ML083080097

Letter Dated September 16, 2008, Providing Background Information for Conference Call with Humboldt Bay on Soil Sampling of New Generation Site

ML083080097
Person / Time
Site:	Humboldt Bay
Issue date:	09/16/2008
From:	Sokolsky D Pacific Gas & Electric Co
To:	Adams W, John Hickman, Whitten J NRC/FSME, NRC Region 4, Oak Ridge Institute for Science & Education
References
Download: ML083080097 (295)

Text

September 16, 2008 Mr. Jack Whitten USNRC Region IV 612 E. Lamar Blvd. Suite 400 Arlington TX 76011-9908 Mr. Wade C. Adams Health Physicist

/Survey Projects Oak Ridge Institute for Science and Education (ORISE)P.O Box 117, Mail Stop 19 Oak Ridge, TN 37831-0117 Mr. John B. Hickman, Project Manager U.S. Nuclear Regulatory Commission Two White Flint North Mail Stop T-8 F5 11555 Rockville Pike Rockville, MD 20852-2738 Gentlemen:

Enclosed are the following items for your information in preparation for the conference call we will have on Tuesday, September 23, 2008 at 10 am (PDT), 1 pm (EDT) to discuss taking near-term soil samples to be used in the Final Status Survey:* Report "Radiological Status of the Humboldt Bay Repowering Project Soils," prepared by Enercon Services, Inc for PG&E/Humboldt Bay Power Plant, dated September 2008* DRAFT Report "Historical Site Assessment," prepared by Enercon Services, Inc for PG&E/Humboldt Bay Power Plant, dated September 2008 (DRAFT DOCUMENT -PLEASEýDO NOT PLACE IN ADAMS)* Two aerial photographs of the Humboldt Bay site showing the outline of the location of the new fossil facility (Humboldt Bay Repowering Plant) where the soil samples will be taken near-term for use in the Final Status Survey* Site Plot Plan used during a PG&E/NRC meeting to discuss Partial Site Characterization, February 21, 2007, in Rockville, MD, showing location of the new fossil facility (Humboldt Bay Repowering Plant) where the soil samples will be taken, near-term for use in the Final Status Survey For the conference call, dial 1-877-481-7043, then hit meeting code *7074440801*

Three NRC Region IV inspectors will be onsite at HBPP during the call. If you have any questions, please do not hesitate to contact me.David Sokolsky Supervisor of Licensing Humboldt Bay Power Plant 707-444-0801 dds2@pge.com Radiological Status of the Humboldt Bay Repowering Project Soils Prepared for Humboldt Bay Power Plant Pacific Gas & Electric Company Eureka, California Prepared by E NERCON Enercon Services, Inc.4499 Old William Penn Hwy Murrysville, Pennsylvania September 2008 OENERCON EXce~ience-Every project. Every dcoy September 2, 2008 DGM-08-004 Mr. David Sokolsky Pacific Gas & Electric Company Humboldt Bay Power Plant 1.000 King Salmon Avenue Eureka, CA 95503

Subject:

Radiological Status of the Humboldt Bay Repowering Project Soils

Dear Mr. Sokolsky:

The intent of this letter is to describe the current radiological status of the soils in the Humboldt Bay Repowering Project (HBRP) area. ENERCON Services, Inc. (ENERCON) has determined that the area has no significant detectable residual contamination from Nuclear Reactor Operations at the Humboldt Bay Power Plant (HBPP). This determination is based upon the review of data from three different sampling efforts of the soils in the HBRP area; specifically, the characterizations performed by IT/Duratek in 1997, ENERCON in 2007, and TRC Solutions in 2008 were reviewed.

Since the characterization performed by ENERCON for the License Termination Plan (LTP) is still underway,.

a summary of the sampling effort and the analysis data from the ENERCON soil sampling effort in the HBRP area in 2007 is attached.The highlights from the different sampling efforts specific to the HBRP area are as follows: IT/Duratek Summary -Subsurface borings were advanced to a depth of 4 feet in 9 locations in the HBRP area. Samples were collected at I-foot intervals beginning at 0.5 feet. One location had 6 additional borings in the immediate area. This grouping of samples was to determine the extent of contamination located at the end of a drainage pipe that ran along the northern edge of the train tracks. The tracks and the drain line had been covered by fill and gravel. All samples in the HBRP area were less than the accepted site background of 0.5 pCi/g Cs-137, except the one location with close grouping of borings had three samples at a depth of 3.0 to 3.5 feet with concentrations ranging from 1.34 pCi/g to 1.84 pCi/g and three samples had detectable Co-60 with a.maximum concentration of 0.9 pCi/g. The location with detectable Co-60 and elevated Cs-137 is on the northern edge of the HBRP boundary and should not be near the foundation of the actual generating plants or ancillary equipment.

Additional samples were not collected to confirm or determine the extent of the elevated radioactive material since the concentrations were less than potential release criteria.

A drawing with IT/Duratek sample data from samples collected in the HBRP area is included in Attachment 1.ENERCON Data Summary -The survey of the area indicated no significant detectable contamination from HBPP Unit 3 nuclear reactor operations.

One surface soil sample result indicated a Cs-137 concentration of 0.653 pCi/g with a two-sigma uncertainty of+0.084pCi/g.

All other samples Cs-137 results were less than the HBPP site established background of 0.5 pCi/g Cs-137. All results for Co-60, Am-241, Pu-239/240, 4490 Old William Penn Highway Murrysville, PA 15668 phone 724.733.8711 fax 724-325.6383 enercon.com Mr. David Sokolsky September 2, 2008 Page 2 of 3 Cm-242/244, Sr-90, and Tritium were not detected.

The result of the soil sample Gamma radiation surveys indicated no levels of gamma radiation greater than twice background.

Laboratory analysis reports from General Engineering Laboratories are attached as well as drawings of the surface soil sample locations and the gamma walkover measurement locations.

Additional samples were not collected to confirm or determine the extent of the elevated radioactive material since the concentrations were less than potential release criteria.

A summary of the ENERCON sample collection process, drawings depicting the sample locations, and laboratory analysis results are included in Attachment 2.TRC Data Summary -TRC Solutions, Inc. advanced 44 borings, with approximately 3 samples per boring, in the HBRP area in support of their Environmental Remedial Investigations in July 2008. In addition to the remedial investigation analyses for non-radiological materials, all samples were submitted for gamma spectroscopy analysis to gain additional knowledge of the subsurface soils in the HBRP area. It was necessary to determine whether or not the soils could be released off site for disposal without restriction, i.e. no radionuclide concentrations derived from Unit 3 operations.

All subsurface samples collected from the borings in HBRP Area were less than the site background of 0.5 pCi/g Cs-137, except for one sample with a concentration of 1.23 pCi/g +/- 0.146 pCi/g at a depth of 4.5 feet. Additional samples were not collected to confirm or determine the extent of the elevated radioactive material since the concentrations were less than potential release criteria.

A drawing of the sample locations and the laboratory analysis results are included in Attachment 3.* The aforementioned soil characterization efforts primarily addressed soil exposure routes from the air or groundwater.

Two additional exposure routes, burial or subsurface migration along subsurface pipe trenches, may be possible.

The operating history and personal accounts do not indicate a high potential for these routes to occur. As a conservative measure, additional sampling will occur during the initial construction phase of the HBRP (i.e. interference removal of buildings, subsurface structures, and pipes and area preparation/grading) to assess whether or not soils were exposed to radioactive material through either of these exposure routes. During the interference removal phase as previously non-accessible soils become accessible, samples will be collected and analyzed for Cs-137. The non-accessible areas include soils below pipes, soils beneath foundations, and soil that does not appear to be native to the immediate area. Objects and other items encountered during excavation of soils in HBRP, will be surveyed with a portable radiation detection instrument before disposal offsite. As a final check, all disposal trucks leaving HBPP with soils or debris for unrestricted release will be scanned independently by the HBPP Radiation Protection Department to ensure compliance with disposal facility waste acceptance criteria Based on the characterization survey results and historical operations at HBPP, a high degree of confidence has been obtained that future worker(s) assigned to the HBRP facility will receive no significant radiation dose above background.

Survey results indicate radioactive material concentrations exist in the surface and subsurface soils;. however, the data also indicates that the average concentration should be significantly less than the Nuclear Regulatory Commission's screening levels for residual radioactive material, and will not require any remediation.

Furthermore,.

it is ENERCON's opinion that these values are significantly below proposed Derived Concentration Guideline Levels (DCGLs) currently in development for the site.During the decommissioning of HBPP Unit 3 Nuclear Reactor, a Cross Contamination Prevention and Monitoring Plan will be implemented to ensure the HBRP area and facilities are not impacted Mr. David Sokolsky September 2, 2008 Page 3 of 3 from Unit 3 decommissioning activities.

As part of this plan, routine surveys will be conducted at the facility and continuous environmental air samples will be collected.

HBPP has also completed the installation of 7 groundwater monitoring wells to augment the existing network of monitoring wells. Additionally, engineering and administrative controls will be implemented to minimize or eliminate the risk of inadvertent releases of radioactive material during decommissioning activities.

Based on the above discussion, there is no significant radiological impact to construction workers or.the future personnel in the HBRP area.Sincerely, Health Physicist/Project Manager DGM:dmm cc: John Albers Keith Mahosky Gerald Williams Attachments ATTACHMENT 1 A Drawing With IT/Duratek Sample Data From Samples Collected In The HBRP Area X:\PROJECT 07\HBPP\UN JUND UTILITIES AND EARTHWORK\08-PGE-052.dwg, SHEET 1, 9/2/2008 5:40:58 PM, I-i"1~ ~'/' ~/ .:~'/N 7\ /I//O O1/Sd////Ce\HUMBOLDT BAY POWER PLANT EUREKA, CA 1997 IT/DURATEK SOIL SAMPLE LOCATIONS AND RESULTS PACIFIC GAS & ELECTRIC SAN FRANCISCO, CA ATTACHMENT 2 A Summary Of The ENERCON Sample Collection Process, Drawings Depicting The Sample Locations, And Laboratory Analysis Results HBRP Area History and ENERCON Surface Soil Characterization Summary EN7ERCON has been contracted by PG&E to develop the License Termination Plan (LTP) for HBPP Unit 3. The characterization effort to support the development of the HBPP LTP is in the final stages and a final report has not been written. Therefore, the following information is summarized from the data contained in the ENERCON Characterization Survey Package 005SS3, New Generation Area: Operational History of Survey Unit The HBRP area was not involved in typical plant work activities during operation of the H3BPP Unit 3 Nuclear Reactor. The northern portion of this area is downwind of the Unit 3 stack, for the typical winter south to southeast winds. A large portion of this area has been covered by fill material with about one third of the fill material placed prior to Unit 3 operation and about half of the fill material placed since the beginning of Unit 3 operation.

The historical activities in filled portions of this survey area are related to landscaping, operation of the Mobile Electric Power Plants (MEPPs), diesel oil storage, material/equipment storage, painting (and sandblasting to prepare for painting), office space and employee parking. The area has underground piping and electrical conduits.

Items of interest in the survey area include the original sanitary sewer leach field for Unit 3 (south of the Oily Water Separator), and the filled drainage ditch/drainpipe that was constructed parallel to the rail spur roadbed.Detailed Physical Description of the HBRP This survey unit contains the land area where the HBRP will occur. Some of the survey unit, approximately 50%, is covered by asphalt and/or rock. The remaining surface soil is covered with grass and other natural vegetation.

This area has been initially classified as a MARSSIM Class 3 area due to the very low potential for radiological contamination to be present based off of soil sample data from the IT/Duratek 1997 Characterization effort.Characterization Survey Instructions Summary The characterization survey consisted of 14 soil samples and a gamma radiation walkover survey.The design of the Characterization Survey was based on criteria from NUREG-1757, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSM).

Soil samples were collected at locations that were determined by random selection using the current version of Visual Sample Plan. Physical collection of the soil samples was delineated in the survey I instructions which included the sampling process, field decontamination of tools, sample labeling requirements, and sample location.

The procedure HPP-OP-002, Chain of Custody, was used to delineate the required chain of custody process and requirements to ensure the integrity of the samples collected.

Soil samples were submitted to General Engineering Laboratories (GEL) for gamma spectroscopy for Cs-137 and Co-60 and for analysis of Am-241, Pu-239/240, Cm-242/244, Sr-90, and Tritium.The survey instructions also described the procedures to be followed for the gamma radiation walkover survey which covered 100% of accessible surface soil areas using a 2x2 Sodium Iodide (Nal) detector with a scanning speed of less than 0.5 m/s. The gamma walkover survey was'performed using a Ludlum Model 44-10 (2" x 2") Nal detector coupled to a Ludlum Model 2221 meter. A Trimble Pathfinder ProXR Global Positioning System (GPS) was used to log the position and radiation measurements collected during the gamma walkover survey. The GPS was also used to located and log the surface soil samples collected in the area.Characterization Data Results The survey of the area indicated no significant detectable contamination from HBPP Unit 3 nuclear reactor operations.

One surface soil sample result indicated a Cs-137 concentration of 0.653 pCi/g with a twO-sigma uncertainty of+/- 0.084pCi/g.

'All other Cs-137 sample results were less than the HBPP site established background of 0.5 pCi/g Cs-137. All results for Co-60, Am-241, Pu-239/240, Cm-242/244, Sr-90, and Tritium were not detected.

The result of the soil sample Gamma radiation surveys indicated no levels of gamma radiation greater than twice background.

Laboratory analysis reports from General Engineering Laboratories are attached as well as drawings of the surface soil sample locations and the gamma walkover measurement locations.

2

~L 2;'~'~GAMMA WALKOVER SURVEY LOCATIONS AND SOIL SAMPLE ANALYTICAL DATA PACIFIC GAS & ELECTRIC HUMBOLDT BAY POWER PLANT CflsfctD~mtlnsO, 30716d..g ipE0,O~ 9t212M 5:2239 1,hd cn-C,-(n(0~~ 02? -o ý0 o.Ký .: 2 -..GAMMA WALKOVER SURVEY LOCATIONS NEW GENERATING AND SOIL SAMPLE ANALYTICAL DATA FACILITY AREA SURVEY LOCATION PACIFIC GAS & ELECTRIC HUMBOLDT BAY POWER PLANT Laboratories LLC a member of The GEL Group ýrc PO Box 30712 Charleston.

SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com November 01, 2007 Mr. Dustin G. Miller Enercon Services, Inc.4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Re: Humboldt Bay NPP soils Work Order: 195257

Dear Mr. Miller:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on October 08, 2007. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.

Our.policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction.

If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.Sincerely, Erin Stanley Project Manager Chain of Custody: 021-07 and 030-07 Enclosures problem solved Page: / ..or Z General Engineering Laboratories, LLC ProjectU:

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For liquid matrices, indicate with a -Y -for yes the sample was field filtered or -N -For somple was not field filtered.4.) Matrix Codes: OW-Drinking Water, GW-Groundwiater.

SW-Suorfce Water, WW=Wate Water, W-Water. SO-Soil. SDlSediment, SL-Sludge, SS-Solid Waste, O-Oil, F-Filier.

P-Wipe, U-Urine, F-fee], N-Nasal 5.) Sample Analysis Requested:

Analytical method requested (i.e. a260B, 6OIOBn470A) and number ofcontainers provided for each (i.e. 8260B -3, 6010,a'74704

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.YELLOW =FILE PINK CLIENT For Lab Receiving Use Only* Custody Seal Intact?YES NO Cooler Temp.: C Page: of General Engineering Laboratories, LLC Projct: -o!0&5 GEL Chain of Custody and Analytical Request 2040SavageRoid GEL Quote H: /Charleston, SC 29401 COCNumberC":

GEL Work Order Number: Phone: (843) 556-8171 PO Number: _Fax: 843) 766-1178 Client Name: Erl__ -Znco Phone : q) 733-) Sample Analysis Requested s (Fill in the number of containers for each test)Project/Site Name: 'A :. O 1 " -, I /J l ,.' v Fax : (7 L, 5 Shou.d th... <-- Preservative Type (6)C ../_0Liollected by ~Vt '.)2C.'"-. ,J'"" Send Results To: extra sample is erequired for sample cieonsdrd CollecD~l Notelexratampe i Sme DCollected QC Code Field Sample specific QC (Millta ry) Filtered i Matrix For coepoaItej

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indicate with a -Y -for yes the sample was field filtered or -N -for sample was not field filtered.4.1 Matrix Codes: DW-Drinking Water. GW-Groundwater.

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GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www-gel.com Certificate of Analysis Report for for ENRC002 Enercon Services, Inc.Client SDG: 195257 GEL Work Order: 195257 Sample(s)

Contained within this report: Lab Sample ID 195257001 195257002 195257003 195257004 195257005 195257006 195257007 195257008 195257009 195257010 195257011 195257012 195257013 195257014 Client Sample ID 005SS3-6 005SS3-8 005SS3-10 005SS3-11 005SS3-12 005SS3-13 005SS3-14 005SS3-05 005SS3-7 005SS3-9 005SS3-4 005SS3-2 005SS3-1 005SS3-3 Sample Description N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Collected 09/18/2007 09:30 09/18/2007 10:00 09/18/2007 10:20 09/18/2007 10:40 09/18/2007 11:00 09/18/2007 11:20 09/18/2007 11:40 09/18/2007 16:00 09/07/2007 11:00 09/07/2007 11:20 09/07/2007 11:40 09/07/2007 12:00 09/07/2007 12:40 09/07/2007 13:00 Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures.

Please direct any questions to your Project Manager, Erin Stanley.Reviewed by GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 195257013 005SS3-1 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 07, 2007 October 08, 2007 November 01, 2007 2 2 Sigma Activity Uncertainty Analyte Run Date Qualifier MDA RL Gamma Spec Co-60 Cs-137 Units pCi/g pCi/g 10/31/07 10/31/07 U 2.19E-02 U -1.56E-02 2.34E-02 2.33E-02 4.47E-02 3.78E-02 1.00E-01 1.00E-01 Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level..2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MIDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61. Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 195257012 005SS3-2 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 07, 2007 October 08, 2007 November 01, 2007 2 2 Sigma Activity Uncertainty Analyte Run Date Qualifier MDA RL Gamma Spec Co-60 Cs- 137 Units pCi/g pCi/g 10/31/07 10/31/07 U U 1.42E-03-5.97E-03 3.55E-02 3.71 E-02 5.90E-02 6.08E-02 1.00E-01 1.OOE-01 Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 195257011 005SS3-4 Soil Client: Enercon Services, Inc.Collect Date: September 07, 2007 Receive Date: October 08, 2007 Report Date: November 01, 2007 2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte Gamma Spec Co-60 Cs-137 MDA 4.32E-02 4.33E-02 RL Units pCi/g pCi/g 10/31/07 10/31/07 U U 1.43E-02 1.49E-02 2-90E-02 3.17E-02 1.00E-01 1.00E-01 Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel-com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 195257014 005SS3-3 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 07, 2007 October 08, 2007 November 01, 2007 Analyte Run Date Qualifier 2 2 Sigma Activity Uncertainty 2.26E-02 2.75E-02 0.OOE+00 5.1 OE-02 MDA RL Units Gamma Spec Co-60 Cs-137 10/31/07 10/31/07 U U 5.20E-02 5.90E-02 1.00E-01 I.OOE-01 pCi/g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 195257008 005SS3-05 Soil Client: Collect Date: Receive Date: Report Date: 2 Sigma Uncertainty Enercon Services, Inc.September 18, 2007 October 08, 2007 November 01, 2007 Analyte Gamma Spec Co-60 Cs-137 Run Date Qualifier 2 Activity-2.33E-03 1.25E-01 MDA RL Units 10/31/07 10/31/07 U 3 2-77E-02 4.26E-02 4.60E-02 4.13E-02 100E-0I 1.00E-01 pCilg pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www-gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 195257001 005S53-6 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 18, 2007 October 08, 2007 November 01, 2007 2 2 Sigma Activity Uncertainty Analyte Run Date Qualifier Gamma Spec Co-60 Cs-137 MDA 5.32E-02 4.8613-02 RL Units pCi/g 10/30/07 10/30/07 U U-3.59E-03 3.43E-02 3.24E-02 4.64E-02 1.001E-01 1.00E-01..................

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Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MIDA, or LOD.Ul Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: .Client Sample ID: Matrix: Geometry Received: 195257009 005SS3-7 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 07, 2007 October 08, 2007 November 01, 2007 2 2 Sigma Activity Uncertainty Analyte Run Date Qualifier MDA RL Gamma Spec Co-60 Cs-]37 Units pCi/g pCi/g 10/31/07 10/31/07 U 1.96E-02 3 3E0 3.05E-02 6.96E-02 5.56E-02 5.01E-02 1.00E-01 1.00E-01 Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MIDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 195257002 005SS3-8 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 18, 2007 October 08, 2007 November 01, 2007 2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte MDA RL Gamma Spec Co-60 Cs- 137 Units pCi/g pCi/g 10/30/07 10/30/07 U 3-2.63E-02 1.24E-01 4.46E-02 7.52E-02 6.47E-02 7.63E-02 1 00E-01 1.00E-01 Note(s): I. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 195257010 005SS3-9 Soil Client: Enercon Services, Inc.Collect Date: September 07, 2007 Receive Date: October 08, 2007 Report Date: November 01, 2007 2 Sigma Activity Uncertainty Analyte Run Date Qualifier INIDA RL Gamma Spec Co-60 Cs- 137 Units pCi/g pCi/g 10/31/07 10/31/07 U 3 1.70E-02 6.53E-01 2.73E-02 8.40E-02 4.98E-02 4.26E-02 1.00E-01 1.OOE-01 Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MIDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -ww.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 195257003 005SS3-10 Soil Client: Enercon Services, Inc.Collect Date: September 18, 2007 Receive Date: October 08, 2007 Report Date: November 01,2007 Analyte Run Date Qualifier 2 Sigma Activityý Uncertainty

-3.29E-02 3.57E-02 0.00E-+00 7.73E-02 MDA RL Gamma Spec Co-60 Cs-137 Units pCi/g pCi/g 10/30/07 10/30/07 U Ul 4.94E-02 5.55E-02 1.00E-01 1.00E-01 Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geomelry Received: 195257004 005SS3-11 Soil Client: Enercon Services, Inc.Collect Date: September 18, 2007 Receive Date: October 08, 2007 Report Date: November 01, 2007 Analyte Run Date Qualifier Ga mma. Spec Co-60 Cs-137 2 Activity-2.1 IE-02 1.63E-01 2 Sigma Uncertainty MDA RL Units pCi/g pCilg 10/30/07 10/30/07 U 3 3.55E-02 6.3 1E-02 5.33E-02 4.79E-02 1.00E-01 1.00E-01 Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MIDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www-gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 195257005 005SS3-12 Soil Client: Enercon Services, Inc.Collect Date: September 18, 2007 Receive Date: October 08, 2007 Report Date: November 01, 2007 2 2 Sigma Activity Uncertainty Analyte Run Date Qualifier MDA RL Gamma Spec Co-60 Cs-137 Units pCi/g pcilg 10/30/07 10/30/07 U 3 2.37E-02 1-50E-01 3.68E-02 5.53E-02 6.65E-02 5.89E-02 I .OOE-01 1.00E-01 Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 195257006 005SS3-13 Soil Client: Enercon Services, Inc.Collect Date: September 18, 2007 Receive Date: October 08, 2007 Report Date: November 01, 2007 2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte MDA RL Units Gamma Spec Co-60 Cs-137 10/30/07 10/30/07 U 3 6.99E-03 2.46E-01 3.251E-02 5.17E-02 5.57E-02 4.82E-02 1.00E-01 1.00E-01 pCi/g pCi/g...... ... .. .... ..... .. ... ... ...... ...... .... ..... .. ...... ... .. ... ... ............... ... .--. ... .. ....... ......... ..... .. .--.. .. ..... .. ....... .. ....... ... ....... ... ... ... ....... .. ...... ........-. ---------- --- -- --- ----- ---- ------ -- -- ----- ------- ----- ----- ----- ---------- --Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample coHect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MIDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: NMatrix: Geometry Received: 195257007 005SS3-14 Soil Client: Enercon Services, Inc.Collect Date: September 18, 2007 Receive Date: October 08, 2007 Report Date: November 01, 2007 2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte MDA RL Gamma Spec Co-60 Cs-137 Units pCi/g 10/31/07 10/31/07 U 2.06E-02 3 1.61E-01 3.03E-02 7.07E-02 5.54E-02 4.95E-02 1.00E-01 1.00E-01 Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty).

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy-Uncertain identification GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www-gel.com QC Summary Enercon Services, Inc.4499 Old William Penn Highway Murrysviile, Pennsylvania Contact: Mr. Dustin G. Miller Report Date: November 1, 2007 Page 1 of 2 Workorder:

195257 Parmname Rad Gamma Spec Batch 691633 QC1201436625 195257004 DUP Cesium-] 37 Cobalt-60 QC1201436626 LCS Americium-241 Cesium-] 37 NOM Sample Qual QC Units RPD%REC% Range Anist Date Time (0%- 100%) MJH1l 11/01/07 10:54 N/A 1.63E-01+/-6.31 E-02 U -2.11E-02+/-3.55E-02 1.64E+01 6.28E+00 8.9 1E+00 l.1 ]E-01+/-5.11 E-02 U -2.42E-02+/-3.22E-02 1.32E+01+/-1.32E+00 6.75E+00+/-6.30E-01 9.61E+00+/-6.95E-01 U 2.51E-02+/-2.13E-02 U 1.71E-03+/-1.93E-02 pCi/g 38 pCug 14 pCi/g Cobalt-60 pCi/g pCi/g pCi/g 81 (75%-125%)

108 (75%-125%)

108 (75%-125%)

11/01/07 12:59 QC1201436624 MB Cesium-I 37 11/01/07 08:49 Cobalt-60 pCi/g Notes: The Qualifiers in this report are defined as follows:*

• Analyie is a surrogate compound* Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated M M if above MDC and less than LLD N/A RPD or %Recovery limits do not apply.ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier R Sample results are rejected U Analyte was'analyzed for, but not detected above the MDL, MDA, or LOD.U1 Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

195257 Page 2 of 2 Parmname NOM Sample Qual QC Units RJPD% REC% Range Anist Date Time Y QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.

h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by~a factor of 4 or more.^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample isgreater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/- the RL is used to evaluate the DUP result.* Indicates that a Quality Control parameter was not within specifications.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

List of current GEL Certifications as of 01 November 2007 State Certification Alaska UST-062 Arizona AZ0668 Arkansas 88-0651 CLIA 42D0904046 California 01151]CA Colorado GenEngLabs Connecticut PH-0169 Dept. of Navy NFESC 413 EPA WG-15J Florida/NELAP E87]56 Georgia E87156 (FL/NELAP)

Hawaii N/A Idaho N/A Illinois 200029 Indiana C-SC-01 Kansas E-10332 Kentucky 90129 Louisiana 03046 Maryland 270 Massachusetts M-SC012 Michigan 9903 Nevada SC12 New Jersey SCO02 New Mexico FL NELAP E87156 New York 11501 North Carolina 233 North Carolina Drinking W 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania 68-00485 South Carolina 10120001/10585001/10120002 Tennessee 02934 Texas NELAP T104704235-07-TX U.S. Dept. of Agriculture S-52597 US Army Corps of Engineer N/A Utah 8037697376 GEL Vermont VT87156 Virginia 00151 Washington C1 641 Laboratories LLC a member of The GEL Group trc PO Box 30712 Charleston.

SC 29417 2040 Savage Road Charleston.

SC 29407 P 843.556.8171 F 843-766.1178 www.gel.corn January 21, 2008 Mr. Dustin G. Miller Enercon Services, Inc.4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Re: Humboldt Bay NPP soils Work Order: 200159

Dear Mr. Miller:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on October 04, 2007 and October 08, 2007. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction.

Jf you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.Sincerely, Erin Stanley Project Manager Chain of Custody: 008-07, 009-07,010-07, 011-07, 012-07, 013-07, 016-07, 018-07, 021-07 and 030-07 Enclosures problem solved Ma Laboratodes c SAMPLE RECEIPT & REVIEW FORM Client: Aq&ý SDG/ARCOC/Work Order: -Received By: , il IDate Received:

10 -(0 ) 7 " S HIf Counts > x2 area background on samples not marked "radioactive", contact Suspected HazardInformation the Radiation Safety Group of further investigation.

COC/Samples marked as radioactive?

-/ Maximum Counts Observed*:

Classified Radioactive HI by RSO? ___COC/Samples marked containing PCBs? -Shipped as a DOT Hazardous?

-" Hazard Class Shipped: LJN#: Samples identified as Foreign Soil? t...__Sample Receipt Criteria Z 0 Comments/Qualifiers (Required for Non-Conforming Items)Circle Applicable.

seals broken 1 Shipping containers received intact and damaged container leaking container other (descrbe)sealed? %./Preservation Methd -ice bags 2 Samples requiring cold preservation blue ice dry ice none -d within (4 +/- 2 C)? :7 I/ P"114 Chain of custody documents included r with shipment?

L/" Circle Applicable seals broken 4 Sample containers intact and sealed? V damaged container leaking container other(describe)

Samples Sample ID's, containers affected and observed pIL 5 ape equiringchemical-preservation at proper pH? 1/ If Preservation added. Lot.#: 6 VOA vials free of headspace (defined asSample ID's and containers affectedi< 6mm bubble)?(If yes, immeiately deliver to Volatiles laboratoyv) 7 Are Encore containers present?Id's and tests affected: 8 Samples received within holding time? /Sample ID's on COC match ID's on Sample ID's and containers affected-bottles?10 Date & time on COC match date & time SatspleIDsaffece&

on bottles?1 Number of containers recived match Sample ID's affected: number indicated on COC?COC form is properly signed in 1 2 relinquished/received sections?Comments: PM (or PMA) review: Ininials n!ý Date 101/y -

Laboratories LLC SAMPLE RECEIPT & REVIEW FORM Client: I--F CC- 2 SDG/ARCOCIWork Order: / q 5O1-)-Received By- IDate Received: , "*If Counts > x2 area background on samples not marked "radioactive", contact Suspected Hazar information Z the Radiation Safety Group of further investigation.

COC/Samples marked as radioactive?

-L Maximum Counts Observed*:

W'O Classified Radioactive 11 by RSO? V COC/Samples marked containing PCBs? _Shipped as a DOT Hazardous?

L'NHazard Class Shipped: UN#-Samples identified as Foreign Soil? __Sample Receipt Criteria < .CommentslQualifiers (Required for Non-Conforming Items)~t4Z ZI Circle Applicable-.

seals broken Shipping containers received intact and damaged container .laking container othr (describe) 1 sealed? V o Prervafion Method: ice bags 2 Samples requiring cold preservation blue ice dry ice none otier (descnibe) within (4 +/- 2 C)?Chain of custody documents included with shipment?Circle Applicable:

seals broken 4,Sample ontainers intact and sealed? -damaged container leaking conmainer other (desraibe)

S4pl Sample containers aintace and scsealded?

Samples requiring chemical preservation at proper pH? If Preservation addedý Lot#: VOA vials free of headspace (defined asSple ID's and containers affected:< 6mm bubble)?(if yes, inamediaetty deliver to Vniatilms latmotali-ym) 7 Are Encore containers present?td's and tests afeceid 8 Samples received within holding time?* Sample ID's and containers affected: Sample ID's on COC match ID's on 9 bottles?10 Date & time on COC match date & time Sample 5ID's afferted-on bottles?Number of containers received match Sample ID's affected: number indicated on COC?12 COC form is properly signed in relinquished/received sections?Comments:

L) Fp s 12! 7'-13 0 oq-74 1 -PM (or PMA) review: Initials tZ'i/ Date /0/ly ,-

Page: Of General Engineering Laboratories, LLC Project- OS GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote 9: Charleston, SC 29407 COC Number"':

0 30 "7 GEL Work Order Number: Pn (4561 PO Number: Fax: (843) 766-1178 Client Name: Eerctvv Sknt sJ i_. Phone 4:/ Sample Analysis Requested s (Fill in the number of containers for each test)Projeet/SiteName: VAJ.-~t~lbOIA". NPP Fax(:/ ,)i 3..i43_ Siu~tdhoudhits Type (6)Project/Site Name: Rum sample be : -9) --e b Address: -S0 considered:

Comments Collected by: .i 1le Send Results To: Note: extra sample is D-ie lle required for sample rDateCollected Colic ted QC Codo FelddSsmo d "e/ime=- specific QC Sample ID (Mit.,ry) , Fillered tl Matrix (md..y hham)____,*For comp~osite~s

-indicate start and stop date/time (mm-dd-yy) (h hirm),.-p9A -oo555 0930 N NIA --I ......I 005553- 5 ogy eoq to 00 sol IO X 0 0 ,ss -C) ýoqj~ / 0-oo so I oo55ss-II io<i o Ig o )~ o r' soI oo5S:3- 0q 18o9 liop so _oo5S,53-13 Q o ec*7 I l7 o dW2 so 1 o o5:5_,3 -14 09 Ie ? 1 U 1 0 _A 50 __II 0oo5 .53 -05' 091 e&7 I e Nr N1 S o 1 A& A 7 1', TAT Requested:

Normal: Rush: Specify, (Subject to Suamharse)

Fax Results: Yes / No Circle Deliverable:

C of A I QC Summary I Level I Lcvel 2 1 Level 3 / Level 4 Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards , amole Collecion TiZon Eastern<1-i Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Received by (signed) Date Time C/fl GEL PM: I ,i,- / 9-0 Ic (Q 0Koo Method ofhip 11. Date Shiped: 0 '9 -077 SO /0' 40" X 2 q Airbill .-Z Fto F9N 03 q0o 09S30 3 3 Arab iI 0: 1.) Chain Or Custody Number- Client Determined 2.) QC Codes: N -Normal Sample. Ta = Trip Blank. FD t Field Duplicate, ER -Equipment BSank, MS = Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample, G = Grab, C- Composite 3.) Field Filtered:

For liquid matrices.

indicate with a -Y -for yes the sample was field fittered or -N -for sample wan not Field filtered.4.1 Matrix Codes: DW-Drinklng Water, GW-Groundwater.

SW-Surface Water, WW-Waste Water, W-Water, SO-Soil. SO-Sediment, SL-Sludge, SS-Solid Waste, O-Oil, F-Filter, P-Wipe, U-Urine, F-Fecal, 5.) Sample Analysis Requested:

Analytical method requested (i.e. 9260B. 6oioBf7470A) and number of containers provided for each (i~e. 8260B .3, 60tIlB/7470A

-1).6.1 Preservative Type: 11A -Iydrochloric Acid. NI -Nitric Acid. SH = Sodium Hydroxide.

SA -Sulfuric Acid, AA -Ascorbic Acid, HX -Hexane, ST -Sodium Thiosulfate, If no preservative is added -leave field blank WHITE = LABORATORY YELLOW = FILE PINK -CLIENT For Lab Receiving Wire Only Custody Seal Intact?YES NO Cooler Temp: C Page: -of f General Engineering Laboratories, LLC ProjectC:

_G_ A- GEL Chain of Custody and Analytical Request 2040SavageRoad GEL Quote 0: Charleston, SC 29407 COC Number(1:

GEL Work Order Number: -hone: (843) 556-8,71 PO Number: 1178 Client Name: Enetr , -nC, Phone, (t.q2 Sample Analysis Requested (Fill in the number of containers for each test)Project/Site Name:- \ L NI Fax #: Should this [ <-- Preservative Type (6)A sampte be ,,-J'17q a)6)C1z5 , considered;

~!Address:

/oo0 Kik-7g SJLM oVY1V 4 VCVin rKct C~\ 9~&5O,3 -o~,.,... .. ' k Comments Collected by- V \ ,'V '$_ AX -Send Results To: C O 6 V )1.- ,"7 Note: extra sample is"DOne Collcted *Time required for sample Sample ID ,,,e ,CCode Field sample Z specific QC For composites

-indicate start and stop date/time tma -dd-y-y) (hhan) I _ýLREl -C)0 SSS- '7 og-o09-o0 to0 t NIA SO I X oo5sS3-q I I 50 ___005 6SQ-,0 0-o07-m 1A0o IL so 0C55S3- I NJo so _ __ so 00o55s -3 69~o-09-09130 N \/ 5o0 I X</Al /f , h / -X) /I TAT Requested:

Normal: Rush: Specify: (Subject to Surcharge)

Fax Results: Yes / No Circle Deliverable:

C ofA / QC Summary / Level I/ Level 2 / Level 3 / Level 4 Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards saale Collecti on e Eastern C Patelfie Central Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Received (ainedL) Date Time GEL PM: 3ool /3oo P MethodorShipment:

llDaSh ed a/L OIYO7 2 n " ,LZJ , 1)/6 9 7 gY Airil 0: 7 Ff24/c3 9 01d3D!3 13 lAirijill 6: 1.) Chain of Custody Number Client Determined 2.) QC Codes: N -Normal Sample. TBx Trip Blank. FD -Field Duplicate.

EB -Equipment Blank, MS = Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample, G = Grab. C = Composite 3.) Field Filtered:

For liquid matrices.

indicate with a -Y -lot yes the sample was field filteed or -N -for aample wass not ield tiltered.4.1 Matrix Codes: DW-Drinking Water. GW-Grotmdwalcr.

SW-Surface Water. WW-Waste Water. W-Water, SO-Soil, SD-Sediment.

SL-Sludge, SS=Solid Waste, O-Oit, F-Filter, P-Wipe, U-Urine, F-Fecal. N=Na3al 5.1 Sample Analysis Requested:

Analytleal method requested (I.e. 8260B. 601 1Bn1470A) and number of containers provided for each (i.e. 8260B -I3 6010d./7470A

-I1.6.) Preservative rype: UA -Hydrochloric Acid. Ni -Nitric Acid. SH -Sodium Hydroxide, SA -Sulfuric Acid. AA Ascorbic Acid, HiX -Ilenane. ST -Sodium Thlasul'ate, Ifno preservative is added o leave lid blunk WHITE -LABORATORY YELLOW = FILE PINK = CLIENT For Lab Receiving Use Only Custody Seal Intact?YES NO Cooler Temp: C c~~!Laboratories L SAMPLE RECEIPT & REVIEW FORM Client: -" 'r SDG/ARCOC/Work Order: tq'X:5q Received By: I'I Date Received: (L.( , S *If Counts > x2 area background on samples not marked "radioactive", contact Z Z the Radiation Safety Group of further investigation.

COC/Samples marked as radioactive?

l Maximum Counts Observed*:

t-0 Classified Radioactive 11 by RSO? "_'__COC/Samples marked containing PCBs? __\_Shipped as a DOT Hazardous?

