ML20352A255

Response to Request for Additional Information Re Revised Final Status Survey Final Reports, L1-SUB-TDS Release Record, Rev. 1, L1-010-102 Excavation

ML20352A255
Person / Time
Site:	La Crosse  File:Dairyland Power Cooperative icon.png
Issue date:	11/02/2020
From:	La CrosseSolutions
To:	Office of Nuclear Material Safety and Safeguards
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References
LC-2020-0023
Download: ML20352A255 (255)

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LACROSSESOLUTIONS LA CROSSE BOILING WATER REACTOR FINAL STATUS SURVEY RELEASE RECORD SURVEY UNIT L1-SUB-TDS REVISION 1

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Robert F. Yetter III PREPARED BY / DATE:

fia~- Oct 29 2020 3:34 PM cosign R. F. Yetter III, FSS Specialist Mitchell Uz REVIEWED BY / DATE:

~it, Oct 29 2020 3:41 PM cosign M. D. Uz, FSS Specialist REVIEWED BY / DATE:

~j.V.etwt Robert F. Yetter Oct 29 2020 5:02 PM cosign R. Yetter, Director, Radiological Site Closure Sarah Roberts SaMI4~~ Oct 29 2020 5:26 PM REVIEWED BY / DATE: cosign S. Roberts, VP Radiological Programs c.:..:~-1/4 . ~p Scott G. Zoller Nov 2 2020 7:16 AM APPROVED BY / DATE: cosign S. Zoller, FSS Manager 1

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS TABLE OF CONTENTS

1. EXECUTIVE

SUMMARY

................................................................................................................................. 5

2. SURVEY UNIT DESCRIPTION ....................................................................................................................... 5

3. CLASSIFICATION BASIS ................................................................................................................................. 6

4. DATA QUALITY OBJECTIVES ...................................................................................................................... 9

5. SURVEY DESIGN ............................................................................................................................................. 12

6. SURVEY IMPLEMENTATION ...................................................................................................................... 18

7. SURVEY RESULTS .......................................................................................................................................... 20

8. QUALITY CONTROL ...................................................................................................................................... 28

9. INVESTIGATIONS AND RESULTS .............................................................................................................. 28

10. REMEDIATION AND RESULTS ................................................................................................................... 28

11. CHANGES FROM THE FINAL STATUS SURVEY PLAN ........................................................................ 28

12. DATA QUALITY ASSESSMENT (DQA) ....................................................................................................... 29

13. ANOMALIES ..................................................................................................................................................... 29

14. CONCLUSION .................................................................................................................................................. 30

15. REFERENCES................................................................................................................................................... 30

16. ATTACHMENTS .............................................................................................................................................. 31 ATTACHMENT 1 FIGURES AND MAPS ............................................................................................................. 32 ATTACHMENT 2 SCAN DATA ............................................................................................................................. 35 ATTACHMENT 3 SIGN TEST ............................................................................................................................... 39 ATTACHMENT 4 QUALITY CONTROL ASSESSMENT ...................................................................................... 41 ATTACHMENT 5 CONSULTATION TRIGGERS FOR RESIDENTIAL SOIL CONCENTRATIONS ................... 43 ATTACHMENT 6 GRAPHICAL PRESENTATIONS ............................................................................................. 45 ATTACHMENT 7 SAMPLE ANALYTICAL REPORTS ......................................................................................... 49 ATTACHMENT 8 GEL LABORATORIES ANALYTICAL REPORTS ................................................................. 210 2

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS LIST OF TABLES Table 3 Statistical Quantities for Cs-137 and Co-60 from the Characterization Survey .................................. 7 Table 4 Dose Significant Radionuclides and Mixture for Soil .......................................................................... 10 Table 4 Base Case DCGLs for Soil (DCGL S)...................................................................................................... 11 Table 4 Operational DCGLs for Soil (OpDCGL S) ............................................................................................. 12 Table 5-1 Soil Surrogate Ratio ............................................................................................................................... 13 Table 5-2 Action Levels for Survey Unit L1-SUB-TDS ........................................................................................ 14 Table 5-3 Systematic Sample Locations ................................................................................................................. 15 Table 5 Judgmental Sample Locations ............................................................................................................... 16 Table 5 Investigation Levels ................................................................................................................................. 17 Table 5 Synopsis of Survey Design ...................................................................................................................... 17 Table 7-1 Synopsis of Scan Results ........................................................................................................................ 20 Table 7 Summary of Gamma Spectroscopy Results for Soil Samples Comprising the Statistical Sample Population ........................................................................................................................................................... 23 Table 7 Basic Statistical Properties of Systematic Sample Population ............................................................. 23 Table 7 Off-Site Analysis Results......................................................................................................................... 24 Table 7 Summary of Gamma Spectroscopy Results for Judgmental Soil Samples......................................... 25 Table 7 Summary of Gamma Spectroscopy Results for QC Soil Samples ....................................................... 26 Table 7 Sum-of-Fractions for Individual Soil Samples (Systematic and QC) ................................................. 26 Table 7 Sum-of-Fractions for Individual Soil Samples (Judgmental) .............................................................. 27 Table 16 L1-SUB-TDS Complete Scan Data ...................................................................................................... 36 Table 16-2 L1-SUB-TDS Sign Test......................................................................................................................... 40 Table 16-3 L1-SUB-TDS QC Assessment .............................................................................................................. 42 LIST OF FIGURES Figure 16 L1-SUB-TDS Systematic Sample Locations Map ............................................................................. 33 Figure 16-2 L1-SUB-TDS Judgmental Sample Locations .................................................................................... 34 Figure 16 Quantile Plot for Cs-137 Concentration ............................................................................................ 46 Figure 16 Histogram for Cs-137 Concentration ................................................................................................. 47 Figure 16 Retrospective Power Curve for L1-SUB-TDS ................................................................................... 48 3

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS LIST OF ACRONYMS AND ABBREVIATIONS ALARA As Low As Reasonably Achievable ASP Alarm Set Point DQA Data Quality Assessment DQO Data Quality Objective DCGL Derived Concentration Guideline Level DCGLS Soil Derived Concentration Guideline Level FSS Final Status Survey GPS Global Positioning System HSA Historical Site Assessment IC Insignificant Contributors LACBWR La Crosse Boiling Water Reactor LBGR Lower Bound of the Gray Region LTP License Termination Plan MARSSIM Multi-Agency Radiation Survey and Site Investigation Manual MDC Minimum Detectable Concentration MDCR Minimal Detectable Count Rate NaI Sodium Iodide OpDCGLS Soil Operational Derived Concentration Guideline Level QAPP Quality Assurance Project Plan QC Quality Control RASS Remedial Action Support Survey ROC Radionuclides of Concern SOF Sum of Fractions TEDE Total Effective Dose Equivalent UBGR Upper Bound of the Gray Region UCL Upper Confidence Limit 4

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS

1. EXECUTIVE

SUMMARY

This Final Status Survey (FSS) Release Record for survey unit L1-SUB-TDS, West Excavation (within open land survey unit L1-010-102), has been generated in accordance with LaCrosseSolutions procedure LC-FS-PR-009, Final Status Survey Data Reporting (Reference 1) and satisfies the requirements of Section 5.11 of the La Crosse Boiling Water Reactor License Termination Plan (LTP) (Reference 2).

An FSS sample plan for this survey unit was developed in accordance with LaCrosseSolutions procedure LC-FS-PR-002, Final Status Survey Package Development (Reference 3), the LACBWR LTP, and with guidance from NUREG-1575, Revision 1, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM) (Reference 4).

This survey unit has a MARSSIM classification of 1. A survey plan was designed based upon use of the Sign Test as the nonparametric statistical test for compliance. Both the Type I ( ) and Type II ( ) decision error rates were set at 0.05. As a systematic sample population using a random start point, fourteen (14) soil samples were acquired from the survey unit.

In addition, soil scanning was performed on 100% of the total surface area in the survey unit.

The analytical results for all soil samples taken in survey unit L1-SUB-TDS indicate that the maximum Sum of Fractions (SOF), considering the concentration of all applicable Radionuclides of Concern (ROC) either by direct measurement or by inference, is equal to 0.0552 when applying the respective Operational Derived Concentration Guideline Levels (OpDCGLS) for soil. Therefore, the null hypothesis is rejected and survey unit L1-SUB-TDS is acceptable for unrestricted release. The mean SOF when applying the respective Base Case DCGLs (DCGLS) for soil is 0.0125. This SOF equates to a dose for the survey unit of 0.3115 mrem/yr.

2. SURVEY UNIT DESCRIPTION L1-SUB-TDS is an impacted Class 1 excavation survey unit. The survey unit consists of the underlying soil post-removal of the Turbine Building/Turbine Building Offices and 1B Diesel Generator Building, as well as associated system lines. The surface area of the survey unit is 1,185.5 m2.

The boundary of the survey unit and the location of the soil samples were defined using a Global Positioning System (GPS). Refer to Attachment 1 of this report for figures and maps depicting survey unit L1-SUB-TDS.

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS This survey unit includes only the western portion of the original L1-SUB-TDS. The eastern portion of the original survey unit did not undergo FSS because of high background readings emanating from the Reactor Building and surrounding environs. The eastern portion of the survey unit (now identified as L1-SUB-TDS A) will undergo FSS under a separate sample plan. Additionally, the Reactor Plant Generator Plant Area (RPGPA) Sump Area, also within the east portion of the original survey unit, experienced groundwater intrusion due to rising Mississippi River levels and has caused it to become inaccessible. The backfilled RPGPA Sump Area (L1-SUB-TDS B) will undergo FSS via use of GeoProbe technology using a separate sample plan.

3. CLASSIFICATION BASIS Based on the Historical Site Assessment (HSA) (Reference 5), open land survey unit L1-010-102 had a past history of minor radiological surface contamination on the grounds and outside the truck bay and therefore was categorized as a Class 1 area. As survey unit L1-SUB-TDS consists of the underlying soils from L1-010-102, it is also deemed Class 1. The following summarizes the results of the characterization surveys for survey unit L1-010-102.

The initial site characterization surveys performed by EnergySolutions were conducted between October 9, 2014, and August 6, 2015. In 2014, a total of two (2) surface soil samples, and seven (7) subsurface soil samples (including one sub-slab soil sample taken beneath the Turbine Building Tunnel Area) were collected in the survey unit. In 2015, as part of a broader site characterization, five (5) locations were selected for angled coring to obtain soil from beneath the Turbine Building at the location of suspected broken drain lines. GeoProbe technology was used to obtain the samples. At each of the 5 locations, samples were collected from the 10', 15' and 20' depths, for a total of fifteen (15) soil samples. A total of 2 surface soil samples and 22 subsurface soil samples were collected in the survey unit prior to FSS.

All samples were analyzed by the on-site gamma spectroscopy system. No ROC were detected at concentrations above Minimum Detectable Concentration (MDC) for the surface soil samples. For subsurface soil samples, Cs-137 was detected at concentrations above MDC in four (4) of the samples, at a maximum concentration of 0.130 pCi/g. Co-60 was not detected at concentrations above MDC for subsurface soil samples. A summary of the analyses for the surface soil and subsurface soil samples taken during site characterization are presented in Table 3-1.

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Table 3 Statistical Quantities for Cs-137 and Co-60 from the Characterization Survey Surface Soil Co-60 Cs-137

1. of Samples 2

1. >MDC 0 0 Mean (pCi/g) 0.049 0.050 Median (pCi/g) 0.049 0.050 Max (pCi/g) 0.054 0.051 Min (pCi/g) 0.044 0.050 Standard Deviation (pCi/g) 0.007 0.001 Subsurface Soil Co-60 Cs-137

1. of Samples 22

1. >MDC 0 4 Mean (pCi/g) 0.058 0.064 Median (pCi/g) 0.058 0.065 Max (pCi/g) 0.080 0.130 Min (pCi/g) 0.043 0.044 Standard Deviation (pCi/g) 0.010 0.017 Four (4) subsurface soil samples, and one (1) surface soil sample, from characterization were sent to Test America Laboratories for off-site analysis. The subsurface soil samples were analyzed for the full suite of initial ROC, while the surface soil sample was analyzed for Co-60, Nb-94, Cs-137, Eu-152, Eu-154, Eu-155, and Am-241. For subsurface samples, H-3 was identified in two (2) samples and Ni-63 was identified in one (1) sample at maximum concentrations of 24.7 pCi/g and 4.0 pCi/g; respectively. No ROC were identified with concentrations greater than MDC for surface soil samples.

In September of 2017, the Turbine Building foundation was removed in its entirety, including all broken drain lines and adjacent soil. As required by Section 5.3.3.4 of the LTP, in the western portion of the excavation, a total of eight (8) samples were collected from the region beneath the broken drain lines, turbine sump, turbine pit, and condenser pit. Although part of continuing characterization, these samples were collected as judgmental samples during the FSS. As per Section 5.1 of the LTP, all samples were analyzed by the on-site gamma spectroscopy system. Gamma spectroscopy results revealed eight (8) samples above MDC for Cs-137 with a maximum concentration of 0.188 pCi/g. Two (2) samples were above MDC for Co-60 with a maximum concentration of 0.257 pCi/g. No samples were identified with concentrations greater than MDC for any other ROC. A summary of the on-7

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS site analytical results for the judgmental soil samples for continuing characterization is provided in Table 7-5.

Section 5.1 of the LTP states that the actual Insignificant Contributor (IC) dose will be calculated for each individual sample result using the DCGLs from TSD RS-TD-313196-004, LACBWR Soil DCGL, Basement Concrete DCGL, and Buried Pipe DCGL, Table 4 (Reference 6) for soil. If the IC dose calculated is less than the IC dose assigned for DCGL adjustment, then no further action is required to be taken. If the actual IC dose calculated from the sample result is greater than the IC dose assigned for DCGL adjustment, then a minimum of five (5) additional investigation samples will be taken around the original sample location. Each investigation sample will be analyzed by the on-site gamma spectroscopy system and sent for HTD analysis (full suite of radionuclides from LTP Table 5-1). As with the original sample, the actual IC dose will be calculated for each investigation sample. In this case, the actual calculated maximum IC dose from an individual sample observed in the survey unit will be used to readjust the DCGLs in that survey unit. If the maximum IC dose exceeds 10%, then the additional radionuclides that were the cause of the IC dose exceeding 10% will be added as additional ROC for that survey unit. The survey unit-specific DCGLs used for compliance, the ROC for that survey unit, and the survey data serving as the basis for the IC dose adjustment are required to be documented in the release record for the survey unit.

Although four (4) of the samples were required to be sent off-site for Sr-90 analysis (per the FSS sample plan), as a conservative measure, all were sent off-site for Sr-90 analysis.

Additionally, seven (7) of the eight (8) samples were sent off-site for HTD analyses for the full initial suite of ROC. An assessment of the results of continuing characterization confirmed that the IC dose is unchanged. The maximum calculated IC dose was 0.1439 mrem/yr, which is below the 2.5 mrem/yr limit provided in the LTP for DCGL adjustment.

A summary of the off-site analytical results for the judgmental soil samples collected for continuing characterization is provided in Table 7-4.

Based upon review of the historical information, the results of the characterization survey data, and completion of a final Survey Unit Classification Worksheet, the correct final classification of survey unit L1-SUB-TDS was determined to be Class 1.

Between December 18, 2017, and December 21, 2017, a Remedial Action Support Survey (RASS) was performed in the survey unit after the excavation was complete and before FSS was performed. The purpose of the RASS was to ensure that residual radionuclide concentrations in the excavation were below the Operational DCGL for soil. 100% of the surface area of soil in the excavation was scanned using a Ludlum Model 2350-1 data logger paired with a Ludlum Model 44-10 detector. The alarm set point (ASP) was set using a gross background of 31,800 cpm and a minimum detectable count rate (MDCR) of 1,906 cpm for 8

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS a total of 33,706 cpm. One (1) alarm was produced and verified during the RASS scan survey. In accordance with the RASS sample plan, five (5) judgmental soil samples were collected in the excavation at areas where scan alarms occurred or where significant increases in count rate were noted. The five (5) samples were analyzed using the on-site gamma spectroscopy system. Gamma spectroscopy revealed Cs-137 concentrations ranging between 3.94E-02 pCi/g and 6.74E-01 pCi/g. Co-60 concentrations ranged between 4.30E-01 pCi/g and 5.52E-01 pCi/g. Areas that alarmed and where judgmental samples were collected were bounded and remediated to levels below the Operational DCGL.

Remediation was deemed sufficient as no further alarms were produced upon rescan of the elevated areas.

4. DATA QUALITY OBJECTIVES Final Status Survey planning and design hinges on coherence with the Data Quality Objective (DQO) process to ensure, through compliance with explicitly defined inputs and boundaries, that the primary objective of the survey is satisfied. The DQO process is described in the LACBWR LTP in accordance with MARSSIM. The appropriate design for a given survey was developed using the DQO process as outlined in Appendix D of MARSSIM. A summary of seven steps of the DQO process are outlined as follows.

The DQO process incorporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline condition is technically known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would indicate that residual activity within the survey unit does not exceed the release criteria. Therefore, the survey unit would satisfy the primary objective of the FSS sample plan.

The primary objective of the FSS sample plan was to demonstrate that the level of residual radioactivity in survey unit L1-SUB-TDS did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).

LaCrosseSolutions TSD RS-TD-313196-001, Radionuclides of Concern during LACBWR Decommissioning (Reference 7) established the basis for an initial suite of potential ROC for decommissioning. LTP Chapter 2 provides detailed characterization data that describes the results of surveys taken of soil. Surface and subsurface soil samples were taken in each impacted open land survey units and analyzed for the presence of plant-derived 9

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS radionuclides. The results of surface and subsurface soil characterization in the impacted area surrounding LACBWR indicate that there is minimal residual radioactivity in soil.

Insignificant dose contributors were determined to be consistent with the guidance contained in Section 3.3 of NUREG-1757, Volume 2, Revision 1, Consolidated Decommissioning Guidance Characterization, Survey, and Determination of Radiological Criteria, Final Report (Reference 8). In all soil and concrete scenarios, Cs-137, Co-60, Sr-90, Eu-152 and Eu-154 contribute nearly 100% of the total dose. The remaining radionuclides were designated as insignificant dose contributors and are eliminated from further detailed evaluation. Therefore, the final ROCs for LACBWR soil, basement concrete and buried piping are Cs-137, Co-60, Sr-90, Eu-152 and Eu-154.

LTP Chapter 6, Section 6.14.1 discusses the process used to derive the ROC for the decommissioning of LACBWR, including the elimination of insignificant dose contributors from the initial suite. Table 4-1 presents the ROC for the decommissioning of soil at LACBWR and the normalized mixture fractions based on the radionuclide mixture.

Table 4 Dose Significant Radionuclides and Mixture for Soil Fraction of Total Activity Radionuclide (normalized)(1)

Co-60 0.064 Sr-90 0.098 Cs-137 0.829 Eu-152 0.005 Eu-154 0.003 (1) Based on maximum percent of total activity from Table 22 of RS-TD-313196-001, normalized to one for the dose significant radionuclides.

LTP, Section 5.2 states that each radionuclide-specific Base Case DCGL is equivalent to the level of residual radioactivity (above background levels) that could, when considered independently, result in a Total Effective Dose Equivalent (TEDE) of 25 mrem/yr to an Average Member of the Critical Group. To ensure that the summation of dose from each source term is 25 mrem/yr or less after all FSS is completed, the Base Case DCGLs are reduced based on an expected, or a priori, fraction of the 25 mrem/yr dose limit from each source term. The reduced DCGLs, or "Operational" DCGLs can be related to the Base Case DCGLs as an expected fraction of dose based on an a priori assessment of what the expected dose should be based on the results of site characterization, process knowledge, and the extent of planned remediation. The Operational DCGL is then used as the DCGL for the FSS design of the survey unit (calculation of surrogate DCGLs, investigations levels, etc.).

Details of the Operational DCGLs derived for each dose component and the basis for the 10

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS applied a priori dose fractions are provided in LC-FS-TSD-002, Operational Derived Concentration Guideline Levels for Final Status Survey (Reference 9).

The dose contribution from each ROC is accounted for using the SOF to ensure that the total dose from all ROC does not exceed the dose criterion. A Base Case DCGL that is established for the average residual radioactivity in a survey unit is equivalent to a DCGL W.

The DCGLW can be multiplied by Area Factors to obtain a Base Case DCGL that represents the same dose to an individual for residual radioactivity over a smaller area within a survey unit.

At LACBWR, compliance is demonstrated through the summation of dose from five (5) distinct source terms for the end-state (basements, soils, buried pipe, above-ground structures, and groundwater). When applied to soil, the DCGLs are expressed in units of activity per unit of mass (pCi/g).

For LACBWR, soil is defined as a layer of soil beginning at the surface but extending to a depth of 1 m to allow for flexibility in compliance demonstration if contamination deeper than 0.15 m is encountered. Based on characterization data and historical information, there are no expectations of encountering a source term geometry that is comprised of a clean surface layer of soil over a contaminated subsurface soil layer. EnergySolutions TSD RS-TD-313196-004 and LTP Chapter 6, Sections 6.4 and 6.8 provide the exposure scenarios and modeling parameters that were used to calculate the site-specific soil DCGLs. The adjusted soil DCGLs for the unrestricted release of open land survey units as provided in Chapter 6, Section 6.16.1 are reproduced in Table 4-2. The insignificant dose contributor percentages for the most limiting basement scenario was used to adjust the DCGLs for soil to account for the dose from the eliminated insignificant contributor radionuclides.

Table 4 Base Case DCGLs for Soil DCGLS Radionuclide (pCi/g)

Co-60 10.6 Sr-90 5470 Cs-137 48.3 Eu-152 23.6 Eu-154 21.9 The Operational DCGLs are then used as the DCGL for the FSS design of the survey unit (calculation of surrogate DCGLs, investigation levels, etc.). The OpDCGLS for the unrestricted release of soil are provided in Table 4-3.

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Table 4 Operational DCGLs for Soil OpDCGLS Radionuclide (pCi/g)

Co-60 3.83 Sr-90 1970.45 Cs-137 17.39 Eu-152 8.51 Eu-154 7.89 Instrument DQOs included a verification of the ability of the survey instrument to detect the radiation(s) of interest relative to the Operational DCGL. Survey instrument response checks were required prior to issuance and after the instrument had been used. Control and accountability of survey instruments was required to assure the quality and prevent the loss of data.

As part of the DQOs applied to laboratory processes, analysis results were reported as actual concentrations, therefore, the actual concentrations are used as the recorded FSS result for measurement and/or sample values even if less than the reported MDC. Negative reported concentrations are recorded as "zero". Results were not reported as "less than MDC"

(<MDC). Sample report summaries included unique sample identification, analytical method, radionuclide, result, uncertainty, laboratory data qualifiers, units, and the observed MDC.

In accordance with the LTP, for laboratory analysis, MDCs less than 10% of the Operational DCGL were preferable while MDCs up to 50% of the Operational DCGL were acceptable.

The minimum acceptable MDC for measurements obtained using field instruments was 50% of the applicable Operational DCGL.

5. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. Guidance for preparing FSS plans is provided in procedure LC-FS-PR-002, Final Status Survey Package Development.

The DQO process validated that Co-60, Sr-90, Cs-137, Eu-152, and Eu-154 would be the ROC in survey unit L1-SUB-TDS as presented in LTP Section 5.1. During the data analysis of the FSS results, concentrations for the HTD ROC Sr-90 are inferred using a surrogate approach. Cs-137 is the principle surrogate radionuclide for Sr-90. During characterization, both Sr-90 and Cs-137 was positively detected in all thirty (30) concrete core samples 12

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS assessed in the Reactor Building, Tunnel, and Waste Treatment Building. The 95% Upper Confidence Limit (UCL) of the Cs-137 fractions was chosen to represent the overall nuclide mix for soils/buried pipe, the Reactor Building, and the Waste Gas Tank Vault. The surrogate ratio for soil is given in Table 5-1.

Table 5-1 Soil Surrogate Ratio Radionuclides Ratio Sr-90/Cs-137 0.502 The equation for calculating a surrogate DCGL is as follows:

Equation 1 Where: DCGLSur = Surrogate radionuclide DCGL DCGL2,3 ... n = DCGL for radionuclides to be represented by the surrogate Rn = Ratio of concentration (or nuclide mixture fraction) of radionuclide "n" to surrogate radionuclide Using the Operational DCGLs presented in Table 4-3 and the ratio from Table 5-1, the following surrogate calculation was performed:

Equation 2 1

SurrogatevcGL (cs- 137) = [( 1 ) +( 0.S0Z )] = 17.31 pCi/g 17 .39(cs-l37) 1970.45(sr-90)

The surrogate Operational DCGL that was used for Cs-137 in this survey unit for direct comparison of sample results to demonstrate compliance was 17.31 pCi/g.

The action levels for survey unit L1-SUB-TDS are based on the Operational DCGL and are presented in Table 5-2.

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Table 5-2 Action Levels for Survey Unit L1-SUB-TDS Action Level ROC (pCi/g)

Co-60 3.83(1)

Cs-137 17.31(2)

Eu-152 8.51(1)

Eu-154 7.89(1)

(1) Based on the Operational DCGL.

(2) Based on the surrogate adjusted DCGL of Cs-137 while inferring Sr-90.

The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set.

The number of soil samples for FSS was determined in accordance with procedure LC-FS-PR-002. The relative shift (/1/cr) for the survey unit data set is defined as shift (Ii), whic h is the Upper Boundary of the Gray Region (UBGR), or the DCGL (SOF of 1), minus the Lower Bound of the Gray Region (LBGR) (SOF of 0.5), divided by sigma (cr), which is the standard deviation of the data set used for survey design. The optimal value for /1/cr should range between one (1) and three (3) . The largest value the /1/cr can have is three (3). If the

/1/cr exceeds three (3), then the value of three (3) will be used for /1/cr. The /1/cr for survey unit L1-SUB-TDS, based on Cs-137 and Co-60 data for subsurface soil samples collected during characterization of L1-010-102, was calculated as follows:

Equation 3 11/cr = 0.5/0.003 = 166.67 As the calculated relative shift (166.67) was greater than three (3), then a value of three (3) was used as the adjusted Mcr. Both the Type I error, or a value, and the Type II error, or

~ value, was set at 0.05. The sample size from Table 5.5 of MARSSIM that equates to the Type I and Type II error of 0.05 for use with the Sign Test is an N value of fourteen (14).

A Prospective Power Curve was generated using COMPASS, a software package developed under the sponsorship of the United States Nuclear Regulatory Commission (USNRC) for implementation of the MARSSIM in support of the decommissioning license termination rule (10CFR20, Subpart E). The result of the COMPASS computer run showed adequate power for the survey design. The survey design specified fourteen (14) soil samples for non-parametric statistical testing.

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS As the survey unit was classified as Class 1, sample locations were selected based on a systematic triangular grid with a random starting point. The systematic locations of the soil samples were selected using Visual Sample Plan (VSP), in accordance with LC-FS-PR-002.

Input parameters included use of aerial photographs, the GPS route of the boundary of the excavation, and seventy (7 0) 20' by 20' grids . The systematic coordinates generated with VSP were integrated with a GPS to identify sample locations in the field. Table 5-3 lists the systematic samples collected for FSS and the corresponding GPS coordinates, based on the Wisconsin State Plane North American Datum 1983 coordinate system.

Table 5-3 Systematic Sample Locations Sample ID Northing Easting L1-SUB-TDS-FSGS-001-SB 570938.3660 1642047.7039 L1-SUB-TDS-FSGS-002-SB 570964.4550 1642002.5164 L1-SUB-TDS-FSGS-003-SB 570964.4550 1642032.6414 L1-SUB-TDS-FSGS-004-SB 570990.5441 1642002.5789 L1-SUB-TDS-FSGS-005-SB 571016.6331 1642002.5164 L1-SUB-TDS-FSGS-006-SB 571016.6331 1642032.6414 L1-SUB-TDS-FSGS-007-SB 571042.7221 1642017.5789 L1-SUB-TDS-FSGS-008-SB 571042.7221 1642047.7039 L1-SUB-TDS-FSGS-009-SB 571042.7221 1642077.8289 L1-SUB-TDS-FSGS-010-SB 571068.8112 1642032.6414 L1-SUB-TDS-FSGS-011-SB 571068.8112 1642062.7664 L1-SUB-TDS-FSGS-012-SB 571068.8112 1642092.8915 L1-SUB-TDS-FSGS-013-SB 571094.9002 1642047.7039 L1-SUB-TDS-FSGS-014-SB 571094.9002 1642077.8289 Although one (1) judgmental sample was required for survey design, ten (10) judgmental soil samples were collected at locations of higher scan readings and for continuing characterization as a conservative measure. In total, twenty-four (24) soil samples were collected for the FSS of survey unit L1-SUB-TDS. The coordinates for the judgmental samples are provided in Table 5-4.

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Table 5 Judgmental Sample Locations Sample ID Northing Easting L1-SUB-TDS-FJGS-001-SB 571044.994 1642039.042 L1-SUB-TDS-FJGS-002-SB 571082.009 1642064.649 L1-SUB-TDS-FJGS-003-SB 571090.293 1642057.744 L1-SUB-TDS-FJGS-004-SB 571051.946 1641998.938 L1-SUB-TDS-FJGS-005-SB 571026.280 1642027.408 L1-SUB-TDS-FJGS-006-SB 571035.204 1642046.196 L1-SUB-TDS-FJGS-007-SB 570944.621 1642068.758 L1-SUB-TDS-FJGS-008-SB 571042.305 1642073.367 L1-SUB-TDS-FJGS-009-SB 571064.010 1642003.777 L1-SUB-TDS-FJGS-010-SB 571075.804 1642049.975 The LACBWR LTP Chapter 5, Section 5.1 states that soil samples will be collected during FSS to confirm the HTD to surrogate radionuclide ratio for continuing characterization. Ten percent (10%) of the FSS samples collected from open land survey units (including excavations where major sub-grade structures previously resided) will be analyzed for HTD ROC. In addition, if any sample has a SOF of 10% of the Operational DCGL or more, it must be sent for HTD ROC analysis. Only the HTD radionuclide included as ROC (Sr-90) will be analyzed in the FSS confirmatory samples. For samples with positive results for both the HTD ROC and the corresponding surrogate radionuclide (Cs-137), the HTD surrogate ratio will be derived and compared against the 95% UCL ratio (see Table 5-1). If the derived ratio from the confirmatory samples exceeds the 95% UCL ratio, then the area-specific ratio as determined by actual survey data will be used.

The selection of one (1) soil sample, L1-SUB-TDS-FSGS-010-SB, from the systematic sample population met the requirement that a minimum of 10% of the samples collected for the FSS of the survey unit be analyzed for HTD ROC. The selected sample was sent off-site (GEL Laboratories) for analysis of the HTD ROC as specified in LTP Chapter 5, Section 5.1. Seven (7) of the eight (8) judgmental samples collected for continuing characterization were sent off-site for full suite ROC analysis, as explained in Section 3 of this release record.

The implementation of quality control measures as referenced by LTP Chapter 5, Section 5.9 and LaCrosseSolutions LC-QA-PN-001, Final Status Survey Quality Assurance Project Plan (QAPP) (Reference 10) includes the collection of a soil sample for "split sample" analysis on 5% of the soil samples taken in a survey unit with the locations selected at 16

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS random. One (1) soil sample, L1-SUB-TDS-QSGS-004-SB, was designated for split sample QC analysis for the FSS of this survey unit.

LTP Chapter 5, Section 5.6.4.4 and Table 5-15 specifies that for Class 1 survey units, surface scans will be performed on 100% of the surface area in the survey unit. For survey unit L1-SUB-TDS, 100% scan coverage equates to 1,185.5 m 2. To encapsulate the entire area of the survey unit, a 20 ' by 20 ' grid pattern was overlaid on a map of the survey unit.

The survey unit spanned through portions of thirty-eight (38) of the sixty-three (63) total grids. A map of the scan grid locations is provided in Attachment 1.

For this Class 1 excavation survey unit, the "Investigation Levels" for area scanning and soil sample measurement results are those levels specified in LTP Chapter 5, Table 5-16, and are reproduced below in Table 5-5.

Table 5 Investigation Levels Direct Investigation Classification Scan Investigation Levels Levels

>Operational DCGL or >MDC scan if Class 1 MDCscan is greater than Operational >Operational DCGL DCGL Table 5-6 provides a synopsis of the survey design for survey unit L1-SUB-TDS.

Table 5 Synopsis of Survey Design Feature Design Criteria Basis Survey Unit Surface 1,185.5 m2 GPS Area

• cr= 0.003

• UBGR = SOF of 1 Number of 14

• LBGR = SOF of 0.5 Systematic Samples

• Type I error = 0.05 (N) Type II error = 0.05

• ti/cr = 3 (adjusted)

• MARSSIM Table 5.5 17

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Feature Design Criteria Basis

• Co-60: 3.83 pCi/g

• Sr-90: 1970.45 pCi/g DCGLs and Action

• Cs-137: 17.39 pCi/g Operational DCGLs for soil, Levels LTP Chapter 5, Table 5-6 (Surrogate Cs-137 DCGL: 17.31 pCi/g)

• Eu-152: 8.51 pCi/g

• Eu-154: 7.89 pCi/g Scan and Direct

>Operational DCGL LTP Chapter 5, Table 5-16 Investigation Levels Scan Areal Coverage 1,185.5 m2 or 100% areal coverage LTP Chapter 5, Table 5-15 Number of 1 Per Sample Plan Judgmental Samples 10 (8 for continuing characterization) Actual Number Obtained 1 sample LTP 5.1 & Signed Sample Plan HTD ROC Analysis 8 (7 for continuing characterization) Actual Number Obtained 1 split sample selected at random LTP Chapter 5, Section 5.9 QC 3 Actual Number Obtained

6. SURVEY IMPLEMENTATION For survey unit L1-SUB-TDS, compliance with the unrestricted release criteria was demonstrated through a combination of soil scanning with a Ludlum Model 44-10 gamma detector and the sampling of soil for isotopic analysis.

An FSS Supervisor performed a visual inspection and walk-down of the survey unit on January 4, 2018, prior to performing FSS. The purpose of the walk-down was to assess the physical condition of the survey unit, evaluate access points and travel paths, and identify potentially hazardous conditions.

FSS field activities were conducted under the FSS Sample Plan, which included DQOs, survey design, detailed FSS instructions, job safety analysis, and related procedures for reference. A "Field Log" was used to document field activities and other information pertaining to the performance of the FSS. FSS field activities commenced on January 5, 2018.

FSS field activities were projected to take ten (10) working days to complete. Daily briefings were conducted to discuss the expectations for job performance and to review safety aspects 18

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS of the job. The survey required field activities were performed during normal working hours and concluded on January 15, 2018.

The fourteen (14) systematic soil sample locations were marked with flags based on GPS coordinates provided. Each soil sample consisted of approximately one (1) liter of soil. The sample media was sifted to remove stones and other media larger than one (1) centimeter in diameter. All soil samples were collected, controlled, transported, stored and transferred to the on-site laboratory using the Chain-of-Custody process from LC-FS-PR-012, Chain of Custody Protocol (Reference 11), and in accordance with LC-FS-PR-004, Sample Media Collection for Site Characterization and Final Status Survey (Reference 12), LC-FS-PR-005, Sample Media Preparation for Site Characterization and Final Status Survey (Reference 13), and LC-FS-PR-001, Sample Storage (Reference 14).

A total of thirty-eight (38) scan grids, constituting a total scan coverage of 1,185.5 m 2, or approximately 100% of the surface area in the survey unit, were established. Background was assessed in the survey unit using a Ludlum 2350-1 paired with a Ludlum Model 44-10 (2"x 2") sodium iodide (Nal) detector. The background was established as the average of five (5) 1-minute static measurements, while maintaining the detector 6" from the soil. In survey unit L1-SUB-TDS, background ranged from 7,263 counts per minute (cpm) up to 8,899 cpm.

All designated scan areas as denoted on Figure 1in Attachment 1 were scanned using a Ludlum 2350-1 paired with a Model 44- 10 2"x 2" Nal detector operated in the rate-meter mode and using audio response. The probe was positioned no more than 3" from the ground and was moved at a scan speed of approximately 0.5 meters per second. In accordance with RS-TD-313196-006, Ludlum Model 44-10 Detector Sensitivity (Reference 15), scan MDC was sufficient to detect residual radioactivity at the action level (adjusted surrogate DCGL of 17.31 pCi/g, which was based on the surrogate adjusted DCGL of Cs-137 while inferring Sr-90). Complete scan results are provided in Attachment 2.

Ten (10) judgmental soil samples were collected during implementation of FSS. These samples were collected to investigate locations where scanning revealed higher readings and for continuing characterization as required by the LTP Chapter 5, Section 5.3.3.4. The locations of the judgmental samples are presented in Figure 2 of Attachment 1.

The survey design specified that a minimum of one (1) sample (10%) was required for HTD ROC analysis. Sample L1-SUB-TDS-FSGS-010-SB was selected for HTD radionuclide analysis. Seven (7) additional samples from continuing characterization (L1-SUB-TDS-FJGS-003-SB, L1-SUB-TDS-FJGS-004-SB, L1-SUB-TDS-FJGS-005-SB, L1-SUB-TDS-FJGS-006-SB, L1-SUB-TDS-FJGS-007-SB, L1-SUB-TDS-FJGS-008-SB, and L1-SUB-TDS-FJGS-010-SB) were selected for HTD analysis of the initial full suite of radionuclides.

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS The survey design specified one (1) sample to be collected for QC split and duplicate analysis. The implementation of survey specific QC measures included the collection of three (3) samples (L1-SUB-TDS-QSGS-004-SB, L1-SUB-TDS-FJGS-008-SB SPLIT, and L1-SUB-TDS-FJGS-009-SB SPLIT) for split and duplicate sample analysis.

7. SURVEY RESULTS All areas identified in the FSS plan were scanned for elevated radiation levels. No elevated measurement locations were identified by surface scan. Table 7-1 provides an overview of the scan results for all scan grids (identified as A1 through G9), the 1 m 2 scan areas around each sample location (identified as SP1 through SP14 and JSP2 through JSP10), and QC locations (identified with a Q). Complete scan results are provided in Attachment 2.

Table 7-1 Synopsis of Scan Results Highest Action Logged # of Scan Judgmental Investigation Scan Area Level Reading Alarms Samples Samples (cpm) (cpm)

A1 8,757 33,706 0 0 0 A2 9,075 33,706 0 0 0 A3 8,879 33,706 0 0 0 A4 9,613 33,706 0 1 0 A5 9,230 33,706 0 1 0 A6 10,041 33,706 0 0 0 A7 9,130 33,706 0 0 0 B1 8,767 33,706 0 0 0 B2 9,005 33,706 0 2 0 B3 9,938 33,706 0 0 0 B4 9,160 33,706 0 0 0 B5 10,039 33,706 0 0 0 B6 10,422 33,706 0 0 0 B7 9,762 33,706 0 0 0 B8 8,514 33,706 0 0 0 C1 8,514 33,706 0 0 0 C2 13,403 33,706 0 1 0 C3 8,747 33,706 0 0 0 C4 11,957 33,706 0 0 0 C4 16,975 33,706 0 2 0 C5 10,934 33,706 0 1 0 20

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Highest Action Logged # of Scan Judgmental Investigation Scan Area Level Reading Alarms Samples Samples (cpm) (cpm)

C5QC 12,588 33,706 0 0 0 C6 12,495 33,706 0 0 0 C7 10,676 33,706 0 0 0 C8 8,914 33,706 0 0 0 C9 7,435 33,706 0 0 0 D1 9,244 33,706 0 0 0 D2 9,297 33,706 0 0 0 D3 9,148 33,706 0 1 0 D8 14,449 33,706 0 0 0 D8 10,462 33,706 0 0 0 D9 7,695 33,706 0 0 0 E1 9,676 33,706 0 0 0 E2 9,570 33,706 0 0 0 E3 10,641 33,706 0 0 0 E8 11,516 33,706 0 0 0 E9 8,950 33,706 0 0 0 F8 13,054 33,706 0 1 0 F9 11,309 33,706 0 0 0 G8 13,320 33,706 0 0 0 G9 14,024 33,706 0 0 0 JSP10 7,297 33,706 0 0 0 JSP2 13,088 33,706 0 0 0 JSP3 8,209 33,706 0 0 0 JSP4 9,009 33,706 0 0 0 JSP5 7,229 33,706 0 0 0 JSP6 9,185 33,706 0 0 0 JSP7 12,952 33,706 0 0 0 JSP8 8,995 33,706 0 0 0 JSP9 8,344 33,706 0 0 0 QC4 9,047 33,706 0 0 0 SP1 13,778 33,706 0 0 0 SP10 8,736 33,706 0 0 0 SP11 8,211 33,706 0 0 0 21

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Highest Action Logged # of Scan Judgmental Investigation Scan Area Level Reading Alarms Samples Samples (cpm) (cpm)

SP12 8,835 33,706 0 0 0 SP13 7,724 33,706 0 0 0 SP14 8,498 33,706 0 0 0 SP2 7,649 33,706 0 0 0 SP3 9,322 33,706 0 0 0 SP4 9,708 33,706 0 0 0 SP5 9,710 33,706 0 0 0 SP6 8,338 33,706 0 0 0 SP7 8,358 33,706 0 0 0 SP8 8,667 33,706 0 0 0 SP9 8,715 33,706 0 0 0 At the time of the FSS, the Action Level was based upon a fraction of the Base Case Cs-137 DCGL and a pre-established background count rate. The Action Level was calculated using a background of 31,800 cpm and an MDCR of 1,906 cpm for a total of 33,706 cpm.

The MDCR value equates to Cs-137 concentration of 9.2 pCi/g, which is equivalent to approximately 20% of the Cs-137 Base case DCGL for soil. A pre-established gross background and ASP was used during FSS because of an anticipated elevated background due to the survey unit's proximity to the Reactor Building.

Retroactively fitting the scan data to Action Levels based on the Operational DCGL and the actual background data collected during the FSS, resulted in fourteen (14) scan measurements that would have alarmed, and in turn would have triggered the collection of investigational soil samples. As can be seen in Table 7-1 above, no investigational samples were collected. Because 100% of the soil in the survey unit was scanned and the maximum Sum-of-Fraction (SOF) of all applicable Radionuclides of Concern (ROC), either by direct measurement or by inference, is equal to 0.0552 when applying the respective Operational Derived Concentration Guideline Levels (OpDCGLS) for soil, the probability of discovering an elevated soil sample is very low, even had investigational samples been collected.

The on-site laboratory analyzed the fourteen (14) soil samples taken for non-parametric statistical testing using the on-site gamma spectroscopy system. A summary of the gamma spectroscopy results for the fourteen (14) samples collected for non-parametric statistical testing is provided in Table 7-2. Gamma spectroscopy results revealed ten (10) samples above MDC for Cs-137 and one (1) sample above MDC for Co-60; there were no samples above MDC for any other ROC. The concentration for Sr-90 was inferred based on the ratio 22

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS specified in Table 5-1. The complete gamma spectroscopy reports are presented in Attachment 7. The basic statistics for the systematic sample population is summarized in Table 7-3.

Table 7 Summary of Gamma Spectroscopy Results for Soil Samples Comprising the Statistical Sample Population Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)

L1-SUB-TDS-FSGS-001-SB 3.94E-02 4.28E-02 4.47E-02 5.51E-02 2.15E-02 L1-SUB-TDS-FSGS-002-SB 3.73E-02 1.88E-02 4.72E-02 2.20E-02 9.44E-03 L1-SUB-TDS-FSGS-003-SB 4.78E-02 7.39E-02 1.14E-01 7.00E-03 3.71E-02 L1-SUB-TDS-FSGS-004-SB 4.69E-02 5.89E-02 1.18E-01 1.04E-01 2.96E-02 L1-SUB-TDS-FSGS-005-SB 1.13E-01 1.26E-01 0.00E+00 1.45E-01 6.33E-02 L1-SUB-TDS-FSGS-006-SB 3.72E-02 1.39E-02 0.00E+00 3.72E-02 6.98E-03 L1-SUB-TDS-FSGS-007-SB 4.15E-02 9.53E-02 8.28E-02 1.89E-03 4.78E-02 L1-SUB-TDS-FSGS-008-SB 6.97E-02 1.37E-01 0.00E+00 0.00E+00 6.88E-02 L1-SUB-TDS-FSGS-009-SB 4.52E-02 6.83E-02 6.66E-02 3.99E-02 3.43E-02 L1-SUB-TDS-FSGS-010-SB 4.72E-02 9.00E-02 1.37E-01 1.00E-01 4.52E-02 L1-SUB-TDS-FSGS-011-SB 3.06E-02 3.85E-02 6.61E-02 1.83E-02 1.93E-02 L1-SUB-TDS-FSGS-012-SB 7.21E-02 1.77E-01 1.02E-01 1.55E-02 8.89E-02 L1-SUB-TDS-FSGS-013-SB 3.11E-02 6.69E-02 1.58E-01 1.65E-01 3.36E-02 L1-SUB-TDS-FSGS-014-SB 7.89E-02 2.08E-01 1.41E-01 3.19E-02 1.04E-01 Note: Bold values indicate concentrations greater than MDC.

Table 7 Basic Statistical Properties of Systematic Sample Population Std. Avg. Avg.

Mean Median Max. Min. BcDCGL ROC Dev. SOF per Dose per (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) ROC ROC Co-60 5.27E-02 4.61E-02 1.13E-01 3.06E-02 0.0230 1.06E+01 0.0050 0.1243 Cs-137 8.68E-02 7.11E-02 2.08E-01 1.39E-02 0.0574 4.83E+01 0.0018 0.0449 Eu-152 7.70E-02 7.47E-02 1.58E-01 0.00E+00 0.0540 2.36E+01 0.0033 0.0815 Eu-154 5.31E-02 3.46E-02 1.65E-01 0.00E+00 0.0539 2.19E+01 0.0024 0.0606 Sr-90 4.36E-02 3.57E-02 1.04E-01 6.98E-03 0.0288 5.47E+03 0.0000 0.0002 23

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS The off-site laboratory, GEL Laboratories, processed the eight (8) samples selected for HTD analysis. Continuing characterization samples L1-SUB-TDS-FJGS-003-SB, L1-SUB-TDS-FJGS-004-SB, L1-SUB-TDS-FJGS-005-SB, L1-SUB-TDS-FJGS-006-SB, L1-SUB-TDS-FJGS-007-SB, L1-SUB-TDS-FJGS-008-SB, L1-SUB-TDS-FJGS-010-SB, and FSS sample L1-SUB-TDS-FSGS-010-SB were selected. All off-site samples were analyzed for the initial suite of radionuclides, except for sample L1-SUB-TDS-FSGS-010-SB, which was only analyzed for Sr-90. All analyses met the required MDC.

Sr-90 was not detected in any of the samples sent for off-site analysis. Therefore, there was no need to re-evaluate the 95% UCL ratio of 0.502 established during continuing characterization. Gamma spectroscopy results revealed six (6) samples above MDC for Cs-137 with a maximum concentration of 0.189 pCi/g. Two (2) samples were above MDC for Co-60, and two (2) samples were above MDC for Tc-99 with maximum concentrations of 0.0816 pCi/g and 0.628 pCi/g, respectively. No samples were above MDC for any other ROC. The positive Tc-99 samples are part of the continuing characterization population. As stated in Section 3 of this release record, the IC dose is unchanged (dose fraction less than 10%). The results are provided in Table 7-4.

