 2 .039E+00 6                  1.843E+006     9.348E+005 911.20    2 5.80 3 .567E+005                   1. 2 09E+004   1.632E+005 964.77      4.99 2 .146E+006                   1.077E+006     9.916E+005 968.97    15.80 6.735E+005                     7.016E+005     3.109E+005 1588.20       3 . 22 2 .512E+006               -1.612E+005      1.082E+006 Pa-23 1      2 7.36   10. 3 0 1.007E+006 1.01E+006 8.709E+005             4.688E+005 283.69      1. 70 3 .757E+006                -7.785E+005      1 .765E+006 300.07      2 .47 2 .774E+006                -2 . 3 05E+006   1 . 3 07E+006 302.65      2 . 2 0 3.080E+006                 1.075E+006     l.449E+006 330. 0 6    1. 40 4.766E+006                   l , 387E+006   2 . 23 3E+006 Th-234        92.38      2 .13 3 .405E+021 3 . 41E+02 1 1.763E+0 2 1       l.646E+0 2 1 92.8 0     2 .10 3 .456E+0 2 1                3.367E+0 2 1   1.670E+0 2 1 112.81       0.21 2 .866E+0 22                -1.200E+0 22     1.382E+022 U- 235      143.76     10.96 7.096E+005 1.37E+005 -l.150E+005              3.409E+005 163.33       5.08 1.434E+006                    9.760E+004     6.869E+005 185.7 1    57.20 1.374E+005                     5. 3 02E+003   6 . 595E+004 202. 1 1    1. 08 6.372E+006                  -4.778E+006      3.035E+006 205.31      5.01 1.383E+006                     1. 373E+005    6.587E+005 Am-2 41       59.54    35.90 4.708E+005 4.71E+005 -3 .201E+005             2 . 2 54E+005
    + = Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calcul a ted
    @ = Half-li fe too short to be able to perform the deca'l correction

[231]

"*************************** *************************; **************
****         GAMM A        SP t CTR UM           AN ALYS IS                    *****
************************************************************************
.lename: C:\GENIE2K\CAMFILES\00001 3 17.CNF iport Generated On                4 /2 7/2017       8:56:01 AM tmple Title                       B306100AFJWC21GD tmple Description                 UNIT 2 EQ DR1TsuMP tmple Identification Lmple Type tmple Geometry iak Locate Threshold                3 .00 iak Locate Range (in channels)         85 -     8 1 92 iak Area Range (in channels)           85 -     8 1 92 lentification Energy Tolerance        10.000 keV tmple Size                          1.000E+OOO SQ METER tmple Taken On

quisition Started 4/11/ 2 016 1:4 2 :0 2 PM

.ve Time 660. 0 seconds ial Time 660.9 seconds iad Time 0. 1 4 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/27/2017 Eff i ciency ID UlEQDRNSUMP NEW Do.+tt Va/idaJ~j b

                                                               ~~r l~-t ... /';' .

II JO [232]

iak Analysis Report 4/ 2 7/ 2 017 8 : 56: 01 AM Page 2

*************************************************************************
****                P E A K        A N A L Y S I S              R E P O R T                  *****
*************************************************************************

Detector Name: 54 5 2 Sample Title: B306100AFJWC21GD Peak Analysis Performed on: 4/27 /2 01 7 8:56 :00 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. s tart end centroid (keV ) (keV) Area Uncert. Counts 1 2 92- 305 300.61 74.81 0.39 1.34E+002 4 9. 4 6 1.70E+00 2 2 843 - 851 846.98 2 11.57 0.61 2 .41E+001 18.56 2 .89E+001 3 2 430 - 2443 2436. 2 1 609.23 1. 01 5. 1 4E+001 17.94 1.06E+001 4 2 637- 2 65 2 2644.65 66 1. 37 1.29 1.15E+00 2 27.15 2 .33E+001 5 3636- 3647 3641.49 910 .69 0.53 2 . 3 0E+001 13.91 1.00E+OOl 6 5829- 5850 5840.51 1460.39 1.17 l. 1 1E+00 2 29. 11 2 .67E+001 First peak in a multiplet region Other pea k in a multiplet region

= Fitted singlet

rors quoted at 2 . 000 s igma

[233]

1terference Corrected Activ: Report 4/27/20 17 8: ' '. 01 AM Page 3

- - - - * **********************
    - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Titl e : B306100AFJWC21GD Nuclide Libr ary Used: C:\GENIE2K\CAMFILES\ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQ M) Uncertainty K-40 1. 000 1460.82* 1 0.66 4.08539E+0 0 6 1.12601E+006 Cs-137 1. 000 661.66* 8 5 .1 0 3. 2 2903E+0 0 5 8.57254E+004

      * = Energy line found in the spectrum.
      @=Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold =        0.30 Errors quoted at 2.000 sigma

[234]

1terference Corrected Activi Report 4/ 2 7 /2 01 7 8: ' 01 AM Page 4

- - - - * *******************************************************
    - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQ M) Uncertainty K-40 1. 000 4.085 39 1E+006 l.126014E+006 Cs-137 1. 000 3 . 229 0 27E+005 8.572540E+004

      ? = Nuclide is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .00 0 sigma
 **********     U N I D E N T I F I E D             P E A K S        **********

Peak Locate Performed on: 4/27/2 01 7 8:56: 00 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second % Uncertainty Type Nuclide 1 74. 81 2 .0 25 4E- 001 37. 00 To l . Pb214-XR Ba-133 Pb212-XR Pb212-XR Pb214-XR 2 2 11.57 3. 656 4E-00 2 76.92 Tol. Th-227 Ac-228 U-235 U-235 3 609. 23 7.7823E- 00 2 3 4 . 93 Tol. Zr-97 Sb-125 Sb-125 Cs-134 Bi-214 5 910 .69 3 . 4780E- 0 02 6 0. 62 Tol. Eu-152 Ac-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [235]

1clide MDA Report 4/27/ 2 017 3:5 6 :01 AM Page 5

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    - N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample Title: B306100AFJWC21GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M)

+      K-40       1460.8 2

10 .66 1. 3 11E+006 1. 3 1E+006 4.085E+006 6.056E+005 Cr-5 1 320.08 9.91 6.618E+005 6.62E+005 -6.987E+004 3.101E+005 Mn-54 834.85 99.98 7.854E+004 7.85E+004 2.681E+004 3.555E+004 Co-58 810.76 99.45 7.648E+004 7.65E+004 -8.139E+00 2 3.457E+004 Co-60 117 3 . 23 99.85 9.893E+004 9.89E+004 2 .216E+004 4.486E+004 1 332 .49 99.98 l.005E+005 -8.963E+00 3 4.527E+004 Nb-94 70 2 .65 99.81 7.616E+004 7.62E+004 4.502E+004 3.471E+004 871. 09 99.89 8.174E+004 5.588E+00 3 3.706E+004 Sn- 1 13 255.13 2 .11 3.131E+006 9.86E+004 -8.610E+005 l.479E+006 391.70 64.97 9.863E+004 1.657E+004 4.573E+004 Cs-134 475.36 1. 48 5.375E+006 9.19E+004 3 . 3 14E+006 2 .509E+006 563.25 8.34 8 .814E+005 1. 4 68E+005 4.055E+005 569.33 15.37 4. 2 90E+005 -2 .673E+005 1.953E+005 604.72 97.62 1.041E+005 -7.520E+004 4.889E+004 795.86 85.46 9.192E+004 4.680E+004 4.174E+004 80 1 .95 8.69 9.568E+005 4.084E+005 4. 36 6E+005 1038.61 0.99 7.653E+006 1 .016E+006 3 . 39 6E+006 1167.97 1. 79 5.345E+006 3 . 33 1E+006 2 .416E+006 1 365.19 3.02 2 .158E+006 - l.031E+006 9.114E+005

+ Cs-137 661.66* 85.10 8 .492E+004 8.49E+ 0 04 3. 22 9E+005 3.865E+004 Eu-1 52 12 1. 7 8 28.67 3. 023E+005 2 .49E+005 -1.661E+005 l.457E+005 2 44.70 7.61 8.438E+005 -1.041E+006 3 .986E+005 2 95.94 0.45 l.769E+007 l.132E+007 8.402E+006 344. 2 8 26.60 2 .487E+005 -2 .618E+005 1.163E+005 3 67.79 0 .86 7.829E+006 l.582E+006 3 .655E+006 411.1 2 2.24 3 .075E+006 -9.564E+005 1.430E+006 44 3 .96 2.83 2 .323E+006 -3 .797E+004 1.073E+006 488.68 0.42 l.799E+007 -3 .805E+006 8.355E+006 563.99 0.49 1.451E+007 3 . 2 89E+006 6.659E+006 586. 2 6 0.46 1.813E+007 -1.080E+006 8.410E+006 678.62 0.47 l.578E+007 - 2 .831E+006 7.194E+006 688.67 0.86 8.052E+006 - 5.420E+006 3 .639E+006 719.35 0. 2 8 2 .898E+007 5.637E+006 1.327E+007 778.90 12.96 5 .903E+005 -2 .644E+005 2 .676E+005 810.45 0.32 2 . 3 69E+007 -4.411E+006 1.071E+007 867.37 4.26 1.885E+00 6 -1.930E+006 8.532E+005 919.33 0.43 1.861E+007 2 .383E+006 8.383E+006 964.08 14.65 6.889E+005 8 .032E+005 3 .167E+00 5 1085.87 10.24 7.445E+005 -5 .510E+005 3. 29 4E+005 1089.74 1. 73 4.513E+006 2 .762E+006 2 .003E+006 111 2 .07 13.69 5 .653E+005 -6.936E+005 2 .501E+005 1 21 2 .95 1. 43 5 .852E+006 1.887E+006 2 .596E+006 [236]

1clide MDA Report 4/27/2017 8:56:01 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Eu-15 2 1249.94 0.19 4.682E+007 2 .49E+005 - 1.709E+007 2 .088E+007 1299.14 1. 63 5.001E+006 - 5.941E+005 2 .199E+006 1408.0 1 21. 07 3.862E+005 1. 509E+005 1.686E+005 1457.64 0.50 4.682E+007 1.151E+008 2.236E+007 1 52 8.10 0. 2 8 1.878E+007 7.164E+006 7.454E+006 Eu-154 123.07 40.40 2 . 1 43E+005 2 .14E+005 1.305E+005 1.033E+005 247.93 6.89 8.929E+005 3.641E+005 4. 2 05E+005 591. 76 4.95 1.434E+006 9.063E+005 6.560E+005 692.42 1. 78 3.963E+006 4.591E+005 1.794E+006 723.30 20.06 3.902E+005 1.302E+005 1.781E+005 756.80 4.52 1.711E +006 6.038E+005 7.779E+005 873.18 12.08 6.863E+005 4.955E+005 3.116E+005 996. 2 9 10.48 7.190E+005 2 .711E+005 3. 198E+005 1004.76 18.01 4.907E+005 -2 .404E+005 2 .221E+005 1274.43 34.80 2 .418E+005 6.427E+004 1.070E+005 1596.48 1. 80 4.365E+006 1.498E+006 l.869E+006 Eu-155 45.30 1. 31 9.453E+006 4. 2 8E+005 -6.699E+006 4.452E+006 60.01 1. 22 1.336E+007 -2 .714E+006 6.392E+006 86.55 30.70 4.277E+005 3.687E+005 2 .074E+005 105.31 21.10 4.852E+005 -1.052E+004 2 .345E+005 Tl -2 08 583.19 85.00 1.040E+005 1.04E+005 3.953E+004 4.850E+004 Bi-2 11 351. 07 13.02 7.054E+005 7.05E+005 1.172E+006 3.360E+005 Pb-211 404.85 3.78 1.760E+006 1.76E+006 1.077E+006 8.170E+005 427.09 1. 76 4. 52 6E+006 3.023E+006 2 .123E+006 8 32 .01 3.5 2 1.909E+006 -2 .713E+006 8.490E+005 Bi-212 39.86 1. 06 1.246E+007 1. 1 0E+006 -2.606E+006 5.890E+006 727.33 6.67 1.102E+006 -6.645E+004 4.997E+005 785.37 1.10 7.170E+006 1.066E+006 3. 2 60E+006 1620.50 1. 47 5.393E+006 1.492E+006 2.309E+006 Pb-212 115.18 0.60 1 .633E+007 2 .06E+005 6.512E+006 7.892E+006 2 38.63 43.60 2 .059E+005 2 .630E+005 9.895E+004 3 00.09 3.3 0 2 .173E+006 -2 .340E+006 1.026E+006 Pb212-XR 74.82 10. 2 8 1.781E+006 9.59E+005 3 .652E+006 8.667E+005 77.11 17.10 9.587E+005 7.539E+004 4.656E+005 87.35 3.97 3.235E+006 3 . 1 45E+006 1. 568E+006 89.78 1. 46 7.955E+006 -2.168E+006 3.848E+006 Bi-2 14 609. 32 45.49 2 .269E+005 2 . 2 7E+005 3 .154E+005 1.067E+005 768.36 4.89 1.971E+006 1.970E+006 9.134E+005 806.18 1. 26 6.677E+006 4.370E+006 3.051E+006 934.06 3.11 2.505E+006 1.378E+006 1.124E+006 1120. 2 9 14.92 7.891E+005 5.401E+005 3.645E+005 1155. 2 1 1. 63 5.063E+006 5.418E+005 2 .252E+006 1238.12 5.8 3 1 .749E+006 -8.655E+005 7.932E+005 1 280.98 1. 43 5.754E+006 2.961E+006 2 .538E+006 1377.67 3.99 2.168E+006 4.740E+005 9.563E+005 1385.31 0.79 9.867E+006 4.761E+005 4. 2 89E+006 1401. 52 1. 33 5.755E+006 2 .452E+006 2 .490E+006 1407.99 2.39 3.399E+006 1. 32 8E+006 1 .484E+006 1509.21 2.13 3.663E+006 1. 2 69E+006 l.577E+006 1661.27 1. 05 5. 367E+006 - 4.196E+006 2 .129E+006 [237]

1clide MDA Report 4 /2 7/ 2 017 8:56:01 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) {%) (pCi/SQ M) {pCi/SQ M) (pCi/SQ M) (pCi/SQ M) Bi -2 14 17 29 . 5 9 2 .88 2 .161E+006 2 . 2 7E+005 9.193E+005 8.7 3 1E+005 1764.49 15.3 0 7.170E+005 4. 12 2E+005 3 .189E+005 1847.4 3 2 .03 3 .409E+006 1.589E+006 1. 3 97E+006

 >                21 18.51      1.16    O.OOOE+OOO                      O.OOOE+OOO O.OOOE+OOO Pb- 2 1 4    2 41.99     7.25    1.160E+006 2 .50E+005 9.453E+00 5 5.559E+005 2 95. 22   18.42    4.178E+005                   - 8.592E+004 1.982E+005 351.93     35.60    2 .501E+005                    2 . 2 60E+005 1.189E+005 785.96      1. 06   7.654E+006                     4. 3 27E+ 00 6 3 .489E+006 Pb214-XR       74.82     5.80    3 .157E+006 1.69E+006 6.473E+006 l .536E+006

77. 11 9.70 1.690E+006 1.329E+005 8.209E+005 87.35 2 . 24 5.733E+006 5.575E+006 2 .780E+006 89.78 0 .82 1.416E+007 -3 .861E+006 6.851E+006 Ra- 226 186. 2 1 3 .64 2 . 2 60E+006 2 . 2 6E+006 1. 52 0E+006 1.087E+006 Ac- 2 2 8 129. 0 7 2 .42 3 .420E+006 4. 3 8E+005 - 7.734E+005 1.646E+006 209.25 3 .89 1.839E+006 - 1.513E+005 8.768E+005 270.24 3 .46 2 .090E+006 8.430E+005 9.907E+005 328.00 2 .95 2 .544E+006 2 .748E+005 1. 2 01E+006 338.32 11.27 6. 938E+005 3.388E+005 3 . 28 0E+005 409.46 1. 92 3 .490E+006 -2 .427E+006 1. 620E+006 463.00 4.40 1.605E+006 -4.519E+005 7 .437E+005 794.95 4.25 1.847E+006 -5.872E+005 8.387E+005 911.20 25.80 4.385E+005 4.099E+005 2 .041E+005 964. 77 4 . 99 2.024E+006 2 .329E+006 9.302E+005 968.97 15.80 6.541E+005 6.443E+005 3.012E+005 1588.2 0 3 . 22 2.512E+006 9.621E+005 1.082E+006 Pa - 2 31 27.36 10.30 8.098E+005 8.10E+005 4.101E+005 3.700E+005 283.69 1. 70 3.800E+006 1 .906E+006 1.787E+006 300.07 2.47 2.903E+006 - 3.127E+006 1. 3 71E+006 302.65 2.20 3.163E+006 - 1.315E+006 1. 490E+006 330.06 1. 40 5.326E+006 2 .192E+006 2 .513E+006 Th-234 92.38 2. 1 3 5.331E+006 5.33E+006 4.963E+005 2 .578E+006

92. 80 2.10 5.401E+006 1 . 762E+006 2 .612E+006 112.8 1 0. 2 1 4.766E+007 2 .891E+007 2 .305E+007 U-235 143.76 10.96 6.994E+005 1.44E+005 -2 .863E+00 5 3 . 35 8E+005 163.33 5. 0 8 1 .565E+006 1.584E+006 7.525E+005 185.71 57. 2 0 1.437E+005 1.422E+005 6.909E+004 202.11 1. 08 6.984E+006 5 .192E+006 3.341E+006 2 05.31 5.01 1.449E+006 -2 .960E+005 6.915E+005 Am- 2 41 59.54 35.90 4.604E+005 4.60E+005 7.031E+003 2 . 2 02E+005

    + = Nuc lide identified during the nuclide identification

Energy line found in the spectrum

    > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Half-life too short to be abl e to perform the decay correction

[238]

*************************~ *************************~ k****************
****         GAMM A       S P E C T R U M         A N A L Y S I S             *****
************************************************************************
.lename: 54 52

!port Generated On 4/ 1 9/2016 12:44:43 PM

~~

tmpl e Title B306100AFJFC02ZGD tmple Description TB 560 ~ tmple Identification tmple Type tmple Geometry !ak Locate Threshold 3 .00 !ak Locate Range (in channels ) 85 - 8192 !ak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Size 1.000E+OOO SQM tmple Taken On

quisition Started 4/19/2016 1 2: 34:42 PM

.ve Time 600.0 seconds !al Time 600.3 seconds iad Time 0.04 ~~ Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/14/20 1 6 Efficiency ID TBFLOOR

                                                                ~Qtd VaJ,*cfa.~,J kJ
                                                                 ~                 lY I,_ t. ~IF
                                                                 /Ila

[239]

iak Analysis Report 4/19/2 0 16 12 :44:4 3 Ph Page 2

- - - P E A K A N A L Y S I S R E P O R T *****

"************************************************************************ Detector Name: 54 52 Sample Title: B306100AFJFC0 2 3GD Peak Anal y sis Performed on: 4/19/ 2 0 1 6 12:44:42 PM Peak Analysi s From Channel: 85 Peak Analysi s To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid ( keV) (keV ) Area Uncert. Counts 1 297- 306 300.61 74.81 0.7 2 4.24E+001 32 .75 9.76E+001 2 332- 346 340.14 84.7 0 0.40 2 .18E+001 36.50 1.07E+00 2 3 1400- 1414 1407.57 351. 86 0. 72 2 .96E+001 19.99 2 .44E+001 4 1958 - 1967 1962.49 490.72 0.46 8.77E+OOO 7.56 2 .23E+OOO 5 2 430 - 2 441 2 435.15 608.97 1. 06 3 .23E+001 15. 05 9.70E+OOO 6 2 635- 2 651 2 645. 29 66 1. 53 1. 32 9 .52E+001 22 . 22 8.76E+000 7 5323- 5334 5328.14 13 32 . 3 5 0.47 1.14E+001 10.15 5.62E+OOO 8 5830- 5848 5839.16 1460.06 0.86 8.88E+001 19.60 2 . 2 3E+OOO First peak in a multipl et region

=  Other peak in a multiplet region

= Fitted singlet -rors quoted at 2.000 sigma [240]

1terference Corrected Acti .ty Report 4/ 1 9 /2 016 l L 44:4 3 PM Page 3 "***********************************************************************

- - - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

"*********************************************************************** Sample Title: B306100AFJFC023GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB

 . . . . . .. . .. . . . . . . . . . . IDENTIFIED NUCLIDES             ............... . ....

Nucl ide Id Energy Yield Activity Acti vi t: 1 Name Confidence (keV) (%) (pCi/SQM ) Uncertainty K-40 0 .999 1460.82* 10.66 6.05122E+00 5 1. 43591E+005 Ba-13 3 0 .579 79.61* 2 . 65 3 .79592E+00 5 3 .03 32 8E+005 81.00* 32.90 1.57523E+004 2 .65196E+004 276.40 7.16 30 2 .85 18.34 356. 01

62.05 1. 71608E+004 1.19050E+004 383.85 8.94 Cs - 137 1. 000 661.66* 85.10 5. 523 83E+004 1.44948E+004

        * = Energy l ine found in th e spectrum.
        @ = Energy line not used for Weighted Mean Activi t r Energy Tolerance :                   10.000 keV Nuclide confidence index threshold=                        0. 3 0 Errors quoted at 2 . 000 sigma

[241]

1terference Corrected Acti .ty Report 4/ 1 9/ 2 01 6 1~ 44:43 PM Page 4 "*********************************************************************** "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** "*********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0.999 6.051 2 23E+005 1.435909E+005 X Cd-109 0.982 Ba-133 0.579 1. 7 3 8888E+004 1.085385E+004 Cs-137 1. 000 5.52 3 8 2 7E+004 1.449484E+004 X Eu-155 0.301 X Bi-211 0.999

      ? = Nuclid e is part of an undetermined solution X = Nuclide rejected by the interference analysi s
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at         2 . 000 sigma
 **********       U N I D E N T I F I E D             P E A K S          **********

Peak Locate Performed on: 4/19/20 1 6 1 2 :44:42 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No . (keV ) Counts per Second ~ Uncertaint~/ Type Nuclide 4 4 90 . 7 2 1 . 46 21 E- 00 2 8 6. 2 3 Tol. Eu-15 2 5 608.97 5.3839E- 00 2 46.58 Tol. Zr-97 Sb-125 Sb-125 Cs - 134 Bi - 2 14 7 1332.35 1 .8971E-00 2 89. 2 0 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [242]

1clide MDA Report 4 / 1 9/2 0lb 12:44:4 3 PM Page 5

- - - N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample Title: B306100AFJFC023GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB Nuclide Energy Line MDA Nuclide MDA Activity Dec. Level Name (keV ) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) (pCi/SQM)

+      K-40       1460. 82

1 0 .66 7.904E+004 7.90E+004 6.051E+005 3.0 3 0E+004 Cr-51 320.08 9.91 1.255E+005 1. 2 5E+005 - 1.438E+004 5.806E+004 Mn-54 834.85 99.98 1.525E+004 1.53E+004 6. 3 47E+00 3 6.883E+00 3 Co-58 810.76 99.45 1.648E+004 1.65E+004 1. 22 6E+004 7.501E+00 3 Co-60 1 173. 2 3 99.85 1.685E+004 1. 68E+004 1. 21 5E+004 7.545E+00 3 1332.49 99.98 2 .001E+004 1. 26 0E+004 9.071E+00 3 Nb-94 7 02 .65 99.81 1. 32 0E+004 1. 2 6E+004 -4.377E+00 3 5.914E+003 871. 09 99.89 1.259E+004 - 9.673E+00 3 5.535E+003 Sn-1 1 3 255.13 2 .11 6.539E + 005 .2 .02E+004 -1. 3 71E+00 5 3 .073E+005 391.70 64.97 2 .024E+004 - 1.156E+004 9. 3 31E+003 Cs- 134 475.36 1. 48 9.418E+005 1.69E+004 5.984E+004 4.325E+00 5 563.25 8.34 1.518E+005 1.358E+004 6.850E+004 569.33 15.37 9.015E+004 5.953E+004 4.104E+004 604.72 97.62 1 .918E+004 -9.100E+00 3 8.933E+003 795.86 85.46 1 .690E+004 2 .300E+00 3 7.601E+003 8 01. 95 8.69 1.696E+005 2 .649E+004 7.641E+004 1 038.61 0 .99 1.202E+006 4.307E+005 5.175E+005 1 167.97 1. 79 8.857E+005 - 4.636E+004 3 .940E+005 1 365.19 3. 02 3.861E+005 6 . 0 49E+004 1.617E+005

+ Cs- 137 661.66* 85 .10 l. 1 70E+004 1.17E+004 5.524E+004 5.066E+00 3 Eu-152 1 21. 7 8 28.67 5.065E+004 5.07E+004 -5.477E+004 2 .421E+004 2 44.7 0 7.61 2.028E+005 9.138E+004 9.605E+004 2 95.94 0.45 3.429E+006 4. 27 0E+005 1.615E+006 344.28 26.60 5.222E+004 1.265E+004 2 .430E+004 367.79 0.86 1 .628E+006 - 2 .020E+005 7.563E+005 411.12 2 . 24 6.367E+005 1.618E+005 2 .948E+005 443.96 2 .8 3 5.626E+005 5. 3 49E+00 5 2 .620E+005 488.68 0.4 2 3.056E+006 9.186E+00 5 1. 3 91E+006 563.99 0.49 2.580E+006 -7. 2 09E+004 1 . 1 64E+006 586. 2 6 0.46 3.763E+006 1.671E+006 1.745E+006 678.62 0.47 2 .797E+006 2 .098E+006 1. 25 5E+006 688.67 0.86 1.406E+006 -1.116E+006 6. 2 40E+005 7 1 9.35 0.28 4.860E+006 1 .7 3 4E+006 2.1 8 1E+006 778.90 12.96 9 .654E+004 - 7.185E+003 4. 2 71E+004 81 0 .45 0.32 5 .037E+006 2 .612E+006 2 . 2 90E+006 867. 3 7 4. 2 6 3 . 2 83E+005 -4.194E+004 1. 4 64E+005 919. 33 0.43 3 .367E+006 -4. 2 71E+00 5 1.501E+006 964.08 14.65 1.307E+005 1. 3 83E+005 5.992E+004 1085.87 10. 2 4 1.334E+005 -8.003E+004 5.845E+004 1089.74 1. 73 8.496E+005 -1.807E+003 3.759E+005 111 2 .07 1 3 .69 1.084E+005 -7. 25 0E+004 4.797E+004 1212.95 1. 4 3 1. 2 41E+006 8.698E+00 5 5 .580E+005 [243]

4/ 1 9 / 2 01 6 12:44:43 PM Page 6 iclide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) Eu-15 2 1 249.94 0.19 6.886E+006 5.07E+004 3 . 12 0E+006 2 .965E+006 1299.14 1. 63 9.403E+005 1.780E+005 4.135E+005 1408.01 21. 07 5.883E+004 -3 . 37 7E+003 2 .484E+004 1457.64 0.50 7.005E+006 1.194E+007 3 . 3 07E+006 1528.10 0. 2 8 3 . 736E+006 1.590E+006 1.510E+006 Eu-154 123.07 40.40 3.632E+004 3. 63E+004 -3.077E+004 1.736E+004 247.93 6.89 2 . 072E+005 8.057E+004 9.766E+004 591. 7 6 4.95 2 .661E+005 3.438E+004 1. 2 03E+005 692.4 2 1. 78 7.497E+005 -4.069E+005 3 . 3 65E+005 723.30 20.06 6 . 892E+004 - 1.139E+003 3 .099E+004 756 . 80 4 . 52 2 .850E+005 5.280E+004 l. 2 68E+005 873.18 12.08 l.042E+005 -8.008E+004 4.582E+004 996. 2 9 10.48 l . 658E+005 1.964E+003 7.518E+004 1004.76 18.01 8.351E+004 8.889E+003 3 . 72 4E+004 1274.43 3 4.80 4.016E+004 -3 . 2 68E+004 1.746E+004 1596.48 1. 80 5.128E+005 - 7. 2 58E+005 1. 987E+005 Eu-155 45.30 1. 3 1 7.492E+005 4.70E+004 l.758E+005 3.501E+005 60.01 1. 22 9.889E+005 -5.646E+005 4.681E+005 86.55* 30.70 4.696E+004 1. 688E+004 2 . 2 43E+004 10 5.31 21.10 7. 2 27E+004 2 .540E+004 3.461E+004 Tl -2 08 583.19 85.00 2 . 098E+004 2 .10E+004 2 .373E+004 9.753E+00 3 Bi -2 11 351.07* 13.02 8. 3 65E+004 8. 3 6E+004 8.178E+004 3.809E+00 4 Pb- 2 11 404.85 3.78 3.467E+005 3 .47E+005 6. 23 0E+004 1.595E+005 427. 0 9 1. 76 7.955E+005 -5.626E+004 3 .673E+005 832. 0 1 3.5 2 4.189E+005 -3.4 1 9E+004 l.883E+005 Bi-212 39 . 86 1. 06 9.004E+005 2 . 1 8E+005 -8. 39 6E+004 4.199E+005 727.33 6.67 2.179E+005 8.812E+004 9.849E+004 785.37 1.10 1.189E+006 2 .071E+005 5. 2 88E+005 1 62 0 .50 1. 47 4.891E+005 -5 . 333E+005 1.733E+005 Pb-2 1 2 11 5.18 0.60 2.437E+006 3.92E+ 00 4 -2 .664E+006 1.164E+006 23 8.63 43.60 3.919E+004 4.470E+004 l.868E+004 30 0 . 0 9 3.30 4. 32 6E+005 -5.7 2 9E+00 5 2 .027E+005 Pb212-XR 74.8 2 10. 2 8 1.876E+005 l.05E+005 2 .712E+005 9.067E+004 77.11 17.10 1.050E+005 - 4.425E+00 3 5.064E+004 87.35 3.97 4.462E+005 5. 2 25E+004 2 .150E+005 89.78 1. 4 6 l.158E+006 7.493E+005 5.571E+005 Bi -2 14 609.32 45. 4 9 4.161E+004 4.16E+004 3 .735E+004 l.939E+004 768.36 4.89 2 . 5 96E+00 5 9.569E+004 l.152E+005 8 0 6. 1 8 1. 26 1 . 187E+006 4.398E+005 5.358E+005 934. 0 6 3.11 4.089E+005 3 .175E+005 l.792E+005 1120. 2 9 14.92 l .122E+005 l.104E+005 5.036E+004 1 155. 2 1 1. 63 9.257E+005 3 .691E+004 4.096E+005 1 238.1 2 5.83 2.680E+005 - 7.408E+004 l.186E+005 1 280.98 1. 43 l .084E+006 8.957E+005 4.781E+005 1377.67 3.99 3.652E+005 -1.1 2 8E+005 l.587E+005 1385.31 0.79 1.673E+006 l.067E+006 7.163E+005 14 01. 52 1. 33 l.198E+006 6.692E+005 5. 2 66E+005 1407.99 2.39 5.177E+005 -2 .972E+004 2 .187E+005 1509.21 2 .13 6.064E+005 -4. 2 99E+005 2 .561E+00 5 1661. 2 7 1. 05 l .25 1E+006 9. 3 84E+004 5. 23 9E+00 5 [244]

1clide MDA Report 4/19 /2 01t 12 : 44: 43 PM Page 7 Nuclide Energy Yield Line MDA Nucli de MDA Activity Dec. Level Name (keV ) Pl (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Bi-2 14 17 29 .59 2 .88 3 .947E+005 4.16E+004 1.679E+005 1.595E+005 1764.49 15. 3 0 1.072E+005 7.461E+004 4.639E+004 1847.43 2 .0 3 4.436E+005 -4.052E+005 1.660E+005

