ML16294A190

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Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey Conducted in 2014, Rev. 0, Appendix G, Part 1 of 11
ML16294A190
Person / Time
Site: West Valley Demonstration Project, P00M-032
Issue date: 08/22/2016
From:
MJW Technical Services
To:
Office of Nuclear Material Safety and Safeguards, State of NY, Energy Research & Development Authority, Office of Nuclear Reactor Regulation
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ML16293A155 List: ... further results
References
Download: ML16294A190 (35)
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{{#Wiki_filter:Appendix G-Area Certificates of Analysis Appendix Area 1 -COA GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: Address: Contact: Project: . ... -* *--* *-... *-* .. --..........

          • .. Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: MJW Corporation l 5 .Hazelwood Drive Suite I 12 Buffalo, New York 14228 Ms. Laurie Losey Soil Radioisotopes ... -**** ...... . I. l.C I 385101005 Soil 22-0CT-15 !"0:05 05-NOV-15 Client 32% Parameter MDC RL Gravimetric Solids ASTM D 22 ! 6 % Moisture "As Received" Moisture Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Actmium-227 r\ntimony-125 Ccsium-137 Cobalt-60 Europium-154 Protacumum-231 32 0 "Dry Weight Corrected" !J -0.598 +/-lJ 511 u 0.143 +/-0 176 3.64 ll fl.Oii l! 00401 lJ -0.936 +/-0 256 -r/-0.-0535 +/-0 155 +/-0.826 0703 .ii 346 0 108 0.112 0.31_6 I 27 074(! Radium-226 +/-0 216 0.200 0 777 Radium-228 +/-0 275 0.308 Tin-126 l.l 0 0572 +/-0 l 74 0. 191 Rad Gas Flow Proportional Counting GFPC, Gross A/B. solid "Dry Weight Corrected" 0.[()0 l\.l1Jh.a 12.6 +1-3 93 3.89 4 00 Beta 25.5 +/-3.89 3 57 IIJ.O !l1e __ __ .. Method Description Analyst br-Y So1i Prep... ... . *-.... "or): Soii"Prcp . . . ... -..... . L)'Ti .. . w.er.e. __ .. . .. ..... . .. .. ..... . . .. . . . . . . .. ... .. .. . ... . .. _ .........

          • ---....................

___ .. -** *-****** [ ASTM D 2216 (Modified) 2 DOE HASL 300, 4 5 2.3iGa-lll-R EPA 900.0iSW846 9310.iSM 71 JOB Modified Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma). Project Client ID: MJWCOOI 15 MJ\VCOOI Units_. . .... i?.f. __ __!)ate Time Batch. percent pCi!g pCi.'g pC1/g pCi/g pC1/g jJC1/g pCilg pC1/g pC1/g pCilg pCi/g L YTI 11110/15 0955 1521927 RXF2 12!03/l:'i 0825 1522386 JXB7 12/02115 1412 152576% Date Time Prep Batch 0955 *****152f927"""-*-*** ............

    • -.. ***-*-* **-..........

_ .. ........ . 2 3 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -{843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: Address: Contact: Project: ................... Client Sample ID: Sample ID: l\!latri.x: Collect Date: Rec*eive Date: Collector: Moisture: MJW Corporation* 15 Hazelwood Drive Suite l 12 Buffalo. New York ! 4228 Ms. Laurie Losey Soil Radioisotopes . -**** ....... -* -... l.2.CJ 38.5101006 Soil 22-0CT-15 !0:55 05-NOV-15 Client 24% . ... . .. . . .. . . ........ ___ .. _ . _ .. . .. RL Gravimetric Solids ASTM D 2216 %i Moisture "As Received" Mrnslure 24 0 Rad Gamma Spec Analysis Gammaspec. Gamma, Solid Dry Weight Corrected" Aclmium-227 ll -0.0837 -t/-0 370 Antimony-12.5 +/-0.151 [.l 00215 Ccsium-137 +/-ll.198 2 52 Cobalt-60 +l-0 .04(15 u 0.0114 Europtum-154 +/-0 13 3 u -0.0436

  • Protactimum-231

.,-/.1) 730 L' U.537 Radium-22.6 Radium-228 Tin-126 U Rad Gas Flow Proportional Counting {) 909 0 595 -00136 GFPC'. Gross AIB, solid "Dry Weight Corrected" Alpha 7 52 BS .. p_e1/()1:llll!d.:_ ... ,.() 223 +/.().287 +/-0 166 +/-3.29 +1-3.81 0.680 () 281 () 102 0 IOtl 0 0856 0245 I 32 0201 0.350 0262 3.92 400 3 69 10 0 Project: Client ID: percent pCifg p('iig pC1!g pC1/g p(."':'1/g pC1/g pCilg pCilg pC1/g pC1/g pCi/g MJWC001 l5 MJWCOOI l. YTI 11110115 0955 I 521927 RXF2. 12iU3115 0826 1522386 JXB7 12102/15 \412 1525768 Method Description Analyst Date Time Prep Batch

    • * *-*-**-*--
    • -*******-**or):
    • -***-***-******
  • .. -****-.. **-*** * "l>i'fl * ...............

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  • .. l)955 * **i si 19ii". *** .................
    • ***** -*** -* * **-** _

..... _ ......... __ ........ -*-_ -*** ........ .. . .........

      • -***---*

Methqtj . . . . .. . .. . . .. . .......... _ . . ... . .... . . _An11.J.l'st . .. _ .. . ASTM D2216(Mod1ITcd) 2 DOE HASL 300, 4523fGa-01-R 3 EPA 900. OiSWS46 93 IOjSM 71 IOB Mod 1ficd Notes: Counting Uncertainty is calculated at the 95% confidence level fl .96-sigma). 2 3 11

-GEL LAB ORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Contact: Ms. Lourie Losey Project: Soil Radioisotopes Client Sample ID: 1.1.C l Sample ID: 3&5101005 Matrix: Soi! Collect Date: 22-0CT-15 Receive Date: 05*NOV-J 5 Col!ector: Client Moisture: 32% Certificate of Analysis Rcpon Dote: December 17, 2015 Project: l\-UWCOOJ 15 Client ID: MJWCOOI .........

  • -.. . ...... . P:u---.unete r Result L)tcert:ti!l!Y

________ :Vl_D( __ . __ __ . _ _ Trr. _____ ... RL,_ Units __ Df_ ___ _I>atc ___ Ti1t1e. Gravimi:tric Solitls .-IS1JJ D 2216 % MoislUre "As Rt:cei1*ed" Mo1s1ure R11d Gam1t1a Spec Alrnlysh J2_0 Gammpspec. Gamma. Sofid "Dry Weigh! Corrected" Actmmm-227 ' U -(l.598 +1-0511 Antunony-125 U 0 143 +1-0 176 Bismuth-212 U 0.236 +l-0.678 Bismuth-214 0.740 +/-cl 216 Ccsmm-137 JM +/-ti 256 Cobalr-60 U !i tl1 I +/-0 05J5 Europium-15-1 U O 040 ! +/-0 155 Lcad-212 0.615 +/-0.142 Lead-214 0.910 +/-0 196 Potassium-40 I0.4 +/-1.92 Protacumum-231 Radium-226 Rad111m-228 Thallium-208 Tin-126 u tJ -0 936 0.740 0.777 0.121 00572 Rad Gas .Flow Proportional Counting GFPC G1*oss A.B. solid "D1:1* Weigh! Cprrec1ed" Alphil Reta 12 6 25.5 . Method Description . .. . ****** Dry*S(11J Prep Dry S(lll Prep GL-RAD*A-02 I Tbe __ __ _ Method Description ASTM D 2216 (Modified) 2 DOE l\ASL 300, 4 5 2 J/Ga-0!-R +/-0 826 f.().2]6

./.Q 275 +/-0.102 +/-0-17-1

+/-3-93 +/-3.89 3 EPA 900_0/SW846 93 !0ISM 7\ IOB Modified Surrogateffraccr Recovery Test 0.703 () 328 () 34& 0.162 !J3 0591 0.200 D.ll9Q(, 0 108 (l 049 {) 112 0.0476 (1.316 0.135 () 155 O_ll724 0403 II 193 0.958 0-396 I 27 0-589 0200 00906 "308 0.132 IW96R l)_[).\36. 0 191 0.0904 3-89 1.57 3-57 1 61 . . .. . **-** --. Analyst ................ L'lTI percent LYTl 11/\ll/15 0955 1521927 +1*0.585 pC1/g RXF2 12103115 0825 1522386 2 +i-0 188 pC1/g +1-0.687 pCi/g +/-0_226 pCtlg +/-tl-416 () 1(1{) pCilg +1-0.0538 pCilg -<-/-0 \56 pC1/g 152 pCilg. i-/-0.212 pCt!g +/-2.12 pC1/g -t-/-0. 952 pCi/g +f-0.226 pCi/g +/-0 Jlll) p('1/g +/-0.102 p('ilg +/-0 175 pC1/g +/.4_62 400 pCi!g JXB7 12102115 1412 1525768 3 +l-5 31 100 pCilg ... -*-*-**. **-!>ate Time Prep Batch ......... --***-* -*******-**-**** -***-* .... .... ... 11/IOflS 0955 1521927 ...... ... . . ******** ..............