Table 7 Off-Site Analysis Results Cm- Pu-Am-241 Am-243 Np-237 Pu-238 Pu-241 Ni-59 Cs-137 Co-60 Sam.. eID 243/244 239/240 (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)

(pCi/g) (pCi/g)

Ll-SUB-TDS-FSGS-010-SB Ll-SUB-TDS-FJGS-003-SB 4.l0E-03 l.94E-02 2.20E-03 5.00E-04 -7.20E-03 -4.S0E-03 -8.95E-02 -7.39E-0l 8.83E-02 l.35E-02 Ll-SUB-TDS-FJGS-004-SB l.91E-02 2.60E-03 -4.S0E-03 0.OOE+-00 l.83E-02 -1.70E-03 -1.09E+-O0 -1.24E-0l 1.03E-01 5.96E-02 Ll-SUB-TDS-FJGS-005-SB l.15E-02 l.70E-02 -1.S0E-03 5.00E-04 -4.20E-03 9.40E-03 -8.41E-0l -7.51E-0l 1.07E-01 8.16E-02 Ll-SUB-TDS-FJGS-006-SB l.76E-02 9.lOE-03 -9.S0E-03 4.00E-04 -4.20E-03 -l.1SE-02 -2.S0E+-00 -l.71E+-OO 1.89E-01 4.34E-02 Ll-SUB-TDS-FJGS-007-SB -l.70E-03 -2.83E-02 l.27E-02 5.00E-04 -2.60E-03 -I.0SE-02 -2.0SE+-00 l .88E-01 3.78E-02 l.41E-02 Ll-SUB-TDS-FJGS-008-SB 9.40E-03 l.47E-02 3.20E-03 l.90E-03 -2.lOE-03 -4.30E-03 -1.34E+-OO -2.60E+-OO 7.19E-02 -9.40E-03 Ll-SUB-TDS-FJGS-010-SB -3.40E-03 l.75E-02 5.20E-03 3.l0E-03 -6.60E-03 -3.03E-03 -3.59E-0l -4.26E-0l 5.63E-02 -3.20E-03 En-152 En-154 En-155 Nb-94 Sr-90 H-3 C-14 Tc-99 Fe-55 Ni-63 Sam.. eID loCi/1d {oCi/2) {oCi/2) {oCi/2) {oCi/2) {oCi/2) {oCi/2) {oCi/2) {oCi/2) {oCi/2)

Ll-SUB-TDS-FSGS-010-SB 2.06E-0l Ll-SUB-TDS-FJGS-003-SB l .20E-03 -3.90E-03 8.40E-03 2.60E-03 6.23E-02 -2.02E-0l l.87E+-O0 -3.29E-01 l.36E+-OO l.89E-01 Ll-SUB-TDS-FJGS-004-SB 9.20E-03 -3.00E-04 -3.0lE-02 6.0lE-03 2.29E-02 -5.28E-0l -8.69E-0l 5.30E-01 2.34E+-OO l.98E-0l Ll-SUB-TDS-FJGS-005-SB 4.S0E-03 -6.60E-03 3.89E-02 -8.00E-03 -3.74E-02 2.93E-0l 1.40E+-O0 2.89E-0l l.59E-0l l.09E+-O0 Ll-SUB-TDS-FJGS-006-SB 4.90E-03 -4.90E-03 3.89E-02 5.40E-03 -6.57E-02 3.40E-0l -1.07E+-O0 6.28E-01 l.02E+-O0 7.96E-0l Ll-SUB-TDS-FJGS-007-SB -4.38E-02 -1.28E-02 -1.75E-02 -1.28E-02 l.39E-02 3.54E+-O0 -l.72E-02 l.58E-0l 7.78E-0l -8.86E-0l Ll-SUB-TDS-FJGS-008-SB 2.03E-03 l.95E-02 3.67E-02 -3.lOE-03 l.13E-0l -l.lSE+-00 -8.32E-0l l .98E-0l 3.00E+-00 -1.60E-0l Ll-SUB-TDS-FJGS-010-SB l.62E-02 3.27E-02 l.32E-02 l.14E-02 -5.03E-02 -8.41E-0l -1.0lE+-00 4.23E-0l 5.15E-0l -4.0SE-01 Note: Bold values indicate concentrations greater than MDC.

The on-site laboratory analyzed the ten (10) judgmental soil samples using the on-site gamma spectroscopy system. A summary of the analytical results for the judgmental soil 24

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS samples is provided in Table 7-5. Gamma spectroscopy results revealed ten (10) samples above MDC for Cs-137 with max concentration 0.188 pCi/g. Two (2) samples above MDC for Co-60 with max concentration 0.257 pCi/g. No samples above MDC for any other ROC.

The concentration for Sr-90 was inferred based on the ratio specified in Table 5-1. The complete gamma spectroscopy reports are presented in Attachment 7.

Table 7 Summary of Gamma Spectroscopy Results for Judgmental Soil Samples Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)

L1-SUB-TDS-FJGS-001-SB 4.45E-02 8.17E-02 9.79E-03 2.71E-02 4.10E-02 L1-SUB-TDS-FJGS-002-SB 7.23E-02 9.80E-02 7.68E-02 1.40E-01 4.92E-02 L1-SUB-TDS-FJGS-003-SB 5.84E-02 2.92E-02 0.00E+00 6.38E-02 1.47E-02 L1-SUB-TDS-FJGS-004-SB 2.57E-01 6.07E-02 6.73E-02 1.40E-01 3.05E-02 L1-SUB-TDS-FJGS-005-SB 5.37E-02 7.31E-02 0.00E+00 1.55E-02 3.67E-02 L1-SUB-TDS-FJGS-006-SB 9.53E-02 1.88E-01 1.23E-01 0.00E+00 9.44E-02 L1-SUB-TDS-FJGS-007-SB 3.63E-02 6.06E-02 1.02E-02 1.96E-02 3.04E-02 L1-SUB-TDS-FJGS-008-SB 2.19E-02 6.16E-02 7.01E-03 1.40E-01 3.09E-02 L1-SUB-TDS-FJGS-009-SB 2.22E-02 1.61E-01 0.00E+00 6.48E-02 8.08E-02 L1-SUB-TDS-FJGS-010-SB 3.17E-02 4.30E-02 7.80E-02 4.34E-02 2.16E-02 Note: Bold values indicate concentrations greater than MDC.

The implementation of survey specific QC measures included the collection of three (3) samples (L1-SUB-TDS-QSGS-004-SB, L1-SUB-TDS-FJGS-008-SB SPLIT, L1-SUB-TDS-FJGS-009-SB SPLIT) for split and duplicate sample analysis. The on-site laboratory analyzed the designated QC samples using the on-site gamma spectroscopy system. A summary of the analytical results for the QC samples is provided in Table 7-6. Gamma spectroscopy results revealed three (3) samples above MDC for Cs-137, with a maximum concentration 0.0695 pCi/g, and no samples above MDC for any other ROC. The concentration for Sr-90 was inferred based on the ratio specified in Table 5-1.

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FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Table 7 Summary of Gamma Spectroscopy Results for QC Soil Samples Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)

L1-SUB-TDS-QSGS-004-SB 6.51E-02 4.39E-02 8.04E-02 8.72E-03 2.20E-02 L1-SUB-TDS-FJGS-008-SB 3.64E-02 6.95E-02 7.33E-02 6.54E-03 3.49E-02 SPLIT L1-SUB-TDS-FJGS-009-SB 7.75E-02 6.20E-02 3.35E-03 1.64E-02 3.11E-02 SPLIT Note: Bold values indicate concentrations greater than MDC.

The SOF or "unity rule" is the mathematical test used to evaluate compliance with radiological criteria for license termination when more than one radionuclide has been determined to be potentially present. The equation for the unity rule is:

Equation 4 Ci + C2 + ......... .. Cn ~l DCGLi DCGL2 DCGLn Where: Cn = concentration of radionuclide n DCGLn = DCGL of radionuclide n.

The results of the unity rule calculation for the ROC in the systematic sample population for survey unit L1-SUB-TDS are provided in Table 7-7.

Table 7 Sum-of-Fractions for Individual Soil Samples (Systematic and QC)

Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L1-SUB-TDS-FSGS-001-SB 0.01029 0.00246 0.00525 0.00698 0.00001 0.02500 L1-SUB-TDS-FSGS-002-SB 0.00974 0.00108 0.00555 0.00279 0.00000 0.01916 L1-SUB-TDS-FSGS-003-SB 0.01248 0.00425 0.01340 0.00089 0.00002 0.03103 L1-SUB-TDS-FSGS-004-SB 0.01225 0.00339 0.01387 0.01318 0.00002 0.04269 L1-SUB-TDS-FSGS-005-SB 0.02950 0.00725 0.00000 0.01838 0.00003 0.05516 L1-SUB-TDS-FSGS-006-SB 0.00971 0.00080 0.00000 0.00471 0.00000 0.01523 L1-SUB-TDS-FSGS-007-SB 0.01084 0.00548 0.00973 0.00024 0.00002 0.02631 L1-SUB-TDS-FSGS-008-SB 0.01820 0.00788 0.00000 0.00000 0.00003 0.02611 L1-SUB-TDS-FSGS-009-SB 0.01180 0.00393 0.00783 0.00506 0.00002 0.02863 L1-SUB-TDS-FSGS-010-SB 0.01232 0.00518 0.01610 0.01267 0.00002 0.04630 26

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L1-SUB-TDS-FSGS-011-SB 0.00799 0.00221 0.00777 0.00232 0.00001 0.02030 L1-SUB-TDS-FSGS-012-SB 0.01883 0.01018 0.01199 0.00196 0.00005 0.04300 L1-SUB-TDS-FSGS-013-SB 0.00812 0.00385 0.01857 0.02091 0.00002 0.05146 L1-SUB-TDS-FSGS-014-SB 0.02060 0.01196 0.01657 0.00404 0.00005 0.05323 L1-SUB-TDS-QSGS-004-SB 0.01700 0.00252 0.00945 0.00111 0.00001 0.03009 L1-SUB-TDS-FJGS-008-SB 0.00950 0.00400 0.00861 0.00083 0.00002 0.02296 SPLIT L1-SUB-TDS-FJGS-009-SB 0.02023 0.00357 0.00039 0.00208 0.00002 0.02629 SPLIT Systematic Measurements Number of Systematic Measurements = 14

1. of Systematic Measurements with SOF > 1 = 0

1. of Systematic Measurements with SOF > 0.1 (HTD Assessment) = 0 Max Individual Systematic Measurement SOF = 0.0552 Mean Systematic Measurement SOF = 0.0345 The results of the unity rule calculation for the ROC in the judgmental sample population for survey unit L1-SUB-TDS are provided in Table 7-8.

Table 7 Sum-of-Fractions for Individual Soil Samples (Judgmental)

Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L1-SUB-TDS-FJGS-001-SB 0.01162 0.00470 0.00115 0.00343 0.0002 0.02092 L1-SUB-TDS-FJGS-002-SB 0.01888 0.00564 0.00902 0.01774 0.00002 0.05131 L1-SUB-TDS-FJGS-003-SB 0.01525 0.00168 0.00000 0.00809 0.00001 0.02502 L1-SUB-TDS-FJGS-004-SB 0.06710 0.00349 0.00791 0.01774 0.00002 0.09626 L1-SUB-TDS-FJGS-005-SB 0.01402 0.00420 0.00000 0.00196 0.00002 0.02021 L1-SUB-TDS-FJGS-006-SB 0.02488 0.01081 0.01445 0.0000 0.00005 0.05019 L1-SUB-TDS-FJGS-007-SB 0.00948 0.00348 0.00120 0.00248 0.00002 0.01666 L1-SUB-TDS-FJGS-008-SB 0.00572 0.00354 0.00082 0.01774 0.00002 0.02784 L1-SUB-TDS-FJGS-009-SB 0.00580 0.00926 0.00000 0.00821 0.00004 0.02331 L1-SUB-TDS-FJGS-010-SB 0.00828 0.00247 0.00917 0.00550 0.00001 0.02543 27

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Judgmental Measurements Number of Judgmental Measurements = 10

1. of Judgmental Measurements with SOF > 1 = 0

1. of Judgmental Measurements with SOF > 0.1 (HTD Assessment) = 0 Max Individual Judgmental Measurement SOF = 0.0963 Mean Judgmental Measurement SOF = 0.0357

8. QUALITY CONTROL The on-site laboratory processed three (3) split and duplicate samples (L1-SUB-TDS-QSGS-004-SB, L1-SUB-TDS-FJGS-008-SB SPLIT, and L1-SUB-TDS-FJGS-009-SB SPLIT) using gamma spectroscopy analysis. The data was evaluated using USNRC acceptance criteria specified in Inspection Procedure No. 84750, Radioactive Waste Treatment, and Effluent and Environmental Monitoring (Reference 16). There was not an acceptable agreement between standard and duplicate results using Cs-137 in one of the comparisons. As an investigation, the samples were evaluated under the same procedure using K-40, and the sample concentrations were compared to the OpDCGL. The result of this evaluation determined that there was an acceptable agreement between standard and comparison samples using K-40, and the concentrations of Cs-137 were well below the OpDCGL. Due to the concentrations of Cs-137 reported well below the OpDCGL and the successful comparison of the results using K-40, the survey data was deemed acceptable and representative of actual radiological conditions in the survey unit. Refer to Attachment 4 for data and quality control analysis results.

9. INVESTIGATIONS AND RESULTS No investigations were performed during the performance or analyses of the survey.

10. REMEDIATION AND RESULTS The purpose of the excavation of the portion of survey unit L1-010-102 was to remove the Turbine Building/Turbine Building Offices and 1B Diesel Generator Building, as well as associated system lines. The purpose of the excavation was not to support removal of contaminated subsurface soil.

11. CHANGES FROM THE FINAL STATUS SURVEY PLAN There were no addendums to the FSS plan.

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FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS

12. DATA QUALITY ASSESSMENT (DQA)

The DQO sample design and data were reviewed in accordance with LC-FS-PR-008, Final Status Survey Data Assessment (Reference 17) for completeness and consistency.

Documentation was complete and legible. Surveys and the collection of samples were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 1. The survey design had adequate power as indicated by the Retrospective Power Curve (see Attachment 6).

The analytical results indicated that all samples were less than a SOF of one (1) when compared to the OpDCGLS. Additionally, the maximum activity for each ROC did not exceed 10% of their respective OpDCGLS.

Although MARSSIM states that the Sign Test need not be performed in the instance that no measurements surpass the Operational DCGL, the test was conducted to demonstrate coherence to the statistical principles of the DQO process. The Sign Test was performed on the data and compared to the original assumptions of the DQOs. The evaluation of the Sign Test results clearly demonstrates that the survey unit passes the unrestricted release criteria, thus, the null hypothesis is rejected. The results of the Sign Test are presented in Attachment 3.

The data assessment and review consisted of calculating basic statistical quantities (e.g.,

mean, median, standard deviation). All data was considered valid including negative values, zeros, values reported below the MDC, and values with uncertainties that exceeded two standard deviations. The mean and median values for each ROC were well below the respective Operational DCGLs. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power. Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs.

The mean of all identified isotopes are less than the Consultation Triggers for Residential Soil Concentration depicted in Table H.1 of NUREG 1757, Vol.1, Rev. 2 (MOU Table 1).

The full table is included in Attachment 5 of this release record.

The data for Cs-137 is presented graphically through a frequency plot and quantile plot. All graphical presentations are provided in Attachment 6.

13. ANOMALIES No anomalies were observed during the performance or analyses of the survey.

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FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS

14. CONCLUSION Survey unit L1-SUB-TDS has met the DQOs of the FSS plan. The ALARA criteria as specified in Chapter 4 of the LTP were achieved and remediation was not required.

All identified ROC were used for statistical testing to determine the adequacy of the survey unit for FSS. Evaluation of the data shows that none of the systematic ROC concentration values exceeds the OpDCGLS; therefore, in accordance with LTP Section 5.11, the survey unit meets the release criteria.

The sample data passed the Sign Test. The null hypothesis was rejected. The Retrospective Power Curve showed that adequate power was achieved. The survey unit is properly classified as Class 1.

The dose contribution from soil in survey unit L1-SUB-TDS is 0.3115 mrem/yr TEDE, based on the average concentration of the ROC in samples used for non-parametric statistical sampling.

Survey unit L1-SUB-TDS is acceptable for unrestricted release.

15. REFERENCES

1. LC-FS-PR-009, Final Status Survey Data Reporting

2. La Crosse Boiling Water Reactor License Termination Plan (LTP)

3. LC-FS-PR-002, Final Status Survey Package Development

4. NUREG-1575, Revision 1, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM)

5. La Crosse Boiling Water Reactor Historical Site Assessment (HSA)

6. RS-TD-313196-004, LACBWR Soil DCGL, Basement Concrete DCGL, and Buried Pipe DCGL

7. RS-TD-313196-001, Radionuclides of Concern during LACBWR Decommissioning

8. NUREG-1757, Volume 2, Revision 1, Consolidated Decommissioning Guidance Characterization, Survey, and Determination of Radiological Criteria, Final Report

9. LC-FS-TSD-002, Operational Derived Concentration Guideline Levels for Final Status Survey

10. LC-QA-PN-001, Final Status Survey Quality Assurance Project Plan (QAPP)

11. LC-FS-PR-012, Chain of Custody Protocol

12. LC-FS-PR-004, Sample Media Collection for Site Characterization and Final Status Survey

13. LC-FS-PR-005, Sample Media Preparation for Site Characterization and Final Status Survey

14. LC-FS-PR-001, Sample Storage 30

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS

15. RS-TD-313196-006, Ludlum Model 44-10 Detector Sensitivity

16. USNRC Inspection Procedure No. 84750, Radioactive Waste Treatment, and Effluent and Environmental Monitoring

17. LC-FS-PR-008, Final Status Survey Data Assessment

16. ATTACHMENTS Attachment 1 Figures and Maps Attachment 2 Scan Data Attachment 3 Sign Test Attachment 4 Quality Control Assessment Attachment 5 Consultation Triggers for Residential Soil Concentrations Attachment 6 Graphical Presentations Attachment 7 Sample Analytical Reports Attachment 8 GEL Laboratories Analytical Reports 31

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS ATTACHMENT 1 FIGURES AND MAPS 32

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Figure 16 L1-SUB-TDS Systematic Sample Locations Map 64207;7'. 8289 94.9002 1642 (northing}'571 10 - (easti (northing)'

7 - (easting *.

(northing) 571042~7221 5 - (easting) 1642002.5164 6 (northing)' 571016.6331 4 (QC) -

(easting) 1642017.5789 *

(northing) 570990.5441 t.

2 - (easting) 1642002.5164 (northing) 570964.455 ~

Legend 0 Sample Locations 1 - (easting) 1642047.7039 (northing) 570938.366

- - - 20' x 20' Grid I' *********

• ..*....*.lL 1010102 (2,315 m 2) \

_..\

0 5 i *. ,

10 15 20 25Ltdmrs N o 20 <<1 1!11:1 8l reca Grid Points Turbine Bui lding Excavation in L 1010102 -

12-11 LACBW R Site D L 1-SU B-TOS inside SU L 1010102 (1 , 185 .5 m 2) ,,.; ;:;-

Genoa . WI Date L\Cl!.OSSliSOLVJJU~ Drawing 17121321.f 10/06/2020 33

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Figure 16-2 L1-SUB-TDS Judgmental Sample Locations Biasecf #003 (easting) 1642057.744 (northing) 571000'293 Biased#010 (easting) 1642049.975 (northing) 571075'.804 Biased #002

~ ~ ~~ ~ : - - c ' " - - -*(easting) 1642064.649

• r.. (northing) 571082.009 Biased #009 (easting) 1642003.'777 ----:....ti Grid C4 biased #01 (northing) 571064.01

~ ~ l : ; ; ~./;L.:.'o/-~f/-(easting) 1642039.042 Biased #004 J. (northing) 571044~994 (easting) 164 1998.938 cl #008 (northing) 571051 .946 2073.367 042.305 4204fo196 1035_ :204 Biased#005 (easting) 16~2027.408 (northing) 571026:28 Biased #007 (easting)~ 64206_8.7~

.. .. (northing) 570944'621

..... ** ** *** ** * * * * ** ., * * * * - * . . . . . ,A Legend 0 Sample Locations

- - - 20' x 20' Grid _\ i iI ~ I ~5 I f  ; ,...~

, ....... -. N o 2:1 <<> <<> aor..

.: L1010102 (2,315 m 2) L 1 SUB TDS Biased Sample Locations

• LACBWRSle Genoa, WI L1 -SUB-TDS FSS Excavation as Scanned (1 ,077.2 m 2) ,r= Date 10/0 02 L\l'J<.OSS!iSOL(:HQ'-5 awi 80 .c 34

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS ATTACHMENT 2 SCAN DATA 35

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Table 16 L1-SUB-TDS Complete Scan Data Scan Avg Action Detector Detector M2350-1 Logged Scan Location Background Level Type ID ID Result Alarms (cpm) (cpm) (cpm) 44-10 318218 120636 A1 8,757 7,263 33,706 No 44-10 357776 325246 A2 9,075 8,082 33,706 No 44-10 318218 120636 A3 8,879 7,263 33,706 No 44-10 357776 325246 A4 9,613 7,812 33,706 No 44-10 318218 120636 A5 9,230 7,482 33,706 No 44-10 318218 120636 A6 10,041 7,482 33,706 No 44-10 318218 120636 A7 9,130 7,482 33,706 No 44-10 318218 120636 B1 8,767 7,263 33,706 No 44-10 357776 325246 B2 9,005 8,082 33,706 No 44-10 318218 120636 B3 9,938 7,263 33,706 No 44-10 357776 325246 B4 9,160 7,812 33,706 No 44-10 318218 120636 B5 10,039 7,482 33,706 No 44-10 318218 120636 B6 10,422 7,482 33,706 No 44-10 318218 120636 B7 9,762 7,482 33,706 No 44-10 357776 325246 B8 8,514 7,812 33,706 No 44-10 318218 120636 C1 8,514 7,263 33,706 No 44-10 357776 325246 C2 13,403 8,082 33,706 No 44-10 318218 120636 C3 8,747 7,263 33,706 No 44-10 357783 325261 C4 11,957 8,891 33,706 No 44-10 357776 325246 C4 16,975 7,812 33,706 No 44-10 357776 325246 C4 9,878 7,812 33,706 No 44-10 318218 120636 C5 10,934 7,482 33,706 No 44-10 162398 126195 C5QC 12,588 8,899 33,706 No 44-10 318218 120636 C6 12,495 7,482 33,706 No 44-10 318218 120636 C7 10,676 7,482 33,706 No 44-10 357776 325246 C8 8,914 7,812 33,706 No 44-10 318218 120636 C9 7,435 7,482 33,706 No 44-10 318218 120636 D1 9,244 7,263 33,706 No 44-10 357776 325246 D2 9,297 8,082 33,706 No 44-10 318218 120636 D3 9,148 7,263 33,706 No 44-10 357783 325261 D8 14,449 8,891 33,706 No 44-10 357776 325246 D8 10,462 7,812 33,706 No 36

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Scan Avg Action Detector Detector M2350-1 Logged Scan Location Background Level Type ID ID Result Alarms (cpm) (cpm) (cpm) 44-10 318218 120636 D9 7,695 7,482 33,706 No 44-10 318218 120636 E1 9,676 7,263 33,706 No 44-10 357776 325246 E2 9,570 8,082 33,706 No 44-10 318218 120636 E3 10,641 7,263 33,706 No 44-10 357776 325246 E8 11,516 7,812 33,706 No 44-10 318218 120636 E9 8,950 7,482 33,706 No 44-10 318218 120636 F8 13,054 7,482 33,706 No 44-10 318218 120636 F9 11,309 7,482 33,706 No 44-10 318218 120636 G8 13,320 7,482 33,706 No 44-10 318218 120636 G9 14,024 7,482 33,706 No 44-10 357776 325246 JSP10 7,297 7,889 33,706 No 44-10 357776 325246 JSP10 7,263 7,889 33,706 No 44-10 357776 325246 JSP2 13,088 7,889 33,706 No 44-10 357776 325246 JSP2 8,948 7,889 33,706 No 44-10 357776 325246 JSP3 8,209 7,889 33,706 No 44-10 357776 325246 JSP3 7,755 7,889 33,706 No 44-10 357776 325246 JSP4 8,217 7,889 33,706 No 44-10 357776 325246 JSP4 9,009 7,889 33,706 No 44-10 357776 325246 JSP5 6,870 7,889 33,706 No 44-10 357776 325246 JSP5 7,229 7,889 33,706 No 44-10 357776 325246 JSP6 9,185 7,889 33,706 No 44-10 357776 325246 JSP6 8,796 7,889 33,706 No 44-10 357776 325246 JSP7 12,527 7,889 33,706 No 44-10 357776 325246 JSP7 12,952 7,889 33,706 No 44-10 357776 325246 JSP8 8,715 7,889 33,706 No 44-10 357776 325246 JSP8 8,995 7,889 33,706 No 44-10 357776 325246 JSP9 8,131 7,889 33,706 No 44-10 357776 325246 JSP9 8,344 7,889 33,706 No 44-10 318218 120636 QC4 9,047 8,201 33,706 No 44-10 357776 325246 SP1 13,778 7,988 33,706 No 44-10 318218 120636 SP10 8,736 7,748 33,706 No 44-10 318218 120636 SP11 8,211 7,748 33,706 No 44-10 318218 120636 SP12 8,835 7,748 33,706 No 37

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS Scan Avg Action Detector Detector M2350-1 Logged Scan Location Background Level Type ID ID Result Alarms (cpm) (cpm) (cpm) 44-10 318218 120636 SP13 7,724 7,748 33,706 No 44-10 318218 120636 SP14 8,498 7,748 33,706 No 44-10 357776 325246 SP2 7,649 7,988 33,706 No 44-10 357776 325246 SP3 9,322 7,988 33,706 No 44-10 357776 325246 SP4 9,708 7,988 33,706 No 44-10 318218 120636 SP5 9,710 7,748 33,706 No 44-10 318218 120636 SP6 8,338 7,748 33,706 No 44-10 318218 120636 SP7 8,358 7,748 33,706 No 44-10 318218 120636 SP8 8,667 7,748 33,706 No 44-10 318218 120636 SP9 8,715 7,748 33,706 No

• Average Background established by taking the average of 5 1-minute static readings in each location.

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FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS ATTACHMENT 3 SIGN TEST 39

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSE SOLUTIONS Table 16-2 L1-SUB-TDS Sign Test SOF

1. 1-WS Sign (WS) 1 0.02500 0.98 +1 2 0.01916 0.98 +1 3 0.03103 0.97 +1 4 0.04269 0.96 +1 5 0.05516 0.94 +1 6 0.01523 0.98 +1 7 0.02631 0.97 +1 8 0.02611 0.97 +1 9 0.02863 0.97 +1 10 0.04630 0.95 +1 11 0.02030 0.98 +1 12 0.04300 0.96 +1 13 0.05146 0.95 +1 14 0.05323 0.95 +1 Number of positive differences 14 (S+)

Critical Value 10 the Acceptance Meets Survey Unit Criteria 40

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION ~

SURVEY UNIT L1-SUB-TDS LACROSSESOLUTIONS ATTACHMENT 4 QUALITY CONTROL ASSESSMENT 41

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION SURVEY UNIT L1-SUB-TDS Table 16-3 L1-SUB-TDS QC Assessment STANDARD COMPARISON Agreement Activity Standard Activity Standard Comparison Acceptable Sample ID Radionuclide Resolution Range (Low Sample ID Value Error Value Error Ratio (YIN) tn J:r;ohl Ll-SUB-IDS-FSGS-004-SB K-40 4.59E+00 5.66E-0l 8.11 0.6 1.66 LI-SUB-IDS-QSGS-004-SB 5.22E+00 6.27E-0l 1.14 y Ll-SUB-IDS-FJGS-008-SB Cs-137 6.16E-02 2.70E-02 2.28 0.4 2.5 Ll-SUB-IDS-FJGS-008-SB SPLIT 6.95E-02 2.93E-02 1.13 y Cs-137 l .61E-0l 3.15E-02 5.11 0.5 2 6.20E-02 2.88E-02 0.39 N Ll-SUB-IDS-FJGS-009-SB Ll-SUB-IDS-FJGS-009-SB SPLIT K-40 5.34E+00 6.21E-01 8.60 0.6 1.66 5.87E+00 6.79E-0l 1.10 y Comments/Corrective Actions: For Ll-SUB-IDS-FSGS-004-SB and Ll-SUB-IDS-QSGS-004- Table is provided to show acceptance criteria used to assess split samples.

SB, K-40 was substituted as the radionuclide for split assessment because Cs-13 7 was only Resolution Acceptab le R atio present in the comparison sample.

<4 0.4-2.5 The split assessment for Ll-SUB-IDS-FJGS-009-SB & Ll-SUB-IDS-FJGS-009-SB SPLIT 4- 7 0.5-2.0 resulted in a failure . Because the values are well below the operational DCGL, and the assessment 8-15 0 .6-1.66 passes using K-40, no further action is necessary.

16- 50 0 .7 5- 1.33 51-200 0 .80- 1.2 5

> 200 0 .85- 1.1 8 42

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SURVEY UNIT L1-SUB-TD LACROSSE SOLUTIONS ATTACHMENT 5 CONSULTATION TRIGGERS FOR RESIDENTIAL SOIL CONCENTRATION 43

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION ~

SURVEY UNIT L1-SUB-TD LACROSSESOLUTIONS Table H.1 Consultation Triggers for Residential and Commercial/Industrial Soil Contamination (MOU Table 1)

Except for radium-226, thorium-232, or total uranium, concentrations should be aggregated using a sum of the fraction approach to determine site-specific consultation trigger concentrations. This table is based on single contaminant concentrations for residential and commercial/industrial land use when using generally accepted exposure parameters. Table users should select the appropriate column based on the site's reasonably anticipated land use.

Radionuclide Residential Soil Concentration Industrial/Commercial Soil Concentration H-3 228 pCi/g 423 pCi/g C-14 46 oCi/g 123,000 oCi/g Na-22 9 pCi/g 14 pCi/g S-35 19,600 pCi/g 32 200,000 oCi/g Cl-36 6 oCi/g 10,700 oCi/g Ca-45 13,500 pCi/g 3 740,000 oCi/e:

Sc-46 105 pCi/2: 169 pCi/g Mn-54 69 oCi/e: 112 oCi/g Fe-55 269,000 pCi/g 2,210,000 oCi/g Co-57 873 pCi/g 1.420 oCi/e:

Co-60 4pCi/g 6 oCi/J!:

Ni-59 20,800 pCi/g 1,230 000 pCi/e:

Ni-63 9,480 oCi/e: 555.000 oCi/g Sr-90+0 23 pCi/g 1,070 oCi/g Nb-94 2 pCi/g 3 oCi/g Tc-99 25 oCi/g 89,400 oCi/g I-129 60 oCi/g 1,080 oCi/i:t Cs-134 16 pCi/g 26 pCi/g Cs-137+0 6 oCi/g 11 pCi/g Eu-152 4oCi/g 7 pCj/g Eu-154 5 oCi/g 8 pCi/g Ir-192 336 pCi/g 544 pCi/g Pb-2IO+D 15 oCi/g 123 oCi/g Ra-226 5 oCi/g 5 pCi/g Ac-227+D 10 pCi/g 21 oCi/e:

Th-228+0 15 oCi/g 25 pCj/g Th-232 5 pCi/g 5 pCi/g U-234 401 pCi/2 3,310 pCi/g U-235+0 20 oCi/e: 39 pCi/g U-238+0 74 pCi/g 179 oCi/g total uranium 47 mg/kg 1230 mg/ki:r Pu-238 297 oCi/g 1.640 oCi/2 Pu-239 259 pCi/g 1,430 pCi/g Pu-241 40,600 pCi/2 172,000 pCi/2 Am-241 187 oCi/g 568 oCi/e:

Cm-242 32.200 pCi/g 344,000 pCi/e:

Cm-243 35 pCi/g 67 pCi/g 44

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSE SOLUTIONS ATTACHMENT 6 GRAPHICAL PRESENTATIONS 45

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSE SOLUTIONS Figure 16 Quantile Plot for Cs-137 Concentration 2.50E-01

,,, ,., '*\

2.00E-01

• Concentration (pCi/g) 1.50E-01 I'

t t 1.00E-01

~

~

'\

5.00E-02

~

0.00E+00 0% 20% 40% 60% 80% 100%

Percentage 46

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSE SOLUTIONS Figure 16 Histogram for Cs-137 Concentration 10 9

8 7

Frequency 6

5 4

3 2

1 0

4.86E-02 8.32E-02 1.18E-01 1.53E-01 1.87E-01 2.22E-01 Upper End Value (pCi/g) 47

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSE SOLUTIONS Figure 16 Retrospective Power Curve for L1-SUB-TDS P.robabili'fy that the Survey U nit Passes, 1.0 0:8 0.6_

0.4 0.2 0.0 10% 3)% 50% - % 90% 1 JO% 110% 130% ,-

True Survey llnit Concentration (percent of DCGL 48

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

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SURVEY UNIT L1-SUB-TDS LACROSSE SOLUTIONS ATTACHMENT 7 SAMPLE ANALYTICAL REPORTS 49

1/15/2019 7:32:05AM Page I of6 Analysis Report for L 1-SUB-TDS-FSGS-001-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FSGS-001-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.039E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 1/5/2018 1:18:00PM Acquisition Started  : 1/8/2018 11:12:42AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.2 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5316 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:31:56AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:32:0SAM Page 2 of6 Analysis Report for L 1-SUB-TDS-FSGS-001-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 75.92 147 - 159 152 .39 2.50E+02 61. 67 1. 23E+03 3 . 92 F 2 185.86 369 - 376 372. 22 4. 79E+0l 27.29 4.74E+02 1. 30 F 3 23 8. 64 472 - 4 85 477.75 3.65E+0 2 48.60 6 . 57E+02 1. 48 F 4 295.32 585 - 595 591.09 1.09E+02 29.54 3 .0 0E+02 1. 43 F 5 338 . 39 671 - 681 677.22 5 . 53E+ 0l 25.01 3 .10E+02 1. 31 F 6 351.86 699 - 709 704.15 l .80E+02 32.61 2.12E+02 1. 56 F 7 583.07 1158 - 1175 1166.48 l.29E+ 02 25.5 9 l . 35E+02 1. 64 F 8 609 .13 1213 - 1226 1218 .6 0 l.40E+ 0 2 27 .34 l.20E+02 1. 88 F 9 727 . 15 144 9 - 1460 1454 .60 2 . 63E+ 0 l 14. 33 8.92E+ 0l 1. 99 F 10 910.65 1817 - 1829 1821.54 6 . 96E+0l 19.12 7 . 23E+0l 1. 31 F 11 968. 93 1933 - 1943 1938.08 3 . 05E+0l 1 5.24 7.53E+0l 1. 50 F 12 1460.44 2914 - 2931 2921.00 5 .94E+ 02 50 . 17 3.56E+0 l 2 . 32 M == First peak in a multiplet region m == Other peak in a multiplet region F == Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:31 :56AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 75.92 2 . 50E+02 61. 67 2.50E+02 6.17E+Ol F 2 185 .8 6 4.79E+0l 27.29 4 . 79E+0l 2 . 73E+0l F 3 238 . 6 4 3.65E+02 48.60 3.65E+02 4.86E+Ol F 4 295.32 l.09E+02 29 .54 1. 09E+02 2.95E+Ol F 5 338 . 39 5 . 53E+0l 25.01 5 . 53E+0l 2.50E+Ol F 6 351.86 l . 80E+02 32 . 61 8.36E+0l 3 . 72E+0l 9 . 69E+0l 4.95E+Ol F 7 583 .07 l.29E+02 25 . 59 l.29E+ 02 2.56E+Ol F 8 609 .13 l .4 0E+02 27 . 34 4.1 2E+0l 2 . 42E+0l 9 . 85E+0l 3.65E+Ol F 9 727 . 15 2.63E+0l 14 . 33 2.63E+0l 1. 4 3E+0 l F 10 910.65 6 . 96E+0l 19.12 6.96E+0l l . 91E+0 l F 11 968 . 93 3.0SE+0l 1 5.2 4 3 . 05E+0l 1. 52E+0l F 12 1460.44 5 . 94E+02 50 . 17 5 . 63E+0l l.71E+0l 5 . 37E+02 5.30E+0 l

1/ 15/2019 7:32:05AM Page 3 of6 Analysis Report for L 1-SUB-TDS-FSGS-001-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 98 1460.75

• 10.67 5 . 64 E+OO 6 . 38E- 01 BI - 212 0 . 60 727 .1 7

• 11. 80 1 . 3 4E-0 1 7 . 36E- 02 785.42 2 . 00 1 620 . 56 2 . 75 PB-212 0 . 56 77 . 11 17.50 2 38. 63

• 4 4 . 60 1 . 81E- Ol 2 . 59E - 02 BI - 21 4 0.34 60 9. 31

• 46.30 1. 09E- 01 4 . 09E - 02 1120 . 29 15.10 1238 . 11 5.94 1377 . 67 4 . 11 1 4 07 . 98 2 . 48 1509 . 19 2 .1 9 1764 . 49 15 . 80 PB-21 4 0. 72 77 .11 10 . 70 295 . 21

• 19 . 20 1. 50E- Ol 4.13E- 02 351. 92

• 37 . 20 8 . 06E - 02 4.13E - 02 RA- 226 0 . 98 186 . 21

• 3 . 28 2. 72E- 01 1.56E- 01 AC- 228 0 . 57 209 . 28 4 . 40 338 . 32

• 11. 40 1 . 45E - 01 6 . 59E- 02 794. 70 4 . 60 911. 60

• 27 . 70 1 . 86E - 01 5.16E- 02 96 4. 60 5 . 20 969 .11

• 1 6.60 1.43E- Ol 7 . 20E- 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/15/2019 7:32:0SAM Page 4 of6 Analysis Report for L1-SUB-TDS-FSGS-001-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K- 40 0.985 5.64E+00 6 . 38E - 01 BI - 212 0.605 l. 34E- 01 7 . 36E- 02 PB- 212 0 . 56 0 l.81 E-0l 2 . 59E - 02 BI - 214 0 . 347 l.09E-01 4 . 09E - 02 PB- 21 4 0 . 721 l. lSE- 01 2.92E - 02 RA- 226 0.980 2 . 72E- 01 l . 56E -01 AC - 228 0 . 576 1. 64E- 01 3 . 54E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/ 15/2019 7:32:0SAM Page 5 of6 Analysis Report for L 1-SUB-TDS-FSGS-001-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:31 :56AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (ke V) Peak Size (CPS) Uncertainty Type Nuclide F 1 75.92 6. 95197E-02 12 . 32 F 7 583.07 3 . 58303E- 02 9.92 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCi/grams)

{keV)

+ K- 40 1 4 60.75

• 10.67 5 . 64E+O0 4.97 E- 01 4 . 97E- 01

+ AR-41 1293.64 99.16 1 . 54E+10 1.86E+l0 1. 86E+l0

+ CO- 60 1173 . 22 100.00 3.18£- 02 4 . 75£- 02 5.llE- 02 1332.49 100.00 3.94£- 02 4.75£- 02

+ KR- 85 513.99 0 . 43 7.67E+00 8.22E+00 8 . 22E+0O

+ Y- 88 898 . 04 93.70 - 5 . 98£- 03 3.12£- 02 4 . 31£- 02 1836.06 99.20 2.51£-03 3 . 12£- 02

+ NB-94 702.63 100 . 00 2.17£-02 3.26£- 02 3 . 26E - 02 871 . 10 100.00 - 1 . 33£- 03 3.83E- 02

+ I - 131 284.30 6 . 06 2 . l0E-01 4.29E- 02 5 . 38£- 01 364.48 81. 20 2.51 E-03 4 . 29E-02 636 . 97 7 . 27 1.09£- 01 5.39£- 01

+ CS - 134 604 . 70 97. 60 -1.35E- 02 3 . 87E- 02 4 . 20E- 02 795.84 85.40 - 7 . 39E- 02 3.87E- 02

+ CS -1 37 661 . 65 85.12 4 . 28 E-02 4.52E - 02 4.52E- 02

+ CE-144 80.12 1. 36 - 8 . 94E- 0l 2.28£- 01 2 . 84E+OO

1/15/2019 7:32:0SAM Page 6 of 6 Analysis Report for L 1-SUB-TDS-FSGS-001 -SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCilgrams) (pCilgrams) (pCilgrams)

{keV)

CE- 14 4 133 . 51 1 1. 09 3.53E- 02 2.28E-01 2 . 28E-01

+ EU-152 121.78 28 . 40 -6 . 25E-03 8 . 79E-02 8 . 79E- 02 3 4 4 . 28 26 . 60 - 8 . 58E-02 1. llE- 01 1408.00 20 . 74 4 . 47E- 02 1.70E- 01

+ EU-154 123 . 07 40.40 - 2 .19E-02 6 . 15E-02 6.15E-02 723 . 30 19 . 70 5 . 03E-02 1. 80E-01 1274.51 35 . 50 5.51E- 02 1.28E- 01

+ EU-155 86.54 32 . 80 - 7.38 E- 02 9 . 71E- 02 9 . 71E-02 1 05 . 31 21. 80 - 4 . 71E- 02 1 . 20E-01

+ BI - 214 609.31

• 46.30 1.09E-01 7 . 15E- 02 7 . 15E-02 1120 . 29 15.10 3 . lO E-01 3.35E- 01 1238 . 11 5 . 94 2 . 94 E- 01 9.46E- 01 1377 . 67 4 . 11 -1 . 60 E-01 8 .13E-01 1407 . 98 2 . 48 3.7 4E- 01 l . 42E+OO 1509 . 19 2 . 19 4 . 95E- 01 l.36E+OO 1764 . 49 15 . 80 2.22E-01 2.57E-01

+ PB-214 77 .11 10 . 70 4.19E- 01 7 . 37E-02 3 . 83E-01 295 . 21

• 19.20 1. 50E-01 8.94E-02 351. 92

• 37.20 8.06E-02 7.37E-02

+ PA- 228 89 . 95 22.00 l.78E+OO 7.55E- 01 1. 30E+OO 93 . 35 35 . 00 1. 4 7E-01 7.55E-01 105.00 16 . 30 -6.86E - 02 1.47E+OO 129 . 22 2.97 2 . 39E+OO 7.87E+OO 338.32 5.30 4.60E+OO 5 . 08E+OO 463 . 00 13 . 80 4.16E - 01 2.02E+00 911.23 16 . 70 3 . 89E+OO 2 . 67E+OO

+ AM-241 59.54 36.30 4 . 63E-02 1.79E- 01 l. 7 9E- 01

+ CM-243 103.76 23.00 - 3 . 88E - 02 1 . 13E-01 l.13E-01 228 . 18 10 . 60 - 2 . 82E-02 2 . 33E- 01 277. 60 14.00 -1 . 87E-02 1 . 89E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDAat 95% confidence level

1/15/2019 7:33:49AM Page I of7 Jt'Apex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-002-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FSGS-002-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.960E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/5/2018 1:23:00PM Acquisition Started  : 1/8/2018 12:17:03PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.8 seconds Dead Time  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 -4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5317 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:33:40AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:33:49AM Page 2 of7 Analysis Report for L 1-SUB-TDS-FSGS-002-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 .4 6 147 - 161 153 .4 6 2.51E+02 61. 53 1 . 30E+03 3.48 F 2 238 . 48 472 - 481 477.44 2.38E+02 42.78 5.71E+02 1. 20 F 3 295.12 587 - 594 590 . 69 1. 21E+02 29 .53 2.12E+02 1. 36 F 4 337 . 77 6 67 - 681 675.96 7.32E+Ol 27 . 22 2.85E+02 2.15 F 5 351.8 6 695 - 708 704.14 2 .3 4E+02 35.43 2 . 81E+02 1. 44 F 6 583 . 13 1161 - 1175 1166.61 7.06E+Ol 21 . 76 1.46E+02 1. 68 F 7 609.19 1211 - 1225 1218.71 1.82E+02 30.70 1. 50E+02 1. 80 F 8 910 . 60 1815 - 1826 1821.44 6.32E+Ol 20 .4 7 7 .7 6E+Ol 2.12 F 9 968 . 65 1 93 3 - 1944 1937.52 4. 52E+Ol 17.45 8.78E+Ol 1. 43 F 10 1120.26 2236 - 2246 2240 . 70 3 .49E+Ol 15 . 75 5.31E+Ol 2.18 F 11 1407.69 2811 - 2820 2815.51 1 . 18E+Ol 7 .1 3 1. 26E+Ol 1. 20 F 12 1460 . 51 2914 - 2928 2921.14 5.37E+02 47.49 3.71E+Ol 2.40 F 13 1763 . 58 3521 - 3533 3527 . 23 2 .6 3E+Ol 11. 31 6 . 50E+OO 2 .2 8 M ::: First peak in a multiplet region m ::: Other peak in a multiplet region F ::: Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:33:40AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.46 2 . 5 1E+02 61. 53 2 . 51E+02 6.15E+ Ol F 2 238.48 2.38E+ 02 42.78 2.38E+02 4. 2 8E+Ol F 3 295.12 1 . 21E+02 29.53 1. 21E+02 2.95E+Ol F 4 337 . 77 7 . 32E+Ol 27 . 22 7.32E+Ol 2. 72E+ Ol F 5 351.86 2 . 34E+02 35.43 8.36E+Ol 3 . 72E+Ol 1 . 50E+02 5 . 14E+Ol F 6 583 . 13 7.06E+Ol 21.76 7.06E+O l 2.18E+Ol F 7 609.19 1.82E+02 30.70 4. 12E+Ol 2 . 42E+Ol 1.41E+02 3 .91E+Ol F 8 910.60 6.32E+Ol 20.47 6 . 32E+O l 2 . 05E+Ol F 9 968 . 65 4.52E+Ol 17.45 4 . 52E+Ol 1.75E+O l F 10 1120.26 3.49E+Ol 15.75 3.49E+Ol 1. 58E+O l F 11 1407 . 69 l . 18E+Ol 7 . 13 1.18E+Ol 7. 13E+ OO F 12 1460.51 5.37E+02 47.49 5 . 63E+Ol 1. 71E+Ol 4 . 81E+02 5.05E+Ol F 13 1763 . 58 2.63E+Ol 11. 31 2 . 63E+Ol 1.13E+Ol

1/15/2019 7:33:49AM Page 3 of7 Analysis Report for L 1-SUB-TDS-FSGS-002-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-4 0 0 . 99 1460 . 75