 >                21 1 8.51     1.16    O.OOOE+OOO                    O.OOOE+OOO O.OOOE+OOO Pb- 2 1 4     241.99      7.25    2 . 2 48E+005 4.58E+004       4. 62 2E+004 1 .069E+005 295. 22   18.42     8.374E+004                    6.776E+004 3 .945E+004 351. 93   35.60     4.582E+004                   2 .880E+004 2 .154E+004 785.96      1. 06   1. 2 36E+006                 2 .177E+005 5.500E+005 Pb21 4-XR       74.82     5.80    3 .325E+005 1.85E+00 5        4.806E+005 1.607E+005

77. 11 9.70 1.852E+005 -7.802E+00 3 8.927E+004 87.35 2.24 7.908E+005 9. 2 60E+004 3.810E+005 89.78 0.82 2.062E+006 1. 3 34E+006 9.918E+005 Ra- 22 6 186.21 3.64 3.916E+005 3 . 92E +005 -1.560E+005 1.860E+005 Ac- 22 8 129.07 2.42 6.766E+005 5 . 5 6E+004 3.786E+005 3 . 2 49E+005 209. 2 5 3.89 3.801E+005 1.058E+005 1.804E+005 270. 2 4 3.46 3.790E+005 O.OOOE+OOO 1.772E+005 328.00 2 .95 4.489E+005 7.081E+004 2 .085E+005 338. 3 2 11. 2 7 1.329E+005 8. 2 64E+004 6. 2 19E+004 40 9.46 1. 92 7.072E+005 3.812E+005 3. 2 62E+005 463.00 4.40 3.218E+005 1.054E+005 1.482E+005 794.95 4. 2 5 3.453E+005 2 .015E+005 1.556E+005 911. 2 0 25 .80 5.561E+004 -3 . 2 86E+004 2 .480E+004 964.77 4.99 3.752E+005 1.713E+005 1.716E+005 968.97 15.80 1.100E+005 1.054E+005 4.996E+004 1588.20 3 . 22 3.768E+005 1.900E+005 1.563E+005 Pa -2 31 27.36 10.30 6.194E+004 6.19E+004 2 .893E+004 2 .785E+004 283.69 1. 70 8.112E+005 6.524E+005 3 .799E+005 300.07 2.47 5.779E+005 -7.654E+005 2 .7 0 8E+005 302.65 2.20 6.309£+005 -5.166E+005 2.950E+005 330. 0 6 1. 40 9.787E+005 2 .363E+005 4.557E+005 Th- 23 4 92.38 2.13 7. 3 53E+005 7. 3 5E+ 00 5 -4.477E+004 3 .526E+005 92.8 0 2 .10 7.478E+005 3 .361E+005 3 .586E+005 11 2 .81 0. 2 1 6.895E+006 -4.732E+006 3 . 2 95E+006 U- 2 3 5 143.76 10.96 1.375E +005 2.5 1E+004 9. 62 4E+00 3 6.574E+004 163.33 5.08 2 .743E+005 -1.732E+00 5 l.304E+005 185.71 57. 2 0 2 .508E+004 -3 .648E+00 2 1.192E+004 202.11 1. 08 1. 2 91E+006 -1. 2 06E+00 6 6.112E+005 205.31 5.01 2 .853E+005 9.150E+004 1.352E+00 5 Am- 2 41 59.54 35.90 3 . 3 16E+004 3 . 3 2E+004 -7.423E+003 1.568E+004

    + = Nuclid e identified during the nuclide identification
    * = Energy line found in the spectrum
    >     Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calcul a ted
    @ = Half-l ife too short to be abl e to perform the decay correction

[245]

- - - - * ****
      - GAMM A S P E C T R U M A N A L Y S I S * ****

Filename: 5452 Report Generated On 4/1 3/2 016 1: 3 1:14 PM Sample Title B30 6 100AFJFSM023GD Sample Description Ul TB COL G2 7 Sample Identification Sample Type Sample Geometry Peak Locate Threshold 3 .00 Peak Locate Range (in channels) 85 - 8192 Peak Area Range (in channels) 85 - 8192 Identification Energy Tolerance 10.000 keV Sample Size 1. OOOE+OOO SQM Sample Taken On Acquisition Started 4/13/ 2 016 1: 2 0:1 2 PM Live Time 660.0 s econd s Real Time 660.9 second s Dead Time 0. 1 4 % Energy Calibration Used Done On 1/1 3 / 2 015 Efficiency Calibration Used Done On 4 / 1 3/ 2016 Efficiency ID DTMUD_FLOOR Ua+A Va}/dtt/c=J bf Q~~ IJ.-,-lr II I tJ [246]

Peak Analysis Report 4/13/2016 1:31:14 PM Page 2

- - - - P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5452 Sample Title: B306100AFJFSM0 23GD Peak Analysis Performed on: 4/13/2016 1: 3 1:14 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 113- 123 116.5 1 28 . 72 1. 29 5.59E+002 96. 96 6.19E+002 2 232 6- 233 7 2 331.64 583. 0 7 0.83 2.53E+001 15.5 0 1.37E+001 3 2428- 2446 2 436.49 609.30 1. 51 9.99E+001 22 .8 0 9.06E+OOO 4 5829- 585 2 5842.73 1 460.95 0.89 1.32E+002 2 5.86 8.84E+OOO 5 7051- 7064 7057.62 1 764.48 0.39 3.54E+001 12.62 1 .64E+OOO M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2. 000 sigma [247]

Interference Corrected Activity Report 4/1 3/2 016 1: 3 1: 14 PM Page 3

- - - - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title: B306100AFJFSM023GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM) Uncertainty K-40 1. 000 1 460.8 2

10.66 8.14524E+005 1.74362E+005 Tl-208 1. 000 583. 1 9* 85. 0 0 1.24484E+004 7 .75903E+003 Bi-2 1 4 0. 32 6 609. 32
45.49 9.37674E+004 2.41767E+004 768.36 4.89 806. 1 8 1. 26 934. 0 6 3.1 1 11 20. 2 9 14.9 2 11 55. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377.6 7 3.99 1385.3 1 0.79 1401.52 1. 33 1407.99 2 .39 1509.21 2 .13 1661. 2 7 1. 05 1729.59 2 .88 1764.49* 15.30 l.70405E+005 6.23228E+004 1847.43 2 .03 2118.51 1.16 P a-23 1 0 .3 7 6 27.36
10.30 l .15 4 8 8E +0 06 3.43648E+0 05 2 83.69 1. 70 300.07 2 .47 302.65 2 . 20 330.06 1. 40 Th- 23 1 0 .43 0 25.64
14.10 8.43633E+005 2 .479 2 7E+005 84.21 6.60 89.95 1. 00

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy TolerRnce :         10.000 keV Nuclide confidence index threshold              0.30 Errors quoted at 2 . 000 sigma

[248]

Interference Corrected Activity Report 4/13/ 2 016 1:31:14 PM Page 4

- - - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 8.145 2 38E+005 1.743619E+005 Tl- 2 08 1. 000 1. 2 44840E+004 7.7590 3 3E+003 Bi- 2 14 0.326 1.037919E+005 2 . 2 54013E+004

   ?  Pa-231        0.376        1.154877E+006      3 .436478E+005
   ?  Th-231        0.430        8.436334E+005      2 .479270E+005
      ?    Nuclide is part of an undetermined solution X    Nuclide rejected by the interference analysis
      @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at      2 .000 sigma
  **********     U N I D E N T I F I E D        P E A K S        **********

Peak Locate Performed on: 4/13/2016 1: 3 1:14 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second % Uncertaint y Type Nu clide Al l peaks were identified. [249]

Nuclide MDA Report 4/13/ 2 016 1:31:14 PM Page 5

N U C L I D E MD A R E P O R T *****

Detector Name: 5452 Sample Geometry: Sample Title: B306100AFJFSM023GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM )

 +      K-40       1460.8 2

10.66 l.367E+005 1. 3 7E+005 8.145E+005 5.999E+004 Cr-51 320.08 9.9 1 l.463E+005 1 .46E+005 7.860E+004 6.897E+004 Mn-54 834.85 99.98 1.417E+004 1 .42E+004 8.830E+003 6.417E+003 Co-58 810.76 99.45 1.542E+004 1 .54E+004 - 1.700E+003 7.046E+003 Co-60 1173.23 99.85 1.601E+004 1.46E+004 1.281E+004 7. 2 11E+00 3 1332.49 99.98 1.464E+004 7.987E+003 6.479E+003 Nb-94 702.65 99.8 1 1.505E+004 1. 2 7E+004 1.132E+004 6.906E+003 871.09 99.89 1.265E+004 2.655E+003 5.642E+003 Sn-113 2 55.13 2.11 7.602E+005 2 .16E+004 6.112E+005 3.624E+005 391.70 64.97 2. 158E+004 - l.004E+004 1 .008E+004 Cs-134 475.36 1. 48 9.161E+005 1.80E+004 3.933E+005 4.236E+005 563.25 8.34 1.581E+005 9.369E+004 7. 2 41E+004 569.33 15.37 8.113E+004 9.393E+003 3.694E+004 604.72 97.62 2.282E+004 -2 .601E+002 1.082E+004 795.86 85.46 1.800E+004 -9.255E+003 8.235E+003 801. 95 8.69 1.756E+005 1.082E+004 8.024E+004 1038.61 0.99 1.748E+006 1. 093E+006 7.985E+005 1167.9 7 1. 79 8 . 617E+005 4.464E+005 3.867E+005 1365.19 3.02 4.462E+005 2.109E+005 1.948E+005 Cs - 137 661.66 85.10 1.679E+004 1.68E+004 3.265E+003 7.687E+003 Eu- 1 52 1 21.78 28.67 6.491E+004 5.45E+004 2.247E+004 3.145E+004 244.70 7.61 2.112E+005 -3.063E+004 1.0 0 8E+005 295.94 0 .45 3.856E+006 5.028E+OOG 1 .839E+006 344. 2 8 26.60 5.445E+004 -2 . 611E+004 2 .560E+004 367.79 0.86 1.617E+006 5.358E+005 7.566E+005 411.1 2 2 .24 6.555E+005 -1.429E+005 3.066E+005 443.96 2 .83 4.980E+005 1.549E+005 2.316E+005 488.68 0.42 3.630E+006 - 6.989E+005 1.692E+006 563.99 0.49 2.656E+OD6 5.623E+005 1. 21 5E+006 586.26 0.46 3.764E+006 -3 .067E+004 1.759E+006 678.62 0.47 2 .562E+006 -1.615E+005 1.152E+006 688.67 0.86 1.509E+006 1.041E+006 6.830E+005 719.35 0. 2 8 5.444E+006 1.718E+006 2 .498E+006 778.90 12.96 1.011E+005 2 .035E+004 4.555E+004 810.45 0.32 4.719E+006 - 1.651E+006 2.154E+006 867.37 4.26 2.720E+005 -5.326E+004 l .200E+005 919.33 0 . 43 3.095E+006 1.568E+005 1 .383E+006 964.08 14.65 1. 2 43E+005 4.509E+004 5.726E+004 1085.87 10.24 l.551E+005 -7.014E+004 7.009E+004 1089.74 1. 73 8.471E+005 -1.631E+004 3.794E+005 111 2 .07 13.69 1. 081E+005 - 1.538E+005 4.842E+004 121 2 .95 1. 43 1.121E+006 -2 .474E+005 5.040E+005

[250]

Nuclide MDA Report 4/13/2016 1 : 3 1 :14 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) Eu-15 2 1249.94 0.19 7.987E+006 5.45E+004 2 .790E+006 3.562E+006 1 29 9.14 1. 63 7.612E+005 -2 .088E+005 3.294E+005 1408.01 2 1.07 7.176E+004 -7.629E+001 3.175E+004 1457.64 0.50 7.811E+006 1 .854E+007 3.729E+006 1528.10 0.28 3 . 3 77E+006 - 5.288E+005 1.365E+006 Eu-1 5 4 123.07 40.40 4.572E+004 4.29E+004 -8.886E+003 2 . 2 15E+004 247.93 6.89 2 .128E+005 -2 . 2 47E+005 1.011E+005 591.76 4.95 2 .762E+005 -2 .479E+005 1.266E+005 692.4 2 1. 78 7.417E+005 -3 . 32 2E+00 5 3 .363E+005 723.30 2 0.06 7.994E+004 2 .858E+004 3 .684E+004 756.80 4. 52 3 . 2 86E+005 3 .899E+004 1.501E+005 873.18 1 2 .08 9 .164E+004 -8.644E+004 4.016E+004 996.29 10.48 1.558E+005 -4.183E+004 7.095E+004 1004.76 18.01 8.362E+ 0 04 -3 .534E+004 3 .773E+004 1274.43 3 4.80 4.294E+ 0 04 l.444E+004 1.910E+004 1596.48 1. 80 6. 1 2 4E+005 -2 .412E+005 2 .540E+OOS Eu-155 45.30 1. 3 1 2 .483E+006 7. 6 6E+004 2. 568E+005 1. 2 19E+006 60.01 1. 22 1.778E+006 -1.774E+006 8.653E+005 86.55 3 0.70 7.659E+004 8. 3 79E+004 3.736E+004 1 05.3 1 2 1.10 9.381E+004 3 .971E+003 4.554E+004 Tl-208 583.19* 85.00 1.085E+004 1.09E+004 1. 2 45E+004 4.761E+00 3

Bi- 2 11 351 . 07 13.02 1.340E+005 1.34E+005 1.418E+005 6.365E+004 Pb-211 404.85 3 .78 4.188E+005 3.90E+ 0 05 1.063E+005 1.970E+005 42 7.09 1. 76 7.542E+005 4.074E+005 3 .497E+005 8 32 . 01 3.52 3.900E+005 7 . 848E+004 1.760E+005 Bi -212 39.86 1. 06 3.730E+006 2 .24E+005 7.795E+005 1 .838E+006 727.33 6.67 2.238E+005 4.493E+004 1.025E+005 785.37 1. 10 1.420E+006 1.045E+006 6.508E+005 16 2 0 . 50 1. 4 7 5.720E+005 l.905E+005 2 . 2 1 6E+005 Pb-2 1 2 1 15 . 1 8 0 .60 3.002E+006 4.32E+004 -l.268E+006 1 .453E+006 238.G3 43.60 4.3 1 5E+004 6.646E+004 2 .075E+004 3 00 . 0 9 3. 3 0 4.532E+005 -4.528E+005 2 .144E+005 Pb2 1 2-XR 74.82 10.28 2 . .531E+005 1.43E+005 4.176E+005 1 .238E+005 77.11 17.10 1.426E+005 1.700E+005 6.964E+004 87.35 3.97 5.874E+005 2 .800E+005 2 .864E+005 89.78 1. 46 1.5 22E +006 1 .718E+005 7.411E+005

+      Bi-21 4      609.3 2

45.49 1. 9 44E+004 1 .94E+004 9 . 3 77E+004 8.451E+00 3 768.36 4.89 3 .0 2 0E+005 9 .172E+004 1.378E+00 5 806. 1 8 1. 2 6 1. 2 10E+006 - 1.806E+005 5. 52 9E+00 5 934.06 3 .1 1 5.657E+005 4.343E+005 2.600E+005 112 0 . 29 14.9 2 1.260E+005 8.684E+004 5.779E+004 1155. 2 1 1. 63 9.064E+005 -4.747E+005 4.051E+005 1 238.1 2 5.83 3.383E+005 2 .174E+005 1.552E+005 1 2 80.98 1. 43 1.086E+006 4. 3 65E+005 4.853E+00 5 1377.67 3.99 3.394E+005 1.433E+005 1.481E+005 1385.31 0.79 1.803E+006 - 1 .049E+006 7.927E+005 1401.52 1. 33 1.158E+006 -3.134E+005 5 .140E+005 1407.99 2 .39 6.315E+005 -6.714E+00 2 2 .794E+005 1509. 2 1 2 .13 6.130E+005 2 .4 2 0E+005 2 .639E+005 1661. 2 7 1. 05 8.899E+005 3 . 39 4E+005 3 .531E+005

[251]

Nuclide MDA Report 4/1 3 / 2 016 1:31:14 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM )

 +     Bi-214      1729.59       2.88    4. 2 18E+005 1.94E+004 2.278E+005 1.766E+005 1764.49* 15.30        4.647E+004                      1.704E+005 l.671E+004 1847.43       2.03    6.493E+005                      3 . 72 7E+005 2 .742E+OOS
   >               2118.51       1.16    O.OOOE+OOO                       O.OOOE+OOO O.OOOE+OOO P b - 21 4    241.99      7.25    2 .462E+005 4.89E+004 1.966E+005 l.181E+00 5 295. 22   18.42     9.178E+004                      3.812E+004 4. 3 72E+004 351.93    35.60     4.888E+004                      2 .540E+004 2 . 32 1E+004 785.96      1. 06   1.477E+006                      1. 064E+006   6.768E+005 Pb214-XR        74.8 2    5.80    4.487E+005 2 .51E+005 7.401E+005 2 .194E+005 77.11     9.70    2 . 5 15E+005                   2 .997E+005 1. 22 8E+005 87.35     2 . 24  1.041E+006                      4.962E+005 5 .077E+005 89.78     0.82    2 .709E+006                     3 .059E+005 1. 3 19E+006 Ra-226        186.21     3.64     4.661E+005 4.66E+005 4.625E+005 2 . 2 43E+005 Ac-228        129.07     2 .4 2   7.306E+005 7.27E+004 -5.128E+005 3 .533E+005 209.25     3 .89    4.301E+005                    -1.440E+005 2 .064E+005 270.24     3 .46    4. 2 30E+005                    7.746E+004 2 .004E+005 328.00      2 .95    4.515E+005                    - l.016E+005 2 .115E+005 338.32    11. 27     1.396E+005                      7.866E+004 6.600E+004 409.46      1. 9 2   7.965E+005                    - 4. 3 19E+004 3.736E+005 463.00      4.40    3 .035E+005                    - 7.522E+004 l.403E+005 794.95      4. 2 5  3 .661E+005                      l.272E+005 1.676E+005 911.20    2 5.80     7. 2 69E+004                    3 .129E+004 3.363E+004 964.77      4.99    3.760E+005                       2 .611E+005 1.736E+OOS 968.97    15.80     1.156E+00 5                      7.667E+004 5.322E+004 1588. 2 0    3.22    2.815E+005                       1.610E+004 l.117E+005
+      Pa- 2 31       2 7.36* 10.30     2 .932E+005 2 .93E+005 1.155E+006 l.438E+005 283.69      1. 70   9. 2 25E+005                     5.883E+005 4. 3 82E+005 300.07      2 .47   6.054E+005                    -6.049E+005 2 .864E+005 302.65      2 . 20  6.309E+005                    -6.969E+005 2 .970E+005 330.06              9 .361E+005                   - 6. 9 68E+004 4. 3 78E+00.5 Th- 2 34        9 2 .38   2 .1 3  1.012E+006 1.01E+006 3.466E+005 4.924E+005 9 2 .80   2 .10   1.014E+006                    -5 .550E+004 4.933E+005 11 2 .81    0. 2 1  8.493E+006                    -5.367E+006 4.109E+006 U- 23 5       143.76    10.96     1.536E+005 2 .94E+004 -6 . 2 02E+004 7.410E+004 163.33     5.08     3.391E+005                      1.168E+005 1.635E+005 185.71    57.20     2.943E+004                      9.309E+003 l.416E+004 2 0 2 .11  1. 08    1.538E+006                    -3 . 2 97E+005 7.382E+005 2 05. 3 1  5.01     3 .461E+005                     1.636E+005 1.664E+00 5 Am- 2 41        59.54   35.90     6 .131E+004 6.13E+004 -3 .899E+004 2 .985E+004
     + = Nuclide identified during the nuclide identification
     * = Energy line found in the spectrum
     > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ Half-life too short to be able to perform the decay correction

[252]

- - - - GAMM A S P E C T R U M A N A L Y S I S *****

Filename: 5452 Report Generated On 4/13/2016 1:48:46 PM Sample Title B306100AFJFSM024GD Sample Description Ul TB COL G25 Sample Identification Sample Type Sample Geometry Peak Locate Threshold 3 .00 Peak Locate Range (in channel s ) 85 8192 Peak Area Range (in channels) 85 8192 Identification Energy Tolerance 10.000 keV Sample Si ze 1. OOOE+OOO SQM Sample Taken On Acquisition Started 4 /13/2016 1 :37:44 PM Live Time 660.0 seconds Real Time 661.0 seconds Dead Time 0 . 15 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/13/2016 Efficiency ID DTMUD_FLOOR T),,J 4 IJ,. J,'J aJecJ by

~~

1:i-t-l'i'

                                                                /I It)

[253]

Peak Analysis Report 4/ 1 3/2 0 16 1:48:46 PM Page 2

- - - - * ********************************************* * *****
      - P E A K A N A L Y S I S R E P O R T *****

Detector Name: 545 2 Sample Title: B306100AFJFSM024GD Peak Analysis Performed on: 4/13/2016 1:48:46 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8 192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Ar e a Uncert. Counts 1 11 3- 124 116.97 2 8.83 1. 51 6.44E+002 99. 1 8 6.11E+00 2 2 5 0 7- 514 510.05 127.23 0.29 -4.36E+ OOO 25.42 8. 2 4E+001 3 5831- 5853 5840.04 1460.28 2.26 l.42E+ 00 2 2 7. 30 l.15E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 .000 sigma [254]

Interference Corr ected Activity Report 4/13/2016 1:48:46 PM Page 3

- - - - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title: B306100AFJFSM024GD Nuclide Library Used: C: \ GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activit~, Activity Name Confidence (keV) (%) (pCi/SQM) Uncertainty K-40 1.000 1460.82* 10.66 8.71840E+005 1 .84443E+005 Co-57 0.787 1 22 .06* 85.60 - 1.0 9 075E+003 6.36534E+00 3 136.47 10.68 P a-23 1 0. 3 76 2 7.36* 10. 3 0 1. 32 949E+006 3 .8 12 04E+00 5 283.69 1. 70 300.07 2 .47 302.65 2 .20 330.06 1. 40 Th-23 1 0.4 2 9 25.64* 14.10 9 .71188E+005 2 . 74755E+005 84.21 6.60 89.95 1. 00

       * = Energy l ine found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :       10.000 keV Nuclide confidence index threshold             0 .3 0 Errors quoted at 2 .000 sigma

[255]

Interference Corrected Activity Report 4/13/ 2 016 1:48:46 PM Page 4

- - - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1.000 8.718399E+005 1.844435E+OOS Co-57 0.787 - l.090751E+003 6.365338E+003

   ?  Pa-231       0. 376        l.329490E+006     3 .812038E+OOS
   ?  Th-231       0.429         9.711879E+005     2 .747548E+005
      ? = Nuclide is part of an undetermined s olution X = Nuclide rejected by the interference analysis
      @    Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .000 sigma
  **********    U N I D E N T I F I E D        P E A K S      **********

Peak Locate Performed on: 4/13/2016 1:48:46 PM Peak Locate From Channel: 85 Peak Locate To Channel: 819 2 Peak Energy Peak Size in Peak CPS Peak Tel. No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified. [256]

Nuclide MDA Report 4/13/ 2 016 1 :48:46 PM Page 5

- - - - N U C L I D E MD A R E P O R T *****
        * ****************************************************************

Detector Name: 5452 Sample Geometry: Sample Title: B306 1 00AFJFSM0 2 4GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM) (pCi/SQM) (pCi/SQM )

 +      K-40                1460.8 2

10.66 1.523E+005 1.52E+005 8.718E+005 6.783E+004 Cr-5 1 320.08 9.91 1. 3 85E+005 1. 39E+005 -2 .020E+004 6.507E+004 Mn-54 834.85 99.98 1.574E+004 1.57E+004 -6.647E+003 7.198E+00 3 Co-58 810.76 99.45 1.579E+004 1.58E+004 8.107E+003 7. 22 9E+003 Co-6 0 1173.23 99.85 1.575E+004 1. 3 6E+004 -1.734E+004 7.081E+003 1332.49 99.98 1.363E+004 - 2 .757E+003 5.973E+003 Nb-94 702.65 99.81 1.211E+004 1. 2 1E+004 -1.093E+004 5.434E+003 871.09 99.89 1.447E+004 - 8.895E+003 6.550E+00 3 Sn- 11 3 255.13 2 .11 7.076E+005 2 .00E+004 1.669E+005 3.361E+005 391.70 64.97 2 .004E+004 -3 .445E+00 3 9.311E+003 Cs- 134 475.36 1. 48 8.735E+005 1.57E+004 -1.654E+00 5 4.023E+005 563.25 8.34 1.669E+005 1 .416E+004 7.680E+004 569.33 15. 3 7 8.914E+004 -1.033E+004 4.094E+004 604.72 97.6 2 2 .008E+004 - 3.975E+003 9.451E+003 795.86 85.46 1.574E+004 4.711E+003 7.101E+003 801.95 8.69 1.6 2 4E+005 1.0 2 1E+005 7.364E+004 1038.61 0.99 1.639E+006 5.5 1 8E+005 7.441E+005 1 167.97 1. 79 9.191E+005 3.364E+005 4.154E+005 1 365. 1 9 3.02 4.338E+005 7.954E+004 1.886E+005 1? r; rt~

1...,::, - .L ..J / 661.66 85.10 1.754E+004 l.75E+004 -1.553E+004 8.062E+003 Eu-1 52 1 21.78 2 8.67 6.150E+004 5.68E+004 - 1.901E+004 2.975E+004 2 44.70 7.6 1 2 .171E+005 4.732E+004 1 .038E+005 2 95.94 0 .45 3.404E+006 1.857E+006 1.613E+006 344.28 2 6.60 5.683E+004 - 1.7 92 E+004 2.679E+004 367.79 0.86 1.585E+006 5.175E+005 7.407E+005 411.1 2 2.24 5.771E+005 -2 . 22 9E+005 2.674E+005 443.96 2.83 4.942E+005 -2 . 23 8E+005 2.297E+005 488.68 0.42 3 .177E+006 2 .023E+006 1.465E+006 563.99 0.49 2 .778E+006 - 1.127E+006 1.276E+006 586. 2 6 0.46 4.058E+006 3 .033E+006 1.9 0 6E+006 678.6 2 0.47 3 .132E+006 1.859E+006 1.437E+006 688.67 0.86 1.825E+006 -1.902E+005 8.410E+005 719.35 0.28 4.454E+006 -6.093E+006 2 .003E+006 778.90 1 2 .96 9.948E+004 1. 22 3E+OO':l 4.473E+004 810.45 0.32 4.946E+006 3 .472E+006 2.267E+006 867.3 7 4.26 3.4 3 5E+005 4.216E+004 1.557E+005 919.33 0.43 3.573E+006 -l.945E+006 l.6 2 2E+006 964.08 14.65 1. 2 68E+005 2 .994E+004 5.849E+004 1085.87 10. 2 4 1.479E+005 -6.632E+004 6.650E+004 1089.74 1. 73 9.055E+005 7.389E+005 4.086E+005 1112.07 13.69 1.137E+005 -1.488E+005 5.124E+004 1 2 12.95 1. 43 1.121E+006 -5.316E+005 5.040E+005 [257]

4/ 1 3 / 2 0 1 6 1:48:46 PM Page 6 Nuclide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Eu-1 52 1249.94 0.19 7.671E+006 5.68E+004 2 .474E+006 3 .403E+006 1299.14 1. 63 6.863E+005 -1 .170E+005 2 . 92 0E+005 1408.01 2 1. 07 7.015E+004 1.602E+004 3.095E+004 1457.64 0.50 8.101E+006 2. 12 6E+007 3.874E+006 1 52 8.10 0. 2 8 4. 3 43E+006 -7.783E+005 1.848E+006 Eu-154 1 23 .07 40.40 4.349E+004 4.35E+004 -8 .949E+003 2 .103E+004 2 47.93 6.8 9 2 .086E+005 -2 .415E+005 9.897E+004 591.76 4.95 2 .882E+005 -2 .569E+005 1. 32 6E+005 692.42 1. 78 8.488E+005 -1.796E+005 3.898E+005 723.30 2 0.06 7.591E+004 3.770E+004 3.483E+004 756.80 4.5 2 3 . 2 46E+005 9.600E+004 1.482E+005 873. 1 8 1 2 .08 1.215E+005 -l.361E+004 5.509E+004 996. 2 9 10.48 1. 2 90E+005 -9 .335E+004 5.751E+004 1004.76 18.01 8.362E+004 l.054E+004 3.773E+004 1274.43 3 4.80 4.463E+ 0 04 -3 .136E+004 1.995E+004 1596.48 1. 80 5.060E+005 -3.570E+005 2 .008E+005 Eu-155 45.30 1. 3 1 2 .080E+006 6.97E+004 4.384E+005 1.018E+006 60.01 1. 22 1.631E+006 -8.201E+005 7.918E+005 86.55 3 0.70 6.973E+004 2 .090E+004 3.393E+004 105. 3 1 2 1.10 8.859E+004 1.512E+003 4. 2 93E+004 Tl- 2 08 583.19 85.00 2 .165E+004 2 .16E+004 1.102E+004 1.016E+004 Bi-21 1 351.07 13.02 1.565E+005 1.57E+005 1.569E+005 7.492E+004 Pb-21 1 404.65 3 .78 3 .798E+00 5 3 .80E+005 6.888E+003 l.775E+005 427.09 1. 76 7.413E+005 -3 .091E+005 3.432E+005 832 .01 3.52 4.616E+005 -7 .024E+004 2 .118E+005 Bi -2 12 39.86 1. 06 3. 2 04E+006 2 .36E+005 -5 .754E+005 1.575E+006 727.33 6.67 2 . 362E+ 00 5 1 .952E+005 l.087E+00 5 785.37 1.10 1. 3 55E+006 8.428E+005 6.182E+0 0 5 16 2 0. 50 1. 4 7 6.715E+005 -1.135E+006 2 .713E+ 00 5 Pb-212 115.18 0.60 2.934E+006 4.39E+004 -4.163E+005 1.419E+006 23 8.6 3 43.60 4.392E+004 4.499E+004 2 .114E+004 3 00.09 3.30 4.342E+005 -3.338E+005 2 .049E+005 Pb21 2 -XR 74.8 2 10. 2 8 2 .355E+005 1 . 3 2E+005 3.850E+005 l .149E+005 77.11 17.10 1.319E+005 9.530E+004 6.426E+004 87.35 3.97 5. 2 97E+005 - 9.884E+004 2 .576E+00 5 89.78 1. 46 1.415E+006 4.896E+004 6.880E+005 Bi-214 609.32 45.49 5 .036E+004 5.04E+004 8.368E+004 2 . 3 91E+004 768.36 4.89 2 .703E+005 l.265E+005 1. 22 0E+005 806.18 1. 2 6 1.087E+006 - 4.453E+005 4 .913E+005 934.06 3.11 4.454E+005 3.383E+005 1.999E+005 1120. 2 9 14.92 l. 2 60E+005 8.948E+004 5.779E+004 1155. 2 1 1. 63 1.017E+006 1.147E+00 3 4.604E+005 1238.1 2 5.83 3.152E+005 2 .9 2 6E+005 1.437E+005 1 2 80.98 1. 43 1.145E+006 -9.306E+004 5.148E+005 1377.67 3.99 3 .485E+005 -1.672E+005 1.527E+005 1 3 85.31 0 .79 1.457E+006 -3 .503E+006 6.197E+005 1401.5 2 1. 33 1.055E+006 1.567E+005 4.625E+005 1407.99 2 .39 6.174E+005 1 .410E+005 2 .724E+005 1509. 2 1 2 .13 5.481E+005 3 .146E+005 2.315E+005 16 6 1. 2 7 1. 05 8.899E+005 -1.154E+005 3.531E+005 [258]