Hazard Class Shipped: UN#-Samples identified as Foreign Soil?Sample Receipt Criteria ; 0 Cormments/Qualifiers (Required for Non-Conforming Items)Circle Applicable:

seals broken Shipping containers received intact and damaged container leaking container other (describe) sealed?I Preservation Method: ice bags 2 Samples requiring cold preservation blue ice dry ice non e other (describe) within (4 +/- 2 C)?Chain of custody documents included with shipment?Circle Applicable:

seals broken 4 Sample containers intact and sealed 9 damaged container leaking container other (describe)

Sample ID's, containers affected and observed pHi-: Samples requiring chemical preservation at proper pH? If Preservation added. Lot#: 6 VOA vials free of headspace (defined as Sample ID's and containers affected:< 6mm bubble)?(If yes, immediately deliver to Volatiles laboraltry) 7 Are Encore containers present?Id's and tests affected: 8 Samples received within holding time? 'Sample ID's on COC match ID's on Sample ID's and containers affected: bottles?10oDate & time on COC match date & time Sample ID's affected: on bottles?Number of containers received match Sample ID's affected: number indicated on COC?COC form is properly signed in 12 relinquished/received sections?Comments: 5LA PM (or PMA) review: Initials qWv Date /01 9 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report for for ENRC002 Enercon Services, Inc.Client SDG: 200159 GEL Work Order: 200159 Sample(s)

Contained within this report: Lab Sample ID 200159001 200159002 200159003 200159004 200159005 200159006 200159007 200159008 200159009 200159010 200159011 200159012 200159013 200159014 200159015 200159016 200159017 200159018 200159019 200159020 200159021 200159022 200159023 200159024 200159025 200159026 Client Sample ID 002SS2-24 002SS2-10 002SS2-7 002SS2-13 001SS2-4 001SS2-14 001SS2-16 001SS2-1 004SS2-16 004SS2-8 004SS2-4 004SS2-14 005SS3-6 005SS3-8 005SS3-10 005SS3-11 005SS3-12 005SS3-13 005SS3-14 005SS3-05 005SS3-7 005SS3-9 005SS3-4 005SS3-2 005SS3-1 005SS3-3 Sample Description N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Collected 08/17/2007 10:30 08/22/2007 10:00 08/21/2007 15:45 08/17/2007 09:15 08/10/2007 15:30 08/14/2007 13:35 08/15/2007 09:00 08/10/2007 14:30 09/04/2007 13:50 09/04/2007 11:20 09/04/2007 09:30 08/30/2007 15:00 09/18/2007 09:30 09/18/2007 10:00 09/18/2007 10:20 09/18/2007 10:40 09/18/2007 11:00 09/18/2007 11:20 09/18/2007 11:40 09/18/2007 16:00 09/07/2007 11:00 09/07/2007 11:20 09/07/2007 11:40 09/07/2007 12:00 09/07/2007 12:40 09/07/2007 13:00 Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures.

Please direct any questions to your Project Manager, Erin Stanley.Reviewed by GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 200159013 005SS3-6 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 18, 2007 October 08, 2007 January 21, 2008 2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte Sr-90 Alpha Spec Pu-238 Pu-239/240 Amn-241 Cm-242 Cm-243/244 01/10/08 01/11/08 01/11/08 01/10/08 01/10/08 01/10/08 U -4.93E-02 U U U U 4.21 E-02 5.521E-02 5.61 E-03 1.04E-01 1.29E-03 1.67E-01 7.89E-02 7.65E-02 7.32E-02 1.44E-01 7.03E-02 MDA 2.97E-01 1.53E-01 8.28E-02 2.11 E-O1 1.56E-01 2.13E-01 RL 2.00E+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MIDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 200159014 005SS3-8 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 18, 2007 October 08, 2007 January 21,2008 2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte Sr-90 Alpha Spec Pu-238 Pu-239/240 Am-241 Cm-242 Cm-243/244 0 1/16/08 01/09/08 01/09/08 01/10/08 01/10/08 01/10/08 U -5.29E-01 U U U U U-3.40E-02 2.30E-02-4.89E-02 4-87E-02-4.35E-02 2.76E-01 9.85E-02 6.I1OE-02 6.3513-02 9.54E-02 6.8 8E-02 MDA 6.36E-01 2.87E-01 1.45E-01 1.83E-01 1.46E-01 2.24E-01 Rb 2.OOE+/-00 I .O0E+00 I .OOE+/-00 I .OOE+00 I .00E+i00 Units pCi/g pCi/g pCi/g pCi/g pCi!g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MIDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www-gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample 1D: Matrix: Geometry Received: 200159015 005SS3-10 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 18, 2007 October 08, 2007 January 21, 2008 2 Sigma Run Date Qualifier Activity Uncertainty Analyte Sr-90 Alpha Spec Pu-238 Pu-239/240 Am-241 Cm-242 Cm-243/244 01/10/08 01/09/08 01/09/08 01/10/08 01/10/08 01/10/08 U 1.38E-01 U U U U U-1.35E-02 3.93E-02-3.62E-02-I -28E-02 2.52E-02 1.59E-01 6.99E-02 8.87E-02 6.61 E-02 1.08E-01 6.68E-02 MDA 2.67E-0 I 2.28E-01 1.87E-01 1 .57E-01 2.56E-01I 1.59E-01 RIL 2.OOE+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 Units pci/g pCi/g pci/g pCi/g pci/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www-gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 200159016 005SS3-11 Soil Client: Enercon Services, Inc.Collect Date: September 18, 2007 Receive Date: October 08, 2007 Report Date: January 21, 2008 2 Sigma Activity Uncertainty Analyte Run Date Qualifier Sr-90 Alpha Spec Pu-238 Pu-239/240 Am-241 Cm-242 Cm-243/244 01/10/08 01/09/08 01/09/08 01/10/08 01/10/08 01/10/08 U U U U U U 1.39E-01-5.06E-02 2.46E-02 3.93 E-02 1.09E-01-4.07E-02 1.67E-01 7.72E-02 9.12E-02 7.11 E-02 1.51E-01 3.56E-02 MADA 2.81E-01 2.76E-01 2.16E-01 1.01E-01 1.64E-01 2.38E-01 RL 2.OOE+00 1 .00E+00 1.00E+00 I .OOE+00 I .00E+00 Units pCi/g pCi/g pCi/g pCi/g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MIDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 200159017 005SS3-12 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 18, 2007 October 08, 2007 January 21, 2008 2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte Sr-90 Alpha Spec Pu-238 Pu-239/240 Am-24I Cm-242 Cm-243/244 01/I 1/08 01/09/08 01/09/08 01/10/08 01/10/08 01/10/08 U -1.74E-01 U U U U U-3.76E-03-7.49E-02-2.86E-02 5.19E-02 0.OOE+00 5.48E-01 1. 19E-O1 4.64E-02 6.25E-02 1.02E-01 6.32E-02 MDA 1.05E+00 2.96E-01 2.7 1E-01 9.57E-02 1.56E-01 9.68E-02 RL 2.OOE i-00 1.00E+00 1.00E+00 1.00E+00 1.OOE+00 1.OOE+00 Units.."........pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL,.MDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 200159018 005SS3-13 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 18, 2007 October 08, 2007 January 21, 2008 2 2 Sigma Run Date Qualifier Activity Uncertainty Analvte...........

n ......Sr-90 Alpha Spec Pu-238 Pu-239/240 Am-241 Cm-242 Cm-243/244 01/11/08 01/09/08 01/09/08 01/10/08 01/10/08 01/10/08 U -1.36E-02 U U U U U-1.36E-0 I 1.35E-01-3.65E-03 3.93E-02-7.70E-03 31.93E-01 1.08E-0OI 1.72E-01 2.66E-02 1 .04E-01 6.47E-02 NI DA 7.62E-01 4.12E-01 2.81 E-01 1.52E-01 2.48E-01 1.54E-01 Rb 2.00E+00 1.00E+00 1.00E+00 1.001E+00 1.00E+00 1.00E+00 Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

.GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel-com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 200159019 005SS3-14 Soil Client: Enercon Services, Inc.Collect Date: September 18, 2007 Receive Date: October 08, 2007 Report Date: January 21, 2008 2 Sigma Run Date Qualifier Activity Uncertainty MDA Anal'te RL Sr-90 Alpha Spec Pu-238 Pu-239/240 Am-241 Cm-242 Cm-243/244 01/11/08 01/09/08 01/09/08 01/10/08 01/10/08 01/10/08 U -1.04E-01 U U U U U 2.67E-02-3.05E-02-1.23E-02-1.12E-02 2.90E-02 4.40E-01 1.17E-01 6.90E-02 2.29E-02 9.41 E-02 5.68E-02 8.62E-01 2.67E-01 2.09E-01 1.59E-01 2.24E-01 8.70E-02 2.00E+00 1.00E+00 1.00E400 1.00E+00 1.00E+00 1.00E+00 Units*pCi/g pCi/g pCi/g pCi/g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www-gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample I): Client Sample ID: Matrix: Geometry Received: 200159020 005SS3-05 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 18,2007 October 08,2007 January 21,2008 2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte Sr-90 Alpha Spec Pu-238 Pu-239/240 Am-241 Cm-242 Cm-243/244 01/11/08 01/09/08 01/09/08 01/10/08 01/10/08 01/10/08 U -4.01E-0I U U U U U-1.39E-02-2.36E-02-3.45E-03 5.333E-02 0.OOE+00 4.53E-01 1.10E-01 8.07E-02 2.81 E-02 1.04E-01 6.48E-02 MDA 9.28E-01 3.02E-01 2.69E-01 1.57E-01 1.60E-01I 9.92E-02 RL 2.OOE+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MIDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www-gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 200159021 005SS3-7 Soil Client: Collect Date: Receive Date:: Report Date: Enercon Services, Inc.September 07, 2007 October 08, 2007 January 21, 2008 2 2 Sigma Run Date Qualifier Activity Uncertainty A nalyte Sr-90 Alpha Spec Pu-238 Pu-239/240 Am-241 Cm-242 Cm-243/244 01/11/08 01/10/08 01/10/08 01/11/08 01/11/08 01/11/08 U -5.30E-02 U U U U U-3.34E-02 5.65E-02-2.75E-02 5.33E-02-3.79E-02 3.02E-01 8.45E-02 6.54E-02 6.11E-02 1.05E-01 3.32E-02 MDA 6.19E-01 2.1OE-01 9.49E-02 9.35E-02 1.60E-01 2.2 1E-01 RL 2.OOE+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 200159022 005SS3-9 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 07, 2007 October 08, 2007 January 21, 2008................................

---- -..... .. .... ...................................

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S2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte Sr-90 Alpha Spec Pu-238 Pu-239/240 Am-241 Cm-242 Cin-243/244 01/11/08 01/10/08 01/10/08 01/11/08 01/11/08 01/11/08 U 7.15E-02 U U U U U-3.93E-02 5.30OE-02-4.24E-02 5.39E-02 8.80E-02 3.97E-01 8.88E-02 7.16E-02 6.52E-02 1.06E-01 1 .09E-01 MDA 7.57E-01 2.15E-01 1.2 1E-01 1.74E-01 1.62E-01 1.53E-01 RL 2.OOEA+00 I .OOE+00 I .OOE+'00 1.OOE+00 I .OOE+00 I .OOEA-00 Units pCi/g pCilg pCi/g pCi/g pCi/g pcilg Note(s): 1. Calculated M1DAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 200159023 005SS3-4 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 07, 2007 October 08, 2007 January 21, 2008 2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte Sr-90 Alpha Spec Pu-238 Pu-239/240 Arn-24 1 Cm-242 Cm-243/244 01/11/08 01/10/08 01/10/08 01/11/08 01/11/08 01/11/08 U LN8E-02 U U U U U 2.30E-02 3.12E-02-1.03E-02 2.84E-02 5.03E-02 3.75E-01 8.92E-02 6.92E-02 3.26E-02 1.13E-01 1.16E-01 MDA 7.22E-01 1.83E-01 1.38E-01 1.77E-01 3.02E-0 I 2.39E-01 RL 1.00E+00 I .OOE+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 Units..U..n.. .....pOi/g pCi/g pCi/g pCi/g pCi/g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www-gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 200159024 005SS3-2 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 07, 2007 October 08, 2007 January 21,2008 2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte Sr-90 Alpha Spec Pu-238 Pu-239/240 Am-241 Cm-242 Cm-243/244 01/11/08 01/10/08 01/10/08 01/11/08 01/11/08 01/11/08 U 2.97E-02 U U U U U-4.4 1E-02 2.56E-02-5.79E-02 4.11 E-02 1.28E-03 3.52E-01 8.15E-02 6.55E-02 6.86E-02 1.09E-01 6.95E-02 MDA 6.78E-01 2.16E-01 1.37E-01 2.08E-01 2.59E-01 2.11 E-OI RL 2.OOE+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 Units pCi/g pCi/g pCi/g pCi/g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www-gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: Client Sample ID: Matrix: Geometry Received: 200159025 005SS3-1 Soil Client: Collect Date: Receive Date: Report Date: Enercon Services, Inc.September 07, 2007 October 08, 2007 January 21, 2008 2 Sigma Run Date Qualifier Activity Uncertainty A nalyte St-90 Alpha Spec Pu-238 Pu-239/240 Am-241 Cm-242 Crn-243/244 01/11/08 01/10/08 01/10/08 01/11/08 01/11/08 01/11/08 U -2.55E-01 U U U U U-6.95E-02 2.01 E-02 4.27E-04-1.39E-02 1.37E-03 2.71E-01 7.14E-02 6.14E-02 8.11 E-02 2.72E-02 7.44E-02 Al DA 6.16E-01 1 .98E-01 1 .28E-01 2.37E-01 2.77E-01 2.25E-01 RL 2.00E+00 1.00E+00 1.00E+00 1.00E+00 1.OOE+00 1.00E+00 Units pCi/g pCi/g pCi/g pCi/g pCi/g pcilg Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -wwwgel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample 11): Client Sample ID: Matrix: Geometry Received: 200159026 005SS3-3 Soil Client: Enercon Services, Inc.Collect Date: September 07, 2007 Receive Date: October 08, 2007 Report Date: January 21, 2008 2 2 Sigma Run Date Qualifier Activity Uncertainty Analyte Sr-90 Alpha Spec Pu-238 Pu-239/240 Am-241 Cm-242 Cm-243/244 01/11/08 01/10/08 01/10/08 01/11/08 01/11/08 01/11/08 U -1.2]E-01 U U U U U 0.O0E+00 1.52E-02-4.92E-02-2.71E-02 1.07E-02 3.56E-01 2.99E-02 2.98E-02 4.98E-02 3.75E-02 1.01E-01 MDA 7.34E-01 4.58E-02 4.56E-02 2.56E-01 3.13E-0 I 2.59E-01 RL 2.00E+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 1.00E+00 Units pCilg pCi/g pCi/g pCi/g pCi/g pCi/g Note(s): 1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis and is decay corrected to the sample collect date.3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analytewas analyzed for, but not detected above the MDL, MDA, or LOD.

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www-gel.com QC Summary Enercon Services, Inc.4499 Old William Penn Highway Murrysville, Pennsylvania Contact: Mr. Dustin G. Miller Workorder:

200159 Revort Date: January 21, 2008 Page 1 of 4 Parmname NOM Sample Oual OC Units RPD%REC% Range Anist Dale Time Rad Alpha Spec Batch 716036 QC120 149 16 IS Arnicrcium-24 I 200159008 DUP Curium-242 Curium-243/244 QC1201491620 LCS Arniricium-24 1 U -2.86E-02+/-7.13E-02

'U 5.31E-02+/-1.41E-01 U -8.86E-03+/- I.74E-02 1.31E+01 Curium-242 Curium-243/244 1.50E+01 QC1201491617 M-B Americium-24 I Curium-242 U -5.45E-03+/-1.97E-02 U 1.01E-01+/-1.61E-01 U 3.02E-02+/-5.91 E-02 1.4]E+01+/-1.28E+00 U 8.42E-02+/-1.05E-01 1.68E+01+/-1 .40E+00 U -2.71E-02+/-5.70E-02 U 0.OOE+00+/-5.77E-02 U -6.98E-03+/-5.87E-02 1.30E+01+/- 1. 19E+00 U 5.41E-02+/-1.06E-01 1.46E+01+/-1 .27E+00 U -1.54E-02+/-7.97E-02 U -3.36E-02+/-7.60E-02 pCi/g pCi/g pCi/g pCilg pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g 136 pCi/g 62 pCi/g 366 N/A MIXA 1 01/10/08 13:46 N/A N/A 108 (75%-125%)

112 (75%-125%)

01/10/08 13:46 01/10/08 13:46 Curium-243/244 QC1201491619 200159008 MS Americium-24 1 Curium-242 Curium-243/244 1.35E+01 U -2.86E-02+/-7.13E-02 U 5.31E-02+/-1.41E-01 1.56E+01 U -8.86E-03+/-1.74E-02 96 (75%-125%)

01/10/08 13:46 94 (75%-125%)

Batch 716037 QC1201491622 200159008 DUP Plutonium-238 Plutonium-239/240 QC1201491624 LCS Plutonium-238 Plutonium-239/240 QC1201491621 MB Plutonium-238 U 2.51E-01+/-2.75E-01 U 1.62E-01+/-2.12E-01 pCi/g 226 pCi/g 305 N/A MiXAI 01/09/08 14:57 N/A U 5.59E-02+/-1.10E-01 1.28E+01 1.27E+01+/-1 .23E+00 pCi/g pcifg (75%-125%)

01/09/08 14:57 99 (75%-125%)

U -5.89E-02 pCi/g+/-7.99E-02 01/09/08 14:57 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

200159 Page 2 of 4 Parmname NOM Sample Qual QC Units. RPD% REC% Range AnIst Date Time Rad Alpha Spec Batch 716037 Plutonium-239/240 QC1201491623 200159008 MS Plutonium-238 Plutonium-239/240 U 2.5]1E-0 I+i/-2.75E-01 1.32E+01 U 1.62E-01+/-2-1 2E-01 Batch 716038 QC1201491626 200159021 DUP Americium-241 Curium-242 Curiun-243/244 QC1201491628 LCS Americium-241 U -2.75E-02+/-6.11 E-02 U 5.33E-02+/-1.05E-0 I U -3.79E-02+/-3.32E-02 1.28E+01 ,rium-242 Curium-243/244 1.47E+01 QC1201491625 M4B Ainericiurn-24 1 U 1.75E-02+/-9.41 E-02 U .-1.38E-02+/-1 .91E-02 1.29E+01+/-1.20E+00 U -2.22E-03+/-3.04E-02 U -2.66E-02+/-3.69E-02 U -7.88E-03+/-1.54E-02 1.23E+01+/-1.20E+00 U 0.OOE+00+/-6.07E-02 1.46E+01+/-1.30E+00 U 4.75E-02+/-8.22E-02 U 2.87E-02+/-7.60E-02 U -8.89E-03+/-1 .74E-02 1.23E+01+/-1.11 E+00 U 0.OOE+00+/-8.71E-02 1.23E+01+/-1.11 E+00 U 5.40E-02+/-6.25E-02 U 4.61E-02+/-6.41E-02 U 1.02E-01+/-1.53E-01 pCi/g 170 pCi/g 599 pCi/g 131 Curium-242 Curiurn-243/244 pci/g pCi/g pci/g pCi/g pCi/g pCi/g pCi/g pcilg pci/g pci/g pci/g PCi/g 96 (75%-125/.o) 98 (75%-125%)

(75%-125%), MXA1 01/09/08 14:57 99 (75%-125%)

N/A TXP2 01/11/08 08:05 N/A N/A 01/11/08 08:05 01/11/08 08:05 QC1201491627 200159021 MS Americium-241 Curiurn-242 Curium-243/244 1.30E+01 U -2.75E-02+/-6.11 E-02 U 5.33E-02+/-I.05E-01 1.50E+01 U -3.79E-02+/-3.32E-02 95 (75%-125%)

01/11/08 08:05 82 (75%-125%)

Batch 716039 QC1201491630 200159021 DUP Plutonium-238 Plutonium-239/240 QC1201491632 LCS Plutonium-238 U -3.34E-02+/-8.45E-02 U 5.65E-02+/-6.54E-02 pCi/g 849 pCi/g 20 N/A TXP2 01/10/08 20:16 N/A pCi/g (75%-125%)

01/14/08 08:02 lutonium-239/240 1 .26E+01I1.4+1 pL/ 8 (5-2%1.24E+01 pCi/g 98 (75%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www-gel.com Workorder:

200159 Parmname NOM Rad Alpha Spec Batch 716039 QC Summary Page 3 of 4 Sample Oual OC Units RPD% REC% Range Anist Date Time+1/-1.20E+00 QC1201491629 MB Plutonium

-238 Plutonium-239/240 QC1201491631 200159021 MS Plutonium-238 Plutonium-239/240 Rad Gas Flow Batch 715660 QC1201490809 200157007 DUP Strontium-90 QC1201490811 LCS-ontium-90 U 7.1OE-03+/-3.15E-02 U 4.29E-02+/-5.97E-02 U 8.63E-02+/-8.59E-02 1.26E+01+/-8-71E-01 pCi/g pCilg pci/g pci/g TXP2 01/10/08 20:16 U -3.34E-02+/-8.45E-02 1.27E4-01 U 5.65E-02+/-6.54E-02 (75%-125%)

01/10/08 20:16 99 (75%-125%)

U 9.59E-03 U 2.36E-01+/-4.06E-01

+/-4.25E-01 pCi/g 0 N/A SLNI 01/08/08 17:55 3.05E+01 QC1201490808 MB Strontium-90 3.38E+01+/-2.09E+/-00 U 4.99E-02+/-/-3 .99E-01I pCilg pCi/g pCi/g Ill (75%-125%)

01/08/08 17:55 01/08/08 17:55 01/08/08 17:55 Qc1201490810 200157007 MS Strontium-90 Batch 715671 QC1201490822 200159008 DUP Strontium-90 QC1201490824 LCS Strontium-90 3.26E+01 U 9.59E-03+/-4.06E-01 3.23E+01+/-2.20E+00 99 (75%-125%)

U 3.15E-01 U 3.39E-01+/-2.58E-01

+/-5.19E-01 pCi/g 8 N/A SLNI 01/11/08 12:23 3.1OE+01 QC1201490821 MB Strondium-90 2.90E+/-01I+/-/-2.06E+00 U -4.48E-02+/-3 .40E-01 pCi/g pCi/g pCi/g 94 (75%-125%)

01/10/08 18:48 01/11/08 12:23 01/11/08 12:23 QC1201490823 200159008 MS Strontium-90 3.17E+01 U 3.15E-01.+/-2.58E-01 3.02E+01+/-1 .88E+00 95 (75%-125%)

Notes: The Qualifiers in this report are defined as follows: Analyle is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensarion product GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary\Vorkordcr:

200159 P_ A, f A Parmname NOM Sample Qual QC Units RPD% REC% Range AnIst Date rime B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated M M if above MDC and less than LLD N/A RPD or %Recovery limits do not apply.ND Analyle concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier R Sample results are rejected U Analyse was analyzed for, but not detected above the MDL, MDA, or LOD.Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +/-RIL. Concentrations are <5X the R-L. Qualifier Not Applicable for Radiochemistry.

h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/- the RL is used to evaluate the DUP result.* Indicates that a Quality Control parameter was not within specifications.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

List of current GEL Certifications as of 21 January 2008 State Certification Alaska UST-062-Arizona AZ0668 Arkansas 88-0651 CLIA 42D0904046 California 0115I1CA Colorado GenEngLabs Connecticut PH-0169 Dept. of Navy NFESC 413 EPA WG-15J Florida/NELAP E87156 Georgia E87156 (FL/NELAP)

Hawaii N/A Idaho N/A Illinois 200029 Indiana C-SC-01 Kansas E-10332 Kentucky 90129 Louisiana 03046 Maryland 270 Massachusetts M-SC012 Michigan 9903 Nevada SC12 New Jersey SC002 New Mexico FL NELAP E87156 New York 11501 North Carolina 233 North Carolina Drinking W 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania 68-00485 South Carolina 10120001/10585001/10120002 Tennessee 02934 Texas NELAP T104704235-07-TX U.S. Dept. of Agriculture S-52597 US Army Corps of Engineer N/A Utah 8037697376 GEL Vermont VT87]56 Virginia 00151 Washington C1641 n ýLaboratories LLC a memter of The GEL Group ;1c PO Box 30712 Charleston.

SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com February 07, 2008 Mr. Dustin G. Miller Enercon Services, Inc.4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Re: Humboldt Bay NPP soils Work Order: 201361

Dear Mr. Miller:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on October 04, 2007 and October 08, 2007. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.'

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction.

If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.Sincerely, Erin Stanley Project Manager Chain of Custody: 008-07, 009-07,010-07, 011-07, 012-07, 013-07,016-07, 018-07, 021-07 and 030-07 Enclosures oroblem solved Laboratories Lc SAMPLE RECEIPT & REVIEW FORM Client: -SDG/ARCOC/Work Order: -Received By: 4)1, -iDate Received:

/0 -0 9 7 S H *lf Counts > x2 area background on samples not marked "radioactive", contact Suspected Hazard Information

Z the Radiation Safety Group of further investigation.

COC/Samples marked as radioactive?

L/ IMaximum Counts Observed*:

Classified Radioactive 11 by RSO? ______COCJSamples marked containing PCBs? -Shipped as a DOT Hazardous?

-Hazard Class Shipped: IU#: Samples identified as Foreign Soil? _._-__Sample Receipt Criteria Z Z Comments/Qualifiers (Required for Non-Conforming Items)Circle Applicable:

seals broken 1 Shipping containers received intact and damaged container knaiLng container other (describe) sealed?Prrsesevaiion Method- c bg 2 Samples requiring cold preservation blue ice dry ice none J'bt rd p -n'-'1 within (4 +/-2 C)? A'Chain of custody documents included with shipment?

LI" Circle Applicable:.

seals broken 4 Sample containers intact and sealed? damaged container hnting container other (describe)

Sample ID's. containers affected and observed pli-Samples requiring chemical preservation at proper pH? If Presemtion added, Lot#:'6 VOA vials free of headspace (defined asSample ID's and cooanes ffccted:< 6mm bubble)?,If yes, immediately deliver to Volatiles labworsoy) 7 Are Encore containers present?Id~s and tests affected.8 Samples received within holding time? /Sample ID's on COC match ID's on ISample ID's and cownainers affected: bottles?10 Date & time on COC match date & time SampleI'salta:

on bottles?1 Number of containers received Catch Sample ID's affece!number indicated on COC?12 COC form is properly signed in relinquished/received sections?Comments: PM (or PMA) review: Initials Date ,

ral Laboratories LLC SAMPLE RECEIPT & REVIEW FORM Client: F-r"7 6rCCe- _Yl- SDG/ARCOC/Work Order: j ] ')62)-Received By: IDate Received: H nr ma* "If Counts > x2 area background on samples not marked "radioactive", contact Suspected HZ the Radiation Safety Group of further investigation.

COC/Samples marked as radioactive?

-Maximum Counts Observed*:

W6O cj;-Classified Radioactive 11 by RSO? -COG/Samples marked containing PCBs? _,," Shipped as a DOT Hazardous?

&7 Hazard Class Shipped: UN#-.Samples identified as Foreign Soil? __Sample Receipt Criteria Comments/Qualtfiers (Required for Non-Conforming Items)oficable seals bmken I Shipping containers received intact and sealed?damaged coutainer leaking container other (describe)

Samples requiring cold preservation within (4+/- 2 C)?pment?Sample containers intact and sealed?Samples requiring chemical preservation at proper pH?VOA vials free of headspace (defined as< 6mm bubble)?I Are Encore containers present?Preservation Method- ice bags blue ice dry ice none other (describe)

Circle Applicable:

seals broken dairaged container leaking container other (descnbe)Sample 1I's, containers affected and observed pH: If Preservation added, Lot#: Sample ID's and containers affected: (i!f yes, imarr iaely deliver to Votatilms Ilbonafor)

Id's and tests affecaed Sample 1D9s and containers affected: Sample ID's affected-Sample ID's affected: ISamples received within holding time?9 Sample ID's on COC match ID's on bottles?10 Date & time on COC match date & time on bottles? I I 11 Ntumber of containers received match number indicated on COC?V 12COC form is properly signed in 1 2 relinquished/received sections?

V Comments:*'D. C- ?,., =_ .III-Ur ) I- LT 'L J l 5I.V~ r~ r~q 0%14LCt PM (or PMA) review: Initials "D____]___*

Date zOq/b-7 Page: or f General Engineering Laboratories, LLC Project 0: j2 & " oS- GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote #: Charleston, SC 29407 COC Number .. 0,3 -GEL Work Order Number: 5'7 Phone: (843) 556-8 171 PO Number: Fax: (843) 766-1178 Client Name: rn S-erv'lC.s Ln.c, Phone #: ?3-6 Sample Analysis Requested (5) (Fill in the number of containers for each test)Project/Site Name: 4 m olA1 R- N Fax :/(72(4) 9233- ql1l3c Should this --Prcaervotivc Type (6)"sampte be 's -Address: 1000 ~nl Sa 'Mo 4 lln re aCA 5 0 o~drd C S lts T Comments Collected by: ii --, -W Send Results To: , Note: extra sample is old Time E required for sample'Date Collected Collected QC Code Field Sample C C Sample ID (Military)

", terd tr Mu " -tFi V .specific QC For composites

-Indicate start and stop date/lime (mn -dd.yy) ( t " f/tPIl'- oo5553-(¢ 0Q4507 0930 N--1 J'005553-S t 000 c Nilq I oo! 3- 11 oqel(S ofo NIA _ so i 0o5SS3- 2 0q o 1+/-S1 (I A D so_ I o20,5 -153 3 OQ o7 i Lo I 1 A. 5o S X 00,5SS3-0,5 09i/ 97 I ('W 7 Al __S__0 A 1A '1 -14 'Z __ _TAT Requested:

Normal: Rush: Specifiy: (Subject to Surcharge)

Fax Results: Yes / No Circle Deliverable:

C ofa / QC Summary / Level I/ Level 2 / Level 3 / Level 4 Remarks, A~e there any known hazards applicable to these samples? Ifso, please list the hazards Samle Colction Time Zone Central Other Mountain -" Chain of Custody Signatures Sample Shipping _ndDelivery Details Relinquished By (Signed) Dale Time Received by (signed) Date Time C.'ý' Q LPGEL PM: 2 M dz ftnu Oý2 ý(0"7 / V19C) 2 !y /ý/'"Lo-?

q lAirbi,#: -Z ý FtO F'N- 03 q 0 0 o ,S30a 3 3 1_ __Airbill 0: 1.) Chain or Custody Number -Client Determined 2.) QC Codes: N -Normal Sample. TR =Trip Blank. FD -Field Duplicate, EH -Equipment Blank, MS =Matrix Spike Sample, MSD -Matrix Spike Duplicate Sample. G -Grab. C -Composile 3.) Field Filtered:

For liquid manlaces, indicate with a -Y -for yes the sample was field filtered or -N -for sample was not Field filtered, 4.) Matrix Codes: DW-Drinklng Water, GW-Groundwater.

SW-Surface Water. WW-Wste Water, W-Water, SO-Soil. SD-SedimenL SL-Sludge.

SS-Solid Waste, O-Oil, F-Filter.

P-Wipe, U-Urine. F-Fccal, N-Nasal 5.) Sample Analysis Requested:

Analytical method requested (i.e. 8260B. 6010Bnf470A) and number of containers provided for each (I.e. 82608 -3, 60108/7470.4

-I ).6.1 Preservative Type: HA -Htydrochloric Acid. NI -Nitric Acid. Sit -Sodium Hydroxide.

SA -Sulfuric Acid, AA -Ascorbic Acid, HX -Hexane, ST -Sodium Thlosulfrae, If no preservative is added -leave field blank WHITE = LABORATORY YELLOW = FILE PINK = CLIENT For Lab Receiving LWe Only Custody Seal Intact?YES NO Cooler Temp: C Page: ofGeneral Engineering Laboratories, LLC Projcct!:

5 0 GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote H: Charleston, SC 29407 COC Number .GEL Work Order Number: POFax: (843) 766-1178 Client Name: 0nox.Cc( C, -Phone#: 1 (r7,2q)7,_:

3 3 1 Sample Analysis Requestedis5 (Fill in the number ofcontainers for each test)En~ efcr sI I _n Project/Site Name: J\ L o P P Fax H: 13<--Should this Preservative Type (6)sample be "-- -Address: /ccQ I-tr?/.C.J S~Armovi i- 0 q5 c 3 considered:

Adres -OoxrqýOW y yvc 4re Comments Collected by \K; ti t,..rro...NG S e ,,, T Sen Resultsnts Collecte C.y ,, VSe Result T o:-y Note: extra sample is.Time required for sample'Dote Collected C-(pllected QC Code Field Sample W -specific QC (military) rl1d1) ori ~ t, i For composites

-indicate start and stop date/time dd-Y) (hhmm) P KE~ CY7',5SS3

-r7 ogl-0909 t lo tL NIA S0 I I X___I_OC- 5S S3_ q oq-oq-M1j laNo tZ A 0 IX 1 Wo550,3- 4 I1`10 N So I1 (YD5Ss3- (4 c9oi-o-o ii~o tL __o _005 -;,-3 Oi -o7-ý IAOCo ji So I X I 0(3_65S33 oq-oo'~0 Iý4O 'SO X oo5ss3- 3 o-07-0I 50oo \V _S 7 TAT Requested:

Normal: Rush: Specify: (Subect to Fax Results: Yes / No Circle Deliverable:

C ofA / QC Summary I Level I / Level 2 / Level 3 L level 4 Remarks: Are there any known hazards applicable to these samples? £so, please list the hazards SampleColletionlime Zone Eastern v.CiT,>Central _____Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Received b 'sned) Date Time GEL PM: ,% w 09017 /300o 111e Rltqo0 7 130D Method orSSfhott

meti DateShip d: 0ý 0ý 0 3p 0" g97 olkkQ 31/ Airbill#:

12 (16 F2L 03 9Q0Y15 93( 3 a _ Airhjill HI: I.) Chain of Custody Number -Client Determined 2.) QC Codes: N -Normal Sample, TB = Trip Blank.,FD

-Field Duplicate, ED -Equipment Blank, MS = Matrix Spike Sample, MSD -Moirix Spike Duplicate Sample. G = Grab. C = Composite 3.) Field Filetered:

For liquid matrlces, indicate vith a -a -for yes the sample was field filtered or -N -for sample was not field tiltered.4.1 Matrix Codes: DW-Drinking Water. GW-Groundwater, SW-Surface Water, WW-Waste Water, W-Water, SO-Soil, SD=Sediment, SL-Sludge, SS=Solid Waste, O-Oil, F=Filter, P.Wipe, U-Urine, F-Fecal, N"Noasa 5.1 Sample Analysis Requested:

Analytical method requested (i.e. 82608, 601i0B7470A) and number of container3 provided for each (i.e. 8260B .3. 60105/7470A

.I).6.) Preservative Type: HA -Hydrochloric Acid. NI -Nitric Acid, SH -Sodium llydroxlde, SA -Sulfuric Acid. AA = Aacorblc Acid, fIX -llexane. ST -Sodium Thinosulfate, fi no preservativc is added = leave field blank WHITE -LABORATORY YELLOW = FILE PINK = CLIENT For Lab Receiving Use Only Custody Seal Intact?YES NO Cooler Temp: C a lLaboratories LLC SAMPLE RECEIPT & REVIEW FORM Client: -AIr SDG/ARCOC/Work Order: i1q65: Received By: IDate Received:

(S ee a dn *If Counts > x2 area background on sarirpes not marked 'radioactive", contact.Suspected Hazard Information Z the Radiation Safety Group of further investigation.

COC/Samples marked as radioactive?

Maximum Counts Observed*:

T-0 Classified Radioactive 11 by RSO? __ _COC/Samples marked containing PCBs? ___Shipped as a DOT Hazardous?

Hazard Class Shipped: UN#-Samples identified as Foreign Soil?n A Sample Receipt Criteria Z Comments/Qualifiers (Required for Non-Conforming Items)Circle Applicable:

seals broken Shipping containers received intac and damaged container le2king container other (describe) sealed?Preservation Method: ice bags Samples requiring cold preservationn blue ice dry ice n : other (describe) w ithin (4 +/- 2 C)?3 tChain of custody documents included w ith shipment?Circle Applicable:

seals broken 4 Sample containers intact and sealed?? damaged container leaking container other (describe)

Sample ID's, containers affected and observed pH: Samples requiring chemical preservation at proper pH? If Preservation added, Lot#: Sapl IDsadcnanr fetd VGA vials free of headspace (defined as Sample ID's and containers affected:< 6mam bubble)?(If yes, immuediately deliver to Votatiles labonatory) 7 Are Encore containers present?1 Id's and tests affected: 8 Samples received within holding time?Sample Dl)'s on COC match ID's on 1 Sample ID's and containers affected: 9bottles?

I SmDale & time on COC match date & time Sample ID's affected: on bottles?Sample tD's affected: Number of containers received match Sample lDs affected: n number indicated on COC?12 COC form is properly signed in relinquished/received sections?Comments: Uj -25 o3W PM (or PMA) review: Initials W Date /01 %1 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report for ENRC002 Enercon Services, Inc.Client SDG: 201361 GEL Work Order: 201361 The Qualifiers in this report are defined as follows:* A quality control analyte recovery is outside of specified acceptance criteria** Analyte is a surrogate compound H Analytical holding time was exceeded U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.The designation ND, if present, appears in the result column when the analyte concentration is not detected above the detection limit.This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures.