• 10 . 67 5.26E+OO 6 . 25E- 01 PB- 212 0.97 77 .11

• 17 . 50 3.61E-01 9.13E- 02 238 . 63

• 44 . 60 1 .23E- 01 2.30E- 02 BI - 214 0 . 79 609.31

• 4 6 . 30 l . 63E-01 4 .61E- 02 1120.29

• 1 5 . 10 2 . 1 4E- 0 1 9 . 72E-02 1238 . 11 5 . 94 1377. 67 4 .11 1407.98

• 2 . 48 5 . 36E-01 3 . 26E - 01 1509 . 19 2 . 19 1764 . 49

• 15 . 80 2 . 27E-01 9 . 89E - 02 PB- 21 4 0 . 98 77 .11

• 10 . 70 5.90E- 01 l. 49E- Ol 295.21

• 1 9. 20 l. 74 E- 01 4.33E- 02 351. 92

• 37 . 20 l . 30E- Ol 4 . 50E- 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

1/15/2019 7:33:49AM Page 4 of 7 Analysis Report for L 1-SUB-TDS-FSGS-002-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pC/lgrams)

K- 40 0.991 5 . 26E+00 6.25E-01 PB- 212 0 . 979 1 . 31E- 01 2.2 4E-02 BI - 21 4 0. 7 99 1 . 86E-01 3 . 81E- 02 PB-21 4 0.988 l . 63E-01 3 . 06E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:33:49AM Page 5 of7 Analysis Report for L1-SUB-TDS-FSGS-002-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:33:40AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 337 . 77 2 . 03296E- 02 1 8 . 60 Tol. AC- 228 PA- 228 F 6 5 83. 1 3 l . 9614 8E-0 2 15. 41 F 8 9 1 0 . 60 l . 75502E- 02 1 6 . 20 Tol. PA- 228 F 9 968 . 65 l . 256 3 9E- 02 19 . 30 Tol. AC- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

+ K-40 1 4 60.75

• 10 . 67 5 . 26E+00 5 . 16E- 01 5.16E - 01

+ AR- 41 1293 . 64 99 . 16 -l . 23E+l0 2.34E+l0 2 . 3 4E+l0

+ CO-60 1173.22 100.00 - l . 79E- 02 4. 70E- 02 5.52E- 02 1332. 4 9 100 . 00 3.73E- 02 4 . 70E- 02

+ KR- 85 513.99 0 . 43 7 . 50E+00 8.62E+00 8 . 62E+00

+ Y- 88 898 . 0 4 93.70 - 2.04E- 03 3 . 0lE- 02 4 . 28E - 02 1836.06 99.20 - l.64E - 02 3.0lE- 02

+ NB- 94 702 . 63 100.00 l . 72E- 02 3 . 40E- 02 3 . 40E-02 871 .1 0 100 . 00 - 3 . S0E - 02 3 . 58E- 02

+ I-131 28 4. 30 6 . 06 3 . 47E - 01 4.5 4E- 02 5 . 94E- 01 364 . 48 81. 20 5 . 20E-03 4 . 54E - 02

1/15/2019 7:33:49AM Page 6 of7 Analysis Report for L1-SUB-TDS-FSGS-002-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCilgrams)

(keV)

I-131 636.97 7 . 27 -3.59E-01 4. 54E-02 5 . 67E- 01

+ CS - 134 604.70 97.60 8 . 97E-03 4.49E-02 4.87E-02 795 . 84 85 . 40 - 1.75E- 02 4.49E-02

+ CS-137 661.65 85.12 1. 88E-02 4 .36E-02 4.36E-02

+ CE-144 80 .1 2 1. 36 - 4 . 71E- 01 2 . 29E-0 1 2.89E+00 1 33.51 11.09 -9.21E-02 2 . 29E-01

+ EU-152 121. 78 28 .4 0 -8.75E-03 8.93E-02 8.93E-02 344.28 26 . 60 -2.78E-02 1.14E-01 1408.00 20.74 4. 72E-02 1.83E- 01

+ EU-154 123.07 40.40 -2.21E-03 6.32E-02 6.32E-02 723.30 19.70 -9.52E-02 1 . 74E- 01 1274.51 35 . 50 2.20E-02 1.44E-01

+ EU-155 86 . 54 32.80 -1.19E-01 9 . 82E-02 9.82E-02 105.31 21. 80 4.15E-02 1. 25E-01

+ BI -214 609.31

• 4 6 . 30 1. 63E-01 7 . 95E-02 7.95E-02 1120.29

• 15.10 2.14E-01 1 . 79E- 01 1238 .11 5.94 4.32E-01 9 . 18E-01 1377. 67 4 .11 -3. 4 8E-01 7.73E-01 1407.98

• 2 .4 8 5 . 36E-01 7.08E-01 1509.19 2.19 -1.30E+00 1.37E+00 1764.49

• 15.80 2.27E-01 1.07E-01

+ PB-214 77 . 11

• 10.70 5 . 90E-01 7.28E-02 3 .4 0E- 01 295.21

• 19.20 1.74E- 01 7 . 28E-0 2 351. 92

• 37.20 1.30E-01 8 . 43E-02

+ PA- 228 89.95 22.00 1.34E+00 8. llE-01 1 . 36E+OO 93 .35 35.00 7 . 12E-01 8. llE-01 105 .0 0 16.30 3 . 78E-01 1.58E+O0 129 . 22 2 . 97 1.l0E+00 8 . 19E+00 338 . 32 5 . 30 2.75E - 0l 5. llE+O0 463.00 13.80 -4.63E-01 2 . 08E+00 911.23 16.70 2 . 68E+0O 2 . 85E+OO

+ AM-241 59.54 36.30 -7.68E-02 1 . 82E-01 1.82E-01

+ CM- 243 103.76 23.00 5.37E-02 1.20E-01 1. 20E-Ol 228.18 10.60 1.44E-01 2.45E- 01 277.60 14.00 3.72E-02 1.99E- 01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 7:33:49AM Page 7 of7 Analysis Report for L 1-SUB-TDS-FSGS-002-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

1/15/2019 7:34:35AM Pagel of6

_.Apex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-003-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FSGS-003-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.555E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/5/2018 10:40:00AM Acquisition Started  : 1/8/2018 1:18:34PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.5 seconds Dead Time  : 0.29 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100- 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5318 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:34:27AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:34:35AM Page 2 of6 Analysis Report for L 1-SUB-TDS-FSGS-003-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 . 90 147 - 161 154.34 l.08E+02 36. 72 l . 34E+03 0.98 F 2 185.84 368 - 379 372 .18 5 . 35E+0l 3 1. 47 7.37E+02 1. 20 F 3 238 . 48 471 - 485 477 .4 3 2 . 65E+ 02 43 . 25 7.31E+02 1. 40 F 4 294.99 585 - 595 590.44 7.89E+0l 27 . 24 3.63E+02 1. 20 F 5 337. 96 671 - 680 676.35 6 . 27E+ 0 1 24.75 2 . 18E+02 1. 51 F 6 351. 87 69 9 - 708 704 . 17 l . 85E+02 32 .13 l.89E+02 1. 39 F 7 582.97 1162 - 1172 1166 . 29 8 . 06E+0l 21. 51 7 . 96E+0l 1. 65 F 8 609 . 09 1214 - 1227 1218.52 l . 44E+02 27 . 27 1.11E+02 1. 75 F 9 661 . 41 1316 - 1331 1323.13 1 . 71E+ 0 2 29 . 15 1 . 31E+02 1. 73 F 10 727 . 76 1451 - 1459 1455 . 81 1 . 82E+0l 1 2.76 6.91E+0l 1.13 F 11 910 . 96 1816 - 1829 1822. 1 7 6 . 27E+ 0 l 1 9.66 7.96E+0l 2. 1 4 F 12 968 . 41 1933 - 1943 1937 . 05 2.26E+0l 11. 7 5 6. 72E+0l 0. 72 F 13 1120 . 16 2235 - 2246 2240.51 3 . 41 E+0l 1 5.48 6.51E+0l 1. 68 F 14 1332 . 06 2659 - 2669 2664.26 2.18E+ 0 l 11. 64 3 . 42E+0l 1.34 F 15 1 460.34 2914 - 2928 2920 . 80 5 . 20E+ 0 2 47 . 45 3.82E+0l 2 . 38 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:34:27AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001 364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76 . 90 1.08E+02 36 . 72 l.08E+02 3 . 67E+0l F 2 185.84 5.35E+0l 31. 47 5 . 35E+0l 3.15E+Ol F 3 238.48 2.65E+02 43 . 25 2 . 65E+02 4.32E+0l F 4 29 4 .99 7.89E+0l 27.24 7 . 89E+0l 2 . 72£+01 F 5 337.96 6.27E+0l 24.75 6.27E+0l 2.48E+0l F 6 351 . 87 l.85E+02 32 . 13 8.36E+Ol 3. 72E+0l l . 02E+02 4 . 92E+0l F 7 582.97 8 . 06E+0l 21. 51 8.06E+0l 2.15E+0l F 8 609 . 09 1 . 44E+02 27 . 27 4.12E+0l 2 . 42E+0l 1. 03£+02 3 . 65E+0l F 9 661.41 1.71E+02 29 . 15 6.61E+0l 2 . 54E+0l 1. 04E+02 3.87E+0l F 10 727. 76 1 . 82E+0l 12.76 1 . 82E+01 1.28E+0l F 11 91 0 . 96 6.27E+0l 19.66 6.27£+01 1.97 £+01 F 12 968.41 2.26E+0l 11. 75 2 . 26E+0l 1.18E+0l F 13 1120.16 3.41E+0l 15.48 3.41£+01 1.55E+0l F 14 1332 . 06 2 . 18E+0l 11 . 64 2.18E+0l 1.16E+0l

1/15/2019 7:34:35AM Page 3 of6 Analysis Report for L1-SUB-TDS-FSGS-003-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 15 1460 . 34 5 . 20E+02 47. 4 5 5.63E+Ol 1 . 71E+Ol 4.6 4E+02 5 . 04E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0.97 1460.75

• 10 . 67 5.29E+OO 6 . 46E-0 1 CS- 137 0.99 661 . 65

• 85.12 7 . 39E- 02 2 . 76E - 02 BI - 212 0.56 727 . 17

• 11. 80 1.0lE- 01 7 . llE - 02 785. 42 2 . 00 1620 . 56 2.75 PB- 212 0.99 77 . 11

• 17 . 50 1 . 59E- 01 5.53E- 02 238.63

• 44 . 60 1. 43E - Ol 2.45E- 02 BI - 214 0.58 609.31

• 46 . 30 1.2 4E- 01 4 . 45E-02 1120 . 29

• 15 . 10 2.18E- 01 9 . 95E - 02 1238 .11 5 . 94 1377 . 67 4 .11 1407 . 98 2 . 48 1509.19 2.19 176 4.4 9 15.80 PB- 214 0.99 77 .11

• 10.70 2 . 61E - 01 9.0SE- 02 295 . 21

• 19.20 1. l BE - 01 4.12E- 02 351 . 92

• 37.20 9 . 19E- 02 4 . 47E- 02 RA- 226 0.97 186 . 21

• 3 . 28 3 . 30E- Ol 1. 95E- 01 AC- 228 0.58 209 . 28 4 . 40 338.32

• 11. 40 l . 78E- 01 7 . 09E- 02 794 . 70 4.60 911. 60

• 27 . 70 1.82E- 01 5 . 76E-02 964 . 60 5 . 20 969 . 11

• 16. 60 1.16E- 01 6 . 03E- 02

1/15/2019 7:34:35AM Page 4 of6 Analysis Report for L 1-SUB-TDS-FSGS-003-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-4 0 0.974 5.29E+O0 6.46E-01 CS-137 0 . 991 7.39E- 02 2.76E-0 2 BI-212 0.566 1.0lE- 01 7 . llE- 02 PB- 212 0.996 1 . 36E-01 2.26E-0 2 BI-2 14 0.581 1. 40E-01 4.06E-02 PB- 214 0 . 996 9.93E-02 2.89E-02 RA-226 0.978 3 . 30E- 01 1. 95E-01 AC- 228 0 . 586 1.58E- 01 3 . 59E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:34:35AM Page 5 of6 Analysis Report for L 1-SUB-TDS-FSGS-003-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:34:27AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 7 582.97 2 . 23890E-02 13 . 34 F 14 1332 . 06 6 . 05301E - 03 26.70 Tol. CO - 60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{3/4) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 5 . 29E+00 5 . 42E- 01 5 . 42E - 01

+ AR-41 1293 . 64 99.16 l . 25E+l0 l . 12E+ll l . 12E+ll

+ CO- 60 1173.22 100.00 l . 37E- 02 5.02E- 02 5.49E-02 1332.49 100.00 4.78E- 02 5 . 02E-02

+ KR-85 513 . 99 0 . 43 6 . 05E+00 8 . 27E+00 8 . 27E+O0

+ Y- 88 898.04 93 . 70 3 . 60E- 03 3 . 48E-02 4 . 58E-02 1836.06 99 . 20 6 . 83E - 03 3.48E- 02

+ NB-94 702 . 63 100 . 00 - 1 . 38E-02 3 . 45E- 02 3.45E- 02 871.10 100.00 - 3 . 00E - 02 3.84E-02

+ I - 131 284.30 6.06 1 . 95E-01 4.70£- 02 6.06E- 01 364 . 48 81.20 3.78E-02 4 . 70E- 02 636 . 97 7.27 - l.79E- 01 5 . 88E- 01

+ CS - 134 604 . 70 97 . 60 -6 . 38£-02 4.51E- 02 4 . 51E- 02 795 . 84 85 . 40 3.15E- 02 4.57E- 02

+ CS-137 661. 65

• 85 . 12 7 . 39E-02 4 . 98E- 02 4.98E-02

+ CE-144 80.12 1. 36 - 1. 32E+00 2. 4 3£ - 01 2.94E+00

1/15/2019 7 :34:35AM Page 6 of6 Analysis Report for L1-SUB-TDS-FSGS-003-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams)

(keV)

CE-144 133.51 11.09 1. 95E- 01 2.43E-01 2.43E-01

+ EU- 152 121. 78 28 . 40 -3 . 05E-02 9.28E-02 9 . 28E- 02 344 . 28 26 . 60 -8 . 84E-02 l.18E-01 1 408 . 00 20.74 l .14E-01 l . 91E-01

+ EU- 154 123 . 07 40.40 - 4 . 14E-02 6.53E-02 6.53E-02 723. 30 1 9.70 4.29E-02 l . 87E-01 127 4 .51 35.50 7.00E- 03 1. 44E- 01

+ EU-155 86.54 32 . 80 - 4.50E-02 l.06E-01 l.06E-01 105 . 31 21. 80 -5. 72E - 02 l.22E-01

+ BI-21 4 609.31

• 4 6.30 l . 2 4E- 01 7 . 68E - 02 7 . 68E- 02 1120 . 29

• 15 .1 0 2.18E-01 2.07E- 01 1238 .11 5 . 94 4.45E-01 l.08E+0O 1377. 67 4 . 11 - 3 . 28E-01 9.35E-01 1407.98 2.48 9.50E- 01 l.60E+00 1509 . 19 2.19 - 3.64E- 01 l.59E+00 1764.49 15.80 2.71E-02 2 . 87E- 01

+ PB-214 77 .11

• 10 . 70 2.61E-01 7.79E- 02 3.57E-01 295.21

• 19 . 20 l.18E-01 l.06E- 01 351.92

• 37 . 20 9.19E-02 7.79E- 02

+ PA- 228 89 . 95 22 . 00 2 . 53E+00 9.3 4E-0l 1. 64E+00 93.35 35 . 00 7.38E- 02 9.34E-01 105.00 16 . 30 -2.39E- 01 l.75E+00 129 . 22 2.97 -l . 31E+00 9 . 54E+00 338 . 32 5.30 l.29E+00 6 . 07E+00 463 . 00 13 .80 l.08E+00 2 . 59E+O0 911 . 23 16.70 l . 06E+00 3.22E+00

+ AM-241 59.54 36.30 -7.87E-02 l . 89E- 01 l.89E-01

+ CM- 243 103 . 76 23.00 l.89E - 02 l.16E- 01 l. 1 6E-01 228 . 18 10 . 60 5 . 66E-02 2 . 57E- 01 277 . 60 1 4 .00 7 . 34E - 03 2.03E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence lev el

1/15/2019 7:35:21AM Page I of7

..t,Apex-Gamma Analysis Report for l 1-SUB-TDS-FSGS-004-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TOS-FSGS-004-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.038E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 1/5/2018 10:10:17AM Acquisition Started  : 1/8/2018 2:25:24PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.7 seconds Dead Time  : 0.30 %

Peak Locate Threshold  : 3.00 Peak locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5319 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:35:12AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:35:21AM Page 2 of7 Analysis Report for L 1-SUB-TDS-FSGS-004-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 .4 6 147 - 161 153.46 2.02E+02 62 . 75 l . 53E+03 3 . 08 F 2 185.76 368 - 377 372. 03 8 . 38E+0l 35 .50 6.03E+02 1. 46 M 3 238.52 472 - 492 4 77 .51 3.45E+02 46 .18 4.62E+02 1. 65 m 4 241.76 472 - 492 4 84.00 l.02E+02 29.81 3 . 90E+02 1. 65 F 5 294.95 583 - 596 590.35 l.44E+02 33 .6 1 4.29E+02 1. 59 F 6 338.39 674 - 682 677.20 4.85E+0 l 23 . 25 2 .13E+02 1. 45 F 7 351.74 698 - 712 703.90 2.00E+02 35.06 3.36E+02 1. 70 F 8 582.98 1160 - 1175 1166.30 8 .48E+0 l 22.65 1. 37E+02 1. 78 F 9 608.99 1211 - 1225 1218 .31 l .56E+02 28 .46 1. 4 2E+02 1. 65 F 10 742.56 1481 - 1489 1485 . 41 l.68E+0l 12 . 75 5.64E+0l 1. 37 F 11 911.07 1817 - 1827 1822.38 6.49E+0l 19.41 7.61E+0l 1. 52 F 12 1119.97 2236 - 2245 2240.13 2.02E+0l 13.94 7.42E+0l 1. 41 F 13 1460.28 29 12 - 2928 2920 . 67 4.93E+02 44.97 2 .13E+0l 2 . 46 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:35:12AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76 .4 6 2.02E+02 62 . 75 2 . 02E+02 6.28E+0l F 2 185 . 76 8.38E+0l 35.50 8.38E+Ol 3.55E+0l M 3 238.52 3.45E+02 46.18 3 .4 5E+02 4 . 62E+Ol m 4 241.76 1 . 02E+02 29 . 81 l . 02E+02 2 . 98E+0l F 5 294 . 95 1.4 4E+02 33 . 61 1.44E+02 3 . 36E+0l F 6 338.39 4.85E+0l 23 . 25 4.8 5E+0 l 2.33E+0l F 7 351.74 2.00E+02 35 .06 8 . 36E+0l 3 . 72E+0l 1 . 16E+02 5. llE+0l F 8 582.98 8.48E+0l 22.65 8.48E+0l 2.27E+ 0l F 9 608.99 1. 56E+02 28 .4 6 4. 12E+0l 2 . 42E+0l l.15E+02 3.74E+0l F 10 7 42 .56 l.68E+0l 12 . 75 l.68E+0l l . 27E+ 0l F 11 911.07 6.49E+0l 19.41 6.49E+0l l.94E+0l F 12 1119 . 97 2.02E+0l 13 . 94 2.02E+0l 1.39E+0l F 13 1460.28 4.93E+02 44. 97 5.63E+0l 1. 71E+0l 4 . 37E+02 4 . 81E+0l

1/15/2019 7:35:21AM Page 3 of7 Analysis Report for L 1-SUB-TDS-FSGS-004-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0.96 1 460 . 75

• 10.67 4.59E+00 5.66E-01 PB- 212 0.98 77 . 11

• 17.50 2.79E - 01 8 . 82E- 02 238.63

• 44 . 60 1 . 71E - 01 2 . 46E- 02 BI - 214 0 . 57 609.31

• 46 . 30 l . 27E - 01 4.2 1E- 02 1120 . 29

• 15.10 l.19E - 01 8.23E- 02 1238 . 11 5.94 1377 . 67 4 . 11 1407 . 98 2.48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB- 214 0.98 77 . 11

• 10 . 70 4 . 56E- 01 l . 44E- 01 295 . 21

• 19.20 l.99E- 0l 4.73E- 02 351.92

• 37.20 9 . 68E- 02 4.28E- 02 RA- 226 0 . 96 186.21

• 3.28 4.76E- 01 2.03E-01

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

1/15/2019 7:35:21AM Page4 of7 Analysis Report for L1-SUB-TDS-FSGS-004-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.965 4.59E+00 5.66E-01 PB-212 0.980 1.73E-01 2.37E-02 BI-214 0.574 1.26E-01 3.75E-02 PB-214 0.983 1.44E-01 3. llE-02 RA-226 0.969 4.76E-01 2.03E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:35:21AM Page 5 of7 Analysis Report for L 1-SUB-TDS-FSGS-004-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7: 35:1 2AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(3/4) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 4 241 . 76 2 . 82116E- 02 14.68 F 6 338.39 1.34679E- 02 23.98 Tol. AC- 228 PA- 228 F 8 582.98 2 . 35672E- 02 13 . 35 F 10 742 . 56 4.67071E- 03 37.90 F 11 911. 07 1 .80271E- 02 14.95 Tol. AC-228 PA- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ K- 40 1460.75

• 10.67 4.59E+OO 4 . 70E-01 4 . 70E- 01

+ AR-41 1293 . 64 99.16 - 1.34E+10 1 . 93E+l l 1 . 93E+ll

+ C0-60 1173.22 100 . 00 3.58E-02 4.46E-02 5.45E - 02 1332. 49 100.00 4.69E-02 4 . 46E - 02

+ KR- 85 513. 99 0 . 43 9.33E+OO 7.89E+OO 7.89E+OO

+ Y-88 898.04 93 . 70 - 4 . 83E - 03 2.43E-02 4 . 15E-02

1/15/2019 7:35:21AM Page 6 of7 Analysis Report for L 1-SUB-TDS-FSGS-004-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

Y-88 1836 . 06 99.20 - 1. 47E-02 2. 4 3E-02 2.43E-02

+ NB-94 702 . 63 100 .0 0 - 4.33E- 03 3.05E- 02 3.05E- 02 871 . 10 100 . 00 -5 . 76E-02 3 . 48E- 02

+ I-131 284.30 6. 0 6 -1.39E-01 4.23E- 02 5.66E- 01 364. 4 8 81.20 -1 . 45E-02 4 . 23E-02 636.97 7 . 27 - 2.l0E- 01 5 . 43E-01

+ CS -1 34 604. 70 97 . 60 - 3.22E- 03 4.18E- 02 4. 30E- 02 795.84 85.40 - 2.90E- 02 4.18E- 02

+ CS - 137 661. 65 85 . 12 5 . 89E-02 5 . 00E- 02 5.00E- 02

+ CE - 14 4 80 . 12 1. 36 - 1 . 25E+00 2 . 29E-0l 2 . 85E+00 133 . 51 11.09 - 8 . 45E- 02 2 . 29E- 01

+ EU-152 121.78 28 .4 0 - 6.60E- 02 8 . 86E-02 8.86E- 02 3 44 .28 26 . 60 -3.07E-02 l.09E-01 14 08.00 20.7 4 l. 1 8E- 01 l.98E- 01

+ EU-154 123.07 4 0. 4 0 -1 . 38E-02 6 . 26E- 02 6 . 26E- 02 723.30 19 . 70 1 . 04E- 01 1.71E- 01 1 274.51 35.50 - 2 . 67E-02 1. 30E-0 1

+ EU-1 55 86.54 32.80 -8.40E- 02 9.78E-02 9. 78E - 02 105 . 31 2 1. 80 -1.1 4E-02 1.17E-01

+ BI - 214 609 . 31

• 46 . 30 1.27E- 01 7 . 59E- 02 7.59E - 02 1120.29

• 15.10 l .1 9E- 01 1. 94E- 01 1 238 .11 5.94 - l.37E- 0 1 9 . 18E-01 1 377 . 67 4 .11 3.05E- 01 8 . 88E- 01 1 4 07.98 2. 4 8 9.86E-0 1 1.66E+00 1 509.19 2 . 19 8 .05E- 0 1 1. 59E+00 1 764 . 49 15 . 80 2 . 73E- 01 2.87E- 01

+ PB-214 77 .11

• 10 .7 0 4 . 56E- 0 1 8.52E- 02 3 . 55E- 01 295.21

• 19.20 l.99E- 01 1 .1 4E- 0 1 351.92

• 37.20 9 . 68E-02 8.52E- 02

+ PA- 228 89 . 95 22 . 00 l.97E+00 9.45E-01 1.60E+00 93 . 35 35.00 - 1 . 08E- 01 9 . 45E-01 105 . 00 16.30 - 1 . 91E- 01 1 . 76E+00 129.22 2 . 97 4.61 E+00 9 . 60E+00 338 . 32 5.30 4.83E+00 5 . 83E+00 463.00 13 . 80 4. l 0E- 01 2.41E+00 9 1 1.23 16.70 3.35E+00 3.l0E+00

+ AM-241 59 . 54 36 . 30 2.32E- 02 1. 80E-01 1. 80E-01

+ CM-243 103 . 76 23 . 00 1.73E-02 l . 12E- 01 1. 1 2E- 01 228.18 10.60 7 . 23E-02 2 . 29E-0l 277 . 60 14 . 00 - 3.88E- 02 l.94E- 01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 7:35:21AM Page 7 of7 Analysis Report for L1-SUB-TDS-FSGS-004-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

1/15/2019 7:36:06AM Page I of6 JIApex-Gamma Analysis Report for L 1-SUB-TDS-QSGS-004-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-QSGS-004-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.806E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/5/2018 10:13:00AM Acquisition Started  : 1/8/2018 3:26:44PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Ttme  : 3610.8 seconds Dead Time  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100- 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5320 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:35:57AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:36:06AM Page 2 of6 Analysis Report for L 1-SUB-TDS-QSGS-004-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 185.86 369 - 379 372 . 21 6.67E+0 l 30 . 85 5 . 99E+02 1.18 F 2 238.52 472 - 485 477. 52 3.32E+02 46.67 6.38E+02 1. 53 F 3 295.05 584 - 595 590.54 1. 14E+02 31. 37 3.21E+02 1. 80 F 4 338.36 671- 680 677.15 3.30E+0l 19 . 10 2.48E+02 0 . 91 F 5 351. 84 698 - 712 704 .11 1.98E+02 34 . 39 3.30E+02 1. 58 m 6 520.57 1015 - 1045 1041.51 2 . 27E+0l 15.09 1.02E+02 1. 52 F 7 582.91 1161 - 1170 1166 . 16 8.68E+0l 23.90 1. 02E+02 1. 91 F 8 609 . 16 1213 - 1226 1218 . 66 l.67E+02 28 . 06 8 .0 2E+0l 1. 71 F 9 661.36 1318 - 1329 1323 .0 4 l . 30E+02 25.66 9.23E+0l 1. 5 4 F 10 911.24 1818 - 1828 1822 . 72 5.57E+0l 19.77 9.90E+0l 1. 64 F 11 1460. 40 2913 - 2931 2920 .92 5 . 26E+02 47.02 2.93E+0l 2.51 F 12 1764 .0 6 3522 - 3535 3528 .1 8 3.96E+0l 13.57 l. 31E+0l 2 . 24 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:35:57AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 185.86 6 . 67E+0l 30.85 6 . 67E+0l 3.09E+0l F 2 238 . 52 3.32E+02 46.67 3.32E+02 4.67E+0l F 3 295 .05 1.14E+02 31. 37 1.14E+02 3.14E+0l F 4 338.36 3.30E+0l 1 9.10 3.30E+0l 1.91E+0l F 5 351.84 1 . 98E+02 34.39 8 . 36E+0l 3. 72E+0l 1. 14E+02 5 . 07E+0l m 6 520.57 2 . 27E+0l 15.09 2.27E+0l 1 .51E+0l F 7 582 . 91 8 . 68E+0l 23 . 90 8.68E+0l 2.39E+0l F 8 609 . 16 1.67E+02 28 . 06 4.12E+0l 2 . 42E+0l 1. 26E+02 3. 71E+0l F 9 661.36 1.30E+02 25 . 66 6.61E+0l 2 . 54E+0l 6.37E+0l 3.61E+0l F 10 911.24 5 . 57E+0l 19.77 5 . 57E+0l 1.98E+0l F 11 1460.40 5.26E+02 4 7 .02 5.63E+0 l 1 . 71E+0l 4.70E+ 02 5 . 00E+0l F 12 1764.06 3.96E+0l 13 . 57 1.52E+0l 9 . 80E+00 2.44E+0l 1.67E+0l

1/15/2019 7:36:06AM Page 3 of6 Analysis Report for L 1-SUB-TDS-QSGS-004-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0 . 98 1460 . 75

• 10 . 67 5 . 22E+OO 6.27E- 01 CS - 137 0 . 98 661. 65

• 85.12 4 . 39 E- 02 2 . 50E- 02 PB- 212 0 . 55 77 . 11 17.50 238 . 63

• 44 . 60 1 .75E - 01 2. 62E- 02 BI - 21 4 0.54 609.31

• 4 6. 30 l .48E- 01 4. 4 3E- 02 1120 . 29 15.10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407.98 2 . 48 1509 . 19 2 . 19 176 4.4 9

• 15.80 2 . 15E- 01 1 .4 8E - 01 PB-214 0.72 77 .11 10.70 295 . 21

• 19 . 20 1.66E-01 4 . 65E- 02 351 . 92

• 37 . 20 1 . 00E- 01 4 .4 9E- 02 RA- 226 0 . 98 186 . 21

• 3 . 28 4 .0lE- 01 1.87E- 01 AC- 228 0 . 30 209 . 28 4.40 338 . 32

• 11. 40 9 . 14E- 02 5.32E-02 794 . 70 4.60 911.60

• 27.70 1 . 58E- 01 5 . 63E - 02 964.60 5 . 20 969 . 11 1 6 . 60

• =Energy line found in the spectrum.

- =Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/15/2019 7:36:06AM Page 4 of6 Analysis Report for L 1-SUB-TDS-QSGS-004-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K- 40 0 . 98 1 5 . 22E+00 6.27E- 01 CS - 137 0 . 987 4.39E-02 2 . 50E - 02 PB- 212 0.559 l.75E-01 2.62E-02 BI - 214 0.545 l.54E-01 4 . 24E-02 PB- 214 0 . 720 1. 32E- 01 3 . 23E - 02 RA- 226 0 . 980 4 . 0lE-01 1. 87E-01 AC - 228 0 . 302 1. 23E- 01 3 . 87E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:36:06AM Page 5 of6 Analysis Report for l 1-SUB-TDS-QSGS-004-SB l 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak locate Performed on  : 1/15/2019 7:35:57AM Peak locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 6 520.57 6 . 30671E- 03 33 . 23 F 7 582 . 9 1 2.40991E- 02 13 . 77 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 5.22E+00 5 . 15E- 01 5 . 15E- Ol

+ AR- 41 1293 . 64 99.16 - 2 . 12E+ll 2. 72E+ll 2 . 72E+ll

+ CO- 60 1173 . 22 100 . 00 2.78E- 02 4 . 97E - 02 5 . 47E- 02 1332. 49 100.00 6 . 51E- 02 4 . 97E-02

+ KR-85 513. 99 0.43 - 6.07E- 01 8.82E+00 8 . 82E+00

+ Y- 88 898 . 04 93 . 70 -7.40E- 04 3.06E-02 4 . 21E-02 1836.06 99 . 20 - 1. 35E- 03 3.06E- 02

+ NB- 94 702.63 100.00 8.37E-03 3.52E- 02 3.64E-02 871.10 100.00 5.07E- 03 3 . 52E-02

+ I - 131 284.30 6 . 06 - 8 . 69E- 02 4 . 67E-02 5 . 94E- 01 364 . 48 81. 20 3 . 92E- 02 4.67E - 02 636 . 97 7.27 3.82E- 01 6.56E - 0l

+ CS-134 604.70 97 . 60 - 3 . 16E- 03 4.46E- 02 4 . 67E-02 795.84 85 . 40 -2 . 47E - 03 4 . 46E-02

+ CS - 137 661. 65

• 85.12 4 . 39E - 02 4 . 38E-02 4 . 38E- 02

+ CE- 144 80.12 1. 36 1. 07E+00 2.41E- 01 3.03E+00

1/15/2019 7:36:06AM Page 6 of6 Analysis Report for L 1-SUB-TDS-QSGS-004-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclfdeMDA LineMDA Name (pCilgrams) (pCilgrams) (pCi/grams)

(keV)

CE-144 133.51 11.09 -4. 34E- 03 2 . 41E-01 2 . 41E- 01

+ EU-152 121.78 28.40 -3.35E-02 9.30£-02 9.30E-02 3 44. 28 26 . 60 -8.05£-02 1.16£-01 1408.00 20.74 8.04E-02 l.96E-01

+ EU-154 123 . 07 40.40 -3.65E-03 6 . 55E-02 6.55E-02 723.30 19.70 8 . 72E- 03 1.90E-01 1274.51 35 . 50 -7.79E-03 1.38E-01

+ EU-155 86.54 32 . 80 -4.64E-02 l . 04E-01 1 . 04E-01 105.31 21. 80 -5.55£-02 l . 27E-01

+ BI - 214 609 . 31

• 4 6.30 l.48E-01 6.99E- 02 6.99£-02 1120.29 15.10 3.91E- 01 3.61E-01 1238.11 5.94 7.73E-01 9 . 58E-01 1377 . 67 4 .11 5.03E-01 9.95E-01 1407.98 2.48 6. 72E-01 l.63E+00 1509 . 19 2 . 19 5.46E-02 l.47E+00 1764.49

• 15.80 2 . 15E-01 2 .4 2E-01

+ PB-214 77 . 11 10.70 6.93E-01 8 . 96E-02 4.llE-01 295.21

• 19.20 1.66E-01 l.00E-01 351 . 92

• 37 . 20 1.00E-01 8 . 96E-02

+ PA-228 89.95 22.00 1.34E+00 l.02E+0O 1. 74E+00 93 . 35 35 . 00 -2 .13E-01 l.02E+00 105 . 00 16 . 30 -5.00E-01 1. 96E+00 129.22 2.97 -2.39E+00 1. 02E+0l 338.32 5 . 30 l.07E+00 6 . 38E+00 463.00 13. 80 - 1.04E-0l 2.58E+O0 911 . 23 16 . 70 3.98E+00 3 . 60E+0O

+ AM-241 59.54 36 . 30 9.49E-02 1.88E- 01 1. 88E- 01

+ CM- 243 1 03.76 23.00 -2 . 91E-03 1.21E-01 l.21E-01 228 . 18 10.60 -4.57E-02 2 . 44E- 01 277.60 14.00 -l.52E-01 l . 94E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 7:36:46AM Page I of7

...ftApex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-005-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FSGS-005-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.023E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 1/8/2018 9:03:00AM Acquisition Started  : 1/8/2018 4:55:16PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live nme  : 3600.0 seconds Real nme  : 3610.8 seconds Dead Time  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100- 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5321 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:36:37AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:36:46AM Page 2 of7 Analysis Report for L 1-SUB-TDS-FSGS-005-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.61 14 7 - 161 153.77 1.82E+02 59.33 1 .4 9E+03 2.73 M 2 86.72 167 - 190 173.98 8.60E+01 35.73 7.14E+02 1.21 m 3 92.77 167 - 190 186.09 9.18E+0l 37.09 7.30E+02 1.23 F 4 185.52 365 - 379 371.53 1.05E+02 39.06 8.81E+02 1. 80 F 5 238.45 473 - 481 4 77. 38 2 . 74E+02 45.19 5.31E+02 1. 34 F 6 295.07 586 - 595 590 . 60 1. 25E+02 30.56 2.74E+02 1. 45 F 7 338.06 668 - 682 676.56 6 . 64E+0l 24.55 3.60E+02 1. 32 F 8 351. 78 698 - 710 703 . 98 1.60E+02 3 4. 26 3.08E+02 2 . 03 F 9 582.85 1157 - 1172 1166.03 1 . 02E+02 24.93 2 . 12E+02 1. 45 F 10 609.16 1214 - 1226 1218.66 1. 24E+02 26.93 l.56E+02 1. 58 F 11 661.44 1316 - 1332 1323.19 2 . 57E+02 34.59 1.37E+02 1. 77 F 12 910.96 1815 - 1829 1822.15 5.0lE+0l 19.20 l.09E+02 2.12 F 13 1120. 03 2236 - 2245 2240 . 25 2.44E+01 14 . 22 5.42E+0l 1. 64 F 14 1172.92 2341 - 2352 2346.02 1. 39E+02 27 . 57 1.14E+02 1.88 F 15 1332.26 2659 - 2672 2664.66 1. 25E+02 24.53 4.88E+0l 2.33 F 16 1460.43 2911 - 2928 2920.97 5.73E+02 49.21 3.69E+01 2 . 35 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:36:37AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.6 1 l.82E+02 59 . 33 l . 82E+02 5 . 93E+0l M 2 86. 72 8.60E+0l 35.73 8.60E+0l 3.57E+0l m 3 92 . 77 9. 1 8E+0l 37 . 09 9.18E+0l 3.71E+0l F 4 185 . 52 1. 05E+02 39 . 06 1. 05E+02 3.91E+0l F 5 238 .4 5 2.74E+02 45.19 2.74E+02 4.52E+0l F 6 295.07 1.25E+02 30.56 l.25E+02 3.06E+0l F 7 338.06 6.64E+0l 24 . 55 6.64E+0l 2 . 45E+0l F 8 351. 78 1 . 60E+02 34.26 8.36E+0l 3. 72E+0l 7 .67E+0l 5 .06E+0l F 9 582.85 1.02E+02 24.93 l.02E+02 2.49E+0l F 10 609.16 1.24E+02 26.93 4 . 12E+0l 2 . 42E+0l 8.30E+0 l 3.6 2E+0l F 11 661.44 2. 57E+02 34.59 6.61E+0l 2.54E+0l l . 90E+02 4.29E+0l F 12 910.96 5.0lE+0l 19 . 20 5.0lE+0l l.92 E+0l F 13 1120. 03 2.44E+0l 14.22 2.44E+0l l.42E+0l

1/15/201 9 7:36:46AM Page 3 of7 Analysis Report for L1-SUB-TDS-FSGS-005-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 14 1172.92 l . 39E+02 27.57 4 . 55E+0l l . 72E+0l 9 . 32E+0l 3.25E+0l F 15 1 332.26 l.2 5E+02 24.53 l. 25E+ 02 2.45E+0l F 16 1460 . 43 5.73E+02 49 . 21 5.63E+0l l . 71E+0l 5 .1 7E+02 5.21E+0l M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCl/grams) Uncertainty K- 40 0 . 98 1460 . 75

• 10 . 67 5.51E+00 6 . 33E- 01 CO- 60 0 . 98 1173 . 22

• 100 . 00 8.76E- 02 3.0 9E- 02 1332 . 49

• 100.00 l. 31E- 01 2 . 66E-02 CS- 137 0 . 99 661.65

• 85 . 12 l. 26E- 01 2 . 91E - 02 EU- 155 0 . 32 86 . 54

• 32 . 80 5 . 36E- 02 2 . 27E- 02 105.31 21. 80 PB- 212 0 . 98 77 . 11

• 17 . 50 2 . 5 4E- 01 8 . 42E- 02 238 . 63

• 44 . 60 1. 38E - 0l 2 . 39E-02 BI - 21 4 0 . 58 609 . 31

• 46 . 30 9 . 34E- 02 4 . llE- 02 1120.29

• 15 . 10 l . 46E- 01 8.52E- 02 1238 . 11 5 . 94 1 3 77 . 67 4 . 11 1407.98 2.48 1509 . 19 2 .1 9 1764 . 49 15 . 80 PB- 214 0.99 77 . 11

• 10.70 4 . 15E- 0l l.38E- 01 295 . 21

• 19 . 20 1 . 74E- 01 4.36E- 02 351 . 92

• 37.20 6.48E - 02 4 . 28E- 02 RA- 226 0 . 92 186 . 21

• 3 . 28 6 . 02E - 01 2 . 27E- 01

1/15/2019 7:36:46AM Page4 of7 Analysis Report for L 1-SUB-TDS-FSGS-005-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

• :a: Energy line found in the spectrum.

- :a: Manually added nuclide.

? :a: Manually edited nuclide.

