ML20352A258
| ML20352A258 | |
| Person / Time | |
|---|---|
| Site: | La Crosse File:Dairyland Power Cooperative icon.png |
| Issue date: | 11/02/2020 |
| From: | La CrosseSolutions |
| To: | Office of Nuclear Material Safety and Safeguards |
| Shared Package | |
| ML20356A041 | List:
|
| References | |
| LC-2020-0023 | |
| Download: ML20352A258 (508) | |
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{{#Wiki_filter:~ LACROSSESOLUTIONS LA CROSSE BOILING WATER REACTOR FINAL STATUS SURVEY RELEASE RECORD SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND REVISION 1
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Robert F. Yetter III Oct 25 2020 1:55 PM PREPARED BY / DATE: cosign R. F. Yetter III, FSS Specialist Mitchell Uz REVIEWED BY / DATE: ~~ Oct 27 2020 8:00 AM cosign M. D. Uz, FSS Specialist Robert F. Yetter
- RJ,.e,uj.~ Oct 27 2020 11 :05 AM REVIEWED BY / DATE: cosign R. Yetter, Director, Radiological Site Closure Sarah Roberts Oct 27 2020 12:55 PM REVIEWED BY / DATE: coogn S. Roberts, VP Radiological Programs Scott G. Zoller Oct 29 2020 9:37 AM APPROVED BY / DATE:
S. Zoller, FSS Manager 1
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS TABLE OF CONTENTS
- 1. EXECUTIVE
SUMMARY
................................................................................................................................. 5
- 2. SURVEY UNIT DESCRIPTION ....................................................................................................................... 5
- 3. CLASSIFICATION BASIS ................................................................................................................................. 5
- 4. DATA QUALITY OBJECTIVES .................................................................................................................... 10
- 5. SURVEY DESIGN ............................................................................................................................................. 14
- 6. SURVEY IMPLEMENTATION ...................................................................................................................... 19
- 7. SURVEY RESULTS .......................................................................................................................................... 21
- 8. QUALITY CONTROL ...................................................................................................................................... 29
- 9. INVESTIGATIONS AND RESULTS .............................................................................................................. 29
- 10. REMEDIATION AND RESULTS ................................................................................................................... 29
- 11. CHANGES FROM THE FINAL STATUS SURVEY PLAN ........................................................................ 29
- 12. DATA QUALITY ASSESSMENT (DQA) ....................................................................................................... 30
- 13. ANOMALIES ..................................................................................................................................................... 30
- 14. CONCLUSION .................................................................................................................................................. 31
- 15. REFERENCES................................................................................................................................................... 31
- 16. ATTACHMENTS .............................................................................................................................................. 32 ATTACHMENT 1 FIGURE ................................................................................................................................... 33 ATTACHMENT 2 SCAN DATA ............................................................................................................................. 35 ATTACHMENT 3 SIGN TEST ............................................................................................................................... 41 ATTACHMENT 4 QUALITY CONTROL ASSESSMENT ...................................................................................... 43 ATTACHMENT 5 CONSULTATION TRIGGERS FOR RESIDENTIAL SOIL CONCENTRATIONS ................... 45 ATTACHMENT 6 GRAPHICAL PRESENTATIONS ............................................................................................. 47 ATTACHMENT 7 SAMPLE ANALYTICAL REPORTS ......................................................................................... 51 ATTACHMENT 8 GEL LABORATORIES ANALYTICAL REPORTS ................................................................. 338 2
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS LIST OF TABLES Table 3 Statistical Quantities for Cs-137 and Co-60 from the Characterization Survey .................................. 7 Table 3-2 Off-site Analysis for Characterization Samples ..................................................................................... 8 Table 3-3 Off-site Analysis for RA Samples ............................................................................................................ 9 Table 4 Dose Significant Radionuclides and Mixture for Soil .......................................................................... 11 Table 4 Base Case DCGLs for Soil ...................................................................................................................... 13 Table 4 Operational DCGLs for Soil ................................................................................................................... 13 Table 5-1 Soil Surrogate Ratio ............................................................................................................................... 14 Table 5-2 Action Levels for Survey Unit L2-011-104 ........................................................................................... 15 Table 5-3 Systematic Sample Locations ................................................................................................................. 16 Table 5-4 Judgmental and Investigational Sample Locations ............................................................................. 17 Table 5-5 Investigation Levels ................................................................................................................................ 18 Table 5-6 Synopsis of Survey Design...................................................................................................................... 18 Table 7-1 Synopsis of Scan Results ........................................................................................................................ 21 Table 7 Summary of Gamma Spectroscopy Results for Samples Comprising the Statistical Sample Population ........................................................................................................................................................... 25 Table 7 Basic Statistical Properties of Systematic Sample Population ............................................................. 25 Table 7 Off-Site Analysis Results......................................................................................................................... 26 Table 7 Summary of Gamma Spectroscopy Results for Judgmental and Investigational Samples .............. 26 Table 7 Summary of Gamma Spectroscopy Results for QC Samples .............................................................. 27 Table 7 Sum-of-Fractions for Systematic and QC Samples .............................................................................. 27 Table 7-8 Sum-of-Fractions for Judgmental and Investigational Samples ........................................................ 28 Table 16-1 Survey Unit L2-011-104 Complete Scan Data .................................................................................... 36 Table 16-2 Survey Unit L2-011-104 Sign Test ....................................................................................................... 42 Table 16-3 Survey Unit L2-011-104 QC Assessment ............................................................................................ 44 LIST OF FIGURES Figure 16 Survey Unit L2-011-104 Systematic and Judgmental Sample Locations Map ............................... 34 Figure 16 Quantile Plot for Cs-137 Concentration ............................................................................................ 48 Figure 16 Histogram for Cs-137 Concentration ................................................................................................. 49 Figure 16 Retrospective Power Curve for L2-011-104 ...................................................................................... 50 3
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS LIST OF ACRONYMS AND ABBREVIATIONS ALARA As Low As Reasonably Achievable DQA Data Quality Assessment DQO Data Quality Objective DCGL Derived Concentration Guideline Level DCGLS Soil Derived Concentration Guideline Level FSS Final Status Survey GPS Global Positioning System HSA Historical Site Assessment HTD Hard-to-Detect IC Insignificant Contributors LACBWR La Crosse Boiling Water Reactor LBGR Lower Bound of the Gray Region LTP License Termination Plan MARSSIM Multi-Agency Radiation Survey and Site Investigation Manual MDC Minimum Detectable Concentration NaI Sodium Iodide OpDCGLS Soil Operational Derived Concentration Guideline Level QAPP Quality Assurance Project Plan QC Quality Control RA Radiological Assessment ROC Radionuclides of Concern SOF Sum-of-Fractions TEDE Total Effective Dose Equivalent UBGR Upper Bound of the Gray Region UCL Upper Confidence Limit 4
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS
- 1. EXECUTIVE
SUMMARY
This Final Status Survey (FSS) Release Record for survey unit L2-011-104, G3 Crib House, Circulating Water Discharge Land, has been generated in accordance with LaCrosseSolutions procedure LC-FS-PR-009, Final Status Survey Data Reporting (Reference 1) and satisfies the requirements of Section 5.11 of the La Crosse Boiling Water Reactor License Termination Plan (LACBWR LTP) (Reference 2). An FSS sample plan for this survey unit was developed in accordance with LaCrosseSolutions procedure LC-FS-PR-002, Final Status Survey Package Development (Reference 3), the LACBWR LTP, and with guidance from NUREG-1575, Revision 1, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM) (Reference 4). Survey unit L2-011-104, an open land survey unit, has a MARSSIM classification of 2. A survey plan was designed based upon use of the Sign Test as the nonparametric statistical test for compliance. Both the Type I (a) and Type II ( ) decision error rates were set at 0.05. As a systematic sample population, fourteen (14) soil samples were acquired from the survey unit. In addition, soil scanning was performed on 25% of the total surface area in the survey unit. The analytical results for all soil samples taken in survey unit L2-011-104 indicate that the maximum Sum-of-Fractions (SOF), considering the concentration of all applicable Radionuclides of Concern (ROC) either by direct measurement or by inference, is equal to 0.0569 when applying the respective Operational Derived Concentration Guideline Levels (OpDCGLS) for soil. Therefore, the null hypothesis is rejected and survey unit L2-011-104 is acceptable for unrestricted release. The mean SOF when applying the respective Base Case DCGLs (DCGLS) for soil is 0.0102. This SOF equates to a dose for the survey unit of 0.2557 mrem/yr.
- 2. SURVEY UNIT DESCRIPTION Survey Unit L2-011-104 is an impacted Class 2 open land survey unit. The surface area of the survey unit is 5,285 m2.
The boundary of the survey unit and the location of the soil samples were defined using a Global Positioning System (GPS). Refer to Attachment 1 of this report for figures and maps depicting survey unit L2-011-104.
- 3. CLASSIFICATION BASIS Survey unit L2-011-104 was not originally identified in the Historical Site Assessment (HSA) (Reference 5). A portion of survey unit L2-011-102, as originally defined in the HSA 5
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS and during characterization, makes up survey unit L2-011-104 in its FSS configuration. The following summarizes the results of the characterization survey for survey unit L2-011-102. The initial site characterization surveys performed by EnergySolutions were conducted between October 9, 2014, and August 6, 2015. In total, ten (10) surface soil samples, seven (7) subsurface soil samples, and six (6) asphalt samples were collected in survey unit L2-011-102. All samples were analyzed by the on-site gamma spectroscopy system. For surface soil samples, Cs-137 was detected at concentrations above Minimum Detectable Concentration (MDC) in six (6) of the samples, at a maximum concentration of 2.00E-01 pCi/g. Co-60 was not detected at concentrations above MDC in any of the surface soil samples. For subsurface soil samples, Cs-137 was detected at concentrations above MDC in two (2) of the samples, at a maximum concentration of 5.20E-02 pCi/g. Co-60 was not detected at concentrations above MDC in any of the subsurface soil samples. For asphalt samples, Cs-137 was detected at concentrations above MDC in three (3) of the samples, at a maximum concentration of 5.50E-02 pCi/g. Co-60 was not detected at concentrations above MDC in any of the asphalt samples. A summary of the analyses for the surface soil, subsurface soil, and asphalt samples taken during site characterization are presented in Table 3-1. One (1) surface soil, two (2) subsurface soil, and one (1) asphalt samples from characterization were sent to Test America Laboratories for off-site analysis. A summary of the off-site analyses is presented in Table 3-2. 6
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Table 3 Statistical Quantities for Cs-137 and Co-60 from the Characterization Survey Surface Soil Co-60 Cs-137
# of Samples 10
# >MDC 0 6 Mean (pCi/g) 6.40E-02 6.50E-02 Median (pCi/g) 6.40E-02 5.40E-02 Max (pCi/g) 8.10E-02 2.00E-01 Min (pCi/g) 5.20E-02 3.00E-02 Standard Deviation (pCi/g) 9.00E-03 4.90E-02 Subsurface Soil Co-60 Cs-137
# of Samples 7
# >MDC 0 2 Mean (pCi/g) 4.90E-02 3.80E-02 Median (pCi/g) 4.80E-02 3.30E-02 Max (pCi/g) 5.50E-02 5.20E-02 Min (pCi/g) 4.20E-02 2.90E-02 Standard Deviation (pCi/g) 4.00E-03 9.00E-03 Asphalt Co-60 Cs-137
# of Samples 6
# >MDC 0 3 Mean (pCi/g) 5.60E-02 4.80E-02 Median (pCi/g) 5.70E-02 5.10E-02 Max (pCi/g) 5.90E-02 5.50E-02 Min (pCi/g) 4.90E-02 9.00E-03 Standard Deviation (pCi/g) 3.00E-03 8.00E-03 7
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Table 3-2 Off-site Analysis for Characterization Samples Fe- Ni- Co- Ni- Sr- Nb- Tc- Cs- Pm- Eu- Eu- Eu- Np- Pu- Pu- Pu- Am- Am- Cm-Radionuclide H-3 C-14 55 59 60 63 90 94 99 137 147 152 154 155 237 238 239/240 241 241 243 243/244 L2011102-QQ- 1.370 1.560 2.260 3.040 0.007 4.390 0.291 0.018 0.537 0.021 0.672 0.044 0.173 0.055 0.031 0.026 0.018 2.680 0.029 0.028 0.024 GS-001-SB L2011102-QQ- 0.533 0.713 2.330 2.820 0.019 4.300 0.361 0.014 0.595 0.014 0.772 0.039 0.111 0.045 0.017 0.036 0.026 2.880 0.026 0.034 0.021 GS-001-SS L2011102-QQ- 0.525 0.702 3.890 2.880 0.031 3.950 0.327 0.016 0.568 0.018 0.717 0.052 0.183 0.051 0.022 0.028 0.020 1.710 0.010 0.028 0.006 GS-002-SB L2011102-QQ- 0.027 0.017 0.018 0.051 0.142 0.038 0.036 PA-001-AV Note: Bold values indicate concentration greater than MDC. Unbolded values indicate the MDC value. All values in pCi/g. Blank cells indicate that a particular radionuclide was not included in the analysis. 8
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Section 5.1 of the LTP states that the actual Insignificant Contributor (IC) dose will be calculated for each individual sample result using the DCGLs from Table 4 of TSD RS-TD-313196-004, LACBWR Soil DCGL, Basement Concrete DCGL, and Buried Pipe DCGL (Reference 6) for soil. If the IC dose calculated is less than the IC dose assigned for DCGL adjustment, then no further action will be taken. If the actual IC dose calculated from the sample result is greater than the IC dose assigned for DCGL adjustment, then a minimum of five (5) additional investigation samples will be taken around the original sample location. Each investigation sample will be analyzed by the on-site gamma spectroscopy system and sent for HTD analysis (full suite of radionuclides from LTP Table 5-1). As with the original sample, the actual IC dose will be calculated for each investigation sample. In this case, the actual calculated maximum IC dose from an individual sample observed in the survey unit will be used to readjust the DCGLs in that survey unit. If the maximum IC dose exceeds 10%, then the additional radionuclides that were the cause of the IC dose exceeding 10% will be added as additional ROC for that survey unit. The survey unit-specific DCGLs used for compliance, the ROC for that survey unit, and the survey data serving as the basis for the IC dose adjustment will be documented in the release record for the survey unit. A Radiological Assessment (RA) in survey unit L2-011-104 was performed in June of 2019. Twenty-seven (27) soil samples were collected and analyzed by the on-site gamma spectroscopy system. The average SOF of the sample set was 0.014, with a standard deviation 0.006. The RA data was used to design the FSS. Four samples from the RA were sent off-site for full suite radionuclide analysis. An assessment of the results of continuing characterization confirmed that the IC dose is unchanged. The maximum calculated IC dose was 0.1050 mrem/yr, which is below the 2.5 mrem/yr limit provided in the LTP for DCGL adjustment. A summary of the off-site analytical results for continuing characterization (RA) samples is provided in Table 3-3 below. Table 3-3 Off-site Analysis for RA Samples L2-SUB- L2-SUB- L2-SUB- L2-SUB-102- 102- 102- 102-Radionuclide AJGS- AJGS- AJGS- AJGS-024-SB 001-SB 019-SB 001-AV H-3 2.40E+00 2.31E+00 2.76E+00 3.40E+00 C-14 6.17E-01 5.26E-02 -8.79E-01 -1.10E+00 Fe-55 2.06E+00 1.36E+00 -1.89E+00 7.46E+00 Ni-59 5.77E-01 -1.02E-01 -7.72E-02 -1.54E-01 Co-60 3.79E-02 -4.19E-04 -1.80E-02 8.50E-03 Ni-63 4.32E-01 -3.71E-01 -4.74E-02 -1.77E-01 Sr-90 -2.23E-01 -1.90E-01 -2.28E-02 -2.85E-03 Nb-94 1.83E-02 -1.02E-02 -1.11E-02 5.19E-02 9
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS L2-SUB- L2-SUB- L2-SUB- L2-SUB-102- 102- 102- 102-Radionuclide AJGS- AJGS- AJGS- AJGS-024-SB 001-SB 019-SB 001-AV Tc-99 1.26E-01 6.69E-01 1.96E-01 -2.89E-01 Cs-137 1.46E-03 0.00E+00 4.45E-02 2.75E-03 Eu-152 9.14E-03 1.63E-02 1.06E-02 1.11E-02 Eu-154 1.49E-02 -3.15E-02 -2.09E-02 -3.00E-03 Eu-155 0.00E+00 2.78E-02 3.60E-02 -4.00E-03 Np-237 1.31E-03 1.70E-03 -1.46E-03 6.68E-04 Pu-238 -7.11E-03 6.62E-03 3.83E-02 7.61E-03 Pu-239/240 3.12E-02 -1.08E-02 6.65E-03 2.05E-03 Pu-241 9.35E-01 1.06E+00 -5.96E-01 -3.14E-01 Am-241 1.36E-02 4.62E-03 5.58E-03 -9.80E-03 Am-243 1.57E-02 -3.66E-03 3.33E-03 8.95E-03 Cm-243/244 -3.38E-05 -1.56E-02 1.11E-02 -1.14E-02 Note Bold values indicate positively identified radionuclide activities. Based upon review of the historical information, the results of the characterization survey data and RA data, and completion of a final Survey Unit Classification Worksheet, the correct final classification of survey unit L2-011-104 was determined to be Class 2.
- 4. DATA QUALITY OBJECTIVES (DQO)
FSS planning and design relies on a properly executed Data Quality Objective (DQO) process to ensure, through compliance with explicitly defined inputs and boundaries, that the primary objective of the survey is satisfied. The DQO process, utilized in accordance with MARSSIM, is described in the LACBWR LTP. The appropriate design for a given survey was developed using the DQO process as outlined in Appendix D of MARSSIM. A summary of seven steps of the DQO process are outlined as follows. The DQO process incorporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline condition is technically known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would indicate that residual activity within the survey unit does not exceed the 10
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS release criteria. Therefore, the survey unit would satisfy the primary objective of the FSS sample plan. The primary objective of the FSS sample plan is to demonstrate that the level of residual radioactivity in survey unit L2-011-104 did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA). EnergySolutions TSD RS-TD-313196-001, Radionuclides of Concern during LACBWR Decommissioning (Reference 7) established the basis for an initial suite of potential ROC for decommissioning. LTP Chapter 2 provides detailed characterization data that describes the results of surveys taken of soil. Surface and subsurface soil samples were taken in each impacted open land survey units and analyzed for the presence of plant-derived radionuclides. The results of surface and subsurface soil characterization in the impacted area surrounding LACBWR indicate that there is minimal residual radioactivity in soil. IC were determined consistent with the guidance contained in Section 3.3 of NUREG-1757, Volume 2, Revision 1, Consolidated Decommissioning Guidance Characterization, Survey, and Determination of Radiological Criteria, Final Report (Reference 8). In all soil and concrete scenarios, Cs-137, Co-60, Sr-90, Eu-152 and Eu-154 contribute nearly 100% of the total dose. The remaining radionuclides were designated as IC and were eliminated from further detailed evaluation. Therefore, the final ROCs for LACBWR soil, basement concrete and buried piping are Cs-137, Co-60, Sr-90, Eu-152 and Eu-154. The LTP, Section 6.14.1 discusses the process used to derive the ROC for the decommissioning of LACBWR, including the elimination of IC from the initial suite. Table 4-1 presents the ROC for the decommissioning of soil at LACBWR and the normalized mixture fractions based on the radionuclide mixture. Table 4 Dose Significant Radionuclides and Mixture for Soil Fraction of Total Activity Radionuclide (normalized)(1) Co-60 0.064 Sr-90 0.098 Cs-137 0.829 Eu-152 0.005 Eu-154 0.003 (1) Based on maximum percent of total activity from Table 22 of RS-TD-313196-001, normalized to one for the dose significant radionuclides. 11
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS The LTP, Section 5.2 states that each radionuclide-specific Base Case DCGL is equivalent to the level of residual radioactivity (above background levels) that could, when considered independently, result in a Total Effective Dose Equivalent (TEDE) of 25 mrem/yr to an Average Member of the Critical Group. To ensure that the summation of dose from each source term is 25 mrem/yr or less after all FSS is completed, the Base Case DCGLs are reduced based on an expected, or a priori, fraction of the 25 mrem/yr dose limit from each source term. The reduced DCGLs, or "Operational" DCGLs can be related to the Base Case DCGLs as an expected fraction of dose based on an a priori assessment of what the expected dose should be based on the results of site characterization, process knowledge, and the extent of planned remediation. The Operational DCGL is then used as the DCGL for the FSS design of the survey unit (e.g., calculation of surrogate DCGLs, investigation levels). Details of the Operational DCGLs derived for each dose component and the basis for the applied a priori dose fractions are provided in LC-FS-TSD-002, Operational Derived Concentration Guideline Levels for Final Status Survey (Reference 9). Multiple ROCs are known to be present at LACBWR. The dose contribution from each ROC is accounted for using the SOF to ensure that the total dose from all ROC does not exceed the dose criterion. A Base Case DCGL that is established for the average residual radioactivity in a survey unit is equivalent to a DCGL W. In Class 1 land survey units, the DCGLW can be multiplied by Area Factors to obtain a Base Case DCGL that represents the same dose to an individual for residual radioactivity over a smaller area within a survey unit. At LACBWR, compliance is demonstrated through the summation of dose from five (5) distinct source terms (i.e., basements, soils, buried pipe, above-ground structures, and groundwater) for the end-state. When applied to soil, the DCGLs are expressed in units of activity per unit of mass (pCi/g). For LACBWR, soil is defined as a layer of soil beginning at the surface but extending to a depth of 1 m to allow for flexibility in compliance demonstration if contamination deeper than 0.15 m is encountered. Based on characterization data and historical information, there are no expectations of encountering a source term geometry that is comprised of a clean surface layer of soil over a contaminated subsurface soil layer. EnergySolutions TSD RS-TD-313196-004 and the LTP, Section 6.8 provide the exposure scenarios and modeling parameters that were used to calculate the site-specific soil DCGLs. The adjusted soil DCGLs for the unrestricted release of open land survey units as provided in Chapter 6, Section 6.16.1 are reproduced in Table 4-2. The IC percentages for the most limiting basement scenario was used to adjust the DCGLs for soil to account for the dose from the eliminated insignificant contributor radionuclides. 12
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Table 4 Base Case DCGLs for Soil DCGLS Radionuclide (pCi/g) Co-60 10.6 Sr-90 5470 Cs-137 48.3 Eu-152 23.6 Eu-154 21.9 The Operational DCGLs are then used as the DCGL for the FSS design of the survey unit (e.g., calculation of surrogate DCGLs, investigation levels). The OpDCGLS for the unrestricted release of soil are provided in Table 4-3. Table 4 Operational DCGLs for Soil OpDCGLS Radionuclide (pCi/g) Co-60 3.83 Sr-90 1970.45 Cs-137 17.39 Eu-152 8.51 Eu-154 7.89 Instrument DQOs included a verification of the ability of the survey instrument to detect the radiation(s) of interest relative to the Operational DCGL. Survey instrument response checks were required prior to issuance and after the instrument had been used. Control and accountability of survey instruments was required to assure the quality and prevent the loss of data. As part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results. The actual reported value was used as the recorded FSS result for measurement and/or sample values that are less than MDC. Negative values were recorded as "zero." Results were not reported as "less than MDC" (< MDC). Sample report summaries included unique sample identification, analytical method, radionuclide, result, uncertainty, laboratory data qualifiers, units, and the observed MDC. 13
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS In accordance with the LTP, for laboratory analysis, MDCs less than 10% of the Operational DCGL were preferable while MDCs up to 50% of the Operational DCGL were acceptable. The minimum acceptable MDC for measurements obtained using field instruments was 50% of the applicable Operational DCGL.
- 5. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. Guidance for preparing FSS plans is provided in procedure LC-FS-PR-002, Final Status Survey Package Development.
The DQO process validated that Co-60, Sr-90, Cs-137, Eu-152, and Eu-154 would be the ROC in survey unit L2-011-104 as presented in LTP Section 5.1. During the data analysis of the FSS results, concentrations for the HTD ROC Sr-90 are inferred using a surrogate approach. Cs-137 is the principle surrogate radionuclide for Sr-90. During characterization, both Sr-90 and Cs-137 was positively detected in all thirty (30) concrete core samples assessed in the Reactor Building, Tunnel, and Waste Treatment Building. The 95% Upper Confidence Limit (UCL) of the Cs-137 fractions was chosen to represent the overall nuclide mix for soils/buried pipe, the Reactor Building, and the Waste Gas Tank Vault. The surrogate ratio for soil is given in Table 5-1. Table 5-1 Soil Surrogate Ratio Radionuclides Ratio Sr-90/Cs-137 0.502 The equation for calculating a surrogate DCGL is as follows: Equation 1 Where: DCGLSur = Surrogate radionuclide DCGL DCGL2,3 ... n = DCGL for radionuclides to be represented by the surrogate Rn = Ratio of concentration (or nuclide mixture fraction) of radionuclide "n" to surrogate radionuclide Using the Operational DCGLs presented in Table 4-3 and the ratio from Table 5-1, the 14
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS following surrogate calculation was performed: Equation 2 1 SurrogatevcGL (cs- 137) = [( 1 ) +( O.SOZ )] = 17.31 pCi/g 17.39ccs-137) 1970.45csr-90) The surrogate Operational DCGL that was used for Cs-137 in this survey unit for direct comparison of sample results to demonstrate compliance was 17.31 pCi/g. The action levels for survey unit L2-011-104 are based on the Operational DCGL and are presented in Table 5-2. Table 5-2 Action Levels for Survey Unit L2-011-104 Action Level ROC (pCi/g) Co-60 3.83(1) Cs-137 17.31(2) Eu-152 8.51(1) Eu-154 7.89(1) (1) Based on the Operational DCGL. (2) Based on the surrogate adjusted DCGL of Cs-137 while inferring Sr-90. The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set. The number of soil samples for FSS was determined in accordance with procedure LC-FS-PR-002. The relative shift (11/u) for the survey unit data set is defined as shift(~), which is the Upper Boundary of the Gray Region (UBGR), or the DCGL (SOF of 1), minus the Lower Bound of the Gray Region (LBGR) (SOF of 0.5), divided by sigma (u), which is the standard deviation of the data set used for survey design. The optimal value for 11/u should range between one (1) and three (3) . The largest value the 11/u can have is three (3). If the calculated value of ~/uexceeds three (3), an adjusted value of three (3) will be used for ~/u. The 11/u for survey unit L2-011-104, based on the data for surface soil samples collected during the RA of survey unit L2-011-104, was calculated as follows: 15
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Equation 3
!).fa = (1 - 0.014) / 0.006 = 164.3 As the calculated relative shift was greater than three (3), a value of three (3) was used as the adjusted !1/cr. Both the Type I error (i.e., a value) and the Type II error (i.e., value) was set at 0.05. The sample size from Table 5.5 of MARSSIM that equates to the Type I and Type II error of 0.05 for use with the Sign Test is an N value of fourteen (14).
A Prospective Power Curve was generated using COMPASS, a software package developed under the sponsorship of the United States Nuclear Regulatory Commission (USNRC) for implementation of the MARSSIM in support of the decommissioning license termination rule (10CFR20, Subpart E). The result of the COMPASS computer run showed adequate power for the survey design. As the survey unit was classified as Class 2 sample locations were selected based on a systematic triangular grid with a random starting point. The systematic locations of the soil samples were selected using Visual Sample Plan (VSP), in accordance with LC-FS-PR-002. Input parameters included use of aerial photographs and the systematic sampling tool set with a predetermined number (14) of samples. The systematic coordinates generated with VSP were integrated with a GPS to identify sample locations in the field. Several systematic sample locations were at areas covered by asphalt. At each of those locations, a surface asphalt sample and an underlying soil sample were collected. The surface asphalt samples are treated as the compliance samples, because they are the top layer and have the most significant dose consequence. The underlying soil samples, for the purposes of this FSS, are treated as judgmental samples. Table 5-3 lists the systematic samples collected for FSS and the corresponding GPS coordinates, based on the Wisconsin State Plane North American Datum 1983 coordinate system. Table 5-3 Systematic Sample Locations Sample ID Northing Easting L2-011-104-FSGS-001-SS 570748.0508 1641711.7891 L2-011-104-FSGS-002-SS 570798.7977 1641682.4904 L2-011-104-FSGS-003-SS 570798.7977 1641741.0878 L2-011-104-FSGS-004-SS 570849.5445 1641711.7891 L2-011-104-FSPA-005-AV 570849.5445 1641828.9840 L2-011-104-FSPA-006-AV 570849.5445 1641887.5814 L2-011-104-FSPA-007-AV 570849.5445 1641946.1788 L2-011-104-FSPA-008-AV 570849.5445 1642004.7763 16
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Sample ID Northing Easting L2-011-104-FSPA-009-AV 570849.5445 1642063.3737 L2-011-104-FSGS-010-SS 570900.2914 1641741.0878 L2-011-104-FSGS-011-SS 570951.0383 1641770.3865 L2-011-104-FSPA-012-AV 570951.0383 1641828.9840 L2-011-104-FSPA-013-AV 571001.7851 1641858.2827 L2-011-104-FSGS-014-SS 571103.2788 1641858.2827 In accordance with the sample plan, at least one (1) judgmental sample is required from the survey unit. The number of judgmental samples actually obtained was eight (8). In addition, two (2) investigational samples (labeled as judgmental) were collected due to scan alarms, which brings the total number of samples collected for the FSS of survey unit L2-011-104 to twenty-four (24). Table 5-4 lists the judgmental and investigational samples collected for FSS and the corresponding GPS coordinates. Table 5-4 Judgmental and Investigational Sample Locations Sample ID Northing Easting L2-011-104-FJPA-015-AV 570845.6220 1641993.8910 L2-011-104-FJGS-015-SS 570845.6220 1641993.8910 L2-011-104-FJGS-015-SB 570845.6220 1641993.8910 L2-011-104-FSGS-005-SS 570849.5445 1641828.9840 L2-011-104-FSGS-006-SS 570849.5445 1641887.5814 L2-011-104-FSGS-007-SS 570849.5445 1641946.1788 L2-011-104-FSGS-008-SS 570849.5445 1642004.7763 L2-011-104-FSGS-009-SS 570849.5445 1642063.3737 L2-011-104-FSGS-012-SS 570951.0383 1641828.9840 L2-011-104-FSGS-013-SS 571001.7851 1641858.2827 The LACBWR LTP, Section 5.1 states that soil samples will be collected during FSS to confirm the HTD to surrogate radionuclide ratio. Ten percent (10%) of the FSS samples collected from open land survey units will be analyzed for HTD ROC. Only the HTD radionuclide included as ROC (Sr-90) will be analyzed in the FSS confirmatory samples. In addition, if any sample has a SOF of 10% of the Operational DCGL or more, it must be sent for HTD ROC analysis. For samples with positive results for both the HTD ROC and the corresponding surrogate radionuclide (Cs-137), the HTD surrogate ratio will be derived and compared against the 95% UCL ratio (see Table 5-1). If the derived ratio from the 17
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS confirmatory samples exceeds the 95% UCL ratio, then the area-specific ratio as determined by actual survey data will be used. The selection of three (3) soil samples (L2-011-104-FSGS-001-SS, L2-011-104-FSGS-010-SS, and L2-011-104-FSGS-011-SS) met the requirement that a minimum of 10% of the samples collected for the FSS of survey unit L2-011-104 be analyzed for HTD ROC. The implementation of quality control measures as referenced by LTP, Section 5.9 and LaCrosseSolutions LC-QA-PN-001, Final Status Survey Quality Assurance Project Plan (QAPP) (Reference 10) includes the collection of a soil sample for "split sample" analysis on 5% of the soil samples taken in a survey unit with the locations selected at random. One (1) soil sample, L2-011-104-FQGS-003-SS, was designated for split sample QC analysis for the FSS of this survey unit. The LTP, Section 5.6.4.4 and Table 5-15 specifies that for Class 2 open land survey units, surface scans will be performed on 5% to 50% of the surface area in the survey unit. For survey unit L2-011-104, 25% scan coverage was selected, which equates to 1,321 m 2. Eighty-six (86) scan lanes within four (4) separate scan areas were established, constituting a total area of 1,344 m2 (more than the required minimum). For this Class 2 open land survey unit, the "Investigation Levels" for area scanning and soil sample measurement results are those levels specified in the LTP, Table 5-16, and are reproduced below in Table 5-5. Table 5-5 Investigation Levels Direct Investigation Classification Scan Investigation Levels Levels
>Operational DCGL or >MDC scan if Class 2 MDCscan is greater than Operational >Operational DCGL DCGL Table 5-6 provides a synopsis of the survey design for survey unit L2-011-104.
Table 5-6 Synopsis of Survey Design Feature Design Criteria Basis Survey Unit Surface Area 5,285 m2 GPS 18
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Feature Design Criteria Basis
- cr=0.0 06
- UBGR = SOF of 1 Number of Systematic Samples 14
- LBGR = SOF of 0.014 (N)
- Type I & II error = 0.05
- Ncr = 3 (adjusted)
- MARSSIM Table 5.5
- Co-60: 3.83 pCi/g
- Sr-90: 1970.45 pCi/g
- Cs-137: 17.39 pCi/g Operational DCGLs for soil, DCGLS and Action Levels (Surrogate Cs-137 LTP, Table 5-6, Release Record, Table 5-2 DCGL: 17.31 pCi/g)
- Eu-152: 8.51 pCi/g
- Eu-154: 7.89 pCi/g Scan and Direct Investigation
>Operational DCGL LTP, Table 5-16 Levels Scan Areal Coverage 1,344, >25% areal coverage LTP, Table 5-15 1 Per Survey Design Judgmental Samples 8 Actual Number Obtained 1 LTP, Section 5.1 HTD ROC Analysis 3 Actual Number Obtained 1 split sample selected at random LTP, Section 5.9 QC 4 Actual Number Obtained
- 6. SURVEY IMPLEMENTATION For survey unit L2-011-104, compliance with the unrestricted release criteria was demonstrated through a combination of soil scanning with a Ludlum Model 44-10 gamma detector and the sampling of soil for isotopic analysis.
An FSS Supervisor performed a visual inspection and walk-down of the survey unit on August 28, 2019, prior to performing FSS. The purpose of the walk-down was to assess the physical condition of the survey unit, evaluate access points and travel paths, and identify potentially hazardous conditions. At the time of survey, the soil in the survey unit was dry and free of any considerable constraint for the collection of samples and scan measurements. 19
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS FSS field activities were conducted under the FSS Sample Plan, which included DQOs, survey design, detailed FSS instructions, job safety analysis, and related procedures for reference. FSS field activities were projected to take four (4) working days to complete. Daily briefings were conducted to discuss the expectations for job performance and to review safety aspects of the job. A "Field Log" was used to document field activities and other information pertaining to the performance of the FSS. FSS field activities commenced on August 28, 2019, and were concluded on September 23, 2019. A total of fifty-five (55) different scan lanes, constituting an areal coverage of 1,344 m 2, were scanned using a Ludlum 2350-1 paired with a Ludlum Model 44- 10 (2"x 2") sodium iodide (NaI) detector. The background was established as the average of five (5) 1-minute static measurements, while maintaining the detector 6" from the soil. In survey unit L2-011-104, background ranged from 3,868 cpm up to 5,977 cpm. All designated scan areas were scanned using a Ludlum 2350-1 paired with a Model 44-10 2"x 2" Nal detector operated in the rate-meter mode and using audio response. The probe was positioned no more than 3" from the ground and was moved at a scan speed of approximately 0.5 meters per second. In accordance with RS-TD-313196-006, Ludlum Model 44-10 Detector Sensitivity (Reference 11), scan MDC was sufficient to detect residual radioactivity at the action level (adjusted surrogate DCGL of 17.31 pCi/g, which was based on the surrogate adjusted DCGL of Cs-137 while inferring Sr-90). Complete scan results are provided in Attachment 2. The fourteen (14) systematic sample locations were marked with flags based on GPS coordinates provided. Each soil sample consisted of approximately one (1) liter of soil. The soil sample media was sifted to remove stones and other media larger than one (1) centimeter in diameter. All soil samples were collected, controlled, transported, stored, and transferred to the on-site laboratory using the Chain-of-Custody process from LC-FS-PR-012, Chain of Custody Protocol (Reference 12), and in accordance with LC-FS-PR-004, Sample Media Collection for Site Characterization and Final Status Survey (Reference 13), LC-FS-PR-005, Sample Media Preparation for Site Characterization and Final Status Survey (Reference 14), and LC-FS-PR-001, Sample Storage (Reference 15). Subsurface soil samples were collected using a hand auger. The survey design specified that a minimum of one (1) sample was required for HTD ROC analysis. In total, three (3) samples (L2-011-104-FSGS-001-SS, L2-011-104-FSGS-010-SS, and L2-011-104-FSGS-011-SS) were selected for HTD radionuclide analysis. 20
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS The implementation of survey specific QC measures included the collection of four (4) samples (L2-011-104-FQGS-003-SS, L2-011-104-FQGS-004-SS, L2-011-104-FSGS-003-SS SPLIT, and L2-011-104-FSGS-009-SS SPLIT) for split and duplicate sample analysis.
- 7. SURVEY RESULTS All areas identified in the FSS sample plan were scanned for elevated activity levels. A total of two (2) alarms were verified during scanning, which prompted the collection of one (1) investigational soil sample and one (1) subsurface soil sample. Table 7-1 provides an overview of the scan results for all scan lanes (identified as A 01 through D 14), the 1 m 2 scan areas around each sample location before and after sample collection (identified with "SP"), and QC locations (identified with a " QC" ). Complete scan results are provided in Attachment 2.
Table 7-1 Synopsis of Scan Results Highest Action # of Logged Investigation Scan Area Level(1) Scan Reading Samples Alarms (cpm) (cpm) 01 SP 4,054 6,937 0 0 02 SP 4,942 6,937 0 0 03 SP 5,478 6,937 0 0 03 SP QC 5,966 7,293 0 0 04 SP 4,849 6,937 0 0 04 SP QC 4,909 7,293 0 0 05 SP 4,926 6,370 0 0 06 SP 5,226 6,370 0 0 07 SP 5,012 6,370 0 0 08 SP 4,857 6,370 0 0 09 SP 4,568 6,370 0 0 10 SP 6,444 6,937 0 0 11 SP 5,744 6,937 0 0 12 SP 4,126 6,370 0 0 13 SP 4,451 6,370 0 0 14 SP 4,525 6,937 0 0 15 SP 5,396 6,375 1 1 A 01 5,894 7,739 0 0 A 02 6,695 7,739 0 0 21
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Highest Action # of Logged Investigation Scan Area Level(1) Scan Reading Samples Alarms (cpm) (cpm) A 03 6,412 7,739 0 0 A 04 6,120 7,739 0 0 A 05 6,785 7,739 0 0 A 06 6,939 7,739 0 0 A 07 6,479 7,739 0 0 A 08 6,996 7,739 0 0 A 09 6,544 7,739 0 0 A 10 7,319 7,739 0 0 A 11 6,178 7,739 0 0 A 12 6,128 7,739 0 0 A 13 6,395 7,739 0 0 A 14 4,583 7,739 0 0 A 15 4,388 7,739 0 0 A 16 4,373 7,739 0 0 A 17 4,198 7,739 0 0 A 18 4,230 7,739 0 0 B 01 6,131 7,423 0 0 B 02 5,336 7,423 0 0 B 03 5,132 7,423 0 0 B 04 5,481 7,423 0 0 B 05 5,082 7,423 0 0 B 06 5,275 7,423 0 0 B 07 5,533 7,423 0 0 B 08 5,206 7,423 0 0 B 09 5,196 7,423 0 0 B 10 5,123 7,423 0 0 B 11 4,949 7,423 0 0 B 12 5,322 7,423 0 0 B 13 5,070 7,423 0 0 B 14 5,354 7,423 0 0 B 15 5,143 7,423 0 0 B 16 5,496 7,423 0 0 22
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Highest Action # of Logged Investigation Scan Area Level(1) Scan Reading Samples Alarms (cpm) (cpm) B 17 5,135 7,423 0 0 B 18 6,053 7,423 0 0 B 19 5,722 7,423 0 0 B 20 5,944 7,423 0 0 B 21 6,169 7,423 0 0 B 22 6,340 7,423 0 0 B 23 6,342 7,423 0 0 B 24 6,479 7,423 0 0 B 25 6,379 7,423 0 0 B 26 6,183 7,423 0 0 C 01 4,738 5,834 0 0 C 02 4,248 5,834 0 0 C 03 4,571 5,834 0 0 C 04 4,481 5,834 0 0 C 05 4,432 5,834 0 0 C 06 4,543 5,834 0 0 C 07 4,525 5,834 0 0 C 08 4,430 5,834 0 0 C 09 4,759 5,834 0 0 C 10 4,541 5,834 0 0 C 11 4,945 5,834 0 0 C 12 4,871 5,834 0 0 C 13 5,258 5,834 0 0 C 14 4,965 5,834 0 0 C 15 5,310 5,834 0 0 C 16 5,478 6,842 0 0 C 17 5,428 6,842 0 0 C 18 5,663 6,842 0 0 C 19 5,795 6,842 0 0 C 20 5,666 6,842 0 0 C 21 5,735 6,842 0 0 C 22 6,055 6,842 0 0 23
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Highest Action # of Logged Investigation Scan Area Level(1) Scan Reading Samples Alarms (cpm) (cpm) C 23 6,006 6,842 0 0 C 24 6,008 6,842 0 0 C 25 6,204 6,842 0 0 C 26 6,619 6,842 0 0 C 27 5,814 6,842 0 0 C 28 6,569 6,842 0 0 D 01 5,057 6,282 0 0 D 02 4,537 6,282 0 0 D 03 4,895 6,282 0 0 D 04 7,632 6,282 1 1 D 05 5,066 6,282 0 0 D 06 4,908 6,282 0 0 D 07 4,975 6,282 0 0 D 08 5,081 6,282 0 0 D 09 4,646 6,282 0 0 D 10 4,724 6,282 0 0 D 11 4,909 6,282 0 0 D 11 QC 4,299 5,630 0 0 D 12 4,797 6,282 0 0 D 12 QC 4,143 5,630 0 0 D 13 5,226 6,282 0 0 D 13 QC 4,361 5,630 0 0 D 14 5,880 6,282 0 0 D 14 QC 4,152 5,630 0 0 (1) Action Level based on the average background plus 1,762 cpm (50% OpDCGL equivalent). The on-site laboratory analyzed the fourteen (14) soil samples taken for non-parametric statistical testing using the on-site gamma spectroscopy system. A summary of the results for the fourteen (14) samples collected for non-parametric statistical testing is provided in Table 7-2. Gamma spectroscopy results revealed that no ROC were positively identified in any systematic sample. The concentration for Sr-90 was inferred based on the ratio specified in Table 5-1. The complete gamma spectroscopy reports are presented in Attachment 7. The basic statistics for the systematic sample population are summarized in Table 7-3. 24
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Table 7 Summary of Gamma Spectroscopy Results for Samples Comprising the Statistical Sample Population Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) L2-011-104-FSGS-001-SS 3.53E-02 7.06E-02 0.00E+00 0.00E+00 3.54E-02 L2-011-104-FSGS-002-SS 6.19E-02 5.98E-02 2.65E-03 1.01E-01 3.00E-02 L2-011-104-FSGS-003-SS 1.90E-02 7.14E-02 0.00E+00 5.64E-02 3.58E-02 L2-011-104-FSGS-004-SS 5.17E-02 5.50E-02 7.75E-02 9.45E-02 2.76E-02 L2-011-104-FSPA-005-AV 6.45E-02 9.60E-02 1.00E-01 1.56E-02 4.82E-02 L2-011-104-FSPA-006-AV 4.22E-02 3.06E-02 0.00E+00 2.24E-01 1.54E-02 L2-011-104-FSPA-007-AV 0.00E+00 8.09E-02 8.17E-03 0.00E+00 4.06E-02 L2-011-104-FSPA-008-AV 4.62E-03 3.76E-02 1.05E-01 0.00E+00 1.89E-02 L2-011-104-FSPA-009-AV 3.30E-02 6.80E-02 6.50E-02 6.96E-02 3.41E-02 L2-011-104-FSGS-010-SS 9.27E-02 6.79E-02 8.63E-02 1.89E-03 3.41E-02 L2-011-104-FSGS-011-SS 5.76E-02 9.98E-02 2.59E-02 6.70E-03 5.01E-02 L2-011-104-FSPA-012-AV 5.14E-02 3.75E-02 8.40E-02 2.84E-02 1.88E-02 L2-011-104-FSPA-013-AV 3.63E-02 9.94E-02 2.08E-02 1.95E-02 4.99E-02 L2-011-104-FSGS-014-SS 6.54E-02 5.54E-02 1.59E-02 2.74E-01 2.78E-02 Note: Bold values indicate concentrations greater than MDC. Table 7 Basic Statistical Properties of Systematic Sample Population Mean Median Max Min Std. Dev. BcDCGL Avg. SOF Avg. Dose ROC (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) per ROC Per ROC Co-60 4.40E-02 4.68E-02 9.27E-02 0.00E+00 2.52E-02 1.06E+01 0.0041 0.1037 Cs-137 6.64E-02 6.80E-02 9.98E-02 3.06E-02 2.25E-02 4.83E+01 0.0014 0.0344 Eu-152 4.22E-02 2.34E-02 1.05E-01 0.00E+00 4.13E-02 2.36E+01 0.0018 0.0447 Eu-154 6.37E-02 2.40E-02 2.74E-01 0.00E+00 8.64E-02 2.19E+01 0.0029 0.0727 Sr-90 3.33E-02 3.41E-02 5.01E-02 1.54E-02 1.13E-02 5.47E+03 0.0000 0.0002 The off-site laboratory, GEL Laboratories, processed the three (3) samples selected for HTD ROC analysis. Samples L2-011-104-FSGS-001-SS, L2-011-104-FSGS-010-SS, and L2-011-104-FSGS-011-SS were selected. Only the HTD ROC Sr-90 was included in the analysis. All analyses met the required MDC. Sr-90 was not detected in the off-site analysis of samples L2-011-104-FSGS-001-SS, L2-011-104-FSGS-010-SS, and L2-011-104-FSGS-011-SS. The results are provided in Table 7-4. 25
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Table 7 Off-Site Analysis Results Result Uncertainty MDC Sample ID ROC >MDC (pCi/g) (pCi/g) (pCi/g) L2-011-104-FSGS-001-SS Sr-90 -3.54E-02 4.46E-02 9.60E-02 No L2-011-104-FSGS-010-SS Sr-90 -1.94E-02 3.67E-02 7.92E-02 No L2-011-104-FSGS-011-SS Sr-90 -5.80E-02 5.08E-02 1.17E-01 No The on-site laboratory analyzed the eight (8) judgmental soil samples and the two (2) investigational samples using the on-site gamma spectroscopy system. A summary of the analytical results for the judgmental and investigational soil samples is provided in Table 7-
- 5. Gamma spectroscopy results revealed that no ROC were positively identified in any judgmental or investigational sample. The concentrations for Sr-90 were inferred based on the ratio specified in Table 5-1. The complete gamma spectroscopy reports are presented in Attachment 7.
Table 7 Summary of Gamma Spectroscopy Results for Judgmental and Investigational Samples Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) L2-011-104-FJPA-015-AV 4.97E-02 4.65E-02 1.89E-01 1.10E-01 2.33E-02 L2-011-104-FJGS-015-SS 5.76E-02 5.47E-02 6.13E-02 2.33E-02 2.75E-02 L2-011-104-FJGS-015-SB 3.41E-02 4.33E-02 0.00E+00 3.50E-02 2.17E-02 L2-011-104-FSGS-005-SS 4.83E-02 3.78E-02 2.31E-03 3.70E-02 1.90E-02 L2-011-104-FSGS-006-SS 8.97E-02 3.29E-03 5.00E-02 3.89E-02 1.65E-03 L2-011-104-FSGS-007-SS 2.36E-02 0.00E+00 1.40E-01 1.09E-01 0.00E+00 L2-011-104-FSGS-008-SS 1.74E-02 4.36E-02 0.00E+00 2.69E-02 2.19E-02 L2-011-104-FSGS-009-SS 2.41E-02 5.46E-04 0.00E+00 1.29E-01 2.74E-04 L2-011-104-FSGS-012-SS 0.00E+00 5.76E-02 0.00E+00 5.78E-02 2.89E-02 L2-011-104-FSGS-013-SS 5.36E-02 4.16E-02 6.98E-02 7.46E-02 2.09E-02 Note: Bold values indicate concentrations greater than MDC. The implementation of survey specific QC measures included the collection of four (4) samples (L2-011-104-FQGS-003-SS, L2-011-104-FQGS-004-SS, L2-011-104-FSGS-003-SS SPLIT, and L2-011-104-FSGS-009-SS SPLIT) for split and duplicate sample analysis. The on-site laboratory analyzed the QC samples using the on-site gamma spectroscopy system. A summary of the analytical results for the QC sample is provided in Table 7-6. 26
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Gamma spectroscopy results revealed that no ROC were positively identified in any QC sample. The concentration for Sr-90 was inferred based on the ratio specified in Table 5-1. Table 7 Summary of Gamma Spectroscopy Results for QC Samples Co-60 Cs-137 Eu-152 Eu-154 Sr-90 Sample ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) L2-011-104-FQGS-003-SS 0.00E+00 3.69E-02 1.38E-02 1.75E-02 1.85E-02 L2-011-104-FQGS-004-SS 2.24E-02 4.35E-02 1.68E-01 6.03E-02 2.18E-02 L2-011-104-FSGS-003-SS 0.00E+00 3.56E-02 0.00E+00 9.08E-02 1.79E-02 SPLIT L2-011-104-FSGS-009-SS 5.29E-02 4.18E-02 2.85E-02 3.49E-02 2.10E-02 SPLIT Note: Bold values indicate concentrations greater than MDC. The SOF or "unity rule" is the mathematical test used to evaluate compliance with radiological criteria for license termination when more than one radionuclide has been determined to be potentially present. The equation for the unity rule is: Equation 4 Ci + C2 +.......... .. C n ::;; l DCGL1 DCGL2 DCGLn Where: Cn = concentration of radionuclide n DCGLn = DCGL of radionuclide n. The results of the unity rule calculation for the ROC in the systematic sample population for survey unit L2-011-104 are provided in Table 7-7. Table 7 Sum-of-Fractions for Systematic and QC Samples Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L2-011-104-FSGS-001-SS 0.0092 0.0041 0.0000 0.0000 0.0000 0.0133 L2-011-104-FSGS-002-SS 0.0162 0.0034 0.0003 0.0128 0.0000 0.0327 L2-011-104-FSGS-003-SS 0.0050 0.0041 0.0000 0.0071 0.0000 0.0162 L2-011-104-FSGS-004-SS 0.0135 0.0032 0.0091 0.0120 0.0000 0.0378 L2-011-104-FSPA-005-AV 0.0168 0.0055 0.0118 0.0020 0.0000 0.0361 L2-011-104-FSPA-006-AV 0.0110 0.0018 0.0000 0.0284 0.0000 0.0412 L2-011-104-FSPA-007-AV 0.0000 0.0047 0.0010 0.0000 0.0000 0.0056 L2-011-104-FSPA-008-AV 0.0012 0.0022 0.0123 0.0000 0.0000 0.0157 27
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L2-011-104-FSPA-009-AV 0.0086 0.0039 0.0076 0.0088 0.0000 0.0290 L2-011-104-FSGS-010-SS 0.0242 0.0039 0.0101 0.0002 0.0000 0.0385 L2-011-104-FSGS-011-SS 0.0150 0.0057 0.0030 0.0008 0.0000 0.0247 L2-011-104-FSPA-012-AV 0.0134 0.0022 0.0099 0.0036 0.0000 0.0291 L2-011-104-FSPA-013-AV 0.0095 0.0057 0.0024 0.0025 0.0000 0.0201 L2-011-104-FSGS-014-SS 0.0171 0.0032 0.0019 0.0347 0.0000 0.0569 L2-011-104-FQGS-003-SS 0.0000 0.0021 0.0016 0.0022 0.0000 0.0060 L2-011-104-FQGS-004-SS 0.0058 0.0025 0.0197 0.0076 0.0000 0.0357 L2-011-104-FSGS-003-SS SPLIT 0.0000 0.0020 0.0000 0.0115 0.0000 0.0136 L2-011-104-FSGS-009-SS SPLIT 0.0138 0.0024 0.0033 0.0044 0.0000 0.0240 Systematic Samples Number of Systematic Samples = 14
# of Systematic Samples with SOF > 1 = 0
# of Systematic Samples with SOF > 0.1 (HTD Assessment) = 0 Max Individual Systematic Sample SOF = 0.0569 Mean Systematic Sample SOF = 0.0284 The results of the unity rule calculation for the ROC in the judgmental and investigational sample populations for survey unit L2-011-104 are provided in Table 7-8.
Table 7-8 Sum-of-Fractions for Judgmental and Investigational Samples Fraction of Operational DCGL Sample ID SOF Co-60 Cs-137 Eu-152 Eu-154 Sr-90 L2-011-104-FJPA-015-AV 0.0130 0.0027 0.0222 0.0139 0.0000 0.0518 L2-011-104-FJGS-015-SS 0.0150 0.0031 0.0072 0.0030 0.0000 0.0284 L2-011-104-FJGS-015-SB 0.0089 0.0025 0.0000 0.0044 0.0000 0.0158 L2-011-104-FSGS-005-SS 0.0126 0.0022 0.0003 0.0047 0.0000 0.0198 L2-011-104-FSGS-006-SS 0.0234 0.0002 0.0059 0.0049 0.0000 0.0344 L2-011-104-FSGS-007-SS 0.0062 0.0000 0.0165 0.0138 0.0000 0.0364 L2-011-104-FSGS-008-SS 0.0045 0.0025 0.0000 0.0034 0.0000 0.0105 L2-011-104-FSGS-009-SS 0.0063 0.0000 0.0000 0.0163 0.0000 0.0227 L2-011-104-FSGS-012-SS 0.0000 0.0033 0.0000 0.0073 0.0000 0.0107 L2-011-104-FSGS-013-SS 0.0140 0.0024 0.0082 0.0095 0.0000 0.0341 28
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Judgmental/Investigational Samples Number of Judgmental/Investigational Samples = 10
# of Judgmental/Investigational Samples with SOF > 1 = 0
# of Judgmental/Investigational Samples with SOF > 0.1 (HTD Assessment) = 0 Max Individual Judgmental/Investigational Sample SOF = 0.0518
- 8. QUALITY CONTROL The on-site laboratory processed four (4) split and duplicate samples (L2-011-104-FQGS-003-SS, L2-011-104-FQGS-004-SS, L2-011-104-FSGS-003-SS SPLIT, and L2-011-104-FSGS-009-SS SPLIT) using gamma spectroscopy analysis. The data was evaluated using USNRC acceptance criteria specified in Inspection Procedure No. 84750, Radioactive Waste Treatment, and Effluent and Environmental Monitoring (Reference 16). K-40 was substituted for the assessment because Cs-137 was not identified in the standard or comparison samples. There was acceptable agreement between field split and duplicate results. Refer to Attachment 4 for data and quality control analysis results.
- 9. INVESTIGATIONS AND RESULTS Two (2) soil samples were collected to investigate alarms in scan lanes D4 and sample location 15. The samples (L2-011-104-FJPA-015-AV and L2-011-104-FJGS-015-SB) were analyzed using the on-site gamma spectroscopy system. Gamma spectroscopy results revealed that no ROC were positively identified in any of the investigational samples. The maximum SOF for investigational samples, when compared to the Operational DCGL, is 0.0518.
- 10. REMEDIATION AND RESULTS No radiological remedial action as described by MARSSIM Section 5.4 was performed in this survey unit prior to or as a result of the FSS. Chapter 4 of the LTP determined that remediation beyond that required to meet the release criteria is unnecessary and that the remaining residual radioactivity in soil was ALARA.
- 11. CHANGES FROM THE FINAL STATUS SURVEY PLAN There were no addendums to the FSS plan.
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS
- 12. DATA QUALITY ASSESSMENT (DQA)
The DQO sample design and data were reviewed in accordance with LC-FS-PR-008, Final Status Survey Data Assessment (Reference 17) for completeness and consistency. Documentation was complete and legible. Surveys and the collection of samples were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 2. The survey design had adequate power as indicated by the Retrospective Power Curve (see Attachment 6). The measurement results indicated that all samples were less than a SOF of one (1) when compared to the OpDCGLS. Although MARSSIM states that the Sign Test need not be performed in the instance that no measurements surpass the Operational DCGL, the test was conducted to demonstrate coherence to the statistical principles of the DQO process. The Sign Test was performed on the data and compared to the original assumptions of the DQOs. The evaluation of the Sign Test results clearly demonstrates that the survey unit passes the unrestricted release criteria, thus, the null hypothesis is rejected. The results of the Sign Test are presented in Attachment 3. The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation). All data was considered valid including negative values, zeros, values reported below the MDC, and values with uncertainties that exceeded two standard deviations. The mean and median values for each ROC were well below the respective Operational DCGLs. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power. Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs. The mean of all identified isotopes are less than the Consultation Triggers for Residential Soil Concentration depicted in Table H.1 of NUREG 1757, Vol.1, Rev. 2 (MOU Table 1). The full table is included in Attachment 5 of this release record. The data for Cs-137 is presented graphically through a frequency plot and quantile plot. All graphical presentations are provided in Attachment 6.
- 13. ANOMALIES No anomalies were observed during the performance or analyses of the survey.
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS
- 14. CONCLUSION Survey unit L2-011-104 has met the DQOs of the FSS plan. The ALARA criteria as specified in Chapter 4 of the LTP were achieved. The Elevated Measurement Comparison for soils was not applicable and remediation was not required.
All identified ROC were used for statistical testing to determine the adequacy of the survey unit for FSS. Evaluation of the data shows that none of the systematic ROC concentration values exceeds the OpDCGLS; therefore, in accordance with LTP Section 5.11, the survey unit meets the release criteria. The sample data passed the Sign Test. The null hypothesis was rejected. The Retrospective Power Curve showed that adequate power was achieved. The survey unit is properly classified as Class 2. The dose contribution from soil in survey unit L2-011-104 is 0.2557 mrem/yr TEDE, based on the average concentration of the ROC in samples used for non-parametric statistical sampling. Survey unit L2-011-104 is acceptable for unrestricted release.