Please direct any questions to your Project Manager, Erin Stanley.Reviewed by GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company Enercon Services, Inc.Address 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: 005SS3-6 Proiect: ENRC00200 Sample ID: 201361025 Client ID: ENRC002 Matrix: Soil Collect Date: 18-SEP-07 09:30 Receive Date: 08-OCT-07 Collector:

Client Parameter Qualifier Result Uncertaint, DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid.Tritium U -6.71E-01

+/-2.96E+00 5.33E+00 6.OOE+00 pCi/g RXEI 02/01/08 1246 720775 1 The following Analytical Methods were performed Method Description Analyst Comments EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Enercon Services, Inc.Address 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Contact: Mr. Dustin G. Miller Report Date: February 7, 2008 Project: Humboldt Bay NPP soils Client Sample ID: 005SS3-8 Project: ENRC00200 Sample ID: 201361026 Client ID: ENRC002 Matrix: Soil Collect Date: 18-SEP-07 10:00 Receive Date: 08-OCT-07 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U -4.69E-01

+/-2.98E+00 5.35E+00 6.00E+00 pCi/g RXEI 02/01/08 1318 720775 1 The following Analytical Methods were performed Method Description Analyst Comments I EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Enercon Services, Inc.Address 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: Sample l1D: Matrix: Collect Date: Receive Date: Collector:

005SS3-10 201361027 Soil 18-SEP-07 10:20 08-OCT-07 Client Project: ENRC00200 Client ID: ENRC002 Units DF AnalystDate Time Batch Method Parameter Qualifier Result Uncertainty DL RL Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U 4.05E-01 +/-3.OOE+00 5.29E+00 6.OOE+00 pCi/g RXE1 02/01/08 1350 720775 1 The following Analytical Methods were performed Method Description Analyst Comments I EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Enercon Services, Inc.Address: 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

005SS3-11 201361028 Soil 18-SEP-07 10:40 08-OCT-07 Client Project: ENRC00200 Client ID:. ENRC002 Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U 0.003E+00

+/-2,93E+00 5.19E+00 6.OOE+00 pCi/g RXEI 02/01/08 1422 720775 I The following Analytical Methods were performed Method Description Analyst Comments EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Enercon Services, Inc.Address 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: 005SS3-12 Project: ENRC00200 Sample ID: 201361029 Client ID: ENRC002 Matrix: Soil Collect Date: 18-SEP-07 11:00 Receive Date: 08-OCT-07 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U 2.56E+00 +/-3.18E+00 5.37E+00 6.00E+00 pCi/g RXEI 02/01/08 1453 720775 1 The following Analytical Methods were performed Method Description Analyst Comments I EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Enercon Services, Inc.Address 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

005SS3-13 201361030 Soil 18-SEP-07 11:20 08-OCT-07 Client Project: ENRC00200 Client ID: ENRC002 Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U 1.86E+00 +/-3.IOE+00 5.30E+00 6.OOE+00 pCilg RXEI 02/01/08 1525 720775 1 The following Analytical Methods were performed Method Description Analyst Comments I EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Enercon Services, Inc.Address 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: 005SS3-14 Project: ENRC00200 Sample ID: 201361031 Client ID: ENRC002 Matrix: Soil Collect Date: 18-SEP-07 11:40 Receive Date: 08-OCT-07 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U 2.00E+00 +/-3.06E+00 5.22E+00 6.OOE+00 pCi/g RXEI 02/01/08 1557 720775 1 The following Analytical Methods were performed Method Description Analyst Comments I EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Enercon Services, Inc.Address 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: 005SS3-05 Project: ENRC00200 Sample ID: 201361032 Client ID: ENRC002 Matrix: Soil Collect Date: 18-SEP-07 16:00 Receive Date: 08-OCT-07 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U 4.03E-01 +/-2.98E+00 5.25E+00 6.00E+00 pCi/g RXEI 02/01/08 1629 720775 1 The following Analytical Methods were performed Method Description Analyst Comments I EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Enercon Services, Inc.Address: 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

005SS3-7 201361033 Soil 07-SEP-07 11:00 08-OCT-07 Client Project: ENRC00200 Client ID: ENRC002 Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U 1.14E-0I +/-2-93E+00 5.20E+00 6.00E+00 pCi/g RXEI 02/01/08 1701 720775 l The following Analytical Methods were performed Method Description Analyst Comments EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company Enercon Services, Inc.Address 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: 005SS3-9 Proiect: ENRCO0200 Sample ID: 201361034 Client ID: ENRC002 Matrix: Soil Collect Date: 07-SEP-07 11:20 Receive Date: 08-OCT-07 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U -5.77E-01

+/-2.93E-00 5.27E+00 6.OOE+00 pCi/g RXEI 02/01/08 1733 720775 1 The following Analytical Methods were performed Method Description Analyst Comments I EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Enercon Services, Inc.Address 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Cl Sa M Co Re Co ient Sample ID: 005SS3-4 mple ID: 201361035 atrix: Soil Illect Date: 07-SEP-07 11:40 eceive Date: 08-OCT-07)llector:

Client Qualifier Result Uncertainty DL Project: ENRC00200 Client ID: ENRC002 Parameter RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U-2.02E+00

+/-2.84Et00 5.26Ei-00 6.OOE+00 pCi/g RXEI 02/01/08 1805 720775 1 The following Analytical Methods were performed Method Description Analyst Comments EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Enercon Services, Inc.Address : 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: 005SS3-2 Proiect: ENRC00200 Sample ID: 201361036 Client ID: ENRC002 Matrix: Soil Collect Date: 07-SEP-07 12:00 Receive Date: 08-OCT-07 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U 4.91E-01 +/-3.OOE+00 5.28E+00 6.00E+00 pCi/g RXEI 02/01/08 1837 720775 1 The following Analytical Methods were performed Method Description Analyst Comments I EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Enercon Services, Inc.Address : 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: 005SS3-1 Project: ENRC00200 Sample ID: 201361037 Client ID: ENRC002 Matrix: Soil Collect Date: 07-SEP-07 12:40 Receive Date: 08-OCT-07 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U 2.12E+00 +/-/-3.07E+0-0 5.22E+00 6.OOE+00 pCi/g RXEI 02/01/08 1909 720775. A The following Analytical Methods were performed Method Description Analyst Comments EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com-Certificate of Analysis Company : Enercon Services, Inc.Address 4499 Old William Penn Highway Murrysville, Pennsylvania 15668 Report Date: February 7, 2008 Contact: Mr. Dustin G. Miller Project: Humboldt Bay NPP soils Client Sample ID: 005SS3-3 Proiect: ENRC00200 Sample ID: 201361038 Client ID: ENRC002 Matrix: Soil Collect Date: 07-SEP-07 13:00 Receive Date: 08-OCT-07 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Tritium U 1.92E1-00

+/-3-07E+00 5.24E+00 6.OOE+00 pCAlg RXEI 02/01/08 1940 720775 The following Analytical Methods were performed Method Description Analyst Comments EPA 906.0 Modified GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Enercon Services, Inc.4499 Old William Penn Highway Murrysville, Pennsylvania Contact: Mr. Dustin G. Miller Report Date: February 7, 2008 Page I of 2 Workorder:

201361 Parmnamc NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Liquid Scintillation Batch 720770 QC1201502016 201361001 DUP Tritiuum U -1.92E+/-00+/-2.2 1 E+/-00 U ,-4.48E-0I

+/-2.40E+00 pCi/g 0 N/A RXEI 02/07/08 02:04 QC1201502018 LCS Tritium QC1201502015 MB Tritium 2.05E+01 1.99E+01+/-/-5.1 3E+00 U -1.00E+00+/-2.18E+00 pCi/g pCi/g pCi/g 97 (75%-125%)

02/07/08 02:44 02/07/08 01:41 02/07/08 02:26 QC1201502017 201361001 MS Tritium Batch. 720775 QC1201502045 201361021 DUP QC1201502047 LCS Tritium 2.16E+0I U -1.92E+00+/-2.21 E+00 2.46E+01I/-5.-S76E+00 114 (75%-125%)

U 69E-01 U 1.66E+00+/-2.90E+00

+/-2.95E+00 pCi/g 0 N/A RXEI 02/01/08 20:44 4.06E+01 3.84E+01+/-6.69E+00 QC1201502044 MB Tritium U -4.30E-01+/-2.74E+00 pCi/g pCi/g pCi/g 95 (75%-125%)

01/27/08 02:47 02/01/08 20:12 01/27/08 02:31 QC1201502046 201361021 MS Tritium 4.20E+0lI U -3.69E-01+/-2.90E+l00 4.69E+01+/-7.29E+00 112 (75%-125%)

Notes: The Qualifiers in this report are defined as follows: Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyse was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyle has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated M M if above MDC and less than LLD N/A RPD or %Recovery limits do not apply.

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www-gel.com QC Summary Workorder:

201361 Page 2 of 2 Parmname NOM Sample Qual QC Units RPD% REC% Range AnIst Date Time ND Analyse concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier R Sample results arc rejected U Analyle was analyzed for, but not detected above the MDL, MDA, or LOD.U] Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.

h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.^The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria When the sample is greater than five times (5X) the contract required detection limit (R-L). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/- the RL is used to evaluate the DUP result.* Indicates that a Quality Control parameter was not within specifications.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

List of current GEL Certifications as of 07 February 2008 State Certification Alaska UST-062 Arizona AZ0668 Arkansas 88-0651 CLIA 42D0904046 California 0115] CA Colorado GenEngLabs Connecticut PH-0169 Dept. of Navy NFESC 413 EPA WG-15J Florida/NELAP E87156 Georgia E87156 (FL/NELAP)

Hawaii N/A Idaho N/A Illinois 200029 Indiana C-SC-01 Kansas E-10332 Kentucky 90129 Louisiana 03046 Maryland 270 Massachusetts M-SCO12 Michigan 9903 Nevada SC12 New Jersey SCO02 New Mexico FL NELAP E87156 New York 11501 North Carolina 233 North Carolina Drinking W 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania 68-00485 South Carolina 10120001/10585001/10120002 Tennessee 02934 Texas NELAP T104704235-07-TX U.S. Dept. of Agriculture S-52597 US Army Corps of Engineer N/A Utah 8037697376 GEL Vermont VT87156 Virginia 00151 Washington C1641 ATTACHMENT 3 A Drawing Of The Sample Locations And Laboratory Analysis Results C M1,ý2, T R C 55 2nd Street Suite 575 San Francisco, CA 94105 , .5.644!.3000 0 -HAE"!.5.541,9378 Ra wiF C~o u-Joll sco ill August 27, 2008 Project No. 161072 C-oo7 Mr. David Sokolsky Pacific Gas and Electric Company lOOO King Salmon Avenue Eureka, CA 95503 Radiological Sampling Data and Demolition/Remediation Schedule Humboldt Bay Repowering Project PG&E Humboldt Bay Power Plant 1oo0 King Salmon Avenue, Eureka, CA g55o3

Dear Mr. Sokolsky:

As discussed during our telephone conference call on August 25, 20o8, please find attached the following items: " Remedial Investigation (RI) Report Table 1, Cesium-137 Radiological Sampling Data* RI Report Table 2, Isotopes Other than Cesium-137

• RI Report Figures 1-5,* July 14-17, 2008 Radiological Field Screening Results* Demolition and Remediation Schedule; and* GEL Laboratory Data sheets.As both TRC and Enercon indicated, this site has been thoroughly investigated and there.are no radiological issues of concern as they relate to the demolition/remediation project scheduled for September 29, 2008 through October 31, 2oo8. Enercon is our team's NRC expert and feel free to contact Keith Mahosky with any detailed questions in that regard.

David Sokolsky August 27, 2008 Page 2 Please contact Deems Padgett at (415) 644-3001 or Alan Lui at (415) 644-3004 with any other questions.

Sincerely, Deems C. Padgett, P Project Director A ft.'e Alan Lui, PE Principal Engineer cc: John Albers, PG&E Joseph Sutton, PG&E Keith Mahosky, Enercon Encl VTRC TABLES Table 1 Radiological Soil Sampling Data (Cesium-137)

Humboldt Bay Repowering Project Eureka, California 1'.,,.c: Sample Number Sample Type Collection Date E .-~ Q)(pCi/g) (pCi/g)B-1-0.5 Gamma SAMPLE 07/15/08 0.200 0.0772 B-1-4.5 Gamma SAMPLE 07/15/08 U -0.00513 0.0374 B-2-1.0 Gamma SAMPLE 07/15/08 U 0.0259 0.0261 B-2-1.0 Gamma DUP 07/15/08 U -0.000777 0.0214 B-2-4.0 Gamma SAMPLE 07/15/08 U 0.0185 0.0244 B-2-7.0 Gamma SAMPLE 07/15/08 U 0.0123 0.0333 B-3-1.0 Gamma SAMPLE 07/15/08 U -0.00295 0.0308 B-3-4.0 Gamma SAMPLE 07/15/08 U -0.0102 0.0283 B-4-1.0 Gamma SAMPLE 07/16/08 U -0.00459 0.0529 B-4-4.0 Gamma SAMPLE 07/16/08 U 0.0104 0.036 B-5-0.5 Gamma SAMPLE 07/15/08 U 0.0126 0.0177 B-5-4.5 Gamma SAMPLE 07/15/08 U 0.0196 0.0432 B-6-1.0 Gamma SAMPLE 07/15/08 U -0.00926 0.0266 B-6-4.0 Gamma SAMPLE 07/15/08 U -0.0163 0.0414 B-6-7.0 Gamma SAMPLE 07/15/08 U -0.00589 0.0511 B-7-0.5 Gamma SAMPLE 07/15/08 U -0.00961 0.0205 B-7-4.5 Gamma SAMPLE 07/15/08 U 0.00887 0.0394 B-7-7.5 Gamma SAMPLE 07/15/08 U -0.00175 0.0443 B-8-0.5 Gamma SAMPLE 07/16/08 0.116 0.0461 B-8-4.5 Gamma SAMPLE 07/16/08 0.175 0.0753 B-9-0.5 Gamma SAMPLE 07/15/08 U -0.000848 0.0219 B-9-4.5 Gamma SAMPLE 07/15/08 U 0.0226 0.0248 B-9-7.5 Gamma SAMPLE 07/15/08 U -0.0176 0.038 B-10-0.5 Gamma SAMPLE 07/16/08 U 0.0104 0.0234 B-10-4.5 Gamma SAMPLE 07/16/08 U -0.0147 0.0371 B-1l1-1.0 Gamma SAMPLE 07/15/08 U -0.00164 0.0178 B-1 1-4.0 Gamma SAMPLE 07/15/08 U -0.00639 0.0345 Page 1 of 5 Table 1 Radiological Soil Sampling Data (Cesium-1 37)Humboldt Bay Repowering Project Eureka, California CqC Sample Number Sample Type Collection Date E (I) c)U) D (pCi/g) (pCi/g)B-1-0.5 Gamma SAMPLE 07/15/08 0.200 0.0772 B-1 1-7.0 Gamma SAMPLE 071i5108 U 0.049 0.0631.B-I2-i.0 Gamma SAMPLE 0716/08 0.096 0.0609 B-12-4.0 Gamma SAMPLE 07/16/08 U 0.0108 0.0347 B-13-0.5 Gamma SAMPLE 07/14/08 U 0.0187 0.0372 B-1 3-4.5 Gamma SAMPLE 07/14/08 U -0.0174 0.0254 B-13-4.5 Gamma DUP 07/14/08 U -0.016i 0.0199 B-13-7.5 Gamma SAMPLE 07/14/08 U -0.0171 0.0292 B-14-0.5 Gamma SAMPLE 07/14/08 U -0.0164 0.0236 B-14-4.5 Gamma SAMPLE 07/14/08 U -0.00831 0.0166 B-14-7.5 Gamma SAMPLE 07/14/08 U -0.0264 0.0233 B-145-i.0 Gamma SAMPLE 07/14/08 U 0.0244 0.0326 B-15-4.0 Gamma SAMPLE 07/14/08 U 0.0128 0.0271 B-16-1.0 Gamma SAMPLE 07/14/08 U 0.0238 0.0306 B-16-1.0 Gamma DUP 07/14/08 0.075 0.0362 B-16-4.0 Gamma SAMPLE 07/14/08 U 0.0208 0.031 B-16-7.0 Gamma SAMPLE 07/14/08 U 0.00401 0.0213 B-17-0.5 Gamma SAMPLE 07/14/08 U 0:0169 0.0294 B-17-4.5 Gamma SAMPLE 07/14/08 U -0.0105 0.0333 B-17-7.5 Gamma SAMPLE 07/14/08 U 0.0274 0.0265 B-18-0.5 Gamma SAMPLE 07/16/08 U 0.0123 0.0203 B-18-4.5 Gamma SAMPLE 07/16/08 U -0.0132 0.0313 B-19-0.5 Gamma SAMPLE 07/16/08 'U -0.0171 0.0337 B-1 9-4.5 Gamma SAMPLE 07/16/08 U -0.0108 0.0327 B-20-0.5 Gamma SAMPLE 07/14/08 U 0.0207 0.0291 B-20-4.5 Gamma SAMPLE 07/14/08 U -0.0114 0.0296 B-20-7.5 Gamma SAMPLE 07/14/08 U -0.00987 0.0243 Page 2 of 5 Table 1 Radiological Soil Sampling Data (Cesium-1 37)Humboldt Bay Repowering Project Eureka, California Sample Number Sample Type Collection Date E 0 :D o__(pCi/g) (pCi/g)B-1-0.5 Gamma SAMPLE 07/15/08 0.200 0.0772 B-21-1.0 Gamma SAMPLE 07/17/08 U 0.0102 0.0583 B-21-4.0 Gamma SAMPLE 07/17/08 U -0.00859 0.0569 B-22-1.0 Gamma SAMPLE 07/17/08 U 0.0421 0.0333 B-22-4.0 Gamma SAMPLE 07/17/08 U 0.00994 0.0555 B-23-1.0 Gamma SAMPLE 07/17/08 U 0.00923 0.0371 B-23-4.0 Gamma SAMPLE 07/17/08 U -0.0454 0.0553 B-24-0.5 Gamma SAMPLE 07/17/08 0.090 0.047 B-24-4.5 Gamma SAMPLE 07/17/08 1.230 0.146 B-24-4.5 Gamma SAMPLE 07/17/08 1.230 0.206 B-24-4.5 Gamma DUP 07/17/08 1.200 0.147 B-25-1.0 Gamma SAMPLE 07/17/08 U -0.00189 0.0375 B-25-4.0 Gamma SAMPLE 07/17/08 U -0.0141 0.01 77 B-26-1.0 Gamma SAMPLE 07/16/08 0.109 0.0494 B-26-4.0 Gamma SAMPLE 07/16/08 U -0.00252 0.0228 B-27-1.0 Gamma SAMPLE 07/17/08 0.152 0,0732 B-27-4.0 Gamma SAMPLE 07/17/08 U 0.00957 0.054 B-28-0.5 Gamma SAMPLE 07/17/08 U 0.00491 0.0241 B-28-4.5 Gamma SAMPLE 07/17/08 U -0.00678 0.0204 B-29-0.5 Gamma SAMPLE 07/17/08 0.113 0.0674 B-29-4,5 Gamma SAMPLE 07/17/08 U 0.00504 0.0217 B-30-1.0 Gamma SAMPLE 07/14/08 U 0.00886 0.0307 B-30-4.0 Gamma SAMPLE 07/14/08 U 0.0315 0.0503 B-30-7.0Gamma SAMPLE 07/14/08 U -0.017 0.0298.B-31-1.0 Gamma SAMPLE 07/14/08 U -0.00836 0.022 B-31-4.0 Gamma SAMPLE 07/14/08 U 0.0241 0.0522 B-32-1.0 Gamma SAMPLE 07/16/08 U 0.031 0.0309 Page 3 of 5 Table 1 Radiological Soil Sampling Data (Cesium-137)

Humboldt Bay Repowering Project Eureka, California Sample Number Sample Type Collection Date E UQ)o (pCi/g) (pCi/g)B-1-0.5 Gamma SAMPLE 07/15/08 0.200 0.0772 B-32-4.0 Gamma SAMPLE 07/16/08 U 0.0137 0.0259 B-32-8.0 Gamma SAMPLE 07/16/08 U -0.0174 0.0294 8-33-0.5-Gamma .SAMPLE 07/16/08 U -0.0054 0.0513 B-33-4.5 Gamma SAMPLE 07/16/08 U -0.0382 0.0412 B-34-1.0 Gamma SAMPLE 07/16/08 U -0.00795 0.0235 B-34-1.0 Gamma DUP 07/16/08 U -0.0593 0.0423 B-34-4.0 Gamma SAMPLE 07/16/08 U -0.0176 0.0282 B-34-8.0 Gamma SAMPLE 07/16/08 U 0.0108 0.0384 PS-01C-1.0 Gamma SAMPLE 07/15/08 U -0.00791 0.029 PS-01C-4.0 Gamma SAMPLE 07/15/08 U 0.0022 0.0308 PS-01C-7.0 Gamma SAMPLE 07/15/08 UL 0.00852 0.0287 PS-02C-0.3 Gamma SAMPLE 07/15/08 U 0.00702 0.0422 PS-02C-4.5 Gamma SAMPLE 07/15/08 U 9.82E-06 0.0299 PS-02C-4.5 Gamma DUP 07/15/08 U 0.0217 0.0361 PS-02C-7.5 Gamma SAMPLE 07/15/08 U -0.0174 0.0442 PS-06C-0.5 Gamma SAMPLE 07/16/08 U 0.0195 0.0262 PS-06C-2.0 Gamma SAMPLE 07/16/08 U 0.00529 0.023 PS-06C-6.5 Gamma SAMPLE 07/16/08 U -0.00126 0.0394 PS-10C-1.0 Gamma SAMPLE 07/14/08 U 0.00963 0.0333 PS-10C-4.0 Gamma SAMPLE 07/14/08 U -0.0209 0.035 PS-10C-7.0 Gamma SAMPLE 07/14/08 U -0.00809 0.0302 PS-11C-0.3 Gamma SAMPLE 07/16/08 U -0.0104 0.040 PS-11C-1.5 Gamma SAMPLE 07/16/08 U -0.00337 0.0388 PS-11C-1.5 Gamma DUP 07/16/08 U 0.022 0.0417 PS-14C-0.3 Gamma SAMPLE 07/14/08 U 0.0338 0.0374 PS-14C-4.5 Gamma SAMPLE 07/14/08 U 0.00679 0.037 Page 4 of 5 Table 1 Radiological Soil Sampling Data (Cesium-137)

Humboldt Bay Repowering Project Eureka, California Sample Number Sample Type Collection Date E U)(pCi/g) (pCi/g)B-1-0.5 Gamma SAMPLE 07/15/08 0.200 0.0772 PS-14C-7.5 Gamma SAMPLE 07/14/08 U -0.00111 0.023 PS-20C-0.3 Gamma SAMPLE 07/17/08 UI 0.00 0.0463 PS-20C-4.5 Gamma SAMPLE 07/17/08 U 0.00448 0.0245 PS-21C-0.3 Gamma SAMPLE 07/17/08 0.199 0.042 PS-21C-4.5 Gamma SAMPLE 07/17/08 UI 0.00 0.0413 PS-23AC-1.0 Gamma SAMPLE 07/16/08 U -0.00992 0.0426 PS-23AC-4.0 Gamma SAMPLE 07/16/08 U 0.00902 0.0335 PS-23BC-0.5 Gamma SAMPLE 07/16/08 U 0.0141 0.0223 Notes: U not detected UI = Uncertain identification pCl/g = picocuries per gram B-24-4.5 Gamma was the only soil samplewith a detected Cesium-137 concentration above 0.5 pCI/g.Page 5 of 5 Table 2 Radiological Soil Sampling Data (Isotopes Other than Cesium-1 37)Humboldt Bay Repowering Project Eureka, California Sample Number Sample Type Collection Date .C E EC a.?0 0 L)2 (pCi/g) (pCi/g) (pC1ig) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pci/g) (pCi/g) (pci/g)B-24-4.5 Gamma SAMPLE 07/17108 Ut 0.00 0.357 U -0.0245 0.059 U 0.026 0.142 U 0.0368 0.139 U 0.0427 0.0705 B-24-4.5 Gamma DUP 07/17/08 Uit 0.00 0.279 U -0.0242 0.147 U 0.0494 0.0687 U 0.0619 0.0993 U 0.0236 0.0505 Notes: U not detected Ul Uncertain identification Page 1 of 8 Table 2 Radiological Soil Sampling Data (Isotopes Other than Cesium-137)

Humboldt Bay Repowering Project Eureka, California Sample Number Sample Type Collection Date o" 0 T' E ib.. M 'E E a) 'D) a)a)Mn :D co: n nn co: (pCi/g) (pCi/g) (pwi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCiug) (pCi/g)B-24-4.5 Gamma SAMPLE 07/17/08 U 0.289 0.456 U -0.195 0.499 U 0.311 0.467 Ut 0.00 0.232 U -0.0109 0.0349 B-24-4.5 Gamma DUP 07/17/08 U 0.183 0.391 U -0.398 0.398 U 0.199 0.341 Ut 0.00 0.124 U -0.00143 0.0252 Notes: U not detected Ut Uncertain identification Page 2 of 8 Table 2 Radiological Soil Sampling Data (Isotopes Other than Cesium-137)

Humboldt Bay Repowering Project Eureka, California Sample Number Sample Type Collection Date C: > " E E E.... ", a7, -Q)Ca , ,C- C (pCi/g) (pCi/D) (pCi/g) (pCig) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)8-24-4.5 Gamma SAMPLE 07/17/08 U 0.0285 0.0859 U -0.232 0.214 U -0.0103 0.0597 U -0.074 0.231 U 0.456 0.580 B-24-4.5 Gamma DUP 07/17/08 U 0.0332 0.0563 U -0.073 0.181 U 0.00798 0.0429 U 0.0295 0.163 U -0.43 0.446 Notes: U not detected Ut Uncertain identification Page 3 of 8 Table 2 Radiological Soil Sampling Data (Isotopes Other than Cesium-1 37)Humboldt Bay Repowering Project Eureka, California Sample Number Sample Type Collection Date c CD E B-4-.5ama UP071708 I 0.06 0.03 -0012 .19 U 0038 051 U -0.043 001 U 2.01 0.98 U-= nt deecte 0 0 0 0 0 C) U U Wi_________

__________________ (pCl/g) (pCi/g) (p0119) (pCi~g) (pCiig) (pCilg) (pCi/g) (pCilg) (pCilg) (pcl/gI B-24-4.5 Gamma SAMPLE 07/17/08 U 0.0501 0.063 U -0.03 0.0258 U -0.0239 0.0669 U -0.0273 0.0607 U -0.0119 0.145 B6-24-4.5 Gamma I DUP 07)17/08 U -0.00669' 0.0435 U -0.0122 0.0198 U 0.0368 0.0514 U -0.00413, 0.0411 U 0.00413 0.0981 Notes: U =not detected Ut Uncertain identification Page 4 of 8 Table 2 Radiological Soil Sampling Data (Isotopes Other than Cesium-137)

Humboldt Bay Repowering Project Eureka, California Sample Number Sample Type Collection Date 'E 0 15" ."- 0 E f , 0 .-2 .1~C c: 0 U U 0 w w -J (pCi/g) (pCi/g) (pCi/g) (pCi!/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCilg)B-24-4.5 Gamma SAMPLE 07/17/08 U -0.021 0.184 U -0.0637 0.0968 U -0.0351 0.049 U 0.0447 0.156 U 0.521 0.950 B-24-4.5 Gamma DUP 07/17/08 U -0.0795 0.120 U 0.0755 0.087 U 0.0117 0.0367 U -0,0472 0.0984 U 154 4.81 Notes: U not detected Ut = Uncertain identification Page 5 of 8 Table 2 Radiological Soil Sampling Data (Isotopes Other than Cesium-137)

Humboldt Bay Repowering Project Eureka, California 0C Sample Number Sample Type Collection Date m _ .C a --e F cu M)- ~ 0 0) 0)00 UUCUU 0U 0>C z)0-J :D ZJ: (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)B-24-4.5 Gamma SAMPLE 07/17/08 0,456 0.128 0.442 0,144 U -0.0285 0.0578 U -0.0488 0.0556 U 0.0155 1.09 B-24-4.5 Gamma DUP 07/17/08 Ut 0.00 0.138 0.318 0.128 U 0.0244 0.0474 U 0.0279 0,0433 U -0.339 0.989 Notes: U not detected Ut = Uncertain identification Page 6 of 8 Table 2 Radiological Soil Sampling Data (Isotopes Other than Cesium-1 37)Humboldt Bay Repowering Project Eureka, California 0C)Sample Number Sample Type Collection Date .E E ! ." aE E I--2 E 2 .2 c 2 z z z Z)_ o-(pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)B-24-4.5 Gamma SAMPLE 07/17/08 U -0.162 0.190 U -0,00447 0.0574 U -0.0684 0.0899 9.02 1.50 U 0.0318 0.0604 B-24-4.SGamma DUP 07/17/08 U -0.0258 0.139 U -0.00647 0.0362 U 0.0779 0.0589 7.19 1.39 U 0.0114 0.0382 Notes: U not detected UI Uncertain identification Page 7 of 8 Table 2 Radiological Soil Sampling Data (Isotopes Other than Cesium-1 37)Humboldt Bay Repowering Project Eureka, California Sample Number Sample Type Collection Date 2 15 E E C (0 C (0 C 2...._(pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (poi/g) (pCi/g)B-24-4.5 Gamma SAMPLE 07/17/08 U -0.0195 0.0645 0.345 0.232 UI 0.00 0.357 U -0.191 0.479 U 0.0353 0.0627 B-24-4.5 Gamma DUP .07/17108 U -0.00427 0.0518 0.427 0.124 Ut 0.00 0.279 U -0.00615 0.334 U -0.00305 0.0435 Notes: U = not detected Ul = Uncertain identification Page 8 of 8 I(71 z r 1 MILE 3/4 1/2 1/4 0 1 MILE SCALE 1 : 24,000 N VICINITY MAP SOURCE: UNITED STATES GEOLOGICAL SURVEY 7.5 MINUTE TOPOGRAPHIC MAPS: FIELDS LANDING QUADRANGLE, CALIFORNIA Humboldt Bay Power Plant Eureka, California POSSIBLE>STORAGE AREA:--"*'._'%.(APPROXJMATE) cO SOURCE Topogsa$.k .p WHwnbo/0I 8.Y P-1e Plant. 7-4 So-ey.U.api,,V -d S Seri yea M2005..7/N SCALE (FEET)0 100 200 SITE PLAN SHOWING DEMOLITION AREAS AND POSSIBLE STORAGE AREA Humboldt Bay Power Plant Eureka. California

~FIGURE 2 LEGEND 15.2 A ..5.10A.p-1 A..-SA A0..1/LOCATION OF MONITORING WELL Or INSTALLED BY ARCADIS. SEPTEMBER 2007 (SUBSEQUENTLY ABANDONOED)

SOIL SAMPLE LOCATION BY CH2MRILL.* JANUARY 2007 APPROXIMATE SOIL SAMPLE LOCATION 9 BY PG&E. AUGUST 2007 (NOT SURVEYED)CONFIRMATORY BORING LOCATION BY a TRC. JULY 2008 RANDOM STRATIGRAPHIC SAMPLE S 3BORING LOCATION BY TRC. JULY 2008 CONTINGENCY BORING LOCATION BY+ TRC. JULY 2008 TEST PILE STAKE LOCATION BY LACO ASSOCIATES.

MARCH 2008 1ý 1. .SOO+PS-10@AS-I.-1 sILI AB11 P,-fl* 5.25-4.APPROXIMATE BOUNDARY OF COASTAL COMMISSION WETLANDS APPROXIMATE BOUNDARY OF SEASONAL WETLANDS P-.-38+ii Aa.10/,//"/'/.//$.1-, A.a21.-3+////?"-K!ISASO Lp002 P100 AT SYRXOSS .dfl -7/i A B-23/A S-s 7 SCALE (FEET)0 NO 120 SOURCES: Topographk masp of HumbooI Bay P0201 Plant. To.ll soo'8pno, Mapping0 a11d 00 SorS',u00, Maoy 2006.EMoY,Metnlla~.

CoIonI,i.

July 21. 2006, ORP.000-0.88-to,.\ p.s- ..:,: /if! 7"--7.//-/., 7,///--7 SITE DETAIL SHOWING SOIL SAMPLE LOCATIONS Humboldt Bay Power Plant Eureka, California tt'//FIGURE 3 I-:-LEGEND LOCATION OF MONITORING WELL 0 0INSTALLED BY ARCAOIS, SEPTEMBER 2007 (SUBSEQUENTLY ABANDONED)

GRAB GROUNDWATER SAMPLE LOCATION BY CH2MAHILL, JANUARY 2007 GRAB GROUNOWATER SAMPLE V LOCATION BY TRC. JULY 2008 APPROXIMATE BOUNDARY OF COASTAL COMMISSION WETLANDS APPROXIMATE BOUNDARY OF SEASONAL WETLANDS.- V -5.IPS.la* 8-20 8.'IV -,V 00-04*( I//@ps-f2 SE3-23'I 1'//%RP.MWWo,4

'://SCALE (FEET)0 60 10 SOURCES'-Top~grphIc mop ofTHIsb~dt Bey PoAP! P/opt, 1o011, SUNT'0t8g, mOepspl end QIS Sofwooo, May 2006, TRS bonnyp locatoI sumye 0:88by PcOnts Ap"t S 0 a00t88 cm,ýAAKAfys'.O

.CoJap.1Ay 2 1. 2008, SITE DETAIL SHOWING GROUNDWATER SAMPLE LOCATIONS H-umboldt Bay Pow~er Plant Eureka. CalifoTnia

• 8102//.f/,* 6 FIGURE 4 LEGEND~S2SP LOCATION OF MONITORING WELL INSTALLED BY ARCADIS. SEPTEMBER 2007 (SUBSEQUENTLY ABANDONED)

SOIL SAMPLE LOCATION BY CH2MHILL.* JANUARY 2007 APPROXIMATE SOIL SAMPLE LOCATION ( BY PG&E, AUGUST 2007 (NOT SURVEYED)CONFIRMATORY BORING LOCATION BY TRC. JULY 2008 RANDOM STRATIGRAPHIC SAMPLE A BORING LOCATION BY TPC. JULY 2008 CONTINGENCY SAMPLE LOCATION BY+ TRC, JULY 2008)APPROXIMATE BOUNDARY OF COASTAL COMMISSION WETLANDS APPROXIMATE BOUNDARY OF SEASONAL WETLANDS EXCA VA TION / REMEDOA TION AREA S SOIL ONLY GROUNDWATER ONLY SOIL AND GROUNDWATER BOB. I 5855 ALL SOIL AND GROUNDWATER RESULTS ARE FOR TOTAL PETROLEUM HYDROCARBONS AS DIESEL [TPH-dJ EXCEPT WHERE NOTED AS BENZO (A)PYRENE [BAP]: DEPTH OF SOIL SAMPLE IN FEET BELOW GROUND SURFACE z depth not specfied SOIL ANALYTICAL RESULT IN MG/KG L- GROUNDWATER ANALYTICAL RESULT IN MG/L NOTES: (1) Al soil and groundwater sample dala shown ere WflecCed by TRC In JuIy 2008 ecept SOn resuls for the excavation area around PS-1 1. wrich was sampled by AreadiS in September 2007./21 Exavaliorfreeredialion areas are appr-ermale and wrfl be Waled based on field co/dirons.

rr /SOURCES: TooograpSc mrap of HrumBIold Say Power Planr, TOMil Slrroretrrr Mpi~eslg and GIS SerbeoeB May 2001 fACBrrr lenngyrr 16dAKrvseyed by Poirr.4 AWoel SUhrepg C6, BOTKnleofrII.

Caldorrrre.

July ZI 1,TEB8 SCALE (FEET)0 60 120 SITE DETAIL SHOWING SOIL AND GROUNDWATER REMEDIATION AREAS Humboldt Bay Power Plant Eureka, California FIGURE 5 FIELD SCREENING RESULTS Date 711412008 Purpose of Survey: Soil Characterization Bore Samples -Marinelli Screen Only Log*Number 08-050 Surveyed by: Phyllis Morrison Signature:

Reviewed By: " .ý ;Seral,. Callbrapion

. Cou nt: .rob.Areai Apha Bkgd -1 Jpha'Static

.:.A.ha.Sc l.e.Ad .B.t.cADA ,Beta Scaler., GammaBkgdc.

CPM Instrument Number: :,.Due 2_ro :M. icm. !"cpm)?:-

z. D M DAD Mdpm. d(cpm) " ;Beta :-! (.d p) .' MDA (dpm)! _ _u- Probe Time .( .n c.. (c m4. P ) ....... r .1 Lud 2221 211772 5112/2009 Nal 1 N/A N/A N/A N/A N/A N/A N/A N/A N/A 1557 2 Detector 206815 5/1212009 Nal 1 2x2 N/A N/A N/A N/A N/A N/A N/A N/A N/A 3 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 4 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 5 N/A N/A N/A N/A N/A N/A NIA N/A N/A N/A N/A N/A N/A N/A N/A Remarks: NB,,,ovab e/Be,,.I.

TotaiStatlcAlpha5Q aa N/A 1 B-13 4.5 1789 232 N/A 1 B-13 7.5 1877 320 ,, N/A 1 8-14 0.5 1826 269 N/A .1 B-14 4.5 1631 74*N/A 1 B-14 7.5 1794 237 ___ _________N/A 1 8-15 1.0 1706 149 ._______N/A 1 8-15 4.0 1749 192 ___ _____N/A 1 .B-15 7.0 N/A N/A Wet N/A 1 B-16 1.0 1943 386 ___________________-

--%.N N/A 1 4.0 1957 400 _________

_____N/A 1 8-16 7.0 1741 184 ________________

N/A 1 8-17 0.5 1866 309 ____N/A 1 8-17 7.0 N/A N/A N/A 1 B-20 0.5 1871 314 4 _N/A N/A 1 B-20 4.5 1846 289 N/A 1 B-20 7.5 2012 455 Page 1 of 2 HBPP-OP-005, Rev. 0 Date 7/1412008 Purpose of :". : .Survey: Soil Characterization Bore Samples -Marinelli Screen Only Log Number: 08-050 Surveyed by: Phyllis Morrison Signature:

Reviewed By:.e ria l C a lib ra tio n ..p hfCo u n t .oaýB tapa ,S t tIc h aL S c a le r : 'Be ta ik g d .B e ta S ta tlc :M P A B ataS c a ler.. G Instrument

..Number. .Due : Probe Time (Mln- .c.(cIbn2)i.

lh- (I ncpn4' i ;MDA )' i;-tA dpm 'A:i' ýi:....> etE (;)' MDA.(dprn.. "mma .. .I Lud 2221 211772 5/12/2009 Nal 1 N/A NIA NIA NIA N/A N/A N/A N/A N/A 1557 2 Detector 206815 5/12/2009 Nat 1 2W2 N/A N/A N/A N/A N/A NIA N/A N/A N/A 3 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A NfA_4 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 5 N/A N/A N/A N/A N/A NIA N/A N/A N/A N/A N/A N/A N/A N/A N/A Remarks: RNA 1 -pleB1re ep4 29amma , 4 N/A 1 8-30 4017 * , .N/A 1 8-30 7.0187 31 ., _ -N/A 1 8-30 .78 .N/A 1 8-31 NA 1 8-3170NA NA -N / Ar 1 1 U r oW e t N/A 1 PS-3C 1.0 2005 448 4 N/A 1 PS-13C 4.0 1982 425 N/A 1 PS-30C 7.0 1876 319 N/A 1 PS-1 4C0 1897 50 NIA 1 PS-14C 4.5 1946 389 N/A 1 PS-14C 7.5 2094 537 Notes: 1. Release Limit = 3(bkgd cpm) 3(1557 cpm) = 4671 cpm 2. MDA = 1757 net cpm (200 cpm above background), 3. Response factor is 350 cpm/pCi/gm of Csl 37 4. Outside of marinelli containers wiped with masselin -massefin counted n no activity above background detected, Page 2 of 2 HBPP-OP-005, Rev. 0 Datc 7/15/2008 Purpose of Survey: Soil Characterization Bore Samples -Marinelli Screen Only Log:Number 08-051 Surveyed by: Phyllis Morrison Signature:

Reviewed By:.-Seria

• airton .1. :~:ounV-,4

Mha baAe ~paBg 146ý iJ, hý!S!Pir ', .Bea1Bkrd; alhaff CalbraaS ScStalIDWret Gammai Skgd. P Instrument Number nMD MD-

icpDuem'.J:etaf..

A.. Probe.. .Tme:(Min):.(cm 2)' -"(cpm), -'- .;dm'M (p)' ,B , .. ...m.. .MDA(dpm), -I Lud 2221 211772 5/1V22009 Nat 1 NIA N/A N/A NIA N/A NIA N/A N/A N/A 1699 2 Detector 206815 5112/2009 Nal 1 2x2 N/A N/A NIA N/A NIA N/A N/A N/A N/A 3 Model 12 78697 511212009 GM N/A N/A N/A N/A N/A N/A N/A N/A NIA N/A 40 4 N/A N/A N/A N/A N/A N/A NIA N/A NIA N/A N/A N/A N/A N/A N/A 5 N/A N/A N/A NIA N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Remarks: ,Sample ;Bore Depthf. Ga. aiScreen R ovabliB;taw

w 1 epy'.,,, Doae, -at ..Smear'# Inet. ' BoreLocation .eet-; x ..ord 'M A;V. .... c 4 P N/A 1 B-i 05 1922 223 4 N/A N/A 1 B-1 4.5 2874 1175 N/A 1 B-1 7.5 NA NA Wet N/A 1 B-2 1.0 1853 154 _N/A 1 B-2 4.0 1710 11 N/A 1 B-2 7.0 2085 386 N/A 1 B-3 1.0 1647 <Bkgd _ _N/A 1 B-3 4.0 1659 <Bkgd N/A 1 B-3 7.0 NA NA Wet N/A 1 B-5 0.5 1870 171 N/A 1 B-5 4.5 1965 266"-,, N/A 1 B-5 7.5 NA NA Wet N/A 1 B-6 1.0 1609 <Bkgd __N/A 1 B-6 4.0 1469 <Bkgd N/A 1 B-6 7.0 1631 <Bkgd N/A 1 8-7 0.5 1835 136 N/A 1 B-7 4.5 1765 66 "_N/A 1 6-7 7.5 1805 106 _Page 1 of 2 I-BPP-OP-005, Rev. 0 Date 7/15/2008 Purpose of Survey

Soil Characterization Bore Samples -Marinelli Screen Only LogwNumber.,08-051 Surveyed by: Phyllis Morrison Signature:

Reviewed By: C~lbauon --ont.-r. Prob Area ;:AlhaýBkgd4

' -7 Aipfla tatilc rAlpha;Sceler, 5,-eta~kgd, -BetaiStatlciMOA-Bta&

~ r caibato --- )**~ p ,~lha'ýEff,ý rw R-~ W,- -- -~.2 ;amaBg.Instrumentf Nubrn *.:`Duev,-, ",'Probe-Tme'(~n 'Ot)hi (p)' -"~~. MDAý(dpmi)'ý9VIDAI(dpmV-Np)

Bt f. )p)~~iM~~p) 1 Lud 2221 211772 5/12/2009 Nal 1 N/A NIA N/A N/A NIA N/A N/A N/A NIA 1699 2 Detector 206815 5/12/2009 Nal 1 2x2 N/A N/A N/A N/A N/A N/A N/A N/A N/A 3 Model 12 78697 5/12/2009 GM N/A N/A N/A NIA N/A NIA N/A N/A N/A N/A 40 4 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 5 N/A NIA NIA N/A NIA N/A N/A N/A NIA N/A N/A N/A N/A _N/A NIA Remarks: 5 SaiilplewBarc;Depth Titain~~e(i-~~~obBt~~~

ota1Saik ~ pa- -TOta1ustaticiataf it--8/DsRate

• ~- s :r; --........a.Smei ~Int. ' ore lction -- -Feet w;I'Coord:,T, 7`CPWc 00CCM-'7~PM 30K~m rc~ 51; ~-s t -~~ hr-N/A 1 B-9 ______ 1_B__107_N/A 1 8-9 4.5 1795 96 N/A 1 B-9 7.5 1676 <Bkgd N/A 1 B-11 1.0 1856 1 57 N/A 1 B-11i 4.0 2502 803 N/A 1 B-11 7.0 2533 834 N/A 1 PS-01C 1.0 1633 <Bkgd _ "_N/A 1 PS-01C 4.0 1607 <Bkgd N/A 1 PS-01C 7.0 1760 61 N/A 1 PS-02C 0.5 1818 119 N/A 1 PS-02C 4.5 1833 134 N/A 1 PS-02C 7.5 1783 84 Notes: 1. Release Limit = 3(bkgd cpm) = 3(1699 cpm) 5097 cpo 2. MDA = 1899 net cpm (200 cpm above background).