@ :a: Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold :a: 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-4 0 0.984 5.51E+00 6 . 33E- 01 CO-60 0.989 1.13E-01 2.02E-02 CS-137 0 .993 1.26£-01 2 . 91E-02 EU-155 0 . 328 5 . 36E-02 2.27E-02 PB-212 0.986 1.41E-01 2.30E - 02 BI - 214 0.582 1.03E-01 3.70E-02 PB- 214 0.991 1 . 22E- 01 2 . 99E-0 2 RA- 226 0.926 6.02£- 01 2 . 27E-0 1

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:36:46AM Page 5 of7 Analysis Report for L 1-SUB-TDS-FSGS-005-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:36:37AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 3 92.77 2 . 54877E- 02 20 . 2 1 Tol. PA- 228 F 7 338 . 06 1 . 84406E- 02 18. 49 Tol. AC- 228 PA-228 F 9 582 . 85 2.83849E- 02 12.20 F 12 9 1 0 . 96 l . 39164E- 02 19 . 16 Tol. AC - 228 PA- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide library Used  : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LlneMDA Name (pC/lgrams) (pCUgrams) (pCi/grams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 5 . 51E+00 5 . 13E-01 5 . 13E- 01

+ AR-41 1293.64 99 . 16 4 . llE- 01 l.l0E+00 1 . l0E+00

+ CO-60 1173.22

• 100.00 8 . 76E-02 3. llE- 02 5 . 31 E- 02 1332 . 49

• 100 . 00 l.31E- 01 3.llE-02

+ KR- 85 513 . 99 0 . 43 9 . llE+00 9 . ll E+OO 9. llE+00

+ Y-88 898 . 04 93 . 70 2.49E-02 2 . 71E- 02 4.73E- 02 1836 . 06 99 . 20 - 4 . 70E - 03 2. 71E-02

+ NB-94 702 . 63 100 . 00 7.78E-03 3.49E- 02 3 . 49E- 02 871 . 10 100.00 -4.78E-02 3.93E-02

1/15/2019 7:36:46AM Page 6 of7 Analysis Report for L 1-SUB-TDS-FSGS-005-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ I-131 284.30 6.06 2.83E-03 3.46E- 02 4.60E- 01 364.48 8 1. 20 -1.57E-02 3.46E-02 636 . 97 7.27 - 1. 39E - 01 4 .67E- 01

+ CS -1 34 604.70 97 . 60 - 4 . 34E-02 4 . 42E- 02 4.49E-02 795.84 85.40 -1. 77E-02 4 . 42E-02

+ CS-137 661.65

• 85.12 l . 26E - 0 1 4. 75E-02 4.75E-02

+ CE-14 4 80.12 1. 36 - 2 . 09E-0 1 2 . 30E-01 2.86E+OO 133 . 51 11.09 - 1 . 21E-0 1 2 . 30E- 0 1

+ EU-152 121.78 28 . 40 -4 .45E - 02 8 . 98E-02 8 . 98E-02 344 . 28 26 . 60 - 5.02E - 02 l.1 6E-0 1 1408 . 00 20 . 74 -6.49E-02 1 . 84E - 01

+ EU- 154 123 . 07 40.40 - 6 . 13E-03 6 . 35E-02 6 . 35E - 02 723 . 30 1 9.70 1. 45E- 01 1.94E-01 127 4 .5 1 35.50 -9 . 38E- 02 1.25E- 01

+ EU-155 86 . 54

• 32 . 80 5 . 36E- 02 5.65E-02 5.65E-02 105 . 3 1 21. 80 -1 . 62E-02 l.22E-01

+ BI-214 609.31

• 46 . 30 9.34E- 02 7 . 66E-02 7 . 66E- 02 1120.29

• 1 5.10 1. 46E-01 1.70E-01 1238.11 5.9 4 4.14E- 01 9 . 58E - 01 1377 . 67 4 . 11 1. 85E- 02 8.83E-0 1 1407 . 98 2.48 -5 . 43E- 01 1. 54E+OO 1509. 1 9 2.19 7.37E-01 1 . 48E+OO 1764. 49 1 5.80 2 . 36E-01 2 . 68E-01

+ PB- 214 77 . 11

• 10 . 70 4 . 15E-01 8 . 27E-02 3 . 53E- 01 295 . 2 1

• 1 9.20 1 . 74E- 01 8 . 48E-02 351 . 92

• 37 . 20 6 . 48E- 02 8.27E-02

+ PA-228 89 . 95 22 . 00 1 . 4 2E- 01 1. llE- 01 1 . 90E- 01 93.35 35.00 l.86E- 03 1. llE- 01 105.00 16 . 30 -1.15E- 02 2.14E-01 129 . 22 2 . 97 - 4.80E- 01 1.12E+OO 338 . 32 5.30 3 . 74E- 01 7.31E-01 463.00 13 . 80 3. 71E- 02 3. llE-01 911.23 1 6.70 1 . 13E- 01 3 . 86E-0 1

+ AM-241 59 . 54 36 . 30 - 1.45E- 01 1. 80E-01 1.80E- 01

+ CM-243 103.76 23 . 00 8.88E-03 1 . 18E-Ol 1 . 18E-01 228.18 10 . 60 -9.96E- 02 2.40E- 0 1 277 . 60 14.00 2.43E-02 1.97E- 01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 7:36:46AM Page 7 of7 Analysis Report for L 1-SUB-TDS-FSGS-005-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

1/15/2019 7:37:35AM Page I of6

__,,Apex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-006-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FSGS-006-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.984E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/8/2018 9:1 0:00AM Acquisition Started  : 1/8/2018 6:01 :35PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.8 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100-4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5322 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:37:26AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:37:35AM Page 2 of6 Analysis Report for L 1-SUB-TDS-FSGS-006-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.76 147 - 158 154.08 1.26E+02 42 . 88 1 . 07E+03 1. 41 F 2 185.83 369 - 376 372 .15 4.63E+Ol 30.19 4.64E+02 1. 28 F 3 238 . 60 469 - 485 477.68 3.30E+02 45 . 81 7.15E+02 1. 56 F 4 295.26 586 - 598 590.97 5 . 79E+Ol 24.67 3.88E+02 1. 20 F 5 338.22 670 - 685 676.87 l . 05E+02 27 .20 2.46E+02 1. 87 F 6 582.98 1160 - 1172 1166.31 8.73E+Ol 23.71 l . 58E+02 1. 53 F 7 609.13 1213 - 1226 1218.59 l . 25E+02 26.20 1. 27E+02 1. 74 F 8 910 . 89 1816 - 1827 1822.02 4.73E+Ol 1 7 . 52 9. llE+Ol 1. 42 F 9 969.15 1932 - 1944 1938.52 3.87E+Ol 16. 89 8 . 22E+Ol 1. 84 F 10 1332.04 2659 - 2670 2664 . 22 2 .7 4E+Ol 13 . 61 3.93E+Ol 2.03 F 11 1460.45 2913 - 2929 2921. 01 5.41E+02 47.95 4.25E+Ol 2.39 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:37:26AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76 . 76 1. 26E+02 42.88 l.26E+02 4 . 29E+Ol F 2 185 . 83 4 . 63E+Ol 30.19 4.63E+Ol 3 . 02E+Ol F 3 238.60 3.30E+02 45 . 81 3 . 30E+02 4 . 58E+Ol F 4 295.26 5.79E+Ol 24. 67 5 . 79E+ Ol 2.47E+Ol F 5 338.22 l.05E+02 27 . 20 l.05E+02 2. 72E+Ol F 6 582.98 8 . 73E+Ol 23.71 8 . 73E+Ol 2.37E+ Ol F 7 609 . 13 l . 25E+02 26.20 4.12E+Ol 2.42E+Ol 8.34E+Ol 3.57E+Ol F 8 910.89 4.73E+Ol 17 . 52 4.73E+Ol 1. 75E+ Ol F 9 969 .15 3 . 87E+Ol 16.89 3.87E+Ol 1 . 69E+Ol F 10 1332.04 2.74E+Ol 13.61 2.74E+Ol l.36E+Ol F 11 1460 .4 5 5 . 4 1E+02 47.95 5.63E+Ol 1 . 71E+Ol 4.85E+02 5.09E+Ol

=

M First peak in a multiplet region

=

m Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2.000sigma

1/15/2019 7:37:35AM Page 3 of6 Analysis Report for l 1-SUB-TDS-FSGS-006-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.98 1460 . 75

• 10.67 5 . 29E+00 6 . 28E- 01 PB- 212 0.99 77 . 11

• 17.50 l.80E- 01 6.20E- 02 238.63

• 44.60 l . 70E- 01 2.53E- 02 BI - 21 4 0 . 34 609.31

• 46 . 30 9 . 61E-02 4.15E- 02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 .11 1407 . 98 2.48 1509.19 2 . 19 1764.49 15.80 RA- 226 0 . 97 186 . 21

• 3 . 28 2 . 73E- 01 l.79E- 01 AC- 228 0 . 60 209.28 4 . 40 338 . 32

• 11. 40 2.87E- 01 7.54E-02 794 . 70 4.60 911. 60

• 27 . 70 l.31E- 01 4 . 90E- 02 964.60 5 . 20 969 . 11

• 16.60 l . 90E-01 8.31E - 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

1/15/2019 7:37:35AM Page4 of6 Analysis Report for L 1-SUB-TDS-FSGS-006-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.986 5.29E+00 6.28E-01 PB-212 0.995 1.72£-01 2.34£-02 BI-214 0.347 9.61E-02 4.15£-02 RA-226 0.977 2.73£-01 l.79E-01 AC-228 0.601 1. B0E-01 3.68£-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:37:35AM Page 5 of6 Analysis Report for L1-SUB-TDS-FSGS-006-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:37:26AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 295.26 1.60892£- 02 2 1. 29 Tol. PB- 2 1 4 F 6 582.98 2 . 42427£- 02 13 . 58 F 10 1332. 04 7 . 59996E- 03 24 . 88 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCl/grams)

(keV)

+ K- 40 1460.75

• 10.67 5 . 29E+00 5.32E- 01 5.32£ - 01

+ AR- 41 1293 . 64 99.16 - l . 65E+00 1. 34E+00 l . 34E+O0

+ CO- 60 1173 . 22 100 . 00 3 . 72 E- 02 4 . 80E- 02 5 . 4 1E- 02 1332.49 100 . 00 1. 39E- 02 4 . 80£- 02

+ KR- 85 513 . 99 0 . 43 l . 45E+0l 8 . 60E+00 8.60E+00

+ Y- 88 898 . 04 93 . 70 -2 . 4 1E-02 3 . 03E- 02 3 . 92E- 02 1836 . 06 99.20 -7 . 56£- 04 3.03E-02

+ NB- 94 702.63 100.00 - l . 28E- 0 2 3.33E- 02 3 . 33£- 02 871.10 1 00 . 00 - 1. 48E-02 3 . 46E - 02

+ I -1 31 284 . 30 6.06 - 1 . 25E - 01 3 . 42E- 02 4.51E - 01 36 4 .48 81.20 7 . 07E- 03 3 . 42£- 02 636 . 97 7 . 27 -l . 37E- 01 4 .74E-Ol

+ CS - 134 604 . 70 97.60 - 8 . 47E- 03 4. 35E-02 4. 39E - 02 795 . 84 85.40 - 5 . 28E-02 4.35E- 02

+ CS - 137 661.65 85 . 12 1. 39E - 02 4 . 70E-02 4 . 70E-02

1/15/2019 7:37:35AM Page 6 of 6 Analysis Report for L 1-SUB-TDS-FSGS-006-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams)

(keV)

+ CE- 144 80.12 1. 36 - 1.92E+00 2.30E-01 2.81E+00 133. 51 11.09 1 . 52E- 01 2 . 30E- 01

+ EU- 152 121.78 28.40 - 3.76E-02 9.04E-02 9 . 04E-02 344.28 26.60 -2.53E- 01 l.12E-01 1408.00 20 . 74 -6.24E-02 1 . 71E-01

+ EU-154 123.07 40.40 -3.06E - 02 6.35E- 02 6 . 35E- 02 723. 30 19 . 70 4 . 36E - 02 1.71E-01 1274 . 51 35.50 3.72E-02 l . 30E- 01

+ EU-155 86 . 54 32.80 2.46E- 02 l . 0lE-01 l.0lE-01 105 . 31 21. 80 1.30E-01 1 . 25E- 01

+ BI - 2 1 4 609 . 31

• 46.30 9.61E- 02 7.55E- 02 7.55E-02 1120.29 15.10 1.54E-01 3.43E- 01 1238 .11 5.94 4.97E-01 9.75E-01 1377 . 67 4.11 9 . 83E-01 1. 0lE+0O 1 407.98 2.48 -5 . 22E-01 1. 4 3E+0O 1509 . 19 2.19 - 5.25E-02 1 . 42E+0O 1764 . 49 15.80 2.28E - 01 2.99E-01

+ PB-214 77 .11 10.70 3.73E-02 8.61E- 02 3 . 82E-01 295 . 21 19 . 20 9.62E-02 1. S0E-01 351 . 92 37 . 20 1 . 53E-01 8.61E-02

+ PA-228 89.95 22 . 00 2.47E-01 1.13E-01 1.96E-0l 93.35 35.00 -9.70E-02 1 . 13E-01 105.00 16 . 30 2 . 27E-0l 2.24E-0l 129 . 22 2 . 97 1.84E-01 1.15E+00 338 . 32 5.30 - 2. llE-02 7.17E-01 4 63 . 00 13.80 -2.12E-01 2 . 79E-0l 911 . 23 16.70 3.77E-01 3.82E-01

+ AM- 241 59 . 54 36 . 30 - 6.64E-02 1. 78E- 01 1.78E-01

+ CM-243 103 . 76 23.00 6. 72E-02 1. l 9E- 01 1. 1 9E - 01 228 . 18 10 . 60 8.82E-02 2 . 38E-Ol 277 . 60 14.00 8.33E - 02 1.95E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 7:38:15AM Page I of6

~~~~pex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-007-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FSGS-007-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.050E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 1/8/2018 9:15:00AM Acquisition Started  : 1/8/2018 7:04:18PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real nme  : 3610.9 seconds Dead nme  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5323 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:38:06AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:38:15AM Page 2 of6 Analysis Report for L 1-SUB-TDS-FSGS-007-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 .56 147 - 161 153.67 2 .28E+02 62.31 1 .48E+03 3.01 F 2 185.99 367 - 378 372.47 9.0lE+0l 38.20 7.48E+02 1. 67 F 3 238.49 469 - 482 477.46 2.68E+02 45.91 7.93E+02 1. 48 F 4 294 .84 584 - 596 590.13 8.0lE+0l 29. 77 4.15E+02 1. 64 F 5 338.21 673 - 685 676.85 8.34E+0l 26.65 2.79E+0 2 1. 70 F 6 351. 62 697 - 709 703.68 l . 50E+02 31. 16 2.86E+02 1. 51 F 7 509 .89 1016 - 1025 1020.15 2 .9 4E+0l 18.01 2.06E+02 0.99 F 8 583.00 1157 - 1175 1166.35 9.17E+0l 23.53 l.63E+02 2.01 F 9 609.05 1213 - 1223 1218.42 l.18E+02 25.54 l.16E+02 1. 47 F 10 661.52 1318 - 1331 1323. 35 2.14E+02 32 .62 1. 50E+02 1. 67 F 11 911.05 1818 - 1829 1822.34 5.39E+Ol 19.02 7.76E+0l 2.15 F 12 968.80 1933 - 1945 1937.82 3.67E+0l 15.94 7 .68E+0l 1. 56 F 13 1237 . 65 2470 - 2481 2475 .4 5 2.53E+0l 14.88 7.70E+0l 1. 72 F 14 1332. 02 2658 - 2671 2664.17 5.32E+0l 16.60 3.18E+0l 2.41 F 15 1460.43 2912 - 2929 2920.98 5 .61E+02 48.00 9.00E+00 2.43 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:38:06AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76 . 56 2.28E+02 62.31 2.28E+02 6 . 23E+0 l F 2 185.99 9 . 0lE+0l 38.20 9 . 0lE+0l 3.82E+0l F 3 238 .49 2 . 68E+02 45.91 2 . 68E+02 4 . 59E+0l F 4 294.84 8 .0 lE+0l 29 . 77 8 . 0lE+0l 2.98E+0l F 5 338 . 21 8.34E+0l 26.65 8.34E+0l 2.67E+0l F 6 351.62 1. 50E+02 31.16 8.36E+0l 3 . 72E+0l 6.66E+0l 4.85E+0l F 7 509 . 89 2.94E+0l 18.01 2.94E+0l l.80E+0l F 8 583 .00 9.17E+0l 23 . 53 9.17E+0l 2 . 35E+0l F 9 609.05 l .18E+02 25.54 4.12E+0l 2 .42E+0 l 7.67E+0l 3 . 52E+0l F 10 661 . 52 2 .1 4E+02 32.62 6.61E+0l 2 . 54E+0l l.48E+0 2 4.13E+0l F 11 911. 05 5.39E+0l 19.02 5.39E+0l l . 90E+0l F 12 968.80 3.67E+0l 1 5 .94 3.67E+Ol 1.59E+0l F 13 1237.65 2.53E+0l 14.88 2.53E+0l 1.49E+0l F 14 1332 .0 2 5 . 32E+0l 16 . 60 5 . 32E+Ol 1 . 66E+0l

1/15/2019 7:38:15AM Page 3 of6 Analysis Report for L1-SUB-TDS-FSGS-007-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 15 1460 . 43 5 . 61E+02 48 . 00 5.63E+Ol l . 71E+Ol 5 . 04E+02 5 . lOE+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0.98 1460 . 75

• 10 . 67 5 . 23E+OO 6.03E- 01 CS- 137 0 . 99 661. 65

• 85 . 12 9 . 53E- 02 2 . 71E-02 PB- 212 0 . 98 77 .11

• 17.50 3 . 09E - 01 8 . 69E - 02 238.63

• 44 . 60 1. 32E- Ol 2.35E - 02 BI- 214 0 . 43 609.31

• 4 6. 30 8 . 41E- 02 3 . 89E- 02 1120 . 29 15.10 1238 . 11

• 5 . 94 4.09E- 01 2 . 41E-01 1377 . 67 4 . 11 1407.98 2.48 1509 . 19 2 . 19 1764.49 15.80 PB- 214 0 . 97 77 . 11

• 10.70 5 . 05E - Ol l . 42E - 01 295.21

• 19 . 20 1. 09E-01 4 . 09E- 02 351.92

• 37.20 5.48E - 02 4 . 00E- 02 RA-226 0 . 99 186.21

• 3.28 5 . 06E-Ol 2 . 16E- 01 AC - 228 0.61 209 . 28 4.40 338 . 32

• 11. 40 2.16E- 01 6.98E-02 794 . 70 4 . 60 911. 60

• 27 . 70 1. 42E - 01 5.06E- 02 964.60 5 . 20 969 . 11

• 16 . 60 1. 71E - 01 7.46E-02

1/15/2019 7:38:15AM Page4 of6 Analysis Report for L 1-SUB-TDS-FSGS-007-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.984 5.23E+00 6 . 03E-0 1 CS - 137 0.997 9.53E- 02 2 . 71E-02 PB- 212 0.984 1.40E-01 2 . 28E-02 BI - 214 0.430 9.23E-02 3.84E-02 PB-214 0.978 8 . 89E-02 2.81E-02 RA-226 0. 992 5.06E-01 2 . 16E-01 AC-228 0 . 610 1 . 68E- 01 3 . 59E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:38:15AM Page 5 of6 Analysis Report for L 1-SUB-TDS-FSGS-007-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:38:06AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 7 509 . 89 8.17684E- 03 30 . 60 F 8 583.00 2.5 4 805E- 02 12 . 82 F 14 1332 . 02 1 . 478 6 2E- 02 1 5 .59 Tol. CO- 60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCl/grams) (pCl/grams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 5 . 23E+OO 4 . 38E- 01 4. 38E - 0 1

+ AR-41 1293.64 99.16 - 7 . 40E- 0l 2 . 13E+00 2 .13E+00

+ CO-60 11 73.22 100 . 00 9 . 74E- 03 4 . 87E-02 5 . 60E - 02 1332 .4 9 100 . 00 4 . 15E- 02 4. 87E - 02

+ KR- 85 513. 99 0 .4 3 6 . 23E+00 8.2 4E+00 8 . 24E+0O

+ Y-88 898.04 93 . 70 - 2 . 45E-03 2 . 81E - 02 4 .13E- 02 1836.06 99 . 20 -2 . 66E- 02 2 . 8 1E- 02

+ NB- 94 702 . 63 100.00 1 . 02E- 0 3 3. 4 4£-02 3.46£- 02 871.10 100 . 00 - 9.43E-03 3 . 44£- 02

+ I - 131 284 . 30 6 . 06 - 5 . 05£- 01 3 . 34£-02 4 . 24£-01 36 4.4 8 81. 20 - 7 . 26E - 04 3 . 34E - 02 636 . 97 7 . 27 - 9 . 35E- 02 4 . 72E-0 1

+ CS-134 604.70 97 . 60 4 . 99E- 02 4.15£- 02 4 . 15£- 02 795 . 84 85 . 40 - 4.03E - 03 4 . 37E- 02

+ CS- 137 661 . 65

• 85.12 9.53£ - 02 4 . 60E - 02 4 . 60E-02

1/15/2019 7:38:15AM Page 6 of6 Analysis Report for L 1-SUB-TDS-FSGS-007-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity Nucl/deMDA LlneMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

+ CE-144 80.12 1. 36 7.36E - 01 2.22E-0l 2 . 80E+00 133.51 11.09 1. 23E-01 2.22E-01

+ EU-152 121. 78 28.40 -2.40E-02 8.52E-02 8.52E-02 344 . 28 26.60 -3.12E-02 1.14E-01 1408 . 00 20.74 8.28E-02 1 . 66E-01

+ EU- 154 123 . 07 40.40 -5 .1 2E-04 6.04E-02 6 . 04E-02 723. 30 19.70 1.29E-01 1.80E-01 1274 . 51 35.50 1.89E- 03 1.30E-01

+ EU-155 86 . 54 32.80 -7.55E-03 9.63E-02 9.63E-02 105 . 31 21. 80 3.86E-03 1.21E-0l

+ BI - 214 609.31

• 46.30 8.41E-02 6.81E- 02 6 . 81E-02 1120.29 15.10 -2.33E-01 3.26E- 01 1238 . 11

• 5.94 4.09E- 01 5.66E-01 1377. 67 4 .11 -8.67E-02 7.33E-01 1407.98 2.48 6.92E-01 1. 39E+00 1509.19 2. 1 9 1.30E- 01 1.30E+00 1764.49 15.80 1.35E-01 2.51E-01

+ PB- 214 77 .11

• 10.70 5.05E-01 7 . 90E-02 3. 45E-01 295.21

• 19 . 20 1. 09E- 01 1.09E-01 351 . 92

• 37.20 5.48E-02 7.90E-02

+ PA-228 89.95 22.00 2.14E-01 1 . 16E-01 1.95E-01 93.35 35 .00 6 . 13E-02 l.16E-01 105.00 16.30 4.45E-02 2.24E-01 129.22 2 . 97 -2.89E-01 1 . 12E+00 338.32 5.30 6.27E-01 7 .63E-01 463.00 13.80 2.75E-02 3. 1 9E-01 911. 23 16 . 70 2 . 50E-01 3.81E- 01

+ AM-241 59.54 36.30 -1 . 09E-01 1 . 75E-0l l.75E- 01

+ CM-243 103.76 23.00 5.37E- 02 1.16E- 01 1. 16E-01 228. 18 10 . 60 -l . l0E-01 2.30E- 0l 277.60 14.00 -1 . 28E-Ol 1. 81E- 01

+ = Nuclide identified during the nuclide identification

• =Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 7:38:58AM Page I of6

~ Apex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-008-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FSGS-008-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.017E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 1/8/2018 9:23:00AM Acquisition Started  : 1/8/2018 8:19:50PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.0 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5324 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:38:49AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:38:58AM Page 2 of6 Analysis Report for L 1-SUB-TDS-FSGS-008-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.29 147 - 159 153 .13 2.15E+02 59. 78 1. 23E+03 3.04 F 2 238.51 472 - 485 477.50 3.62E+02 48.07 6.65E+02 1. 46 F 3 269 .8 1 532 - 544 540.09 4.12E+0l 25 . 47 4.40E+02 1. 31 F 4 295.00 584 - 596 590.45 9.38E+0l 30.07 4.47E+02 1. 45 F 5 338.19 672 - 680 676 . 82 6.09E+0l 24.10 2.20E+02 1. 29 F 6 351.74 695 - 710 703 . 90 1.89E+02 34.42 3.84E+02 1. 59 F 7 583.00 1161- 1173 1166.35 8.42E+0l 22.68 1.62E+02 1. 28 F 8 609 . 26 1213 - 1225 1218.86 1 . 22E+02 26. 41 1.39E+02 1. 75 F 9 661 .4 2 1315 - 1328 1323.15 2. 72E+02 35.82 1. 18E+02 1. 89 F 10 910 . 79 1816 - 1831 1821.82 6.70E+0l 19.76 7.85E+0l 2 .11 F 11 968 . 72 1933 - 1943 1937.66 2.66E+0l 15.26 8.52E+0l 1.50 F 12 1332 . 06 2659 - 2672 2664.26 3 . 44E+0l 15.23 5.18E+0l 2 .4 2 F 13 1460.46 2915 - 2929 2921.03 5.21E+02 46 . 68 2.26E+0l 2 . 39 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:38:49AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. {keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.29 2 .1 5E+02 59.78 2.15E+02 5.98E+0l F 2 238 . 51 3.62E+02 48.07 3 . 62E+0 2 4.81E+0l F 3 269.81 4.12E+0l 25.47 4. 12E+0l 2.55E+0l F 4 295.00 9.38E+0l 30.07 9.38E+0l 3.0lE+0l F 5 338.19 6 . 09E+0l 24.10 6 . 09E+0l 2.41E+0l F 6 351. 74 1.89E+02 34.42 8.36E+0l 3. 72E+ 0 l 1.05E+02 5.07E+0l F 7 583.00 8.42E+0l 22 . 68 8 . 42E+0l 2 . 2 7E+0l F 8 609 . 26 1.22E+02 26.41 4.12E+0l 2 . 42E+0l 8.04£+01 3.58E+0l F 9 661.42 2. 72E+02 35.82 6 . 61 E+0l 2.54E+0l 2.06E+02 4.39E+0l F 10 910.79 6 . 70E+0l 19.76 6.70E+ 0l 1.98E+0l F 11 968.72 2.66E+0l 1 5 .26 2.66E+0l 1 . 53E+0l F 12 1332.06 3.44E+0l 15.23 3.44E+0l 1.52E+0l F 13 1460 . 46 5.21E+02 46 . 68 5 . 63E+0l 1.71E+ 0l 4.64E+0 2 4.97E+0l

1/15/2019 7:38:58AM Page 3 of 6 Analysis Report for L 1-SUB-TDS-FSGS-008-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 98 1460.75

• 10.67 4.97E+OO 6.00E-01 CS - 137 0 . 99 661.65

• 85 . 12 l . 37E - 01 3 . 0 l E- 02 PB-212 0 . 96 77 .11

• 17.50 3 . 03E - 01 8 .65E- 02 238.63

• 44 . 60 l .84E - 01 2 . 62E-02 BI-214 0.34 609.31

• 46.30 9 . lOE - 02 4. 09E- 02 1120.29 15 . 10 1238 .11 5 . 94 1377 . 67 4 . 11 1407.98 2.48 1 5 09.19 2.19 1764.4 9 15 .8 0 PB- 21 4 0 . 97 77 .11

• 10 . 70 4 . 96E- 01 1. 41E- 01 295.21

• 19.20 l.32E- 01 4 . 28E-02 351 . 92

• 37 . 20 8 . 96E-02 4 . 33E- 02 AC- 228 0 . 58 209 . 28 4.40 338 . 32

• 11. 40 l. 63E- Ol 6.49E- 02 794 . 70 4 . 60 91 1. 60

• 27 . 70 1. 83E- Ol 5.44E - 02 964.60 5 . 20 969 . 11

• 16 . 60 1. 28E - Ol 7.36E-02

• = Energy line found in the spectrum.

- :;;: Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean A ctivity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/15/2019 7:38:58AM Page 4 of6 Analysis Report for L 1-SUB-TDS-FSGS-008-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.986 4.97E+OO 6.00E-01 CS-137 0.991 1. 37E-01 3.0lE-02 PB-212 0.969 1. 88E-01 2.SlE-02 BI-214 0.349 9.lOE-02 4.09E-02 PB-214 0.978 1.14E-01 2.98E-02 AC-228 0.586 l.63E-01 3.63E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:38:58AM Page 5 of6 Analysis Report for L 1-SUB-TDS-FSGS-008-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:38:49AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 3 269 . 81 1.14359E-02 30 . 94 F 7 583 . 00 2 . 33793E- 02 13 . 4 7 F 12 1332.06 9 . 54359E- 03 22 . 16 Tol. CO- 60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCl/grams) (pCilgrams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 4 . 97E+00 4.75E - 01 4 . 75E- 01

+ AR- 41 1293.64 99 . 16 2.05E- 01 3.31E+00 3.31E+00

+ CO-60 1173 . 22 100.00 3 . 46E- 02 5.23E - 02 5.85E - 02 1332 . 49 100 . 00 6 . 97E- 02 5 . 23E-02

+ KR- 85 513.99 0 . 43 7.l0E+00 8.77E+00 8 . 77E+00

+ Y- 88 898.04 93.70 3 . 45E- 02 3 . 06E-02 4 . 32E - 02 1836 . 06 99.20 -3.39E-02 3.06E-02

+ NB-94 702.63 100.00 - l.83E- 02 3 . 48E- 02 3 . 48E- 02 871.10 100 . 00 - l.84E- 02 4.13E - 02

+ I - 131 284.30 6.06 -2.68E-0l 3 . 69E- 02 4.74E - 01 364 . 48 81.20 - l.22E- 03 3.69E-02 636 . 97 7 . 27 2.37E-01 4.73E - 01

+ CS- 134 604 . 70 97.60 3.24E- 03 4.34E- 02 4.34E - 02 795 . 84 85 . 40 - 3.24E-02 4.40E-02

+ CS-137 661. 65

• 85.12 l.37E- 01 4.50E- 02 4.50E- 02

1/15/2019 7:38:58AM Page 6 of6 Analysis Report for L 1-SUB-TDS-FSGS-008-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ CE-144 80.12 1. 36 -6.53E-01 2.34E-Ol 2.86E+OO 133.51 11.09 9 . 94E-02 2.34E-01

+ EU-152 121. 78 28.40 -2.94E-02 8.87E-02 8.87E-02 344.28 26 . 60 -5.46E-02 l.18E-01 1408.00 20.74 -2.63E-02 l.6 4E-01

+ EU-154 123.07 40 . 40 -3.22E-02 6.21E-02 6.21E-02 723. 30 19.70 -4.74E-0 2 1. 69E-01 1274.51 35.50 -3.67E-02 l . 31E-01

+ EU-155 86.54 32 . 80 -3.03E-02 9.91E-02 9.91E- 02 105.31 21. 80 6. 72E-03 1. 23E-01

+ BI-214 609.31

• 46 . 30 9 . lOE-02 7.48E-02 7.48E-02 1120.29 15.10 l.91E-01 3.39E-01 1238 .11 5.94 4.35E-01 l.OlE+OO 1377 . 67 4 .11 -1 . 71E-01 9 . lSE-01 1407.98 2.48 - 2.20E- 01 1.37E+OO 1509.19 2 . 19 -5.08E-01 1.32E+OO 1764 .4 9 15.80 2.61E- 01 2 . 75E-01

+ PB-214 77 .11

• 10.70 4 . 96E-01 9 . 09E-02 3 . llE-01 295.21

• 19 . 20 1. 32E-01 1.16E-01 351.92

• 37 . 20 8.96E-02 9 . 09E-02

+ PA-228 89.95 22.00 1 . 99E-Ol l.22E-01 2 . 07E-01 93 . 35 35.00 l . 83E-03 l.22E-01 105.00 16 . 30 -l.81E-02 2.37E-01 129.22 2.97 -8.76E-Ol 1. 22E+OO 338.32 5.30 8.68E-0 1 8 . 20E- 01 463.00 13 . 80 3.31E-02 3.35£- 01 911 . 23 16.70 1.23E-01 3.96E-01

+ AM-241 59.54 36.30 3.14E-02 1.89E-01 1.89£-01

+ CM-243 103 . 76 23.00 -9.38E-03 1.1 7E- 01 1.17E-01 228 . 18 10.60 - 1. 88E-01 2.49E-01 277.60 14.00 -5.82E-03 2.00E-01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 7:39:41AM Page I of6

~~~~pex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-009-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FSGS-009-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.896E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/8/2018 9:32:00AM Acquisition Started  : 1/8/2018 9:24:00PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real lime  : 3611.0 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5325 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:39:32AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:39:41AM Page 2 of6 Analysis Report for L 1-SUB-TDS-FSGS-009-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 . 11 147 - 161 152.76 2 . 21E+02 60.89 1.39E+03 3 . 36 F 2 185 . 54 367 - 377 371.58 5.44E+0l 33.39 6 .61 E+02 1. 43 F 3 238.55 470 - 485 477 . 57 3 .05E+02 44.69 6 . 96E+02 1. 46 F 4 295.17 587 - 594 590.78 l.13E+02 30.18 2 . 10E+02 1. 73 F 5 338.13 673 - 682 676 . 68 4.65E+0l 23.28 2.61E+02 1. 30 F 6 351. 71 695 - 707 703 . 85 1. 72E+02 33.00 2.47E+02 1. 79 F 7 582.98 1161 - 1172 1166 . 31 9.79E+0l 25 . 38 1.42E+02 1. 89 F 8 609 . 23 1214 - 1227 1218.78 1 . 16E+02 26.18 1. 37E+02 1. 89 F 9 66 1. 40 1313 - 1329 1323.12 1 . 66E+02 29. 40 1.37E+02 1. 97 F 10 910.80 1816 - 1828 1 821. 85 6.20E+0l 19.74 9.38E+0l 1. 73 F 11 968.55 1933 - 1943 1937.33 3.25E+0l 16.14 6 . 96E+0l 1. 82 F 12 1120.16 2234 - 2247 2240.51 2 . 72E+0l 14.38 6.58E+0l 1. 90 F 13 1331 . 92 2659 - 2670 2663 . 98 3.17E+0l 13.54 4.36E+0l 1. 43 F 14 1460.45 2914 - 2930 2921.01 5.25E+02 46.28 l.90E+0l 2 . 46 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:39:31AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76 .11 2.21E+02 60.89 2 . 21E+0 2 6.09E+0l F 2 185 . 54 5.44E+0l 33.39 5.44E+0l 3.34E+0l F 3 238.55 3 . 05E+02 44 . 69 3.05E+02 4.4 7E+0l F 4 295 .17 l.13E+02 30 . 18 l.13E+02 3.02E+0l F 5 338. 1 3 4.65E+0l 23.28 4.65E+0l 2 . 33E+0l F 6 351 . 71 1. 72E+02 33 . 00 8.36E+0l 3 . 72E+0l 8 . 84E+Ol 4.97E+0l F 7 582.98 9.79E+0l 25 . 38 9.79E+Ol 2.54E+0l F 8 609 . 23 l.16E+02 26.18 4.12E+0l 2.42E+0l 7.49E+0l 3.57 E+0l F 9 661. 40 1.66E+02 29.40 6 . 61E+0l 2 . 54E+0l 1.00E+02 3 . 88E+0l F 10 910.80 6.20E+0l 19.74 6 . 20E+0l l.97E+0l F 11 968.55 3 . 25E +0l 16.14 3.25E+0l 1.61E+0l F 12 1120.16 2.72E+0l 14.38 2. 7 2E+0l l.44E+0l F 13 1331.92 3.17E+0l 13.54 3.17E+0l 1.35E+0l F 14 1 460.45 5.25E+02 46.28 5 .63E+0l 1 . 71E+0l 4.69E+02 4 . 94E+Ol

1/15/2019 7:39:41AM Page 3 of6 Analysis Report for L 1-SUB-TDS-FSGS-009-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0 . 98 1460 . 75

• 10.67 5 . 16E+OO 6.14E-Ol CS- 137 0 . 99 661 . 65

• 85.12 6 . 83E- 02 2 . 68E-02 PB-212 0 . 55 77 .11 17.50 238 . 63

• 44 . 60 1. 59E - Ol 2 . 47E-02 BI-214 0 . 58 609 . 31

• 46.30 8. 72E- 02 4.18E- 02 1120. 29

• 1 5.10 l. 68E- 01 8.91E- 02 1238 . 11 5.94 1377. 67 4 . 11 1407.98 2.48 1509.19 2 . 19 1764 . 49 15 . 80 PB-214 0 . 71 77 .11 10 . 70 295 . 21

• 1 9.20 l . 63E- 01 4.43E - 02 351.92

• 37 . 20 7.71E- 02 4 . 36E - 02 RA- 226 0.93 186.21

• 3 . 28 3.24E- 01 l.99E - 01 AC- 228 0 . 58 209 . 28 4 . 40 338 . 32

• 11. 40 l . 28E - 01 6.43E- 02 794 . 70 4 . 60 911 . 60

• 27 . 70 l . 74E - Ol 5 . 58E - 02 964. 60 5.20 969 . 11

• 16 . 60 l . 60E - 01 8.00E - 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/15/2019 7:39:41AM Page 4 of6 Analysis Report for L 1-SUB-TDS-FSGS-009-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-4 0 0.985 5 . 16E+00 6.14E-01 CS-137 0.990 6 . 83E- 02 2 . 68E- 02 PB-212 0 . 559 1. 59E- 01 2.47E-02 BI-214 0 . 584 1. 02£- 01 3.78E- 02 PB-214 0. 717 l. l 9E - 01 3. llE- 02 RA-226 0 . 931 3.24E-01 l . 99E- 01 AC-228 0.581 1 . 55£- 01 3 . 73E-02

?  :;: nuclide is part of an undetermined solution X  :;: nuclide rejected by the interference analysis

@  :;: nuclide contains energy lines not used in Weighted Mean A ctivity Errors quoted at 2.000sigma

1/15/2019 7:39:41AM Page 5 of6 Analysis Report for L 1-SUB-TDS-FSGS-009-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Perfomied on  : 1/15/2019 7:39:31AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 76 . 11 6 .1 4001 E- 02 13 . 77 F 7 582 . 98 2 . 71848E- 02 12 . 97 F 13 1331. 92 8 . 796 8 2E- 03 21. 38 Tol. CO- 60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(3/4) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ K-40 1460.75

• 10.67 5 . 16E+00 4. 85E- 0 1 4 . 85E - 01

+ AR- 41 1293 . 64 99 . 16 l.76E+00 5.22E+0O 5 . 22E+0O

+ CO- 60 1173 . 22 100 . 00 4.52E- 02 5 . 29E-02 5 . 44E-02 1332 .4 9 1 00.00 3.27E- 02 5 . 29E- 02

+ KR- 85 513 . 99 0 .4 3 2.60E+00 8 . 00E+00 8 . 00E+00

+ Y-88 898 . 04 93 . 70 - 2 . 46E- 02 2.28E- 02 3.98E- 02 1836.06 99 . 20 -2. 96E-02 2.28E - 02

+ NB- 94 70 2 .63 100.00 2 . 93E - 02 3.32E- 02 3 . 72E - 02 871 . 10 100.00 - 2.25E - 02 3 . 32E- 02

+ I-131 284.30 6 . 06 5 . 24E - 03 3 . 50E-02 4.74E- 01 364 .4 8 81. 20 8.29E-03 3 . 50E- 02 636 . 97 7 . 27 l . 88E- 01 4 . 77E- 01

+ CS - 134 604 . 70 97.60 - 2 . 73E- 02 4.35E- 02 4 . 42E- 02 795 . 84 85.40 l.60E - 02 4 . 35E-02

+ CS- 137 661 . 65

• 85 . 12 6 . 83E - 02 4 . 90E - 02 4.90E- 02

1/15/2019 7:39:41AM Page 6 of 6 Analysis Report for L 1-SUB-TDS-FSGS-009-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ CE- 144 80. 1 2 1.36 -3 . 8 4E-0 1 2 . 29E-01 2 . 88E+O0 133.5 1 11.09 1. 85E- 01 2.29E- 0 1

+ EU-152 121. 78 28.40 - 3 .1 5E- 03 8 . 98E-02 8 . 98E-02 3 4 4.28 26.60 - 1. 27E- 02 1.13E-01 1408 . 00 20.74 6.66E- 02 1. 78E- 01

+ EU-154 123 . 07 40 . 40 -9 . 7 1E-03 6.31E-02 6 . 31E-02 723. 30 19.70 - 4 . 64E- 02 l . 81E-01 1 27 4 .51 35.50 3 . 99E- 02 1.36E-01

+ EU-155 86.54 32 . 80 - 2 . 85E- 02 l.02E- 01 l . 02E- 01 105.31 21. 80 8 . 58E- 02 l.26E- 01

+ BI - 214 609.31

• 46 . 30 8. 72E- 02 7.77E-02 7.77E- 02 1120.29

• 15. 1 0 1. 68E- 01 2. ll E-01 1 238 . 11 5.94 2.63E- 01 9.90E-01 1377 . 67 4 . 11 - 1.37E+00 9 . 41E- 01 1 4 07 . 98 2 . 48 5 . 57E- 01 l.49E+00 1509 . 19 2 . 19 -7 . 4 9E- 01 1. 33E+00 1764 .4 9 15.80 2.05E- 01 2.92E- 01

+ PB- 214 77 .11 10.70 5.70E- 01 7 . 28E- 02 3.96E- 01 295.21

• 19.20 l . 63E- 01 7 . 28E-02 351. 92

• 3 7 .20 7. 71E-02 8 . 13E-02

+ PA- 228 89.95 22 .0 0 2.73E- 01 l . 29E- 01 2.19E - 01 93 . 35 35.00 2.37E-02 l.29E - 01 105. 0 0 16 . 30 1 . 31E-0l 2 . 49E - 0 l 129 . 22 2 . 97 3 . 03E-01 l.26E+00 338 . 32 5 . 30 5 . 79E-01 8 . 23E-01 463 . 00 13 . 80 7 .46E - 02 3.40E-0l 911. 23 16.70 4 . 37E - 0l 4 . 34E- 01

+ AM- 241 59.54 36.30 5 . 28E - 02 1.86E- 0 1 l.86E - 01

+ CM- 243 103 . 76 23 .00 8.55E - 02 l.21E-0l l . 21E - 01 228.18 10 . 60 -7.02E - 02 2 . 43E - 01 277.60 14 . 00 - 2 . 91E - 02 l . 93E - 01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 7:40:21AM Page I of7

...ftApex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-010-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYS/S Sample Identification  : L 1-SUB-TDS-FSGS-010-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.965E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/8/2018 12:20:00PM Acquisition Started  : 1/9/2018 7:31 :09AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.3 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100-4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5326 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:40:12AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:40:21AM Page 2 of7 Analysis Report for L 1-SUB-TDS-FSGS-010-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

M 1 7 4 .91 147 - 161 150.37 9.27E+Ol 38 . 89 8.76E+02 1. 38 m 2 77 .0 1 147 - 161 154.57 l . 41E+02 42.70 9.35E+02 1. 39 F 3 238 . 47 472 - 481 477.41 2.48E+02 44 . 62 6.47E+02 1. 26 F 4 295.05 586 - 596 590.54 1. 28E+02 33 . 14 4.00E+02 1. 49 F 5 338 . 09 673 - 684 676.62 6.91E+Ol 25 . 31 2.99E+02 1. 33 F 6 351 . 76 700 - 710 703.95 2.09E+02 36.09 2.90E+02 1. 64 F 7 463.02 923 - 932 926.42 2 . 20E+Ol 9.59 l.46E+02 0.55 F 8 583.17 1162 - 1173 1166 . 67 l.12E+02 25.72 1. 25E+02 1. 76 F 9 609.09 1212 - 1224 1218.52 2.03E+02 32.17 l .40E+02 1. 74 F 10 661. 4 7 1316 - 1329 1323. 25 l.99E+02 31. 75 1. 36E+02 1. 77 F 11 910 . 77 1814 - 1829 1821 . 78 6.30E+Ol 19 . 13 9.63E+Ol 1. 69 F 12 968 . 78 1933 - 1942 1937 . 78 2.85E+Ol 14 . 72 8.38E+Ol 1.16 F 13 1332 . 14 2659 - 2670 2664.42 3.36E+Ol 14.36 4.76E+Ol 1. 60 F 14 1460 . 42 2912 - 2930 2920.95 5. 71E+02 48.94 2.29E+Ol 2.37 F 15 1764.10 3524 - 3535 3528 . 27 2 . 63E+Ol 10 . 85 4.27E+OO 2.14 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:40:12AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

M 1 74.91 9.27E+Ol 38.89 9.27E+Ol 3 . 89E+Ol m 2 77 . 01 1.41E+02 42.70 1.41E+02 4.27E+Ol F 3 238 .47 2 . 48E+02 44.62 2 .48E+0 2 4.46E+Ol F 4 295.05 1. 28E+02 33.14 1. 28E+02 3 . 31E+Ol F 5 338 . 09 6.91E+Ol 25.31 6 . 91E+Ol 2.53E+Ol F 6 351. 76 2 .09E+02 36 .09 8 . 36E+Ol 3 . 72E+Ol l.25E+02 5.18E+Ol F 7 463.02 2.20E+Ol 9.59 2.20E+Ol 9 . 59E+OO F 8 583 .1 7 1 . 12E+02 25 . 72 1.12E+02 2 . 57E+O l F 9 609.09 2.03E+02 32.17 4.12E+Ol 2 . 42E+Ol l.61E+02 4.03E+Ol F 10 661. 4 7 l . 99E+02 31. 75 6.61E+Ol 2.54E+Ol 1. 33E+02 4.07E+Ol F 11 910.77 6 .30E+Ol 19 .13 6.30E+Ol 1.91E+Ol F 12 968.78 2.85E+Ol 14.72 2.85E+Ol l.4 7E+Ol F 13 1332 .14 3.36E+Ol 14 .36 3.36E+Ol l. 44E+Ol F 14 1460 . 42 5 . 71E+02 48.94 5.63E+Ol 1.71E+Ol 5.15E+02 5 . 19E+Ol

1/15/2019 7:40:21 AM Page 3 of7 Analysis Report for L1-SUB-TDS-FSGS-010-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 15 1764 . 10 2.63E+0l 10.85 1.52E+0l 9 . 80E+00 1.llE+0l 1. 4 6E+0l M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigrna NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0.98 1460.75

• 10.67 5 . 63E+00 6.47E- 0l CS-137 0 . 99 661 . 65

• 85 . 12 9 . 00E-02 2.80E- 02 PB- 212 0 . 99 77 . 11

• 17 . 50 2 . 00E- 01 6 . 18E- 02 238 . 63

• 44.60 1.28E- 01 2 . 40E-02 BI-214 0.54 609.31

• 46 . 30 l . 87E-01 4.77E - 02 1120 . 29 15 . 10 1238 . 11 5.94 1377 . 67 4 .11 1407.98 2 . 48 1509.19 2 . 19 1764.49

• 15 . 80 9 . 62E - 02 l.27E-01 PB- 21 4 0.99 77 .11

• 10.70 3 . 28E - 01 l.0lE - 01 295.21

• 19.20 l.84E-01 4 . 84 E- 02 351. 92

• 37.20 1. 08E- 01 4.52E - 02 AC-228 0.58 209 . 28 4 . 40 338 . 32

• 11. 40 l . 88E-01 6.97E - 02 794.70 4.60 911.60

• 27.70 l . 75E- 01 S . 38E- 02 964.60 5 . 20 969 .11

• 16 . 60 l . 40E - 01 7.25E- 02

1/15/2019 7:40:21 AM Page 4 of7 Analysis Report for L 1-SUB-TDS-FSGS-010-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

• ::: Energy line found in the spectrum.

- ::: Manually added nuclide.

? ::: Manually edited nuclide.