- 15. REFERENCES
- 1. LC-FS-PR-009, Final Status Survey Data Reporting
- 2. La Crosse Boiling Water Reactor License Termination Plan
- 3. LC-FS-PR-002, Final Status Survey Package Development
- 4. NUREG-1575, Revision 1, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM)
- 5. La Crosse Boiling Water Reactor Historical Site Assessment
- 6. RS-TD-313196-004, LACBWR Soil DCGL, Basement Concrete DCGL, and Buried Pipe DCGL
- 7. RS-TD-313196-001, Radionuclides of Concern during LACBWR Decommissioning
- 8. NUREG-1757, Volume 2, Revision 1, Consolidated Decommissioning Guidance Characterization, Survey, and Determination of Radiological Criteria, Final Report
- 9. LC-FS-TSD-002, Operational Derived Concentration Guideline Levels for Final Status Survey
- 10. LC-QA-PN-001, Final Status Survey Quality Assurance Project Plan
- 11. RS-TD-313196-006, Ludlum Model 44-10 Detector Sensitivity
- 12. LC-FS-PR-012, Chain of Custody Protocol
- 13. LC-FS-PR-004, Sample Media Collection for Site Characterization and Final Status Survey 31
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS
- 14. LC-FS-PR-005, Sample Media Preparation for Site Characterization and Final Status Survey
- 15. LC-FS-PR-001, Sample Storage
- 16. USNRC Inspection Procedure No. 84750, Radioactive Waste Treatment, and Effluent and Environmental Monitoring
- 17. LC-FS-PR-008, Final Status Survey Data Assessment
- 16. ATTACHMENTS Attachment 1 Figure Attachment 2 Scan Data Attachment 3 Sign Test Attachment 4 Quality Control Assessment Attachment 5 Consultation Triggers for Residential Soil Concentrations Attachment 6 Graphical Presentations Attachment 7 Sample Analytical Reports Attachment 8 GEL Laboratories Analytical Reports 32
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS ATTACHMENT 1 FIGURE 33
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSE SOLUTIONS Figure 16 Survey Unit L2-011-104 Systematic and Judgmental Sample Locations Map Legend L2-011-104 (5,285 m 2) 3'.) 11
, 1 S> U.ars I I I 15 50 75 100 125 l50 175 Fec 0 Systematic Samples L2--011 -104 Samples
- LACBWR Site Genoa, WI Biased Samples .,..::::= Date 0912612019 L.\CROSSESOL£;TIO,,:s- Drawing 908 04.c 34
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS ATTACHMENT 2 SCAN DATA 35
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Table 16-1 Survey Unit L2-011-104 Complete Scan Data Scan Avg Action Detector Detector M2350-1 Logged Scan Location Background Level Type ID ID Result Alarms (cpm) (cpm) (cpm) 44-10 215123 216185 01 SP 3,886 5,175 6,937 0 44-10 215123 216185 01 SP 4,054 5,175 6,937 0 44-10 215123 216185 02 SP 4,744 5,175 6,937 0 44-10 215123 216185 02 SP 4,942 5,175 6,937 0 44-10 215123 216185 03 SP 5,417 5,175 6,937 0 44-10 215123 216185 03 SP 5,478 5,175 6,937 0 44-10 226940 117014 03 SP QC 5,868 5,531 7,293 0 44-10 226940 117014 03 SP QC 5,966 5,531 7,293 0 44-10 215123 216185 04 SP 4,849 5,175 6,937 0 44-10 215123 216185 04 SP 4,530 5,175 6,937 0 44-10 226940 117014 04 SP QC 4,739 5,531 7,293 0 44-10 226940 117014 04 SP QC 4,909 5,531 7,293 0 44-10 215123 216185 05 SP 3,578 4,608 6,370 0 44-10 215123 216185 05 SP 4,926 4,608 6,370 0 44-10 215123 216185 05 SP 3,987 4,608 6,370 0 44-10 215123 216185 06 SP 4,630 4,608 6,370 0 44-10 215123 216185 06 SP 5,226 4,608 6,370 0 44-10 215123 216185 06 SP 4,434 4,608 6,370 0 44-10 215123 216185 07 SP 4,857 4,608 6,370 0 44-10 215123 216185 07 SP 5,012 4,608 6,370 0 44-10 215123 216185 07 SP 4,723 4,608 6,370 0 44-10 215123 216185 08 SP 4,342 4,608 6,370 0 44-10 215123 216185 08 SP 4,857 4,608 6,370 0 44-10 215123 216185 08 SP 4,427 4,608 6,370 0 44-10 215123 216185 09 SP 4,457 4,608 6,370 0 44-10 215123 216185 09 SP 4,568 4,608 6,370 0 44-10 215123 216185 09 SP 4,301 4,608 6,370 0 44-10 215123 216185 10 SP 6,163 5,175 6,937 0 44-10 215123 216185 10 SP 6,444 5,175 6,937 0 44-10 215123 216185 11 SP 5,744 5,175 6,937 0 44-10 215123 216185 11 SP 5,280 5,175 6,937 0 44-10 215123 216185 12 SP 3,984 4,608 6,370 0 36
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Scan Avg Action Detector Detector M2350-1 Logged Scan Location Background Level Type ID ID Result Alarms (cpm) (cpm) (cpm) 44-10 215123 216185 12 SP 4,126 4,608 6,370 0 44-10 215123 216185 12 SP 3,952 4,608 6,370 0 44-10 215123 216185 13 SP 4,451 4,608 6,370 0 44-10 215123 216185 13 SP 4,393 4,608 6,370 0 44-10 215123 216185 13 SP 4,389 4,608 6,370 0 44-10 215123 216185 14 SP 3,871 5,175 6,937 0 44-10 215123 216185 14 SP 4,525 5,175 6,937 0 44-10 226940 117014 15 SP 7,046 4,613 6,375 1 44-10 226940 117014 15 SP 5,198 4,613 6,375 0 44-10 226940 117014 15 SP 5,396 4,613 6,375 0 44-10 226940 117014 A 01 5,894 5,977 7,739 0 44-10 226940 117014 A 02 6,695 5,977 7,739 0 44-10 226940 117014 A 03 6,412 5,977 7,739 0 44-10 226940 117014 A 04 6,120 5,977 7,739 0 44-10 226940 117014 A 05 6,785 5,977 7,739 0 44-10 226940 117014 A 06 6,939 5,977 7,739 0 44-10 226940 117014 A 07 6,479 5,977 7,739 0 44-10 226940 117014 A 08 6,996 5,977 7,739 0 44-10 226940 117014 A 09 6,544 5,977 7,739 0 44-10 226940 117014 A 10 7,319 5,977 7,739 0 44-10 226940 117014 A 11 6,178 5,977 7,739 0 44-10 226940 117014 A 12 6,128 5,977 7,739 0 44-10 226940 117014 A 13 6,395 5,977 7,739 0 44-10 226940 117014 A 14 4,583 5,977 7,739 0 44-10 226940 117014 A 15 4,388 5,977 7,739 0 44-10 226940 117014 A 16 4,373 5,977 7,739 0 44-10 226940 117014 A 17 4,198 5,977 7,739 0 44-10 226940 117014 A 18 4,230 5,977 7,739 0 44-10 226940 117014 B 01 6,131 5,661 7,423 0 44-10 226940 117014 B 02 5,336 5,661 7,423 0 44-10 226940 117014 B 03 5,132 5,661 7,423 0 44-10 226940 117014 B 04 5,481 5,661 7,423 0 37
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Scan Avg Action Detector Detector M2350-1 Logged Scan Location Background Level Type ID ID Result Alarms (cpm) (cpm) (cpm) 44-10 226940 117014 B 05 5,082 5,661 7,423 0 44-10 226940 117014 B 06 5,275 5,661 7,423 0 44-10 226940 117014 B 07 5,533 5,661 7,423 0 44-10 226940 117014 B 08 5,206 5,661 7,423 0 44-10 226940 117014 B 09 5,196 5,661 7,423 0 44-10 226940 117014 B 10 5,123 5,661 7,423 0 44-10 226940 117014 B 11 4,949 5,661 7,423 0 44-10 226940 117014 B 12 5,322 5,661 7,423 0 44-10 226940 117014 B 13 5,070 5,661 7,423 0 44-10 226940 117014 B 14 5,354 5,661 7,423 0 44-10 226940 117014 B 15 5,143 5,661 7,423 0 44-10 226940 117014 B 16 5,496 5,661 7,423 0 44-10 226940 117014 B 17 5,135 5,661 7,423 0 44-10 226940 117014 B 18 6,053 5,661 7,423 0 44-10 226940 117014 B 19 5,722 5,661 7,423 0 44-10 226940 117014 B 20 5,944 5,661 7,423 0 44-10 226940 117014 B 21 6,169 5,661 7,423 0 44-10 226940 117014 B 22 6,340 5,661 7,423 0 44-10 226940 117014 B 23 6,342 5,661 7,423 0 44-10 226940 117014 B 24 6,479 5,661 7,423 0 44-10 226940 117014 B 25 6,379 5,661 7,423 0 44-10 226940 117014 B 26 6,183 5,661 7,423 0 44-10 226940 117014 C 01 4,738 4,072 5,834 0 44-10 226940 117014 C 02 4,248 4,072 5,834 0 44-10 226940 117014 C 03 4,571 4,072 5,834 0 44-10 226940 117014 C 04 4,481 4,072 5,834 0 44-10 226940 117014 C 05 4,432 4,072 5,834 0 44-10 226940 117014 C 06 4,543 4,072 5,834 0 44-10 226940 117014 C 07 4,525 4,072 5,834 0 44-10 226940 117014 C 08 4,430 4,072 5,834 0 44-10 226940 117014 C 09 4,759 4,072 5,834 0 44-10 226940 117014 C 10 4,541 4,072 5,834 0 38
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Scan Avg Action Detector Detector M2350-1 Logged Scan Location Background Level Type ID ID Result Alarms (cpm) (cpm) (cpm) 44-10 226940 117014 C 11 4,945 4,072 5,834 0 44-10 226940 117014 C 12 4,871 4,072 5,834 0 44-10 226940 117014 C 13 5,258 4,072 5,834 0 44-10 226940 117014 C 14 4,965 4,072 5,834 0 44-10 226940 117014 C 15 5,310 4,072 5,834 0 44-10 226940 117014 C 16 5,478 5,080 6,842 0 44-10 226940 117014 C 17 5,428 5,080 6,842 0 44-10 226940 117014 C 18 5,663 5,080 6,842 0 44-10 226940 117014 C 19 5,795 5,080 6,842 0 44-10 226940 117014 C 20 5,666 5,080 6,842 0 44-10 226940 117014 C 21 5,735 5,080 6,842 0 44-10 226940 117014 C 22 6,055 5,080 6,842 0 44-10 226940 117014 C 23 6,006 5,080 6,842 0 44-10 226940 117014 C 24 6,008 5,080 6,842 0 44-10 226940 117014 C 25 6,204 5,080 6,842 0 44-10 226940 117014 C 26 6,619 5,080 6,842 0 44-10 226940 117014 C 27 5,814 5,080 6,842 0 44-10 226940 117014 C 28 6,569 5,080 6,842 0 44-10 226940 117014 D 01 5,057 4,520 6,282 0 44-10 226940 117014 D 02 4,537 4,520 6,282 0 44-10 226940 117014 D 03 4,895 4,520 6,282 0 44-10 226940 117014 D 04 7,632 4,520 6,282 1 44-10 226940 117014 D 04 4,438 4,520 6,282 0 44-10 226940 117014 D 05 5,066 4,520 6,282 0 44-10 226940 117014 D 06 4,908 4,520 6,282 0 44-10 226940 117014 D 07 4,975 4,520 6,282 0 44-10 226940 117014 D 08 5,081 4,520 6,282 0 44-10 226940 117014 D 09 4,646 4,520 6,282 0 44-10 226940 117014 D 10 4,724 4,520 6,282 0 44-10 226940 117014 D 11 4,909 4,520 6,282 0 44-10 211680 98620 D 11 QC 4,299 3,868 5,630 0 44-10 226940 117014 D 12 4,797 4,520 6,282 0 39
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Scan Avg Action Detector Detector M2350-1 Logged Scan Location Background Level Type ID ID Result Alarms (cpm) (cpm) (cpm) 44-10 211680 98620 D 12 QC 4,143 3,868 5,630 0 44-10 226940 117014 D 13 5,226 4,520 6,282 0 44-10 211680 98620 D 13 QC 4,361 3,868 5,630 0 44-10 226940 117014 D 14 5,880 4,520 6,282 0 44-10 211680 98620 D 14 QC 4,152 3,868 5,630 0 40
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS ATTACHMENT 3 SIGN TEST 41
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Table 16-2 Survey Unit L2-011-104 Sign Test SOF
# 1-Ws Sign (Ws) 1 0.0133 0.99 +1 2 0.0327 0.97 +1 3 0.0162 0.98 +1 4 0.0378 0.96 +1 5 0.0361 0.96 +1 6 0.0412 0.96 +1 7 0.0056 0.99 +1 8 0.0157 0.98 +1 9 0.0290 0.97 +1 10 0.0385 0.96 +1 11 0.0247 0.98 +1 12 0.0291 0.97 +1 13 0.0201 0.98 +1 14 0.0569 0.94 +1 Number of positive differences (S+) 14 Critical Value 10 Survey Unit Meets the Acceptance Criteria 42
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS ATTACHMENT 4 QUALITY CONTROL ASSESSMENT 43
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FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Table 16-3 Survey Unit L2-011-104 QC Assessment STANDARD COMPARISON Activity Standard Agreement Range Activity Comparison Acceptable Sample ID Radionuclide Resolution Sample ID Value Error (Low to High) Value Ratio (YIN) L2-0I 1-104-FQGS-003-SS 6.36E+00 0.91 y L2-0I I-I 04-FSGS-003-SS K-40 6.96E+00 I.0IE+00 7 0.5 2 y L2-0 I I- 104-FSGS-003-SS SPLIT 7.44E+00 1.07 L2-0l 1-104-FSGS-004-SS K-40 5.16E+00 8.37E-0l 6 0.5 2 L2-0l 1-104-FQGS-004-SS 5.34E+00 1.03 y L2-011-104-FSGS-009-SS K-40 4.48E+00 8.03E-0l 6 0.5 2 L2-011-104-FSGS-009-SS SPLIT 3.73E+00 0.83 y Comments/Corrective Actions: K-40 was substituted for the assessment because Cs-13 7 was not Table is provided to show acceptance criteria used to assess split samples. identified in either the standard or comparison sample. Re so lution Acceptable R a tio
<4 0.4-2.5 4 -7 0 .5-2.0 8- 15 0.6- 1.66 16-50 0 .75 - 1.33 51 -200 0 .80- 1.25
> 200 0 .85 -1.1 8 44
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS ATTACHMENT 5 CONSULTATION TRIGGERS FOR RESIDENTIAL SOIL CONCENTRATION 45
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Table H.1 Consultation Triggers for Residential and Commercial/Industrial Soil Contamination (MOU Table 1) Except for radium-226, thorium-232, or total uranium, concentrations should be aggregated using a sum of the fraction approach to determine site-specific consultation trigger concentrations. This table is based on single contaminant concentrations for residential and commercial/industrial land use when using generally accepted exposure parameters. Table users should select the appropriate column based on the site's reasonably anticipated land use. Radionuclide Residential Soil Concentration Industrial/Commercial Soil Concentration H-3 228 pCi/g 423 pCi/g C-14 46 oCi/g 123,000 oCi/g Na-22 9 pCi/g 14 pCi/g S-35 19,600 pCi/g 32 200,000 oCi/g Cl-36 6 oCi/g 10,700 oCi/g Ca-45 13,500 pCi/g 3 740,000 oCi/e: Sc-46 105 pCi/2: 169 pCi/g Mn-54 69 oCi/e: 112 oCi/g Fe-55 269,000 pCi/g 2,210,000 oCi/g Co-57 873 pCi/g 1.420 oCi/e: Co-60 4pCi/g 6 oCi/J!: Ni-59 20,800 pCi/g 1,230 000 pCi/e: Ni-63 9,480 oCi/e: 555.000 oCi/g Sr-90+0 23 pCi/g 1,070 oCi/g Nb-94 2 pCi/g 3 oCi/g Tc-99 25 oCi/g 89,400 oCi/g I-129 60 oCi/g 1,080 oCi/i:t Cs-134 16 pCi/g 26 pCi/g Cs-137+0 6 oCi/g 11 pCi/g Eu-152 4oCi/g 7 pCj/g Eu-154 5 pCi/g 8 pCi/g Ir-192 336 pCi/g 544 pCi/g Pb-2IO+D 15 oCi/g 123 oCi/g Ra-226 5 pCi/g 5 oCi/g Ac-227+D 10 pCi/g 21 oCi/e: Th-228+0 15 oCi/g 25 pCj/g Th-232 5 pCi/g 5 oCi/g U-234 401 pCi/2 3,310 pCi/g U-235+0 20 oCi/e: 39 oCi/g U-238+0 74 pCi/g 179 oCi/g total uranium 47m2'h 1230 me/ki:r Pu-238 297 oCi/g 1.640 oCi/2 Pu-239 259 pCi/g 1,430 pCi/g Pu-241 40,600 pCi/2 172,000 pCi/2 Am-241 187 oCi/g 568 oCi/e: Cm-242 32.200 oCi/g 344,000 oCi/e: Cm-243 35 pCi/g 67 pCi/g 46
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS ATTACHMENT 6 GRAPHICAL PRESENTATIONS 47
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Figure 16 Quantile Plot for Cs-137 Concentration 48
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS Figure 16 Histogram for Cs-137 Concentration 49
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSE SOLUTIONS Figure 16 Retrospective Power Curve for L2-011-104 Probability th t the un e .,.. -nit Passes 1.0 "'I i I I 0.8 I I I 0.6 I 0.4 0.2 I 0.0 1)% 3)% 5J% -0% 9)% 100% " 110% 1JO% 1510% True u "e
- nit 'oncent , tion (perce t of D 'GL) 50
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS ATTACHMENT 7 SAMPLE ANALYTICAL REPORTS 51
9/11/2019 3:52:15PM Page 1 of6 Analysis Report for L2-011-104-FSGS-001-SS L2-011-104 GAMMA SPECTRUM ANALYSIS Sample Identification : L2-011-104-FSGS-001-SS Sample Descnptlon : L2-011-104 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.521 E+02 grams Faclllty : Dairyland_NPP Sample Taken On : 919/2019 2:08:00PM Acquisition Started : 9/11/2019 3:21:53PM Procedure : 500ml Marinelli Operator : Administrator Detector Name :HOTLAB Geometry : 500ml Marinelli Live Time : 1BOO.a seconds Real Time : 1805.7 seconds Dead Time : 0.32% Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4098 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Description Sample Number : 7-440 PEAK ANALYSIS REPORT Pasl. Analy&iS Performed on : 9/11/2019 3:52:06PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/11/2019 3:52:15PM Page2 of6 Analysis Report for L2-011-104-FSGS-001-SS L2-011-104 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 77.21 147 - 162 154.97 7.53E+Ol 28.04 6.29E+02 1.18 M 2 238.48 473 - 489 477.44 9.44E+Ol 27.03 2.25E+02 1.47 m 3 241.72 473 - 489 483.92 4.49E+Ol 20.40 2.04E+02 1. 47 F 4 295.22 586 - 595 590.89 6.65E+Ol 22.22 1.20E+02 1. 66 F 5 351.77 696 - 708 703.97 9.26E+Ol 23.08 l.30E+02 1.35 F 6 609.20 1212 - 1225 1218.73 5.55E+Ol 17.05 7.00E+Ol 1.17 F 7 1460.59 2914 - 2927 2921.29 1. 7*2E+02 26.83 1.07E+Ol 2.42 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 9/11/2019 3:52:06PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Baclcgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 77.21 7.53E+Ol 28.04 7.53E+Ol 2.80E+Ol M 2 238.48 9.44E+Ol 27.03 9.44E+Ol 2.70E+Ol m 3 241.72 4.49E+Ol 20.40 4.49E+Ol 2.04E+Ol F 4 295.22 6.65E+Ol 22. 2.2 6.65E+Ol 2.22E+Ol F 5 351. 77 9.26E+Ol 23.08 4.18E+Ol 1.86E+Ol 5.0BE+Ol 2.96E+01 F 6 609.20 5.55E+Ol 17.05 2 .. 06E+Ol 1. 21E+Ol 3.49E+Ol 2.09E+Ol F 7 1460.59 1. 72E+02 26.83 2.82E+Ol 8.57E+OO 1.44E+02 2.82E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
9/11/2019 3:52:15PM Page3 of6 Analysis Report for L2-011-104-FSGS-001-SS L2-011-104 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Ubrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (k*VJ (pCVgrams) Uncertainty K-40 0.99 1460.75
- 10.67 3.68E+OO 7.49E-Ol PB-212 0.99 77 .11
- 17.50 2.48E-01 9.39E-02 238.63
- 44.60 1.14E-01 3.32E-02 BI-214 0.34 609.31
- 46.30 9.44E-02 5.68E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2 . 48 1509.19 2.19 1764.49 15.80 PB-214 0.99 77.11
- 10.70 4.06E-01 1.54E-01 295.21
- 19.20 2.23E-01 7.54E-02 351.92
- 37.20 1.03E-Ol 6.03E-02
* =Energy line found in the spectrum.
- =Manually added nuclide.
? =Manually edited nuclide.
@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
K-40 0.996 3.68E+OO 7.49E-Ol PB-212 0.997 1.19E-Ol 3.lSE-02 BI-214 0.349 9.44E-02 5.68E-02
9/11/2019 3:52:15PM Page4of6 Analysis Report for L2-011-104-FSGS-001-SS L2-011-104 Nuclide Nuclide Wt mean Wtmean Comments Name Id . Activity Activity Confidence (pCUgrams) Uncertainty PB-214 0.998 l.SSE-01 4.53E-02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
9/11/2019 3:52:15PM Page 5 of6 Analysis Report for L2-011-104-FSGS-001-SS L2-011-104 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/11/2019 3:52:06PM Peak Locate From Channel : 100 Pauk Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (lraV) Peak Size (CPS) Uncertalnfy Type Nuclide rn 3 241. 72 2.49468E-02 22.72 M = First peak In a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide E1181J1Y Yield{%) Activity Nuc/ldeMDA UneMDA Name (pCVgrama) (pCVgrams) (pCVgrams) (keVJ + K-40 1460.75
- 10.67 3.68E+00 7.29E-01 7.29E-01
+ AR-41 1293.64 99.16 -7.25E+06 1. 04E+07 1. 04E+07 + CO-60 1173.22 100.00 -3.39E-03 7.32E-02 8.33E-02 1332.49 100.00 3.53E-02 7.32E-02 + KR-85 513.99 0.43 6.llE+00 1.40E+0l 1. 40E+0l + Y-88 898.04 93.70 -3 .0lE-02 4.42E-02 5.59E-02 1836.06 99.20 -7.lSE-02 4.42E-02 + NB-94 702.63 100.00 5. 76E-02 5 .l0E-02 5.21E-02 871.10 100.00 -5. S0E-02 5.l0E-02 + I-1 31 284.30 6.06 7.73E-01 6.17E-02 8.70E-0l 364.48 81.20 2.llE-02 6.17E-02 636.97 7.27 4.21E-01 8.SSE-01 + CS-134 604.70 97.60 -1.0 l E-02 6.67E-02 7.17E-02 795.84 85.40 -4.77E-02 6.67E-02 + CS-137 661.65 85.12 7.06E-02 7.SBE-02 7.58E-02
9/11/2019 3:52:15PM Page6of6 Analysis Report for l2-011-1Q4..FSGS-001*SS L2-011-104 Nuclide Energy Yield(%) Activity Nuclide MDA LlneMDA Name (pCVgrams) {pCVgrams) {pCVgrams) (keV) + CE-144 80.12 1.36 -1.35E+OO 3.74E-01 4.SOE+OO 133.51 11.09 -1.52E-Ol 3.74E-Ol + EU-152 121. 78 28.40 -3.70E-02 1. 41E-Ol l.41E-Ol 344.28 26.60 -5.90E-03 l.85E-01 1408.00 20.74 -1.55E-02 2.4BE-01 -t; EU-154 123.07 40.40 -4.29E-02 9.90E-02 9.90E-02 723.30 19.70 -2 .04E-02 2.77E-01 1274.51 35.50 -1.BSE-02 1. 96E-01 + EU-155 86.54 32.80 -5.21E-02 1. 59E-01 1. 59E-01 105.31 21.80 -1. 05E-01 1.94E-01 + BI-214 609.31
- 46.30 9.44E-02 1.17E-Ol 1.17E-01 1120.29 15.10 -1.30E-Ol 5.25E-01 1238 .11 5.94 5.74E-01 1.53E+OO 1377.67 4.11 9.35E-Ol 1. 78E+OO 1407.98 2.48 -1.29E-01 2.0SE+OO 1509.19 2.19 -1.22E-Ol 2.66E+OO 1764.49 15.80 1.97E-01 4.76E-01
+ PB-214 77.11
- 10.70 4.06E-Ol 1.21E-Ol 5.61E-01 295.21
- 19.20 2.23E-01 1.38E-01 351.92
- 37.20 1. 03E-01 1. 21E-Ol
+ PA-228 89.95 22.00 -9.79E-02 6.70E-01 1.llE+OO 93.35 35.00 -8.26E-02 6.70E-01 105.00 16.30 -1.45E+OO l.22E+OO 12 9. 22 2.97 8.43E+OO 6.69E+OO 338.32 5.30 9.77E-01 4.23E+OO 463.00 13.80 -S.23E-02 l.69E+OO 911. 23 16.70 2.00E+OO 1. 88E+OO + AM-241 59.54 36.30 1.82E-Ol 2.94E-Ol 2.94E-Ol + CM-243 103.76 23.00 -2.74E-01 1.82E-Ol l.82E-Ol 228.18 10.60 -5.23E-Ol 3.SlE-01 277.60 14.00 -4.27E-02 3.07E-Ol
+ = Nuclide identified during the nuclide identification * = Energy line found in the spectrum > = MDA value not calculated @ = Half-life too short to be able to perform the decay correction ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
9/11/2019 4:27;13PM Page 1 of7
-1i'Apex-Gamma Analysis Report for L2-011-104-FSGS-002-SS L2-011-104 GAMMA SPECTRUM ANALYSIS Sample Identification * : L2-011-104-FSGS-002-SS Sample Description : L2-o11-104 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.670E+02 grams Facllity : Dalryland_NPP Sample Taken On : 919/2019 2:15:00PM Acquisition Started : 9/11/2019 3:56:SSPM Procedure : 500ml Marinelli Operator : Administrator Detector Name :HOTLAB Geometry : 500ml Marinelli live Time : 1800.0 aec:onds Real lime : 1805.4 seconds Dead Time : 0.30 %
Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy CaDbratlon Used Done On : 7/812014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Description Sample Number : 7441 PEAK ANALYSIS REPORT Peak Anaiysis Pertom1ed on : 9/11/2019 4:27:04PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/11/2019 4:27:13PM Page2of7 Analysis Report for L2-011-104-FSGS-002-SS L2-011-104 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 76.53 147 - 160 153.60 1. 87E+02 52.35 9.21E+02 3.11 F 2 185.68 368 - 375 371. 86 5.98E+Ol 30.22 3.48E+02 1.46 M 3 238.58 471 - 488 477.64 2.66E+02 38.73 2.44E+02 1.37 m 4 241.79 471 - 488 484.05 7.07E+Ol 22.92 2.33E+02 1.38 F 5 295.14 582 - 595 590.73 1.18E+02 27.74 2.65E+02 1.37 F 6 338.27 672 - 683 676.97 6.07E+Ol 20.91 1.65E+02 1.28 F 7 351.82 695 - 710 704.07 2.30E+02 34.12 2.31E+02 1.44 F 8 583.02 1158 - 1175 1166.38 9.92E+Ol 22.66 9.0SE+Ol 2.08 F 9 609.14 1213 - 1224 1218.61 1.64E+02 27.91 7.48E+Ol 1. 61 F 10 910.42 1815 - 1826 1821.08 3.86E+Ol 15.20 6.47E+Ol 1.24 F 11 1119.85 2235 - 2245 2239.87 2.62E+Ol 14.42 6.75E+Ol 1.49 F 12 1460.58 2914 - 2929 2921.27 2.78E+02 34.12 2.68E+Ol 2.27 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/11/2019 4:27:04PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76.53 1.87E+02 52.35 1.87E+02 5.24E+Ol F 2 185.68 5.98E+Ol 30.22 5.98E+Ol 3.02E+Ol M 3 238.58 2.66E+02 38.73 2.66E+02 3.87E+Ol m 4 241.79 7.07E+Ol 22.92 7.07E+Ol 2 . 29E+Ol F 5 295.14 1 .. 18E+02 27.74 1.18E+02 2.77E+Ol F 6 338.27 6.07E+Ol 20.91 6.07E+Ol 2.09E+Ol F 7 351. 82 2.30E+02 34.12 4.18E+Ol 1. 86E+Ol 1.88E+02 3.89E+Ol F 8 583.02 9.92E+Ol 22.66 9.92E+Ol 2.27E+Ol F 9 609.14 l.64E+02 27.91 2.06E+Ol 1.21E+Ol 1.43E+02 3.04E+01 F 10 910.42 3.86E+Ol 15.20 3.86E+Ol 1.52E+Ol F 11 1119.85 2.62E+Ol 14.42 2.62E+Ol 1. 44E+Ol F 12 1460.58 2.78E+02 34.12 2.82E+Ol 8.57E+OO 2.50E+02 3.52E+Ol
9/11/2019 4:27:13PM Pagc3 of7 Analysis Report for L2-011-104-FSGS-002-SS L2-011-104 M = First peak In a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTlAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Vleld(3/4) Activity Activity Name Confidence (kaV) (pCVgrams) Uncertainty K-40 0.99 1460.75
- 10.67 6.27E+OO 9.50E-Ol PB-212 0.98 77 .11
- 17.50 6.lSE-01 l.77E-Ol 238.63
- 44. 60 3.17E-01 4.89E-02 BI-214 0.57 609.31
- 46.30 3.81E-Ol B.35E-02 1120.29
- 15.10 3.69E-Ol 2.04E-01 1238.11 5.94 1377.67 4.11 1407. 98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.99 77.11
- 10. 70 1.0lE+OO 2.89E-Ol 295.21
- 19.20 3.88E-01 9.35E-02 351. 92
- 37.20 3.74E-Ol 7. 96E-02 RA-226 0. 95 186.21
- 3.28 8.12E-01 4.13E-01
=Energy line found In the spectrum.
- =Manually added nuclide.
? =Manually edited nuclide.
@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT
9/11/2019 4:27:13PM Page4of7 Analysis Report for L2-011-104-FSGS-002-SS L2-011-104 Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Conndence Uncertainty (pCi/grams) K-40 0.995 6.27E+OO 9.SOE-01 PB-212 0.985 3.21E-01 4~72E-02 BI-214 0.577 3.79E-01 7.73E-02 PB-214 0.990 3.SSE-01 5.94E-02 RA-226 0.956 8.12E-01 4.13E-01
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000sigma
9/11/2019 4:27:13PM PageSof7 Analysis Report for L2-011-104-FSGS-002-SS L2-011-104 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 9/11/2019 4:27:04PM Peak Locate Frcm Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (lceV) Peak Size (CPS) Uncertainty 1)-pe Nuclide m 4 241.79 3.93054E-02 16.20 F 6 338.27 3.37429E-02 17.21 Tol. AC-228 PA-228 F 8 583.02 S.51331E-02 11.42 F 10 910.42 2.14347E-02 19.70 Tol. PA-228 M = First peak In a multiplet region m ::: Other peak in a multiplet region F::: Fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C;\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide IIDA UneMDA Name (lrev,J (pCVgnuns) (pCVgrams) (pCVgrams) + K-40 1460.75
- 10.67 6.27E+OO B.35E-Ol 8.35E-01
+ AR- 41 1293.64 99 .1 6 O.OOE+OO 1.31E+07 1.31E+07 + C0-60 1173.22 100.00 3 .37E-02 9.lSE-02 1.0lE..;01 1332.49 100.00 6.19E-02 9.lSE-02 + KR-85 513.99 0.43 l . 76E+Ol 1.53E+Ol 1. 53E+Ol + Y-88 898.04 93.70 1.75E-02 5 ,26E-02 7.66E-02 1836.06 99.20 -7.SOE-02 5.26E-02 + NB-94 702 . 63 100.00 1.47E-02 6.67E-02 6.67E-02 871.10 100.00 2.llE-02 7.23E-02 + I-131 284.30 6 .06 -7.09E-02 7.25E-02 9.67E-01
9/1112019 4:27:13PM Page6of7 Analysis Report for L2-011-104-FSGS-002-SS L2-011-104 Nuclide Energy Vleld(%) Activity NuclldeMDA UneMDA Name (keV) (pCVgrams) (pCVgrams) (pCVgrams) I-131 364.48 81.20 -3.57E-02 7.25E-02 7.25E-02 636.97 7.27 -5.0BE-01 8.60E-Ol + CS-134 604.70 97.60 -4.27E-02 7.24E-02 9.SlE-02 795.84 85.40 -7.52E-02 7.24E-02 + CS-137 661.65 85.12 5.98E-02 7.85E-02 7.85E-02 + CE-144 80.12 1.36 -2.79E+OO 4.34E-Ol 5.67E+OO 133.51 11.09 9.0lE-02 4.34E-Ol + EU-152 121. 78 28.40 -4 .15E-02. 1. 70E-Ol 1. 70E-01 344.28 26.60 2.65E-03 2.18E-Ol 1408.00 20.74 1.54E-01 3.07E-Ol + EU-154 123.07 40.40 -3.62E-02 1. 20E-01 1.20E-01 723.30 19.70 1. 71E-Ol 3.35E-Ol 1274.51 35.50 1.0lE-01 2.58E-01 + EU-155 86.54 32.80 -2.20E-01 1. 92E-01 1. 92E-01 105.31 21.80 9.llE-02 2.25E-01 + BI-214 609.31
- 46.30 3.81E-01 l.lSE-01 1.lSE-01 1120.29
- 15.10 3.69E-Ol 4.64E-01 1238.11 5.94 3.22E-02 1.77E+OO 1377.67 4.11 -l .16E+OO 1. 7 5E+OO 1407.98 2.48 l.28E+OO 2.57E+OO 1509.19 2.19 1.25E+OO 3.27E+OO 1764.49 15.80 6.31E-01 6.53E-01
+ PB-214 77 .11
- 10.70 1. OlE+OO 1. 48E-Ol 6.46E-01 295.21
- 19.20 3.88E-Ol 2.16E-01 351.92
- 37.20 3.74E-Ol 1. 48E-Ol
+ PA-228 89.95 22.00 1. 78E+OO 7.90E-01 1.37E+OO 93.35 35.00 1.19E-01 7.90E-Ol 105.00 16.30 -1.75E-01 1. 44E+OO 129.22 2.97 1.28E+OO 7.77E+OO 338.32 5.3"0 3.29E+OO 5.0lE+OO 463.00 13.80 -2.llE+OO 1. 83E+OO 911.23 16.70 3.0SE+OO 2.80E+OO + AM-241 59.54 36.30 8.54E-02 3.41E-01 3.41E-Ol + CM-243 103.76 23.00 -7.79E-02 2.llE-01 2. llE-01 228.18 10.60 -1.73E-01 4.44E-01 277.60 14.00 2.18E-Ol 3.63E-01
+ = Nuclide identified during the nuclide Identification * = Energy line found in the spectrum ,. = MDA value not calculated @ = Half-life too short to be able to perform the decay correction ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
9/11/2019 4:27:13PM Page 7of7 Analysis Report for L2-011-104-FSGS-002-SS L2-011-104
9/12/2019 6:34:39AM Page l of6 JApex-Gamma Analysis Report for L2-011-104-FSGS-003-SS L2-011-104 GAMMA SPECTRUM ANALYSIS Sample ldentificatle>n : L2-011-104-FSGS-003-SS Sample Description : l.2-011-104 Sample Type : 500 ml Marinelll Unit Sample Point Sample Size : 8.283E+02 grams Facility : Dairyland_NPP Sample Taken On : 9/9/2019 1:44:00PM Acquisition Started : 9/1 2/2019 6:04:20AM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Resllime : 1805.5 seconds Dead Time : 0.31 o/o Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration U~d Done On : 7/812014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Catlbratlon Description Sample Number : 7443 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 9/12/2019 6:34:30AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/12/2019 6:34:39AM Page2 of6 Analysis Report for L2-011-104-FSGS-003..SS L2-011-104 Peale Energy ROI ROI Peak NetPeak Net Area Continuum FWHIII No. {keV) start and Centroid Area Uncertainty Counts (keV) F 1 77.02 147 - 158 154.58 8.98E+Ol 29.63 6.56E+02 0.85 F 2 238.52 474 - 485 477.52 2.72E+02 39 . 10 3.17E+02 1.42 F 3 295.29 588 - 596 591.02 6.60E+Ol 23.36 1.88E+02 1.33 F 4 338.36 674 - 682 677 .16 4.45E+Ol 19.10 1.47E+02 1.09 F 5 351.92 699 - 7 10 704.27 1.57E+02 29.25 1.47E+02 1.58 F 6 419.02 834 - 843 838.45 1. 80E+Ol 12.25 5.82E+Ol 1.25 F 7 510.09 1016 - 1025 1020.54 3.0lE+Ol 14.46 7.58E+Ol 1.05 F 8 583.04 1163 - 1172 1166.43 7.06E+Ol 19.41 5.39E+Ol 1. 63 F 9 609.20 1213 - 1224 1218.73 9.49E+Ol 22.56 7.39E+Ol 1. 75 F 10 910.94 1816 - 1829 1822.11 4.89E+Ol 16.48 4.90E+Ol 1.90 F 11 968.74 1933 - 1944 1937.70 2.08E+Ol 14.14 6.23E+Ol 1. 92 F 12 1460.42 2912 - 2929 2920.96 2.93E+02 34.53 9.00E+OO 2.59 F 13 1764.02 3522 - 3534 3528.11 2.96E+Ol 11.59 6.SOE+OO 2.49 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/12/2019 6:34:30AM Env. Background File : C:\Canbena\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted. Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 77.02 8.98E+Ol 29.63 8.98E+Ol 2. 96E+Ol F 2 238.52 2.72E+02 39.10 2. 72E+02 3.91E+Ol F 3 295.29 6.60E+Ol 23.36 6.60E+Ol 2.34E+Ol F 4 338.36 4.45E+Ol 19.10 4.45E+Ol 1. 91E+Ol F 5 351. 92 1.57E+02 29.25 4.18E+Ol 1. 86E+Ol l.15E+02 3.47E+Ol F 6 419.02 1. BOE+Ol 12.25 1. BOE+Ol 1. 23E+Ol F 7 510.09 3.0lE+Ol 14.46 3.0lE+Ol 1. 45E+Ol F 8 583.04 7.06E+Ol 19.41 7.06E+Ol 1.94E+Ol F 9 609.20 9.49E+Ol 22.56 2.06E+Ol 1.21E+Ol 7.43E+Ol 2.56E+Ol F 10 910.94 4.89E+Ol 16.48 4.89E+Ol l.65E+Ol F 11 968.74 2.0BE+Ol 14.14 2.08E+Ol 1.41E+Ol F 12 1460.42 2.93E+02 34.53 2.82E+Ol 8.57E+OO 2.65E+02 3.56E+Ol F 13 1764.02 2.96E+Ol 11.59 7.59E+OO 4.90E+OO 2.21E+Ol l.26E+Ol
9/12/2019 6:34:39AM Page3 of6 Analysis Report for L2-011-104-FSGS-O0~S L2-011-104 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yleld(%) Activity Activity Name Confidence (kell) (pCVgrams) Uncettalnty* K-40 0.98 1460.75
- 10.67 6.96E+OO 1.0lE+OO PB-212 0.99 77 .11
- 17.50 3.06E-Ol 1.03E-01 238.63
- 44.60 3.3BE-01 5.17E-02 BI-214 0.54 609.31
- 46.30 2.07E-01 7.21E-02 1120.29 15.10 1238 .11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49
- 15.80 4.59E-Ol 2.64E-01 PB-214 1.00 77.11
- 10.70 5.0lE-01 l.68E-01 295.21
- 19.20 2.28E-01 8.lSE-02 351.92
- 37.20 2.41E-Ol 7.33E-02 AC-228 0.60 209.28 4.40 338.32
- 11.10 2.93E-01 1. 26E-01 794.70 4.60 911.60
- 27.70 3.27E-01 1. llE-01 964. 60 5.20 969 .11
- 16.60 2.45E-01 1. 67E-01
~ = Energy line found in the spectrum.
- .. Manually added nudide.
? = Manually edited nuclide.
=
@ Energy line not used tor Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.30 Errors quoted at 2.000sigma
9/12/2019 6:34:39AM Page4of6 Analysis Report for L2-011-104-FSGS-003-SS L2-011-104 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams) K-40 p.983 6.96E+00 1.0lE+OO PB-212 0.998 3.06E-01 4.67E-02 BI-214 0.545 2.24E-Ol 6.95E-02 PB-214 1.000 2.13E-01 5.23E-02 AC-228 0.600 2.99E-Ol 7.47E-02
? = nuclide is part of an undetermined solution X = nuclide rejected by the Interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
9/12/2019 6:34:39AM Pages of6 Analysis Report for L2-011-104-FSGS-003-SS L2-011-104 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/12/2019 6:34:30AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(3/4) Peak Tolerance Peak No. Energy (lreV) Peak Size (CPS) Uncertainty Type Nuclide F 6 419.02 1.00189E-02 33.97 F 7 510.09 1.66968E-02 24.06 F 8 583.04 3.92229E-02 13.75 M = First peak In a multiplet raglan m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%} Activity Nuclide IIDA LineMDA Name (pCVgrams) (pCVgrama) (pCVgrams) (hVJ + K-40 1460.75
- 10.67 6.96E+OO 7.48E-Ol 7.48E-01
+ AR-41 1293.64 99.16 2.57E+08 3.94E+09 3.94E+09 + C0-60 1173.22 100.00 1.90E-02 7. 5_4E-02 1.0lE-01 1332.49 100.00 -7.71E-03 7.54E-02 + KR-85 513.99 0.43 l.55E+Ol 1.47E+Ol 1.47E+Ol + Y-8B 898.04 93.70 -5.22E-02 4.91E-02 6.95E-02 1836.06 99.20 -2.09E-02 4.91E-0 2 + NB-94 702.63 100.00 -1.70E-02 6.llE-02 6.llE-02 871.10 100.00 -1.9SE-02 7.42E-02 + I-131 284.30 6.06 -4.23E-Ol 7 .36E-02 l.03E+OO 364.48 81.20 -2.17E-02 7.36E-02 636.97 7.27 -1.21E-Ol 1 .04E+OO + CS-134 604 . 70 97 . 60 -1.35E-02 7 .75E-02 8. 46E-02 795.84 85.40 -3.47E-02 7.75E-02 + CS-137 661. 65 85.12 7.14E-02 8.47E-02 8.47E-02
9/12/2019 6:34:39AM Page 6 of6 Analysis Report for L2-011-104-FSGS-003-SS L2-011-104 Nuclide Energy Yield(%) Activity NuclldeMDA UneMDA Name (pCUgrams) (pCVgrams) (pCUgrams) (keV) + CE-144 80.12 1.36 -5.85E+OO 4.45E-Ol 5.41E+OO 133.51 11.09 4.60E-01 4.45E-01 + EU-152 121.78 28.40 -1.28E-01 1.67E-01 1. 67E-01 344.28 26.60 -5.24E-02 2.17E-01 1408. 00 20.74 -4.56E-02 3.09E-Ol + EU-154 123.07 40.40 -8.14E-02 1.18E-01 1.lBE-01 723.30 19.70 -1.84E-Ol 3.16E-01 1274.51 35.50 5.64E-02 2.SSE-01 + EU-155 86.54 32.80 -8.27E-02 1. 91E..:.01 1.91E-01 105.31 21.80 -5 .26E-02 2.24E-Ol + BI-214 609.31
- 46.30 2.07E-01 1.19E-01 1.19E-Ol 1120. 29 15.10 4.54E-Ol 6.62E-01 1238 .11 5.94 -l.59E-Ol 1. 85E+OO 1377.67 4.11 1. 68E+OO 1.83E+OO 1407.98 2.48 -3.BlE-01 2.58E+OO 1509.19 2.19 1. 65E-Ol 2.81E+OO 1764.49
- 15.80 4.59E-01 3.78E-Ol
+ PB-214 77.11
- 10.70 5.0lE-01 1.27E-Ol 5.41E-Ol 295.21
- 19.20 2.28E-Ol 1.73E-01 351.92
- 37.20 2.41E-Ol 1. 27E-Ol
+ PA-228 89.95 22.00 2.75E+OO 1.25E+OO 2.16E+OO 93.35 35.00 -1. 75E-01 1. 25E+OO 105.00 16.30 -4.86E-01 2.29E+OO 129.22 2.97 -6.22E-01 1. 24E+Ol 338.32 5.30 8.27E+OO 8.34E+OO 463.00 13.80 1.56E+OO 3.03E+OO 911.23 16.70 s. 84E+*oo 4. 4o'E+OO + AM-241 59.54 36.30 3.86E-02 3.35E-01 3.35E-01 + CM-243 103.76 23.00 -8.84E-02 2.13E-01 2.13E-01 228.18 10.60 -l.04E-Ol 4.43E-Ol 277.60 14.00 l.25E-Ol 3.67E-01
+ = Nuclide identified during the nuclide identification * = Energy line found in the spectrum > = MDA value not calculated @ = Half-life too short to be able to perfonn the decay correction ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
9/12/2019 8: 18:23AM Page 1 of7 pex-Gamma Analysis Report for L2-011-104-FSGS-004-SS L2-011-104 GAMMA SPECTRUM ANALYSIS Sample Identification : L2-011-104--FSGS-004-SS Sample Description : L2-011-104 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 9.353E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/9/2019 2:21 :52PM Acquisition Started : 9/12/2019 7:48:0SAM Procedure : 500ml Marinelli Operator ; Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Tlme : 1800.0 seconds Realllme : 1805.4 seconds Dead Tlme : *0.30% Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range On channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Csllbration Used Done On : 7/812014 Efficiency CaUbration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7446 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 9/12/2019 8:18:14AM Peak Analysis From Channel : 1OD Peak Analysis To Channel : 4096
9/12/2019 8:18:23AM Page2 of7 Analysis Report for L2-011-104-FSGS-004-SS L2-01M04 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 77.02 147 - 159 154.60 1. 01E+02 32.94 7.29E+02 1.19 M 2 238.51 470 - 488 477.49 1.83E+02 32.08 l.99E+02 1.33 rn 3 241. 52 470 - 488 483.52 5.98E+Ol 21. 75 2.05E+02 1.33 F 4 295.16 584 - 594 590.77 7.77E+Ol 22. 92 1.56E+02 1.32 F 5 351.88 699 - 710 704.20 1.64E+02 28.87 1.16E+02 1.56 F 6 582.73 1160 - 1173 1165.81 6.24E+Ol 18.00 5.66E+Ol 1.61 F 7 609.19 1213 - 1224 1218.72 1.16E+02 23.69 5.69E+Ol 1. 71 F 8 911.43 1816 - 1830 1823.09 4.0lE+Ol 14.45 2.59E+Ol 2.41 F 9 969.45 1935 - 1944 1939.13 1. 74E+Ol 10.85 3.05E+Ol 1.40 F 10 1460.66 2914 - 2931 2921.44 2.50.E+02 32.64 3.12E+Ol 2.56 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 9/12/2019 8:18:14AM Env. Background File : C:\Canberra\Apex\Root\Oairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Atea Uncertainty Background Uncert. Area Uncert. F 1 77.02 1.01E+02 32.94 1.01E+02 3.29E+Ol M 2 238.51 1.83E+02 32.08 1.83E+02 3.21E+01 m 3 241. 52 5.98E+Ol 21. 75 5.98E+Ol 2.18E+Ol F 4 295.16 7.77E+Ol 22.92 7.77E+Ol 2.29E+Ol F 5 351. 88 1.64E+02 28.87 4.18E+Ol 1. 86E+Ol 1.22E+02 3.43E+Ol F 6 582.73 6.24E+Ol 18.00 6.24E+Ol 1.BOE+Ol F 7 609.19 l.16E+02 23.69 2.06E+Ol 1.21E+Ol 9.58E+Ol 2.66E+Ol F 8 911. 43 4.0lE+Ol 14.45 4.0lE+Ol 1.45E+Ol F 9 969.45 l.74E+Ol 10.85 1.74E+Ol l.09E+Ol F 10 1460.66 2.50E+02 32.64 2.82E+Ol 8.57E+OO 2.22E+02 3.37E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
9/12/2019 8:18:23AM Page3 of7 Analysis Report for L2-01M04-FSGS-004-SS L2-011-104 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Cenberra\Apex\Root\Deiryland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Vleld{%) Activity Activity Name Confidence (k*VJ (pCVgrama) Uncertainty K-40 0. 99 1460.75
- 10.67 5.16E+OO 8.37E-01 PB-212 0. 99 77.11
- 17.50 3.05E-01 1.0lE-01 238.63
- 44. 60 2.02E-Ol 3.69E-02 BI-214 0. 34 609.31
- 46.30 2.36E-01 6.68E-02 1120.29 15.10 1238.11 5.94 1377.67 4 .11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 1.00 77.11
- 10.70 4.99E-Ol 1. 66E-Ol 295.21
- 19.20 2.38E-01 7.llE-02 351.92
- 37.20 2.26E-Ol 6.44E-02
* =Energy line found in the spectrum.
- =Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
K-40 0.999 5.16E+OO 8.37E-Ol PB-212 0.998 1. 98E-Ol 3.48E-02 BI-214 0.349 2.36E-01 6.68E-02
9/12/2019 8:18:23AM Page4of7 Analysis Report for l2-011-104-FSGS-004-SS L2-011-104 Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity
- Activity Confidence Uncertainty (p~Vgrams)
PB-214 1.000 2.27E-01 4.61E-02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysts
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000slgma
9/12/2019 8:18:23AM Page5 of7 Analysis Report for L2-011-104-FSGS-004-SS L2-011-104 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/12/2019 B:18:14AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peale CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 3 241.52 3.32236E-02 18.18 F 6 582.73 3.46642E-02 14.42 F 8 911.43 2.22617E-02 18.04 Tel. AC-228 PA-228 F 9 969.45 9.66028E-03 31.21 Tol. AC-228 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Actlvlty Nuclide IIIDA LlnellDA Name (keV} (pCUgrams) (pCVgrams) (pCUgrams) + K-40 1460.75
- 10.67 5.16E+OO 8.07E-01 8.07E-Ol
+ AR-41 1293.64 99.16 4.78E+08 4.71E+09 4.71E+09 + CO-60 1173.22 100.00 3.0lE-02 7.56E-02 7.72E-02 1332.49 100.00 5.17E-02 7.56E-02 + KR-85 513.99 0.43 8.93E+OO 1. 31E+Ol 1. 31E+Ol + Y-88 898.04 93.70 3.87E-02 6.21E-02 6.66E-02 1836.06 99.20 1.39E-02 6.21E-02 + NB-94 702.63 100.00 1.SOE-02 5.44E-02 5.44E-02 871.10 100.00 -8.lSE-02 5.92E-02 + I-131 284.30 6.06 -7.04E-02 6.79E-02 8.72E-Ol 364.48 81.20 3.67E-04 6.79E-02
9/12/2019 8:18:23AM Page 6 of7 Analysis Report for L2-011-104-FSGS-004-SS L2-011-104 Nuclide Energy Yield(%} Activity Nuclide ltfDA LlneAfDA Name (pCVgramsJ (pCVgramsJ (pCVgramsJ (keVJ I-131 636.97 7.27 6.22E-Ol 6.79E-02 1.0lE+OO + CS-134 604.70 97.60 O.OOE+OO 6.87E-02 8.0lE-02 795.84 85.40 -6.55E-02 6.87E-02 + CS-137 661. 65 85.12 5.50E-02 7.38E-02 7.38E-02 + CE-144 80.12 1.36 7.46E-01 3.67E-Ol 4.85E+OO 133.51 11.09 -7.22E-03 3.67E-Ol + EU-152 121.78 28.40 -7.SOE-02 1. 40E-01 1. 40E-01 344.28 26.60 -l.20E-01 1. 79E-01 1408.00 20.74 7.75E-02 2.61E-01 + EU-154 123.07 40.40 -1.53E-02 9.84E-02 9.84E-02 723.30 19.70 9.45E-02 2.98E-Ol 1274.51 35.50 -1. l 7E-Ol 2.09E-Ol + EU-155 86.54 32.80 l.44E-02 1. 67E-01 1. 67E-01 105.31 21. 80 8.SOE-02 1. 96E-01 + BI-214 609.31
- 46.30 2.36E-01 9.84E-02 9.84E-02 1120.29 15.10 l.92E-01 5.62E-Ol 1238 .11 5.94 -7.26E-02 1. 57E+OO 1377.67 4.11 1.04E+OO 1. 57E+OO 1407.98 2.48 6.48E-01 2.18E+OO 1509.19 2.19 l.23E+OO 2.49E+OO 1764.49 15.80 6.0SE-01 5.79E-01
+ PB-214 77.11
- 10.70 4.99E-01 1.06E-01 5.17E-01 295.21
- 19.20 2.38E-Ol 1.45E-Ol 351.92
- 37.20 2.26E-Ol 1.06E-01
+ PA-228 89.95 22.00 2.53E-Ol 1. llE+OO 1. 88E+OO 93.35 35.00 1.18E+OO l.llE+OO 105.00 16.30 8.71E-01 2.09E+OO 129.22 2.97 4.35E+OO l.08E+01 338.32 5.30 l.24E+OO 6.59E+OO 463.00 13.80 1. 87E-Ol 2.81E+OO 911. 23 16.70 -5.84E-02 3.41E+OO + AM-241 59.54 36.30 -1. 29E-02 2.96E-01 2.96;E-01 + CM-243 103.76 23.00 7.92E-03 1.SBE-01 1.88E-01 228.18 10.60 8.17E-02 3.86E-Ol 277.60 14.00 l.97E-Ol 3.0SE-01
+ = Nuclide identified during the nuclide identification * = Energy line found in the spectrum > = MDA value not calculated @ = Half-life too short to be able to perform the decay correction ? = CAUTION: MDA value is inconsistent with CUrrie MDA at 95% confidence level
9/12/2019 8:18:23AM Page? of7 Analysis Report for L2-011-104-FSGS-004-SS L2-011-104
9117/2019 11:29:49AM Pagel ofS
.-..t'Apex-Gamma Analysis Report for L2-011-104-FSPA-005-AV L2-011-104 GAMMA SPECTRUM ANALYSIS Sample Identification : L2-011-104-FSPA-005--AV Sample Description : L2-011-104 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 6.769E+02 grams Faa1ity : Dairyland_NPP Sample Taken On : 9/12/2019 12:29:00PM Acquisition Started : 9/17/2019 10:59:31AM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real lime : 1805.4 seconds Daadllme ~ 0.30 %
Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 718/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency CaHbration Description Sample Number : 7455 PEAK ANALYSIS REPORT Peak Analysis Per.formed on : 9/17/2019 11:29:40AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/17/2019 11:29:49AM Page2of5 Analysis Report for L2--011-104-FSPA-005-AV l2--011-104 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 295.05 586 - 595 590.55 6.93E+Ol 21.38 1.07E+02 1. 49 F 2 351. 89 699 - 710 704.20 9.06E+Ol 23.50 1.16E+02 1. 69 F 3 609.04 1212 - 1225 1218.42 7.96E+Ol 19.67 4.20E+Ol 1.82 F 4 1460.55 2914 - 2927 2921.21 1.48E+02 25.26 1. 7 SE+Ol 2.26 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted slnglet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 9/17/2019 11:29:40AM Env. Background File : C:\Canberra\Apex\Root\Oalryland_NPP\Data\0000001364.CNF Peak Energy Original Orig.Area Ambient Baclcgr. Subtracted Subtracted No. (keV) Anta Uncertainty Background Uncert. Area Uncert. F 1 295.05 6.93E+Ol 21.38 6.93E+Ol 2.14:E+Ol F 2 351.89 9.06E+Ol 23.50 4.18E+Ol 1.86E+Ol 4.88E+Ol 3.00E+Ol F 3 609.04 7.96E+Ol 19. 67 2.06E+Ol 1.21E+Ol 5.90E+Ol 2.31E+Ol F 4 1460.55 1.48E+02 25.26 2.82E+Ol 8.57E+OO 1.20E+02 2.67E+Ol
=
M First peak in a multiplet region
=
m Other peak in a multiplet region
=
F Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES
9/17/2019 11:29:49AM Pagc3 of5 Analysis Report for L2-011-104-FSPA-005--AV L2-011-104 Nuclide Id Energy VleldrA) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.99 1460.75
- 10.67 3.86E+OO 8.85E-Ol BI-214 0.34 609.31
- 46.30 2.0lE-01 7.94E-02 1120.29 15.10 1238.11 5. 94 1377.67 4 .11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.72 77.11 10.70 295.21
- 19.20 2 , 93E-Ol 9.lSE-02 351.92
- 37.20 1.25E-01 7.68E-02
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
K-40 0.994 3.86E+OO 8.BSE-01 BI-214 0 .344 2.0lE-01 7.94E-02 PB-214 0.720 l.94E-Ol 5.88E-02
? = nucllde Is part of an undatannlned solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000slgma
9/17/2019 11:29:49AM Page4of5 Analysis Report for L2-011-104-FSPA-005-AV L2-011-104 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/17/2019 11:29:40AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(3/4) Peak Tolerance Peak No. Energy (keV} Peak Size (CPS} Uncertainty Type Nuclide All peaks were identified. M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nucl/deMDA LlneMDA Name (pCVgrams) (pCVgrams) (pCVgrams) (keVJ + K-40 1460.75
- 10.67 3.86E+00 9.77E-01 9.77E-0l
+ AR-41 1293.64 99.16 1. 20E+18 3.20E+18 3.20E+18 + CO-60 1173.22 100.00 6.45E-02 8.llE-02 1.06E-01 1332.49 100.00 -6.lBE-02 8. llE-02 + KR-85 513.99 0.43 1. 04E+0l 1. 62E+0l 1.62E+0l + Y-88 898.04 93.70 -l.21E-01 6.96E-02 6.96E-02 1836.06 99.20 3.89E-02 7.21E-02 + NB-94 702.63 100.00 8.0lE-03 6.84E-02 6.84E-02 871.10 100.00 3.43E-03 7.76E-02 + I-131 284.30 6.06 7.29E-0l l.0BE-01 1.32E+00 364.48 81.20 3.l0E-03 l.0BE-01 636.97 7.27 -2.35E-01 1. 20E+00 + CS-134 604.70 97.60 -3.22E-03 9.llE-02 9. llE-02 795.84 85.40 6.09E-02 9.57E-02 + CS-137 661.65 85.12 9.60E-02 9. llE-02 9. llE-02 + CE-144 80.12 1.36 3.45E-01 4.32E-0l 5.29E+00 133.51 11.09 3.04E-02 4.32E-0l + EU-152 121.78 28.40 1.00E-01 1.70E-01 l.70E-0l
9/17/2019 11:29:49AM Pages ofS Analysis Report for L2-011-104-FSPA-005-AV L2-011-104 Nuclide En8111Y Yleld("A,J Activity Nuclide IIDA LlneMDA Name (pCVgrams) (pCl/grams) (pCllgramsJ (keVJ EU-152 344.28 26.60 -1.59E-01 1. 70E-Ol 2.llE-01 1408.00 20.74 2.37E-Ol 3.69E-01 + EU-154 123.07 40.40 l.56E-02 1. lBE-01 l. lSE-01 723. 30 19.70 -2.57E-02 3.48E-01 1274.51 35.50 -5.74E-02 2.24E-Ol + EU-155 86.54 32.80 6.78E-04 1. 84E-Ol 1.84E-0l 105.31 21.80 2.88E-02 2.33E-01 + BI-214 609.31
- 46.30 2.0lE-01 l .29E-Ol 1.29E-01 1120.29 15.10 1. 89E-Ol 7.00E-01 1238.11 5.94 -6.27E-Ol 1. 72E+OO 1377.67 4.11 4.48E-Ol l.60E+OO 1407.98 2.48 1.9BE+OO 3. 09E+OO 1509.19 2.19 -1. 54E+OO 3.88E+OO 17 64. 4 9 15.80 2.SOE-02 5.12E-01
+ PB-214 77.11 10.70 4.19E-02 1. 4 6E-01 7.0SE-01 295.21
- 19.20 2.93E-01 1.65E-01 351. 92
- 37.20 1. 25E-Ol l.46E-01
+ PA-228 89.95 22.00 -2.93E+OO 6.53E+OO 1. lOE+Ol 93.35 35.00 -3.79E+OO 6.53E+OO 105.00 16.30 6.97E+OO 1.31E+Ol 12 9. 22 2.97 -2.79E+Ol 6.72E+Ol 338.32 5.30 l.80E+Ol 4.50E+Ol 463.00 13.80 -l. 07E+Ol 1.70E+Ol 911.23 16.70 l.53E+Ol 2.19E+Ol + AM-241 59.54 36.30 -1.28E-01 3.55E-01 3.55E-Ol + CM-243 103.76 23.00 -1.lOE-02 2.21E-Ol 2.21E-01 228.18 10.60 4.44E-02 4.71E-01 277.60 14.00 -1. 33E-01 3.78E-Ol
+ = Nuclide identified during the nuclide identification * = Energy line found In the spectrum > = MDA value not calculated @ = Half-life too short to be able to perfonn the decay correction ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
9/17/2019 1:11:10PM Page 1 of6
~Apex-Gamma Analysis Report for l2-011-104-FSPA-006-AV l2-01M04 GAMMA SPECTRUM ANALYSIS Sample Identification : l2-011-104-FSPA-006-AV Sample D88Cl'iptlon : l.2-011-104 sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.398E+02 grams Facility : Dairyland_NPP Sample Taken On ; 9/12/2019 12:58:00PM Acquisition Started : 9/17/2019 12:40:52PM Procedure : 500ml Marinelli .
Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Liva Time : 1800.0 seconds Real Time : 1805.4 seconds Dead Time : 0.30% Peak Locate Threshold : 3.00 Peak Locate Range (In channels) ; 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Callbratlon Description Sample Number : 7457 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 9/17/2019 1:11:01PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/17/2019 1:11:10PM Pagc2of6 Analysis Report for L2-011-104-FSPA-006-AV L2-011-104 Peale Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 77.09 152 - 157 154.74 3.30E+Ol 23.91 2.79E+02 0.96 F 2 238.33 472 - 482 477.13 7.21E+Ol 24.84 3.23E+02 1.03 F 3 2 94. 94 583 - 596 590.34 6.60E+Ol 23.64 1.96E+02 1.88 F 4 351. 84 698 - 710 704.11 1.01E+02 23.60 l.12E+02 1. 61 F 5 582.77 1161 - 1170 1165.89 3.lOE+Ol 14.37 4.78E+Ol 1.45 F 6 608.96 1211 - 1223 1218.25 8.00E+Ol 19.86 4.BSE+Ol 1. 65 F 7 969.02 1934 - 1943 1938.26 l.77E+Ol 11 .32 3.31E+Ol 1.53 F 8 1460.46 2913 - 2927 2921.03 l.95E+02 29.02 3.04E+Ol 2.23 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/17/2019 1:11:01PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig.Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 77.09 3.30E+Ol 23.91 3.30E+Ol 2.39E+Ol F 2 238.33 7.21E+Ol 24.84 7.21E+Ol 2.48E+Ol F 3 294.94 6.60E+Ol 23.64 6.60E+Ol 2 *.36E+Ol F 4 351.84 1.01E+02 23.60 4.18E+Ol 1.86E+Ol 5~88E+Ol 3.00E+Ol F 5 582.77 3.lOE+Ol 14.37 3.lOE+Ol 1.44E+Ol F 6 608.96 8.00E+Ol 19.86 2.06E+Ol 1. 21E+Ol 5.94E+Ol 2.33E+Ol F 7 969.02 1. 77E+Ol 11.32 1. 77E+Ol 1.13E+Ol F 8 1460.46 l.95E+02 29.02 2.82E+Ol 8.57E+OO 1.67E+02 3.03E+Ol M = First peak in a multiplet region
=
m Other peak in a multiplet region
=
F Fitted singlet Errors quoted at 2.000sigma
9/17/2019 1:11:10PM Page3 of6 Analysis Report for L2-011-104-FSPA-006-AV L2-011-104 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Oairyland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.98 1460.75
- 10.67 4.91E+OO 9.32E-01 PB-212 0 .99 77.11
- 17.50 1.26E-Ol 9.14E-02 238.63
- 44.60 1.00E-01 3.SOE-02 BI-214 0.34 609.31
- 46.30 1.85E-01 7.31E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0 .99 77.11
- 10.70 2.06E-Ol 1.49E-Ol 295.21
- 19.20 2.SSE-01 9.22E-02 351.92
- 37.20 1. 37E-01 7.0SE-02
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
K-40 0.986 4.91E+OO 9.32E-01 PB- 21 2 0.990 9.0SE-02 3.29E-02 BI-214 0.340 1.BSE-01 7.31E-02
9/17/2019 1:11:10PM Page4of6 Analysis Report for L2-011-104-FSPA-006-AV L2-011-104 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgramsJ PB-214 0.996 l.66E-Ol 5.29E-02
? = nuclide is part of an undetermined solution X = nuclide rejected by the Interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
9/17/2019 1:11 :10PM Page5of6 Analysis Report for L2-011-104-FSPA-006-AV L2-01M04 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/17/2019 1:11:01PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 PeakCPS(") Peak Tolerance Peak No.. Energy (kaV) Peak Size (CPS) Uncertainty 'fype Nuclide F 5 582.77 l.71991E-02 23.20 F 7 969.02 9.81660E-03 32.03 Tol. AC-228 M = First peak In a multiplet region m .. Other peak in a multiplet region F .. Fitted singlet Eff'Ors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dai,yland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide lfDA LineMDA Name (lreVJ (pCl/gnms) (pCVgrams) (pCVgramsJ + K-40 1460.75
- 10.67 4.91E+00 1. 00E+00 1.00E+O0
+ AR-41 1293.64 99.16 3.56E+18 4.76E+18 4.76E+18 + CO-60 1173.22 100.00 - .7 . 41E-:-03 8.68E-02 9.18E~02 1332.49 100 .00 4.22E-02 8.68:E-62 + KR-85 513.99 0.43 1. 86E+0l 1.57E+01 1.57E+0l + Y-88 898.04 93.70 -1. 91E-02 5.19E-02 7.89E-02 1836.06 99.20 -6.65E-02 5.19E-02 + NB-94 702.63 100.00 -5.89E-03 6.46E-02 6.46E-02 871.10 100.00 6.59E-03 6.SSE-02 + I-131 284.30 6.06 -7.19E-0l 8.68E-02 l.22E+00 364.48 81.20 -2.84E-02 8.68E-02 636.97 7.27 -4.59E-01 1.19E+00 + CS-134 604.70 97.60 1.40E-01 7.18E-02 8.48E-02 795.84 85.40 -3.67E-03 7.lSE-02 + CS-137 661. 65 85.12 3. 06E-02 8.60E-02 8.60E-02
9/17/2019 1:11:10PM Page 6 of6 Analysis Report for l2-011-104-FSPA-006-AV l2-011-104 Nuclide Energy Yield(%) Activity Nuclide IIDA LlnellDA Name (pCVgrams) (pCVgrams) (pCUgrams) (keV) + CE-144 80.12 1. 36 -2.68E+OO 4.02E-Ol 5.06E+OO 133.51 11.09 -1.00E-01 4.02E-Ol + EU-152 121.78 28.40 -1.91E-02 l.57E-01 1. 57E-01 344.28 26.60 -4.99E-02 2.09E-Ol 1408.00 20.74 -4.09E-02 3.60E-01 + EU-154 123.07 40.40 -3.93E-02 1. lOE-01 1.lOE-01 723.30 19.70 2.24E-Ol 3.37E-Ol 1274.51 35.50 -6.~lE-02 l.97E-Ol + EU-155 86.54 32.80 --8.87E-02 1.84E-Ol 1.84E-Ol 105.31 21. 80 8.88E-02 2.22E-01 + BI-214 609.31
- 46.30 1. 85E-01 1.21E-01 l.21E-01 1120.29 15.10 -7.llE-02 6.69E-01 1238.11 5.94 2.95E-01 1.71E+OO 1377.67 4.11 -9.64E-01 1.SSE+OO 1407.98 2.48 -3.42E-Ol 3.0lE+OO 1509.19 2.19 1.52E+OO 3.31E+OO 1764.49 15.80 1. 41E-01 5.60E-01
+ PB-214 77 .11
- 10.70 2.06E-01 1. 34E-01 3.40E-01 295.21
- 19.20 2.SSE-01 2.20E-Ol 351.92
- 37.20 l.37E-01 1. 34E-Ol
+ PA-228 89.95 22.00 1.24E+Ol 7.09E+OO l.19E+Ol 93.35 35.00 3.83E+OO 7.09E+OO 105.00 16.30 8.21E+OO l.31E+Ol 129.22 2.97 3.52E+OO 6.44E+Ol 338.32 5.30 4.04E+OO 4.46E+Ol 463.00 13.80 4.62E-01 1. 79E+01 911.23 16.70 5.24E+OO 2.21E+Ol + AM-241 59.54 36.30 -5.14E-02 3.24E-Ol 3.24E-Ol + CM-243 103.76 23.00 1.28E-01 2.16E-01 2.16E-01 228.18 10.60 6.74E-02 4.38E-Ol 277.60 14.00 -3.0SE-01 3.46E-Ol
+ = Nuclide identified during the nuclide identification * = Energy line found in the spectrum > = MDA value not calculated @ = Half-life too short to be able to perform the decay correction ? = CAUTION: MDA value Is inconsistent with Currie MDA at 95% confidence level
9/17/2019 2:15:33PM Page 1 of6 JApex-Gamma Analysis Report for L2-011-104-FSPA-007-AV L2-011-104 GAMMA SPECTRUMANALYSIS Sample Identification : L.2-011-104-FSPA-007-AV Sample Description : L.2-011-104 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.287E+02 grams Faclllty : Dalrylend_NPP Sample Taken On : 9/12/2019. 9:25:00AM Acquisition Started : 9/17/2019 1:45:15PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli LiveTlme : 1800.0 seconds Real Time : 1805.3 seconds Dead Tlrne : 0.29% Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Desaiptlon Sample Number : 7459 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 9/17/2019 2:15:23PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/17/2019 2:15:33PM Page2of6 Analysis Report for L2-011-104-FSPA-007-AV L2-011-104 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. {lceV) start end Centroid Area Uncertainty Counts {lceV) F 1 238.45 470 - 485 477.38 8.60E+Ol 24.96 3.12E+02 1.33 F 2 295.37 584 - 596 591.19 6.12E+Ol 20.66 1.62E+02 1.27 F 3 351.78 698 - 710 704.00 9.38E+Ol 24.30 l.53E+02 1. 61 F 4 609.15 1213 - 1224 1218.63 7.70E+Ol 19.71 3.92E+Ol 2.01 F 5 910.89 1816 - 1828 1822.01 2.81E+Ol 12.19 2.SOE+Ol 1.57 F 6 1460.34 2912 - 2928 . 2920.78 1. 99E+02 28.42 ... 4.37E+OO 2.46 M = First peak in a multlplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/17/2019 2:15:23PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NP?\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 238.45 8.60E+Ol 24.96 8 . 60E+Ol 2.SOE+Ol F 2 295.37 6.12E+Ol 20.66 6.12E+Ol 2.07E+Ol F 3 351.78 9.38E+Ol 24.30 4.18E+Ol 1. 86E+Ol 5.20E+Ol 3.06E+Ol F 4 609.15 7.70E+Ol 19.71 2.06E+Ol 1. 21E+Ol 5.65E+Ol 2.31E+Ol F 5 910.89 2.81E+Ol 12.19 2.81E+Ol 1.22E+Ol F 6 1460.34 l.99E+02 28.42 2.82E+Ol 8.57E+OO 1.71E+02 2.97E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
9/17/2019 2:15:33PM Page3 of6 Analysis Report for L2..011-104-FSPA-007-AV L2..011-104 NUCLIDE IDENTIFICATION REPORT Nuclide Library Uaed : C:\Canberra\Apex\Root\Dalryland_NPP\Library\HOll.AB.NLB IDENTIFIED NUCLIDES Nu,:1/de Id Energy Yield(%) Activity Activity Name Conlldence (keV) (pCVgrams) Uncertainty K-40 0.97 1460.75
- 10.67 5.llE+OO 9.32E-01 PB-212 0. 55 77.11 17.50 238.63
- 44.60 1.22E-01 3.59E-02 BI-214 0.34 609.31
- 46.30 1. 7BE-Ol 7.38E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0. 71 77.11 10.70 295.21
- 19.20 2.40E-01 8.20E-02 351.92
- 37.20 l.23E-Ol 7.28E-02
* =Energy line found In the spectrum.
- =Manually added nuclide.
? =Manually edited nuclide.
@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
K-40 0.973 5.llE+OO 9.32E-Ol PB-212 0.557 1.22E-Ol 3.59E-02 BI-214 0.348 1. 78E-01 7.38E-02
9/17/2019 2:15:33PM Page4of6 Analysis Report for l2-011-104-FSPA-007-AV L2-011-104 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) PB-214 0.719 1.75E-Ol S.44E-02
? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000slgma
9/17/2019 2:15:33PM Pages of6 Analysis Report for L2-011-104-FSPMX>7-AV L2-011-104 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/17/2019 2:15:23PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy(hV} Peak Size (CPS) Uncertainty Jype Nuclide F 5 910.89 1 .56326E-02 21.65 Tol. AC-228 PA-228 M = First peak in a multlplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Library\HOTLAB.NLB Nuclide Energy Yleld(3/4J Activity NuclldeMDA LlneMDA Name (keV) (pCVgramsJ (pCVfll'Bms) (pCVgrainsJ + K-40 1460.75
- 10.67 5. llE+00 8 . 00E-01 8 . 00E-01
+ @ AR-41 1293.64 99.16 1.00E+26 1. 00E+26 1. 00E+26 + CO-60 1173.22 100.00 -1.02E-02 7.BlE-02 9.92E-02 1332.49 100.00 -2.28E-02 7.81E-02 + KR-85 513.99 0.43 1. llE+0l l.54E+0l 1. 54E+0l + Y-88 898.04 93.70 -4.54E-03 7.30E-02 7.95E-02 1836.06 99 . 20 2 . 46E-02 7.30E-02 + NB-94 702.63 100.00 2.63E-03 6.41E-02 6.41E-02 871.10 100.00 -1.S0E-02 6.SlE-02 + I-131 284.30 6.06 3.20E-0l 8.88E-02 1.30E+0O 364.48 81.20 -5.94E-02 8.88E-02 636.97 7.27 7.0lE-01 1. 26E+00 + CS-134 604.70 97.60 - 5.93E-0 2 7.29E-02 8.13E-02 7 95. 84 85.40 -5.93E-02 7.29E- 02 + CS-137 661. 65 85.12 8.09E-02 8.82E-02 8.82E-02
9/17/2019 2:15:33PM Page6of6 Analysis Report for L2-011-104-FSPA-007-AV L2..011-104 Nuclide Energy Yleld('1/4) Activity Nuclide MDA UneMDA Name (pCVgrams) (pCVgrams) (pCVgrams} (keVJ + CE-144 80.12 1.36 -6.95E-Ol 4.23E-01 5.35E+OO 133.51 11.09 -l.68E-02 4.23E-Ol + EU-152 121.78 28.40 8.17E-03 1.62E-01 l.62E-Ol 344.28 26.60 1.79E-01 2.19E-Ol 1408.00 20.74 9.20E-02 3.59E-Ol + EU-154 123.07 40.40 -3.44E-02 1.13E-01 l.13E-01 723.30 19. 70 -5.82E-02 3.lOE-01 1274.51 35.50 -3.17E-02 2.26E-01 + EU-155 86.54 32.80 -7.79E-02 1. *a5E-Ol 1.BSE-01 105.31 21. 80 2.SOE-02 2.lSE-01 + BI-214 609.31
- 46.30 1. 78E-01 1.16E-01 l.16E-01 1120.29 15.10 3.02E-Ol 6.24E-01 1238.11 5.94 -3.54E-02 1.69E+OO 1377.67 4.11 -l.98E-Ol 1. 77E+OO 1407.98 2.48 7.69E-Ol 3.00E+OO 1509.19 2.19 -2 .45E+OO 2.61E+OO 1764.49 15.80 3.00E-01 5.31E-01
+ PB-214 77.11 10.70 7.55E-Ol 1. 48E-01 7.21E-Ol 295.21
- 19.20 2.40E-Ol 2.00E-01 351.92
- 37.20 l.23E-Ol 1. 48E-Ol
+ PA-228 89.95 22.00 l.51E+Ol 7.89E+OO 1.38E+Ol 93.35 35.00 1.33E+OO 7.89E+OO 105.00 16.30 -l.54E+OO 1. 45E+Ol 129.22 2.97 -3.65E+Ol 7.80E+Ol 338.32 5.30 4.33E+Ol 5 .24E+Ol 463.00 13.80 -4.44E+OO 2.07E+Ol 911.23 16.70 1.33E+Ol 2.80E+Ol + AM-241 59.54 36.30 2. 78E-lJ:1 3.46E-01 3.46E-Ol + CM-243 103.76 23.00 -8.89E-02 2.04E-01 2.04E-Ol 228.18 10~60 6.23E-02 4.44E-01 277.60 14.00 2.37E-01 3.74E-Ol
. == Nuclide + identified during the nuclide identification Energy line found in the spectrum > = MDA value not calculated @ = Half-life too short to be able to perform the decay correction ? = CAUTION: MDA value is inconsistent with Currie MOA at 95% confidence level
9/17/2019 3:20:28F'M Page 1 of6 JApex-Gamma Analysis Report for L2-011-104-FSPA-008-AV L2-011-104 GAMMA SPECTRUMANALYSIS Sample Identification : L2-011-104-FSPA-008-AV Sample Description : L2-011-104 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.526E+02 grams Faallty : Dairyland_NPP Sample Taken On : 9/12/2019 9:00:00AM Acquisition Started : 9/17/2019 2:50:10PM Procedure : 500ml Marinelli Operator : Administrator Detector Name :HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.5 seconds Dead Time : 0.30% Peak Locate Threshold : 3.00 Peak Locate Range On channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 71812014 Efficiency Calibration Description Sample Number : 7461 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 9/17/2019 3:20:19PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/17/2019 3:20:28PM Page2of6 Analysis Report for L2-011-104-FSPA-OO&-AV L2-011-104 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Al8a Uncertainty Counts (lreV) F 1 238.45 469 - 485 477.37 1. 20E+02 27.15 2.22E+02 1.77 F 2 295.18 587 - 595 590.81 4.62E+Ol 18.50 1.20E+02 1.11 F 3 337.49 672 - 679 675.41 2.16E+Ol 1.80 6.62E+Ol 0.52 F 4 351. 98 698 - 711 704.39 9.43E+Ol 24.31 l.54E+02 1. 72 F 5 582.87 1160 - 1172 1166.07 3.SOE+Ol 14.15 3.96E+Ol 1. 71 F 6 609.11 1212 - 1226 1218.56 7.30E+Ol 20.05 6.07E+Ol 2.29 F 7 1460.30 2913 - 2928 2920 . 70 2.09E+02 29*_5a 1.63E+Ol 2 .56 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Enors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/17/2019 3:20:19PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPp\Data\0000001364.CNF Peale Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 238.45 1.20E+02 27.15 l.20E+02 2.71E+Ol F 2 295. 1 8 4 . 62E+Ol 18.50 4 . 62E+Ol 1. 85E+01 F 3 337.49 2.16E+Ol 1.80 2.16E+Ol 1. BOE+OO F 4 351.98 9.43E+Ol 24.31 4.18E+Ol 1. 86E+01 5.26E+Ol 3.06E+Ol F 5 582.87 3.SOE+Ol 14.15 3.SOE+Ol 1.42E+Ol F 6 609.11 7.30E+Ol 20.05 2.06E+Ol 1. 21E+Ol 5 . 24E+Ol 2.34E+Ol F 7 1460.30 2 .09E+02 29.58 2.82E+Ol 8.57E+OO 1.81E+02 3.0BE+Ol M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
9/17/2019 3:20:28PM Pagc3 of6 Analysis Report for L2-011-104-FSPA-008-AV L2-011-104 NUCLIDE IDENTIFICATION REPORT Nuclide Library Uaed : C:\Canbarra\Apex\Roct\Dairyland_NPP\Llbrary\HOTIAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0. 96 1460.75
- 10.67 5.24E+OO 9.38E-01 PB-212 0. 55 77.11 17.50 238.63
- 44.60 1.64E-Ol 3.SlE-02 BI-214 0. 34 609.31
- 46.30 l.60E-01 7.22E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0 .72 77 .11 10.70 295.21
- 19.20 1.76E-01 7.09E-02 351.92
- 37.20 1.21E-01 7.06E-02
" = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy Hne not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide wt mean wt mean Comments Name Id Activity Activity Conffdence Uncertainty (pCUgrams)
K-40 0.967 5.24E+OO 9.38E-01 PB-212 0.557 1.64E-Ol 3.BlE-02 BI-214 0.346 l.60E-01 7.22E-02
9/17/2019 3:20:28PM Page4of6 Analysis Report for L2-011-104-FSPA-008-AV L2-011-104 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams) PB-214 0.721 1. 48E-01 5.00E-02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
9/17/2019 3:20:28PM PageSof6 Analysis Report for L2-011-104-FSPA-008,,AV L2-011-104 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/17/2019 3:20:19PM Peak locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 3 337.49 1. 19979E-02 4.16 AC-228 PA-228 F 5 582.87 1. 94479E-02 20.21 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberre\Apex\Root\Oalryland_NPP\Llbrary\HOTLAB.NLB Nucllde Enargy Yleld('K,) Activity Nuclide IIDA UneMDA Name (pCVgnms) (pCUgnms) (pCUg,ams) (keVJ + K-40 1460.75
- 10.67 5,24E+00 8.83E-0l 8.83E-0l
+ @ AR-41 1293.64 99.16 1.00E+26 1. 00E+26 l.0OE+26 + CO-60 1173.22 100.00 2.72E-03 8~06E-02 9.28E-02 1332.49 100.00 4.62E-03 8.06E-02 + KR-85 513.99 0.43 2.04E+0l 1.54E+0l 1.54E+0l + Y-88 898. 04 93.70 2.48E-02 6.81E-02 6.81E-02 1836.06 99.20 3.23E-02 7.34E-02 + NB-94 702.63 100.00 6.95E-03 5.BSE-02 5.90E-02 871.10 100.00 -3.83E-02 5.BSE-02 + I-131 284.30 6.06 5.47E-0l 9,38E-02 1. 30E+00 364.48 81.20 -2.77E-02 9.38E-02 636 . 97 7.27 -1. 95E-02 1.22E+00 + CS-134 604.70 97.60 7.59E-03 7,14E-02 8.31E-02 795.84 85.40 -8.20E-02 7.14E-02
9/17/2019 3:20:28PM Page6 of6 Analysis Report for L2-011-104-FSPA-008-AV L2-011-104 Nuclide Energy Yield(%) Activity NuclldeMDA UneMDA Name (pCVgrams) (pCVgrams) (pCVgrams) (keV) + CS-137 661.65 85.12 3.76E-02 8.46E-02 8.46E-02 + CE-144 80.12 1.36 8.SOE-01 3.95E-Ol 5.00E+OO 133.51 11.09 -1.23E-Ol 3.95E-01 + EU-152 121.78 28.40 -1.32E-01 1.50E-01 1. 50E-01 344.28 26.60 -1.65E-02 2.00E-01 1408.00 20.74 1.05E-01 3.16E-Ol + EU-154 123.07 40.40 -7.16E-02 1.05E-01 1.0SE-01 723.30 19.70 -1.65E-01 3.26E-Ol 1274.51 35.50 -1.97E-02 2.43E-01 + EU-155 86.54 32.80 -l.30E-01 1.77E-Ol 1.77E-01 105.31 21. 80 1.65E-01 2.llE-01 + BI-214 609.31
- 46.30 1.60E-01 1.30E-01 1.30E-01 1120.29 15.10 2.82E-01 6.04E-Ol 1238.11 5.94 6.03E-01 1.83E+OO 1377.67 4.11 3.57E-02 1. 68E+00 1407.98 2.48 8.75E-Ol 2.64E+OO 1509.19 2.19 -4.SOE-01 2.53E+OO 1764.49 15.80 2.98E-01 4.46E-01
+ PB-214 77.11 10.70 3.00E-01 1.45E-01 6.71E-Ol 295.21
- 19.20 1. 76E-01 1.52E-01 351.92
- 37.20 1. 21E-01 1.45E-01
+ PA-228 89.95 22.00 9.27E+OO 7.91E+OO 1. 36E+Ol 93.35 35.00 -l.03E+OO 7.91E+OO 105.00 16.30 4.41E+OO 1. 48E+Ol 129.22 2.97 6.13E+Ol 7.80E+Ol 338.32 5.30 -1.0lE+Ol 4.88E+Ol 463.00 13.80 2.llE+Ol 2.16E+Ol 911.23 16.70 l.38E+01 2.35E+Ol + AM-241 59.54 36~30 -7.SOE-02 3.24E-01 3.24E-Ol + CM-243 103.76 23.00 8.72E-02 2.00E-01 2.00E-01 228.18 10.60 2.79E-02 4.29E-01 277.60 14.00 .l.37E-01 3.68E-01
+ = Nuclide identified during the nuclide identification * = Energy line found in the spectrum > = MCA value not calculated @ = Half-life too short to be able to perform the decay correction ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
9/18/2019 6:55:02AM Page 1 ofS JApex-Gamma Analysis Report for L2-011-104-FSPA-009-AV l2-011-104 GAMMA SPECTRUM ANALYSIS Sample Identification : L2-011-104-FSPA-009-AV Sample Description : L2-011-104 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.330E+02 grams Facility : Dairyland_NPP Sample Taken On : 9/12/2019 8:40:00AM Acquisition Started : 9/18/2019 6:24:43AM Procedure : 500ml Marinelli Operator : Administrator DeCector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real lime : 1805.6 seconds Deadllme : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 7/8/2014 Efficiency CalibratlOl'l Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7466 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 9/18/2019 6:54:53AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/18/2019 6:55:02AM Page2of5 Analysis Report for L2-011-104-FSPA-009-AV L2-011-104 Pealr Energy ROI ROI Pealr NetPeak NetArea Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts {lceV) F 1 76.76 147 - 158 154.07 5.70E+Ol 28.94 5.02E+02 1.41 F 2 238.59 474 - 485 477.65 9.31E+Ol 24.82 1.95E+02 1.25 F 3 338.07 672 - 684 676.58 3.SlE+Ol 16.55 l.OOE+02 1. 53 F 4 351.71 697 - 710 703.86 9.24E+Ol 23.35 l.23E+02 1. 73 F 5 582.90 1160 - 1171 1166 .15 4.27E+Ol 15.92 4.46E+Ol 1. 96 F 6 *1460.37 2914 - 2927 2920. 84 2.13E+02 29.99 1. 72E+Ol 2.39 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/18/2019 B:54:53AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Baclcgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76. 76 5.70E+Ol 28.94 5.70E+Ol 2.89E+Ol F 2 238.59 9.31E+Ol 24.82 9.31E+Ol 2.48E+Ol F 3 338.07 3.51E+Ol 16.55 3.SlE+Ol 1. 66E+Ol F 4 351.71 9.24E+Ol 23.35 4.18E+Ol 1.86E+Ol 5.06E+Ol 2.99E+Ol F 5 582.90 4.27E+Ol 15.92 4.27E+Ol . 1. 59E+Ol F 6 1460.37 2.13E+02 29.99 2.82E+Ol 8.57E+OO 1.85E+02 3.12E+Ol M = First peak in a multiplet region
=
m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
9/18/2019 6:S5:02AM Page 3 of5 Analysis Report for L2-011-104-FSPA-009-AV L2-011-104 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llhrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV} (pCVgrams) Uncettalnty K-40 0.97 1460.75
- 10.67 5.SlE+OO 9.76E-Ol PB-212 0.99 77.11
- 17.50 2.21E-Ol 1.13E-01 238.63
- 44.60 1.31E-Ol 3.56E-02 PB-214 0 .52 77.11
- 10.70 3.61E-01 1.BSE-01 295.21 19.20 351.92
- 37.20 1.19E-01 7 .06E-02
* = Energy line found in the spectrum.
- = Manually added nucllde.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Talerance : 1.000 keV Nuclide confidence Index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams}
K-40 0.977 5.51E+OO 9.76E-01 PB-212 0.994 1.32E-Ol 3.41E-02 PB-214 0.520 1.23E-01 6.63E-02
? = nuclide Is part of an undetermined solution X = nuclide rejected by the Interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000slgma
9/18/2019 6:55;02AM Page4of5 Analysis Report for L2-011-104-FSPA-009-AV L2-011-104 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 9/18/2019 6:54:53AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 3 338.07 l.95157E-02 23.56 Tol . AC-228 PA-228 F 5 582.90 2.37123E-02 18.65 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dalryland_NPp\Library\HOTLAB.NLB Nuclide Enerr,y Y,eld(%} Activity Nuclide IIOA UneMDA Name (pCUgrams} (pCUgrams} (pCVgrams) (keVJ + K-40 1460.75
- 10.67 5.SlE+00 8.99E-01 8.99E-0l
+ @ AR-41 1293. 64 99.16 1. 00E+26 1. 00E+26 1. 00E+26 + CO-60 1173.22 100.00 3.04E-02 7.76E-02 9.61E-02 1332.49 100.00 3.30E-02 7.76E-02 + KR-85 513.99 0.43 2.27E+0l 1.54E+0l 1.54E+01 + Y-88 898.04 93.70 -l.lSE-02 5.67E-02 6.94E-02 1836.06 99.20 -5.83E-02 5.67E-02 + NB-94 702.63 100.00 4.SBE-03 5.62E-02 5.62E-02 871.10 100.00 -5.96E-02 7.17E-02 + I-131 284.30 6.06 3.43E-01 9.48E-02 1. 34E+00 364.48 81.20 -4.18E-02 9.48E-02 636.97 7.27 -2.46E-01 l.38E+00 + CS-134 604.70 97.60 5.97E-02 6.67E-02 6.67E-02 795.84 85.40 7.46E-02 8.20E-02
9/1812019 6:55:02AM PageS ofS Analysis Report for L2-011-104-FSPA-009-AV L2-011-104 Nuclide En81J1y Yield(%) Activity NuclldeMDA LinelfDA Name (keV) (pCVgrams) (pCVgrams) (pCVgrams) + CS-137 661. 65 85.12 6.SOE-02 8.64E-02 8.64E-02 + CE-144 80.12 1.36 -2.32E+OO 4.16E-01 5.21E+OO 133.51 11.09 2.67E-02 4.16E-Ol + EU-152 121. 78 28.40 6.SOE-02 1.57E-01 1. 57E-01 344.28 26.60 -6.60E-02 2.04E-01 1408.00 20.74 -9.20E-02 2 .69E-01 + EU-154 123.07 40.40 -l.89E-04 1. llE-01 l. llE-01 723. 30 19.70 5.SSE-03 2.96E-Ol 1274.51 35.50 6.96E-02 2.50E-Ol + EU-155 86.54 32.80 -6.96E-02 1. 7 6E-01 1.76E-Ol 105.31 21.80 -6.32E-03 2.lOE-01 + BI-214 609.31 46.30 8.22E-02 1.45E-Ol 1.45E-Ol 1120.29 15.10 4.00E-01 6.SlE-01 1238.11 5.94 9.36E-01 1. 72E+OO 1377.67 4.11 6.79E-01 1. 69E+OO 1407.98 2.48 -7.69E-01 2.25E+OO 1509.19 2.19 -9 . 45E-0l 2.36E+OO 1764.49 15.80 4.23E-01 5.28E-01 + PB-214 77.11
- 10.70 3.61E-Ol 1. 40E-01 5.40E-01 295.21 19.20 2.61E-Ol 2.82E-Ol 351. 92
- 37.20 1.19E-01 l.40E-Ol
+ PA-228 89.95 22.00 2.12E+Ol 1. 28E+Ol 2.23E+Ol 93.35 35.00 -3.79E+OO l.28E+Ol 105.00 16.30 4.39E+OO 2.47E+Ol 129.22 2.97 -2.03E+Ol 1.33E+02 338.32 5. 30 4.75E+Ol 8.59E+Ol 463.00 13.80 4.48E+Ol 3.71E+Ol 911.23 16. 70 7.37E+OO 3.77E+Ol + AM-241 59.54 36.30 -7.02E-02 3.25E-Ol 3.25E-Ol + CM-243 103.76 23.00 2.32E-02 2.00E-01 2.00E-01 228.18 10.60 -1. 31E-01 3.BBE-01 277 . 60 14.00 1. 92E-Ol 3.56E-01
. ==Nuclide + Identified during the nuclide Identification Energy line found in the spectrum > = MDA value not calculated @ = Half-life too short to be able to perform the decay correction ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
9/12/2019 9:24:52AM Page 1 of7
*.tApex-Gamma Analysis Report for l2-01M04-FSGS-010-SS L2-011-104 GAMMA SPECTRUM ANALYSIS Sample Identification ~ L2-011-104-FSGS-010-SS Sample Description : L2-011-104 Sample Type : 500 ml Mannelli Unit Sample Point Sample Size : 7.685E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/9/2019 2:46:00PM Acquisition Started : 9/12/2019 8:54:33AM Procedure : 500ml Marinelli Operator : Administrator Detector Name :HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.9 seconds Dead Time : 0.32 %
Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy CaUbration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7448 PEAK ANALYSIS REPORT Peak Analysis Performed on : 9/12/2019 9:24:43AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/12/2019 9:24:52AM Page2of7 Analysis Report for L2-011-104-FSGS-010-SS L2-011-104 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 77.03 147 - 161 154.61 1.94E+02 44.37 9.78E+02 1. 74 F 2 185.87 367 - 379 372.24 1.36E+02 36.12 4.96E+02 1. 87 M 3 238.54 474 - 489 477.55 2 . 77E+02 39.72 2.41E+02 1. 41 m 4 241.78 474 - 489 484.04 1.07E+02 26. 62 2.56E+02 1.42 M 5 270.71 536 - 563 541. 89 3.55E+Ol 20.22 1. 96E+02 1.11 m 6 277.60 536- 563 555.. 66 2.75E+Ol 16.90 1. 58E+02 1.12 F 7 295.19 586 - 597 590.82 1 . 90E+02 33.53 3.02E+02 1.31 F 8 338.35 672 - 685 677.13 6.lBE+Ol 21. 60 2.19E+02 1.32 F 9 351. 7 5 698 - 712 703.93 3.05E+02 38.49 2.19E+02 1.50 F 10 462.67 920 - 932 925.72 2.51E+Ol 15.14 1.09E+02 1.42 F 11 583.04 1160 - 1171 1166.42 7.89E+Ol 20.57 7.lSE+Ol 1. 62 F 12 609.19 1212 - 1226 1218.72 2.63E+02 33.92 6.68E+Ol 1. 75 F 13 726.81 1449 - 1458 1453.91 2.39E+Ol 13.28 4.00E+Ol 1. 68 F 14 911.00 1817 - 1829 1822.23 6.07E+Ol 18 . 56 4.54E+01 2.47 F 15 968.96 1934 - 1943 1938.14 2.89E+01 13.35 3 . 43E+01 1.53 F 16 1120.19 2234 - 2246 2240.57 5 .96E+Ol 17.87 4.21E+Ol 2.14 F 17 1377.00 2750 - 2759 2754.14 1. 45E+01 8.66 1.25E+01 1.14 F 18 1460.68 2914 - 2928 2921.47 2.0BE+02 29 . 74 2.62E+Ol 2.23 F 19 1764.34 3523 - 3536 3528.75 3 .96E+Ol 12.99 2.83E+OO 3.16 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 9/12/2019 9:24:43AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orlg.AIH Ambient Backgr. Subtracted Subtracted No. (keVJ Area Uncertainty Background Uncert. Area Uncert. F 1 77.03 l .94E+02 44.37 1 . 94E+02 4.44E+Ol F 2 185.87 1.36E+02 36 . 12 1.36E+02 3.61E+Ol M 3 238.54 2.77E+02 39.72 2.77E+02 3.97E+Ol m 4 241. 78 1.07E+02 26.62 l.07E+02 2.66E+O l M 5 270.71 3.55E+Ol 20.22 3.SSE+Ol 2.02E+Ol m 6 277.60 2.75E+Ol 16.90 2 . 75E+Ol 1. 69E+Ol F 7 295.19 1.90E+02 33.53 l.90E+02 3.35E+Ol F 8 338.35 6.lBE+Ol 21.60 6 . 18E+Ol 2.16E+Ol F 9 351.75 3.05E+02 38.49 4.18E+Ol 1.86E+Ol 2.63E+02 4.27E+Ol F 10 462.67 2.51E+Ol 15.14 2.SlE+Ol 1.51E+Ol
9/12/2019 9:24:52AM Page3 of7 Analysis Report for L2-011-104-FSGS-010-SS L2-011-104 Peak Energy Original Orig.Ates Ambient Baclcgr. Subtracted Subtracted No. (ks\? Area Uncertainty Background Uncert. Area Uncert. F 11 583.04 7.89E+Ol 20.57 7.89E+Ol 2.06E+Ol F 12 609.19 2.63E+02 33.92 2.06E+Ol l.21E+Ol 2.42E+02 3.60E+Dl F 13 726.81 2.39E+Dl 13.28 2.39E+Ol l.33E+Ol F 14 911.00 6.07E+Ol 18.56 6.07E+Ol 1. 86E+Ol F 15 968.96 2.89E+Ol 13.35 2.89E+Ol 1.33E+Ol F 16 1120.19 5.96E+Ol 17.87 5.96E+Ol 1.79E+Ol F 17 1377.00 1.45E+Ol 8.66 1. 45E+Ol 8.66E+OO F 18 1460. 68 2.08E+02 29. 74 2.82E+Ol 8.57E+OO 1. 80E+02 3.09E+Ol F 19 1764.34 3.96E+Ol 12.99 7.59E+OO 4.90E+OO 3.20E+Ol 1. 39E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Enors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTI.AB.NLB i* IDENTIFIED NUCLIDES Nuclide Id Energy Yleltl(D"') Activity Activity Name Contfdence (keV) (pCUgrams) Uncertainty K-40 0.99 1460.75
- 10.67 5.llE+OO 9.22E-01 BI-212 0.59 727.17
- 11.80 3.30E-01 1.84E-01 785.42 2.00 1620.56 2.75 PB-212 0.99 77.11
- 17.50 7.12E-Ol 1.69E-01 238.63
- 44.60 3~72E-Ol 5.67E-02 BI-214 0.84 609.31
- 46.30 7._25E-Oi 1.lSE-01 1120.29
- 15.10 9.48E-01 2.88E-01 1238.11 5. 94 1377.67
- 4.11 1.02E+OO 6.08E-01 1407.98 2.48 1509.19 2.19 1764.49
- 15.80 7.19E-01 3.lSE-01 PB-214 0.99 77. 11
- 10.70 1. 16E+OO 2.77E-Ol 295.21
- 19.20 7.06E-Ol 1.29E-01 351.92
- 37.20 5.92E-Ol 1.00E-01 RA-226 0.98 186.21
- 3.28 2.0BE+OO 5.66E-Ol AC-228 0.60 209.28 4.40 338.32
- 11.40 4.38E-01 l.54E-01 794.70 4.60
9/12/2019 9:24:52AM Page4of7 Analysis Report for L2-011-104-FSGS-010-SS L2-011-104 Nuclide Id Energy Yleld{°/4) Activity Activity Name Confidence (keV) (pCUgrams) Uncertainty AC-228 0.60 911.60
- 27.70 4.38E-01 1.35E-01 964.60 5.20 969.11
- 16.60 3.68E-01 1. 71E-01
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)
K-40 0.999 5.llE+OO 9.22E-01 BI-212 0.590 3.30E-01 1. 84E-01 PB-212 0.999 3.67E-Ol 5.39E~02 BI-214 0.841 7.59E-Ol 9.99E-02 PB-214 0.997 6. 29E-Ol 7.6SE-02 RA-226 0.982 2.08E+OO 5.66E-Ol AC-228 0.609 4.20E-01 8.74E-02
? = nuclide is part of an undetermined solution X = nuclide rejected by the Interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
9/12/2019 9:24:52AM Page5of7 Analysis Report for L2-011-104-FSGS-010-SS L2-011-104 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/1212019 9:24:43AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 4 241.78 5. 91922E-02 12.49 M 5 270.71 1. 97312E-02 28.46 m 6 277.60 1.52892E-02 30.71 CM-243 F 10 462. 67 1.39601E-02 30.13 PA-228 F 11 583.04 4.38190E-02 13.04 M = First peak In a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LlneMDA Name (lreV) (pCVgrams) (pCVgrams) (pCVgrams) + K-40 1460.75
- 10.67 5 .llE+00 9,33E-0l 9.33E-01
+ AR-41 1293.64 99.16 -1 . 49E+09 8.26E+09 8.26E+09 + CO-60 1173.22 100.00 9.27E-02 9.96E-02 l.07E-01 1332.49 100.00 8 . 45E-02 9.96E-02 + KR-85 513.99 0.43 2 , 76E+00 l.76E+01 1. 76E+0l + Y-88 898.04 93.70 2.00E-02 8.64E-02 8.68E-02 1836.06 99.20 -5 . 54E-03 8.64E-02
9/12/2019 9:24:52AM Page 6 of7 Analysis Report for L2-011-104-FSGS-01~SS L2-011-104 Nuclide En&IJIY Yield(%) Activity NuclldeMDA LlneMDA Name (lceV) (pCVgrams) (pCUgrams) (pCVgrams) + NB-94 702.63 100.00 -1. 49E-02 7.26E-02 7.71E-02 871.10 100.00 -2.67E-02 7.26E-02 + I-131 284.30 6.06 2.09E-01 8.65E-02 1.23E+OO 364.48 81.20 -7.34E-02 8.65E-02 636.97 7.27 -3 .36E-Ol 1. lOE+OO + CS-134 604.70 97.60 -2.31E-02 8.82E-02 1.25E-01 795.84 85.40 -6.58E-02 8.82E-02 + CS-137 661. 65 85.12 6.79E-02 9.62E-02 9.62E-02 + CE-144 80.12 1.36 -1.78E+OO 4.87E-01 6.71E+OO 133.51 11.09 -1. 67E-01 4.87E-01 + EU-152 121.78 28.40 8.63E-02 l.97E-Ol l.97E-01 344.28 26.60 -5.19E-02 2.65E-Ol 1408.00 20.74 2.04E-01 4.70E-Ol + EU-154 123.07 40.40 1. 89E-03 l.38E-01 1.38E-Ol 723.30 19.70 -7.78E-02 4.lOE-01 1274.51 35.50 -6.83E-02 2.60E-01 + EU-155 86.54 32.80 -1. 92E-01 2.26E-Ol 2.26E-Ol 105.31 21.80 5.59E-02 2.60E-Ol + BI-214 609.31
- 46.30 7.25E-01 1. 30E-01 l.30E-01 1120. 29
- 15.10 9.48E-Ol 4.32E-Ol 1238.11 5.94 1. 37E+OO 2.llE+OO 1377.67
- 4.11 1.02E+OO 1.05E+OO 1407.98 2.48 1. 70E+OO 3.93E+OO 1509.19 2.19 -2.68E-01 3.62E+OO 1764.49
- 15.80 7.19E-01 3.66E-01
+ PB-214 77.11
- 10.70 l.16E+OO 1.63E-Ol 7.58E-01 295.21
- 19.20 7.06E-Ol 2.53E-01 351.92
- 37.20 5.92E-Ol 1.63E-01
+ PA-228 89.95 22.00 3.04E+OO l.58E+OO 2.71E+OO 93.35 35.00 1. 09E+OO 1. 58E+OO 105.00 16.30 1.81E+OO 2.83E+OO 129.22 2.97 5.07E+OO 1.SOE+Ol 338.32 5.3 0 3.99E+OO 1.02E+Ol 463.00 13.80 -l.58E+OO 3.72E+OO 911. 23 16.70 5.00E+OO 5.24E+OO + AM-241 59.54 36.30 1.BlE-02 3.99E-Ol 3.99E-Ol + CM-243 103.76 23.00 -9.98E-03 2.46E-01 2.46E-01 228.18 10.60 -2,57E-02 5.lOE-01 277.60 14.00 -1.88E-02 4.36E-Ol
+ = Nuclide identified during the nuelide identification * = Energy line found in the spectrum > = MDA value not calculated @ = Half-life too short to be able to perform the decay correction ? : CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
9/12/2019 9:24:52AM Page7 of7 Analysis Report for L2-011-104-FSGS-010-SS L2-011-104
9112/2019 10:01:39AM Page 1 of6
~pex-Gamma Analysis Report for L2-011-104-FSGS-011-SS L2-011-104 GAMMA SPECTRUM ANALYSIS Sample Identification : l2-011-104-FSGS-011-SS Sample Description : l2-011-104 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.697E+02 grams Facility : Dairyland_NPP Sample Taken On : 9/912019 2:52:00PM Acquisition Started : 9/12/2019 9:31:16AM Procedure : 500ml Marinelli Operator * : Administrator .
Detector Name :HOTLAB Geometry : 500ml Marinelli Live Time : 1800.0 seconds Real Time : 1805.6 seconds Dead lime : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in chsnn*) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7449 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 9/12/2019 10:01;30AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/12/2019 10:01:39AM Pagc2of6 Analysis Report for L2-011-104-FSGS-011-SS L2-011-104 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 77.02 147 - 158 154.59 8.23E+Ol 27.59 4.91E+02 0.94 F 2 238.51 469 - 485 477.49 2.03E+02 34.68 2.85E+02 2.13 F 3 295.29 585 - 595 591.03 6.60E+Ol 23.57 1.78E+02 1.70 F 4 351.72 696 - 710 703.86 1.04E+02 25.98 1. 84E+02 1.84 F 5 582.86 1163 - 1170 1166.06 2.92E+Ol 14.77 5.90E+Ol 1.33 F 6 609.09 1213- 1223 1218.51 7.83E+Ol 20.41 5.7BE+Ol 1. 66 F 7 727.23 1450 - 1459 1454.76 1.SOE+Ol 10.17 2.96E+Ol 1.26 F 8 910.72 1815 - 1826 1821.69 2.47E+Ol 13.29 3.85E+Ol 1. 96 F 9 968.94 1934 - 1943 1938.10 1.31E+01 9.96 3.0BE+Ol 1.41 F 10 1460.53 2912 - 2929 2921.17 2.13E+02 29.77 l.80E+Ol 2.54 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 9/12/2019 10:01:30AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 77.02 8.23E+Ol 27.59 8.23E+Ol 2.76E+Ol F 2 238.51 2.03E+02 34.68 2.03E+02 3.47E+Ol F 3 295.29 6.60E+Ol 23.57 6 . 60E+Ol 2.36E+Ol F 4 351.72 1.04E+02 25.98 4.18E+Ol 1.86E+01 6.22E+01 3.20E+Ol F 5 582.86 2.92E+Ol 14.77 2.92E+01 1. 48E+Ol F 6 609.09 7.83E+01 20.41 2.06E+Ol 1.21E+Ol 5.78E+Ol 2.37E+Ol F 7 727.23 1.50E+Ol 10 .17 1.SOE+Ol 1. 02E+Ol F 8 910.72 2.47E+Ol 13.29 2.47E+Ol 1. 33E+Ol F 9 968.94 1. 31E+01 9.96 1. 31E+Ol 9.96E+OO F 10 1460.53 2.13E+02 29.77 2.82E+Ol 8.57E+OO l.85E+02 3.lOE+Ol
=
M First peak In a multiplet region
=
m other peak in a multiplet region
=
F Fitted singlet Errors quoted at 2.000sigma
9/12/2019 10:01 :39AM Pa.ge3 of6 Analysis Report for L2-011-104-FSGS-011-SS L2-011-104 NUCLIDE IDENTIFICATION REPORT Nucllde Library Used : C:\Canberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nudlde Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCVgrams) Uncertainty K-40 0.99 1460.75
- 10.67 4.63E+OO 8.17E-Ol BI-c212 0.60 727.17
- 11.80 1.83E-01 1.25E-01 785.42 2.00 1620.56 2.75 PB-212 0.99 77 .11
- 17.50 2.67E-Ol 9.12E-02 238.63
- 44.60 2.41E-Ol 4.30E-02 BI-214 0.34 609.31
- 46.30 1.53E-01 6.34E-02 1120.29 15.10 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.99 77 .11
- 10.70 4.36E-01 1. 49E-01 295.21
- 19.20 2.17E-Ol 7.83E-02 351.92
- 37.20 1.24E-01 6.38E-02
* =Energy line found in the spectrum.
- =Manually added nuclide.
? =Manually edited nuclide.
@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
9/12/2019 10:01 :39AM Page4 of6 Analysis Report for L2-011-104-FSGS-011-SS L2-011-104 Nuclide Nuclide Wtmean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams) K-40 0.992 4.63E+OO 8.17E-01 BI-212 0.605 1. 83E:..01 1. 25E-01 PB-212 0.998 2.29E-01 3.92E-02 BI-214 0.346 1.53E-Ol 6.34E-02 PB-214 0.996 1.SlE-01 4.73E-02
? = nuclide is part of an undetennined solution X = nucllde rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
9/12/2019 10:01 :39AM Pages of6 Analysis Report for L2-011-104-FSGS-011-SS L.2-011-104 UNIDENTIFIED PEAKS Peak Locate Performed on : 9/12/2019 10:01 :30AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(") Peak Tolerance Peak No. Energy (lceV) Peak Size (CPS) Uncertainty Type Nuclide F 5 582.86 l.62378E-02 25.26 F 8 910.72 1.37201E-02 26. 90 Tol. AC-228 PA-228 F 9 968.94 7.27580E-03 38.04 Tol . AC-228 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Ubrary Used : C:\Canbena\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Yield(") Activity NuclldeMDA LlneMDA Name (lreV) (pCl/grams) (pCl/grams) (pCVgrams) + K-40 1460.75
- 10.67 4.63E+OO 7.86E-Ol 7.86E-01
+ AR-41 1293.64 99.16 -2.86E+09 7.43E+09 7.43E+09 + C0-60 1173.22 100.00 5.76E-02 7.18E-02 9.09E-02 1332.49 100.00 -6.22E-03 7.18E-02 + KR-85 513.99 0.43 4.0SE+OO l.42E+Ol 1.42E+Ol + Y-88 898.04 93.70 2.64E-02 4.68E-02 6.93E-02 1836.06 99.20 -6.93E-02 4.68E-02 + NB-94 702.63 100.00 -2.83E-02 5.15E-02 5.lSE-02 871.10 100.00 -3.68E-02 5.93E-02 + I-131 284.30 6.06 -1. 4 GE-01 7.22E-02 9.08E-Ol 364.48 81.20 -1.80E-03 7.22E-02 636.97 7.27 -5.79E-01 9.49E-Ol
9/12/2019 10:01:39AM Page6of6 Analysis Report for L2-011-104-FSGS-0 11-SS L2-011-104 Nuclide Enerr,y Yield(%) Activity NuclldeMDA LlneMDA Name (keV) (pCVgrams) (pCVgrams) (pCVgrams) + CS-134 604.70 97.60 9.50E-02 7.44E-02 7.49E-02 795.84 85.40 -8.54E-03 7.44E-02 + CS-137 661.65 85.12 9.98E-02 8,41E-02 8.41E-02 + CE-144 80.12 1.36 -2.63E+OO 3.74E-Ol 4.75E+00 133.51 11.09 -2.23E-01 3.74E-Ol + EU-152 121.78 28.40 -1. 04E-01 1.42E-Ol 1. 42E-01 344.28 26.60 2.59E-02 1.89E-01 1408.00 20.74 2.67E-Ol 3.36E-01 + EU-154 123.07 40.40 -7.23E-02 9.94E-02 9.94E-02 723.30 19.70 1. 71E-01 3.0lE-01 1274.51 35.50 6.70E-03 2.lSE-01 + EU-155 86.54 32.80 -1. 63E-02 1. 65E-Ol 1. 65E-01 105.31 21. 80 1. 48E-01 2.03E-Ol + BI-214 609.31
- 46.30 1. 53E-01 1. 05E-Ol 1. OSE-01 1120.29 15.10 S.35E-02 6.30E-01 1238.11 5.94 3.19E-01 1.64E+OO 1377. 67 4.11 4.99E-Ol 1.52E+OO 1407.98 2.48 2.23E+OO 2.81E+OO 1509.19 2.19 7.0lE-01 2.82E+OO 1764.49 15.80 4.56E-01 4.96E-01
+ PB-214 77 .11
- 10.70 4.36E-Ol 1. 35E-Ol 4.48E-Ol 295.21
- 19.20 2.17E-01 1.67E-01 351. 92
- 37.20 l.24E-01 1. 35E-Ol
+ PA-228 89.95 22.00 1.82E+OO 1.14E+OO 1. 97E+OO 93.35 35.00 1.23E-01 l.14E+OO 105.00 16.30 6.SOE-01 2.23E+OO 129.22 2.97 S.84E+OO 1.lSE+Ol 338.32 5.30 -1.llE+OO 7.42E+OO 463.00 13.80 '.f:.39E+OO 3.06E+OO 911. 23 16.70 1. 34E+OO 3.97E+OO + AM-241 59.54 36.30 2.62E-02 3.04E-01 3.04E-01 + CM-243 103.76 23.00 8.22E-02 1.93E-01 1.93E-Ol 228.18 10.60 2.llE-03 3.88E-01 277.60 14.00 9.61E""'.'02 3.llE-01
+ = Nuclide identified during the nuclide identification * = Energy line found in the spectrum > = MCA value not calculated @ = Half-life too short to be able to perfonn the decay correction ? = CAUTION: MCA value is inconsistent with Currie MCA at 95% confidence level
9118/2019 8:10:19AM Page 1 of6 Analysis Report for L2-011-104-FSPA-012-AV L2-011-104 GAMMA SPECTRUMANALYSIS Sample Identification : L2-011-104-FSPA-012-AV Sample Description : L2-011-104 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 7.929E+02 grams Facility : Dalryland_NPP Sample Taken On : 9/12/2019 8:11:00AM Acquisition Started : 9118/2019 7:40:01AM Procedure : 500ml Marinelli Operator : Administrator DetectorName : HOTLAB Geometry : 500ml Marinelli Llvellme : 1800.0 seconds Real llme : 1805.5 seconds Deadllme : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 ldenUfication Energy Tolerance : 1.000 keV Energy CaHbration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7468 PEAK ANALYSIS REPORT Peak Analysis Perfonned on : 9118/2019 8:10:10AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/18/2019 8:10:19AM Pagc2 of6 Analysis Report for L2-011-104-FSPA-012-AV L2-011-104 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 238.67 474 - 481 477.81 7.34E+Ol 25.41 1. 89E+02 1.38 F 2 295.04 585 - 595 590.54 7.64E+01 22.43 1.35E+02 1.44 F 3 351.77 698 - 712 703.98 1. 20E+02 25.78 l.68E+02 1.51 F 4 609.15 1212 - 1225 1218.63 1.03E+02 21. 78 4.56E+Ol 1. 75 F 5 1120. 27 2235 - 2246 2240.72 2.44E+Ol 11. 75 1. 97E+Ol 2.05 F 6 1460.67 2913 - 2929 2921.45 l.67E+02 26.47 2.07E+Ol 2.26 M ::: First peak in a multiplet region m ::: Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/18/2019 8:10:10AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. An,a Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 238.67 7.34E+Ol 25.41 7.34E+Ol 2.54E+Ol F 2 295.04 7.64E+Ol 22.43 7.64E+Ol 2.24E+Ol F 3 351.77 l.20E+02 25.78 4.18E+Ol 1. 86E+Ol 7.80E+Ol 3.18E+Ol F 4 609.15 l.03E+02 21. 78 2.06E+Ol l.21E+Ol 8.27E+Ol 2.49E+Ol F 5 1120.27 2.44E+Ol 11.75 2.44E+Ol 1.18E+Ol F 6 1460.67 l.67E+02 26.47 2.82E+01 8.57E+OO l.39E+02 2.78E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
9118/2019 8:10:19AM Pagc3 of6 Analysis Report for L2-011-104-FSPM>12-AV L2-011-104 NUCLIDE IDENTIFICATION REPORT Nucllcle Library Used : C:\C~nberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yietdr/4) Activity Activity Name Conffdence (keV) (pCVgrama) Uncertainty K-40 0.99 1460. 75
- 10.67 3.82E+OO 7 .94E-01 PB-212 0.56 77.11 17.50 238.63
- 44.60 9.SSE-02 3.34E-02 BI-214 0.58 609.31
- 46.30 2.40E-01 7 .36E-02 1120.29
- 15.10 3.76E-01 1.82E-01 1238.11 5.94 1377.67 4.11 1407.98 2.48 1509.19 2.19 1764.49 15.80 PB-214 0.71 77.11 10.70 295.21
- 19.20 2.75E-Ol 8 .20E-02 351. 92
- 37.20 1 .70E-01 6.98E-02
* =Energy line found in the spectrum.
- =Manually added nuclide.
? =Manually edited nuclide.
@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nucllde Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams)
K-40 0.999 3.82E+OO 7.94E-Ol PB-212 0.560 9.SSE-02 3.34E-02 BI-214 0.583 2.59E-Ol 6.82E-02
9/18/2019 8:10:19AM Page4of6 Analysis Report for L2-011-104-FSPA-012-AV L2-011-104 Nuclide Nuclide . Wt mean wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams) PB-214 0.718 2.14E-01 5.31E-02
? = nuclide is part of an undetermined solution X = nuclide rejected by the Interference analysis
@ = nuclide contains energy llnes not used in Weighted Mean Activity Errors quoted at 2.000sigma
9/1812019 8:10:19AM PageSof6 Analysis Report for L2-011-104-FSPA-012-AV L2-011-104 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 9/18/2019 8:10:10AM Peak Locate From Channel : 100 Peak locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified. M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbena\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Ene,gy Yield(%) Acllvity NuclldeltlDA LinelfDA Name (pCVgrams) (pCVgrams) (pCl/grams) (keV) + K-40 1460.75
- 10.67 3.82E+00 8.77E-0l 8.77E-01
+ @ AR-41 1293.64 99.16 l.00E+26 1. 00E+26 1. 00E+26 + CO-60 1173.22 100.00 5.14E-02 6.24E-02 8.89E-02 1332.49 100.00 2.04E-02 6.24E-02 + KR-85 513.99 0.43 l.16E+0l 1.34E+0l 1. 34E+0l + Y-88 898.04 93.70 7.43E-03 5.SBE-02 7.96E-02 1836.06 99,20 2.60E-02 5.58E-02 + NB-94 702.63 100.00 1.79E-02 5.98E-02 5.98E-02 871.10 100.00 -1.26E-02 6.llE-02 + I-131 284.30 6.06 3.48E-01 9.77E-02 1.21E+00 364.48 81.20 -8.26E-03 9.77E-02 636. 97 7.27 1.94E-0l 1.24E+00 + CS-134 604.70 97.60 -1.SlE-02 7.45E-02 8.65E-02 795.84 85.40 -5.88E-02 7.45E-02 + CS-137 661.65 85.12 3.75E-02 8.lSE-02 8.lSE-02 + CE-144 80.12 1.36 5.23E-0l 3.BBE-01 4.88E+00 133.51 11.09 1.02E-0l 3.88E-01 + EU-152 121. 78 28.40 8.40E-02 1.55E-0l 1.55E-01
9/18/2019 8:10:19AM Page 6 of6 Analysis Report for L2-011-104-FSPA-012-AV L2-011-104 Nuclide Energy Yield(%} Activity Nuc/ldeMDA LlnaMDA Name (pCVr,rams) (pCUgrams) (pCVgrams) (keV} EU-152 344.28 26.60 2.98E-02 l.SSE-01 1. 91E-01 1408.00 20.74 5.58E-02 3.15E-Ol + EU-154 123.07 40.40 2.84E-02 l.08E-01 1. 08E-Ol 723.30 19.70 7.59E-02 3.07E-Ol 1274.51 35.50 4.53E-02 2.34E-01 + EU-155 86.54 32.80 1.33E-01 1.70E-01 1.70E-Ol 105.31 21.80 3.69E-02 2.04E-Ol + BI-214 609.31
- 46.30 2.40E-01 1.13E-01 1.13E-Ol 1120.29
- 15.10 3.76E-01 3.00E-01 1238.11 5.94 7.20E-02 1. 59E+OO 1377.67 4.11 l.03E+OO l.82E+OO 1407.98 2.48 4.66E-Ol 2.63E+OO 1509.19 2.19 1.29E+OO 2.85E+OO 1764 .49 15.80 3.26E-01 5.llE-01
+ PB-214 77.11 10.70 1. 45E-01 1. 46E-Ol 6.37E-Ol 295.21
- 19.20 2.75E-01 l.60E-Ol 351. 92
- 37.20 1. 70E-01 1. 46E-01
+ PA-228 89.95 22.00 1.36E+Ol 1. 28E+Ol 2.23E+Ol 93.35 35.00 -3.26E+OO 1.28E+Ol 105.00 16.30 2.72E+OO 2.52E+Ol 129.22 2.97 2.39E+Ol 1.34E+02 338.32 5.30 7.86E+01 9.llE+Ol 463.00 13.80 -9.18E+00 3.37E+Ol 911. 23 16. 70 1.92E+Ol 4.07E+Ol + AM-241 59.54 36.30 -9.74E-02 3.0SE-01 3.0SE-01 + CM-243 103.76 23.00 -4.48E-03 1. 93E-Ol 1.93E-Ol 228.18 10.60 -5. 0SE-02 4.17E-01 277.60 14.00 -1. 57E-01 3.09E-01
+ = Nuclide identified during the nuclide identification * = Energy line found in the spectrum > = MDA value not calculated @ = Half-life tao short to be able to perform the decay correction ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
9/18/2019 9:12:21AM Page l of6 JApex-Gamma Analysis Report for L2-011-104-FSPA-013-AV L2-011-104 GAMMA SPECTRUM ANALYSIS Sample Identification : L2-011-104-FSPA-D13--AV Sample Description : L2-011-104 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size : 8.348E+02 grams Facility : Dairyland_NPP Sample Taken On ; 9/12/2019 7:49:00AM Acquisition Started : 9/18/2019 8:42:03AM Procedure : 500ml Marinelli Operator : Administrator DetectorName :HOTLAB Geometry : 500ml Marinelli Live lime : 1800.0 seconds Real lime : 1805.5 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096
- Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8J2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency CaHbratlon Description Sample Number : 7470 PEAK ANALYSIS REPORT Peak Analysis Performed on : 9/18/2019 9:12:12AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/18/2019 9:12:21AM Pagc2of6 Analysis Report for L2-011-104-FSPA-013-AV L2-011-104 Peal< Energy ROI ROI Peak Net Peak NetArea Continuum FWHM No. (keV) start end Centroid Araa Uncertainty Counts (keV) F 1 185.82 368 - 379 372.13 3.92E+01 22.16 3.36E+02 1.11 M 2 238.52 472 - 490 477.51 9.67E+Ol 25.12 1. 87E+02 1.55 m 3 241. 75 472 - 490 483.98 5.37E+Ol 20.10 1. 51E+02 1.56 F 4 295.00 586- 594 590.45 6.13E+Ol 22.24 1. 40E+02 1.46 F 5 351.88 699 - 709 704.19 9.78E+Ol 23.72 1.02E+02 1.54 F 6 583.02 1161 - 1171 1166.39 3.68E+Ol 13.83 3.21E+Ol 1.37 F 7 609.19 1212 - 1226 1218.71 7.50E+Ol 19.21 3.82E+Ol 2.06 F B 1460.39 2 914 - 2929 2920.89 1. 73E+02* 27.10 1.94E+Ol 2.42 F 9 1763.86 3523 - 3533 3527.78 1.85E+Ol 9.37 5.SOE+OO 2.02 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/18/2019 9:12:12AM Env. Background FIie : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area . Uncert. F 1 185.82 3.92E+Ol 22.16 3.92E+Ol 2.22E+Ol M 2 238.52 9.67E+Ol 25.12 9.67E+Ol 2.51E+Ol m 3 241. 75 5.37E+Ol 20.10 5.37E+Ol 2.0lE+Ol F 4 295.00 6.13E+Ol 22.24 6.13E+Ol 2.22E+Ol F 5 351.88 9.78E+Ol 23.72 4.18E+Ol 1. 86E+Ol 5.60E+Ol 3.0lE+Ol F 6 583.02 3.68E+Ol 13.83 3.68E+Ol 1. 38E+Ol F 7 609.19 7.SOE+Ol 19.21 2.06E+Ol 1. 21E+Ol 5.44E+Ol 2.27E+Ol F 8 1460.39 1. 73E+02 27.10 2.82E+Ol 8.57E+OO 1.45E+02 2.84E+Ol F 9 1763.86 l.85E+Ol 9.37 7.59E+OO 4.90E+OO l.09E+Ol l.06E+Ol M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
9/18/2019 9:12:21AM Pagc3 of6 Analysis Report for L2-011-104-FSPA-013-AV L2-011-104 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canbana\Apex\Root\Dalryland_NPP\l.lbrary\HOTlAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Acthtlty Activity Name Conlfdence (keV) (pCVgrams) Uncertainty K-40 0 .97 1460.75
- 10.67 3.78E+OO 7.71E-Ol PB-212 0 .55 77 .11 17.50 238.63
- 44.60 1.19E-01 3.16E-02 EI-2 14 0.54 609.31
- 46.30 1.SOE-01 6.32E-02 1120.29 15.10 1238.11 5. 94 1377.67 4.11 1407.98 2.48 1509 .1 9 2.19 1764.49
- 15.80 2.26E-Ol 2.19E-Ol PB-214 0.71 77. 11 10.70 295.21
- 19.20 2.lOE-01 7.69E-02 351.92
- 37.20 1.16E-01 6.27E-02 RA-226 0.97 186.21
- 3.28 5.54E-01 3.14E-01
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy llne not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Act/Vlty Confidence Uncertainty (pCilgrams)
K-40 0.979 3 . 78E+OO 7. 71E-Ol PB-212 0 . 559 1.19E-Ol 3 . 16E-02
9/18/2019 9:12:21AM Page 4 of6 Analysis Report for L2-011-104-FSPA-013-AV L2-011-104 Nuclide Nuclide Wtmear, Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCUgrams) BI-214 0.540 1.56E-Ol 6.07E-02 PB-214 0.719
- i.53E-01 4.86E-02 RA-226 0.975 S.54E-01 3.14E-01
? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
9/18/2019 9:12:21AM PagcS of6 Analysis Report for L2-011-104-FSPA*013-AV L2-011-104 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 9/1812019 9:12:12AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS ("/4) Peak Tolerance Peak No. Energy (keV) Peak Sin (CPS) Uncertainty 'fype Nuclide m 3 241.75 2.98580E-02 18.70 F 6 583.02 2.04652E-02 18.77 M = First peak in a multiplet region m = Other peak in a multiplet region F "' Fitted singlet Enors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Csnberra\Apex\Root\Dalryland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Ylald(3/4J Activity Nuclide AIDA LlneMDA Name (keV) (pCUgrams) (pCUgrams) (pCUgrams) + K-40 1460.75
- 10.67 3.78E+00 8.l?E-01 8.17E-01
+ @ AR-41 1293.64 99.16 1.00E+26 l.00E+26 1. 0OE+26 + CO-60 1173.22 100.00 3.63E-02 6.70E-02 8.73E-02 1332.49 100.00 2.32E-02 6.70E-02 + KR-85 513.99 0.43 1.39E+0l 1. 34E+0l 1. 34E+0l + Y-88 898.04 93. 70 -1. lSE-02 7.llE-02 7.31E-02 1836.06 99.20 l.32E-02 7.llE-02 + NB-94 702.63 100.00 -3.27E-02 4.73E-02 4.73E-02 871.10 100.00 -2.84E-02 5.74E-02 + I-131 284.30 6. 06 4.16E-0l 9.46E-02 l.25E+00 364.48 81.20 -5.30E-03 9.46E-02 636.97 7.27 7 ,0lE-01 1. 2 6E+00 + CS-134 604.70 97.60 -1. 79E-02 6.96E-02 6.99E-02 795.84 85.40 -1. 66E-02 6.96E-02
9/18/2019 9:12:21AM Page 6 of6 Analysis Report for L2-011-104-FSPA-013-AV L2-011-104 Nuclide Energy Yield{%) Activity NuclldeMDA UneMDA Name (pCVgrams) (pCVgrams) (pCVgrams) (keV) + CS-137 661.65 85.12 9.94E-02 7.42E-02 7.42E-02 + CE-144 80.12 1.36 -3.82E+OO 3.65E-01 4.60E+OO 133.51 11.09 7.27E-02 3.65E-01 + EU-152 121.78 28.40 2.08E-02 1. 39E-Ol 1. 39E-01 344.28 26.60 -l.14E-01 1.78E-01 1408.00 20.74 8.31E-02 3.13E-01 + EU-154 123.07 40.40 1.95E-02 9.82E-02 9.82E-02 723.30 19.70 2.39E-01 3.lOE-01 1274.51 35.50 1.97E-02 2.14E-01 + EU-155 86.54 32.80 5.94E-03 1.63E-01 1.63E-01 105.31 21.80 -2.25E-02 1. 90E-Ol + BI-214 609.31 ** 46.30 l.SOE-01 1. 04E-Ol 1.04E-Ol 1120 .29 15.10 -l.29E-01 5.49E-01 1238 .11 5.94 3.91E-01 1. 49E+OO 1377.67 4 .11 2.llE-01 1. 76E+OO 1407.98 2.48 6.94E-01 2.61E+OO 1509.19 2.19 2.60E-01 2.86E+OO 1764.49
- 15.80 2.26E-01 3.61E-Ol
+ PB-214 77 .11 10.70 4.04E-01 1.13E-Ol 6.40E-Ol 295.21
- 19.20 2.lOE-01 1.47E-01 351.92
- 37.20 1.16E-01 1. 13E-Ol
+ PA-228 89.95 22.00 8.74E+OO 1.34E+Ol 2.27E+Ol 93.35 35.00 2.03E+OO 1.34E+Ol 105.00 16.30 -5.72E-01 2.47E+Ol 129.22 2.97 -4.98E+Ol 1. 30E+02 338.32 5.30 -4.25E+01 8.40E+Ol 463.00 13.80 -2. 98E+Ol 3.27E+Ol 911. 23 16.70 -6.98E+OO 3.73E+Ol + AM-241 59.54 36.30 -8.89E-03 2. 83*E-01 2.83E-01 + CM-243 103.76 23.00 -l.22E-01 1.82E-01 1. 82E-Ol 228.18 10.60 -3.36E-02 3.64E-Ol 277.60 14.00 -4.00E-02 3.16E-01
+ = Nuclide identified during the nuclide identification * = Energy line found in the spectrum > = MCA value not calculated @ = Half-life too short to be able to perfonn the decay correction ? = CAUTION: MCA value is inconsistent with Currie MCA at 95% confidence level
9/12/2019 10:51:0SAM Page I of6
----'Apex-Gamma Analysis Report for L2-011-104-FSGS-014-SS L2-011-104 GAMMA SPECTRUM ANALYSIS Sample Identification : L2-011-104-FSGS-014-SS Sample Daacrfptlon ~ L2-011-104 Semple Type : 500 ml Marinelli Unit Semple Point Sample Size : 8.984E+o2 grams Fadllty : Dairyland_NPP Sample Taken On : 9/9/2019 3:22:00PM Acquisition Started : .9/12/2019 10:20:SOAM Procedure : *500ml Marinelli Operator : Administrator Detector Name :HOTLAB .