3. Response factor is 350 cpnmpCi/gm of Cs137 4. Outside of marinetli containers wiped with niasselin

-nasselin counted -no activity above background detected.5. Background taken in air and repeated at least three times during the day.Page 2 of 2 HBPP-OP-005, Rev. 0 Date 7/16/2008 Purpose of Survey: Soil Characterization Bore Samples -Marinelli Screen Only Log Number 08-054 Surveyed by: Phyllis Morrison Signature:

Reviewed By:: era:. ,Calibration-Count. ýProbeAfrea,, -A~pha'Bkgd7' 4" -'A] Ila"Stai' U Apt~se :~eakd:Betawstaw D BeaclýAlph I I i. cleý-ýGammaiBkgd, CPM,'Instrument" Due`:. Probeý. Time (Mn) (cm 2) ; D&t(dpm) .MDA(dLm).Icpm) (M IBetaf. Idpm): IMDA (dpm): ; __...........___

1 Lud 2221 211772 5/12/2009 Nal 1 N/A N/A N/A N/A N/A N/A N/A N/A N/A 1545 2 Detector 206815 5/12/2009 Nal 1 2x2 N/A N/A N/A N/A N/A N/A NIA N/A N/A 3 Model 12 78697 5/12/2009 GM N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 40 4 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 5 N/A NIA NIA N/A N/A N/A N/A NIA N/A N/A N/A N/A N/A N/A NIA Remarks:ýSsmple B~ore;Depth-s .am4rer f.~~eoa~1ea~'XttSa______________

i0pa' oa8at~e~/'01 4 ~ ~ ~ r '4" *.-'~Y w ~ a Go~oV OS Smear " * " t.4 " :. -," ..- " ' ... .....A/ t W s ,.* ," -'h... ... ; .. ... "06i N/A 1 B-4 1.0 1808 263 4 N/A N/A 1 8-4 4.0 2148 603 __N/A 1 B-4 7.0 NA NA Wet N/A I B-8 0.5 1894 349 N/A 1 6-8 4.5 2044 499 N/A 1 B-B 7.5 NA NA :Wet N/A 1 B-10 0.5 1590 45 N/A 1 B-10 4.5 2020 475 _\N/A 1 B-10 7.5 NA NA Wet N/A 1 8-12 1.0 1687 142 " _ _N/A 1 B-12 4,0 1749 204 _N/A 1 B-12 7.0 NA NA Wet N/A 1 B-18 1.0 1712 167 _,_N/A 1 B-18 4.0 1787 242 ___,,_--N/A 1 B-18 7.0 NA NA Wet N/A 1 8-19 0.5 1920 375"N/A 1 B-19 4.5 1898 353 N/A 1 8-19 7.5 NA NA Wet Page 1 of 3 HBPP-OP-005, Rev. 0 Date 7/16/2008 Purpose of Survey: Soil Characterization Bore Samples -Marinelli Screen Only LoglNumber 08_054 Surveyed by: Phyllis Morrison Signature:

Reviewed By: Serial, Calibration.

Count Probe Are Alp .ha Bkgd: :AlPhaiSatii V.p BStatr iDA t' ataSlr,-'Alpha Eff.' 1 mwpacir .BtaBg:Bt

~ ar nstru men: Probe ma (MT i )1 _,:'_ _ "Mcm MDA ...)... Betae ff. ' ! ......1 Lud 2221 211772 5/12/2009 Nal 1 N/A N/A N/A N/A NIA NIA N/A N/A N/A 1545 2 Detector 206815 5112/2009 Nal I 2x2 N/A N/A N/A N/A N/A N/A N/A N/A N/A Model 12 78697 5112/2009 GM N/A N/A NIA N/A N/A N/A NIA N/A N/A N/A 40 4 N/A NIA N/A N/A N/A N/A NIA NIA N/A N/A N/A N/A N/A N/A N/A 4 N/A N/A N/A N/A NIA N/A N/A NIA N/A A N N/A N/A N/A NIA N/A Remarks:~sampteBore,ýDepthý Gmaren~ 'Zotali¶.R.Y oo{ ',;:. .-,.CCPM,.: ,:10 e %Smear 0 hut. 0 Bore Location v-Feet -/~or~~CM :CP -&CPMI" UOucm-,ý k CP~ i~m "pM DP hOc-'NIA I B-26 1.0 1669 124 N/A 1 83 N/A 1 B-32 1.0 1673 128 N/A 1 8-32 4.0 1713 168 N/A 1 8-32 80 1621 76 N/A 1 B-33 05 1547 N/A 1 83-3 43 1961 416 N/A 1 8-33 7.5 NA NA Wet N/A 1 B-34 0.5 1761 216 N/A 1 13-34 4.5 1979 434 ____ ___ _____ ___N/A 1 B-34 7.5 1906 361 N/A 1 PS-06C 0.5 2155 610 N/A 1 PS-06C 4.5_ 1962 417 N/A 1 PS-06C 7.5 2130 585 N/A 1 PS-11C 0.5 1884 339 N/A 1 PS-11C 4.5 1968 423 N/A 1 PS-11C 7.5 NA I NA Wet Page 2 of 3 HBPP-OP-005, Rev. 0 Date J 7/16/2008 Purpose of -I Survey: Soil Characterization Bore Samples -Marinelli Screen Only Log Number+ I 08-054 Surveyed by: Phyllis Morrison Signature:

Reviewed By: Seripl ' Zlbaonont4.Poer.

phBkd ApaEff~ -Býes'SC 1;~--,-.: , 'G mm kd. CPM'.-: mDe'. cpý-' MDA mý Mrdp m )MABt clr Instrument Number: _:,,Due_ _ probe -T- 4meý(Min) , c rn. j ' .,dpm)a t MDA' c m Beta; B f.ý (dpm)

_____G __ " 1 Lud 2221 211772 511212009 Nat 1 NIA NIA NIA N/A N/A N/A N/A NIA N/A 1545 2 Detector 206B15 511212009 Nal 1 2x2 N/A N/A N/A N/A N/A N/A N/A N/A N/A 3 Model 12 78697 511212009 GM NIA NIA N/A NIA N/A N/A N/A N/A N/A NIA 40 4 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 5 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Remarks:.Sample Bore Depth " Gammaiscreenrýf 7:ý:! oW-movable etai ..;:::,'.'roal StatIc ,Pha : i;

' A- :yDoae Rate y% A,+ W,++y .-Contact N.+

N/A 1 PS-23AC 1.0__784 239_____N/A 1 PS-23AC 4.0 2026 461 _ _ _ _"_"-N/A 1 PS-23AC 7.0 A NAWet N/A 1 PS -23BC __.5_1908_

__363 __ _ _ _ -_ ___._\raq --I--- ir N/A 1 PS-23BC 4.5 NA NA239_ Wet N/A 1 PS-23BC 7.5 NA_ NA__ _ Wet Ne@te _t 1 euleeae Limilt -a 3(1546 tcjp ) 4058 rpm, 2. MDA = 1745 net cpm (200 cpm above background).

3. Response factor is 350 cprn/pCi/gm of Gs137.4. Outside of marinelli containers wiped with masselin -masselin counted -no activity above background detected.5. Background taken in air and repeated at least three times during the day.Page 3 of 3 HBPP-OP-005, Rev. 0 Date 7117/2008 Purpose of Survey : Soil Characterization Bore Samples -Marinelli Screen Only Log Number 08-058 Surveyed by: Phyllis Morrison Signature:

Reviewed By: "Serial Calbration.'

... , Count,-:

ý,Ajpha.Bkgd; -Alh'E,. Aipha;Stiatic' mpha.ScalerJ BetaBkgd:+

.. BetaStati'MDA BetaScler GammaBkgd.

CPM Instrument

-Number.., Due-. Probe 2. h.T.me (Mln) .,] 2 .L p fMDAdpmY 1 OA:(dpmy :-:,c' 2 Bata E ... (dpm) ,MOA(dpm);

__"Ga__a__kgd.__

1 Lud 2221 211772 5/12/2009 Nal I N/A N/A N/A N/A NIA N/A N/A N/A N/A 1403 2 Detector 206815 5/12/2009 Nal I 2x2 N/A N/A N/A N/A N/A NIA N/A N/A N/A 3 Model 12 78697 5/12/2009 GM N/A N/A NIA N/A N/A N/A N/A N/A N/A N/A 40 4 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A NIA N/A N/A N/A 5 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A NIA NIA N/A N/A Remarks:* .ampl Bar43epls-Gansmia;creen

..A 4 RmvbeeBeta~i'~~-,oa Statcph1 ' Toa'ai Bt -yDsae I--' "-100m <CPM/ Dped'1eornh t smear,# Inst: .# Bore Locaton Flýeetý b.T Coord.- P (Qp7b¶,_ 1, Z~p V_5ýT. 10cm fO*( tn,'A'ý_PM DPW-f-100cah N/A 1 B-21 1.0 1699 296 4 N/A N/A 1 8-21 4.0 1612 209 N/A 1 B-22 1.0 1483 80 _N/A 1 B-22 4.0 1469 66 N/A 1 B-23 1.0 1492 89 N/A 1 P-23 4.0 1362 <Bkgd __N/A 1 B-24 0.5 1775 372 N/A 1 B-24 4.5 1785 382 N/A 1 B-25 1.0 1293 <Bkgd "_N/A 1 B-25 4.0 1446 43 "_N/A 1 B-27 1.0 1515 112 _,,_N/A 1 B-27 4.0 1324 <Bkgd __N/A 1 B-28 0.5 1716 313 N/A 1 B-28 4.5 1768 363 N/A 1 B-29 0.5 1792 389 N/A 1 B-29 4.5 1744 341 N/A 1 PS-20C 0.3 1804 401 N/A 1 PS-20C 4.5 1780 377 Page 1 of 2 HBPP-OP-005, Rev. 0 Date 7/17/2008 Purpose of Survey: Soil Characterization Bore Samples -Marinelli Screen Only Log Number 08-058 Surveyed by: Phyllis Morrison Signature:

Reviewed By:.- (B~tiBTa,.:

Apt '.S'ae lo

....Serial :, Callbratln

-r. count ,..ProbeAeaý ' -:: p t c A h ae B a k 'BstatlcP,.m et S calem: Instrument pNumber- Due Probe Tia-me'Mlnl'!

3,; .". Ef f'MDA:(dpn)...(cp

,, ?d........

1 Lud 2221 211772 511212009 Nal 1 N/A N/A N/A N/A N/A N/A N/A N/A N/A 1403 2 Detector 206815 5/1212009 Nal 1 2x2 N/A N/A N/A N/A N/A N/A N/A N/A N/A 3 Model 12 78697 5/12/2009 GM N/A N/A N/A N/A N/A N/A NIA N/A N/A NIA 40 4 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A NIA NIA NIA N/A N/A 5 NIA NIA N/A N/A N/A NIA N/A N/A NIA NIA NIA NIA N/A N/A N/A Remarks:.' :....: -Sample BoreDpth :.Gamma:Scee.' .Removable/Bcta., ta;.Tota1' Static " ',TotaiStatlciBeta'

' :Dose Rate ., .V-/ 07/tv,~ ,'"~' ;0,i`~ , 3 " 't- Co'aM' NOTES Smear # Inst. h#" Bore Locatio ' -' 917 Feet : Coord 'CPM C CPM ., ..s: '.'OO rGroas $ slrl Bt, , 4 0'..R./Dh..

N/A 1 PS-21.C 0.3 1866 463 bm C/N/A 1 PS-21C 45 1836 433 4 NA Notes: 1. Release Limit = 3(bkgd cpm) = 3(1403 cpm) = 4209 cpm.2. MDA = 1603 net cpm (200 cpm above background).

3. Response factor is 350 cprTtpCl/,gm of Co137.4. OutsIde of marinelli containers wiped With mrssetin -masselin counted -no activity above background detected.5. Background taken in air and repeated at least three times during the day.Page 2 of 2 FlBPP-OP-005, Rev. 0 LAB SHEETS DEMOLITION AND REMEDIATION SCHEDULE Project Award & Start UD 100 1 0251 86 IOJUN08 AI 29DEC08 A101 Proiect Kickoff Meeting with PG&E 100 1 0 10JUN08 A 10JUN08 A A102 Notice to Proceed 100 0 0 09JUL08 A A105 Contract Award " 100 0 0 181JUL08 A Al15 Pre-Order Hydroseparator 0 0 0 1SEP08 1 A120 CEC Permit Issued 0 0 0 24SEP08 A130 Project Complete 0 0 0 2 i Project Kickoff Meeting winth PG&E Notice to Proceed* Contract Award a Pre-Order Hydroseparator M, CEC Permit Issued..Project Complete------ -------rr F _t ~ ~A~S888u8~9w44~d1Sa0~9f/JSu.

~-~J~i-2 1`134i 1 1051 12 SOM-Na Il II-C ______________

____________________

p *_________

L __________________

L 4- J-P I-RI Workplan k10 1 I 0 124JUN08AI03JUL08 A A1305 Develop/Submit Draft RI Workplan to PG&E 10 1 0 124JUN08 A 30JUN08 A A1310 PG&E Review Draft RI Workplan 100 1 0 30JUN08 A 30JUN08 A A1320 Develop/Submit Final Workplan to RWOCB 100 1 0 30JUN08 A 30JUN08 A A1330 RWOCB Review Final Workplan 100 1 0 01JUL08 A 03JUL08 A A1340 RWQCB Approves RI Workptan to0 1 0 03JUL08 A 03JUL08 A A1350 ! Rt Worr-knaan Crinw-nrat 10O 1 r3 o[ii.l ovt (3 r A 1I II o evelop/Submit Draft RI Workplan to PG&E G&E Review Draft RI Workplan I I revelop/Submit Final Workplan to RWQC8 RWQCB Review Final Workplan RWQCB Approves RI Workplan-RI Workplan Complete II II II A1350~~~~____

R1Wrea opeeIIo1 0 10JL8A 0 11 California Energy Commission Plan/Reviews 100 1o 19 1 0 125JUNO AI 22JUL08 A-I I Traffic Contro and Implementation Plan/Review o;mNoiseControlProgram I I I A168605 Traffic Control and Implementation Plan/Review 6100 1 i 0 25JUN08 A 02JUL08 A A108 Noise Control Prograw 106 i ____ 6 A 22JUL08A ii ii iI ii it it ii A161 IU Ai~t -u ll -' Ii UI -l -: M l I V W IiU PI Ri Ai OJLU a ItUvU Co sru to ...........

Plan/Review...

.... ........Remedial Action Plan I___I S1 511 38 1 17 107JULO8AI 27AUG08 e DIi P III SA1400 Develop/Submit Draft RAP to PG&E 80 22 4 07JUL08 A 08AUG08 Develop/ ubRie Draft RAP ro PO&E A1410 PG&E Review Draft RAP 0 5 1 5 11AUG08 15AUG08 PG&E Review Draft RAP A1420 I Develop/Submit Final RAP to CEC 0 3 3 18AUG08 _AUG08 DeveloptSulbmit Final RAP to CEC A1430 CEC Review Final RAP 0 -5 21AUG08 27AUG08 -* CEC Review Final RAP A1440 CEC Aproves Final RAP- RAP Comp lte 0 0 I 0 27AUG08 _ CEC Approves Final RAP -RAP Complete I RP Soil Screening/Handling Procedures

____ 14 1 18 [22JUL08 A 28AUG08 -I A1700 Dev/Submit Draft Rem Drawing to PG&E/ENERCON 50 7 4 22JUL08 A 08AUG08 Dev/Submil Draft Rei Drawing to PGE/ENERCON,*.A1710 Soil Screening/Handling Procedure-ENERCON 0 8 8 08AUG08 19AUG08 -- Soil Screening/Handling Procedure-ENERCON II A1730 TRC Review Enercon Procedure I 20AUG08 21AUG8 -TRC Review Enercon Procedure A1740 HBPP PSRC Review/Approval 0 5 5Ji 22AUG08 28AUG08 -HBPP PSRC Review/Approval

-___RAP Data Compilation Report V= ý0 201 20 06oOCTo0l 31OCT08 ==="'AD500 Develop(Submit Draft RAP Comp. Report to PG&E 15 15 060CT08 24OCT08 Develop/Submit Draft RAP Comp. Report to PG&E I11 PG&E Review Draft RAP Como. Report 2 2 2 I,70CT08 280CT08 ,, ,P EReiwDatAPop'eor IStart date 20JUN08 I Early bar Finish date 29DEC08 TRC i Progress bar Data date 05AUG08 G Critical bar Run date 06AUG08 PG&E Humboldt Bay Power Plant -Summary bar Page number 1A Demolition/Rernediation Project Schedule 0 Start milestone point© Primavera Systems, Inc. 0 Finish milestone point A 1520Final Report 0 47 47 24QctTtne I 7OflFC[OR[ A7 ... .. ... .... ... ....A4320 TRC Develop Draft Proj. Completion Report 0 I22 22 24OC08 O0-Ueveap'OoumIX

--ina. rn/" t.omp, re-ri b.RAP Compilation Report Complete S II irTRC Develop Draft Proj. Completion Report F PG&E Review Draft Proj. Completion Report TRC Develop/Submit Final Proj. Completior

'Final Report Complete II A4.311 IPG&F Review Draft Prot. Completion Report 15 15 25NOV08 15DEC08 A,6330 PG&E A4340 TRC C A4350 Final F Final Proj. Completion Report 0 10 10 16DEC08 29DEC08 0 0 0 29DEC08-Irs.,,, 2~P~E1b~ftI4ffl

~ 5 1 1 TI r.~,vi~86 6 t 0 ~4S vy a/vk,*0fnuO5~

/ C bnav~A1 C vNp~r, 17 38 22 28OCT08-~ S -A2100 Mobilize Dnlling Crew 100 1 0 14JUL08 A 14JUL08 A A2200 Mobilize Demolition/Remediation Crew 0 I I t 29SEPOB 29SEP08 A4210 Demobilize Remediation Crew 0 t 1 16OCT08 16OCT08 A4220 Demobilize Demolition Crew I 0 1 I 1 24OCT08 28OCT08 I t100 1 20 0 1 09JULO A 05AUG08 A A3100 Stake Bodngs and Utility Clearance 100 1 2 1 0 109JUL08A 10JUL08A K Mobilize Drilling Crew-Ii MobilizeDemolitionlRemediation CrewDemobilize Remediation Crew Demobilize Demolition Crew I,[Borm,,and Utility Cleary Perform Field lnvestigation/F Analyze Samples AQ ONOC Laboratory icreening 3 ii ii ii ii ii ,1 ii Ii 61 A3300 Perform Field Investiaation/RP Screenian 1t0 5 0 14JUL08 A 1 17JUL08 A A3400 Analyze St A3500 1,ACC Lal 100. 7. [ 1 Induce er4 vULVO A a1 yv Dat inn 0 71 tIIIt na a ovur to A t 1J 11 A 11 1l I I I I#ntvvoeea t " a "" L "" C ..... T F IIflfl/fflfAffilOrOdZvt0;PPJC

~0ffl ~ICO~i k PGJt- 6~t~ 464r0 y easp~z~sv~duvrarvrvsaevIavezdeaveevvme.v, .n 'eS' e .r7vever ~ z rmw/evereedy C v,~v7ze.'4 fleet I f It I1 fr I rr I 71 I 71 I 7onurtP I 1~ ~ 0 1 21 __2_1_9SPOB 27_T0 Drainage Improvements 0o [6 6 29SEP08 06O CT08 A4060 Install aed Seed Veetated Area ! 0 6 6 29SEP08 08OCT08 Install and Seed Vergetated Area Install Contech Devices ii ii ii A4I gta I In~tnll Cri1nfrh £1i~I I a I u I ouceutri I Demolition 0 21 J 21I 29SEP08 I 27OCT08 A4000 Set Up Erosion Control BMPs I0 4 4 29SEP08 02CT08 [_4a Set Up Erosion Control BMPs A4004 Demo MEPP Foundation I 0 2 2 03OT6 06OCTOB lI Demo MEPP Foundation

_________

_______________________________

0 2 2 03OCT08 06OCT08 .A4008 Demo Diesel Fuel Storage Facility D5 0 4 4 07OCT08 10OCT08 Demo Diesel Fuel Storage Facility D S D6 A4010 Demo Circuit Breaker Switch Slab & Tower Slab D6 0 4 4 13OCT08 16OCT08 Demo Circuit Breaker Switch Slab & Tower Stab D6 A4020 IDemo Underground Utilities D7 0 15 15 07OCT08 27CT08 Demo Underground Utilities 7 A4030 -Demo Sandblast and Paint Building D1 0 6 6 09OCT08 160CT08 Demo Sandblast and Paint Building D1 A4040 Demo Miscellaneous Site Facilities D8 0 3 _3 09O0CT 1CT08 Demo Miscellaneous Site Faclities D8 A4050 Demo Storaqa Buildin and Additions 02 0 4 4 I 16OCT08 21OCT08 DLa[cemo Storage Building and Additions D2 A4070 Demo Proects Office 5-Wde D4 0 -2 2 22OCT08 230CT08 E-Demo Projects Office 5-Wede 04 Remediation

t I 0 13 13 29SEP08 15OCT08 '.A4100 Eecavate Impacted Soil 0 4 4 29SEP08 02OCT08 L Excavate Impacted Soil A4110 Sample Excavation Bottoms and Stockpiled Soil 0 4 4 02OCT08 07OCT08C..

Sample Excavation Buoms and Stockpiled Soil A4120 Load, Transport and DisPose of Contaminated Soil 1 0 4 4 0OCT08 09OCT08 Transport and Dispose of Contaminated Soil Start date 20JUN08 Finish date 29DEC08 Data date 05AUG08 Run date 06AUG08 Page number 2A© Primavera Systems, Inc.TRC PG&E Humboldt Bay Power Plant Demolition/Remediation Project Schedule Early bar Progress bar 1 Critical bar-Summary bar Start milestone point 0 Finish milestone point 21 Access Tank and Determine Tank Bottom Thickness I 100 t1 0 OSAUG08 O5AUG08 A A141 Mobilize Demolition and Remediation Crew 0 0 0 0 0 25AUG08 A151 Demobilize Demolition and Remediation Crewj OJ0 0 0 26SEP08 A231 Mobilize Drll Rig ] 0 1 1 01OCT08 01OCT08 A241 Demobilize Drill Rig 0 1 1 02OCT08 02OCT08 Access Tank and Determine Tank Bottom Thickness Mobilize Demolition and Remediation Crew.e-Demobilize Demolition and Ri n Mobilize Drill Rig.Demobilize Drill Rig , I I ýýI aroject Complete mediation Crew A251 I Project Complete Plans and Permits-0 1 0 0 17OCT08_ ]O il 54 54 05AUG08 17OCT08 A121 Work Plan 2 9 9 05AUG08 S1AUGO8 A131 Health and Safety Plan 2 9 9 05AUG08 1SAUG08 A161 Stormwater Pollution Prevention Plan .. 2 g 9 05AUG08 15AUG08 A321 Humboldt County Drilling Permit 2 9 9 Q05AUG08 15AUG08 A331 Humboldt County Demo Permit2 2 9 9 05AUG08 15AUG08 II11 II MdorIak, Plan.ealth and Safety Plan lStormwater Pollution Prevention Plan d'Humboldt County"Drilling*

Permit=11"umboldt County Demo Permit.I L Prtc inR o I saul Prni=rf I I I ~IA381 ProjecC ___t______I___1___._____o_

eporv -L 0,1Jul of "--' Pe r ep.'~r Demolition and Remediation

____ I 25AUG08 Fi________

] B 3 15tOCT08 --AVIl Remove Transite Panels and Fiberglass 0 15 15 25AUG08 12SEPOB -Remove Transite Fers and Fiberglass A171 Clean LFO 2 0 15 15 2SAUG08 12SEP08 L. --- Clean LEO'2 A181 Transport Waste 0 15 15 26AUG08 15SEP08 r ---- Transport Waste A201 Demolish LFO 2 0 5 5 15SEPO8 19SEP08 Demolish LFO 2 A211 Remove Support Equipment (e.g., Heat Exchangers) 0 15 15 25AUG08 12SEP08 -.., JRemove Support Equipment (e g., Heat Exchangers)

A291 Break Out Concrete 0 2 2 22SEP08 22SEP08 ý Break Out Concrete A301 Import Clean Fill/Use Berm Fill 0 2 2 22SEP08 .23SEP08 import Clean Fill/Use Berm Fill A311 Site Restoration 0 3 3 24SEP08 26SEP08 Site Restoration A31 1Soil Removal 0 5 5 08OCT08 14OCT08 3r Soil Removal A371 Soil Transport 0 5 5 09OCT08 1SOCT08 T I Soi Transpor, Site Assessment I 1 0 1 12_ 12 29SEP08 140CT08 A221 Utility Clearance 0 2 2 29SEP08 30SEP08 Utility Clearance A261 Drilling and Samplin 0 2 2 I01OCT08 02OCT08 DrFfilting and Sampling A271 Site Restoration I0 1 1 03OCT08 03OCT08 Restoraton A281 Waste Management 0 10 10 01OCT08 140CT08 t-,. -Waste Management A341 Analytical Testing Program (48-hour TAT) 0 3 3 02OCT08 06OCT08 -Analytical Testing Program (48-hour TAT)A351 Ry Analytical/Finalize Soil Removal Quantities I 0 I 2 2 I 06OCT08 07OCT08 -Rv Analytical/Finalize Soil Removal Quantities Start date 20JUN08 .. .. Early bar Finish date 29DEC08 TRC Progress bar Data date 05AUG08 G Critical bar Run date 06AUG08 PG&E Humboldt Bay Power Plant -Summary bar Page number 3A Demolition/Remediation Project Schedule 4, Start milestone point© Primavera Systems, Inc. , Finish milestone point Laboratories LLC a member of The GEL Group INc PO Box 30712 Charleston.

SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com July 25, 2008 Mr. Moises Carvalho TRC Solutions, Inc.55 2nd Street, Suite 575 San Francisco, California 94105 Re: Humboldt Bay NPP Project 161072, Task 2400 Work Order: 212047

Dear Mr. Carvalho:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on July 16, 2008. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction.

If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.Sincerely, Erin Stanley Project Manager Purchase Order: 161072 Enclosures problem solved GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report for TRCS002 TRC Solutions Client SDG: 212047 GEL Work Order: 212047 The Qualifiers in this report are defined as follows:* A quality control analyte recovery is outside of specified acceptance criteria** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.The designation ND, if present, appears in the result column when ihe analyte concentration is not detected above the detection limit.This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures.

Please direct any questions to your Project Manager, Erin Stanley.Reviewed by GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-16-1.0 Gamma Proiect: TRCS00200 Sample ID: 212047001 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 10:00 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Cor,'ected" Cesium-137 U 0.0238 +/-0.0306 0.0467 0.100 pCi/g MJ-HI 07/17/08 1425 774961 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 25, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-1 6-4.0 Gamma Project: TRCS00200 Sample ID: 212047002 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 10:40 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0208 +/-0.031 0.0572 0U100 pCi/g MJH1 07/18/08 0626 774961 1 The following Prep Methods were performed

'Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 6 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

B-16-7.0 Gamma 212047003 Soil 14-JUL-08 11:10 16-JUL-08 Client Project: TRCS00200 Client ID: TRCS002 Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.00401 +/-0.0213 0.0367 0.100 pCi/g MJH1 07/18/08 0626 774961 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description.

Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address: 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: PS-IOC-LO Gamma Project: TRCS00200 Sample ID: 212047004 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 11:30 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.00963 +/-0.0333 0.0586 0.100 pCi/g MJHI 07/18/08 0627 774961 1 The following Prep Methods were performed.Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: PS-IOC-4.0 Gamma Project: TRCS00200 Sample ID: 212047005 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 11:55 Receive Date: 16-JUL-08 Collector:

Client I 'Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method* -Rad Gamma Spec Analysis Ganiniaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0209 +/-0.035 0.0552 0.100 pCi/g MIH 1 07/18/08 0831. 774961 1 The following Prep Methods were performed-Method Description Analyst Date Time , Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed-Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 240f1 Report Date: July 25, 2008 Client Sample ID: PS-IOC-7.0 Gamma Project: TRCS00200 Sample .ID: 212047006 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 12:25 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate.

Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00809 +/=0.0302 0.0419 0.100 pCi/g MJHI 07/18/08 0832 774961 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep .Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corn Certificate of Anaqlvqi T Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

B-30-1.0 Gamma 212047007 Soil 14-JUL-08 13:45 16-JUL-08 Client Proiect: TRCS00200 Client ID: TRCS002 Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gamnnaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.00886 +/-0.0307 0.0547 0.100 pCi/g MJHI 07/18/08 0833 774961 1 The following Prep Methods were performed Method Description Analyst Date. Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed-Method Description Analyst Comments EML HASL 300, 45.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-30--4.0 Gamma Project: TRCS00200 Sample ID: 212047008 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 14:05 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137.

U ' 0.0315 +/-0.0503 0.0886 0.100 pCi/g MJHI 07/18/08 0910 774961 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-7021 CXCI -07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis of Analvsis Company: TRC'Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 25, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

B-30-7'0 Gamma 212047009 Soil 14-JUL-08 14:20 16-JUL-08 Client Project: TRCS00200 Client ID: TRCS002 Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method". Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.017 +/-0.0298 0.0483 0.100 pCi/h MJHI 07/18/08 0910 774961 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch-Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4,5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address: 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400.Report Date: July 25, 2008 Client Sample ID: B-31-1.0 Gamma Proiect: TRCS00200 Sample ID: 212047010 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 14:45 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Ganmnaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00836 +/-0.022 0.0355 0.100 pCi/g MJHI 07/18/08 0911 774961 1 (The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 C:

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corn Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-31-4.0 Gamma Project: TRCS00200 Sample ID: 212047011 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 15:00 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0241 +/-0.0522 0.0922- 0.100 pCi/g MJI1l 07/18/08 0912 774961 1 The following Prep Methods were performed Method Description Analyst Date Time, Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 25, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 C Client Sample ID: B 1.0 Gamma Proiect: TRCS00200 Sample ID: 212047012 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 16:10 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0244 +/-0.0326 0.0604 0.100 pCi/g MJH1 07/18/08 1045 774961 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corn Certificate of Analysis Company TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco.

California 94105 Report Date: July 25, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-15-4.0 Gamma Project: TRCS00200 Sample ID: 212047013 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 16:15 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Methot Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0128 +/-0.0271 0.0468 0.100

• pCi/g MJHI 07/18/08 1045 774961 The following Prep Methods were performed Method Description Analyst Date .Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments i , IEML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (Company: Address TRC Solutions, Inc.55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 25, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-20-0.5 Gamma Project: TRCS00200 Sample ID: 212047014 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 10:00 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gamnimaspec; Gamma, Solid "Dry Weight Corrected" Cesium-7137 U 0.0207 +/-0.0291 0.054 0.100 pCi/g MJHI 07/18/08 1046 774961 1 The following Prep Methods were performed (Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 C GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corn Certificate of Analysis.Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 25, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-20-4.5 Gamma Project: TRCS00200 Sample ID: 212047015 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JIUL-08 10:25 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gamnhaspec, Gamma, Solid "Dry Weight Corrected" Cesium.-137 U -0.0114 +/-0.0296 0.0485 0.100 pCi/g MJHI 07/18/08 1228 774961 .I The following Prep Methods were performed M~ethod Depwrintinn Analyst -. gt Timep Pren flateh Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL. LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (.Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-20-7.5 Gamma Project: TRCS00200 Sample ID: 212047016 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 10:48 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rod Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00987 +/-0.0243 0.0399 0.100 pCi/g MJHI 07/18/08 1228 774961 1 (The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address: 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

PS-14C-0.3 Gamma 212047017 Soil 14-JUL-08 11:30 16-JUL-08 Client Project: TRCS00200 Client ID: TRCS002 Parameter Qualifier Result Uncertainty DL RL , Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid 'Dry Weight Corrected" Cesium-137 U 0.0338 +/-0.0374 0.069 0.100 pCi/g MJHI 07/18/08 1229 774961 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI : 07/16(08 1748 774803 The. following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis/Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: PS-14C-4.5 Gamma Proiect: TRCS00200 Sample ID: 212047018 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 11:57 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.00679+/-0.037 0.064 0.100 pCi/g MIJHI 07/18/08 1229 774961 .I The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 K.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 25, 2008 Contact: Mr. MoisesCarvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: PS-14C-7.5 Gamma Project: TRCS00200 Sample ID: 212047019 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 12:16 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesiumr-137 U -0.00111 +/-0.023 0.0384 0.100 pCi/g MJ-HI 07/18/08 1230 774961 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1748 774803-The following Analytical Methods were performed Method Description Analyst Comments* 1 EML HASL 300, 4.5.2.3 I -...

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-13-0.5 Gamma Project: TRCS00200 Sample ID: 212047020 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 14:05 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Ganimaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0187 +/-0.0372 0.0674 0.100 pCi/g MJHI 07/18/08 1231 774961 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/16/08 1748 774803 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis...................s i-Company TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-13-4.5 Gamma Project: TRCS00200 Sample ID: 212047021 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 14:20 Receive Date: 16-JUL-08 Collector:

Client.Parameter Qualifier Result Uncertainty DL RI, Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0174 +/-0.0254 0.0399 0.100 pCi/g MJi1II 07/18708 1607 774962 1 The following Prep Methods wereperformed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-817.1

-www.gel.com Certificate of Analysis.Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-13-7.5 Gamma Proiect: .TRCS00200 Sample ID: 212047022 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 14:23 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0171 +/-0.0292 0.0472 0.100 pCi/g MJHI 07/19/08 0853 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com C prtit r-ntp nf af Analyqiv-Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-17-0.5 Gamma Project: TRCS00200 Sample ID: 212047023 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 14:50 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0169 +/-0.0294 0.0527 0.100 pCi/g MJHI 07/19/08 0854 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-17-4.5 Gamma Project: TRCS00200 Sample 1D: 212047024 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 15:10 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamina Solid "Dry Weight Corrected" Cesium-137 U -0.0105 +/-0.0333 0.0544 0.100 pCi/g MJHI 07/19/08 0854 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-17-7.5 Gamma Project: TRCS00200 Sample ID: 212047025 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 15:25 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate -Time Batch Method Rad Gamma Spec Analysis Ganmmaspec, Gamma, Solid "DTy Weight Corrected" Cesium-137 U 0.0274 +/-0.0265 0.0494 0.100 pCi/g MJH1] 07/19/08 0855 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corn Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 25, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 (Client Sample ID: B-14-0.5 Gamma Project: TRCS00200 Sample ID: 212047026 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 15:55 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnialystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0164 +/-0.0236 0.0371 0.100 pCi/g MJHI 07/19/08 0855 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample JD: B-7-0.5 Gamma Project: TRCS00200 Sample ID: 212047027 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 09:20 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Methom Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00961 +/-0.0205 0.0325 0.100 pCi/g MJHI1 07/19/08 0856 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/16/08 1757 774806 The following Analytical Methods were performed.Method Description Analyst Comments S1 EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address: 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-7-4.5 Gamma Proiect: TRCS00200 Sample ID: 212047028 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 09:40 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.00887 +/-0.0394 0.0667 0.100 pCi/g MJHI 07/19/08 0856 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3{1 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

B-7-7.5 Gamma 212047029 Soil 15-JUL-08 10:00 16-JUL-08 Client Proiect: TRCS00200 Client ID: TRCS002 Parameter.

Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch. Metho Rad Gamma Spec Analysis Gammaspec, Gamma, Solid 'Dry Weight Corrected" Cesium-137 U -0.00175 +/-0.0443 0.0709 0,100 pCifg MJHI 07/19/08 0857 7.74962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RtAD-A-021 CXCI1 *07/16)08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 25, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 (Client Sample ID: PS-01 C-I1.0 Gamma Project: TRCS00200 Sample ID: 212047030 Client lID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 08:20 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00791+/--0.029 0.0485 0.100 pCi/g MJHI 07/19/08 0857 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed'Method Description Analyst Comments EML HASL 300, 4.5.2.3 (.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 25, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-14-4.5 Gamma Project: TRCS00200 Sample ID: 212047031 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 16:05 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" " Cesium-137 U -0.00831 +/-0.0166 0.0273 0.100 pCi/g MJHI 07/19/08 0858 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 .CXCI 07/16/08 1757 774806 The following Analytical Methods were performed Method.' Description Analyst Comments, EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 25, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 (Client Sample ID: B-14-7.5 Gamma Proiect: .TRCS00200 Sample ID: 212047032 Client ID: TRCS002 Matrix: Soil Collect Date: 14-JUL-08 16:13 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis.Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0264 +/-0.0233 0.0356 0.100 pCi/g MJH1 07/19/08 0858 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis....... [Company: TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalbo Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-9-0.5 Gamma Project: TRCS00200 Sample ID: 212047033 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 08:43 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Methe Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.000848

+/-0.0219 0.038 0.100 pCi/g MJ`H1 07/19/08 0859 774962 1_The following

'Prep Methods were performed Method Description -Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-9-4.5 Gamma Project: TRCS00200 Sample ID: 212047034 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 08:55 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method.Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0226 +/-0.0248 0.0444 0.100 pCi/g MJH1I 07/19/08 0859 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-9-7.5 Gamma Proiect: TRCS00200 Sample ID: 212047035 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 09:10 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Methow Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0176 +/-0.038 0.0595 0.100 pCi/g MJHI 07/19/08 0901 774962 1 The following Prep Methods were performed Method Description Analyst Date. Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: PS-01C-4.0 Gamma Proiect: TRCS00200 Sample ID: 212047036 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 08:40 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0022 +/-0.0308 0.0533 0.100 pCi/g MJHI 07/19/08 1136 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis.....................

j -- _--Company : TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: PS-01C-7.0 Garrmma Project: TRCS00200 Sample fD: 212047037 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 09:15 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho, Rad Gamma Spec Analysis Gaminaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.00852 +/-0.0287 0.0503 0.100 pCilg MJH-1I 07/19/08 1136 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed NMethod Description Analyst Comments EML HASL 300, 4.5.2:3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (Company : TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-3-1.0 Gamma Proiect: TRCS00200 Sample ID: 212047038 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 09:35 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00295 +/-0.0308 0.0523 0.100 pCi/g MJHI 07/19/08 1137 774962 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16/08 1757 774806 The following Analytical Methods were performed Method Description Analyst Comments EMIL HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 25, 2008 Client Sample ID: B-3-4.0 Gamma Project: TRCS00200 Sample ID: 212047039 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 09:50 Receive Date: 16-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho(Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Di-y Weight Corrected" Cesium-137 U -0.0102 +/-0.0283 0.0471 0.100 pCi/g MJHI 07/19/08 1137 774962 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/16108 1757 77,4806 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary TRC Solutions, Inc.55 2nd Street, Suite 575 San Francisco, California Contact: Mr. Moises Carvalho Workorder:

212047 Revort Date: July 25, 2008 Page 1 of 2 Parmname Rad Gamma Spec Batch 774961 QC1201623294 212047001 DUP Cesium- 137 QC1201623295 LCS Americium-241 Cesium- 137 Cobalt-60 NOM Sample Qual QC Units RPD% REC% Range Anist Date Time U 0.0238+/-0.0306 15.9 6.02 7.86 0.0747+/-0.0362 13.0+/-1.10 5.78+/-0.500 7.96+1-0.655 pCi/g 103 *(0% -100%) MJHI 07/18/08 12:48 pCi/g pCi/g pCi/g pCi/g 82 (75%-125%)

96 (75%-125%)

101 (75%-125%)

07/23/08 06:11 QC1201623293

.MB Cesium-137 U -0.00669+/-0.0206 07/18/08 12:47 Batch 774962 QC1201623297 212047021 DUP Cesium- 137 U -0.0174 .U+/-0.0254 QC1201623298 LCS Americium-241 Cesium- 137 Cobalt-60 15.9 6.02 7.86-0.0161+/-0.0199 13.5+1-1.14 6.24+/-0.480 8.03+/-0.600 pCi/g 8 pCi/g pCi/g pCi/g pCi/g 85 (75%-125%)

104 (75%-125%)

102 (75%-125%)

07/19/08 11:39 N/A MJHI 07/19/08 11:39 QC1201623296 MB Cesium-137

• U -0.00263+/-0.012 07/19/08 11:38 Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C .Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded GEL LABORATORIES LLC.2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

212047 Page 2 of 2 Parmname NOM Sample Qual QC Units R.PD%, REC% Range AnIst Date Time J Value is estimated M M if above MDC and less than LLD N/A RPD or %Recovery limits do not apply.ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.Ut Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.

h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more." The Relative Percent Difference (RtPD) obtained from the sampleduplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the R-L, a control limit of+/- the RL is used to evaluate the DUP result.* Indicates that a Quality Control parameter was not within specifications.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

__,___"_ of GEL Chain of Custodv and Analvtical Reauest:'+.,,,,u

\\ p ; ,GEL Work Order Number: t t -0 d7 49 Phone #: ~_ _¢.' *GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178 Sample Analysis Pqluested (s) (Fill in the number of containers for each test)* V I V r'S.¶--r-----,-

V r r 7 7-'I ~'i~v 'ame: ~ a,, ~ ~Fax#U: q3 Shoild this sampln be considered:

<-- Preservative Type (6),' j (A. 5 pr, ,, Send Results To:,A.\11 I*acnioietSample ID-*cnpoie indicate salrt an id stoap daiet chne*Date Collected (mm.dd-,yy)

• Timet Colleetcd (Military)(hhmam)0\an r-E a 0 I.-1'-Q('C ode Field Sample 411 Filtered 01 1 Matrix" 1 Comments Note: extra sample is required for sample specific QC 7I 1 16-1 MO:OO & I t;A~4i I. .-Y' _______-71 I11a IW~ Nvo1/,VA o0\' ý \\-\'O GO.~rO.7 Iloiob \cc c Th~ GCI.W~CrCI.

.711ailor wi~o Ga9Y ym ex~_ ___ _ ________________7jI1/

\\4 14 & /V -________ __ ___ __ ___ 2ILtk* \A~ 2.Ai +50 _ __ _ _ _ _5 1V 'boI I A, f..aTL~ I Il, A'!,uas: theNoreal:

Rush appcable to 1ltthes lrsaes) IfX R suills: Yes Ia l1 mar!As: Are there any known hazards applicable to tAh~se sa~nzples?

If so, please list the hazards Xn- f-' C6irc-ic Deliverable:

C of A I OC Summrarv I Level I/ Level 3/ Level 4 Samale Collection TimmeZofi Eastern uay Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details fiwhitished By (Signed)5,\I-+Date Time-2/cfbm Received by (signed) Dale , ..O.., Timec GEL PM: IF AY/Iflnt,. Shirnn.,il.

"7 h~J 1~q,__________________________________

2 4LAirbill

1. 3 Airbill,#at., Clutnly Number -Client I)ctennined.jý "adcs: N -Normal Sample.T8

= Trip Blank, FD -Field Duplicate.

Ell -Equipmecnt Blank, MS -Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample. C -Grab C = Composite I d Filtered:

For liquid matrices.

indicate with a -V -obr yes the sample was field filtered or- N- nbr satiple was not field ilicrer.t'+.ý;ýj_,x Coden- DW-Drinking Water, GW-Oroundnwater.

SW-Surface Water. WW-Wase Water. W-WaiCr. SO-Soil. SD=Sedimcnt..S..Sludge.

SS-Solid Waste. 0-0i1, FPFilter, P=Wipe. U-urine, F-Feeal, N-Nasal 11.,c Analy. N_-qucseld:

Analytical method requested (i.e. 82606. 60F8tt70Al acid numhnto containers pravided ftr each (i4. 82600 -3. 60108,7470A -I).', otive A- Hydrochloric Acid, NI -Nitric Acid. Si = Sodium llydroxide, SA -Sullfuric Acid, AA -Atcorbic Acid. HX = li.y T-.Sodium "hiesullatc.

itro preservative is added -lesa Ild blank WHITE= LABORATORY YELLOW = FILE PINK = CLIENT For Lab Receiving Use Only C>ktqy Seal Intact?NO Cooler Temnp: C Page: orf GEL Laboratories, LLC Project: Ia GEL Chain of Custody and Analytical Request 2 040 Savage Road GEL Quote 9: Charleston, SC 29407 COC Number t..: GEL Work Order Number: Phone: (843) 556-8171 PO Number: \Fax: (843) 766-1178 Client Name: Phone #: q, 3000 Sample Analysis Requestedist (Fill itt bte number of containers for each test)ProectSt~

Nme: ~ ~ ~ Fa 4:x~~ ~i~\ ~ Shonutd this <-- Preservative Type (6)Proec/Sie am : '> aXsample be 1; -Address:;JA~

considered..

_7 " \0 -)Comments Colete by:Send Result.To:N-\

_-_Note: extra sample is X ', I " required for sample'Datc Collected Collected QC Code Field Sampl .r Sample ID (Mililtry)

C Filteredld Matrixp 0 specific QC For conitositcm

-indicate start and stop date/time( (hhMim) lr i P u_ _ _ _ _ _ _- _ _ __,o_ _ _ _ _ _ g I \ 5 ( A /A E o ___ Y X S-30--1,o G, 2It°i , \W'o &' NtA L 5D \ L _\ -0 7 1/1 10-6 1, , 1 Lo 5. ;G I I X _ __I b. )l -0\.o Nu ,1..J l1- 50 _ "_,, 1~~~~uma Leve "-3 Lee 4 t c ~X & __ _ _ _ _TAT Reqesed Normal, Ruh--- v is ocuSub oarc'honav" Fax Resitlts:

Yes tCrcle Deliverttble:

C or A /QC Summary /Lel I/ Lvl3ILcl4 Remnarks.

Ape there any known hazards applicable to these samples? If so, please list the hazards 1 Samole Collection Time Zo.e Eastern <P~s~\\ ~ ~ "" ~ ~ "'~Central Other-___Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed).

Date Time Received by (signed) Date Tinme GEL PM: `P ro ' fa S3 nDat AShiped: -7)22 Airbilt II 3 ~~~~3 -Arit 1.) Chain ol'Cintody Nomher -Client Deterinired 2.) QC Codes: N = Normal Samole. TB -Trip IBlank, FD -Field Duplicate.

EB -tquaipmelt Blank, MS -Muarix Spike Sample. MSD -Matrix Spike Duplicate Sample. G -Grab. C -Composite 3J. Field Filtered:

For tictuid matrices.

iodieote with d -V -for yes tlie sample was field filered tor -N -[or sample was nrt lield tittered.4.1 Matris Codes: DW=Drinking Water. GW-Groundwster.

SW-Suarace Water, WW-Wasie Water. W-Water. SO-Sol, SD-Sediient.

SL=Sludgc.

SS-Soaid Wasi. O-Oil. F=Fiter. P-Wipe. U=Urinc. F-Focal. N-Nasal 5.1 Sample Requested:

Analylicat method requested (i.e. 82608, 601oBfl470A) and number ofrcvtiners provided for caeci (i.e. 8260B -3. 601011t747lA

-I).6.) treservlive Type: HA -I lydmchltaric Acid, NI -Nitric Acid. SH = Sodium Hydroxide.

SA = Sulltric Acid, A A = Ascorbic Acid. 11X = I lcxtce. ST = Sodium Thiasullate.

Irto preservative is added leace field blank WHITE = LABORATORY YELLOW = FILE PINK = CLIENT For Lab Receiving Use Only C , S ea Intact?n, No Cooler Tempi: C 16N : ,GEL Chain , " mGEL Work Order Number: of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178 Phone#U: ~\c ~ ~ __,,, .Name: " b r Fax#: xA"'-j " Should hi, sample be dli ~ .~ ~-c~ ~ (~ ~considered

'>,-f r* aIL ,c " Send Results To'N\N, _.-- (ýý 41. ý ) _2 iDate Collected

• 'rim SSample ID Collectd QCCode Field Steeple " S m l ID(Military)

Filtered

.,,r cOm sites -indicate start and stop date/time (mm-did-yy) (hhml t .UG qvn,, o1,\o )5,00 (0 A/hp 1_____ __-___-___

__-__ __ ')s:15 C, " 7/LAI 0 k6 \1'i C /VA ý2D , \__,-\.o __ 7j1L1)0 \I5 Ct /VA 5-7/14.10 , 5o C5o'Aoý,:jtriestd:

Nonnao: .ush: s pial t he sacple Ifo s o, pateax iResut s Yh c h i A 1 6,twrk.ý.ý Are there any known hazards applicable to these samples? If so, please list the hazards Sample Analysis Requested (5) (Fill in the number of containers for each test)$C as C C U C B C C I-<- Preservative Type (6),0 5S%J Comments Note: extra sample is required for sample specific QC 4- 4- 4.-----.

-+ -I.-. 4-4-4-I I- 1- f 4-- t -I I I>( Ix\X I _ __XX_ I I J-1~.. -I -[.I -X L.... ..i-I...1___________

--~ 4- '-5 -a- ~ 44 -1.- 4-4-4 Ic T-Lv I je~ I In~ i LJi I ____________

Circle Deliverable:

CofA / QC Summary / Level e 3 / /Level4.Cole-ton Tome Zone Eastern <Central Other[7_Mountain Chain of Custody Signatures Sample Shipping and Delivery Details i,.ihed By (Signed) Date Time Received by ig ed) Date Time GEL PM: -1 0 4 731t\o/CZ 14Ui* , cleot ofoShipmeat:

FA e Date Shipped: 7 I r 2 Airbill N: j3 lAirbill #:.' :'aundy Nuaber -Client Detemtined i.:. ,: N -Normal Sample. TB -Trip Blank. FD -Field Duplicatlc.

E0 -Equipmcen t lank, MS Matrix Spike Sample. MSD -Matrix Spike Duplicale Sample. C -Grab. C -Conmiosii i .rd: tFer liquid matrices.

indicate with a -Y -for yes the sample was rield littered or -N -for sample was not lIed tiltered.;ýj '.w. )ts: DW-Drinking Water. CW.Groundwuatr.

SW-Surfaec Water. WWWuste Water. W-Wuirr. SOmSoil.SD..Seudiment.

St.Sludge.

SS=Solid Waste. O-Oil. F-l'itcr.

P-Wipe. U-Urinc, F-Fecal. N-Nasal n::.alysis Rcquesed:

Analytical method requested (i.e. 826111. 6010B1/7470A) and number aofcontainers provided tor each (i.e. 82608 .-3.6010,7/74704

-It)., ive Type: HA = Hydrochloric Acid. NI -Nitric Acid. SH = Sodium Hydmide. SA -Sulfuric Acid. AA -Ascorbic Acid. H-X -I lxana. ST -Sodium Thltsulrate.

Irno preservative is added -leave icid blank.WHITE = LABORATORY YELLOW =FILE ' PINK a CLIENT For Lab Receiving Use Only'V.akSeal Intact?) NO a/655ler Temp.C Page: --of GEL Laboratories.

LLC-ijcct#: .o GEL Chain of Custody and Analytical Request 2o4oSavage Road GEL Quote #: Charleslon.

SC 29407 COC Number GEL Work Od Number: Phone: (843) 556-8171 P0 Number: 07 Fax: (843) 766-1178 Client Name: L Phone #: L 3oq a Sample Analysis Pgquested s (Fill in the number of containers foreach test)Project/Site Namne: Fax 9: IA I C -rAI- t3 7g Should this -Preservative Type (6)X' &.A ~saroptebe

--Address: considered:

r omet Arlne~: .0010c --Comments Collected y: .-- Send Results To: -Note: extra sample is* l colleetea " "E .required for sample Dat Coleced Collected QC Ckdc Field Sample spcfcQ Sample ID N'ltrr -7 Mt1~ ~ t5 S ~~~d D'(Military)

Fitee Matrix" [ For comptnsiies

-indicate start and stop date/time (mm -d.yy) (hhmm)G-- .-4c -,r .(72-5* -...114(,~~ lii -S-p. L v.el ,, I.. 'L...d 3.. ...TAT Requested:

Normal: .Rsh: Speeify";SnbjcttoSurehaepl faestts Yes R CireleDellverable CorA I CSuinma / Lcvel /'I " /"Level"3

.Level4 Rentarks:

Are there any known hazards applicable to these samples? If so. please list the hazards SEample________nTime Eastern 4mg SM -reý (Sý-A Central Other_ _]Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Received by (signed) Date Time GEL PM:*~5 '~O7 1 -7. / %1&1 -0 0`0 Method ofShipnicol:

k Date Slieped: 715LY 12 U2 lAirbill 8: 3 3Airtill : 1.1 tCain ofCsttody Number -Client t)Ctertinred 2.1 QC Codes: N -Normal Satplc.TB

=Trip ltank. FD -Field Duplicate.

EB -Equipment Blank, MS -Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample. G -Grab. C -Composite 3.1 Field Filtered:

For liquid matrices, indicate with a -Y. Ior yes the sample was Iield liltered or -N -for sample was nut lield filtered.

" 4,) Matrix Codes: DW-Drinking Water. GW-Grotndwater.

SW=Surfacc Water, WW-Wasic Water. W=Waler. SO-Soil. SD-Stdim-nt.

SL-Sludge.

SS-Solid Waste. O=Oil. F=Filter.

PýWipe. U=Urina. F'Fccal. N-Nasal 5.1 Sample Analysis Requested:

Analytical etlbod requested (i.e. 8260B. 6010R/7470A) and nuomber ofcontaincrs provided 'or each (.e. 82601B .3, 6010&/74717A

-I),........................." x.c Atd C.l -Sodium Hydroxide, SA ý Sulfuric Acid. AA = Ascorbie Acid, IIX = Icxuane. ST = Sodiumt l'hioultatc.

Ifno preservative is added = leave field blank.... OINW = *"t .lVTNT For Lob Receiving Use Only Intact?I'rES ) NO"Coolev" Ternp: I -C

.. 61 ____n_ GEL Chain!lI NUIflDICg"t

\< , -b-GEL Work Order Number: Phon of Custody and Analytical.

Request GEL Laboratories.

LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1179 e #: -01f4- o Sample Analysis Requested (s) (Fill in the number of containers for each test)O~*ti-ample be'~¶,, ~,7 Sor~ CA. C~L\O5considered:

'~~~ ~~ K ~~Send Results o r\=~v.xO@

r.5i 4, a C 0 Li 0.0 0 0 I-.<-- Preservative Type (6)5 Sample ID*Date Collected (mm-dd-yy).rimse Callcoted (Military)(hhnsm)QC ('ode Ficld) Fj~ilered tat)Sample Matrix 9;5 0: Zj Comments Note: extra sample is required for sample.specific QC i or canttttoalfs

-indicate start and .sto q Lf ~ AAt p date/time 1 Ilt.dog iz lb A, S l-0r I I I.l~4.m1;I I 1 I[ vLl d'K4'L4,.2_ -_/_ _,._ _,.I-,- b -- ._.A_._7-1',- IH -.-_______, q, '--1 Z-3.

Fax Results: Yes Circlc Deliverable:CofA I Qd uma!X I Level I' I er/ eve m/ r kv /(IA: Are there any known hazards applicable to these samples? Ifso, please list the hazards Sample Collection TIMe Zon Eastern t Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details ,hed By (Signed)Date Time Received by (signed) Date Time GEL Pm: XrNc~a~e, Method of'Shioment:

ý- OF,/ Date Shinned: "'7 I I ~- : -'-- .'1 2 ~ ~ '~ Airbill #:___________________________

1___ 3 Airbill II: i ,;"Custody Number -Client I)etermne.d I , s N -Normal Sample..TB

-Trip Blank. FD -Field Duplicate.

ES -LEquipment Blank, MS Matrix Spike Sample. MSDO Matrix Spike Duplicate Sample. C -Grab, C -Composite yi .!i For liquid matrices, indicate with a -Y -for yes the sample wnas feld filtered or- N- oIr sample was not ietld filtered.:;.!+, , W-odca: nW=Drinking Water. GW-Groundwater.

SW=Surface Water. WWWastc Water. W-Water. SO-Soil. SO-Sediment, SL-Sludge.

SS=Solid Waste. O-Oil. F-Filter, P-Wipe, U-Urine, F-Fecal, N-Nasal* l ' ;-_Anayis Requested:

Analytical nmethod requested (i.e. 82608. 60OBn/7470A ) and numberorcontoincru pmvvided For each (i.e. 82600 .3. 60101117470A

-I).,tive IHA -Hydrochloric Acid. NI -Nitric Acid, SiH -Sodium Hydroxide, SA Sulfurie Acid. AA -Ascorhic Acid. HX -Hexanc, ST -Sodium Thlmulflate.

Irno preservative is added -leave field blank WHITE = LABORATORY YELLOW -FILE PINK = CLIENT For Lab Receiving Use OnlySeal Intact?I NO.Cooler Tempi: 'C Page: of GEL Laboratories, LLC tProiceth:

\rto1". GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote #: Charleston, SC 29407 COC Number It: GEL Work Order Number: Phone: (843) 556-8171 1P0 Number: b\umber: Fax: (843) 766-1178 ClientName: "Ii.. Phone #:1 Ir t- 3 Sample Analysis Requested (5) (Fill in the number of containers for each test.)Project/Site Name: a ldh <-- Preservative Type (6)0 a H % -541- k./g_________

Address: _ £ , ,, " t , -.considered:

-.-, Comments Collected by: ; , -.\, .Send Results To: r- Note: extra sample is E required for sample ttate Collected

.a ~Collected

=lp specific QC Sample ID , tal t',d< erd 13, <..* (Military) cre M m i x For couot rssiti.f -indicate start and stop date/time (mm-.dd-yy) (hhnam) _ _ ._,_.(bmm I I 4 -.3 -11 .5) ,-44'_ _ _ _ _ _ _ _ _ 1ii N/, X TAT Requested., Normal: ... Rush'._ S eei(:'$ lbcetloSo ,e) Pax Results. Y, / " 'rCircle Deliverable:

CofA / QC Lcvel 1 Lev 3 /Level Remarks: Are there any known hazdrds applicable to these samples? If so, please list the hazards 1aster n Eastern ct vm5 iei-e ACentral Other____Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Reteived by (signed) Date tinc GEL PM: -0"s .\ , e?/t d tot'hipmeat:

e- Date S#xi ied: 22 Airbill U 33 Airbill #: l.t (Chain of lCustody Number -Client Detcrmiined 2.1 QC Codes: N -Normal Swample. TB -Trip illank. FD = Field Duplicate.

ElB Equipment.

Blank. MS P Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample. G -Grab, C ý Composite 3.) Field Fillered )-or liquid matrices. with a -V -for yes the sample was field iltered or -N -tar sample was not field tiltered.4d. Matrix Cades: DW-Drining Water, GW-Gromtdwatcr.

SW-Surface Water. WW-Waste Water, W-Water. SO-Soil, SD-=Sedimenl.

SL-Sludgc.

SS=Solid Waste. O-Oil. F-Filter.

P-Wipe, U-Urinc, F=Fecal. N-Nasal 5.1 Santpte Atalysis Requested:

Analytical method requested (i.e. 8260B. 6010iB1747OA) and number aFcotmaincrs pruvided for each (i.e. 826011 -. 360101117470A

-I.' 1...... -... -Hydrochloric Acid, NI -Nitric Acid. SHi Sodium Hydroxide.

SA = Sullaric Acid. AA ý Ascorbic Acid, HX = ilexane. ST = Sodium Thiosuarate.

ls'no preservative is added = leave field blank V... lAw =' F1 'IlF PINK =CLIENT For Lab Receiving Use On(y" j Cooler Tempp: C or 1" .) 0 GEL Chain G(E I, Orde Nu: ber SL '].'\ it ~ l It: )(9" Work Order Number:.of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8 171 Fax: (843) 766-1178 Phone #: 916 -(,,.4- 306o Sample Analysis.

uested (s) (Fill in the number of containers for each test)Fax #: 4 IS -54 1 373-Should thi sample be considered: , k Lj_. COP ', Ur qLA I d 5 I. Vt,- lend Results To: 0 a 0 C U 0 a.0 2 0 0 C I-.Sample ID i or eotmpsites-indicate start and stop date/time Date Collected (mm,-dd.yy)

<-- Preservative Type (6)Collected (Military)(hbmm)oC *Timew Field Filtered *Sample Matrix I" U Ut I..I: C-Si Comments Note: extra sample is required for sample specific QC¶I N4 S t Y I I- I I V_ _ __ _~;~-:~.- L~3 p a,, 4 il hiIe A--- __ _ _LI/-7~ 1__ v ----_ _ __ _ _ _ _ _AM_ _ _ _ to -0j____ __ __ ___ __ _ ___L v W V-0 L-A _ ~-o \C. ._ __ _ _ _ _ _I11/I I.A (ciuested:

Normal: Rush: SpecifY4 S uo ritr ) Fax Results: Yes / Circle Deliverable:

Cao A / Lcvel-I / Level 3 / Level 4 Iitflhtl)A Are thare any known hazards applicable to these samples? Ifso, please list the hazards ISampile Tcatin TiJM.ZMn Eastern Pa cife Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details 1,ýizL,,hed By (Signed) Date Time Received by (signed) Date Time GEL PM:_________________________-6_

0 'Method orSltipment:

.Date Shipped: -71151 2. Airbill #: Cutody Number- Clitent l)ct ined For Lob Receiving Use Only i :1' t, N -Ntornal Sample. TB -Trip Blank. FD -Fied Duplicate.

Eu -U2qupmcnt lBlank, MS -Matrix Spike Sample. MSD Matrix Spike Duplicate Sample. G -Grab. C = Composite lJ[';itcrcd:

For liquid matrices.

indicate with a -Y -for yes the sample was field filtered or -N -for sample was not field filtered.

CltsjodjzSeal Ihtoct?i odes: DW=Drinking Water. GW-Gmundwater.

SW-Surface Water. WW-Wastc Water. W-Water. SO-Soil, SD[Sediment, SL-Sludgc.

SS-Solid Waste. -OiL F.1 lilter. P-Wipe. U-Urine, F-Fecal. N-Nosal (.f&.S NO.:,,o,;,i,:

AalysisRequested:

Analytical method requested (i.e. 826GB. 6010V7Bf470A) and numberofcorntainers provided for each (i.. 8260 3. 3,601087470A

.1). Cooler Temp., tve Type: HA- Ilydrochlnric Acid. 1t -Nitric Acid. SH Sodium IHydroxide.

SA = Sulturic Acid. AA =Ascorbic Acid. 1IX -lexuan. STr- Sodium Thiosultate.

Ifno preservative is added -leave tictd blank C WHITE = LABORATORY YELLOW -FILE '- PINK = CLIENT -I Page: of GEL Laboratories, LLC Project : N\0\ -GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote 9: _ Charleston, SC 29407 COC Number :GEL Work Order Number: Phone: (843) 556-8171 P0 Number: 0 -Fax: (843) 766-1178 Client Name: " .Phone : ~.~3~ 00 Sample Analysis Requested (5) (Fill in the number of containers for each test)Paojectedbye an- , Preservative Type (6)b N Address: 1 0r,\\ aadrd C Comments Collected by: 'x\7Send Reul s To.(V Note: extra sample isrequired for sample Sample ID tspecific QC For composites

-indicate start and stop date/lime (mni-dd-yy)

C lc dt( e...n, J3-1Lk ~ I --,' 5 o Q'64 3 \13 q. 5x ....5_13$- --41. Sf q n," 1 G-q'- h -I V WU r3 -4~,5 0414D_ __ __TAT Reuested:

Normal: Rush: bL SpecSf:t~f.-sabjcc, sarehur "i axResults:

Yes .Circle Deliverable:

CofA A QCSuinmmary

'fLvel/"1 Level 3 / Level 4" Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Sample Collection Time Zone IEastern Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Received by (signed) Date Time GEL PM. -3 ITi #ethodof~hipmen:

Dat S e 2 13 _ _ _ _ _ _ _ _ __ ___ __ ___ __1.1 (lOtJn It 'Cstoddy -Client I)ecrfinaed 2i QOC Codes: N -Normal Sample. TB -Trip plank. FD -Field Duplicate.

EB -Equipment ilank, MS -Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample. G = Grab, C Composite 3.) Field Filtered:

For liquid matrices, indicate With a -Y -Imr yes tlh sample was field filtered or -N -for sample was not field filtered.4.) Matrix Codes: DW-Drinking Water. GW=Groundsvaler.

SW=Surfaee Waler. WW-Waste Water. W-Waler. SO-Soil. SD-Sediment.

SL=Slodge.

SS=Solid Waste. O=Oil. F'Filter.

P-Wipe. U=Urinc. F-Fecal, N-Nasal 5.1 Sample Analysis Requested; Analytical method requested (i.e. 82601, 6010B/7470A) and nuniber orconltiners provided lir each (I.e. 8260B -3, 6010817470A

-1).6.) preservative Type: HA -IHydrochloric Acid. NI -Nitric Acid. SHt -Sodium Hydroxide, SA -Sullfric Acid. AA Ascorbic Acid. IIX Hlcxane, ST = Sodium lhisulfarc, lWo preservative is added = leave field blank WHITE = LABORATORY YELLOW = FILE PINK =CLIENT For Lab Receiving Use Ol)y C Seal Intact?.YES NO.ooler Temp.C

,, \I GEL Chain.: !h ; l GEL Work Order Number: ('Kij:l,, > ine: ¶ 4... Phon-~ J'~h ~ ~Fax #i of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleslon, SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178 e #: _;O000 I Sample Analysis Requested (sl (Fill in the number of containers for each test)I: -1 Ský 'w Should this sample be I I ~( ~ ~ 5 ~~ ~considered t\t% Send Results To: xl a as 0 U C E a (5 0 I-Sample ID iat contpositei

-indicate aart and stop daleltime<-- Preservative Type (6)*Date Collected (mm.dd-yy)"Tii ic Collected (Military)(hhmm)QC C.ode Field Sample"It Filtered 1i1 Matrix "'.t ax 1-0.I-.Comments Note: extra sample is required for sample specific QC J~:tw C, AV 4 4 -____________________

1%6 I_ _ _ __o _ __ '_ F " i _,_,/_ __ _...._._.

.... r ._(.01Mt t , C2 I I-.t---t-------1

)cl.,,,,,.,/.d,, I A 7.....,' e .,ve 1: ýi iuested: Normal: Rush: 1 C. SP at:\s'~ibjct to Suretatrc Px Results., Yes I Circle Deliverable:

C of A QC Summary I Lve~l /'Are there Ofny known hazards applicable 4o these samples? If so, please list the hazards Ilmoe Qel3/n TI e Z.Central Other ____....._ _ _ _ _ _ _ _ _ _ Mountain Chain of Custody Signatures Sample Shipping and Delivery Details-he;:ihcd By (Signed) Date Time " Received by (signed) Dae ' Time GEL PM:-tL Wo \1y'zk, 24% Method of Shipment:

--Date'Sh:'pd:

'71610l4 2 Airbill #: 13 Airbill #: L; .r,;:. , 'Cetody Number -Client Dclteroincd iL, : ,iss: N -Normal Sample.'TB

=Trip Blank. FD -Field Duplicate.

EB -ENuipmcan Blank, MS -Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample. G -Grab, C -Composite I I I ;;tcrod: For liquid matrices, indicate with a -Y -Ior yes the sample was field filtered or -N -for sample was not field fillteed.(:odes: OW-Drinking Water. GW=Oroundwater.

SW-Surfacc Water. WW-Wste Water. W-Water. SO-Soil. SD-Sediment, SLSltalge.

SS=Solid Waste. O-OiL F-Fiter. PoWipe, U-Urine. F-Fecal, NKNasal , , Analysis Requested:

Analytical method requested (i.e. 8260B,60108f7470A) and nutber ol'coataincrs provided forcach (i.e. 826011 -3, 60100l7470A -I).,tive Type: ISA -tilydrochlnric.Acid.

NI -Nitric Acid. SH -Sodium Hydroxide, SA -Sulfuric Acid. AA -Ascorbic Acid, HX -tIcxanc, ST- Sodium Thiuosullac, Il'no preservative is added -lease feld blank WHITE = LABORATORY YELLOW = FILE ' PINK = CLIENT I For Lab Receiving Use Only 5 Seal Intact?S NO Cooler Temp: C Laboratories LLC SAMPLE RECEIPT & REVIEW FORM Client: SDG/ARCOCWork Order-' ' .ReceivedBy:

D ae e ev 7- .I ea SmpetedHazrd iforatin ~Couts>x2 area backkru oji samples not marked "radioactive", contact ,__ _,,_ _ _ _ E the Radiation Safety Group of furtlter investigation.

COC/Samples marked as radioactive?

7 -Maximum Counts Observed*:

Classified Radioactive 19 by RSO? " " COCISamples marked containing PCBs? ,_ .....__ _" Shipped as a DOT Hazardous?

'azard Class Shipped: UN#:-Samples identified as Foreign Soil? i __" Sample Receipt Criteria .Comments/Qnalifiers (Required for Non-Conforming Items)Circde Applicable.

Shipping containers received intact and seals broken damaged lcenaine laking container othe (describe) sealed?Pirnysatn Method: Samples requiring cold preservation " blue ice dry ice nond other (describe) 2 within (4 +/- 2 C)?3 Chain of custody documents included with shipment?"Cirele Applicable:

4 Sample containers intact and sealed? ase broken damaged container leaking container other (describe) 5 Samples requiring chemical SSr~ ~,cnanr fetdadd vdP preservation at proper pH? If Preservation added, Lott.VOA vials free of beadspace'(defimed as% Sample ID's and container affected:< 6mm bubble)?,yes, imdately deliver to Volatil.s laboratory) 7 Are Encore containers present?ld's and tests affected 8 Samples received within'holding tihm?sa...le 's e and containers affected: 9 Sample IDls on COC match ID'son J bottles?Date & time on COC match date & time Sample ID% affected:" on bottles?1 Number of containers received match Sampe s- IU's affete: &.,-'.number indlcated on COC? c. e .'c-_r.f-" .,e- , 12 COC form i properly signed in relinquished/received sections?Com nts: PM (or PMA) review: Initials /t Date 1 1 Io SAMPLE RECEIPT & REVIEW FORM CONTINUATION FORM Cfient:- 1cZ& Date.Received:

Page of__:l-qs- o{,5- 3 J. (ociq O c-(-.

List of current GEL Certifications as of 25 July 2008 State Certification Arizona AZ0668 Arkansas 88-0651 CLIA 42D0904046 California

-NELAP 0115]CA Colorado GEL Connecticut PH-0169 Dept. of Navy NFESC 413 EPA Region 5 WG-15J Florida -NELAP E87156 Georgia E87156 (FIJNELAP)

Georgia DW 967.Hawaii N/A ISO 17025 2567.01 Idaho SCO0012 Illinois -NELAP 200029 Indiana C-SC-0 I Kansas -NELAP E-10332 Kentucky 90129 Louisiana

-NELAP 03046 Maryland 270 Massachusetts M-SC012 Nevada SCO0012 New Jersey -NELAP SC002 New Mexico FL NELAP E87156 New York -NELAP -11501 North Carolina 233 North Carolina DW 45709 Oklahoma 9904 Pennsylvania

-NELAP 68-00485 South Carolina 10120001/10120002 Tennessee TN 02934 Texas -NELAP T104704235-07B-TX U.S. Dept. of Agriculture S-52597 Utah -NELAP GEL Vermont VT87156 Virginia 00151 Washington C1641 iLaboratories LLC a member of The GEL Group INC P0 Box 30712 Charleston, SC 29417 2040 Savage Road Charleston.

SC 29407 P 843.556.8171 F 843.766.1178 July 30, 2008 www.gel.com Mr. Moises Carvalho TRC Solutions, Inc.55 2nd Street, Suite 575 San Francisco, California 94105 Re: Humboldt Bay NPP Project 161072, Task 2400 Work Order: 212150

Dear Mr. Carvalho:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on July 17, 2008. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction.

If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.Sincerely, Erin Stanley Project Manager Purchase Order: 161072 Enclosures

(

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report for TRCS002 TRC Solutions Client SDG: 212150 GEL Work Order: 212150 The Qualifiers in this report are defined as follows:* A quality control analyte recovery is outside of specified acceptance criteria** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.The designation ND, if present, appears in the result column when the analyte concentration is not detected above the detection limit.This data report has been prepared and reviewed in accordance wvith GEL Laboratories LLC standard operating procedures.

Please direct any questions to your Project Manager, Erin Stanley.Reviewed by GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (Company: TRC Solutions, Inc.Address: 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-2-1.0 Gamma Project: TRCS00200 Sample ID: 212150006 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 13:50 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Ganmna, Solid "Dry Weight Corrected" Cesium-137 U 0.0259 +/-0.0261 0.0499 0.100 pCi/g MJHI 07/24/08 1330 775737 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-2-4.0 Gamma Project: TRCS00200 Sample ID: 212150007 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 14:20 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0185 +/-0.0244 0.0431 0.100 pCi/g MIHi 07/24/08 1331 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis C Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-2-7.0 Gamma Project: TRCS00200 Sample ID: 212150008 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 14:30 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0123 +/-0.0333

.0.0591 0.100 pCi/g MJHI 07/24/08 1332 775737 1 The following Prep Methods were performed Method Description Analyst Date .Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

B-6-1.0 Gamma 212150009 Soil 15-JUL-08 15:15 17-JUL-08 Client Proiect: TRCS00200 Client ID: TRCS002 Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho(Rad Gamma Spec Analysis Gamninaspec, Gamma, Solid "Diy Weight Corrected" Cesium-137 U -0.00926 +J-0.0266 0.0449 0.100 pCilg MJHl1 07/24/08 1508 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep. Batch Dry Soil Prep Dry Soil PrepGL-RAD-A-021 BSWI 07/J18108 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5,2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com (Certificate of Analysis Company: TRC Solutions, Inc.Address: 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-6-4.0 Gamma Project: TRCS00200 Sample ID: 212150010 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 15:20 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137.

U -0.0163 +/-0.0414 0.0682 0.100 pCi/g MJHI 07/25/08 0802 775737 1 The following Prep Methods were performed C Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-AL021 BSWI 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments I EEML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corn Certificate of Analysis.....................

,.3 7---Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-6-7.0 Gamma Project: TRCS00200 Sample ID: 212150011 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 15:35 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Methoo Rad Gamma Spec Analysis Gamninaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00589 +1-0.0511 0.0834 0.100 pCi/g MJHI 07/25/08 0857 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-02]

BSWI 07/18/08 1226 775220.The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (I Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-I 1-1.0 Gamma Project: TRCS00200 Sample ID: 212150012 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 16: 10 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid 'Dry Weight Corrected" Cesium-137 U -0.00164 +/-0.0178 0.030 0.100 pCi/g MJHI 07/25/08 0858 775737.I The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address: 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B- 11-4:0 Gamma Proiect: TRCS00200 Sample ID: 212150013 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 16:20 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Ganimaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00639 +/-0.0345 0.0589 0.100 pCi/g MJ'HI 07/25/08 0858 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/18/08 1226 775220.The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (*..Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-1 1-7.0 Gamma Project: TRCS00200 Sample ID: 212150014 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 16:55 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.049 +/-0.0631 0.112 0.100 pCi/g MJH1 07/26/08 0614 775737 1 (The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis[Company: TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-4-1.0 Gamma Project: TRCS00200 Sample ID: 212150015 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 07:50 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "D'y Weight Corrected" Cesium-137 U -0.00459 : +/-0.0529 0.0865 0.100 pCi/g MJHI 07/25/08 1001 775737 .1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-4-4.0 Gamma Project: TRCS00200 Sample ID: 212150016 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 08:10 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0104 +/-0.036 0.062 0.100 pCi/g MJHl 07/26/08 0614 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300,4.5.2.3

(

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: PS-06C-0.5 Gamma Project: TRCS00200 Sample ID: 212150017 Client ID: TRCS002.Matrix: Soil Collect Date: 16-JUL-08 08:40 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Ganiniaspec, Gamma, Solid "Diy Weight Corrected" Cesium-137 U 0.0195 +/-0.0262 0.049 0.100 pCi/g MJlI 07/26/08 0615 775737 1 The following Prep Methods wvere performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 (.Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: PS-06C-2.0 Gamma Project: TRCS00200 SampleID:

212150018 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 08:50 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Ganimaspec, Ganinia, Solid "Dry Weight Corrected" Cesium-137 U 0.00529 +/-0.023 0.0395 0.100 pCi/g MJHI 07/26/08 0616 775737 1 The following Prep Methods were performed

.Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: PS-06C-6.5 Garmna Project: TRCS00200 Sample ID: 212150019 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 09:20 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gamniaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00126 +/-0.0394 0.0667 0.100 pCi/g MJ-H-1 07/26/08 0902 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSW] 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corfi Certificate of Analysis Company: TRC Solutions, Inc, Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-12-1.0 Gamma Proiect: TRCS00200 Sample ID: 212150020 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 10:00 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gannmaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 0.0962 +/-0.0609 0.0507 0.100 pCi/g MIHI 07/26/08 0903 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSW1 07/18/08 1226 775220 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (

GEL'LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-12-4.0 Gamma Project: TRCS00200 Sample ID: 2121.50021 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 10: 15 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Methoi Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Diy Weight Corrected" Cesium-137 U 0.0108 +/-0.0347 0.0577 0.100 pCi/g MJHI 07/26/08 0903 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep DrySoil Prep GL-RAD-A-021 CXCI 07/18/08 1310 7175221 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis C Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072,Task 2400 Report Date: July 30, 2008 Client Sample ID: B-32-1.0 Gamma Proiect: TRCS00200 Sample 1D: 212150022 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 10:40 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method.Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.031 +/-0.0309 0.060 0.100 pCi/g MJHI 07/26/08 0904 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 C GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corn Certificate of Analysis Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvaiho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-32-4.0 Gamma Project: TRCS00200 Sample ID: 212150023 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 11:00 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho Rad Gamma Spec Analysis Gammaspec, Gainma, Solid "Dry Weight Corrected" Cesium-137.