            • -* ***-**** *****-****

Batch m ReCO\'Cry% Acccp!ablc Limits GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -{843) 556-8171 -www.gel.com . Company: Address: M.IW Corporation 15 Hazelwood Dri\*e Suite 112 Bu!Tnlo. New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 1.1.C I Sample ID: 385101005 Certificate of Analysis Report Date: December 17. 2015 Project: MJWCOOI 15 Client ID: MJWC_OO ! .. .Qu,nlilfcr. ...... ..... ...... ........ __ .... __ .. Tr..L ....... ... ... .Df. l}l_tlc __ Sur1*ogatc/Traccr Recovery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma). GEL LABORATORIES LLC 2*040 Savage Road Charleston SC 29407 -{843} 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 Huzelwoo<l Drive Suite 112 Buffalo. New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 1.1.C.2 388092001 Soil 22-0CT-15 23-DEC-15 Client 17.8% Sample ID: Matrix: Collect Date: Receive Date: Collector; Moisture: Parameter Gravimetric Solids ...... 911.al_ilil'.'.. -* 1JSTM D 2.216 % Moisture "As Received" Mornturc Rad Gamma Spec Analysis 17.8 Gammaspec, Gum ma. Solid "DIJ' H'eighr .Corrected" Actmmm-227 lJ 0.039 Antm1011y-!25 ll -0.0086 UI 0 OU 0.599 Cl.lS\UID-137 0.182 u -000744 Emopium-154. u 00456 1.cau-212 0.522 Lead-214 () 878 Potassium-40 9 so ProUictimum-231 lJ 0 00 Radium-226 0599 Radium-228 0.6f>3 Thall1um*20& 0 248 Tm-!26 u 0 0313 Rad Gas Flow Prupurticmal CiFPC, Gross A:B. solid 11 D1:1' Weight Carn!l'ted' 1 Alplla 9 22 Beta 14 3 }l.1_c:_ "'-cr.e_pcr..form_e_d .... Method Description Dry Soil Prep Dry Sml Prep GL-RAD-A-02 l .. :VIethod Description ASTM D 2216 (Modil1ed) 2 DOE HASI. 300, 4.5.2JiGa-01-R +/-0.193 +/-0 072 ;./.(l 40') +/-0l12 +1-0.0431 +1-0.0317 +/-0.0908 H-0 !04 +/-0 14(, +/-I 00 +1-0561 +/.() l 12 +/-0.230 +/-Q.0628 +l-0 0955 +/-l.49 +./-! 24 EPA 900.0!S\V846 93l0/SM 71 lOB Modified Surrogatc/frncer Recovery Test MDC Le 0.355 0 \69 0 134 0.0626 0.824 0.385 00%(> 00448 00264 IU)l 12 0 0.575 0.0256 0 180 . 0.08l3 0. !06 (). 0513 0106 00498 0 601 0 269 0.599 0 281 O.ll%(1 l) 169 0.0465 0 130 0 0448 () n759 \10215 0063 l 62 () 748 1.28 0614 TPl' +l-0 \94 +l-0 0721 .. f.tJ.471 +/-0 123 +/-0.0458 +/-0.0319 +/-0 0932 +/-0 113 +/-0 164 +/-1 30 +1-0 592 +1-0 123 +/-0.250 +/-0.0663 +/-0.0964 +/-2.31 +1-2.34 Analyst Date Report Date: January 2.0, 2016 Project: Client ID: MJWC00115 MJWCOOl RJ, l'nits ...

.\n'.11.Ys.t

.. Date Time Batch Mttl. pC1/g pCi/g pC1/g pC1/g 0.1()0 p('1/g pC1fg . pCilg pCi/g p(.'1lg pCifg pCi!g pC1/g pC1tg pCi/g pCi/g 4 00 p('ilg 10 0 pCi.1 g Time LYTI 12124115 0703 1533555 MJB I 12i29/15 1154 1533562 2 JXB7 01/11/16 1859 1534760 3 Prep Blitch LYTI 12/24-115 11703 1533555 Batch ID Reco,*c1j% Acceptable Limits GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -{843) 556-8171 -WWW.!;jel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite 1!2 BufTalo. New York 14228 Contact: Ms. Laurie Project: Soil Client Sample ID: l. l.C.2 Sample ID: 388092001 Certificate of Analysis Parameter Qualifier ....... R.csu_lt .... l'nc.er..ta_inty ...... MDC ...... I:c . Report Dare; Project: MJWCOO I 15 Client JD: MJWCOOI January 20. 2016 Surrogateffraeer Recovery Test Batch ID Recovcry 0 k Acceptable Lin1its Notes: TPU and Counting Uncertainty arc calculated at the 95% confidence level (1.96-sigma). -....;::;-'", GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 Ha:;o;clwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Lallrie Losey Project: Soil Radioisotopes Client Sample ID: 1.1.C.2 Sample JD: 388092011 Matrix: Soil Collect Date: 22-0CT-15 Receive Date: 23-DEC-l 5 Collector: Clieut Moisture: l Pa ram etc.-Rad Gmnma Spec Analysis c;ammaspec, Gamma, Solid "D1:v H-'eiglu Corrected" Acumum-227 0 189 +/-(J.366 Anmnony-125 u ().()0955 +f-0.0883 Bismuth-212 Ul 0 00 +/.] 04 Bismuth-214 {) 814 +l-1) 159 0.150 +/-0.0613 Cobalt-60 ll 0.00777 +/-0 0336 Europium-154 !J -II U0312 +/-0 l !3 Lead-2!2 0646 +/-0 I \9 Lead-2\4 0.946 +1-0.168 l'otassmm-40 9.18 +/-1.34 UI 000 +1-0.454 Ratlium-226 08l4 .,./.(1 [59 Radium-228 06&5 +/-0.271 Thallium-208

0. 191 +/-0 0609 Tm-126 UI 0.00 +l-00805 !!.if:!_ foll()wing.

l'rcp. . , . , ............. . Method Description Dry Soll Prep Dry Soil Prep GL-RAD-A-021 !_h1: .. 'Y.e1*e. Method Description DOE HASL 300.4.5.2 3/Ga-01-R Re<:overy Test Le 0420 0.196 0 168 0 0769 1 31 0.607 0 l19 0.0536 1).(1615 0.{]274 00701 0 0.298 0.220 0.0958 0.0981 00461 n.296 0 143 tl.716 llJl2 0 626 0.284 0.119 0.0536 0.223 0 0972 ll.0636 (J 0288 ll0794 0 0375 Analyst . *-*** LYTI Report Date: January 20. 20 I 6 Project: Client ID: MJWCOOJJS MJWCOOJ TPl' RL ll11its +/.() 37} pCi/g MJHI 01118116 1)627 I 534020 +/-0 0884 pCilg +/-1 25 +l-0 173 pCilg +/-0.0625 0.100 pCl/g +/-0.0338 pC1/g +1-0 113 pCi/.g +J-!l 148 pCi/g +1-0 I'll pC1lg +I-I 57 pCi/g +/-0.473 pC1/g +1-0.173 pCllg t-1-0291 pCill! +/-0 063 pCi/g +/-0 0823 pC1fg. . .. .. .. . . ***-* Date Time Prep Balch ..... -** ... *!2124/l.5 0703 1533924 Batch ID Recovery% Ac:ceptable GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8i71 -www.gel.com Company: Address: MJ\\' Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotapes Client Sample 10: 1..1.C'.2 Sample ID: 388092011 Certificate of Analysis ..... .. . . ...... ******** Report Date: Project: MJWC00115 Client ID: MJWCOOI January 20. 20 l 6 P:ir:imeter ...... Result ... . !\-'IJ)C Le ........ T..f:'.l! ......... _l_lL .... l:n.ils .. ll.F. .. .. M.ttL Surroii,atcffraccr Recovery Test Batch ID Recovery% Limits Notes: TPU and Counting Uncertainty arc calculated at the 95% confidence level ( 1.96-sigma). GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Ce.-tificate of Analysis Company: Address: MJW Corporation 15 HaLelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample fD: 1.2.C 1 Sample ID: 385101006 Matnx: Solt Collect Date: 22-0CT-tS Receive Date: 05-NOV-i5 Collector: Client Moisture: 24% Parameter Gravimetric Solids ASTJf D 2216 % Moi11ture Received Moisture 240 Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry Corrected" Actmium-227 \J -0.0837 **/-0 370 Anlimony-125 IJ 00215 +/.() \51 Bismuth-212 u 0.529 +/-0 674 Bismuth-214 0.909 +/.().223 Ccsium-137 2 52 +/-0.198 Cobalt*60 u 00114 +/-0.0405 Europium-154 LT -0.0436 +l*O 133 Lead-212 0.621 +/-0 130 Lead-214 0.926 +/-0.244 Potassrnm-40 11 7 +/-1 50 Prolactmrum-231 u 0 S37 +/-0 730 Radium-226 0.909 +/-0 223 Radium-228 0.595 +/-0.287 Thallium-208 0246 +/-0 090 Tin-12(> LI -0.0136 +/-0.1()6 Rad Gas Flow Proportional Counting GFPC. Gross :J.B. solid Dry Weight Corrected" Alplia 7.52 +/-3 29 Beta 24.5 Jh.i: f.o_l_Io_l.v.i!ll,1 ... . ... !\1ctho<l Description . . .. .. ..... **-.. -*-**.. -* . **-. ***--**--*-*-* .. -* ..... . Ory Soil Prep Dry Soil Prep U L-RAD-A-021 f[Jll(J1Vill,f,{ A1rn!r.t!c:1l _'.\'.t:'.:.e_