Geometry : 500ml Marinelli Llvellme : 1800.0 seconds Real Time : 1805.4 seconds DeadTime : 0.30% Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 7/8/2014 Efficiency CaUbration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 7450 PEAK ANALYSIS REPORT Peak Analysis Performed on : 9/12/2019 10:50:59AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096
9/12/2019 10:51:0SAM Page2of6 Analysis Report for L2-011-104-FSGS-014-SS L2-011-104 Peak Energy ROI ROI Peak NetPeak NetArea Continuum FWHM No. {keV) s'tart end Centroid Area Uncertainty Counts (keV) F 1 92.47 178 - 189 185.47 5.0SE+Ol 23.95 4.56E+02 0.94 F 2 238.57 473 - 485 477.61 7.34E+Ol 24.74 3.40E+02 1.14 F 3 295.19 587 - 594 590.83 2.20E+Ol 14.97 l.33E+02 0.56 F 4 351.89 698 - 710 704.22 1.33E+02 26.65 l.30E+02 1.57 F 5 609.38 1212 - 1226 1219.09 7.73E+Ol 19.64 5.02E+Ol 1.88 F 6 911.01 1817 - 1829 1822.26 1.88E+Ol 10.07 2.91E+Ol 0.96 F 7 1460.64 2913 - 2931 2921. 40 2.34E+02 30.82 8.30E+OO 2.44 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 9/12(2019 10:50:59AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak. Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (lreV) Area Uncertainty Background Uncert. Area Uncert. F 1 92.47 5.0SE+Ol 23.95 5.0SE+Ol 2.39E+Ol F 2 238.57 7.34E+Ol 24.74 7.34E+Ol 2.47E+Ol F 3 295.19 2.20E+Ol 14.97 2.20E+Ol 1. SOE+Ol F 4 351.89 1.33E+02 26.65 4.lBE+Ol 1.86E+Ol 9.llE+Ol 3.25E+Ol F 5 609.38 7.73E+Ol 19.64 2.06E+Ol 1.21E+Ol 5.67E+Ol 2.31E+01 F 6 911.01 l.88E+Ol 10.07 1.88E+Ol 1.0lE+Ol F 7 1460.64 2.34E+02 30.82 2.82E+Ol 8.57E+OO 2.06E+02 3.20E+Ol
=
M First peak in a multiplet region
=
m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma
9/12/2019 10:51 :08AM Page3 of6 Analysis Report for L2-011-104-FSGS-014-SS L2-01M04 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (lceV) (pCVgrams) Uncertainty K-40 0 .99 1460.75
- 10.67 4.99E+OO 8.24E-01 PB-212 0.56 77.11 17.50 238.63
- 44.60 8.43E-02 2.87E-02 BI-214 0.34 609.31
- 46.30 1. 45E-Ol 5.97E-02 1120.29 15.10 1238.11 5.94 1377;67 4.11 1407.98 2.48 1509.19 2 . 19 1764. 49 15.80 PB-214 0.72 77.11 10.70 295.21
- 19.20 7.00E-02 4.78E-02 351. 92
- 37.20 1. 75E-Ol 6.31E-02
* = Energy line found in the spectrum.
* = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCVgrams)
K-40 0.998 4.99E+00 8.24E-Ol PB-212 0.560 8.43E-02 2.87E-02 BI-214 0.349 l. 45E-01 5.97E-02
9/12/2019 10:51:0BAM Pege4of6 Analysis Report for L2-011-104-FSGS-014-SS L2-011-104 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity
- Activity Contidence Uncertainty (pCilgrams)
PB-214 0.721 1. 0BE-01 3.81E-02
? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis
@ = nucllde contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma
9/12/2019 10:51 :08AM PagcS of6 Analysis Report for L2-011-104-FSGS-014-SS L2-011-104 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 9/12/2019 10:50:59AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty fype Nuclide F 1 92.47 2.80669E-02 23.70 Tol. PA-228 F 6 911. 01 l.04377E-02 26. 79 Tol. AC-228 PA-228 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Enors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LlnellDA Name (pCVgrams) (pCVgrams) (pCVgrams) (keV) + K-40 1460.75
- 10.67 4.99E+00 6.81E-0l 6.SlE-01
+ AR-41 1293.64 99.16 -8.42E+08 8.59E+09 8.59E+09 + CO-60 1173.22 100.00 6.54E-02 6.85E-02 9.04E-02 1332.49 100.00 6.26E-02 6.85E-02 + KR-85 513.99 0.43 6.02E+00 1.21E+0l 1. 21E+0l + Y-88 898.04 93.70 8.20E-03 4.83E-02 6.59E-02 1836.06 99.20 -6.23E-02 4.83E-02 + NB-94 702.63 100.00 1. 65E-02 4.90E-02 4.90E-02 871.10 100.00 -1. 46E-02 5.28E-02 + I-131 284.30 6.06 2.63E-01 6.SSE-02 8.60E-01 364.48 81.20 -1.27E-02 6.SSE-02 636.97 7.27 -3.63E-01 7.78E-01 + CS-134 604.70 97.60 -3.86E-03 6.61E-02 7.llE-02
9/12/2019 10:51:0BAM Page6 of6 Analysis Report for L2-011-104-FSGS-014-SS L2-011-104 Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Name (pCVgrams) (pCVgrams) (pCUgrams) (keV) CS-134 795.84 85.40 -5.lOE-02 6.61E-02 6.61E-02 + CS-137 661. 65 85.12 5.54E-02 7.0SE-02 7.0SE-02 + CE-144 80.12 1.36 6.62E-01 3.45E-Ol 4.28E+OO 133.51 11.09 -4.97E-02 3.4SE-Ol + EU-152 121.78 28.40 -3.89E-02 l.34E-Ol 1. 34E-01 344.28 26.60 1.59E-02 1. 69E-Ol 1408.00 20.74 l.36E-01 2.91E-01 + EU-154 123.07 40.40 -3.77E-03 9.50E-02 9.SOE-02 723.30 19.70 l.85E-02 2.84E-01 1274.51 35.50 2.74E-Ol 2.35E-01 + EU-155 86.54 32.80 -1.46E-02 1. 45E-01 1. 45E-Ol 105.31 21.80 -l.43E-01 l.77E-Ol + BI-214 609.31
- 46.30 l.45E-01 1. 04E-01 l.04E-01 1120.29 15.10 4.38E-01 5.67E-01 1238.11 5.94 l.03E+OO 1. 63E+OO 1377.67 4.11 l.44E+OO 1.53E+OO 1407.98 2.48 l.14E+OO 2.43E+OO 1509.19 2.19 l.SBE+OO 2.37E+OO 1764.49 15.80 l.30E-01 4.20E-Ol
+ PB-214 77.11 10.70 5.69E-01 1. lSE-01 5.86E-Ol 295.21
- 19.20 7.00E-02 l.32E-01 351.92
- 37.20 1. 75E-01 l.lSE-01
+ PA-228 89.95 22.00 1.22E+OO l.06E+OO 1. 77E+OO 93.35 35.00 5.88E-01 1.06E+OO 105.00 16.30 -9.77E-01 1.99E+OO 12 9. 22 2.97 6.63E+OO 1.08E+Ol 338.32 5.30 5.84E+OO 6.73E+OO 463.00 13.80 -l.42E+OO 2.86E+OO 911.23 16. 70 3.07E+OO 3.59E+OO + AM-241 59.54 36.30 4.58E-02 2 . 86E-Ol 2.86E-Ol + CM-243 103.76 23.00 4.63E-02 1.73E-Ol 1.73E-01 228.18 10.60 -2.77E-Ol 3.63E-01 277.60 14.00 1.42E-01 2.93E-01
+ = Nuclide identified during the nuclide identification * = Energy line found in the spectrum > = MDA value not calculated @ = Half-life too short to be able to perform the decay correction ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 4:18:48PM Page I of7 pex-Gamma Analysis Report for l2-SUB-102-AJGS-001-AV L2-011-102 RA CWD SOIL/ PACKAGE #:l2-SUB-102 RA cw SOIL GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-001-AV / Sample Description : L2-011-102 RA CWD SOIL / PACKAGE #:L2-SUB-102 RA CWD SOIL Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 7.962E+02 grams / Facility : Dairyland_NPP Sample Taken On : 3/30/2018 10:40:00AM Acquisition Started : 3/30/2018 3:18:25PM Procedure : 500ml Mari nelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3610.6 seconds Dead Time : 0.29% Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4181 PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/3012018 4:18:39PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 12
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 4:18:48PM Page 2 of7 Analysis Report for L2-SUB-102-AJGS-001-AV L2-011-102 RA CWD SOIL / PACKAGE #:L2-SUB-102 RA CWD SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 75 . 84 148 - 158 152 . 22 2 . 10E+02 52 . 76 7 . 60E+02 4 . 36 F 2 185 . 84 368 - 376 372 . 18 5 . 85E+Ol 28.33 4 . 96E+02 0 . 98 F 3 238 . 57 471- 482 477 . 62 1. 36E+02 35 . 15 6 . 47E+02 1.17 F 4 295 . 13 582 - 596 590 . 71 l.18E+02 31. 42 3 . 56E+02 1. 99 F 5 351. 92 696 - 710 704 . 27 l . 93E+02 32 . 65 2 . 74E+02 1. 43 F 6 582 . 85 1161 - 1173 1166 . 05 5 . 43E+Ol 19 . 76 1 . 05E+02 2 . 02 F 7 609 . 15 1214 - 1225 1218 . 62 l . 67E+02 28 . 96 l . 04E+02 1. 69 F 8 968.97 1934 - 1943 1938 . 17 3 . 29E+Ol 14 . 63 3 . 91E+ Ol 1. 91 F 9 1460 . 55 2915 - 2930 2921.22 3 . 92E+02 40 . 51 3 . 34E+Ol 2 . 39 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 3/30/2018 4:18:39PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 75 . 84 2 . 10E+02 52 . 76 2 . 10E+02 5 . 28E+Ol F 2 185 . 84 5 . 85E+Ol 28.33 5 . 85E+Ol 2 . 83E+Ol F 3 238 . 57 1 . 36E+02 35 . 15 1 . 36E+02 3 . 51E+Ol F 4 295 . 13 l . 18E+02 31. 42 l . 18E+02 3 . 14E+Ol F 5 351 . 92 1 . 93E+02 32 . 65 8 . 36E+Ol 3 . 72E+Ol 1 . 09E+02 4 . 95E+Ol F 6 582 . 85 5 . 43E+Ol 19 . 76 5 . 43E+Ol 1 . 98E+Ol F 7 609 . 15 l . 67E+02 28 . 96 4 . 12E+Ol 2 . 42E+Ol 1. 26E+02 3 . 77E+Ol F 8 968 . 97 3 . 29E+Ol 14 . 63 3 . 29E+Ol 1 . 46E+Ol F 9 1460 . 55 3 . 92E+02 40 . 51 5 . 63E+Ol 1 . 71E+Ol 3 . 36E+02 4 . 40E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma 10/7/2020 Page 13
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/201 8 4:18:48PM Page 3 of? Analysis Report for L2-SUB-102-AJGS-001-AV L2-011 -102 RA CWD SOIL/ PACKAGE # :L2-SUB-102 RA CWD SOIL NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\H OTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 99 1460 . 75
- 10 . 67 4 . 59E+OO 6 . 54E - 01 PB- 212 0 . 56 77 . 11 17 . 50 238 . 63
- 44 . 60 8 . 78E - 02 2 . 32E - 02 BI-21 4 0 . 34 609 . 31
- 4 6 . 30 l . 82E - 01 5 . SSE - 02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB- 21 4 0 . 72 77 . 11 10 . 70 295 . 21
- 19 . 20 2 . 12E- Ol 5 . 74E - 02 351 . 92
- 37 . 20 l. 19E - Ol 5 . 40E - 02 RA- 226 0 . 97 186 . 21
- 3 . 28 4 . 33E- 01 2 . llE - 01
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty
{pCi/grams) K-40 0 . 994 4 . 59E+OO 6 . 54E - 01 PB- 212 0 . 560 8 . 78E - 02 2 . 32E- 02 10/7/2020 Page 14
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 4:18:48PM Page4 of7 Analysis Report for l2-SUB-102-AJGS-001-AV L2-011-102 RA CWD SOIL / PACKAGE #:L2-SUB-102 RA CWD SOIL Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty {pCi/grams) BI-214 0 . 347 1 . 82E - 01 5 . SSE - 02 PB-214 0 . 721 1 . 62E - 01 3 . 93E - 02 RA-226 0 . 978 4 . 33E - 01 2 . llE - 01
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 15
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 4:18:48PM Pagc5 of7 Analysis Report for L2-SUB-102-AJGS-001-AV L2-011-102 RA CWD SOIL/ PACKAGE #:L2-SUB-102 RA CWD SOIL UNIDENTIFIED PEAKS Peak Locate Performed on : 3/30/2018 4:18:39PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 75 . 84 5 . 83842E- 02 12 . 55 fl.,,z;oS F F 8 6 582 .8 5 968 . 97 1 . 50852E- 02 9 . 14417E- 03 18 . 20 22 . 23 Tol. 11..-' z,o~ C- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_ NPP\library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCilgrams) (pCilgrams) (pCi/grams) (keV)
+ K-40 1460 . 75
- 10 . 67 4 . 59E+OO 6 . 40E-Ol 6 . 40E-01
+ AR-41 1293 . 64 99 . 16 4 . 34E - 02 3 . 65E - 01 j 3 . 65E-01
+ C0-60 1173 . 22 100 . 00 3 . 61E-02 4 . 94E-02 6 . 06E-02 1332 . 49 100 . 00 3 . 20E - 02 4 . 94E-02 KR - 85 513 . 99 0 . 43 1.lOE+Ol 9 . 96E 00 9 . 96E+OO
+ Y-88 898.04 93.70 2 . 27E- 02 3 . 59E - 02 4.96E-02 1836 . 06 99 . 20 -3 . 22E-02 3 . 59E-02
+ NB-94 702 . 63 100 . 00 6 . 16E-03 3 . 91E-02 3 . 91E-02 871 . 10 100 . 00 -2.83E-03 4.32E-02
+ I - 131 284 . 30 6 . 06 4 . BOE-02 4. lSE -02 5 . 29E-01 364 . 4 8 81. 20 1 . 28E-02 4 . lSE - 02 636 . 97 7 . 27 1. OBE - 01 5.20E-01
+ CS - 134 604 . 70 97 . 60 -6 . 86E-02 5 . 61E-02 5 . 61E-02 795 . 84 85. 40 4 . 22E-02 5 . 82E-02 10/7/2020 Page 16
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 4:18:48PM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-001-AV L2-011-102 RA CWD SOIL/ PACKAGE # :L2-SUB-102 RA CWD SOIL Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV)
+ CS -1 37 661 . 65 85 . 12 5 . 72E - 02 5 . 63E- 02 5 . 63E - 02
+ CE- 144 80 . 12 1. 36 - 2 . 64E+OO 2 . 78E- 01 3 . 24E+OO 133 . 51 1 1. 09 1 . 70E - 01 2 . 78E- 01
+ EU-152 121 . 78 28 . 40 - 2 . 04E - 02 1. 06E- 01 J l . 06E- 01 244 . 69 7 . 49 - l . 46E - 01 4 . 78E- 01 964 . 00 14 . 44 3 . 15E- 01 3 . 83E- 01
+ EU - 154 1408 . 00 123 . 07 20 . 74 40 . 40 1 . 30E - 01
- 1 . 60E - 02 7 . 47E - 02
- 12. 24E- 01 7 . 47E - 02 247 . 94 6 . 60 - 7 . 64E - 01 5 . 06E-01 723 . 30 19 . 70 - 1 . 2 4E- 01 2 . 00E - 01 873 . 20 11 . 50 l . 55E - 01 3 . 90£ - 01 1004 . 76 17 . 90 -9 . 18E- 02 2 . 54E-Ol 127 4. 51 35 . 50 7 . 52E - 02 1 . 56E - 01
+ EU - 155 86 . 54 32 . 80 - 3 . 89E - 02 l . 13E-01 1 . 13E- Ol 105 . 31 21.80 -2 . 73£ - 02 l . 44E-01
+ BI - 214 609 . 31
- 46 . 30 1 . 82£ - 01 8 . 91E- 02 8 . 91E - 02 1120 . 29 15 . 10 3 . 50E - 01 4 . 20E-01 1238 . 11 5 . 94 -l . 05E - 01 1 . lOE+OO 1377 . 67 4 . 11 7 . 80E - 01 l . 18E+OO 1407 . 98 2 . 48 1 . 09E+OO 1 . 87E+OO 1509 . 19 2 . 19 -2 . 63E-Ol 1. 54E+OO 1764 . 49 15 . 80 4 . 61£ - 01 3 . 75£-01
+ PB- 214 77 . 11 10 . 70 5 . 77E - 01 1 . 05E -0 1 4 . 4 2E- Ol 295 . 21
- 19 . 20 2 . 12E- 01 l . 39E- Ol 351 . 92
- 37 . 20 1 . 19E - 01 l . 05E - 01
+ PA- 228 89 . 95 22 . 00 l . 35E - 01 1.16E- 01 l . 9 6E- 01 93 . 35 35 . 00 9 . 75E - 02 1.16E- 01 1 05 . 00 16 . 30 - 6 . 00E - 02 2 . 25E- 01 129 . 22 2 . 97 - 8 . 04E - 02 1. 21E+OO 338 . 32 5 . 30 2 . 39E - 01 7 . 74E- 01 463 . 00 13 . 80 2 . 47E - 02 3 . llE - 01 911 . 23 16 . 70 3 . 05E - 01 3 . 77£-01 AM- 241 59 . 54 36 . 30 1 . 70E - 02 2 . 22£ - 01 2 . 22E-01
+ CM- 243 103 . 76 23 . 00 6 . 90£-03 l . 37E - 01 1 . 37E - Ol 228 . 18 10 . 60 - 1 . 06E- 01 2 . 82E - 01 277 . 60 14 . 00 - 2 . 34£ - 01 2 . 32E - 01
+ = Nuclide identified during the nuclide identification
=Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 17
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 4:18:48PM Page 7 of 7 Analysis Report for L2-SUB-102-AJGS-001-AV L2-011-102 RA CWD SOIL / PACKAGE #:L2-SUB-102 RACWD SOIL 10/7/2020 Page 18
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 5:23:15PM Page I of7 pex-Gamma Analysis Report for L2-SUB-102-AJGS-002-AV L2-011-102 RA CWD SOIL/ PACKAGE #:L2-SUB-102 RA CWD SOIL GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-002-AV Sample Description : L2-011 -102 RA CWD SOIL/ PACKAGE #:L2-SU8-102 RA CWD SOIL Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 7.337E+02 grams Facility : Dairyland_NPP Sample Taken On : 3/30/2018 11 :28:00AM Acquisition Started : 3/30/2018 4:22:52PM Procedure : 500ml Marinelli Operator : Adm inistrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611 .2 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4182 PEAK ANALYS/S REPORT Peak Analysis Performed on : 3/30/2018 5:23:06PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 19
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/20 18 5:23:15PM Page 2 of7 Analysis Report for L2-SUB-102-AJGS-002-AV L2-011-102 RA CWD SOIL/ PACKAGE #:L2-SUB-102 RA CWD SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (ke V) start end Centroid Area Uncertainty Counts (keV) F 1 76 . 00 148 - 160 152 . 54 l . 95E+02 55 . 64 l . OOE+03 4 . 25 F 2 185 . 76 367 - 379 372 . 02 6 . 81E+Ol 33 . 37 6 . 59E+02 1 . 59 F 3 238 . 68 473 - 485 477 . 83 2 . 02E+02 37 . 24 4 . 69E+02 1. 42 F 4 294 . 98 583 - 596 590 . 41 1. 14E+02 29 . 89 3 .4 0E+02 1. 58 F 5 338 . 39 672 - 681 677 . 20 4 . 04E+Ol 22 . 08 2 . 11E+02 1. 45 F 6 351 . 84 700 - 712 70 4. 12 1 . 77E+02 32 . 96 2 . 52E+02 1. 78 F 7 583 . 13 1162 - 1173 1166 . 60 4 . 45E+Ol 17 . 26 9 . 27E+Ol 1. 41 F 8 609 . 18 1212 - 1226 1218 . 69 l . 06E+02 23 . 92 1 . 09E+02 1. 70 F 9 911 . 11 1818 - 1827 1822 . 46 3.25E+Ol 14 . 66 6 . 55E+Ol 1.16 F 10 1120 . 19 2235 - 2246 2240 . 56 4 . 18E+Ol 15 . 96 4 . 44E+Ol 2 . 09 F 11 1332 . 10 2660 - 2670 2664 . 34 l . 81E+Ol 11.18 3 . 76E+Ol 1. 44 F 12 1460 . 68 2914 - 2930 2921.47 4 . 16E+02 41. 33 2 . 07E+Ol 2 . 51 M = First peak in a multlplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 3/30/2018 5:23:06PM Env. Background File : C:\Canberra\Apex\Root\Oai,yland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76 . 00 l . 95E+02 55 . 64 l . 95E+02 5 . 56E+Ol F 2 185 . 76 6 . 81E+Ol 33 . 37 6 . 81E+Ol 3 . 34E+Ol F 3 238 . 68 2 . 02E+02 37 . 24 2 . 02E+02 3 . 72E+Ol F 4 294 . 98 l.14E+02 29 . 89 l.14E+02 2 . 99E+Ol F 5 338 . 39 4 . 04E+Ol 22 . 08 4 . 04E+Ol 2 . 21E+Ol F 6 351 . 84 l . 77E+02 32 . 96 8 . 36E+Ol 3 . 72E+Ol 9 . 32E+Ol 4 . 97E+Ol F 7 583 . 13 4 . 45E+Ol 17 . 26 4 . 45E+Ol l.73E+Ol F 8 609.18 l . 06E+02 23 . 92 4 . 12E+Ol 2 . 42E+Ol 6 . 50E+Ol 3 . 40E 01 F 9 911 . 11 3 . 25E+Ol 14.66 3 . 25E+Ol l.47E+Ol F 10 1120 . 19 4 . 18E+Ol 15 . 96 4 . 18E+Ol 1. GOE 01 F 11 1332 . 10 l . 81E+Ol 11.18 1 . 81E+Ol l . 12E+Ol F 12 1460.68 4 . 16E+02 41. 33 5 . 63E+Ol 1 . 71E+Ol 3 . 60E+02 4 . 47E+Ol 10/7/2020 Page 20
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 5:23:15PM Page 3 of7 Analysis Report for L2-SUB-102-AJGS-002-AV L2-011-102 RA CWD SOIL/ PACKAGE #:L2-SUB-102 RA CWD SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000srgma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence {keV) (pCilgrams) Uncertainty K-40 0 . 99 1460 . 75
- 10 . 67 5 . 35E+00 7 . 28£-01 PB-212 0 . 56 77 . 11 17 . 50 238 . 63
- 44 . 60 1 . 42E - 01 2 . 72E- 02 BI-214 0 . 58 609 . 31
- 4 6 . 30 l . 02E - 01 5 . 37E-02 1120 . 29
- 15 . 10 3 . 48E-01 1. 34E-01 1238 . 11 5 .94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509.19 2 . 19 1764 .4 9 15 . 80 PB-214 0 . 71 77 .11 10.70 295 . 21
- 19 . 20 2 . 23E-01 5 . 93E-02 351 . 92
- 37 .2 0 1 . l0E-01 5 . 88E-02 RA-226 0.96 186 . 21
- 3 .2 8 5 . 47E-01 2 . 70E-01
* = Energy line found In the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT 10/7/2020 Page 21
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 5:23:15PM Page 4 of7 Analysis Report for L2-SUB-102-AJGS-002-AV L2-011-102 RA CWD SOIL / PACKAGE #:L2-SUB-102 RA CWD SOIL Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) K-40 0 . 999 5 . 35E+00 7.28E-01 PB - 212 0 . 560 l.42E - 01 2 . 72E-02 BI - 214 0 . 583 l.36E-01 4 . 99E-02 PB-214 0 . 718 l . 66E-01 4 . 17E-02 RA-226 0 . 968 5 . 47E-01 2 . 70E - 01
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 22
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 5:23:1SPM Page 5 of7 Analysis Report for L2-SUB-102-AJGS-002-AV L2-011-102 RA CWD SOIL I PACKAGE #:L2-SUB-102 RA CWD SOIL UNIDENTIFIED PEAKS Peak Locate Performed on : 3/30/2018 5:23:06PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy {keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 76 . 00 5 . 409 90E - 02 14. 2 8 fl.,, ,it,~ F 5 338 . 39 l . 12258E- 02 27 . 32 Tol. AC- 228 PA- 228 F 7 583 . 13 l . 23500E - 0 2 19 .4 1 -r, . . ~2, F 9 911 . 11 9 . 0253 4E - 03 22 .56 Tol. AC - 228 PA- 228 F 11 1332 . 10 5 . 01752E- 03 30 . 93 Tol. CO- 60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{%) Activity Nuclide MDA LineMDA Name (pCl/grams) (pCl/grams) (pCl/grams) (keV)
+ K- 40 1460 . 75 10 . 67 5 . 35E 00 6 . 62E - 01 6 . 62E- 01
+ AR - 41 1293 . 64 99 . 16 - 7 . 28E - 02 4. 0SE - 01 4 . 0SE - 01
+ CO- 60 1173 . 22 100 . 00 7 . S0E - 03 6 . 49E- 0 2 6 . 81E- 02 1332 .4 9 100 . 00 4 . 76E- 02 6 .4 9E-0 2
+ KR- BS 513 . 99 0 . 43 l . 38E+0l l . 08 E+0l l . 08E+0l
+ Y-8 8 8 98 . 0 4 93 . 70 l . 35E - 02 3 . 77E - 02 5 . 76E- 02 1836 . 06 99 . 20 5 . 32 E- 03 3 . 77E- 02
+ NB - 94 702 . 63 100 . 00 - 2 . 65E- 02 4 . 25E - 02 4. 25E- 02 871 . 10 100 . 00 - 3 . 68E - 02 4 . 48E- 02 10/7/2020 Page 23
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 5:23:15PM Page 6 of 7 Analysis Report for L2-SUB-102-AJGS-002-AV L2-011-102 RA CWD SOIL/ PACKAGE #:L2-SUB-102 RA CWD SOIL Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCi/grams) (pCilgrams) (pCi/grams) (keV)
+ I - 131 284 . 30 6 . 06 - l . 04E - 0 2 4 . 54E- 02 5 . 63E - 01 364 . 48 81. 20 l. 08E - 02 4 . 54E - 02 636 . 97 7 . 27 2 . 94E- 01 6 . 05E- 01
+ CS- 134 604 . 70 97 . 60 l . 35E- 02 5 . 41E- 02 5 . 41E - 02 795 . 8 4 85 . 40 - 8 . 4 2E - 03 5 . 49E-02
+ CS- 137 6 61. 65 85 . 12 4 . 50E - 02 6 . 20£- 02 6 . 20E - 02
+ CE - 144 80 . 12 1.36 - 1 . 96E+OO 2 . 89E- 01 3 . 56E+OO 133 . 51 11.09 - 6 . 29E - 02 2 . 89E - 01
+ EU - 152 12 1. 78 28 . 40 - 3 . 48E - 02 1 . lSE - 01 / 1 . lSE - 01 244 . 69 7 . 49 - 2 . 84E - 01 5 . lSE - 01 964 . 00 14 . 44 2 . 05E - 01 4 . 0lE - 01 1 408 . 00 20 . 74 - 5 . 00E - 02 2 . 43E- 01
+ EU - 154 123 . 07 40 . 40 3 . 37E - 04 0 . 12£- 02 I 0 . 12£- 02 247 . 94 6 . 60 -4 . 3 6E- 01 5 . 34E - 01 723 . 30 19 . 70 3 . 09E - 02 2 . 44£ - 01 873 . 20 11. so - 1 . 4 4E - 01 3 . 86E - 01 1004 . 76 17 . 90 2 . 75E - 02 3 . 14£- 01 1274 . 51 35 . 50 - 5 . 95E - 02 1 . 57£ - 01
+ EU- 155 86 . 54 32 . 80 - 7 . 92E - 02 1 . 2 4£ - 01 1 . 24E - 01 105 . 31 21. 80 - 6 . 66E - 02 1 . SlE-01
+ BI - 214 609 . 31
- 4 6 . 30 1 . 02E - 01 1 . 00E- 01 1 . 00E - 01 1120 . 29
- 15 . 10 3 . 48E-01 2 . 27E- 01 1238 . 11 5 . 94 9 . 63E - 01 1. 21E+OO 1377 . 67 4 . 11 1. 35E+OO l . 32E 00 1407 . 98 2 . 48 - 4 . 18E- 01 2 . 03E+OO 1509 .1 9 2 . 19 - 1 . 02E+OO l . 90E+OO 1764 . 4 9 15 . 80 l . 84E- 01 3 . 60E- 01 PB- 214 77 . 11 10 . 70 7 . 5 4E- 01 l . llE - 01 4. 89E - 01 295 . 21
- 19 . 20 2 . 23E - 01 l . 44E - 01 351 . 92
- 37 . 20 l . lOE - 01 1 . llE-01
+ PA- 22 8 89 . 95 22 . 00 2 . 6 9E - Ol l . 2 7E- 01 2 . 17E- Ol 93 . 35 35 . 00 -2. SOE- 02 1 . 27E - 01 105 .0 0 16 . 30 - l . 67E - 02 2 . 41E - 01 129 . 22 2 . 97 6 . 22E- 01 1 . 29E +OO 338 . 32 5 . 30 6 . 7 4£ - 01 8 . 6 5E- 01 463 . 00 13 . 80 l . 45E - 02 3 . 48E - 01 911. 23 16 . 70 3 . 4 4E- 01 4 . 19E- 01
+ AM - 241 59 . 5 4 36 . 30 2 . 59E - 01 2 .49 E- 01 2 . 49E - 01
+ CM- 243 103 . 76 23 . 00 - 8 . 13E- 02 l . 4 3E - 01 l.43E -0 1 228 . 1 8 10 . 60 - 1 . 1 4£ - 01 3 . 08E - 01 277 . 60 14 . 00 - 6 . 13E- 03 2 . 44£-0 1
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 24
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 5:23:1SPM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-002-AV L2-011-102 RA CWD SOIL I PACKAGE #:L2-SUB-102 RA CWD SOIL 10/7/2020 Page 25
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 7:24:25PM Page I of7 pex-Gamma Analysis Report for L2-SUB-102-QJGS-002-AV l2-011-102 RA CWD SOIL / PACKAGE #:L2-SUB-102 RA CWD SOIL GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-QJGS-002-AV / Sample Description : L2-011-102 RA CWD SOIL / PACKAGE #:L2-SUB-102 RA CWD SOIL Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 7.737E+02 grams / Facility : Dairyland_ NPP Sample Taken On : 3/30/2018 11 :38:00AM Acquisition Started : 3/30/2018 6:24:02PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611 .2 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100
- 4096 Peak Area Range (in channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4184 PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/30/2018 7:24 :15PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 26
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 7:24:25PM Page 2 of7 Analysis Report for L2-SUB-102-QJGS-002-AV L2-011-102 RA cw SOIL/ PACKAGE #:L2-SUB-102 RA cw SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (keV) M 1 238 . 56 472 - 4 90 477 . 60 2 . 16E+02 37.54 3 . 62E+02 1. 74 m 2 241.84 472 - 490 484 . 16 9 . 71E+Ol 28 . 03 3.50E+02 1. 75 F 3 295 . 00 582 - 595 590 . 46 9.62E+Ol 29 . 98 3 . 71E+02 1. 73 F 4 338 . 13 672 - 681 676 . 69 3.96E+Ol 21 . 77 l . 95E+02 1. 53 F 5 351. 82 698 - 709 704 . 07 1.94E+02 33 . 12 2.19E+02 1. 52 F 6 583 . 07 11 57 - 1174 1166 . 48 7 . 25E+Ol 21. 54 1 . 58E+02 1. 70 F 7 609 . 23 11 92 - 1224 1218 . 78 1 . 60E+02 28 . 57 3 . 32E+02 1. 77 F 8 911 . 06 1 818 - 1827 1822 . 37 2 . 90E+Ol 15 . 03 8 . 40E+Ol 1. 20 F 9 969 . 50 1 934 - 194 6 1939 . 23 3 . 22E+Ol 17 . 19 7 . 20E+Ol 2 . 67 F 10 1120 . 17 2234 - 2245 2240 . 52 l . 90E+Ol 13 . 36 6 . 20E+Ol 1.58 F 11 1332 . 02 2659 - 2669 2664 . 18 2 . 67E+Ol 12 . 12 1 . 91E+ 01 1. 90 F 12 1460 . 73 2912 - 2931 2921.57 4.61£+02 43 . 69 3 . 96E + Ol 2 . 28 M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 3/30/2018 7:24:15PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. {keV) Area Uncertainty Background Uncert. Area Uncert. M 1 238 . 56 2 . 16E+02 37 . 54 2 . 16E+02 3 . 75E+Ol m 2 241 . 84 9 . 71£+01 28 . 03 9 . 71E+Ol 2 . 80E+Ol F 3 295 . 00 9 . 62E+01 29 . 98 9 . 62E+Ol 3 . 00E+Ol F 4 338 . 13 3 . 96E+Ol 21.77 3 . 96E+Ol 2 . 18E 01 F 5 351. 82 1 . 94£+02 33 . 12 8 . 36E+Ol 3 . 72E+Ol l . 10E+02 4.98E 01 F 6 583 . 07 7 . 25E+Ol 21. 54 7 . 25£+01 2 . 15E+Ol F 7 609 . 23 l . 60E+02 28 . 57 4.12£+01 2 .4 2E + Ol 1 . 19E+02 3 . 75£+01 F 8 911. 06 2 . 90£+01 15 . 03 2 . 90E+Ol 1. 50E+Ol F 9 969 . 50 3 . 22E+Ol 17 . 19 3 . 22E+Ol 1 . 72E+Ol F 10 1120 . 17 1.90£+01 13 . 36 l . 90E+Ol 1 . 34£+01 F 11 1332 . 02 2 . 67E+Ol 12 . 12 2.67£+01 l . 21E+Ol F 12 1460 . 73 4 . 61£+02 43 . 69 5.63E+Ol 1. 71£+01 4 . 05E+02 4 . 69E+Ol 10/7/2020 Page 27
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 7:24:25PM Page 3 of7 Analysis Report for L2-SUB-102-QJGS-002-AV L2-011-102 RA CWD SOIL / PACKAGE # :L2-SUB-102 RA CWD SOIL M = First peak in a multiplet reg ion m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide library Used : C:\Canberra\Apex\Root\Dairyland_ NPP\library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 1.00 1460 . 75
- 10 . 67 5 . 71£+00 7 . 33E- 01 PB- 212 0 . 56 77 . 11 17 . 50 238 . 63
- 44 . 60 1. 4 4E-Ol 2 . 61E-02 BI - 214 0 . 58 609 . 31
- 46 . 30 l . 77E-01 5 . 66E- 02 1120 . 29
- 15 . 10 1. 50E - 01 l . 06E-01 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB- 214 0 . 71 77 . 11 10 . 70 295 . 21
- 19 . 20 l . 78E- 01 5 . 61£- 02 351 . 92
- 37 . 20 l . 23E- 01 5 . 59£- 02 AC - 228 0 . 60 209 . 28 4 . 40 338 . 32
- 11. 40 l . 39E- 01 7 . 68£ - 02 794 . 70 4 . 60 911. 60
- 27 . 70 1. 04£-01 5 . 41E-02 964 . 60 5 . 20 969 . 11
- 16 . 60 2 . 03£ - 01 1 . 09E-Ol
* = Energy line found in the spectrum.
- =Manually added nuclide.
? =Manually edited nuclide.
@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma 10/7/2020 Page 28
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 7 :24:25PM Page 4 of7 Analysis Report for L2-SUB-102-QJGS-002-AV L2-011-102 RA cw SOIL/ PACKAGE #:L2-SUB-102 RA CWD SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams) K-40 1 . 000 5 . 71 E+O0 7 . 33E - 01 PB-212 0 . 560 1 . 44E-01 2 . 61E - 02 BI - 214 0 . 584 1 . 71E- 01 4 . 99E- 02 PB - 214 0 . 719 1. S0E - 01 3 . 96E - 02 AC-228 0 . 608 l . 28E - 01 4. l0E - 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the Interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 29
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 7:24:25PM Page S of7 Analysis Report for L2-SUB-102-QJGS-002-AV L2-011-102 RA CWD SOIL/ PACKAGE #:L2-SUB-102 RA CW SOIL UNIDENTIFIED PEAKS Peak Locate Performed on : 3/30/2018 7:24:15PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 2 241.84 2 . 69736E - 02 14 . 43 ?J,,--,:,,1,/ F 6 583 . 07 2 . 01428E- 02 14 . 85 -(7-z,tfo F 11 1332 . 02 7 . 42499E- 03 22 . 68 Co-(ii) M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCi/grams) (pCilgrams) (pCilgrams) (keV)
+ K- 40 1460 . 75
- 10 . 67 5 . 71E+00 6 . 91E - 01 6 . 91E-01
+ AR-41 1293 . 64 99 . 16 - 1. 89E- 01 7 . 89E - 01 7 . 89E- 01
+ CO - 60 1173 . 22 100 . 00 5 . 61E-02 5 . 78E-02 6 . 98E-02 1332 . 49 100 . 00 7 . 0lE - 02 5 . 78E-02
+ KR-85 513 . 99 0 . 43 l . 25E+0l l . 03E+0l 1 . 03E+0l
+ Y-88 898 . 04 93 . 70 - 2 . 12E-03 3 . BlE-02 5 . 28E- 02 1836 . 06 99 . 20 2 . 75£- 02 3 . BlE-02
+ NB- 94 702 . 63 100 . 00 - 3 . 0lE-03 4 . 0BE- 02 4 . 0BE-02 871.10 100 . 00 3 . 51E-02 4 . 80E- 02
+ I - 131 284 . 30 6 . 06 - 5 . 0SE - 01 4 . 06E - 02 5 . 40E - 01 364 . 4 8 81.20 -2 . 4 0E - 02 4 . 06E - 02 636 . 97 7 . 27 l.73E - 01 5 . 79E- 01
+ CS-134 604 . 70 97 . 60 l . 40E - 01 5 . S0E- 02 5 . 99E- 02 10/7/2020 Page 30
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 7:24 :25PM Page 6 of7 Analysis Report for L2-SUB-102-QJGS-002-AV L2-011-102 RACWD SOIL/ PACKAGE #:L2-SUB-102 RACWD SOIL Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCilgrams) (pCilgrams) (pCi/grams) (keV) CS-134 795 . 84 85 . 40 2.88E-03 5.SOE- 02 ~ - 50E-02
+ CS-137 661 . 65 85 . 12 7 . 44E-02 6 . 29E-02 6 . 29E-02
+ CE-144 80 . 12 1. 36 4 . 34E+OO 2 . 90E-01 3 . 49E+OO 133 . 51 11 . 09 3 . 29E - 01 2 . 90E-01
+ EU-152 121 . 78 28.40 -1 . 72E - 01 l . 06E-Ol / l . 06E-01 244 . 69 7 . 49 5 . 77E - 02 4 . 88E- 01 964 . 00 14 . 44 - l . 40E - 01 4 . 13E-01 1408 .00 20 . 74 5 . 16E- 02 2 . 28E-01
+ EU-154 123 . 07 40 . 40 - 5 . 34E - 02 7 . 54E - 02 / 7 . 54E-02 247 . 94 6 . 60 1.17E- 01 5 . 12E - 01 723 . 30 19 . 70 l . lSE - 01 2 . 26E - 01 873 . 20 11. 50 - 5 . 02E - 03 4 . 05E-01 1004 . 76 17 . 90 - l . 07E -0 1 3 . 05E - 01 1274 . 51 35 . 50 l . 31E - 01 1 . 64E-01
+ EU - 155 86 . 54 32 . 80 -4 . 55E - 02 1 . 21E-01 l . 21E- Ol 105 . 31 21. 80 3 . 43E - 02 l.48E-01
+ BI - 214 609 . 31
- 46.30 1 . 77E-01 1. 68E-01 l . 68E-01 1120 . 29
- 15 . 10 1. SOE- 01 2 . 55E-01 1238 . 11 5 . 94 - 1 . 82E - 01 l.lOE+OO 1377 . 67 4 . 11 8 . 57E-01 l . 38E+OO 1407 . 98 2 . 48 4 . 32E - 01 1 . 91E+00 1509 . 19 2 . 19 2 . 0SE+OO 2 . llE+OO 1764 . 49 15 . 80 2 . 97E- 01 3 . 23E- 01
+ PB- 214 77 . 11 10 . 70 8 . 38E-02 l . OlE-01 4 . 63E- 01 295 . 21
- 19 . 20 1. 78E-01 l . 43E-01 351 . 92
- 37 . 20 1. 23E- 01 l .O lE-01
+ PA - 228 89 . 95 22 . 00 8 . 22E-02 1. 32E-Ol 2 . 20E-01 93 . 35 35 . 00 7 . 68E- 02 l . 32E- 01 105 . 00 16 . 30 l . 61E - 02 2 . 49E - 01 129 . 22 2 . 97 8 . 06E- 01 1 . 34E+OO 338 .3 2 5 . 30 5 . 22E-01 8.25E-Ol 463 . 00 13.80 -5 . 24E - 02 3 . 42E-01 911.23 16.70 5 . 32E - 01 4 . 33E-01
+ AM-241 59 . 54 36.30 l . 06E - 01 2 .4 0E - 01 2 . 40E - 01
+ CM-243 103 . 76 23.00 -2 . 62E-02 1 .4 2E-01 l . 42E-01 228 . 18 10.60 2 .0 7E-01 2 . 93E-01 277 . 60 14 . 00 l . OSE - 01 2 . 48E - 01
+ Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 31
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 7:24:25PM Page 7 of7 Analysis Report for L2-SUB-102-QJGS-002-AV L2-011-102 RA CW SOIL / PACKAGE #:L2-SUB-102 RA CWD SOIL 10/7/2020 Page 32
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 8:29:54PM Page I of7 pex-Gamma Analysis Report for L2-SUB-102-AJGS-001-SS SU: L2-011-102 RACWD SOIL/ PACKAGE: L2-SUB-102 GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-001-SS / Sample Description : SU : L2-011-102 RA CWD SOIL/ PACKAGE: L2-SUB-102 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 5.699E+02 grams / Facility : Dairyland_NPP Sample Taken On : 3/30/2018 12:05:00PM Acquisition Started : 3/30/2018 7:29:32PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611 .0 seconds Dead Time : 0.30 % Peak Locate Threshold : 3.00 Peak Locale Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100
- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4185 PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/30/2018 8:29:45PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 33
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 8:29:54PM Page 2 of7 Analysis Report for L2-SUB-102-AJGS-001-SS SU : L2-011-102 RA CWD SOIL/ PACKAGE: L2-SUB-102 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) M 1 74 . 73 147 - 193 150 . 02 2 . 03E+02 43 . 47 7 . 49E+02 1. 40 m 2 77 . 06 147 - 193 154 . 66 2 . 49E+02 46 . 76 8 . 15E+02 1. 40 m 3 83 . 93 147 - 193 168 .4 0 7 . 61E+Ol 38 . 88 7 . 49E+02 1. 42 m 4 87 . 07 147 - 193 174 . 68 l . 19E+02 35 .2 5 7 . 21E+02 1. 42 m 5 92 . 87 147 - 193 186 . 28 1 . 62£+02 38 . 84 7 . 38E+02 1. 43 F 6 186 . 03 364 - 378 372 . 56 1 . 52E+02 40 . 47 9 . 29E+02 l. 58 M 7 238 . 66 472 - 490 477 . 79 3.54E+02 46.78 4 . 38E+02 1. 38 m 8 241 . 74 472 - 490 483 . 95 l . 28E+02 31.13 4.32E+02 1. 38 F 9 295 . 12 582 - 598 590 . 69 2 . 23E+02 38 . 02 5 . 86E+02 1. 45 F 10 338 . 39 672 - 685 677 . 21 7 . 98E+Ol 25 . 37 2 . 73E+02 1.54 F 11 351 . 86 695 - 712 704 . 14 4 . 25E+02 46 . 89 3 . 91E+02 1. 60 F 12 582 . 98 1162 - 1171 1166 . 30 9 . 19E+Ol 24.97 l . 52E+02 1. 48 F 13 609 . 31 1213 - 1226 1218 . 96 2.61E+02 35 .4 7 1 . 52E+02 1. 68 F 14 911 . 11 1816 - 1828 1822 . 45 8 . 31E+Ol 21 . 64 7 . 79E+Ol 1. 92 F 15 968 . 97 1934 - 1943 1938 . 17 4 . 34E+Ol 16 . 79 5 . 49E+Ol 1. 87 F 16 1120 . 46 2234 - 2249 2241.10 5.23E+Ol 18 . 35 7 . 48E+Ol 2 . 43 F 17 1238 . 52 2470 - 2482 2477 . 20 2 . 91E+Ol 13 . 68 4 . 87E+Ol 1. 66 F 18 1333 . 23 2662 - 2671 2666 . 59 1 . 63E+Ol 11 . 75 4 . 29E+Ol 1.50 F 19 1460 . 80 2913 - 2931 2921 . 71 3 . 45E-t-02 37 . 82 2 . 76E+Ol 2 . 39 F 20 1764 . 29 3523 - 3535 3528 . 66 4 . 32E+Ol 14 . 42 l . 30E+Ol 2 . 43 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 3/30/2018 8:29:45PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. M 1 74 . 73 2 . 03E+02 43 .4 7 2 . 03E+02 4 . 35E+Ol m 2 77 . 06 2 . 49E+02 46 . 76 2 . 49E+02 4 . 68E+Ol m 3 83 . 93 7 . 61E+Ol 38 . 88 7 . 61E+Ol 3 . 89E+Ol m 4 87 . 07 1 . 19E+02 35 . 25 l . 19E+02 3 . 53E+Ol m 5 92 . 87 l . 62E+02 38 . 84 l . 62E+02 3 . 88E+Ol F 6 186 . 03 l . 52E+02 40 . 47 1.52E+02 4.05E+Ol M 7 238 . 66 3 . 54E+02 46.78 3 . 54E+02 4.68E+Ol m 8 241.74 1. 28E+02 31.13 1 . 28E+02 3 . llE-t-01 F 9 295.12 2 . 23E+02 38 . 02 2 . 23E+02 3 . 80E+Ol 10/7/2020 Page 34
LAC LTP - Final Status Survey Package - 3/21/2018 3130/2018 8:29:54PM Page of7 Analysis Report for L2-SUB-102-AJGS-001-SS SU: L2-011 -102 RA cw SOIL/ PACKAGE: L2-SUB- 102 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 10 338.39 7 . 98E+Ol 25 . 37 7 . 98E+Ol 2 . 54E+Ol F 11 351. 86 4 . 25E+02 46 . 89 8 . 36E+Ol 3 . 72E 01 3 . 42E+02 5 . 99E+Ol F 12 582 . 98 9 . 19E+Ol 24 . 97 9 . 19E+Ol 2 . 50E+Ol F 13 609 . 31 2 . 61E+02 35 . 47 4 . 12E+Ol 2 . 42E+Ol 2 . 20E+02 4 . 29E+Ol F 14 911 . 11 8 . 31E+Ol 21. 64 8 . 31E+Ol 2 . 16E+Ol F 15 968 . 97 4 . 34E+Ol 16 . 79 4 . 34E+Ol 1 . 68E+Ol F 16 1120 . 46 5 . 23E+Ol 18 . 35 5 . 23E+Ol 1. 83E+Ol F 17 1238 . 52 2 . 91E 01 13 . 68 2 . 91E+Ol l . 37E+Ol F 18 1333 . 23 l . 63E+Ol 11 . 75 l . 63E+Ol 1. 18E+Ol F 19 1460 . 80 3 . 45E+02 37 . 82 5 . 63E 01 1 . 71E+Ol 2 . 89E+02 4 . lSE+Ol F 20 1764 . 29 4 . 32E+Ol 14 . 42 l . 52E+Ol 9 . 80E+OO 2 . 80E+Ol l . 74E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB IDENTI FIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence {keV) {pCilgrams) Uncertainty K- 40 1.00 1460 . 75
- 10 . 67 5 . 52E+OO 8 . SlE - 01 EU - 155 0 . 30 86 . 54
- 32 . 80 l . 33E - 01 4 . 06E-02 105 . 31 21. 80 PB - 212 1.00 77 . 11
- 17 . 50 6 . 15E-01 l . 22E-01 238 . 63
- 44 . 60 3 . 20E - 01 4 . SSE-02 BI - 214 0 . 87 609 . 31 4 6 . 30 4 . 44E - 01 9 . 03E-02 1120 . 29
- 15 . 10 5 . 61£ - 01 l . 99E-01 1238 . 11 5 . 94 8 . 67E-01 4 . lOE - 01 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49
- 15 . 80 4 . 24E - 01 2 . 65E- 01 PB - 214 0 . 99 77 . 11
- 10 . 70 l . OlE+OO 2 . 00E-01 295 . 21
- 19 . 20 5 . 59E-01 9 . 92E-02 351 . 92
- 37 . 20 5 . 18E-01 9 . 42£-02 RA-226 0 . 99 186 . 21
- 3 . 28 l.58E+OO 4 . 28E-01 AC-228 0 . 61 209 . 28 4 . 40 338 . 32
- 11. 40 3 . 81E- 01 l . 23E- 01 10/7/2020 Page 35
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 8:29:54PM Page4 of7 Analysis Report for L2-SUB-102-AJGS-001-SS SU: L2-011-102 RA CWD SOIL I PACKAGE: L2-SUB- 102 Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty AC-228 0 . 61 794 . 70 4 . 60 911 . 60
- 27 . 70 4 . 04£ - 01 1 . 07£-01 964 . 60 5 . 20 969 . 11
- 16 . 60 3 . 73E - 01 l . 45E - 01
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)
K- 40 1 . 000 S . 52E+OO 8 . SlE - 01 EU - 155 0 . 304 l . 33E-01 4 . 06E - 02 PB- 212 1 . 000 3 . 16£- 01 4 . 29E-02 BI - 214 0 . 873 4 . 75E-01 7 . 71E- 02 PB- 214 0 . 999 5 . 32E- 01 6 . SlE- 02 RA- 226 0 . 995 l . 58E+OO 4 . 28£ - 01 AC - 228 0 . 617 3 . 89E - 01 7 . 04 £ -02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 36
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 8:29:54PM Page 5 of7 Analysis Report for L2-SUB-102-AJGS-001-SS SU: L2-011-102 RA CWD SOIL/ PACKAGE: L2-SUB-102 UNIDENTIFIED PEAKS Peak Locate Perfonned on : 3/30/2018 8:29:45PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 1 74 . 73 5 . 64094E - 02 10 . 70 ?k-z. 1z-/z,,1f m 3 83 . 93 2 . 11411E-02 25 . 54 -(t./t:Z-~ m 5 92 . 87 4.50999E-02 11 . 96 Tol. PA-228 m B 241.74 3 . SSB0SE- 02 12 . 15 ?/J ,vt/ F 12 582 . 98 2 . 55405E- 02 13 . 58 1J. . zo'b F 18 1333 . 23 4.52470E - 03 36 . 07 lo .(£D M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{%) Activity Nuclide MDA UneMDA Name (pCl/grams) (pCilgrams) (pCl/grams) (keV)
+ K-40 1460 . 75
- 10 . 67 5 . 52E+00 8 . BSE-01 8 . BSE-01
+ AR-41 1293 . 64 99 . 16 2 . 31E - 01 1 . 34E+0O l . 34E+00
+ CO-60 1173 . 22 100 . 00 B. SlE- 02 8 . 45E-02/ 8 . 73E - 02 1332 . 49 100 . 00 -l . 74E-03 8 . 45E-02 KR-BS 513 . 99 0 . 43 l . 69E+0l 1. 53E+0l l . 53E+0l
+ Y-88 898 . 04 93.70 S.26E-02 4 . 69E-02 7.36E-02 1836 . 06 99 . 20 -1. 03E- 0l 4 . 69E- 02 10/7/2020 Page 37
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 8:29:54PM Page 6of7 Analysis Report for L2-SUB-102-AJGS-001-SS SU: L2-011-102 RA CWD SOIL I PACKAGE: L2-SUB-102 Nuclide Energy Yield(%) Activity Nuclide MDA LlneMDA Name (pCilgrams) (pCl/grams) (pCi/grams) (keV) NB-94 702 . 63 100 . 00 -l . 88E-02 6 . 13E-02 6 . 13E- 02 871 . 10 100 . 00 2 . 40£-02 6 . 64E-02
+ I - 131 284 . 30 6 . 06 l . 96E-01 6 . 36E-02 8 . 45E-01 3 64 . 4 8 81. 20 - 1 . 66£-02 6 . 36E-02 636 . 97 7 . 27 - 1 . 24£ - 01 8 . 59E - 01
+ CS -1 34 604 . 70 97 . 60 6 . 42£-04 7.68£-02 9 . 52E - 02 795 . 84 85.40 -7 . llE-02 7 . 68E-02
+ CS- 137 661 . 65 85 . 12 1 . 15E-01 8. 50E - 02 8 . 50E - 02
+ CE - 144 80 . 12 1. 36 2 . 90E+OO 4.12E-01 5 . 49E+OO 133 . 51 11 . 09 2 . 76E - 01 4 . 12E- 01
+ EU-152 121 . 78 28 . 40 - l . 04E - 01 1. 58E - 01 J 1 . 58E - 01 244 . 69 7 . 49 l . 32E - 02 8 . lOE - 01 964 . 00 14 . 44 5 . 03£ - 01 6 . 08£-01 1408.00 20 . 74 1. 09E - 02 4 . 00E-01
+ EU - 154 123 . 07 40 . 40 - 3 . 92E - 02 l . llE - 01 / l . llE-01 247 . 94 6.60 8.02E-02 7 . 94E - 01 723 . 30 19 . 70 6 . 37£- 02 3 . 38E - 01 873 . 20 11 . 50 3 .6 1E- 01 5 . 73E-01 1004 . 76 17 . 90 - 4 . 48E- 01 3 . 56E - 01 1274 . 51 35 . 50 l . 32E-01 l . 99E-01
+ EU-155 86 . 54
- 32 . 80 l . 33E- 01 l . OlE- 01 l.OlE-01 105 . 31 21. 80 4 . 53E-02 2 . 21E-01
+ BI-214 609 . 31
- 4 6 . 30 4 . 44E - 01 l . 39E-01 l . 39E-01 1120 . 29
- 15 .1 0 5 . 61E - 01 4 . 03E-01 1238 . 11
- 5 .94 8 . 67E-01 8 . 64E-01 1377 . 67 4 . 11 4.63E-01 l . 74E+OO 1407 . 98 2 . 48 9 . 15E-02 3 . 34E+OO 1509 . 19 2 .1 9 -4.27£-01 2 . 57E+OO 1764 . 49
- 15 . 80 4 . 24E-01 4.15E-0 1
+ PB-214 77 . 11
- 10.70 1 . 0lE+OO 1. 67£-01 3 . 91E-Ol 295 . 21
- 19 . 20 5 . 59E - 01 2 . 57E- 01 351 . 92
- 37 . 20 5 .1 8£-01 l . 67E - Ol
+ PA- 228 89 . 95 22.00 6 . 18E-01 2 . 04£-01 3 . 54E-01 93 . 35 35 .0 0 - 5 . 65E-02 2 .0 4E-01 105 . 00 16 . 30 1 . 53£-01 3 . 78E-01 129 . 22 2 . 97 4 . 61E-01 1 . 97E+OO 338 . 32 5 . 30 l . 03E+OO 1 . 27E+00 463.00 13 . 80 3 . 97£- 01 5 . 25E-01 911 . 23 16 . 70 5 . 69E-Ol 6 . 92E- 01
+ AM-241 59 . 54 36 .3 0 l . 62E- 01 3 .4 5E- 01 3 . 45E - 01
+ CM - 243 103 . 76 23 . 00 -3.68E-02 2 . lOE-01 2 . lOE-01 228 . 18 10 . 60 -1. 72£-01 4 . 44E - 01 277 . 60 14 . 00 -l . 04E-01 3 .6 0E-Ol
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ Half-life too short lo be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 38
LAC LTP - Final Status Survey Package - 3/21/2018 3/30/2018 8:29:54PM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-001 -SS SU : L2*011*102 RA CWD SOIL / PACKAGE: L2-SUB-102 10/7/2020 Page 39
LAC LTP - Final Status Survey Package - 3/21/2018 3/31/2018 12:08:29AM Page I of7 pex-Gamma Analysis Report for L2-SUB-102-AJGS-001-SB SU : LZ-011-102 RA CWD SOIL/ PACKAGE: L2-SUB-102 GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-001-SB / Sample Description : SU: L2-011-102 RA CWD SOIL / PACKAGE: L2-SUB-102 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 7.648E+02 grams / Facility : Dairyland_NPP Sample Taken On : 3/30/2018 1:29:00PM Acquisition Started : 3/30/2018 11 :08:06PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611 .1 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibratlon Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4186 PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/31 /2018 12:08:20AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 40
LAC LTP - Final Status Survey Package - 3/21/2018 3/31 /2018 12:08:29AM Page 2of7 Analysis Report for L2-SUB-102-AJGS-001-SB SU: L2-011 -1 02 RA CWD SOIL/ PACKAGE: L2-SUB-102 Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 76 . 36 147 - 161 153.26 5 . 55E+02 80 . 38 l . 92E+03 3 . 50 F 2 92 . 88 183 - 193 186 . 31 l . 49E+02 51 . 68 l . 35E+03 1. 55 F 3 186 . 10 367 - 380 372. 70 2 . 64E+02 51. 22 l . 18E 03 1. 69 F 4 209 . 32 416 - 423 419 . 14 4.79E+0l 31. 83 6 . 03E+02 1.09 M 5 238 . 57 473 - 488 477 . 61 5 . 97E+02 59 . 36 6 . 58E+02 1. 48 m 6 241. 73 473 - 488 483.93 2 . 17£+02 38.50 5 . 32£+02 1. 4 9 F 7 270 . 14 534 - 548 540 . 73 7 . 45E+0l 34 . 64 7 . 10E+02 1. 82 M 8 295 . 21 587 - 604 590 . 87 3 . 79E+02 47 . 53 3 . 51E+02 1. 53 m 9 300 . 31 587 - 604 601. 08 3 . 34E+0l 23 . 78 3 .40E+02 1. 53 F 10 327 . 77 652 - 659 655 . 98 4 . 57E+0l 25 . 36 2 . 61E+02 1. 33 E' 11 338 . 25 670 - 685 676 . 94 l . 30E+02 32 . 31 5 . 17E+02 1. 49 F 12 351 . 93 696 - 712 704 . 29 6.49E+02 57 . 27 4 . 82£+02 1. 67 f 13 583 . 13 1159 - 1173 1166 . 60 l . 76E+02 30 . 50 1 . 83£+02 1. 63 f 14 609 . 30 1213 - 1226 1218 . 92 4 . 50E+02 46 . 10 1 . 71£+02 1. 74 f 15 727 . 29 1447 - 1462 1454 . 88 6 . 90E+0l 21 . 33 1 . 28£+02 2.01 F 16 768 . 06 1529 - 1542 1536.39 4 . 17£+01 18 . 73 1 . 26£+02 1.85 F 17 786 . 10 1569 - 1578 1572 . 48 2.26£+01 15 . 20 8 . 38£+01 1. 49 F 18 911.15 1815 - 1830 1822 . 53 1 . 07£+02 24 . 67 1. 05E 02 2 . 33 F 19 969 . 13 1933 - 1944 1938 . 49 7 . 56£+01 22 . 37 l . 03E+02 2 . 11 F 20 1120 . 03 2234 - 2248 2240 . 25 1 . 00£+02 23 . 96 8.77£+01 2 . 50 F 21 1332 . 02 2658 - 2670 2664 . 18 2 . 87E+0l 14 . 77 5 .4 7£+01 2.10 F 22 1407 . 77 2811- 2820 2815 . 67 1 . 68£+01 10 . 64 l . 96E+0l 1. 97 F 23 1460 . 78 2913 - 2930 2921. 66 4 . 97£+02 45 . 26 3.51£+01 2 . 49 F 24 1764 . 37 3522 - 3536 3528 .8 2 7.58£+01 18 . 89 2 . 59E+0l 2 . 59 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 3/31/2018 12:08:20AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76 . 36 5.55£+02 80 . 38 5 . 55£+02 8 . 04E+0l F 2 92.88 1. 4 9E+02 51 . 68 1 . 49E+02 5 . 17£+01 F 3 186 . 10 2 . 64£+02 51 . 22 2 . 64E+02 5 . 12E+0l F 4 209 . 32 4 . 79£+01 31. 83 4 . 79E+0l 3 . 18E+0l M 5 238 . 57 5 . 97E+02 59 . 36 5.97£+02 5 . 94E+0l 10/7/2020 Page 41
LAC LTP - Final Status Survey Package - 3/21/2018 3/31/2018 12:08:29AM Page 3 of7 Analysis Report for L2-SUB-102-AJGS-001-SB SU: L2-011 -102 RA CW SOIL/ PACKAGE: L2-SUB-102 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. m 6 241 . 73 2 . 17E+02 38 . 50 2 . 17E+02 3 . 85E+Ol F 7 270 .14 7 . 45E+Ol 34 . 64 7 . 45E+Ol 3 . 46E+Ol M 8 295 . 21 3 . 79E+02 47 . 53 3 . 79E+02 4 . 75E+Ol m 9 300 . 31 3 . 34E+Ol 23 . 78 3 . 34E+Ol 2 . 38E+Ol F 10 327 . 77 4 . 57E+Ol 25 . 36 4 . 57E+Ol 2 . 54E+Ol F 11 338 . 25 l . 30E+02 32 . 31 1 . 30E+02 3 . 23E+Ol F 12 351 . 93 6 . 49E+02 57 . 27 8 . 36E+Ol 3 . 72E+Ol 5 . 65E+02 6 . 83E+Ol F 13 583 . 13 1. 76E 02 30 . 50 l . 76E+02 3 . 05E+Ol F 14 609 . 30 4 . SOE+02 4 6 . 10 4 . 12E+Ol 2 . 42E+Ol 4 . 09E+02 5 . 21E+Ol E' 15 727 . 29 6 . 90E+Ol 21. 33 6 . 90E+ Ol 2 . 13E+Ol F 16 768 . 06 4 . 17E+Ol 18 . 73 4 . 17E+Ol l . 87E+Ol F 17 786 . 10 2 . 26E+Ol 15 . 20 2 . 26E+Ol l . 52E+Ol F 18 911 . 15 l . 07E+02 24 . 67 1. 07E+02 2 . 47E+Ol F 19 969 . 13 7 . 56E+Ol 22 . 37 7 . 56E+Ol 2 . 24 E+Ol F 20 1120 . 03 l . OOE +02 23 . 96 l . OOE+02 2 . 40E+Ol F 21 1332 . 02 2 . 87E+Ol 14 . 77 2 . 87E+Ol 1.48E+Ol F 22 1407 . 77 l . 68E+Ol 10 . 64 l . 68E+Ol l . 06E +Ol F 23 1460 . 78 4 . 97E+02 45 . 26 5 . 63E+Ol 1 . 71E+Ol 4 . 41E+02 4 . 84E+Ol F 24 1764 . 37 7 . 58E+Ol 18 . 89 l . 52E+Ol 9 . 80E+OO 6 . 06E+Ol 2 . 13E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.D00sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 1.00 1460 . 75
- 10 . 67 6 . 28E+OO 7 . 72£ - 01 BI - 212 0 . 79 727 . 17
- 11 . 80 4 . 79E - 01 1. SOE-01 785 . 42
- 2 . 00 9 . 94E- 01 6 . 70E-01 1620 . 56 2 . 75 PB - 212 0 . 97 77 . 11
- 17 . 50 l . 04E+OO 1. 65E-01 238 . 63
- 44 . 60 4 . 03E - Ol 4 . 51E-02 BI - 21 4 0 . 82 609 . 31
- 4 6 . 30 6 . 16E- Ol 8 . 56E- 02 1120 . 29
- 15 . 10 7 . 99E- 01 1. 95E- 01 1238 . 11 5 . 94 1377 . 67 4 . 11 10/7/2020 Page 42
LAC LTP - Final Status Survey Package - 3/21/2018 3/31/2018 12:08:29AM Page 4 of 7 Analysis Report for L2-SUB-102-AJGS-001-SB SU : L2-011-102 RA CWD SOIL/ PACKAGE: L2-SUB-102 Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty BI - 214 0 . 82 1407 . 98 2 . 48 9 . 96E- 01 6 . 34E-01 1509 . 19 2 . 19 1764 . 49
- 15 . 80 6 . 83E- 01 2 . 44E - 01 PB-214 0 . 98 77 . 11
- 10 . 70 l . 70E+OO 2 . 69E-01 295 . 21 19 . 20 7 . 09£- 01 9 . 54£ - 02 351 . 92
- 37 . 20 6 . 39E- 01 8 . 32£ - 02 RA - 226 0 . 99 186 . 21
- 3 . 28 2 . 04E+OO 4 . llE- 01 AC - 228 0 . 78 209 . 28
- 4 . 40 2 . 97£ - 01 1 . 98E-01 338 . 32
- 11 . 40 4 . 63E-01 1 . 17E- 01 794 . 70 4 . 60 911. 60
- 27 . 70 3 . 89£ - 01 9 . lOE - 02 964 . 60 5 . 20 969 . 11
- 16 . 60 4 . 83E- 01 1. 4 5E-01
* = Energy line found in the spectrum.
* = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)
K- 40 1 . 000 6 . 28E+OO 7 . 72E-01 BI-212 0 . 792 5 . 04E - Ol 1 . 46£ - 01 PB-212 0 . 974 4 . 18£-01 4 . 36E - 02 BI - 214 0 . 821 6 . 53E- 01 7 . 41E- 02 PB- 214 0 . 986 6 . 87E- 01 6 . 12E- 02 RA- 226 0 . 998 2 . 04E+OO 4 . llE - 01 AC - 228 0 . 788 4 . 17£- 01 6 . 12E- 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 43
LAC LTP - Final Status Survey Package - 3/21/2018 3/31/2018 12:08:29AM Page 5 of7 Analysis Report for L2-SUB-102-AJGS-001-SB SU: L2-011-102 RA CWD SOIL/ PACKAGE: L2-SUB-102 UNIDENTIFIED PEAKS Peak Locate Performed on : 3/31/2018 12:08:20AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV} Peak Size (CPS) Uncertainty Type Nuclide F 2 92 . 88 4 .1 5039E-02 17 . 29 Tol. PA- 228 m 6 241.73 6 . 02860E-02 8 . 87 fb ,z.11/ F 7 270 . 14 2 . 06980E - 02 23 . 25 /-1--6 - i,z.8 m 9 300 . 31 9 . 27051E- 03 35 . 63 ~ -~J"Z-F 10 327 . 77 1 . 26958E- 02 27 . 74 Al- -t: -z:. 't, F 13 583 . 13 4 . 89037E- 02 8 . 66 Z,,~~ F 16 768 . 06 1 .1 5833E- 02 22 .4 5 'f,, - ~13/ F 21 1332 . 02 7 . 96927E-03 25 . 74 Tol. CO- 60 M = First peak in a multiplet reg ion m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide library Used : C:\Canberra\Ape x\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(3/4) Activity Nuclide MDA LlneMDA Name (pCi/grams) (pCilgrams) (pCilgrams) (keV}
+ K-40 1460 . 75
- 10 . 67 6 . 28E+00 6 . 78E-01 6 . 78E- 01
+
+
AR- 41 CO- 60 1293 . 64 1173 . 22 99 . 16 100 . 00
-1 . 44E+00 l . 64E- 02 2.86E+00 7 . 33E - 02 1 2 . 86E+00 7 . 33E- 02 10/7/2020 Page 44
LAC LTP - Final Status Survey Package - 3/21/2018 3/31/2018 12:08:29AM Page of7 Analysis Report for L2-SUB-102-AJGS-001-SB SU: L2-011-102 RA CWD SOIL/ PACKAGE: L2-SUB-102 Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV) CO-60 1332 . 49 100 . 00 1 . 08E-01 7 . 33E-02 7 . 42E-02
+ KR-85 513 . 99 0 . 43 3 . SSE+00 1.19E 01 l . 19E+0l
+ Y- 88 898 . 04 93.70 -l . 37E-03 4.74E-02 5 . 72E-02 1836 . 06 99.20 -7 . 12£-02 4 . 74£-02
+ NB- 94 702 . 63 100 . 00 -4 . 06£-02 5 . 05£-02 5 . 05E-02 871 . 10 100 . 00 - 4 . 23E- 02 5 . 57E - 02
+ I-131 284 . 30 6 . 06 4 . 97£-01 5 . 32E - 02 7 . 29E - 01 364 . 48 81.20 l . 38E-02 5 . 32E - 02 636 . 97 7 . 27 - 2 . 04E- 01 7 . 05E- 01
+ CS - 134 604 . 70 97 . 60 - 3 . 21E - 02 6 . 33E - 02 8 . 58£ - 02 795 . 84 85 . 40 -4 . 21£-02 / 6 . 33£-02
+ CS-137 661. 65 85.12 9 . 87E-02 6 . 81£ - 02 6 . 81E - 02
+ CE-144 80.12 1. 36 -2 . 0SE+0O 3 . 51E-01 4 . 77E+00 133. 51 11 . 09 6 . 38£-02 3 . 51E - 01
+ EU - 152 121 . 78 28 . 40 - l . 06E - 01 1. 34£-01 / l . 34E-01 244.69 7 . 49 -5 . 53£ - 01 7 . 18E- 01 964 . 00 14 . 44 8 . 21E- 01 5 . 29£- 01 1408 . 00 20 . 74 l . 51E-01 / 2 . 88E-01
+ EU-154 123.07 40.40 l . 70E-02 9 . 55E-02 9 . 55E-02 247 . 94 6 . 60 -8.24E-01 6 . 96E-01 723 . 30 19 . 70 5 . 17E- 02 2 . 98E - 01 873 . 20 11 . 50 - 9 . 98E- 02 4.94E - 01 1004 . 76 17 . 90 8 . 0lE-02 3 . 29£ - 01 1274 . 51 35 . 50 l . 23E-01 2.04E-01
+ EU - 155 86 . 54 32 . 80 - 8 . 17£-02 l . 60E-01 l . 60E-01 105 . 31 21. 80 -l . 80E-02 1 . 89E-01
+ BI-214 609 . 31
- 46 . 30 6 . 16E-01 1 . 06E-01 l . 06E - 01 1120 . 29
- 15 . 10 7 . 99E-01 3 . 1 7 E-01 1238 . 11 5 . 94 9 . 31£-01 l . 32E+00 1377 . 67 4 . 11 -2. llE-01 l . 48E+00 1407 . 98
- 2 . 48 9 . 96E-01 1 . 08E+00 1509 . 19 2 . 19 7 . 60E-01 2 . 70E+00 1764 . 49
- 15 . 80 6 . 83E- Ol 3 . 54E - 01
+ PB-214 77 . 11
- 10 . 70 l . 70E+00 1 . 20E-01 5.39E-01 295 . 21
- 19 . 20 7 . 09E - 01 l.20E - 01 351 . 92
- 37 . 20 6 . 39E-01 l . 31E-01
+ PA- 228 89.95 22 . 00 2 . 70E-02 l . 90E-01 3 . 28E-01 93 . 35 35 . 00 5 . 26£ - 02 1 . 90E- 01 105 . 00 16 . 30 1. 59E-01 3 . 49E-01 129 . 22 2 . 97 -3.58E-01 l . 79E+OO 338 . 32 5 . 30 1.73E+00 1.26E+00 463 . 00 13 . 80 -2.03E-01 4 . 60E-01 911 . 23 16 . 70 8 . 47E-01 5 . 89E-01
+ AM-241 59 . 54 36.30 2 . 29E-01 2.92E-0l 2.92E-01
+ CM-243 103 . 76 23 . 00 -l . 84E-02 1 .80E-01 l . 80E-0l 228 . 18 10 . 60 - 4 . 26E - 01 3 . 64E-01 277 . 60 14 . 00 - 7 . 0lE-02 3 . 09£-01 10/7/2020 Page 45
LAC LTP - Final Status Survey Package - 3/21/2018 3131/2018 12:08:29AM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-001-SB SU: L2-011-102 RACWD SOIL/ PACKAGE: L2-SUB-102
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able lo perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA al 95% confidence level 10/7/2020 Page 46
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 12:48:43PM Page I of pex-Gamma Analysis Report for L2-SUB-102-AJGS-002-SB 04/03/18 - 0830 L1.-01 ( - /oz_ R.,4 c.v-1u So; ( GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-002-SB / Sample Description : 04/03/18 - 0830 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 6.759E+02 grams Facility : Dairyland_NPP Sample Taken On : 4/3/2018 8:30:00AM Acquisition Started : 4/4/2018 11 :48:20AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611.8 seconds Dead Time : 0.33% Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100- 4096 Peak Area Range (in channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4207 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/4/2018 12:48:34PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 47
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 12:48:43PM Page 2 of Analysis Report for L2-SUB-102-AJGS-002-SB 04/03118 - 0830 Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) M 1 63 . 03 120 - 191 126 . 62 1 . 69E+02 51.01 1 . 67E+03 1. 76 m 2 67 . 31 120 - 191 135 . 18 l . 25E+02 42 . 39 l . 79E+03 1. 77 m 3 74 . 52 120 - 191 149 . 58 3 . 59E+02 56 . 27 1. 59E+03 1. 78 m 4 76 . 95 120 - 191 154 . 45 8 . 06E+02 79 . 74 1. 56E+03 1. 79 m 5 83 . 81 120 - 191 168 . 16 l . 68E+02 49 . 66 1 . 64Et03 1. 80 m 6 87 . 12 120 - 191 174 . 77 3 . 77E+02 68 . 85 l . 61E+03 1. 80 m 7 92 . 90 120 - 191 186 . 33 4 . 15E+02 60 . 92 l . 57E+03 1. 82 F 8 185 . 93 369 - 377 372 . 35 3 . 58E+02 57 . 07 l . 10E+03 1. 39 M 9 238 . 59 469 - 492 477 . 66 1 . 01E+03 72 . 90 7 . 47E+02 1. 57 m 10 241 . 72 4 69 - 492 483 . 92 4 . 62E+02 52 . 70 6 . 19E+02 1. 58 M 11 295 . 18 584 - 605 590 . 82 7 . 73E+02 65 . 69 5 . 98E+02 1. 63 m 12 300 . 13 584 - 605 600 . 70 7.46E+Ol 30.65 5 . 68E+02 1. 63 F 13 338 . 28 671 - 680 676 . 99 1 . 82E+02 38 . 31 4 . 70E+02 1. 44 F 14 351. 83 695 - 709 704 . 09 l . 24E+03 76 . 48 6 . 84E+02 1. 48 F 15 462 . 69 919 - 932 925 . 77 6 . 57E+Ol 26 . 05 3 . 24E+02 1. 67 F 16 510 . 53 1013 - 1028 1021.44 1 . 39E+02 35 . 17 3 . 84E+02 2 . 59 F 17 583 . 14 1162 - 1172 1166 . 61 2 . 56E+02 37 . 15 1 . 95E+02 1. 72 F 18 609 . 20 1211 - 1227 1218 . 73 8 . 99E+02 63 . 77 2 . 11E+02 1. 87 m 19 665 . 25 1318 - 1335 1330 . 82 3 . 68E+Ol 17 . 64 1. 25E+02 1. 75 F 20 727 . 38 1451 - 1464 1455 . 06 4 . 89E+Ol 21 . 77 2 . 17E+02 1. 57 F 21 768 . 35 1530 - 15 46 1536 . 98 9 . 05E+Ol 25 . 73 2 . 26E+02 2 . 03 F 22 910 . 95 1816 - 1831 1822 . 13 l . 98E+02 31.03 9 . 87E+Ol 2 . 21 F 23 968 . 99 1934 - 1945 1938 . 21 l . 01E+02 24 . 56 l . 27E+02 1. 58 F 24 1120 . 17 2232 - 2248 2240 . 53 l . 80E+02 30 . 19 l . 02E+02 2 . 64 F 25 1237 . 89 2469 - 2485 2475 . 95 7 . 63E+Ol 22 . 18 8 . 40E+Ol 3 . 62 F 26 1376 . 89 2747 - 2761 2753 . 91 5 . 51E+Ol 17 . 90 4 . SOE+Ol 2 . 85 F 27 1460 . 64 2911 - 2930 2921 . 39 3 . 31E+02 37 . 57 6 . 0lE+Ol 2 . 43 F 28 1764 . 15 3522 - 3536 3528 . 36 l . 28E+02 23 . 60 1 . 92E+Ol 2 . 49 F 29 1847 . 54 3691 - 3700 3695 . 15 1 . 40E+Ol 10.04 2 . 30E+Ol 1. 67 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/4/2018 12:48:34PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. 10/7/2020 Page 48
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 12:48:43PM Page 3 of 8 Analysis Report for L2-SUB-102-AJGS-002-SB 04/03/18 - 0830 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. M 1 63 . 03 1 . 69E+02 51.01 1 . 69E+02 5 .l OE+Ol m 2 67 . 31 1 . 25E+02 42 . 39 1. 25E+02 4 . 24E+Ol m 3 74 . 52 3 . 59E+02 56 . 27 3 . 59E+02 5 . 63E+Ol m 4 76 . 95 8 . 06E+02 79 . 74 8 . 06E+02 7 . 97E+Ol m 5 83 . 81 l . 68E+02 49 . 66 1 . 68E+02 4 . 97E +Ol m 6 87 . 12 3 . 77E+02 68 . 85 3 . 77E+02 6 . 88E+Ol m 7 92 . 90 4 . 15E+02 60 . 92 4 . 15E+02 6 . 09E+Ol F 8 185 . 93 3 . 58E+02 57 . 07 3 . 58E+02 5 . 71E+Ol M 9 238 . 59 1. 01E+03 72 . 90 1 . 01E+03 7 . 29E+Ol m 10 241 . 72 4 . 62E+02 52 . 70 4 . 62E+02 5 . 27E+Ol M 11 295 . 18 7 . 73E+02 65 . 69 7 . 73E+02 6 . 57E+Ol m 12 300 . 13 7 . 46E+Ol 30 . 65 7 .4 6E+Ol 3 . 06E+Ol F 13 338 . 28 l . 82E+02 38 . 31 1 . 82E+02 3 . 83E+Ol F 14 351 . 83 1. 24E+03 76 . 48 8 . 36E+Ol 3 . 72E+Ol l . 16E+03 8 . SlE+Ol F 15 462 . 69 6 . 57E+Ol 26 . 05 6 . 57E+Ol 2 . 61E+Ol F 16 510 . 53 l . 39E+02 35 . 17 7 . 28E+Ol 2 . 85E+Ol 6 . 59E+Ol 4 . 53E+Ol F 17 583 . 14 2 . 56E+02 37 . 15 2 . 56E+02 3 . 72E 01 F 18 609 . 20 8 . 99E+02 63 . 77 4. 12E+Ol 2 . 42E+Ol 8 . 58E+02 6 . 82E+Ol m 19 665 . 25 3 . 68E+Ol 17 . 64 3 . 68E+Ol 1 . 76E+Ol F 20 727 . 38 4 . 89E+Ol 21. 77 4 . 89E+Ol 2 . 18£+01 F 21 768 . 35 9 . 05E+Ol 25 . 73 9 . 05E+Ol 2 . 57E+Ol F 22 910 . 95 l . 98E+02 31. 03 l . 9 8 E+02 3 . lOE+Ol F 23 968 . 99 1 . 01E+02 24 . 56 l. 0 1 E+02 2 .4 6E+Ol F 24 1120 . 17 l . 80E+02 30 . 19 1 . 80E+02 3 . 02E+Ol F 25 1237 . 89 7 . 63E+Ol 22 . 18 7 . 63E+Ol 2 . 22E+Ol F 26 1376 . 89 5 . 51E+Ol 17 . 90 5 . SlE+Ol l . 79E+Ol F 27 14 60 . 6 4 3 . 31E+02 37 . 57 5 . 63E+Ol 1 . 71E+Ol 2 . 7 4E+02 4 . 13E+Ol F 28 176 4 . 15 l . 28E 02 23 . 60 1 . 52E+Ol 9 . 80E 00 1 . 13E+02 2 . 55E+Ol F 29 18 4 7 . 5 4 l . 40E+Ol 10 . 0 4 1 . 4 0E+Ol l . OOE+Ol
=
M First peak in a multiplet region
=
m Other peak in a multiplet region
=
F Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty 10/7/2020 Page 49
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 12:48:43PM Page 4 of8 Analysis Report for L2-SUB-102-AJGS-002-SB 04/03/18 - 0830 Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460 . 75
- 10 . 67 4 . 42E+OO 7 . 09E-Ol BI-212 0 . 60 727 . 17
- 11 . 80 3 . 84E-01 1. 72E-01 785 . 42 2 . 00 1620.56 2 . 75 PB - 212 0 . 99 77 . 11
- 17 . 50 l . 69E+OO 1 . 99E-01 238 . 63
- 44 . 60 7 . 71E - 01 6 . 84E- 02 BI - 214 0 . 92 609.31
- 4 6 . 30 1 . 46E+OO l . 42E - 01 1120 . 29
- 15 . 10 1 . 63E+00 2 . 83E - 01 1238 . 11
- 5 . 94 l . 91E+OO 5 . 65E-01 1377. 67
- 4 . 11 2 . 19E+OO 7 . 21E-01 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 l . 44E+OO 3 . 38E-Ol PB-214 0 . 99 77 . 11
- 10 . 70 2 . 76E+OO 3 . 26E-Ol 295 . 21
- 19 . 20 l . 64E+OO 1. 60E-01 351 . 92
- 37 . 20 l . 48E+OO l . 31E - 01 RA- 226 0 . 98 186 . 21
- 3 . 28 3 . 12E+OO 5 . 26E - 01 AC-228 0 . 60 209 . 28 4 . 40 338 . 32
- 11 . 40 7 . 32E - 01 l . 58E-01 794 . 70 4 . 60 911 . 60
- 27 . 70 8. llE-01 l . 32E-01 964 . 60 5 . 20 969 . 11
- 16 . 60 7 . 33E-01 l . SOE-01 PA- 228 0 . 30 89 . 95 22 . 00 93 . 35
- 35 . 00 8 . 21E - 01 3 . 17E-01 105 . 00 16 . 30 129 . 22 2 . 97 338 . 32
- 5 . 30 3 . 78E+OO l . 04E+OO 463.00 13 . 80 6 . 99E - 01 3 . 00E-01 911 . 23
- 16.70 3 . 23E+OO 7 . 00E-01
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index th reshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT 10/7/2020 Page 50
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 12:48:43PM Page 5 of8 Analysis Report for L2-SUB-102-AJGS-002-SB 04/03/18 - 0830 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) K- 40 0 . 998 4 . 42E+OO 7 . 09E- 01 BI - 212 0 . 600 3 . 84E-01 1 . 72E- 01 PB-212 0 . 999 7 . 68 £- 01 6 . SOE- 02 BI - 214 0 . 926 l . 52 E+OO l . lSE- 01 PB- 214 0 . 999 1 . 54E+OO 9 . 71E- 02 RA- 226 0 . 987 3 . 12£+00 5 . 26£- 01 AC - 228 0 . 605 6 . 31E- 01 9 . 07£- 02 PA- 228 0 . 307 7 . 90E- 01 l . 33E - 01
? = nuclide Is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 51
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 12:48:43PM Page 6 of 8 Analysis Report for L2-SUB-102-AJGS-002-SB 04103/ 18 - 0830 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/4/2018 12:48:34PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 1 63 . 03 4 . 69082E - 02 15 . 10 f1--~ zst/ m 2 67 . 31 3 . 46166E- 02 17 . 01 m 3 74 . 52 9 . 97472E- 02 7 . 84 ?J -i1z!-e ,,t *'1$ 1 m 5 83 . 81 4 . 66674E- 02 14 . 78 m 6 87 . 12 l . 04827E- 01 9 . 12
~ ,v11:,,fa1-I 'K/'1"/1 m 10 241 . 72 l . 28397E - 01 5 . 70 ?'t ,t,,.t/
m 12 300 . 13 2 . 07143E- 02 20 . 55
?z-t1 't.-
F 16 510 . 53 l . 83181E - 02 34 . 33 -r1 t,,8~ F 17 583 . 14 7 . 10529E- 02 7 . 26 '17- z:,ofJ m F 19 21 665 . 25 768 . 35 1 . 02274£- 2 . 51 44 8E-02 02 23 . 95 14 . 21
!: .-z.,141'
. z,1'7' F 29 1847 . 54 3 . 90008£ - 03 35 . 76 Sum M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB 10/7/2020 Page 52
LAC LTP - Final Status Survey Package - 3/21/2018 41412018 12:48:43PM Page? of8 Analysts Report for L2--SUB-102-AJGS-002-SB 04103/18 - 0830 Nuclide Energy Yield(3/4) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV}
+ K- 40 1460 . 75 10 . 67 4 . 42E+OO 8 . 57E- 01 8 . 57E - 01
+ AR- 41 1293 . 64 99 . 16 - 4 . 83E+02 2 . 90E+03 / 2 . 90E+03
+ C0- 60 1173 . 22 100 . 00 - 2 . 41E - 03 8 . 27E-02 8 . 27E- 02 1332 . 49 100 . 00 8 . 23E- 02 8 . 36E - 02
+ KR- 85 513 . 99 0 . 43 -4 . 29E+ OO 1 . 62E+Ol 1 . 62E+Ol
+ Y- 88 898 . 04 93 . 70 - 9 . lOE - 03 6 . 95£ - 02 7 . 88E- 02 1836 . 06 99 . 20 -4 . 4 4E- 02 6 . 95E- 02
+ NB - 94 702 . 63 100 . 00 - 2 . 29E - 02 6 . 73E - 02 6 . 73E- 02 871 . 10 100 . 00 -8 . 86E - 02 7 . 24E-02
+ I-131 284 . 30 6 . 06 9 . 49E- 02 7 . 37E - 02 9 . 8SE-Ol 364 . 48 81. 20 - 2 . 03E-0 3 7 . 37E-02 636 . 97 7 . 27 -7 . 73E - 02 9 . 34E-01
+ CS - 134 604 . 70 97 . 60 - 2 . 60E - 03 8 . 31E - 02 l . 28E - 01 795 . 84 85 . 40 -l . 18E- 01 / 8 . 31E-02
+ CS-137 661. 65 85 . 12 7 . 92E - 02 8 . 35E - 02 8 . 35E- 02
+ CE - 144 80 . 12 1. 36 7 . 93E+OO 4 . 53E - 01 6 . 4 9E+OO 133 . 51 11 . 09 - l . 08E - 01 4 . 53E - 01
+ EU - 152 121 . 78 28 . 40 - 8 . 06E - 02 1 . 73E - 01 ./ 1 . 7 3E - 01 244 . 69 7 . 49 - 5 . 12E- 02 1 . 00E+OO 964 . 00 14 . 44 - 5 . 4 6E - Ol 6 . 79E - 01 1408 . 00 20 . 74 l . BlE - 01 3 . 98E - 01
+ EU - 154 123 . 07 40 . 40 - 6 . 27E- 02 1 . 21E - 01 / 1 . 21E - 01 247 . 94 6 . 60 - 2 . 88E - 01 9 . 35E-Ol 723 . 30 19 . 70 - 1 . 84E - 01 3 . 90E - Ol 873 . 20 11 . 50 - 2 . 52E - 01 6 . 21E- 01 1004 . 76 17 . 90 9 . 66E- 02 4 . 06E - 01 1274 . 51 35 . 50 l . 51E - 01 2 . 29E - 01
+ EU - 155 86 . 54 32 . 80 - 4 . 81E - Ol 2 . 12E - 01 2 . 12E - 01 105 . 31 21. 80 -1 . 30E - 01 2 . 37E - 01
+ BI-214 609.31
- 46 . 30 1. 4 6E+OO 1 . 32E - 01 1. 32E-01 1120 . 29
- 15 . 10 l . 63E+OO 4 . 00E-01 1238 . 11 5 . 94 l . 91E+OO 1 . 02E+OO 1377 . 67
- 4 . 11 2 . 19E+OO l . l 6E+OO 1407 . 98 2 . 48 1. 52E+OO 3 . 32E+OO 1509 . 19 2 . 19 -3 . 92E-01 3 . 74E+OO 1764 . 49
- 15 . 80 l . 44E+OO 3 . 79E-01
+ PB-214 77 . 11
- 10 . 70 2 . 76E+OO 1 . 63E-Ol 4 . 53E-Ol 295 . 21
- 19 . 20 l . 64E+OO 1. 76E - 01 351 . 92
- 37 . 20 1. 48E+OO 1 . 63E - 01
+ PA - 228 89 . 95 22 . 00 2.12E+OO 2 . 63E - 01 7 . 60E - 01 93 . 35
- 35 . 00 8 . 21E- Ol 2 . 63E - 01 105 . 00 16 . 30 -1 . 27E- Ol 7 . 6SE- Ol 129 . 22 2 . 97 5 . 75E- 01 4 . 05E+OO 338 . 32
- 5 . 30 3 . 78E+OO l . 63E+OO 463 . 00
- 13 . 80 6 . 99E - 01 7 . 71E - 01 911 . 23
- 16 . 70 3 . 23E+OO 6 . 9 4E- 01
+ AM-241 59 . 54 36 . 30 -1 . 97E - 02 3 . 75E- 01 3 . 75E - 01 + CM- 243 103 . 76 23 . 00 2 . 00E-01 2 . 30E-01 2 . 30E-01 228 . 18 10 . 60 - 3 . 04E - 01 4 . 78E- 01 10/7/2020 Page 53
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 12:48:43PM Page ofS Analysis Report for L2-SUB-102-AJGS-002-SB 04/03/18 - 0830 Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCi/grams) (pCi/grams) (keV) CM- 243 277 . 60 14 . 00 - 9 . 92E - 02 2 . 30E- 01 4. 00E - 01
+ = Nuclide identified during the nuclide Identification
= Energy line found ln the spectrum
> = MDA value not calculated
@ Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is Inconsistent w ith Currie MDA at 95% confidence level 10/7/2020 Page 54
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 1:51 :14PM Page I of7 pex-Gamma Analysis Report for L2-SUB-102-AJGS-003-SB 04/03/18 - 0850 L 1-- Dtl ---(<Y2.. iA Cv-> D $07 l GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-003-SB / Sample Description : 04/03/18 - 0850 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 7 .338E+02 grams Facility : Dairyland_NPP Sample Taken On : 4/3/2018 8:50:00AM Acquisition Started : 4/4/2018 12:50:51 PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611 .3 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4208 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/4/2018 1:51:05PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 55
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 1:51 :14PM Page 2 of7 Analysis Report for L2-SUB-102-AJGS-003-SB 04/03/18 - 0850 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 77 . 06 147 - 161 154 . 66 3 . 42E+02 58 . 54 l.90E+03 1. 48 M 2 87 . 27 171- 192 175 . 09 l. l 9E+02 46 . 57 l . 12E+03 1. 64 m 3 92 . 82 171- 192 186 . 17 2.20E+02 51. 67 l . 15E+03 1. 65 F 4 186 . 06 368 - 376 372 . 61 l . 66E+02 43 . 36 8 . 02E+02 1. 23 M 5 238 . 57 4 69 - 491 477 . 62 5 . 54E+02 56 . 22 6 . 06E+02 1. 56 m 6 241. 73 469 - 4 91 483 . 93 2 . 19E+02 37 . 63 4 . 44E+02 1. 56 F 7 270 . 08 534 - 545 540 . 63 5 . 86E+Ol 27 . 46 4 . 92E+02 1.19 M 8 2 95 . 16 585 - 608 590 . 78 3 . 43E+02 44 . 81 3 . 54E+02 1. 64 m 9 300 . 24 585 - 608 600 . 92 6 . 02E+Ol 24 . 77 3 . 34E+02 1. 64 F 10 338 . 35 650 - 682 677 . 13 9 . 75E+Ol 31. 48 l . 14E+03 1.53 F 11 351. 83 695 - 712 704 . 09 6 . 66E+02 57 . 00 4 . 35E+02 1. 69 F 12 583 . 04 1161 - 1173 1166 . 43 l . 61E+02 30 . 04 l . 79E+02 1. 66 F 13 609 . 25 1214 - 1227 1218 . 83 4 . 76E+02 47 . 81 l . 85E+02 1. 65 F 14 727 . 51 1451 - 1461 1455 . 31 3 . 44E+Ol 16 . 56 1. 20E+02 1.14 F 15 768 . 59 1533 - 1542 1537 . 47 3 . 24E+Ol 17 . 70 1. 08E+02 1. 58 F 16 911 . 05 1816 - 1830 1822 . 34 9 . 14E+Ol 22 . 65 8 . 57E+Ol 2 . 22 F 17 968 . 93 1933 - 1942 1938 . 09 4 . 75E+Ol 18 . 67 l . 11E+02 1. 38 F 18 1120 . 35 2233 - 2250 2240 . 89 8 . 22E+Ol 22 . 82 l . 17E+02 2 . 68 F 19 1460 . 67 2913 - 2931 2921 . 45 3 . 97E+02 40 . 50 2 . 94E+Ol 2 . 44 F 20 1764 . 59 3523 - 3536 3529 . 25 5 .4 0E+Ol 15 . 46 l . OlE+Ol 2 . 85 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/4/2018 1:51 :05PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. {keV) Area Uncertainty Background Uncert. Area Uncert. F 1 77 . 06 3 . 42E+02 58 . 5 4 3 . 42E+02 5 . 85E+Ol M 2 87 . 27 l . 19E+02 46 . 57 1 . 19E+02 4 . 66E+Ol m 3 92 . 82 2 . 20E+02 51. 67 2 . 20E+02 5 . 17E+Ol F 4 186 . 06 1 . 66E+02 43 . 36 l . 66E+02 4 . 34E+Ol M 5 238 . 57 5 . 54E+02 56 . 22 5 . 54E+02 5 . 62E+Ol m 6 241 . 73 2 . 19E+02 37 . 63 2 . 19E+02 3 . 76E+Ol F 7 270 . 08 5 . 86E+01 27 . 46 5 . 86E+01 2 . 75E+Ol M 8 295 . 16 3 . 43E+02 44 . 81 3 . 43E+02 4 . 48E+Ol m 9 300 . 24 6 . 02E+Ol 24 . 77 6 . 02E+Ol 2 . 48E+Ol 10/7/2020 Page 56
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 1:51 :14PM Page 3 of7 Analysis Report for L2-SUB-102-AJGS-003-SB 04/03/1 8 - 0850 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 10 338 . 35 9 . 75E+Ol 31. 48 9 . 75E+Ol 3 . 15E+Ol F 11 351 . 83 6 . 66E+02 57 . 00 8 . 36E+Ol 3 . 72E+Ol 5 . 82E+02 6 . 81E+Ol F 12 583 . 04 l . 61E+02 30 . 04 1 . 61E+02 3 . 00E+Ol F 13 609 . 25 4 . 76E+02 47 . 81 4 . 12E+Ol 2 . 42E+Ol 4 . 35E+02 5 . 36E+Ol F 14 727 . 51 3 . 44E+Ol 16 . 56 3 . 44 E+Ol 1. 66E+Ol F 15 768 . 59 3 . 24E+Ol 17 . 70 3 . 24E+Ol l . 77E+Ol F 16 911 . 05 9 . 14E+Ol 22 . 65 9 . 14E+Ol 2 . 27E+Ol F 17 968 . 93 4 . 75E+Ol 18 . 67 4 . 75E+Ol l . 87E+Ol F 18 1120 . 35 8 . 22E+Ol 22 . 82 8 . 22E +Ol 2 . 28E+Ol F 19 1460 . 67 3 . 97E+02 40 . 50 5 . 63E+Ol 1 . 71E+Ol 3 . 41E+02 4 . 40E+Ol F 20 1764 . 59 5 .4 0E+Ol 15 . 46 l . 52E+Ol 9 - 80E+OO 3 . 88E+Ol 1. 83E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0 . 99 1460 . 75
- 10 . 67 5 . 06E+OO 7 . llE- 01 BI - 212 0 . 59 727 . 17
- 11 . 80 2 . 49E- 01 1 . 21E-01 785.42 2 . 00 1620 . 56 2 . 75 PB - 212 1.00 77 . 11 17 . 50 6 . 57E - 01 1. 20E - 01 238 . 63
- 44 . 60 3 . 90E - 01 4 . 44E - 02 BI - 214 0 . 78 609 . 31
- 46 . 30 6 . 83E - 01 9 . 23E- 02 1120 . 29
- 15 . 10 6 . 85E-01 l . 93E-01 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49
- 15 . 80 4 . 56E - 01 2 . 17E- 01 PB-214 0 . 99 77 . 11
- 10 . 70 1 . 07E+OO l . 97E - 01 295 . 21
- 19 . 20 6 . 69E- 01 9 . 32E - 02 351 . 92
- 37 . 20 6 . 85E - 01 8 . 69E-02 RA- 226 0 . 99 186 . 21
- 3 . 28 1. 34E+OO 3 . 56E - 01 AC - 228 0 . 61 209 . 28 4 . 40 10/7/2020 Page 57
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 1:51 :14PM Pagc4 of7 Analysis Report for L2-SUB-102-AJGS-003-SB 04/03/18 - 0850 Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty AC-228 0 . 61 338 . 32
- 11 . 40 3 . 62E- 01 l . 18E- 01 794 . 70 4 . 60 911 . 60 27 . 70 3 . 45E- 01 8 . 69E - 02 96 4. 60 5 . 20 969 . 11 16 . 60 3 . 16E- 01 1. 25E - 01
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty
{pCilgrams) K- 40 0 . 999 5 . 06E+OO 7 . llE - 01 BI - 212 0.593 2 . 4 9E - 01 1 . 21E - 01 PB-212 1. 000 3 . 73E - 01 4 . 18E - 02 BI - 214 0 . 787 6 . 54E - 01 7 . 77E - 02 PB-214 0 . 999 6 . 58E - 01 6 . 0SE - 02 RA- 226 0.996 l . 34E+OO 3 . 56E-Ol AC - 228 0 . 613 3 . 43E - 01 6 . llE - 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 58
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 1:51 :14PM Page 5 of7 Analysis Report for L2-SUB-102-AJGS-003-SB 04/03/18 - 0850 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/4/2018 1:51:0SPM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(3/4) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 2 87 . 27 3 . 30402£-02 19 . 58 Tol. EU-155 m 3 92 . 82 6 . 11015E-02 11 . 74 Tol. PA- 228 m 6 241 . 73 6 . 07829E - 02 8 . 60 11; --ui/ Ac:--- v i-~ F 7 270 . 08 1 . 62640E-02 23 . 45 m 9 300 . 24 1 . 67185E-02 20 . 58 r1 .,z,, "t-F 12 583 . 04 4 . 46736£ - 02 9 . 34
--r7,z.0B F 15 768 . 59 9 . 00247£- 03 27 . 31 3, - z1~
M == First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(3/4) Activity Nucllde MDA LlneMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV)
+ K- 40 1460 . 75
- 10 . 67 5 . 06E+OO 6 . 97E-01 6 . 97E -0 1
+ AR-41 1293 . 64 99 . 16 1 . 63E+03 3 . 22E+03 3 . 22E+03 10/7/2020 Page 59
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 1:51:1 4PM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-003-SB 04/03/18 - 0850 Nuclide Energy Yield{%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams) {keV)
+ CO-60 1173 . 22 100 . 00 -6 . 59E-03 6 . 86£-02 7 . 28£ - 02 1332 .4 9 100 . 00 3 . 42E- 02 6 . 86E-02
+ KR-85 513 . 99 0 . 43 l . 48E+0l 1 . 27E+0l 1 . 27E+0l
+ Y-88 898 . 04 93 . 70 1. 43E-02 5 . 41E-02 6 . 31E-02 1836 . 06 99 . 20 - 2 . 34E - 02 5 . 41E-02
+ NB - 94 702 . 63 100 .0 0 7 . 20E - 03 5 . 26E-02 5 . 26E-02 871 . 10 100.00 -1.89E-02 5 . 87E - 02
+ I - 131 284 . 30 6 . 06 -1. 33E - 02 5 . 50E - 02 7 . 33E - 01 364 . 48 81. 20 7 . 60£ - 03 5 . 50E - 02 636 . 97 7.27 3 . 18E- 01 6 . 91E - 01
+ CS - 134 604 . 70 97 . 60 -l . 30E - 01 6 . 17E- 02 9 . 21E - 02 795 . 84 85 . 40 -5 . 73E - 02 6 . 17E- 02
+ CS-137 661 . 65 85 . 12 7 . 78E - 02 6 . 67E-02 ,r 6 . 67E - 02
+ CE-144 80 . 12 1. 36 -4 . 66E-01 3.55E-01 4 . 79E+00 133 . 51 11 . 09 - 9 . 76E- 02 3 . SSE-01
+ EU-152 121 . 78 28 . 40 3 . 72E- 03 1.40E-01 J l.40E-01 244 . 69 7 . 49 2 . 88E - 02 7 . 17E-01 964 . 00 14 . 44 5 . 79E - 01 5 . 30E - 01 1408 . 00 20 . 74 9 . 81E-02 2 . 91E- 0l EU-154 123 . 07 40 . 40 - 6 . 82E - 02 9 . 77E-02 j 9. 77E-02 247 . 94 6 . 60 1 . 30E - 01 6 . 86E- 01 723. 30 19 . 70 2.13E - 01 2 . 90E-01 873 . 20 11 . 50 - 8 . 25E - 02 5 . 0lE-01 1004 . 76 17 . 90 l . 98E - 01 3 . 64E-0l 1274 .5 1 35 . 50 - 4 . 06E - 02 1. 76E-01
+ EU-155 86 . 54 32 . 80 - l . 74E-02 l . 64E - 01 1 . 64E-0l 105 . 31 21. 80 - l . 02E - 01 1.84E-01
+ BI-214 609 . 31
- 46.30 6 . 83E - 01 l.14E-01 l.14E-01 1120 . 29
- 15 . 10 6 . 85E-01 4 . 02E- 01 1238.11 5 . 94 9 . 54E - 0l l . 28E+00 1377 . 67 4 . 11 1. 44E+00 l . 74E+00 1407 . 98 2 . 48 8 . 20E-01 2 . 44E+00 1509 . 19 2 . 19 6 . 59E-01 2 . 50E+00 1764 . 4 9
- 15 . 80 4 . 56E-Ol 3 . 13E- 0l
+ PB-214 77 . 11
- 10 . 70 l . 07E+00 l.26E-01 5 . S0E-01 295 . 21
- 19 . 20 6.69E - 01 1. 26E-01 351 . 92
- 37 . 20 6 . 85E - 01 l . 34E-01
+ PA-228 89 . 95 22 . 00 -3 . 92E-02 3 . 45E-01 5 . 93E-0l 93.35 35 . 00 -7 . 15E-03 3 . 45E - 01 105 . 00 16 . 30 -2.99E-01 6 . 04E-01 129 . 22 2 . 97 1. 28E+00 3 . 30E+00 338 . 32 5 . 30 l . 24E-01 2 . 26E+00 463 . 00 13 . 80 -6.24E-01 8 . 33E-01 911 . 23 16 . 70 1.29E+00 1 . 07E+00
+ AM-241 59 . 54 36 . 30 l . 48E - 01 2 . 94E- 01 2 . 94E - 01
+ CM-243 103 . 76 23 . 00 3 . 41E-02 1 . 77E-01 1 . 77E - 01 228 . 18 10 . 60 1 . llE-01 3 . 70E- 01 277 . 60 14 .0 0 -1.80E-01 2 . 96E - 01 10/7/2020 Page 60
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 1:51 :14PM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-003-S8 04/03/18 - 0850
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION : MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 61
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 4:59:23PM Page I of7
~pex-Gamma Analysis Report for L2-SUB-102-AJGS-004-SB 04/03/ 18 - 0908
~ '2- - o, , -t o ""2- r2-A
(>.,JD ~o; ( GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-004-SB / Sample Description : 04/03/18 - 0908 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 8.373E+02 grams Facility : Dairyland_NPP Sample Taken On : 4/3/2018 9:08:00AM Acquisition Started : 4/4/2018 3:58:57PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611 .1 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4096 Peak Area Range {in channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4213 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/4/2018 4:59:11PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 62
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 4:59:23PM Page 2 of7 Analysis Report for L2--SUB-102-AJGS-004-SB 04/03/18 - 0908 Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) M 1 76 . 29 147 - 192 153 . 13 4 . 20E+02 57.02 1 . 92E+03 3 . 37 m 2 87 . 98 147 - 192 176 . 51 l.12E+02 40 . 20 2 . 05E+03 3 . 37 m 3 92 . 69 147 - 192 185 . 91 2 . 18E+02 44 . 50 1 . 66E+03 3 . 36 F 4 185 . 89 368 - 378 372 . 27 l . 43E+02 41 . 68 8 . 10E+02 1. 49 M 5 238 . 53 470 - 492 477 . 54 5 . 12E+02 55 . 14 5 . 45E+02 1. 72 m 6 241. 77 470 - 492 484 . 02 l . 67E+02 35 . 44 5 . 35E+02 1. 72 F 7 270 . 24 532 - 548 540 . 93 6 . 25E+Ol 28 . 30 5 . 81E+02 1. 53 F 8 295 . 06 584 - 596 590 . 57 2 . 52E+02 40 . 04 4 . 78E+02 1. 44 F 9 338 . 45 673 - 685 677 . 34 l . 02E+02 30 . 72 3 . 65E+02 1. 87 F 10 351. 90 698 - 710 704 . 23 3 . 94E+02 46 . 53 3 . 65E+02 1.56 F 11 583 . 23 1160 - 1175 1166 . 80 l . 38E+02 28 . 24 l . 68E+02 1. 97 F 12 609 . 26 1212 - 1225 1218 . 86 3 . 14E+02 38 . 55 1. 4 7E+02 1. 76 F 13 727 . 18 1451 - 1459 1454 . 65 2 . 97E+Ol 16 . 37 7 . 46E+Ol 1. 84 F 14 911 . 11 1816 - 1828 1822 . 46 6 . 69E+Ol 20 . 04 1. 01E+02 1. 52 F 15 969 . 05 1934 - 19 4 5 1938 . 32 6 . 62E+Ol 19 . 24 6 . 37E+Ol 1. 65 F 16 1017 . 76 2031 - 2040 2035 . 73 l . 44E+Ol 8 . 99 3 . 05E+Ol 0 . 75 F 17 1120 . 13 2234 - 2245 2240 . 45 6 . 99E+Ol 18 . 88 4 . 19E+Ol 1. 76 F 18 1460 . 78 2911 - 2930 2921 . 67 4 . 39E+02 42 . 77 5 . 58E+Ol 2 . 30 F 19 1764 . 19 3522 - 3537 3528 . 46 4 . 05E+Ol 13 . 91 2 . 05E+Ol 1. 98 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/4/2018 4:59:11PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. M 1 76 . 29 4 . 20E+02 57 . 02 4 . 20E+02 5 . 70E+Ol m 2 87 . 98 l . 12E+02 40 . 20 1 . 12E+02 4 . 02E+Ol m 3 92 . 69 2 . 18E+02 44 . 50 2 . 18E+02 4 . 45E +Ol F 4 185 . 89 1. 4 3E+02 41. 68 l.43E+02 4 . 17E+Ol M 5 238 . 53 5 . 12E+02 55 . 14 5 . 12E+02 5 . SlE+Ol m 6 241 . 77 l . 67E+02 35 . 44 l . 67E+02 3 . 54E+Ol F 7 270 . 24 6 . 25E+Ol 28 . 30 6 . 25E+Ol 2 . 83E+Ol F 8 295 . 06 2 . 52E+02 40 . 04 2 . 52E+02 4. 00E+Ol F 9 338 . 45 l . 02E+02 30 . 72 l . 02E+02 3 . 07E+Ol F 10 351. 90 3 . 94E+02 4 6 . 53 8 . 36E+Ol 3 . 72E+Ol 3 . 10E+02 5 . 96E+Ol 10/7/2020 Page 63
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 4:59:23PM Page 3 of7 Analysis Report for l2-SUB-102-AJGS-004-SB 04/0311 8 - 0908 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 11 583 . 23 l . 38E+02 28 . 24 1 . 38E+02 2 . 82E+Ol F 12 609 . 26 3 . 14 E+02 38 . 55 4 . 12E+Ol 2 . 42E+Ol 2 . 73E+02 4 . 55E+ Ol F 13 727 . 18 2 . 97E+Ol 1 6. 37 2 . 97E+O l l . 64E+O l F 14 911 . 11 6 . 69E+Ol 20 . 04 6 . 69E+Ol 2 . 00E+Ol F 15 969 . 05 6 . 62E+Ol 19 . 24 6 . 62E+Ol 1 . 92E+Ol F 16 1017 . 76 1 . 44 E+Ol 8 . 99 1 . 44E+Ol 8 . 99E+OO F 17 1120 . 13 6 . 99E+Ol 1 8 . 88 6 . 99E+Ol 1 . 8 9E+Ol F 18 1460 . 78 4 . 39E+02 42 . 77 5 . 63E+Ol 1 . 71E+O l 3 . 83E+02 4. 61E+Ol F 19 1764 . 19 4 . 05E+Ol 13 . 91 l . 52E+Ol 9 . 80E+OO 2 . 54E+Ol l . 7 0E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted al 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\H OTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 1.00 1460 . 75
- 10 . 67 4 . 98E+OO 6 . 60E- 01 B1 - 212 0 . 60 727 . 17
- 11. 80 l . 88E- 01 1 . 04E- 01 785 . 42 2 . 00 1620 . 56 2 . 75 PB - 212 0 . 96 77 . 11
- 17 . 50 7 . 19E- 01 l . 08E - 01 238 . 63
- 44 . 60 3 . 1 5E - 01 3 . 77E- 02 BI - 214 0 . 78 609 . 31
- 46 . 30 3 . 75E- 01 6 . 60E - 02 1120 . 29 15 . 10 5 . llE- 01 l . 40E-01 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 4 9 15 . 80 2 . 61E - 01 1 . 76E - 01 PB- 2 1 4 0 . 98 77 . 11
- 10 . 70 l . 18E+OO l . 77E - 01 295 . 21
- 19 . 20 4 . 31E - 01 7 . 16E- 02 351 . 92
- 37 . 20 3 . 20E - 01 6 . 34E-02 RA- 226 0 . 98 186 . 21
- 3 . 28 l . OlE+OO 2 . 99E- 01 AC - 228 0 . 61 209 . 28 4 . 40 338 . 32
- 11 . 40 3 . 30E - 01 l.OlE -0 1 794 . 70 4 . 60 10/7/2020 Page 64
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 4:59:23PM Page 4 of7 Analysis Report for L2-SUB-102-AJG S-004-SB 04/03/18 - 0908 Nuclide Id Energy Yield(%) Activity Activity Name Confidence {keV) (pCilgrams) Uncertainty AC - 228 0 . 61 911 . 60
- 27 . 70 2 . 21E- 01 6 . 70E-02 964 . 60 5 . 20 969 . 11
- 16 . 60 3 . 87E- Ol l . 14E-01
* = Energy line found in the spectrum .
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
K- 40 1.000 4 . 98E+OO 6 . 60E - 01 BI - 212 0 . 605 l . 88E - 01 1. 04E-01 PB - 212 0 . 969 3 . 33E - 01 3 . 57E-02 BI - 214 0 . 785 3 . 86E - 01 5 . 65E - 02 PB-214 0 . 982 3 . 86E- 01 4 . 60E- 02 RA- 226 0 . 983 l . OlE+OO 2 . 99E - 01 AC - 228 0 . 617 2 . SOE - 01 5 . 0lE - 02
? = nuclide is part of an undetermined solution X nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted al 2.000sigma 10/7/2020 Page 65
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 4:59:23PM Page5 of7 Analysis Report for l2-SUB-102-AJGS-004-SB 04/03/18- 0908 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/4/2018 4:59:11 PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 2 87 . 98 3 . 09813E- 02 18 . 02 m 3 92 . 69 6 . 04395E-02 10 . 23 Tel. PA-228 m 6 241 . 77 4.64670E-02 10 . 59 7l;'t-nl F 7 270 . 24 1 . 73749E-02 22 . 63 Ac--.,z:,~ F 11 583 . 23 3 . 84281E- 02 10 . 21 --rr t"~ F 16 1017 . 76 4 . 00768E - 03 31.15 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams) {keV)
+ K-40 1460 . 75 10 . 67 4 . 98E+O0 6.83E-01 6 . 83E-01
+ AR-41 1293.64 99.16 - 4.78E+03 8 .42E+03 8 . 42E+03
+ CO-60 1173 . 22 100 . 00 - 3 . 00E - 02 5 . 24E-02 / 6 . 09E- 02 1332 .4 9 100 . 00 1. 15E-02 5 . 24E-02 10/7/2020 Page 66
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 4:59:23PM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-004-SB 04/03/1 B - 0908 Nuclide Energy Yield(%} Activity Nuclide MDA LineMDA Name (pCilgrams) (pCilgrams) (pCi/grams) (keV)
+ KR-85 513 . 99 0 . 43 l . 40E+Ol 1 . 0SE+Ol 1. OSE+Ol
+ Y-88 898 . 04 93 . 70 -1.02E-02 3 . 44E - 02 5 . 21E - 02 1836 . 06 99 . 20 -2.12E-02 3 . 44E-02
+ NB-94 702 . 63 100 . 00 2 . 54E-03 4 . 36E-02 4 . 36E-02 871 . 10 100 . 00 2 . 59E-02 4 . 97E-02
+ I - 131 284 . 30 6 . 06 7 . 17E-01 4 . 63E-02 6 . 49E-01 364 . 48 81. 20 - 2 . 86E-02 4 . 63E-02 636 . 97 7 . 27 -1.69E-01 6 . 30E-01
+ CS - 134 604 . 70 97 . 60 6.60E-03 5 .4 0E - 02 6 . 76E-02 795 . 84 85 . 40 -1 . 12E- 02 / 5 . 40E-02
+ CS - 137 661 . 65 85 . 12 7 . 30E-02 6 . 07E-02 6 . 07E-02
+ CE-144 80 . 12 1. 36 6 . 56E+00 2 . 96E - 01 4 . 02E+00 133 . 51 11.09 -4.lOE-02 2 . 96E-01
+ EU-152 121 . 78 28 . 40 -7.30E-02 1 . 14E- 01 / l . 14E- 01 244 . 69 7 . 49 -2 . 12E-02 5 . 92E-01 964 . 00 14 . 44 -3.79E-01 4 . 33E - 01 1408 . 00 20 . 74 1 . 98E-01 2 . 61E - 01
+ EU-154 123 . 07 40 . 4 0 -6 . 47E- 03 8 . llE - 02 / 8 . llE - 02 247 . 94 6.60 -8.60E-02 5 . 82E- 01 723 . 30 19 . 70 -l . 64E-02 2 . 33E-01 873 . 20 11 . 50 -l . OlE-01 4 . 22E-01 1004 . 76 1 7 . 90 2 . 98E - 01 2 . 88E-01 1274 . 51 35 . 50 8 . 92E - 02 1 . 73E-01
+ EU - 155 86 . 54 32 . 80 -1.57E-01 l . 33E-01 1 . 33E-01 105 . 31 21 . 80 - 4 . 66E - 02 1. SSE - 01
+ BI-214 609 . 31
- 46 . 30 3 . 75E - 01 9 . 31E - 02 9 . 31E- 02 1120 . 29
- 15 . 1 0 5 . llE- 01 l . 94E-0 1 1238 . 11 5 . 94 1 . 65E + OO 1 . 23E+OO 1377 . 67 4 . 11 4 . 13E- 01 1.26E+OO 1407 . 98 2 . 48 1 . 65E+OO 2 . 18E+OO 1509 . 19 2 . 19 1 . 44E+OO 2 . 17E+OO 1764 .4 9
- 15 . 80 2 . 61E - 01 3 . 13E- 01 PB- 214 77 . 11
- 10 . 70 l.18E+OO l . 05E-Ol 4 . llE-01 295 . 21
- 19 . 20 4 . 31E - 01 l.45E - 01 351 . 92
- 37 . 20 3 . 20E - 01 l . OSE-01
+ PA-228 89 . 95 22.00 6 . 20E-01 3.09E-01 5 . 24E-01 93 .3 5 35 . 00 - l . 34E - 02 3.09E-01 105 . 00 16 . 30 -l.lOE-01 5 . 56E-01 129 . 22 2 . 97 -l . llE-01 2 . 98E+OO 338 . 32 5 . 30 l . 40E+OO 2 . 00E+OO 463 . 00 13 . 80 3 . 66E-01 7 . 77E-01 911. 23 16.70 l . 26E+OO 9 . 98E-Ol
+ AM-241 59 . 54 36 . 30 2 . 27E-01 2 . 4 6E-01 2 . 46E-01
+ CM-243 103 . 76 23 . 00 -l.34E-02 l .48 E- 01 l.48E-01 228 . 18 10 . 60 - 8 . 22E - 02 3 . lSE - 01 277 . 60 14.00 7 . 06E-03 2 . 52E-01 10/7/2020 Page 67
LAC LTP - Final Status Survey Package - 3/21/2018 4/4/2018 4:59:23PM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-004-S8 04/03/18 - 0908
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION : MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 68
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 6:25:12AM Page I of6 pex-Gamma Analysis Report for L2-SUB-102-AJGS-005-SB 04/03/18- 1443 L2.-v11-<02- RA_ c_µ.:, j:) So; { GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-005-SB Sample Description : 04/03/18-1443 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 1.061 E+03 grams / Facility : Dairyland_NPP Sample Taken On : 413/2018 2:43:00PM Acquisition Started : 4/5/2018 5:24:50AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3610.8 seconds Dead Time : 0.30 % Peak Locate Threshold : 3.00 Peak locate Range (in channels) : 100- 4096 Peak Area Range (in channels) : 100- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/812014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4215 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/5/2018 6:25:03AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 69
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/20 18 6:25:12AM Page 2 of6 Analysis Report for L2-SUB-102-AJGS-005-SB 04/03/18 - 1443 Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 77 . 05 147 - 161 154 . 65 l . 30E+02 42 . 28 1 . 37E+03 1. 35 F 2 185 . 94 368 - 376 372 . 37 3 . 99£ +01 26 . 53 5 . 23E+02 0 . 86 M 3 238 . 55 473 - 490 477 . 57 3 . 25E+02 44 . 15 3 . 56E+02 1. 36 m 4 241. 52 473 - 490 483 . 51 9 . 62E+Ol 27 . 67 3 . 36E+02 1.36 F 5 295 . 08 587 - 596 590 . 62 7 . 24E+Ol 26 . 09 3 . 17E+02 1.20 F 6 338 . 35 670 - 681 677 . 14 5 . 24E+Ol 19 . 94 2 . 86E+02 0 . 77 F 7 351. 65 699 - 709 703 . 72 l . 56E+02 30 . 61 2 . 40E+02 1. 29 F 8 583 . 12 1162 - 1171 1166 . 59 9 . 03E+Ol 22 . 45 7 . 77E+Ol 1. 59 I: 9 609 . 26 1214 - 1226 1218 . 85 1. 21E+02 25 . 31 1.15E 02 1.50 F 10 911 . 04 1815 - 1829 1822 . 31 7 . 25E+Ol 20 . 88 8 . 48E 01 2 . 08 F 11 968 . 97 1934 - 1945 1938 . 16 3 . 37E+Ol 15 . 41 7 . 49E+Ol 1.43 F 12 1460 . 53 2911 - 2931 2921 . 18 4 . 61E+02 43 . 39 2 . 64E 01 2 . 43 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/5/2018 6:25:03AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_N PP\Data\0000001 364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 77 . 05 1. 30E+02 42 . 28 l . 30E+02 4 . 23E+Ol F 2 185 . 94 3 . 99E+Ol 26 . 53 3 . 99E +Ol 2 . 65E+Ol M 3 238 . 55 3 . 25E+02 44 . 15 3 . 25E + 02 4 . 41E+Ol m 4 241 . 52 9 . 62E+Ol 27 . 67 9 . 62E+Ol 2 . 77E+Ol F 5 295 . 08 7 . 24E+Ol 26 . 09 7 . 24E+Ol 2 . 61E+Ol F 6 338 . 35 5 . 24E+Ol 19 . 94 5 . 24E+Ol 1 . 99E+Ol F 7 351 . 65 l . 56E+02 30 . 61 8 . 36E+Ol 3 . 72E+Ol 7 . 22E+Ol 4 . 82E+Ol F 8 583 . 12 9 . 03E+Ol 22 . 45 9 . 03E+Ol 2 . 25E+Ol F 9 609 . 26 l . 21E+02 25 . 31 4 . 12E+Ol 2 . 42E+Ol 7 . 97E +Ol 3 . 50E+Ol F 10 911 . 04 7 . 25E+Ol 20 . 88 7 . 25E +Ol 2 . 09£+01 F 11 968 . 97 3 . 37E+Ol 15 . 41 3 . 37E+Ol 1. 54E+Ol F 12 1460 . 53 4 . 61E+02 43 . 39 5 . 63E+Ol 1 . 71E+Ol 4 . 04E+02 4 . 66E+Ol 10/7/2020 Page 70
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 6:25:12AM Page3 of6 Analysis Report for L2-S UB-102-AJGS-005-SB 04/03/18 - 1443 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{3/4) Activity Activity Name Confidence {keV) (pCilgrams) Uncertainty K-40 0 . 99 1460.75
- 10 . 67 4 . 15E+00 5 . 31E-01 PB-212 0 . 99 77 . 11
- 17 . 50 l . 73E -0l 5 . 73E- 02 238 . 63
- 44 . 60 l.58E - 01 2 . 30E-02 BI - 214 0 . 34 609 . 31
- 46 . 30 8 . 65E-02 3 . 83E-02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB-214 0 . 99 77 . 11
- 10 . 70 2 . 83E-01 9 . 37E-02 295 . 21
- 19 . 20 9 . 76E-02 3 . 55E-02 351 . 92
- 37 . 20 5 . 87E - 02 3 . 93E- 02 RA-226 0 . 98 186 . 21
- 3 . 28 2 . 22E-01 1.48£-01 AC-228 0 . 61 209 . 28 4.40 338 . 32 11 . 40 l . 34E-01 5 . 15E-02 794 . 70 4 . 60 911 . 60
- 27 . 70 l . 89E-01 5 . 52£-02 964 . 60 5 . 20 969 .1 1
- 16 . 60 1 . SSE-01 7 . 13E-02
* =Energy line found in the spectrum.