Nuclide MDA Report 4/13/ 2 016 1:48:46 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (%) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) Bi-2 14 17 2 9.59 2 .88 5. 2 46E+005 5.04E+004 3 .796E+005 2.280E+005 1764.49 15.30 l.4 3 8E+005 1. 26 0E+005 6.538E+004 1847.43 2 .03 5.914E+005 O.OOOE+OOO 2 .453E+005

   >                2118.51        1.16 O.OOOE+OOO                     O.OOOE+OOO O.OOOE+OOO Pb-214        2 41.99      7. 2 5 2. 601E+005 5.73E+004 1.650E+005 1. 25 1E+005 2 95. 22   1 8.42 8.375E+004                     2 .1 8 3E+004 3.970E+004 351.93     35.60 5.732E+004                      6.516E+004 2.743E+004 785.96       1. 06 l.391E+006                    2.975E+005 6.342E+005 Pb214-XR         74.82      5.80 4.173E+005 2 .32E+005 6.824E+005 2 .037E+005

77. 1 1 9.70 2 .325E+005 l.680E+005 l.1 33 E+005 87.35 2.24 9.388E+005 - l.752E+005 4.565E+005 89.78 0.82 2 .520E+006 8.718E+004 1. 22 5E+006 Ra-226 186. 2 1 3.64 4.1 26 E+005 4.13E+005 5.811E+004 1 .976E+005 Ac-228 12 9.07 2.42 7. 2 46E+005 7.07E+004 -5.371E+005 3 .503E+005 209. 2 5 3.89 3.941E+005 2 .038E+005 1.884E+005 2 70 . 24 3.46 4.441E+005 4. 33 4E+005 2 .110E+005 32 8.00 2.95 4.684E+005 1.566E+005 2 .199E+005 338.32 11. 27 1.350E+005 9.801E+004 6. 3 70E+004 409.46 1. 9 2 6.535E+005 -4.945E+005 3 .021E+005 463.00 4.40 3.062E+005 -4.969E+004 1.417E+005 794.95 4. 2 5 3.259E+005 2 .820E+004 1.476E+005 911. 2 0 2 5.80 7.072E+004 6.117E+004 3.265E+004 964.77 4.99 3.652E+005 - 1.9 2 4E+005 1.682E+005 968.97 15.80 1.179E+005 6.116E+004 5.437E+004 1588.20 3 . 22 4. 0 42E+005 2 .577E+005 1 .730E+005

+      Pa - 23 1       27.36*   10.30 2.951E+005 2 .95E+005 1 . 32 9E+006 1 .448E+005 283.69       1. 70 8.435E+005                  -2 .449E+005 3 .987E+005 300.07       2.47 5.801E+005                   - 4.460E+005 2 .737E+005 302.65       2.20 6 . 475E+005                   6.611E+004 3 .053E+005 330.06       1. 40 9.842E+005                    7.585E+004 4.619E+005 Th- 23 4        9 2 .38    2 .13 9.330E+005 9. 3 3E+005 -1.934E+005 4.530E+005 92.8 0     2 .10 9.451E+005                  -2 .430E+005 4.588E+005 112.81       0. 2 1 8.287E+OOG                 - 1.716E+006 4.007E+006 U-235         143.76     10.96 1.483E+005 2 .63E+004 1.979E+004 7 .143E+004 163.33       5.08 3 .1 2 6E+005                  7. 3 04E+003 l.503E+005 185.71     57. 2 0 2 .6 2 9E+004                 9. 3 95E+003 1.259E+004 202.11       1. 08 l.412E+006                  -2 . 22 7E+005 6.752E+005 205.31      5.01 2 .995E+005                     l.558E+004 1.431E+005 Am- 2 41        59.54    35.90 5.542E+004 5 . 54E+004 -3 .134E+004 2 .691E+004
     +     Nuclide identified during the nuclide identification

Energy line found in the spectrum

     >     Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @     Half- life too short to be able to perform the decay correction

[259]

************************** ************************* *             ****************
****         GAMM A       S P E C T R U M         ANALYSIS                         *****
************************************************************************
.lename: 54 52 iport Generated On                 4/ 2 0/2016       1:34:36 PM tmple Title                        B306100AFIFC025GD tmple Description                  TB 560,Flooi Drain Sump tmple Identification tmple Type tmple  Geometry iak Locate Threshold                 3 .00

!ak Locate Range (in channels) 85 - 81 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 1 0.000 keV tmple Size 1.000E+OOO SQM tmple Taken On

quisition Started 4/20/2 01 6 1 :24:34 PM

.ve Time 6 00.0 seconds !al Time 6 00 .4 seconds iad Time 0. 07 !i5 Energy Calibration Us ed Don e On 1/13/ 2 015 Efficiency Calibration Used Done On 4/20 /2 016 Efficiency ID TBFLRDRNSUMP Dat "- Vo. ),do. t~J by

                                                                ~~
                                                                 /J- /,- /8
                                                                  //JO

[260]

~ak Analysis Report                       4/ 2 0/ 2 016     1: 3 4: 3 6 Pl               Page   2
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****                P E A K        A N A L Y S I S           R E P O R T                   *****
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Detector Name: 545 2 Sample Title: B306100AFIFC025GD Peak Analysi s Performed on: 4/20/2016 1:34:35 PM Pe a k Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 297- 3 05 301.51 75.03 0.97 7.14E+001 3 6.17 1 . 2 0E+002 2 794 - 801 7 97. 60 199.21 0.34 8.04E+OOO 17.21 3 . 3 0E+001 3 2 428- 2 445 2436. 3 2 609.26 0.4 2 6.lOE+OOl 2 1. 91 1.80E+001 4 2637- 2653 2644.91 661.44 1. 3 8 1.09E+00 2 23 .86 1.05E+001 5 3867- 3878 387 2 .89 968.55 0.59 1.40E+001 10.77 6.00E+OOO 6 5833- 5853 5841. 97 1460.76 1. 03 1.12E+00 2 25 .6 2 1.52E+001

= First peak in a multiplet region
= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 .000 sigma

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1terference Corrected Acti _ty Report 4/ 2 0/ 2 016 34: 36 PM Page 3

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Sample Title: B306100AFIFC025GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQM) Uncertainty K-40 1. 000 1460.82* 10.66 1.15653E+007 2 .83453E+006 Cs - 137 1. 000 661.66* 85.10 9.33912E+005 2 .32375E+005

       * = Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :     10.000 keV Nuclide confidence index threshold =       0.30 Errors quoted at 2 .000 sigma

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1terference Corrected Acti ty Report 4/ 2 0/ 2 016 34: 3 6 PM Page 4

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"*********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 1.156525E+007 2 .834 52 9E+006 Cs-137 1. 000 9.339121E+005 2 . 323 750E+005

      ?   = Nuclide is part of an undetermined solution X     Nuclide rejected by the interference analysis
      @     Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at       2 .000 sigma
 **********      U N I D E N T I F I E D          P E A K S        **********

Peak Locate Performed on: 4/20/2016 1: 34:35 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Si ze in Peak CPS Peak Tol. No. (keV) Counts per Second % Uncert ai nty Type Nuclide 1 75.03 l . 1 896E-0 01 50.68 Tol. Pb214-XR Ba-133 Pb212-XR Pb212-XR Pb214-XR 2 199. 21 1.3404E-00 2 2 13.93 Tol. Fe-59 3 609. 2 6 1.0167E-001 35 . 91 Tol.

                                                                                  ~Zr-97 Sb-125 Sb-125
                                                                                   ~       -
                                                                                  ~

5 968.55 2 .3333E-00 2 7 6 . 93 Tol. Eu-152

Ac-228 M = First peak in a multiplet region m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000 sigma [263]

1clide MDA Report 4/20/ 2 01 1: 3 4: 36 PM Page 5

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      - * ************************************************************** ****

Detector Name: 5452 Sample Geometry: Sample Title: B306100AFIFC025GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (% ) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM )

+      K-40       1460.8 2

10 .66 2 .742E+006 2 .74E+006 1.157E+007 1.231E+006 Cr-51 320.08 9.91 2 .187E+006 2. 1 9E+006 8.488E+005 1.026E+006 Mn-54 834.85 99.98 2 . 2 21E+005 2 . 2 2E+005 1.738E+005 1.001E+005 Co-58 810.76 99.45 2 .404E+005 2 .40E+005 1.343E+005 1.093E+005 Co-60 117 3 . 23 99.85 2 .672E+005 2 .67E+005 1.313E+005 1. 2 04E+005 1 332 .49 99.98 2 .699E+005 1.169E+005 l . 2 09E+005 Nb - 94 702.65 99.8 1 2 .407E+005 2 .41E+005 1. 3 4 6E+005 l .102E+005 871.09 99.89 2 .575E+005 6. 2 12E+004 1.175E+005 Sn-113 2 55.13 2 . 11 1.054E+007 3.17E+005 4. 32 8E+006 4.985E+006 3 91. 7 0 64. 97 3 .170E+005 -2 .082E+004 1. 4 71E+005 Cs-134 475.36 1. 48 1.481E+007 2 .58E+005 - 2 .376E+006 6.848E+006 563.25 8.34 2.220E+006 -4.971E+005 1.002E+006 569.33 15.37 1.2 8 4E+006 - 1.884E+004 5.830E+005 604.72 97.62 3 .459E+005 - 3 .046E+004 1.634E+005 795.86 85.46 2 .580E+005 4.726E+003 1.164E+005 801.95 8.69 2 .466E+006 6.651E+005 1.109E+006 1038.61 0.99 2.073E+007 -8.852E+005 9.116E+006 1 167.97 1. 79 1.413E+007 6.665E+006 6. 32 9E+006 1 365.19 3.02 6.095E+006 - 1 .073E+007 2.574E+006

+      Cs-13 7      661. 66*   85.10    1.838E+005       1 .84E+005     9.339E+005    8. 0 38E+004 Eu-15 2      121.78     2 8.67   9.732E+005       9.07E+005      1.031E+006    4.690E+005 244.70       7.61   3 .028E+006                   -2 . 2 72E+006  1.437E+006 295.94       0.45   5.476E+007                    -9.130E+006     2 .594E+007 344. 2 8   2 6.60   9.074E+005                      5.058E+ 0 05  4.276E+005 3 67.79      0.86   2 . 2 51E+007                 -1.813E+007     1.042E+007 411.12       2 . 24 1 .069E+007                   - 3.711E+006    5.005E+006 443.96       2 .8 3 8.098E+006                    -5.2 61E+005    3.768E+006 488.68       0.4 2  4.781E+007                    - 1 .383E+007   2 .192E+007 563.99       0.49   3.714E+007                    -2 . 2 81E+006  1 .673E+007 586. 2 6     0.46   5.782E+007                      1 .959E+007   2.691E+007 678.62       0.47   4. 2 56E+007                    8.566E+006    1.917E+007 688.67       0.86   2 .705E+007                     3.275E+007    1. 2 36E+007 719.35       0. 2 8 8.404E+007                      1.135E+007    3.835E+007 778.90     1 2 .96  1.735E+006                    -2 .049E+005    7.854E+005 81 0 .45     0. 32  7.346E+007                      2 .371E+007   3 . 3 35E+007 867.37       4.26   5.641E+006                    -1. 766E+006    2 .558E+006 919. 3 3     0.43   5.000E+007                    -1.144E+008     2 . 23 0E+007 964. 0 8   14.65    1.926E+006                      6.743E+00 3   8.819E+00 5 1085.87      10. 2 4  2 .198E+006                     7.545E+005    9.750E+005 1 089.74       1. 73  1 .409E+007                     6.107E+006    6.309E+006 111 2 .07    1 3 .69  1.893E+006                    -2.061E+006     8.530E+00 5 1 212 .95      1. 4 3 1.839E+007                      4.028E+006    8. 2 55E+00 6

[264]

tclide MDA Report 4/21/ 2 01 9: 2 5: 1 5 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( Z, ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Eu-1 52 1249.94 0.19 8.125E+006 5. 3 6E+004 2 .032E+006 3 .584E+006 1299. 1 4 1. 63 8.426E+005 -6 .074E+005 3 .646E+005 1408.01 21.07 5.358E+004 -1. 9 42E+004 2 . 2 22E+004 1457.64 0.50 8.964E+006 2 .082E+007 4. 2 87E+006 1528.10 0. 28 2 .460E+006 5. 2 98E+005 8.716E+005 Eu-154 123.07 40.40 4.408E+004 4.13E+004 -2.962E+004 2 .124E+004 247.93 6.89 2 .312E+005 -8.042E+004 l.097E+005 591.76 4.95 2.998E+005 1. 2 63E+005 1.371E+005 69 2 .4 2 1. 78 8.903E+005 -1.986E+005 4.068E+005 723.30 2 0.06 8.143E+004 6.836E+003 3 .725E+004 756.80 4. 52 3. 22 5E +005 -1.619E+005 1.455E+00 5 87 3 . 1 8 12 .08 1.385E+005 -3 . 33 5E+004 6.297E+004 996. 2 9 10.48 1.282E+005 - 5.792E+00 3 5.638E+004 1004.76 18.01 8.668E+004 3.858E+004 3.882E+004 1 27 4.43 34.80 4.131E+004 -3.040E+004 1.803E+004 1 596.48 1. 80 7.437E+005 -4.024E+005 3 .141E+00 5 Eu-155 45. 3 0 1. 31 1.470E+006 7.52E+004 7.215E+004 7.103E+00 5 60.01 1. 22 1.540E+006 -6. 53 8E+005 7.436E+005 86.55 30.70 7.519E+004 8.651E+004 3 .655E+004 105.31 21.10 8.856E+004 3 .015E+00 3 4. 276E+004

+     Tl -2 08     583.19*    85.00    1 .121E+004      1.12E+004       2 .117E+004    4.867E+003 Bi -2 11     351. 07    1 3 .02  1.390E+005       1.39E+005       1.086E+005     6.578E+004 Pb- 211      404.85       3 .78  4 .42 3E+005     4.12E+005       3.782E+005     2 .073E+00 5 427.09       1. 76  8.601E+005                     -4.413E+005      3.996E+005 83 2 .01     3.52   4.118E+005                     -4.465E+004      1.848E+005 Bi- 212       39.86       1. 06  1.907E+006       2 . 2 4E+00 5 -1. 35 6E+005    9. 2 30E+005 727. 33      6.67   2 . 2 44E+005                    8.455E+004     l.017E+005 785 . 37     1.10   1.346E+006                     - 6.083E+005     6.072E+005 1 620.5 0      1. 47  5 .670E+005                      1 .580E+005    2 .122E+005
+     Pb-21 2      115.18       0.60   3 .197E+006      2 .35E +00 4    5.851E+005     1. 545E+00 6 238.63*    43.60    2 .345E+004                      1.426E+004     1 .081E+004 300.09       3.30   4.999E+005                       2 .585E+005    2 .364E+005 Pb212-XR      74.82     10. 2 8  2 .411E+005      1. 3 7E+005     4.475E+005     1.174E+005 77.11     17.10    1. 3 73E+005                     6. 2 2 8E+004  6.680E+004 87.35       3 .97  5.752E+005                       3.852E+005     2 .795E+005 89.78       1. 4 6 1.501E+006                     - 6.326E+005     7.284E+005 Bi - 2 14    609. 32    45.49    4.619E+004       4.62E+004       3.970E+004     2 .168E+004 768. 3 6     4.89   3 .511E+005                      5.731E+00 3    1.609E+005 806.18       1. 2 6 1 . 2 93E+006                  -9.848E+00 5     5 .886E+005 934.06       3 . 11 4.582E+005                     - 1. 036E+005    2 .038E+005 112 0 . 2 9  14.9 2   1 .425E+005                    - 1 . 55 9E+00 5 6.552E+004 1155. 2 1      1. 6 3 1. 004E+006                    -5.610E+00 5     4.487E+005 1 238.1 2      5.83   3.164E+005                     - 1. 2 25E+005   1.428E+005 1280.98        1. 43  9.483E+005                     - 1.028E+006     4.104E+005 1 377.67       3.99   3.316E+005                     -4.111E+004      1.420E+005 1385.31        0 .79  1.788E+006                       6. 3 17E+005   7.737E+005 1401.52        1. 33  1.039E+006                       6.936E+005     4.476E+005 1407.99        2 .39  4.716E+005                     -1.709E+005      1.956E+005 1509.21        2.13   4. 5 64E+005                   - 1.114E+005     l.811E+005 1661. 2 7      1. 05  9 .017E+005                      3 .003E+005    3 .493E+005

[265]

1clide MDA Report 4 /21/2 0 1 l 9: 2 5:15 AM Page 7 Nuc l ide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) (% ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) Bi-2 14 1729.59 2 .88 2 .599E+005 4.62E+004 5.598E+004 9.208E+004 1764.49 15.30 1 . 2 80E+005 1.119E+005 5.681E+004 1847.43 2 .0 3 5 .812E+005 3. 2 62E+004 2 . 3 48E+005

 >                2 118.51      1.16 O.OOOE+OOO                      O.OOOE+OOO O.OOOE+OOO Pb- 2 1 4    241.99      7. 2 5 2.567E+005 4.90E+004        -2 .439E+005 1 .228E+005 295. 22   18.42 9.006E+004                     -2 .400E+003 4.261E+004 351.93   35.60 4.903E+004                        1.441E+004 2 .315E+004 785.96     1. 06 1 .442E+006                     3 .984E+004 6. 52 9E+005 Pb2 14 -XR    74.82     5.80 4. 27 3E+005 2 .42E+00 5         7.931E+005 2 .081E+005

77. 11 9.70 2 .421E+005 1.098E+005 1 . 178E+005 87.35 2. 2 4 1.019E+006 6.8 2 8E+005 4.954E+005 89.78 0.8 2 2 .672E+006 - 1.126E+006 l. 2 97E+00 6 Ra-226 186.2 1 3 .64 4.771E+005 4.77E+005 2 .334E+005 2 . 2 88E+005 Ac-228 129.07 2 .42 7.581E+005 6 .07E+004 -1.651E+005 3.656E+005 209.25 3. 89 4.354E+005 4.471E+004 2.081E+005 270.24 3. 4 6 5.112E+005 3 .305E+005 2.433E+005 328 .00 2.95 5.277E+005 - 8.410E+004 2 .479E+005 338.32 11. 2 7 1.489E+005 8.7 2 9E+004 7.020E+004 409.46 1. 92 8.971E+005 6. 3 25E+005 4. 2 12E+005 463. 00 4.40 3.639E+005 1.973E+005 1.693E+005 794.95 4.25 3.720E+005 1. 2 01E+005 1.689E+005 911. 2 0 25.80 6.073E+004 2 .687E+004 2 .7 3 6E+004 964.77 4.99 3.839E+005 1.892E+005 1.760E+005 968.97 15.80 1.319E+005 1.580E+005 6.088E+004 1588. 2 0 3. 22 4.778E+005 1. 4 93E+005 2 .067E+005

+ Pa - 23 1 2 7.36* 1 0 .30 8.951E+004 8.95E+004 9.875E+004 4.164E+004 283.69 1. 70 9.521E+005 9.097E+005 4.504E+005 300.07 2 .47 6.679E+005 3.454E+005 3.158E+005 302.65 2 . 2 0 6.756E+005 -4.397E+003 3.173E+005 330. 0 6 1. 40 1.043E+006 -1. 2 87E+005 4.876E+005 Th-234 92.38 2 .13 1 .000E+006 1.00E+006 1 .672E+005 4.850E+005 92.8 0 2 .10 1 .003E+006 2 .089E+005 4.863E+005 11 2 .8 1 0. 2 1 9.261E+006 6.535E+006 4.478E+006 U-235 143.76 10.96 1.548E+005 3 .02E+004 -3 .4 3 6E+004 7.436E+004 163.33 5.08 3.395E+005 3. 058E+004 1.630E+005 185.71 57. 2 0 3.024E+004 -4.583E+002 1 .450E+004 202.11 1. 08 1.638E+006 4. 2 75E+005 7.847E+00 5 2 05.31 5.01 3.557E+005 9.837E+004 1.704E+00 5 Am-241 59.54 35.9 0 5. 2 05E+004 5 . 2 0E+004 -9.292E+003 2 .513E+004

    + = Nuclide identified during the nuclide identification

Energy line found in the spectrum

    >     Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
    @ = Half-l ife too short to be able to perform the decay correction

[266]

*************************    ' *************************         *****************
****        GAMM A       S P E C T R U M            A N A L Y S I S                   *****
************************************************************************
.lename: 5452 iport Generated On                  4/21/ 2 016       9:25:15 AM

r: ~..\'"'

tmple Title B306100AF7FC~26GD tmple Description TB 560,Fire Sump 1mple Identification tmple Type tmple Geometry iak Locate Threshold 3 .00 iak Locate Range (in channels) 85 - 81 92 iak Area Range (in channels) 85 - 81 92 lentification Energy Tolerance 10.000 keV 1mple Size 1.000E+OOO SQM tmple Taken On

quisition Started 4/21/2 01 6 9:15:12 AM

.ve Time 600.0 seconds ial Time 601. 3 seconds iad Time 0.21 % Energy Calibration Us ed Done On 1/13/ 2 015 Efficiency Calibration Used Done On 4/14/2016 Efficiency ID TBFLOOR b a+a \J °' \\cL,.:(. ed b

                                                             ~~ 1
                                                              /J,-6,-/f
                                                               )/J.s

[267]

!ak Analys i s Report 4 / 2 1 / 2 0 16 9: 2 5:15 Al Page 2

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Detector Name: 5452 Sample Title: B306100AFJFC0 2 6GD Peak Analysis Performed on: 4/21/2016 9:25:14 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV ) ( keV ) Area Uncert. Counts 1 1 13 - 119 115.93 28.5 7 0.55 4. 2 9E+001 2 5.58 4.81E+001 2 950 - 958 954.75 2 3 8.54 0.69 2 .10E+001 2 1. 43 4.40E+00 1 3 2 0 39- 2 050 2044.49 51 1. 23 0.78 1.86E+001 15.44 1.64E+001 4 2 137- 2 146 2141.31 535.45 0.71 2.38E+OOO 10.51 1.06E+001 5 232 5- 2 337 2330.40 582.76 0.83 3.88E+001 16.5 2 1.12E+001 6 2 636- 2 654 2644.83 661. 42 1. 22 1. 28E+00 2 25.99 1.20E+001 7 5832- 5850 5841. 1 7 1 4 60.56 0.88 1.31E+00 2 27.75 1.83E+001 First peak in a multiplet region = Other peak in a multiplet region Fitted singlet -rors quoted at 2. 000 sigma [268]

1terference Corrected Acti ty Report 4/2 1 / 2 01 6 ~5: 15 AM Page 3

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Sampl e Title: B306100AFJFC026GD Nuclide Library Used: C:\GENIE2K\CAMFILES \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence ( keV) (%) (pCi/SQM) Uncertainty K-40 1. 000 1460.8 2

10.66 8.91296E+005 2 .04409E+005 Rb-83 0.638 520.40* 45.00 1.79735E+004 1.52925E+004 5 2 9.59* 2 9.30 3.61787E+003 1.59595E+004 552.55 16.00 Sr-85 0.988 514. 01
96.00 8.4 2 515E+00 3 7.07986E+003 Cs-137 1. 000 661. 66* 85.10 7.42368E+004 1.75142E+004 Tl-208 1. 000 583. 1 9* 85.00 2 .11700E+004 9.36499E+003 Pb-212 0.872 115.18 0.60 2 38.63* 43.60 1.4 2 638E+004 1.47211E+004 300.09 3.30 Pa-231 0.376 2 7.36* 10.30 9.87545E+004 6.35876E+004 283.69 1. 70 300.07 2 .47 302.65 2 .20 330. 0 6 1. 40 Th -23 1 0.431 25.64* 14.10 7.21 3 98E+004 4.63284E+004 84.2 1 6.60 89.95 1. 00

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance :         10.000 keV Nuclide confidence index threshold =           0.30 Errors quoted at 2 .000 sigma

[269]

1terference Corrected Act i .ty Report 4/ 2 1 /2 016 ..25 :15 AM Page 4

"*** I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertaint: 1 K-40 1. 000 8.91 2 959E+005 2 .044093E+005 Rb-83 0.638 3.617875E+00 3 1 .595112E+004 Sr-85 0.988 6.729 2 60E+003 1.029720E+004 Cs-137 1. 000 7.423683E+004 1. 751416E+004 Tl-2 0 8 1. 000 2 . 1 17003E+004 9.364992E+003 Pb-2 1 2 0.87 2 1.426375E+004 1.472113E+004

  ?  Pa-231        0.376            9.875450E+004        6.358764E+004
  ?  Th-231        0. 4 3 1        7.21 3 981E+004       4.632838E+004
     ?    Nuclid e is part of an undetermined solution X    Nuclide rejected by the interference analysis
     @=Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at        2 . 000 sigma
 ***** *****    U N I D E N T I F I E D             P E A K S       **********

Peak Locate Performed on: 4 /2 1/20 1 6 9:25 :1 4 AM Peak Locate From Channel: 85 Peak Locate To Channel: 81 92 Peak Energy Peak Size in Peak CPS Peak ToL No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified. [270]

iclide MDA Report 4/21/201 9: 2 5:15 AM Page 5

- - - - * ****************************
    - N U C L I D E M D A R E P O R T *****
      - ~*****

Detector Name: 54 52 Sample Geometry: Sample Title: B306100AFJFC026GD Nuclide Library Us ed: C: \ GENIE2K\CAMFILES \ Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) (~ ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM )

+      K-40       1460. 82

10 .66 l. 94 7E+005 l .95E+005 8.913E+005 8.814E+004 Cr-51 320.08 9.91 l. 52 5E+005 l.52E+005 -5.503E+004 7.156E+004 Mn-54 834.85 99.98 l.572E+004 1. 57E+004 -2 .800E+003 7.117E+003 Co-58 810.76 99.45 l.751E+004 l.75E+004 -3.910E+003 8.018E+00 3 Co-60 1173. 23 99.85 1.744E+004 l.74E+004 5.496E+00 3 7.841E+00 3 133 2 . 4 9 99.98 1.822E+004 l. 3 01E+004 8.177E+00 3 Nb-94 702.65 99.81 l.496E+004 l.50E+004 -3 .074E+003 6.794E+00 3 871. 09 99.89 1.673E+004 9.013E+003 7.607E+003 Sn-113 255.13 2 .11 8. 2 89E+005 2 .55E+004 l.036E+006 3 .948E+005 391. 70 64.97 2 .547E+004 - 8.078E+00 3 l.194E+004 Cs-134 475.36 1. 48 1.000E+006 l.75E+004 -4.571E+004 4.617E+005 563.25 8.34 l.696E+005 l.181E+00 5 7.738E+004 569.33 15.37 9.1 3 1E+004 4.970E+003 4.162E+004 604.7 2 97. 62 2 .028E+004 5.864E+003 9.484E+003 795.86 85.46 1.746E+004 -l.860E+004 7.877E+003 8 01. 95 8.69 l.8 02E+005 l. 3 53E+004 8.168E+004 1038.61 0.99 1.631E+006 -2 .509E+006 7. 3 19E+005 1167.97 1. 79 9 .543E+005 2 . 62 5E+005 4. 2 83E+005 1365.19 3.02 4.035E+005 6.89 2E+004 l.704E+005 Cs - 137 661.66~ 85.10 l.377E+004 l . 38E+004 7.424E+004 6.102E+003

+                                                                                  2 .977E+004 Eu-152      121. 78     2 8.67  6.178E+004      5. 3 6E+004 -2 .610E+004 244.70        7.61  2.187E+005                  -7.980E+00 3    1.040E+005 295.94        0 .45 3.724E+006                  -8.900E+005     l.762E+006 344. 2 8    2 6.6 0 6 .298E+004                 - l.407E+004    2 .968E+004 367.79        0.86  1.692E+006                  - 1. 22 0E+006  7.882E+005 411 .12       2.24  7.438E+005                    3.964E+005    3 .484E+005 443.96        2.83  4. 3 79E+005                -1. 1 11E+005   1.996E+005 488.68        0.4 2 3.464E+006                  - 4. 25 3E+005  l.595E+006 563.99        0. 49 2.772E+006                    3 .006E+005   l. 2 60E+006 586. 26       0.46  4.375E+006                    2 .858E+006   2 .051E+006 678.62        0.47  2.844E+006                  -l. 3 11E+006   1.279E+006 688.67        0.86  l.837E+006                  -3 . 3 96E+005  8.394E+005 719.35        0.28  5.412E+006                    2 .826E+006   2 .457E+006 778.90      12.96   l.157E+005                    l.040E+004    5. 2 31E+004 81 0 .45      0.32  5.362E+006                  -l.350E+006     2 .452E+006 867.37        4.26  3.528E+005                  -2 .481E+005    1. 586E+005 919.33        0.43  2.946E+006                  -2 .658E+006    1. 2 91E+00 6 964. 0 8    14.65   1. 2 92E+005                  9.402E+004    5.918E+004 1085.87      1 0.24  l.187E+005                  -3 .258E+004    5.111E+004 1089.74        1. 73 8.496E+005                    5.194E+005    3 .759E+00 5 1112.07      13.69   l.482E+005                  - 7.446E+004    6.784E+004 1212.95        1. 43 l.061E+006                  -3 .772E+00 5   4.681E+005

[271]