U 0.0137 +/-0.0259 0.0451 0.100 pCi/g MJH1 07/26/08 0905 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: thumboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-32-8.0 Gamma Proiect: TRCS00200 Sample ID: 212150024 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 11:40 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0174 +/-0.0294 0.0479 0.100 pCi/g MJH1 07/26/08 0905 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300; 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of.Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: PS-02C-0:3 Gamma Project: TRCS00200 Sample ID: 212150025 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 10:20 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho Rad Gamma Spec Analysis Ga7mmaspec, Gamma, Solid "Diy Weight Corrected" Cesium-]37 U, 0.00702 +/-0.0422 0.0727 0.100 pCi/g MJHI 07/26/08 1120 775737 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: PS-02C-4.5 Gamma Project: TRCS00200 Sample ID: 212150026 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 10:45, Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gamniaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 9.82E-06 +/-0.0299 0.0505 0.100 .pCi/g MJHI 07/24/08 1031 775746 1 The following Prep Methods were performed

(.Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: PS-02C-7.5 Gamma Project: TRCS00200 Sample ID: 212150027 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 11:00 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho Rad Gamma Spec Analysis Gommaspec, Gamma, Solid "Diy Weight Corrected" Cesium-137 U -0.0174 .+/-0.0442 0.0697 0.100 pCifg MJHI 07/24/08 1032 775746 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC] 07/1 V08 1310 77522]The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www gel.com Certificate of Analysis (Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-5-0.5 Gamma Project: TRCS00200 Sample ID: 212150028 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 14:20 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0,0126 +/-0.0177 0.0337 0.100 pCi/g MJHI 07/24/08 1043 775746 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 C-,

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis.....................

r Company: TRC Solutions, Inc.Address :. 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-5-4.5 Gamma Proiect: TRCS00200 Sample ID: 212150029 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 15:45 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Methoi Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0196 +/-0.0432 0.0772 0.100 pCilg MJHI 07/24/08 1043 775746 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/18108 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3

.i GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-1-0.5 Gamma Proiect: TRCS00200 Sample ID: 212150030 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 16:25 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 0.200 +/-0.0772 0.0553 0.100 pCi/g MJHI 07/24/08 1048 775746 1 The following Prep Methods were performed (Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments'EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-1-4.5 Gamma Project: TRCS00200 Sample ID: 212150031 Client ID: TRCS002 Matrix: Soil Collect Date: 15-JUL-08 16:40 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammospec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00513 +/-0.0374 0.0625 0.100 pCi/g MJI1 07/24/08 1055 775746 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (.Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-10-0.5 Gamma Project: TRCS00200 Sample ID: 212150032 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 08:00 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0104 +/-0.0234 0.0413 0.100 pCi/g MJHI 07/24/08 1056 775746 1 The following Prep Methods were performed (Method Description Analyst Date -Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 (.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-10-4.5 Gamma Proiect: TRCS00200 Sample ID: 212150033 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JIUL-08-09:05 Receive Date: 17-J1UL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Methoc Rad Gamma Spec Analysis Gamimaspec, Gamnmta, Solid "Dry Weight Corrected" Cesium-137 U -0.0147 +/-0:0371 0.0575 0.100 pCi/g MIH1 07/24/08 1110 775746 t The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 30, 2008 Client Sample ID: B-8-0.5 Gamma Proiect: TRCS00200 Sample ID: 212150034 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 09:30 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result. Uncertainty DL' RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 0.116 +/-0.0461 0.0444 0.100 pCi/g MJHI 07/24/08 1111 775746 I (The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-8-4.5 Gamma Proiect: TRCSOO200 Sample ID: 212150035 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 09:50 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesiurn-137 0.175 +/-0.0753 0.0602 0.100 pCi/g MuHI 07/24/08 1126 775746 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3

.GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corn Certificate of Analysis I Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-18-0.5 Gamma Proiect: TRCS00200 Sample ID: 212150036 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 10:47 Receive Date: 17-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gaminaspec, Gamina, Solid "Dry Weight Corrected" Cesium-137 U 0.0123 +/-0.0203 0.0376 0.100 pCi/g MJ-HI 07/24/08 1201 775746 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments 1 EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California.

94105 Report Date: July 30, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

B-18-4.5 Gamma 212150037 Soil 16-JUL-08 11:05 17-JUL-08 (-l; f'Project: TRCS00200 Client ID: TRCS002 Parameter Qualifier Result Uncertainty DL RL Units DF .AnalystDate Time Batch.Method Rad Gamma Spec Analysis Gantmaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137.

U -0.0132 +/-0.0313 0.0509 0.100 pCilg MJH1 07/24/08 1219 775746 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/18/08 1310 775221 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com (QC Summary TRC Solutions, Inc.55 2nd Street, Suite 575 San Francisco, California Contact: Mr. Moises Carvalho Workorder:

212150 Renort Date: July 30, 2008 Page 1 of 2 Parmname Rad Gamma Spec Batch 775737 QC1201625032 212150006 DUP Cesium-137 QC1201625033 LCS Americium-241 Cesium-137 NOM Sample Qual QC Units RPD% REC% Range AnIst Date Time U 0.0259+/-0.0261 U -0.000777+/-0.0214 15.9 6.02 7.85 13.9+/-1.67 5.82+/-0.410 7.63+/-0.687 pCi/g pCi/g pCi/g pCi/g pCi/g 212 N/A MlHI" 07/26/08 11:21 87 (75%-125%)

97 (75%-125%)

97 (75%-125%)

07/26/08 11:22 Cobalt-60 QC1201625031 MB Cesium-137 Batch 775746 QC1201625057 212150026 DUP Cesium- 137 QC1201625058 LCS Americium-241 Cesium-137 U 0.0138+/-0.0192 U 0.0217+/-0.0361 07/26/08 11:21 N/A MJHI 07/24/08 13:02 U 9.82E-06+/-0.0299 pCi/g 200 15.9 6.02 7.85 13.3+-1. 11 5.88+1-0.451 7.72+/-0.576 pCi/g pCi/g pCi/g pCi/g 84 (75%-125%)

98 (75%-125%)

98 (75%-125%)

07/24/08 13:02 Cobalt-60 QC1201625056 MB Cesium-137 U 0.00132+/-0.0125 07/24/08 12:20 Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-c6ndensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD. Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded C GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

212150 Page 2 of 2 Parmna J N/A ND NJ R U U'S x Y h rue NOM Sample Qual QC Units RPD% REC% Range AnIst Date Tit me Value is estimated M if above MDC and less than LLD RPD or %Recovery limits do not apply.Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.

Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more." The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/- the RL is used to evaluate the DUP result.* Indicates that a Quality Control parameter was not within specifications.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

_______"_

of GEL Laboratories, LLC___,______,___________

GEL Chain of Custody and Analytical Request 2040 Savage Road, ;.Charleston, SC 29407 GEL WokOdr ubr Phone: (843) 556-8171-GEL2WorkOrderaNumber:

1,4 I.l t.-t , 5~/9 [ Fax: (843) 766-1178 Phone 9: 1'\"c3 ý -Sample Analysis Requested tat (Fill in the number of containers for each test)Aarne: Fax P: '-\\Cý -5L\N -Cý37_6 Should this sample be A '> , .considered:

Send Results To: _-\1,o @ o ,.a in a 0 5, 0 I-a in 0 I--6 1.-I-p p-2 4'<-. Preservative Type (6)I. -I- P -t~------

I~ -I C.Sample ID composites

-indicate start and stop daieltime\ mL-k VC Dlate Collected (ms-dd-yy)

• Time Collected (Mlitatry)(Ihmmu)QC ticl Field Sample) Fihernt '1 MalMatrix Z W S Comments Note: extra sample is required for sample specific QC-~ + 4--~-+ I-+--P--~--~-4-~-+-4--4--4-6-1.--- G'V-~ -r I,-4-- -4/I 0l J~-K 3-1 1.[ l t I\L_ -7.0 -_ _ _ _ _ _-\0 V131111~E 1.___-YJ/ jt 4, I A-- -.---- -a.......,........................a4aL 1 a16aa Vuo /ec Fax.29..IliAII flUODI Its: " "'.C*u * ~ , ,. ,...m ,s, ,v 8i'inur,'s:

• 4re there any known hazards applicable to those samples? If so, please list the hazards SnMtMle calliction Tlrn ZoM Eastern P4 Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details*.A*i y ISigned)S -P Date Time Recciv d y (snd) Date Timte GEL PMV: t\\-P r v Method olShipment:

" YDate Shipped: -7/16 u/12 JAirbillU 3 Airbill #:..Number- Client lDe-enntncd

., NtNomatSamlple.

TB =Trip lank. FD -Field Duplicate.

EB -Equipment ilank. MS Matrix.Spike Sample. MSD =Matrix Spike DuplicateSample.

G=Grah, C=CompcaPsite

.,;,. I: For liquid matrices, indicate with a -V -for yes the sample was field tilttcrd or -N -tftr sample was not rtc1d ilttered.,, s: DW-Drinking Water. GW-Groundwatcr.

SW=Surface Water, WW-Wastc Watcr. W-Water. SO-Soil. SD-Sediment.

SL=Sludgc.

SS=Solid Waste. O-Oil, F=Filter.

P-Wipc. U-Urin.e F-Fecal. N-Nasal , ysis Requested:

Analytical method requested (lie. 82601. 60l0B//4'a70A) and nuntber oftonlaincrs provided for each (i~e. 82603 .3.6010017470A I).i, .. Type: 1A -tydrochloric Acid. NI -Nitric Acid. SUt -Sodium Hydroxide.

SA -Sullaric Acid. AA -Ascttbic Acid. nX -I .cxant. ST -Sodium Thiosullatc.

Wfno preservative is added -leave ictd blank WHITE = LABORATORY YELLOW = FILE PINK=CLIENT For Lab Receiving Use Only Custody Seal Intact?YES NO C

'age: -. -or GEL Laboratorics, LLC ,rcjot6: GEL Chain of Custody and Analytical Request 2040Savage Road 3EL Quote (-: Charleston, SC 29407:OC Number it: GELWorkOrderNumber__Phone:

(843) 556-8171'0 Nmber \~ 1 ~GEL Work Order Number: 110 Number: \6 _1 Fax: (843) 766-1 ) 78 Cliet Name: Phone #: AS -a Sample Analysis Requested s (Fill in the number of containers for each test)Pro ect/Site Name: Fax h: L-t 5 LI I -'b Should this ' <-- Preservative Type (6)Samiiplebe Ms ----Address:t~

N\S¶$'v A~~Zt consitdered: (A iComments Collected by: Send Res s To: V Note: extra sample is*ttteCotete nte! required for Sample* Date Collected C "Z a 7 SClmcted CDCod Htetd Sampte specific QC Sample ID (Military)

(1 't ittered Matrix" etFor cotmtposieetei

-indicate 1rt anrd slop date/ltime tid h)htsmi,)'I '~-~~~-\.o

-2) 1c) I I'f~-'~--Vc~

C~N~r~ ___I\~SOLLLi~ivIi1ILIi~LLitiIIt_____________-b -\_ _-. -/ ?- K ....... ..ý- -Vo ,,,.1 TAT Requested:

Nontal: Rush: SpeCify:ýA (Sujct to SuchurpeT Fax Result: Yes ICircle Deliverable:

C of A //C Summary L vel I Level 3 / Level 4 Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Sample Collection Time Zone_ Eastern 2 p~ ~" "\~3:~ ~\~~%J/Central Other___Mountain Chain of Custody Signat es Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Receiv y (signed) Date Time GEL PM: S A('Atr )F- .\.\I Z"zb 7 & 9. K:N Method of hj snti: ea Dot Ssi ecd 7 2 Airbill #: 33 WihtlI:___________________

1.( Chain ur Custody Ntnber Client Detcnttincd 2.l)1Q Codecs: N -Nonnal Sample. TB -Trip Blank. Fo -Field Ouplicate, ElR t='touipotent t3ank. MS -Matrix Spike Sample. tsn = Matrix Spike Duplicate Sample. G Grab, C = Composite 1 FiHeld Filtered; For liquid matrices, indicate with a -V -for yes the sample was tield titcrcd or -N -for somple was not field fittered.,.l Matrix Codes: DW=Drinking Water. GW-Groundwater, SW=Surraee Water. WW-Wate Water. We-ater. SOoSoil. SD-Sediment.

SLoSudge.

SS=Solid Waste. O=Oil. FFilter, P-Wipe. U-Urine, F=Fecal, N-Nasal 5.1 Sample Analysis Requested:

Analytical method requested (i.e. 8260B. 60o1tsar475A) and number olcontainers provided [or cach (i.e. 82603 -3.60110B/74704

-I)..- '. xi141 S-odium Itydroxide, SA = Sulltric Acid. AA , Ascorbic Acid. iIX t tcxune. ST = Sodium Thiosulfic,-tetno preservative is added -leave field blank I,'r,,. l I I¢o Custody Seal Intact?YES NO Co Teirrp: C

_____of\61 01 GEL Chain GEL Work Order Number:_ :J,,:i,. 1 (.1 011ýof Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-817l Fax: (843) 766-I178~ý jiclý: Phone f: ii -(fO, -. 30 0 Sample Analysis Requested

() (Fill in the number of containers for each test)-are: ,, (. o,\\~, Send Sample ID I cntttlSilte

-indicate start and slop date/time Fax 1: L(4 itr~ cu~c~eCoA e~l~Should this campei be considered:

Results To.:\- r ý 1 L'a a St a 0 C.0 a a C I-.I -r r r r<-- Preservative Type (6)*Date Collected (mm-dd-yy)

• Timc Collected (Military)QC to Field Sample Filtcred Matrix i i 3.U I-I, pC.-ft Comments Note: extra sample is required for sample specific QC~K\~-ThO G lPff\o IIV A-- --T _ $ _ __ _ _ _C)' ._ _ ___ _ _ _ _ _ __ ~ __ _ ____ ___0~A\-.o ~_ _ ____ __%____ ____ ____ 7h &:'k__ _7ý' _Lý_.Vo j ,llILJa1 k7116 4ý I 15U 111 J, 41Y I I ~Fax i i. uested; Normal: Rush: Y SPCly4 ýr (SubSj'cct 'rFfx Results: Yes /,:marh s: Are there any known hazards applicable to these samples? If so, please list the hazards Circle Deliverable:

C of A / QC Summary / Level I / K2 / Level 3 / Level 4 I I I 1 m I I1 I m II Satntle Collection Time Eastern .m~Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Detailsýcl ,;,ished By (Signed) Date Time Received by (signed) Date Tint C GEL PM: F %it\ C$i-rA. !:: MVethod of Shienment:

'+ ", I Date ShirsnecF 7/I~,Irf~_+'__ ..Z-'.'-7_711bk-ý q oo Method ol'Shininent:

C-CA-,K IDateShin ed: -7 // 6, / r-f), r 2 Airbill #:_.._ __...... .. _ _ 13 Airbitl 9: t; o,;: 'oisntody Number -Client D)etermined ,t ,dcs: N N Noml Sample. TB -Trip Ilank. FD -Field Duplicate.

El = lquipment Blank, MS -Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample. G = Gral. C = Composite.. Filtered:

For liquid matrices, indicate with a -Y -for yes the sample was field filtered or -N -ror sample was not field fti-ered.,.nx Codes: DW-Drinking Water. CW-Gt'oundwater.

SW-Surfacc Water. WW=Waste Water. W-Water. SO-Soil. SD-Sediment.

SS-Solid Waste. OOil, F-Filter.

P-Wipe. U-Urinc. FFat.al, N-Naal-, ic Anal .utacted:

Analytical method requested (i.e. 8260B. 601OB17470A) and anmbikrofcontainers provided for each (i.e. 26178 -3,60108/7470A

.I .-vativei tlA -Hydrochloric Acid. NI = Nitric Acid. SH -Sodium Hydroxide.

SA -Sulfuric Acid. AA = Aseorbic Acid. HIX -Hc- ' Sodium Thiaulltc.

If no preservative is added -leave Ileld blank-YELLOW = FILE PINK =CLIENT I For Lab Receiving Use Only Custoy seal Intact?YES ' NO CoI Temp.C age: __of 5 GEL Laboratories, L.C oiject 8: , o GEL Chain of Custody and Analytical Request 20,0 Savage Road iEL Quote 8: Charleston, SC 29407 ,OC Number GEL Wor: Order Number: Phone: (843) 556-8171'0 Num eber: er:__Fax:

(843) 766-1178-lient Name: Phionelt:

1-l. I 34 43o Sample Analysis Requested (Fill in the numrber of containers for each test)Project/Site Name: Fax #: _ q -Should .<s- Preservative Type (6)samptlse be Address: contsidtered:

bs~~~. .0ý 6Y k h 0 ,Comlments Collected by: Send Results To: +/- Note: extra sample is*Iat nColketed

.--3 r : required for sample*Dae Clleted Collected QC Codtae Field Sample ccseifcQ Scample specific QC a e D( ndd-yy) (M iltary) " ... iltred M Mtri "', rot ¢ontlaxitc$.

indicate start and stop da-(herta;)

I I-. I____ ___- __ ___ 6 /VA .Al 2 * ), _i L5-oL,.-0

.,t K .w _ -7"-____-__

ý 5-nL,- -.o I TAT Requedted!

Normal! -Rush: X Speel,: ,, t t.(Sbolutl, iFAXrtcxuit!

Ye / on Ch'eleDeiverable:

C of A / QC Summary / Lel( I./ c / Levl 3 / Level 4 Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Sample Collcrlion Time Zone[Eastern ý(&VI Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Received by (si ned) Date Time GEL PM: SFUcs &'S\ L-, Mý,Iehodeof Shipiment:

ri. 4Y- ~ Date Shipped: 7f(2 Airbill 'I: 3 3 Airbill It: i.) chain oc'u.stody Numtshr = Client Detentnined 2.) Ox: Codes: N = Ntrmal Sarnple.TB

= Trip Ilank. FD -Field Duplicate.

EB -Equipment Blank, MS -Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample. G -Grah. C -Composite 3. Field Fillered:

For liquid matrices, indicate with .-V -for yes lhe sample was field Iillered ori- N -for sjanple was not field liltered.4.) Matrix Cotdls: OW-Drinking Water. GW-Groundwracr.

SW-Surfacc Water. WW-Wastc Water, W-Water. SO-Soil. SD-Sedinrent.

SLiSludge.

SS-Solid Waste. OOil. F=Filter.

PWipe. U-Urine, F-Fecal, N-Ntsal 5.) Samiple AnalysiS Requested:

Analytical method requested (i.e. 82600. 60tu10,7470A) and number ol'contairers provided Ibr each (i.e. 82608- .3. 6010B17470A -I1).&t I n,',vt"ivelpe:

IIA -Hydrochloric Acid. NI =Nitric Acid, Sit -Sodium Hydroxide.

SA -Sulfuric Acid. AA = Ascorbic Acid. lIX -Ilcxanc. ST -Smliunt Throsulfatc.

Iron preservative is added -leave licid blank.. ....a.ItI PNT For Lab Receiving Use Only Custody Seal Intact?YES NO rTemp: egC

_of ,,,, ,_GEL Chain" GEL Work Order Number: of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178 Phone #: L ,.t , t Sample Analysis Requested s (Fill in the number of containers for each test)4.'~Fax III: Should this sample be I ~ ~4 ~ ~ ~ Str~ C. ~ considered K.. ~~~~~~Send ReSLults To: rck 0 Qiaur. JI: 0)a Sample ID Sit- mposites -indicate start and stop date/time<-- Preservative Type (6)-1-1* -..1- 14 ----,* Dale Collected (mm-dd.yy)

• Tirne Collected (Military)(htssm)QC Code Field Sample c Filtered o Matrix '><.Za$'If ,I,'/Comments Note: extra sample is required for sample specific QC L;____________________

7 /161_ <A2- 5t-I IVA .I 2~ 1 1 1 1 _______1*!____________

---

iIitit________

~- ~ 1-2 I\~4~o Fi2TI11rWv~t I~1 lit ___________

)~\\WOw I 2j~~~~.K $. _ _\__ _____________ -W- 40 E I__ _ _-C I I-" 4'l...o l I It Rlt ies 1 C Vs- _11610 0,- wo G.-Rsh sjeclry,,tlhd (Norjah tourhm ) kax'Results:

I Yes I_. circle Deliverable:

Cof A I QCSmmr Lcvel I Level 3 Level 4 i!ý,cnrks.:

Are thora any known hazards applicable to these samples? If so, please list the hazards Eastern k Central Other Mountain Chain of Custody Signatures

.Sample Shipping and Delivery Details k .2By (Signed) Date Time Received by (sined) Date Time GEL PM: £~r Slr~'of Shinment:

e.I flat..5 lsinnevt.

'7 IlL1r',~ýjýIlbfas eoZ-7-1 v-?\3,00 co"?Wý- elhod of Shipment: 12 IDateShied:

71100.lAirbill 4: St, s, u 'tody Number ('tieat t)einnined Nost 3,t No lSample.TB -trip Blank. FD =Field Duplicate, EB -Equipment Blank. MS -Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample. G Grah. C -Composite For liquid matrices, indicate with a -Y -for yes the sample was field filtered or -N -Ibr sample was not field filtered.r DW-Drinking Water. GW-ouandwaiter.

SW-Surface Water. WW-Wasle Water. W-Water. SO-Soil, SD-Sediment.

SIL-Sludge.

SS.Solid Waste. O"Oil. F-Fihler.

P-WIpe. U-Urine, F-Fecal. N-Nasal* ,,*.", is R.questcd:

Analytical method requested (i.e. 8260B. 6010171470A) and numtberofconlainers provided for each li.e. 8260B -3. 610174701A- Type: IIA-Zydrochtoric Acid. NI -Nitric Acid, S1 -Sodium Hydroxide.

SA -Sulluric Acid. AA -Ascorbic Acid, HX -IFlxane, ST :.- iuam himsulfate.

irno preservative is added -cave field blank WHITE = LABORATORY YELLOW = FILE PINK = CLIENT Fo'r Lob Receiving Use Only Custody Seal Intact?YES NOTemp: C Page: of. 3 Project N: .4 7LPZ_- GEL Chain GEL Quote 4: COC Number (l): GEL Work Order Number: PO Number: '- (. k G Wr deN r of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178 Client Name: Phone#: £tfi ) 44/ -'oo Sample Analysis Requested (Fill in the number of containers for each test)Project/SiteName:

1-4 j Fax #: (Lis Should this "< , <-- Preservative Type (6)sample be 0.! Z ------Address:i s-i-, 1-5 ." t c. C. Io.K considered:

C0 Comments Collected by: Vyi- 5C, Send Results To:

6o 4

Note: extra sample is'D"%0meld "V ] Cd" l required for sample Sam ple ID (m, ,(Milt'ary " Filtered Matrix 0 specific QC For composites

-indicate start and stop date/ltime (m -dd-yy) (hhmm) .. c" ¢)C -.3-, OZ I N s- ?S o7C-"7, 5' ,_,,___,_,t__

ps--- --LZC_ L -Pie u_- -DO," ,t a.,L m coLo 2- 14 7-00--5--o,5 ' .__ _ __ _B-- , XOXc& 'X22___ __ _ __TAT Requested:

Normal: Rush: STc( S ife .tlj': e( ubject Fx Results: Yes / _Circle Deliverable:

C ofA /QC Summary / Level I/ I/ Level 3 / Level 4.Remarks. Are there any known hazards applicable to these samples? If so, please list the hazards Sample CoTtioia e Zon.4( .Ke Mountain Chain of Custody. Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date" Time c -.Date Time i " GEL PM: SipYl' " 'O ].&,/I/O 11~tif 2 -f..S 9tfo /oD Cl ellodof'lhii neal: re E Date Shipped: )( t5 2 2 Airhill 0: 13 .3 Airbill #t: I .) Cltalr, of Custody Num'sber C client Deconnined 2.) QC Codes: N -Nonral Samplc.TB -Trip Blank. FD -Field Duplicate.

EB -Equipmenttt Blank. MIS -Matrix Spike Sample. MSD = Matrix Spike Duplicate Sample. C -Grab. C -Compossile 3.) Field Filtered:

For liquid mtilrices.

indicate with a -Y -Iror yes sample was Field liltered or -N -l1sr sample was .X field filtered.4.1 Matrix Codes: DW-Irinking Water. tW-Grovondwater.

SW=Surface Water. WW-Wastc Water. W-Watcr. SO-Soil. SD-Scdirneln.

SL-Sludlc.

SS-Solid Waste. O-Oil. F-Filter.

P=Wipe. F=Vccal. N=Nutal 5.) Sample Analysis Requested:

Analylical method requested (i.e. 8260B. 600oBn470A) and numherbecontaincrs provided firecach (i.e. 8260DB- 3. 60101/TJ1T7 A -I).6.) Ireservative Type: UA = Hydrocmhlric Acid. Nt = Nitric Acid. SII -Sodium Illydrixide.

SA -Sulluric Acid. AA= Ascorbic Acid. Itx IXlexone.

ST- Sodium rlsiosulfate.

II no preservative is added = leave field blank WHITE = LABORATORY YELLOW = FILE PINK =CLIENT For- Lob Receiving Uve Only, Custody Seal Intact?YES NO C( / r Te~np:

_____of GEL'GEL Chain i( )k:" -m~ber M): GEL Work Order Number: of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 Fax: (843) 7 66-1178 a iK c ,a e Phon #: 3 1W Sample Analysis Requested ( (Fill in the number of'containers for each test)i 4 il'i,ýcc ,,ite Name: Fax #: ( 411$) 5'LfI -n~~~~~o, 2~~SI~Li ~ ,cfreimc 4'sto ,LFA q4 o5 Should this sample be considered:

4--iCd,,,ýby:

VV1. &le 1600 Send Results To: V' C.arV'C( I kO _ go , a Cu a C Ci a 2 a C I-<- Preservative Type (6)Sample ID"For composites

-indicate start and stop date/time*Date Collected (mm-dd.yy)

Time Collected (Military)(hhmm)QC Code 11)Field Filtered l Sample Matrix Z 04 tA Comments Note: extra sample is required for sample specific QC-I iA q, 13-4 l-4 C i/VI a N I y 211~~ 1r ol 55 I I ZI XYL)I (,,Lq f 2JYI~('IX Uo r--, -I D amvn a t_1i0V ~~_ _ _ _0 X~.I~. X~I~o _ _____I3 i -9 t~yvi-~ _ __I_5_ _ _f~tQ~LJ OA MAfV~¶oqo5 4, I I I l-e-----F 4-4-I.4-.-.~-----4----,4.------4'-----l.-4--------4--------l.-------4---.-.----4-t.

2 A\! K,_quested:

Normal: Rush: )'( Specify:', ,Fax Results: Yes I v ! Circle Deliverable:

CofA I QC Summary / Levj.,l Leve.,.. Level4./lu,'s: Are there any known hazards applicable to these samples? If so, please list the hazards , i" *aEastern ff1 YY.XMI ave. cz , Central Mier _Mountain Chain of Custody Signatures Sample Shipping and Delivery Details.,fished By (Signed) Date Time RIeeved (s d Date Tilne Rece d (s d GEL PM: E-,, S..w ,, T~(DO log IS 1 007______________________

Melhcdol`Shiprmeat:

De ate Shipped: JO_.__2 Airbill #: , 3___ __ Airbill U: h.,a, nlCustody Number Client Detcrmined

(.Ides: N -Nomtal Sample. TB 1Trp Blank, FD -tField Duplicate, EB- Equipment Blank. MS -Matrix Spik¢iSample.

MSD- Matrix Spike Duplicatc Sample. G -Grob. C- Composite: itc:,ttilcrcd:

Fort liquid atlrices.

indicate witha -Y -for yets (h sample wi...c fldtittercd or -N -for sample was not Feld filtered.i ..Codes: DWVDrinking Water. GW.Groundwata, SW-SurFacc Water, WWWastc Water. W=Waler. SO-Soil, SD-Scdimcnt.

SL-Sladgu, SS-Solid Waste. O-Oil. F-Filler.

P-Wipe. U-Urine. F=Fccal. N=Nasal ,,.,,;iic Analysis Requested:

Analytical method requested (i.e. 8260B. 6010B1/7470A) and numberaorcollainers provided ro each (i.e. 8260D -3.6010817470A .I).vative Type; HA -Hydrochloric Acid. NI -Nitric Acid, SH -Sodium Hydroxide.

SA -Sulfuric Acid. AA -Ascorbic Acid. 1IX -tcxask. ST -Sodium Thiasuttab.

Wl'on pescarvaive is added -leave Field blank WHITE = LABORATORY YELLOW= FILE PINK = CLIENT For Lab Receiving Use Only Custody Seal Intact?YES NO Cooaer Temp./

GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-817 1 Fax: (843) 766-1178 iGEL Work Order Number: ClientName:

Phone #: (L) 1 50 Lq -ýOcq Sample Analysis Requested (5) (Fill in the number of containers for each test)*Project/Site Name: Fax 4 5) Slhi<-- Preservative Type (6)J7.f..~ Ob1T~tzl(4L, .~ 1KivSconsidered:

Address:*

55 5.ý Comments Collected by: "

Send Results To: lCarVal hoo.frCsoiecv.S, WAI, W M Note: extra sample is d "-Time O olleced"required for sample'Date ID .Collected QC Code field Sample ie ,0 specific QC'For composites

-indicate start and stop date/lijne (m-dd-yy) (Miim) lhlscd t Matrix -o -__- _- ____ _____ 09 &I 'OV C ..A- S /--o. I 0 /-, -- ---- --9-t -O. t ,'-A 101 ." x-I I_\__ L -t5_ _Ja 5 -Li .,,, i1 h TAT Requested:rNormal:

Rush: spetiý:tl h t Fax Results: Yes / Circle Deliverable:

C ofA / QCSummary Level I / ( vel* / Level 3 / Level 4.to- S mpe o eceton Time Zone Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Easter n "/ 1 Eastern PaciltZýc f O £i;rd L 4) Central t oCor_ _[ Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Received b sgse) Date Time GEL PM: & ,^ S-.,ku Is* I1 l _15 _iU EZ # 7/7ia 0'? MethedofShi meal: Fc DaleShi ed: to log 2 2 Airbill fl: A trhtll ___________________________________________________

P:, 'I.) Chain of Custody Ntmibcr = Client tetennined 2.) QC Codes: N -Normal Sample. TB -Blank, FD -field Duplicate.

EB -Etquipment Blank, MS -Matrix Spike Sample. MSD -Matrix Spike )upliciate Sample. G =Grab. C = ComnlpXsile 3.) Field Filtered:

For liquid matrices, indicate with a -Y a for yes the sample was field tittered or -N -for sample wos not fiecd filtered.4.) Matrix Codes: DW-Drinking Water, GW=Groundoater.

SW-Surface Water, WW-Wastc Water. W-Wtter. SO-Soil. SO=Scdiment.

SL=Sludgc.

SS-Solid Waste..O=Oil.

F-Filter, P=Wipc. U-Urine, F=Fceal. N=N'snl 5.) Samople Analysis Requested:

Analytical ruethod requested (i.e. 8260B. 60[tB/7470A) and ntumber orcontaincrs provided Itr each (i.e. W260B -3. 6010t.17470A

-I..) Preservative Type: HA = Hydrochloric Acid. NI = Nitric Acid. SIt = Sodium Hydroxide.

SA = Sulfuric Acid. AA = Ascorbic Acid. iX = Flexane. ST = Sodium Thtotulfttie.

If Ont preservsoive is added = lcve field blank WHITE = LABORATORY YELLOW = FILE PINK =CLIENT For Lab Receiving Use Only Custody Seal Intact?YES NO Co.Teip:

Laboratories LLC SAMPLE RECEIPT & REVIEW FORM Client: ISD)GARCOC!Work Order: d1"Xi4It J6 i`ýO) c~u1lLl Received By: I e ,,-... 1,te Received 7-/7--99 S *If Counts > x2 area background on samples not marked,"radioactive", contact Suspected Hazard Information ;__ the Radiation Safety Group of furnher investigation.

Marked as radioactive?

-/ Maximum Counts Observed*:

y Classified Radioactive 11 by RSO? _ __-_,_' _" Marked containing PCBs? 'Shipped as a DOT Hazardous?

-7' azard Class Shipped: -lUN#: Identified as Foreign Soil? __Sample Receipt Criteria Z Comments/Qualif (Required for Non-Conforming Items)Shipping containers received intact and seClsmenos/Quamaged Qrc Applicable:

Isealed stie bc (descri/,e) 2 Samples requiring cold preservation within (4 +/- 2 C)?V/, cc ba blue ice dry Ice none other (describe) l~J. I-3 Chain of custody documents included with shipment?,/__ I ________4 Sample containers intact and sealed? V Orcle Applicable:

seals broken damaged contaiz leaking coair otber (describe)

I I 6 6 Samples requiring chemical preservation at proper pH?VOA vials free of headspace (defined as < 6mm bubble)?'11 Sample ID's, containrs affected and obsuved pH: If Presrva don added, LoI: II I I I -I (I i sample 113D's and contaitiers affected: IL of yes, Immediately deliver to Volatiles laboratory) 7 Are Encore containers present?VI-I 8 ISamples received within holding time?VI,/Id's and tests affected:.1-11 Sample ID's on COC match ID's on bottles?Date & time on COC match date &10 time on bottles?Number of containers received match number indicated on COC?V/L Sample ID's and containers affectld: Sample ID's affected: smnple ID's affected: V COC form is properly signed in 1 relinquished/received sections?Comments:

7-

• h 0 ov C06c w-, 777"V 7 Y-60 -(75- 4P -C.-7+P M ur M A ) rc ic~ : l tia s ...........

... ........ ..... ..a-te (I U111^k -/I t -fl il A List of current GEL Certifications as of 30 July 2008 State Certification Arizona AZ0668 Arkansas 88-0651 CLIA 42D0904046 California

-NELAP 01151 CA Colorado GEL Connecticut PH-0169 Dept. of Navy NFESC 413 EPA Region 5 .WG-15J Florida -NELAP E87156 Georgia E87156 (FL/NELAP)

Georgia DW 967 Hawaii N/A ISO 17025 2567.01 Idaho SC00012 Illinois -NELAP 200029 Indiana C-SC-01 Kansas -NELAP E-10332 Kentucky 90129 Louisiana

-NELAP 03046 Maryland 270 Massachusetts M-SC0 12 Nevada SC00012 New Jersey -NELAP SCO02 I New Mexico FL NELAP E87156 New York -NELAP 11501.North Carolina 233 North Carolina DW 45709 Oklahoma 9904 Pennsylvania

-NELAP 68-00485 South Carolina 10120001/10120002

-Tennessee TN 02934 Texas -NELAP T104704235-07B-TX U.S, Dept. of Agriculture S-52597 Utah -NELAP GEL Vermont VT87156 Virginia 00151 Washington C1641 EI Laboratories LLC a member of The GEL Group INC PO Box 30712 Charleston.

SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com July. 31, 2008 Mr. Moises Carvalho TRC Solutions, Inc.55 2nd Street, Suite 575 San Francisco, California 94105 Re: Humboldt Bay NPP Project 161072, Task 2400 Work Order: 212233

Dear Mr. Carvalbo:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on July 18, 2008. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs ontime every time. We trust that you will find everything in order and to your satisfaction.

If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.Sincerely, Erin Stanley Project Manager (Purchase Order: GELL-071408-001 Enclosures

(

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report.for TRCS002 TRC Solutions Client SDG: 212233 GEL Work Order: 212233 The Qualifiers in this report are defined as follows:* A quality control analyte recovery is outside of specified acceptance criteria** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.The designation ND, if present, appears in the result column when the analyte concentration is not detected above the detection limit.This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures.

Please direct any questions to your Project Manager, Erin Stanley.Reviewed by GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalbo Project: Humboldt Bay NPP Project 161072, Task 2400 (Client Sample ID: B-34-1.0 Gamma Project: TRCS00200 Sample ID: 212233001 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 14:10 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00795 +/-0.0235 0.0372 0.100 pCi/g MJHI 07/28/08 1531 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco.

California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-34-4.0 Gamma Project: TRCS00200 Sample ID: 212233002 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 14:25 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier

.Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gamnaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0176 +/-0.0282 0.0437 0.100 pCi/g MJHI 07/.28/08 1532. 775743 1 The following Prep Methods were performed Method Description Analyst Date .Time TPrep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC 1 07/21/08, 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments I EMiL HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 (Client Sample ID: B-34-8.0 Gamma Project: TRCS00200 Sample ID: 212233003 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 14:35 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamnina, Solid "Dry Weight Corrected" Cesium-137 U 0.0108 +/-0.0384 0.0656 0.100 pCi/g MiH] 07/28/08 1532 775743 1 The following Prep Methods were performed (Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 C GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: PS-23AC-1.0 Gamma Project: TRCS00200 Sample ID: 212233004 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JlJL-08 15:30 Receive Date: I 8-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time' Batch Methot Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00992 +/-0.0426 0.0701 0.100 pCi/g MJHI 07/28/08 1533 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corn Certificate of Analysis (ji.Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: PS-23AC-4.0 Gamma Project: TRCS00200 Sample ID: 212233005 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 15:45 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamna, Solid "Dry Weight Corrected" Cesium-137 U ".0.00902

+/-0.0335 0.059 0.100 pCilg MJHI1 07/28/08 1656 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July31, 2008 Client Sample ID: B-26-1.0 Gamma Project: TRCS00200 Sample ID: 212233006 Client ID: TRCS002 Matrix: Soil Collect Date- 16-JUL-08 16:05 Receive Date: 18-JIJL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL Rib Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 0.109 +/-0.0494 0.0541 0.100. pCilg MJHlI 07/28/08 1657 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep.GL-RAD-A-021 CXCI1 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com (Certificate of Analysis..... .... ........ A n lv -- -Company: TRC Solutions, Inc.Address: 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: B-26-4.0 Gamma Project: TRCS00200 Sample ID: 212233007 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 16:20 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00252 +/-0.0228 0.0375 0.100 pCi/g MJHI 07/28/08 1657 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCl 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3-.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-25-1.0 Gamma Proiect: TRCS00200 Sample ID: 212233008 Client iD: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 08:20 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gommaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00189 +/-0.0375 0.0647 0.100 pCi/g MJHI 07/28/08 1658 775743 1 The following Prep Methods were performed Method Description Analyst Date Time -Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments I EML FIASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: B-25-4.0 Gamma' Proiect: TRCS00200 Sample ID: 212233009 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 08:45 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0141 +/-0.0177 0.0276 0.100 pCi/g MJHI 07/28/08 1658 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (I GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corn Certificate of Analysis Company .TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: B-22-1.0 Gamma Project: TRCS0020.0 Sample ID: 212233010 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 09:00 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gamniaspec, Gamma, Solid "TDy Weight Corrected" Cesium-137 U 0.0421 +/-0.0333 0.0636 0.100 pCi/g MJHl 07/28/08 1658 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.corn Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 (.Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-22-4.0 Gamma Proiect: TRCS00200 Sample ID: 212233011 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 09:20 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.00994 +/-0.0555 0.0975 0.100 pCi/g MJHI 07/28/08 1904 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: B-27-1.0 Gamma Project: TRCS00200 Sample ID: 212233012 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 09:35 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho(Rad Gamma Spec Analysis Ganniaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 0.152 +/-0.0732 0.0695 0.100 pCi/g MJHI 07/28/08 1700 775743 1 The following.Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvaiho Project: Humboldt Bay NPP Project 161072, Task 2400 (Client Sample ID: B-27-4.0 Gamma Proiect: TRCS00200 Sample ID: 212233013 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 09:45 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Ganimaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.00957 +/-0.054 0.0951 0.100 pCi/g MJHI 07/28/08 2107 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 (.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-21-1.0 Gamma Project: TRCS00200 Sample ID: 212233014 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 10:10 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammuspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0102 +/-0.0583 0.102 0.100 pCi/g: MIHI 07/28/08 2314 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (Company:.

TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: B-21-4.0 Gamma Project: TRCS00200 Sample ID: 212233015 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 10:30 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gamraspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00859 +/-0.0569 0.0947 0.100 pCi/g MJHI 07/29/08 0738 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021' CXCl 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-23-1.0 Gamma Project: TRCS00200 Sample ]D: 212233016 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 11:10 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Methow Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.00923 +/-0.0371 0.0665 0.100 pCi/g MJHI 07/29/08 1010 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC1 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 (Client Sample ID: B-23-4.0 Gamma Project: TRCS00200 Sample ID: 212233017 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 11:35 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0454 +/-0.0553 0.0863 0.100 pCi/g MJHI 07/29/08 1245 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments 1 EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-33-0.5-Gamma Project: TRCS00200 Sample ID: 212233018 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 13:15 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0054 +/-0.0513 0.0883 0.100 pCi/g MJHI 07/29/08 1516 775743 The following Prep Methods wereperformed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3

-GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address: 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 (Client Sample ID: B-33-4.5 Gamma Project: TRCS00200 Sample ID: 212233019 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 13:25 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Ganmaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0382 +/-0.0412 0.0648 0.100 pCi/g MJHI 07/29/08 1720 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

PS- I C-0.3 Gamma 212233020 Soil 16-JUL-08 13:45 18-JUL-08 Client Proiect: TRCS00200 Client ID: TRCS002 Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho(Rad Gamma Spec Analysis Gammiaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0104 +/-0.040 0.068 0.100 pCi/g MJlHI 07/29/08 1951 775743 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXCI 07/21/08 1540 775720 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2,3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (.Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: PS- I C-1.5 Gamma Project: TRCS00200 Sample ID: 212233021 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 13:55 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch-Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.00337 +/-0.0388 0.0653 0.100 pCi/g MJHI. 07/29/08 0841 775744 1 The following Prep Methods were performed Method Description (Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-19-0.5 Gamma Project: TRCS00200 Sample ID: 212233022 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 14:50 Receive Date: 18-JUJL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho(Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0171 +/-0.0337 0.0546 0.100 pCi/g MJHI 07/29/08 1103 775744 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 (Client Sample ID: B-19-4.5 Gamma Project: TRCS00200 Sample ID: 212233023 Client lID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 15:15 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U -0.0108 +/-0.0327 0.0536 0.100 pCi/g MJHI 07/29/08 1103 775744 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Dale: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: PS-23BC-0.5 Gamma Proiect: TRCS00200 Sample ID: 212233024 Client ID: TRCS002 Matrix: Soil Collect Date: 16-JUL-08 15:40 Receive Date: 18-J1UL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho, Rad Gamma Spec Analysis Garnntaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.0141 +/-0.0223 0.0414 0.100 pCi/g MJHI 07/29/08 1104 775744 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry' Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 ('Client Sample ID: B-29-0.5 Gamma Project: TRCS00200 Sample ID: 212233025 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 08:25 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 0.113 +/-0.0674 0.0508 0.100 pCi/g MJHI 07/29/08 1104 775744 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments IEML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Daie: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-29-4.5 Gamma Proiect: TRCS00200 Sample ID: 212233026 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 08:35 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Methoc Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.00504 +/-0.0217 0.0373 0.100 pCi/g MJH1. 07/29/08 1104 775744 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: PS-20C-0.3 Gamma Project: TRCS00200 Sample ID: 212233027 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 09:00 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Ganinaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 UI 0.00 +/-0.0463 0.0374 0.100 pCi/g MJH1 07/29/08 1241 775744 I The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact. Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: C, it PS-20C-4.5 Gamma 212233028 Soil 17-JUL-08 09:10 18-JUL-08 Proiect: TRCS00200 Client ID: TRCS002 o-.ctAor.

Cltent Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho, Rad Gamma Spec Analysis Gammniaspec, Gamma, 'Solid "DTy Weight Corrected" Cesium-137 U 0.00448 +1-0.0245 0.0428 0.100 pCi/g MJHI 07/29/08 1241 775744 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch.Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: B-28-0.5 Gamma Project: TRCS00200 Sample ID: 212233029 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 09:40 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Ganimaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 U 0.00491 +/-0.0241 0.0423 0.100 pCi/g MJHI 07/29/08 1242 775744 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3.

A , GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: B-28-4.5 Gamma Project: TRCS00200 Sample ID: 212233030 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 10:00 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Methom Rad Gamma Spec Analysis Gammaspec, Gamma, Solid !"Driy Weight Corrected" Cesium-137 U -0.00678 +/-0.0204 0.0335 0.100 pCi/g MJHI 07/29/08 1316 775744 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 (Client Sample ID: B-24-0.5 Gamma Proiect: TRCS00200 Sample ID: 212233031 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 10: i5 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 0.0896 +/-0.047 0.0512 0.100 pCi/g MJHI 07/29/08 1430 775744 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 (

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-24-4.5 Gamma Project: TRCS00200 Sample ID: 212233032 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 10:40 Receive Date: 18-JUL-08 Collector:

Client'Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho, Rad Gamma Spec Analysis Ganmmaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 1.23 +/-0.146 0.0394 0.100 pCi/g MJHI 07/29/08 1447 775744 1 The following Prep Methods were performed Method Description Analyst Date Time. Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSW1 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis (Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Report Date: July 31, 2008 Client Sample ID: PS-21 C-0.3 Gamma Project: TRCS00200 Sample ID: 212233033 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 11:15 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 0.199. +/-0.042 0.0391 0.100 pCi/g MJHI 07/29/08 1648 775744 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments I EML HASL 300, 4.5.2.3 (.

• ~: ~'~*GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address : 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: July 31, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: PS-21 C-4.5 Gamma Project: TRCS00200 Sample ID: 212233034 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 12:30 Receive Date: 18-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho Rad Gamma Spec Analysis Gommaspec, Gamma, Solid "Dry Weight Corrected" Cesium-137 UI 0.00 +/-0.0413 0.0384 i 0.100 pCi/g MJ-HI 07/29/08 1649 775744 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 775723 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary TRC Solutions, Inc.55 2nd Street, Suite 575 San Francisco, California Contact: Mr. Moises Carvalho Workorder:

212233 Renort Date: July 31, 2008 Page 1 of 2 Parmname Rad Gamma Spec Batch 775743 QC1201625045 212233001 DUP Cesium-137 QC1201625046 LCS Americium-241 Cesium-137 NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time U -0.00795+/-0.0235 U -0.0593+/-0.0423 16.8 6.34 8.26 12.9+/-1.14 5.93+/-0.599 8.11+/-0.648 pCi/g pCi/g pCi/g pCi/g pCi/g 153 N/A MJHI 07/29/08 22:32 77 (75%-125%)

94 (75%-125%)

98 (75%-125%)

07/30/08 06:4 1 Cobalt-60 QC1201625044 MB Cesium-137 U -0.0314+/-0.0272 07/30/08 01:10 Batch 775744 QC1201625048 212233021 DUP Cesium- 137 QC1201625049 LCS Amnericium-241 Cesium-137 U -0.00337+/-0.0388 U 15.9 6.02 7.84 0.022+/-0.0417 13.5+/-1.13 6.02+/-0.469 7.89+/-0.591 pCi/g 272 N/A MWEI 07/29/08 16:5(Cobalt-60 pCi/g pCi/g pCi/g pCilg pCi/g pCi/g 85 (75%-125%)

100 (75%-125%)

101 (75%-125%)

07/29/08 16:55 QC1201625047 MB Americium-241 Cesium-137 Cobalt-60 U 0.0167+/-0.0464 U -0.00371+/-0.0145 U -0.00974+/-0.0151 07/30/08 12:48 Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound* Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

212233 Page 2 of 2 Parmname NOM Samplep Qual QC Units RPD% REC% Range Anist Date Time C Analyte has been confirmed by GCUMS analysis D Results are reported from a diluted aliquot of the sample-H Analytical holding time was exceeded J Value is estimated M M if above MIDC and less than LLD N/A RPD or %Recovery limits do not apply.ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning ihis qualifier R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the R.L. Qualifier Not Applicable for Radiochemistry.

h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more." The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+i- the RL is used to evaluate the DUP result.* Indicates that a Quality Control parameter was not within specifications.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

.. l. Iof K: I:_________

_ , ther" S(! it Aare: Name;!:) *ieName: GEL Chain of Custody and Analytical Request GEL Work Order Number: I 0A I aL ; ,2iJ 2;33 GEL Laboratories, LLC 2040 Savage Road Charleston.

SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178 Phone ll: -LA5 -l~9 3ioo0 Sample Analysis Requested (s) (Fill in the number of containers for each test)f Fax#): LIiIG £-t li- q3 -7 Ii ,, ~ ~ c3.~ ~ 'Sekf~ flc~SLa. 9HIo$Should this sample be considered:

U ~ by: \~.V Send Results To: Pr<c. .ar1ý (Z~iM50UiCA'S.

C a a 0 U 0.0 2 a a a 0 I-<-- Preservative Type (6)Sample ID For conposibes

-indicate start and slop dateltime"Date Collected (mm-dd-yy)-Time Collected (Military)(hhmm)QC Codc Field Sample (1t ' iltcred lit Mntrit {1 i ,v U.t2 I-U 0'Jo r T Comments Note: extra sample is required for sample specific QC 15 5ht1, 0~o C A% -Zl, A- -t,_ 'i _ _ _ _ _ _I) Pirc -1A I A eguested:Normal:

Rush: X SctfY.H r. (ubjec t urcha I Fax Results: Y CircleDeliverable:

CofA QC Summary L vel I i Level3 / Level4 KI!ImrkS.

Are there any known hazards applicable to these samples? If so, please Its! thg hazards Sample Co nl14m 6 ahTe.n, Eastern C6 ,I ,-Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details i;:t ushed Bjy (S igned)Date Timle Reciedby (sg ed )Date Time GEL PM: Prin trse 7IV-i1n~4

!Cy~~ It Method orShn ment: F! ey flst, ~hinnneI ) hi I O~__________________________

2 jAirbill h:__________________________________

3 .Airbill 0I: oi l(*uody Nutmber -Clicnt 1)it¢ciined mttcs: N -Nortal Sample. TB -Trip Blank. FD -Field Duplicate.

EB = Equipment Blank. MS Matrix Spike Sample. MS D -Matrix Spike Duplicate Sample. G -Grab. C -Cnmposite* Filtcred:

Fur liquid matrices.

indicate with a -Y.- lbtryes the sample was field itctred or- N -tibrmple was not licld litlte'd.Pi LCodsc: DW-Drinklng Water. GWC Groundwaier.

SW-Surtacc Water. WW-Wuite Water. W-Waler. SO-Soil. SDSediment.

SL-Sludge.

SS-Solid Waste. O0il. F-Filteo.

P-Wipe. figUrine.

F-Fecal. N-Nasal->re Analysis tcquated:

Analytical method requested (i.e. 8260B. 601OBnl470A and number ofcotntainers provided for each (i.e. 82608 -3. 601Ot17470A

.I ).'7.rativeýaeotq HA -Hydrochloic Acid. Nt -Nitric Acid. SH -Sodium Ilydroxide.

SA -Sull'uric Acid. AA -Ascorbic Acid. HX --ST -Sodium Thiosull'ate.

It I' preservative it added -leave kield blank WHITE= LABORATORY YELLOW = FIL PINK =CLIENT For Lab Receiving Use Only Custody Seal lIntact?YES NO Cooler Temp:

Page: or ~FChi_.ro.ect#:

w GEL Chain GEL Quote #: COC Ntumber _____________

I'D Number: ... GEL Work Order Number:[P0 Number: ,tl'of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 Fat: (843) 766-1178 Client Name: Phone #: t.i .-., "14 -3 0,oo Sample Analysis Requested 1s) (Fill in the number of containers for each test)Project/Site Name: Fax 4: LiI -5"1 -3"-79 Should this; <-- Preservative Type (6)samplebe --Address: r* £ C A e.Considered: " CA -k- Comments Collected by: \/ -Send Results To: 17vt a '., o ,, .,ý .- -Z Note: extra sam ple is.ie E for sam ple*ttetc Collected tk Cotlected QD'(oitc, Ficld S.,,pte Z; ; -. -A- specific QC Sample(Military Filtered _.h_ Mtrix _For co,,,Ipoites-indicate start and stop dateltitte (mm -d-dyy (hhmity TAT Requested:

Normal:, Rush: Specily.:14" ýr-Nus~eci~oSurchaucl lFax Results: ..Yes I CN.7 Circle Deliverable:

C of A I _QC Sulmnar7 Level I /lý Level 3 /Level 4.Remarks:

Are there any known hazards applicable to these samples? If so, please list (he hazards Sample Collectiona Time Zone_ _ _ _I-_.Mountain_.-

Chain of Custody Signatures Sample Shipping an(l Delivery Details Relinq 'uished By (Si'gned)

D ate T iime Received by (signed) D ate T i meG L P M i'c y......2 IAirbil 11 13 13 Airbili 4: 1.h Cthin ofCustodv Number = Client I)etcritined 2.1 QC Codes: N Normsal Sample. TB -Trip Blank. FD = Fietd Duplicate, EB -Equipntet tBlank. MS = Matrix Spike Sample. MSD -Matrix Spike Duplicate SUmpte. G -Grah, C -Composite 3.1 Field Filtered:

Fur liquid matrices.

indicate with a -V -ftr yes the sample was field liltcred or -N -for sample was not fietd ilttered.4.t Matrix Codes: DW-Drinking Wuter. GW=Groundwater.

SW=Surfucc Water. WW-Watc Wuter. W-Water. SO-Sail. SDSediment.

SL-Sludc.

S=.-Solid Waste. O-Oil. FFilter. P=Wipe. It=Urinc.

F-Fecal. NNasul 5.) Sanple Analysis Analytical mstobod requested (i.e. 8260D. 60iaB,"47aAt and number ofcontaincrs provided ireoch (i.e. 82601 -. .6010611470A

-t).6.) Prsener-atic "lyc: 11A -tHydrochloric Acid. NI -Nitric Acid.SII -Sodium Hydroxide.

SA -Sulltbric Acid, AA -.Ascorbic Acid. HX = t(exanc. ST = Sttdium Thit-ulfate.

Itno presenative is added -lcane fictd blank WHITE= LABORATORY YELLOW = FILE PINK = C(.1FINT For Lob Receiving Use Only Custody Seal Intact?YES NO CooI Temnp.C GEL Chain;iC(, N!i umber G L k er it'(' \

Work Order Number: of Custody and Analytical Request GEL Laboratories.

LLC 2040 Savage Road Charleston.

SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178ý c::, Name: Phone 4: VC J- )bOb Samplc Analysis Requested (5) (Fill in the number of containers for each test)Fax.: " -Site Name: Fax: Should this <- Preservative Type (6)-samle be "_7i\L~~s ~considered:

0ýýe (5V 5 F7-)7Z'G CA 41405'1;c_ _Ledby:_ _SendResults To:A Com m ents VT: -- 6A > 17. Note: extra sample is~I teb'Sn el-Time " required for sample tDate Collected STimpile Collected QC Codec Field Sample : Sample ID (Military) -ilerd' Msipeci' i Q For conmpositet

-Indicate start and slop daleltime (mm-ddyy) (hmm)~ _ _---1-t--4 3ýS I x_ x_ __ _4 ". , _ -- 10 ....logo S R._!V\ V Requested:

Normal: Rush: & SpeifyMA 6r. (Subi.-ttoSurchurge)

Fax Results: Yes .Circle Delive.rable:

CofA , QC SUmniary / Level I , e I Level 3 Level4 Acmarks: Are there any known hazards applicable to these samples? If so, please list the hazards Sample Collection Tiren Zone 4k *kkce I Eastern ( ajf3l--ere (GWCentral Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details i,:ý, quished By (Signed) Date Time R;e7 aned) Date Time GEL PM:_7.., ji AAUr, "45 'i3 691...S MethodofShipsent:

j' 'Date Shipped: "71%110 7 2 Airbill #: 3 Airbill 9: S : t Number Client Dermined For Lab Receiving Use Only: odes: N -Noratal Sample Ta = Trip Bltank. FD Field Duplicate.

EB LEquipment Ilank. MS- Matrix Spike Sample. NlSD = Maids Spike Duplicate Sample. G -Grab, C -Composite r 1 i F-r liquid matrices.

indicate with a -Y -ror yes the sumple was fieid filtcred or -N -rca sample was not licld fillercd.

Ctsltody Seal Intucl?., , ixs Codes: DW-Drinking Water. CW-Gronnd.ater.

SW-Surfaee Water. WW-Waste Water. WWater. SOSoil. SDSedintent.

SL-Sludgc.

SS-Solid Waste, OOil. F-Filter.

P-Wipe, -Urine. F-Fecal. N-Nasal YES NO" :nle Aialysis Requesited:

Analytical mtlhod requested (i.e. 8260B. 60108/7470A) and number orcontainersprovided rbu each (i.e. 82600 -3. 60101/7470, -I1. Coot rTemp: 1%, adveType:

HA -lydrochloric Acid. N1 -Nitric Acid. SH -Sodium Hydroxide.

SA -Sulluric Acid. AA -Ascorbic Acid. HX -

Sodium Thiosullte.

If no preservative is added -leave field blank WHITE -LABORATORY YELLOW -FIL' PINKa=CLIENT Page: -.of Chain PlroteJCt

IC GELChi GEL Quote #: COC I: I'O Number: -GEL Work Order Number: of Custody and Analytical Request GEL Laboraiorics, LLC 2040 Savage Road Charleston.

SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178 Client Name: 'V... Phone #: A -:)ot-" -300t0t Sample Analysis Requested

15) (Fill in the number of containers for each test)Ii Project/Site Name: V. $ýFax #: M-SqltV ýT Address: sr- ;*-7 SK $.lk , 'ScAr ~c~ (-A- `1411 5 t Collected by: ` .,. .\Z5 Send Results To: t\Should this sample be 1!considered:

o E-C 5D 4 -I- --4-I l-+-------

~ -<- Presenative Type (6)Sample ID For compo.ites

-indicate start and slop date/ltime tDate Collected (mm-dd-yy).iTne Collected (Milt-,)(hhmm)QC Codec Ml Field Sumplec Matrix "'V.'r--s4l Comments Note: extra sample is required for sample I specific QC_.. "e -----6,- W 1',o V.M 'y &w 3 ..>z.TAT Requestcd:

Normal:, Rush: T4 pciyI (Subjeecttlo Su byp) Fax R~esults:

Yes / 9 Cirele Delilverable:

C of A I.C Summar I Level I /e /Level 3 /Level 4 Remarks: Are there any known hazards applicable to these samples? Ifso, please list the hazards .am o Eastern j\ e(4 ( ) Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Received by (signed) Dale Time GEL PM: 9r-\ 9 ,\..Method of Shipment:

re Date Shipped: 22 Airbill 4: I I AirhbIl H: I 131 Chaii o T'uslody Number -Clietn Deteilined 21 QC Codes: N -Normal Sample. TB -Trip tlank. FtD Field Duplicate.

EDl Equipment Blank. MS -Malrix Spike Sample. MSD -Matrix Spike Duplicate Sample. G Gorals C -Composite 3.1 Field Filtered:

For liquid matrices.

indicate willh a -V -tor yes the sample was iteld filtcr.d or -N -rot sample was not eield liltered.4.) .lMai,-

Water. GW-maundwatcr, Water. WW-Wasie Water. W-Water. SO-Soil. SO-Sediment.

SL-Slude.

SS-Solid Wuste. O=Oil. F-Filter.

P-Wipe. U-Urine. F-Fral. N-Na.ýl J.A Sample Analysi. Requested:

Analytical method ercqucsted (i.e. 8260B. 60101B7470A) and nutmher ormetainers provded tor each (i.e. 8260D -3, 6010817470A

-I).6.) Preservative T. pe: HA -Ilydrochhloric Acid. NI -Nitric Acid. SH -Sodium Hydroside.SA

= Sulliric Acid. AA -Ascohic Acid. HX -tlexane. ST -Sodium Thiosulitc.

KIno preservative is added -leave fieid blank WHITE = LABORATORY V E!.I .nW = FIT V nwh ,- -,.For Lab Receiving Use Onty Custody Seal Intact?YES NO Cooler retnp;f=-C -

of 1,1,,Cft:

15 GEL Chain tQuote #: IC umber 0 Work Order Number: ti: 'mber:. ,ln of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178':.: Name: Phone #: , .3iO' Sample Analysis Requested (s) (Fill in the number of containers for each test)(ixj-,.t/Site Name: Fax#: 41 5 9W ",Shoiuld

<- Preservative Type (6)amebe ------*ir"ss: '-i-t considered:

Comment (IL L t led by: -,Send Results T. O-, Note: extra sample is"Timerequired for sample I p-Date Collected Colle.cted IQ C Cd.l Field JSample' " Sample ID o" Ftl)iltered t Matrix", , -specific QC*For composites.

-ndicate start and stop dateltime (m.-dd-yy) .. mm 1 CC --, WAiN._ _7 .... ..... .. ..-1 C- 2,1 -5 I_-P s-\ kc- .I -V-3 5 2- X 75 k CI --9 19 0,- 5 14 _ 5_151 T._!A Itequested:

Normal: Rush: X SpeCiiy:49ýr.(SubjegtoSurehere) lFax Results: Yes able: CofA /QC Summa / Level I 1= Level3 /Level 4.!,,,r ~eqe~sed:Noral Ruh: e) ..... Cr~e~eiveabl:

ClA ! ei / / Lv0_3r/Levl4 i /,:nwrks:

Are there any known hazards applicable to these samples? Ofso, pleaa list the hagards 1timple lgnlgeton Time-Zone Eastern Central. Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details ,..;uished By (Signed)Date Time x 'YV'lK (DiMiI& .-21,.I Received by (signed) Date Time GEL PM: a 4\ _1 Method ofShinment:

I Date S h i Ded: -7117 / bg-I I~1~ -- K 7 -/7 -01 67 IS Mehdo-iie 3 'airbill 0: ol'Causody Number- Client Detennined

2. Li , odes: N -Normal Sample. T8 -Trip Blank. FD -Field Duplicate.

ED E.quipment Blank. MS -Matrix Spike Satple. MSD -Matrix Spike Duplicate Sample. G -Grab. C -Camposite Filtered:

For liquid matrices.

indicate with a -Y -for yes the sample was field filtered or -N -fio sample was not field littered.1,c Codes: DW-Drinking Water. GW-Groundwaier.

SW-Suarfe Water. WW=Wastc Water. W-Water. SO=SoiL SD=Sediment.

SL-Sludge.

SS-Solid Waste. O-Oil. FFilter. P-Wipe. U-Urine. F-Fecal. N'Naxal.ple Analysis Requeteld:

Analytical method requested (i.e. 8260B. 6010Bfl470A) and number orcoatainers provided Imr cach (i.e. 82608 -3. 6010BI/7470A

-I).P., -.vative Type: HA -Hydrochloric Acid. NI -Nitric Acid. SH -Sodium I lydmxolde, SA -Sulturic Acid. AA = Ascorbic Acid. lIX -I lerxatST -Sodium TMiawsulate.

If no prscrvative is added -leave field blank WHITE = LABORATORY YELLOW = FILF PINK = CLIENT For Lab Receiving Use Only Custody Seal Intact?YES NO Cooler Tempp:

Page: of v GEL Laboratories, LLC Project,9:

0lo17 GEL Chain of Custody and Analytical Request 2040SavageRoad GEL Quote #i: Charleston.

SC 29407 COC Number ll:GEL Work Order N b Phone: (843) 556-8171 PO Number: (0krOl Fax: (843) 766-1178 Client Name: Phone #: HlS-,tA 11oo00 Sample Analysis (Fill in the number ofcontainers for each test)Project/Site Namne: Fax #:- ' -Should th is <-- Preservative Type (6)oamnple be ----Address: -~~(k ~ ~considered.:~Cmet

• ' "; I Comments Collected by: (A .-Send Results To: ...'-"[ti Note: extra sample is od required for sample*Dat~ollct " *Timc Sam ple ID %le led Collected -e Fiel I specific QC For composites

-indicate start and stop date/lime (mm-dd-yy) ( , a Filtered Matrix"' 0_ __S_ _ -2_6 , 14 1. _ _ _ _ 1.I'5T 19' -2 o 3 _ S- 5, q:ou V,- VV,,, ,154n_ _-__ __.5I o 5 , -L5 0. , 91?P5-ao7-0 , -L~ 0'a. Nil 2- L -TAT Requested:

Normal: Rush: /.s Seeci:fy 6 1Results: Yes " I Circle Deliverable:

C orA / QC Summar / Level I I LeC? I Level 3 / Level 4.Rearks: Are there any known hazards applicable to these samples? lf so, please list the hazards qal Colletion Tie on IMountain Chain 61' Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Tirne/ Recie sind) Date Tintc GE-L PM: : ,,, 4 \-d k ,- i 53D ," Method .ol'Shipinenul e-,. nc Date Shi ed: '7 /2 2 Airbill 0: 3 13 Airbill M: 1.i (.hUi, ofttCmtody Num:Lr -Client OcDtrtenined 2.) OC Ctdcs: N -Normnal Sample. TO -]Trip Blank. FD O Field Duplicate.

EB =Equipment

[Slank. MS- Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample. G -irah.C -Comnposile 3.1 Field Hiltcred:

For lisquit nairics. indictntc with a -Y -for yes the sanmpie was tield liltered or -N -1hr sample was not fiecld filtered.4 ,larin C'odes: DWIDrinking Water, GW-Grotmdwater.

SW-Surfact Water. WWWnsasc Water. W=Waler. SO-Soil. SD=Sediment.

SL-Sludge.

SS=Solid Waste. O iOil. F-Mlier. P-Wipe. U-Urine. F-Fecal. N-Nusal..) Sample Anatysis Reqtuetled:

Analytical mnethod requsted (i.e. RZl600. 60108t7470A ) and number or caotainers provided tir each (i.e. 8260B .3. 60 1OB/7470A

-I.6.) Preservativc Type: HA -Hydrochloric Acid. Ni = Nitric Acid, Ski -Sodium Ilydroxldc.

SA. Siulfuric Acid. AA -Ascorbic Acid. ltX -tcas. ST -Sodium 1lhiosauluta.

lfnt preservntive is added -leave field blank WHITE= LABORATORY YELLOW = FIr.E PlNJle -Pl ItE'w'ot" Lab Receiving Use Only Cutstody Seal Intact?Y'ES NO C f Tcmp: C 2 ~ 'Y't 4~ ~bof~.Clt:Name:

It-fc- Plion of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 Fax: (843) 766-I178 e #: `-ý\G LL44- ýCVD Sample Analysis Requested s (Fill in the number of containers for each test)o I t./Site Name: "Fax: LShould this <- Preservative Type (6)saample be 4 CA ct`Aý considered:.s: & 5r CA y/Oj 0" Comments-ted by. Send Results To: Note: extra sample is Date. collected l r required for sample Collected QC Code Field Sample -%" specific QC Sample ID < tI For- composites

-indicate st(i~Ir)Plte tMti art and stop date/f ima Am-dy) (hi)___ ____ ------A I~i-S-.It~J

~~+I I!I r3- ~ ~ j C Y-0--, VCV~I VA I 4 j%2~~~nI Dono -A32~OS~mA

-- -____I 'li~i~t-~s 1Zi~i~EL i~iI~IV ~ti~)040,ii V -[*\Te. uested: Normal: Rush: ?M Specify:'l N. (subject to Surchnrge) 1Fax Results: Yes /lU'nttrks:

Are there any known hazards applicable to these samples? Ifso, please list the hazards I bl C S Lvel I Level 3 Levl 4.Samole Collection Time Zone Eastern Central Other Mountain~r\~ ~te~~5 Chain of Custody Signatures Sample Shipping and Delivery Details 1 utshed By (Signed) Date Time y (signed) Date Time GEL PM: r~~'4 1~]Dnte Shinned: -AA IM ment: IDale Shipped: ý111/ 07 2 Airbill 9: I.I" ...3___________________________

Airil 0:'s-1:

Number -Client Determined

t. Ad: N -Normal Santpl. TB -Trip Blank, FO = Field Dupticatc.

EB = Equipment Blank, MS Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample. G -Grab. C -Cmtipoasile 1., Filtered:

For liquid ntatriccs.

indicate with a -Y -foryea the samnple was tield tittercd or -N -tir sample was not lIdd filttend.c x ..c Codes: DW-Drinking Water. GW-Groundwatc., SW-Surracc Water. WW-Wasir Water. W=Water. SO-Soit. SU-Stdintat.

SL-Sludgc.

SS-Solid Waste. O-Oil. FaFiter. P=Wlpc. UUrinc. F-Fccal. N-Nwal , ,: Analysis Requested:

Analytical method requested (i.e. 8260S. 60oiBfl470A) and number ofcontainers provided itr each (i.e. 82600 -3,

-I1.<I t,-sativc rypc: HA -

Acid. N1 -Nitric Acid. SH -Sodium Hydrtoxlde.

SA -Sulfuric Acid. AA -Ascorbic Acid. HX t tlcxtST -Sodium Thiosltulatc.

Ifno prescrvativc is added -'leave ield blank WHITE=LABORATORY YELLOW=FILE PINK=CLIENT For Lub Receiving Use Only Citviody Seal Intact?Y&5 NO Cooler 7Teip." (

Page: f 'o f GEL Laboratories, LLC Project \: GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote #: Charleston, SC 29407 COC GEL Work Order Number: Phone: (843) 556-8171 PO Number: , Fax: (843) 766-I 178 Client Name: Phone #:.J\ 3'0 Sample Analysis Requested s (Fill in the number ofcontainers for each test)ProjectSiteNare:

Fax #: L °l -93,-7g Should lths -- Preservative Type (6)sample e 0 " -" A~ddress:

5C. 0 osdrd co,, nsided- Comments Collected by: Send Results To:c Note: extra sample is-'rim 5 ..3, required for sample Co llct ed Qc code Field sample 2 I specific QC Sampete DC Cod Fiel Sapl SamplearD..

+.+a n P Filltoed a Mario1 0 1 Fore composites .indicate start and stop datretilne imm-dd-yy)

U r \, 14 D3-l c cm0 ----X ----z -. : ...... .... ..o l- k-,yo? ' , S .. .. -i .... .. .. 7.. .ij.. ... ... ... ..........

.....Zlc I li ý C '*N 'X 's-1z~- 9, i... L- .. 1 -- -)__________

____ Iz-3L I -C_ -._ -V\ Ma TAT Requested:

Normal: .Rush:/---

Spaeif (SubjicttoSurchsrgcl Fax Results: Yes I Circle Deliverable:

C ofA QC Summa / Level I Level3 /3 Level 4.Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Sample Collection Time Zone Eastern Central Other_Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Received by Asigned) Date Time EL PM: f C"A e2n-i'i-f "0AMethod orShipmenlt:

Date LDate Shipped: /016K..2 2 Airbill U: 3 lAirhill #: I.) Chain ofCuslody Number -Client Denrinised 2.1 QC Codes: N -Norma.l Sample.TB

-Trip Blank. I'D = Field )uplictc.

EB -Equipment Blank. MS -Mutrix Spike Sample. MSD -Matrix Spikc I)uplicate Sample. G = Grab. C = Composite 3.) Field I 'illered:

For liquid matrices, indicate with a -Y V i- r yes the sample ons field liltered or -N -Ior sample woas not fihld 4.) Matri6 DMW-Drinking Water, GW =Oroundmater, SW =Stulhcc Water. WWW .,tc Water. WoWater, SO-Soil. SD-Sdinnt.

SL=Sludge.

SS-Solid Waste. O=Oil. F-Filter.

P=Wipe. U-Urine. F-Vec.I. N-Nas,.l 5.l Samphl Analysis kequested:

Analytical method requested (i.e. 8260B.601B/7470A ) and numberol'conminets provided lIr each (i~e. 82619B. -3.600t4ItOA

-t).6.) Prescrvativc Type: HA -Ilydrochboric Acid. Nt = Nitric Acid. SH -Sodium Hlydmxide.

SA -Sol (uric Acid. AA -Ascorbic Acid. tIX = Ilexane. ST -Sodium Tlimsullate.

tIno preservative is added -leave lield blank WHITE = LABORATORY YELLOW = FIPc DI FUV --' ,. r K'_, For Lobs Receiving Use On/se Custody Seal Intact?YES NO Coo Tenp:.i _.. r C SAMPLE RECEIPT & REVIEW FORM T I Laboratories LLc: 1By: .d aIzrd Infor"atin6 leA marked as radiocive?,A Radioactive n1 by RSO?ixples .arked containing PCBs?as a POT Hazardous?

identified as Foreign Soil?E Sample Receipt Crit'ris Shipping containers received intact and--- v-41 (ate &8 time on COCmatcb date & tim , bottles?unibr of contaimer received match umber indicated on COC."OC form is properly signed in~.. irwjk iv ed secti S?t1V y-710 , (p!~¶c-~ ~7\A) ~~i~v: ~jtaASD'aw f 'i I m- (I

..'.1 List of current GEL Certifications as of 31 July 2008 State Certification Arizona AZ0668 Arkansas 88-0651 CLIA 42D1904046 California

-NELAP 01151CA Colorado GEL Connecticut PH1-0169 Dept. of Navy NFESC 413 EPA Region 5 WG-15J Florida -NELAP E87156 Georgia E87156 (FL/NELAP)

Georgia DW 967 Hawaii N/A ISO 17025 2567.01 Idaho SC00012 Illinois -NELAP 200029 Indiana C-SC-01 Kansas -NELAP E-10332 Kentucky 90129 Louisiana

-NELAP 03046 Maryland 270 Massachusetts M-SC012 Nevada SC00012 New Jersey -NELAP SCO02 New Mexico FL NELAP E87156 New .York -NELAP 11501 North Carolina 233 North Carolina DW 45709 Oklahoma 9904 Pennsylvania

-NELAP 68-00485 South Carolina 10120001/10120002 Tennessee TN 02934 Texas -NELAP T104704235-07B-TX U.S. Dept. of Agriculture S-52597 Utah -NELAP GEL Vermont VT87156 Virginia 00151 Washington C 1641 ELaboratories LLC a member of The GEL Group INC P0 Box 30712 Charleston, SC 29417 2040 Savage Road Charleston.

SC 29407 (P 843.556.8171 F 843.766.1178 August 11, 2008 www.gel.com Mr. Moises Carvalho TRC Solutions, Inc.55 2nd Street, Suite 575 San Francisco, California 94105 Re: Humboldt Bay NPP Project 161072, Task 2400 Work Order: 213274

Dear Mr. Carvalho:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on July 18, 2008. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction.

If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.Sincerely, Erin Stanley Project Manager (Purchase Order: Agreement No: GELL-Enclosures

(

Page! or GEL Laboratories.

LLC ,roiedt,:

,: 7 GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote #: Charleston.

SC 29407 COC Number t t t: GEL Work Order Number: 6 I .'21. ; 33 Phone:- (843)1556-817t17t tLO3ornttcrI Fax: (843) 766-1 178 Client Name: Phone U: LA 15 -LiLi -3Q0oo Sample Analysis Requested fs' (Fill in the number ofcontainers for each test)ProjectlSite Name: '-ir Fax 4: qll- _ -4Iq3-73 Should this <-- Prcservative Type (6)sample be ---" Adrs considered:

rsC , '+ Comments Collected by: Send Results To: a, r- Note: extra sample is*tlate Collectd+ " ". , , required for sample Satnple ectD QCm OC ode FIeld Saorac cc 5:i I -_ specific QC S a m p l e I D ( M d y ) ( iltam .r y) F i lt,+ , e r e d " M a g + " For composites

-indicate start and stop dole/time- (hhmm) M j ...B-SMH-\o t I.L I,__.___..__..

-_ _ ....- -TAT Requested:

Normal: Rush: _S ecifyý Y((Sublecl tosurcharge)

Fax Results: Yes I a Circle *Deliverable:

C oCA /C Summa /Lcvel I I ec4I Level I Level 4 Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Sasier 0 _me.Zonc.3Eastern citi.pCentral Other___Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Received by (signed) Date C GELTPM: ¢er_.., I~- h1Iito% q-1 Method orShipincat.

IDate Shipped: *I jI 2 Airbill N: 3 .Airbill tt:.CThain of (.usiody Number -icint 4)¢ecrminied 2.1 QC Ccdc.s: N -Nonnal Sample.TB -Trip Blank. FD -Field Duplicate.

EB = Equilpmnt, Olznk. MS- Matrix SpikeeSample.

MSD -Marix Spike Ouplicate Sample. G =CGrab. C -Composite I.) Field Filtered:

For liquid matrices, indicate with a -V -for yet the sample was Field ilttered or -N -litr sample was not Feld fillered.4.1 Metatrixi Codes:

Waer. GW-Gmaondwater.

Water. WWWuscte Water. W-Water. SO=Soil. SDDSeditteni.

SL-Sludge.

SSSolid Waste. O=Oil. F=Filter.

P=Wipe. U=trine. F-Fecul. NýNasal ,.t Sample Analysis Rcqucestd:

Analytical method requested (i.e. 1260B. 6o10Bi7470A) and number oflontainers pnovided far each (i.e. 82608 -3. 60109/17479A

-I ).fi.1 tivescatiee T vpe: 11A -Hydrncbhhric Acid. Ni = NitricAcid.

SH -Sodium Ilydroxide.

SA -Sulfuric Acid. AA -Ascorbic Acid. HX = Ilcxune. ST -Sotdium Thitisullate.

irno preservative is added -leave field blank WHITE= I,ABORATORV V .El 11 ,OW = F1 ItF. PI N W = CI .IVNT For Lab Receiving Use OnlY Cuttsody Seal Intact?YES NO Cooler Tetmp: t C

.5 GEL Chain GEL W eote 8e!ii)buibr t,\b". GEL Work Order Number: of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178Name: Phone 0l: H ICr, -(.t iq.. 2coo Sample Analysis Requested (s) (Fill in the number of containers for each test)'Sile Name: lt.;V Fax #: L 51t 9 3-7s_Should this sample be considered:

Iicss: IS 1 lk. , Sk&- ['5i1, C-A 9LMio.(Uo ;ed by: \l 6 \~Samy For coonxulessle

-indices U C 0 U C.5-C m a I-Send Results To: t1n NcoxvoWo PAr soL, an ous 'on<-' Preservative Type (6)*Date Collectaed lie ID to start and stop date/time Collected (Military) thhmm)QC Code (1)Field Filtered li Sarnple Matri 11 cc I--4-Il-'-p Comments Note: extra sample is required for sample specific QC (mm-dd-yy)

I , tt--d 1F-o XI2 2".AT l, equested:

Normal: Rush: Specify,:'qg isoSurciar7el Fax Results: Yes I Circle Deliverable:

C ofA QC Summary / Level I / Level 3 / Level 4 Rc/m,:i ks: Are there any known hazards applicable to these samples? If so, please list the hazards ..mile Collection Time ZonM~ ~ \e~\O~Central Other___Mountain Chain of Custody Signatures Sample Shipping and Delivery Details C .. h uished By (Signed)Date Time-Received by (signed) Date Time/-N GEL PM: itf 6t LMk -ýlA~Method of ShiotneeL: ¢ex I Date Shitied: _71714-.eto of. -hoet 1F, -.-, -__________________________________

2 1 Airbill II: 1~3 JAirbill 9:1______________

_i of Custody Number -Client I)etermiied odes: N -Normal Sample. TB = Trip Blank. FD -Field Duplicate.

El -Equipment Blank, MS -Matrix Spike Sample. MSD -Matrix Spike Duplicate Sample. C -Grah. C -Composilte

.............

Filtered:

For liquid matrices, indicate with a -V -fbr yes the sample was felud fillcred or- N -itr sample wa. not field filtered.:i; .e: x Codes: DW-Drinking Water. GWGromandwater.

SW=Suiface Water. WW-Wuste Water. W-Water. SO-Soil. SDi-Sediment.

SL-Sludge.

SS-Solid Waste. O-Oil. F-Filter.