\1ctb11d Description

..... ASTM D 22 I 6 (Mo<l1Jicd) DOE HASL 300. 4 5.2.J.'Ga-01-R 2 3 EPA 900 O!SWS46 9310/SM 71 lOB Modified Surrogaterrracer Reco1*cry Test 0.680 0 281 I 36 ()201 0 102 0.085<-0.245 !) 153 0205 0 645 132 0 201 0 350 0 094(, n.2n2 3. 92 3 69 Project: Client lD: Report Date: December 17. 2015 MJWCOOl 15 MJWCOOI Le TPC RL (:nits OF Analvst Date Time Batch :VHd. 0 322 0131 0619 0.0931 0.0465 () 0363 0 l05 () 0727 0.0%3 () 257 0.621 () 0931 0.157 OJJ434 0.126 I SY 1.68 Analyst !.YTl

  • 000**** >O* ** OOHO 0 M >O 0 0 0 0 00000 0 ..... 00 0 ****** **** 00 ., 00 *** 0 00 0 ., 0 0 00 0 ... 0 percent LYTI 11/lQ.1150955 1521917 +1-0 373 pCi/g RXF2 l 2103.115 0826 152:;!386 2 +1-0 151 pC1/g +1-tl 717 pCilg +/-0 236 pCi/g +/-0.286 () 100 pC1/g +/-{) 0409 pCt/g +l-0 JJ4 pCi/g t-/.() 139* pCi/g +f-0 255 pC1/g +/-1 82 pC1/g "'-/-0 778 pCi/g +f-0.136 pCt/g +1-0.298 pCi!g +1-0.tl924 p('i/g +!-016.6 pCi!g, +/-3 63 4*00 pCt/g .JX!l7 1412 1525768 3 +1-5.17 100 pCt!g -*-* Date Time Prep Batch -* ... I III 1)/15 0955 1521927 Batch ID Recovery%

Acceptable I,imits GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843} 556-8171 -www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drh:e Suite 112 13uffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 1.2.Cl Sample ID: 385101006 Certificate of Analysis Report Date: December 17, 2015 Project: MJWCOOl 15 Client ID: MJWCOOl __ ........ *****-* ............... -*-*--** .. --***** .. -***--***-*-* .. *-** -*-* .... **-****** ..... -........ -****** **-*** ..... ***-*-. .......... . **-**-** **-*******-***** ..................................... -'** .. , ..... ' .. _ .. ____ . _____ .. ,, _ .... _ .... .... Le _. __ }ll,;. ____ Lt11.i1!1 .. ll.1'.'.. .. Surrogalcffraccr Recovery Test Batch ID Reco\'ery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma). GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -W"Ww.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 !*Ia:i:eh\ood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project; Soil Radioisotopes Client Sample ID: 1.2.C.2 Sample ID; 388092002 Matrix: Soil Collect Date: 22-0CT-l 5 Receive Date: 23-DEC-15 Collector: Client Moisture: 15.8% Result GraYimch'ic Solids i!STM D 2216 % Mois/l/re "As Rect'iw:d" Moisture Rud Gamma Spec Anal)*sis 15.S Gommaspec. Gamma. Solid "DI')' lFl!ight Corrected" Actinium-227 U !}.()35 +1-0.176 Antmiony-125 ll U.033 +/-0 0658 l31smuth-212 lJ IJ 00 +f-0 523 Bismuth-214 Cesmm-137 Cobalt-60

  • Europmm-154 Lead-212 Lead-214 Pornssmm-40 Protactmium-231 Rmhum-226 . Radium-228 Tbalhum-208 Tin-126 lJ lJ ll UI 0 605 0 139 (I 0124 0.{1494 0.715 0 812 13 n 0.110 n 605 0 456 0.226 000 Rad Gns Proportional Counting GFPC. Gross A. B, solid D1J* Weight Corrected" Bc1<1 170 fo_ll()Wi_n_g

__ P_:r.e.p ..... .\1ethod Description Dry Soil Prep Dry Sotl Prep GL-RAD-A-021 The following Anal)iical Methods W!;rC 11crformed

    • * * * * * *
  • iics.ci*i!>!iiiii
  • * ** * ** * * -* ** * * * ** * ***** ** ASTM D 2216 [:>.fod1fied)

DOE HAS!. 30G, 4.5.2 3/Ga-01-R +t-O 120 +!-0 0437 +f-0.03Q +f-0 128 +l-ll,132 +/-0 114 +/-1 ()6 +l-0 388 +f-0 126 +/-0 233 +/.().0531 +f.JJ lll7 +/-1.68 +1-145 EPA 900 OISW846 9310iSM 7! lOB Modified Surrc>gatc/Tracer Recovery Test 11343 0.128 0.&52 ()(1912 0.05\ 0.()606 0 tSO 00806 0.200 0.348 iJ5J(I 00912 () 00445 () 129 2 2') l.tW Le ... TPJ'.. 0.163 +1-0.177 00601 +1*0.0675 0400 +1-0.843 00422 +/-() 136 0.0236 +/-0.0452 0.0273 +/.(l.0305 0()818 +1-0.130 00385 +i-0.14(1 0 0972 +J-0 133 0 144 +/-1 53 0248 +1-0.431 0.0422 H-0.1311 00711 +1-0 24() 0.0205 +/-U.0563 0U625 +l-0 107 1 08 +/-2 09 0 818 +/-2.77 Analyst Date Report Date: January 20. 2016 Project: Client !D: MJWCOOl 15 MJWCOOl RL l'.nits Dr< Analnt Date Time Batch :\-1td. . ......................................

        • ' '* ....... '* ............... . percent LYTI 12124115 0703 1533555 p('1lg MJH I 12/29115 1154 1533562 2 pCi!g pC1!g pCilg 0 100 pCi/g pC1ig pCi/g pCi/g pC'i/g pC'1/g pCl/g pC1!g pCi/g pC1/g pC1/g 4.00 pCiig JXB7 Olil 1/16 1859 1534760 3 10.0 pCilg Time Prep Batch .. ******* .............. . I.YT! 12/24115 0703 1533555 Batcll JO Recovery%

Acceptable Limits GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact MJW Corporation 15 Hazelwood Drive Suite 112 New York 1.:/.228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 1.2.C.2 Sample ID: 388092002 l'arnmeter Surrogatcn'racer Recovery Test Notes: Certificate of Analysis Report Onie: January 20. 2016 Project MJWC00115 Client ID: MJWCOO l Le .... 'f P.t:. _. *-* *-_RL.. _ _D.f A11a_lyst ___ _Time .. .. Batch ID Rccm*cry% Acceptable Limits TPU and Counting Uncertainty are calculated at the 95% confidence level ( ! .96-sigma). GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 Hazelwood Drive Suite I 12 Buffalo, New York 14228 Contact: Laurie Losey Project: Soil Radioisotopes Client Sample IO: 1.2.C.2 Sample ID: 388092012 Matrix: Soi I Collect Date: 22-0CT-l 5 Receive Date: 23-DEC-15 Collector: Client Moisture: 15.8% Parameler Rad Gamma Spec Aualysis Gamma:;pec. Gamma. Solid "Dry 1-Veight Corrected Acnrnum-227 u 0017 +/-0 253 Antimony-125 ur 0 00 +/-0 0944 Bismuth-212 u 0.557 +1-U.587 Bismuth-214 D.730 +/-0 170 Ces!um-137 () l43 +/-() 063() Cohalt-6(1 u -0.00831 +/-2() 0.194 ().()851* 0434 0.187 () 104 0.0465 0 106 () 0501 J 97 1.60 3 05 l 35 Analyst ... __ ................................... . Dry Soil Prep Dry Soil l'rcp GL-RAD-A-021 .. ... Method Description 2 3 ASTM D22\6 (Modified) DOE HASL 300,4.5.2 J/Ga-()1-R EPA 90().0!SW846 93 IOISM 71 !0B Modified Surrogate{fracer Recovery Test LVTl Report Date: December 17, 2015 Project: Client ID: MJWCOOll5 MJWCOOI percent LYTI 11/10115 0955 1521927 +/-0.316 pC1/g RXF2 t:\103/!5 0826 1522386 2 +1-0 \()8 pCi/g +(-1 24 pCt/g +l-0 251 pCtlg *-1-0.148 0.!00 pC1/g +/-0.0664 pCt/g +l-0 202 pCt/g +/-I 04 4.00 pCi/r; +l-0 168 pCi/g +/-() 25\ pC1lg +/-2.58 pCilg +/-0.8\7 p(i/g +/-0 25 [ pCilg +/-0 423 pCi!g +/-0 ! I! pCrlg +/-00958 pC1/g +/-3.81 4 00 pClig JXB7 12'02/ l 5 1420 1525 768 3 +t-S 21 ]{) 0 pCilg Date Time Prep !latch l l/10!15 0955 1521927 Batch ID Recover}*% Acceptable Li111its --I GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive *Suite 112 Buffalo, New York 14228 Co11tact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 1.3.Cl Sample !D: 385101007 Certificate of Analysis P:ir:tmcter .. ....... _Result .. {P:C..cr.tai1_1h* .. Jvl_J!(. Le TPl' Surrogatefl.'racer Recovery Test Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma). Report Date: December 17. 2015 Project: MJWCOOl 15 Clien1 JD: MJWCOO\ RL ..... ... D_F __ A11!1l:p_t ___