4 /2 0 /2 01 1:34: 3 6 PM Page 6 1clide MDA Report Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQM) (pCi/SQM ) {pCi/SQM ) (pCi/SQM ) Eu-1 52 1 2 49.94 0 . 19 1. 333E+008 9.07E+005 -l.519E+008 5.945E+007 1299.14 1. 63 l.383E+007 3 .474E+006 6.058E+006 140 8.01 2 1. 07 l .202E+006 1.022E+006 5.318E+005 1457.64 0.50 l. 2 90E+008 3 .197E+008 6.155E+007 1528.10 0. 2 8 7.014E+007 l. 3 29E+007 2 .962E+007 Eu-154 12 3 .07 40.40 6.753E+005 6. 75E+005 3 .177E+005 3 . 2 52E+005 247.93 6.89 3.211E+006 l .661E+005 1.520E+006 591. 76 4.95 4.181E+006 -1.077E+005 1.903E+006 692.42 1. 78 1.195E+007 -7.738E+006 5.411E+006 723.30 2 0.06 1. 3 58E+006 1 .077E+006 6.279E+005 756.80 4 . 52 4.532E+006 -2 .105E+006 2 .034E+006 873.18 1 2 .08 2 .051E+006 1.929E+006 9. 32 7E+005 996. 2 9 10 . 48 2 .093E+006 -1.371E+006 9.310E+005 1004.76 18.01 1.173E+006 - 1.546E+006 5.189E+005 1 274.43 34.80 7. 3 10E+005 6.720E+005 3. 2 60E+005 1596.48 1. 80 1.179E+007 - 6.262E+006 5.014E+006 Eu-1 55 45. 3 0 1. 3 1 1. 3 46E+007 1.09E+006 1.394E+006 6.333E+006 60.01 1. 22 l.923E+007 -8.218E+006 9.188E+006 86.55 3 0.70 1.086E+006 5.689E+005 5. 2 61E+005 105.31 2 1.10 1.359E+006 2.873E+005 6.551E+005 Tl-208 583.19 85.00 3 .305E+005 3.31E+005 3.548E+005 1.544E+005 Bi-2 11 351.07 13.0 2 2 .011E+006 2.01E+006 1. 2 19E+006 9.519E+005 Pb-2 11 404.85 3.78 6.112E+006 6.11E+006 l.539E+006 2 .856E+006 427.09 1. 76 1. 2 15E+007 -l.419E+007 5.635E+006 832.01 3.52 6.196E+006 -l.925E+006 2 .786E+006 Bi-21 2 39.86 1. 06 1 .480E+007 3 .79E+006 -9.384E+006 6.908E+006 727. 33 6.67 3.786E+006 - 7.090E+005 l.7 3 9E+006 785.37 1.10 2 .049E+007 - 5.433E +006 9. 2 74E+006 1620.5 0 1. 4 7 l.052E+007 -2 .326E+006 4.173E+006 Pb- 212 115.18 0.60 4.783E+007 6.04E+005 -9.239E+00 6 2 . 3 07E+007 2 38.63 43.60 6 . 042E+005 2 .831E+005 2 .888E+005 300.09 3.30 7.676E+006 -5.150E+006 3.641E+006 Pb212-XR 74.82 1 0.28 3.634E+006 2 .10E+006 5.914E +006 l.766E+006 77.11 17.10 2.103E+006 - l.191E+006 l.021E+006 87.35 3 . 97 8. 2 10E+006 - 8.465E+005 3 .974E+006 89.78 1. 46 2 .1 2 1E+007 - 6. 2 76E+006 1. 025E+007 Bi- 2 14 609.3 2 45.49 7 . 489E+005 7.49E+005 9.764E+005 3 .538E+005 768.36 4.89 4.695E+006 2 .485E+006 2 .132E+006 8 0 6.18 1. 2 6 1.809E+007 l. 2 1 7E+007 8. 1 88E+006 934. 0 6 3 .11 8.505E+006 -2 . 28 0E+006 3 .877E+006 1120. 2 9 14.92 2 . 0 97E+006 2 . 32 8E+006 9. 62 4E+005 1155. 2 1 1. 63 1 .567E+007 7.195E+006 7.033E+006 1 238. 1 2 5.83 4.4 62 E+006 - 1.443E+006 1.999E+006 1280.98 1. 43 1.778E+007 1 . 816E+006 7.930E+006 1 377.67 3 .99 6. 3 98E+006 2 .5 9 9E+005 2 .839E+006 1385.31 0.79 2 .437E+007 -2 .935E+007 l.037E+007 1401.52 1. 33 1.856E+007 -8.828E+006 8. 1 87E+006 1407.99 2 .39 1.058E+007 8.997E+006 4.680E+006 1509.21 2 .13 8.390E+006 -3 . 3 05E+006 3 .480E+006 1 661. 2 7 1. 05 l.500E+007 - 5. 2 64E+006 5.953E+006 [272]

tclide MDA Report 4 /2 0/ 2 01 1:34: 3 6 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi-214 1729.59 2 .88 5 .601E+006 7.49E+005 2 .136E+006 2 . 22 2E+006 1764.49 15. 3 0 2 . 26 0E+006 2 .361E+006 1. 020E+006 1 847.43 2 .0 3 9.451E+006 4.406E+006 3.874E+006

  >               2 118.51      1.16    O.OOOE+OOO                    O.OOOE+OOO    O.OOOE+OOO Pb- 214      2 41.99     7. 2 5  3 . 6 68E+006   7. 3 3E+005   2 .033E+006   1.754E+006 2 95. 22  18. 42    1. 2 95E+006                  1.734E+005    6.128E+005 35 1. 93 35.60      7.332E+005                    8. 52 9E+005  3.469E+005 785.96     1. 06    2 .130E+007                 -4.023E+006     9.645E+006 Pb2 14 -XR     74.8 2   5.80     6.441E+006      3 .71E+006    1.048E+007    3.131E+006 77.11     9.70    3 .708E+006                 -2 .100E+006    1.800E+006 87.35    2 . 24   1. 455E+007                 - 1.500E+006    7.043E+006 89.78    0.82    3.776E+007                   - 1.117E+007    1.825E+007 Ra-226       186.21     3 .64    6.650E+006      6.65E+006   - 1.346E+006   3. 180E+006 Ac-228        129.07     2 .4 2  1.091E+007       1.16E+006   -4.839E+005    5 . 2 48E+006 2 0 9.25   3.89     6.147E+006                  -2 .933E+006   2 .931E+006 270.24     3. 46   6.041E+006                   -6 . 676E+006  2 .842E+006 328.00     2 .95   7. 2 52E+006                 -2.889E+006    3.396E+006 338.3 2  11. 2 7   2 . 2 20E+006                  1.002E+006   1 .049E+006 409.46     1. 92   1. 2 35E+007                 -2 .372E+006   5.778E+006 463. 00    4.40    4.947E+006                   -2.807E+00 5   2 . 2 89E+006 794.95     4.25    5.184E+006                     1. 518E+006  2 . 33 9E+006 911.20   25 .80    1.164E+006                     1.004E+006   5. 3 72E+005 964.77     4.99    5.657E+006                   -3 .180E+005   2 .590E+00 6 968.97   15.8 0    1. 770E+006                    7.034E+005   8.097E+00 5 1588. 2 0    3 . 22  6.556E+006                     1.561E+006   2 .789E+006 Pa -2 31       27.36   10.30     1. 2 13E+006     l. 2 1E+006   6.463E+005   5.561E+005 283.69      1. 70   1.306E+007                    1. 3 52E+007  6.159E+006 30 0 . 07   2 .47   1.025E+007                   -6.881E+006    4.865E+006 302.65      2 . 20  1.137E+007                    1. 3 11E+007  5.389E+006 330.06      1. 40   1.483E+007                   -5.492E+006    6.932E+006 Th-23 4        92.38     2 . 13  1.440E+007      1 .43E+007     6.088E+006   6.955E+006 92.8 0    2 .10   1.429E+007                   -6.310E+006    6.896E+006 11 2 .8 1   0. 2 1  1.397E+008                    1 . 285E+008  6.743E+007 U- 235       14 3.76   1 0.96    2 .240E+006     4.3 4E+005    5 .895E+005   1.074E+006 163.33      5.08    4.807E+006                    1.037E+006    2 .302E+006 185. 7 1  57. 2 0   4. 33 9E+005                  2.626E+005    2 .077E+005 2 02.11     1. 08   2 . 2 56E+007                 1.864E+006    1 .078E+007 2 05. 3 1  5.01     4.862E+006                    1.589E+006    2 .322E+006 Am- 2 41       59.54   35.90     6.494E+005      6 . 49E+005   3 .030E+004   3 .102E+005
    + = Nuclide identified during the nuclide identi f ication
     * = Energy l ine found in the spectrum
    > = Calculated MDA is zero due to zero counts in the region, o r the region is outside the spectrum, or MDA has not been calculated
     @ = Half-life too short to be abl e to perform the decay correction

[273]

"******** ****** * **********"   ************************* ****************
"***         GAMM A        S E> E C T R U M        A N A L Y S .i S            *****
"************************************************ ******* ****************
.lename: C:\GENIE2K\CAMFILES\00001387.CNF iport Generated On                   4/25/2016        9:09:00 AM 1mple Title                          B306100AFJWC027GD 1mple  Description                    TB 560,Fire Sump 1mpl e Identification 1mple  Type 1mple  Geometry iak Locate Threshold                   3.00 iak Locate Range (in channels)             85 -   8192 iak Area Range {in channels)               85 -   8 1 92 lentification Energy Tolerance           10.000 keV 1mple Size                             1.000E+OOO SQM 1mple Taken On

quisition Started 4/ 2 1/2016 9:45:04 AM

.ve Time 600.0 seconds ial Time 600.7 seconds

ad Time 0.11 %

Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 4/25/2016 Efficiency I D TBWALL2

                                                               /.:1- t. .. /<J
                                                                 /Its

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iak Analysis Report 4/ 2 5/20 1 6 9:09:00 AM Page 2

*************************************************************************
****               P E A K       A N A L Y S I S               REPORT                    *****
*************************************************************************

Detector Name: 545 2 Sample Title: B306100AFJWC0 2 7GD Peak Analysis Performed on: 4/25/ 2 0 16 9:09:00 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV ) Area Uncert. Counts 1 170- 176 172.93 42 .84 0. 33 1.llE+OOl 15.5 3 2.59E+001 2 296- 308 300.37 74.74 0.77 5 . 2 4E+001 60.65 3.26E+002 3 949- 96 0 953.76 238.29 0.48 4.46E+001 29 . 11 6.64E+001 4 1106- 1114 1110.36 277.48 0. 2 5 5.58E+OOO 15. 52 2 .44E+001 5 2 428- 2445 2436.46 609.29 1. 08 6.45E+001 20. 26 1.15E+001 6 2 633- 2 656 2 644.57 661. 35 1. 64 2 .41E+00 2 34.08 1. 22E+ 001 7 4473- 4485 4478.90 1 1 20.07 0. 35 2 .41E+001 12 .58 5.93E+OOO 8 5829- 585 2 5841.36 1460. 61 2 .05 1.80E+00 2 31. 83 1.82E+001 First peak in a mul tiplet region Other peak in a mul tiplet region

= Fitted singlet

rors quoted at 2 . 000 sigma

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1terference Corrected Acti' .y Report 4/ 25 / 2 016 9 3:00 AM Page 3 "***********************************************************************

- - - N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

'*********************************************************************** Sample Title: B306100AFJWC027GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/SQM) Uncertaint~/ K-40 1. 000 1460.8 2* 10.66 2 .19797E+006 4.3 32 89E+005 Cs-137 1. 000 661.66* 85.10 2 .55572E+005 4.74329E+004 Hg-203 0.995 2 79.20* 81. 56 4.30 23 0E+003 1.19785E+004 Pb-21 2 0.87 2 115.18 0.60 238.63* 43.60 6. 0 4919E+004 4.064 22 E+0 0 4 30 0 .09 3.30 Bi -2 1 4 0. 3 4 2 609. 32

45.49 1. 2388 1E+005 4.16334E+004 768.36 4.89 806.18 1.26 93 4.06 3.11 1120. 2 9* 14.92 1 .83743E+005 9.71985E+004 1155.2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.2 1 2.13 1661.27 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2 11 8.51 1.16 Th -22 7 0.367 5 0 .13* 8.40 8.11582E+004 l.1608 2E+005 79.69* 1. 95 1 .46688E+006 1. 74311E+006 94.97 0.0 3 210.62 1.25 235.96* 12.90 2.04453E+005 1.4 1 643E+0 05 256. 2 3 7.00 286. 0 9* 1. 74 2.01654E+005 5.63551E+005 299.98 2 .21 304 . 5 0 1.15 329.85 2 .90 334.37 1.14

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1t e rference Corrected Acti* :y Report 4/25/2016 9 9:00 AM Page 4

       * = Energy line found in the spectrum.
       @ = Energy line not used for Weighted Mean Ac tivity Energy Tolerance :    10.000 keV Nuclide confidence index threshold       0.30 Errors quoted at 2 .000 sigma

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1terference Corrected Acti :y Report 4/25/ 2 016 c 9:00 AM Page 5

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 2.197968E+006 4. 332 890E+005 Cs-137 1. 000 2.555724E+005 4.743287E+004 Hg-203 0.995 2.439392E+00 3 1. 22 2630E+004 Pb-21 2 0.87 2 3.465741E+004 5.294723E+004 Bi-214 0.34 2 1. 33 1609E+005 3 .8 2 7040E+004 X Rn-219 0.385 Th-227 0.367 8.731658E+004 1.147 92 6E+005

     ?  = Nuclide is part of an undetermined solution X  = Nuclide rejected by the interference analysis
     @ = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     2 .000 sigma
 **********    U N I D E N T I F I E D         P E A K S        *******~' **

Peak Locate Performed on: 4/ 25/2 0 1 6 9:09:00 AM Peak Locate From Channel: 85 Peak Locate To Channel: 81 92 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second t Uncertainty Type Nuclide All peaks were identified. [278]

tclide MDA Report 4/ 2 5/201 9:09:00 AM Page 6

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"****************************************************************************** Detector Name: 54 52 Sampl e Geometry: Sample Title: B306100AFJWC027GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) (pCi/SQM)

+      K-40       1460.8 2

1 0 .66 3 .776E+005 3.78E+005 2 .198E+006 1.722E+005 Cr-51 32 0.08 9.91 3 .197E+005 3.20E+005 1. 250E+005 1.508E+005 Mn-54 834.85 99.98 3 .008E+004 3.01E+004 2 .313E+004 1. 3 69E+004 Co-58 810.76 99.45 2 .743E+004 2.74E+004 - 3 .577E+00 2 1.238E+004 Co-60 1173. 23 99.85 3 . 2 3 6E+004 2.85E+004 5.145E+003 1.460E+004 1332.49 99.98 2 .846E+004 - 2 .834E+003 1. 255E+004 Nb-94 7 02 .65 99.8 1 2 .877E+004 2 .16E+004 3 .185E+003 1.313E+004 871. 09 99.89 2 .160E+004 -1. 34 7E+004 9.430E+00 3 Sn-11 3 255.1 3 2 .11 1.599E+006 4.97E+004 -1.072E+006 7.606E+005 391.70 64.97 4.970E+004 2 .088E+003 2 .334E+004 Cs- 134 475.36 1. 48 1.947E+006 3.22E+004 -1. 2 61E+006 9.016E+005 563.25 8.34 3.507E+005 3.178E+005 1.616E+005 569.33 15. 3 7 1.733E+005 - 2 .144E+005 7.918E+004 604.72 97.6 2 4.155E+004 - 2 .833E+004 1.957E+004 795.86 85.46 3 . 2 16E+004 -1.797E+004 1.454E+004 801. 95 8.69 2 . 92 4E+005 -1.259E+005 1.310E+005 1 038.61 0.99 3.036E+006 2.475E+006 1. 3 68E+006 1 167.97 1. 79 1.655E+006 -4.413E+005 7.395E+005 1365.19 3.02 8.619E+005 5 .198E+004 3.747E+005

+ Cs - 137 661.66* 85.1 0 2 .743E+004 2.74E+004 2.556E+005 1.228E+004 Eu-15 2 121.78 28.67 l.554E+005 1.10E+005 -5.890E+004 7.530E+004 244.70 7.6 1 4.959E+005 -l.822E+005 2.373E+005 295.94 0 .45 7.999E+006 - 2 .357E+006 3 .805E+006 344.28 2 6.60 1.275E+005 -7.349E+004 6.029E+004 367.79 0 .86 3.473E+006 3 .2 2 7E+005 1.626E+006 411. 12 2.24 l.320E+006 -l. 2 55E+006 6.150E+005 443.96 2.83 1.153E+006 3.081E+005 5.401E+005 488.68 0.42 7.508E+006 l.241E+006 3.498E+006 563.99 0. 4 9 5.958E+006 3.583E+006 2.746E+006 586. 2 6 0.46 7.568E+006 7.678E+006 3.531E+006 678.62 0.47 5.770E+006 2 . 25 3E+006 2.623E+006 688.67 0.86 2 .968E+006 -1.246E+006 l.339E+006 719.35 0. 2 8 8.547E+006 -4.958E+006 3.820E+006 778.90 12.96 2 .134E+005 - 2 .304E+005 9.659E+004 810.45 0. 32 8. 62 8E+006 1. 785E+006 3.900E+006 867.37 4.26 5. 32 4E+005 -1 .364E+005 2.341E+005 919.33 0.43 7.146E+006 4.488E+005 3.245E+006 964.08 14.65 2 .304E+005 8.456E+004 l.054E+005 1085.87 10.24 2 .578E+005 7.950E+004 l.141E+005 1089.74 1. 73 1.595E+006 5.762E+005 7.094E+005 111 2 .07 13.69 1.950E+005 -2 .160E+005 8.628E+004 1 2 1 2 .95 1. 43 2 .475E+006 1.7 2 1E+006 1.125E+006 [279]

4/25/ 2 01( 9: 09:00 AM Page 7 1clide MDA Repo rt Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Eu-15 2 1249.94 0.19 1. 8 43E+007 1.10E+005 3.492E+006 8. 35 6E+006 1299.14 1. 63 1. 6 04E+006 -1.400E+006 7.002E+005 1408.01 21 .07 1.099E+005 6.664E+004 4.674E+004 1457.64 0.50 1.802E+007 5.100E+007 8.660E+006 1528.10 0. 2 8 9.550E+006 3.298E+006 4.133E+006 Eu-154 123.07 40.40 1.102E+005 8. 5 4E+004 2 .501E+004 5.338E+004 2 47.93 6.89 5. 2 18E+005 -4. 2 66E+005 2 .491E+005 591.76 4.95 5.664E+005 3 .580E+005 2 . 5 96E+005 692.42 1. 78 1.504E+006 9. 2 27E+005 6.817E+005 723.30 2 0.06 l.431E+005 6.853E+004 6.522E+004 756.80 4.52 5.183E+005 2 .497E+004 2 .305E+005 873. 1 8 12.08 1.738E+005 -7.130E+004 7.557E+004 996. 2 9 10.48 2 .902E+005 - 1 .591E+005 1.312E+005 1004.76 18.01 1.505E+005 -5.655E+004 6 .710E+004 1274.43 34.8 0 8.539E+004 -1.915E+004 3 .798E+004 1596.48 1. 80 1. 53 9E+006 - 8.183E+005 6.659E+005 Eu-155 45.30 1. 31 2 .7 2 5E+006 1. 79E+005 -3.997E+005 l. 2 99E+006 60.01 1. 22 4.104E+006 2 .518E+006 l.984E+006 86.55 3 0 .70 1.790E+005 2 .097E+005 8.725E+004 105.31 21.10 2 .164E+005 - 2 . 52 5E+004 1.050E+005 Tl-2 0 8 58 3 .19 85.00 4.058E+004 4.06E+004 3.469E+004 1 .892E+004 Bi-2 11 351. 07 13.0 2 3 .169E+005 3 .17E+005 4.078E+005 1.513E+005 Pb-211 404.85 3.78 8.561E+005 7. 3 3E+005 - 8.313E+004 4.018E+005 427.09 1. 76 1.801E+006 4.502E+005 8.427E+005 832 .01 3.5 2 7. 3 28E+005 -9.466E+005 3.282E+005 Bi-21 2 39.86 1. 06 3.119E+006 4.37E+005 -1.123E+006 1.48 1E+006 727. 33 6.67 4. 3 67E+005 2 . 52 8E+005 1.993E+005 785.37 1.10 2 .554E+006 2 .379E+005 1.1.58E+006 1 62 0 .50 1. 47 l.417E+006 5.392E+004 5.808E+005 + Pb- 2 12 115.18 0.60 7.833E+006 6.13E+004 5.338E+006 3.801E+006 238.63* 43.60 6.132E+004 6.049E+004 2 .883E+004 300.09 3.30 1.051E+006 -9.057E+005 4.989E+005 Pb212-XR 74.82 10. 2 8 6.499E+005 3.62E+005 1.555E+006 3.178E+005

77. 11 17.10 3.617E+005 -2 .503E+004 1.766E+005 87.35 3.97 1. 368E+006 1 .0 8 7E+006 6.666E+005 89.78 1. 46 3.429E+006 - 3 .4 3 5E+006 1 .668E+006

+ Bi -2 1 4 609.32* 45.49 4.414E+004 4.41E+004 1. 23 9E+005 1. 947E+004 768.36 4.89 6.163E+005 4.551E+005 2 .816E+005 806.18 1. 26 2.085E+006 - 6.384E+005 9.375E+005 934.06 3. 11 9.354E+005 -2.611E+005 4. 22 1E+005 112 0 . 2 9* 14.92 1.196E+005 1 .837E+005 4.948E+004 1155.21 1. 63 1 .770E+006 - 1. 769E+005 7.895E+00 5 1 23 8.12 5.83 5.023E+005 - 1. 92 9E+005 2 . 23 4E+005 1280.98 1. 43 2 . 314E+006 6.510E+005 l.042E+006 1377.67 3.99 6. 3 61E+005 - 1.468E+005 2.752E+005 1 385. 3 1 0 .79 2 .893E+006 5.547E+005 1. 2 31E+006 1 401. 52 1. 33 1. 92 6E+006 1. 3 40E+006 8. 3 33E+005 1 407.99 2.39 9.671E+005 5 . 8 65E+005 4.114E+005 1509. 21 2.13 1. 29 3E+006 3 .754E+00 5 5. 62 1E+005 1 661. 27 1. 05 1.616E+006 - 1.513E+006 6. 25 8E+005 [280]

1cl i d e MDA Report 4/25/ 2 01( 9:09:00 AM Page 8 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM)

+         Bi-2 1 4   1729.59        2 .88  7.070E+005 4.41E+004           3.008E+005 2 .857E+005 1764.49      15.3 0   2 .691E+005                    2 . 1 22E+005 1. 2 16E+005 1 847.43       2 .03  1.040E+006                     4.426E+005 4. 2 03E+005
  >                  2 11 8.51      1.16   O.OOOE+OOO                     O.OOOE+OOO O.OOOE+OOO Pb- 2 14     241.99       7.25   6.107E+005 1.13E+005           2 . 2 41E+004 2 .943E+005 295.22     18.42    1. 93 6E+005                   1.867E+004 9. 2 08E+004 351. 93    35.60    1.127E+005                     3.623E+004 5.370E+004 785.96       1. 06  2 .656E+006                    2 .359E+005 1.204E+006 Pb2 1 4-XR     74.82      5.80   1.152E+006 6. 3 8E+005         2 .757E+006 5 .632E+005 77.11      9.70   6.376E+005                   -4.413E+004 3 .113E+005 87.35     2 .24   2.424E+006                     1.926E+006 1.181E+006 89.78      0.82   6.106E+006                   -6.116E+006 2 .969E+006 Ra-226        186.21      3 .64   1.055E+006 1.06E+006         -1.005E+004 5.075E+00 5 Ac-228        12 9. 0 7   2 .4 2  1.731E+006 1. 3 5E+005        5. 2 43E+005 8.370E+00 5 209.25      3 .89   9.722E+005                   -4.795E+005 4.665E+005 2 70. 2 4   3 . 46 1.016E+006                     2 .890E+005 4. 83 9E+005 328. 00     2 .95  1.074E+006                    -3.192E+005 5.059E+005 338. 32    11. 27   2 .975E+005                    2 . 3 22E+004 1.406E+005 409.46      1. 92  1 .642E+006                    1.052E+006 7.692E+005 463.00      4.40    6.576E+005                  -1.4 1 2E+005 3 .049E+005 794.95       4. 2 5  6.750E+005                    3 . 32 0E+005 3 .065E+005 911. 2 0   2 5.80   1. 3 46E+005                   1.273E+005 6.189E+004 964.77       4.99   6.685E+005                   -2.343E+005 3 .054E+005 968.97     15.80    2.141E+005                     5.060E+004 9.793E+004 1588.20       3 . 22 1.001E+006                     5.911E+005 4.428E+005 Pa-23 1        2 7.36   10.30    2.110E+005 2 .11E+005          8.714E+004 9.739E+004 283.69       1. 70  1.986E+006                     8.081E+005 9.426E+005 300.07       2 .47  1.404E+006                   -1. 2 10E+006 6.665E+005 30 2 .65     2 . 20 l .!:>37E +0 06                6.2 7 6E+005 7 . 2 85E+005 33 0.0 6     1. 40  2.291E+006                     8.099E+005 l.080E+006 Th- 23 4       92 . 3 8   2 .13  2.319E+006 2 .32E+006          1 .786E+004 1 .127E+006 92 .80     2 .10  2.346E+006                   - 9.102E+005 1 .140E+006 112.81       0. 21  2.167E+007                     2. 841E+006 1.051E+007 U-235        143.76     10.96    3.685E+005 6.71E+004           3.3 20E+004 l.779E+005 163.33       5.08   7.610E+005                     2 .934E+005 3 .665E+005 185.71     57. 2 0  6.708E+004                     4.506E+003 3. 22 6E+004 2 02 .11     1. 08  3.517E+006                   -1.549E+006 1.689E+006 2 05. 3 1    5.01   7.625E+005                     9.909E+004 3 . 662 E+005 Am- 2 41       59.54    3 5.90   1 .353E+005 1. 3 5E+005        6.209E+003 6. 53 1E+004
       +     Nuclide identified during the nuclide identification
       * = Energy line found in the spectrum
       > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
       @    Half-life too short to be able to perform the decay correction

[281]

GA MM A s p C T R U M A N A L Y S s *****

 "************* *************~ ~*************************** ****************

_lename: E:\4 17\00001521.CNF

!port Generated On                  5/1/2017        9:47:33 AM tmple  Title                        B306100AFJFC028GD 1mple   Description                  turbine BUILDING tmple  Identification tmple  Type tmple Geometry

?ak Locate Threshold 3. 00 1ak Locate Range (in channels) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV 1mple Size 1.800E+001 sq meter tmple Taken On 1/28/2 01 3 1 2 : 00 : 00 PM

quisition Started 1/21/2 01 6 2 : 22 : 23 PM ve Time 152.3 seconds

al Time 153.6 seconds ad Time 0.86 %

Energy Calibration Used Done On 1/27/ 2 015 Efficiency Calibration Used Done On 4/18/2017 Efficiency ID TB 560 EVS 1)"\°' \JI\ \,c\c:\\eJ b, 9~~ V I'-* l,-f<r

                                                                   ///¢

[282]

                                         ....JI .J.. / L U.J.. /      ::J ; "+/- I ; .J .J fi..l.'J

'************************************************************************ '*** P E A K A N A L Y S I S R E P O R T *****

Detector Name: 5456 Sample Title: B306100AFJFC0 2 8GD Peak Analysis Performed on: 5/1/2017 9:47:33 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV ) Area Uncert. Counts 1 1 23- 134 129.19 32 .00 1. 03 2.36E+002 59.05 2 .53E+002 2 2 03 - 209 205.40 5 1. 06 0.25 -8.95E+000 3 9.30 2 .04E+002 3 2 96 - 306 300.46 74.85 0.68 1.48E+00 2 79.48 5.97E+00 2 4 333 - 346 340.0 2 84.74 0.45 1. 4 9E+002 91. 39 6.99E+00 2 5 2 430- 2443 2434.7 0 608.58 1. 2 8 4.96E+001 27. 41 4.64E+001 6 2 634- 2 654 2643.78 660.85 1. 28 6.78E+003 166.18 3.50E+001 7 4682- 4694 4688.04 1171. 64 0. 4 9 3.31E+001 13.58 4.90E+000 8 5829- 5847 5838.60 1458.97 1. 36 9:16E+00 1 19.97 2 . 3 6E+000 = First peak in a multiplet region = Other peak in a multiplet region = Fitted singlet rors quoted at 2 .000 sigma [283]

_, * ,

_,....., .c-:l..1. "~

--------- .... --..-v----.'f 4'\._.t""....., -'- '-

'*** N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title: B3 0 6100AFJFC028GD Nuclide Library Used: C: \ GENIE2K\CAMFILES \ Zion Lib-BNL.NLB I DENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/sq m) Uncertainty K-40 0.995 1460.82* 10.66 2 .29264E+004 5 .377 3 4E+00 3 Cd- 1 09 0.956 88.03* 3.70 1.25209E+005 8.11237E+004 Cs-13 7 0.999 661. 66* 85.10 1.42180E+005 1.74 2 67E+004 Th - 23 1 0.884 2 5.64* 14.10 1.06380E+004 3.67117E+003

84. 2 1

6.60 1.36896E+004 8. 9922 5E+00 3 89.95 1. 00 Am- 2 41 0.891 59.54* 35.90 - 1.59462E+002 7.00872E+002

       * = Energy l ine found in the spectrum.
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance:            10.000 keV Nuclide confidence index threshold =                                 0.30 Errors quoted at 2 .0 00 sigma

[284]

                                                      ..J/ ~ / £..V ..L I

'*********************************************************************** "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** '*********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/sq m) Uncertainty K-40 0.995 2 . 2 92 641E+004 5. 3 77341E+003 Cd-109 0.956 2 .791014E+004 8.664495E+004 Cs-137 0.999 1.42 1 801E+00 5 1. 742670E+004 X Eu-155 0.341 X Pa-231 0.379 Th-23 1 0.884 1.063805E+004 3 .410752E+003 Am-241 0.89 1 -1.594619E+002 7.008718E+00 2

      ?    Nuclide    is part of an undetermined solution X = Nuclid e    rejected by the interference analysis
      @ = Nuclide contains energy l ines not used in Weighted Mean Activity Errors quoted at        2. 000 sigma
 **********      U N I D E N T I F I E D             P E A K S            **********

Peak Locate Performed on: 5/1/2017 9: 47 :33 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. ( keV) Counts per Se cond % Uncertainty Type Nuclide 3 74.85 9.7268E-001 53.65 Sum 5 608.58 3.2579E-001 55.24 Tol. Zr-97 Sb-125 Sb-125 Cs-134 Bi-214 7 11 71.64 2 .1730E- 001 41. 02 Tol. Co-60 Cs - 134 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2 . 000 sigma [285]

......... ..L...l.. \,,A\,;;;;; ... -J.J.JJ..J,. 4\. 1-;;" ,t..l'\J..1- ' - ..J/.J../ L. U.J../ ::J ~ ~ I * ...J 'i ttL"l .l:'ct(:J e ;:J

- - - - * *******************************************************

'*** N U C L I D E MD A R E P O R T ***** '****************************************************************************** Detector Name: 5456 Sample Geometry: Sample Title: B306100AFJFC0 2 8GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nucli de MDA Activity Dec. Level Name (keV) (%) (pCi/sq m) (pCi/sq m) (pCi/sq m) (pCi/sq m)

+                              K-4 0                                       1 460. 82

10 .66 3.008E+003 3 .01E+003 2 .293E+004 1 . 1 66E+003 Cr-51 320.08 9.91 6.955E+015 6.95E+015 -l.501E+015 3 . 3 84E+015 Mn- 54 834.85 99.98 4.926E+003 4.93E+0 0 3 -1.974E+002 2 .173E+003 Co-58 810.76 99.45 l.543E+007 l.54E+007 -2 . 3 79E+007 6.642E+006 Co-60 1173. 2 3 99.85 l. 2 44E+00 3 l.24E+00 3 7.007E+002 5.750E+002 1 332 .49 99.98 1. 25 0E+003 1.462E+003 5.744E+002 Nb-94 7 02 .65 99.81 3.689E+002 3 .69E+00 2 -1. 414E+00 2 l.610E+002 871. 09 99.89 3.692E+002 l.381E+002 l.581E+002 Sn-113 255.1 3 2 .11 3.367E+007 1. 2 5E+006 2.482E+007 l.643E+007 391. 70 64.97 l.253E+006 - l.681E+004 6.090E+005 Cs-134 475.36 1. 48 2 .516E+005 l. 3 6E+003 5.355E+004 l. 22 4E+005 563.25 8.34 2 .789E+004 1.842E+00 3 l. 32 8E+004 569.33 15.37 1. 457E+004 4.704E+00 3 6.924E+003 604.72 97.62 2 .743E+00 3 -2 .665E+003 l.312E+003 795.86 85 . 46 1 .358E+00 3 5.171E+002 5.992E+00 2 801. 95 8.69 l.403E+004 6.200E+003 6.225E+003 1038.61 0.99 1. 275E+005 3 .532E+004 5.565E+004 1167.97 1. 79 1 .305E+005 1.368E+005 6.048E+004 1 365.19 3.02 3.456E+004 3. 2 88E+002 1.417E+004

