ML17024A021
| ML17024A021 | |
| Person / Time | |
|---|---|
| Site: | La Crosse File:Dairyland Power Cooperative icon.png |
| Issue date: | 01/23/2017 |
| From: | Altic N A Oak Ridge Institute for Science & Education |
| To: | Vaaler M Reactor Decommissioning Branch |
| VAALER M, 415-3178, T08F05 | |
| References | |
| DCN 5299-SR-01-0, DE SC0014664 | |
| Download: ML17024A021 (62) | |
Text
REPORT FOR THE INDEPENDENT CONFIRMATORY SURVEY OF THE NON-IMPACTED LAND AREAS AT THE LA CROSSE BOILING WATER REACTOR, GENOA, WISCONSIN
N. A. Altic ORAU FINAL REPORT Prepared for the U.S. Nuclear Regulatory Commission JANUARY 2017
Further dissemination authorized to NRC only; other requests shall be approved by the originating facility or higher NRC programmatic authority.
REPORT FOR THE INDEPENDENT CONFIRMATORY SURVEY OF THE NON-IMPACTED LAND AREAS AT THE LA CROSSE BOILING WATER REACTOR GENOA, WISCONSIN
Prepared by N. A. Altic ORAU
JANUARY 2017
FINAL REPORT Prepared for the U.S. Nuclear Regulatory Commission
CONTENTS
FIGURES TABLES ACRONYMS SolutionsSolutions REPORT FOR THE INDEPENDENT CONFIRMATORY SURVEY OF THE NON-IMPACTED LAND AREAS AT THE LA CROSSE BOILING WATER REACTOR GENOA, WISCONSIN EXECUTIVE SUMMARY
Solutions REPORT FOR THE INDEPENDENT CONFIRMATORY SURVEY OF THE NON-IMPACTED LAND AREAS AT THE LA CROSSE BOILING WATER REACTOR GENOA, WISCONSIN
- 1. INTRODUCTION
Solutions
- 2. SITE DESCRIPTION Figure 2.1. Open Land Survey Unit Boundaries
Table 2.1. Summary of Non
-Impacted Land Area Survey Units Survey Unit IDSurvey Unit DescriptionApproximate Survey Unit Area (m 2)3. DATA QUALITY OBJECTIVES Guidance on Systematic Planning Using the Data Quality Objectives Process 3.1 STATE THE PROBLEM 3.2 IDENTIFY THE DECISION Table 3.1. LACBWR Confirmatory Survey Decision Process Principal Study QuestionsAlternative Actions Decision Statement 3.3 IDENTIFY INPUTS TO THE DECISION Solutions 3.3.1 Radionuclides of Concern
Table 3.2.
Cs-137 Investigation Levels Specified in the Licensee's LTP (pCi/g) Soil Condition As Referenced in the TSD Decay Corrected to Confirmatory Survey Measured Range Range for 95% Confidence Level Measured Range Range for 95% Confidence Level 3.4 DEFINE THE STUDY BOUNDARIES
3.5 DEVELOP A DECISION RULE
3.6 SPECIFY LIMITS ON DECISION ERRORS 3.7 OPTIMIZE THE DESIGN FOR OBTAINING DATA
- 4. PROCEDURES ORAU Radiological and Environmental Survey Procedures ManualORAU Environmental Services and Radiation Training Quality Program Manual4.1 REFERENCE SYSTEM 4.2 SURFACE SCANS 4.3 SOIL SAMPLING
- 5. SAMPLE ANALYSIS AND DATA INTERPRETATION Radiological and Environmental Analytical Laboratory Procedures Manual6. FINDINGS AND RESULTS 6.1 SURFACE SCANS
6.2 SOIL SAMPLING Table 6.1. Cs-137 Concentration in Surface Soil Samples (pCi/g)
Mean Median Standard Deviation Min Max
Figure 6.1. Q
-Q Plot of ORISE Random Confirmatory Sample Results and LS Background Sample Results 6.3 EVALUATION OF ANALYTICAL DATA Figure 6.2 Sign Test Output Using ProUCL