\:ltcL Batch ID Accc1>tabfc Limits GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 * (843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York !4228 Ms. Laurie: Lose)' Project Soil Radioisotopes Client Sample ID: 1.3.C.2 Sample ID: 388092013 Matrix: Soil Colh'lct Date: 21-0CT-15 Receive Date: 23-D EC -15 Collector:

Client

  • Moisture:

21.6% Parameter Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry Wei1?111 Corrected" Actmium-227 u 0 166 +/-OJI I Antimony-125 u *0.0396 +/*O.l 16 Bismuth-2 l2 UI 0 00 +i-107 Bismuth-214 I 08 +/-0 170 Ccsium-137 0.482 +1-0 []947 Cobalt-60 u (I 0129 .,.1-0.0444 f,urcp*um-154 u 0.0122 +/-0 138 LeHd-212 1.07 +/-0 J3B Lead-214 I 31 +/-0211 Potassmm-40 14.2 f/-1 72 Protnct1111um-23 l \JI 0.00. +/-fl 623 Radium-226 I 03 +/-0.170 Radiuni-228 . I 02 +/-0 272 Thalhum-208 0 360 +l-0 093B Tin-121i lJI 000 +/-0.130 r.i:i:.e .. JV!ethods_ ____ ... Method .Description DI)' Soil Prep Dry Soil Prep GL-RAD-A-021 Le 0.595 0280 *0203 0.0928 1 59 0742 () 152 0.06&9 l) 0637 0.0279 0.0907 0 ()393 (l.268 O.l 18 () 126 () 0594 0.388 0.1&8 0.877 0.379 l 05 0,+90 0 152 006S9 0.309 0.138 ti 0771 0.035 0.209 0 IOI *Analyst !,YTI . _ .. . ..... .. .. . ... .. . ... ... . . ..... __ . Method Description DOE HASL 300. 4.5.2 3/Ga--01-R Surrogateffracer Recovery Test +/-0.321 +/.().118 +I-I 68 ... /-0.192 +/-0.102 +1-li 0448 +/-0. 138 .,./-0 162 +/../,) 234 +1-2 15 :..1.0 632 -+/-0. \92 .,.f-0.0985 +1-0 \31 Project: Cllent lD: Report Date: MJWCOOl 15 MJWCOOl January 20. 20 ! 6 RL . l:'n [t.s ... .I:>.F.: Analys_t ... 1)1_1 le_ Ti.r.nc .. Batch .. .. pCi.lg MJHI 01/18/16 0705 1534020 pC1/g pCi!g pCi/g 0 JOO pC!lg pCi/g pC1/g pC'ili; pCi/g pC!!g pC)/g pC1/g pCilg pCi!g pCtlg Date "Time Prep Batch -*-*-. . .. . ..... .... ... -.... . . ... ***-* ....... -..... ... . ........ . 12/24f15 U703 1533924 Batch JD Recovery% Acceptable Limits L GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843} 556-8171 -www.gel.com Company: Address: MJW Corporation l 5 I!azelwood. Drive Suite 112 Buffalo. New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioi5otopcs Client Sample JD: 1.3.C.2 Sample ID: 3&8092013 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOO 1 .... " . .......... .. . ........................ --** ....... -. .... ......... ...... . .. , ............................................ -....... , .. , ................ , .. , .. . January 20, 2016 ........ _ .... . . ...... .. -... l'.nce.rta.i11t.v ...... i>l!)C ...... ...... -* RL l;nils IW r\ni1lvst Dale Time B1ttch Mtll. ............

    • -* ,. . . .. . . .. .. -... . . .. . . .. . ....... , . . ....... . Surrogate!Tr:iccr Recovery Test Butch ID Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite l L2 13uffalo, New York 14228 Contact: *Ms. Laurie J ,osey Project Soil Radioisotopes Client Sample ID: 1.3.C.1 Sample ID: 388092003 Matrix: Soil Co!lect Date: 21-0CT-15 Receive Date: 23-DEC-l 5 Collector: Client Moisture: 21.6% Certificate of Analysis Project: Client ID: Report Date: MJWCOOl 15 MJWC001 January 20. 2016 Parameter .... . RcsuH ___ . ........ MDC Le . . .. ..... _DF .. .... Date . .. G r:ivimctric Solids ASTA-ID 12 J 6 % Moisture "As Receivl!d" Mmsture 216 Rail Gamma Spec Analysis Gammaspec, Gamma, Solid "D1:r !Veigf1t Corrected" Actinium-227 U -0.0784 +/-0.231 Antimony-125 lJ 00254 +/-00997 Bismutll-212 1.39 +l-0 700 Bismutii-214 0678 +/-0122 Ccsium-137 0 405 +/-0 067B Cobnit-60 U 0.0136 +/-!J.0426 l..:uropium-154 U -D.0175 +1-0 121 . *

  • I 06 +/.() 104 l.ead-214 Potassium-40 Protactmium-231 Rarlium-226 Radium-228 Thaltium-208 lJ 0.776 15.2 0.00 0 678 I 03 0.286. +/-0 142 +/-l 34 +f-0 728 +f-0 122 +/-0216 +/.() 0695 Tm-126 U 0.00 Rad Gas Flaw Proportional Counting.

GFPC. Gross A-8. solid "DI')' Ti'eight Corre,*1ed". Alpha 11 I +/-2 15 Beta 212 *-1-1.80 * .......... _ ... . ;\.let hod D.escription Dry Soil Prep Dry Soil Prep GL*R1\D-A-02 I 1:h.c _ .. __ ... Method Description ASThl D 2216 (Modified) DOE HASL 300, 4 5.2 3/Ga-01-R 3 EPA 9000.ISW.846 93 IO/SM 71 IOB Modilied Surrogatcffracc .. Recovery Test 0.413 () 166 n 852 (). 114 0 0658 0 0739 0.217 0.0882 0.129 0.547 0769 0l14 () 215 0 0568 0.111 2.78 2 19 0.1% 0.0782 0.394 005:'.l (I 0306 00332 ll.098i 0(142 00612 0.236 IJ 364 0.0531 0.0974 ll.0263 0.0534 I 31 1.06 Analyst ********-**** --* .......... . LYTl +l-0 234 +/-0 JOO +/-0.713 +l-0.134 +1-0 0752 +l-0 043 +l-0 12.l +/-0.140 +/-0.157 +/-1.R7 +/-0 762 +l*O 134 +/-0.260 +/-(1.(1735 +/..{] 115 +/-3 06 +/.J.53 Date 12/24115 percent LYTI 12i24/l5 0703 1533555 pCtlg MJHI 12129115 \ 154 1533562 2 pC1/g pC1.lg pCt/g () 100 p('tlg pC11g. pC1tg pCi/g pC11g pCi/g pC1/g pC1lg pCi!g pCi/g pCilg 4 00 pCtlg JXB7 Ol fl 1/16 1859 1534760 3 HI Cl pC'1/g. Time Prep Batch 0703 1533555 Batch![) Recovery% Acceptable Limits I I I GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite I 12 Buffalo. New York 14228 Contact:

  • Lnurie Losey Project: Soil RJldioisolopes Client Sample ID: 1.3.C.2 Sample ID: 388092003 Parameter Surrogate/Tracer Recovery Test Notes: Certificate of Analysis Le TP!J and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).