+ Cs-137 661.66* 85.10 8. 22 0E+00 2 8.22E+002 l.422E+005 3.826E+00 2 Eu-15 2 121.78 2 8.67 3 .889E+00 3 2 .03E+003 - 1. 491E+003 1.910E+00 3 2 44.70 7.61 l.539E+004 -8.496E+003 7. 51 6E+003 295.94 0.45 2 .675E+005 1. 23 7E+005 1.303E+005 344. 2 8 26.60 4.784E+003 1.707E+00 3 2 . 32 8E+00 3 367.79 0.86 1.413E+005 - 3 .456E+004 6.856E+004 411.12 2.24 6.471E+004 3 .905E+004 3 .149E+004 44 3 .96 2.83 5.506E+004 -2 .069E+004 2 .681E+004 488.68 0 .42 3.257E+005 1. 784E+005 l.577E+005 563.99 0. 4 9 2. 0 31E+005 1. 305E+005 9.672E+004 586.26 0.46 2.323E+005 -2 .055E+004 1 . 1 09E+005 678.62 0.47 9.373E+004 5.162E+004 4.1 2 2E+004 688.67 0.86 4.032E+004 5.786E+002 1.703E+004 719.35 0.28 1.641E+005 2 .640E+004 7.215E+004 778.90 12.96 3.701E+003 -3 .580E+00 3 1.628E+00 3 810.45 0. 32 l.412E+005 -7.189E+004 6.140E+004 867.37 4. 26 1.041E+004 1. 4 69E+00 3 4.482E+003 919.33 0.43 1. 2 68E+005 7.739E+00 4 5.595E+004 964.08 14.65 4.458E+003 2 .612E+003 2 .005E+00 3 1085.87 10. 2 4 6.107E+003 5.338E+003 2 .7 1 0E+00 3 1089.74 1. 73 3. 2 14E+004 7.161E+00 3 1.403E+004 1112.07 13.69 3.628E+00 3 -1.023E+004 1.553E+00 3 1212.95 1. 43 3.086E+004 4.073E+00 3 1. 2 80E+004 [286]

. ___ ..... __ . . _.......... -~-- - ..J/ .J.../ £. V.J.. I J * "':t I * ..J &:t: .t'1.l"'1 raye u Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/sq m) (pCi/sq m) (pCi/ sq m) (pCi/sq m) Eu-1 52 1249.94 0 .19 2.602E+005 2 . 0 3E+003 -3.585E+005 1.099E+005 1299.14 1. 63 2.819E+004 -5.108E+004 1.169E+004 1408.01 21. 07 2.032E+00 3 -9.726E+00 2 8. 2 1 1E+002 1457.64 0 .50 2.981E+00 5 5.926E+005 1.407E+005 1528.10 0. 2 8 1.056E+005 2 . 2 74E+004 3 .740E+004 Eu- 1 54 123.07 40.4 0 3.036E+003 1.69E+00 3 -8.105E+001 1.491E+003 2 47.9 3 6.89 1.811E+004 -3 .531E+00 3 8.837E+003 591. 76 4.95 2.128E+004 -9.405E+00 3 1.010E+004 692.42 1. 78 2.134E+004 -4.931E+00 3 9.012E+00 3 723.30 2 0.06 2.675E+003 6.084E+002 1.187E+00 3 756.8 0 4.5 2 1.166E+004 -1.763E+003 5.145E+003 873.18 12.08 3.887E+00 3 -2 .895E+003 1.664E+003 996. 2 9 10.48 5.5 0 0E+00 3 2 . 62 0E+003 2 .401E+003 1004.76 18.01 2.840E+003 1.886E+001 1 . 2 16E+00 3 1274.43 34.80 1. 686E+003 1 .5 3 0E+002 7.216E+002 1596.48 1. 80 1.863E+004 -3.435E+004 6.600E+003 Eu-1 55 45. 3 0* 1. 3 1 5.109E+004 4.50E+003 -6.716E+003 2 .453E+004 60.01 1. 22 1.032E+005 1.109E+003 5 .052E+004 86.55* 30.70 4 .505E+003 4.544E+00 3 2 .211E+003 105.31 21.10 6.749E+003 -3.292E+00 3 3.314E+00 3 Tl - 2 08 583. 1 9 85.00 1.079E+003 1.08E+003 9.341E+002 5.151E+00 2 Bi -2 11 3 51. 07 13.02 8.650E+00 3 8.65E+003 2 .966E+003 4. 2 10E+003 Pb-2 11 4 0 4.85 3 .78 3 . 2 72E+004 1. 36E+004 1.893E+004 1.593E+004 427.09 1. 76 7.333E+004 -1.999E+004 3.570E+004 832.01 3 . 52 1.356E+004 -1.042E+00 3 6.045E+003 Bi-212 39. 86 1. 06 5.916E+004 5.93E+003 -6.658E+004 2 .877E+004 727.33 6 . 67 5.931E+00 3 -8 . 3 67E+002 2 .608E+003 785.37 1.10 3 .662E+004 3.026E+003 1.605E+004 1 620.50 1 . 47 1. 4 34E+004 1.949E+003 4.533E+00 3 Pb - 2 1 2 115.18 0.60 1.662E+005 2 .51E+ 00 3 7.849E+003 8.168E+004 2 38 . 63 43.60 2.509E+003 7 .491E+002 1. 22 8E+00 3 300.09 3.30 3.098E+004 2 . 3 43E+004 1.508E+004 Pb212-XR 74.82 10.28 1 .067E+004 6.11E+00 3 2 . 2 99E+004 5 . 2 53E+00 3 77.11 17.10 6.112E+003 7.609E+OOO 3 .007E+00 3 87.35 3.97 2.510E+004 1.315E+00 2 1. 23 5E+004 89.78 1. 46 6.494E+004 2 . 800E+004 3.191E+004 Bi -2 1 4 609. 32 45.49 2.166E+00 3 2 .17E+00 3 2 .311E+00 3 1.036E+00 3 768.36 4.89 9.317E+00 3 - 2 .886E+003 4.155E+00 3 806.18 1. 26 3.246E+004 1.064E+004 l.422E+004 93 4.06 3. 11 1.618E+004 -5.389E+00 3 7.197E+003 11 2 0 .2 9 14.92 4.849E+003 2.227E+00 3 2.218E+003 1155.2 1 1. 63 2 .942E+004 -2 . 2 71E+004 1. 279E+004 1 23 8.12 5.83 9.055E+00 3 -8.577E+002 3.968E+00 3 128 0 .98 1.43 2.723E+004 -6.437E+003 l.1 2 9E+004 1377.67 3.99 1 .124E+004 -5.695E+003 4.747E+003 1385.31 0 .79 4.890E+004 2 . 2 80E+004 2.005E+004 1401.5 2 1. 33 3 .260E+004 4.782E+003 1 . 3 65E+004 1407.99 2 .39 1 .537E+004 -7.359E+003 6.212E+00 3 1509. 2 1 2 .13 1 .926E+004 -2 .062E+003 7.896E+00 3 1661. 2 7 1. 05 2 .999E+004 - 2 .856E+004 1 .123E+004 [287]

.., ....,

           **-** **-t' - - -                                      -'/..J../L..V..L/     .J * ~ I * ...J "'% .C"l.J.*.1        J:" Q'::jC:

Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV ) ( %) (pCi/sq m) (pCi/sq m) (pCi/sq m) (pCi/sq m) Bi-2 14 1729.59 2 .88 1.121E+004 2 .17E+003 3 .125E+ 0 03 4.198E+003 1764.49 1 5.30 4.117E+00 3 1.900E+003 l.790E+00 3 1847.43 2 . 03 1.849E+004 6.158E+00 3 7.163E+00 3

   >                         2 118.51      1.16    O.OOOE+OOO                           O.OOOE+OOO                      O.OOOE+OOO Pb- 2 14            2 41.99     7. 2 5  1.456E+004 3 .17E+00 3 5.535E+003                                    7.120E+003 2 95. 22  18.42     5.600E+003                          1.026E+003                       2 . 72 8E+003 351. 93   35.60     3.169E+003                          2 .387E+003                      l.543E+00 3 785.96     1. 06    3.611E+004                        -1.919E+004                        1. 570E+004 Pb2 1 4-XR            74.8 2   5.80     1.893E+004 1.08E+004 4.081E+004                                      9. 3 23E+00 3 77.11     9.70    1.079E+004                          1. 3 43E+001                     5 . 3 08E+003 87.35     2.24     4.455E+004                          2 .334E+002                      2 .191E+004 89.78     0.82     1.1 5 8E+005                        4.992E+004                       5.689E+004 Ra-226              186.21     3.64     2 .801E+004 2 .80E+004 8. 2 69E+00 3                                 1.374E+004 Ac-228              129.07     2.42     4.007E+004 2 .03E+003 - 9.415E+00 3                                  1.968E+004 209.25      3.89     2.833E+004                          1.786E+004                      1. 3 89E+004 270. 2 4    3.46     2.911E+004                          8.236E+003                      1.420E+004 32 8.00     2.95     3.577E+004                        -1.581E+004                       1. 740E+004 338. 32   11.27      9.060E+00 3                       -6.772E+003                       4.401E+00 3 409.46      1. 92    6.300E+004                        - 5. 2 32E+004                    3 .064E+004 463.00      4.40    3.249E+004                           1. 3 59E+004                    1.584E+004 794.95      4.25     9.806E+003                          1. 2 92E+003                    4. 3 12E+00 3 91 1. 20  2 5.80    2 .0 3 0E+00 3                    -4.494E+002                        9.092E+00 2 964.77      4.99    1.086E+004                           1.045E+00 3                     4.864E+00 3 968.97    15.80     3.438E+00 3                          5.336E+00 2                     1.540E+00 3 1 588.20       3 . 22  l.237E+004                           5. 2 65E+00 3                   5.000E+00 3 Pa- 2 31              27.36*  1 0.30    5.295E+003 5 .30E+00 3 1.456E+004                                    2 .564E+003 283.69      1. 70   5.7 3 1E+004                         8.429E+00 3                     2 .790E+004 300.07      2.47    4.1 3 9E+004                         3.130E+004                      2 .015E+004 3 02.65     2.20    4.590E+004                        - 2 . 2 54E+004                    2 . 23 4E+004 330.06     1. 40    7.824E+004                          1.157E+005                       3 .810E+004 Th-234                92.38    2.13     1.738E+018 1.74E+0 1 8 1.180E+018                                    8.542E+017 92.8 0   2 .10    1. 771E+018                         1.252E+018                       8.703E+017 112.81      0.2 1    1. 783E+01 9                        3 .056E+018                      8.760E+018 U-235              143.76     10.96     8.795E+00 3 1.78E+003 1. 25 0E+003                                   4.317E+00 3 163. 33     5.08     1.850E+004                        -5 .5 9 6E+00 3                    9 .067E+00 3 185.71     57.20     1.779E+003                          1. 0 33E+00 3                    8.725E+002 202.11      1. 08    1 .019E+005                       -5.581E+004                        4.999E+004 2 05. 3 1   5.01     2.223E+004                        -8.245E+002                        1. 091E+004

+ Am-2 41 59.54* 35.90 1.213E+00 3 1. 2 1E+003 - l.595E+002 5 .825E+00 2

         + = Nuclide identified during the nuclide identification
         * = Energy line found in the spectrum
         > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
         @ = Half-life too short to be able to perform the decay correction

[288]

"*************************      ' *************************            k***************
"***        G A M M A     S P E C T R U M          A N A L Y S .L S               *****
'***********************************************************************
.lename: C:\User s \Zion Solutions\Documents\5-3-16\B306100AFIWC030GD.CN iport Generated On                    5/3/2016       1 2 :58 :2 7 PM tmple Title                           B306100AFIWC030GD tmple Description                     UNIT- 2 tmple Identification tmple Type tmple Geometry iak Locate Threshold                    3 .00 iak Locate Range (in channels)             85 -    8192 iak Area Range (in channels)               85 -   8192 lentification Energy Tolerance           10.000 keV tmpl e Size                             1. OOOE+OOO SQM tmple Taken On

quisition Started 5/3/2016 10: 2 1:0 2 AM

.ve Time 600.0 seconds ial Time 600.7 seconds iad Time 0. 12 % Energy Calibration Used Done On 1/1 3/ 2 015 Efficiency Calibration Used Done On 5/3/2016 Efficiency ID STWALL

                                                                ~dly
                                                                 /,.'1-6-1&1
                                                                   //16

[289]

ia k Anal y sis Report 5/ 3/2 01 6 12 : 5 8:27 PM Page 2 "************************************************************************

- - - P E A K A N A L Y S I S R E P O R T *****

Detector Name: 545 2 Sample Title: B306100AFIWC0 3 0GD Peak Analysis Performed on: 5/3/2016 12:58: 2 7 PM Peak Analysis From Channel: 85 Pea k Analysis To Channel: 81 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid ( keV) ( keV ) Area Uncert. Counts 1 947- 96 1 954. 00 23 8.35 0.59 4.55E+001 3 1. 3 8 6.95E+001 2 2429- 24 41 2433.85 608.64 0.86 4.40E+001 2 0.47 2 .30E+001 3 5828- 585 1 5839.46 1460.1 3 1. 32 1.56E+00 2 2 8.05 1.07E+001 First peak in a multiplet region = Other peak in a multiplet region = Fitted singlet ~rors quoted at 2 .000 sigma [290]

1t erference Corrected Acti * -Y Report 5/3/2 016 12 3:27 PM Page 3 "* * ********************************************************************* "*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** "*********************************************************************** Sample Title: B306100AFIWC030GD Nucl ide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nucl ide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM ) Uncertainty K-40 0. 999 1460.82* 10.66 1. 0 5762E+006 2 .10842E+0 0 5 Pb-21 2 0 .87 2 115.18 0.60 238.63* 43.60 3.01270E+004 2 .13402E+004 300.09 3 .30

       * = Energy line found in the spect rum .
       @ = Energy line not used for Weighted Mean Activity Energy Tolerance :      10.000 keV Nuclide confidence index threshold          0 .30 Errors quoted at 2 .000 sigma

[291]

1terference Corrected Act i * -Y Report 5/ 3/2 01 6 12 3:2 7 PM Pag e 4 "************** * * ******************************************************* "*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** "*********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0 .999 1 . 057617E+006 2 .1084 2 5E+005 Pb-2 1 2 0. 87 2 3 . 012696E+004 2 .134018E+004

      ?     Nuclide is part of an undetermined solution X   = Nuclid e rejected by the interference analysi s
      @     Nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at         2.000 sigma
 **********       U N I D E N T I F I E D           P E A K S         **********

Peak Locate Performed on: 5/3/2 01 6 1 2 :58: 2 7 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Peak Energy Peak Size in Peak CPS Peak Tol . No . (keV) Counts per Second %~ inty Type Nucl ide 2 608.64 7 .3327E- 00 2 Tol. Zr- 97 V Sb-125 Sb-125 Cs - 1 34 Bi -2 14 M = First peak in a multipl et region m Other peak in a multipl et region F Fitted singlet Errors quoted at 2 .000 sigma [292]

1clide MDA Report 5/3/2 0 16 ~2 : 58: 2 7 PM Page 5

- - - N U C L I D E MD A R E P O R T *****

Detector Name: 54 52 Sample Geometry : Sample Title: B306100AFIWC030GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec . Lev e l Name (keV ) (%) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) K-40 1 460.82* 10 .66 l.598E+005 l.60E+00 5 l .058E+006 7.074E+004

Cr-5 1 320.08 9.91 l.361E+005 1. 3 6E+005 -1.076E+005 6.348E+004 Mn-54 834.85 99.98 l.327E+004 l. 33E+004 - 8.114E+002 5.903E+00 3 Co-58 810.76 99.45 l.534E+004 1. 53E+004 1.007E+004 6.947E+00 3 Co-60 11 73.23 99.85 l. 3 69E+004 1. 37E+004 6. 3 80E+003 5.974E+00 3 1 332 .49 99.98 1.498E+004 - 3 .855E+003 6.565E+00 3 Nb-94 702.65 99.81 l.249E+004 1 . 2 5E+004 -2 .756E+003 5.568E+003 871. 09 99.89 1.485E+004 1.213E+004 6.679E+003 Sn-113 2 55.13 2 . 11 6.773E+005 2 .11E+004 2 .739E+005 3.195E+00 5 391.70 64.97 2 .113E+004 -4.812E+003 9.790E+00 3 Cs -1 34 475.36 1. 48 8. 62 0E+005 1.89E+ 00 4 -5. 2 09E+005 3 .934E+00 5 563.25 8.34 l.558E+005 6.711E+ 0 03 7.066E+004 569.33 15.37 9.300E+004 7. 3 76E+003 4.254E+004 604.72 97. 62 2 .360E+004 -1.8 1 9E+004 1.116E+004 795.86 85.46 l.894E+004 4.639E+00 2 8.634E+003 801. 95 8.69 1 .642E+005 -l.252E+005 7.382E+004 1038.61 0.99 l .555E+006 -4.574E+004 6.951E+005 1167.97 1. 79 9.112E+005 -3.886E+005 4.072E+005 1 365.19 3 . 02 3 . 454E+005 4.928E+003 1.416E+005 Cs-137 661.66 85. 10 1 .890E+004 l.89E+004 5.262E+003 8.678E+00 3 Eu-152 12 1.78 2 8.67 6.030E+004 5. 3 4E+004 4. 22 4E+003 2 .906E+004 2 44.70 7 . 61 2.213E+005 1 . 21 5E+004 1.054E+005 2 95.94 0.45 3.967E+006 5.349E+006 1.886E+006 344. 2 8 26.60 5.337E+004 - 3.337E+004 2 .492E+004 367.79 0.86 l.528E+006 -2.873E+005 7.075E+005 411.12 2 . 24 6.502E+005 1.545E+005 3 .020E+005 443.96 2 .83 5.258E+00 5 5.115E+005 2 .440E+005 488.68 0.4 2 3.431E+006 2 .627E+006 l.581E+006 563.99 0.49 2.685E+006 -7.299E+005 l. 2 19E+006 586. 2 6 0.46 3.788E+006 3 .398E+006 l .7 5 9E+006 678.62 0.47 3.448E+006 -2 .076E+005 l.584E+006 688.67 0.86 1.737E+006 -4.895E+005 7.906E+005 719.35 0.28 4.934E+006 -7.094E+004 2 . 22 3E+006 778.90 1 2 .96 l.121E+005 2 .624E+004 5.058E+004 810.45 0. 32 4.753E+006 2 .224E+006 2 .152E+006 867.37 4. 2 6 3 .805E+005 2 .064E+005 1 . 72 8E+005 919.33 0.43 3 .513E+006 l.994E+005 l.577E+006 964. 0 8 14.65 1.362E+005 l.490E+005 6. 2 71E+004 1085.87 10.24 l.448E+005 - 6.421E+004 6.425E+004 1089.74 1. 73 8. 5 86E+005 5.194E+005 3.810E+005 1112.07 1 3 .69 l.184E+005 -8.939E+004 5. 3 05E+004 1212.95 1. 43 1.308E+006 -2 .755E+005 5 .9 2 3E+00 5 [293]

1cl i de MDA Report 5/3/ 2 016 ~2: 58: 27 PM Page 6 Nuclide Energy Yi eld Line MDA Nuclide MDA Activit y Dec. Level Name (keV) ( ~) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM) Eu- 1 52 1249.94 0.19 9. 2 60E+006 5.34E+004 1.866E+006 4. 1 56E+006 1299.14 1. 63 8.861E+005 3 .579E+005 3.868E+005 140 8. 01 21.07 7.525E+004 -2 .682E+004 3.309E+004 1457.64 0.50 9.305E+006 2 .564E+007 4.459E+006 1528 . 10 0. 2 8 3 .158E+006 -1.216E+006 l. 22 3E+006 Eu-154 123.07 40.40 4. 2 67E+004 4. 2 7E+004 7.275E+003 2 .056E+004 247.93 6.89 2 .095E+005 - 1.685E+005 9.895E+004 591.76 4.95 2 .691E+005 6.518E+00 3 l.220E+005 692.42 1. 78 8.081E+005 3.254E+00 5 3.664E+005 723.30 2 0.06 6.176E+004 -2 .083E+004 2 .748E+004 756.80 4. 52 2 .857E+005 -7. 2 85E+004 1. 27 4E+005 873.18 12. 08 1.166E+005 -8.862E+003 5.213E+004 996. 2 9 10.48 1. 4 92E+005 -3.713E+004 6.696E+004 1004.76 18.01 8.566E+004 - 8.579E+004 3.837E+004 1274.43 34.80 4.519E+004 -2.931E+003 2. 000E+004 1596.48 1. 80 5.090E+005 1.695E+005 1.972E+005 Eu -155 45.30 1. 31 1 . 052E+006 7.44E+004 1.075E+006 5.024E+005 60.0 1 1. 22 1 .362E+006 -7. 2 78E+005 6.556E+00 5 86.55 30.70 7.439E+004 4.891E+004 3 .6 1 8E+004 105. 3 1 21.10 8.699E+004 -7. 2 07E+004 4.202E+004 Tl-208 583.19 85.00 2 .125E+004 2 .12E+004 1.989E+004 9 . 899E+003 Bi-211 351. 07 13.02 1.432E+005 1.43E+005 2 .034E+005 6.794E+004 Pb-211 404.85 3.78 4.140E+005 4.14E+005 2 .481E+005 1 .934E+005 427.09 1. 76 8.560E+005 4. 3 83E+005 3 .981E+005 832.01 3.52 4.259E+005 -5.223E+004 1.922E+005 Bi-212 39.86 1. 06 1 . 2 15E+006 1 .82E+005 3.494E+005 5.784E+005 727.33 6.67 1.824E+005 -5.315E+004 8.095E+004 785.37 1.10 1 . 238E+006 3.261E+005 5.545E+005 1 620.50 1. 47 6 . 853E+005 -2.875E+004 2 .7 1 9E+005 + Pb-2 1 2 11 5.18 0.60 3.074E+006 3 .27E+004 -1.318E+006 1.485E+006 238.63

43.60 3.265E+004 3.013E+004 1.543E+004 30 0 . 0 9 3.30 4.910E+005 - 4.015E+005 2 .322E+005 Pb212-XR 74.8 2 10.28 2.4 1 9E+005 1. 3 5E+005 4.328E+005 l.179E+005

77. 11 17.10 1. 34 6E+005 1.137E+005 6.548E+004 87.35 3.97 5.804E+005 7. 22 1E+005 2 .824E+005 89.78 1. 46 1 .497E+006 3 .145E+005 7.273E+005 Bi -2 14 60 9.32 45.49 5 . 084E+004 5.08E+004 6.184E+004 2 .403E+004 768.36 4.89 2 .709E+005 -5.654E+004 1.211E+005 806.18 1. 2 6 1. 2 04E+006 5.559E+005 5.451E+005 934. 0 6 3 .1 1 4.142E+005 -2 .530E+005 1.8 2 1E+005 1120.29 14.9 2 1. 2 86E+00 5 1.870E+004 5.863E+004 1155.2 1 1. 63 9 . 934E+005 -6.006E+004 4.440E+005 1238.12 5.83 3.792E+005 2 .695E+005 1.743E+005 1 2 80.98 1. 43 9 . 968E+005 3 .770E+005 4.352E+005 1377.67 3.99 3 .518E+005 -1.337E+005 1. 52 2E+005 1385.31 0.79 1.775E+006 -1.116E+006 7.681E+005 1401. 52 1. 33 1.245E+006 3.893E+005 5.511E+005 1407.99 2 .39 6.623E+005 - 2 .360E+005 2 .912E+005 1509. 2 1 2 .13 7.563E+005 9.501E+004 3 . 3 14E+005 1661. 2 7 1. 05 8.951E+005 -l.425E+006 3 .467E+005

[294]

1clide MDA Report 5/3 / 2 016 ~2 : 58: 2 7 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi / SQM) (pCi/SQM ) (pCi/SQM) Bi -2 14 1729.59 2 .88 2 .991E+005 5 .08E+004 8.334E+004 1.119E+005 1764.49 15.30 1.535E+005 1.693E+005 6.961E+004 1 847.43 2 .0 3 7.127E+005 1.586E+005 3 .010E+005

 >                2 118.5 1       1.16    O.OOOE+OOO                    O.OOOE+OOO      O.OOOE+OOO Pb- 2 14     2 41.99       7. 2 5  2 .735E+005    5.18E+004      1. 3 01E+004    1. 3 13E+005 2 95.22     18.42     9.527E+004                    4.849E+004      4. 52 7E+004 351.93      35 .60    5.179E+004                    3 .893E+004     2 .456E+004 785.96        1. 06   1. 24 0E+006                -6 .073E+005      5.531E+005 Pb214-XR       74.8 2      5.80    4.287E+005     2 .37E+005     7.671E+005      2 .090E+005 77.11       9.70    2 .373E+005                   2 .004E+005     1.1 5 4E+005 87.35       2 . 24  1.029E+006                    1.280E+006      5.004E+005 89.78       0.82    2.666E+006                    5.600E+005      1. 2 95E+006 Ra-22 6       186. 2 1     3 .64    4.364E+005     4. 3 6E+005   2.132E+005      2.087E+005 Ac-22 8       129.07       2 .4 2   7. 33 3E+005   8.77E+004    -6.061E+004      3.537E+005 209.25       3 .89    4.069E+005                  -1.151E+005      1.941E+005 27 0 . 2 4   3 . 46   4.501E+005                  -3 .014E+004     2 .130E+005 328. 00      2 .95    4.950E+005                   5.180E+004      2 .319E+005 338.32     11. 2 7   1.549E+005                    1. 2 63E+005    7.332E+004 409. 4 6     1. 92   7.620E+005                    1.382E+005      3.542E+005 463. 00      4.40    3 .217E+005                 -8.647E+004       1.484E+00 5 794.95        4. 2 5  3 .807E+005                   9. 32 4E+00 3   1.735E+00 5 911.20      25 .80    8.766E+004                    1. 25 3E+005    4.086E+004 964.77        4.99    4.078E+005                    5.602E+005      1 .881E+005 968.97      15.80     1. 2 53E+005                  3.048E+004      5.765E+004 1588.2 0       3 . 22  2 .189E+005                 -9.135E+004       7 . 756E+004 Pa -2 31       27.36     10.30     7.659E+004     7.66E+004      4.685E+004      3.5 27E+004 283.69        1. 70   8.272E+005                  -7.582E+004       3 .885E+005 300.07        2 .47   6.560E+005                  -5.364E+005       3 .1 02E+005 302.65        2 . 20  6.941E+005                    l.952E+005      3.270E+005 330.06        1. 40   1.085E+006                    9.936E+004      5.095E+005 Th- 234        92.38       2 .1 3  9.635E+005     9.64E+005    -2 .332E+005      4.671E+005 92.80       2 .1 0  9 . 909E+005                  1.248E+006      4.8 0 6E+005 11 2.8 1      0. 2 1  9.104E+006                    3 .401E+006     4.4 0 4E+006 U- 235       14 3.76     10.96     1 .565E+005    2 .77E+004     2 .693E+003     7.534E+004 1 63.33      5.08     3 .117E+005                   1.688E+005      1. 4 94E+005 185.71      57. 2 0   2 .774E+004                 -4.710E+003       1. 32 7E+004 2 02.11      1. 08    1.496E+006                    8.509E+005      7.150E+005 2 05.31      5.01     3.067E+005                  -1. 649E+005      1.461E+005 Am-241         59.54     35.90     4. 630E+004    4.63E+004    -6.935E+0 0 3     2.228E+004
    +=Nuclide identified during the nuclide identification
    * = Energy line found in the spectrum
    >     Calculated MDA is zero due to zero counts in the region, or the region i s outside the spectrum, or MDA has not been calculated
    @ = Half-l ife too short to be abl e to perform the decay correction

[295]

"************************* *   *************************          ****************
"***         G A M MA     S P E C T R U M         A N A L Y S .L S                  *****
"***********************************************************************
.lename: 54 52 iport Generated On                 5/ 3 /20 1 6     10:50:50 AM tmple  Title                       B306100AFIWC031GD          " ~~     s T"Ct>---- -ht ~

tmple Description UNIT-1 tmple Identification tmple Type tmpl e Geometry iak Locate Threshold 3. 00 iak Locate Range (in channels ) 85 - 8 1 92 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmpl e Size 1.000E+OOO SQM tmple Taken On

quisition Started 5/3/2016 10:40:48 AM

.ve Time 600.0 seconds ial Time 600.6 seconds iad Time 0.09 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 5/3/2 01 6 Efficiency ID STWALL Po.to. \Jd),c\q_-\eJ k, 0~4 r

                                                                ;:i.- 1,--/'l
                                                                 /J/6-

[296]

!ak Analysis Report                         5/ 3/2 01 6     10:50:50 Afl.              Page   2
*************************************************************************
****                  P E A K        A N A L Y S I S            R E P O R T
*************************************************************************

Detector Name: 5452 Sample Title: B306100AFIWC0 3 1GD Peak Analysis Performed on: 5/3/2016 10:50:49 AM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8 1 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV ) Area Uncert. Counts 1 2 97- 309 30 1. 4 0 75.00 0.64 7.57E+001 51. 55 2 .20E+00 2 2 947 - 959 954.86 238.57 1. 2 4 5.33E+001 28.46 5.67E+001 3 1174- 1 1 88 11 82. 00 295.42 0.90 4.39E+001 2 1. 82 2 .61E+001 4 2 428- 2442 2435 .0 5 608.94 1.11 5.90E+001 19.63 1.30E+001 5 2 63 1 - 2653 2643.66 661.13 1. 45 2 .99E+002 38. 2 5 1.73E+001 6 58 2 6 - 5848 5838.06 1459.78 1. 98 1.55E+00 2 27.46 8.57E+OOO

= First peak in a multiplet region Other peak in a multiplet region
= Fitted singlet

rors quoted at 2. 000 sigma

[297]

1terference Corrected Acti* ~y Report 5/ 3 / 2 016 10 J:50 AM Pa ge 3 "************** * ******************************************************** "*** N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample Title : B306100AFIWC031GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( %) (pCi/SQM ) Uncertainty K-40 0.998 1460.82* 10 .66 1.05149E+006 2 .07020E+005 Cs-137 1. 000 661.66* 85.10 1 .69885E+005 2 .98 22 4E+004 Pb-212 0.975 115.18 0.60 2 38.63* 4 3 .60 3 .5 3 122E+004 1. 97001E+004 300.09* 3 . 30 4.28133E+005 2 . 23 900E+005

      * = Energy line found in the spectrum.
      @ = Energy line not used for Weighted Mean Activity Energy Tol erance :     10.000 keV Nuclide confidence index threshold             0 .3 0 Errors quoted at 2 .000 sigma

[298]

1terference Corrected Acti, -Y Report 5/3/2 01 6 10 ):5 0 AM Page 4

- - - I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 0.998 1 .051488E+006 2.07 01 99E+005 Cs-137 1. 000 1.698852E+005 2.982237E+004 Pb-212 0.975 3.832991E+004 1.9624 2 6E+004

      ?    Nuclid e is part of an undetermined solution X = Nuclide rejected by the interference analysis
      @ = Nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at        2 .000 sigma
 **********       U N I D E N T I F I E D          P E A K S       **********

Peak Locate Performed on: 5/ 3 /2016 10:5 0 :49 AM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. ( keV ) Counts per Second % Uncertainty Type Nuclide 1 75. 00 1 . 2 61 8E- 001 El Tol. Pb214-XR Ba-133 Pb212-XR Pb212-XR Pb214-XR 4 608.94 9.8345E-0 02 Tol. Zr-97 Sb-125 Sb- 125

                                                                                 & =?ii)

M = First peak in a multiple t region m Other peak in a multiple t region F Fitted singlet Errors quo t ed at 2 . 000 s igma [299]

1clide MDA Report 5/3/2 01 6 10:50:50 AM Page 5 "************** * *************************************************************** "*** N U C L I D E MD A R E P O R T ***** "****************************************************************************** Detector Name: 5 4 52 Sample Geometry: Sample Title: B306100AFIWC031GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( %) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) + K-40 1 46 0 .8 2