- = Manually added nuclide.
=
? Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma 10/7/2020 Page 71
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 6:25:1 2AM Page 4 of6 Analysis Report for L2-SUB-102-AJGS-005-SB 04/03/18 - 1443 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) K- 40 0 . 993 4.15E+00 5 . 31E-01 PB-212 0 . 999 1. 54E-01 2 . 14E- 02 BI-214 0 . 349 8 . 65E-02 3 . 83£- 02 PB-214 0 . 993 7 . 66E-02 2 . SSE-02 RA-226 0 . 988 2 . 22E - 01 l . 48E-01 AC - 228 0 . 612 1. 59E - 01 3 . 33E-02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 72
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 6:25:12AM Page5of6 Analysis Report for L2-SUB-102-AJGS-005-SB 04/03/18 - 1443 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/5/2018 6:25:03AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 4 241.52 2 . 67164£ - 02 14 . 38 {b,t,.1~ F 8 583 . 12 2 . 50766£-02 12 . 43 ~--z,1Jb M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{3/4) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV)
+ K-40 1460 . 75
- 10 . 67 4 . 15E+00 4 . 78E-01 4 . 78E-01
+ AR - 41 1293 . 64 99 . 16 6 . 70E+03 l.16E+05 / l.16E+05 + CO-60 1173 . 22 100 . 00 6 . 57£ - 03 4 . 33E-02 4 . SSE-02 1332 . 49 100 . 00 1. 20E- 02 4 . 33E- 02 + KR-85 513 . 99 0 . 43 l . 87E+0l 8 . 20E+00 8 . 20E+00 + Y- 88 898 . 04 93 . 70 - 3 . 42E- 02 2 . 80E - 02 3 . 78E - 02 1836 . 06 99 . 20 -4.23E- 02 2 . B0E - 02 + NB - 94 702 . 63 100 . 00 - 1 . 95E - 02 3 . 26E - 02 3 . 26E - 02 871.10 100 . 00 4 . 50E-03 3 . 53E-02 + I-131 284 . 30 6 . 06 -4 . 99E- 02 3 . 49E - 02 4 . 59£ - 01 364 . 48 81 . 20 -l . 98E- 02 3 . 49E-02 636 . 97 7 . 27 1 . 74£- 01 4 . BSE - 01 + CS - 134 604 . 70 97 . 60 - 1 . 60£- 02 4 . 08£ - 02 4 . 0SE - 02 795 . 84 85 . 40 -3 . 12E- 02 4 . l0E-02 + CS-137 661. 65 85 . 12 8 . 85£- 02 4 . 66E-02 V 4 . 66£-02 10/7/2020 Page 73
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 6:25:12.AM Page 6 of6 Analysis Report for L2-SUB-102-AJGS-005-SB 04/03/18- 1443 Nuclide Energy Yield(%) Activity NuclideMDA Line MDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV)
+ CE -144 80 . 12 1.36 - 6 . 09E-0 1 2 . 12E- 01 2 . 62E+OO 133 . 51 11 . 09 - 1 . 62E - 01 2 . 12E - 01
+ E0 - 152 121.78 28 . 40 - 9 . 36E-02 8 . 29E - 02 / 8 . 29E- 02 244 . 69 7 . 49 4 . 56E-02 4 . 0SE- 01 964 . 00 14 . 44 -l . 67E-0 1 2 . 97E - 01 1408 . 00 20 . 74 l . 15E-01 l . 77E - 01
+ EU-154 123 . 07 40 . 40 - 3 . 0lE-02 5 . 87£-02 5 . 87E-02 247 . 94 6 . 60 - l . 65E - 01 4.0SE-01 723 . 30 19 . 70 4 . BSE-02 1 . 72E-01 873 . 20 11. 50 1 . 24E-Ol 3 . 09E-Ol 1004 . 76 17 . 90 - 9 . 56E - 02 2 . lOE - 01 1274 . 51 35 . 50 1 . 29E - 02 1.20E- 01
+ EU - 155 86 . 54 32 . 80 - 2 . 88E - 02 9 . 20E- 02 9 . 20£ - 02 105 . 31 21. 80 3 . 42E - 02 l.16E - 01
+ BI - 214 609 . 31
- 46 . 30 8 . 65E - 02 6 . 89E- 02 6 . 89E - 02 1120 . 29 15 . 10 - 2 . 91E-01 3 . 04E-01 1238 . 11 5 . 94 4 . 70E - 01 8 . 48E-01 1377 . 67 4 . 11 l . 82E- 01 9 . 51E - 01 1407 . 98 2 . 48 9 . 64E-01 1. 4 8E+OO 1509 . 19 2 . 19 8 . 44E -0 2 l.34E+OO 1764 . 49 15 . 80 2 . 27E - 01 2 . 87E - 01
+ PB- 214 77 . 11
- 10 . 70 2 . 83E - 01 7 . 38E- 02 3 . 25E - 01 295 . 21
- 19 . 20 9 . 76E-02 8 . 88E-02 351 . 92
- 37 . 20 5 . 87E - 02 7 . 38E-02
+ PA- 228 89 . 95 22 . 00 5 . 22E - 01 2 . 67E - Ol 4 . 62E - 01 93 . 35 35 . 00 -2 . 06E- 01 2 . 67E-01 105 . 00 16 . 30 -1 . 22E-Ol 5 . 31E-01 129 . 22 2 . 97 2 . 27E+00 2 . 79E+00 338 . 32 5 . 30 - 2 . 34E-01 l . 76E+OO 463 . 00 13 . 80 - 2 . 55£- 02 6 . 78E-01 911.23 16 . 70 5 . 37E - 01 9 . 68E - 01
+ AM-241 59 . 54 36 . 30 3 . 85E - 02 l . 73E - 01 1 . 73E -0 1
+ CM-243 103 . 76 23 . 00 -2 . 0SE - 02 1. lOE - 01 l . lOE-01 228 . 18 10 . 60 2 . 77E-03 2 . 29E- Ol 277 . 60 14 . 00 - 8 . 47E - 03 1. 79E -O l
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 74
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 7:27:35AM Page 1 of 6 I(
~~~pex-Gamma Analysis Report for L2-SUB-102-AJGS-006-SB 04/03/ 18 - 1530 L-z.. - o \\ - l o L iP_A
(_u-J \) ~o; ( GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-006-SB / Sample Description : 04/03/18 - 1530 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 9.428E+02 grams Facility : Dairyland_NPP Sample Taken On : 4/3/2018 3:30:00PM Acquisition Started : 4/5/2018 6:27:12AM Procedure : 500ml Marinelli Operator : Adm inistrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611 .1 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100- 4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4216 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/5/2018 7:27:26AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 75
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 7:27:35AM Page2 of6 Analysis Report for L2-SUB-102-AJGS-006-SB 04/03/18 - 1530 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 238 . 55 469 - 485 4 77 . 57 3 . 22E+02 45 . 03 6 . 38E+02 1. 63 F 2 295 . 18 572 - 595 590 . 80 l . 13E+02 30 . 14 6 . 52E+02 1. 61 F 3 338 . 34 672 - 685 677 . 12 5 . 77E+Ol 22 . 02 3 . 05E+02 1.06 F 4 351.79 697 - 710 704 . 01 l .7 3E+02 31 . 73 2 . 71E+02 1. 45 F 5 582 . 95 1159 - 1174 1166 . 25 9 . 44E +Ol 22 . 54 1. 23E 02 1.50 F 6 609 . 23 1212 - 1224 121 8. 79 9 . 51E+Ol 23 . 49 1. 26E+02 1. 57 F 7 911.09 1816 - 1828 1822 . 42 6 . 44E+Ol 20 . 01 8 . 49E+Ol 1. 88 F 8 969 . 11 1934 - 1945 1938 . 4 4 4 . 50E+Ol 16 . 82 7 . 22E+Ol 1.51 F 9 1460 . 51 2913 - 2929 292 1. 14 4 . 70E+ 02 43 . 86 2 . llE+Ol 2 . 40 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/5/2018 7:27:26AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert Area Uncert. F 1 238 . 55 3 . 22E+02 45 . 03 3 . 22E+02 4 . 50E+Ol F 2 295 . 18 1 . 13E+02 30 . 14 l . 13E+02 3 . OlE+Ol F 3 338 . 3 4 5 . 77 E +Ol 22 .0 2 5 . 77E+Ol 2 . 20E+Ol F 4 351. 79 1 . 73E+02 31 . 73 8 . 36E+Ol 3 . 72E+Ol 8 . 94E+Ol 4 . 89E+Ol F 5 582 . 95 9 . 44E+Ol 22 . 54 9.44E+Ol 2 . 25E+Ol F 6 609 . 23 9 . 51E+Ol 23 . 49 4. 12E+Ol 2 . 42E+Ol 5 . 39E+Ol 3 . 37E+Ol F 7 911.09 6 . 44 E+Ol 20 .0 1 6 . 4 4E+Ol 2 . 00E+Ol F 8 969 . 11 4 . 50E+Ol 16 . 82 4 . 50E+Ol 1 . 68E+Ol F 9 1460 . 51 4 . 70E+02 43 . 86 5 . 63E+Ol 1 . 71E+Ol 4 . 1 4E+02 4 . 71E+Ol M = First peak in a multiplet region m = Other peak in a multiplet reg ion F = Fitted singlet Errors quoted at 2.000sigma 10/7/2020 Page 76
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 7:27:35AM Page 3 of6 Analysis Report for L2-SUB-102-AJGS-006-SB 04/03/18 - 1530 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0 . 99 1460 . 75
- 10 . 67 4 . 78E+00 6 . 05E- 0l PB - 212 0 . 55 77 . 11 17 . 50 238 . 63
- 44 . 60 l.76E-01 2 . 63E- 02 BI - 214 0 . 34 609 . 31 46 . 30 6 . 58E- 02 4 . 14E- 02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB - 214 0 . 72 77 . 11 10 . 70 295 . 21
- 19 . 20 1 . 71E- 01 4 . 65E - 02 351. 92
- 37 . 20 8 . 19E-02 4 . SOE - 02 AC - 228 0 . 61 209 . 28 4 . 40 338 . 32
- 11 . 40 l . 66E - 01 6 . 40E - 02 794 . 70 4 . 60 911 . 60
- 27 . 70 l . 89E - 01 5 . 94E - 02 964 . 60 5 . 20 969 . 11
- 16 . 60 2 . 33E- 01 8 . 78E-02
* =Energy line found in the spectrum.
- =Manually added nuclide.
? =Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT 10/7/2020 Page 77
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 7:27:35AM Page4 of6 Analysis Report for L2-SUB-102-AJGS-006-SB 04/03/18 - 1530 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) K-40 0 . 991 4 . 78E+OO 6 . 0SE-01 PB-212 0 . 559 1. 76E - 01 2.63E-02 BI-214 0 . 349 6 . 58E-02 4 . 14E-02 PB - 214 0 . 720 l . 25E-01 3 . 23E - 02 AC-228 0 . 616 1 . 89E - 01 3 . 90E-02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 78
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 7:27:35AM Page 5 of6 Analysis Report for L2-SUB-102-AJGS-006-SB 04/03/18 - 1530 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/5/2018 7:27:26AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 5 582 . 95 2 . 62 1 08£- 02 11 . 95 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(3/4) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCilgrams) (pCi/grams) (keV}
+ K- 40 1460 . 75
- 10 . 67 4 . 78E+00 5 . 16E-01 5 . 16E- 01
+ AR- 41 1293 . 64 99 . 16 5 . 59E+04 1 . 47E+05 ,./ 1 . 47E+05 + CO-60 1173 . 22 100 . 00 3 . 41E - 02 4 . 52E - 02 5 . 37E- 02 1332 . 49 100 . 00 2 . 17E-02 4 . 52E-02 KR - 85 513 . 99 0 . 43 7 . 64E+00 8 . 36E+00 8 . 36E+00 + Y-88 898 . 04 93 . 70 -8 . 40E - 03 3 . 2 4E- 02 4 . 33E - 02 1836 . 06 99 . 20 8 . 7 4E-03 3 . 24E - 02 + NB - 94 70 2 . 63 100 . 00 7 . 79E - 03 3 . 57 E- 02 3 . 57£ - 02 871 . 10 100 . 00 - 4 . 55E - 02 3 . 76E - 02 + I - 131 28 4. 30 6 . 06 3 . 55E - 03 3 . 74E- 02 5 . 17E- 01 364 . 48 81. 20 - 8 . 29£- 04 3 . 74E- 02 636 . 97 7 . 27 5 . 66E- 02 5 . 45E-Ol + CS - 134 604 . 70 97 . 60 2 . 74E - 03 4 . 27E - 02 4 . 27E - 02 795 . 84 85 . 40 3 . 13E- 02 / 4 . 65E- 02 + CS - 137 661 . 65 85 . 12 4 . 48E - 02 4 . 69E-02 4 . 69E- 02 + CE-144 80 . 12 1. 36 6 . 75 E- 01 2 . 32E - 01 2 . 97E +00 133 . 51 11 . 09 1 . 08E - 02 2 . 32E - 01 10/7/2020 Page 79
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 7:27:35AM Page 6 of 6 Analysis Report for L2-SUB-102-AJGS-006-SB 04/03/18 - 1530 Nuclide Energy Yield(%) Activity Nuclide MDA LlneMDA Name (pCilgrams) (pCilgrams) {pCilgrams) (keV)
+ EU - 152 121. 78 28 . 40 - 1. OSE- 02 8 . 95E - 02 / 8 . 95E - 02 244 . 69 7 . 49 - 3 . 88E - 01 4 . 30E - 01 964 . 00 14 . 44 -1. 29E-01 3 . 54E - 01 1408 . 00 20 . 74 9 . SlE- 02 / 1. 76E- 01
+ EU - 154 123 . 07 40 . 40 - 2 . 04E- 02 6 . 27E-02 6 . 27E - 02 247 . 94 6 . 60 - 5 . 95E- 01 4 . 20E-01 723 . 30 19 . 70 9 . 32E - 02 2 . 00E - 01 873 . 20 1 1. 50 - l . 90E - 02 3 . 33E- 01 1004 . 76 17 . 90 - 6 . 94E-02 l . 94E - 01 1274 . 51 35 . 50 4 . 57E- 02 1.43E-01
+ EU - 155 86 . 54 32 . 80 - 4 . 50E-02 l . 04E-01 l . 04E - 01 105 . 31 21. 80 - 4 . 55E-02 l . 27E-01
+ BI-214 609 . 31
- 4 6 . 30 6 . 58E-02 7 . 89E - 02 7 . 89E - 02 1120 . 29 15 . 10 5 . 39E- 01 3 . 73E-Ol 1238 . 11 5 . 94 4 . 75E - 01 9 . 23E - 01 1377 . 67 4 . 11 5 . 41E - 01 1. 03E+OO 1407 . 98 2 . 48 7 . 95E- 01 1 . 48E+OO 1509 . 19 2 . 19 - 5 . 17E- 02 l . 58E+OO 1764 . 4 9 15 . 80 1. 0 4E- 01 2 . 46E - 01
+ PB - 214 77 . 11 10 . 70 3 . 56E- 01 8 . 79E - 02 4 . 03E - 01 295 . 21
- 19 . 20 1 . 71E-Ol 1 . 85E - Ol 351 . 92
- 37 . 20 8 . 19E- 02 8 . 79E-02
+ PA-228 89 . 95 22 . 00 3 . 83E-01 3 . lOE - 01 5 . 25E- 01 93 . 35 35 . 00 - 4 . 62E - 02 3 . lOE - 01 105 . 00 16 . 30 7 . 20E-02 5 . 92£ - 01 129 . 22 2 . 97 - 9 . llE- 02 2 . 98E+OO 338 . 32 5 . 30 1 . 40E+OO 2 . 02E+OO 463 . 00 13 . 80 - 1 . 58£ - 01 7 . 94E - 01 911 . 23 16 . 70 l . 58E+OO l . 08E+00
+ AM - 241 59 . 54 36 . 30 6 . 86E - 02 l . 93E - 01 l . 93E-01
+ CM - 243 103 . 76 23 . 00 - 2 . 91E - 02 1 . 21E - 01 1 . 21E - 01 228 . 18 10 . 60 - 1 . 46E - 01 2 . 42E - 01 277 . 60 14 . 00 l . 27E- 01 l . 96E - 01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life loo short to be able to perfonn the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 80
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 2:15:40PM Page I of 7
~~~pex-Gamma Analysis Report for L2-SUB-102-AJGS-007-SB 04/04/18 - 0825 l-. -z_ - o I\ - loL R_A LuJ{) So; L GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-007-SB /
Sample Description : 04/04/18 - 0825 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 1.091 E+03 grams / Facility : Dairyland_NPP Sample Taken On : 4/4/2018 8:25:00AM AcQuisition Started : 4/5/2018 1:15:14PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live nme : 3600.0 seconds Real nme : 3611 .0seconds Dead Time : 0.30 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100- 4096 ldentlfrcation Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4224 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/5/2018 2:15:28PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 81
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 2:15:40PM Page 2 of7 Analysis Report for L2-SUB-102-AJGS-007-SB 04/04/ 18 -- 0825 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 76 . 61 148 - 160 153 . 77 1. 26E+02 45 . 65 l . 40E+03 1. 97 F 2 186.07 364 - 377 372 . 63 6 . 40E +Ol 32 . 48 8 . 03E+02 1. 29 F 3 238 . 56 470 - 481 477 . 60 2 . 27E+02 43 . 23 7 . 21E+02 1. 27 F 4 295 . 08 586 - 595 590 . 61 6 . 70E+ Ol 25 . 43 2 . 6 4E+02 1.32 F 5 327 . 88 652 - 660 656 . 20 2 . 84E+Ol 17 . 34 2 . 20E+02 0 . 76 F 6 338 . 28 670 - 681 676 . 99 6 . 74E+Ol 23 . 64 2 . 40E 02 1. 32 F 7 352 . 09 699 - 709 7 0 4 . 61 l . 54E+02 30 . 26 2 . 13E 02 1. 41 F 8 582 . 8 4 1159 - 1171 1166 . 03 9 . llE+Ol 23 . 68 1. 39E 02 1. 57 F 9 609 . 26 1213 - 1225 1218 . 85 1. 03E+ 0 2 24 . 67 1 . 32E+02 1. 72 F 10 911 . 03 1817 - 1829 1822 . 29 7 . 39E+Ol 20 .4 4 6 . 88E+Ol 2 . 05 F 11 1460 . 66 2915 - 2930 2921 . 42 5 . 4 1E+02 47 . 57 2 . 08E+Ol 2 . 27 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/5/2018 2:15:28PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 7 6. 61 1. 2 6E+02 45 .6 5 1 . 2 6E+ 0 2 4 . 56E+Ol F 2 186 . 07 6 . 40E+Ol 32 . 48 6 . 40E+Ol 3 . 25E+Ol F 3 238 . 56 2 . 27E+02 43 . 23 2 . 27E+02 4 . 32E+Ol F 4 295 . 08 6 . 70E +Ol 25 . 4 3 6 . 70E+Ol 2 . 54E+Ol F 5 327 . 88 2 . 8 4E+Ol 17 . 34 2 . 8 4E+Ol 1 . 73E+Ol F 6 338 . 28 6 . 74E+Ol 23 . 64 6 . 74E+Ol 2 . 36E+Ol F 7 352 . 09 1 . 5 4E+02 30 . 26 8 . 36E+Ol 3 . 72E+Ol 7 . 04E+Ol 4 . 80E+Ol F 8 582 . 8 4 9 . llE+Ol 23 . 68 9 . llE 01 2 . 37E+01 F 9 609 . 26 1. 03 E+02 2 4 . 67 4. 12E+Ol 2 .4 2E+Ol 6 . 16E+O l 3 . 46E+Ol F 10 91 1.03 7 . 39E+Ol 20 .44 7 . 39E+Ol 2 . 04E+Ol F 11 1460 . 66 5 . 4 1E+02 47 . 57 5 . 63E+Ol 1 . 71E+Ol 4 . 85E+02 5 .0 6E +Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted al 2.000sigma 10/7/2020 Page 82
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 2:15:40PM Page 3 of7 Analysis Report for l2-SUB-102-AJGS-007-SB 04/04/18 - 0825 NUCLIDE IDENTIFICATION REPORT Nuclide library Used : C:\Canberra\Apex\Root\Dairyland_NPP\llb rary\H OTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0 . 99 1460 . 75
- 10 . 67 4 . 84E+OO 5 . 72E - 01 PB-212 0 . 98 77 . 11
- 17 . 50 1 . 64£-01 6 . 0SE-02 238 . 63
- 44 . 60 1 . 07£-01 2 . 12£-02 BI-214 0 . 34 609 . 31
- 46 . 30 6 . SOE-02 3 . 67E- 02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB- 214 0 . 99 77 . 11
- 10 . 70 2 . 68E - Ol 9 . 90E - 02 295 . 21
- 19 . 20 8 . 79E-02 3 . 36E-02 351 . 92
- 37 .2 0 5 . 58E - 02 3 . 81E -0 2 RA-226 0 . 99 186 . 21
- 3 . 28 3 . 46E - 01 l . 77E - 01
* =Energy line found in the spectrum.
- =Manually added nuclide.
? =Manually edited nuclide.
@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) 10/7/2020 Page 83
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 2:15:40PM Page 4 of 7 Analysis Report for l2-SUB-102-AJGS-007-SB 04/04/18 - 0825 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams) K-40 0 . 999 4 . 84E+OO 5 . 72E - Ol PB - 212 0 . 988 1. 08E - 01 2 . 0lE - 02 BI - 214 0 . 349 6 . SOE - 02 3 . 67E - 02 PB-214 0 . 990 7 . 49E-02 2 . 45E-02 RA-226 0 . 997 3 . 46E - 01 1 . 77£ - 01
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted al 2.000sigma 10/7/2020 Page 84
LAC LTP - Final Status Survey Package - 3/21/2018 4/512018 2:15:40PM Page 5 of7 Analysis Report for L2-SUB-102-AJGS-007-SB 04104/ 18 - 0825 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/512018 2:15:28PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 5 327 . 88 7 . 88083£-03 30 . 55 fte,, . 1rt!O F 6 338 . 28 1 . 87356£ - 02 17 . 52 Tol. AC - 228 PA- 228 F F 10 8 582 . 84 911.03 2 . 53156E- 02 2 . 05356E - 02 12 . 99 13 . 82 Tol. f/ . u/b AC - 228 PA - 228 M = First peak in a multiplet reg ion m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(3/4) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCllgrams) (pCilgrams) (keV)
+ K- 40 1 4 60 . 75
- 10 . 67 4 . 8 4E+00 4 . 41E - 01 4. 41E - 0l
+ AR - 41 1293 . 64 99 . 16 7 . 39E+02 2 . 89E+03 / 2 . 89E+03 + CO - 60 1173 . 22 100 . 00 l . 04E - 02 4 . 39E - 02 4 . 79E - 02 1332 . 49 100 . 00 2 . 69E- 02 4 . 39E - 02 + KR - 85 513 . 99 0 . 43 8 . 30E+00 7 . 70E+00 7 . 70E+O0 + Y- 88 898 . 04 93 . 70 - 2 . 76E - 02 2 . 47E - 02 3 . 54E- 02 1836 . 06 99 . 20 3 . 93E - 03 2 .4 7E - 02 + NB-94 702 . 63 100 . 00 6 . 49E - 03 3 . 16E- 02 3 . 16E-02 87 1. 10 100 . 00 -5 . 4 6E - 02 3 . 30E- 02 10/7/2020 Page 85
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 2:15:40PM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-007-SB 04/04/1 8 - 0825 Nuclide Energy Yield(%) Activity Nuclide MDA LlneMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV)
+ I-131 284 . 30 6.06 l . 52E-0l 3 . 23E- 02 4 . 62E-01 364 . 48 81 . 20 1. 39£-02 3 . 23E - 02 636 . 97 7 . 27 -3 . 74E-01 4.24£-01
+ CS-134 604 . 70 97 . 60 -6 . 45£-03 3 . 80E- 02 3 . 80£-02 795 . 84 85 . 40 1 . 30£-02 3 . 99E-02
+ CS - 137 661. 65 85 . 12 6 . 99E - 02 4. 47E - 02 { 4 . 47E-02
+ CE - 144 80.12 l. 36 1 . 80£ - 04 2 . 09E-01 2 . 64E+00 133 . 51 11.09 -l . 98E-02 2 . 09E - 01
+ EU - 152 121 . 78 28 . 40 - 1 . 21£-02 8 . l0E - 02 / 8 . l0E-02 244 . 69 7 . 49 - 8 . 82E-01 3 . 81E-01 964 . 00 14 . 44 8 . 85E-02 2 . 88E-01 1408 . 00 20 . 74 8 . 68E - 02 1 . 64E-01
+ EU-154 123 . 07 40 . 40 -1 . 60E-02 5. 70E - 02 / 5 . 70E -02 247 . 94 6 . 60 - 1 . 89E+00 3 . 85E-01 723 . 30 19 . 70 9 . 35E-02 1 . 72E - 01 873 . 20 11. 50 -1 . 89E-01 2 . 96E-01 1004 . 76 17 . 90 - l . 32E-0l 1 . 99E- 01 1274 . 51 35 . 50 4 . l0E - 03 l . llE- 01
+ EU - 155 86 . 54 32 . 80 -1 . 82E - 02 9 . 33E-02 9 . 33E-02 105 . 31 21 . 80 -7 . 05E-03 1 . 13E-01
+ BI-214 609 . 31 46 . 30 6 . S0E - 02 6 . 89E - 02 6 . 89E- 02 1120 . 29 15 . 10 9 . 54E- 03 3 . 09E-01 1238 . 11 5 . 94 8 . 16E- 02 8 . 58E-0l 1377 . 67 4 . 11 6 . 41E- 01 8 . 02E- 01 1407 . 98 2 . 48 7 . 26E-01 l . 37E+00 1509 . 19 2 . 19 6 . 90E- 01 l . 49E+00 1764 . 49 15 . 80 l.88E - 01 2 . 36£- 01
+ PB-214 77 . 11
- 10 . 70 2 . 68E - 01 7 . 03E - 02 3 . 08E-01 295 . 21
- 19 . 20 8 . 79E - 02 7 . 84E- 02 351. 92
- 37 . 20 5 . 58E-02 7 . 03E-02
+ PA - 228 89 . 95 22 . 00 3 . lSE-01 2 . 02£-01 3 . 40E-01 93 . 35 35 . 00 l . 36E- 0l 2 . 02E-01 105 . 00 16 . 30 9 . 29£ - 02 3 . 83E - 0l 129 . 22 2 . 97 1. 31E+00 l.99E+00 338 . 32 5 . 30 5 . 47E-01 l.26E+00 463 . 00 13 . 80 -1 . 63£-01 4 . 85E-01 911.23 16 . 70 4 . 79£- 01 6 . 85E-01
+ AM-241 59 . 54 36 . 30 - 7 . 00E - 02 l . 64E- 01 l . 64E-01
+ CM - 243 103 . 76 23 . 00 2 . 29E - 02 1 . 09E- 01 l . 09E - 01 228 . 18 10 . 60 -8 . 12E- 02 2 . 19E-01 277 . 60 14 . 00 1. 88E-02 1 . 84E - 01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 86
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 2:15:40PM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-007-SB 04/04/18 - 0825 10/7/2020 Page 87
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 3:35:16PM Page I of6 pex-Gamma Analysis Report for L2-SUB-102-AJGS-008-SB 04/04/18 - 0848 L-'1.- - (::. \ l - lD 'Z.._ ()...A. C..,'->-1 ~ So; { GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-008-SB ,,,,,, Sample Description : 04/04/18 - 0848 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 1.085E+03 grams / Facility : Dairyland_NPP Sample Taken On : 4/4/2018 8:48:00AM Acquisition Started : 4/5/2018 2:34:53PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611.0 seconds Dead Time : 0.30 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4226 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/5/2018 3:35:07PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 88
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 3:35:16PM Page 2 of6 Analysis Report for L2-SUB-102-AJGS-008-SB 04/04/18 - 0848 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 77 . 10 148 - 162 154 . 74 l . 95E+02 54 . 27 1 . 41E+03 2.19 F 2 186 . 05 367 - 380 372 . 60 l . 10E+02 41 . 32 7 . 99E+02 2 . 10 F 3 238 . 61 473 - 485 477 . 69 3 .4 6E+02 47 . 86 5 . 89E+02 1. 60 F 4 295 . 01 585 - 595 590.46 8 . 84E+0l 29 . 20 3 . 58E+02 1. 42 F 5 338 . 37 672 - 684 677 . 18 6 . 86E+0l 26 . 03 3 . 13E 02 1. 55 F 6 351. 83 698 - 711 704 . 08 1 . 83E+02 33 . 21 2 . 68E+02 1. 74 F 7 583 . 08 1161 - 1171 1166.51 l . 06E+02 24.19 l . 05E+02 1. 4 6 F 8 609 . 22 1213 - 1223 1218 . 77 1 . 35E+02 27.03 1 . 13E+02 1. 67 F 9 911.06 1817 - 1828 1822 . 36 5 . 57E+0l 19. 41 8 . 29E+0l 1. 94 F 10 968 . 74 1933 - 1943 1937 . 70 4 . 38E+0l 18 . 04 9 . 89E+0l 1.52 F 11 1119 . 84 2235 - 2245 2239 . 87 2 . 69E+0l 15.10 5 . 83E+0l 2 . 08 F 12 1460 . 60 2914 - 2930 2921 . 31 5 . 16E+02 46 . 45 2 . 81E+0l 2 . 48 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/5/2018 3:35:0?PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 77 . 10 1 . 95E+02 54 . 27 l . 95E+02 5 . 43E+0l F 2 186 . 05 l . 10E+02 41 . 32 l . 10E+02 4 . 13E+0l F 3 238 . 61 3 . 46E+02 47 . 86 3 . 46E+02 4 . 79E+0l F 4 295 . 01 8 . 84E+0l 29 . 20 8 . 84E+0l 2 . 92E+0l F 5 338 . 37 6 . 86E+0l 26 . 03 6 . 86E+0l 2 . 60E+0l F 6 351. 83 l . 83E+02 33 . 21 8 . 36E+0l 3 . 72E+0l 9 . 94E+0l 4 . 99E+0l F 7 583 . 08 1 . 06E+02 24 . 19 1. 06E+02 2 .4 2E+0l F 8 609 . 22 l . 35E+02 27 . 03 4.12E+0l 2 .4 2E 01 9 . 41E+0l 3 . 63E+0l F 9 911.06 5 . 57E+0l 19 . 41 5 . 57E+0l 1. 94E+0l F 10 968 . 74 4 . 38E+0l 18 . 04 4 . 38E+0l l . 80E+0l F 11 1119 . 84 2 . 69E+0l 15 . 10 2 . 69E+0l l . 51E+0l F 12 1460 . 60 5 .1 6E+02 46 . 45 5 . 63E+0l 1 . 71E+0l 4 . 60E+02 4.95E+0l 10/7/2020 Page 89
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 3:35:16PM Page 3 of6 Analysis Report for L2-SUB-102-AJGS-008-SB 04/04/18 - 0848 M :e First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted al 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460 . 75
- 10 . 67 4 . 62E+OO 5 . 59E-01 PB-212 1.00 77 . 11
- 17 . 50 2 . 54E-01 7 . 24E - 02 238 . 63
- 44 . 60 1 . 65E - 01 2 . 43E - 02 BI-214 0 . 57 609 . 31
- 46 . 30 9 . 99E - 02 3 . 89E- 02 1120 . 29
- 15 . 10 l . SlE-01 8 . 54E - 02 1238 . 11 5.94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB-214 0 . 99 77 . 11
- 10 . 70 4 . lSE-01 1 . 18E- 01 295 . 21
- 19 . 20 l . 16E- 01 3 . 89E- 02 351 . 92
- 37 . 20 7 . 92E - 02 3 . 99E-02 RA- 226 0 . 99 186 . 21
- 3 . 28 5 . 96E-01 2 . 27E-01 AC - 228 0 . 61 209 . 28 4 . 40 338 . 32
- 11 . 40 1 . 72E-01 6 . 58E-02 794 . 70 4 . 60 911 . 60
- 27 . 70 l . 42E-01 5 . 00E-02 964 . 60 5 . 20 969 . 11
- 16 . 60 1. 97E-01 8 . 17E-02
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted al 2.000sigma 10/7/2020 Page 90
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 3:35:16PM Pagc 4 of6 Analysis Report for L2-SUB-102-AJGS-008-SB 04/04/1 8 - 0848 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) K- 40 0 . 996 4 . 62E+OO 5 . 59E - 01 PB-212 1 . 000 l . 68E - 01 2 . 31E - 02 BI-214 0 . 579 l . 09E- 01 3 . 54£-02 PB-214 0 . 997 l . OlE - 01 2 . 72E-02 RA-226 0 . 996 5 . 96E-01 2 . 27E-01 AC-228 0 . 610 l . 62E-01 3 . SSE-02
? = nuclide is part of an undetermined solution X nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000slgma 10/7/2020 Page 91
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 3:35:16PM Page 5 of 6 Analysis Report for L2-SUB-102-AJGS-008-SB 04/04/18 - 0848 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/5/2018 3:35:07PM Peak Locale From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 7 583 . 08 2 . 95130E- 02 ll . 38 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide library Used : C:\Canberra\Apex\Root\Dairyland_NPP\library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams) (ke V)
+ K- 40 1460 . 75 10 . 67 4 . 62E+00 4.61E-01 4.61E-01
+ AR-41 1293 . 64 99 . 16 -4 . 04E+02 3 . 88E+03 / 3 . 88E+03
+ CO-60 1173 . 22 100 . 00 2 . 44E-02 3 . 96E-02 4.85E-02 1332 . 49 100 . 00 1. 09E-02 3 . 96E-02
+ KR-85 513 . 99 0 . 43 9 . 45E+00 7 . 61E+00 7 . 61E+00
+ Y- 88 898 . 04 93 . 70 7 . 43E- 04 2 . 65E- 02 4 . 04E- 02 1836 . 06 99 . 20 -5.55E-03 2 . 65E- 02
+ NB-94 702 . 63 100 . 00 1 . 04E-02 3 . 20E-02 3 . 20E-02 871 . 10 100 . 00 - 2 . 57E-02 3 . 52E-02
+ I - 131 284 . 30 6 . 06 -3.46E-03 3.44£-02 4 . 71£-01 364 . 48 81. 20 l . 0SE-02 3 . 44E - 02 636 . 97 7 . 27 - 3 . 27£- 01 4.30E - 01
+ CS-134 604 . 70 97 . 60 5 . 34E-02 4 . 03E-02 4 . 03£-02 795.84 85 . 40 1 . 66£- 05 / 4 . 14£-02
+ CS-137 661 . 65 85 . 12 9 . 06£-02 4 . 49£-02 4 . 49£-02
+ CE-144 80 . 12 1. 36 -5 . 82E-01 2 . 17E-01 2 . 68E+00 133 . 51 11.09 -3 . 67E-02 2 . 17E-01 10/7/2020 Page 92
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 3:35:16PM Page 6 of 6 Analysis Report for L2-SUB-102-AJGS-008-SB 04/04/18 - 0848 Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV)
+ EU-152 121 . 78 28 . 40 - 5 . 58E - 02 8 . 43E - 02 / 8 . 43E-02 244 . 69 7 . 49 -3 . 05E - 01 3.96E - 01 964 . 00 14 . 44 1 . SlE - 01 3 . 30E - 01 1408 . 00 20 . 74 8 . 27E - 02 / 1 . 53E-01
+ EU-154 123 . 07 40.40 -l . 76E-02 5 . 95E- 02 5 . 95E-02 247 . 94 6 . 60 -5 . 82E-01 3 . 85E-01 723 . 30 19 . 70 7 . 42E-02 l . 77E-01 873 . 20 11 . 50 1. 34E-01 3 . 17E-01 1004 . 76 17 . 90 -7 . 07E-02 2 . 04E - Ol 1274 . 51 35 . 50 -4 . 77E-02 1 . 12E- 01
+ EU-155 86 . 54 32 . 80 - 9 . 68E - 02 9 . 14E- 02 9 . 14E- 02 105 . 31 21 . 80 9 . 46E- 03 l . 15E- 01
+ BI-214 609 . 31
- 46 . 30 9 . 99E- 02 6 . 56E-02 6 . 56£-02 1120 . 29
- 15 . 10 1 . 51£-01 l . 70E-01 1238 . 11 5 . 94 -8 . 50E-02 8 . 33E - 0 1 1377 . 67 4 . 11 -7 . 44E - 02 7 . 59£-01 1407 . 98 2 . 48 6 . 91E - 01 1. 28E+OO 1509 . 19 2 . 19 4 . 80E-01 l . 31E+OO 1764 . 49 15 . 80 1. 35E - 01 2 . 34E.-01 PB-214 77 . 11
- 10 . 70 4 . 15E-01 7 . 66E - 02 3 . 22E- 01 295 . 21
- 19 . 20 l . 16E- Ol 9 . 31E-02 351 . 92
- 37 . 20 7 . 92E- 02 7 . 66E- 02
+ PA- 228 89 . 95 22 . 00 3 . 42E - Ol 2 . 08E - 01 3 . 51E- 01 93 . 35 35 . 00 -2 . 17£- 02 2 . 08£ - 01 105 . 00 16 . 30 1 . 14E- 01 4 . 03E - 01 129 . 22 2 . 97 1 . 14E+OO 2 . llE+OO 338 . 32 5 . 30 1 . 30E+OO l . 35E+OO 463 . 00 13 . 80 4 . 70E - 01 5 . 22£- 01 911 . 23 16 . 70 5 . 76E - 01 6 . 88£- 01
+ AM - 241 59 . 54 36 . 30 - 1. 23E-02 1 . 74E - 01 1. 74E- 01
+ CM- 243 103 . 76 23 . 00 4 . 66E - 02 1 . llE - 01 l . llE - 01 228 . 18 10 . 60 -1 . 0lE- 01 2 . 25E - 01 277 . 60 14 . 00 1. 16E- 01 1 . 81E - Ol
+ = Nuclide identified during the nuclide identification
= Energy line found ln the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 93
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 8:41:45AM Page I of7 pex-Gamma Analysis Report for L2-SUB-102-QJGS-008-SB 04/04/18 - 1038 L"2- -C>l\ - \ c?.- (<_A C...u-)t) ~o~ ( GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-QJGS-008-SB / Sample Description : 04/04/18 -1038 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 1.123E+03 grams / Facility : Dairyland_NPP Sample Taken On : 4/4/2018 10:38:00AM Acquisition Started : 4/6/2018 7:41 :22AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 361 1.2 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4231 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/6/2018 8:41 :36AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 94
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 8:41 :45AM Page 2 of7 Analysis Report for L2-SUB-102-QJGS-008-SB 04/04/18 -1038 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 75 . 82 147 - 161 152 . 19 2 . 58E+02 65 . 43 1 . 43E+03 4 . 71 F 2 185 . 70 366 - 375 371 . 90 5 . 08E+Ol 28 . 95 6 . 10E+02 1 . 03 F 3 238 . 61 470 - 485 477 . 69 3 . 64E+02 47 . 08 6 . 47£+02 1. 56 F 4 295 . 01 586 - 596 590 . 48 8 . 72E+Ol 27 . 09 3 . 73£+02 1.05 F 5 338 . 37 672 - 682 677 . 18 4 . 32E+Ol 22 . 79 3 . 14E+02 1.16 F 6 351. 82 697 - 711 704 . 06 l . 96E+02 34 . 43 3 . 48£+02 1.53 F 7 583 . 03 1157 - 1173 1166 . 41 l . 02E+02 24 . 84 l.79E+02 1. 77 F 8 609 . 12 1211 - 1225 1218 . 57 1. 53E+02 29 . 03 l . 92E+02 1 . 57 F 9 910 . 74 1815 - 1830 1821 . 71 7 . 95E+Ol 20 . 71 7 . 20E+Ol 2 . 11 F 10 1120 . 03 2236 - 2246 2240 . 25 3 . 36E+Ol 16 . 49 7 . 27E+Ol 1 . 98 F 11 1237 . 39 2470 - 2482 2474 . 94 2 . 45E+Ol 14 . 14 6.50E+Ol 1.80 F 12 1331 . 57 2658 - 2669 2663 . 27 2 . 16E+Ol 10 . 98 l . 62E+Ol 2 . 05 F 13 1460 . 46 2912 - 2928 2921 . 02 5 . 12E+02 46 . 32 3 . 29E+Ol 2 . 37 F 14 1764 . 07 3522 - 3535 3528 . 20 3 . 27E+Ol 12 . 10 3 . 88E+OO 2 . 71 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfom1ed on : 4/6/2018 8:41 :36AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 75 . 82 2 . 58E+02 65 . 43 2 . 58E 02 6 . 54E+Ol F 2 185 . 70 5.08E+Ol 28 . 95 5 . 08E+Ol 2 . 89E+Ol F 3 238 . 61 3 . 64E+02 47 . 08 3 . 64E+02 4 . 71E+Ol F 4 295 . 01 8 . 72E+Ol 27 . 09 8 . 72E+Ol 2 . 71E+Ol F 5 338 . 37 4 . 32E+Ol 22 . 79 4 . 32E+Ol 2 . 28E+Ol F 6 351 . 82 l . 96E+02 34 . 43 8 . 36E+Ol 3 . 72E+Ol l . 12E+02 5 . 07E+Ol F 7 583 . 03 l . 02E+02 24 . 84 l . 02E+02 2 . 48E+Ol F 8 609 . 12 1. 53E+02 29 . 03 4 . 12E+Ol 2 . 42E+Ol l . 11E+02 3 . 78E+Ol F 9 910 . 74 7 . 95E+Ol 20 . 71 7 . 95E+Ol 2 . 07E+Ol F 10 1120 . 03 3 . 36E+Ol 16 . 4 9 3 . 36E+Ol l . 65E+Ol F 11 1237 . 39 2 . 45E+Ol 14 . 14 2 . 45E+Ol 1 . 41E+Ol F 12 1331 . 57 2 . l 6E+Ol 10 . 98 2 . 16E+Ol l . lOE+Ol F 13 1460 . 46 5 . 12E+02 46 . 32 5 . 63E+Ol l . 71E+Ol 4 . 56E+02 4 . 94E+Ol F 14 1764 . 07 3 . 27E+Ol 12 . 10 l . 52E+Ol 9 . 80£+00 1 . 75E+Ol 1 . 56E+Ol 10/7/2020 Page 95
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 8:41 :45AM Page 3 of? Analysis Report for L2-SUB-102-QJGS-008-SB 04/04/18 -1038 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0 . 98 1460 . 75
- 10 . 67 4 . 42E+OO 5 . 38E- 01 PB-212 0.56 77 . 11 17.50 238 . 63
- 44 . 60 1 . 67E-Ol 2 . 33E- 02 BI-214 0 . 86 609 . 31
- 46 . 30 1 . 14E - 01 3 . 93E - 02 1120 . 29
- 15 . 10 1.83E-01 9 . 02E-02 1238 . 11
- 5 . 94 3 . 70E - 01 2 . 14E-01 1377 . 67 4 . 11 1407.98 2 . 48 1509 . 19 2 . 19 1764 . 49
- 15 . 80 1. 34E-01 1. 20E-01 PB-214 0 . 71 77 . 11 10 . 70 295 . 21
- 19 . 20 1 . llE-01 3 . 49E-02 351 . 92
- 37 . 20 8 . 65E-02 3 . 92£-02 RA-226 0 . 95 186 . 21
- 3 . 28 2 . 67E - 01 1 . 53E - 01
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT 10/7/2020 Page 96
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 8:41 :45AM Pagc4 of7 Analysis Report for L2-SUB-102-OJGS-008-SB 04/04/18 --1038 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams) K- 40 0 . 986 4 . 42E+OO 5 . 38E-01 PB-212 0 . 560 1 . 67E - 01 2 . 33E-02 BI-214 0 . 862 1. 32E-01 3 . 41E-02 PB- 214 0 . 719 l . OOE-01 2 . 61E-02 RA- 226 0 . 959 2 . 67E- 01 1 . 53E - 01
? = nuclide is part of an undetermined solution X nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 97
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 8:41 :45AM Page 5 of? Analysis Report for L2-SUB-102-QJGS-006-SB 04/04/18 -1038 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/6/2018 8:41 :36AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 75 . 82 7 . l 7751E - 02 12 . 66 -(J,,~e; F 5 338 . 37 l . 20095E - 02 26 . 36 Tol. AC - 228 PA-228 F 7 583 . 03 2 . 84312E - 02 12 . 13 /;/-- t,df? F 9 910 . 74 2 . 20790£-02 13 . 03 Tol. AC - 228 PA- 228 F 12 1331 . 57 6 . 00965E - 03 25 . 37 Tol. CO- 60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCl/grams) (pCi/grams) (pCl/grams) (keV)
+ K- 40 1460 . 75
- 10 . 67 4 . 42E+00 4 . SSE - 01 4 . 55E - 01
+ AR- 41 1293 . 64 99 . 16 - 1 . 10E+06 1 . 24E+06 l . 24E+06
+ CO-60 1173 . 22 100 . 00 1. 39E - 02 3 . 62E - 02 / 4 . 67E - 02 1332 . 49 100 . 00 9 . 49E - 03 3 . 62E - 02 KR- 85 513 . 99 0 . 43 8 . 86E+00 7 . 65E+00 7 . 65E+00
+ Y- 88 898 . 04 93 . 70 2 . 86E-02 2 . 49E - 02 3 . 82E- 02 1836 . 06 99 . 20 9 . 0SE - 03 2 . 49£ - 02
+ NB- 94 702 . 63 100 . 00 - 2 . 41E - 02 3 . 08E - 02 3 . 08E - 02 871 . 10 100 . 00 - l . 91E-02 3 . 30E-02 10/7/2020 Page 98
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 8:41 :45AM Page 6 of 7 Analysis Report for L2-SUB-102-QJGS-008-SB 04(04(18 -1038 Nuclide Energy Yield(%) Activity Nuclide MDA UneMDA Name (pCilgrams) (pCi/grams) (pCilgrams) (keV)
+ I-131 284 . 30 6 . 06 3 . 77E - 01 3 . 58E-02 4 . 88E - 01 364 . 48 81. 20 5.47E - 03 3 . 58E - 02 636 . 97 7 . 27 - 4 . 48E - 02 4 . 55E-0l
+ CS-134 604 . 70 97 . 60 -6 . 21£-03 4 . 19£-02 4 . 19E- 02 795 . 84 85 . 40 3 . 19E-02 4 . 28E-02
+ CS - 137 661 . 65 85 . 12 4 . 14E-02 4. 33E-02 / 4 . 33E - 02 CE-144 80 . 12 1. 36 -4 . 04£-01 2.13E-01 2 . 67E+00 133 . 51 11.09 4 . 00E - 02 2 . 13E-01
+ EU-152 121 . 78 28 . 40 -9.64E-03 8 . 36E-02 / 8 . 36E-02 244 . 69 7 . 49 -3 . 43E-01 3 . 91E - 01 964 . 00 14 . 44 3 . 49E - 0l 3 . 20E - 01 1408 . 00 20 . 74 6.06E - 02 l . 61E-01
+ EU - 154 123 . 07 40 . 40 4 . 39E - 03 5 . 91E-02 / 5 . 91E-02 247 . 94 6 . 60 -7 . 71E- 01 3 . 88E - 01 723 . 30 19 . 70 -l.06E- 02 l . 70E - 01 873 . 20 11 . 50 - 6 . 99E-02 2 . 89E-01 1004 . 76 17 . 90 -7.23E-02 2 . 0lE-01 1274 . 51 35 . 50 4 .4 5E- 02 1. 27E-0l
+ EU - 155 86 . 54 32 . 80 - 3 . 23E-02 9 . 39E-02 9 . 39E-02 105 . 31 21. 80 - 6 . 85E - 02 1 . l0E - 01
+ BI-214 609 . 31 46.30 l . 14E-01 7 . 54E-02 7 . 54E - 02 1120 . 29
- 15 . 10 1. 83E-01 1. 82E-01 1238 . 11
- 5 . 94 3 . 70E-01 S . 06E-01 1377 . 67 4 . 11 9 . 65E-01 8 . 53E - 01 1407 . 98 2 .4 8 5 . 07E- 01 1 . 34E+00 1509 . 19 2 . 19 - 1 . 82E-01 1.31E+00 1764 . 49
- 15 . 80 1. 34E- 01 1 . 90E - 01
+ PB - 214 77 . 11 10 . 70 1 .8 1E- 01 7 . 93E - 02 3 . 59E - 01 295 . 21
- 19 . 20 l . llE-01 9 . 29E - 02 351. 92
- 37 . 20 8 . 65E-02 7 . 93E - 02
+ PA-228 89 . 95 22 . 00 2 . 0lE- 01 3 . 36E - 01 5 . 66E - 01 93 . 35 35 . 00 1 . 58E- 02 3 . 36E-01 105 .0 0 16 . 30 -5.53E-01 6 . 18E- 01 129 . 22 2 . 97 2 . 92E+00 3 . 39E+00 338 . 32 5 . 30 l . 99E+00 2 . 17E+00 463 . 00 13 . 80 1. 03E-01 8 . 34E-01 911 . 23 16 . 70 1 . 18E+00 1. 09E+00
+ AM-241 59 . 54 36 . 30 4 . 79E - 02 l . 70E - 01 l . 70E- 01
+ CM - 243 103 . 76 23 . 00 -6 . 48E-0 2 l . 06E - 0l l . 06E - 01 228 . 18 10 . 60 -2 . 12E-0 1 2 . 07E-0l 277 . 60 14 . 00 -l.20E-01 1.81E-01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 99
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 8:41 :45AM Page 7 of7 Analysis Report for L2-SUB-102-QJGS-008-SB 04/04/18 -1038 10/7/2020 Page 100
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 4:38:11 PM Page J of6
~~~pex-Gamma Analysis Report for L2-SUB-102-AJGS-009-SB 04/04/18 - 1054 L- L - D\l - {02 l<.A
(._v-J t> So~ ( GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-009--SB j Sample Description : 04/04/18- 1054 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 1.071E+03 grams j Facility : Dairyland_NPP Sample Taken On : 4/4/2018 10:54:00AM Acquisition Started : 4/5/2018 3:37:48PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611.4 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4227 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/5/2018 4:38:02PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 1
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 <+:38:11PM Page 2 of6 Analysis Report for L2-SUB-102-AJGS-009-SB 04/04/ 18 - 1054 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 76 . 61 147 - 161 153 . 77 l . 97E+02 61 . 77 1 . 47E+03 3 . 15 F 2 238 . 69 4 69 - 485 477 . 85 3 . 63E+02 47 . 41 6 . 98E+02 1. 69 F 3 295 . 22 586 - 594 590 . 88 8 . 93E+Ol 27 . 60 2.55E+02 1. 26 F 4 338 . 31 671 - 684 677 . 06 5 . 58E+Ol 24 . 48 3 . 31E 02 1. 49 F 5 351. 90 699 - 717 704 . 22 l . 60E+02 32 . 19 3 . 97E+02 1. 53 F 6 402 . 40 802 - 809 805 . 21 2 . 34E+Ol 16 . 48 1 . 14E+02 1. 21 F 7 583 . 25 1161 - 1174 1166 . 85 1 . 29E+02 26 . 47 1 . 39E+02 1. 62 F 8 609 . 33 1212 - 1227 1218 . 99 l . 23E+02 25 . 60 l . 40E+02 1. 67 F 9 726 . 98 1449 - 1460 1454 . 25 3 . 59E+Ol 16 . 68 8 . 72E+Ol 1. 70 F 10 911 . 11 1814 - 1830 1822 . 46 8 . 51E+Ol 22 . 36 8 . 09E+Ol 2 . 93 F 11 968 . 73 1933 - 1945 1937 . 68 3 . 07E+Ol 15 . 20 7 . 43E+Ol 1. 66 F 12 1460 . 66 2913 - 2929 2921.44 5 . 18E+02 46 . 43 2 . 97E+Ol 2 . 42 M = First peak in a multiplet reg ion m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/5/2018 4:38:02PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76 . 61 l . 97E+02 61 . 77 l . 97E+02 6 . 18E+Ol F 2 238 . 69 3 . 63E+02 47 . 41 3 . 63E 02 4 . 74E+Ol F 3 295 . 22 8 . 93E+Ol 27 . 60 8 . 93E+Ol 2 . 76E+Ol F 4 338 . 31 5 . 58E+Ol 24 . 48 5 . 58E+Ol 2 . 45E+Ol F 5 351. 90 l . 60E+02 32 . 19 8 . 36E+Ol 3 . 72E+Ol 7 . 64E+Ol 4 . 92E+Ol F 6 402 . 40 2 . 34E+Ol 16 . 48 2 . 34E+Ol 1 . 65E+Ol F 7 583 . 25 l . 29E+02 26 . 47 1 . 29£+02 2 . 65E+Ol F 8 609 . 33 1. 23£+02 25 . 60 4 . 12E+Ol 2 . 42E+Ol 8 . 18£+01 3 . 52E+Ol F 9 726 . 98 3 . 59E+Ol 1 6 . 68 3 . 59E+Ol 1 . 67E+Ol F 10 911 . 11 8 . SlE+Ol 22 . 36 8 . SlE+Ol 2 . 24E+Ol F 11 968 . 73 3 . 07E+Ol 15 . 20 3 . 07E+Ol l. 52E+Ol F 12 1460 . 66 5 . 18E+02 4 6 . 43 5 . 63E+Ol 1 . 71E+Ol 4 . 61E+02 4 . 95E+Ol 10/7/2020 Page 2
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 4:38:1 1PM Page 3 of6 Analysis Report for L2-SUB-102-AJGS-009-SB 04/04/18 - 1054 M = First peak in a multiplet region m = Other peak in a multiplet reg ion F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0 . 99 1460 . 75
- 10 . 67 4 . 69E+OO 5 . 67E- Ol BI-212 0 . 60 727 . 1 7
- 11. 80 1. 78E - 01 8 . 32E-02 785 . 42 2 . 00 1620 . 56 2 . 75 PB-212 0 . 98 77 . 11
- 17 . 50 2 . 61E-01 8 . 38E- 02 238 . 63
- 44 . 60 1. 75E - 01 2 . 46E - 02 BI - 214 0 . 35 609 . 31
- 4 6 . 30 8.79E - 02 3 . 82E - 02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB- 214 0 . 99 77 . 11
- 10 . 70 4 . 28E - 01 1 . 37E- 01 295 . 21
- 19 . 20 l.19E-01 3 . 73E - 02 351 . 92
- 37 . 20 6 . 16E- 02 3 . 98E - 02 AC-228 0 . 61 209 . 28 4 . 40 338 . 32
- 11. 40 l . 42E - 01 6 . 25E-02 794 . 70 4 . 60 911 . 60
- 27 . 70 2 . 20E - 01 5 . 87E- 02 964.60 5 . 20 969 . 11
- 16 . 60 l . 40E - 01 6.96E-0 2
* = Energy line found in the spectrum.
* = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma 10/7/2020 Page 3
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 4:38:11PM Page 4 of6 Analysis Report for L2-SUB-102-AJGS-009-SB 04/04/18 - 1054 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) K- 40 0 . 999 4 . 69E+00 5 . 67E-01 BI-212 0 . 601 l . 78E - 01 8 . 32£- 02 PB- 212 0 . 988 l . 77E - 01 2 . 36£ - 02 BI - 214 0 . 350 8 . 79£- 02 3 . 82E- 02 PB- 214 0 . 994 9 . 40E - 02 2 . 678 - 02 AC - 228 0 . 612 l . 71E-0l 3 . 64£-02
? = nuclide Is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 4
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 4:38:11PM Page 5 of 6 Analysis Report for l2-SUB-102-AJGS-009-SB 04104/18 - 1054 UNIDENTIFIED PEAKS Peak locate Performed on : 4/5/2018 4:38:02PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (ke V) Peak Size (CPS) Uncertainty Type Nuclide F 6 402 . 40 6 . 48731£-03 35 . 28 F 7 583 . 25 3 . 58366£-02 10 . 26 M = First peak in a multiplet reg ion m = Other peak in a multiplet reg ion F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCl/grams) (pCilgrams) (pCilgrams) (keV)
+ K- 40 1460 . 75
- 10 . 67 4 . 69E+00 4 . 71E - 01 4 . 71E- 01
+ AR- 41 1293 . 64 99 . 16 8 . 25E+02 2 . 58E+ 03 2 . 58E+03
+ CO-60 1173 . 22 100 . 00 2 . 32E- 03 4 . 26E - 02 / 4 . 60E- 02 1332 . 49 100 . 00 3 . 94E- 02 4 . 26E - 02
+ KR - 85 513 . 99 0 . 43 7 . 72E+00 7 . 78E+00 7 . 78E+00
+ Y- 88 898 . 04 93 . 70 - 7 . 72E - 03 3 . 27E-02 3 . 89E-02 1836 . 06 99 . 20 -3 . 90E-02 3 . 27E - 02
+ NB - 94 702 . 63 100 . 00 -2 . 4 4E-02 3 . 32E - 02 3 . 32E-02 871.10 100 . 00 - 4 . 67E - 02 3 . 36E - 02
+ I-131 284 . 30 6 . 06 2 . 14E - 02 3 . 41E - 02 4 . 54E - 01 36 4. 48 81. 20 3 . 26E - 03 3 . 41E- 02 636 . 97 7 . 27 l . 99E-02 4 . 38E- 01
+ CS - 134 604 . 70 97 . 60 -5 . l0E - 03 4 . 07E-02 4 . 07E - 02 795 . 84 85 . 40 - l . 79E- 02 / 4 . 30E- 02
+ CS - 137 661 . 65 85 . 12 4 . 06E- 02 4 . 41E-02 4 . 41E- 02 10/7/2020 Page 5
LAC LTP - Final Status Survey Package - 3/21/2018 4/5/2018 4:38:11PM Page 6 of6 Analysis Report for L2-SUB-102-AJGS-009-SB 04/04/18 - 1054 Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV)
+ CE - 144 80 . 12 1. 36 - 9 . 63E - 01 2 . 20E - 01 2 . 72E+OO 133 . 51 11.09 1. 21E-01 2 . 20E - 01
+ EU-152 121 . 78 28 . 40 -5 . 18E-02 8 . 30E-02 ./ 8 . 30E - 02 244 . 69 7 . 49 -3 . 70E - 01 3 . 94E - 01 964 . 00 14 . 44 - l . 45E - 01 3 . 04E - 01 1408 . 00 20 . 74 7 . 66E - 02 1. 79E-01
+ EU-154 123 . 07 40 . 40 -3 . 20E-02 5 . 83E-02 v' 5 . 83E - 02 247 . 94 6 . 60 - 4 . 54E - 01 3 . 87E-01 723 . 30 19 . 70 7 . 55E - 02 1 . 82E - 0 1 873 . 20 1 1.50 l . 37E - 01 3 . 04E - 01 1004 . 76 17 . 90 - l . 58E- 02 2 . 16E- 01 1274 . 51 35 . 50 - 1 . 93E- 02 l . 23E-01
+ EU-155 86 . 54 32 . 80 - 3 . 51E-02 9 . 42E-02 9 . 42E - 02 105 . 31 21. 80 6 . 46E - 03 l . 14E-Ol
+ BI-214 609.31
- 4 6 . 30 8 . 79E - 02 7 . 35E-02 7 . 35E-02 1120 . 29 15 . 10 - l . 65E - 01 3 . 00E - 01 1238 . 11 5 . 94 4 . 14E - 01 9 . 18E-Ol 1377 . 67 4 . 11 7 . 72E - 01 9 . 34E - 01 1407 . 98 2 . 48 6 . 41E-01 1 . 50E+OO 1509 . 19 2 . 19 - 1 . 35E+OO 1. 32E+OO 1764 . 49 15 . 80 l . 38E-Ol 2 . 16E- 01
+ PB- 214 77 . 11
- 10 . 70 4 . 28E- 01 7 . 62E-02 3 . 35E - 01 295 . 21
- 19 . 20 l . 19E- 01 7 . 62E-02 351. 92
- 37 . 20 6 . 16E- 02 9 . 08E - 02
+ PA- 228 89 . 95 22 . 00 2 . 94E - 01 2 . 03E- 01 3 . 43E-01 93 . 35 35 . 00 - 3 . lBE - 02 2 . 03E - 01 105 . 00 16 . 30 - 1 . 47E-02 3 . 84E- 01 129 . 22 2 . 97 - 6 . 16E- 01 1 . 99E+OO 338 . 32 5 . 30 l . 14E +OO 1.29E+OO 463 . 00 13 . 80 1 . 61E - 01 5 . 37E - Ol 911 . 23 16 . 70 9 . 66E- 01 7 . 12E- 01
+ AM- 241 59 . 54 36 . 30 6 . 78E- 02 l . 73E - 01 l.73E - 01
+ CM - 243 103 . 76 23 . 00 - 3 . lSE-02 l.09E-01 l . 09E-01 228 . 18 10 . 60 - 1 . 63E-01 2 . 2 1 E-Ol 277 . 60 14 . 00 - l . 31E - 0 1 1. 82E - 01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 6
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/21J1d 6:10:11 AM Page I of7 pex-Gamma Analysis Report for L2-SUB-102-AJGS-010-SB 04/04/18 - 1254 L 2.-. O\\ i.. ~ A. c_v t> sq~ I GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-010-SB / Sample Descriptlon : 04/04/18 - 1254 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 1.016E+03 grams / Facility : Dairyland_ NPP Sample Taken On : 414/2018 12:54:00PM Acquisition Started : 4/6/2018 5:09:48AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live nme : 3600.0 seconds Real Time : 361 1.5 seconds Dead Time : 0.32% Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100- 4096 Peak Area Range (in channels) : 100- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Description Sample Number : 4229 PEAK ANALYSIS REPORT Peak Analysis Perfomned on : 4/6/2018 6:10:02AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 7
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 6:10:11AM r age 2 of 7 Analysis Report for L2-SUB-102-AJ GS-010-SB 04/04/18 -- 1254 Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) M 1 74 . 49 145 - 161 149 . 52 9 . 22E+Ol 37 . 41 8 . 72E 02 1. 43 m 2 76 . 98 145 - 161 154 . 50 1 . 67E+02 42 . 49 7 . 93E+02 1. 44 F 3 186 . 03 369 - 378 372 . 57 7 . 37E+Ol 33 . 76 5 . 70E 02 1. 43 F 4 238 . 49 471- 481 477 . 45 2 . 82E+02 44 . 34 5 . 20E+02 1.38 F 5 338 . 29 670 - 681 677 . 01 6 . 17E+Ol 24 . 33 2 . 92E+02 1.28 F 6 351 . 86 697 - 712 704 . 15 1 . 66E+02 32 . 48 3 . 58E+02 1.59 F 7 582 . 99 1159 - 1174 1166 . 31 1 . 10E+02 24 . 51 l . 19E+02 1.85 F 8 609 . 14 1210 - 1224 1218 . 61 1 . 06E+02 23 . 96 1. 24E 02 1. 57 F 9 910 . 89 1815 - 1829 1822 . 02 8 . 30E+Ol 21 . 64 9 . 82E+Ol 1.85 F 10 1120 . 22 2235 - 2245 2240 . 63 2 . 54E+Ol 13 . 43 5 . 98E+Ol 1 . 25 E' 11 1460 . 54 2911 - 2930 2921 . 20 5 . 00E+02 45 . 18 2 . 52E+Ol 2 . 57 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/6/2018 6:10:02AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\000000 1364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. M 1 7 4 . 49 9 . 22E+Ol 37 . 41 9 . 22E+Ol 3 . 74E+Ol m 2 76 . 98 l . 67E +02 42 . 49 1 . 67E+02 4 . 25E+Ol F 3 186 . 03 7 . 37E+Ol 33 . 76 7 . 37E+Ol 3 . 38E+Ol F 4 238 . 49 2 . 82E+02 44 . 34 2 . 82E+02 4 . 43E+Ol F 5 338 . 29 6 . 17E+Ol 24 . 33 6 . 17E+Ol 2 . 43E+Ol F 6 351 . 86 1 . 66E+02 32 . 48 8 . 36E+Ol 3 . 72E+Ol 8 . 19E+Ol 4 . 94E+Ol F 7 582 . 99 l . 10E+02 24 . 51 1 . 10E+02 2 . 45E+Ol F 8 609 . 14 l . 06E+02 23 . 96 4 . 12E+O l 2 . 42E+Ol 6 . 49E+Ol 3 . 41E+Ol F 9 91 0 . 89 8 . 30E+Ol 21. 64 8 . 30E+Ol 2 . 16E+Ol F 10 1120 . 22 2 . 5 4E+Ol 13 . 43 2 . 5 4E+Ol 1 . 34E+Ol F 11 1460 . 5 4 5 . 00E+02 45 . 18 5 . 63E+ Ol 1 . 71E+Ol 4 . 43E+02 4. 83E+Ol M = First peak in a multiplet reg ion m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma 10/7/2020 Page 8
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/201 o 6:10:11AM Page 3 of7 Analysis Report for L2-SUB-102-AJGS-010-SB 04/04/18 - 1254 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0 . 99 1460 . 75
- 10 . 67 4 . 75E+OO 5 . 81E - 01 PB-212 0 . 99 77 . 11
- 17 . 50 2 . 32E-01 6 . 09E-02 238 . 63
- 44 . 60 1 . 43E - 01 2 . 37E - 02 BI - 214 0 . 58 609 . 31
- 46 . 30 7 . 35E - 02 3 . 88E - 02 1120 . 29
- 15 . 10 l . 53E - 01 8 . llE - 02 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 176 4 . 4 9 15 . 80 PB - 214 0 . 52 77 . 11
- 10 . 70 3 . 80E - 01 9 . 97 E- 02 295 . 21 19 . 20 351 . 92
- 37 . 2 0 6 . 97E - 02 4 . 21E -0 2 RA- 226 0 . 99 186 . 21
- 3 . 28 4. 28E - 01 l . 97E - 01
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) 10/7/2020 Page 9
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 6:10:11AM Page4 of7 Analysis Report for L2-SUB-102-AJGS-010-SB 04/04/18 - 1254 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) K- 40 0 . 993 4 . 75E+00 5 . 81E-01 PB-212 0 . 997 l . 48E - 01 2 . 23E - 02 BI-214 0 . 582 8 . 82E - 02 3 . S0E - 02 PB- 214 0 . 526 7 . 99E - 02 3 . 92E-02 RA- 226 0 . 995 4 . 28E - 01 l . 97E-01
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used In Weighted Mean Activity Errors quoted al 2.000sigma 10/7/2020 Page 10
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 6:10:11 AM Page 5 of7 Analysis Report for L2-SUB-102-AJGS-010-SB 04/04/18 - 1254 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/6/2018 6:10:02AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 1 74 . 49 2 . 56207£-02 20.28 r1, ~ vz../i i' + t,-41i F 5 338 . 29 1. 71282E-02 19 . 73 Tol. AC-228 PA-228 F 7 582 . 99 3 . 06625E-02 11 . 10 -r1--l,A)i F 9 910 . 89 2.30672£-02 13 . 03 Tol. AC - 228 PA-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCilgrams) (pCl/grams) (keV)
+ K-40 1460 . 75
- 10 . 67 4 . 75E+00 4 . 94E-01 4.94E-01
+ AR-41 1293 . 64 99 . 16 -3 . 41E+05 1 . 90E+05 / 1 . 90E+0S
+ CO-60 1173 . 22 100 . 00 3 . 0SE-02 4 . 52E - 02 5 . 52E-02 1332 . 49 100 . 00 3 . 22E-02 4 . 52E- 02
+ KR-85 513 . 99 0 . 43 8 . 89E+00 8 . 28E+00 8 . 28E+00
+ Y-88 898 . 04 93 . 70 7 . 03E-03 2 . 92£-02 4 . 24E- 02 1836 . 06 99 . 20 7 . 90E-03 2 . 92E-02
+ NB-94 702 . 63 100 . 00 l . 62E-02 3 .4 8£-02 3 .4 8E- 02 871.10 100 . 00 -1 . 07E-02 3 . 56E-02 10/7/2020 Page 11
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 6: 10:11AM Page 6 of 7 Analysis Report for L2-SUB-102-AJGS-010-SB 04/04/1 8 - 1254 Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCilgrams) (keV)
+ I - 131 284 . 30 6 . 06 4.35E - 01 3 . 89E- 02 5.12E - 01 364 . 48 81. 20 2 . 32E-02 3 . 89E-02 636 . 97 7 . 27 7 . 43E- 02 5 . 25E - 01
+ CS - 134 604 . 70 97 . 60 5 . 85E - 03 4 . 00E- 02 4 . 00E- 02 795 . 84 85 . 40 - 7 . 06E-03 4 . 39E-02
+ CS - 137 661 . 65 85 . 12 6 . 82E-02 4 . 79E - 02 / 4 . 79E-02
+ CE - 144 80 . 12 1. 36 - 4 . 20E-01 2 . 19E- 01 2 . 83E+OO 133 . 51 11 . 09 -5 . 70E-02 2 . 19E-Ol
+ E0-152 121 . 78 28 . 40 l . 05E - 02 8 . 77E - 02 . / 8 . 77E - 02 244 . 69 7 . 49 -9 . 96E-Ol 4 . 08E- 01 964 . 00 14 . 44 3 . 08E - 01 3 . 07E - 01 1408 . 00 20 . 74 2 . 67E-02 l . 80E-01 EU-154 123 . 07 40 . 40 3 . 40E-02 6 .14E-02 j 6 . 14E-02 247 . 94 6 . 60 -l . 92E+OO 4 . 12E-01 723 . 30 19 . 70 l.14E-02 l . 85E-01 873 . 20 11. 50 -8 . 93E-02 3 . 12E-01 1004 . 76 17 . 90 l . 59E-02 2 . 40E-01 1274 . 51 35 . 50 2 . 78E-02 1 . 33E - 01
+ EU - 155 86 . 54 32 . 80 2 . 96E- 02 9 . 7BE - 02 9 . 7BE - 02 105 . 31 21. 80 - l . 56E- 02 1.20E- 01
+ BI-214 609 . 31
- 46 . 30 7 . 35E-02 7 . 43E - 02 7 . 43E-02 1120 . 29 15 . 10 l . 53E-01 1 . 83E-Ol 1238 . 11 5 . 94 -2 . 85£-01 9 . 28E-Ol 1377 . 67 4 . 11 4 . 90E-Ol 8 . 31E-01 1407 . 98 2 . 48 2 . 24E-01 1 . 50E+OO 1509 . 19 2 . 19 5 . lOE - 01 1. 54E+OO 1764 . 49 15 . 80 4 . 49E- 02 2 . 43E - 01
+ PB - 214 77 . 11
- 10 . 70 3 . 80E- 01 8 . 94E - 02 2 . 17E- 01 295 . 21 19 . 20 2 . 66E- 02 l . 48E - 01 351 . 92
- 37 . 20 6 . 97E-02 8 . 94E- 02
+ PA - 228 89 . 95 22 . 00 5 . llE- 01 2 . 99E - 01 5 . lOE - 01 93 . 35 35 . 00 - l . 78E- 03 2 . 99E - 01 105 . 00 16 . 30 2 . 57E- 01 5 . 83E - 01 129 . 22 2 . 97 l . 02E+OO 3 . 00E+OO 338 . 32 5 . 30 l . 28E+OO 2 . 0lE+OO 463 . 00 13 . 80 - l . 54E- 02 7 . 83E - 01 911 . 23 16 . 70 9 . 83E - 01 l . 05E+OO
+ AM - 241 59 . 54 36 . 30 -l . 66E-02 1 . 77E-01 l . 77E - 01
+ CM - 243 103 . 76 23 . 00 5 . 07E- 02 1 . 15E- 01 l . 15E- 01 228 . 18 10 . 60 1. 08E- 01 2 . 32E - 01 277 . 60 14 . 00 - 1.59E- 01 l . 91E - 01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 12
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 6:10:11AM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-010-SB 04/04/18 - 1254 10/7/2020 Page 13
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 7:20:01AM Page I of6
~~~pex-Gamma Analysis Report for l 2-SUB-102-AJGS-011-SB 04/04/18 - 1454 L- -z.. - o \ l - \ o --i.. {<..A L.-v-.) D c; o 7 (
GAMMA SPECTRUM ANALYSIS Sample Identification : l2-SUB-102-AJGS-011-SB 7' Sample Description : 04/04/18 - 1454 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 1.116E+03 grams / Facility : Dairyland_NPP
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/ 4..
1 0 Sample Taken On : 4/4/2018 2:~00PM Acquisition Started : 4/6/2018 6:19:38AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611.4 seconds Dead Time : 0.32 % Peak locate Threshold : 3.00 Peak locate Range (in channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4230 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/6/2018 7:19:52AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 14
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 7:20:0 1AM Page 2 of 6 Analysis Report for L2-SUB-102-AJGS-011-SB 04/04/18 - 1454 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 75 . 87 147 - 159 152 . 28 2 . 64E+02 63 . 07 l.31E -r- 03 3 . 67 F 2 238.52 472 - 485 477.52 3 . 35E+02 46 . 4 9 6 . 58E + 02 1. 45 F 3 295 . 15 584 - 596 590.75 1 . 06E+02 30 . 87 3 . 57E+02 1. 75 F 4 338 . 24 668 - 683 676.92 8 . 80E+Ol 28 . 67 3.52E +02 1. 96 F 5 351 . 89 699 - 712 704 . 20 l . 53E+02 32.19 3 . 21E +02 1. 59 F 6 583 . 25 1161 - 1172 1166 . 83 l . 15E+02 25 .6 8 l . 35E+02 1 . 55 F 7 609 . 14 1212 - 1225 1218 . 61 l . 07E+02 25 . 76 1 . 55E+ 02 1. 91 I F 8 911. 19 1816 - 1827 1822.62 7.24E+Ol 20.97 8 . lOE+O l 1. 96 F 9 968 . 59 1933 - 1942 1937 . 41 2 . 66E+Ol 16 . 38 9 . 21E + Ol 1. 60 F 10 1237 . 83 2471 - 2482 2475 . 82 2 . 36E+Ol 14 . 04 7 . 87E 01 1. 41 F 11 1460 . 47 2914 - 2929 2921 . 06 5 . 22E+02 47 . 63 3 . 29E +Ol 2 . 39 F 12 1763 .66 3523 - 3532 3527 . 40 2 . 0lE+Ol 9. 46 5 . 30E +OO 1. 36 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted al 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/6/2018 7:19:52AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 75 . 87 2 . 64E+02 63.07 2 . 64£+02 6 . 31E+Ol F 2 238 . 52 3.35E+02 46 .49 3 . 35E+02 4 . 65E+Ol F 3 295 . 15 l . 06E+02 30 . 87 1 . 06E+02 3.09E+O l F 4 338 . 24 8 . 80E+Ol 28 . 67 8 . BOE+Ol 2 . 87E+Ol F 5 351.89 1 .53 E+02 32 . 19 8.36E+Ol 3. 72E+Ol 6.98E+Ol 4 . 92E+Ol F 6 583 . 25 1. 15E+02 25 . 68 1.15E+02 2 . 57E+Ol F 7 609 . 14 l . 07E+02 25 . 76 4 . 12E+Ol 2 . 42E+Ol 6 . 56E+Ol 3 .5 4E+Ol F 8 911 . 19 7 . 24E+Ol 20 . 97 7 . 24E+Ol 2 . lOE+Ol F 9 968 . 59 2 .66E+Ol 16.38 2.66E+Ol l .6 4E+Ol F 10 1237 . 83 2 . 36E+Ol 14 . 04 2 . 36E+Ol 1 . 40E+Ol F 11 1460.47 5.22E+02 47 . 63 5 . 63E+Ol 1 . 71E+Ol 4 . 66E+02 5 . 06E+Ol F 12 1763 . 66 2 . 0lE+Ol 9 . 46 2 . 0lE+Ol 9 . 46E+OO 10/7/2020 Page 15
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 7:20:01 AM Page 3 of6 Analysis Report for L2-SUB-102-AJGS-011-SB 04/04/18 - 1454 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 98 1460 . 75
- 10 . 67 4 . 54E+OO 5 . 55E- 01 PB-212 0 . 55 77 . 11 17 . 50 238 . 63
- 44 . 60 1 . 55E-01 2 . 29E- 02 BI-214 0 . 61 609 . 31
- 46. 30 6 . 77E - 02 3 . 67E-02 1120 . 29 1 5 . 10 1238 . 11
- 5.94 3 . 59E-01 2 . 14E-01 1377 . 67 4 . 11 140 7 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49
- 15 . 80 l . 55E - 01 7 . 36E-02 PB-214 0 . 72 77 . 11 10 . 70 295 . 21
- 19 . 20 l . 35E-01 4.0lE-02 35 1 . 92
- 37 . 20 S .4 0E - 02 3 . 82E - 02 AC - 228 0 . 61 209 . 28 4 . 40 338 . 32
- 11 . 40 2 . 14E- 01 7 . 06E - 02 794 . 70 4 . 60 911 . 60
- 27 . 70 l . 80E-01 5 . 27E-02 964 . 60 5 . 20 969 . 11
- 16 . 60 1 . 16E- 01 7 . 19E- 02
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma 10/7/2020 Page 16
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 7:20:01AM Page 4 of6 Analysis Report for L2-SUB-102-AJGS-011-SB 04/04/18 - 1454 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams) K- 40 0 . 988 4 . 54E+00 5 . SSE - 01 PB-212 0 . 559 1 . SSE-01 2 . 29E-02 BI-214 0 . 619 9 . 13E- 02 3 . 24E-02 PB-214 0 . 721 9.26E-02 2 . 76£-02 AC-228 0 . 612 l . 73E-01 3 . 64£ - 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used In Weighted Mean Activity Errors quoted al 2.000sigma 10/7/2020 Page 17
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 7:20:01AM Page of 6 Analysis Report for l2-SUB-102-AJGS-011-SB 04/04/18 - 1454 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/6/2018 7:19:52AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(3/4) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 75 . 87 7 . 32501E - 02 11. 96 -z..o~ F 6 583 . 25 3 . 18932E- 02 11.18
--ft - ~t M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCilgrams) (pCi/grams)
(keV)
+ K-40 1460 . 75
- 10 . 67 4 . 54E+0O 4 . 58E - 01 4 . 58E - 0l
+ AR - 41 1293 . 64 99 . 16 8 . 23E+04 l . 50E+05 l . 50E+05
+ CO-60 1173 . 22 100 . 00 l.lBE - 02 4 . 14E- 02 / 4 . 86E - 02 1332 . 49 100 . 00 2 . 58E - 02 4 . 14E-02
+ KR - 85 513 . 99 0 . 43 1 . 17E+0l 7 . 67E+00 7 . 67E+00
+ Y- 88 898 . 04 93 . 70 -1 . 39E - 02 2 . 42E-02 3 . 95E-02 1836 . 06 99 . 20 l . 93E - 03 2 . 42E - 02
+ NB - 94 702 . 63 100 . 00 1 . 48E - 02 2 . 99E - 02 2 . 99E- 02 871 . 10 100 . 00 - 3 . 99E - 03 3 . 43E - 02
+ I-131 284 . 30 6 . 06 7 . 44E - 02 3 . 49E- 02 4 . 38E-01 364 . 48 81. 20 1. 42E- 02 3 . 49E-02 636 . 97 7 . 27 - 3 . 14E-01 4 . 80E-01
+ CS - 134 604 . 70 97 . 60 - 2 . 38E - 03 3 . 87E-02 3 . 87E-02 795 . 84 85 . 40 3 . 41E - 02 4 . 00E-02
+ CS - 137 66 1. 65 85 . 12 3 . 81E- 02 4 . 30E-02 / 4 . 30E- 02
+ CE - 144 80 . 12 1. 36 - 7 . 98E-01 2 . 07E-01 2 . 71E+0O 10/7/2020 Page 18
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 7:20:01AM Page 6 of6 Analysis Report for l2-SUB-102-AJGS-011-SB 04/04/ 18 - 1454 Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCilgrams) (pCilgrams) (pCl/grams) (keV) CE-144 133 . 51 11.09 -9 . 53E - 02 2 . 07E-Ol / 2 . 07E - 01
+ EU-152 121 . 78 28 . 40 -3 . 88E-02 8 . 0SE-02 8 . 08£-02 244 . 69 7 . 49 -3 . 34E-01 3 . 93E-01 964 . 00 14 . 44 3 . 23£ - 01 2 . 99E-01 1408 . 00 20 . 74 l . 60E-02 1. 68E- 01
+ EU - 154 123 . 07 40 . 40 4 . 56E - 03 5 . 73E-02 .I 5 . 73E - 02 247 . 94 6 . 60 - 5 . 25E - 01 3 . 92E - 01 723 . 30 19 . 70 5 . 72E- 02 1 . 74£ - 01 873 . 20 11 . 50 1 . 29E-01 3 . 03E-01 1004 . 7 6 17 . 90 -l.36E-02 2 . 00E - 01 1274 . 51 35 . 50 2 . 30£-02 1 . 09E-01
+ EU - 155 86 . 54 32 . 80 - 7 . 39£-02 9 . 13E- 02 9 . 13£-02 105 . 31 21 . 80 l . 14E- 02 1 . 12E-01
+ BI - 214 609 . 31
- 46 . 30 6 . 77£ - 02 7 . 0BE-02 7 . 08E - 02 1120 . 29 15 . 10 4 . 47E- 02 3 . 04E - Ol 1238 . 11 5 . 94 3 . 59E - Ol 5 . 40£ - 01 1377 . 67 4 . 11 9 . 91E - 02 7 . 56E-01 1407 . 98 2 . 48 l . 34E - 01 l . 41E+OO 1509 . 19 2 . 19 - 8 . 78E - 01 1. 25E+OO 1764 . 4 9
- 15 . 80 1 . 55£- 01 8 . 58£- 02
+ PB-214 77 . 11 10 . 70 5 . 94£-01 7 . 74E- 02 3 . 68E-01 295 . 21
- 19 . 20 l . 35E - 01 9 . SOE- 02 351. 92
- 37 . 20 5 . 40£-02 7 . 74E- 02
+ PA - 228 89 . 95 22 . 00 2 . 85£- 01 2 . 75£-01 4 . 61E- 01 93 . 35 35 . 00 3 . 94E - 03 2 . 75£-01 105 . 00 16 . 30 3 . 14E-Ol 5 . 32E-Ol 129 . 22 2 . 97 l . 65E+OO 2 . 76E+OO 338 . 32 5 . 30 7 . 08E-01 1 . 79E+OO 463 . 00 13 . 80 3 . 38E - Ol 7 . 03E- 01 911.23 16 . 70 l . 32E+OO 9 . 13E- 01
+ AM-241 59 . 54 36 . 30 - 7 . 63£- 03 1 . 66£-01 l . 66E - 01
+ CM- 243 103 . 76 23 . 00 3 . 22£-03 1. 07E - 01 l . 07E - 01 228 . 18 10 . 60 9 . 86E-03 2 . 14E- Ol 277 . 60 1 4 . 00 6 . 69E - 02 1 . 69£ - 01
+ = Nuclide identified during the nuclide identification
"' Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 19
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 7:35:04PM Page I of 6 pex-Gamma Analysis Report for L2-SUB-102-AJGS-012-SB L2-011-102 RACWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL GAMMA SPECTRUM ANAL YS/S Sample Identification : L2-SUB-102-AJGS-012-S8 Sample Description : L2-011-102 RACWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 8.718E+02 grams / Facility : Dairyland_NPP Sample Taken On : 4/5/2018 9:05:00AM Acquisition Started : 4/9/2018 6:34 :42PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3610.8 seconds Dead Time : 0.30% Peak Locate Threshold : 3.00 Peak Locale Range (in channels) : 100-4096 Peak Area Range (in channels) : 100- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/812014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4247 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/9/2018 7: 34:55PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 20
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 7:35:04 PM Page 2 of6 Analysis Report for L2-SUB-102-AJGS-012-SB L2-011-102 RA CWD SOIL / PACKAGE#: L2-SUB-102 RA CWD SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 77 . 03 147 - 158 154 . 61 l.29E+02 39 . 87 l.16E+03 1. 06 F 2 92 . 86 183 - 192 186 . 27 6 . 60E+Ol 35 . 42 8 . 48E+02 1.11 F 3 185.91 369 - 379 372 . 31 5 . 47E+Ol 27 . 46 5 . 91E+02 0 . 89 F 4 208 . 85 414 - 422 418 .1 9 4.81E+Ol 29 . 10 4 . 13E+02 1. 36 F 5 238 . 53 472 - 485 477 . 53 3 . 26E+02 44 . 98 5 . 74E+02 1. 46 F 6 295 . 18 586 - 597 590 . 82 7 . 72E+Ol 28 . 96 4 . 17E+02 1. 43 F 7 338 . 57 673 - 685 677 . 57 4 . 79E+Ol 23 . 57 3 . 15E+02 1 . 38 F 8 351 . 78 698 - 709 703 . 99 1 . 73E+02 32 . 31 2 . 56E+02 1. 45 F 9 582 . 93 1160 - 1171 1166 . 20 8 . 54E+Ol 23 . 22 1 . 35E+02 l. 56 F 10 609 . 10 1212 - 1223 1218 . 54 9 . 67E+Ol 23 . 63 l . 35E+02 1. 32 E' 11 726 . 86 1446 - 1459 1454 . 02 3.79E+Ol 16 . 13 6 . 93E+Ol 1 . 72 F 12 910 . 98 1817 - 1827 1822 . 19 5 .4 8E+Ol 18 . 22 5 . 93E+Ol 1. 68 M 13 964 . 46 1924 - 1943 1929 . 15 2 . 03E+Ol 12 .1 7 5 . 18E+Ol 1.57 m 14 968 . 61 1924 - 1943 1937 . 45 4 . 61E+Ol 16 . 74 6 . 21E+Ol 1. 57 F 15 1460 . 54 2914 - 2930 2921.19 5 . 61E+02 48 . 05 7 . 19E+OO 2 . 50 M = First peak in a multiplet region m ::: Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/9/2018 7:34:SSPM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 77 . 03 1 . 29E+02 39 . 87 1 . 29E+02 3 . 99E+Ol F 2 92 . 86 6 . 60E+Ol 35 . 42 6 . 60E+Ol 3 . 54E+Ol F 3 185 . 91 5 . 47E+Ol 27 . 46 5 . 47E+Ol 2 . 75E+Ol F 4 208 . 85 4 . 81E+Ol 29 . 10 4 . 81E+Ol 2 . 91E+Ol F 5 238 . 53 3 . 26E+02 44 . 98 3 . 26E+02 4 . 50E+Ol F 6 295 . 18 7 . 72E+Ol 28 . 96 7.72E+Ol 2.90E+Ol F 7 338 . 57 4 . 79E+Ol 23 . 57 4 . 79E+Ol 2 . 36E+Ol F 8 351 . 78 l . 73E+02 32 . 31 8 . 36E+Ol 3 . 72E+Ol 8 . 97E+Ol 4 . 93E+Ol F 9 582 . 93 8 . 54E+Ol 23 . 22 8 . 54E+Ol 2.32E+Ol F 10 609.10 9 . 67E+Ol 23 . 63 4 . 12E+Ol 2 . 42E+Ol 5 . SSE+Ol 3.38E+Ol F 11 726 . 86 3.79E+Ol 16.13 3.79E+Ol 1 . 61E+Ol F 12 910 . 98 5 . 48E+Ol 18 . 22 5 . 48E+Ol l.8 2E+Ol M 13 964 . 46 2 . 03E+Ol 12 . 17 2 . 03E+Ol 1.22E+Ol m 14 968.61 4 . 61E+Ol 16 . 74 4 . 61E+Ol 1 . 67E+Ol 10/7/2020 Page 21
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 7:35:04PM Page J of 6 Analysis Report for L2-SUB-102-AJGS-012-SB L2-011-102 RA CWD SOIL I PACKAGE#: L2-SUB-102 RA CWD SOIL Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. {keV) Area Uncertainty Background Uncert. Area Uncert. F 15 1460 . 54 5 . 61E+02 48 . 05 5 . 63E+Ol 1 . 71E+Ol 5 . 04E+02 5 . lOE+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 99 1460.75
- 10 . 67 6 . 30E+OO 7 . 27E -0 1 BI-212 0 . 59 727 . 17
- 11 . 80 2 . 31E - Ol 9 . 89E- 02 785 . 42 2 . 00 1620 . 56 2 . 75 PB- 212 0 . 99 77 . 11
- 17 . 50 2 . 09E- 01 6 . 59E - 02 238 . 63
- 44 . 60 l . 93E-Ol 2 . 8 4E- 02 BI - 214 0 . 34 609 . 31
- 4 6 . 30 7 . 33E - 02 4 . 49E - 02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 176 4.4 9 15 . 80 PB - 214 0 . 99 77 . 11
- 10 . 70 3 . 42E - 01 l . 08E- 01 295 . 21
- 19 . 20 l . 27E-01 4 . 79E - 02 351. 92
- 37 . 20 8 . 89E - 02 4 . 90E - 02 RA- 226 0 . 98 186 . 21
- 3 . 28 3 . 70E- 01 1 . 87£- 01 AC-228 0 . 86 209 . 28
- 4 . 40 2 . 62E - 01 l . 59E- 01 33 8 . 32
- 11 . 40 1 . SOE - 01 7 _40E - 02 794 . 70 4 . 60 911 . 60
- 27 . 70 l .7 4E - 01 5 . 84E - 02 964 . 60
- 5 . 20 3 . 62£ - 01 2 . 17E- 01 969 . 11
- 16 . 60 2 . 58E- 01 9 . 45£ - 02 10/7/2020 Page 22
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 , .J5:04PM Pagc4 of6 Analysis Report for L2-SUB-102-AJGS-012-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)
K-40 0 . 993 6 . 30E+00 7 . 27E - 01 BI-212 0 . 595 2 . 31E - 01 9 . 89E- 02 PB- 212 0 . 999 l . BSE - 01 2 . 63E-02 BI - 214 0 . 346 7 . 33E - 02 4 . 49E-02 PB- 214 0 . 998 l . 02E-01 3 . 29E-02 RA- 226 0 . 985 3 . 70E-01 l . 87E-01 AC - 228 0 . 865 l . 93E - 01 3 . 93E-02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 23
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 7:35:04PM Page 5 of6 Analysis Report for L2-SUB-102-AJGS-012-SB l2-011-102 RA CWD SOIL / PACKAGE#: L2-SUB-102 RA CWD SOIL UNIDENTIFIED PEAKS Peak Locate Performed on : 4/9/2018 7:34:55PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(3/4) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 92 . 86 l . 83377E - 02 26 . 82 Tol. PA- 228 F 9 582 . 93 2 . 37345E- 02 13 . 59 11-- l;l)'b M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{3/4) Activity Nuclide MDA LineMDA Name (pCflgrams) (pCl/grams) (pCilgrams) (keV)
+ K- 40 1460 . 75
- 10 . 67 6 . 30E+00 5 . 20E- 01 5 . 20E- 01
+ AR- 41 1293 . 64 99 . 16 - 9 . 50E+15 1 . 35E+16 j 1 . 35E+16
+ CO- 60 1173 . 22 100 . 00 2 . 40E - 02 5 . 24E - 02 6 . 42E - 02 1332 . 49 100 . 00 2 . l0E - 02 5 . 24E - 02
+ KR- 85 513 . 99 0 . 43 1.43E+0 l l . 02E+0l 1 . 02E+0l
+ Y- 88 898 . 04 93 . 70 4 . 86E - 02 3 . 66E - 02 4 . 96E - 02 1836 . 06 99 . 20 - 2 . 72E - 02 3 . 66E - 02
+ NB - 94 702 . 63 100 . 00 - 5 . 24E- 03 3 . 84E-02 3 . 84E - 02 871.10 100 . 00 - 7 . 33E - 02 3 . 96E- 02
+ I - 131 284 . 30 6 . 06 4 . 20E-01 5 . 46E- 02 7 . S0E- 01 364 .4 8 81 . 20 -5 . 92E - 02 5 . 46E - 02 636 . 97 7 . 27 7 . 69E-02 7 . 36E- 01
+ CS-134 604 . 70 97 . 60 6 . 59E - 02 4 .79E-02 4 . 79£- 02 795 . 84 85 . 40 4 . 06E - 02 / 5 . 08E - 02
+ CS - 137 661 . 65 85 . 12 8 . 03E - 02 5 . S0E- 02 5 . 50£- 02 10/7/2020 Page 24
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 7:35:04PM Page 6 of 6 Analysis Report for L2-SUB- 102-AJGS-012-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Nuclide Energy Yield(%) Activity NuclideMDA Line MDA Name (pCi/grams) (pCilgrams) (pCilgrams) (keV}
+ CE- 144 80 . 12 1. 36 - 3 . 93 E+O0 2 . 64E-0l 3 . 27E+00 133 . 51 11. 09 - 3 . 12E-0 2 2 . 64E - 01
+ EU - 152 121 . 78 28 . 40 - 3 . 79E - 02 1 . 0lE - 01 / 1 . 0lE - 01 244 . 69 7 . 49 - 3 . 00E- 01 4. 90E - 01 964 . 00 14 . 44 2 . 72E- 01 4 . 05E - 01 1408 . 00 20 . 74 7 . 67E - 02 / 2 . 07E - 01
+ EU - 154 123 . 07 40 . 40 5 . 89E - 03 7 . 14E- 02 7 . 14E-02 2 4 7 . 94 6 . 60 - 4 . 56E - 01 4. 96E - 01 723 . 30 19 . 70 l. l 9E - 02 2 . 13E - 01 873 . 20 11. 50 1 . 07E - 01 3 . 55E - 01 100 4 . 76 17 . 90 - 7 . 50E - 02 2 . 40E - 01 1274 . 51 35 . 50 l . 83E - 03 1. 29E- 01 EO- 155 86 . 54 32 . 80 5 . 21E - 03 1 . 14E- 01 l . 14E-01 105 . 31 21. 80 - 3 . 23E - 02 1 . 38E- 01
+ BI - 214 609 . 31
- 4 6 . 30 7 . 33E- 02 8 . 56E - 02 8 . 56E - 02 1120 . 29 15 . 10 1.29E- 01 3 . 87E-01 1238 . 11 5 . 94 9 . 12E - 01 1 . 09E+O0 1377 . 67 4 . 11 3 . 54£ - 01 1 . 06E+00 1407 . 98 2 . 48 6 . 41£ - 01 l . 73E+00 1509 . 19 2 . 19 6 . 15E - 01 l . 77E+00 1764 . 4 9 15 . 80 2 . SSE - 01 3 . 03E - 01
+ PB-214 77 . 11
- 10 . 70 3 . 42E- 01 9 . 20E- 02 3 . 39E-01 295 . 21
- 19 . 20 1 . 27E - 01 1 . 29E- 01 351 . 92
- 37 . 20 8 . 89E - 02 9 . 20E- 02 PA - 228 89 . 95 22 . 00 1 . 20E+00 2 . 75E+0O 4 . 71E+O0 93 . 35 35 . 00 - l . 82E+00 2 . 75E+0O 105 . 00 16 . 30 l.44 E+00 5 . 24E+0O 129 . 22 2 . 97 5 . 80E - 04 2 . 73E+0l 33 8. 32 5 . 30 1 .6 9E+0l 1 . 77E+0l 463 . 00 13 . 80 - l . 21E+0O 7 . llE+00 911. 23 16 . 70 5 . 25£+00 8 . 88E+O0
+ AM- 241 59 . 54 36 . 30 - 4 . 36E- 02 2 . 0SE - 01 2 . 05E - 01
+ CM - 243 103 . 76 23 .0 0 4 . 75E - 02 l . 33E - 01 l . 33E - 01 228 . 18 10 . 60 l . 09E - 01 2 . 62E - 01 277 . 60 1 4. 00 - 1. 38E - 01 2 . 19E - 01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 25
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 1:22:47PM Page I of 6 pex-Gamma Analysis Report for L2-SUB-102-QJGS-012-SB 04105/18 -0910 L. 7..,,- Ol l - l 'DZ... (<.t\: c....w ~ $ 0 ';° ( GAMMA SPECTRUM ANALYSIS Sample Identification : l2-SUB-102-QJGS-012-SB / Sample Description : 04/05/18 -0910 Sample Type : 500 ml Marinelli Unit Sample Point Sample Siz.e 8.790E+02 grams / Facility : Dairyland_NPP Sample Taken On : 4/5/2018 9:10:O0AM Acqu isition Started : 4/6/2018 12:22:24PM Procedure : 500ml Marinelli Operator : Adm inistrator Detector Name : HOTLAB Geometry : 500ml Marinelli live Time : 3600.0 seconds Real Time : 3611.3 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (In channels) : 100 - 4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/812014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Description Sample Number : 4235 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/6/2018 1:22:38PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 26
LAC LTP - Final Status Survey Package - 3/21/2018 4/612018 1:22:47PM Page 2 of 6 Analysis Report for L2-SUB-102-QJGS-012-SB 04/05/1 8 -0910 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 76 . 88 147 - 159 154 . 30 1 .36E+02 43 . 77 1. 12E 03 1. 52 F 2 238 . 50 470 - 481 477 . 47 2 . 68£+02 44 . 56 6 . 24E+02 1. 37 F 3 295 . 12 586 - 594 590 . 70 7 . 17E+Ol 27 . 68 2 . 98E+02 1. 33 F 4 338 . 4 9 671 - 681 677 . 41 6 . 41E+Ol 24.70 2.37E+02 1. 52 F 5 351 . 75 698 - 710 703 . 92 1 . 58E+o2 31. 35 2 . 70E+02 1.50 F 6 583 . 19 1159 - 1174 1166 . 73 1 . 03£+02 24 . 93 l .34 E+02 2.26 F 7 609 . 02 1214 - 1226 1218.37 9 . 90E+Ol 24 . 13 1 . 20E+02 1. 73 F 8 910 . 94 1813 - 1828 1822 . 11 5 . 59E+Ol 18 . 30 8 . 05E+Ol 2 . 04 F 9 969 . 24 1933 - 1943 1938 . 70 3 . 28E+Ol 14 . 38 5 . 93E+Ol 1. 38 F 10 1120 . 28 2236 - 2247 2240 . 75 2 . 88E+Ol 13 . 29 4.33 E+Ol 1. 48 F 11 1331 . 99 2660 - 2669 2664 . 12 l.44E+Ol 9 . 34 2 . 77E+Ol 0 . 98 F 12 1460 . 47 2911- 2930 2921 . 06 4.96E+02 45 . 32 4.50 E+Ol 2 .4 2 F 13 1763 . 96 3523 - 3532 3527 . 99 3 . 04E+Ol 12 . 35 l.24E+Ol 2 .11 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/6/2018 1:22:38PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. {keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76 . 88 1.36E+02 43 . 77 1 . 36E+02 4 . 38E+Ol F 2 238 . 50 2 . 68E+02 44 . 56 2 . 68E+02 4.46E+Ol F 3 295 . 12 7 . 17E+Ol 27 . 68 7 . 17E+Ol 2 . 77E+Ol F 4 338 . 49 6 . 41E+Ol 24 . 70 6 . 41E+Ol 2 . 47E+Ol F 5 351. 75 1. 58E+02 31. 35 8 . 36E+Ol 3 . 72E+Ol 7 . 48E+Ol 4 . 87E+Ol F 6 583 . 19 1. 03E+02 24 . 93 l . 03E+02 2 . 49E+Ol F 7 609 . 02 9 . 90E+Ol 24 . 13 4.12E +Ol 2 . 42E+Ol 5 . 78E 01 3 . 42E+Ol F 8 910 . 94 5 . 59E+Ol 18 . 30 5 . 59E+Ol l . 83E+Ol F 9 969 . 24 3 . 28E+Ol 14 . 38 3 . 28E+Ol l . 44E+Ol F 10 1120 . 28 2 . 88E+Ol 13 . 29 2 . 88E+Ol 1. 33E+Ol F 11 1331 . 99 l.44E+Ol 9 . 34 1 . 44£+01 9.34E+OO F 12 1460 .4 7 4 . 96E+02 45.32 5 . 63E+Ol l . 71E+Ol 4 . 40E+02 4 . 85E+Ol F 13 1763 . 96 3 . 04E+Ol 12 . 35 l . 52E+Ol 9.BOE+OO 1 . 53E+Ol 1 . 58£+01 10/7/2020 Page 27
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 1:22:47PM Page 3 of6 Analysis Report for L2-SUB-102-QJGS-012-SB 04/05/18 -0910 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 98 1460 . 75
- 10 . 67 5 . 45E+OO 6 . 72E - 01 PB- 212 0 . 99 77 . 11
- 17 . 50 2 . 19£- 01 7 . 19E- 02 238 . 63
- 44 . 60 l. 57E- 01 2 . 74E - 02 BI - 214 0 . 77 609 . 31
- 4 6 . 30 7 . 57E - 02 4 . 50E - 02 1120 . 29
- 15 . 10 2 . 00E- 01 9 . 29E - 02 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49
- 15 . 80 1. SOE- 01 1. 55E - 01 PB - 214 0 . 99 77 . 11
- 10 . 70 3 . 58E-Ol l.18E- 01 295 . 21
- 19 . 20 1 . 17£- 01 4 . 54E- 02 351 . 92
- 37 . 20 7 . 35E- 02 4 . 79E- 02 AC - 228 0 . 60 209 . 28 4 . 40 338 . 32
- 11. 40 1 . 99E - 01 7 . 71E - 02 794 . 70 4 . 60 911 . 60
- 27 . 70 1 . 76E - 01 5 . 82E-02 964 . 60 5 . 20 969 . 11
- 16 . 60 1. 83E- 01 8 . 04E - 02
* = Energy line found In the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma 10/7/2020 Page 28
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 1:22:47PM Page 4 of 6 Analysis Report for L2-SUB-102-QJGS-012-SB 04/05/18 -0910 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) K- 40 0 . 988 5 . 45E+00 6 . 72E - 01 PB- 212 0 . 996 l . 57E - 01 2 . 5 7 E- 02 BI - 214 0 . 773 l . 03E - 01 3 . 92£-02 PB- 214 0 . 996 9 . 66£- 02 3 . 1 9E- 02 AC-228 0 . 604 l . 84E - 01 4 . 02E- 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000slgma 10/7/2020 Page 29
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 1:22;47PM Page 5 of6 Analysis Report for L2-SUB-102-QJGS-012-SB 04/05/18 -0910 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/6/2018 1:22:38PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 6 583 . 19 2 . 84839E - 02 12 . 16 -1'J,-,r,,,fl1 E' 11 1331 . 99 3 . 98745E-03 32 . 53 ?a . . l,1) M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(3/4) Activity Nuclide MDA LlneMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV)
+ K- 40 1460 . 75
- 10 . 67 S . 45E+OO 6.22E - 01 6 . 22E- 01
+ AR- 41 1293 . 64 99 . 16 2 . 22E+03 l . 93E+03 1 . 93E+03
+ C0-60 1173 . 22 100 . 00 5 . 56E-02 5 . 22E-02 5 . 87E- 02 1332 . 49 100 . 00 4 . 0lE - 02 5 . 22E- 02
+ KR-85 513 . 99 0 . 43 9 . 39E+OO 9 . 32E+OO 9 . 32E+OO
+ Y-88 898 . 04 93 . 70 3 . 56E- 02 3 .4 6E - 02 4 . 71E- 02 1836 . 06 99 . 20 - 1 . 59E - 02 3 . 46E- 02
+ NB- 94 702 . 63 100 . 00 2 . 49E - 03 4 . 02E - 02 4 . 02E- 02 871 . 10 100 . 00 -2 . 26E-02 4. llE-02
+ I - 131 284 . 30 6 . 06 -2.19E-02 3.92E-02 5 . 52£ - 01 364 . 48 81. 20 -2.23E-02 3 . 92E - 02 636 . 97 7 . 27 2 . 02E- 01 5 . 41E-01
+ CS-134 604 . 70 97 . 60 - 3 . 47E-02 4 . 58E- 02 4 . 58E- 02 795 . 84 85 . 40 1 . 55E-02 4 . 83E-02
+ CS-137 661 . 65 85 . 12 6 . 48E-02 5 . llE-02 / 5 . llE-02
+ CE - 144 80 . 12 1. 36 - l . 24E+OO 2 . 60E- 01 3 . 13E+OO 10/7/2020 Page 30
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 1:22:47PM Page 6of6 Analysis Report for L2-SUB-102-QJGS-012-SB 04/05/18 - 091 0 Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV) CE - 144 133 . 51 11. 09 -1 . 71E - 02 2 . 60E-01 2 . 60E - 01
+ EU-152 121 . 78 28 . 40 -2 . 81E- 02 9 . 89E - 02 if 9 . 89E - 02 244 . 69 7 . 49 -9 . 90E-01 4 . 72E-Ol 964 . 00 14 . 44 2.34E-01 3 . 60E - 01 1408 . 00 20 . 74 - 6 . 25E - 02 1. 96E - 01
+ EU - 154 123 . 07 40 . 40 - 1 . 67E - 02 6 . 97E - 02 / 6 . 97E - 02 247 . 94 6 . 60 - 1 . 93E+OO 4 . 62E - 01 723 . 30 19 . 70 2 . 19E- 01 2 . 16E- Ol 873 . 20 11 . 50 - 3 . 21E - 01 3 . 46E - 01 1004 . 76 17 . 90 - 1 . 04E- 01 2 . 50E-01 1274.51 35 . 50 -3 . 89E-02 1 . 43E-01
+ EU - 155 86.54 32 . 80 -2 . 53E-02 1 . 09E - 01 1 . 09E - 01 105 . 31 21. 80 2 . 28E-02 l . 36E-01
+ BI - 214 609 . 31
- 4 6 . 30 7 . 57E-02 8 . 43E-02 8 . 43E-02 1120 . 29
- 15 . 10 2 . 00E-01 l . 88E-01 1238 . 11 5 . 94 1 . 22E+OO l. lOE 00 1377 . 67 4 . 11 5 . 61E-01 1. 02E+OO 1407 . 98 2 . 48 - 5 . 23E- 01 l.64E+OO 1509 . 19 2 . 19 2 . 96E - 01 1. 61E+OO 1764 . 4 9
- 15 . 80 1 . 50E-01 2 . 62E-01
+ PB-214 77 . 11
- 10 . 70 3 . 58E- 01 9 . 33E - 02 3 . 41E - 01 295 . 21
- 19 . 20 l. l 7E - 01 1. OOE-01 351 . 92
- 37 . 20 7 . 35E-02 9 . 33E-02
+ PA-228 89 . 95 22 . 00 2 . 37E-01 2 . 20E-01 3 . 75E-01 93 . 35 35 . 00 -5 . 13E- 02 2 . 20E - 01 105 . 00 16 . 30 5 . 86E-03 4 . 34E - 01 129 . 22 2 . 97 2 . 78E- 01 2 . 30E+OO 338 . 32 5 . 30 l . 53E+OO l . 49E+OO 463 . 00 13 . 80 - 1 . 52E - 01 5 . 46E - 01 911. 23 16 . 70 7.95E-01 7 . SOE - 01
+ AM-241 59 . 54 36 . 30 5 . 42E- 02 2 . 05E - 01 2 . 0SE-01
+ CM- 243 103 . 76 23 . 00 -8 . 21E-02 1 . 28E-01 l.28E-01 228 . 18 10 . 60 -9 . 14E-02 2 . 62E-01 277 . 60 14 . 00 -1.40E-01 2 . 19E-01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction 7 = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 31
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 9:29:56PM Page 1 of7 pex-Gamma Analysis Report for l2-SUB-102-AJGS-013-SB L2-011-102 RACWD SOIL/PACKAGE#: L2-SUB-102 RACWD SOIL GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-013-SB / Sample Description : l2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 8.709E+02 grams / Facility : Dairyland_NPP Sample Taken On : 4/5/2018 9:12:00AM Acquisition Started : 4/9/2018 8:29:33PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611.0 seconds Dead Time : 0.30 % Peak locate Threshold : 3.00 Peak locale Range {in channels) : 100 - 4096 Peak Area Range (in channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4248 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/9/2018 9:29:47PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 32
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 9:29:56PM Page 2 of7 Analysis Report for L2-SUB-102-AJGS-013-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 77.00 147 - 160 154 . 54 1 . 66E+02 42 . 92 1 . 38E+03 1. 04 F 2 185 . 48 365 - 378 371. 45 9.82E+Ol 40 . 69 9 . 29E+02 1. 80 M 3 238 . 59 474 - 4 91 477 . 66 3 . 48E+02 45.44 3.70E+02 1. 56 m 4 241 . 74 474 - 491 483 . 96 l . 44E+02 31. 81 3.60E+02 1. 57 F 5 295 . 06 584 - 596 590 . 57 1 . 69E+02 34.27 4 . 39E+02 1. 34 F 6 338.33 672 - 681 677 . 09 4 . 54E+Ol 22 . 09 2 . 58E+02 1.13 F 7 351. 88 699 - 710 704 . 18 2 . 51E+02 37 . 37 2.74E+02 1.50 F 8 583 . 06 1161 - 1171 1166 . 47 7 . 72E+Ol 23 . 48 l . 44E+02 1. 60 F 9 609 . 15 1211- 1225 1218 . 62 l . 97E+02 31. 03 l . 39E+02 1 . 58 F 10 911 . 00 1814 - 1828 1822 . 24 7 . 58E+Ol 20 . 57 8 . 22E+Ol 1. 84 F 11 969 . 02 1933 - 1944 1938 . 26 3 . 68E+Ol 17 . 73 l . 01E+02 1. 79 F 12 1460 . 54 2913 - 2929 2921 . 20 4 . 86E+02 45 .4 7 4 . 93E 01 2.37 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/9/2018 9:29:47PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 77 . 00 l . 66E+02 42 . 92 1 . 66E+02 4.29E+Ol F 2 185 . 48 9 . 82E+Ol 40 . 69 9 . 82E+Ol 4.07E+Ol M 3 238 . 59 3 . 48E+02 45 . 44 3 . 48E+02 4 . 54E+Ol m 4 241 . 74 l.44E+02 31. 81 l.44E+02 3 . 18E+Ol F 5 295 . 06 l . 69E+02 34 . 27 1 . 69E+02 3 . 43E 01 F 6 338 . 33 4 . 54E+Ol 22 . 09 4 . 54E+01 2 . 21E+Ol F 7 351 . 88 2.51E+02 37 . 37 8 . 36E+Ol 3. 72E+Ol l . 67E+02 5 . 27E+01 F 8 583 . 06 7 . 72E+Ol 23 .4 8 7 . 72E+01 2 . 35E+Ol F 9 609 . 15 l.97E+02 31 . 03 4.12E+Ol 2 .4 2E+01 1. 56E+02 3 . 94E+Ol F 10 911 . 00 7 . 58E+Ol 20 . 57 7 . 58E+Ol 2 . 06E+Ol F 11 969 . 02 3 . 68E+Ol 17 . 73 3 . 68E+01 1 . 77E+Ol F 12 1460 . 54 4 . 86E+02 45 . 47 5 . 63E+Ol 1 . 71E+Ol 4 . 30E+02 4.86E+Ol 10/7/2020 Page 33
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 9:29:56PM Page 3 of7 Analysis Report for L2-SUB-102-AJGS-013-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0 . 99 1460 . 75
- 10 . 67 5 . 38E+OO 6 . 77E-Ol PB - 212 0 . 99 77 . 11
- 17 . 50 2 . 69E-01 7 . 17E- 02 238 . 63
- 44 . 60 2 . 06E-01 2 . 89E- 02 BI - 214 0 . 34 609 . 31
- 46 . 30 2 . 06E-01 5 . 33E- 02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 .4 8 1509 . 19 2 . 19 1764 . 49 15 . 80 PB - 214 0 . 99 77 . 11
- 10.70 4.40E-01 1.17E-01 295 . 21
- 19.20 2 . 78E-01 5 . 79E - 02 351 . 92
- 37 . 20 1 . 66E - Ol 5 . 29E - 02 RA - 226 0 . 91 186 . 21
- 3 . 28 6 . 64E- 01 2 . 77E - 01 AC - 228 0 . 61 209 . 28 4 . 40 338 . 32
- 11. 40 l . 42E - 01 6.93E-02 794 . 70 4 . 60 911. 60 27 . 70 2 . 41E - 01 6 . 63E - 02 964 . 60 5 . 20 969 . 11
- 16 . 60 2 .0 6E - 01 9 . 99E-02
* = Energy line found in the spectrum.
- =Manually added nuclide.
? =Manually edited nuclide.