Report Date: Januai-y 20, 2016 Project: MJWCOOi 15 Client ID: MJWCOOI . Y.*i.its . .D.-1'... .. .. _ . .l\l,td:. Batch ID Reco\*ery% Acceptable GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.get.com Certificate of Analysis Company: Address: Contact: Project: **-*

  • H*** *OOOO O*OOO OOOOO*o*****'*

0 H0 .. 0* Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Moisture: Parameter Gravimetric Solids MJW Corporation 15 Hazelwood Drive Suite I 12 Buffalo, New York 14228 Ms. Laurie Losey Soil Radioisotopes l.3.C5 385101008 Soil 2 l-OCT-l5 09:40 05-NOV-15 Client 39.7% ASTM D 2216 % Moisture "As Received" Moisture 39 7 Rad Alpha Spec Analysis ASP Plutonium lsotopic, Solid "Dry Weight Corrected" [>lutomum-238 U -0.0042 +/-0 0363 f'lutomum-239/240 ll 0 0\47 +/-0 0734 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 U 0 0644 +/-0 127 Uramum-233i234 0.656 +/-0 320 Uranium-2351231;i U O 0709 +/-0.121 Urnmum-238 0 954 t/-0 367 Alphaspec Np237, Solid "D1y Weight Corrected" Neptumwn-237 U -0 146 +/-0 252 Alphaspec Th229 + 228,230.232 Solid "Dry Weight Corrected" Thorium-228 I 40 +/-0 595 Thonum-229 U -0 0406 +/-0 122 Timrium-230 0 8()3 .. /-0.444 Thonum-232 0 616 +/-0.381 Am241, Cm Solid ;'Dry Weight Corrected" Amcncium-241 lJ O 0173 +1-0.0593 Curmm-242 U -0.00457 +1-00394 Curium-2431244 ll -0 0119 +1-0 0359 Cunum-245/246 l: 0 0382 +1-0.0654 Liquid Scinl Pu241, Solid Dry Weight Corrected" Plutonium-241 U -\ S2 +/-5.SO Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" lodine-129 lJ O 130 +/-0 576 Gammaspec, Gamma. Solid "Dry Weight Corrected" Actimum-227 1; 0.18 I -;-/-0 . .293 Antimony-125 l; 0 06D3 +/.() \O\J Ccsium-137 CJ 481 +/-0 110 Coball-60 l) -0 00427 +f-Q.0412 Europium-154 l! * -0.0!18 +/.() 149 U (l 0888 +/-0.620 MDC 0 084 0.147 0.225 0.261 Cl.106 ll.106 0.714 CJ.449 ll.344 0.343 0.168 011() II 0913 fLIOl () 0573 10.l (] 92& 0 56l! ll 213 0.0796 0(l7RR 0.277 I (J3 RL 1 00 I 00 I OD I 00 I 00 1 on l 00 I 00 l 00 100 1 00 1 00 t 00 1 ao l (l(I 15.0 IUD 0 100 Project: Client ID: Units percent pC'1/g pC1!g pc1lg pct.lg pctfg pr:i/g pCilg pCrlg pCilg pC1lg pC1/g pC1lg pCilg pC1/g pCilg pCilg pC1/g pCtlg pCilg pCtlg pCilg pC1/g pCilg Report Date: December 4. 2015 MJWC00!15 MJWCOOl. L YTI 11/\(}/I S 0955 1521927 HAKB 11/23115 1502 1522517 HAKB 1 l/24/15 0851 1522580 HAKB T l/23115 17 fl 1522576 HAKfl 11/24/15 11114 1522579 HAKB l l/24115 1039 1.522571 llAKB 11125/15 1739 1522578 MJHI 12/021!5 1805 1522374 RXF2 12/03/15 0827 1522386 l 4 5 6 7 8 9 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December4, 2015 *Company: Address: Contact: Project: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Soil Radioisotopes .. .. ..... .. . -***-*-*-....... *-** .. *-****-**-* .... . Client Sample ID: 1.3.C5 Sample ID: 38510100& Rad Gamma Spec Analysis

  • Gammaspec, Gamma, Solid "D1y Weight Con'Ccted" Radium-226 0 803 +/-0 169 () 156 Ra<lium-228 0 665 +l-ll.382 OJOO Tm-126 U! 0 00 +/.(). \6J O.IJO Rad Gas Flow Proport[onal Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha 9.43 +/-3.61 3.99 Beta 27.0 +1-346 152 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 U -0.321 +/-0.8S9 1 76 Rad Liquid Scintiflation Analysis LSC, Tritium Dist, Solid "DI)' Weight Corrected" Tntium t; 2.71 +l-2 71 4.45 Liquid Scint C' l 4, Solid "Dry Weight Corrected" Carbon-14.

U -0 459 +/-0 768 1.32 Liquid Sein.! Tc99, Solid Dry Weight Corrected" Tcchnetium-99 U I 57 +/-2 OIJ 338 .. .. __ ...... _ ........ -* Method Description oi-y soii>rep.

  • * **** ori sO:ifi>rcii Project: Client ID: MJWCOO!l5 MJWCOO! ... ..........

.... . ................... pC'*lg pCilg pCtlg 400 pCilg JXn7 12f02/l5 ]l),() pCtlg 2 ()() pCi.lg KSDI 12/02/15 I> ()CJ pC1/g TXJI 12!0211 s 2 00 pC1lg TXJI 12104/15 5.00 pCilg MY!\11 11/29/15 Date Time Prep Batch .. iiifoh5 (l\155 1521927 1422 1525768 LO 1710 1525755 II 1944 1522724 12 0357 1522716 13 1349 1522715 14 GEL LABO RA TORIES LLC *2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 Hazelwood Drive Suite l 12 Buffalo, New York !4228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes

    • -* .... -.......................

-................... . Client Sample ID: l .3.C5 Sample ID: 385101008 _ __ __ . _ .... .......... . . . ... . . .. . .. . .. ... ... . . ... . Qll_.... . ........ . 2 J 4 5 6 7 8 9 lO ll 12 l3 14 i\STM D 2216 (Modified) DOE EML HASL-300. Pu-I !-RC Modilkd DOE EML HASL-300, U-02-RC Modilicd ASTM C 1476-00 Modified DOE EML HASL-300. Th-OJ-RC Mod1Jied DOE EML HASL-300. Am-05-RC Modified DOE EML HASL-300. Pu-1 I -RC Modified DOE EML HASL-300J-Ol Modified DOE HAS\. .100, 4 5 23/Ga-Ol*R EPA 900 OiSW846 93 !0ISM 7l IOJ3 Mod1f1cd EPA 905.0 Mod1ficdiDOE RP501 Rev 1 EPA 906.0 Modified EPA EERF C-\)1 Modified DOE EML HASL-300. 'fo*U2-RC' Modified Test Result Plutonium-242 Tr<.icer ............................................................................

      • -** llranium-232 Tracer !Jranium-235/236 Tracer Amcricmm-243 Tracer Aclmium-22 7 Tracer Americium-243 Trru::cr Plutomum-242 Tracer Stronlium Carner Tcchnctirn11-99m Tracer Notes: ASP Plutomum !sotop1c, Solid "Dry Weight Corrected" ASP Uiamurn Solid "Dry Wc1gh! Corrected" ASP Uranium lsotop1c_