10.66 1.464E+005 1. 4 6E+005 1.051E+0 0 6 6 .406E+004 Cr-51 32 0 .08 9.91 1.4 2 8E+005 1.43E+005 -5. 2 46E+004 6.681E+004 Mn-54 834.85 99.98 1.478E+004 1.48E+004 1. 22 4E+004 6.659E+00 3 Co-58 8 1 0.76 99.45 1. 2 89E+004 1. 2 9E+004 -1.341E+003 5.717E+00 3 Co-60 117 3 . 23 99.85 1.575E+004 1.50E+004 -6.515E+003 7.005E+00 3 1 332 .49 99.98 1.498E+004 7.418E+00 3 6.565E+00 3 Nb-94 702.65 99.8 1 1 .407E+004 1 . 3 8E+004 - 1.166E+004 6.360E+00 3 8 7 1. 09 99.89 1. 3 82E+004 -2 .7 62 E+00 2 6.164E+003 Sn-113 2 55.13 2 .11 7. 2 64E+005 2 .48E+004 -3 .713E+005 3.440E+005 391.70 64.97 2 .478E+004 1.731E+004 1.161E+004 Cs-134 475.36 1. 48 1.069E+006 1.74E+004 -4.141E+005 4.968E+005 563.25 8.34 1.840E+005 -5 . 3 16E+004 8.471E+004 569.33 15.37 1.043E+005 -2 .036E+004 4.817E+004 604.72 97.62 2 . 32 7E+004 -1.061E+004 1.099E+004 795.86 85.46 1.744E+004 6.0 3 1E+00 2 7.882E+00 3 801.95 8.69 1.586E+005 5. 2 09E+004 7.103E+004 10 38.6 1 0. 99 1.667E+006 1 . 35 9E+006 7.508E+005 11 67.97 1. 79 8.940E+005 - 1.0 2 9E+005 3 .987E+005 1365.19 3 .0 2 3.833E+005 2 .070E+005 l.605E+005

+ Cs- 13 7 661.66* 85.1 0 1.686E+004 1.69E+004 l.699E+005 7.659E+00 3 Eu-152 121. 78 28.67 6.558E+004 5.97E+004 2.968E+004 3 .171E+004 244.70 7.61 2.243E+005 3.855E+004 1.070E+005 295.94 0.45 3.907E+006 2 .557E+006 1.856E+006 344. 2 8 2 6.60 5.967E+004 2 .167E+004 2 .806E+004 367.79 0 .86 1.785E+006 -2 . 2 79E+005 8.360E+005 411. 12 2. 2 4 6.905E+005 -9.105E+004 3 . 2 22E+005 44 3 .96 2 .8 3 6.100E+005 -1 .109E+005 2 .861E+005 488.68 0.4 2 3.149E+006 -2 .708E+006 l.440E+006 563.99 0.49 2.998E+006 -1. 3 14E+006 1. 3 76E+006 586.26 0. 4 6 3.848E+006 1.887E+006 1 . 790E+006 678. 62 0.47 3.013E+006 4.015E+005 1. 3 66E+006 688.67 0.86 1 .759E+006 1.486E+006 8.0 1 8E+00 5 719.35 0. 2 8 6.061E+006 3.427E+005 2 .786E+00 6 778.90 12.96 1 .085E+005 -1.080E+004 4.880E+004 8 10 .45 0. 32 3 .906E+006 -2 .965E+006 1.7 2 8E+006 867.37 4. 2 6 3 . 2 35E+005 -5.183E+005 1.442E+005 919.33 0.4 3 3.194E+006 8.799E+005 1.417E+006 964.08 14.65 1. 2 62E+005 1.350E+005 5.774E+004 1 085.87 10.24 1 . 3 85E+005 -1.586E+003 6.111E+004 1 089.74 1. 73 8.402E+005 -1.965E+005 3.718E+005 1 11 2 .07 13.69 1.072E+005 -1 .883E+005 4.745E+004 1 2 1 2 .95 1. 4 3 1. 32 7E+006 8.574E+005 6.018E+00 5 [300]

iclide MDA Report 5/3/2 01 6 10:50:50 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( %) (pCi/SQM) (pCi/SQM) (pCi/SQM ) (pCi/SQM) Eu-1 52 1249.94 0.19 8.934E+006 5.97E+004 -5. 2 55E+00 5 3 .993E+006 1299.14 1. 63 1.020E+006 -8.001E+00 5 4.536E+005 1408.01 2 1. 07 6.743E+004 -2 .401E+004 2 .918E+004 1457.64 0.50 9.154E+006 2 .401E+007 4.383E+006 1528.10 0. 2 8 3 .948E+006 1.841E+006 1.618E+006 Eu-154 12 3 .07 40.40 4.660E+004 4.52E+004 4.113E+004 2 . 2 53E+004 247.93 6.89 2 . 2 39E+005 - 2 .444E+005 1.062E+005 591.76 4.95 2 .910E+005 2 .555E+004 1.329E+005 692.42 1. 78 8.081E+005 2 .645E+005 3 .664E+005 723.30 2 0.06 7.711E+004 -3 .836E+004 3 .515E+004 756.80 4.52 3. 070E+005 -2 .055E+005 1.380E+00 5 873.18 12 .08 1.144E+005 2 .640E+004 5 .103E+004 996. 2 9 10.48 1.662E+005 -6 .723E+004 7.544E+004 1004.76 18.01 9.841E+004 -5 .607E+004 4.474E+004 1274.4 3 34.80 4.519E+004 -1.480E+004 2 .000E+004 1596.48 1. 80 7. 3 82E+005 1.483E+005 3. 118E+005 Eu-155 45.30 1. 31 8.775E+005 7.49E+004 -2 .506E+005 4.150E+005 60.01 1.22 1.348E+006 -6. 3 13E+005 6.482E+005 86.55 30.70 7.489E+004 7.476E+004 3 .643E+004 105. 3 1 2 1.10 9.001E+004 8. 23 4E+003 4.353E+004 Tl -2 08 583.19 85.00 2 .045E+004 2 .04E+004 1.179E+004 9.498E+00 3 Bi -2 11 351.07 13.02 1.403E+005 1.40E+005 8.471E+004 6.647E+004 Pb-2 11 404.85 3 .78 4.168E+005 4.05E+005 -2.395E+005 1.948E+005 427.09 1. 76 9. 32 0E+005 -1.510E+005 4.361E+005 832.01 3.52 4.054E+005 -5. 2 80E+004 1.820E+005 Bi-212 39.86 1. 06 1.124E+006 2.38E+005 -4.655E+005 5. 32 4E+005 727.33 6.67 2 .383E+005 1. 2 06E+005 l.089E+005 785.37 1.10 1.344E+006 2. 804E+005 6.074E+005 1620.50 1. 47 7.850E+005 3.659E+00.5 3. 2 18E+005

+     Pb-2 1 2    115.18     0.60   3.139E+006       2 .84E+004 -1.589E+006     1.517E+006 23 8.63* 43 .60   2.842E+004                    3 .531E+004   1.331E+004 300.09*    3.30   3.047E+005                    4.281E+005    1.391E+005 Pb2 12 -XR   74.8 2  10.28    2.455E+005       1.35E+005 4.967E+005       1.197E+005 77.11   17.10    1.349E+005                  -2 .128E+004    6.563E+004 87.35     3.97   5.824E+005                    9.402E+005    2.833E+005 89.78     1. 4 6 1.456E+006                  -1. 54 6E+006   7.066E+005 Bi - 2 14   609. 32  45.49    4.940E+004       4.94E+004 7.242E+004       2 . 3 32E+004 768. 36    4.89   3.127E+005                  -1.275E+005     1.420E+005 806.18     1. 2 6 1.093E+006                    8.374E+004    4.895E+00 5 934.06     3.11   5.356E+005                    3 .645E+005   2 .429E+005 1120.29   14.92    1 .334E+005                   7.738E+004    6.102E+004 1155.2 1    1. 63  9.747E+005                  - 9.739E+004    4.346E+005 1238.1 2    5.83   3 .415E+005                   2 . 3 85E+005 1 .555E+005 1280.98     1. 43  1.124E+006                    3 . 3 90E+005 4.985E+005 1377.67     3 .99  3 .926E+005                   2 .106E+005   1.726E+005 1385.31     0. 79  1.881E+006                    7.969E+005    8. 211E+005 1401. 52    1. 33  1.065E+006                    7.415E+005    4.611E+005 1407.99     2 .39  5.935E+005                  - 2 .113E+005   2.568E+005 1509.21     2 .13  5 .482E+005                   2 .764E+005   2 .273E+005 1661.27     1. 05  1.051E+006                    4.471E+005    4.246E+005

[301]

iclide MDA Report 5/ 3/2 01 6 ~0 :50:50 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activit y Dec. Level Name (keV ) ( %) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM ) Bi -2 14 1729.59 2 .88 5 . 22 9E+005 4.94E+004 3 . 33 4E+005 2.239E+005 1764.49 15.30 1.349E+005 1. 2 70E+005 6.029E+004 1847.4 3 2 .03 6.144E+005 2 .864E+00 5 2 .518E+005

  >               2 118.51      1.16    O.OOOE+OOO                     O.OOOE+OOO     O.OOOE+OOO Pb- 2 14     241.99      7.25    2.807E+005      5 .18E+004 -6. 3 79E+004      1.349E+005 2 95. 22  18.42     9.490E+004                     2 . 3 88E+004  4.509E+004 351.93    35.60    5.179E+004                      4.016E+004     2 . 456E+004 785.96      1. 06  1.398E+006                      2 .809E+005    6.317E+005 Pb2 1 4-XR      74.8 2    5.80    4.352E+005      2 . 3 8E+005 8.803E+005       2 .122E+005 77.11     9.70   2 . 3 78E+005                 -3 .752E+004     1.157E+005 87.35     2 . 24 1.032E+006                      1 .666E+006    5.022E+005 89.78      0.82   2 .592E+006                   -2 .753E+006     1.258E+006 Ra- 2 26     186. 21      3.64   4.777E+005       4.78E+005 -7.882E+004         2.294E+005 Ac-228       1 2 9.07     2 .4 2 7.176E+005       7.60E+004 -3.727E+005         3.458E+005 2 0 9.25     3.89   4.343E+005                     2.263E+005      2.077E+005 270.24       3 .46  4.620E+005                     3.734E+004      2.190E+005 328.00       2 .95  4.563E+005                    -3 .806E+005    2.126E+00 5 338.3 2    11. 2 7  1.535E+005                      6. 2 16E+004  7.262E+004 409.46       1. 92  8. 2 52E+005                 -3 .088E+005     3.858E+005 463. 00      4.40   3.568E+005                   -3.426E+004      1.659E+005 794.95       4.25   3.505E+005                   -2.391E+005      1.584E+005 911. 2 0   2 5.80   7.597E+004                     1.913E+004     3.502E+004 964.77       4.99   3.664E+00 5                    3.006E+005     1.674E+005 968.97     15.80    1.187E+005                     7.432E+004     5.435E+004 1588.20        3 . 22 5. 2 92E+005                   2.511E+005     2 . 32 7E+005 Pa- 23 1       27.36    10.30    6.845E+004       6.85E+004 2.223E+004         3.120E+004 283.69      1. 70   9.760E+005                     7.085E+005     4. 62 9E+005 300. 0 7    2.47    6.590E+005                   -1.819E+005      3 .117E+005 3 02 .65    2.20    7. 2 95E+005                   7.724E+005     3 .447E+005 330.06      1. 40   9.716E+005                   - 1.001E+006     4. 52 9E+005 Th- 23 4       92.38     2.13    9.595E+005      9.59E+005 1.606E+005          4. 65 1E+005 92.80     2.10    9.704E+005                   - 1.293E+005     4.704E+005 112.81      0. 2 1  9.366E+006                     3.613E+006     4.535E+006 U-23 5       143.76     10.96    1.521E+005      3 .04E+004 -4.488E+004        7. 3 14E+004 163.33      5.08    3 . 3 20E+005                -1.586E+005      1.595E+005 185.71     57. 2 0  3 .043E+004                  -6.671E+003      1.461E+004 2 02 . 1 1  1. 08   1.581E+006                   -1.137E+006      7.572E+005 2 05. 3 1   5.01    3.388E+005                   - 1.617E+005     1 .622E+005 Am-241         59.54    35.90    4.436E+004      4.44E+004 -4.473E+ 00 4       2 . 1 3 1E+004
     +=Nuclide identified during the nuclide identification
     *=Energy line found in the spectrum
     >= Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
     @ = Half-life too short to be able to perform the decay correction

[302]

' ***        GAMM A       S P E C T R U M         A N A L Y S I S          *****
'************** * ************************* * ******** ~******* * ***** ~****** ~

_lename: 54 52 iport Generated On 9/ 1 3/20 1 6 2:31:45 PM tmple Title B306100BFRFC007GD tmpl e Descriptio n Steam Tunnel Unit-1 tmple Identification 007 tmple Type tmple Geometry 1 meter iak Locate Threshold 3 .00 iak Locate Range (in channels ) 85 - 8192 ~ak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Size 1.000E+OOO S meters tmple Taken On

quisition Started 9/13/ 2 01 6 2:21:42 PM

.ve Time 6 00 . 0 second s ial Time 6 01 .5 seconds ,ad Time 0 .25 i Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 8/9/2016 Efficiency ID UNNELSTS 1 METER DATA VALIDATED DATE 1- B-t1 TIME osoo Q.?~' [303]

J /.J...J/ L V.J..U L ; .J .J.. ; <,+/- ..J r L'l

' ** * ** 1 * ********************************************* * **** * *********** * ** ' *** P E A K A N A L Y S I S R E P O R T ***** '*************************** * ******************************************** Detector Name: 545 2 Sample Title: B306 1 00BFRFC007GD Peak Analysis Performed on: 9/13/2 01 6 2 :31:44 PM Peak Anal y sis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts 1 288- 307 300.37 74.75 0.74 2 .93E+002 115.05 8.59E+002 2 949- 960 955.4 2 23 8.71 1. 35 6.69E+001 42.78 1.56E+002 3 11 75 - 1190 1180.87 295.13 0.83 8.65E+001 39.58 1.00E+00 2 4 1348 - 1357 1352.88 338. 1 8 0.4 2 l .38E+001 2 1. 97 4.72E+001 5 1400 - 1416 1407.76 351. 91 0.74 l.54E+002 4 0 .64 8.16E+001 6 2037- 2047 2042.20 51 0 .66 1. 01 2 .62E+001 22 .68 4.28E+001 7 2327- 2339 2333.44 583.5 2 0.39 5.73E+001 21. 1 3 2 .07E+001 8 2428- 2446 2 436.54 609.31 1. 32 1 .97E+00 2 35.94 3 .75E+001 9 3635- 3650 3643.01 911. 07 0.41 5. 52 E+001 20.88 1 .78E+001 10 4472- 4487 4479.63 1120. 2 5 1.10 5.19E+001 2 1. 80 2 . 2 1E+001 11 4948- 4959 4953.66 1238.75 1. 03 2 .35E+001 15.11 1. 2 5E+001 12 5832- 5854 5843. 23 1461.07 1. 44 3 .09E+002 37.45 1.lOE+OOl 13 7052- 7067 7 0 60.19 1765.1 2 0.45 4.71E+001 16.16 5.89E+OOO = First peak in a mult iplet region = Other peak in a mult iplet region Fitted singlet rors quoted at 2 . 000 sigma [304]

ll...eriereuce I....ULL\:::C Leu l"iCL.L V .L LY r<.e_!JUL L ::J / .L.:)/ L U .L O L;.:) .L ; 'f J .t"l'J .t'a.ye .:) ' ****************************1****************************************** '*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** '************** * ******************************************************** Sample Title: B306100BFRFC007GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL . NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( ~o ) (pCi/S me) Uncertainty K-40 1. 000 1460.8 2* 10.66 1.61 62 4E+007 ~ .40944E+006 Sr-85 0.98 2 5 14.01* 96.00 8.70872E+004 7.6337.2E+004 Ba-1 33 0. 322 79.61* 2 .65 1. 77645E+007 7.86081E+006

81. 00 32 .90 2 76.40 7.16 3 02.85* 18.34 1.09566E+006 5. 312 11E+005 3 56.01* 62.05 6.41027E+005 1. 974 3 3E+005 3 83.85 8.94 Tl -2 0 8 1.000 583. 1 9* 85.00 2 . 32 181E+005 8.99971E+004 Pb-212 0.975 115. 1 8 0.60 238.63* 43.60 3 .14441E+005 2 .07 3 81E+005 300.09* 3.30 6. 08 92 1E+006 2 .95467E+006 Bi-214 0. 612 609.32* 45.49 1. 52 158E+006 3.33025E+005 768.36 4 .89 806.18 1. 2 6 934.06 3.11 1120. 2 9* 1 4.92 1. 68162E+006 7.1 942 9E+00 5 1 155. 2 1 1. 63 1238.1 2* 5.83 2 .04731E+006 1. 32 822E+006 1280.98 1. 43 1377.67 3 . 99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 1661. 27 1. 05 17 2 9.59 2.88 1764.49* 15.30 1.9 327 9E+006 6.80799E+005 1847.43 2.03 2 118.51 1.16 Pb-2 14 0.977 241. 99* 7.25 1.8 9 072E+006 1. 24625E+006 2 95. 22* 18.42 1. 0 9 090E+006 5. 2 8699E+005 351.93* 3 5.60 1.117 3 0E+006 3.44150E+005 785.96 1. 06

       * = Energy l ine found in the spectrum.
       @ = Energy l ine not used for Weighted Mean Activity Energy Tolerance :                  10.000 keV Nuclide confidence index threshold                                  0.30 Errors quoted at 2.000 sigma

[305]

1 1...t::LLt::Lt::U\....t:: \....ULL C::\.... LC::U r:l.\....L..L.V..L.LY J:'\.t::]:--'ULI... ::J / ..L..J/ L U..L.U L ; -J .l. * ":I: J r l"l ' ****************+************************************ * ***************** '*** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** '********************************************************************* *

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/S me ) Uncertainty K-40 1. 000 1.6162 40E+007 2 .409441E+006 Sr-85 0.98 2 8.708724E+004 7.6337 2 5 E+004 Ba-133 0. 32 2 3.020642E+005 8.948579E+005 Tl-208 1. 000 2.321810E+005 8.999706E+004

     ~
     "-.... Bi-211                     0.999 Pb-212                    0.975                         2 .115146E+00 5                     3 . 22 6768E+005 Bi-214                     0.612                         1. 630877E+006                      2 .704369E+005 Pb-214                     0.977                         6.378 3 72E+005                     1. 40793 1E+00 6
             ?        Nuclide is part of an undetermined solution X    = Nuclide rejected by the interference analysis
            @ = Nuclide contains energy l ines not used in Weighted Mean Activity Errors quoted at                              2 . 000 sigma
  **********                      U N I D E N T I F I E D                                       P E A K S               **********

Peak Locate Performed on: 9/13/ 2 01 6 2:3 1:44 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8 1 92 Pea k Energy Peak Si ze in Peak CPS Peak Tol. No. (keV) Counts per Second % Uncertainty Type Nuclide 4 338.18 2 . 2 992E-0 02 159. 2 2 Tol. Eu-152 Th-227 Th-227 Ac-228 Pa-231 9 911. 07 9.1924E-002 37.86 Sum M First peak in a multiplet region m = Other peak in a multiple t region F = Fitted singlet Errors quo t ed at 2 .000 sigma [306]

tC.L.Lue 1*1ul"i rs..e1-1uL L ::;, / .L..J/ L U.LU L. * ..J .1- * ':f ..J r 1*1 '** * *********** * ****************** ~************************ * *** * *************** '*** N U C L I D E MD A R E P O R T **** -r ' ************** * ***************** * ********************************************* Detector Name: 5 4 52 Sample Geometry: 1 meter Sample Title : B306100BFRFC007GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( ';; ) (pCi/S me ) (pCi/S me ) (pCi/S me ) (pCi/S me)

+       K-40                 1460.8 2

10.66 1. 2 50E+006 1.25E+006 1.616E+007 5.545E+005 Cr-51 320. 0 8 9.91 1. 680E+006 1.68E+006 8. 23 3E+005 8 .068E+005 Mn-54 834.85 99.98 1.632E+005 1.63E+005 1.378E+005 7.599E+004 Co-58 810.76 99.45 1.664E+005 1.66E+005 - 5.667E+004 7.764E+004 Co-60 117 3 . 23 99.85 1. 93 6E+005 1.53E+005 - 8.697E+00 3 9.009E+004 1 332 .49 99.98 1 . 533 E+005 -3.597E+004 6.949E+004 Nb-94 702.65 99.81 1.540E+005 1.54E+0 0 5 -3 .193E+005 7.185E+004 871.09 99.89 1. 606E+005 6 .3 00E+004 7.453E+004 Sn-113 255.1 3 2 .11 8.547E+006 2 .48E+005 4.514E+006 4.137E+006 391. 70 64.97 2 .485E+005 -9.620E+003 1 .185E+005 Cs- 134 475.36 1. 4 8 1.096E+007 2 .05E+005 6.991E+006 5. 2 01E+006 563. 2 5 8.34 1.866E+006 -6.885E+005 8.782E+005 569.33 15.37 1.128E+006 - 1 .077E+005 5 . 3 39E+005 604.72 97.6 2 2 .671E+005 - 1.531E+005 1. 2 87E+005 795.86 85.46 2 .049E+005 2 .657E+004 9.602E+004 8 01. 95 8.69 2 .035E+006 2 .518E+005 9.545E+005 1038.61 0.99 1. 440E+007 -7.5 2 6E+006 6.565E+006 1167.97 1. 79 1.009E+007 -8.162E+006 4.674E+006 1 365.19 3.02 5.225E+006 -4.599E+005 2 .372E+006 Cs- 1 37 661. 66 85.10 2 .004E+005 2 .00E+005 1 .421E+005 9.434E+004 Eu-152 121. 78 2 8.67 7.646E+005 6.53E+005 -8.783E+004 3.747E+005 2 44.70 7.61 2 .578E+006 6.587E+005 1. 2 52E+006 2 95.94 0.45 4.311E+007 4.585E+007 2 .085E+007 3 44. 2 8 26.60 6.533E+005 3.575E+005 3 .1 3 7E+005 3 67.79 0.86 1.884E+007 -3.593E+006 9 .004E+006 411. 12 2.24 7.293E+006 1.085E+006 3 .476E+006 443.96 2.83 5.726E+006 1. 766E+005 2 .722E+006 488.68 0.42 3.581E+007 -1.617E+007 1.690E+007 56 3 .99 0.49 3.188E+007 7.388E+006 1.501E+007 586. 2 6 0.46 4.244E+007 4.062E+007 2 .020E+007 678.62 0.47 3.500E+007 2 .066E+007 1. 643E+007 688.67 0.86 2 .016E+007 8.630E+006 9.487E+006 719.35 0. 28 5.375E+007 -1.298E+005 2 .501E+007 778.90 12.96 1.268E+006 -8.927E+005 5.923E+005 810.45 0.32 5.226E+007 - 1. 4 71E+007 2 .441E+007 867.37 4.26 3 .877E+006 -2.296E+006 1. 804E+006 919.33 0.43 3 .768E+007 -1.963E+007 1.746E+007 964.08 14.65 1.492E+006 7.930E+005 7.045E+005 1085.87 10.24 1.477E+006 -1. 686E+006 6.756E+005 1089.74 1. 73 1.009E+007 7.513E+006 4.670E+006 1112.07 13.69 1. 2 76E+00 6 - 6.200E+005 5.906E+00 5 1212.95 1. 4 3 1. 430E+007 6.971E+006 6.673E+00 6

[307]

                                                             -:::J / .l.::>/L U.LO   L. ; ::> .l. ; ':I ~ t' 1v1      t' ctye 0 lC1-lUe lVJUJ-i Ke}JUL L Nuclide          Energy      Yield      Line MDA Nuclide MDA Activity                                     Dec. Level Name              (keV )       ( \;)   (pCi/S me) (pCi/S me)                   (pCi/S me)                  (pCi/S me)

Eu-1 52 1249.94 0.19 8.489E+007 6.53E+005 -2 .8 52 E+007 3.879E+007 1 2 99.14 1. 63 1.065E+007 4.972E+006 4.893E+006 1408.01 2 1. 07 7.826E+005 -1.065E+005 3.563E+005 1 457.64 0.50 9.725E+007 3.595E+008 4.713E+007 1528.10 0. 2 8 4.988E+007 -7.256E+006 2.219E+007 Eu-154 123.07 40.40 5.355E+00 5 4.60E+005 - 4. 92 1E+003 2.624E+005 247.93 6.89 2 .425E+006 - 2 .710E+006 l.171E+006 591. 76 4.95 3 .177E+006 1. 606E+006 1. 4 94E+OO 6 692.4 2 1. 78 9 .665E+006 -1.843E+006 4.546E+006 723.30 20.06 8.256E+005 9.031E+004 3 .868E+005 756.80 4. 52 4.043E+006 1. 242 E+006 1. 904E+006 873.18 12.08 1.2 8 5E+006 -9.778E+004 5.951E+005 996. 2 9 10.48 1.7 12 E+006 9.993E+005 7.970E+005 1004.76 18.01 9.462E+005 -1. 067E+005 4. 3 87E+005 1274.43 34.80 4.599E+005 1.409E+005 2 .099E+005 1596.48 1. 80 8.363E+006 -3. 2 11E+006 3.738E+006 Eu-155 45.30 1. 31 1. 1 48E+007 8.51E+005 1. 373E+006 5.573E+006 60.01 1. 22 l.614E+007 - 3.881E+006 7.894E+006 86.55 30.70 8.512E+005 1. 3 04E+006 4.185E+005 105.31 21.10 l.086E+006 4.588E+005 5. 3 27E+005

+      Tl-208             58 3 .19* 85.00    1.091E+005            l.09E+005 2.322E+005                          4.907E+004 Bi-211             351.07*   13.02    1.100E+006            1.10E+006 3 .055E+006                         5. 2 32E+005 Pb- 2 11           404.85      3.78   4. 22 0E+006          4. 2 2E+006 -4.878E+006                       2 .010E+006 4 2 7.09    1. 76  8.801E+006                            -1.145E+007                   4.179E+006 8 32 .01    3 . 52 4. 26 4E+006                            1.807E+006                  1.973E+006 Bi-212               39.86     1. 06  l. 23 9E+007          2 .64E+006 - 2 .740E+006                      5.988E+006 727.33      6.67   2.641E+006                              7. 22 2E+005                1.242E+006 785.37      1.10   l.607E+007                            - 8.345E+006                  7.540E+006 1620.50       1. 4 7 9.084E+006                              4.367E+006                  3 .994E+0 0 6
+      Pb-2 1 2           115.18      0.60   3.900E+007            3.18E+005         3.971E+007                  1.914E+0 0 7 23 8.63*  43.60    3.183E+005                              3.144E+005                  1. 52 8E+005 300.09*     3.30   4. 23 5E+006                            6.089E+006                  2 .022E+006 Pb212-XR             74.82   10. 2 8  2.741E+006            1.55E+00 6        5.897E+005                  1. 349E+006 77.11   17.10    1. 555E+006                             2 .604E+005                 7.646E+005 87.35     3.97   6.535E+006                              4.737E+006                  3. 2 13E+006 89.78     1. 46  1.748E+007                              7.775E+006                  8.592E+006
+      Bi-214             609. 32

45.49 3.074E+005 3 .07E+005 1. 52 2E+006 1.432E+005 768.36 4.89 3.513E+006 1.569E+006 1. 64 7E+006 806.18 1. 2 6 1. 445E+007 9.154E+006 6.788E+006 934.06 3.11 5.411E+006 - 3.828E+005 2 .513E+006 1120. 2 9* 14.9 2 9.603E+005 1. 682E+006 4.363E+005 1155. 2 1 1. 63 l.100E+007 4.143E+006 5.095E+006 1238.12* 5.8 3 1.900E+006 2 .047E+006 8.319E+005 1280.98 1. 4 3 l.199E+007 4. 3 22E+00 5 5.506E+006 1377.67 3 .99 4.082E+006 -3 .442E+006 1. 858E+006 1385.31 0.79 2.005E+007 -7.065E+006 9.104E+006 1401. 52 1. 33 1 . 2 04E+007 -l.435E+006 5.466E+006 1 407.99 2 .39 6.888E+006 -9.374E+005 3.136E+006 1 509. 2 1 2 .13 8.484E+006 4.644E+006 3.881E+006 1 661. 2 7 1. 05 1.124E+007 3.196E+006 4.841E+006

[308]

J /.l. ..J / L. V.l.U L. . J .l. . ":IJ r1*1 JCQ'jC::

!C.L.LUe l 'JU.t-i .Kef,JUL L. Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (~ ) (pCi/S me ) (pCi/S me) (pCi/S me ) (pCi/S me)

+         Bi -2 14               1729.59      2 .88   5.884E+006          3 .07E+005            l. 13 8E+006           2 .651£+006 1764 . 49*  15. 3 0  6.864E+005                                1. 93 3E+006           2 .877E+005 1847.43      ;2 . 03 6.181E+006                              -7 .1 3 9E+005           2 .661E+006 2118.51      1.16    O.OOOE+OOO                                O.OOOE+OOO             O.OOOE+OOO
   >                                                                                            1. 8 91E+006           9.188E+00 5
+          Pb-214                 24 1. 99*   7. 2 5  1.914E+006          4.02E+005 295. 22

18. 42 7.587E+005 1. 091E+006 3.623E+005 351. 93* 35.60 4.023E+005 1.117E+006 1.913E+005 785.96 1. 06 1.681E+007 - 5.405E+005 7.892E+006 Pb2 1 4-XR 74.8 2 5.80 4.857E+006 2 .74E+006 1.045E+006 2 .391E+006 77.11 9.70 2 .741E+006 4.590E+005 1.348E+006 87.35 2 . 24 1.158E+007 8.396E+006 5.694E+006 89.78 0.8 ~ 3 .113E+-007 1. 384E+007 1.530E+007 Ra- 2 26 186. 2 1 3.64 5.223E+006 5. 2 2E+006 1.343E+006 2 .545E+006 Ac-22 8 129.07 2 .4 2 8.761E+006 9.01E+005 - 1.859E+006 4.290E+006 209.25 3 .89 4.791E+006 1. 044E+006 2 .329E+006 27 0 .24 3 .46 5. 2 56E+006 2 .814E+006 2 .542E+006 32 8.00 2 .95 5.725E+006 9.021E+005 2 .749E+006 338.3 2 11. 2 7 1.570E+006 3.741E+005 7.547E+005 409.46 1. 92 8.677E+006 4.403E+006 4.140E+006 463.00 4.40 3 .786E+006 -1. 705E+006 1.800E+006 794.95 4.25 3 . 9 88E+006 -1. 632E+006 1. 865E+006 911. 20 25 .80 9.015E+005 6.821E+005 4.279E+005 964.77 4.99 4.527E+006 5.072E+006 2.142E+006 968.97 15.80 1.452E+006 1. 330E+006 6.876E+005 1588 . 2 0 3 . 22 5.862E+006 4.698E+006 2.684E+006 Pa - 23 1 2 7.36 10.30 7.538E+005 7.54E+005 9.043E+005 3.558E+005 28 3 .69 1. 70 9.960E+006 - 6.029E+006 4.800E+006 300.07 2.47 7.143E+006 8. 2 46E+005 3.443E+006 302.65 2 . 20 7.650E+006 2 .732E+006 3.6808+006 330. 0 6 1. 40 1. 217E+007 -4 . 800E+006 5.8448+006 Th-234 92.38 2 .13 1.164E+007 1.16E+007 -7.714E+00 5 5.717E+006 92.80 2 .10 1.173E+007 3 .951E+00 6 5.7618+006 112 . 81 0. 21 1.095E+008 -6 .141E+00 6 5.3708+007 U-2 35 1 43.76 10.96 1.887E+006 3 .34E+005 4. 29 0E+005 9.229E+005 1 63.33 5.08 3.884E+006 7.036E+005 1. 896E+006 185.71 57. 2 0 3 .342E+005 2 .588E+005 1. 629E+005 202. 11 1. 08 1.756E+007 -7.199E+006 8.5448+006 205.31 5.01 3 .695E+006 4.207E+005 1. 796E+00 6 Am- 2 41 59.54 35.90 5.454E+005 5 . 45E+005 l .652E+005 2 .666E+00 5