@ ::: Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0 . 982 5.63E+OO 6.47E-01 CS-137 0 . 995 9 . 00E-02 2 . 80E-02 PB-212 0 . 997 1. 27E- 01 2 .2 5E-02 BI-214 0.544 1. 7 5E- 01 4 . 46E - 02 PB-214 0.996 1.42E-01 3.16E-02 AC-228 0 . 585 1 .70E-Ol 3 . 67E-02

?  ::: nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@  ::: nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:40:21AM Page 5 of7 Analysis Report for L 1-SUB-TDS-FSGS-010-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:40:12AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 1 74 . 91 2 . 57600E- 02 20 . 97 F 7 463 . 02 6 . lll 70E- 03 2 1. 80 Tol. SB- 125 PA- 228 F 8 583 . 17 3.10089E- 02 11. 52 F 13 1332 . 14 9 . 33 4 07E- 03 21.37 Tol. CO- 60 M :::: First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCilgrams) (pCl/grams)

(keV)

+ K-40 1460.75

• 10 . 67 5.63E+00 4.95E- 01 4 . 95E- 01

+ AR-41 1293 . 64 99.16 2 . 68E+0l 8.70E+01 8 . 70E+0l

+ CO-60 1173 . 22 100 . 00 4 . 72E - 02 5 . 18E-02 5.99E - 02 1332 . 49 100.00 2 . 50E - 02 5 . 18E- 02

+ KR-85 513.99 0.43 7 . 54E+00 8 . 76E+00 8.76E+00

+ Y-88 898.04 93.70 - l.96E- 02 2 . lSE-02 4 . 13E- 02 1836 . 06 99.20 -3.35 E-02 2 . lSE- 02

+ NB- 94 702 . 63 100.00 2 . 39E-03 3.47E-02 3 . 47E-02 871.10 100 . 00 - l . 21E-02 4.16E- 02

+ I - 131 284 . 30 6.06 2.S0E-01 3.63E- 02 5.12E-01 364 . 48 81. 20 - 4 . 47E - 03 3 . 63E-02

1/15/2019 7:40:21 AM Page 6 of7 Analysis Report for L 1-SUB-TDS-FSGS-010-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCilgrams) (pCilgrams)

(keV)

I-131 636.97 7.27 - 4.29E-02 3.63E-02 4.85E-01

+ CS-1 34 604.70 97 . 60 -3.16E-03 4. 57E-02 4 . 90E-02 795.84 85.40 -1. 43E-02 4 . 57E-02

+ CS-137 661 . 65

• 85.12 9 . 00E-02 4.73E-02 4 . 73E- 02

+ CE-144 80.12 1. 36 -l.17E+00 2 . 37E-01 3.02E+00 133.51 11.09 5.94E- 02 2.37E-01

+ EU-152 121.78 28.40 -8.04E-03 9.49E-02 9 .4 9E-02 344.28 26.60 - 1. 76E- 0 1 1. 22E-0 1 1408.00 20.74 1.37E-01 l . 92E-01

+ EU-154 123 . 07 40 . 40 -9.54E-03 6.69E-02 6 . 69E-02 723.30 19.70 5.03E-02 l . 91E-01 1274.51 35.50 l . 00E-01 l.35E-0l

+ EU-155 86.54 32.80 -8.37E-02 1. 03E-01 l.03E- 01 105 . 31 21. 80 -3.68E-02 l.26E- 01

+ BI-214 609.31

• 46.30 1.87E-01 7.65E-02 7 . 65E-02 1120.29 15.10 3.70E-01 3 . 85E-01 1238 .11 5.94 l.08E+00 1. 04E+00 1377. 67 4 .11 9.22E-02 9.34E-01 1407.98 2.48 l.15E+00 l . 61E+00 1509 . 19 2 . 19 8.84E- 01 l.59E+00 1764.49

• 15.80 9.62E-02 2.12E- 01

+ PB- 214 77 .11

• 1 0.70 3 . 28E-01 8.21E-02 2 . 39E-01 295.21

• 19.20 l.84E-01 l .07E-01 351. 92

• 37.20 l . 08E-01 8.21E-02

+ PA-228 89.95 22.00 2 . 46E- 01 l.65E-01 2. 7 9E-0l 93.35 35.00 3.66E- 02 l.65E- 01 105.00 16.30 6.47E-02 3.14E-0l 129 . 22 2.97 1. 20E+00 l.69E+00 338.32 5.30 1 . 66E- 01 1 .0 8E+00 463 . 00 13. 80 -9.58E-02 4.34E-01 91 1.23 16. 70 3.65E- 01 5. 3 6E-0 1

+ AM- 241 59.54 36 . 30 l.lOE-01 1.96E- 01 1 . 96E-01

+ CM-243 103.76 23.00 -7.30E-02 1 . 20E-01 l.20E-0 l 228.18 10.60 5 . 7 7E-02 2 . 50E-01 277.60 14.00 -3.37E-02 2.04E-0l

+

. = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 7:40:21AM Page 7 of7 Analysis Report for L1-SUB-TDS-FSGS-010-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

1/15/2019 7:41:04AM Page I of7

,.Apex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-011-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FSGS-011-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.858E+02 grams Facility  : Dairytand_NPP Sample Taken On  : 1/8/2018 12:26:00PM Acquisition Started  : 1/9/2018 9:07:41 AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.8 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5327 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:40:55AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7 :41:04AM Page 2 of7 Analysis Report for L 1-SUB-TDS-FSGS-011-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.63 147 - 161 153.81 2 . 68E+02 60 . 30 1. 31E+03 2.86 M 2 238.48 471 - 491 477.43 3.15E+02 45 . 13 4 . 44E+02 1. 52 m 3 2 41. 92 471 - 491 484.30 7 .4 9E+Ol 27.82 4.12E+02 1. 53 F 4 295.02 585 - 595 590.49 7. 71E+Ol 26.09 3 . 32E+02 1.12 F 5 351.89 698 - 710 704.21 1 . 68E+02 31. 32 2 .75E+02 1. 33 F 6 583.05 1 1 59 - 1173 1166.45 1 . 05E+02 24.45 1.44E+ 02 1. 68 F 7 60 9 . 11 1213 - 1222 1218 .5 6 1.08E+02 25.21 1 . 06E+ 02 1. 61 F 8 661.34 1319 - 1327 1322.99 1.22E+02 25.91 9.61E+ Ol 1. 45 F 9 9 1 1.10 1817 - 1828 1822.43 6.38E+Ol 20 .0 5 6.93E+Ol 2.24 F 10 968. 72 1933 - 1943 1937.66 2.26E+Ol 13 .13 6.12E+Ol 1. 34 F 11 1460.47 2910 - 2928 2921 . 06 5 . 63E+02 48 .05 1.90E+Ol 2.37 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:40:55AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.63 2 . 68E+02 60.30 2.68E+02 6.03E+Ol M 2 238.48 3.15E+02 45 . 13 3 . 15E+02 4.51E+Ol m 3 241 . 92 7.49E+Ol 27.82 7.49E+Ol 2 . 78E+Ol F 4 29 5 .02 7.71E+Ol 26.09 7. 71E+Ol 2.61E+Ol F 5 351.89 1.68E+02 31. 32 8 . 36E+Ol 3. 72E+Ol 8.40E+Ol 4 . 86E+Ol F 6 583.05 1 . 05E+02 24 . 45 1 . 05E+02 2 . 44E+ Ol F 7 609 . 11 1. 08E+02 25.21 4.12E+Ol 2.42E+Ol 6.67E+Ol 3 . 50 E+Ol F 8 661.34 1. 22E+02 25.91 6 . 61E+Ol 2 . 54E+Ol 5.62E+Ol 3.63E+Ol F 9 911.10 6 . 38E+Ol 20.05 6.38E+Ol 2 . 00E+Ol F 10 968 . 72 2.26E+Ol 13.13 2.26E+Ol 1. 31E+Ol F 11 1460.47 5 . 63E+02 48.05 5.6 3 E+Ol 1 . 71E+ Ol 5.06E+02 5 . lOE+Ol

=

M First peak in a multiplet region

=

m Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2.000sigma

1/15/2019 7:4 1:04AM Page 3 of7 Analysis Report for L 1-SUB-TDS-FSGS-011-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\ Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCl/grams) Uncertainty K- 40 0 . 98 1460 . 75

• 10 . 67 5 . 59E+O0 6 . 44E- 01 CS - 137 0 . 98 661. 65

• 85 . 12 3.85E- 02 2.49E- 02 PB- 212 0.98 77 . 11

• 17 . 50 3.87E-01 9.0SE-02 238 . 63

• 4 4.60 l.65E- 01 2 . SlE- 02 BI - 214 0 . 34 609 . 31

• 46 . 30 7 . 79E - 02 4. llE- 02 1120 . 29 15.10 1238 .11 5. 94 1377 . 67 4.11 1407 . 98 2 . 48 1509.19 2 . 19 1764 . 49 15 . 80 PB- 214 0.99 77 .11

• 10.70 6.33E-0l l.48E- 01 295 . 21

• 19.20 l.12E - 01 3 . 82E- 02 351.92

• 37.20 7 . 36E- 02 4 . 28E- 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

1/1 5/2019 7:41:04AM Page4 of7 Analysis Report for L 1-SUB-TDS-FSGS-011-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.988 5.59E+00 6.44E-01 CS-137 0.985 3.85E-02 2. 49E-02 PB-212 0.987 1. 7 6E-01 2.42E-02 BI-214 0.346 7.79E-02 4. llE-02 PB-214 0 . 992 1 . 04E-01 2.80E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:41 :04AM Page 5 of7 Analysis Report for L 1-SUB-TDS-FSGS-011-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:40:55AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (ke V) Peak Size (CPS) Uncertainty Type Nuclide m 3 241 . 92 2.07953£- 02 18 . 58 F 6 583 . 05 2 . 90330£- 02 11. 70 F 9 911.10 1 . 77138E- 02 15. 72 Tol. AC-228 PA- 228 F 10 968. 72 6 . 28759E - 03 29.01 AC - 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCUgrams) (pCl/grams)

(keV)

+ K- 40 1460.75

• 10 . 67 5 . 59E+00 4.93E- 01 4 . 93E- 01

+ AR-41 1293.64 99 . 16 - 3.58E+Ol l.40E+02 l . 40E+02

+ CO- 60 1173.22 100 . 00 2 . 93£- 02 4.63E- 02 5 . 00E-02 1332 . 49 100.00 3 . 06£-02 4 . 63E - 02

+ KR- 85 513.99 0 . 43 5.19E+OO 8.65E+00 8.65E+OO

+ Y- 88 898.04 93.70 2.20E- 02 2.82£- 02 4 . 47E- 02 1836.06 99.20 -2.61E-02 2.82E- 02

+ NB- 94 702.63 100.00 7 . 85E-03 3.35£-02 3 . 35£-02 871 . 10 100.00 -6.26£ - 03 3 . 98E- 02

1/15/2019 7:41:04AM Page 6 of7 Analysis Report for L 1-SUB-TDS-FSGS-011-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ I - 131 284.30 6 . 06 7.25E-02 3.67E- 02 4.81E- 01 364.48 8 1. 20 l.65E- 02 3.67E- 02 636.97 7.27 6 . 79E- 02 4. 81E- 01

+ CS- 1 34 604.70 97.60 6. llE- 02 4.28E- 02 4.28E- 02 795.84 85.40 -2 . 80E-02 4 .39E-02

+ CS - 137 661.65

• 85.12 3 . 85E- 02 4.29E- 02 4.29E-02

+ CE-144 80 . 12 1. 36 -9 . 21 E-01 2 . 28E- 01 2 . 91E+00 133.51 11.09 - 4.80E- 02 2.28 E-01

+ EU-1 52 121. 78 28 . 40 -3 . 42E- 02 9.13E- 02 9 . 13E-02 3 4 4.28 26.60 6 . 61 E- 02 l . llE- 01 1408.00 20.74 l.1 8E- 0 1 1. 79E-01

+ EU-154 123.07 40.40 -3 . 21E- 02 6.43E- 02 6 . 43E- 02 723.30 19 . 70 l . 54 E-01 l.92E- 01 127 4 .51 35.50 1. 83 E- 02 1 . 26E- 01

+ EU- 155 86.5 4 32 . 80 - 8.99E - 02 9 . 92E- 02 9 . 92E- 02 105.31 21. 80 1 . 05E-02 1. 24E- 01

+ BI - 214 609.31

• 4 6 . 30 7.79E- 02 7.05E-02 7 . 05E-02 112 0 .29 15.10 9 . 38 E-02 3.41E- 01 1238 .11 5 . 94 8 . 33 E- 01 9 . 24E- 01 1377. 67 4 .11 - 6 . 56E- 01 8.77E-01 1407 . 98 2 . 48 9 . 91E- 01 l.50E+00 1509 .1 9 2 . 19 1 . 14E- 01 l . 15E+00 1764.49 15.80 3 . 23E-01 2.87E-01

+ PB-21 4 77 .11

• 10 . 70 6 . 33E-01 8 . 34E-02 3.44E-01 295 . 21

• 19 . 20 l.12E- 01 9 . 91E- 02 351. 92

• 37.20 7 . 36E- 02 8.34E- 02

+ PA- 228 89.95 22 . 00 2 . 33E - 01 l.69E- 01 2 . 84E- 01 93.35 35 . 00 9.14E - 02 l . 69E- 01 105.00 16 . 30 l.19E-01 3.23E- 01 129 . 22 2.97 3 . 04E - 01 l . 69E+O0 338 . 32 5.30 4.92E- 0 1 l.06E+00 463 . 00 13 . 80 l.16E-01 4.45E- 01 911 . 23 16 . 70 2.27E-02 5 . 83E-0l

+ AM-241 59 . 5 4 36.30 l . 15E- 01 l . 87E- 01 1. 87E- 01

+ CM- 243 103 . 76 23 . 00 3 . 22E-04 l . 18E-01 l . 18E- 01 228.18 10 . 60 3.89E-02 2.45E-01 277 . 60 14 . 00 -1. 09E-01 1. 90E- 01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confide nce level

1/15/2019 7:41:04AM Page 7 of7 Analysis Report for L1-SUB-TDS-FSGS-011-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

1/15/2019 7:41:46AM Page I of6

__,,,Apex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-012-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYS/S Sample Identification  : L 1-SUB-TDS-FSGS-012-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.014E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 1/8/2018 12:33:00PM Acquisition Started  : 1/9/2018 10:11:11AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.2 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 -4096 Peak Area Range (in channels)  : 100 -4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5328 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:41:37AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7 :41 :46AM Page 2 of 6 Analysis Report for L 1-SUB-TDS-FSGS-012-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.58 147 - 156 153.71 2 . 31E+ 02 58.99 1 . 04E+03 4 . 32 M 2 238.58 472 - 488 4 77 . 64 3 . 55E+02 46 . 87 4 . 36E+02 1. 45 m 3 2 41. 49 472 - 4 88 4 83. 45 1.07E+02 30 . 24 3 . 99E+02 1. 45 F 4 295. 4 0 587 - 595 591 . 24 6 . 63E+0l 30.56 3.45E+02 1. 66 F 5 338.0 6 669 - 682 676 . 56 7 . 59E+ 0 l 28.33 3 .4 4E+02 1. 86 F 6 351. 79 69 5 - 710 70 4 .01 2 . 11E+02 36.63 3. 92E+02 1. 83 F 7 582.75 1160 - 1174 1165.8 4 1 . 08E+02 24.35 1.04E+02 2 . 00 F 8 60 9 . 14 1212 - 1223 12 1 8.62 l. 46E+02 28 . 40 1 . 35E+02 1. 74 F 9 661.46 1317 - 1330 1323.23 3 . 32E+02 39 . 69 1 . 76E+02 1. 64 F 10 9 1 0.89 1818 - 1827 1822 . 02 7. 36E+0l 20 . 49 7 . 92E+0l 1. 4 2 F 11 968 . 83 1 933 - 1943 1937.89 3 . 61E +0 l 1 5 . 76 7 . 13E+0l 1. 4 4 F 12 1332 . 08 2656 - 2671 266 4 .30 4. 97E +0l 1 7 . 08 5.60E+0l 2.16 F 13 1460 .4 5 2912 - 293 0 2921. 02 6 . 27 E+02 50.68 4 . 50E+00 2 . 54 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:41:37AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.58 2.3 1E+02 58.99 2 . 31E+02 5 .90E+0l M 2 238.58 3.55E+02 46.87 3 . 55E+02 4 . 69E+0l m 3 241. 49 1.07E+02 30.24 1. 07E+02 3 . 02E+0l F 4 295.40 6 . 63E+0l 30 . 56 6 .63E+0l 3.06E+Ol F 5 338.06 7. 59E+0 l 28 . 33 7.5 9E+0l 2 .83E+ Ol F 6 351.79 2 . 1 1E+02 36 . 63 8.36E+0l 3 . 72E+0l 1. 27E+02 5 . 22E+0l F 7 582 . 75 l . 08E+02 24 . 35 1.08E+02 2 . 44E+0l F 8 609 . 1 4 1.46E+02 28.40 4 . 12E+0l 2.42E+0l 1 .05E+ 02 3.73E+0l F 9 661. 4 6 3 . 32E+02 39.69 6 . 61E+0 l 2 . 54E+0l 2 . 66E+02 4 . 71E+0l F 10 910 . 89 7 . 36E+0l 20 . 4 9 7 . 36E+0 l 2 . 05E+Ol F 11 968 . 83 3.6 1E+ 0 l 15.76 3 . 6 1E+0l 1.58E+0l F 12 1332. 08 4.97E+0l 17 . 08 4.97E+0l 1 . 71E+Ol F 13 1460.45 6.27E+02 50.68 5.63E+0l 1.71E+0l 5.70E+02 5 . 35E+0l

1/15/2019 7:41:46AM Page 3 of6 Analysis Report for L 1-SUB-TDS-FSGS-012-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.98 1460.75

• 10.67 6.12E+00 6.68E-01 CS-137 0.99 661.65

• 85.12 1 . 77E-01 3.28E-02 PB-212 0 . 98 77 .11

• 17.50 3.25E-01 8.54E-02 238.63

• 44.60 1. 80E-01 2.56E-02 BI-214 0.34 609.31

• 46 . 30 l.19E-01 4.29E-02 1120.29 15.10 1238.11 5.94 1377.67 4 .11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.99 77 .11

• 10.70 5.31E-01 1. 40E-01 295.21

• 19.20 9.36E-02 4 . 34E-02 351. 92

• 37.20 l.08E-01 4.48E-02 AC-228 0.59 209.28 4.40 338.32

• 11. 40 2.03E-01 7.66E-02 794 . 70 4.60 911.60

• 27 . 70 2.0lE-01 5.67E-02 964.60 5.20 969 .11

• 16.60 l.74E-01 7.63E-02

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/15/2019 7:41:46AM Page4 of6 Analysis Report for L 1-SUB-TDS-FSGS-012-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.986 6.12E+00 6.68E-01 CS-137 0.994 l.77E-01 3.28E-02 PB-212 0.987 1. 87E-01 2.46E-02 BI-214 0.347 l.19E-01 4.29E-02 PB-214 0.990 1. 07E-01 3.0SE-02 AC-228 0.597 1.95E-01 3.91E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:41 :46AM Page 5 of6 Analysis Report for L 1-SUB-TDS-FSGS-012-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:41 :37AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (ke V) Peak Size (CPS) Uncertainty Type Nuclide m 3 241.49 2 . 97708E - 02 14 .11 F 7 582.75 3 . 01202E- 02 11. 23 F 12 1332 . 08 1.37933E- 02 17.20 Tol. CO- 60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(3/4) Activity NuclideMDA LineMDA Name (pCl/grams) (pCilgrams) (pCl/grams)

(keV)

+ K- 40 1460.75

• 10 . 67 6.12E+00 4.43E- 01 4 . 43E-01

+ AR-41 1293. 64 99.16 1 . 36E+02 2 . 10E+02 2.10E+02

+ CO- 60 1173.22 100 . 00 7.21E - 02 5 . 41E - 02 6.29E- 02 1332 . 49 100.00 6.28E- 02 5.41E- 02

+ KR-85 513 . 99 0 . 43 1 . 30E+0l 8.75E+0O 8 . 75E+00

+ Y-88 898.04 93.70 2 . 88E- 03 2.65E- 02 4 . 39E- 02 1836 . 06 99. 20 - 1. 20E-02 2.65E-02

+ NB-94 702 . 63 100 . 00 1.27E-02 3 . 47E-02 3.47E-02 871.10 100.00 - 2 . 17E- 02 3.73E- 02

+ I-131 284.30 6.06 -1 . 02E-01 3 . 64E- 02 4.98E-01 364.48 81. 20 -1 . 25E-02 3.64E-02 636 . 97 7 . 27 - 1.89E- 01 4.96E - 01

+ CS - 134 60 4 .70 97 . 60 8 . 92E-02 3.98E-02 4.62E-02 795 . 84 85.40 - 5.27E-02 3.98E-02

1/15/201 9 7:41 :46AM Page 6 of6 Analysis Report for L1-SUB-TDS-FSGS-012-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCVgrams) (pCi/grams) (pCilgrams)

(keV)

+ CS - 137 661.65

• 85.12 l . 77E-01 4 .94E - 02 4 . 94E-02

+ CE-144 80.12 1. 36 -5.64E+00 2 . 37E-01 2.95E+OO 133.51 11.09 l . 69E-01 2.37E-01

+ EU-152 121.78 28.40 -2.09E-02 9.llE-02 9. llE-02 344.28 26 . 60 -4.29E-03 1. 25E- 01 1408 . 00 20.74 l.02E-01 1. 96E-01

+ EU-154 123 . 07 40 . 40 -7.48E-03 6.41E-02 6.41E-02 723.30 19.70 7 . 47E-03 1. 96E - 0l 1274 . 51 35.50 1. 55E-02 1. 37E - 01

+ EU- 155 86 . 54 32.80 -7.25E-02 1. 04E-01 l.04E-01 105 . 31 21.80 3.9 4E- 02 1. 28E-01

+ BI-214 609.31

• 46.30 l.19E-01 7.37E- 02 7 . 37E-02 1120 . 29 15.10 l . 8 1E- 02 3.16E-01 1238 .11 5.94 -4.33E-01 9.69E-01 1377 . 67 4 . 11 -l.21E-01 8.90E-01 1407 . 98 2.48 8 . 55E-01 l . 64E+00 1509.19 2.19 1. 77E-0l l . 47E+00 1764 . 49 15.80 l.48E-01 2.85E-01

+ PB-214 77 . 11

• 10 . 70 5.31E- 01 9 . 17E- 02 2.65E-0l 295.21

• 19 . 20 9.36E-02 9.30E- 02 351. 92

• 37.20 1. 08E-01 9.17E-02

+ PA-228 89 . 95 22.00 4.89E-01 1.81E- 01 3 . 09E - 01 93 . 35 35.00 3.58E-02 1.81E-Ol 105 . 00 16.30 -8.30E - 02 3.43E-01 129.22 2.97 1. 38E-01 1.76E+00 338 . 32 5.30 1.08E-02 l.19E+00 463 . 00 13. 80 1.94E-0l 4.95E - 01 9 1 1. 23 16.70 8 . 38E-01 6 . 37E - 01

+ AM- 241 59.54 36 . 30 1. 33E-01 1. 90E- 01 1. 90E - 01

+ CM- 243 103 . 76 23 . 00 3.80E-02 1. 22E-01 1 . 22E-01 228.18 10 . 60 1.90E-02 2 . 53E-01 277 . 60 14.00 1. 4 7E-0 l 2 . 05E- 01

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence lev el

1/15/2019 7:42:30AM Page I of6 Jt'Apex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-013-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYS/S Sample Identification  : L 1-SUB-TDS-FSGS-013-SB Sample Description  ; L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.001 E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 1/8/2018 12:40:00PM Acquisition Started  : 1/9/2018 11 :12:17AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live nme  : 3600.0 seconds Real nme  : 3611.1 seconds Dead nme  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5329 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:42:21AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:42:30AM Page 2 of6 Analysis Report for L 1-SUB-TDS-FSGS-013-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 . 13 147 - 159 152 . 80 2 . 08E+02 61. 35 l . 30E+03 3.38 F 2 185 . 94 364 - 379 372 . 37 8 . 13E+0l 35.28 9.70E+02 1. 45 F 3 238.50 469 - 485 477.47 3 . 31E+02 45.95 7.01E+02 1. 62 F 4 295.06 586 - 595 590 . 57 7.93E+0l 27.43 3 . 26E+02 1. 25 F 5 337.84 672 - 682 676 . 12 5 . 70E+0l 24 . 39 2 . 88E+02 1. 31 F 6 351.74 699 - 709 703 . 92 l . 87E+02 33 . 42 2 . 33E+02 1. 54 F 7 4 62. 88 920 - 931 926.14 4.98E+0l 21. 38 1 . 50E+02 1. 95 F 8 583 . 12 1161 - 1171 1166.59 9.19E+Ol 23. 42 l.25E+02 1. 45 F 9 609.18 1212 - 1225 1218.69 l . 10E+02 25.15 l.55E+02 1. 51 F 10 661.44 1314 - 1328 1323 . 20 1 . 65E+ 0 2 29.33 l.55E+02 1. 68 F 11 785.75 1567 - 1578 1571. 78 2.22E+0l 13 . 58 6.67E+0l 1. 48 F 12 910 . 63 1816 - 1827 1 821. 51 4 . 07E+0l 17.03 8 . 67E+0l 1. 58 F 13 968.57 1933 - 1942 1937.37 2.63E+0l 16.29 8.63E+0l 1. 73 F 14 1460.40 2912 - 2928 2920 . 91 6.17E+02 50 . 85 2.99E+0l 2.36 M :: First peak in a multiplet region m :: Other peak in a multiplet region F :: Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:42:21AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76 .13 2.08E+02 61. 35 2.08E+02 6.14E+0l F 2 185.94 8 .13E+0l 35.28 8 .13E+0l 3.53E+0l F 3 238.50 3.31E+02 45.95 3.31E+02 4.59E+0l F 4 295.06 7.93E+0l 27.43 7.93E+0l 2.74E+Ol F 5 337.84 5 . 70E+0l 24 . 39 5.70E+0l 2.44E+0l F 6 351. 74 l.87E+02 33 .4 2 8.36E+Ol 3 . 72E+0l 1. 03E+02 5.00E+Ol F 7 462.88 4 . 98E+0l 21. 38 4.98E+0l 2.14E+Ol F 8 583.12 9 . 19E+0l 23.42 9.19E+0l 2.34E+0l F 9 609 . 18 l . 10E+02 25.15 4.12E+0l 2 . 42E+0l 6 . 91E+0l 3 . 49E+0l F 10 661.44 l.65E+02 29.33 6.61E+0l 2.54E+0l 9.92E+0l 3.88E+0l F 11 785.75 2.22E+0l 13.58 2.22E+0l 1. 36E+0l F 12 910 . 63 4.07E+0l 17 . 03 4.07E+0l l. 70E+0l F 13 968 . 57 2.63E+0l 16. 29 2.63E+0l l.63E+0l F 14 1460.40 6.17E+02 50.85 5.63E+0l 1.71E+0l 5 . 61E+02 5.37E+0l

1/15/2019 7:42:30AM Page 3 of6 Analysis Report for L 1-SUB-TDS-FSGS-013-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence {keV) (pCl/grams) Uncertainty K- 40 0 . 98 1460 . 75

• 10 . 67 6.lOE+OO 6 . 75E- 01 CS- 137 0 . 99 661 . 65

• 85 . 12 6 . 69E- 02 2.64E- 02 PB- 212 0 . 95 77 .11

• 17.50 2 . 99E- 01 9.03E- 02 238 . 63

• 44.60 1. 71E- 01 2 . 53E- 02 BI - 214 0 . 34 609 . 31

• 46 . 30 7.95E- 02 4.04E- 02 1120.29 15.10 1238 .11 5 . 94 1377 . 67 4 .11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB- 214 0 . 97 77 .11

• 10 . 70 4 . 89E- 01 l . 48E-01 295 . 21

• 19 . 20 1.13E-01 3.96E- 02 351. 92

• 37 . 20 8.92E- 02 4 . 34E - 02 RA- 226 0.98 186.21

• 3 . 28 4 . 79E- Ol 2 . 09E - 01 AC- 228 0.56 209 . 28 4 . 40 338.32

• 11. 40 l.55E - 01 6 . 66E- 02 794.70 4 . 60 911 . 60

• 27.70 l.13E- 01 4.74E - 02 964 . 60 5 . 20 969 . 11

• 1 6.60 1. 28E - Ol 7.97E-02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean A ctivity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/15/2019 7:42:30AM Page4 of6 Analysis Report for L1-SUB-TDS-FSGS-013-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-4 0 0.980 6.l0E+00 6.75E-01 CS-137 0.993 6.69E- 02 2 . 64E-02 PB-212 0 . 955 1.75E- 01 2.44E- 02 BI-214 0.348 7.95E-02 4.04E-02 PB-214 0 . 972 1.06E- 01 2.87E- 02 RA-226 0.988 4.79E-01 2.09E-01 AC-228 0.560 1. 27E-01 3.48E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:42:30AM Page5 of6 Analysis Report for L 1-SUB-TDS-FSGS-013-SB L1-SUB-TOS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:42:21AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 7 4 62 . 8 8 1 . 38293£- 02 21. 47 Tol. PA- 228 F 8 583 . 12 2 . 55278E- 02 1 2.74 F 11 785 . 75 6 . 17509E- 03 30.55 Tol. BI - 212 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(3/4) Activity NuclideMDA LineMDA Name (pCJ/grams) (pCl/grams) (pCUgrams)

(keV)

+ K- 40 1460 . 75

• 10.67 6.l0E+00 5.05E- 01 5 . 0SE-01

+ AR- 41 1293 . 64 99.16 8 . 50E+0l 2.92E+02 2.92E+02

+ CO- 60 1173 . 22 100.00 2 . 95E- 02 4 . 62E- 02 5.86E - 02 1332.49 100 . 00 3 . llE - 02 4 . 62E-02

+ KR- 85 513.99 0.43 9 . 30E+00 8.78E+00 8 . 78E+O0

+ Y-88 898 . 04 93.70 l . 14E- 02 3 . 28E-02 4 . 21E-02 1836 . 06 99.20 3 . 38E - 03 3 . 28E-02

+ NB- 94 702 . 63 100.00 - 2 . 63E- 02 3 . 40E- 02 3.40E-02 871.10 100.00 - 4.92E- 02 3 . 91E- 02

+ I - 131 284.30 6.06 - 3.53E- 01 3 . 62E-02 4 . 85E-01 364 . 48 81 . 20 5.02E- 03 3.62E- 02 636 . 97 7.27 -1.19E-01 4.76E- 01

1/15/ 2019 7:42:30AM Page 6 of6 Analysis Report for L 1-SUB-TDS-FSGS-013-S8 L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ CS - 134 60 4 .70 97 . 60 1. 38E- 02 4 . 32E-02 4.4 2E- 02 795 . 84 85 . 40 2 . 41E- 02 4.32E- 02

+ CS - 137 661 . 65

• 85 . 12 6 . 69E- 02 4 . 92E- 02 4.92E- 02

+ CE- 1 44 80.12 1. 36 - 1.30E+00 2.35E-01 2 . 92E+00 133.51 1 1.09 1.03E- 01 2.35E- 01

+ EU-152 121. 78 28 . 40 - 3 . 89E- 02 9 . 05E-02 9.05E-02 344.28 26.60 - 6. 94E-02 1.18E- 01 1 40 8. 00 20 . 7 4 1 . 58E- 01 1. 99E-01

+ EU-1 54 123.07 4 0 .4 0 - 1 . 05E- 02 6 . 38E- 02 6.38E - 02 723 . 30 19 . 70 1 . 65E- 0 1 1 . 92E - 01 127 4. 5 1 35 . 50 -8 . 51E- 02 1. 30E-01

+ EU- 155 86 . 54 32 . 80 - 1.39E- 02 1.0lE- 01 1 . 0lE-01 105.31 2 1. 80 - 1 . 97E- 02 1.24E-01

+ BI - 21 4 609.3 1

• 4 6 . 30 7.95E- 02 7.90E- 02 7 . 90E- 02 1120.29 1 5.10 3 . 64E- 01 3.39E- 01 1238 . 11 5 . 94 4.29E-01 9.48E- 01 137 7. 67 4 .11 - 5 . 95E- 02 8.83E- 01 1407 . 98 2 . 48 1.32E+00 l . 66E+00 1509.19 2 . 19 9.00E- 0 1 l.69E+00 1764 . 49 1 5 . 80 4 . 56E- 0 1 3 .1 5E- 01

+ PB- 2 1 4 77 . 11

• 10.70 4.89E- 0 1 7. 7 9E-02 3 . 27E- 01 295.21

• 19.20 1 . 13E- 01 9 . 42E- 02 35 1 .92

• 37.20 8 . 92E- 02 7. 79E-02

+ PA- 228 89.95 22. 0 0 1.77E-01 1. 79E-01 3.02E- 01 93 . 35 35 . 00 2 . 62E- 02 1 . 79E- 01 105.00 1 6 . 30 3.86E-02 3 .4 5E-01 12 9. 22 2 . 97 - 3 . 96E- 01 1.77E+00 338.32 5 . 30 1. 7 5E- 01 1.17E+00 4 63.00 13 . 80 4 . 29E- 0 1 4 . 84E- 0 1 911.23 16 . 70 9 . 07E- 01 5 . 63E- 0 1

+ AM-241 59.54 36.30 1.38E- 01 1.93E- 01 1.93E- 0 1

+ CM-2 4 3 103.76 23.00 -3 . 39E-02 1.19E- 01 1.19E-01 228.18 10.60 - 2 . 28£- 01 2 . 40E- 0 l 277 . 60 14 . 00 1.06E- 01 1. 98E-0 1