Do Not Reject H0 at the specified level of significance (0.05), Conclude Median <= 0.135 One Sample Sign Test for Uncensored Full Data Sets Without Non-Detects
- 7. CONCLUSIONS
- 8. REFERENCES Guidance on systematic Planning Using the Data Quality Objectives ProcessORAU Radiation Protection ManualORAU Radiological and Environmental Survey Procedures ManualORAU Environmental Services and Radiation Training Quality Program ManualORAU Radiological and Environmental Analytical Laboratory Procedures ManualORAU Health and Safety ManualProject-Specific Plan for the Confirmatory Survey Activities at the La Crosse Boiling Water Reactor in Genoa, WisconsinSolutionsLACBWR: Supporting Information for Request for Partial Site ReleaseSolutionsExamination of Cs
-137 Global Fallout in Soils at Zion Station, Rev 0. Solutions APPENDIX A FIGURES Figure A-1. Gamma Walkover Scan of L4012103
Figure A-2. Gamma Walkover Scan of L4012105 Figure A-3. Gamma Walkover Scan of L4012106
Figure A-4. Gamma Walkover Scan of L4012107
Figure A-5. Soil Sampling Locations in L4012103
Figure A-6. Soil Sampling Locations in L4012105
Figure A-7. Soil Sampling Locations in L4012106
Figure A-8. Soil Sampling Locations in L4012107
APPENDIX B SOIL SAMPLE ANALYTICAL RESULTS Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0001 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET07Smp Qty.:
805.62Lab Sample ID:
12375S0001 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/15/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 910.81 911.200.130.160.80N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0450.106
-0.038N/AN/AAm-241pCi/g 726.98 727.330.280.520.78N/AN/ABi-212pCi/g 609.320.0900.228 0.749N/AN/ABi-214pCi/g 1332.49U0.0280.055
-0.015N/AN/ACo-60pCi/g 661.06 661.66U0.0190.040 0.033N/AN/ACs-137pCi/g 1460.821.32.915.3N/AN/AK-40pCi/g 1001.03U3.26.91.1N/AN/APa-234pCi/g 238.50 238.630.0590.060 0.664N/AN/ATh-228 by Pb-212pCi/g 351.78 351.930.0750.070 0.791N/AN/ARa-226 by Pb-214pCi/g 185.95 186.210.300.551.43N/AN/ARa-226pCi/g 67.67U3.89.41.5N/AN/ATh-230pCi/g 63.22 63.29U0.330.670.66N/AN/AU-238 by Th-234 pCi/g 143.76U0.110.260.07N/AN/AU-235Page 1 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0002 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET08Smp Qty.:
722.92Lab Sample ID:
12375S0002 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/15/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.12 911.200.140.151.18N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0560.124
-0.156N/AN/AAm-241pCi/g 727.36 727.330.280.471.29N/AN/ABi-212pCi/g 609.26 609.320.170.072.24N/AN/ABi-214pCi/g 1332.49U0.0260.057 0.027N/AN/ACo-60pCi/g 661.54 661.66U0.0160.037 0.025N/AN/ACs-137pCi/g 1460.81 1460.821.10.613.2N/AN/AK-40pCi/g 1001.15 1001.03U2.04.42.6N/AN/APa-234pCi/g 238.56 238.630.0710.086 0.873N/AN/ATh-228 by Pb-212pCi/g 351.82 351.930.150.072.57N/AN/ARa-226 by Pb-214pCi/g 185.91 186.210.470.684.71N/AN/ARa-226pCi/g 67.85 67.67U3.17.23.5N/AN/ATh-230pCi/g 63.15 63.290.810.913.13N/AN/AU-238 by Th-234pCi/g 143.94 143.76U0.0840.194 0.129N/AN/AU-235Page 2 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0003 SDG: 201212375-1 Geometry:
FMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET09Smp Qty.:
922.72Lab Sample ID:
12375S0003 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/15/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.39 911.200.0900.105 0.560N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0310.074
-0.049N/AN/AAm-241pCi/g 727.10 727.330.180.310.58N/AN/ABi-212pCi/g 609.29 609.320.0540.047 0.474N/AN/ABi-214pCi/g 1332.49U0.0170.034
-0.007N/AN/ACo-60pCi/g 661.66 661.660.0170.025 0.081N/AN/ACs-137pCi/g 1460.86 1460.821.10.512.9N/AN/AK-40pCi/g 1001.03U2.14.60.3N/AN/APa-234pCi/g 238.61 238.630.0420.043 0.456N/AN/ATh-228 by Pb-212pCi/g 351.91 351.930.0480.046 0.481N/AN/ARa-226 by Pb-214pCi/g 186.00 186.210.240.441.18N/AN/ARa-226pCi/g 67.67U2.87.01.6N/AN/ATh-230pCi/g 63.53 63.290.260.500.61N/AN/AU-238 by Th-234 pCi/g 143.76U0.0820.199 0.099N/AN/AU-235Page 3 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0004 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET10Smp Qty.:
528.41Lab Sample ID:
12375S0004 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/15/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 910.76 911.200.150.190.97N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.120.30-0.08N/AN/AAm-241pCi/g 727.50 727.330.310.570.96N/AN/ABi-212pCi/g 609.21 609.320.0760.085 0.603N/AN/ABi-214pCi/g 1332.49U0.0290.059
-0.008N/AN/ACo-60pCi/g 661.62 661.660.0360.041 0.260N/AN/ACs-137pCi/g 1460.18 1460.821.50.916.9N/AN/AK-40pCi/g 1001.03U3.37.10.3N/AN/APa-234pCi/g 238.77 238.630.0750.075 0.856N/AN/ATh-228 by Pb-212pCi/g 352.03 351.930.0690.079 0.611N/AN/ARa-226 by Pb-214pCi/g 186.07 186.210.420.772.12N/AN/ARa-226pCi/g 67.67U8.420.90.7N/AN/ATh-230pCi/g 63.59 63.29U0.811.691.41N/AN/AU-238 by Th-234 pCi/g 143.76U0.150.360.06N/AN/AU-235Page 4 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0005 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET07Smp Qty.:
815.55Lab Sample ID:
12375S0005 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/15/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 910.85 911.200.0630.081 0.227N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0290.061
-0.065N/AN/AAm-241pCi/g 727.17 727.33U0.160.320.24N/AN/ABi-212pCi/g 609.320.0530.146 0.276N/AN/ABi-214pCi/g 1332.49U0.0120.037 0.016N/AN/ACo-60pCi/g 661.39 661.660.0220.025 0.113N/AN/ACs-137pCi/g 1460.820.701.896.50N/AN/AK-40pCi/g 1001.03U2.55.3-0.0N/AN/APa-234pCi/g 238.47 238.630.0260.038 0.165N/AN/ATh-228 by Pb-212pCi/g 351.80 351.930.0390.054 0.237N/AN/ARa-226 by Pb-214pCi/g 185.90 186.210.200.390.67N/AN/ARa-226pCi/g 67.67U2.35.7-0.7N/AN/ATh-230pCi/g 63.42 63.29U0.240.500.45N/AN/AU-238 by Th-234pCi/g 144.23 143.76U0.0430.096 0.055N/AN/AU-235Page 5 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0006 SDG: 201212375-1 Geometry:
FMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET08Smp Qty.:
863.46Lab Sample ID:
12375S0006 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/15/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.22 911.200.0780.096 0.513N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0270.064
-0.015N/AN/AAm-241pCi/g 727.27 727.330.170.300.54N/AN/ABi-212pCi/g 609.28 609.320.0420.045 0.319N/AN/ABi-214pCi/g 1332.49U0.0170.034 0.005N/AN/ACo-60pCi/g 661.66U0.0160.034 0.005N/AN/ACs-137pCi/g 1460.84 1460.820.980.4612.20N/AN/AK-40pCi/g 1001.03U2.03.7-1.9N/AN/APa-234pCi/g 238.51 238.630.0420.044 0.473N/AN/ATh-228 by Pb-212pCi/g 351.83 351.930.0390.044 0.363N/AN/ARa-226 by Pb-214pCi/g 185.81 186.210.210.390.93N/AN/ARa-226pCi/g 67.67U2.45.8-1.3N/AN/ATh-230pCi/g 63.22 63.29U0.230.480.42N/AN/AU-238 by Th-234 pCi/g 143.76U0.0720.171 0.015N/AN/AU-235Page 6 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0007 SDG: 201212375-1 Geometry:
FMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET07Smp Qty.:
888.25Lab Sample ID:
12375S0007 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/16/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity Ratio pCi/g 911.20U0.0850.272
-0.146N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0320.076
-0.016N/AN/AAm-241pCi/g 726.80 727.330.190.310.55N/AN/ABi-212pCi/g 609.08 609.320.0480.054 0.317N/AN/ABi-214pCi/g 1332.49U0.0220.043
-0.008N/AN/ACo-60pCi/g 661.66U0.0200.048 0.017N/AN/ACs-137pCi/g 1460.12 1460.820.920.499.25N/AN/AK-40pCi/g 1001.03U2.65.2-0.6N/AN/APa-234pCi/g 238.47 238.630.0340.043 0.278N/AN/ATh-228 by Pb-212pCi/g 351.77 351.930.0450.054 0.337N/AN/ARa-226 by Pb-214pCi/g 185.84 186.210.210.420.65N/AN/ARa-226pCi/g 67.67U2.66.50.2N/AN/ATh-230pCi/g 63.40 63.29U0.260.550.44N/AN/AU-238 by Th-234 pCi/g 143.76U0.0760.181 0.030N/AN/AU-235Page 7 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0008 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET08Smp Qty.:
797.61Lab Sample ID:
12375S0008 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/16/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.15 911.200.170.111.73N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0490.114
-0.101N/AN/AAm-241pCi/g 727.40 727.330.330.432.18N/AN/ABi-212pCi/g 609.26 609.320.130.061.67N/AN/ABi-214pCi/g 1332.49U0.0210.043 0.006N/AN/ACo-60pCi/g 661.66U0.0190.045
-0.020N/AN/ACs-137pCi/g 1460.76 1460.820.420.433.49N/AN/AK-40pCi/g 1001.20 1001.03U1.63.62.7N/AN/APa-234pCi/g 238.57 238.630.100.081.51N/AN/ATh-228 by Pb-212pCi/g 351.80 351.930.120.061.90N/AN/ARa-226 by Pb-214pCi/g 185.85 186.210.400.633.70N/AN/ARa-226pCi/g 67.31 67.67U2.96.82.0N/AN/ATh-230pCi/g 63.21 63.290.700.832.65N/AN/AU-238 by Th-234pCi/g 143.42 143.76U0.0780.182 0.087N/AN/AU-235Page 8 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0009 SDG: 201212375-1 Geometry:
FMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET07Smp Qty.:
889.12Lab Sample ID:
12375S0009 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/16/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.07 911.200.0700.111 0.240N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0290.067