Sohd "Dry Weight Corrected"' Alphaspcc Np237, Solid "Dry Wc1gln Correcccd" Alphaspec Th229 + 228,230.232 Sohd Dry Weight Corrected" Am24 I, C't11 Solid "Dry Wcigln Comx:lcd" Liquid Scmt Pu24 l, Solid Dry Weight Correc1cd Gl'l'C, Sr90, solid "Dry Weight Corrected" L1qu1d Scint Tc99, Solid "Dry Weight Counting Uncet1ainty is calculated at the 95% confidence level ( 1.96-sigma). Project: Client ID: Report Date: December 4. 2015 MJWCOOI 15 MJWCOOI _ ...... -* 84.:5 (15%-125%) 42 (15%-125%) 64.9 (15%-125%) 86.2 (15%-125%) 89.2 (15%-125%) 88 3 (15%-125%) 84 . .5 (1.5%-125%) 86.7 (25%-l2S%} 94 5 (l5%-125%i GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 .. (843) 556-8171 -www.gel.com Certificate of Analysis Compan>*: Address: MJW Corporation 15 Halclwood Drive Suite 112 Buffo.lo. New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotor-:s Client Sample ID: l .3.C5 Sample ID: 385101008 Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 39.7% Parameter Gravimetric Solids Result . [\-:I.Dr .... J,.c. . . .... .. IP.t.: .. ASTM D 2216 % Moisl!Jre As Received" Moisture 397 Rad Alpha Spec Analysis ASP Pi11to11i11111 Isotopic. Solid "Dry Weight Corrected" Plutonium-238 ll -0 0042 +!-0036.3 (I 084 0 0157 i/-0 0363 Plutomum-239/240 u 0.0147 t/-00734 (J t.17 (J0.171 +l-0 0734 ASP Ura11i11111 Jsotopic, Solid "Dry 1-f'eight llranium-232 lJ 00644 +1-0 127 0225 00853 +l-0 128 Uranium-:!331234 0.656 +/-0 320 0.261 00777 +/.() 355 Urnrnum-2351236 007t)<) t/-0.121 0.106 l)I)[) +(-0 123 Uramurn-238 () 954 367 O.Hl6 0.00 +f-0.429 tflphaspec .Vpi37, Solid "D1:1* TVeight Corrected" ll -0.146 '!-/-0.252 0714 0 241 +1-0252 .4.fphaspec Tl1229 ;-228:230.232 Solid "Dr.i* Weighr Corrected" Thonum-228 140 595 t'J.449 (\ \38 +/-0.631 Thonum-229 lJ -0.04011 +-1-0 122 0 344 () ()876 +.'-0.123 Thonum-230 0.803 +l-0 444 0.343 00874 Thonum-232 ()616 +/-0.381 O. lfi8 000 +1-0 392 AmUJ, Cm Solid "Dry Weig/it Corl'ected Amcncium-24 I u 00173 +/-0 0593 (l.l]O 00299 +1-0 0:593 Curium-242 u -0 00457 +1-0.0394 0 0913 00171 +1-0 0395 Cunum-243i244 u -ll.0119 +/-0.0359 0 WI 0 025(> +/-0 0359 Curmm-2451246 0.0382 +1-0Q(,54 00573 0.00 +f-0 0656 liquid Seim Pit24 I. Solid "Dry Weight Corrected Plutonium-241 ll -1.82 +/-5.80 10.1 4.92 +/-5.80 Rad Gamma Spec Ane.lysis Gamma I I 29, Solid "Di:v Weight Comxted" lodme-\29 u 0 130 +/-0 576 0.928 0 4::!8 +l-0 576 Gammaspec. Gamma, Solid "Di:v Weight Corrected" Actmium-227 ll 0 181 +/-0 293 () 568 () 265 +l-0 305 Anlmwny-125 ll 0.0603 +/-0.109 0.213 0.0971 +/.() 112 Brnmuth-2 J 2 1.39 +/-0.906 I 12 0 499 ... /.() 916 Bismuth-214 0.803 +/-0 169 0 156 00704 +/-0.181 0.481 +/-0. l 10 *o.u796 0 0354 +/-0.117 Cobalt-60 lJ -0.00427 +-/.() 0412 0.0788 0.0327 +/-0.0412 Europmm-154 ll -00118 +l-0 149 0.277 0.120 */-0.149 Lcad-212 0.928 +/-0 127 0 112 0 0522 +/-0 148 Lcad-214 l OS +/-0 188 0 .l84 (J 185 +f-0 :W6 Report Date; December 17, 2015 Project: Client lD: MJWCOOJl5 MJWCOOI percent L YT! I I /10/1 S 0955 15219i7 l 00 pC1lg HAKB 11123115 1502 1522577 2 I 00 pC'ilg l.00 pci/g HAKB 11124115 0851 1522580 3 l.Oll pc1/g 1.00 pcilg I 00 pci/g 1 00 pCi!g HAKB 11123115 1711 l 522576 4 I 00 pC1lg HAKB 11/24115 1014 1522579 5 1.00 pCi/g I 00 pCi!g ll\O pC1/g 1.00 pC1/g HAKE l 1124115 1039 152257,l 6 l 00 pCi/g \ 00 pCslg l.00 pCilg IS 0 pCi!g HAKB 11125115 1739 1522578 7 100 pCilg MHll 12/02/15 1805 1522374 8 pCi/g IL'XF2 \2/03/15 0827 1522386 9 pC1/g pCi!g pCilg 0 100 pC1/g pC!/g pCilg pCt!g pCs/g Company: Address: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com MJ W Corporation 15 Hazelwoml Drive Suite! !2 Certificate of Analysis Buffalo, New York 14228 Report Date: . December 17, 20 l5 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: l.3.C5 Sample ID: 385101008 Parameter Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "D1:v Weigli! C01*1*ected" Potassium-40 14.2 Pmtnctinmm-23 l U 0.0888 Radium*226 Radium-22.8 Thallium-208 Tin-126 U! Rl'ld Gas Flow Proportional Counting 0.803 0.665 0.354 000 GFPC.. Gross A-'B. solid "Dry Weig/rt Corrected" M* Bem .27.0 GFPC. Sr90. solid "Dr,\' Weight Correc1ed" Strontium-90 U -0 321 Rad Liquid Scintillation Analysis LSC. Tritium Dis1, Solid "Dry Weig/rt Corrected" Tritium 2 71 liquid Seim Cl 4. Solid "DI')' Weig/It Corrected" Carbon-14 U -0.459 liquid Scint Tc99. Solid "Dry WeiRhl Corrected" Techncuurn-99 U 1.57 . Description Dry Soil Prep DI}' Sml Prep GL-RJ\D-A-02 l +/-l.66 +/-0.620 t/-(l.J 69 +l-0 382 +/-0.0817 +/-0.163 +1-3 61 +1-3 .i6 +/-0.889 +1-171 +l-200 __ _ Method Description 2 3 4 5 (l 7 8 9 10 II 12 13 ASTM D 2216 (Modified) OOE EML HASLoJOO. Pu-11-RC Modified DOE EML l!ASL-300, U-02-RC ASTM C 1476-00 Modilicd DOE EML HASL-3UU, Th-CH-RC Modified DOE E"ML HASL-300. Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASl.-300.l*O I Modified DOE HASL 30(), 4 5 2.3/Ga-01-R EPA 900.0.iSW846 93!0iSM 71 IOB Modified EPA 905.0 Modified/DOE RP50\ Rev 1 Modified EPA 9{)6 0 Modified EPA f.ERF C-0 I Modified 0 8C>7 0 336 +/-2.to 1.03 ll.475 +/-0 621 0 15(1 () 0704 +l-0 181 030() (J 132 +1-U 393 !Ui70ol [J.(l312 0867 0 130 ll.0612 +/-0.165 3 99 16! +/-4.06 2 52 I 12 +/-5.28 1 76 0 7S3 +/-0.889 4 45 1.93 *H-2 71 1.32 0.651 +/-0.768 3 38 I 63 +1-2 01 . .............

  • -**. Analyst Oatc ........ Project: Client ID: MJWCOOJ15 MJWCOOI 400 10 u 200 6(1(1 2.00 5.00 pC1tg pCrlg pC1lg pC1tg pCi/g pC1 1 1r pCtfg pCi/g pCilg pC'1lg pCt/g pCi/g . .............

Time JXB7 KSDJ TXJI TXJ1 MYM I . .. Prep B:itch l2i02f\5 1422 1525768 12102115 1710 1525755 \2/02/15 1944 1522724 \2i04/\5 0357 1522716 11/29115 1349 1522715 ..... -*-**-**-*******"'"' -* .. -..............

    • -* *-. -*-*-***********

-** *-**--*-**** -* ... .................

          • LYTI I 1/l0Jt5 0955 1521927 IO 11 12 13 \4 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -{843) 556-8171 -www.gel.com Company: Address: Contact: MJW C'orp()ration 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 l\*fa. Laurie Losey Project: Soil RadiC1isotopes Client Sample ID: l.3.C5 Sample ID: 38510!008 Certificate of Analysis Parnmeter J.c 14 DOE El\IL HASL-300, Tc-02-RC' Modified Sun*ogatcfl"racer Recovery Plutonhnn-242 Tracer llranium-232 Urnniurn-235/236 Tracer Americium-243 Tracer Actinium-227 Trnccr Amcricium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technelium-99m Tracer Notes:* Test ASP Plutonium Isotopic.

Solid "DI}* Weight Corrected" AS!' Uranium Isotopic. Solid "Dry Weight Com.>c!ed" ASP Uranium Isotopic. Solid "Dry Weight Corrected" Alphaspec Np237. Solid "Dry Weight Corrected" Alphaspcc Th229 + 228,230,232 Solid "Dry Weight Corrected" Am24 L Cm Solid "Dry Weight Corrected" Liquid Sein! Pu24 l. Solid "Di) Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99. Solid "DI)' Weight Corrected" TPU and Counting Uncertainty are calculated at the 95% confidence level { 1.96-sigma). Project: Client ID: Report Date: December 17. 2015 MJWCOOl 15 MJWCOOI Batch ID Recovery% Acceptable Limits 1522577 84.5 ( 15%-125%) 1522580 42 (15%-125%) 1522580 64.9 (15%-125%) 1522576 86.2 (15%-125%) 1522579 89.2 (15%-125%} 1522571 88.3 (15%-125%) 1522578 84.5 (15%-125%) 1525755 86.7 (25%-125%) 1522715 94.5 (15%-125%} GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) -www.geLcom Certificate of Analysis Report Date: December 4, 2015 Company: Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector; Moisture: MJW Corporation ! 5 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Soil Radioisotopes ..... -** . 1.3.C6 385101009 Soil 21-0CT-!5 09:55 05-NOV-15 Client 23.6% ................ __ _ _ Result UncMainty lVIDC ****-****

      • -*-** **-** .... ***-****-*
                    • .