        + = Nuclide identified during the nuclide identification

Energy line found in the spectrum

        >           Calculated         MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
        @ = Half-life too short to be able to perform the decay correction

[309]

'***         GA MM A      S P E C T R U M            A N A L Y S I S             **'~**
'******************* +* ****** * ********* * **' '~*****************************
.lename: 54 52 iport Generated On                   9/13/20 1 6        2 :45:03 PM tmple  Title                         B306100BFRFC008GD tmple  Description                   Steam Tunnel Unit-1 tmple  Identification                008 tmpl e Type tmple  Geometry                      1 meter iak Locate Threshold                   3. 00 iak Locate Range (in channels )            85 -      81 92 iak Area Range (in channels)               85 -      81 92 ientification Energy Tolerance           10 . 0 0 0 keV tmple Siz e                            1 . 000E +OOO S meters tmple Taken On

quisition Started 9/13/ 2 01 6 2: 35: 01 PM

.ve Time 6 00 . 0 seconds ial Time 60 1 .4 seconds iad Time 0 .24 % Energy Calibration Used Done On 1/13/2 01 5 Efficiency Calibration Used Done On 8/9/20 1 6 Efficiency ID UNNELSTS 1 METER DATA VALIDATED DATE L-6-!2 TIME osao o.,~4.: [310]

!d J\. l"l.!!ct.J..y;::,.J..;::, I'l.t::1-'V.L L                  J / .LJ/ L V.J..U     L * <,t .J

V J r 1*1

' ********************* * **********************+***************************
'***                                    P E A K         A N A L Y S I S                   R E P O R T                      *****
' ************************************************************************

Detector Name: 54 52 Sample Title: B306100BFRFC008GD Peak Analysis Performed on: 9/13/20 1 6 2 :45:03 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid ( keV) ( keV) Area Uncert. Counts 1 297- 306 300.69 74.83 0.94 1.45E+002 69.89 4.72E+002 2 947- 962 954.73 23 8.54 0.8 3 9.70E+001 54.16 2 .12E+002 3 1173- 1190 1180.62 2 95.07 1. 22 1. 11E+00 2 44.49 1.18E+002 4 1 401- 1417 1407.64 351.88 1. 30 1. 4 7E+00 2 42.84 9.78E+001 5 232 6- 2338 23 31. 53 583.04 0.47 4.65E+001 26.23 4.75E+001 6 2428 - 2 446 2436.94 609.41 1. 62 2 .08E+002 35.81 3 .33E+001 7 2635- 2656 2 645.64 661.62 1. 56 3.92E+002 48.45 5.20E+001 8 3637- 365 1 3643.45 911. 18 0.49 3.03E+001 22.63 3.38E+001 9 4473- 4489 4480.45 11 2 0.45 0.87 6.54E+001 24.27 2 .56E+001 10 5829- 5854 5843.03 14 61. 0 2 1. 88 3.23E+00 2 35.94 O.OOE+OOO

= First peal: in a multiplet region Other peak in a multiplet region Fitted singlet

rors quoted at 2.000 sigma

[311]

rcerrerence 1....ULLC::CLt::U i"iCL.J.V.J.LY !'i.t::l,)UL L ::J / L .:J / LV LU L ; 'f J ; V J r l"l raye J ' *********** * ****************** * ************************** +************* ' *** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** ' *********************************************************************** Sample Title: B306100BFRFC008GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( *'ci ) (pCi/S me) Uncertainty K-40 1.000 1460.82* 10.66 1. 68 92 6E+007 2 .38446E+006 Ba-1 33 0. 32 1 79.61* 2.6 5 8.78755E+006 4.60204E+006

81. 00 32.90 276.40 7.16 302.85* 18.34 1. 40398E+006 6.06784E+00 5 356.01* 62.05 6.11293E+005 2 .02965E+005 383.85 8.94 Cs - 1 3 7 1. 000 661.66* 85.10 l.69440E+006 2 .92002E+005 Tl-208 1. 000 583.19* 85.00 1 .88 1 61E+005 1 .08552E+005 Pb-212 0.974 115.18 0.60 23 8.63* 43.60 4.55691E+005 2 .64883E+005 300.09* 3.30 7.80272E+006 3 .37574E+006 Bi-2 1 4 0. 3 50 609. 32* 45.49 1. 6 0 868E+006 3 .38048E+005 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120.29* 1 4.92 2 .12020E+006 8.04956E+0 0 5 11 55.21 1. 63 1238. 1 2 5.83 1 2 80.98 1. 43 1 377.67 3.99 1 385.31 0.79 1 401. 52 1. 33 1407.99 2 .39 1509.21 2 .13 1661.27 1. 05 1729.59 2 .88 1764.49 15.3 0 1847.43 2 .03 2 118.51 1.16 Pb-21 4 0.977 2 41. 99* 7.25 2 .74005E+006 1. 5 9154E+006 2 95. 2 Z* 18.42 1.39788E+006 6.03854E+005 351.93* 35.60 1.06547E+006 3 .53788E+005 785.96 1. 06

        *=Energy line found in the spectrum.
        @ = Energy line not used for Weighted Mean Activity Energy Tolerance :                 10. 000 keV Nuclide confidence index threshold =                                  0. 3 0 Errors quoted at 2 .000 s igma

[312]

l LCL.LCLCl!I...... C::: VV.L.LC::1......,l-C::U L"l.Vl-.LV .L l-Y l."\'C.t""'V..1...L.. J/ J.....J/ .£. VJ....U L.. * "":::t ....J

V....J L l."l

' ************** ******** * ************************************************ I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** ' **************************************************** ******************* Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/S me ) Uncertainty K-40 1. 000 1. 68 92 61E+007 2 .384455E+006 Ba- 133 0.321 1.121905E+004 9.781 2 79E+005 Cs- 137 1. 000 1. 694396E+006 2 .920016E+005 Tl-2 08 1. 000 1 .88161 3E+005 1.0855 2 4E+005 X Bi-2 11 0.999 Pb-212 0.974 2 .771693E+005 3.844690E+005 Bi-214 0.350 1.685369E+ 00 6 3.116785E+005 Pb-~14 0.977 1.118649E+ 00 6 1.565014E+006

       ?         Nuclide is part of an undetermined solution X  = Nuclide rejected by the interference analysis
       @  = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at                             2 .000 sigma
  '~********'"               U N I D E N T I F I E D                                      P E A K S               **********

Peak Locate Performed on: 9/13/20 1 6 2 :45:03 PM Peak Locate From Channel: 85 Pea k Locate To Channel: 81 92 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV ) Counts per Second % Uncertainty Type Nuclide 8 911.18 5.0417E-002 7 4.8 1 Sum M = First peak in a multiple t region m Other peak in a multiple t region F Fitted singlet Errors quoted at 2 . 000 sigma [313]

lC.L.LUe 1*1u.M. I',e]:.JUL L. ::J / .L ..)/ L V.LU L , ":I ..J

V ..J r t*J

'* +**** * *********************************************************************** ' *** N U C L I D E MD A R E P O R T ***** '****************************************************************************** Detector Name: 5452 Sample Geometry: 1 meter Sample Title: B306100BFRFC008GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) (t ) (pCi/S me ) (pCi/S me) (pCi/S me ) (pCi/S me )

+       K-40                 1460.8 2*    10.66    1.415E+005        1.42E+005 1. 689E+007                            O.OOOE+OOO Cr-51                  320.08       9.91   1.775E+006        1. 77E+006 - 6.834E+005                          8.540E+005 Mn-54                  834.85     99.98    1.692E+005        1. 69E+005 9.234E+004                            7.899E+004 Co-58                  810.76     99.45    1.616E+005        1.62E+005 6.327E+004                             7.525E+004 Co-6 0               117 3 . 23   99.85    1.682E+005        1.68E+005 - 1.498E+005                           7.738E+004 1332.49       99.98    l.697E+005                             l. 3 86E+00 5               7.769E+004 Nb-94                  702.65     99.81    1.714E+005        1 .33E+005 1 .021E+005                           8.057E+004 871. 09    99.89    1. 332 E+005                         -8.806E+004                   6.086E+004 Sn- 1 13               2 55. 1 3    2 .11  8.8 62 E+006      2 .85E+005 1.558E+006                            4. 2 94E+006 391. 7 0   64.97   2 .849E+005                           -9.019E+003                   1.367E+005 Cs-134                 475.36       1. 48 1 .170E+007        2 .14E+005 1.824E+006                            5.569E+006 563. 2 5     8.34  2 .093E+006                           - 1.501E+006                  9.920E+005 569.33     15.37   1.133E+006                            -4.106E+005                  5.364E+005 6 0 4.72   97. 62  2 .772E+005                             6.028E+004                 1.338E+005 795.86     85.46   2 .135E+005                             8.598E+004                 1.003E+005 801. 95      8.69  1.972E+006                              7.111E+004                  9. 2 30E+005 1 038.61        0.99  1.675E+007                              7.509E+006                 7.737E+006 1167.97         1. 79 9.360E+006                           -5.521E+006                   4.307E+006 1 365.19        3.02  4.081E+006                              1.841E+006                 1.800E+006

+ Cs- 1 37 661.66* 85.10 2 .102E+005 2 .10E+005 1.694E+006 9.925E+004 Eu-1 52 121. 78 2 8.67 7.940E+005 6.89E+005 -1.771E+004 3.894E+005 244.70 7.61 2 .578E+006 1.451E+006 1 .252E+006 295.94 0.45 4.743E+007 6.148E+007 2.301E+007 344.28 2 6.60 6.886E+005 - 6.599E+005 3.314E+005 367.79 0. 86 1.872E+007 - 1.005E+007 8.947E+006 411.12 2.24 8.202E+006 2 .160E+006 3.930E+006 443.96 2.83 6.359E+006 -4.233E+005 3 .038E+006 488.68 0.4 2 3.964E+007 8.365E+005 1.882E+007 563.99 0.49 3.573E+007 -3.898E+006 1.693E+007 586. 2 6 0.46 4.808E+007 6.555E+007 2 .302E+007 678.62 0.47 3.479E+007 - 4. 2 03E+006 1.633E+007 688.67 0.86 1.892E+007 -3 .8 2 5E+005 8.867E+006 719.35 0. 2 8 6. 2 78E+007 1.490E+006 2 .953E+007 778.90 12.96 1 . 2 51E+006 -2 .198E+005 5 .835E+005 810.45 0.32 5.043E+007 3 .5 3 1E+007 2 . 3 49E+007 867.37 4.26 3.695E+006 -1. 2 90E+006 1. 713E+006 919.33 0.43 4.500E+007 -2 . 5 86E+007 2 .112E+007 964.08 14.65 1. 418E+006 1.038E+006 6 .676E+005 1085.87 10.24 1.759E+006 3.059E+003 8.168E+005 1089.74 1. 73 1. 085E+007 4.788E+006 5.051E+006 1112.07 13.69 1. 2 30E+006 4.404E+005 5.674E+005 1212.95 1. 4 3 1 . 2 10E+007 -1.376E+007 5.571E+006 [314]

1*JLJ.l"1 !'I.C:]:JU L L :J / .l. .J/ L. U.l.V '-" * "":t .J

V ...J r: 1*1 ra~ c: V IC.L.l.Ut::

Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( ~) (pCi/S me ) (pCi/S me) (pCi/S me ) (pCi/S me) Eu-1 52 1249.94 0.19 9.450E+007 6.89E+005 2 . 32 4E+007 4.359E+007 1299.14 1. 63 8.905E+006 4.811E+005 4.018E+006 1408.01 2 1 . 07 7.514E+005 - 6.753E+005 3.407E+005 1 457.64 0.50 9.669E+007 3.573E+008 4.685E+007 1 528.10 0 .2 8 3.828E+007 - 2 .114E+007 1.639E+007 Eu -15 4 123.07 40.40 5.633E+005 4.8 2 E+005 -1. 68 OE+OO 4 2 .762E+005 247.93 6.89 2 .606E+006 -1.688E+006 1.262E+006 591. 76 4.95 3 .417E+006 3 .514E+005 1 .614E+006 692.4 2 1. 78 8.998E+006 -4.645E+004 4. 2 1 2E+006 723.3 0 20.06 8.995E+005 7. 52 7E+005 4. 23 8E+005 756.80 4. 52 3 .632E+006 2 .1 8 1E+005 1. 698E+006 873.18 12.08 1. l 79E+006 8. 0 65E+004 5 . 422E+005 996.29 10.48 1. 591E+006 4. 3 47E+005 7.369E+005 1004.76 18.01 8.077E+005 - 1.174E+004 3 .694E+005 1274.43 34.80 4. 82 1E+005 -9.587E+004 2 . 2 10E+005 1596.48 1. 80 5.713E+006 -4.526E+006 2 .413E+006 Eu-1 5 5 45. 3 0 1. 3 1 1.174E+007 8.88E+005 6.074E+006 5.703E+006 60.01 1. 22 1.699E+007 -8.576E+006 8. 3 17E+006 86.55 30.70 8.876E+005 1. 355E+006 4. 3 67E+005 10 5.31 2 1.10 1.110E+006 -4.931E+005 5.449E+005

+          Tl-208                     58 3 .19* 85.00    1.601E+005        1.60E+ 005           1.882E+005                    7.459E+004 Bi-211                     3 51. 07* 1 3 .02  1. 2 02E+006      1. 2 0E+006          2 .913E+006                   5.745E+005 Pb-211                     404.85      3.78   5.038E+006        4.34E+006            3 .059E+006                   2 .419E+006 427.09      1. 76  1.074E+007                             1.078E+007                    5.146E+006 8 32 .01    3 . 52 4. 33 9E+006                         -5.717E+004                     2 .011E+006 Bi-212                       39.86     1. 06  1 .317E+007       2 .67E+006         -1. 164E+OO 6                   6.381E+006 727.33      6.67   2.670E+006                           -5 .873E+005                    1. 2 57E+006 785.37      1.10   1.548E+007                             3 .142E+006                   7. 2 48E+006 1 620.5 0     1. 4 7 8.627E+006                           -6.577E+006                     3.766E+006
+          Pb-2 1 2                   115.18      0.6 0  3.869E+007        4.03E+005            5.191E+006                    1 .898E+007 238.63*   43.6 0   4.026E+ 0 05                           4.557E+005                    1.949E+005 30 0 .09*   3.3 0  4.727E+006                             7.803E+006                    2 . 26 8E+006 Pb212-XR                     7 4.82  10.28    2 .733E+006       l.56E+00 6           7.569E+006                    1.345E+006 77.11   17.10    1.559E+006                           -1. 669E+005                    7.668E+005 87.35     3 .97  6.790E+006                             5.040E+006                    3 . 3 40E+006 89.78     1. 46  1.770E+007                             1.130E+007                    8.702E+006
+          Bi -2 14                   609.3 2

45.49 2 .915E+005 2 .92E+005 1. 609E+006 l.353E+005 768.36 4.89 3.620E+006 3 .850E+006 1. 700E+006 806. 1 8 1.26 1. 2 58E+007 -1. 322 E+007 5.855E+006 934.06 3.1 1 6.138E+006 6. 622 E+006 2 .877E+006 1120.29* 14.9 2 l.053E+006 2 .120E+006 4.8 2 5E+005 1155.21 1. 63 l .061E+007 -2 .540E+006 4.899E+006 1238.12 5.83 4.042E+006 4.903E+006 1. 903E+006 1280.98 1. 43 1. 249E+007 9.420E+006 5.756E+006 1377.67 3.99 4.339E+006 2 .803E+006 1. 987E+006 1385.31 0.79 l.920E+007 -1.899E+007 8.680E+006 1401.5 2 1. 33 l.220E+007 -5.476E+006 5.548E+006 1407.99 2.39 6.613E+006 -5.943E+006 2 .998E+006 1509. 2 1 2.13 8.076E+006 3.352E+006 3 .676E+006 1 661. 2 7 1. 05 l .086E+007 -3.715E+006 4.651E+006

[315]

lC.L.LUt::! 1*JLJh !'.t::!.f:JUL L. :J/.LJ/L. U.LO L. ; ':f;J; UJ r-1*1 J:'df::lt::! Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( \; ) (pCi/S me ) (pCi/S me ) (pCi/S me) (pCi/S me)

+           Bi-214                  1729.59       2 .88    5.388E+006 2.92 E+005           4.953E+006             2 .4 02E+006 1764.49     15.30      1 .589E+006                     1.528E+006             7. 3 91E+005 1847.43       2 .03    6.945E+006                      5.394E+006             3.043E+006
    >                               2 118.51      1.16     O.OOOE+OOO                      O.OOOE+OOO             O.OOOE+OOO
+           Pb- 2 14                  2 41.99*    7. 2 5   2 .421E+006 4.40E+005           2 .740E+006            1.172E+006 2 95. 22* 1 8.42     8.468E+005                      1.398E+006             4.064E+005 351.93*   3 5.60     4.398E+005                      1.065E+006             2 .101E+005 785.96      1. 06   1 .610E+007                    - 3.582E+006             7.538E+006 Pb2 14 -XR                  7 4.82    5.80     4.843E+006 2 .75E+006           1.341E+007             2 .384E+006 77 .11    9.70    2 .748E+006                    -2 .942E+005             1.352E+006 87.35     2 . 24  1. 2 03E+007                     8.933E+006             5. 92 0E+006 89.78     0.8 2   3.152E+007                       2 .013E+007            1. 54 9--E+007 Ra-2 2 6                   186.2 1     3.64    5.607E+006 5.61E+006             6.543E+006             2 .737E+006 Ac-228                     1 2 9.07    2 .42   9.117E+006 8.98E+005             1.113E+006             4.468E+006 209.25      3.89    5.089E+006                       3.409E+006             2 .478E+006 270.2 4     3.46    5.133E+006                     - 8.754E+005             2 .480E+006 328. 00     2 .95   5.982E+006                       1.403E+006             2 .878E+006 338.32    11. 27    1. 793E+006                      1.768E+006             8.663E+005 409.46      1. 92   9.379E+006                       1.667E+006             4.491E+006 463.00      4.40    4.098E+006                       1.888E+005            1. 956E+006 794.95      4.25    4. 2 42E+006                  -7.753E+004              1. 992E+006 911.20    2 5.80    8.979E+005                       3.007E+005            4. 2 61E+005 964.77      4.99    4.120E+006                       1 .805E+006           1. 938E+006 968.97     15.80     1.304E+006                       5.498E+005            6.136E+005 1588. 2 0       3. 22   4.565E+006                    - 4. 2 75E+006           2.035E+006 Pa- 2 3 1                   27.36    10.30     8.411E+005 8.4 1E+005            1.198E+006            3.994E+005 28 3 .69     1. 70   1.004E+007                    -3 .770E+006             4.840E+006 300.07      2 .47    7.675E+006                       1.856E+006            3.709E+006 302.65      2.20     7.866E+0 0 6                    1.156E+006             3.788E+006 330.06      1. 40    1. 222E+0 0 7                 -3.606E+006              5.873E+006 Th-234                      92.38     2 .13    1.156E+007 1.16E+007          -1.731E+006              5.677E+006 92.8 0    2 .10    1.163E+007                    - 2 .553E+006            5.711E+006 112.8 1     0.21     1.120E+008                      2 .359E+007            5.496E+007 U-235                     143.76     10.96     1. 871E+006 3.56E+005         -5.450E+005              9.149E+005 163.33      5.08     3 .945E+006                     1. 270E+006            1.927E+006 185.71     57. 2 0   3 .563E+005                     2 .789E+005            1. 739E+005 2 02.11     1. 08    1. 816E+007                     3 .123E+006            8.844E+006 2 05.3 1    5. 0 1   3 .911E+006                   -1.216E+006              1.905E+006 Am-24 1                     59.54    35.90     5.701E+005 5.70E+005          -6.719E+004              2 .790E+005
        +        Nucl ide identified during the nuclide identification

Energy line found in the spectrum

        > = Calculated MDA is zero due to zero counts in the region, or the region is outside the spectrum, or MDA has not been calculated
        @ = Half-life too short to be able to perform the decay correction

[316]

'***           GA MM A       S P E C T R U M           A N ALYSIS                   *****
' *** * ***********~***** +* * ******************* * *************** * ***********

_lename: 5452

!port Generated On                     8/10/2016         4:01:17 PM tmple    Title                         B306100BFRWC009GD tmple    Description                   ST SE. WALL NUMB 9A SHOT tmple    Identification                9 tmple    Type tmple    Geometry

!ak Locate Threshold 3. 00 !ak Locate Range (in channels ) 85 - 8192 iak Area Range (in channels) 85 - 8192 lentification Energy Tolerance 10.000 keV tmple Si ze 1. OOOE+OOO SQM tmple Taken On

quisition Started 8/ 10 /2 0 16 3:5 1 : 1 5 PM

_ve Time 600.0 seconds !al Time 601. 2 seconds iad Ti me 0.2 1 % Energy Calibration Used Done On 1/13/2015 Efficiency Calibration Used Done On 8/9/2016 Efficiency ID UNNELSTS 1 METER DATA VAUDA1l:D DATE/* 8-11 Tl ME_o 5:LO ar&/4" [317]

U/ .LV/ L...V..J..V -:I

V .L * .J.. I .L J.".1

' * * **************** * ************** * ********************************** * ***

P E A K A N A L Y S I S R E P O R T **** *

' ****** +*****************************************************************

Detector Name: 5452 Sample Title: B306100BFRWC009GD Peak Analysis Performed on: 8/10/2016 4:01:17 PM Peak Analysi s From Channel: 85 Peak Analysi s To Channel: 8 1 92 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid ( keV) (keV) Area Uncert. Counts 1 11 3- 123 116.05 2 8 . 60 0.50 5. 3 9E+001 30.00 5.71E+001 2 259- 2 70 2 63.10 65.41 0. 42 9.92E+OOO 56.15 3 .10E+00 2 3 288- 306 300.40 74.75 1. 03 2 .16E+002 98. 2 0 6.50E+00 2 4 739- 749 743.08 185.56 0. 35 1.41E+001 41. 08 1 . 71E+00 2 5 950 - 959 954.99 2 38.60 0.50 9.13E+001 34.59 9.17E+001 6 1076 - 1086 1080.92 2 70.1 2 0. 2 5 1.15E+001 27.57 7.35E+001 7 1400- 1413 1407.59 3 51. 8 7 0.87 9.65E+001 32.26 5.95E+001 8 1847- 1 856 1851. 52 4 62. 95 0.55 1. 89E+00 1 16.32 2 .llE+OOl 9 2 326- 2 338 2 331 .93 583.14 0.42 2 .97E+001 20.04 2 .63E+001 10 2 425- 2 446 2435.86 6 0 9.14 0.89 1.52E+002 31. 92 2 .75E+001 11 4474- 4485 4479.38 1120.19 0.98 3 .22E+001 14.03 6.79E+000 12 4947 - 4958 4952.89 1238.56 0.32 1. 78E+OOO 14.94 2 .12E+001 13 5828 - 5853 5842.08 1 460.79 1. 86 2 .88E+002 36.35 9.84E+OOO First peak in a multiplet region

= Other peak in a multiplet region
= Fitted singlet

rors quoted at 2 .000 sigma

[318]

lLt::L L t::Lt::lH;e l..,UL.L\::::l_;Lt::;:U hl_;L.l.V.l.LY J:\.t::.f:JU.LL U/ .l.V/ L V.l.U ':I

V .L * .l. I r 1*1

' **** * ***************** * ************** * *************************** * ***** '*** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** '*********************************************************************** Sample Title: B306100BFRWC009GD Nuclide Libr a ry Used: C:\GENIE2K\CAMFILE S \ Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( ~) (pCi/SQM) Uncertainty K-40 1. 000 1460.82* 10.66 1.50689E+007 2 .30775E+006 Hg-203 0.876 279.20* 81. 56 3 .11740E+004 7.46791E+004 Tl-208 1. 000 58 3 .19* 85.00 1. 2 0160E+005 8. 2392 5E+004 Pb-21 2 0.873 115.18 0.60 23 8.63* 43.60 4. 2 8843E+005 1. 76695E+005 300.09 3.3 0 Bi- 2 1 4 0.4 2 8 609.3 2

45.49 l . 1 72 84E+006 2 .84479E+00 5 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120. 2 9* 14.92 1.04430E+006 4. 62403E+005 1 155. 2 1 1. 63 1238.1:* 5.83 1. 55472E+005 1. 3034 9E+006 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1 401.5 2 1. 33 1407.99 2.39 1509. 2 1 2.13 1661. 2 7 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.491 2 41. 99* 7. 2 5 2 .57862E+006 l.06088E+006 2 95. 22 18.42 3 51. 93* 35.60 6 .98493E+005 2 .58780E+005 785.96 1. 06 Rn-219 0.43 5 271. 2 3* 10.80 2 . 3 5409E+005 5.64543E+005 401. 81 6 .60 Ra-226 0.999 186. 2 1* 3.64 6.95573E+005 2 .02363E+006 Th-231 0.875 2 5.64* 14.10 6.14949E+005 3 .71914E+005 84.21* 6 . 60 5 . 2 7017E+006 2 .69096E+006 89.95 1. 00 Th- 232 0.996 6 3 .81* 0.26 6. 0 6712E+006 3 .43516E+007 U-235 0.548 143.76 10.96 1 63.33 5.08 185.71* 57 .2 0 4.4 263 7E+00 4 1. 2 8779E+005 20 2 .11 1. 08 205.31 5.01 Arn-241 0.94 6 59.54* 35.90 4.44471E+00 4 2 .51 62 0£+005

[319]

lL.C::LLC::LC::!ll.,C:: l..,ULLC::l.,l..C:U rll..,l...LV.LL.Y I'I.C:_l:-IV.LL. U/ .l.V/ LV.l.U ""i

V .1. * .L I r l"l Nuclide Id Energy Yield Activity Acti-vity Name Confidence (keV) ( %) (pCi/SQM ) Uncertaint y

          * = Energy line found in the spectrum.
          @ = Energy line not used for Weighted Mean Activity Energy Tolerance :                           10.000 keV Nuclide confidence index threshold                                          0 .3 0 Errors quoted at 2 .000 sigma

[320]

U/ J.U/ L UJ.U '"i

u J.
J. , r 1*i

' ******* * ********************************************************** * **** ' *** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** '************************ * ********************************************** Nucl ide Wt mean Wt mean Nuclide Id Activi t 11 Activity Name Confidence (pCi/SQM) Uncertainty K-40 1. 000 l.506890E+007 2 . 3 07749E+006

   ?   Hg-203         0.876         3.117397E+004        7.467914E+004 Tl-208         1. 000        1. 2 01602E+005      8. 2392 47E+004 X   Bi-211         0.999 Pb-21 2        0.873         3.126785E+005        1. 815942E+005 Bi-214          0.428         1.104748E+006        2 .382165£+005 Pb-214         0.491         6.984931E+005        2.587653£+005
   ?  Rn-219          0.435         2 .354090£+005       5.645429£+005
   ?  Ra-2 2 6        0.999         6.955728£+005        2.023635£+006 X   Pa-231         0.384 Th-231          0.875         7.022051E+005        3.684124£+005
   ?  Th-232          0.996         6.067120E+006        3.435155E+007
   ?  U-235           0.548         4.426372E+004        l. 2 87790E+005
   ?  Arn-241         0.946         4.444715E+004        2.516198E+005
      ?   = Nuclide is part of an undetermined solution X   = Nuclide rejected by the interference analysis
      @   = Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at        2 . 000 sigma
  **********       U N I D E N T I F I E D          P E A K S        **********

Peak Locate Performed on: 8/10/ 2 01 6 4: 01: 16 PM Peak Locate From Channel: 85 Peak Locat e To Channel: 81 92 Peak Energy Peak Size in Peak CPS Pea k Tol. No. (keV) Counts per Second i Uncertainty Type Nuclide 8 4 62 .95 3.1448E-00 2 86.48 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F Fitted singlet Errors quoted at 2 .000 sigma [321]

0/J.V/ L VJ.U ':t

V J. * .L I r l"l lC..L..LUe 1*1u.H KefJUL L

' * * *** * ****~********************** * ******************************************** N U C L I D E M D A R E P O R T ***** '***************************************************************************'~** Detector Name: 5452 Sample Geometry: Sample Title: B306100BFRWC009GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL. NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name ( keV) ( i5 ) (pCi/SQM ) (pCi/ SQM ) (pCi/SQM ) (pCi/SQM )

 +         K-40           1460.82*    10.66    1.259E+006       1 .26E+00 6 1.507E+007                  5.587E+00 5 Cr-51            320.08      9.91   1.618E+006       1. 62E+00 6 9.871E+005                  7.758E+00 5 Mn-54             834.85    99.98    1 . 582E+005     l.58E+00 5 -1.009E+005                  7.349E+004 Co-58             810.76    99.45    1.592E+005       1.59E+005 3.069E+004                    7.402E+004 Co-60           1173. 23    99.85    1.749E+005       1.47E+005 2 .553E+004                   8.075E+004 1 33 2 .49  99.98    1.466E+005                     -3.159E+004               6.615E+004 Nb-94            70 2 .65  99.81    l.496E+005       1. 5 0E+005 -6.530E+004                 6.964E+004 871. 09   99.89    1. 579E+005                      8.381E+004              7.321E+004 Sn-113           255.13      2 .11  7.477E+006       2 .38E+005 4. 22 3E+004                 3 .602E+006 391.70    64.97    2 . 3 84E+005                  -9.701E+003               1. 135E+005 Cs-134            475.36      1. 48  1.017E+007       1.98E+005 -2 .957E+006                  4.805E+006

563. 2 5 8.34 1.846E+006 5.363E+005 8.680E+005 569.33 15.37 1.051E+006 3. 651E+005 4.955E+005 604.72 97. 62 2 . 38 4E+005 - 4.077E+004 1.143E+005 795.86 85.46 1.984E+005 1.158E+005 9. 2 81E+004 801.95 8.69 1.894E+006 -2 .402E+005 8.837E+005 1038.61 0.99 1.422E+007 -1.529E+006 6.474E+006 1167.97 1. 79 1.061E+007 4.251E+006 4.931E+006 1365.19 3.02 4. 3 54E+006 -2 .243E+006 1. 937E+006 Cs-137 661.66 85.10 1. 949E+005 1 . 95E+0 0 5 8.861E+004 9. 1 62E+004 Eu-1 52 1 21. 78 2 8.67 7.050E+005 5.76E+005 - 5 .844E+005 3 .449E+005 2 44.7 0 7. 61 2 .348E+006 1.721E+006 1.137E+006 2 95.94 0.45 3.788E+007 2 .583E+007 1.824E+007 3 44.28 2 6.60 5.761E+005 -5.799E+005 2 .751E+005 3 67.79 0.86 1.634E+007 -2.176E+006 7.756E+006 411.12 2 . 24 6.750E+006 2.525E+005 3.204E+006 443.96 2 .8 3 4.959E+006 -4.018E+00 6 2 . 33 9E+006 488.68 0.42 3 .753E+007 -4.701E+00 6 1.776E+007 563.99 0.49 3 .137E+007 1.849E+007 1.475E+007 586.26 0.46 3 .963E+007 1. 562E+007 1. 880E+007 678.62 0.47 2 .963E+007 -1. 837E+007 1.375E+007 688.67 0.86 1.667E+007 3.145E+006 7.746E+006 719.35 0.28 4.947E+007 1.507E+007 2 . 2 87E+007 778.90 12.96 1.079E+006 -1.7 5 6E+005 4.977E+005 810.45 0 . 32 5.006E+007 3. 2 84E+007 2.331E+007 867.37 4. 26 3.535E+006 -2 .7 3 6E+006 1. 633E+006 919.33 0.43 3.895E+007 -4.154E+007 1.809E+007 964.08 14.65 1.148E+006 7.063E+005 5.326E+005 1085.87 10. 2 4 1.745E+006 2 .325E+005 8.096E+005 1089.74 1. 7 3 9.818E+006 -2 .758E+005 4.536E+006 1112.07 13.69 1. 2 06E+006 -5. 22 7E+005 5.555E+005 1212.95 1. 43 1. 2 69E+007 8.650E+006 5.866E+006