-0.052N/AN/AAm-241pCi/g 726.80 727.33U0.150.310.22N/AN/ABi-212pCi/g 609.320.0490.139 0.290N/AN/ABi-214pCi/g 1332.49U0.0180.042 0.008N/AN/ACo-60pCi/g 661.39 661.66U0.0100.025 0.005N/AN/ACs-137pCi/g 1460.820.812.007.63N/AN/AK-40pCi/g 1001.03U2.25.52.6N/AN/APa-234pCi/g 238.49 238.630.0300.038 0.232N/AN/ATh-228 by Pb-212pCi/g 351.83 351.930.0390.051 0.268N/AN/ARa-226 by Pb-214pCi/g 185.93 186.210.180.370.54N/AN/ARa-226pCi/g 67.67U2.46.11.6N/AN/ATh-230pCi/g 63.35 63.29U0.220.450.42N/AN/AU-238 by Th-234 pCi/g 143.76U0.0730.174 0.015N/AN/AU-235Page 9 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0010 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET08Smp Qty.:
703.21Lab Sample ID:
12375S0010 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/16/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.17 911.200.180.131.85N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0540.129
-0.037N/AN/AAm-241pCi/g 727.23 727.330.310.461.69N/AN/ABi-212pCi/g 609.25 609.320.130.081.65N/AN/ABi-214pCi/g 1332.49U0.0180.053
-0.010N/AN/ACo-60pCi/g 661.66U0.0200.049
-0.008N/AN/ACs-137pCi/g 1460.84 1460.820.920.5510.59N/AN/AK-40pCi/g 1001.03U2.86.33.3N/AN/APa-234pCi/g 238.56 238.630.100.091.53N/AN/ATh-228 by Pb-212pCi/g 351.83 351.930.120.071.82N/AN/ARa-226 by Pb-214pCi/g 185.80 186.210.400.673.22N/AN/ARa-226pCi/g 67.67U4.611.33.3N/AN/ATh-230pCi/g 63.22 63.290.570.931.79N/AN/AU-238 by Th-234pCi/g 143.63 143.76U0.0820.189 0.132N/AN/AU-235Page 10 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0011 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET09Smp Qty.:
645.19Lab Sample ID:
12375S0011 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/16/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.20 911.200.200.191.61N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0660.152
-0.130N/AN/AAm-241pCi/g 727.33 727.330.360.621.37N/AN/ABi-212pCi/g 609.32 609.320.300.093.61N/AN/ABi-214pCi/g 1332.49U0.0320.072 0.014N/AN/ACo-60pCi/g 662.03 661.66U0.0220.055
-0.008N/AN/ACs-137pCi/g 1460.93 1460.821.20.712.8N/AN/AK-40pCi/g 1001.23 1001.032.75.36.1N/AN/APa-234pCi/g 238.64 238.630.100.091.37N/AN/ATh-228 by Pb-212pCi/g 351.91 351.930.250.094.18N/AN/ARa-226 by Pb-214pCi/g 185.99 186.210.630.836.77N/AN/ARa-226pCi/g 67.65 67.67U4.610.93.1N/AN/ATh-230pCi/g 63.00 63.290.860.993.28N/AN/AU-238 by Th-234pCi/g 144.01 143.760.120.270.29N/AN/AU-235Page 11 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0012 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/28/2016 Live Time(s):
3,600Detector ID:
DET10Smp Qty.:
569.96Lab Sample ID:
12375S0012 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/16/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 910.94 911.200.100.130.55N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0990.250 0.045N/AN/AAm-241pCi/g 727.10 727.330.240.440.63N/AN/ABi-212pCi/g 609.20 609.320.0660.074 0.504N/AN/ABi-214pCi/g 1332.49U0.0230.044