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 7:43:11AM Page I of7

~~~~pex-Gamma Analysis Report for L 1-SUB-TDS-FSGS-014-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FSGS-014-SB Sample Description  : L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.806E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/8/2018 12:45:00PM Acquisition Started  : 1/9/2018 12:13:01PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.7 seconds Dead Time  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5330 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 7:43:02AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 7:43: 11AM Page 2 of7 Analysis Report for L 1-SUB-TDS-FSGS-01 4-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

M 1 74.92 146 - 162 150.39 1. 0 4E+02 37 . 19 8.68E+02 1.28 m 2 77.17 146 - 162 154.88 1. 29E+02 38.80 7 . 36E+02 1. 29 M 3 87 . 33 171 - 193 175.21 5.31E+0l 35.39 8.04E+02 1. 49 m 4 92.91 171 - 193 186.36 9 . 79E+0l 39 .11 7.79E+02 1.50 F 5 238.46 4 69 - 481 477 . 39 2.85E+02 46 . 43 7.51E+02 1. 41 F 6 295.08 586 - 594 590 . 62 7 . 23E+0l 27.90 3 . 24E+02 1.28 F 7 338 . 12 668 - 680 676 . 68 5.79E+0l 24 . 42 3.12E+02 1. 44 F 8 351 . 75 699 - 709 7 0 3.93 l.70E+02 33 . 18 2.56E+02 1. 58 F 9 582.98 1158 - 1173 1166 . 31 1. 03E+02 24.87 l.67E+02 1. 73 F 10 609 . 16 1 215 - 1223 1218.66 l.12E+02 25 . 62 l . 08E+02 1. 66 F 11 661. 48 1315 - 1331 1323 . 27 3.67E+02 40.51 1.23E+02 1. 92 F 12 910 . 81 1816 - 1828 1821.86 7.33E+0l 20 . 90 8 . 51E+0l 1. 90 F 13 968 . 61 1931 - 1942 1937.44 2 . 51E+0l 14 . 69 9 . 25E+0l 1. 44 F 14 1332 . 05 2658 - 2670 266 4. 24 4 . 50E+0l 16 . 84 5.25E+0l 2 . 09 F 15 1460 . 46 2911- 2930 2921.03 5.29E+02 46 . 55 3.48E+0l 2.45 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 7:43:02AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

M 1 74.92 1. 04E+02 37.19 1 . 04E+02 3.72E+Ol m 2 77.17 1.29E+02 38.80 1 . 29E+02 3 . 88E+0l M 3 87 . 33 5.31E+0l 35 . 39 5.31E+0l 3 . 54E+0l m 4 92.91 9.79E+0l 39 . 11 9 . 79E+0l 3 . 91E+0l F 5 238 . 46 2 . 85E+02 46 . 43 2.85E+02 4.64E+Ol F 6 295.08 7.23E+0l 27.90 7.23E+0l 2 . 79E+Ol F 7 338.12 5.79E+0l 24 . 42 5.79E+0l 2 . 44E+0l F 8 35 1 . 75 1 . 70E+02 33 . 18 8.36E+0l 3.72E+0l 8.62E+0l 4.99E+0l F 9 582.98 l.03E+02 24.87 1.03E+02 2.49E+0l F 10 609 . 16 1.12E+02 25.62 4.12E+0l 2.42E+0l 7 .07E+0l 3 . 53E+0l F 11 661.48 3.67E+02 40.51 6.61E+0l 2.5 4E+0l 3.01E+02 4 . 78E+0l F 12 910 . 81 7.33E+0l 20 . 90 7 . 33E+0l 2 . 09E+0l F 13 968.61 2 . 51E+0l 1 4.69 2.51E+0l 1 . 47E+Ol F 14 1332 . 05 4.50E+0l 16 . 84 4.50E+0l 1.68E+Ol

1/15/2019 7:43:11AM Page 3 of7 Analysis Report for L1-SUB-TDS-FSGS-014-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 15 1460.46 5 . 29E+02 46 . 55 5.63E+0l l . 71 E+0l 4 . 73E+02 4 . 96E+0l M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-4 0 0 . 98 14 6 0 . 75

• 10 . 67 5 . 26E+00 6 . 23E- 01 CS- 137 0 . 99 661 . 65

• 85 . 12 2 . 0 8E-01 3 .4 8E - 02 PB- 212 0 . 99 77 .11

• 17.50 1.8 4E- 01 5 . 69E - 02 238 . 63

• 44 . 60 l . 50E- 01 2 . 56E - 02 BI- 214 0 . 34 609.31

• 46 . 30 8 . 30E- 02 4 .1 7E - 02 11 20 . 29 15 . 10 1238 . 11 5. 94 1377 . 67 4 .11 1407.98 2 . 48 1 509 . 19 2 .19 1764. 49 15.80 PB- 21 4 0 . 99 77 .11

• 1 0 . 70 3 . 0lE- 01 9 . 31 E- 02 295 . 21

• 19. 20 l.05E- 01 4. l 0E - 02 35 1 .92

• 37 . 20 7 . 59E - 02 4 .4 1E- 02 AC - 228 0 . 58 209 . 28 4 . 40 338.32

• 11. 40 l.61E - 0l 6.82E- 02 79 4 .70 4 . 60 911. 60

• 27 . 70 2 . 07E- 01 5 . 98E- 02 96 4 . 60 5 . 20 969 . 11

• 16 . 60 l . 25E- 01 7.34E- 02

1/15/2019 7:43:11AM Page 4 of7 Analysis Report for L 1-SUB-TDS-FSGS-014-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K- 4 0 0 . 987 5 . 26E+O O 6 . 23E- 0 1 CS- 137 0.995 2 . 08E - 01 3.48E- 02 PB- 212 0.997 1. 4 7E- 01 2 . 35E- 02 BI- 214 0.348 8.30E - 02 4 . 17E-02 PB- 21 4 0 . 997 8 . 89E- 02 2 . 88E-02 AC-228 0 . 584 1 . 70E- 01 3.83E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 7:43:11AM Page 5 of7 Analysis Report for L1-SUB-TDS-FSGS-014-SB L1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 7:43:02AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 1 74.92 2.8932 1£ - 02 17.85 M 3 87 . 33 1.47604£-02 33 . 30 Tol. EU - 155 m 4 92. 91 2.72038£- 02 19. 97 Tol. PA-228 F 9 582 . 98 2 . 85228£-02 12 . 11 F 14 1332 . 05 1.25099£- 02 18.69 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCUgrams) (pC/lgrams) (pC/lgrams)

(keV)

+ K-40 1460.75

• 10 . 67 5 . 26E+00 5.35E-01 5 . 35E- 01

+ AR-41 1293. 64 99 . 16 -1 . 31£+02 4 . 04E+02 4.04E+02

+ CO-60 1173 . 22 100.00 2.46£- 02 5 . 62£-02 5.85E- 02 1332 . 49 100 . 00 7 . 89E- 02 5.62E- 02

+ KR- 85 513.99 0 . 43 6 . 39E+00 8.83E+00 8.83E+00

+ Y- 88 898.04 93.70 -2.40E - 02 2.84E- 02 4.05E-02 1836.06 99.20 1. 96E - 03 2.84E- 02

+ NB-94 702 . 63 100 . 00 1 . 28E-03 3.70£- 02 3.70E-02 871 . 10 100 . 00 -5.27£-02 3 . 70E-02

1/15/2019 7:43:11AM Page 6 of 7 Analysis Report for L 1-SUB-TDS-FSGS-014-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nucllde Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams)

(keV}

+ I-131 28 4. 30 6. 06 2.63E - 0 1 3 . 82E-02 5 . 20E-0 1 364 .4 8 81.20 -l . 2 4E- 02 3.82E- 02 636 . 97 7 . 27 -2 . 99E-02 4 . 82E- 01

+ CS- 134 60 4. 70 97 . 60 7 . 47E- 02 4 . 41E- 02 4.56E- 02 795.84 85.40 3.81E- 03 4 .41E- 02

+ CS-137 661.65

• 85 . 12 2 . 08E- 01 4 . 82E- 02 4 . 82E- 02

+ CE- 144 80.12 1. 36 2 . 04E- 01 2 . 30E-Ol 2.93E+OO 133.5 1 1 1.09 - 2 . 13E- 01 2 . 30E- 01

+ EU-152 121. 78 28 . 40 - 1. 59E- 02 9.23E- 02 9.23E- 02 34 4 .28 26 . 60 -l.46E-O l l . 17E-01 1 408 . 00 20.74 l.41E- 01 l . 90E-Ol

+ EU-154 1 23.07 40.40 - 4.64E- 03 6.48E- 02 6 . 48E- 02 723.30 19.70 l.23E- 0 1 l.82E- 01 1274.51 35.50 3. 1 9E- 02 1. 31E- 01

+ EU- 155 86.54 32 . 80 7.62E- 03 l . OOE-01 l . OOE-01 105 . 31 21. 80 - 2.92E - 02 l.28E-01

+ BI-21 4 609 . 31

• 4 6 . 30 8.30E - 02 7.05E- 02 7 . 05E-0 2 1120.29 15. 1 0 8.02 E-02 3.53E- 01 1238 .11 5 . 94 - 5.02E-01 9.65E - 01 1377.67 4 . 11 -5.0lE-01 9.30E - 01 1 407.98 2 . 48 l . 18E+OO l . 59E+OO 1509 . 19 2.19 3.53E-01 l . 62E+OO 1764.49 15 . 80 l . 33E-01 2.51E-01

+ PB- 2 1 4 77 . 11

• 10 .7 0 3.0lE- 01 8.lOE- 02 2.16E- 01 295 . 21

• 19 . 20 l.05E - 01 9 . 30E - 02 351. 92

• 37 . 20 7.59E-02 8.lOE- 02

+ PA- 228 89.95 22 . 00 l . 24E-02 l . 84E- 01 3 . 14E- 0 1 93 . 35 35. 00 - 4 . 02E - 02 l . 84E-01 105 . 00 16 . 30 - 7.51E - 02 3.65E-01 129 . 22 2 . 97 -6 . 75E- 02 l. 84E+00 338 . 32 5 . 30 1.05E+00 1. 21E+OO 463 . 00 13 .80 - 4.36E-Ol 4 . 86E - 01 911 . 23 16 . 70 6.68E-01 6 . 52E-01

+ AM- 2 41 59 . 54 36 . 3 0 3 . 08E - 02 1. 88E-01 l.88E-01

+ CM-243 103 . 76 23 . 00 7 . 23E-02 l .23E- 01 1.23E- 01 228 . 18 10 . 60 - 7.73E - 02 2.53E - 01 277 . 60 14.00 -l . 53E - 01 2 . 00E-0 1

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 7:43:11AM Page 7 of7 Analysis Report for L 1-SUB-TDS-FSGS-014-SB L 1-SUB-TDS COMBINEDTB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

1/15/2019 8:08:22AM Page 1 of 7

...t,Apex-Gamma Analysis Report for L 1-SUB-TDS-FJGS-001-SB BIASED SAMPLE GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FJGS-001-SB Sample Description  : BIASED SAMPLE Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.576E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/10/2018 12:36:00PM Acquisition Started  : 1/12/2018 6:49:51AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.1 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100-4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5331 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 8:08:13AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 8:08:22AM Page 2 of7 Analysis Report for L 1-SUB-TDS-FJGS-001-SB BIASED SAMPLE Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 . 29 147 - 160 153.12 2 . 29E+02 59 . 67 1. 21E+03 3 . 14 F 2 238.54 469 - 485 477.55 3.83E+02 48.08 6.97E+02 1. 55 F 3 295.03 585 - 594 590.51 9.41E+Ol 28.58 2.48E+02 1. 63 F 4 338.38 672 - 683 677.19 7.lOE+Ol 26. 94 2.97E+02 1. 66 F 5 351.74 695 - 709 703.90 l.36E+02 30.66 3 . 69E+02 1. 50 F 6 582.91 1163 - 1173 1166.16 9.36E+Ol 23.33 l.20E+02 1. 47 F 7 609.24 1212 - 1224 1218 . 81 l . 06E+02 24 . 67 1.24E+02 1. 77 F 8 661.46 1316 - 1329 1323 . 23 l.82E+02 31. 06 l.61E+02 1. 71 F 9 910.85 1817 - 1827 1821.95 5 . 97E+Ol 19.43 7.15E+Ol 1. 76 F 10 1460.50 2913 - 2930 2921.11 5.67E+02 49.37 5.39E+Ol 2.39 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 8:08:13AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.29 2.29E+02 59.67 2 . 29E+02 5.97E+Ol F 2 238.54 3.83E+02 48 . 08 3.83E+02 4.81E+Ol F 3 295 . 03 9.41E+Ol 28.58 9 . 41E+Ol 2.86E+Ol F 4 338 . 38 7.lOE+Ol 26.94 7.lOE+Ol 2 . 69E+Ol F 5 351. 74 1.36E+02 30.66 8.36E+Ol 3 . 72E+Ol 5.22E+Ol 4 . 82E+ Ol F 6 582 . 91 9 . 36E+Ol 23.33 9.36E+Ol 2 . 33E+Ol F 7 609 . 24 l.06E+02 24 .67 4.12E+Ol 2 . 42E+Ol 6.44E+Ol 3 . 46E+Ol F 8 661. 4 6 1 . 82E+02 31. 06 6.61E+Ol 2 . 54E+Ol l .16E+02 4 . 0lE+Ol F 9 910.85 5 . 97E+Ol 19 . 43 5.97E+Ol l.94E+ Ol F 10 1460 . 50 5 . 67E+02 49.37 5.63E+Ol 1 . 71E+Ol 5.11E+02 5.23E+Ol

=

M First peak in a multiplet region

=

m Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2.000sigma

1/15/2019 8:08:22AM Page 3 of7 Analysis Report for L 1-SUB-TDS-FJGS-001-S8 BIASED SAMPLE NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 99 1 460.75

• 10.67 5 . 81E+00 6 . 76E- 01 CS - 137 0 . 99 661. 65

• 85 . 12 8 . 17E- 02 2.86E- 02 PB- 212 0 . 96 77 . 11

• 17 . 50 3.43E- 01 9 . 20E- 02 238 . 63

• 44.60 2.06E - 0 1 2.80E- 02 BI - 214 0 . 34 609 . 31

• 46.30 7 . 75E - 02 4.18E- 02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407.98 2.48 1509 . 19 2 . 19 1764.49 15.80 PB-214 0 . 97 77 . 11

• 10 . 70 5.61E- 01 1. 50E-01 295.21

• 19 . 20 1 . 41E- 0l 4 . 32E - 02 35 1. 92

• 37 . 20 4 . 71E- 02 4 . 35E - 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold= 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K- 40 0.990 5.81E+0O 6.76E-01 CS-137 0.994 8.17E-02 2.86E- 02

1/15/2019 8:08:22AM Page4 of7 Analysis Report for L 1-SUB-TDS-FJGS-001-SB BIASED SAMPLE Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

PB-212 0.969 2.13E-0l 2.68E-02 BI-214 0.349 7.75E-02 4.18E-02 PB-214 0.978 9.89E-02 3.0lE-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 8:08:22AM Page 5 of7 Analysis Report for L1-SUB-TDS-FJGS-001 -SB BIASED SAMPLE UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 8:08:13AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 338.38 1 . 97313E- 02 18 . 96 Tol. AC- 228 PA- 228 F 6 582.91 2.60076E- 02 12.46 F 9 910 . 85 l . 6570 1E- 02 1 6.29 Tol. AC - 228 PA- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCl/grams) (pCilgrams) (pCi/grams)

(keV)

+ K- 40 1460 . 75

• 10.67 5.81E+O0 5.78E-0l 5 . 78E-0l

+ AR- 41 1293 . 64 99.16 - 7 . 39E+04 5 . 15E+05 5 . 15E+05

+ CO- 60 1173 . 22 100.00 1.86E-02 5.00E- 02 5 . S0E-02 1332 . 49 100.00 4 . 45E- 02 5 . 00E-02

+ KR- 85 513. 99 0 . 43 6.32E+00 8 . S0E+00 8 . S0E+00

+ Y- 88 898 . 04 93 . 70 7 . 33E- 03 2.61 E- 02 4 .13E- 02 1836.06 99.20 - 1 . 57E - 02 2 . 61E-02

+ NB- 94 702.63 100.00 9 . 62E- 03 3 . 64E- 02 3 . 64E - 02 871.10 100 . 00 -5.04E- 03 3.98E-02

+ I - 131 284 . 30 6 . 06 - 1 . 19E-01 3 . 92E-02 5 . 24E-01 364.48 81. 20 - 1. 58E- 02 3.92E- 02

1/15/2019 8:08:22AM Page 6 of7 Analysis Report for L1-SUB-TDS-FJGS-001-SB BIASED SAMPLE Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCilgrams) (pCUgrams) (pCilgrams)

(keV)

I-131 636.97 7.27 1.44£-01 3.92£- 02 5.50£-01

+ CS-134 604 . 70 97.60 -1.62E-02 4.43£-02 4.43£-02 795.84 85.40 -l.03E-02 4.59E-02

+ CS-137 661. 65

• 85.12 8 .17E-02 5. lOE-02 5.l0E-02

+ CE-144 80.12 1. 36 - 5.58£-01 2.36£-01 2 . 96£+00 133. 51 11.09 -1. 04£-02 2.36£-01

+ EU- 152 121.78 28 .4 0 -4.30£-02 9.39£-02 9 . 39£-02 344.28 26.60 9.79£-03 1 . 24£-01 1408.00 20.74 1. 36£-01 1.82£-01

+ EU-154 123.07 40.40 -6. 72E-03 6 . 62£-02 6.62E-02 723. 30 19.70 2 . 71£-02 1.86£-01 1274.51 35.50 -1.38£-01 l.43E-01

+ EU-155 86.54 32.80 -4.38£-02 1.04£-01 1.04£-01 1 05.31 21. 80 4 . 08£- 02 1 . 30£-01

+ BI-214 609 . 31

• 46.30 7.75£-02 7 . 74£-02 7.74£-02 1120.29 15.10 2.25£-01 3.57£-01 1238 .11 5.94 3 . 70£-01 9 . 66£-01 1377.67 4 .11 4.12£-01 9.91E-01 1407.98 2.48 l.14E+00 1.52£+00 1509.19 2.19 - 1.57£-01 l.56E+00 1764.49 15 . 80 1.44£-01 2.79£-01

+ PB-214 77 .11

• 10 . 70 5.61£-01 8.61£-02 3.37£-01 295.21

• 19.20 1.41£-01 8.61£-02 351.92

• 37.20 4 . 71£-02 9.45£-02

+ PA-228 89 . 95 22.00 7.75£-01 3.48£-01 5.92£-01 93 . 35 35 . 00 -6.82£-02 3.48£-01 105.00 16.30 2.61E-0l 6.68£-01 129.22 2 . 97 3.05£-01 3.35£+00 338 . 32 5.30 1.38E+00 2.27£+00 463.00 13.80 2.47£- 01 8.85£-01 911. 23 16.70 8.96£-01 1.13£+00

+ AM-241 59.54 36 . 30 4.89£-02 1.89£-01 1.89£-01

+ CM-243 103.76 23 . 00 7.23£-02 1. 25E-01 1.25£-01 228 . 18 10.60 2.17£-01 2 . 52£-01 277.60 14.00 1.76£- 01 2.06£-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 8:08:22AM Page 7 of7 Analysis Report for L 1-SUB-TDS-FJGS-001-SB BIASED SAMPLE

1/15/2019 8:09:06AM Page I of6

_.Apex-Gamma Analysis Report for L1-SUB-TDS-FJGS-002-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FJGS-002-SB Sample Description  : L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.620E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/15/2018 9: 15:00AM Acquisition Started  : 1/15/2018 3:45:35PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live nme  : 3600.0 seconds RealTime  : 3611.2 seconds Dead nme  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 -4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5332 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 8:08:57AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 8 :09:06AM Page 2 of6 Analysis Report for L 1-SUB-TDS-FJGS-002-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 92.70 183 - 192 1 85.94 6 . 32E+Ol 34.02 8.22E+02 1.07 F 2 238 . 57 472 - 485 4 77. 62 3 . 12E+ 02 45 . 52 6.06E+02 1. 62 F 3 29 4 .99 582 - 595 59 0.4 3 9 . 15E+Ol 29 . 57 4.1 0E+02 1. 57 F 4 338. 55 672 - 68 4 677.54 5 . 17E+Ol 25 . 13 3 . 12E+02 1. 65 F 5 35 1. 88 699 - 712 70 4 .18 l . 92E+02 33 . 27 2.52E+02 1. 63 F 6 583.09 1161- 1172 1166.52 8 . 80E+Ol 23.61 1. 24E+02 1. 74 F 7 609 . 01 1214 - 1224 1218.35 l.20E+02 25.94 1. 02E+02 1. 87 F 8 661 .36 1317 - 1330 1323.04 2 . 06E+02 32 . 2 1 1.33E+02 1.88 F 9 9 1 0.9 4 1817 - 1828 1822 . 12 7 . 59E +O l 20 . 42 5. 4 8E+Ol 2 . 05 F 10 969 . 0 7 1933 - 19 4 3 1938.36 2 . 00E+ Ol 1 1. 29 7 . 49E+Ol 0 . 65 F 11 1332. 01 2658 - 2669 2664 . 16 3 . 51E+Ol 13. 85 2 . 90E+Ol 1. 93 F 12 1460.31 2911 - 2929 2920 . 73 5.35E+02 46 . 80 1 .4 3E+Ol 2. 4 2 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 8:08:57AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 92.70 6.32E+Ol 34 . 02 6.32E+Ol 3.40E+Ol F 2 238.57 3 . 12E+02 45.52 3.12E+02 4.55E+Ol F 3 294.99 9.15E+Ol 29.57 9.15E+Ol 2.96E+Ol F 4 338.55 5.17E+Ol 25 .13 5.17E+Ol 2.51E+Ol F 5 351.88 1.92E+02 33.27 8.36E+Ol 3. 72E+Ol 1. 08E+02 4 . 99E+Ol F 6 583 . 09 8 . 80E+Ol 23 . 61 8 . 80E+Ol 2.36E+Ol F 7 609.01 l.20E+02 25.94 4.12E+Ol 2 . 42E+Ol 7.92E+Ol 3.55E+Ol F 8 661.36 2.06E+02 32 . 21 6 . 61 E+Ol 2.54E+Ol l . 40E+02 4.lOE+Ol F 9 910.9 4 7 . 59E+Ol 20.42 7 . 59E+Ol 2.04E+Ol F 10 969 . 07 2.00E+Ol 11 . 29 2 . 00E+Ol l.13E+Ol F 11 1332 . 0 1 3 . 51E+Ol 13 . 85 3 . 51E+Ol 1. 39E+Ol F 12 1460 . 31 5.35E+02 46.80 5.63E+Ol 1. 71E+Ol 4.79E+02 4.98E+Ol

1/15/2019 8:09:06AM Page 3 of6 Analysis Report for L 1-SUB-TDS-FJGS-002-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.96 1460.75

• 10.67 5.42E+00 6.40E-01 CS-137 0.98 661.65

• 85.12 9.80E-02 2.93E-02 PB-212 0.56 77 .11 17.50 238.63

• 44.60 l.67E-01 2.59E-02 BI-214 0.34 609.31

• 46.30 9.48E-02 4.28E-02 1120.29 15.10 1238 .11 5.94 1377. 67 4 .11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.71 77 .11 10.70 295.21

• 19.20 1. 36E-01 4.44E-02 351.92

• 37.20 9.71£-02 4.51£-02 AC-228 0.60 209.28 4.40 338.32

• 11. 40 l.46E-01 7.14E-02 794 .70 4.60 911. 60

• 27. 70 2.19E-01 5.96E-02 964.60 5.20 969 .11

• 16.60 1.02£-01 5.75E-02

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV

=

Nuclide confidence index threshold 0.30 Errors quoted at 2.000sigma

1/15/2019 8:09:06AM Page4 of6 Analysis Report for L 1-SUB-TDS-FJGS-002-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.969 5.42E+00 6.40E-01 CS-137 0.987 9.S0E-02 2.93E-02 PB-212 0.560 1.67E-01 2.59E-02 BI-214 0.342 9.48E-02 4.28E-02 PB-214 0. 719 1 .17E-01 3.16E-02 AC-228 0.604 1.SSE-01 3.SSE-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 8:09:06AM Page 5 of6 Analysis Report for L1-SUB-TDS-FJGS-002-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 8:08:57AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 92 . 70 1.75445£- 02 26 . 93 Tol. PA- 228 F 6 583.09 2 . 44396£- 02 13 . 42 F 11 1332.01 9 . 76036£- 03 19. 71 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCVgrams) (pCi/grams)

(keV)

+ K- 40 1460.75

• 10 . 67 5.42E+00 4.93E - 01 4 . 93E- 01

+ AR- 41 1293.64 99.16 - 6.S0E-02 6 . 00E- 01 6 . 00E - 01

+ CO- 60 1173 . 22 100.00 1. 4 9E- 02 5 . 34E- 02 6.28E - 02 1332 . 49 100 . 00 7 . 23E- 02 5 . 34E - 02

+ KR- 85 513 . 99 0 . 43 1. 72E+O0 8 . 95E+00 8 . 95E+O0

+ Y- 88 898 . 04 93.70 6.2 4E- 03 3 . 06E-02 4 . 38E-02 1836.06 99 . 20 - 4 . 23E-02 3 . 06E- 02

+ NB- 94 702.63 100 . 00 - 2 . 92E-03 3.68E- 02 3.68E-02 871.10 100.00 -3.45E- 03 3.81E-02

+ I - 131 284.30 6 . 06 6 . 86E-02 3.54E-02 4 . 83E - 01 364.48 81. 20 l.44E-02 3 . 54E-02 636.97 7 . 27 l . 13E- 01 4.78E-01

+ CS-134 604 . 70 97.60 -5 . 87E-02 4. l 9E- 02 4 . 35E- 02 795 . 84 85 . 40 -3.19E - 02 4.19E-02

1/15/2019 8:09:06AM Page 6 of6 Analysis Report for L1-SUB-TDS-FJGS-002-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ CS-13 7 661.65

• 85 . 12 9 . 80E-02 4.88E-02 4.88E-02

+ CE-1 44 80.12 1. 36 1.62E+00 2.45E-01 3.04E+00 133.51 11. 09 5 . 15E-02 2.45E- 01

+ EU-152 121.78 28.40 -1.47E-02 9.40E-02 9.40E-02 344.28 26.60 -9.87E-03 1. 1 7E- 01 1 408.00 20 . 74 7.68E-02 1. 7 5E- 0l

+ EU-154 123.07 40.40 -4.26E-03 6.63E-02 6 . 63E-02 723.30 19.70 1.40E-01 1.80E-01 1274 .51 35 . 50 -l.79E-02 l.28E-01

+ EU-155 86 . 54 32.80 -l.85E-02 1. 04E -0 1 1.04E-01 105 .31 21. 80 1. 24E-02 1.32E- 01

+ BI-214 609.31

• 4 6.30 9.48E-02 7.27E-02 7.27E - 02 1120.29 15 . 1 0 6 . 78E -02 3.50E- 01 1238 .11 5 . 94 7 .14E- 01 9.65E-01 1377. 67 4.11 7 . 13E- 01 9 .4 8E-01 1 407 . 98 2.48 6 . 42E-01 1. 4 6E+00 1509 . 19 2 .19 -l.69E-0l 1.4 2E+00 1764 .4 9 15.80 1.41E-01 2.56E- 01

+ PB- 214 77.11 10 . 70 5 . 71E-01 8.49E-02 4.14E-01 295 . 21

• 19.20 1 . 36E-01 1. 20E-Ol 351.92

• 37.20 9.71E-02 8.49E- 02

+ PA-228 89.95 22.00 1.47E- 02 1 . l0E- 01 1.88E- 01 93 . 35 35.00 - 8.91E-02 1.l0E- 01 105.00 16.30 7.22E-02 2 .21E-01 12 9. 22 2 . 97 2.llE - 01 l.14E+00 338.32 5.30 l.61E-01 7 . 02E- 01 463.00 13 . 80 7.61E-02 2 . 82E-01 911.23 16 . 70 4.33E-01 3 . 81E- 01

+ AM-241 59 . 54 36 . 30 l.14E-01 1 . 94E-01 1.94E-01

+ CM-243 103.76 23 . 00 5 . 08E-0 2 l.2 6E-01 1.26E-0l 228.18 10.60 1 . 70E-01 2.55E-01 277.60 14 . 00 -8.41E-02 2.03E- 0 1

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 8:09:48AM Page I of 6

_.Apex-Gamma Analysis Report for L1-SUB-TDS-FJGS-003-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FJGS-003-SB Sample Description  : L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.008E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 1/15/2018 9:57:00AM Acquisition Started  : 1/15/2018 5:07:36PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli live Time  : 3600.0 seconds Real lime  : 3610.9 seconds Dead lime  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5333 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 8:09:38AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 8:09:48AM Page 2 of6 Analysis Report for L 1-SUB-TDS-FJGS-003-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 . 44 14 7 - 1 61 153.42 2 . 62E+02 61. 36 l . 30E+03 3 . 41 M 2 23 8 .5 4 473 - 489 477 . 56 2 . 87 E+02 44.88 5 . 03E+ 02 1. 65 m 3 2 41. 78 473 - 4 89 484 . 0 4 8 . 73E+0 l 29 . 93 4.78E+02 1. 66 F 4 29 5.0 1 587 - 596 5 90 . 48 l . 30E+02 30 . 66 2.95E+02 1. 34 F 5 338. 00 673 - 680 676 . 43 6.71E+0l 24 . 88 l.85E+02 1. 47 F 6 351. 72 697 - 711 703 . 86 l.86E +02 33 . 37 3 . 02E+02 1. 64 F 7 582 . 93 1159 - 117 0 1166 . 20 7 .87E+0l 22 . 26 1 . 11E+ 02 1. 61 F 8 609 . 12 1214 - 1227 1218 . 57 l . 53E +02 28 . 30 l . 19E+02 1. 84 F 9 661 . 48 1318 - 1328 1323.28 l.10E+02 25 . 46 l . 10E+02 1. 83 F 10 910 . 78 1816 - 182 8 182 1. 80 5 . 92E+0l 20.51 l.14E+02 1. 82 F 11 968.52 1932 - 194 2 1937 . 26 3 .lOE+0l 15 . 7 6 1. 01E+02 1.27 F 12 1119 . 51 223 4 - 22 4 4 2239 . 20 3 . 22E+0l 1 6 . 63 6 . 94E+0l 2 . 06 F 13 1331. 80 2660 - 2670 2663 . 74 l . 93E+0l 11 . 72 4 . 63E+0l 1.26 F 14 1 4 60. 4 6 2912 - 2928 2921. 03 5.69E+02 49 . 00 4 . 36E+0l 2. 4 0 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 8:09:38AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.44 2.62E+02 61 . 36 2.62E+02 6 . 14E+0l M 2 2 38 . 5 4 2 . 87E+02 44 . 88 2.87E+0 2 4 . 49E+0l m 3 241 . 78 8 . 73E+0l 29 . 93 8 . 73E+0l 2 . 99E+0l F 4 295.01 l . 30E+ 02 30 . 66 1 . 30E+0 2 3 . 07E+0l F 5 338 . 00 6. 71E+0 l 24 . 88 6 . 71E+0l 2.49E+0l F 6 351. 72 1. 8 6E+02 33.37 8.36E+0l 3 . 72 E+0l l . 02E+0 2 5 . 00E+Ol F 7 582.93 7 . 87E+0 l 22 . 26 7.87E+0l 2.23E+0l F 8 609.12 l . 53E+02 28 . 30 4. 12E+0l 2 . 42E+0l 1. 11E+02 3 . 72E+Ol F 9 661.48 l.10E+02 25 . 46 6.61E+01 2 . 5 4E+0l 4 . 36E+0l 3 . 60E+0l F 10 910 . 78 5 . 92E+O l 20. 51 5.92E+0l 2 . 05E+Ol F 11 968 . 52 3 . l0E+0l 15 . 76 3 . l 0E+0l 1.58E+0 l F 12 1 119 . 5 1 3 . 22E+0 l 16.63 3.22E+0l 1 . 66E+0l F 13 1 331 . 80 l . 93E+0l 11. 72 1.93E+01 1.1 7 E+ 0l F 14 1460.46 5 . 69E+02 49 . 00 5 . 63E+0l l . 71E+0l 5 . 13E+02 5.19E+0l

1/15/2019 8:09:48AM Page 3 of6 Analysis Report for L 1-SUB-TDS-FJGS-003-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 98 1460 . 75

• 10 . 67 5.55E+OO 6.40E- 01 CS - 137 0 . 99 661 . 65

• 85 . 12 2 . 92E- 02 2.41E - 02 PB- 212 0 . 97 77 .11

• 17.50 3 . 72E - 01 9.02E- 02 238 . 63

• 44.60 1. 4 7E-Ol 2.42E- 02 BI - 214 0 . 56 609.31

• 46.30 l . 27E - 01 4.31E- 02 1120 . 29

• 15 . 10 1. 95E - 01 1. OlE- 01 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509.19 2 . 19 1764 . 49 15 . 80 PB- 214 0 . 98 77 .11

• 10 . 70 6.08E - 01 l.48E- 01 295 . 21

• 19.20 1. 85E-01 4 .44 E-02 351 . 92

• 37 . 20 8 . 75E- 02 4 . 30E- 02 AC- 228 0 . 57 209.28 4.40 338 . 32

• 11. 40 1.81E- 01 6 . 77E- 02 794 . 70 4 . 60 911. 60

• 27 . 70 1.63E- 01 5.68E-02 964.60 5 . 20 969 . 11

• 1 6 . 60 1.50E-01 7.67E- 02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/15/2019 8:09:48AM Page 4 of6 Analysis Report for L1-SUB-TDS-FJGS-003-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.986 5 .55E+00 6 . 40E-01 CS-137 0.995 2.92E-02 2.41E-02 PB-212 0.979 l.56E-01 2.34E-02 BI-214 0.566 l.38E-01 3.97£-02 PB-214 0.983 l.44E-01 3.03£-02 AC-228 0.576 l.65E-01 3.78E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 8:09:48AM Page 5 of6 Analysis Report for L 1-SUB-TDS-FJGS-003-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 8:09:38AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(3/4) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 3 241.78 2.42409E- 02 17 . 15 F 7 582 . 93 2 . 18550E- 02 14 . 14 F 13 1331. 80 5 . 36119E- 03 30.37 CO- 60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ K- 40 1460 . 75

• 10.67 5.55E+00 5 . 31E- 01 5.31E- 01

+ AR- 41 1293 . 64 99.16 - 8 . 88E- 02 7.49E-01 7 . 49E-01

+ CO-60 1173.22 100 . 00 5 . 84E- 02 4.83E- 02 5 . 32E - 02 1332 . 49 100 . 00 2 . 26E- 02 4 . 83E- 02

+ KR- 85 513 . 99 0 . 43 - 1. 06E- 01 8.28E+00 8 . 28E+00

+ Y-88 898 . 04 93.70 l.70E- 02 3 . 09E- 02 4 . 35E - 02 1836 . 06 99.20 8.29E- 04 3 . 09E-02

+ NB-94 702 . 63 100 . 00 - l . 19E- 02 3.31E- 02 3.31E-02 871 . 10 100 . 00 - 8 . 77E-03 3.80E- 02

+ I-131 284 . 30 6.06 3.92E-01 3 . 26E-02 4.53E- 01 364.48 81. 20 - 3.56E-03 3.26E- 02 636.97 7.27 l . 75E-01 4.77E - 0l

+ CS - 134 604 . 70 97.60 -3.12E-02 4 . 45E-02 4.5 1E-02

1/15/2019 8:09:48AM Page 6 of6 Analysis Report for L1-SUB-TDS-FJGS-003-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCilgrams)

(keV)

CS-134 795.84 85.40 -9.39E-03 4.45E-02 4.45E-02

+ CS- 137 66 1. 65

• 85 . 12 2 .92E-02 4.36E-02 4.36E-02

+ CE-144 80. 1 2 1. 36 -4.91E-01 2.30E-01 2.85E+O0 133.51 11.09 -4. 8 4E- 02 2.30E-01

+ EU-152 121 . 78 28.40 -6. 31E-02 9.05E-02 9.05E-02 344.28 26.60 -8.0lE-02 l.12E-0l 1408 . 00 20.74 -2.30E-03 l.75E-01

+ EU-154 123.07 40.40 -2.36E-02 6 . 39E- 02 6.39E-02 723.30 19. 70 2 . 61E-01 2.0lE-01 1274 .5 1 35.50 6.38E-02 l.30E-0l

+ EU- 155 86 .54 32.80 -3.87E-02 9.92E-02 9.92E-02 105.31 21. 80 3.39E-02 l.24E-01

+ BI-214 609.31

• 46 . 30 1. 27E-0l 7.38E-02 7.38E-02 1120 . 29

• 15 . 10 l.95E-0l 2.03E-01 1238 .11 5 . 94 4.18E-01 9.85E-01 1377.67 4 .11 3.57E-01 l.0lE+0O 1407.98 2 . 48 -1.92E-02 1. 4 6E+00 1509.19 2.19 1. 07E+00 l.53E+0O 1764 .49 15 . 80 2.54E-01 2.75E-01

+ PB-21 4 77 .11

• 10.70 6 . 08E-01 8 . 54E-02 3.37E-0l 295.21

• 19.20 l.85E-01 8 . 99E-02 351. 92

• 37.20 8.75E-02 8.54E-02

+ PA-228 89.95 22.00 2 .4 9E-01 l.08E- 0l l . 86E-01 93.35 35.00 - 1. 31E-02 1. 08E-0 l 105.00 16 . 30 1. 06E-01 2. llE-0 1 129.22 2.97 6.19E-02 l.l0E+00 338.32 5.30 1.07E+00 7.06E-01 463.00 13.80 -l.41E-01 2.74E- 01 911. 23 16.70 3. 72E-01 3.77E-01

+ AM-241 59.54 36.30 l.00E-02 l . 85E-0l l.85E-01

+ CM- 243 103.76 23.00 2. 31E-02 l.18E- 01 l.18E-01 228 .1 8 10.60 -1.08E-01 2 . 41E-0l 277 . 60 14.00 -l.26E-01 l.90E-Ol

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 8: 10:29AM Page I of6 Jt'Apex-Gamma Analysis Report for L 1-SUB-TDS-FJGS-004-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FJGS-004-SB Sample Description  : L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.977E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/15/2018 10:07:00AM Acquisition Started  : 1/15/2018 6:10:46PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.1 seconds Dead Time  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 -4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5334 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 8:10:20AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 8:10:29AM Page 2 of6 Analysis Report for L 1-SUB-TDS-FJGS-004-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 75.89 14 7 - 159 152.33 1. 71E+02 59.20 l.32E+03 3.18 F 2 185.85 366 - 376 372 . 19 7 . 14E+Ol 35 . 45 7 . 33E+02 1. 39 F 3 238.53 469 - 485 477 . 53 3.78E+02 49.55 7.56E+02 1. 71 F 4 269.89 535 - 546 540 . 24 5 . 15E+ Ol 27.02 4 . 08E+02 1. 46 F 5 295.15 586 - 595 590.76 9. llE+Ol 29 . 32 3.56E+02 1. 28 F 6 338.25 669 - 683 676.93 5.60E+Ol 27 . 05 4.22E+02 1. 68 F 7 351.86 699 - 712 704 . 14 l.48E+02 33.86 4 . 05E+02 1. 72 F 8 583.19 1160 - 1171 1166 . 72 8.18E+Ol 24.73 1.74E+0 2 1. 76 F 9 609 . 26 1214 - 1224 1218.85 8.64E+Ol 24 . 34 l. 4 6E+02 1. 68 F 10 661. 4 7 1315 - 1328 1323.25 l.56E+02 29.50 l.55E+02 1.88 F 11 911.16 1814 - 1832 1822.55 7.lOE+Ol 22.63 1 . 60E+02 2.40 F 12 968 . 18 1932 - 194 5 1936.58 2 . 93E+Ol 16 . 23 1. 31E+02 1. 32 F 13 1172 . 92 2339 - 235 4 2346 . 02 2 . 98E+02 37.62 l.30E+02 2 . 19 F 14 1331 . 99 2657 - 2673 266 4 .12 2.49E+02 33 . 2 4 6 . 26E+Ol 2.27 F 15 1460 . 48 2913 - 292 9 2921. 07 5 . 48E+02 47.87 l.61E+Ol 2.51 M == First peak in a multiplet region m == Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 8:10:20AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001 364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 75.89 1 . 71E+02 59 . 20 l.71E+ 02 5.92E+Ol F 2 185.85 7.14E+Ol 35 . 45 7 . 14E+Ol 3.5 4E+Ol F 3 238 . 53 3 . 78E+02 49.55 3 . 78E+02 4. 96E+Ol F 4 269 . 89 5 . 15E+Ol 27 . 02 5.15E+Ol 2.70E+Ol F 5 295 .1 5 9 . llE+Ol 29.32 9. llE+ Ol 2 . 93E+Ol F 6 338.25 5 . 60E+Ol 27 . 05 5.60E+ Ol 2 . 71E+Ol F 7 351.86 l . 48E+02 33 . 86 8.36E+ Ol 3 . 72E+Ol 6.40E+ Ol 5 . 03E+Ol F 8 583.19 8. 1 8E+Ol 24 . 73 8.18E+ Ol 2 . 47E+Ol F 9 609 . 26 8.64E+Ol 24 . 34 4. 12E+Ol 2 . 42E+Ol 4.52E+Ol 3 . 43E+Ol F 10 661.47 1. 56E+02 29.50 6.61E+Ol 2 . 54E+Ol 8 . 96E+Ol 3 . 89E+Ol F 11 911 . 16 7. lOE+Ol 22.63 7.lOE+Ol 2 . 26E+O l F 12 968. 1 8 2 . 93E+Ol 16 . 23 2 . 93E+Ol 1 . 62E+Ol F 13 1172 .92 2.98E+02 37.62 4.55E+Ol 1. 72E+Ol 2.52E+02 4 . 14E+Ol F 14 1331 .99 2.49E+02 33.24 2.49E+02 3.32E+Ol

1/15/2019 8: 10:29AM Page 3 of6 Analysis Report for L 1-SUB-TDS-FJGS-004-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 15 1460.48 5.48E+02 47.87 5 . 63E+0l l . 71E+0l 4 . 92E+02 5 . 08E+0l M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0.98 1460.75

• 10 . 67 5.37E+00 6 .3 0E- 01 CO- 60 0.97 1173 . 22

• 100 . 00 2 . 43E- 01 4 . 15E- 02 1332 . 49

• 100.00 2.68E-01 3 . 83E- 02 CS- 137 0 . 99 661. 65

• 85.12 6.07E- 02 2 . 66E- 02 PB- 212 0 . 55 77 . 11 17 . 50 238 . 63

• 44 . 60 l . 95E- 0l 2 . 75E-02 BI - 214 0.34 609 . 31

• 46 . 30 5 . 22E- 02 3 . 97E- 02 1120 . 29 15.10 1238 . 11 5. 94 1377 . 67 4 .11 1407.98 2 . 48 1509.19 2.19 1764 . 49 15 . 80 PB- 214 0 . 72 77 . 11 10 . 70 295.21

• 19 . 20 1. 31E- 01 4 . 25E- 02 351 . 92

• 37 . 20 5 . 54E-02 4 . 37E-02 RA- 226 0.97 186.21

• 3.28 4 . 22E - 01 2 . llE - 01 AC- 228 0 . 58 209.28 4 . 40 338.32

• 11. 40 l.53E - 0l 7.41E - 02 794 . 70 4 . 60 911.60

• 27 . 70 l.97E-01 6.35E-02 964 . 60 5.20 969 .11

• 16 . 60 l.43E-01 7.97E- 02

1/15/2019 8:10:29AM Page 4 of6 Analysis Report for L 1-SUB-TDS-FJGS-004-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.988 5.37E+00 6 . 30E - 01 CO- 60 0.974 2.57E-01 2 . 82E - 02 CS - 137 0 . 995 6.07E- 02 2.66E-02 PB- 212 0.559 l.95E- 01 2.75E-02 BI-214 0.349 5 . 22E- 02 3.97E- 02 PB-21 4 0 . 721 9.40E-02 3 .0 5E - 02 RA-226 0 . 979 4.22E-01 2. llE - 01 AC- 228 0.588 1. 69E-01 4.12E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 8:10:29AM Page 5 of6 Analysis Report for L 1-SUB-TDS-FJGS-004-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 8:10:20AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 75.89 4. 73627E- 02 17 . 36 F 4 269 . 89 1.42947E-02 26. 25 F 8 583 . 19 2 . 27092E- 02 15 . 13 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCllgrams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 5 . 37E+0O 4 . 76E- 01 4 . 76E - 01

+ AR-41 1293 . 64 99 . 16 -4.86E- 02 1. 22E+0O 1. 22E+00

+ CO- 60 1173.22

• 100 . 00 2.43E- 01 3.88E- 02 5 . 88E- 02 1332 . 49

• 100 . 00 2 . 68E- 01 3.88E- 02

+ KR- 85 513 . 99 0.43 l.07E+0 l 9 . 3 2E+00 9.32E+O0

+ Y- 88 898.0 4 93 . 70 8 . 17E- 03 3.27E- 02 5 . 05E- 02 1836 . 06 99.20 l . 57E- 02 3 . 27E - 02

+ NB- 94 702.63 100 . 00 -4 .32E- 03 3.99E-02 3 . 99E-02 871 . 1 0 100 . 00 - 4.42E- 02 4. 5 4E- 02

+ I - 131 28 4. 30 6 . 06 8 . 31E- 02 3 . 91E- 02 5 . llE- 01 364 .4 8 8 1. 20 -8 . 13E-03 3 . 91E- 02 636 . 97 7 . 27 l . 71E- 03 5 . 44E - 01

+ CS- 134 604 . 70 97 . 60 - 2 . 83E-02 4 .45E-02 4. 45E - 02 795 . 84 85 . 40 - 4 . 65E- 03 5.24E - 02

+ CS-137 661. 65

• 85.12 6 . 07E- 02 4 . 86E- 02 4 . 86E - 02

1/15/2019 8:10:29AM Page 6 of6 Analysis Report for L 1-SUB-TDS-FJGS-004-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCi/grams)

(keV)

+ CE-144 80.12 1. 36 -6.04E-01 2 . 37E-01 2 . 95E+OO 133.51 11.09 -3.74E-02 2 . 37E-01

+ EU-152 121.78 28.40 - 4.22E-0 2 9 .4 9E- 02 9.49E-02 344.28 26 . 60 -5.72E-02 1. 25E-01 1408.00 20 . 74 6 . 73E-02 1.94E-01

+ EU-154 123 .0 7 40 . 40 1.22E-02 6 . 73E-02 6 . 73E-02 723.30 19 . 70 1.40E-01 2 . 16E-01 1274.51 35 . 50 - 6 .95E- 02 1. 28E-01

+ EU-155 86.54 32 . 80 - 2.05E-02 1.05E-01 1 . 05E-01 105 . 31 21. 80 1.53E-01 1 . 34E-Ol

+ BI-2 14 609 . 31

• 46.30 5.22E-02 7 . 55E- 02 7.55E-02 1120 . 29 15 . 10 -2.62E-02 3 . 85E- 01 1238 .11 5 . 94 4.80E-01 9.48E-01 1377 . 67 4 .11 4.79E-01 9.33E - 01 1407 . 98 2 . 48 5.63E-01 1.62E+OO 1509.19 2. 1 9 5.53E-01 1. 42E+OO 1764.49 15.80 1.24E-01 2.61E - 01

+ PB- 214 77 . 11 10.70 5. llE- 01 9.20E-02 3 . 95E-01 295 . 21

• 19.20 1.31E-01 9.86E-02 351.92

• 37 . 20 5.54E - 02 9 . 20E- 02

+ PA-228 89.95 22.00 2.61E-01 1.16E-Ol 1. 98E-01 93 . 35 35.00 -2 . 0SE- 02 l.16E-01 105.00 16.30 1.92E- 01 2 . 34E-01 129.22 2.97 1.16E+OO 1. 1 9E+OO 338.32 5.30 3 . 94E-01 8.00E-01 463.00 13.80 4 . lOE-02 3 . 21E- 0 1 911. 23 16 . 70 1.91E-01 4 . 53E- Ol

+ AM-241 59.54 36.30 -l.05E-0 1 1 . 90E- 01 l.90E-01

+ CM- 243 103 . 76 23.00 1. l 7E-01 1. 28E-01 1 . 28E- 01 228 . 18 10.60 l.66E-Ol 2.60E-01 277 . 60 14 .0 0 6 . 24E-02 2 . 12E- 01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 8:11 :09AM Page I of7

~~~~pex-Gam ma Analysis Report for L1-SUB-TDS-FJGS-005-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FJGS-005-SB Sample Description  : L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.220E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/15/2018 10:20:00AM Acquisition Started  : 1/15/2018 7:13:14PM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.7 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5335 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 8:11:00AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 8 :11 :09AM Page 2 of7 Analysis Report for L 1-SUB-TDS-FJGS-005-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peal< Energy ROI ROI Peal< NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 92.77 183 - 189 186.08 5.92E+0l 34 . 95 6 .13E+02 1.10 F 2 225.96 449 - 456 452.40 4.44E+0l 26. 59 3.33E+02 1.23 F 3 238 . 64 471 - 485 477.76 3.56E+02 47.07 5.77E+02 1. 70 F 4 295.04 582 - 594 590.53 8 .7 3E+0l 28.15 3.48E+02 1. 52 F 5 338 . 37 672 - 681 677.17 8.45E+0l 26.78 2. 11E+02 1. 67 F 6 351. 73 697 - 710 703 . 88 1 .4 2E+02 31. 03 3.43E+02 1. 44 F 7 583 . 08 1161 - 1174 1166.50 9.59E+0l 24 . 65 1.44E+02 1. 92 F 8 609.15 1212 - 1227 1218.63 1 . 17E+02 24 . 52 1.12E+02 1. 63 F 9 661.38 131 4 - 1330 1323.08 1.66E+02 28 . 91 1.30E+02 1. 82 F 10 910 .9 1 1816 - 1829 1822.05 7 .05E+0l 20 .9 3 8.47E+0l 2.19 F 11 1172.79 2341 - 2352 2345.75 7. 55E+0l 21.79 8 . 67E+0l 2 .1 6 F 12 1332.03 2657 - 2671 266 4.1 9 5.56E+0l 17.32 4.84E+0l 2 .0 3 F 13 1460.38 2912 - 2929 2920 . 87 5 . 30E+02 46.88 2 . 70E+0l 2.47 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 8:11:00AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peal< Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 92 . 77 5.92E+0 l 34.95 5.92E+0l 3.49E+0l F 2 225.96 4 .44E+0l 26.59 4.44E+0l 2.66E+0l F 3 238.64 3.56E+02 47.07 3.56E+02 4.71E+Ol F 4 295.04 8.73E+0l 28.15 8.73E+Ol 2 . 82E+0l F 5 338.37 8.45E+0l 26.78 8.45E+0l 2 . 68E+Ol F 6 351 .7 3 1. 42E+02 31. 03 8.36E+0l 3. 72E+0l 5.88E+0l 4 . 84E+0l F 7 583 . 08 9.59E+0l 24.65 9.59E+0l 2.46E+0 l F 8 609.15 1.17E+02 24.52 4.12E+0l 2 .4 2E+0l 7.54E+0l 3 . 45E+0l F 9 661.38 1.66E+02 28 . 91 6.61E+0l 2.54E+0l 9.99E+0l 3 . 85E+0l F 10 910 .9 1 7 .0 5E+0l 2 0. 93 7.05E+0l 2 .0 9E+0l F 11 1172.79 7.55E+0l 21 . 79 4.SSE+0l 1.72E+ 0l 3 . 00E+Ol 2 . 78E+0l F 12 1332 .0 3 5 .56E+0l 17 . 32 5 . 56E+ 0 l 1. 7 3E+0l F 13 1460.38 5.30E+02 46 . 88 5 . 63E+0l 1. 71E+0l 4 . 74E+02 4.99E+0l

1/15/2019 8:11:09AM Page 3 of7 Analysis Report for L 1-SUB-TDS-FJGS-005-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.97 1460.75

• 10.67 5.60E+00 6.66E-01 CO-60 0.96 1173.22

• 100.00 3.13E-02 2.90E-02 1332.49

• 100.00 6 . 48E-02 2.05E-02 CS-137 0.98 661.65

• 85.12 7.31E-02 2.85E-02 PB-212 0.56 77 .11 17.50 238.63

• 44.60 1.99E-01 2.83E-02 BI-214 0.34 609.31

• 46.30 9.41E-02 4.34E-02 1120.29 15.10 1238 .11 5.94 1377.67 4 .11 1407.98 2.48 1509.19 2.19 1764 . 49 15.80 PB-214 0.71 77 .11 10.70 295.21

• 19.20 1.35E-01 4.42E-02 351.92

• 37.20 5.51E-02 4.55E-02

• =Energy line found in the spectrum.

- =Manually added nuclide.

? = Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV

=

Nuclide confidence index threshold 0.30 Errors quoted at 2.000sigma

1/15/2019 8:11:09AM Page4 of7 Analysis Report for L 1-SUB-TDS-FJGS-005-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.978 S.60E+00 6.66E-01 CO-60 0.969 S.37E-02 l.67E-02 CS-137 0.989 7.31E-02 2.8SE-02 PB-212 0.560 l.99E-01 2.83E-02 BI-214 0.347 9.41E-02 4.34E-02 PB-214 0.717 9.64E-02 3.17E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 8: 11 :09AM Page 5 of7 Analysis Report for L1-SUB-TDS-FJGS-005-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 8 :11 :00AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 92.77 l . 64462E- 02 29.51 Tol. PA- 228 F 2 225 . 96 l . 23238E-02 29 . 97 F 5 338 .37 2 . 34738E- 02 1 5 . 85 Tol. AC- 228 PA- 228 F 7 583.08 2.664 4 4E - 02 12.85 F 10 910 . 91 l.95808E - 02 14.85 Tol. AC-228 PA- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(3/4) Activity NuclideMDA LineMDA Name (pCi/grams) (pCl/grams) (pCl/grams)

(keV)

+ K- 40 1460 . 75

• 10.67 5 . 60E+00 5.44E- 01 5 . 44E- 01

+ AR- 41 1293 . 64 99.16 -l . 05E+00 l.55E+00 l . 55E+00

+ CO-60 1173 . 22

• 100 . 00 3 . 13E-02 3.52E- 02 5 . 47E - 02 1332 . 49

• 100 . 00 6 . 48E-02 3 . 52E - 02

+ KR- 85 513 . 99 0 . 43 4 . 08E+00 9.07E+00 9 . 07E+00

+ Y- 88 898 . 04 93.70 l . 6 1E- 02 3.l0E- 02 4.94E-02 1836 . 06 99.20 -2 . 06E-03 3 . l0E- 02

1/15/2019 8:11 :09AM Page 6 of7 Analysis Report for L 1-SUB-TDS-FJGS-005-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCilgrams)

(keV)

+ NB-94 702.63 100.00 2 . 12E-02 3.88E- 02 4. 1 5E-02 871.10 100.00 -2 . 42E-02 3.88E-02

+ I-131 2 84 . 30 6.06 3 . 13E-02 3.75E-02 4.92E-01 364.48 81. 20 -2. 0lE-02 3. 7 5E-02 636.97 7 . 27 6 . 83E-02 5.28E-01

+ CS-134 604 . 70 97.60 1. 44E-03 4.65E-02 4.65E-02 795 . 84 85.40 -4.76E-02 4.73E-02

+ CS-137 661.65

• 85 . 12 7 . 31E- 02 5 .19E-02 5 .1 9E-02

+ CE-144 80.12 1. 36 1.28E+00 2.54E-01 3 . llE+00 133 . 51 11.09 2.12E-01 2.54E-01

+ EU-152 121.78 28 . 40 -1.55E-02 9.60E-02 9 . 60E-02 344.28 26.60 -5. llE-02 1 . 22E-0 1 1408 . 00 20.74 -2.28E-02 1. 98E-01

+ EU-154 123.07 40.40 l.55E-02 6.77E-02 6 . 77E-02 723 . 30 19.70 l.l0E-01 1. 95E-01 1274 . 51 35.50 3.09E-02 1 . 39E-01

+ EU-155 86 . 54 32 . 80 -2.43E-02 l. llE-01 1 . llE - 0 1 105.31 21. 80 -2 . 89E-02 1.33E-01

+ BI-214 609.31

• 46.30 9.41E-02 8.12E-02 8 . 12E-02 1120.29 15.10 2.89E-02 3.63E-01 1238 .11 5.94 8. 1 9E-01 1. 07E+00 1377 . 67 4 .11 4.63E-01 l.09E+00 1407.98 2.48 -1.90E-01 1.65E+00 1509.19 2 . 19 -l.22E-01 l.48E+ 00 1764.49 15.80 8.65E-02 2.43E-01

+ PB-214 77 .11 10 . 70 2 . 58E-01 9.51E-02 4.21E-01 2 95.2 1

• 19.20 1. 35E-01 l.13E-01 351.92

• 37.20 5 . 51E-02 9 . 51E- 02

+ PA-228 89.95 22.00 1.28E-01 l . 27E- 01 2 . 13E-01 93.35 35.00 4 . 41E-02 1.27E-01 105.00 16 . 30 -2.02E-01 2.38E-01 129.22 2 . 97 - 9.33E-02 l.26E+00 338 . 32 5.30 6.16E-01 8 .13E-0l 463 . 00 13 . 80 2.44E-01 3.30E-01 911.23 16.70 5.36E-01 4.3 7E-01

+ AM-241 5 9.54 36.30 1. 33E-Ol 2.00E-01 2.00E-01

+ CM- 2 43 103.76 23.00 -2 .13E-03 1. 28E-01 1. 28E-01 228.18 10.60 - 1.24E-01 2.59E-0l 277 . 60 14.00 -5.12E-02 2.1 2E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 8: 11 :09AM Page 7 of7 Analysis Report for L1-SUB-TDS-FJGS-005-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

1/15/2019 8:11:50AM Page I of7 JtApex-Gamma Analysis Report for L 1-SUB-TDS-FJGS-006-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FJGS-006-SB Sample Description  : L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.007E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 1/15/2018 12:13:00PM Acquisition Started  : 1/16/2018 7:48:44AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live nme  : 3600.0 seconds Real Time  : 3610.7 seconds Dead nme  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100 - 4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5336 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 8:11:41AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 8:11 :50AM Page 2 of7 Analysis Report for L 1-SUB-TDS-FJGS-006-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76. 62 147 - 161 153.79 1 . 97E+02 61. 36 1.49E+03 3.00 F 2 185.86 368 - 377 372 . 22 7 . 39E+0l 31.74 6.1 4E+02 1. 10 F 3 238.46 472 - 485 477.39 3 . 22E+02 45 . 61 6.19E+02 1. 50 F 4 295 . 11 582 - 595 590.68 9 . 88E+0 l 30.56 4.17E+02 1. 61 F 5 338 . 10 672 - 680 676.63 6 . 39E+0 l 25.91 2.25E+02 1. 54 F 6 35 1. 88 697 - 708 704.19 1.59E+ 02 31. 67 2.76E+02 1. 44 F 7 583.05 1162 - 1172 1166.43 8 . 74E+0l 24 . 80 1.39E+02 1. 95 F 8 609.39 1216 - 1225 1219.12 1 . 12E+02 25.09 1.15E+02 1. 56 F 9 661.44 1316 - 1329 1323.19 3.47E+02 40.23 1. 36E+02 1. 60 F 10 910 .5 2 1815 - 1828 1821.28 7. l0E+0l 20.97 8.83E+0l 2 . 08 F 11 968.63 1933 - 1943 1937.47 3. 48E+0l 17 . 05 7.51E+0l 2 . 07 F 12 1120. 01 2234 - 2246 2240 . 20 4. 36E+0l 17.10 5 . 54E+0l 2. 71 F 13 1332. 27 2658 - 2673 2664 . 68 6 .1 6E+0l 17.97 4.22E+0l 2.51 F 14 1460 .4 4 2914 - 2928 2921.00 5. 40E+02 47.24 l .85E+0l 2 . 48 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 8:11:41AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.62 l.97E+02 61. 36 l.97E+0 2 6.14E+Ol F 2 185 . 86 7.39E+0l 31. 74 7 . 39E+0l 3.17E+0l F 3 238 . 46 3.22E+02 45.61 3 . 22E+02 4.56E+Ol F 4 295 .11 9 . 88E+0l 30.56 9.88E+0l 3 . 06E+0l F 5 338 .1 0 6 . 39E+0l 25.91 6.39E+0l 2 .59E+0l F 6 351 .88 l. 59E+02 31. 67 8 . 36E+0l 3 . 72E+0l 7.55E+0l 4.89E+0 l F 7 583.05 8.74E+0l 24.80 8.74E+0l 2 .48E+0l F 8 609.39 l.12E+02 25.09 4 . 12E+0l 2.42E+0l 7 .13E+0l 3 .49E+0l F 9 661 .4 4 3 .4 7E+02 40 . 23 6 . 61£+01 2.54£+01 2 . 81E+02 4 . 76£+0 1 F 10 910.52 7 .l 0E+0l 20 . 97 7.l 0E+ 0l 2.l0E+0l F 11 968. 63 3 .48£+01 17 . 05 3.48E+0l 1.70E+0l F 12 1120 . 01 4.36E+0l 17.10 4.36E+0l 1 . 71E+0l F 13 1332.27 6.16E+0l 17 . 97 6 . 16E+01 1 . 80E+0l F 14 1460.44 5.40E+02 47.24 5.63E+01 1. 7 1E+0l 4.83E+ 02 5 . 02E+Ol

1/15/2019 8 :11 :S0AM Page 3 of7 Analysis Report for L 1-SUB-TDS-FJGS-006-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m ::: Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0.98 1 460.75

• 10 . 67 5 . 23E+OO 6 . 16E-01 CS- 137 0.99 661. 65

• 85 . 12 l . 88E - 01 3.35E- 02 PB- 212 0 . 98 77 . 11

• 17.50 2 . 79E - 01 8.86E- 02 238.63

• 44.60 1 . 65E- 01 2. 4 9E- 02 BI - 214 0 . 58 609 . 31

• 46 . 30 8 . 15E- 02 4.02E-02 1120 . 29

• 15.10 2.6 4E- 01 1. 05E- 01 1238 .11 5 . 94 1377 . 67 4 .11 1407 . 98 2.48 1509 . 19 2 . 19 1764.49 15.80 PB- 214 0 . 99 77 . 11

• 10 . 70 4 . 56E- 01 1.45E- 01 295.21

• 19 . 20 1 . 40E-01 4.39E - 02 351 . 92

• 37 . 20 6 . 47E- 02 4 . 20E-02 RA- 226 0 . 98 186.21

• 3 . 28 4.33E - 01 1 . 87E- 01

• = Energy line found in the spectrum.

- ::: Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT

1/15/2019 8:11:S0AM Page 4 of7 Analysis Report for L 1-SUB-TDS-FJGS-006-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.985 5.23E+00 6.16E-01 CS-137 0.993 1. 88E-01 3.35E-02 PB-212 0.986 1. 69E-01 2.40E-02 BI-214 0.582 1. 05E-01 3.75E-02 PB-214 0.993 1. 04E-01 2.98E-02 RA-226 0.980 4.33E-01 1. 87E-01

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 8:11 :S0AM Page 5 of7 Analysis Report for L 1-SUB-TDS-FJGS-006-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Perfonned on  : 1/15/2019 8:11 :41AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(3/4) Peak Tolerance Peak No. Energy (ke V) Peak Size (CPS) Uncertainty Type Nuclide F 5 338.10 l . 77457E- 02 20 . 28 Tol. AC- 228 PA- 228 F 7 583 . 05 2.42805E - 02 14.19 F 10 910.52 l.97266E- 02 14 . 77 Tol. PA- 228 F 11 968.63 9 . 67605E- 03 24.47 Tol. AC- 228 F 13 1332.27 1. 71118E- 02 14 . 59 Tol. CO- 60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nucl/deMDA LineMDA Name (pCilgrams) (pCl/grams) (pCi/grams)

(keV)

+ K- 40 1460.75

• 10 . 67 5 . 23E+00 4 . 74E- 01 4 . 74E - 01

+ AR- 41 1293 . 64 99.16 3.19E+0l 8.46E+0l 8 . 46E+0l

+ CO- 60 1173.22 100.00 9 . 53E-02 5 . 73E - 02 6.43E- 02 1332 . 49 100.00 9 . 12E- 02 5.73E-02

+ KR- 85 513 . 99 0 . 43 8.62E+00 8 . 43E+00 8.43E+00

+ Y- 88 898 . 04 93 . 70 2.02E- 02 3.54E- 02 4 . 34E - 02 1836.06 99 . 20 l . 17E- 02 3.54E-02

+ NB- 94 702.63 100 . 00 - l.13E - 02 3.46E- 02 3 . 46E-02 871 . 10 100.00 -1. 36E - 02 4.20E-02

+ I - 131 284.30 6 . 06 - l.80E-0l 3.70E-02 4 . 81E- 01

1/15/2019 8:11:S0AM Page 6 of?