[322]

CJ/ .l.V/ L. V.l.U ":i

U ..L *..LI r: l'J r: Cl ~ c:;

l(.;.L .L Ue 1*1u11. rs.e.!,JUL L Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) h) (pCi/SQM ) (pCi/SQM) (pCi/SQM) (pCi/SQM ) Eu-15 2 1249.94 0.19 9. 2 67E+007 5.76E+005 5.274E+007 4.267E+007 1299.14 1. 63 9.697E+006 2 .025E+006 4 .415E+00 6 1 408.01 2 1.07 7.5 1 4E+005 -2 .124E+005 3 .407E+005 1457.64 0.50 9.337E+007 3 .032E+008 4.519E+007 1528.10 0. 2 8 3. 22 6E+007 -l.271E+006 l. 3 38E+007 Eu- 1 54 123.07 40.40 5.055E+005 3.9.=:E+005 8.010E+004 2. 474E+005 247.93 6.89 2.351E+006 -2 .637E+005 1.1 3 4E+006 591. 76 4.95 3.230E+006 -1.227E+006 1. 52 0E+006 692.42 1. 78 7.820E+006 7.594E+005 3 . 62 3E+006 723.30 20.06 7. 2 64E+005 1. 4 4 OE+004 3 .372E+005 756.8 0 4. 52 2 .928E+006 -5.506E+005 1.346E+006 873.18 12 .08 l.296E+006 8.808E+005 6.006E+005 996. 2 9 10.48 1.633E+006 2 .175E+005 7.574E+005 1004.76 18.01 9.054E+005 4.216E+005 4.183E+005 1274.43 34.80 3.921E+005 - 4.376E+005 1.760E+005 1596.48 1. 80 8.045E+006 4.607E+006 3 .579E+006 Eu-155 45. 3 0 1. 3 1 1.001E+007 7.80E+005 - 1.869E+006 4.837E+006 60.01 1. 22 1 .432E+007 -2 . 3 09E+006 6.984E+006 86.55 30.70 7.800E+005 1. 2 04E+006 3.829E+005 105.31 21.10 1.037E+006 -9.616E+004 5.082E+005

+           Tl-208                 583.19*   85.00    1.229E+005        1.23E+005          1. 2 02E+005             5.599E+004 Bi-211                 351. 07*  13.02    8.860E+005        8.86E+005          1. 910E+006              4.162E+005 Pb-2 11                404.85      3.78   4.160E+006        4. 1 6E+006        3.872E+004               1. 980E+006 427.09      1. 76  8.696E+006                           2.677E+005               4.126E+006 832.01      3.52   4.522E+006                           1. 325 E+006             2 .102E+006 Bi - 2 1 2               39. 86    1. 06  1.150E+007        2 . 2 4E+ 00 6   -4. 2 72E+006              5.545E+006 727.33      6.67   2 .244E+006                          5.526E+005               1. 044E+006 785.37      1.10   1.237E+007                         - 1.136E+007               5.691E+006 1 62 0.50     1. 4 7 9.303E+006                         -9.319E+005                4.104E+006
+           Pb-2 1 2               1 15. 1 8   0.60   3.603E+007        2 .36E+005         6.786E+006               1.765E+007 23 8.63*  43.60    2.356E+005                           4. 2 88E+005             1.114E+005 300.09      3.30   4.616E+006                         -9 .037£+006               2 . 212E+006 Pb2 12-XR                74.82   10.28    2 .437E+006       l.42E+006          2 .432E+004              1.197E+006 77.11   17.10    1. 42 3E+006                       -1.428E+005                6.989E+005 87.35     3 .97  5.951E+006                           5.863E+006               2 .921E+006 89.78     1. 46  1. 57 5E+007                       -7. 92 1E+006              7.728E+006
+           Bi- 214                609.32*   45.49    2 .797E+005       2 .80E+005         l.173E+006               1.294E+005 768.36      4.89   3 . 2 18E+006                        5.342E+005               1. 499E+006 806.18      1. 2 6 1. 2 49E+007                       - 1. 58 4E+005             5 .807E+006 934.06      3.11   5.051E+006                           9.172E+005               2 . 33 4E+006 1120. 2 9*  14.92    5 . 2 73E+005                        1. 044E+006              2 .198E+005 1155.21       1. 63  1.010E+007                         -2 .051E+004               4.642E+006 1238.12*      5.83   2 . 3 46E+006                        l.555E+005               1 .055E+006 128 0 .98     1. 43  1 .017E+007                          5.817E+006               4.599E+006 1377.67       3.99   4. 2 38E+006                         3 . 2 74E+006            1. 93 6E+006 1385.31       0.79   1.862E+007                         -1. 12 8E+007              8. 3 86E+006 1401. 5 2     1. 33  1.135E+007                           2 .094E+006              5.124E+006 1407.99       2.39   6.613E+006                         -l.869E+006                2.998E+006 1509. 2 1     2.13   6.812E+006                           4.349E+006               3.044E+006 1661. 2 7     1. 05  1 .047E+007                          1.403E+006               4.453E+006

[323]

lC.L.LUe t*JLJl"i I"\t:: .f:JU L L U/ .l.V/ L V.l.U ',I. VL * .l. I r 1*1 r a~c:: u Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve l Name (keV) ( ~:) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM )

+       Bi-2 14                    17 29 .59    2 .88   4. 33 1E+006    2 .80E+005         1.096E+006 1.874E+006 1764.49    15.30     1. 39 1E+006                       1. 22 0E+006 6.401E+005 1847.43      2 .03   6.382E+006                         4.442E+006 2 .762E+006
   >                               2118.51      1. 1 6  O.OOOE+OOO                         O.OOOE+OOO O.OOOE+OOO
+        Pb-214                      2 41.99*   7.25    1.417E+006      3.24E+005          2 .579E+006 6.701E+005 2 95. 22 18.42     9. 2 77E+005                      7 .12 9E+005 4.468E+005 351.93*  35.60     3. 2 40E+005                       6.985E+005 1. 522E+005 785.96     1. 06  1.246E+007                        -1. 748E+007 5.718E+006 Pb214-XR                       74.8 2   5.80    4.319E+006      2 .51E+006        4.311E+004 2 .122E+006 77.11    9.70   2 .509E+006                       -2 .517E+005 1 .232E+006 87.35    2 .24  1.055E+007                         1.039E+007 5.176E+006 89.78     0.82   2 .805E+007                      -1.410E+007 1.376E+007
+       Ra- 22 6                    186. 2 1*   3 .64  3.401E+006       3 .40E+006        6.956E+005 1.634E+006 Ac- 22 8                    129.07      2 .4 2 8.531E+006       7.82E+005         4.025E+006 4.175E+006 209.25      3.89   4.472E+006                       - l.110E+006 2 .169E+006 270.24      3.46   4.727E+006                         2 .050E+006 2 . 27 7E+006 328.00      2 .95  5.324E+006                         4.094E+006 2 .549E+006 338.32    11. 2 7  l.466E+006                         1.573E+006 7.028E+00 5 409.46      1. 92  7.971E+006                         3 .093E+006 3 .787E+006 463.00      4.40   3.596E+006                         1.164E+006 1.705E+006 794.95      4.25   3 .799E+006                      -3 .376E+006 1. 771E+006 911. 2 0  2 5.80   7.816E+005                         7.619E+005 3 .680E+005 964.77      4.99   3 . 3 99E+006                      2 .436E+006 1.578E+006 968.97    15.80    l.110E+006                         6.897E+005 5.167E+005 1 588.20      3. 22  4.384E+006                       -1. 614E+006 1. 945E+006 Pa -2 31                      2 7.36* 10. 3 0  7.140E+005       7 . 14E+005       8.418E+005 3 .359E+005 283.69      1. 70  1.010E+007                         2 .697E+006 4.869E+006 300.07      2.47   6.167E+006                       -1. 2 07E+007 2 .955E+006 302.65     2. 2 0  6.846E+006                       -1.904E+005 3 . 2 78E+006 330.06     1. 40   1.071E+007                         4.423E+006 5.115E+006 Th- 23 4                      92.38    2.13    1. 068E+007     1 .07E+007       -3 .455E+006 5.236E+006 92.8 0   2.10    1.079E+007                       -9. 32 6E+005 5.293E+006 112.81     0.21    1.047E+008                         8.135E+007 5.132E+007

+ U-23 5 143.76 10.96 1.715E+006 2 .16E+00 5 - 1.059E+006 8.369E+005 163.33 5.08 3 .653E+006 2 . 2 09E+006 1. 781E+006 185.71* 57. 2 0 2 .164E+005 4.426E+004 1.040E+005 202.11 1. 08 1.610E+007 1.598E+007 7.817E+006 2 05.31 5.01 3 .501E+00 6 -8.994E+005 1. 699E+006 + Arn-241 59.54* 35.90 4. 232E+ 00 5 4. 23 E+005 4.445E+004 2 .055E+005

      +        Nuclide identified during the nuclide identification
      * = Energy line found in the spectrum
      > = Calculated MDA is zero due to zero counts in the region, or the region is outside th e spectrum, or MDA has not been calculated
      @ = Half-life too short to b e able to perform the decay correction

[324]

'***         GA MM A       S P E C T R U M            A N A L Y S I S           *****
' **************~ * ********** * *******************************************~
.lename: 545 2 iport Generated On                    8/10/ 2 016        3:36:03 PM tmple  Title                          B306100BFRWC0l0GD tmple  Description                    STE. WALL NUMB 10 SHOT tmple  Identification                 10 1mple   Type tmple   Geometry iak Locate Threshold                    3. 00 iak Locate Range (in channels )             85 -     8192 iak Area Range (in channels)                85 -     8 1 92 ientification Energy Tolerance            10.000 keV tmple Siz e                             l.OOOE+OOO SQM tmple Taken On

quisition Started 8/10/ 2 016 3:26:01 PM

.ve Time 600.0 second s ial Time 601.4 seconds iad Time 0 . 23 9a Energy Calibration Used Done On 1 /13/ 2 015 Efficiency Calibration Used Done On 8/9/2016 Efficiency ID UNNELSTS 1 METER DATA-VALIDATED DATE/ .. i-1'1 TIME os*10

                                                           .a ,~4

[325]

                                           \.JI ..J.. v / ~ '\.J ..J.. \.J
'************************* * *** * ******* * ************************** * *******

P E A K A N A L Y S I S R E P O R T *****

'******************************** * ***************************************

Detector Name: 5452 Sample Title: B306100BFRWC010GD Peak Analysis Performed on: 8/10/~016 3:36:03 PM Peak Analysis From Channel: 85 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No . start end centroid (keV) (keV) Area Uncert. Counts 1 1 13- 121 116. 2 8 28.66 0.92 1.89E+002 54.52 2 .06E+002 2 2 84- 308 300.86 74.87 0.70 3.04E+002 126.41 8.94E+002 3 391- 399 395.08 98.45 0.38 -6.56E+000 48.17 2 .74E+002 4 945- 96 1 955.07 238.62 0.90 9.14E+001 54.01 2 . 0 3E+002 5 1175- 118 7 1180.53 2 95.05 0.57 7.36E+001 34.54 8.54E+001 6 1349- 1358 1 353 .09 338.23 0.91 2 .70E+001 22.31 4.30E+001 7 1401- 1417 1 407.50 351. 85 0.77 1.49E+002 39.57 7.65E+001 8 2 036- 2 051 2 042.90 510.8 3 1. 70 4.43E+001 26.50 4.37E+001 9 2 326- 2 34 0 2332 .1 3 583.19 1. 3 0 6.33E+001 25.39 3.38E+001 10 2 427- 2 44 2 2 435.7 3 609.11 1. 74 1.50E+002 31. 55 3.30E+001 11 2 638- 2 65 1 2 645.15 661. 50 1. 2 9 6.48E+001 2 1. 69 1. 92E+001 12 3635- 3649 3 64 2 .85 911.03 0.44 4.73E+001 2 0.70 2 .07E+001 13 3869- 388 0 3 874.19 968.88 1. 2 5 1.60E+001 13.61 1. 2 0E+001 14 447 3- 4486 4478.75 1120.03 0.43 3 .99E+001 15.86 8.13E+OOO 15 5830- 5852 5841. 72 1460.70 1. 66 3.40E+002 41. 86 2 .54E+001 16 7050- 70 64 7057.11 1764.35 0.50 3.80E+001 1 3.28 1.99E+OOO First peak in a multiplet region Other peak in a multiplet region

= Fitted singlet

rors quoted at 2 .000 sigma

[326]

1~erierence ~orrecLeu ttcL~V~LY ~epuLL 0 / l. U / L Ul.U ..J ; ..J u . u J r 1*l '********** * *********** i ******************** * ************************* * * ' *** N U C L I D E I D E N T I F I C A T I O N R E P O R T ***** '***********************+*********************************************** Sample Title: B306100BFRWC010GD Nuclide Library Used: C:\GENIE2K\CAMFILES\Zion Lib-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) ( ii ) (pCi/SQM ) Uncertainty K-40 1. 000 1460. 82

10.66 1. 77571E+007 2 .67754E+006 Sr- 85 0.984 514.01* 96.00 1.47 2 93E+005 9.03670E+004 Ba- 13 3 0. 32 1 79.61* 2 .65 1. 84460E+007 8.53845E+006

81. 00 32 .9 0 2 76.40 7.16 302.85* 18. 3 4 9.3 1 685E+005 4.62182E+005 356.01* 62 .05 6.16446E+005 l.91583E+005 383.85 8.94 Cs-137 1.000 661. 66* 85.10 2 .80004E+0 0 5 9 . 96089E+004 Tl-208 1. 000 58 3 .19* 85.00 2 .56094E+0 0 5 1. 07 32 3E+005 Pb-2 1 2 0.974 115.18 0.60 23 8.63* 43.60 4. 2 9497E+005 2 .63121E+005 30 0 .09* 3 . 30 5.17791E+006 2 .57063E+006 Bi -2 14 0.534 609. 32

45.49 l.16145E+006 2 .81336E+005 768.36 4.89 806.18 1. 2 6 934. 0 6 3 . 11 11 2 0. 2 9* 14.92 1. 2 9266E+ 0 06 5.24361E+0 0 5 1155. 2 1 1. 63 1238. 1 2 5.83 1280.98 1. 43 1 3 77.67 3.99 1 3 85.3 1 0.79 1401.52 1. 33 1407.99 2 .39 1 509.21 2 .13 1661.27 1. 05 17 2 9.59 2 .88 1764.49* 15. 3 0 1 .55877E+006 5.58771E+005 1847.43 2.03 2118.51 1.16 Pb-2 14 0 .977 2 4 1. 99* 7.25 2 . 5 8 2 55E+006 1.58107E+006 295. 2 2* 18.42 9. 2 7639E+005 4.60004E+005 351.93* 35.60 1. 0 7 445E+006 3.33952E+005 785.96 1. 06 Ac-228 0 . 3 51 129.07 2 .42 209. 2 5 3.89 270. 2 4 3.46 32 8.00 2.95 338.32* 1 1. 27 6.02499£+0 0 5 5.07809E+005 409.46 1. 92

[327]

re.er I erenc..:e ~ULLeC..:Leu 1-iC..: L .L '.' .L Ly J:\ei-)UL L 0/ .LV / L. V.L O ..J; ..JO; V..J r 1*i rayc:: '-f Nuclide Id Energy Yield Activity Activity Name Confidence ( ke\T) ( ~; ) (pCi/SQM ) Uncertainty Ac- 22 8 0.351 463.00 4.40 794.95 4. 2 5 91 1. 2 0* 25.80 7.97364E+005 3.55740E+005 964.77 4.99 968. 97 ,~ 15.80 4.55019E+005 3.89145E+005 1588. 2 0 3 . 22 Th - 23 1 0.944 2 5.64* 14.10 2 .15010E+006 8.04152E+005 84.2 1 1* 6.60 7.40635E+006 3.53287E+006 89.95* 1. 00 -1.05435E+006 7.74874E+006

        * = Energy line found in the spectrum.
        @ = Energy line not used for Weighted Mean Activity Energy Tolerance :                    10.000 keV Nuclide confidence index threshold =                              0.3 0 Errors quoted at 2 .000 sigma

[328]

L"-'-'..L. ..L.'-'..L.'-'J.J..._... _ _ _ _.__.__..._,.__,....... ..,..,_._..._ v ...._._ .J ..,.,.._..t""'_.._._ '**** +************************* * **********~***************************** ' *** I N T E R F E R E N C E C O R R E C T E D R E P O R T ***** ' *********************************************************************** Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/SQM ) Uncertainty K-40 1. 000 1. 775713E+007 2.677545E+006 Sr-85 0.984 1. 47 29 29E+005 9.036700E+004 Ba-133 0. 32 1 3 .859891E+005 8.084119E+005 Cs-137 1. 000 2 .800035E+005 9.960890E+004 Tl-208 1. 000 2 .560940E+005 1.0732 2 7E+005 X Bi-211 0.999 Pb-212 0.974 3.613463E+005 3.499975E+005 Bi-214 0.534 1. 2 51300E+006 2.266063E+005 Pb-214 0.977 4. 2 77001E+005 l.248575E+006 Ac-228 0.351 6. 332 8 3 7E+005 2 . 3323 13E+005 X Ac228-XR 0.366 X Pa-231 0.674 Th-231 0.944 2 .388086E+006 7. 3 81714E+005

                ? = Nuclide                         is part of an undetermined solution X       =       Nuclide rejected by the interference analysi s
                @               Nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at                                       2 .000 sigma
  **********                              U N I D E N T I F I E D                                                 P E A K S        **********

Peak Locate Performed on: 8/10/ 2 0 1 6 3:36:03 PM Peak Locate From Channel: 85 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol. No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified. [329]

ic.1..1.ue 1v1uh !'l.ef_.)VL L 0 / .l.V/ L V.l.U rayc: u '**************************************** * ************************************* '*** N U C L I D E M DA R E P O R T ***** '****************************************************************************** Detector Name : 545 2 Sample Geometry: Sample Title: B306100BFRWC010GD Nuclide Library Used: C:\GENIE2K\CAMFILES\ Zion Lib-BNL.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( s-, ) (pCi/SQM) (pCi/SQM ) (pCi/SQM ) (pCi/SQM)

+         K-40                1460.8 2

10.66 1.849E+006 1. 85E+006 1. 776E+007 8.537E+005 Cr-51 32 0.08 9.91 1. 52 7E+006 1.53E+006 -1.680E+006 7.302E+005 Mn-54 834.85 99.98 1.692E+005 1. 69E+005 -6.292E+004 7.899E+004 Co-58 810.76 99.45 1. 579E+005 1.58E+005 3.243E+004 7. 3 40E+004 Co-60 117 3 . 23 99.85 1.537E+005 1.44E+005 1.202E+005 7.016E+004 1 332 .49 99.98 1.443E+005 3.710E+004 6.500E+004 Nb-94 702.65 99.81 1.724E+005 1. 4 7E+005 1. 670E+004 8.106E+004 871. 09 99.89 1.468E+005 -9.973E+004 6.768E+004 Sn-1 13 2 55.13 2 .11 8.426E+006 2 .53E+005 3 . 2 46E+005 4.077E+006 391. 70 64. 97 2 .533E+005 4.373E+004 1. 209E+005 Cs-134 475. 3 6 1. 48 1.119E+007 1. 97E+005 -6 .871E+006 5.312E+006 563. 2 5 8.34 1.794E+006 -4. 92 7E+005 8.421E+005 569.33 15.37 9.788E+005 -2 .091E+005 4.595E+005 604.72 97.62 2 .520E+005 -1.112E+005 1. 2 11E+005 795.86 85.46 1.971E+005 8. 2 03E+004 9. 2 15E+004 801.95 8.69 2 .048E+006 8.821E+005 9.606E+005 1038.61 0.99 1. 562E+007 -1 . 1 74E+007 7.175E+006 1 167.97 1. 79 8.451E+006 6.198E+006 3 .852E+006 1365. 1 9 3.0 2 4. 2 65E+006 1. 2 87E+006 1.892E+006

+ Cs-137 661.66* 85.1 0 1.151E+005 1.15E+005 2 .800E+005 5.169E+004 Eu-15 2 121. 7 8 28.67 7.396E+005 5.83E+005 5.561E+005 3 .622E+005 244.70 7.61 2 . 52 9E+006 5.640E+005 1. 2 28E+00 6 295.94 0.45 4. 2 89E+007 1.1 22 E+007 2 .074E+007 344.28 26.60 5.832E+005 - 3 .113E+005 2 .787E+005 367.79 0.86 1. 855E+007 1 . 1 02E+007 8.861E+006 411.12 2.24 7. 2 68E+006 1.478E+006 3.463E+006 443.96 2.83 5.748E+006 -2 .505E+006 2 .733E+006 488.68 0.42 3.819E+007 -2 .123E+007 1.809E+007 563.99 0.49 3.137E+007 2 .239E+007 1. 4 7 5E+007 586. 2 6 0.46 4.406E+007 2 .177E+007 2 .102E+007 678. 62 0.47 3 .266E+007 - 9.456E+006 1. 526E+007 688.67 0.86 1. 892E+007 -2 .071E+006 8.867E+006 719.35 0. 2 8 5.693E+007 - 5.671E+006 2 .660E+007 778.90 12 .96 1.159E+006 - 1.050E+006 5. 3 75E+005 810.45 0.32 4.968E+007 1.713E+007 2 . 3 12E+007 867.37 4.26 3 .535E+006 - 1.559E+006 1. 63 3E+006 919.33 0.43 3 .568E+007 -1. 987E+007 1. 646E+007 964.08 14.65 1. 2 91E+006 1 .251E+005 6 .039E+005 1085.87 10.24 1. 656E+006 -6.394E+005 7.650E+005 1089.74 1. 73 9.448E+006 -6.850E+006 4.351E+006 1112.07 13.69 1. 2 53E+006 -1.241E+006 5.791E+005 1 2 1 2 .95 1. 4 3 1. 31 4E+007 1. 794E+006 6.092E+006 [330]

lC.LlOe MLJH. .r1.epoL L 0/ 1.U/ L UJ.0 ..) : ..) 0 : U ':I .t't*1 rctye Nuclide Energy Yield Line MDA Nucli de MDA Activity Dec. Level Name (keV) (i ) (pCi/SQM ) (pCi/SQM ) (pCi/SQM) (pCi/SQM ) Eu-15 2 1249.94 0.19 9.173E+007 5.83E+005 5. 2 00E+007 4.221E+007 1299.14 1. 63 8.765E+006 -5.166E+006 3 .949E+006 1408.01 2 1. 07 6. 2 20E+00 5 3.957E+005 2. 760E+005 1457.64 0.5 0 1 .044E+008 3.930E+008 5.072E+007 1528.10 0.28 3.961E+007 2.643E+007 1. 706E+007 Eu - 154 123.07 40.40 5.182E+005 4.82E+005 - 1. 810E+005 2 .537E+005 247.93 6.89 2 .590E+006 - 1. 903E+006 1. 25 4E+006 591.76 4.95 3 .032E+006 1. 019E+006 1.421E+006 692 .4 2 1. 78 9.338E+006 7.691E+006 4.382E+006 723 . 3 0 2 0.06 8.609E+005 1. 462E+005 4.045E+005 756.80 4. 52 3 . 3 80E+006 -6.542E+005 1.572E+006 87 3 .18 12 .08 1. 2 28E+006 -9.662E+004 5.663E+005 996.29 10.48 1. 535E+006 -5.738E+005 7.085E+005 1004.76 18.01 9.542E+005 5.433E+005 4.427E+005 1274.4 3 3 4.80 4.821E+005 2 .003E+005 2 .210E+005 1596.48 1. 80 6.798E+006 -5.395E+006 2 .955E+006 Eu-155 45. 3 0 1. 31 l.330E+007 8.42E+005 3 .464E+006 6.485E+006 60.01 1. 22 l.659E+007 1 .493E+007 8.117E+006 86.55 30.70 8.4 2 3E+005 5.609E+005 4.140E+005 105.31 2 1.10 1. 0 33E+006 -2. 3 16E+005 5.060E+005

+      Tl-208             583.19*   85.00    1. 428E+005      1. 43E+005      2.561E+005                 6.592E+004 Bi-21 1            351. 07*  13.02    1. 068E+006      1.07E+006       2.938E+006                 5.072E+005 Pb-2 1 1           404.85      3 .78  4.408E+006       4.4 1E+006      l.598E+006                 2 .104E+006 427.09      1. 76  8.905E+006                     -7.010E+006                  4.231E+006 832.01      3.52   4.864E+006                     -3.584E+006                  2 .273E+006 Bi-212              39.86      1. 06  1.832E+007       2 .46E+006      l.022E+007                 8.954E+006 727.33      6.67   2 .459E+006                    -4.562E+004                  1 .151E+006 785.37      1.10   1.445E+007                       3 .791E+006                6.734E+006 1 62 0.5 0    1. 47  7.618E+006                     - 1.349E+006                 3.261E+006 115.18      0.60   3.625E+007       4.03E+005       6.890E+006                 1. 776E+007
+      Pb-212 1.952E+005 23 8.63*  43.60    4.032E+005                       4.295E+005 300.09*     3.30   3.660E+006                       5.178E+006                 1.735E+006 Pb212-XR            74.8 2   10.28    2 .572E+006      1.44E+006       2 .543E+005                1. 265E+006 77.11    17.10    l.442E+006                     -1. 569E+005                 7.081E+005 87.35      3.97   6. 5 44E+006                     9.848E+006                 3 .217E+006 89.78      1. 46  1.704E+007                       3.248E+005                 8.372E+006 Bi- 214            609.32*   45.49    2 .742E+005      2. 74E+005      l.161E+006                 1. 266E+005
+                                                                                                        1. 689E+006 768.36      4.89   3.599E+006                       3.290E+006 806.18      1. 2 6 1. 2 96E+007                   - 3.755E+006                 6 .044E+006 934.06      3. 11  5.323E+006                       1. 624E+006                2 .470E+006 1120.29*    14.92    5.990E+005                       1. 293E+006                2 .557E+005 1155.21       1. 63  l .010E+007                      3.622E+006                 4.642E+006 1238.12       5.83   3 .4 3 1E+006                  -2 .961E+005                 1.597E+006 1280.98       1. 43  l .077E+007                    -5 .408E+006                 4.896E+006 1 377.67      3.99   4.082E+006                       2 .112E+006                1. 858E+0 0 6 1385. 3 1     0.79   1. 5 66E+007                   -3 . 3 16E+007               6.908E+006 1401. 52      1. 33  1.062E+007                        4.601E+006                4.757E+006 1407.99       2 .39  5.474E+006                       3.483E+006                 2 .429E+006 1509. 2 1     2 .13  6.812E+006                       1. 82 0E+006               3.044E+006 1661.27       1. 05  l. 2 30E+007                      4. 32 9E+005              5.371E+006

[331]

Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Level Name (keV) ( ":: ) (pCi/SQM ) (pCi /S QM ) (pCi/SQM ) (pCi/SQM ) + Bi-214 17 29 .59 2 .88 4.950E+006 2 .74E+00 5 8.075E+005 2 .184E+006 1764.49* 15. 3 0 4.437E+005 1.559E+006 1.664E+005 1847.43 2 . 03 6.945E+006 5 .553E+005 3 . 043E+006 2 118.51 1.16 O.OOOE+OOO O.OOOE+OOO O.OOOE+OOO

 >                                                                                 1.174E+006

+ Pb- 2 14 2 41. 99* 7. 2 5 2 .424E+006 3 .91E+005 2 . 5 83E+006 2 95. 22

18.42 6.557E+005 9 .2 7 6E+005 3 .108E+005 3 51. 93* 35.60 3.905E+005 1.074E+006 1.855E+005 785.96 1. 06 1.525E+007 9. 1 37E+006 7.113E+006 Pb21 4-XR 74.82 5.80 4.559E+006 2 .54E+00 6 4.507E+005 2 . 2 42E+006 77.11 9.70 2.541E+006 -2 .765E+005 1. 2 48E+006 87.35 2 . 24 1.160E+007 1.745E+007 5.702E+006 89.78 0. 82 3.034E+007 5.783E+005 1.491E+007 Ra-226 1 86. 2 1 3 . 64 5.244E+006 5.24E+006 2 .814E+006 2 .555E+006

+ Ac- 22 8 129.07 2 .42 8.755E+006 4.75E+005 9.376E+006 4. 2 87E+006 209.25 3 .89 4.779E+006 -1.666E+006 2 . 32 3E+006 2 70. 2 4 3 .46 5.026E+006 4.819E+006 2.427E+006 328.00 2 .95 5.835E+006 -3 .410E+004 2 .804E+006 338. 32 1* 11. 2 7 7.856E+005 6.025E+005 3 . 62 6E+005 4 0 9.46 1. 92 8.449E+006 1 . 854E+006 4.0 2 6E+006 463.00 4.40 3.596E+006 -1. 743E+006 1.705E+006 794.95 4. 2 5 4.040E+006 4.129E+006 1. 891E+006 911 . 2 0* 25.80 4.746E+005 7.974E+005 2 .145E+005 964.77 4.99 3.741E+006 5.140E+005 1. 749E+006 968.97* 15.80 5. 92 1E+005 4.550E+005 2 .575E+005 1 588.20 3 . 22 5.143E+006 - 9.411E+005 2 . 3 25E+006 Pa - 23 1 2 7.36* 10.30 1. 2 51E+006 1. 2 5E+006 2 .943E+006 6.0.46E+005 2 8 3 .69 1. 70 l.018E+007 6.420E+006 4.909E+006 3 00.07* 2 .47 4.890E+006 6.918E+006 2 .318E+006 3 02 .65 2 . 20 7. 392 E+006 1.2 1 0E+006 3 .551E+006 330.06* 1. 40 6.324E+006 4.850E+006 2.919E+006 Th- 23 4 92 . 38 2. 1 3 l.129E+007 1 . 13E+00 7 6.171E+006 5.545E+006 92.8 0 2 .10 1 .136E+007 4.575E+006 5.576E+006 112.8 1 0. 2 1 1. 051E+008 2 .689E+007 5.153E+007 U- 235 1 43.76 10.96 1. 845E+006 3 .34E+005 5. 23 5E+005 9.020E+005 163.33 5.08 3 .861E+006 l. 52 8E+006 1. 885E+006 185.71 57. 2 0 3 .342E+005 l. 2 62E+005 1. 629E+005 202.11 1. 08 l .797E+007 9.839E+005 8.752E+006 205.31 5.01 3 .821E+006 -7.178E+005 1. 860E+006 Am-241 59.54 35.90 5.559E+005 5.56E+005 l.964E+00 5 2 .719E+005

   + = Nucl ide identified during the nuclide identification

Energy line found in the spectrum

   > =    Calculated    MDA is zero due to zero counts in the region, or the region i s outside the spectrum, or MDA has not been calculated
   @ = Half-life too short to be able to perform the decay correction

[332]}}

ML19295G791

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