-0.004N/AN/ACo-60pCi/g 661.56 661.660.0550.036 0.566N/AN/ACs-137pCi/g 1460.19 1460.820.960.859.28N/AN/AK-40pCi/g 1001.03U2.76.00.3N/AN/APa-234pCi/g 238.76 238.630.0540.067 0.521N/AN/ATh-228 by Pb-212pCi/g 352.00 351.930.0650.076 0.573N/AN/ARa-226 by Pb-214pCi/g 186.11 186.210.340.691.10N/AN/ARa-226pCi/g 67.67U6.917.53.0N/AN/ATh-230pCi/g 63.42 63.29U0.691.401.20N/AN/AU-238 by Th-234 pCi/g 143.76U0.130.320.09N/AN/AU-235Page 12 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0013 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/29/2016 Live Time(s):
3,600Detector ID:
DET07Smp Qty.:
434.23Lab Sample ID:
12375S0013 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/16/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 910.79 911.200.110.170.33N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0490.114
-0.067N/AN/AAm-241pCi/g 727.33U0.401.070.72N/AN/ABi-212pCi/g 608.99 609.320.0670.100 0.277N/AN/ABi-214pCi/g 1332.49U0.0270.064 0.008N/AN/ACo-60pCi/g 661.38 661.660.0990.043 0.978N/AN/ACs-137pCi/g 1460.24 1460.821.20.910.1N/AN/AK-40pCi/g 1000.42 1001.03U2.86.81.4N/AN/APa-234pCi/g 238.57 238.630.0490.066 0.324N/AN/ATh-228 by Pb-212pCi/g 351.68 351.930.0650.105 0.305N/AN/ARa-226 by Pb-214pCi/g 185.91 186.21U0.320.710.49N/AN/ARa-226pCi/g 67.67U3.89.5-0.8N/AN/ATh-230pCi/g 63.49 63.290.400.740.86N/AN/AU-238 by Th-234 pCi/g 143.76U0.110.270.00N/AN/AU-235Page 13 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0014 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/29/2016 Live Time(s):
3,600Detector ID:
DET08Smp Qty.:
666.16Lab Sample ID:
12375S0014 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/16/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.12 911.200.0830.123 0.413N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0350.084
-0.023N/AN/AAm-241pCi/g 726.70 727.33U0.170.350.35N/AN/ABi-212pCi/g 609.07 609.320.0460.055 0.324N/AN/ABi-214pCi/g 1332.49U0.0220.044 0.003N/AN/ACo-60pCi/g 661.48 661.660.0300.025 0.256N/AN/ACs-137pCi/g 1460.68 1460.821.40.618.1N/AN/AK-40pCi/g 1001.03U2.45.21.2N/AN/APa-234pCi/g 238.51 238.630.0380.050 0.354N/AN/ATh-228 by Pb-212pCi/g 351.73 351.930.0420.055 0.350N/AN/ARa-226 by Pb-214pCi/g 185.77 186.210.220.460.70N/AN/ARa-226pCi/g 67.67U2.86.9-0.3N/AN/ATh-230pCi/g 63.29 63.29U0.280.590.49N/AN/AU-238 by Th-234 pCi/g 143.76U0.0780.189 0.061N/AN/AU-235Page 14 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0015 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/29/2016 Live Time(s):
3,600Detector ID:
DET09Smp Qty.:
539.55Lab Sample ID:
12375S0015 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/16/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.41 911.200.0940.090 0.457N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0380.093
-0.017N/AN/AAm-241pCi/g 727.49 727.33U0.220.460.34N/AN/ABi-212pCi/g 609.45 609.320.0540.060 0.323N/AN/ABi-214pCi/g 1332.49U0.0230.046