Analysis Report for L 1-SUB-TDS-FJGS-006-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCi/grams) (pCi/grams) (pCilgrams)

(keV)

I -1 31 36 4 . 4 8 8 1 .20 5 . 16E- 03 3 . 70E-02 3 . 70E- 02 636 . 97 7.27 8.60E-02 4 . 90E-0 1

+ CS -1 34 604.70 97.60 - 1.02E- 01 4. 35E - 02 4 . 35E- 02 795.84 85.40 - 3.99E-03 4 . 54E-02

+ CS-13 7 661 . 65

• 85.12 1 . 88E - 01 4 .68E- 02 4 . 68E-02

+ CE-1 44 80 . 12 1. 36 -1.02E+00 2 . 37E-01 2 . 90E+00 133 . 51 11. 0 9 1.57E- 01 2 . 37E-01

+ EU- 1 52 121 . 78 28.40 - 8 . 75E-02 8.9 9E- 02 8 . 99E- 02 3 44. 28 26 . 60 - 8 . 80E-02 1 .14E- 01 1 408 . 00 20 . 7 4 1. 23E- 01 1. 87E-0 1

+ EU-154 123 . 07 4 0. 4 0 - 6.93E- 02 6.37E- 02 6.37E- 02 723 . 30 1 9.70 - 5 . 33E-02 1 . 77E-O l 127 4 .51 35.50 -9.14 E-02 1.26E- 0 1

+ EU-1 55 86 . 54 32 . 80 3 . 61E-03 1 . 02E- 01 1. 02E- 01 1 05 . 31 21. 80 5.14E- 02 1. 30E- 0 1

+ BI - 2 1 4 609.31

• 46 . 30 8 . lSE-02 7 . 09E- 02 7 . 09E-02 1120 . 29

• 15.10 2 . 6 4E-0 1 1 . 87E-0 1 1238 . 11 5 . 94 9 . 19E-0 l 9 . 67E-0 1 1377.67 4 .11 l . 58E-0 2 9.77E-0 1 1407 . 98 2 . 48 1.03E+0O 1. 56E+O0 1 509.19 2 . 19 9. llE- 0 1 l.30E+O0 1764. 49 1 5 . 80 7 . 82E- 02 2 . 45E- 0 1

+ PB-214 77 .11

• 10.70 4.56E- 0 1 8 . l0E- 02 3 . 59E- 0 1 295 . 2 1

• 19.20 1.40E- 01 1.16E-0l 351. 92

• 37 . 20 6.47E-02 8 . l0E-02

+ PA-228 89.95 22.00 1 . 77E- 01 1 . 6 4E- 01 2 . 77E-01 93.35 35 . 00 4 . 98E- 02 l . 64E- 01 105.00 16 . 30 1 . 22E-01 3 . 26E-01 129 . 22 2.97 3 . 26E-0 l l.64E+00 338.32 5 . 30 1.08E+00 1.07E+O0 463.00 13 . 80 3 . 26E- 0 1 4.56E- 0 1 911.23 16 . 70 2 . 95E- 01 5 . 39E-0 1

+ AM- 241 59.54 36 . 30 2.19E- 0 1 1.87E- 01 l . 87E- 0 1

+ CM-243 103.76 23 . 00 - 8 . 16E- 03 1.24E- 01 1.24E-0 1 228.18 10.60 2.31E- 0 1 2 . 50E- 0 1 277 . 60 1 4 . 00 - 2 . 03E- 0 1 1.95E- 0 1

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 8:11:50AM Page 7 of7 Analysis Report for L1-SUB-TDS-FJGS-006-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

1/15/2019 8:12:30AM Page I of7 J,Apex-Gamma Analysis Report for L 1-SUB-TDS-FJGS-007-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FJGS-007-SB Sample Description  : L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.680E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/15/2018 12:20:00PM Acquisition Started  : 1/16/2018 8:49:48AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3611.0seconds Dead Time  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 -4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5337 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 8:12:21AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 8:12:30AM Page2 of?

Analysis Report for L 1-SUB-TDS-FJGS-007-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 .2 5 148 - 162 153.05 2 . 13E+02 65.81 l . 56E+03 4.44 M 2 87.27 172 - 193 175.08 6.09E+0l 37.42 7 . 99E+02 1. 77 m 3 92.79 172 - 193 186 . 11 l .4 1E+02 45.32 9 . 97E+02 1. 78 F 4 238.50 472 - 484 477.48 3.08E+02 46 . 19 6.83E+02 1. 46 F 5 295.06 587 - 594 590.57 9 . 24 E+0l 29 .4 0 2 .4 9E+02 1. 52 F 6 338.15 672 - 684 676 . 73 9 . 91E+0l 26.70 2 .4 5E+02 1. 58 F 7 351. 68 698 - 710 703.80 l.57E+02 31.15 3 . 03E+02 1. 32 M 8 502.23 1000 - 1029 1004.82 2 . 08E+0l 2.28 l.05E+02 1. 41 F 9 582.93 1157 - 1174 1166.20 l.12E+02 26.18 1. 80E+ 02 2.09 F 10 609.24 1215 - 1225 1218.81 l . 28E+02 26.74 l.18E+ 02 1. 65 F 11 661.35 1315 - 1329 1323 . 02 l . 53E+02 29 . 49 l.61E+ 02 1. 96 F 12 910. 72 1815 - 1828 1821.68 7.15E+0l 20.60 9.88E+ 0l 1. 73 F 13 968.73 1933 - 1943 1937.69 3 . 36E+0l 16.47 1. 06E+ 02 1. 31 F 14 1460.45 2911 - 2927 2921.01 5.70E+02 49.05 4.39E+0l 2.32 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 8:12:21AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76 . 25 2 . 13E+02 65.81 2 .13E+0 2 6.58E+0l M 2 87.27 6.09E+0l 37.42 6.09E+ 0l 3 . 74E+0l m 3 9 2 . 79 1. 41E+02 45.32 1 . 4 1 E+02 4.53E+0l F 4 238.50 3.08E+02 46 . 19 3.08E+02 4 . 62E+0l F 5 295.06 9.24E+0l 29.40 9 . 24E+0l 2.94E+0l F 6 338.15 9.91E+0l 26.70 9.91E+0l 2.67E+0l F 7 351 . 68 1. 57E+02 31.15 8.36E+0l 3 . 72E+0l 7.30E+0l 4 . 85E+0l M 8 502 . 23 2.08E+0l 2.28 2 . 08E+0l 2.28E+00 F 9 582.93 1.12E+02 26 . 18 1 . 12E+02 2 . 62E+0l F 10 609.24 1.28E+02 26. 74 4.12E+0l 2.42E+0l 8.73E+0l 3.61E+0l F 11 661. 35 1.53E+02 29. 49 6 . 61E+0l 2 . 54E+0l 8 . 69E+0l 3.89E+0l F 12 910.72 7.15E+0l 20.60 7.15E+0l 2 .06E+0l F 13 968 . 73 3.36E+0l 16.47 3 . 36E+0l l.65E+0l F 14 1460 . 45 5 . 70E+02 49 . 05 5 .63E+0l 1 . 71E+0l 5.14E+0 2 5.20E+0l

1/15/2019 8:12:30AM Page 3 of7 Analysis Report for L 1-SUB-TDS-FJGS-007-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-4 0 0 . 98 1460 . 75

• 10.67 5.79E+00 6 . 67E- 01 CS- 137 0 . 98 661 . 65

• 85.12 6.06E- 02 2.73E- 02 PB- 212 0 . 96 77 .11

• 17 . 50 3 . 16E- 0 1 9.96E- 02 238 . 63

• 4 4. 60 1. 64E- 01 2.60E- 02 BI - 21 4 0 . 34 609 . 31

• 46.30 l.04 E- 01 4 . 33E- 02 1120.29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 .11 1407 . 98 2 . 48 1509.19 2 . 19 1764.4 9 15.80 PB-21 4 0.97 77 .11

• 1 0.70 5 . 16E- 0l l . 63E - 01 295.21

• 19 . 20 l . 36E- 01 4 . 39E - 02 351 . 92

• 37 . 20 6 . 51E- 02 4 . 34 E- 02 AC- 228 0 . 57 209 . 28 4.40 338.32

• 11 . 40 2 . 78E- 01 7.62E- 02 794.70 4.60 9 11 . 60

• 27 . 70 2.05E - 01 5 . 97E-02 964 . 60 5.20 969 .11

• 16.60 l.69E - 01 8 . 35E - 02

• =Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma

1/15/2019 8:12:30AM Page4 of7 Analysis Report for L 1-SUB-TDS-FJGS-007-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.986 5.79E+OO 6.67E-01 CS-137 0.986 6.06E-02 2.73E-02 PB-212 0.966 1.70E-01 2.52E-02 BI-214 0.349 1. 04E-01 4.33E-02 PB-214 0.976 1. OSE-01 3.04E-02 AC-228 0 . 579 2.18E-01 4.09E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 8:12:30AM Page 5 of7 Analysis Report for L 1-SUB-TDS-FJGS-007-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 8:12:21AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(3/4) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 2 8 7 . 27 1 . 69144E- 02 30.73 Tol. EU- 155 m 3 92 . 79 3 . 91 758E-02 1 6 . 07 Tol. PA-228 M 8 502 . 23 5.78048E- 03 5 .4 7 F 9 5 82. 93 3 . 11558E- 02 11. 67 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA L/neMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ K-40 1460 . 75

• 10 . 67 5.79E +O0 5 . 56E- 01 5 . 56E- 01

+ AR- 41 1293 . 64 99 . 16 - 1.28E+0l 1 . 39E+02 1 .39E+02

+ CO-60 1173 . 22 100 . 00 3 . 63E- 02 4.98E- 02 6 . 04E- 02 1 332 . 49 100 . 00 2 . 12E-02 4 . 98 E-02

+ KR- 85 513 . 99 0.43 - 2 . 18E+0O 8 . 79E+00 8.79E+00

+ Y- 88 898.04 93 . 70 - 6 . 33E- 03 2 . 08E- 02 4 . 35E- 02 1836 . 06 99 . 20 -3 . 41E-02 2 . 08E- 02

+ NB- 94 702 . 63 100.00 - 7 . 53E- 03 3 . 37E- 02 3 . 37E- 02 871.10 100 . 00 - 1. 71E- 02 3 . 80E- 02

+ I - 131 284 . 30 6 . 06 - 1. 32E- 02 3.74E- 02 5 . 05E- 01

1/15/2019 8:12:30AM Page 6 of7 Analysis Report for L1-SUB-TDS-FJGS-007-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCilgrams)

(keV)

I - 131 364. 48 81. 20 - 2 .65E-02 3 . 74E - 02 3.74E-02 636 . 97 7.27 -l.77E-02 4.97E-0l

+ CS- 134 604.70 97.60 -8.83E-02 4 . 42E-02 4 . 46E-02 795.84 85.40 -5. 78E-02 4.42E - 02

+ CS-137 661.65

• 85. 12 6.06E-02 5. llE-02 5. llE-02

+ CE-144 80.12 1. 36 -6.07E-01 2.39E-01 3.09E+00 133 . 51 11. 09 6 . 84E-02 2.39E-01

+ EU-152 121. 7 8 28.40 - 1. 34E-01 9.20E-02 9.20E- 02 344 . 28 26.60 -2.52E-02 l.19E-01 1408.00 20.74 1. 02E-02 2 . 07E- 01

+ EU-154 123 . 07 40.40 -4 .87E-02 6.50E-02 6.50E-02 723. 30 19 . 70 -4 .82 E-02 l.98E-01 1274.51 35.50 l.96E-02 l.45E-01

+ EU-155 86.5 4 32 . 80 -2.27E-02 1. 06E-01 1.06E-01 105.31 21. 80 -3.21E-02 l.30E-01

+ BI-214 609.31

• 46.30 1. 04E-01 7.45E - 02 7 . 45E-02 ll20.29 15.10 1 . 76E- 01 3.67E-01 1238 .11 5.94 -l . 14E-01 9 . 77E-01 1 377 . 67 4 . 11 8.76E-01 9 . 99E-01 14 07.98 2 .48 8.49E-02 l.73E+00 1 509 . 19 2. 1 9 -5.51E-01 l.52E+00 1 764.49 15.80 -2.91E-02 2.66E- 01

+ PB-214 77 .11

• 10.70 5.16E-01 8 . 09E-02 3 . 86E-01 295 .21

• 19.20 l.36E-01 8.09E-02 351.92

• 37 . 20 6.51E-02 8.73E-02

+ PA-228 89 . 95 22.00 -5.42E-02 l . 80E-01 3.03E-01 93.35 35.00 -9.04E-03 l.80E-0l 105.00 16 . 30 - 3.53E-02 3.38E- 01 129.22 2 . 97 l . 17E+00 1.74E+00 338 . 32 5.30 1. 30E+00 l.12E+O0 463.00 13. 80 l.69E-02 4.59E-01 911 . 23 16.70 6 . 59E-01 6 . 09E-01

+ AM-241 59.54 36 . 30 8 . 93E-02 1 . 96E-01 1. 96E-01

+ CM-243 103 . 76 23.00 4.60E-02 1.24E-01 l.24E-01 228.18 10 . 60 -l.66E-01 2.55E-01 277.60 14.00 6.15E-02 2 . llE-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 8:12:30AM Page 7 of7 Analysis Report for L1-SUB-TDS-FJGS-007-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

1/15/2019 8:13:10AM Page I of6

__.Apex-Gamma Analysis Report for L 1-SUB-TDS-FJGS-008-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FJGS-008-SB Sample Description  : L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 9.814E+02 grams Facility  : Dairyland_NPP Sample Taken On  : 1/15/2018 12:23:00PM Acquisition Started  : 1/16/2018 9:54:39AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.8 seconds Dead Time  : 0.30 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100 -4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5338 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 8: 13:01 AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 8:13:10AM Page 2 of6 Analysis Report for L 1-SUB-TDS-FJGS-008-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76 . 32 14 7 - 161 153. 1 9 3 . 07E+02 63 . 37 l.32E+03 3.55 F 2 93.16 184 - 190 186 . 87 6.08E+0l 33 . 69 5 . 68E+02 1. 07 F 3 238 . 46 471 - 485 477 . 40 3.22E+ 02 46 . 32 7.26E+02 1. 50 F 4 295 . 00 585 - 595 590.45 8.16E+0l 25 . 06 3 . 07E+02 1.02 F 5 338 . 32 672 - 681 677.06 5 . 52E+0l 22 . 57 2 . 02E+02 1. 33 F 6 351. 96 700 - 709 704 . 35 l . 78E+02 3 1 .79 1. 81E+02 1. 46 M 7 502 . 63 1001 - 1030 100 5 . 62 l . 94E+ 0 l 1. 58 l . 03E+02 1. 41 F 8 582 . 87 1162 - 1173 1166 . 08 9. 17E+0l 23 . 08 1.30E+02 1. 31 F 9 609 . 05 1211 - 1223 1218. 4 3 1 . 27E+02 26 . 60 1.31E+02 1. 75 F 10 661.38 13 1 6 - 1327 1323. 08 1 . 56E+02 29 . 62 1 . 28E+02 1. 94 F 11 727 . 63 1452 - 1 4 62 1455 . 55 2.56E+0l 13 . 60 8 .4 1E+0l 0.99 F 12 9 1 0 . 83 1817 - 1827 1821.91 4 . 14E+0l 17.08 6.85E+ 0l 1. 67 F 13 968 . 88 1933 - 1943 1937.98 2 . 34E+0l 15 . 30 8 . 7 4E+0l 1. 62 F 14 1 4 60 . 34 2913 - 2929 2920.79 5.35E + 02 46 . 49 9.20E+00 2.54 F 15 1763 . 50 3523 - 3532 3527 . 07 l . 95E+0l 9 . 77 5 . 00E+00 2 . 03 M :;: First peak in a multiplet region m :;: Other peak in a multiplet region F :;: Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 8: 13:01AM Env. Background File  : C :\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 76.32 3.07E+02 63 . 37 3.07E+02 6.34E+0l F 2 93 . 16 6.08E+0l 33.69 6 . 08E+0l 3.37E+0l F 3 238 . 46 3 . 22E+02 46.32 3.22E+ 02 4.63E+0l F 4 295.00 8 . 16E+0l 25.06 8 . 16E+0l 2.51E+0l F 5 338.32 5 . 52E+0l 22 . 57 5.52E+0l 2 . 26E+0l F 6 351.96 1.78E+02 31. 79 8.36E+0l 3.72E+0l 9 . 44E+0l 4.89E+0l M 7 502.63 1 . 94E+0l 1. 58 l . 94E+0l 1. 58E+00 F 8 582 . 87 9 . 17E+0l 23 . 08 9 . 17E+0l 2.31E+0l F 9 609 . 05 1.27E+02 26.60 4 . 12E+0l 2.42E+0l 8 . 62E+ 0l 3 . 60E+0l F 10 661.38 l . 56E+02 29 . 62 6.61E+0l 2 . 54E+0l 8 . 95E+0l 3.90E+0l F 11 727 . 63 2.56E+0l 13. 60 2 . 56E+ 0l 1 .36E+0l F 12 910 . 83 4.14E+0l 17.08 4 .1 4E+0l 1 . 71E+0l F 13 968 . 88 2 . 34E+0l 15.30 2 . 34E+ 0l 1. 53E+0l F 14 1460 . 3 4 5.35E+02 46.49 5.63E+Ol 1.71E+0l 4 .7 9E+ 02 4.95E+0l

1/15/2019 8:13:10AM Page 3 of6 Analysis Report for L 1-SUB-TDS-FJGS-008-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 15 1763 . 50 1 . 95 E+0l 9.77 1.95E+0l 9 . 77E+00 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0.97 1460 . 75

• 10 . 67 5 . 31E+00 6 . 2 4E- 01 CS- 137 0 . 98 661.6 5

• 85. 12 6 . 16E- 02 2.70E- 02 BI - 212 0 . 58 727.17

• 11 . 80 1 . 39E- 01 7 . 40E - 02 785.42 2 . 00 1620.56 2 . 75 PB- 212 0.96 77 . 11

• 17 . 50 4 . 48E- 01 9 . 69E- 02 238.63

• 44 . 60 1 . 69E- 01 2 . 59E- 02 BI- 214 0 . 52 609 . 31

• 46 . 30 1. OlE- 01 4 . 26E- 02 1120 . 29 1 5 .1 0 1238 . 11 5 . 94 1377.67 4.11 1407 . 98 2 . 48 1509 .1 9 2 . 19 1764. 4 9

• 15.80 1.71E- 0l 8 . 65E- 02 PB- 21 4 0.98 77 . 11

• 10 . 70 7 . 32E- 01 1. 58E- 01 295.21

• 19 . 20 l . 19E- 01 3 . 70E- 02 351.92

• 37.20 8.31E- 02 4 . 33E-02 AC- 228 0.59 209.28 4 . 40 338 . 32

• 11. 40 1. 53E- 01 6 . 30E- 02 794 . 70 4 . 60 911 . 60

• 27 . 70 1.17E- 01 4.85E- 02 964 . 60 5.20 969 .11

• 16.60 1 . 16E-01 7 . 64E-02

1/15/2019 8:13:1 0AM Page 4 of6 Analysis Report for L1-SUB-TDS-FJGS-008-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.974 5 . 31E+00 6.24E-01 CS-137 0.989 6.16E-02 2 . 70E-02 BI-212 0 . 582 1. 39E-01 7 . 40E-02 PB - 212 0. 969 1.83E-01 2.50E-02 BI - 214 0 . 520 1 . 15E-01 3.82E- 02 PB-214 0.982 1.14E-01 2.77E- 02 AC-228 0.594 1.28E-01 3.43E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 8:13:10AM Page 5 of6 Analysis Report for L 1-SUB-TDS-FJGS-008-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 8: 13:01AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(3/4) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 93 . 16 1 . 68891E-02 27.70 Tol. PA- 228 M 7 502 . 63 5. 38723E- 03 4.07 F 8 582.87 2.5 4 663E- 02 12.59 M == First peak in a multiplet region m ::: Other peak in a multiplet region F == Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams)

(keV)

+ K-40 1460.75

• 10 . 67 5.31E+00 4 . 70E- 01 4 . 70E - 01

+ AR- 41 1293 . 64 99.16 3 . 77E+00 l.82E+02 l.82E+02

+ CO- 60 1173.22 100 . 00 2 . 19E-02 4.50E - 02 5 . 44E- 02 1332 . 49 100 . 00 l . 83E-02 4.50E-02

+ KR- 85 513 . 99 0 . 43 1. 87E- 01 8 . 51E+00 8 . 51E+00

+ Y- 88 898 . 04 93 . 70 l.51E-02 2 . 92E- 02 4 . 43E - 02 1836 . 06 99.20 - 9 . 45E - 03 2.92E- 02

+ NB- 94 702.63 100 . 00 -2 . 07E-02 3.48E- 02 3 . 48E- 02 871 . 10 100 . 00 2.79E-03 3 . 84E-02

+ I - 131 284.30 6.06 l.48E- 01 3 . 57E- 02 5 . 0lE- 01 364.48 81. 20 l . 03E-04 3 . 57E-02 636.97 7 . 27 -8 . 58E - 02 4.73E-0l

+ CS-134 604 . 70 97.60 8 . l0E - 02 4 . 44E- 02 4.44E-02

1/15/2019 8:13:10AM Page 6 of6 Analysis Report for L 1-SUB-TDS-FJGS-008-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams)

(keV)

CS-134 795 . 84 85 .4 0 7.28E-03 4.44E-02 4.48E-02

+ CS - 137 661. 65

• 85.12 6 . 16E- 02 4 .6 4E-02 4.64E-02

+ CE - 144 80.12 1. 36 -4.63E-01 2.38E-01 2.98E+OO 133.51 11.09 6.22E-02 2.38E-01

+ EU- 152 121.78 28.40 -1. 52E-02 9 . llE-02 9. llE- 02 344.28 26 .60 - 1.47£-01 1.12£- 01 1408.00 20.74 7 . 0lE -0 3 1 . 61E-Ol

+ EU- 154 123.07 40 .40 -6.15£-02 6 . 35£ - 02 6.35E-02 723.30 19.70 -1. 84E-01 1. 97E- 01 1274 . 51 35.50 1. 40E-01 1.49E-01

+ EU-155 86.54 32 .8 0 - 2.64E- 02 1 . 0lE- 01 1.0lE-01 105. 31 21. 80 -1.16E-02 1.25E-01

+ BI-214 609.31

• 46.30 1.0lE-01 7 . 64 E-02 7.64E- 02 1120.29 15. 1 0 -1 . 91£-01 3 . 37E-01 1238 .11 5.94 l . 82E- 02 9.67E-01 1377.67 4 .11 7.34E-01 9.85E-01 1407 . 98 2 .4 8 5.86E- 02 l.34E+OO 1509.19 2.19 -5.83E-01 1. 83E+OO 1764.49

• 15.80 1.71E-01 9.26E- 02

+ PB-214 77 .11

• 10.70 7.32E-01 7.54E - 02 3.50E- Ol 295.21

• 19.20 1.19E- 01 9.57E-02 351.92

• 37 . 20 8.31E-02 7.54E-02

+ PA- 228 89 . 95 22.00 1. 55E-Ol 1.72E- 01 2.91E-01 93.35 35.00 - 1 . 84E-02 1.72E- 01 1 05.00 16 . 30 - l.23E- 02 3 . 34E-01 129 . 22 2.97 -5.98E-01 1.75E+OO 338 . 32 5 . 30 4.72E - 02 1. llE+OO 463 . 00 13.80 2.02E-01 4.51E-01 911.23 16.70 1.44E-01 5.60E-01

+ AM-241 59.54 36.30 l.60E-01 1.93E- 01 1.93E-01

+ CM-243 1 03 . 76 23 . 00 - 3.52£-02 1.19E-01 1 .1 9E- 01 228.18 10.60 -1.79E - 02 2.42E-01 277 . 60 14.00 -1.90E-01 1 . 97E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 8:13:50AM Page I of6

_.Apex-Gamma Analysis Report for L1-SUB-TDS-FJGS-009-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANALYSIS Sample Identification  : L 1-SUB-TDS-FJGS-009-SB Sample Description  : L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.012E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 1/15/2018 12:29:00PM Acquisition Started  : 1/16/2018 10:55:41AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live Time  : 3600.0 seconds Real Time  : 3610.8 seconds Dead Time  : 0.30%

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100- 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5339 PEAK ANALYSIS REPORT Peak Analysis Performed on 1/15/2019 8:13:41AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 8:13:50AM Page 2 of6 Analysis Report for L 1-SUB-TDS-FJGS-009-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

M 1 74.50 143 - 161 149.54 1 . 16E+02 39.91 9.61E+02 1. 50 m 2 77.09 143 - 161 154.72 1.48E+02 42.36 9.41E+ 0 2 1. 5 0 F 3 186.01 369 - 377 372. 52 5.62E+0l 29.45 5 . 54E+02 0 . 95 F 4 238.53 473 - 485 477.53 3.16E+02 45.97 6.17E+02 1. 53 F 5 295.09 583 - 598 590. 62 8 . 06E+0l 25.51 5 . 04E+02 1.00 F 6 337.94 667 - 684 67 6. 32 1.04E+02 32.35 3.77E+02 2.82 F 7 351 . 79 697 - 712 704.01 1 . 67E+02 33.05 3.26E+02 1. 89 F 8 582.93 1162 - 1175 1166.20 9.64E+0l 23.87 1.39E+02 1. 75 F 9 609 .0 7 12 1 3 - 1224 1218.48 1. 03E+02 25 . 00 1. 30E+02 1. 68 F 10 661 . 43 1318 - 1330 1323 . 17 3 . 08E+02 37.62 1.01E+02 1. 83 F 11 860.38 1716 - 1726 1721. 01 2 . 95 E+0l 14.33 5 . 79E+0l 1. 50 F 12 910 . 81 1813 - 1828 1821.85 7. 72E+0l 20 . 56 6.42E+0l 2 . 51 F 13 968 . 85 1932 - 1942 1937.92 2.26E+0l 15. 77 9 .1 4E+0l 1. 86 F 14 1119.98 2235 - 2245 2240 .1 5 2.84E+0l 15. 72 6.71E+0l 1. 90 F 15 1460 . 41 29 1 2 - 2930 2920.93 5.52E+02 47.71 9.50E+00 2.51 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 8:13:40AM Env. Background File  : C :\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

M 1 74.50 1.16E+02 39.91 1 . 16E+02 3.99E+ 0l m 2 77 . 09 1.48E+02 42 . 36 1.48E+02 4 . 2 4E+0l F 3 186.01 5.62E+0l 29 . 45 5.62E+0l 2.95E+0l F 4 238.53 3.16E+02 45.97 3.16E+02 4 . 60E+0l F 5 295.09 8.06E+0l 25 . 51 8.06E+0l 2 . 5 5E+ Ol F 6 337.94 1.04E+02 32.35 1.04E+02 3.24E+0l F 7 351 . 79 1.67E+02 33.05 8.36E+0l 3. 72E+0 l 8 . 31E+0l 4.98E+0l F 8 582.93 9.64E+0l 23.87 9.64E+0l 2 . 39E+0l F 9 609 . 07 1.03E+02 25.00 4.12E+0l 2 . 42E+0 l 6. 2 1E+0l 3 .48E+0l F 10 661.43 3.08E+02 37.62 6.61E+0l 2 . 54E+0 l 2.41E+02 4.54E+0l F 11 860 . 38 2 . 95E+0l 14.3 3 2 .95E+0l 1. 43E+0l F 12 910.81 7 . 72E+0l 20 . 56 7. 72E+0l 2.06E+Ol F 13 968 . 85 2.26E+0l 15.77 2.26E+0l l.58E+0l F 14 1119.98 2 . 84E+0l 15. 72 2.84E+Ol 1.57E+0l

1/15/2019 8:13:S0AM Page 3 of 6 Analysis Report for L 1-SUB-TDS-FJGS-009-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 15 14 6 0 . 41 5 . 52 E+02 47. 71 5.63E+0l 1. 71E+0l 4.95E+02 5.07E+0l M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 98 1 4 60.75

• 10 . 67 5 . 34E+00 6 . 21 E- 01 CS- 137 0 . 99 661. 65

• 85.12 1 . 61E- 01 3.15E- 02 PB- 212 0 . 99 77 .11

• 17 . 50 2 . 06E- 01 6.05E- 02 238 . 63

• 44.60 1 . 61E- 01 2.49E- 02 BI- 214 0 . 57 609 . 31

• 46 . 30 7.07E- 02 3 . 98E- 02 1120.29

• 15 . 10 1. 72E- 01 9 . 53E- 02 1238 .11 5 . 94 1377. 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15.80 PB-214 0 . 99 77 .11

• 10 . 70 3 . 38E- 01 9 . 89E-02 295 . 2 1

• 19.20 l .14E - 01 3 . 65E-02 351 . 92

• 37.20 7 . l0E-02 4 . 26E- 02 RA- 226 0.99 186.21

• 3 . 28 3 . 28E - 01 l.73E-01 AC-228 0 . 58 209 . 28 4.40 338 . 32

• 11. 40 2 . 79E-01 8 . 79E - 02 794 . 70 4 . 60 911 . 60

• 27 . 70 2.12E - 01 5.71E- 02 964.60 5 . 20 969 .11

• 16 . 60 l . 09E- 0l 7 . 63E- 02

1/15/2019 8:13:S0AM Page4 of6 Analysis Report for L1-SUB-TDS-FJGS-009-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K- 40 0.982 5 . 34E+00 6.21E-01 CS-137 0.992 1.61E-01 3.15E-02 PB-212 0.999 l.59E-01 2.31E-02 BI-214 0 . 578 8 . 57E - 02 3.67E-02 PB-214 0 . 998 9 .4 4E- 02 2 . 68E-02 RA- 226 0.993 3 . 28E-01 l.73E-01 AC-228 0.588 l . 97E-0l 4.06E-02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 8:13:S0AM Page 5 of6 Analysis Report for L 1-SUB-TDS-FJGS-009-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/2019 8:13:40AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(3/4) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 1 74 . 50 3. 21630E-02 17.23 F 8 582 . 93 2.67 8 95E- 02 12.38 F 11 8 60.38 8.20120E-03 24 . 26 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCi/grams) (pCl/grams) (pCilgrams)

(keV)

+ K- 40 1460 . 75

• 10 . 67 5.34E+00 4.57E- 01 4 . 57E - 01

+ AR- 41 1293 . 64 99.16 8 . 3 1E+00 2.8 4E+02 2.84E+02

+ CO- 60 1173.22 100 . 00 2 . 22E-02 4 . 87E- 02 5 . 55E - 02 1332.49 100.00 1.39E- 02 4 . 87E-02

+ KR-85 513.99 0 . 43 5.65E+OO 8 . S0E+00 8 . 50E+00

+ Y- 88 898 . 04 93 . 70 - 1 . 48E-02 2 . 75E- 02 3.92E- 02 1836 . 06 99.20 - 3.31E- 03 2 . 75E-02

+ NB- 94 702 . 63 100.00 - 1.09E- 02 3 . 41E-02 3.41E- 02 871.10 100 . 00 1.19E-03 3 . 76E-02

+ I-131 284 . 30 6 . 06 5. llE - 02 3.68E-02 4 . 82E- 01 364 . 48 81.20 1.82E-03 3 . 68E- 02 636.97 7.27 2.52E-0l 4 . 85E-01

+ CS-134 604 . 70 97 . 60 - 4.87E - 03 4.0SE - 02 4 . 0SE - 02 795.84 85.40 - 4.28E-02 4.28E- 02

1/15/2019 8:13:50AM Page 6 of6 Analysis Report for L 1-SUB-TDS-FJGS-009-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCilgrams) (pCi/grams) (pCilgrams)

(keV)

+ CS-137 661.65

• 85.12 1. 61E- 01 4.37E-02 4.37E-02

+ CE-144 80. 1 2 1. 36 -l.34E+OO 2 . 31E-01 2.89E+OO 133 . 51 11.09 2 . 23E-02 2.31E-01

+ EU-152 121.78 28 .4 0 -5.25E- 02 8.83E-02 8.83E-02 344 . 28 26.60 -2.50E-02 l.19E-0 1 1408.00 20.74 - l.12E-01 1. 37E-01

+ EU-154 123.07 40.40 -6.70E-02 6.19E-02 6.19E-02 723. 30 19.70 -2.02E-02 1. 69E-01 1274.51 35.50 6.48E-02 l.28E- Ol

+ EU-1 55 86.54 32 . 80 -5.71E-02 9 . 93E-02 9.93E-02 1 05.31 21. 80 -l .62E- 02 1. 23E-0 1

+ BI-214 609.31

• 46.30 7.07E-02 7.34E-02 7.34E-02 1120.29

• 15.10 l.72E-01 l . 96E-01 1238 .11 5.94 3.05E-01 9.91E-01 1377 . 67 4 .11 1. 80E-01 8 . 64E-01 1407.98 2.48 -9.34E-01 l.14E+OO 1509.19 2 . 19 - 4.22E - 01 l.47E+OO 1764.49 15.80 2 .48E- 0 1 2 . 71E-01

+ PB-214 77 .11

• 10.70 3.38E-0 1 8.74E- 02 2 . 36E-Ol 295.21

• 19.20 l.1 4E-01 1. 32E-01 351.92

• 37.20 7 . lOE-02 8.74E- 02

+ PA-228 89 . 95 22.00 2 . 95E-01 l.77E-01 2.97E-01 93 . 35 35 . 00 9.27E- 02 l.77E-01 105.00 16.30 - l.49E- 01 3.37E-Ol 129.22 2.97 1. 45E+OO l.78E+OO 338 . 32 5 . 30 8.34E-01 l . 18E+OO 463.00 13. 80 -2. 72E-01 4 . 69E- 01 911 . 23 16 . 70 6.56E- 01 5.70E-01

+ AM-241 59.54 36 . 30 l . 36E- 01 l.86E-01 l . 86E- 01

+ CM- 243 103.76 23.00 -l . 02E-02 l.17E-01 l.17E-01 228.18 10 .6 0 -6 . 02E- 02 2 .4 0E-Ol 277 . 60 14 . 00 l.42E-02 2.0lE- 01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