Gravimetric Solids ASTM D 22 l 6 % Moisture "As Received" Moisture 23.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic. Solid "Dry Weight Corrected" Plutomum-238 lJ 0.00979 . +/-0 0544 Ptutonirnn-2391240 U 0.00677 +/-U 0799 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 lJ 0.0473. +/-0.121 Uranium-2331234 0 799* +1-0 30 I IJranmm-2351236 U 0 0469 /-0 0921 Urnnium-238 I 14 +/-0 345 Alphaspec Np237, Solid "Dry Weight Corrected" Ncptunium-237 U -0 0342 +/-0 236 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thomim-228 0 984 +/-0 482 Thormm-229 U 0 131 +/-0 207 Thormm-230 l.lti +!-{l.498 Thorium-232 0.979 +1-0.452 Am241,.Cm Solid "Dry Weight Con*ected" t\mencium-241 U 0.0315 +/-0 062 C11rium-242 U 0 00 +/-0 0412 Cunum-24 3/244 U 0 00921 +/-0. 0512 Curium-2451246 U 0.0361 +/-D 0709 Liquid Scint Pu241. Solid "Dry Weight Corrected" Plutonmm:241 lJ -2 07 +/*6 40 Rad Gamma Spec Analysis Gnmma I129, Solid "Dry Weight Corrected" lodine-129 U 0.214 +/-0.383 Gammaspec, Gamma. Solid "Dry Weight Con*ected" Actmium-227 l! -0.478 +/-0 4M Antimony-125 U 0 0263 * +/-0 202 Cesium-137 O 357 -ti-0. \22 Cobalt-60 U -0 0195 t/-(J.081<1 Europium-I 54 U co ()()356 +/-0 241 Prolactinium-231 lJ 0 80 I +/-0 980 0 !04 0 168 fJ 222 0 214 () 128 0.0796 0 575 0 395 0 287 0 280 0 155 (}.0859 00613 0 098l ()()'}83 11 2 0.76') 0 775 0 361) 0178 () 153. O 46B I 81 Project: MJWCOOll5 Client JD: MJWCOOJ * . ..... *-______ .... _ ... _ J::)ate Time Batch Method I !HJ I 00 I 00 I 00 I 00 I O!J I 00 I 00 l.Q{) I 00 I 00 I 00 1.00 I 00 I 00 150 I 00 !l 100 percent pci!g pcilg pc1lg pc1lg pCifg pC1/g pC1lg pCi!g pC'1/g pC1lg pC'1!g pCt/g. pC1/g pCi/g pCi/g pCtlg p('Jlg pC'ilg µCtlg pC1lg LYTl 11/I0/15 0955 1521927 UAKB 11/23/15 1502 1522577 2 HAKB l 1124i15 0851 1522580 3 HAKB 11123115 !711 1522576 4 HAKB 11124115 IQl4 1522579 5 HAKB 11124115 1039 1522571 6 llAKB 11125115 \840 1522578 7 MHll J2i02/15 1806 !522374 8 R.XF2 \2i0:>/l 5 0828 1522386 9 GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company : MJW Corporation Address : 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes

    • fi*******-**

.............. ,. **-*** ... ******** ........ . ............ . Client Sample ID: l .3.C6 Sample ID: 385101009 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Dl)* Weight Corrected" Radmm-226 I .08 +/-0 289 Radium-228 0.891 +1-0.403 Tin-1215 U 0 143 +/.() 185 Rad Gas Flow Proportional Counting GFPC. Gross AiB, solid "Dry Weight Corrected" Alpha 7 80 +/-3 22 Beta 18 3 +r-2 99 GFPC, Sr90, solid "Dry Weight Corrected" Stronuum-90 U -0 122 -+*l-0 65'1 Rad Liquid Scintillation Analysis LSC. Tritium Dist, Solid "Dry Weight Corrected" Tritium lJ I 95 +/-2.00 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 ll -0 833 +/-0.891 Liquid Scint Tc99, Solid "Dry Weight Corrected" Tcchneuum-99 ll 1 60 +/-1.76 .. P.£ee.

        • -.... Method Description Dry-Soii f:ire*;i*

...... . () 255 0 526 0 177 3.91 2.69 [ 34 3.30 1.55 2 \15 4.00 100 200 6.00 2.UO 5.00 Analyst *******-******-****** Project: Client ID: pCi/g pCilg pC1/g pCi/g pC1/g pCi!!_! pC1/g pC1!g pCitg MJWC00! 15 MJWCOOl JXB7 12103115 123<> 1:\25768 KSOI 12/02il5 1712 1525755 TXJ! 121()2/15 2031 1522724 nm 12104r15 0520 1s2271r, MYMI 11129115 1416 1522715 Date Time Pl'ep Batch i Wib/15 . ... . .. 0955 1521927 lO II 13 14 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company; Address: MJW Corporation 15 Hazelwood Drive Suite 112 Certificate of Analysis Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes

  • -***--* *-* ....... *-. .. . ...........

-. -........ *******. .. .. . .. . . Client Sample ID: l .3.C6 Sample JD: 385101009 The r.\n_alY.tical ..... . Report Date: December 4, 20 I 5 ........... ,. Project: MJWCOOll5 Client JD: MJWCOOI .. " .........

          • -** .. .. . . -.... -**-**** .. . ....... . ... . ..... ... .... .. .. . ... . r\STM D 2216 (Modified)

.. ...... __ ........ _ .. *--.. f .................... -* *-....... _ .......... __ 2 DOE EML !-!ASL-JOO, Pu-l 1-RC Modified 3 DOE EML HASL-300. tJ-02-RC Modified 4 5 6 7 8 9 10 II 12 13 14 ASTM C 14 76-00 Modi ficd DOE EML J-IASL-300, *111-0l-RC' Modified OOE EML HASL-300, Am-05-RC" Modilicd DOE EML HASL-300. Pu-11-RC Modified DOB EML HASL-300,1-01 Modified DOE HASL JOO. 4 5.2 JIGn-01-R EPA 900.0iSW8% 93 IO!SM 71 lOB EPA 905 0 Mod11icd/OOE RP50l Rev 1 Mod11led EPA 906.0 Mod1fie<l EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modilfod . Test Pl1aonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Amcncium-243 Tracer Actimum-227 Tracer Amencmm-.243 Tracer Plutomum-242 Tracer Strontium C<1mer Tcclme!lum-99m Notes; ASP Plutonium Isotopic. Solid Dty Weight Corrected" ASP Uranium Isotopic. Sohd Dry Weight Corrected" ASP Uranium Isotopic, Solid "IJry Corrected" Alphaspec Np237, S<ll1d "OT)* Weight Corrected' A!phaspec Th229 + 228.230,232 Solid Dry Weight Am241,Cm Solid "Dry Weight Corrected Liquid Semi Pu24I, Solid "Dry Corrected" GFPC', Sr90, "Dry Weight Corrected" L1qmd Scint Tc99, Solid "Dlj' Weight Corrected" Counting Uncertainty is calculated at the 95% confidence !eve! ( 1.96-sigma). Result 76.6 (15%-125%) 55.9 (IS%-125%} 654 (15%-125%) 74.8 (15%-125%) 88 6 (15%-125%) 86.4 {15%-125%) 76 6 (15%-125%) 88 9 {25%-125%) 98.4 (!5%-125%) _j GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Corporation

  • .! 5 Tfozc:lwood Drive Snite I 12 Bu/T[l)O.