-0.006N/AN/ACo-60pCi/g 661.70 661.660.0590.037 0.514N/AN/ACs-137pCi/g 1461.00 1460.820.880.628.09N/AN/AK-40pCi/g 1001.03U2.75.9-0.3N/AN/APa-234pCi/g 238.63 238.630.0450.050 0.415N/AN/ATh-228 by Pb-212pCi/g 352.00 351.930.0530.063 0.400N/AN/ARa-226 by Pb-214pCi/g 185.79 186.210.260.520.75N/AN/ARa-226pCi/g 67.67U3.17.70.6N/AN/ATh-230pCi/g 62.87 63.29U0.290.590.54N/AN/AU-238 by Th-234pCi/g 143.17 143.76U0.0670.156 0.052N/AN/AU-235Page 15 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0016 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/29/2016 Live Time(s):
3,600Detector ID:
DET10Smp Qty.:
568.06Lab Sample ID:
12375S0016 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/16/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 910.88 911.200.140.160.98N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.130.320.02N/AN/AAm-241pCi/g 727.19 727.330.300.501.11N/AN/ABi-212pCi/g 609.27 609.320.1000.086 1.007N/AN/ABi-214pCi/g 1332.49U0.0280.061 0.007N/AN/ACo-60pCi/g 661.54 661.660.0550.042 0.550N/AN/ACs-137pCi/g 1460.22 1460.821.20.813.2N/AN/AK-40pCi/g 1001.03U2.65.80.1N/AN/APa-234pCi/g 238.77 238.630.0820.080 1.012N/AN/ATh-228 by Pb-212pCi/g 352.02 351.930.0910.083 1.036N/AN/ARa-226 by Pb-214pCi/g 186.06 186.210.410.801.74N/AN/ARa-226pCi/g 67.67U8.822.211.1N/AN/ATh-230pCi/g 63.67 63.29U0.892.011.03N/AN/AU-238 by Th-234pCi/g 144.46 143.76U0.100.240.08N/AN/AU-235Page 16 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0017 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/29/2016 Live Time(s):
3,600Detector ID:
DET07Smp Qty.:
835.50Lab Sample ID:
12375S0017 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/17/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 910.94 911.200.120.160.65N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0420.097
-0.089N/AN/AAm-241pCi/g 726.84 727.330.260.440.86N/AN/ABi-212pCi/g 609.11 609.320.0630.066 0.480N/AN/ABi-214pCi/g 1332.49U0.0220.049 0.005N/AN/ACo-60pCi/g 661.44 661.660.0260.033 0.148N/AN/ACs-137pCi/g 1460.40 1460.821.20.414.5N/AN/AK-40pCi/g 1001.03U3.06.61.1N/AN/APa-234pCi/g 238.60 238.630.0530.053 0.570N/AN/ATh-228 by Pb-212pCi/g 351.84 351.930.0550.064 0.462N/AN/ARa-226 by Pb-214pCi/g 185.71 186.210.280.481.55N/AN/ARa-226pCi/g 67.67U3.48.4-0.9N/AN/ATh-230pCi/g 63.20 63.290.330.770.90N/AN/AU-238 by Th-234 pCi/g 143.76U0.0960.229 0.037N/AN/AU-235Page 17 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0018 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/29/2016 Live Time(s):
3,600Detector ID:
DET08Smp Qty.:
646.75Lab Sample ID:
12375S0018 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/17/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.18 911.200.140.161.08N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0560.130
-0.096N/AN/AAm-241pCi/g 727.37 727.330.280.461.26N/AN/ABi-212pCi/g 609.24 609.320.170.082.23N/AN/ABi-214pCi/g 1332.49U0.0300.064 0.024N/AN/ACo-60pCi/g 661.68 661.66U0.0180.039 0.030N/AN/ACs-137pCi/g 1460.73 1460.821.10.612.8N/AN/AK-40pCi/g 1000.99 1001.03U2.14.62.9N/AN/APa-234pCi/g 238.54 238.630.0710.094 0.836N/AN/ATh-228 by Pb-212pCi/g 351.73 351.930.160.092.58N/AN/ARa-226 by Pb-214pCi/g 185.84 186.210.460.694.36N/AN/ARa-226pCi/g 67.67U4.511.22.5N/AN/ATh-230pCi/g 63.23 63.290.730.922.69N/AN/AU-238 by Th-234pCi/g 143.99 143.76U0.0870.202 0.108N/AN/AU-235Page 18 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0019 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/29/2016 Live Time(s):