P-Wipe, i-Urinc. F-Fccal. N-Nasal Analysis Rieqested:

Analytical method requested (i.e. 8260B. 601Bo/'47eA) and number of containcrs provided libreach i.e. 82600 .3. 6010&/7470A

-I).%. , ,:.. .li..tvc Type: I IA- Hydrochloric Acid. NI -Nitric Acid. Sl -Sodium Hydroxide.

SA -Sulturic Acid. AA -Ascorhic Acid. HX I lesxune. ST-Sodium

'himsullatC.

Ir nopeescrvative is added -leave field blank WHITE = LABORATORY YELLOW = FILF--"' PINK = CLIENT For Lab Receiving Use, Only Cutstody Seat Intact?YES NO!0ooIl IV:p Page: of " GEL Laboratories, LLC'ro0.,ct:

-,+-GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote #: Charleston, SC 29407 COC Number GEL Work Od N b Phone: (843) 556-8171 PO Number: A, "\1 Fax: (843) 766-1178 Client Name: Phone #: VW(, -(Cý -W ) Sample Analysis Requested (51 (Fill in the number of containers for each test)Project/Site Name: Fax 9: \ Shoutd this PrcseativeTypc(6)

'A sample be " -_ -..... be.M Adres CHO consaidered:

0-Comments Collctedby,, L -

Collected by' Send Results To: McNote: extra sample is*Date Collected

'Time' required for sample Sample ID Collected QC Code I;eld Sample aoSpecific QC Far c,,,posiles

-indicatt start and stop datellime (mm-dd-yy) (hhmm) "' ' ... .-..... ..... ..... ---- --+ ......... ... .............. ........................~ , ts ' ._ _ _I "'_ __ -_ ____ ___ ,,,,i .'.'.., t I _ _ _ _TAT Requested:

Normal: Rush:

o (iubietotSuarchr)

I Fax Results: yes / _o Circle Deliverable:

C aIf / QC Suimina / Level I / 4e I Level 3 Level 4----1Sam ple Collection

'Tim e Zone Remtarks; Are there any known hazards applicable to thes samples? If so, please list the hazards 01Esce n~~rere~ (4L~fEastern 6ii Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinqirtshed By (Signed Date ,Time Reeie by(in DF -ate Time GEL PM: qI- (". , _71 rlt)$ I SO. Method orShipt~r.

ient: ,', IDatv Shipped: "/'" 2 2 lAirbill #13 13 lAirbill 11 Chairn ot("stody Nuanmber -Cltent Dltencied QC Codes: N -Nornial Sample. TB = Trip Blank. FD -Field Duplicate.

EB "Equipment Itlank. MS -Matrix Spike Sample. NISD = Matrix Spike Duplicate Sample. G = Grab. C -Composite 3.1 FcId Filtered:

For liquid matrices.

indicate with a -Y -for yes the sample was field liltcred or -N -fte stmple wa noat kitld lihcred.4.1 Matrix Codcs: DW-Di-king Water. .dwater. SW-Suaracc Water. WW-Wase Water. WWater. SO=Sil. SD-Sediment.

SL-Sludge.

SS-Solid Waste. O=Oil. F=Fihter.

P-Wipe. tuUrine, Flrccal. N-Nasal 5.1 Sample Requested:

Analytical method requested (i.e. 8260B. 601tlBfl470A a and nunbhr o'containert provided (bo each (i.e. 8260B -3. 601OB17470A

-I t.6h. Preservtlivce Type: IIA Ilydrochloric Acid. NI = Nitric Acid. SIt -Sodium Hydroxide.

SA = Sulfuric Acid. AA = Ascorbic Acid. IIX -lIkxane. ST -Sodiumn Thinmulale.

If n's preservative is added -leave field blank *WHITE = LABORATORY YELLOW -FI LE PINK -= CLIENT For Lab Receiving, Usc On/v Custody seal Intat e?YES N'O to4r Temap:/

-~~ofChi GEL Chain#-* her #;i.mber: i""GEL Work Order Number: icni flame: Phon P:oicc;iSite Name: Fax of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston.

SC 29407 Phone: (843) 556-8171 Fax: (843) 766-1178 e 4 itt 14-90 Sample Analysis Requested (s) (Fill in the number of containers for each test)#: 4V; -S4 k -113-77 5k, 5"r.. $WE Should this sample be considered:

S"ý5 , 'SMA 'ý-AINUI Q1 '1411>5 ,L.:N:d by: Send Results To: C C a C e a I-.0 E 5 C a a I-<- Preservative Type (6)Sample ID For conltpsites

-indicate start and stop date/time-l11 -I --1-- I t -____________________________________

'Dote Collcctcd (mm-drd-yy)

• Time Collected (Mlitasry) thhmm)QC (ode III F~ick lFiltcrctl i Sample Matrix 141 Y_D I-.I S~1/Comments Note: extra sample is required for sample' specific QC Gw 3~u \)o Y &Ai Requested:

Normal: Rush: '1:: SpeciY:LA..

\rNC (Subjieetto Surcharge)

Fax Results: Yes / CircleDelivrable:

CofA / Q/ L1evel3/ -Level+/- 4:ttt-'ks; Are there any known hazards applicable to these samples? If so, please list the hazards Soma CoMl ime SEastern o-)~\\ J~*, l.NtCB ~e'o ~O~\'t~tt)%

tJ8L~iJCentral Other____Mountain Chain of Custody Signatures Sample Shipping and Delivery Details At 0. ihe y Signed) Daic Q WA Time Received by (signed) Date Time I /4&i-i VVo 1 GEL PM: F-r\N %9rank&'Method of'Shipment:

re ' .I .IDate Shipped: "71\7 I/S 2 Airbill #: t I 3 Airbill #: , -',,lCustody Number -Clien D)etemincd , Nies: N -Normal Sample. TB -Trip Blank. Ft -Field Duplicate.

EB t Equipment Blank. MS = Malrix Spike Sample. MSD -Matrix Spike Duplicate Sample. C -Grah, C -Composite 1, N iltertd: tar liquid matrices.

indicate with a -Y -for yes Ihe sample was fid filtered or -N -for sample was not field lllhtted.S* %i,, Codes: DW-Drinking Water. GW-Gmundwater.

SW-Surltce Water. WW-Wastc Water. W-Watcr. SO-Sail. SD-Sediment.

SLSludge.

SS-Solid Waste. O=Oil. F-Fiter. P-Wipe. U-Urine. F-Fecal, N-Naal*,m,-, Atealyaig Requested:

Analytical method requested (i.e. 8260B. 6010817470A) and number or ctatainms prnvidcd tor each (i.e. 82600 -3. 6010/7470A

-I).Pc-, atioeTyIe:

HA -Ilydoochloriu Acid. NI -Nitric Acid.SH-Sodium Hydroxide.SA -SullrricAcid.

AA -Ascorbic Acid. HX -tlcxanc. ST-Sodiam Thiosullste.

trnoprscrvativc isadded -leave field blank WHITE = LABORATORY YELLOW -FILE,' PINK =CLIENT For Lab Receiving Use Onlp Custody Seal Intact?YES NO CooaleTamp:

Page: _ of Project#:

_ Q Q1'- GEL Chain GEL Quote N: COC Number ii: POC Number: G GEL Work Order Number: of Custody and Analytical Request GEL Laboratories.

LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-9171 Client Name: Phone #: 4L15 -4:'f-. "-- -Sample Analysis Requested ( (Fill in the number of containers for each test)eFa#: Shoutd ihis = <-- Preservative Type (6)PomSe mbe Fam:. ----I Address: G-71 % C.. .L fl .considered:

-a Y-. r,5, c.-, Comments Collected by: Send Results .: 4 , Note: extra sample is Noe extr -a*.utc Clteeted ".required for sample*oeCletd Collected QC Code Field Sample spciicQ Sample ID specific QD ID (Mitary) (' Filtered "I lvltui" "1 .-'For composites

-indicate start and stop date/time tmmdd-yy) (hthmml V -... .--,"g3 ...0-,-_'3,......

-,r

+ N+0--I- ....-------

_4 -152- J r2 3 -q 3 -n -5._ _ __S_ _. W2-___ __ ___ ___-__ 3, J -- . --- --45 -I'sc.- .a __,,A its5 I I 19 19!0,550 2. "x -TAT Re uested:Normal:

Rush: Specift r(subject toSurchrge)

Fax Results: Yes / Co .ircleDDeliverable:

Cof A / QC Summary / Level I / l Level 3 / Level 4.Remarks: Are there.any known hazards applicable to these samples? Ifso, please list the hazards Sample Collecion Time Zoneý",\ ý"\r ull atern Q(Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) Date Time Received by (signed) Date Time GEL PM: F'1"-n 5" -an.,.?...J 1-"4(/V S McthodofShip ent: Date Shipped: 77/b/2 Airbill M: 3 3 Airbill #: 1. Cthain ol'Cosiody Nuniber -Clien tueiem. iocd 2.) QC Codes: N -Normal Sample. TR -Trip tlank. FD = Field Duplicate.

E I Equipmeint Blank, NIS [ Matrix Spike Samiple. MSD -Matrix Spike Duplicale Sample. G = Grab. C = Composite 3.t Field Filtered:

For liquid matrices.

indicate with a -Y -far yes the sample wnas field filtered or .N -[or sample was not fieid 'ihered.A.) Marlri. Codes: DW=Drinking Water. GW-GroUndwater.

SW-Surface Water. WW=Waste Water. W"Waler, SO=Soil. SD=Sediaront.

SL-Sludge.

5S-Solid Waste. O-Oi. F-ither. P-Wipe. U-Urine. F-Fcal. N-Nasai 5.) Sample Aiaiyis K"qumted:

Anstlytintl method rnquested (i.e. 8260B. 60t1oB3f470A) and number of uconainers provided ior each (i.e. 32608 -3. d601081/7470.A

-1, 1.) Ircservic iv rype:; BA -Hydmehloric Acid. NI -Nitric Acid. SFi -Sodium tlydroexide.

SA -Sulfuric Acid. AA = Ascorbic Acid. IIX i Ixanv, ST -Sodium Th Iut'llite.

fo pr,cscrveuiyc i; added -lcave lield blank WHITE = LABORATORY YELLOW = FILE PINK = CLIENT For Lab Receiving Use Only Custody Seal Infact?YES NO Cooler Temp.IC ve of 1GEL Laboratories, LLC , : GEL Chain of Custody and Analytical Request 2040 Savage Road Qutote #: Charleston, SC 29407)C .,jmber : GEL Work Order Number: Phone: (843) 556-8171 IPk_ __, ___ber: ___O'_ __ý _Fax: (843) 766-1178 Cc';i; Name: .Phone #: Sample Analysis Requested ( (Fill in the number of containers for each test).,,.,:'SttName:

Fax 0: L4jt_ [ q,3 n Should ,hi "<- Preservative Type (6)samnplebe Au ---K's: $~ ~~{~;considered:

g Send esul..To:.

-, i- Comments by: Send Results To: Note: extra sample is Tm Z required for sample*Date Collected ri ._ fr Collected QC Code Field Sample cc specific QC Fo onpslsSample ID ( d (Miltlary)

(1) L izrc' Mai<~ ~ ~- I Far composites-indicate start and stop date/time (bhmm) l t_ _ _ _ __ J .----------

_ _ _ _ _ __-Z313C--

),S 1540 t 2-X X .!.. 1-. 4 q.5 5 I :ZX________________

>5Lj io'-. -L J' ------_ _ _ _FAV; keguested:

Normal: Rush: : .SbjecSurcharge)

Fax Results: Yes I iAcnitt'ks:

Are there any known hazards applicable to these samples? If so, please list the hazards Circle Deliverable:

C ofA I QC Summary I Level I "I Le4 / Level 3 1 Level 4, w 1 Samdle Collection Theie Zone Eastern Central Other _Mountain Chain of Custody Signatures Sample Shipping and Delivery Details'jished By (Signed) Date Time Received y (signd Date Time GEL PM: " 1 j L ( .530 *l 2',1-- MethodooShipment:

ef C Date Shipped: 2 .Airbill N: t3 lAirbill #: i-. I,'!

Nilumr -Client Determined Q( i des: N- Normal Sample.TB

-Trip Blank. FD = Field Duplicate.

EB = Equipment Blank. MS -MatrLS Spike Sample. MS0 -Matrix Spike Duplicate Sample. G = Grab. C -Composite illtred: For liquid matrices, indicate with a -Y -for yes the sample %was field filtered to -N -lor saumple was not field filtered.I. ;i,: K CKics: DW-Drinking Water. CW=Grotmdwalcr, SW-Surlacc Water. WW=Wastc Water. WWater. SO-Soil. SDeSdimntm.

SL-Sludge.

SS-Solid Wase. O-Oil. F-Filier, P-Wipe. U-Urine. F-Fecal. N-Nusal:,v, ;Analysis Requested:

Analytical method reque.-tcd (i.e. 82608. 6010817470A) and number of cootaincen provided v" each li.e. 82600 -3. 60108174T7tA

-I).I',, vative rypc: HA -Flydrochloeic Acid. N1 -Nitric Acid. SH -Sodium Hydroxide.

SA -Sullfuric Acid. AA -Ascorbic Acid. 11X -licxcn. ST -Sodium Thiofuicae.

I'(no presevative is added -leave field blank WHITE = LABORATORY YELLOW = FILE PINK = CLIENT For Lab Receiving Usie Onlv Custody Seal Intact?YES- NO C I r Temp:

Page: of GEL Laboratories, LLC Project 8: \1 O1'ý- GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote #: Charleston, SC 29407 COC Number i(l: G Phone: (843) 556-8171 PO Number: GEL Work Order Number:Fa:83)6617 Pi "mbr ll-]---Fax:

(943) 766-1178'Client Name: ' Phone #: ilAl -t4t- "42 Sample Analysis Requested

-(Fill in the number of containers for each test)Project/Site Name: UW Fax 4: iL4Iq -bt1\-. Should his Preservative Type (6)sample be n;-Address: consider'd:

" IC. Comments Collected by: ,f \ Send Results To: Z + Note: extra sample is a Dlcdcd id. required for sample Sample ID C(t = Matrix specific QC For corposiees-indicate .Ort and stop dot elf ine mm-dd-yy) lmm)_-2,- 0 -a,5 ___, -.3-2-~- 5k f_ I~Vtz~f -, 2 b^A__TTRqst:Noa:

Rsh

¢) Fax Results: Yes I Circle Deli#¢erble:

C ofa / QCSummar .. Level l / "/ Level 3 ILevel4.Remarks: Are there any known az rdapplicable to these samples? If so, please list the hazards [Sample Collection Time Zone*K U[w Central Other_ __-. .[Mountain Chaien of Custody Signatures Sample Shipping and Delivery Details I7, k* Ind ,\X 1,Aibll 2 DAirbilt I: 1. Chain ol'Ctsltdy Nutnibr -Client 2.1 QC Covdes: N = Ntrmnal Sample. TB =Trip Blank. FD -Field Duplcate.

EB -Equipment tlank, MS = Matrix.Ppike Sample. -Marix 'Spike t)uplitca Sample. G = Grab. C -Comrxsilc 1.) Field Filtcred:

Fr" liquid nmatriccs.

indicalc with a -Y -Ior yes the samnple tnws held 11itcred or -N -Icr sample tas not fihcritd.4.1 Matrix Codcks: DW=Driaking Wattr. GW-Grotndwatt.r.

SW-Sdrfacc Water. WW-Wastc Water. W-Water. SOSil. SO-Scdintcnt.

SLySludge.

SSmSolid Waste. O=Oil. F..=ilicr.

P-Wip. U-Urine. F-Fecal. N-Nasol 53 Sample Analysis Requerted:

Analytical mnelhod reque.sted (i.e. 8260a. 6010B'470A) and number ot'cuttaincrs ptnvidcd Vttr each ti.c. 82600 .3. 60111617470A

-I l.61t Presenative Type: ItA -Hydrochloric Acid. NI -Nitric Acid. SH -Sodium Hydraxide.

SA -Sulfuric Acid. AA -Ascorbic Acid. FIX z I Icanac. ST = Sodium l-hiotull-mc.

Ifnc presccativc is added c leave tfild blank WHITE = LABORATORY YELLOW = FILE PINK = CLIENT For Lab Receiving Ute Only Ctcrtody Seal Intact'?YES NO Cooler Temp: t4 c GELChi.:[ 1lote C u ' (.

'U N GEL Work Order Number: 2_, N) :wber: ýW " ,1 or i\ {iw;i'i Name: (. Phon PSite Name: Fax Ch Tv of Custody and Analytical Request GEL Laboratories, LLC 2040 Savage Road Charleston.

SC 29407 Phone: (843) 556-8171 Fax: (843) 7 6 6-1 1 7 8 e Sample Analysis Requested (s1 (Fill in the number of containers for each test): HIS-1;4ý-93-7g Should this sample be considered:

i( Lcc d by: Jk .Sample ID.For composites

-indicate start and stop datch Send Results To: -G- L -eO'LAo-0 1 o $. c.."'" r -*Dale Collected (mm-dd.yy),lime Collected (Military)(hhmm)QC Code Field') Filtered Sample Matrix "I1 U a a a 0 0 5-.0 E a a 0-I-I<-- Preservative Type (6)--I -t I --4 -F -I -2 LA Q Comments Note: extra sample is required for sample specific QC_ _ _ _ _ _ _ _ _ _ Y-- -.....~~2S-Y1 -+/-X C ,1 L,4 4, ,5)v i sC- RYem/'i A11,:uestedi Normal: Rush: 1 ,X- specif'y~

'( (SubjecitoSurchargo) lFax Results: Yes I c Circle Deliverable:

C ofA I QC Summary L Lvel I I Level I Level 4.Remark:,.!

Are there any known hazards applicable to these samples? If sa, please list the hazards Samole Collection Time Zone Eastern Central Other Mountain Chain of Custody Signatures Time Received by signed) Date Time:lai r)?Sample Shipping and Delivery Details GEL PM: 'jrC-'A -~~Method orShinment:

ý-tCL-,-1Date Shipoed: 7/or I..... .." -. ... ...Airhill fit 2 Airbill 9: 13 Airbill #: iot-aý ,"todyNumbernClicni Detennrned For Lab Receiving Use Only) ,: N -Normal Sample, TB -Trip Blank, FD -Field D)uplicate.

EB -Equipment Blank. MS = Matrix Spike Sample. MSO -Matrix Spike Duplicate Sample. C Grab. C "Compoxite i ,.-red: For liquid mutriccn, indicate with a -Y -for yes the sample was field tiltered or -N -1'tv sample was not field tiltercdc.

Claswod) Seal Intact?Cilcdei: DW-Drinking Water. CW=Ground.voer.

SW-Sutafec Water. WW-Waste Water. W=Water. SO-Soil. SO=Sedimen.

SLtSludle.

SS-'lid Wa.se. --Oil. -Filhr. P-Wipe. U-Urine, F-Fccal. N-Nasal YES NO A.I -nalysis ILequesteed:

Analytical method reiqucsted (i.e. 8260B. 6010/117470A) and number orcomtaincrs provided tir each (i.e. 82608 .3. 6010&/7470.A

-i). Coo t,:..-,,,,,e Type: HA -flydrrmehhric Acid. Ni -Nitric Acid. SH -Sodium Hydroxide-SA -SuIcOric Acid. AA -Ascorbl Acid. UX -I.texan,.-=

Sodium Thiosulfatc.

Irno prservative is added -leave field blank WHITE = LABORATORY YELLOW = FILE PINK = CLIENT Ea Laboratories uLc SAMPLE RECEIPT & REVIEW FORM Client: ISDGARCOC(ork Order: o1;10'304 4i-)7 c~!ta,)-~33 Received By: --IIDate Received:

7 -['-C;T'Srd Information

• If Counts > x2 area background on samples not marked "radioactive", contact SU ceda. Zthe Radiation Safety Group of further investigation.

COC/Samples marked as radioactive?

7"' Maximum Counts Observed*:

Classified Radioactive I1 by RSO? __ __COCSamples marked containing PCBs? 7_ _.Shipped as a DOT Hazardous?

Haz d Class Shipped: LN#-Samples identified as Foreign Soil?Sample Receipt Criteria Z .Comments/Qualifiers (Required for Non-Conforming Items)Circle Applicable:

Shipping containers received intact and seas broken damaged container laking container od (describe) sealed?Preservation Method 2 Samples requiring cold preservation blue ice dry ice nodn oar (describe) within (4 +/- 2 C)?Chain of custody documents included'with shipment?Circle Applicablt 4 Sample containers intact and sealed? als broke damagol cratier lak coainer otbu (desibe)Saaple ID's, cootinr affected and obselrved pH: Samples requiring chemical preservation at proper pH? If Preservation added, 6 VOA vials free of headspace (defined as Sample IDw and containes affcct<6mm bubble)?11 ye. immediately deliver to Volaziles labortory) 7 Are Encore containers present?Id's and tests affccwtd: 8 Samples received within holding time?mSample ID's on COC match ID's On Sample IDls and containm affected: bottles?Date & time on COC match date & time on bottles?Number of containers received maich ; les aU'C-1C: number indicated on COC?1 COC form is properly signed in relinquished/received sections?Commrnts: 1-2,6 5'7/V 9r 7 t (L7 *--PM (or PMA) review: Initials Y-"/4A1 Date : 1. 0f GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report for TRCS002 TRC Solutions Client SDG: 213274 GEL Work Order: 213274 The Qualifiers in this report are defined as follows:* A quality control analyte recovery is outside of specified acceptance criteria** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.Ul Gamma Spectroscopy-Uncertain identification Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.The designation ND, if present, appears in the result column when the analyte concentration is not detected above the detection limit.This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures.

Please direct any questions to your Project Manager, Erin Stanley.Reviewed by C.

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: August 11, 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-24-4.5 Gamma Proiect: TRCS00200 Sample ID: 213274001 Client ID: TRCS002 Matrix: Soil Collect Date: 17-JUL-08 10:40 Receive Date: 1 8-JUL-08 Collector:

Client Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Metho Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Drv Weight Corrected" Actinium-228 UI -0.00 +/-0.357 Americium-241 U -0.0245 +/-0.059 Antimony-124 U 0.026 +/-0.142 Antimony-125 U 0.0368 +/-0.139 Barium-133 U 0.0427 +/-0.0705 Barium-140 U 0.289 +/-0.456 Beryllium-7 U -0.195 +/-0.499 Bismuth-212 U 0.311 +/-0.467 Bismuth-214 UI 0.00 +/-0.232 Cerium-139 U -0.0109 +/-0.0349 Cerium-141 U 0.0285 +/-0.0859 Cerium-.144 U -0.232 +/-0.214 Cesium-134 U -0.0103 +/-0.0597 Cesium-136 U -0.074 +/-0.231 Cesium-137 1.23 +/-0.206 Chromium-51 U 0.456 +/-0.580 Cobalt-56 U 0.0501 +/-0.063 Cobalt-57 U -0.03 +/-0.0258 Cobalt-58 U -0.0239 +/-0.0669 Cobalt-60 U -0.0273 +/-0.0607 Europium-152 U -0.0119 +/-0.145 Europium-1 54 U -0.021 +/-0.184 Europium-155 U -0.0637 +/-0.0968 Iridium-192 U -0.0351 +/-0.049 Iron-59 U 0.0447 +/-0.156 Lead-210 U 0.521 +/-0.950 Lead-212 0.456 +/-0.128 Lead-214 0.442 +/-0.144 Manganese-54 U -0.0285 +/-0.0578 Mercury-203 U -0.0488 +/-0.0556 Neodymium-147 U 0.0155 +/-1.09 Neptunium-239 U -0.162 +/-0.190 Niobium-94 U -0.00447 +/-0.0574 Niobium-95 U -0.0684 +/-0.0899 Potassium-40 9.02 +1-1.50 Promethium-144 U 0.0318 +/-O.0604 Promethium-146 U -0.0195 +/-0.0645 0.324 0.0818 0.240 0.222 0.0998 0.769 0.796 0.767 0.249 0.0522 0.123 0.303 0.093 0.364 0.0872 0.963 0.111 0.0368 0.102 0.0953 0.200 0.291 0.145 0.0741 0.261 0.725 0.118 0.154 0.0915 0.0839 1.79 0.279 0.0913 0.133 0.884 0.101 0.0979 pCilg pCi/g pCi/g pCi/g pCilg pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g 0.100 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCifg pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g MJHI 08/07/08 1405 781879 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: TRC Solutions, Inc.Address 55 2nd Street, Suite 575 San Francisco, California 94105 Report Date: August 1], 2008 Contact: Mr. Moises Carvalho Project: Humboldt Bay NPP Project 161072, Task 2400 Client Sample ID: B-24-4.5 Gamma Proiect: TRCS00200 Sample ID: 213274001 Client ID: TRCS002 Parameter Qualifier Result Uncertainty DL RL Units DF AnalystDate Time Batch Method Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Radium-226 0.345 +/-0.232 0.154 pCi/g Radium-228 UI 0.00 +/-0.357 0.324 pCi/i Ruthenium-106 U -0.191 +/-0.479 0.747 pCi/g Silver-IOm U 0.0353 +/-0.0627 0.093 pCi/g Sodium-22 U -0.00755 +/-0.066 0.105 pCi/g Thallium-208 0.122 +/-0.0854 0.0879 pCi/g Thorium-230 0.345 +/-0.232 0.154 pCi/g (Thorium-234 U 0.602 +/-1.17 0.824 pCi/g Tin-I 13 U -0.0209 +/-0.0647 0.099 pCi/g Uranium-235 U 0.261 +/-0.246 0.319 pCi/g Uranium-238 U 0.602 +/-1.17 0.824 pCi/g Yttrium-88 U -0.0426 +/-0.0588 0.0793 pCi/g Zinc-65 U -0.0374 +/-0.137 0.215 pCi/g Zirconium-95 U -0.0359 +/-0.123 0.191. pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 BSWI 07/22/08 1137 781754 The following Analytical Methods were performed Method Description Analyst Comments EML HASL 300, 4.5.2.3 (.

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com.QC Summary TRC Solutions, Inc.55 2nd Street, Suite 575 San Francisco, California ReDort Date: August 11, 2008 Page 1 of 8 Contact: Mr. Moises Carv=Workorder:

213274 Parmname Rad Gamma Spec Batch 781879 QC1201639219 213274001 DUP Actiniurn-228 Arnericium-241 Antimony-124 Antimony-125 Barium-133 Barium-140 Beryllium-7 Bismuth-212 Bismuth-214 Cerium-139 Cerium-141 Cerium-144 Cesium- 134 Cesium-136 Cesium- 137 Chromium-51 Cobalt-56 Cobalt-57 Cobalt-58 Cobalt-60 alho NOM Samnle Oual OC Units RPD%REC% Ranee AnIst Date Time U] 0.00 UI 0.00+/-0.357 +/-0.279 U -0.0245 U -0.0242+/-0.059 +/-0.147 U 0.026 U 0.0494+/-0.142 +/-0,0687 U 0.0368 U 0.0619+/-0.139 +/-0.0993 U 0.0427 U 0.0236+/-0.0705

+/-0.0505 U 0.289 U 0.183+/-0.456 +/-0.391 U -0.195 U -0.398+/-0.499 +/-0.398 U 0.311 U 0.199+/-0.467 +/-0.341 Ul 0.00 UI 0.00+/-0.232 +/-0.124 U -0.0109 U -0.00143+/-0.0349

+/-0.0252 U 0.0285 U 0.0332+/-0.0859

+/-0.0563 U -0.232 U -0.073+/-0.214 +/-0.181 U -0.0103 U 0.00798+/-0.0597

+/-0.0429 U -0.074 U 0.0295+/-0.231 +/-0.163 1.23 1.20+/-0.206 +/-0.147 U 0.456 U -0.43+/-0.580 +/-0,446 U 0.0501 U -0.00669+/-0.063 +/-0.0435 U -0.03 U -0.0122+/-0.0258

+/-0.0198 U -0.0239 U 0.0368+/-0.0669

+/-0.0514 U -0,0273 U -0,00413+/-0.0607

+/-0.0411 pCi/g 18 pCi/g I pCi/g 62 pCi/g 51 pCi/g 58 pCi/g 45 pCi/g 68 pCi/g 44 pCi/g 21 pCi/g 154 pCi/g 15 pCi/g 104 pCi/g 1570 pCi/g 465 pCi/g 2 pCi/g 6810 pCi/g 262 pCi/g 84 pCi/g 944 pCi/g 148 N/A MJHI 08/08/08 08:21 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A (0%- 20%)N/A N/A N/A N/A N/A GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary (Woricorder:

213274 Parmname Rad Gamma Spec Batch 781879 Europium-152 Europium-I 54 Europium-155 Iridium-192 Iron-59 Lead-210 Lead-212 Lead-214 M anganese-54 Mercury-203 Neodymium-147 Neptunium-239 Niobium-94 Niobium-95 Potassium-40 Promethium-144 Promethium-146 Radium-226 Radiurn-228 Ruthenium-I 06 Silver- IOim Sodium-22 Thallium-208 Page 2 of 8 NOM Sample Qua] QC .Units RPD% REC% Range Anist Date Time U -0.0119 U 0.00413+/-0.145 +/-0.0981 U. -0.021 U -0.0795+/-0.184 +/-0.120 U -0.0637 U 0.0755+/-0.0968

+/-0.087 U -0.0351 U 0.0117+/-0.049.

+/-0.0367 U 0.0447 U -0.0472+/-0.156 +/-0.0984 U 0.521 U 1.54+/-0.950 +/-4.81 0.456 U] 0.00+1-0.128 +/-0.138 0.442 0.318+/-0.144 +/-0.128 U -0.0285 U 0.0244+/-0.0578

+/-0.0474 U -0.0488 U 0.0279+/-0.0556

+/-0.0433 U 0.0155 U -0.339+/-1.09 +/-0.989 U -0.162 U -0.0258+/-0.190 +/-0.139 U -0.00447 U -0.00647+/-0.0574

+/-0.0362 U -0.0684 U 0.0779+/-0.0899

+/-0.0589 9.02 7.19+/-1.50 +/-1.39 U 0.0318 U 0.0114+/-0.0604

+/-0.0382 U -0.0195 U -0.00427+/-0.0645

+/-0.0518 0.345 0.427+/-0.232 +/-0.124 UI 0.00 UI 0.00+/-0.357 +/-0.279 U -0.191 U -0.00615+/-0.479 +/-0.334 U 0.0353 U -0.00305+/-0.0627

+/-0.0435 U -0.00755 U -0.0299+/-0.066 +/-0.0429 0.122 0.169 pCi/g .412 pCi/g 116 pCi/g 2370 pCi/g 400 pCi/g 7290 pCi/g 99 pCi/g 29 pCi/g 33 pCi/g 2570 pCi/g 734 pCi/g 2.19 pCi/g 145 pCi/g 37 pCi/g 3070 pCi/g 23 *pCi/g 95 pCi/g 128 pCi/g 21 pCi/g 18 pCi/g 188 pCi/g 238 pCi/g 119 pCi/g 32 N/A N/A MJHI 08/08/08 08:21 N/A N/A N/A N/A (0%- 100%)(0%- 100%)N/A N/A N/A N/A N/A N/A (0%- 20%)N/A N/A (0% -100%)N/A N/A N/A N/A (0%- 100%)

~ij. ., GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com Workorder:

213274 Parmname Rad Gamma Spec Batch 781879 QC Summary pie Qual 0C NOM Samj Units RPD%Page 3 of 8 REC% Ranee AnIst Date Time Thorium-230 Thorium-234 Tin-113 Uranium-235 Uranium-238 Yttrium-88 Zinc-65 Zirconium-95 QC1201639220 LCS Actinium-228 Americium-241 Antimony-124 Antimony-125 Barium-]133 Barium- 140 Beryllium-7 Bisimuth-212 Bismuth-214 Cerium- 139 Cerium-141 Cerium- 144 Cesium-134 U U U U U U U+/-0.0854 0,345+/-0.232 0.602+/-117-0.0209+/-0.0647 0.261+/-0.246 0.602+/-1.17-0.0426+/-0.0588-0.0374+/-0.137-0.0359+/-0.123 42.9+/-0.0705 0.427+/-0.124 U -0.133+/-1.31 U -0.0176+/-0.0517 U -0.0574+/-0.166 U -0.133+/-1.31 U -0.0467+/-0.0487 U -0.0978+/-0.0935 U 0.0615+/-0.0807 U 0.378+/-0.940 45.2+/-4.13 U 0.00215+/-0.315 U 0.153+/-0.459 U 0.0074+/-0.177 U 0.533+/-1.28 U 0.210+/-1.80 U 0.486+/- 1.48 U 0.140+/-0.316 0.297+/-0.108 U 0.142+/-0.144 U -0.341+/-0.599 U -0.111+/-0.234 PCi/g PCilg pCilg pCilg PCi/g PCilg PC i/g pCilg pCi/g pCi'g pCi/g pCi/g pCi/g pdi/g pCi/g pCilg pCi/g pCi/g PCi/g Pci/g PCilg 21 314 17 313 314 9 89 760 08/07/08 14:06 (0%- 100%) MJHI 08/08/08 08:21 N/A N/A N/A N/A N/A N/A N/A 105 (75%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com Workorder:

213274 Parmname Rad Gamma Spec Batch 781879 Cesium- 136 Cesium-137 Chromium-51 Cobalt-56 Cobalt-57 Cobalt-58 Cobalt-60 Europium-152 Europium-1 54 Europium-155 Iridiumi-192 Iron-59 Lead-2 10 Lead-212 Lead-214 Manganese-54 Mercury-203 Neodymium-147 Neptunium-239 Niobium-94 Niobium-95 Potassium-40 Promethium-144 QC Sumi SamDle Oual (nary Page 4 of 8 OC Units RPD%. REC% Range Anist Date Time NOM 16.9 20.8 U 0.212 pCi/g+/-0.753 19.2 pCi/g+/-1.78 U -0.341 pCi/g+/-1.43 U -0.0625 pCi/g+/-0.253 1.39 pCi/g+/-0.225 U -0.0718 pCi/g+/-0.232 22.2 pCi/g+/-1.79 U 0,0691 pCi/g+/-0.387 U 0.448 pCi/g+/-0.362 U 0.00863 pCi/g+/-0.226 U 0.0863 pCilg+/-0.133 U 0.152 pCi/g+/-0.695 6.18 pCi/g+/-1.98 U 0.0239 pCi/g+/-0.176 U -0.0216 pCi/g+/-0.281 U 0.00684 pCi/g+/-0.219 U 0.00148 pCi/g+/-0.137 U -0.0613 pCi/g+/-2.82 U 0.225 pCi/g+/-0.472 U 0.0381 pCi/g+/-0.159 U -0.13 pCi/g+/-0.244 U 0.341 pCi/g+/-1.14 U -0.0518 pCi/g 114 (75%-125%)

MJHIl 08/07/08 14-06 107 (75%-125%)

(

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com Workorder:

213274 Parmname Rad Gamma Spec Batch 781879 QC Summary Samole Oual OC Page 5 of 8 REC% Ranee Anist Date Time NOM Units RPD%Promethium-146 Radium-226 Radium-228 Ruthenium-106 Silver-0 mOn Sodium-22 Thallium-208 Thorium-230 Thorium-234 Tin-I 13 Uranium-235 Uranium-238 Yttriumn-88 Zinc-65 Zirconium-95 QC1201639218 MB Actinium-228 Americium-241 Antimony-124 Antimony-125 Barium- 133 Barium-140

+/-0.161-0.0484+/-0.239 0.140+/-0.316 0.378+/-0.940 0.802+/-1.51 0.862+/-0.236 0.149+/-0.131-0.148+/-0.172 0.140+/-0.316-2.97+/-1.71 0.211+/-0.208-0.13+/-0.488-2.97+/-1.71 0.240+/-0.186 0.737+/-0.606-0.295+/-0.379 0.028+/-0.135 0.1.16+/-0.234-0.00941+/-0.097-0.0688+/-0.0883-0.0345+/-0.0453 0.0886+/-0.265 pCi/g pCilg pCi/g pCi/g pCi/g pCi/g pCilg pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCilg pCi/g pCi/g pCilg pCi/g pCig pCi/g MJH 1 08/07/08 14:06 U U U U U U 08/07/08 14:06 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Page 6 of 8 Sample Oual OC Units RPD% REC% Ranee Anist Date Time Workorder:

213274 Parmname Rad Gamma Spec Batch 781879 Beryllium-7 Bismuth-212 Bismuth-214 Cerium- 139 Cerium-141 Cerium- 144 Cesium-134 Cesium- 136 Cesium-137 Chromium-5I Cobalt-56 Cobalt-57 Cobalt-58 Cobalt-60 Europium-I152 Europium-154 Europium-155 Iridium- 192 Iron-59 Lead-210 Lead-212 Lead-214 Manganese-54 NOM U -0.27 pCi/g+/-0.292 U 0.107 pCi/g+/-0.278 U -0.0161 pCi/g+1-0.0825 U -0.0168 pCi/g+/-0.0232 U 0.0436 pCi/g+/-0.0537 U -0.00561 pCi/g+/-0.168 U -0.0153 pCi/g+/-0.038 U 0.0212 pCi/g+/-0.0911 U 0.0084 pCi/g+/-0.0305 U -0.231 pCi/g+/-0.344 U 0.00644 pCi/g+/-0.0409 U 0.00127 pCi/g+/-0.0219 U 0.00847 pCi/g+/-0.0368 U 0.0255 pCi/g+/-0.0401 U -0.0437 pCi/g+/-0.0955 U -0.0659 pCi/g+1-0.105 U 0.0576 pCi/g+/-0.0913 U -0.0131 pCi/g+/-0.0324 U -0.0286 pCi/g+/-0.0796 U -0.836 pCi/g+/-11.3 U -0.0136 pCi/g+/-0.0801 U 0.0084 pCi/g+/-0.0824 U 0.00592 pCi/g MJHI 08/07/08 14:06 (

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com Workorder:

213274 Parmname Rad Gamma Spec Batch 781879 QC Summary Sample Oual OC NOM Page 7 of 8 Units RPD% REC% Range Anist Date Time Mercury-203 Neodyrnium-147 Neptunium-239 Niobium-94 Niobium-95 Potassium-40 Promethium-144 Promethium-146 Radium-226 Radium-228 Ruthenium-106 Silver-I 10m Sodium-22 Thallium-208 Thorium-230 Thorium-234 Tin- 113 Uranium-235 Uranium-238 Yttrium-88 Zinc-65 Zirconium-95 U U U U U U U U U U U U U U U U U U U U U+/-0.0333-0.0151+/-0.036 0.156+/-0.612-0.145+/-0.178-0.0149+/-0.0338-0.022+/-0.0419 0.0696+/-0.405 0.0251+/-0.0331 0.0167+/-0.0385-0.0161+/-0.0825 0.028+/-0.135-0.0251+/-0.299 0.0038+/-0.0285-0.0188+/-0.0367-0.0202+/-0.054-0.0161+/-0.0825 2.14+/-1.93-0.00582+/-0.0397-0.0125+/-0.192 2.14+/-1.93 0.0123+/-0.0423-0.048+/-0.0729-0.0484 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g.pCi/g pCi/g pCi/g pCi/g pCi/g MJHI 08/07/08 14:06 GEL LABORATORIES LLC.2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

213274 Page 8 of 8 Parmname NOM Samole Oual OC Units RPD% REC% Ranee AnIst Date Time Rad Gamma Spec Batch 781879+/-0.0642 Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated M M if above MDC and less than LLD N/A RPD or %Recovery limits do not apply.ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.U1 Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable, for Radiochemistry.

h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five titnes (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.* Indicates that a Quality Control parameter was not within specifications.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary., (1 4~I

Location ISFSl 100m L-" Exclusion

),' .. Zone Unit 3 Restricted

-Area Boundary A, Approximately 30 Feet Separation New Fossil Plant (HBRP)from Unit 3 to HBRP Fence (Approximate)

I 9