New York 14228 Contact: Ms. Project: Soil Radioisotopes Client Sample ID: I .3.C6 Sample ID: 38510 I 009 Matrix: Soil Collect Date; 21-0CT-!5 Receive Date: 05-NOV-15 Collector: Client Moisture: 23.6% Parameter ................... .......... .... Gravimetric Solids ASTA!/ D 2216 % Mois1ure "As Received" Moisture 23.6 Rod Alpha Spec Analysis ASP Plutonium Isotopic. Solid "D1:r Weigh/ Corrected" Plutomum-238 lJ 0 00979 +/-0.0544 Plutm1ium-23W240 U 0 00677 +/-0 0799 ASP Uranium Isotopic. Solid "Dry Weight Corrected" Uronium-232 U (} ()4 73 +/-ll 121 Un:mfom-2331134 0.799 +f.() 30 I llromum-2351236 00469 Uranium-238 l 14 Alplmspec Xp237. Solid "Dr)' Weight Correaed" +/-[) 0921 .,./.() 345 Neptunium-237 ti -0.0342 +/-0.236 Alphaspec Th229 2:!8,230.232 Solid "D1y Weight Corrected" Thorium-228 0.9&4 *l-IH&2 Thonum-229 0 13 l +l-0 207 Thormm-230 Thorium-232 t.16 0.979 A 11124 l. Cm Solid "Dry Weight Corrected" Amenciurn-241 0.0315 Curi u m-242 Curium-2431244 ti 000 0.00921 Curium-2451246 0 0361 liquid Sein/ Pu:.!41. Solid "Dry Weifdll C on*ected" Plutomum-24l lJ -2.07 Rall Camma Spec Analysis Gamma 1129. Solid "Dry Weight Corrected" !odinc-129 ll 0.214 +/-l! 498 /-[} 452 +l-0 062 +/-0.0412 +/-0.0512 +!-O.o709 +/-6..JO +/-ll.383 Gammaspec. Gamma. Solid "Dry Weight Corrected Acunium-227 ll -0.478 +f-0 464 /\ntimony-125 U 1).0263 +f-0.202 Bismuln-212 lI 0.725 +/-I 19 Bismu(h-214 I 08 +/-0.289 Cesium-137 0 357 +/-0.122 Coba!t-60 U -0.0195 +/-00816 Europium-154 U -0 00356 +/-0.241 Lcad-212 I 34 +/-0. 197 Lcud-214 l.09 +/-0.363 t\lDC Le ............. _, ....... . 0 104 0.0239 0 168 0 056 0222 0214 0.128 00796 0.575 0.395 0 2&7 0 () 155 0 0859 0.0613 0.0981 0.()*)&3 11 2 0 0&21 0.0674 00239 000 0.171 0 117 ()0657 0.0656 000 0 016.1 000 () 0225 00184 H3 0 769 0 345 0 775 () 355 !1369 IJ. !69 2 35 1 07 0.255 () 114 0.178 IJ.0812 0 153 lUl64 0.468 0 200 (} 181 l) 0839 0 5SO 0 279 +/-00545 +!-0 0799 +/-0121 +/-0 347 +/-0.0927 +/-0.424 +/-0 236 +1-0505 +/-0208 +1-0 527 +/-(}475 +1-0.0621 +l-0 0413 +/-0 0512 +/.()()711 +/-6 40 +/-0396 +/-0.517 +/-0 202 +f-1 23 t-/-0 303 +/-0 126 +1-0.0821 241 't-/-0'236 -rl-0 374 Report Date: December 17, 2015 Project: Client ID: MJWCOOl 15 MJWCOOI . l 'nits__ .. O..F.. .. ... ... !ipc .. :vi Id ... percent 1.00 rC1lg 1.00 pCi/g 1.00 1.00 l.00 1 00 1.00 I 00 1.no 1 00 l.00 1.00 !.00 1.00 100 150 pc1/g pci/g pc1/g pc1.lg pCilg pC1/g pCi/g pCiig pCi/g pCi/g pCi/g pC1lg pC1lg pCilg 1.00 pCUg pCi/g pC'i/g pCi/g pC1/g O. lOO pCi/g pC1/g pCi/g pC1/g pCiig LYTl l \IJOil5 0955 1521927 HAKB 11123115 1502 1522577 2 1-!AKB 11124115 0851 1522580 3 HAKB I l123/l5 1711 1522576 1-!AKB I J/24/l5 1014 1522579 HAKB 11/24115 .1039 1522571 6 HA.KB ll/25115 1840 1522578 MJH I 12102115 1806 1521374 8 RXF2 12i03/\5 0828 1522386 9 Company: Address: GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com MJ\V Corporntion 15 Ha:zelwoocl Drive Suite 112 Certificate of Analysis Buffalo, New York 14228 Report Date: December 17. 20 LS Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample JD: l.3.C6 Sample ID: 385101009 Project: MJWC001 l5 Client ID: MJWCOO! 1':1n1metcr. ...................

      • -...

___ ...

    • -... :VJ.I_).( ........ l.:C: .. . Tl'F . **-* *******-*

.. **-**-*** Rad Gamma Spee Annl)'sis Gammaspec. Gamma. Solid "Dry Weight CorrecNd Potassium-.40 I 3 9 Piatactmium-23! lJ 0 80! Radium-226 1.08 Radmm-228 Tlmllnun-208 0.892 0381 Tin-126 UI 0 00 Rat! Gos Flow Proportional Cou11ti11g GPPC. Gross A.* B, solid "Dry Weigltr Corrected" Alpha 7.80 Beta 18 3 GFPC. Si*9fJ. solid "D1:i* Weight Corrected" Stromium-90 ll -0.122 Rad Lic111il.I Scintillation Analysis LSC. Triti11m Dis/, Solid "D1:v Weight f'orracted" Triuum I 95 Liquid Seim C/4. Solid "D1:r Weight Corrected" Carbon-14 U -0 833 Liquid Sein/ Tc99, Solid "D1J-* Wf!ighl Con*ec/ed" Technetium-99 1.60 Method Oescriptio11 +/-227 +/-0 980 +/-0.28'1 +1-0403 +l-0168 +/.() 185 +!-3 22 -+*/-2 99 +/-0 659 +/-2.llO +l-l.76 1.05 I.St 0.255 0 526 0 131 ll.177 3.91 2 69 I 34 3 30 1 55 2.95 . ...... ... **-0 402 +/-2.5(;> . 0 841 +1-1.06 0.114 +/-0 303 0.229 +/-0415 00584 t-1-0 171 00839 +/-0 185 1 63 +/-3.56 \ 20 +/-393 0.573 +/-0 660 l 44 +/-2.00 o 1r,2 +i-0.891 1.42 +1-1 77 . ......... .... -* *-....... Analyst "Date 4 OU 10.0 2HO 6.00 2.00 5.0(J pCi/g pC1/g pC1fg pCitg pC1/g p('ilg pCiig pC'i/g pCifg pCl/g pCifg pCi/g *****-... ***** Time JXl37 KSDI TXJ! TXJI MYM I Prep Batd1 12/03!15 1234 1525768 I 2i02/l 5 1712 152.5755 12/02/15 2031 \522724 I 21lW15 0520 1522716 11129/15 1'116 15227!5 ..... ...... -* ........ .. ...... -*********** .........

            • -****

...... ...... ... . ..... -* --* ***-***********- -* --* Dry Soil Piep Dry Sml Prep GL-RAD-A-021 Tl1c_ _11crfor111e_q Method Description 2 3 5 6 7 8 9 10 II 12 13 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1476-00 Mod1tied DOE EMI. HASL-300, Th-01-RC Modified DOE EML l IASL-300, Am-05-RC Modified DOE liML HASl.-300, Pu-11-RC Modified DOE EMLJ!ASL-300,1-01 Mollified DOE HASL 300, 4 5.2 Ji<la-01-R EPA 900 O.'SW84G 93 lOiSM 71 \OB IV!od1ficd EPA 905 0 Mod1licd!DOE RP501 Rev l EPA 906 0 Modified EPA EERF C-01 Modified LYTI I J/J0/15 0955 1521927 10 II 12 13 14 .-1 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 13u1Talo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample lD: 1.3 .C6 Sample ID: 385!0J009 Certificate of Analysis P:m1mcter .. *-**** _ .......

      • -_

.:\IDC Le 14 DOE EML llASL-300. T,-02-RC Mod1fieJ Surrogate{fraeer Recovery Tes I ............... . ..... -....... **-*** -**-**** -* ... . ****-* .. ....... ... . -**. Plutonium-242 Tmccr ASP Plutcmium Isotopic. Solid "Dry Weight Corrected" lJranium-232 Tracer ASP Uranium Isotopic. Solid "Dry Weight Corrected" lJranium-235/236 Tracer ASP Uranium Isotopic, Solid "Dry Weight Corrected" ., Americium-243 Tracer Alphaspcc Np237, Solid "!Jr)' Weight Corrected" Actiniuin-227 Tracer Alphaspec Th229 + 228.230,232 Solid "Dry Weight Corrected" A1m:rici11m*243 Tracer i\m24l. Cm Solid "Dry Weight Corrected Plutmiium-242 Tracer Liquid Scint Pu24 l. Solid "Dry Weight Corrected" Strontium Carrier GFPC. Sr90, solid "Dry Weight Corrected" Tcchnetiurn-99m Tracer Liquid Scint Tc99. Solid "D1y Weight Corrected Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma). Project: Client ID: Reporl Date: December 17, 20 l S MJWCOO! 15 MJWCOO! Batch JD Rcc1n*ery%

              • t522'.i77 76.6 1522580 55.9 1522580 65.4 152257fr 74.8 !522579 88.6 1522571 86.4 1522578 76.6 1525755 88.9 1522715 98.4 AccertabJc Limits ...............

(15%-125%) (15%-125%) (15%-125%) Cl 5%-125'lol 05%-125%) (15%-125%) (! (25%-125%)}}

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