3,600Detector ID:
DET09Smp Qty.:
783.44Lab Sample ID:
12375S0019 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/17/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.23 911.200.120.130.76N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0390.092
-0.035N/AN/AAm-241pCi/g 727.19 727.330.230.360.82N/AN/ABi-212pCi/g 609.28 609.320.0730.059 0.647N/AN/ABi-214pCi/g 1332.49U0.0120.043
-0.011N/AN/ACo-60pCi/g 661.55 661.660.0170.028 0.064N/AN/ACs-137pCi/g 1460.83 1460.821.20.513.7N/AN/AK-40pCi/g 1001.03U2.35.31.1N/AN/APa-234pCi/g 238.66 238.630.0600.052 0.762N/AN/ATh-228 by Pb-212pCi/g 351.90 351.930.0660.055 0.757N/AN/ARa-226 by Pb-214pCi/g 186.00 186.210.280.461.81N/AN/ARa-226pCi/g 67.67U3.38.21.9N/AN/ATh-230pCi/g 63.13 63.290.370.670.97N/AN/AU-238 by Th-234pCi/g 143.60 143.76U0.0650.156 0.024N/AN/AU-235Page 19 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: December 05, 2016 Client Sample ID:
5299S0020 SDG: 201212375-1 Geometry:
LMUnits: gramsCount Date:
11/29/2016 Live Time(s):
3,600Detector ID:
DET10Smp Qty.:
798.54Lab Sample ID:
12375S0020 Batch Number:
GS0392Project Name:
La Crosse Project # :
201212375 SOP (Rev. #):
CP1 (21)
Analyst: smithwCOC # :
1611-005Receipt Date:
11/21/2016 Collection Date:
11/17/2016 AnalyteResultTPU (2s)MDC UnitsEnergy (keV)Duplicate
Error RatioEnergy Signature
(keV)Qualifier Meas./Known Activity RatiopCi/g 911.01 911.200.0840.101 0.488N/AN/ATh-232 by Ac-228 pCi/g 59.54U0.0790.201 0.064N/AN/AAm-241pCi/g 726.90 727.330.200.330.68N/AN/ABi-212pCi/g 609.21 609.320.0510.055 0.422N/AN/ABi-214pCi/g 1332.49U0.0190.038 0.002N/AN/ACo-60pCi/g 661.44 661.660.0160.028 0.060N/AN/ACs-137pCi/g 1460.25 1460.820.840.608.95N/AN/AK-40pCi/g 1001.03U2.04.30.1N/AN/APa-234pCi/g 238.77 238.630.0420.050 0.430N/AN/ATh-228 by Pb-212pCi/g 351.99 351.930.0520.057 0.499N/AN/ARa-226 by Pb-214pCi/g 186.42 186.210.230.450.93N/AN/ARa-226pCi/g 67.67U5.513.71.8N/AN/ATh-230pCi/g 63.52 63.29U0.511.110.69N/AN/AU-238 by Th-234 pCi/g 143.76U0.100.24-0.02N/AN/AU-235Page 20 of 22 Qualifier Flags:U = Analyte not detected (< MDC)TPU =Total Propagated Uncertainty MDC =Minimum Detectable Concentration APPENDIX C MAJOR INSTRUMENTATION C.1 SCANNING AND MEASUREMENT INSTRUMENT/DETECTOR COMBINATIONSC.1.1 GAMMA C.2 LABORATORY ANALYTICAL INSTRUMENTATION
APPENDIX D SURVEY PROCEDURES D.1 PROJECT HEALTH AND SAFETYORAU Radiation Protection ManualORAU Health and Safety ManualORAURadiological and EnvironmentalSurvey Procedures Manual ORAU Radiological and Environmental Survey Procedures Manual D.2 CALIBRATION AND QUALITY ASSURANCE ORAURadiological and EnvironmentalSurvey Procedures Manual ORAU Radiological and Environmental Analytical Laboratory Procedures Manual D.3 SURVEY PROCEDURESD.3.1 SURFACE SCANS D.3.3 SOIL SAMPLING D.4 RADIOLOGICAL ANALYSISD.4.1 GAMMA SPECTROSCOPY
Radionuclide a TAP (keV) MDC (pCi/g)
D.4.2 DETECTION LIMITS