1/15/2019 8:14:32AM Pagel of 6

~~~~pex-Gamma Analysis Report for L 1-SUB-TDS-FJGS-010-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL GAMMA SPECTRUM ANAL YS/S Sample Identification  : L 1-SUB-TDS-FJGS-010-SB Sample Description  : L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Sample Type  : 500 ml Marinelli Unit Sample Point Sample Size 1.023E+03 grams Facility  : Dairyland_NPP Sample Taken On  : 1/15/2018 12:35:00PM Acquisition Started  : 1/16/2018 11:56:53AM Procedure  : 500ml Marinelli Operator  : Administrator Detector Name  : HOTLAB Geometry  : 500ml Marinelli Live nme  : 3600.0 seconds Real Time  : 3611.1 seconds Dead nme  : 0.31 %

Peak Locate Threshold  : 3.00 Peak Locate Range (in channels)  : 100 - 4096 Peak Area Range (in channels)  : 100-4096 Identification Energy Tolerance  : 1.000 keV Energy Calibration Used Done On  : 7/8/2014 Efficiency Calibration Used Done On  : 7/8/2014 Efficiency Calibration Description Sample Number  : 5340 PEAK ANALYS/S REPORT Peak Analysis Performed on 1/15/2019 8:14:23AM Peak Analysis From Channel  : 100 Peak Analysis To Channel  : 4096

1/15/2019 8 :14:32AM Page 2 of6 Analysis Report for L1-SUB-TDS-FJGS-010-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 75.66 147 - 160 151.86 2.19E+02 59 . 47 l.29E+03 3.74 F 2 92 . 53 183 - 192 185.60 6.60E+0l 37.92 8.60E+02 1. 38 F 3 185.71 364 - 378 37 1. 92 6.40E+0l 34.36 9.10E+02 1. 46 F 4 238 . 56 4 69 - 4 85 477.60 3.49E+02 47.85 7.66E+02 1. 65 F 5 295.2 1 586 - 594 590.86 9 . 38E+0l 27 . 26 2.50E+02 1. 22 F 6 337.95 668 - 680 676 . 34 4.68E+0l 24.70 2 . 99E+02 1. 68 F 7 351. 90 697 - 710 704 . 22 l . 88E+02 33 . 26 2.79E+02 1. 55 F 8 582.93 1159 - 1172 1166 . 21 9.99E+0l 23.40 1. 05E+02 1. 71 F 9 609.07 1212 - 1222 1218 . 48 l . 16E+02 25 . 89 l.10E+02 1. 74 F 10 661. 4 9 1318 - 1332 1323 . 30 1. 31E+02 25.65 l . 06E+02 1. 62 F 11 727 . 43 1451 - 1 4 62 1455 . 16 2 . 33E+0l 14 . 10 8.54E+0l 1. 35 F 12 911. 08 18 1 8 - 1828 1822.40 5 . 0lE+0l 18 . 48 8.42E+0l 1. 66 F 13 968 . 71 1933 - 19 4 4 1937.63 3.0lE+0l 16.53 9 . 36E+0l 1. 80 F 14 1460.43 2911 - 2929 2920 . 97 5.55E+02 48.20 2 . 85E+0l 2.44 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on  : 1/15/2019 8:14:23AM Env. Background File  : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert.

F 1 75.66 2.19E+02 59 . 47 2.19E+02 5.95E+0l F 2 92 . 53 6.60E+0l 37.92 6.60E+0l 3.79E+Ol F 3 185. 71 6 . 40E+0l 34.36 6 . 40E+0l 3.44E+Ol F 4 238 . 56 3.49E+02 47 . 85 3 . 49E+02 4.78E+Ol F 5 295 . 21 9.38E+0l 27 . 26 9 . 38E+0l 2.73E+0l F 6 337.95 4.68E+0l 24.70 4 . 68E+0l 2 . 47E+ 0l F 7 351. 90 1.88E+02 33.26 8 . 36E+0l 3. 72E+0l l . 04E+02 4 . 99E+0l F 8 582 . 93 9 . 99E+0l 23.40 9.99E+0l 2.34E+0l F 9 609 . 07 l.16E+02 25 . 89 4.12E+Ol 2 . 42E+0l 7 . 50E+0l 3 . 55E+0l F 10 661. 4 9 l.31E+02 25.65 6 . 61E+0l 2 . 54E+0l 6.52E+0l 3.61E+0l F 11 727. 43 2.33E+0l 14.10 2.33E+0l l.41E+0l F 12 911. 08 5 . 0lE+0l 18.48 5 . 0lE+0l l . 85E+0l F 13 968 . 71 3 . 0lE+0l 16.53 3.0lE+0l l.65E+0l F 14 1460 . 43 5.55E+02 48 . 20 5 . 63E+0l 1 . 71E+0l 4.99E+02 5.12E+0l

1/15/201 9 8:14:32AM Page 3 of6 Analysis Report for L1-SUB-TDS-FJGS-010-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0 . 98 1460 . 75

• 10.67 5 . 31E+00 6 . 19E- 01 CS - 137 0.99 661 . 65

• 85.12 4.30E - 02 2 . 39E-02 BI - 212 0 . 59 727.17

• 11. 80 1.21E- 01 7.35E- 02 785. 42 2 . 00 1620 . 56 2.75 PB- 212 0.56 77 . 11 17.50 238 . 63

• 44.60 l . 76E-01 2 . 58E- 02 BI - 214 0.34 609 . 31

• 46.30 8 . 44E- 02 4 . 02E-02 1120 . 29 15.10 1238 . 11 5 . 94 1377. 67 4 . 11 1407.98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB-214 0. 72 77 . 11 10.70 295 . 21

• 19 .20 1 . 31E- 01 3 . 86E- 02 351 . 92

• 37 . 20 8.80E- 02 4.24E- 02 RA- 226 0 . 96 186 . 21

• 3.28 3.68E- 01 1.99E- 01 AC- 228 0.60 209.28 4 . 40 338 . 32

• 11 . 40 1. 24E - 0l 6.59E - 02 794 . 70 4.60 911 . 60

• 27 . 70 l.36E-01 5.04E- 02 964 . 60 5.20 969 . 11

• 16.60 1. 44E-0l 7 . 92E- 02

1/15/2019 8:14:32AM Page 4 of6 Analysis Report for L 1-SUB-TDS-FJGS-010-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL

• = Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2 .000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K- 40 0.984 5 . 31E+OO 6 . 19E-01 CS- 137 0 . 996 4 . 30E- 02 2 . 39E-02 BI - 212 0 . 598 1.21E- 01 7.35E-02 PB- 2 1 2 0 . 560 1.76E- 01 2 . 58E- 02 BI - 21 4 0 . 345 8 . 44E- 02 4 . 02E- 02 PB- 214 0 . 721 1.12E-01 2 . 85E- 02 RA- 226 0 . 961 3.68E- 01 1 . 99E-0 1 AC- 228 0 . 606 1. 3 4E- 01 3 . 57E- 02

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma

1/15/2019 8:14:32AM Page 5 of6 Analysis Report for L1-SUB-TDS-FJGS-010-SB L1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL UNIDENTIFIED PEAKS Peak Locate Performed on  : 1/15/201 9 8:14:23AM Peak Locate From Channel  : 100 Peak Locate To Channel  : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 75 . 66 6. 09165E- 02 13 . 56 F 2 92. 53 l . 83196E- 02 28.75 Tol. PA- 228 F 8 582 . 93 2.77364E- 02 11 . 72 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used  : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams)

(keV)

+ K- 40 1460 . 75

• 10.67 5.31E+00 4 . 96E- 01 4. 96E- 01

+ AR- 41 1293 . 64 99.16 1. 23E+02 3 . 70E+ 02 3.70E+02

+ CO- 60 1173 . 22 100 . 00 1. 32E- 02 4.68E- 02 5.24E- 02 1332 . 49 100 . 00 3.17E- 02 4.68E- 02

+ KR- 85 5 1 3.99 0 . 43 5.65E+00 7 . 78E+00 7 . 78E+00

+ Y- 88 898 . 04 93.70 - 3 . 39E- 02 2 . 53E- 02 4.l0E- 02 1836.06 99 . 20 1. 0SE - 03 2 . 53E - 02

+ NB-94 702 . 63 100.00 4 . 58E-03 3 . 38E- 02 3.38E- 02 871.10 100 . 00 1. 38E - 02 3.73E-02

+ I - 131 284 . 30 6 . 06 l.91E-0l 3 . 52E-02 4.73E-0l 364.48 81. 20 - 4.21E- 03 3.52E- 02 636 . 97 7.27 7.61E- 02 4 . 73E- 0l

+ CS - 134 604.70 97 . 60 7 . 29E- 02 4.20E-02 4 . 20E- 02

1/15/2019 8 :14:32AM Page 6 of6 Analysis Report for L 1-SUB-TDS-FJGS-010-SB L 1-SUB-TDS COMBINED TB SLAB, PIT & SUMPS, DIESEL SLAB SOIL Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCi/grams)

(keV)

CS-134 795.84 85.40 -4 . 76E- 03 4. 20E- 02 4 . 28E- 02

+ CS-137 661.65

• 85.12 4.30E-02 4 . 43E- 02 4.43E-02

+ CE- 1 44 80 . 12 1. 36 -4.84E-01 2 . 24E- 0 1 2.83E+00 133 . 51 11.09 -5 . 17E-02 2.24E- 01

+ EU-152 121.78 28. 4 0 - 5 . 63 E- 02 8.69E- 02 8 . 69E-02 344.28 26 . 60 - 1. 59E- 02 1. 05E-01 1408 . 00 20 . 74 7 . 80E- 02 1 . 69E- 01

+ EU- 154 123 . 07 40 . 40 -1. 09E- 02 6 . 16E- 02 6.16E- 02 723. 30 19.70 - 2 . 76E- 02 1 . 76E-01 1274.51 35 . 50 4 . 34 E- 02 1 . 24E- 01

+ EU- 155 86 . 54 32 . 80 1.30E-03 1. 02E- 01 1 . 02E-01 1 05.31 21. 80 - 4 . 68E- 02 1.18E-0l

+ BI - 214 609.31

• 4 6 . 30 8.44 E-02 6.92E-02 6.92 E- 02 1120 . 29 15 . 10 7 .80E-02 3 . 13E- 01 1 238 . 11 5 . 94 1.07E+00 9.77E- 01 1377 . 67 4 . 11 4 . 23E- 0 1 1.09E+00 1 407.98 2 . 48 6.52 E- 01 1.41E+00 1509 . 19 2.19 3.95E- 0 1 1. 31E+00 1764.49 15. 8 0 1. 6 4E -01 2 . 71E- 01

+ PB- 214 77 . 11 10 . 70 1.65E-01 7.87E- 02 3 . 80E- 0 l 295 . 21

• 19 . 20 1 . 31E-01 7 . 8 7 E-02 351. 92

• 37.20 8.80E-02 8.16E-02

+ PA- 228 89.95 22.00 2.76E-02 1. 80E-01 3 . lJE-01 93 . 35 35.00 - 3 . 29E - 0 2 1 .80E- 01 105 . 00 16 . 30 -2.l0E-01 3.33E- 01 129 . 22 2 . 97 1.77E+00 l. 82E+00 338 . 32 5 . 30 9 . 35E-01 1 . 13E+00 463 . 00 13 . 80 2 . 37E - 01 4 . 80E- 01 911 . 23 16 . 70 9 . 92E- 0 1 6. llE- 01

+ AM- 241 59.54 36 . 30 -8.95E - 02 1.76E- 0l 1. 7 6E- 01

+ CM-243 103.76 23.00 -8 . 51E - 03 1 . 12E-01 1.12E-01 228 . 18 10 . 60 l . 62E- 0 1 2 . 33E-01 277 . 60 14 . 00 - 6 . 96E - 02 1. 90E-01

+

. = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perfonn the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

FSS RELEASE RECORD REVISION 1 L1-010-102 EXCAVATION

~

SURVEY UNIT L1-SUB-TDS LACROSSE SOLUTIONS ATTACHMENT 8 GEL LABORATORIES ANALYTICAL REPORTS 210

le;'l~* ILaboratories LLC POB01r:i07t2 Chn~esron SC29417 a member of The GEL Group INC 2040 Sa*,*age Rond Charleston SC 29407 P 84:i_556.8171 F 84'.3766-1 178' ge l. com February 26, 2018 Mr. Jason Q. Spaide LaCrosseSolutions S4601 State Hwy 35 Genoa, Wisconsin 54632 Re: LACBWR Site Restoration Project Work Order: 442612

Dear Mr. Spaide:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on January 30, 2018. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4453.

Sincerely,

~

Kaitlyn Stone for Edith Kent Project Manager Purchase Order: 672583 Enclosures

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report for ENRG070 LaCrosseSolutions, LLC (672583)

Client SDG: 442612 GEL Work Order: 442612 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a Tracer compound

• • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the 'U' qualifier above.

This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Edith Kent.

Reviewed by Page 2 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FSGS-010-SB Project: ENRG07001 Sample ID: 442612001 Client ID: ENRG070 Matrix: Soil Collect Date: 08-JAN-18 12:20 Receive Date: 30-JAN-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.206 +/-0.172 0.271 0.400 pCi/g KSDI 02/14/18 1410 1736879 The following Prep Methods were performed:

Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOl 01/30/18 1256 1735459 The following Analytical Methods were performed:

Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. l Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 90.7 (25%-125%)

Notes:

Counting Uncertainty is calculated at the 95% confidence level (1 .96-sigma).

Column headers are defmed as follows :

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 3 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-003-SB Project: ENRG07001 Sample ID: 442612002 Client ID: ENRG070 Matrix: Soil Collect Date: 15-JAN-18 09:57 Receive Date: 30-JAN-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 u 0.00405 +/-0.0225 0.0431 0.400 pCi/g JXR5 02/08/18 1341 1735499 Americium-243 u 0.0194 +/-0.0868 0.170 0.400 pCi/g Curium-243/244 u 0.00215 +/-0.0225 0.047 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 u 0.000501 +/-0.00354 0.00672 0.010 pCi/g JXR5 02/17/18 1552 1735500 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 u -0.00713 +/-0.0215 0.0605 0.400 pCi/g JXR5 02/13/18 1214 1738612 3 Plutonium-239/240 u -0.00475 +/-0.021 0.0548 0.400 pCi/g Liquid Scint Pu241 , Solid "Dry Weight Corrected" Plutonium-241 u -0.895 +/-2.01 3.46 5.00 pCi/g JXR5 02/15/18 0629 1738613 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 u -0.739 +/-1.51 2.55 5.00 pCi/g TXJI 02/16/18 0849 1736387 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu 154, Eu155 "Dry Weight Corrected" Cesium-137 0.0883 +/-0.0335 0.0245 1.00 pCi/g RXF2 02/01/18 1033 1735521 6 Cobalt-60 u 0.0135 +/-0.0161 0.0365 pCi/g Europium-152 u 0.00115 +/-0.0301 0.0613 pCi/g Europium-154 u -0.00388 +/-0.0407 0.0816 pCi/g Europium-155 u 0.00836 +/-0.0364 0.0708 pCi/g Niobium-94 u 0.00262 +/-0.013 0.0255 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 u 0.0623 +/-0.122 0.219 0.400 pCi/g KSDI 02/14/18 1410 1736879 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium u -0.202 +/-4.32 7.61 10.0 pCi/g MXH8 02/09/18 1651 1736372 8 Liquid Scint C14, Solid "As Received" Carbon-14 u 1.87 +/-2.37 3.99 5.00 pCi/g BXM4 02/08/18 1230 1736377 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 u -0.329 +/-0.284 0.495 2.00 pCi/g CXS7 02/24/18 0720 1741806 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 u 1.36 +/-3.24 4.64 10.0 pCi/g TXJI 02/21/18 0830 1736325 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 4 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-003-SB Project: ENRG07001 Sample ID: 442612002 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U 0.189 +/-1.56 2.69 5.00 pCi/g TXJl 02/16/18 1518 1736338 12 The following Prep Methods were performed:

Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOl 01/30/18 1256 1735459 The following Analytical Methods were performed:

Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-0l-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1 , Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 104 (15%-125%)

Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 30 (15%-125%)

Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 86.6 (15%-125%)

Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 79.8 (15%-125%)

Corrected" Plutonium-242 Tracer Liquid Scint Pu241 , Solid "Dry Weight Corrected" 79.8 (15%-125%)

Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 105 (25%-125%)

Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 97.7 (25%-125%)

Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 94 (15%-125%)

Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 74.8 (15%-125%)

Nickel Carrier Liquid Scint Ni 63, Solid "Dry Weight Corrected" 79 (25%-125%)

Notes:

Page 5 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-003-SB Project: ENRG07001 Sample ID: 442612002 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1 .96-sigma).

Column headers are defined as follows :

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 6 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-004-SB Project: ENRG07001 Sample ID: 442612003 Client ID: ENRG070 Matrix: Soil Collect Date: 15-JAN-18 10:07 Receive Date: 30-JAN-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 u 0.0191 +/-0.0327 0.0286 0.400 pCi/g JXR5 02/08/18 1341 1735499 Americium-243 u 0.00256 +/-0.0268 0.0559 0.400 pCi/g Curium-243/244 u -0.00453 +/-0.020 0.0522 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 u -4.00E-10 +/-0.00326 0.00644 0.010 pCi/g JXR5 02/17/18 1609 1735500 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 u 0.0183 +/-0.0401 0.0712 0.400 pCi/g JXR5 02/14/18 1048 1738612 3 Plutonium-239/240 u -0.00165 +/-0.0163 0.037 0.400 pCi/g Liquid Scint Pu241 , Solid "Dry Weight Corrected" Plutonium-241 u -1.09 +/-1.67 2.88 5.00 pCi/g JXR5 02/15/18 0833 1738613 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 u -0.124 +/-1.18 2.14 5.00 pCi/g TXJI 02/16/18 0907 1736387 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu 154, Eu155 "Dry Weight Corrected" Cesium-137 0.103 +/-0.0413 0.0324 1.00 pCi/g RXF2 02/01/18 1033 1735521 6 Cobalt-60 0.0596 +/-0.0478 0.0315 pCi/g Europium-152 u 0.0092 +/-0.0353 0.0713 pCi/g Europium-154 u -0.000326 +/-0.052 0.104 pCi/g Europium-155 u -0.0301 +/-0.0435 0.0843 pCi/g Niobium-94 u 0.00601 +/-0.0172 0.0335 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 u 0.0229 +/-0.178 0.334 0.400 pCi/g KSDl 02/14/18 1410 1736879 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium u -0.528 +/-4.12 7.28 10.0 pCi/g MXH8 02/09/18 1737 1736372 8 Liquid Scint C14, Solid "As Received" Carbon-14 u -0.869 +/-2.03 3.52 5.00 pCi/g BXM4 02/08/18 1311 1736377 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 0.530 +/-0.310 0.513 2.00 pCi/g CXS7 02/24/18 0921 1741806 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 u 2.34 +/-3.47 4.92 10.0 pCi/g TXJI 02/21/18 0917 1736325 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 7 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-004-SB Project: ENRG07001 Sample ID: 442612003 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U 0.198 +/-1.84 3.18 5.00 pCi/g TXJl 02/16/18 1539 1736338 12 The following Prep Methods were performed:

Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOl 01/30/18 1256 1735459 The following Analytical Methods were performed:

Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-0l-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1 , Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 78.6 (15%-125%)

Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 78 (15%-125%)

Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 90.6 (15%-125%)

Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 96.4 (15%-125%)

Corrected" Plutonium-242 Tracer Liquid Scint Pu241 , Solid "Dry Weight Corrected" 96.4 (15%-125%)

Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 102 (25%-125%)

Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%)

Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 93.4 (15%-125%)

Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 74.2 (15%-125%)

Nickel Carrier Liquid Scint Ni 63, Solid "Dry Weight Corrected" 69.4 (25%-125%)

Notes:

Page 8 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-004-SB Project: ENRG07001 Sample ID: 442612003 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1 .96-sigma).

Column headers are defined as follows :

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 9 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-005-SB Project: ENRG07001 Sample ID: 442612004 Client ID: ENRG070 Matrix: Soil Collect Date: 15-JAN-18 10:20 Receive Date: 30-JAN-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 u 0.0115 +/-0.0263 0.0418 0.400 pCi/g JXR5 02/08/18 1341 1735499 Americium-243 u 0.017 +/-0.0408 0.0739 0.400 pCi/g Curium-243/244 u -0.00149 +/-0.0224 0.0522 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 u 0.000487 +/-0.00287 0.00539 0.010 pCi/g JXR5 02/17/18 1609 1735500 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 u -0.00419 +/-0.0185 0.0483 0.400 pCi/g JXR5 02/13/18 1214 1738612 3 Plutonium-239/240 u 0.00942 +/-0.0363 0.0704 0.400 pCi/g Liquid Scint Pu241 , Solid "Dry Weight Corrected" Plutonium-241 u -0.841 +/-1.91 3.29 5.00 pCi/g JXR5 02/15/18 1037 1738613 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 u -0.751 +/-1.41 2.37 5.00 pCi/g TXJl 02/16/18 1008 1736387 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu 154, Eu155 "Dry Weight Corrected" Cesium-137 0.107 +/-0.0375 0.0307 1.00 pCi/g RXF2 02/01/18 1033 1735521 6 Cobalt-60 0.0816 +/-0.0295 0.0336 pCi/g Europium-152 u 0.00482 +/-0.0394 0.0803 pCi/g Europium-154 u -0.00657 +/-0.0706 0.119 pCi/g Europium-155 u 0.0389 +/-0.044 0.0925 pCi/g Niobium-94 u -0.008 +/-0.0191 0.0339 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 u -0.0374 +/-0.155 0.306 0.400 pCi/g KSDl 02/14/18 1632 1736879 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium u 0.293 +/-4.16 7.29 10.0 pCi/g MXH8 02/09/18 1823 1736372 8 Liquid Scint C14, Solid "As Received" Carbon-14 u 1.40 +/-2.37 4.01 5.00 pCi/g BXM4 02/08/18 1352 1736377 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 u 0.289 +/-0.305 0.512 2.00 pCi/g CXS7 02/24/18 1122 1741806 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 u 0.159 +/-3.36 4.85 10.0 pCi/g TXJl 02/21/18 1004 1736325 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 10 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-005-SB Project: ENRG07001 Sample ID: 442612004 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U 1.09 +/-1.67 2.83 5.00 pCi/g TXJI 02/16/18 1601 1736338 12 The following Prep Methods were performed:

Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOI 01/30/18 1256 1735459 The following Analytical Methods were performed:

Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-0l-R 7 EPA 905.0 Modified/DOE RP501 Rev. l Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1 , Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 97.7 (15%-125%)

Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 94.6 (15%-125%)

Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 102 (15%-125%)

Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 85.7 (15%-125%)

Corrected" Plutonium-242 Tracer Liquid Scint Pu241 , Solid "Dry Weight Corrected" 85.7 (15%-125%)

Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 98.8 (25%-125%)

Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 86 (25%-125%)

Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 93.6 (15%-125%)

Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 77 (15%-125%)

Nickel Carrier Liquid Scint Ni 63, Solid "Dry Weight Corrected" 71 (25%-125%)

Notes:

Page 11 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-005-SB Project: ENRG07001 Sample ID: 442612004 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1 .96-sigma).

Column headers are defined as follows :

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 12 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-006-SB Project: ENRG07001 Sample ID: 442612005 Client ID: ENRG070 Matrix: Soil Collect Date: 15-JAN-18 12:13 Receive Date: 30-JAN-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 u 0.0176 +/-0.0345 0.0479 0.400 pCi/g JXR5 02/08/18 1341 1735499 Americium-243 u 0.00905 +/-0.038 0.0745 0.400 pCi/g Curium-243/244 u -0.00947 +/-0.0219 0.065 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 u 0.000427 +/-0.00414 0.00846 0.010 pCi/g JXR5 02/22/18 1352 1735500 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 u -0.0042 +/-0.029 0.0707 0.400 pCi/g JXR5 02/13/18 1214 1738612 3 Plutonium-239/240 u -0.0115 +/-0.0217 0.067 0.400 pCi/g Liquid Scint Pu241 , Solid "Dry Weight Corrected" Plutonium-241 u -2.8 +/-1.96 3.42 5.00 pCi/g JXR5 02/15/18 1242 1738613 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 u -1.71 +/-1.24 2.03 5.00 pCi/g TXJI 02/16/18 1010 1736387 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu 154, Eu155 "Dry Weight Corrected" Cesium-137 0.189 +/-0.0465 0.0243 1.00 pCi/g RXF2 02/01/18 1034 1735521 6 Cobalt-60 u 0.0434 +/-0.0259 0.0546 pCi/g Europium-152 u 0.00471 +/-0.0393 0.0712 pCi/g Europium-154 u -0.00487 +/-0.0422 0.0829 pCi/g Europium-155 u 0.0389 +/-0.0374 0.0786 pCi/g Niobium-94 u 0.00539 +/-0.0129 0.0259 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 u -0.0657 +/-0.125 0.262 0.400 pCi/g KSD1 02/14/18 1410 1736879 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium u 0.340 +/-4.43 7.76 10.0 pCi/g MXH8 02/09/18 1910 1736372 8 Liquid Scint C14, Solid "As Received" Carbon-14 u -1.07 +/-2.24 3.91 5.00 pCi/g BXM4 02/08/18 1434 1736377 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 0.628 +/-0.302 0.496 2.00 pCi/g CXS7 02/24/18 1323 1741806 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 u 1.02 +/-3.37 4.83 10.0 pCi/g TXJI 02/21/18 1052 1736325 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 13 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-006-SB Project: ENRG07001 Sample ID: 442612005 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U 0.796 +/-1.57 2.68 5.00 pCi/g TXJI 02/16/18 1622 1736338 12 The following Prep Methods were performed:

Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOI 01/30/18 1256 1735459 The following Analytical Methods were performed:

Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-0l-R 7 EPA 905.0 Modified/DOE RP501 Rev. l Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1 , Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 75 (15%-125%)

Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 89.5 (15%-125%)

Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 95.7 (15%-125%)

Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 80.8 (15%-125%)

Corrected" Plutonium-242 Tracer Liquid Scint Pu241 , Solid "Dry Weight Corrected" 80.8 (15%-125%)

Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 104 (25%-125%)

Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 93 (25%-125%)

Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 93.2 (15%-125%)

Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 77.3 (15%-125%)

Nickel Carrier Liquid Scint Ni 63, Solid "Dry Weight Corrected" 81.3 (25%-125%)

Notes:

Page 14 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-006-SB Project: ENRG07001 Sample ID: 442612005 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1 .96-sigma).

Column headers are defined as follows :

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 15 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-007-SB Project: ENRG07001 Sample ID: 442612006 Client ID: ENRG070 Matrix: Soil Collect Date: 15-JAN-18 12:20 Receive Date: 30-JAN-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 u -0.00172 +/-0.0148 0.0343 0.400 pCi/g JXR5 02/17/18 1134 1735499 Americium-243 u -0.0283 +/-0.0351 0.0984 0.400 pCi/g Curium-243/244 u 0.0127 +/-0.0288 0.0495 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 u 0.000528 +/-0.00373 0.00707 0.010 pCi/g JXR5 02/17/18 1609 1735500 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 u -0.00262 +/-0.0226 0.0523 0.400 pCi/g JXR5 02/13/18 1214 1738612 3 Plutonium-239/240 u -0.0105 +/-0.0242 0.0718 0.400 pCi/g Liquid Scint Pu241 , Solid "Dry Weight Corrected" Plutonium-241 u -2.05 +/-2.38 4.13 5.00 pCi/g JXR5 02/15/18 1446 1738613 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 u 0.188 +/-1.11 2.09 5.00 pCi/g TXJl 02/16/18 1021 1736387 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu 154, Eu155 "Dry Weight Corrected" Cesium-137 u 0.0378 +/-0.0262 0.0562 1.00 pCi/g RXF2 02/01/18 1034 1735521 6 Cobalt-60 u 0.0141 +/-0.0284 0.0509 pCi/g Europium-152 u -0.0438 +/-0.0662 0.0922 pCi/g Europium-154 u -0.0128 +/-0.0643 0.120 pCi/g Europium-155 u -0.0175 +/-0.0423 0.0807 pCi/g Niobium-94 u -0.0128 +/-0.0222 0.0387 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 u 0.0139 +/-0.117 0.229 0.400 pCi/g KSDl 02/14/18 1410 1736879 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium u 3.54 +/-5.41 9.20 10.0 pCi/g MXH8 02/10/18 1041 1736372 8 Liquid Scint C14, Solid "As Received" Carbon-14 u -0.0172 +/-2.09 3.60 5.00 pCi/g BXM4 02/08/18 1515 1736377 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 u 0.158 +/-0.320 0.542 2.00 pCi/g CXS7 02/24/18 1525 1741806 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 u 0.778 +/-3.54 5.09 10.0 pCi/g TXJl 02/21/18 1139 1736325 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 16 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-007-SB Project: ENRG07001 Sample ID: 442612006 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U -0.886 +/-1.71 3.03 5.00 pCi/g TXJI 02/16/18 1644 1736338 12 The following Prep Methods were performed:

Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOl 01/30/18 1256 1735459 The following Analytical Methods were performed:

Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-0l-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1 , Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 96.l (15%-125%)

Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 63.5 (15%-125%)

Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 84.2 (15%-125%)

Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 67.2 (15%-125%)

Corrected" Plutonium-242 Tracer Liquid Scint Pu24l , Solid "Dry Weight Corrected" 67.2 (15%-125%)

Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 105 (25%-125%)

Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%)

Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 91.2 (15%-125%)

Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 75.6 (15%-125%)

Nickel Carrier Liquid Scint Ni 63, Solid "Dry Weight Corrected" 73.4 (25%-125%)

Notes:

Page 17 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-007-SB Project: ENRG07001 Sample ID: 442612006 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1 .96-sigma).

Column headers are defined as follows :

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 18 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-008-SB Project: ENRG07001 Sample ID: 442612007 Client ID: ENRG070 Matrix: Soil Collect Date: 15-JAN-18 12:23 Receive Date: 30-JAN-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 u 0.0094 +/-0.0216 0.0343 0.400 pCi/g JXR5 02/2 1/18 0920 1735499 Americium-243 u 0.0147 +/-0.0316 0.0558 0.400 pCi/g Curium-243/244 u 0.00318 +/-0.0177 0.0338 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 u 0.00191 +/-0.00296 0.00458 0.010 pCi/g JXR5 02/17/18 1609 1735500 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 u -0.00214 +/-0.0211 0.0479 0.400 pCi/g JXR5 02/14/18 1048 1738612 3 Plutonium-239/240 u -0.00428 +/-0.0214 0.0549 0.400 pCi/g Liquid Scint Pu241 , Solid "Dry Weight Corrected" Plutonium-241 u -1.34 +/-2.47 4.26 5.00 pCi/g JXR5 02/15/18 1650 1738613 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 u -2.6 +/-1.50 2.21 5.00 pCi/g TXJI 02/16/18 1134 1736387 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu 154, Eu155 "Dry Weight Corrected" Cesium-137 0.0719 +/-0.0329 0.0211 1.00 pCi/g RXF2 02/01/18 1035 1735521 6 Cobalt-60 u -0.00941 +/-0.0133 0.0185 pCi/g Europium-152 u 0.00203 +/-0.036 0.0654 pCi/g Europium-154 u 0.0195 +/-0.0362 0.0752 pCi/g Europium-155 u 0.0367 +/-0.0382 0.0812 pCi/g Niobium-94 u -0.00305 +/-0.0108 0.0206 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 u 0.113 +/-0.183 0.319 0.400 pCi/g KSDI 02/14/18 1410 1736879 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium u -1.18 +/-4.10 7.31 10.0 pCi/g MXH8 02/09/18 2043 1736372 8 Liquid Scint C14, Solid "As Received" Carbon-14 u -0.832 +/-2.19 3.80 5.00 pCi/g BXM4 02/08/18 1556 1736377 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 u 0.198 +/-0.314 0.529 2.00 pCi/g CXS7 02/24/18 1726 1741806 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 u 3.00 +/-3.42 4.82 10.0 pCi/g TXJI 02/21/18 1226 1736325 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 19 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-008-SB Project: ENRG07001 Sample ID: 442612007 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U -0.16 +/-1.80 3.14 5.00 pCi/g TXJI 02/16/18 1705 1736338 12 The following Prep Methods were performed:

Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOI 01/30/18 1256 1735459 The following Analytical Methods were performed:

Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-I 6 DOE HASL 300, 4.5.2.3/Ga-0l-R 7 EPA 905.0 Modified/DOE RP501 Rev. I Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-I, Modified 12 DOE RESL Ni-I , Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 89 (15%-125%)

Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 89.5 (15%-125%)

Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 96 (15%-125%)

Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 66 (15%-125%)

Corrected" Plutonium-242 Tracer Liquid Scint Pu241 , Solid "Dry Weight Corrected" 66 (15%-125%)

Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 104 (25%-125%)

Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 81.4 (25%-125%)

Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 94.8 (15%-125%)

Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 77.7 (15%-125%)

Nickel Carrier Liquid Scint Ni 63, Solid "Dry Weight Corrected" 66.3 (25%-125%)

Notes:

Page 20 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-008-SB Project: ENRG07001 Sample ID: 442612007 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1 .96-sigma).

Column headers are defined as follows :

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 21 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-010-SB Project: ENRG07001 Sample ID: 442612008 Client ID: ENRG070 Matrix: Soil Collect Date: 15-JAN-18 12:35 Receive Date: 30-JAN-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 u -0.00335 +/-0.0148 0.0386 0.400 pCi/g JXR5 02/17/18 1134 1735499 Americium-243 u 0.0175 +/-0.0345 0.0584 0.400 pCi/g Curium-243/244 u 0.00523 +/-0.0196 0.033 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 u 0.00307 +/-0.00434 0.0068 0.010 pCi/g JXR5 02/2 1/18 1337 1735500 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 u -0.00662 +/-0.0153 0.0454 0.400 pCi/g JXR5 02/13/18 1214 1738612 3 Plutonium-239/240 u -0.00303 +/-0.0209 0.051 0.400 pCi/g Liquid Scint Pu241 , Solid "Dry Weight Corrected" Plutonium-241 u -0.359 +/-1.57 2.70 5.00 pCi/g JXR5 02/15/18 1854 1738613 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 u -0.426 +/-1.16 2.03 5.00 pCi/g TXJI 02/16/18 1135 1736387 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu 154, Eu155 "Dry Weight Corrected" Cesium-137 0.0563 +/-0.0312 0.0348 1.00 pCi/g RXF2 02/01/18 1036 1735521 6 Cobalt-60 u -0.00318 +/-0.014 0.0269 pCi/g Europium-152 u 0.0162 +/-0.0474 0.0848 pCi/g Europium-154 u 0.0327 +/-0.0471 0.104 pCi/g Europium-155 u 0.0132 +/-0.0435 0.0827 pCi/g Niobium-94 u 0.0114 +/-0.0178 0.0367 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 u -0.0503 +/-0.132 0.277 0.400 pCi/g KSDI 02/14/18 1411 1736879 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium u -0.841 +/-4.53 8.04 10.0 pCi/g MXH8 02/09/18 2129 1736372 8 Liquid Scint C14, Solid "As Received" Carbon-14 u -1.01 +/-2.22 3.87 5.00 pCi/g BXM4 02/08/18 1638 1736377 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 u 0.423 +/-0.312 0.519 2.00 pCi/g CXS7 02/24/18 1927 1741806 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 u 0.515 +/-3.29 4.69 10.0 pCi/g TXJI 02/21/18 1313 1736325 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 22 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-010-SB Project: ENRG07001 Sample ID: 442612008 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U -0.408 +/-1.62 2.84 5.00 pCi/g TXJI 02/16/18 1727 1736338 12 The following Prep Methods were performed:

Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOI 01/30/18 1256 1735459 The following Analytical Methods were performed:

Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-0l-R 7 EPA 905.0 Modified/DOE RP501 Rev. l Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1 , Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 79.6 (15%-125%)

Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am24 l Am243, Cm243/244, 76 (15%-125%)

Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 71.5 (15%-125%)

Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 105 (15%-125%)

Corrected" Plutonium-242 Tracer Liquid Scint Pu241 , Solid "Dry Weight Corrected" 105 (15%-125%)

Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 101 (25%-125%)

Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 81.4 (25%-125%)

Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 93.8 (15%-125%)

Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 84.7 (15%-125%)

Nickel Carrier Liquid Scint Ni 63, Solid "Dry Weight Corrected" 74.2 (25%-125%)

Notes:

Page 23 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: February 26, 2018 Company : LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632

Contact:

Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-010-SB Project: ENRG07001 Sample ID: 442612008 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1 .96-sigma).

Column headers are defined as follows :

DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 24 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 -www.gel.com QC Summa!:! Report Date: February 26, 2018 LaCrosseSolutions Page 1 of 7 S4601 State Hwy 35 Genoa, Wisconsin

Contact:

Mr. Jason Q. Spaide Workorder: 442612 Parmname NOM Sam~le Qual QC Units RPO% REC% Range Anlst Date Time Rad Alpha Spec Batch 1735499 QC1203962043 442612002 DUP Americium-241 u 0.00405 u 0.0105 pCi/g NIA NIA JXR5 02108118 13 :41 Uncertainty +l-0.0225 +l-0.0288 Americium-243 u 0.0194 u 0.0315 pCilg NIA NIA Uncertainty +l-0.0868 +l-0.0443 Curium-2431244 u 0.00215 u -0.00194 pCilg NIA NIA Uncertainty +l-0.0225 +l-0.0167 QC1203962044 LCS Americium-241 1.92 2.02 pCilg 106 (75%-125%) 02108118 13 :41 Uncertainty +l-0.280 Americium-243 u -0.00247 pCi/g (75%-125%)

Uncertainty +l-0.0231 Curium-2431244 2.40 2.44 pCi/g 101 (75%-125%)

Uncertainty +l-0.305 QC1203962042 MB Americium-241 u -0.00577 pCi/g 02117118 11 :35 Uncertainty +l-0.0134 Americium-243 u 0.000465 pCi/g Uncertainty +l-0.0214 Curium-2431244 u -0.00687 pCilg Uncertainty +l-0.0186 Batch 1735500 QC1203962046 442612002 DUP Neptunium-237 u 0.000501 u 5.03E-10 pCi/g NIA NIA JXR5 02117118 16:09 Uncertainty +l-0.00354 +l-0.00468 QC1203962047 LCS Neptunium-237 1.48 1.59 pCilg 107 (75%-125%) 02110118 16:03 Uncertainty +l-0.072 QC1203962045 MB Neptunium-237 u -0.0012 pCi/g 02110118 16:03 Uncertainty +l-0.0029 Page 25 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 -www.gel.com QC Summa!:!

Workorder: 442612 Page 2 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1738612 QC1203970080 442612002 DUP Plutonium-238 u -0.00713 u -0.00563 pCi/g NIA NIA JXR5 02113118 12:14 Uncertainty +l-0.0215 +l-0.017 Plutonium-2391240 u -0.00475 u 0.00625 pCi/g NIA NIA Uncertainty +l-0.021 +l-0.028 QC I203970081 LCS Plutonium-238 u -0.00663 pCilg 02113118 13 :56 Uncertainty +l-0.020 Plutonium-2391240 1.94 1.95 pCilg 100 (75%-125%)

Uncertainty +l-0.263 QC1203970079 MB Plutonium-238 u 0.0108 pCilg 02/13118 14:03 Uncertainty +l-0.0296 Plutonium-2391240 u 0.00437 pCilg Uncertainty +l-0.0243 Batch 1738613 QC1203970083 442612002 DUP Plutonium-241 u -0.895 u -1.53 pCi/g NIA NIA JXR5 02115118 23 :02 Uncertainty +l-2.01 +l-1.77 QC1203970084 LCS Plutonium-241 70.1 55.7 pCilg 79.6 (75%-125%) 02116118 01 :06 Uncertainty +l-3 .03 QC1203970082 MB Plutonium-241 u -0.222 pCi/g 02115118 20:58 Uncertainty +l-1.93 Rad Gamma Spec Batch 1735521 QC1203962085 442612002 DUP Cesium-137 0.0883 0.0764 pCilg 14.5 (0%- 100%) RXF2 02101/18 15 :34 Uncertainty +l-0.0335 +l-0.0308 Cobalt-60 u 0.0135 u -0.00256 pCilg NIA NIA Uncertainty +l-0.0161 +l-0.0182 Europium-152 u 0.00115 u -0.0269 pCi/g NIA NIA Uncertainty +l-0.0301 +l-0.0465 Page 26 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 -www.gel.com QC Summa!:!

Workorder: 442612 Page 3 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1735521 Europium-154 u -0.00388 u 0.0249 pCilg NIA NIA RXF2 02101/18 15 :34 Uncertainty +l-0.0401 +l-0.0582 Europium-155 u 0.00836 u 0.000633 pCi/g NIA NIA Uncertainty +l-0.0364 +l-0.0439 Niobium-94 u 0.00262 u 0.00666 pCi/g NIA NIA Uncertainty +l-0.013 +l-0.0164 QC1203962086 LCS Americium-241 488 504 pCilg 103 (75%-125%) 02101/18 10:37 Uncertainty +l-8.25 Cesium-137 174 171 pCilg 98.1 (75%-125%)

Uncertainty +l-2.94 Cobalt-60 135 132 pCi/g 97.8 (75%-125%)

Uncertainty +l-3 .13 Europium-152 u -0.485 pCi/g Uncertainty +l-1 .23 Europium-154 u -0.0339 pCi/g Uncertainty +l-0.907 Europium-155 u -0.0701 pCi/g Uncertainty +l-1.12 Niobium-94 u 0.257 pCi/g Uncertainty +l-0.407 QC1203962084 MB Cesium-137 u -0.00302 pCi/g 02101/18 10:36 Uncertainty +l-0.0137 Cobalt-60 u -0.00916 pCi/g Uncertainty +l-0.0121 Europium-152 u 0.0278 pCi/g Uncertainty +l-0.0283 Europium-154 u -0.049 pCi/g Uncertainty +l-0.0463 Europium-155 u 0.0503 pCi/g Uncertainty +l-0.0469 Page 27 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 -www.gel.com QC Summa!:!

Workorder: 442612 Page 4 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1735521 Niobium-94 u 0.00513 pCilg RXF2 02101/18 10:36 Uncertainty +l-0.012 Batch 1736387 QC1203964316 442612002 DUP Nickel-59 u -0.739 u -0.997 pCi/g NIA NIA TXJl 02116118 13 :23 Uncertainty +l-1.51 +l-1.26 QC1203964317 LCS Nickel-59 87.3 77.9 pCilg 89.3 (75%-125%) 02116118 13 :23 Uncertainty +l-5 .17 QC1203964315 MB Nickel-59 u 0.108 pCilg 02116118 11 :36 Uncertainty +l-1.42 Rad Gas Flow Batch 1736879 QC1203965530 442612005 DUP Strontium-90 u -0.0657 u -0.0745 pCilg NIA NIA KSDl 02114118 14:10 Uncertainty +l-0.125 +l-0.133 QC1203965531 LCS Strontium-90 14.6 14.1 pCi/g 96.7 (75%-125%) 02114118 14:10 Uncertainty +l-0.765 QC1203965529 MB Strontium-90 u -0.155 pCilg 02114118 14:10 Uncertainty +l-0.160 Rad Liquid Scintillation Batch 1736325 QC1203964127 442612002 DUP Iron-55 u 1.36 u 3.45 pCi/g NIA NIA TXJl 02121/18 14:47 Uncertainty +l-3.24 +l-3 .26 QC1203964128 LCS Iron-55 112 115 pCi/g 103 (75%-125%) 02121/18 15 :34 Uncertainty +l-5 .55 QC1203964126 MB Iron-55 u 0.546 pCilg 02121/18 14:00 Uncertainty +l-3 .02 Page 28 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 -www.gel.com QC Summa!:!

Workorder: 442612 Page 5 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1736338 QC1203964166 442612002 DUP Nickel-63 u 0.189 u -0.80 pCilg NIA NIA TXJI 02116118 18:10 Uncertainty +l-1.56 +l-1.82 QC1203964167 LCS Nickel-63 80.0 89.0 pCi/g 111 (75%-125%) 02116118 18:31 Uncertainty +l-3 .76 QC1203964165 MB Nickel-63 u 0.549 pCi/g 02116118 17:48 Uncertainty +l-1.84 Batch 1736372 QC1203964267 442612002 DUP Tritium u -0.202 u 8.42 pCi/g NIA NIAMXH8 02109118 23 :02 Uncertainty +l-4.32 +l-5 .66 QC1203964269 LCS Tritium 59.9 52.4 pCilg 87.4 (75%-125%) 02110118 00:34 Uncertainty +l-6.04 QC1203964266 MB Tritium u -0.151 pCi/g 02109118 22 :15 Uncertainty +l-3 .96 QC1203964268 442612002 MS Tritium 184 u -0.202 149 pCilg 80.9 (75%-125%) 02109118 23 :48 Uncertainty +l-4.32 +l-18.4 Batch 1736377 QC1203964283 442612002 DUP Carbon-14 u 1.87 u -1.07 pCi/g NIA NIABXM4 02108118 18:00 Uncertainty +l-2.37 +l-2.22 QC1203964285 LCS Carbon-14 130 125 pCi/g 96 (75%-125%) 02108118 19:23 Uncertainty +l-4.20 QC1203964282 MB Carbon-14 u -0.0748 pCilg 02108118 17:19 Uncertainty +l-2.04 QC1203964284 442612002 MS Carbon-14 298 u 1.87 291 pCi/g 97.7 (75%-125%) 02108118 18:41 Uncertainty +l-2.37 +l-9.69 Page 29 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 -www.gel.com QC Summary Workorder: 442612 Page 6 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1741806 QC1203977935 442612002 DUP Technetium-99 u -0.329 u 1.08 pCi/g NIA NIA CXS7 02/26/18 06:08 Uncertainty +/-0.284 +/-1.03 QC1203977936 LCS Technetium-99 40.1 38.8 pCi/g 96.7 (75%-125%) 02/25/18 00:27 Uncertainty +/-0.893 QC1203977934 MB Technetium-99 u 0.428 pCi/g 02/24/1821 :28 Uncertainty +/-0.292 Notes:

Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

The Qualifiers in this report are defined as follows :

• • Analyte is a Tracer compound

< Result is less than value reported

> Result is greater than value reported BD Results are either below the MDC or tracer recovery is low FA Failed analysis.

H Analytical holding time was exceeded J Value is estimated K Analyte present. Reported value may be biased high. Actual value is expected to be lower.

L Analyte present. Reported value may be biased low. Actual value is expected to be higher.

M M if above MDC and less than LLD M REMP Result> MDC/CL and < RDL NIA RPD or %Recovery limits do not apply.

Nl See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.

R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.

UI Gamma Spectroscopy--Uncertain identification UJ Gamma Spectroscopy--Uncertain identification UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.

X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y Other specific qualifiers were required to properly define the results. Consult case narrative.

Page 30 of 44

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 -www.gel.com QC Summary Workorder: 442612 Page 7 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.

h Preparation or preservation holding time was exceeded NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable.

/\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/- the RL is used to evaluate the DUP result.

• Indicates that a Quality Control parameter was not within specifications.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

Page 31 of 44

Radiochemistry Technical Case Narrative LaCrosseSolutions, LLC (ENRG)

SDG #: 442612 Product: Alphaspec Isotopic Am241 Am243, Cm243/244, Solid Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1735499 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1735459 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612002 Ll-SUB-TDS-FJGS-003-SB 442612003 L l-SUB-TDS-FJGS-004-SB 442612004 Ll-SUB-TDS-FJGS-005-SB 442612005 L l-SUB-TDS-FJGS-006-SB 442612006 L l-SUB-TDS-FJGS-007-SB 442612007 L l-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203962042 Method Blank (MB) 1203962043 442612002(Ll-SUB-TDS-FJGS-003-SB) Sample Duplicate (DUP) 1203962044 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Recounts The Am-243 traced portion of samples 1203962042 (MB), 442612006 (Ll-SUB-TDS-FJGS-007-SB) and 442612008 (Ll-SUB-TDS-FJGS-010-SB) were recounted due to a peak shift. The recounts are reported. The Cm-244 traced portion of sample 1203962043 (L 1-SUB-TDS-FJGS-003-SBDUP) was recounted due to results more negative than the three sigma TPU and then counted again due to a suspected false positive. The third count is reported. The Am-243 traced portion of sample 442612007 (Ll-SUB-TDS-FJGS-008-SB) was recounted due to a peak shift and then counted again due to a suspected false positive. The third count is reported.

Miscellaneous Information Manual Integration Manual integration of alpha spectroscopy spectra 442612006 (Ll-SUB-TDS-FJGS-007-SB) was performed to fully separate counts in Regions of Interest which would have been biased.

PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

Additional Comments The tracer peak centroid for the Cm-244 traced portion of sample 442612005 (Ll-SUB-TDS-FJGS-006-SB) is greater than 50 keV from the expected library energy value for the tracer; however, the tracer yield requirement was met and the tracer peak is within the tracer region of interest.

Product: Alphaspec Np, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-032 REV# 21 Analytical Batch: 1735500 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1735459 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612002 Ll-SUB-TDS-FJGS-003-SB 442612003 Ll-SUB-TDS-FJGS-004-SB 442612004 Ll-SUB-TDS-FJGS-005-SB 442612005 Ll-SUB-TDS-FJGS-006-SB 442612006 L l-SUB-TDS-FJGS-007-SB 442612007 Ll-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203962045 Method Blank (MB) 1203962046 442612002(Ll-SUB-TDS-FJGS-003-SB) Sample Duplicate (DUP) 1203962047 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Recounts Samples 1203962046 (Ll-SUB-TDS-FJGS-003-SBDUP), 442612002 (Ll-SUB-TDS-FJGS-003-SB),

442612003 (Ll-SUB-TDS-FJGS-004-SB), 442612004 (Ll-SUB-TDS-FJGS-005-SB), 442612006 (Ll-SUB-TDS-FJGS-007-SB) and 442612007 (Ll-SUB-TDS-FJGS-008-SB) were recounted due to high MDCs. The recounts are reported. Sample 442612005 (Ll-SUB-TDS-FJGS-006-SB) was recounted twice due to high MDC. The third count is reported. Sample 442612008 (Ll-SUB-TDS-FJGS-010-SB) was recounted due to high MDC and then again due to a false positive. The third count is reported.

Pa~l.8~1Qtories u.c PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

Product: Alphaspec Pu238, 239/240, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1738612 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1735459 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612002 Ll-SUB-TDS-FJGS-003-SB 442612003 Ll-SUB-TDS-FJGS-004-SB 442612004 Ll-SUB-TDS-FJGS-005-SB 442612005 Ll-SUB-TDS-FJGS-006-SB 442612006 L l-SUB-TDS-FJGS-007-SB 442612007 Ll-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203970079 Method Blank (MB) 1203970080 442612002(Ll-SUB-TDS-FJGS-003-SB) Sample Duplicate (DUP) 1203970081 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Sample Re-prep/Re-analysis Samples were reprepped due to low carrier/tracer yield. The re-analysis is being reported.

Recounts Samples 442612003 (Ll-SUB-TDS-FJGS-004-SB) and 442612007 (Ll-SUB-TDS-FJGS-008-SB) were recounted due to a peak shift. The recounts are reported.

Product: Dry Weight Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1735459 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612001 Ll-SUB-TDS-FSGS-010-SB 442612002 Ll-SUB-TDS-FJGS-003-SB 442612003 Ll-SUB-TDS-FJGS-004-SB PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

442612004 L l-SUB-TDS-FJGS-005-SB 442612005 L l-SUB-TDS-FJGS-006-SB 442612006 L l-SUB-TDS-FJGS-007-SB 442612007 L l-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB The samples in this SDG were analyzed on an "as received" basis.

Data Summary:

There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.

Product: Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 Analytical Method: DOE HASL 300, 4.5 .2.3/Ga-0l-R Analytical Procedure: GL-RAD-A-013 REV# 27 Analytical Batch: 1735521 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1735459 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612002 Ll-SUB-TDS-FJGS-003-SB 442612003 Ll-SUB-TDS-FJGS-004-SB 442612004 Ll-SUB-TDS-FJGS-005-SB 442612005 Ll-SUB-TDS-FJGS-006-SB 442612006 L 1-SUB-TDS-FJGS-007-SB 442612007 Ll-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203962084 Method Blank (MB) 1203962085 442612002(Ll-SUB-TDS-FJGS-003-SB) Sample Duplicate (DUP) 1203962086 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.

Product: Gamma Ni59, Solid Pa~l.8~1Qtories u.c PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

Analytical Method: DOE RESL Ni-1 Analytical Procedure: GL-RAD-A-022 REV# 18 Analytical Batch: 1736387 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1735459 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612002 Ll-SUB-TDS-FJGS-003-SB 442612003 L l-SUB-TDS-FJGS-004-SB 442612004 Ll-SUB-TDS-FJGS-005-SB 442612005 Ll-SUB-TDS-FJGS-006-SB 442612006 L 1-SUB-TDS-FJGS-007-SB 442612007 Ll-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203964315 Method Blank (MB) 1203964316 442612002(Ll-SUB-TDS-FJGS-003-SB) Sample Duplicate (DUP) 1203964317 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.

Product: GFPC, Sr90, Solid Analytical Method: EPA 905 .0 Modified/DOE RP50l Rev. 1 Modified Analytical Procedure: GL-RAD-A-004 REV# 19 Analytical Batch: 1736879 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1735459 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612001 Ll-SUB-TDS-FSGS-010-SB 442612002 Ll-SUB-TDS-FJGS-003-SB 442612003 Ll-SUB-TDS-FJGS-004-SB 442612004 Ll-SUB-TDS-FJGS-005-SB 442612005 Ll-SUB-TDS-FJGS-006-SB 442612006 Ll-SUB-TDS-FJGS-007-SB 442612007 Ll-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203965529 Method Blank (MB)

Pa~ ~ ( Qtories u.c PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

1203965530 442612005(Ll-SUB-TDS-FJGS-006-SB) Sample Duplicate (DUP) 1203965531 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Recounts Sample 442612004 (Ll-SUB-TDS-FJGS-005-SB) was recounted due to results more negative than the three sigma TPU. The second count is reported.

Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 19 Analytical Batch: 1738613 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1735459 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612002 Ll-SUB-TDS-FJGS-003-SB 442612003 Ll-SUB-TDS-FJGS-004-SB 442612004 Ll-SUB-TDS-FJGS-005-SB 442612005 Ll-SUB-TDS-FJGS-006-SB 442612006 L 1-SUB-TDS-FJGS-007-SB 442612007 Ll-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203970082 Method Blank (MB) 1203970083 442612002(Ll-SUB-TDS-FJGS-003-SB) Sample Duplicate (DUP) 1203970084 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Sample Re-prep/Re-analysis Pa~'M~!Qtories u.c PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

Samples were reprepped due to low carrier/tracer yield. The re-analysis is being reported.

Product: Liquid Scint Fe55, Solid Analytical Method: DOE RESL Fe-1, Modified Analytical Procedure: GL-RAD-A-040 REV# 13 Analytical Batch: 1736325 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1735459 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612002 Ll-SUB-TDS-FJGS-003-SB 442612003 Ll-SUB-TDS-FJGS-004-SB 442612004 Ll-SUB-TDS-FJGS-005-SB 442612005 Ll-SUB-TDS-FJGS-006-SB 442612006 L l-SUB-TDS-FJGS-007-SB 442612007 Ll-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203964126 Method Blank (MB) 1203964127 442612002(Ll-SUB-TDS-FJGS-003-SB) Sample Duplicate (DUP) 1203964128 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.

Product: Liquid Scint Ni63, Solid Analytical Method: DOE RESL Ni-1, Modified Analytical Procedure: GL-RAD-A-022 REV# 18 Analytical Batch: 1736338 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1735459 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612002 Ll-SUB-TDS-FJGS-003-SB Pa~l.8~1Qtories u.c PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

442612003 L l-SUB-TDS-FJGS-004-SB 442612004 L l-SUB-TDS-FJGS-005-SB 442612005 L l-SUB-TDS-FJGS-006-SB 442612006 L l-SUB-TDS-FJGS-007-SB 442612007 L l-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203964165 Method Blank (MB) 1203964166 442612002(Ll-SUB-TDS-FJGS-003-SB) Sample Duplicate (DUP) 1203964167 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

Data Summary:

There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.

Product: LSC, Tritium Distillation, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 22 Analytical Batch: 1736372 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612002 Ll-SUB-TDS-FJGS-003-SB 442612003 Ll-SUB-TDS-FJGS-004-SB 442612004 Ll-SUB-TDS-FJGS-005-SB 442612005 Ll-SUB-TDS-FJGS-006-SB 442612006 L 1-SUB-TDS-FJGS-007-SB 442612007 Ll-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203964266 Method Blank (MB) 1203964267 442612002(Ll-SUB-TDS-FJGS-003-SB) Sample Duplicate (DUP) 1203964268 442612002(Ll-SUB-TDS-FJGS-003-SB) Matrix Spike (MS) 1203964269 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on an "as received" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Recounts Sample 442612006 (Ll-SUB-TDS-FJGS-007-SB) was recounted to verify sample results. Recount is reported.

Miscellaneous Information Pa~~(Qtories u.c PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

Additional Comments The matrix spike, 1203964268 (Ll-SUB-TDS-FJGS-003-SBMS), aliquot was reduced to conserve sample volume.

Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 15 Analytical Batch: 1736377 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612002 Ll-SUB-TDS-FJGS-003-SB 442612003 Ll-SUB-TDS-FJGS-004-SB 442612004 Ll-SUB-TDS-FJGS-005-SB 442612005 Ll-SUB-TDS-FJGS-006-SB 442612006 L 1-SUB-TDS-FJGS-007-SB 442612007 Ll-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203964282 Method Blank (MB) 1203964283 442612002(Ll-SUB-TDS-FJGS-003-SB) Sample Duplicate (DUP) 1203964284 442612002(Ll-SUB-TDS-FJGS-003-SB) Matrix Spike (MS) 1203964285 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on an "as received" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Miscellaneous Information Additional Comments The matrix spike, 1203964284 (Ll-SUB-TDS-FJGS-003-SBMS), aliquot was reduced to conserve sample volume.

Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 5 Analytical Batch: 1741806 The following samples were analyzed using the above methods and analytical procedure(s).

GEL Sample ID# Client Sample Identification 442612002 Ll-SUB-TDS-FJGS-003-SB Pa~ ~ ( Qtories u.c PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

442612003 L l-SUB-TDS-FJGS-004-SB 442612004 L l-SUB-TDS-FJGS-005-SB 442612005 L l-SUB-TDS-FJGS-006-SB 442612006 L l-SUB-TDS-FJGS-007-SB 442612007 L l-SUB-TDS-FJGS-008-SB 442612008 Ll-SUB-TDS-FJGS-010-SB 1203977934 Method Blank (MB) 1203977935 442612002(Ll-SUB-TDS-FJGS-003-SB) Sample Duplicate (DUP) 1203977936 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on an "as received" basis.

Data Summary:

All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.

Technical Information Sam pie Re-prep/Re-analysis Samples were reprepped due to high relative percent difference/relative error ratio. The re-analysis is being reported.

Recounts Sample 1203977935 (Ll-SUB-TDS-FJGS-003-SBDUP) was recounted due to results more negative than the three sigma TPU. The second count is reported.

Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com

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within (0 ~ 6 deg. C)?* "all leo,peralW'CI are recudcd In Celsius TEMP: ~d '~

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Sampla ID'* wl Contalnera Affcctod:

Samples requiring chemical prcservadon 6

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If Yes, Aro Encores or Soil Kits present? Yes_ No_ (Jfyes, take to VOAFi:cezcr)

Po VOA vials contain acid preservation? Yes . No_N/A.__'(lfunknown, select No)

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7 Analysis? Sample ID's and containers affected:

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8 Samples received within hi>lding time?

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Comments (Use Continuatio11 Fonnifneedcd):

I I PM (or PMA) review: Initials eljit-/ Date tJ1 /3/ //f Page__L.orL r

GL*CHL..SR-001 Rev 5 Page 43 of 44 '

List of current GEL Certifications as of 26 February 2018 State Certification Alaska 17-018 Arkansas 88-0651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 Delaware SC00012 DoD ELAP/ ISOl 7025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283, P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho Chemistry SC00012 Idaho Radiochemistry SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana NELAP 03046 (AI33904)

Louisiana SDWA LA180011 Maryland 270 Massachusetts M-SC012 Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada SC000122018-1 New Hampshire NELAP 205415 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 S.Carolina Radchem 10120002 South Carolina Chemistry 10120001 Tennessee TN 02934 TexasNELAP T104704235-18-13 UtahNELAP scooo 122017-25 Vermont VT87156 Virginia NELAP 460202 Washington C780 West Virginia 997404 Page 44 of 44