@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma 10/7/2020 Page 34
LAC LTP - Final Status Survey Package - 3/21/2018 Analysis Report for L2-SUB-102-AJGS-013-SB L2-011-102 RA CW SOIL/ PACKAGE#: L2-SUB-102 RA cw SOIL 4/9/2018 9:29:56PM Page4 of7 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams) K- 40 0 . 993 5.38E+OO 6 . 77E - 01 PB-212 0 . 999 l . 97E-01 2 . 70E-02 BI - 214 0 . 347 2 . 06E-Ol 5 . 33E-02 PB-214 0 . 998 2 . 07E-01 3 . 73E-02 RA- 226 0 . 917 6 . 64E-01 2.77E-Ol AC - 228 0 . 610 l . 96E - 01 4 . 32E - 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 35
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 9:29:56PM Page 5 of7 Analysis Report for L2-SUB-102-AJGS-013-SB L2-011-102 RA cw SOIL/ PACKAGE#: L2-SUB-102 RA cw SOIL UNIDENTIFIED PEAKS Peak Locate Performed on : 4/9/2018 9:29:47PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 4 241 . 74 4.00707E-02 11 . 03 'if>~z.,4
-rJ,z,DS F 8 583 . 06 2 . 14563£-02 15 . 20 M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pC/lgrams) (pCl/grams) (pCl/grams)
(keV)
+ K-40 1460 . 75
- 10 . 67 5 . 38E+00 6.24E-01 6 . 24E-01
+ AR-41 1293 . 64 99 . 16 2 . 28E+16 3 . 27£+16 3 . 27E+l6
+ CO-60 1173 . 22 100 . 00 3.29£-02 4. 97£- 02 / 6 . l0E-02 1332 . 49 100 . 00 9 . 93E-03 4 . 97£-02
+ KR-85 513 . 99 0 . 43 1 . 08£+01 9 . 98E +00 9 . 98E+00
+ Y-88 898 . 04 93 . 70 1 . 74E-03 3 . 57E-02 4.88£-02 1836.06 99 . 20 -3.83E-02 3 . 57E-02
+ NB-94 702 . 63 100 . 00 -1 . 90E-02 3 . 95E-02 3 . 95E-02 871 . 10 100 . 00 - 5 . 33E - 02 4 . 13E-02
+ I - 131 284 . 30 6 . 06 - 2 . 43E- 01 S . 65E- 02 7 . 83E - 01 364 . 48 81 . 20 -2.59E-02 5.65E-02 636 . 97 7 . 27 - 4.12E- 01 7.31E - 01
+ CS - 134 604 . 70 97 . 60 -1.37E-03 5 . l 0E-02 5 . 59£-02 795 . 84 85 . 40 4 . 36E- 03 5 . l0E - 02 10/7/2020 Page 36
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 9:29:56PM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-013-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RACWD SOIL Nuclide Energy Yield(%) Activity NuclideMDA Line MDA Name (pCi/grams) (pCilgrams) (pCi/grams) (keV)
+ CS - 137 661 . 65 85.12 4 . 72E-02 5 . 32E- 02 ./ 5 . 32E - 02
+ CE-144 80 . 12 1. 36 - l . 14E+00 2 . 74E-01 3 . 44E+00 133 . 51 11.09 1. 43E-01 2 . 74E-01
+ EU-152 121 . 78 28 . 40 -8 . 26E-02 1. 05E - 01 / 1. 05E - 01 244 . 69 7 .49 l . 19E-02 5 . 16E - 01 964 . 00 14 . 44 4 . 45E-01 3 . 98E - 01 1408 . 00 20 . 74 6 . 55E - 03 2 . 14E - 01
+ EU-154 123 . 07 40 . 40 - l . 14E - 02 7 . 41E-02 7 . 41E-02 247 . 94 6 . 60 7 . 32E - 02 5 . 18E- 01 723 . 30 19 . 70 - 1 . 71E - 02 2 . 17E-01 873 . 20 11 . 50 -7.46E-03 3 . 64E-01 1004 . 76 17 . 90 5 . 52E-02 2 . SlE - 01 1274 . 51 35 . 50 -2.15£-02 l.45E - 01
+ EO - 155 86 . 54 32 . 80 -l.85E-02 l . 19E- 01 l . 19E- 01 105 . 31 21.80 3 . 78E-02 l.44E- 01
+ BI - 214 609 . 31
- 46.30 2 . 06E-01 8 . 92E - 02 8 . 92E- 02 1120 . 29 15 . 10 2 . 13E- 01 4 . 04E-0l 1238 . 11 5 . 94 3.42E-01 l . 06E+00 1377 . 67 4 . 11 -1 . 56E-01 9 . 09E - 01 1407 . 98 2 . 48 5 . 47E - 02 l . 79E+00 1509 . 19 2 . 19 l . 09E+00 1 . 87E+00 1764 . 49 15.80 l.07E-01 2 . 83E-01
+ PB-214 77 . 11
- 10 . 70 4 . 40E-01 9 . 35E-02 3 . 88E-01 295 . 21
- 19 . 20 2 . 78E - 01 l . 34E-01 351 . 92
- 37 . 20 1. 66E-01 9 . 35E-02
+ PA-228 89 . 95 22 . 00 4.92E+00 2 . 98E+00 5 . 12E+00 93 . 35 35 . 00 - l . 52E+00 2 . 98E+00 105 . 00 16 . 30 1. 27E+00 5 . 75E+00 129 . 22 2 . 97 l . 14E+0l 3 . 03E+0l 338 . 32 5 . 30 5 . 87E+00 l . 91E+0l 463 . 00 13 . 80 -5 . 80E+00 7 . 44E+00 911.23 16 . 70 1 . 35E+0l l . 02E+0l
+ AM-241 59 . 54 36 . 30 -1.52E-0 1 2 . 09E -01 2 . 09E-01
+ CM- 243 103 . 76 23 . 00 2 . 90E - 03 l . 37E - 01 l.37E-01 228 . 18 10 . 60 4 . 68E-02 2 . 80E-01 277 . 60 14 . 00 3 . 16E- 02 2 . 37E-01
+ = Nuclide Identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MOA at 95% confidence level 10/7/2020 Page 37
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 9:29:56PM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-013-SB L2-011 -102 RA cw SOIL / PACKAGE#: L2-SUB-102 RA cw SOIL 10/7/2020 Page 38
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 10:36:02PM Pagel of6
~~~~pex-Gam ma Analysis Report for L2-SUB-102-AJGS-014-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-014-SB /
Sample Description : L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 9.014E+02 grams Facility : Dairyland_ NPP Sample Taken On : 4/5/2018 9:26:00AM Acquisition Started : 4/9/2018 9:35:39PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live nme : 3600.0 seconds Real Time : 3610.7 seconds Dead Time : 0.30 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100- 4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4249 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/9/2018 10:35:53PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 39
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 10:36:02PM Page 2 of6 Analysis Report for L2-SUB-102-AJGS-014-SB L2-011-102 RACWD SOIL / PACKAGE#: L2-SUB-102 RA CWD SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 76 . 12 147 - 161 152 . 79 2 . 51E+02 63 . 26 1 . 35E+03 4 . 40 F 2 238 . 58 4 69 - 485 477 . 63 3 . 26E+02 45 . 38 6 . 48E+02 1. 59 F 3 295 . 06 587 - 595 590.57 1 . 35E+02 31. 20 2 . 32E+02 1. 63 F 4 338 . 34 674 - 681 677. 11 4.75E+Ol 21. 87 l . 97E+02 1.11 F 5 351 . 70 698 - 709 703 . 83 l . 63E+02 31. 92 2 . 61E+02 1. 49 F 6 583 . 16 1162 - 1172 1166 . 66 8 . 14E+Ol 22 . 69 1. 27E+02 1. 44 F 7 609 . 18 1213 - 1226 1218 . 69 1 . 31£+02 26 . 64 l . 32E+02 1. 67 F 8 726 . 87 1451- 1458 1454 . 04 1 . 74E+Ol 11 . 22 5 . 08E+Ol 1. 40 F 9 911. 01 1816 - 1828 1822 . 25 5 . 41E+Ol 19 . 43 9 .4 4E+Ol 1. 97 F 10 968 . 93 1934 - 1943 1938 . 09 3 . 22E+Ol 15 . 70 7 . 29E+Ol 1. 43 F 11 1332 . 86 2661- 2671 2665.85 2 . 05E+Ol 11 . 24 2 . 68E+Ol 1. 63 F 12 1460 . 59 2913 - 2930 2921.29 5.17E+02 46 . 25 9.00E+OO 2 . 35 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted al 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/9/2018 10:35:53PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtrac ted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76 . 12 2 . 51E+02 63 . 26 2 . 51E+02 6 . 33E+Ol F 2 238 . 58 3 . 26E+02 45 . 38 3 . 26E+02 4 . 54E+Ol F 3 295 . 06 l . 35E+02 31.20 1 . 35£+02 3 . 12E+Ol F 4 338 . 34 4 . 75E+Ol 21 . 87 4.75E+Ol 2.19E+Ol F 5 351 . 70 1 .63E+02 31. 92 8 . 36E+Ol 3. 72E+Ol 7.93E+Ol 4 . 90E+Ol F 6 583 . 16 8 . 14E+Ol 22 . 69 8 . 14E+Ol 2 . 27E+Ol F 7 609 . 18 1 . 31E+02 26 . 64 4.12E+Ol 2 . 42E+Ol 8 . 98E+Ol 3 . 60E+Ol F 8 726 . 87 l . 74E+Ol 11 . 22 1 . 74E+Ol 1.12E+Ol F 9 911. 01 5 .41 E+Ol 19 . 4 3 5 .4 1E+Ol 1 . 94E+Ol F 10 968 . 93 3 . 22E+Ol 15 . 70 3 . 22E+Ol 1. 57E+Ol F 11 1332.86 2 . 05E+Ol 11 . 24 2 . 05E+Ol l.12E+Ol F 12 1460.59 5 . 17E+02 46 . 25 5 . 63E+Ol 1 . 71E+Ol 4 . 61E+02 4.93E+Ol 10/7/2020 Page 40
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 10:36:02PM Page 3 of 6 Analysis Report for L2-SUB-102-AJGS-014-SB L2-011-102 RA CWD SOIL I PACKAGE#: L2-SUB-102 RA CWD SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0 . 99 1460 . 75
- 10 . 67 5 . 57E 00 6 . 71E - 01 BI - 212 0 . 59 727 . 17
- 11 . 80 l . 03E-01 6 . 63E-02 785 . 42 2 . 00 1620 . 56 2 . 75 PB - 212 0 . 95 77 . 11
- 17 . 50 4 . 0lE - 01 1 . 04E - 01 238 . 63
- 44 . 60 1. 86E - 01 2 . 77E - 02 BI - 214 0 . 34 609 . 31
- 4 6 . 30 l.15E - 01 4 . 64E - 02 1120 . 29 15 . 10 1238 .11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 .4 9 15 . 80 PB - 214 0 . 97 77 . 11
- 10 . 70 6 . 57E - 01 1 . 70E-01 295 . 21
- 19 . 20 2 . 14E-Ol 5 . 06E - 02 351 . 92
- 37 . 20 7 . 59E- 02 4 . 71E-02 AC-228 0 . 61 209 . 28 4 . 40 338 . 32
- 11 . 40 1 . 43E- 01 6 . 64E - 02 794 . 70 4 . 60 911 . 60
- 27 . 70 1 . 66E - 01 6 . 02E - 02 964 . 60 5 . 20 969 .11
- 16 . 60 1 . 75E-01 8 . 55E-02
* = Energy line found in the spectrum .
- =Manually added nuclide.
? =Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma 10/7/2020 Page 41
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 10:36:02PM Page 4 of 6 Analysis Report for L2-SUB-102-AJGS-014-SB L2-011-102 RA CWD SOIL I PACKAGE#: L2-SUB-102 RA CWD SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams) K- 40 0 . 996 5 . 57E+OO 6 . 71E-0 1 BI-212 0 . 595 1 . 03£ - 01 6 . 63£ - 02 PB- 212 0 . 956 1. 95E - 01 2 . 68£ - 02 BI - 214 0 . 348 1 . 15£- 01 4 . 64E- 02 PB-214 0 . 970 l . 48E-01 3 . 38E - 02 AC - 228 0 . 610 1 . 60E - 01 3 . 95E - 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 42
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 10:36:02PM Page S of6 Analysis Report for L2-SUB-102-AJGS-014-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL UNIDENTIFIED PEAKS Peak Locate Performed on : 4/9/2018 10:35:53PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 6 583.16 2 . 26141E -02 13 . 94 -(1-*zoS F 11 1332 . 86 5 .6 9635E- 03 27 .4 1 ~-/,/0 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV}
+ K- 40 1460 . 75
- 10 . 67 5 . 57E+00 5 . llE-01 5 . llE - 01
+ AR-41 1293 . 64 99 . 16 9 . 06E+l5 4 . 30£+16 / 4.30E+l6
+ CO-60 1173.22 100 . 00 5 . 54E-02 S . 04E-02 6 . 61E-02 1332. 49 100 . 00 3 . 36E-02 5 . 04E-02
+ KR-85 513 . 99 0 . 43 1 . 55E+0l 9 . 37E+00 9 . 37E+00 Y-88 898 . 04 93 . 70 -1.74E-02 3 . 72E-02 4 . 64E-02 1836 . 06 99 . 20 -6 . 54E - 03 3 . 72E-02
+ NB-94 702 . 63 100 . 00 9 . 60£ - 03 3 . 92£-02 3 . 92£-02 871 . 10 100 . 00 9 . 90£ - 03 4.34E-02
+ I - 131 284 . 30 6 . 06 -9 . 99£ - 02 5 . 64E-02 7.28E-0l 364.48 81 . 20 2 . 35E-02 5 . 64£-02 636.97 7 . 27 2 . 99£-01 7 .3 3£-01
+ CS-134 604 . 70 97 . 60 -4.85£-03 4 . 78E-02 4 . 78E-02 795 . 84 85 . 40 -2 . 51E-02 / 5 . 09E-02
+ CS - 137 661 . 65 85 . 12 8 . 91E - 02 5 . 54E-02 5 . 54E-02
+ CE-144 80 . 12 1. 36 -1 . SSE+00 2 . 57E - 01 3 . 19E+00 10/7/2020 Page 43
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 10:36:02PM Page 6 of6 Analysis Report for L2-SUB-102-AJGS-014-SB l2-011 -102 RA cw SOIL/ PACKAGE#: l 2-SUB-102 RA cw SOIL Nuclide Energy Yleld{3/4) Activity NuclideMDA LineMDA Name (pCilgrams) (pCi/grams) (pCilgrams) (keV) CE-144 133 . 51 11.09 2 . 83E - 02 2 . 57E - 01 2 . 57E - 01
+ EU - 152 121. 78 28 . 40 -5 . 02£-02 9 . 84E - 02 9 . 84E - 02 244 . 69 7 . 49 - 3 . 99E - Ol 4 . 68E - 01 964 . 00 14 . 44 4 . 60E-01 3 . 87E - 01 1408 . 00 20 . 74 -l . 21E-01 2.05E-01 EU-154 123 . 07 40 . 40 -2 . 78E-02 6 . 94E-02 6 . 94E-02 247 . 94 6 . 60 -6 . 89E-01 4 . 73E-01 723 . 30 19 . 70 -1 . 07E - 01 2 . 00E-01 873 . 20 11. so 2 . 23E-Ol 3 . 83£-01 1004 . 76 17 . 90 -6 . 30E - 02 2 . SlE-01 1274 . 51 35 . 50 2 . 49E - 02 l . 43E-01
+ EU - 155 86 . 54 32 . 80 - l . 24E- 01 1 . 08E - 01 1 . 08E - 01 105 . 31 21. 80 2 . 54E - 04 1 . 36E - 01
+ BI - 214 609 . 31
- 46 . 30 l . 15E- 01 8 . 43E-02 8 . 43E-02 1120 . 29 15 . 10 3 . 40E-01 3.94E-01 1238 . 11 5 . 94 3.32E - 01 1 . 06E+OO 1377 . 67 4 . 11 -2 . 19E-01 9 . 59E - 01 1407 . 98 2 . 48 -1 . 0lE+OO 1 . 71E+OO 1509 . 19 2 . 19 -l . 15E+OO l . 49E+OO 1764 . 49 15 . 80 1. 59E-01 2 . 53E-01
+ PB-214 77 . 11
- 10.70 6 . 57E-01 8 . 67E - 02 3 . 87E-01 295 . 21
- 19 . 20 2 . 14£-01 8 . 67E-02 351. 92 'Ir 37 . 20 7 . 59E-02 8 . 93E-02
+ PA-228 89 . 95 22 . 00 2 . 35E+OO 2 . 89E+OO 4 . 82E+OO 93.35 35 . 00 5 . 98E-01 2 . 89E+OO 105 . 00 16 . 30 -2 . 80E-01 5 . 60E+OO 129 . 22 2 . 97 -1.52E+OO 2 . 96E+Ol 338 . 32 5 . 30 1 . 44E+Ol l . 88E+Ol 463 . 00 13 . 80 l . 19E+OO 7 . 63E+OO 911. 23 16 . 70 8 . 53E+OO l . OlE+Ol
+ AM-241 59 . 54 36 . 30 -1 . 09E-01 l . 95E-Ol l . 95E-01
+ CM-243 103 . 76 23 . 00 5. llE-02 l . 32E - 01 1. 32E - 01 228 . 18 10 . 60 - 4 . 98E- 02 2 . 55£- 01 277 . 60 14 . 00 - 6.18E - 02 2 . 17E- 01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculate d
@ = Half-life too short to be able lo perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 44
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 11 :37:58PM Page I of7 Analysis Report for L2-SUB-102-AJGS-015-SB L2-011 -102 RACWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-015-SB / Sample Description : L2-011 -102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 8.810E+02 grams / Facility : Dairyland_NPP Sample Taken On : 4/5/2018 10:13:00AM Acquisition Started : 4/9/2018 10:37:35PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3610.8 seconds Dead Time : 0.30% Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4250 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/9/2018 11 :37:49PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 45
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 11 :37:SBPM Page 2 of7 Analysis Report for L2-SUB-102-AJGS-015-SB l2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 76 . 48 147 - 161 153 . 50 2 . 53E+02 61 . 74 l. 40E+03 2 . 96 M 2 238 . 52 472 - 492 477 . 51 3 . 55E+02 45 . 77 3 . 45E+02 1. 49 m 3 2 41. 72 472 - 492 483 . 91 1 . 16E+02 28 . 70 3 . 17E+02 1.50 F 4 270 . 48 536 - 545 54 1. 43 4 . 72E+Ol 25 . 71 3 . 35E+02 1. 38 F 5 2 95 . 14 582 - 595 590 . 73 l . 51E+02 33 . 28 4 . 22E+02 1. 43 F 6 351 . 85 697 - 710 704 . 13 2 . 47E+02 37 . 71 3 . 35E+02 1. 60 F 7 582 . 95 1161 - 1172 1166 . 24 9 . 32E+Ol 24 . 12 l . 41E+02 1. 57 F 8 609 . 12 1210 - 1226 1218 . 58 l . 61E+02 28 . 54 l.44E+02 1. 66 F 9 910 . 90 1814 - 1830 1822 . 03 8 . 42E+Ol 22 . 01 7 . 71E+Ol 2 . 87 F 10 969 . 25 1933 - 1945 1938 . 73 3 . 42E+Ol 17 . 28 9 . 0lE+Ol 2 . 10 F 11 1120 . 34 2236 - 2248 2240 . 86 2 . 75E+Ol 15 . 08 7 . 22E+Ol 1. 85 F 12 1460 . 49 2913 - 2930 2921 . 08 4 . 98E+02 45 . 73 2 . 70E+Ol 2 . 44 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/9/2018 11 :37:49PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76 . 48 2 . 53E+02 61 . 74 2 . 53E+02 6 . 17E+Ol M 2 238 . 52 3 . 55E+02 45 . 77 3 . 55E+02 4 . 58E+Ol m 3 241.72 l.16E+02 28 . 70 l.1 6E+02 2 . 87E+Ol F 4 270 . 48 4 . 72E+Ol 25 . 71 4 . 72E+Ol 2 . 57E+Ol F 5 295 . 14 1 . 51E+02 33 . 28 l . 51E+02 3 . 33E+Ol F 6 351 . 85 2 . 47E+02 37 . 71 8 . 36E+Ol 3 . 72E+Ol l . 63E+02 5 . 30E+Ol F 7 582 . 95 9 . 32E+Ol 24 . 12 9 . 32£+01 2 . 41E+Ol F 8 609 . 12 l . 61E 02 28 . 54 4. 12E+01 2 .4 2E+Ol 1 . 20E+02 3 . 74E+Ol F 9 910 . 90 8 . 42E+Ol 22 . 01 8 . 42E+Ol 2 . 20E+Ol F 10 969 . 25 3 .4 2E+Ol 17 . 28 3 . 42E+Ol l . 73E+01 F 11 1120 . 34 2 . 75E+Ol 15 . 08 2 . 75E+Ol l . 51E+Ol F 12 1460 . 49 4 . 98E+02 45 . 73 5 . 63E+Ol 1 . 71E+Ol 4 . 42E+02 4 . 88E+Ol 10/7/2020 Page 46
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 11 :37:SBPM Page 3 of7 Analysis Report for L2-SUB-102-AJGS-015-S8 L2-011-102 RA CWD SOIL I PACKAGE#: L2-SUB-102 RA CWD SOIL M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000s1gma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0 . 98 1460 . 75
- 10 . 67 5 . 47E+OO 6 . 76E - 01 PB-212 0 . 98 77 . 11
- 17.50 4.lOE - 01 l . 03E - 01 238 . 63
- 44 . 60 2 . 08E-01 2 . 89E-02 BI-214 0 . 58 609 . 31
- 46 . 30 l . 57E - 01 4 . 978-02 1120 . 29
- 15 . 10 1. 91£-01 l . 05E-01 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 .49 15 . 80 PB-214 0 . 98 77 . 11
- 10 . 70 6 . 70E - 01 1 . 69E-01 295 . 21
- 19 . 20 2 .4 5E-01 5 . 53E- 02 351. 92
- 37 . 20 l.60E-01 5 . 25E-02
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT 10/7/2020 Page 47
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 11 :37:58PM Page4 of7 Analysls Report tor L2-SUB-102-AJGS-015-SB L2-011-102 RA CWD SOIL / PACKAGE#: L2-SUB- 102 RA CWD SOIL Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) K- 40 0 . 989 5 . 47E+00 6 . 76E - 01 PB-212 0 . 981 2 . 13E- 01 2 . 78E - 02 BI - 214 0 . 582 1 . 63£ - 01 4 . 49E - 02 PB - 214 0.989 2 . 06E - 01 3 . 72E - 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 48
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 11 :37:58PM Page 5 of 7 Analysis Report for L2-SUB-102-AJGS-015-SB L2-011-102 RA CW SOI L / PACKAGE#: L2-SUB-102 RA cw SOIL UN IDENTIFIED PEAKS Peak Locate Performed on : 4/9/2018 11:37:49PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 3 241.72 3 . 23227E- 02 12 . 33 '?Z-vl/- F 4 270 . 48 l . 31064E- 02 27 . 24 At:-; t,z,fJ F 7 582 . 95 2.58967E - 02 12 . 94 Yf ..- z_t)i F 9 910 . 90 2 . 33843E-02 13.07 Tol. AC-228 PA-228 F 10 969 . 25 9 . 51203E-03 25 . 23 Tol. AC-228 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted al 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(3/4) Activity Nuclide MDA LineMDA Name (pCl/grams) (pCilgrams) (pCilgrams) {ke V}
+ K-40 1460 . 75
- 10 . 67 5 . 47E+00 5 . 70E-01 5 . 70E-0l
+ AR-41 1293 . 64 99 . 16 3 . 31E+16 4 . 4 OE 16 / 4 . 4 OE+ 16
+ CO-60 1173 . 22 100 . 00 1. l0E-02 5 . SlE- 02 5 . 89E-02 1332 . 49 100 . 00 5 . 93E-02 5 . 51E-02
+ KR- 85 513 . 99 0 . 43 l . 18E+0l 9 . 63E 00 9 . 63E+00
+ Y- 88 898 . 04 93 . 70 5 . 76E-03 4.lSE-02 4 . 79E-02 1836 . 06 99 . 20 4 . 20E-03 4 . lSE-02 10/7/2020 Page 49
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 11 :37:SBPM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-015-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Nuclide Energy Yield(3/4) Activity Nuclide MDA LineMDA Name (pCl/grams) {pCilgrams) (pCi/grams) (keV)
+ NB - 94 702 . 63 100 . 00 1 . 48E - 02 3 . 82E-02 3 . 82 E- 02 87 1. 10 100 . 00 - 1 . 81E - 02 4 . 46E - 02
+ I - 131 284 . 30 6 . 06 - 3 . 91E-02 5 . 56E - 02 7 . 52E-Ol 364 . 48 81.20 - 1 . 63E - 02 5 . 56E - 02 636 . 97 7 . 27 - 1 . 09E - 01 7 . 51E-01
+ CS- 134 60 4. 70 97 . 60 - l . 34E-02 5 . 18E- 02 5 . 18£- 02 795 . 84 85 . 40 2 . 35E - 02 5 . 22E - 02
+ CS - 137 661. 65 85 . 12 4 . 34E-02 5 . 4 4E-02 ,/ 5 . 44E-02
+ CE - 144 80 . 12 1. 36 - 9 . 08E - 01 2 . 62E - 01 3 . 37E+OO 133 . 51 11 . 09 - 8 . 44E- 02 2 . 62E - Ol
+ EU - 152 121 . 78 28 . 40 - 2 . 69E - 02 1 . 04E-01 / 1 . 04E - 01 244 . 69 7 . 49 - 1 . 73£ - 01 4 . 90E- 01 964 . 00 14 . 4 4 - 8 . 53E - 02 3 . 73E - Ol 1408 . 00 20 . 74 3 . 59E - 02 l . 84E - 01
+ EU - 154 123 . 07 40 . 40 - 3 . 67E - 02 7 . 28E - 02 7 . 28E - 02 247 . 94 6 . 60 - 1 . 04E - Ol 4 . 87E- 01 723 . 30 19 . 70 4 . 72E- 03 2 . 03E- Ol 873 . 20 11 . so - 2 . 19E- 01 3 . 76E-0 1 1004 . 76 17 . 90 - 1 . 32E - 01 2 . 27E - 01 1274 . 51 35 . 50 1 . 49E- 03 1.48E-01
+ EU - 155 86 . 54 32 . 80 - 6 . 41E- 02 1 . 16E- Ol l.16E - 01 105 . 31 21 . 80 3 . 68E - 02 l. 44E- 01
+ BI - 214 609 . 31
- 4 6 . 30 1. 57E-01 9 . lOE-02 9 . lOE - 02 1120 . 29
- 15 . 10 l . 91E - 01 2 . 42E- 01 1238 . 11 5 . 94 4 . 65E - 02 l . 06E+OO 1377 . 67 4 . 11 - 8 . 65E- 02 9 . 35E- 01 1407 . 98 2 . 48 3 . 00E-01 1. 54E+OO 1509 . 19 2 . 19 - 6 . 48E - 01 1 . 75E+OO 1764 . 49 15 . 80 2 . 98E - 01 3 . 00E-01
+ PB- 214 77 . 11
- 10 . 70 6 . 70E- 01 9 . 89E- 02 4 . 00E-01 295 . 21
- 19 . 20 2 . 45E-01 l . 33E- 01 351 . 92
- 37 . 20 1 . 60E - 01 9 . 89E- 02
+ PA- 228 89 . 95 22 . 00 6 . 09E +OO 3 . 09E+OO 5 . 27E+OO 93 . 35 35 . 00 1. 05E+OO 3 . 09E+OO 105 . 00 16 . 30 - 2 . 78E+OO 5 . 88E+OO 129 . 22 2 . 97 - l . 55E+Ol 3 . 02E+Ol 338 . 32 5 . 30 8 . 73E+OO 1. 98E+Ol 463 . 00 13 . 80 8 . 93E - 01 7 . 56E+OO 911 . 23 16 . 70 l . 70E+Ol 1. 06E+Ol
+ AM - 241 59 . 54 36 . 30 7 . 40E - 02 2 . llE - 01 2 . llE - 01
+ CM- 243 103 . 76 23 . 00 - 9 . 60E - 02 l . 36E - 01 1. 36E-01 228 . 18 10 . 60 - 6 . 36E- 02 2 . 69E - 01 277 . 60 14 . 00 - 5 . 95E - 02 2 . 25E- 01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA al 95% confidence level 10/7/2020 Page 50
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 11 :37:58PM Page 7 of 7 Analysis Report for L2-SUB-102-AJGS-015-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL 10/7/2020 Page 51
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 1:13:16AM Page I of7 pex-Gamma Analysis Report for L2-SUB-102-AJGS-016-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL GAMMA SPECTRUM ANALYS/S Sample Identification : L2-SUB-102-AJGS-016-SB Sample Description : L2-011-102 RA CWD SOIL/ PACKAGE#: l2-SUB-102 RA CWD SOIL Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 8.781E+02 grams / Facility : Dairyland_NPP Sample Taken On : 4/5/2018 10:29:00AM Acquisition Started : 4/10/2018 12:12:53AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611 .3 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100-4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Description Sample Number : 4251 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/10/2018 1:13:07AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 52
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 1:13:16AM Page 2 of7 Anal ysis Report for L2-SUB-102-AJGS-016-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncerta inty Counts (keV) F 1 76 . 83 147 - 161 154 . 21 1 . 48E+02 4 6 . 74 l . 39E+03 1. 66 F 2 185 . 64 364 - 376 371 . 77 8 . 93E+Ol 37 . 58 7 . 05E+02 1. 77 F 3 238 . 50 471- 481 477 . 47 2 . 48E+02 43 . 72 6 . 48E 02 1. 21 F 4 295 . 26 587 - 595 590 . 96 l . 03E+02 29 . 10 2 . 43E+02 1. 48 F 5 338 . 35 672 - 685 677 . 14 5 . 57E+0l 24 . 81 3 . 20E+02 1. 59 F 6 351 . 90 697 - 710 704 . 23 1 . 63E+02 31. 88 2 . 87E+02 1. 58 F 7 583 . 05 1159 - 1172 1166 . 43 1 . 05E+02 25 . 13 l . 26E+02 1. 99 F 8 609 . 15 1214 - 1226 1218 . 64 1 . 34E+02 26 . 66 l . 15E+02 1. 67 F 9 910 . 74 1817 - 1828 1821 . 72 6 . 72E+0l 20 . 70 9 . 80E+0l 1. 72 F 10 1332 . 18 2658 - 2669 2664 . 49 2 . 31E+0l 11 . 51 3 . 26E+0l l. 31 F 11 1460 . 50 2914 - 2931 2921 . 11 5 . 20E+02 46 . 36 3 . 60E+0l 2 . 48 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/10/2018 1:13:07AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76 . 83 l . 48E+02 4 6 . 74 l . 48E+02 4 . 67E+Ol F 2 185 . 64 8 . 93E+0l 37 . 58 8 . 93E+0l 3 . 76E+0l F 3 238 . 50 2 . 48E+02 43 . 72 2 . 48E+02 4 . 37E+0l F 4 295 . 26 1 . 03E+02 29 . 10 1 . 03E+02 2 . 91E+0l F 5 338 . 35 5 . 57E+0l 24 . 81 5 . 57E 01 2 . 48E+0l F 6 351. 90 l . 63E 02 31. 88 8 . 36E+0l 3 . 72E+Ol 7 . 92E+0l 4 . 90E+0l F 7 583 . 05 1. OSE 02 25 . 13 1. 05E+02 2 . SlE 01 F 8 609 . 15 1. 34E 02 26 . 66 4. 12E+0l 2 . 42E+0l 9 . 26E+0l 3 . 60E+0l F 9 910 . 74 6 . 72E+0l 20 . 70 6 . 72E+0l 2 . 07E+0l F 10 1332 . 18 2 . 31E+0l 11 . 51 2 . 31E+0l l . lSE+0l F 11 1460 . 50 5 . 20E+02 46 . 36 5 . 63E+0l 1. 71E 01 4 . 64E+02 4 . 94E+0l M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma 10/7/2020 Page 53
LAC LTP - Final Status Survey Package - 3/21/2018 4/1012018 1:13:16AM Page 3 of 7 Analysis Report for L2-SUB-102-AJGS-016-S8 L2-011-102 RA CWD SOIL / PACKAGE#: L2-SUB- 102 RA CWD SOIL NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0 . 99 1460 . 75
- 10 . 67 5 . 75E+OO 6 . 91E-01 PB- 212 0 . 99 77 . 11
- 17 .so 2 . 40E-01 7 . 70E - 02 238 . 63
- 44 . 60 1 . 46E-01 2 . 68E - 02 BI - 214 0 . 34 609 . 31
- 46 . 30 l . 21E - Ol 4 . 77E- 02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB - 214 0 . 99 77 . 11 10 . 70 3 . 92E- 01 l . 26E - Ol 295 . 21
- 19 . 20 1 . 67E-Ol 4 . SlE - 02 351 . 92
- 37 . 20 7 . 79E - 02 4 . 84E - 02 RA- 226 0 . 94 186 . 21
- 3 . 28 5 . 99E - 01 2 . 54E - 01
~ =Energy line found In the spectrum.
- =Manually added nucllde.
? =Manually edited nuclide.
@ =Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted al 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams) 10/7/2020 Page 54
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 1:13:16AM Pagc 4 of7 Analysis Report for L2-SUB-102-AJGS-016-SB L2-011-102 RA CWD SOIL / PACKAGE#: L2-SUB-102 RA CWD SOIL Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) K-40 0 . 990 5 . 75£+00 6 . 91£-01 PB- 212 0 . 995 1 . 47E-01 2 . 54£-02 BI - 214 0 . 348 1 . 21E - 01 4 . 77E - 02 PB- 214 0 . 998 l . 25E- 01 3 . 30E - 02 RA - 226 0 . 948 5 . 99E - 01 2 . 54E - 01
? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 55
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 1:13:16AM Page 5 of7 Analysis Report for L2-SUB-102-AJGS-016-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL UNIDENTIFIED PEAKS Peak Locate Performed on : 4/10/2018 1: 13:07 AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 5 338.35 l . 54741E-02 22 . 27 Tol. AC - 228 PA- 228 F 7 583 . 05 2 . 93053E - 02 11. 91 -rJ ..~~ F 9 910 . 74 l . 86587E - 02 15.41 Tol. AC - 228 PA-228 F 10 1332 . 18 6 . 42199E-03 24 . 89 Tol. CO-60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Yield{%) Activity NuclldeMDA LlneMDA Name (pCilgrams) (pCilgrams) (pCilgrams) {keV)
+ K-40 1460.75
- 10 . 67 5 . 75E+00 5.96E-01 5 . 96E-0l
+ AR- 41 1293 . 64 99 . 16 - 1 . 46E+l6 7 . 71E+l6 7 . 71E+l6
+ CO - 60 1173 . 22 100 . 00 5 . 14E-02 5 . 1 4E - 02 V 6 . S0E-02 1332 . 49 100.00 2 .2 9E-02 5 . 14E-02
+ KR-85 513 . 99 0 . 43 8 . 15E+00 9 . 62E+00 9 . 62E+00
+ Y- 88 898 . 04 93 . 70 l . 22E-03 3 . 55E-02 4 . 63E-02 1836 . 06 99 . 20 - 7 . 49E - 03 3 . 55E-02
+ NB- 94 702.63 100.00 8 . 46E-03 4.12E-02 4.12E-02 871 . 10 100 . 00 - 2 . 92E - 02 4 . 1 2E-02
+ I-131 284 . 30 6 . 06 2 . 92E- 01 5 . 73E - 02 7 . 34E-01 10/7/2020 Page 56
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 1:13:16AM Page 6 of? Analysis Report for L2-SUB-102-AJGS-016-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV) I - 131 364 .4 8 81. 20 -3.00E-02 5 . 73E- 02 5 . 73E - 02 636 . 97 7 . 27 8 . 39£ - 02 7 . 31E-01
+ CS-134 604 . 70 97 . 60 - 4 . 25E-02 4.97E-02 4 . 97E-02 795 . 84 85 . 40 -9 . 06£-03 / 5. 04£ - 02
+ CS-137 661. 65 85 . 12 3 . 26£-02 5 . 21E- 02 5 . 21E - 02
+ CE-144 80 . 12 1. 36 -l . 45E+00 2 . 63E- 01 3 . 23E+00 133 . 51 11 . 09 -2.52E-02 2 . 63E-01
+ EU - 152 121. 78 28 . 40 -7 . 17E-02 1 . 0lE-01 / 1 . 0lE - 01 244 . 69 7 . 49 - 8 . 18E- 01 4 . 98E-0l 964.00 14 . 44 3 . 86E-01 3 . 66E-01 1408 . 00 20 . 74 6 . 20E-02 2 . 08E-0l
+ EU - 154 123.07 40 . 40 -2.77E-02 7 . 15E - 02 7 . 15E - 02 247 . 94 6.60 - l . 55E+00 4 . 97E-0l 723 . 30 19 . 70 -7.46E-02 2 . 05E-01 873 . 20 11. 50 -5 . 79E-03 3 . 52E-01 1004 . 76 17 . 90 -8 . 78E-02 2 . 65E - 01 1274 . 51 35 . 50 6 . 04E-02 1 . 44E - 01
+ EU-155 86 . 54 32 . 80 -3 . 56E-02 l.14E- 01 l.14E - 01 105 . 31 21 . 80 5 . 73E-02 1 . 38E-01 BI-214 609 . 31 46 . 30 1 . 21E-01 8 . 32E-02 8 . 32E-02 1120 . 29 15 . 10 -1.4 5E-01 3 . 54E - 01 1238 . 11 5 . 94 3 . 20E-01 l . 16E+00 1377 . 67 4 . 11 3 . 06E - 02 9 . 84E-01 1407 . 98 2 . 48 5 . 18E-01 l . 74E+00 1509 . 19 2 . 19 -4.82E-01 l . 56E+00 1764 . 49 15 . 80 2 . 70E-01 3 . 04E-01
+ PB-214 77 . 11 10 . 70 3.92E-01 9 . 09£-02 3 . 95E-01 295 . 21
- 19 . 20 1 . 67E-01 9 . 09E-02 351. 92
- 37 . 20 7.79E-02 9 . 56E -02
+ PA-228 89 . 95 22 . 00 4.37E+00 3 . l0E+00 5 . 27E+00 93 . 35 35 . 00 1 . 16E+00 3 . l0E+00 105 . 00 16 . 30 3 . 54E-01 5 . 91E+00 129 . 22 2 . 97 8. 71E+00 3 . 18E+0l 338 . 32 5 . 30 1. 22E+0l 2 . 03E+0l 463 . 00 13 . 80 1. 4 7E+00 8 . 07E+00 911 . 23 16 . 70 1 . 28E+0l l . 13E+0l
+ AM- 241 59 . 54 36.30 7 . 79E-02 2 . llE - 01 2 . llE-01
+ CM-243 103 . 76 23 . 00 -5 . 09E-02 l . 30E-01 l . 30E-01 228 . 18 10 . 60 - 1 . 22E-02 2 . 62E - 01 277 . 60 14 . 00 5 . 09E-02 2 . 21E - 01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA al 95% confidence level 10/7/2020 Page 57
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 1:13:16AM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-016-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL 10/7/2020 Page 58
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 2:20:51AM Page I of7
.lrf'Apex-Gamma Analysis Report for L2-SUB-102-AJGS-017-SB L2-011 -1 02 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-017-SB /
Sample Description : L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 9.003E+02 grams Facility : Dairy1and_NPP Sample Taken On : 4/5/2018 10:36:00AM Acquisition Started : 4/10/2018 1:20:28AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611 .1 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4252 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/10/2018 2:20:42AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 59
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 2:20:51 AM Page 2 of7 Analysis Report for L2-SUB-102-AJGS-017-SB L2-011 -102 RA CWD SOIL / PACKAGE#: L2-SUB-102 RA CWD SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 76 . 33 147 - 159 153 . 20 2 . 14E+02 61 . 61 1 . 34E+03 2 . 93 F 2 185 . 82 366 - 377 372 . 13 8 . 68E+0l 39 . 09 7 . 15E+02 1. 86 M 3 238 . 64 470 - 490 477 . 75 3 . 25E+02 44 . 89 4 . 07E+02 1. 41 m 4 241. 93 470 - 490 484 . 34 9.23E+0l 28 . 37 3 . 66E+02 1. 42 F 5 295 . 15 584 - 594 590 . 75 1 . 58E+02 33 . 49 3 . 15E+02 1. 60 F 6 337 . 89 669 - 684 676 . 21 5 . 32E+0l 23 . 64 3 . 12E+02 1. 66 F 7 351. 79 699 - 710 704 . 01 2.32E+02 36 . 38 2 . 66E+02 1. 58 F 8 583 . 03 1161 - 1174 1166 . 40 l . 14E+02 25 . 89 1 . 35E+02 2 . 01 F 9 609 . 17 1213 - 1226 1218 . 67 l . 78E+02 30 . 29 l . 41E+02 1. 72 F 10 784 . 79 1566 - 1573 1569 . 86 1. 55E+0l 11.23 4 . 61E+0l 1.03 F 11 910 . 88 1815 - 1827 1822 . 01 6 . 32E+0l 19 . 19 8 . l0E+0l 1. 65 F 12 968 . 95 1933 - 1942 1938 . 11 3 . 00E+0l 16 . 97 8 . 35E+0l 1. 92 F 13 1460 . 48 2912 - 2928 2921. 07 4 . 49E+02 43 . 66 5 . 90E+0l 2 . 33 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Perfonned on : 4/10/2018 2:20:42AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Oata\000000 1364 .CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76 . 33 2 . 14E+02 61 . 61 2 . 14E+02 6 . 16E+0l F 2 185 . 82 8 . 68E+0l 39 . 09 8 . 68£+01 3 . 91E+0l M 3 238 . 64 3 . 25E+02 44 . 89 3 . 25E+02 4 . 498+01 m 4 241. 93 9 . 23E+0l 28 . 37 9 . 23E+0l 2 . 84E+0l F 5 295 . 15 1. 58E+02 33 . 49 1. 58E+02 3 . 35E+0l F 6 337 . 89 S . 32E+0l 23 . 64 5 . 32E+0l 2 . 36E+0l F 7 351 . 79 2 . 32E+02 36 . 38 8 . 36E+0l 3 . 72E+0l 1 . 48E+02 5 . 20E+0l F 8 583 . 03 1 . 14E+02 25 . 89 1 . 14E+02 2 . 59E+0l F 9 609 . 17 1 . 78E+02 30 . 29 4 . 12E+0l 2 . 42E+0l 1. 36E+02 3 . 88E+01 F 10 784 . 79 1. 55E+0l 11 . 23 1 . 55E+0l 1 . 12E+0l F 11 910 . 88 6 . 32E+0l 19 . 19 6 . 32E+0l 1 . 92E+0l F 12 968 . 95 3 . 00E+0l 16 . 97 3 . 00E+0l l . 70E+0l F 13 1460 . 48 4 . 49E+02 43 . 66 5 . 63E+0l 1 . 71E+0l 3 . 93E+02 4 . 69E+0l 10/7/2020 Page 60
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 2:20:51 AM Page 3 of7 Analysis Report for L2-SUB-102-AJGS-017-SB l2-011-102 RA CWD SOIL/ PACKAGE#: l2-SUB-102 RA CWD SOIL M = First peak in a multiplet reg ion m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K- 40 0 . 98 1460 . 75
- 10 . 67 4 . 75E+OO 6 . 26E - 01 PB - 212 0 . 97 77 .11
- 17 . 50 3 . 40E-01 l . OOE - 01 238 . 63
- 44 . 60 1 . 86E-01 2 . 75£ - 02 BI-214 0 . 34 609 . 31
- 46 . 30 l . 75E-01 5 . 0SE - 02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB-214 0 . 98 77 . 11
- 10 . 70 S . 57E-01 1 . 64E - 01 295 . 21
- 19 . 20 2 . SlE-01 5 . 46E-02 351 . 92
- 37 . 20 l .4 2E - 01 5 . 04E - 02 RA - 226 0 . 97 186 . 21
- 3 . 28 5 . 69E- 01 2 . 58E - 01 AC - 228 0 . 59 209 . 28 4 . 40 338.32
- 11. 40 l . 61E-01 7 . 18E- 02 794 . 70 4 . 60 911 . 60
- 27 . 70 1 . 95E - 01 5 . 97E - 02 964 . 60 5 . 20 969 . 11
- 16 . 60 1 . 63E-Ol 9 . 2 4E - 02
* =Energy line found in the spectrum.
- =Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma 10/7/2020 Page 61
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 2:20:51AM Page 4 of7 Analysis Report for L2-SUB-102-AJGS-017-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams) K-40 0 . 988 4 . 75E+OO 6 . 26E - 01 PB - 212 0 . 973 l . 88E- 01 2 . 65E- 0 2 BI-214 0 . 348 l . 75E-01 5 . 0S E-02 1?B- 21 4 0 .9 83 l . 95E -0 1 3 . 62E - 02 RA - 226 0 . 976 5 . 69E - 01 2 . 58E-01 AC-228 0 . 595 l . 77E-01 4 . llE - 02
? nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 62
LAC LTP - Final Status Survey Package - 3/21/2018 4/1012018 2:20:51 AM Page 5 of7 Analysis Report for L2-SUB-102-AJGS-017-SB L2-011-102 RA CWD SOIL / PACKAGE#: L2-SUB-102 RA CWD SOIL UNIDENTIFIED PEAKS Peak Locate Performed on : 4/1012018 2:20:42AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide m 4 241 . 93 2 . 56479£-02 15 . 36 f"b.-z,, ti F 8 583 . 03 3 . 16827E- 02 11 . 35 -r1-VJ!J F 10 784 . 79 4 . 31370E - 03 36 . 17 Tol. BI - 212 M = First peak in a multiplet region m :: Other peak in a multiplet region F :: Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_ N PP\Library\HOTLAB. NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV)
+ K-40 1460 . 75 ... 10 . 67 4.75£+00 6.26E - 01 6.26£ - 01
+ AR-41 1293 . 64 99 . 16 8 . 77E+l6 l . 16E+l7 l . 16E+l 7
+ CO - 60 1173 . 22 100 . 00 3 . 71E - 02 5 . 0lE - 02 / 5 . 79E - 02 1332 . 4 9 100.00 4 . 62£-02 5 . 0lE - 02
+ KR-85 513 . 99 0 . 43 l . 13E+0l 9 . 33E+00 9 . 33E+00
+ Y-88 898.04 93.70 - 8 . 94E - 03 3 . 26E- 02 4 . 93E- 02 1836.06 99 . 20 - l . 83E - 02 3 . 26E - 02
+ NB-94 702.63 100.00 l . 30E - 02 3 . 65E - 02 3 . 65E - 02 871 . 10 100.00 7 . 33E - 03 4 . 36E-02
+ I - 131 284.30 6 . 06 9 . 85E-02 5 . 68E-02 7 . 58E-01 364 . 48 81 . 20 5 . 88E - 04 5 . 68E-02 636 . 97 7 . 27 5 . 15E-0l 7 . 65E-01
+ CS-134 604 . 70 97 . 60 - 1 . 98£ - 02 5 . 22E- 02 5 . 30E-02 10/7/2020 Page 63
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 2:20:51AM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-017-SB L2-011-102 RA CWD SOIL / PACKAGE#: L2-SUB-102 RA CWD SOIL Nuclide Energy Yield(3/4) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCilgrams) (pCilgrams) (keV) CS - 134 795 . 84 85 . 40 2 . 54E - 03 5 . 22E-02 5 . 22E - 02
+ CS - 137 661 . 65 85 . 12 8 . 96E-02 5 . 45E-02 5 . 45E-02
+ CE - 144 80 . 12 1. 36 - l . 36E+O0 2 . 66E- 01 3 . 33E+OO 133 . 51 11 . 09 -6 . 85E- 02 , / 2 . 66E - 01
+ EU-152 121 . 78 28 . 40 - 1. 39E - 01 1 . 00E-01 l . 00E-01 244 . 69 7.49 -4 . 00E- 02 4 . 88E - 01 964 . 00 14 . 44 3 . 42E - 01 3 . 71E - 01 1408 . 00 20 . 74 -1 . 24E- 01 l . 90E-0l
+ EU - 154 123 . 07 40 . 40 - S . 06E - 02 7 . 16E-02 / 7 . 16E-02 247 . 94 6 . 60 6 . 56E - 02 4 . 93E-Ol 723 . 30 19 . 70 1. 0OE- 01 2 . 03E-0l 873 . 20 11. 50 2 . 59E - 01 3 . 82E-01 1004 . 76 17 . 90 9 . 15E- 02 2 . 68E - 01 1274 . 51 35 . 50 - l . llE - 01 1. 33E - 01
+ EU-155 86 . 54 32 . 80 - 6 . 35E-02 l . 14E- 01 l.14E - 01 105 . 31 21. 80 - 1. 37E - 02 1 . 45E - 01
+ BI-214 609 . 31
- 46 . 30 1. 75E - 01 8 . 57E-02 8 . 57E - 02 1120 . 29 15 . 10 3 . 56E - 01 3 . 80E-01 1238 . 11 5 . 94 1. 20E+00 l.06E+00 1377 . 67 4 . 11 l. 78E - 01 9 . 49E - 01 1407 . 98 2 . 48 - 1 . 03E+00 1 . 58E+00 1509 . 19 2 . 19 7 . 96E - 01 1. 68E+O0 1764 . 49 15 . 80 2 . 92E- 01 3 . 44E-01
+ PB- 214 77 . 11
- 10 . 70 5 . 57E - 01 9 . 00E -0 2 3 . 67E - 01 295 . 21
- 19 . 20 2 . 51E- 01 l . 06E- 01 351. 92
- 37 . 20 1 . 42E- 01 9 . 00E- 02
+ PA- 228 89 . 95 22 . 00 7 . 66E+0O 3 . 27E+00 5 . 56E+00 93 . 35 35 . 00 - 4 . 98E- 01 3 . 27E+00 105 . 00 16 . 30 2 . 57E+00 6 . 48E+00 129 . 22 2 . 97 6 . 28E+00 3 . 30E+0l 338 . 32 5 . 30 l . 04E+0l 1 . 96E+0l 463 . 00 13 . 80 l . 46E+00 8 . 24E+0O 911 . 23 16 . 70 9 . 85E+00 l. llE+Ol
+ AM- 241 59 . 54 36 . 30 3 . 68E-02 2 . 08E- 01 2 . 08E- 01
+ CM- 243 103 . 76 23 . 00 8 . 48E - 02 l . 38E- 01 l . 38E - 01 228 . 18 1 0. 60 - 6 . 45E-02 2 . 71E- 01 277 . 60 14 . 00 - 4 . 1 4E- 02 2 . 19E- 01
+ = Nuclide identffied during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 64
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 2:20:51 AM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-017-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL 10/7/2020 Page 65
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 3:24:56AM Page I of6 pex-Gamma Analysis Report tor L2-SUB-102-AJGS-018-SB L2-011 -102 RA cw SOIL I PACKAGE#: L2-SUB-102 RA cw SOIL GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-018-SB / Sample Description : L2-011-102 RA cw SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 9.183E+02 grams / Facility : Dairyland_ NPP Sample Taken On : 4/5/2018 10:53:00AM Acquisition Started : 4/10/2018 2:24:34AM Procedure : 500ml Marinelli Operator : Adm inistrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3610.9 seconds Dead nme : 0.30 % Peak locate Threshold : 3.00 Peak Locate Range (In channels) : 100 - 4096 Peak Area Range (in channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/812014 Efficiency Calibration Description Sample Number : 4253 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/1012018 3:24:47AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 66
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 :$:24:56AM Page 2 of6 Analysis Report for L2-SUB-102-AJGS-018-SB L2-011-102 RA CWD SOIL I PACKAGE#: L2-SUB-102 RA CWD SOIL Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 75 . 78 147 - 158 152 . 12 l . 94E+02 58 . 28 l . 17E+03 3 . 38 F 2 238 . 57 473 - 485 477 . 62 3.15E+02 45 . 99 5 . 88E+02 1. 61 F 3 295 . 30 586 - 595 591. 05 9 . 47E+Ol 28 . 49 3 . 18E 02 1. 27 F 4 338 . 51 670 - 684 677 . 46 6.06E+Ol 25 . 03 3 . 40E+02 1. 60 F 5 351. 80 699 - 709 704 . 02 l . 80E+02 32 . 50 2 . 46E+02 l. 34 F 6 582 . 98 1162 - 1172 1166 . 29 5 . 93E+Ol 21 . 99 1 . 35E+02 1. 96 F 7 609 . 18 1213 - 1223 1218 . 69 1 . 22E+02 26 . 01 l . 24E+02 1. 49 F 8 911 . 13 1816 - 1827 1822 . 51 4.70E+Ol 17 . 89 9 . 36E+Ol 1. 61 F 9 968 . 92 1934 - 1945 1938 . 06 3 . 25E+Ol 15 . 34 7 . 19E+Ol 1. 43 F 10 1120 . 06 2236 - 2245 2240 .3 1 2 .8 0£+01 14 . 35 5 . 38E+Ol 1.57 F 11 1460 . 65 2914 - 2931 2921.41 5 . 20E+02 47 . 01 2 . 75E+Ol 2 . 32 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/10/2018 3:24:47AM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F l 75.78 l . 94E+02 58 . 28 1 . 94£+02 5 . 83E+Ol F 2 238 . 57 3 . 15E+02 45 . 99 3 . 15£+02 4 . 60E+Ol F 3 295 . 30 9 . 47E+Ol 28 . 49 9 . 47E+Ol 2 . 85E+Ol F 4 338 . 51 6 . 06E+Ol 25 . 03 6 . 06E+Ol 2 . 50E+Ol F 5 351 . 80 l . 80E+02 32 . 50 8 . 36E+Ol 3 . 72E+Ol 9 . 65E+Ol 4 . 94E 01 F 6 582 . 98 5 . 93E+Ol 21 . 99 5 . 93E+Ol 2 . 20E+Ol F 7 609 . 18 l . 22E+02 26 . 01 4. 12E+Ol 2.42E+Ol 8 . 0SE+Ol 3 . 55E 01 F 8 911.13 4 . 70E+Ol 17 . 89 4 . 70E+Ol 1. 79E+Ol F 9 968 . 92 3 . 25E+Ol 15 . 34 3 . 25E+Ol 1. 53E+Ol F 10 1120 . 06 2 . 80E+Ol 14 . 35 2 . 80E+Ol 1.44E+Ol F 11 1460 . 65 5 . 20E+02 47 . 01 5 . 63E+Ol 1 . 71E+Ol 4 . 64E+02 5 . 00E+Ol
=
M First peak in a multiplet region
=
m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000s!gma 10/7/2020 Page 67
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/201 8 3:24:56AM Page 3 of6 Analysis Report for L2-SUB-102-AJGS-018-SB L2-011-102 RA CWD SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0 . 99 1460 . 75
- 10 . 67 5 . SOE+OO 6 . 68E - 01 PB - 212 0 . 56 77 . 11 17 . so 238 . 63
- 44 . 60 1 . 77E - 01 2 . 74E - 02 BI - 214 0 . 58 609 . 31
- 4 6 . 30 1. OlE - 01 4 . 49E-02 1120 . 29
- 15 . 10 1. 86E-01 9 . 59E-02 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB-214 0 . 72 77 . 11 10 . 70 295 . 21
- 19 . 20 l . 48E-01 4 . SOE - 02 351 . 92
- 37 . 20 9 . 0BE - 02 4 . 67E - 02 AC-228 0 . 61 209 . 28 4 . 40 338 . 32
- 11 . 40 l . 80E- 01 7 . 47E-02 794 . 70 4 . 60 911 . 60
- 27 . 70 l . 42E-Ol 5 . 44E- 02 964 . 60 5 . 20 969 . 11
- 16 . 60 l . 73E- 01 8 . 20E - 02
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
=
@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERE NCE CORRECTE D REPORT 10/7/2020 Page 68
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 3:24:56AM Page4 of6 Analysis Report for L2-SUB-102-AJGS-018-S8 L2-011 -102 RA CWD SOIL I PACKAGE#: L2-SUB-102 RA CWD SOIL Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams) K-40 0.998 5 . SOE+OO 6 . 68E- Ol PB - 212 0 . 560 l . 77E-01 2 . 74E - 02 BI - 214 0.582 l . 16E-Ol 4 . 07E - 02
?B- 214 0 . 720 l . 20E-Ol 3 . 24E - 02 AC-228 0 . 617 1. 59E-01 3 . 87E-02
? nuclide is part of an undetennined solution X nuclide rejected by the interference analysis
@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 69
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 3:24:56AM Page 5 of6 Analysis Report for L2-SUB-102-AJGS-0 18-SB L2-011-102 RA CWO SOIL/ PACKAGE#: L2-SUB-102 RA CWD SOIL UNIDENTIFIED PEAKS Peak Locate Performed on : 4110/2018 3:24:47AM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 75 . 78 5 . 389llE-02 15 . 02 -;1., z,o'o F 6 582 . 98 1. 64838E-02 18 . 53 '7/ -t,DfJ M = First peak in a multiplet region m = Other peak in a multiplet region F = Fftted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_N PP\Library\HOTLAB.N LB Nuclide Energy Yield(3/4) Activity NuclideMDA Line MDA Name (pCl/grams) (pCi/grams) (pCilgrams) (keV)
+ K- 40 1460 . 75
- 1 0 . 67 S . 50E+00 5.43E - 01 5 . 43E - 01
+ AR- 41 1293 . 64 99 . 16 - 1 . 50E+l7 l . 23E+17 / l . 23E+l7
+ CO - 60 1173 . 22 100 . 00 -2 . 27E - 02 5 . 22E - 02 5 . 45E - 02 1332 . 49 100 . 00 4 . 45E- 02 5 . 22E - 02
+ KR - 85 513 . 99 0 . 43 1 . 03E+0l 9 . 05E+00 9 . 05£+00
+ Y- 88 898 . 04 93 . 70 - 3 . 20E- 02 3 . 39E - 02 4 . 39E - 02 1836 . 06 99 . 20 -2 . 35E- 02 3 .3 9E - 02
+ NB-94 702 . 63 100 . 00 2 . 28£- 02 3 . 90E - 02 3 . 90E - 02 871 . 10 100 . 00 3 . 31E-02 4 . 21E - 02
+ I - 131 284.30 6 . 06 - 3 . SlE-01 5 . 40E - 02 6 . 93E - 01 364 . 48 81 . 20 L21E - 02 5 . 40E- 02 636 . 97 7 . 27 4 . 00E - 01 7 . 35E - 01
+ CS - 134 604 . 70 97 . 60 6 . 58£ - 02 4 . 77E - 02 4 . 80E - 02 795 . 84 85 . 40 - 1 . llE - 03 4 . 77E - 02
+ CS-137 661 . 65 85 . 12 8 . 15E- 02 S . 21E - 02 5 . 21£-02 10/7/2020 Page 70
LAC LTP - Final Status Survey Package - 3/21/2018 4/10/2018 J:24:56AM Page 6 of 6 Analysis Report for L2-SUB-102-AJGS-018-SB L2-011-102 RA CWO SOIL/ PACKAGE#: L2-SUB-102 RA CWO SOIL Nuclide Energy Yield(%) Activity Nuclide MDA LlneMDA Name (pCilgrams) (pCilgrams) (pCi/grams) (keV)
+ CE - 144 80 . 12 1. 36 -2.50E+OO 2 . 49£ - 01 3.17E+OO 133 . 51 11 . 09 l.30E-01 2 . 49E-01
+ EU-152 121.78 28 . 40 -2.53E-02 9 . 66E - 02 / 9 . 66E - 02 244 . 69 7 . 49 -3 . lOE - 01 4 . 70E - 01 964 . 00 14 . 44 - 3 . 50E - 02 3 . 67E - 01 1408 . 00 20 . 74 - 8 . 82E-02 1 . 97E-01
+ EU-154 123 . 07 40 . 40 l.23E-02 6 . 83E-02 6 . 83E-02 247 . 94 6 . 60 - 7 . 43E-01 4 . 70E-01 723 . 30 19 . 70 l . 78E - 01 2 . 14E-01 873 . 20 11. 50 -2 . 20E-01 3 . SOE-01 1004 . 76 17 . 90 8 . llE-02 2 . SOE-01 1274 . 51 35 . 50 l . 89E-02 l . 40E - 01
+ EU-155 86 . 54 32.80 -5.04E - 02 l . lOE - 01 l . lOE - 01 105 . 31 21. 80 8 . 71E-02 1 . 33E - 0 1
+ BI-214 609 . 31
- 46 . 30 l . OlE-01 7 . 89E- 02 7.89E - 02 1120 . 29
- 15.10 l.86E-01 1. 89E-01 1238 . 11 5 . 94 -l . 99E-01 9 . 76£-01 1377 . 67 4 . 11 8 . 06E - 01 l . OlE+OO 1407 .9 8 2 . 48 - 7 . 37E - 01 l . 64E+OO 1509 . 19 2 . 19 9 . 21E-01 1 . 82E+OO 1764 . 49 15 . 80 l . 57E - 01 2 .9 1E- 01
+ PB- 214 77 . 11 10 . 70 4 . 75E - 01 8 . 58E - 02 4 . 27E - 01 295 . 21
- 19 . 20 l.48E-01 l . OlE-01 351 .9 2
- 37 . 20 9.08E-02 8 . 58E-02
+ PA - 228 89 . 95 22 . 00 6 . 91E+OO 3 . 16E+OO 5 . 43E+OO 93 . 35 35.00 6 . 0lE-01 3 . 16E+OO 105 . 00 16 . 30 2 . 34E+OO 6 . 02E+OO 129 . 22 2 .9 7 - 8 . 43E+OO 3 . 08E+Ol 338 . 32 5 . 30 5 . 54E+OO 2 . 06E+Ol 463.00 13 . 80 -5 . 23E - 01 8 . 0lE+OO 911.23 16 . 70 l . 34E +Ol l . 04E+Ol
+ AM-241 59 . 54 36 . 30 3 . 64E - 02 1. 97E -O l l . 97E-01
+ CM-243 103 . 76 23 . 00 6 . 88E - 02 l . 27E - 01 l.27E - 01 228 . 18 10 . 60 l . 61E - 02 2 . 61E - 01 277 . 60 14 . 00 3 . 70E - 02 2 . 09E - 01
+ = Nuclide identified during the nuclide Identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 71
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 2:32:39PM Page I of7
.JApex-Gamma Analysis Report for L2-SUB-102-AJGS-019-SB 04/05/18 - 1229 L_ 1-, o, l - I o-i- rtA C,)..>.J t So, I GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-019-SB ,r" Sample Description : 04/05/18 - 1229 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 6.967E+02 grams /
Facility : Dairyland_NPP Sample Taken On : 4/512018 12:29:00PM Acquisition Started : 4/6/2018 1:32:16PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real nme : 3611.2 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/812014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4236 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/6/2018 2:32:30PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 72
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 2:32 :39PM Page 2 of 7 Analysis Report for L2-SUB-102-AJGS-019-SB 04/05/18 - 1229 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) M 1 74 . 60 142 - 161 149 . 74 1 . 82E+02 44 . 41 1. 05E+03 1. 43 m 2 76 . 97 142 - 161 154 . 48 2 . 71E+02 49 . 68 9 . 17E+02 1. 43 M 3 87 . 12 167 - 192 174 . 78 1 . 74E+02 59 . 69 1. 84E+03 3 . 77 m 4 91 . 91 167 - 192 184 . 36 2 . 22E+02 62 . 77 1 . 73E+03 3 . 78 F 5 186 . 21 366 - 380 372 . 92 1. 28E+02 44 . 19 8 . 86E+02 2 . 33 F 6 238 . 50 472 - 481 477 . 47 4 . 22E+02 52 . 82 6 . 98E+02 1. 24 M 7 295 . 30 588 - 604 591.06 l . 32E+02 31. 71 2 . 78E 02 1.19 m 8 300 . 08 588 - 604 600 . 61 3 . 84E+Ol 22 . 61 3 . 19E+02 1. 20 F 9 338 . 29 671- 683 677 . 02 l . 22E+02 28 . 74 2 . 81E+o2 1. 43 F 10 351. 80 700 - 709 704 . 02 2 . 60£+02 37 . 37 2 . 08E+02 1. 51 F 11 583 . 00 1158 - 1171 1166 . 35 1 . 13E+02 25 . 90 l . 69E+02 1. 54 F 12 609 . 22 1213 - 122 4 1218 . 77 2 . 12E+02 32 . 99 1 . 38£+02 1. 77 F 13 910 . 95 1814 - 1828 1822 . 14 8 . 82E+Ol 22 . 13 9 . 33£+01 1. 87 F 14 968 . 82 1933 - 1945 1937 . 87 5 . 70E+Ol 20 . 73 1 . 15£+02 2 . 01 F 15 1120 . 1 4 2232 - 2245 2240 . 46 4 . SOE+Ol 17 . 03 7 . llE+Ol 2 . 10 F 16 1332 . 54 2660 - 2672 2665 . 21 2 . 57E+Ol 12 . 72 2 . 53E+Ol 2 . 19 F 17 1460 . 56 2914 - 2929 2921.24 5 . 19E+02 46 . 96 3 . 84E+Ol 2 . 42 F 18 1764 . 38 3523 - 3535 3528 . 83 2 . 81E+Ol 11 . 75 l . 39E+Ol 1. 67 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/6/2018 2:32:30PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. M l 74 . 60 l . 82E+02 4 4. 41 l . 82Et02 4 . 44E+Ol m 2 76 . 97 2 . 71E+02 49 . 68 2 . 71E+02 4 . 97E+Ol M 3 87 . 12 1 . 74£+02 59 . 69 l . 74E+02 5 . 97£+01 m 4 91. 91 2 . 22E+02 62 . 77 2 . 22£+02 6 . 28E+Ol F 5 186 . 21 1 . 28E+02 44 . 19 1 . 28E+02 4 . 42E+Ol F 6 238 . 50 4 . 22E+02 52 . 82 4 . 22E+02 5 . 28E+Ol M 7 295 . 30 1 . 32E+02 31 . 71 l . 32E+02 3 . 17E+Ol m 8 300 . 08 3 . 84E+Ol 22 . 61 3 . 84E+Ol 2 . 26E+Ol F 9 338 . 29 1 . 22E+02 28 . 74 l . 22E 02 2 . 87E+Ol F 10 351. 80 2 . 60E+02 37 . 37 8 . 36E+Ol 3 . 72E+Ol 1 . 77E+02 5 . 27E+Ol F 11 583 . 00 1 . 13E+02 25 . 90 l . 13E+02 2 . 59E+01 10/7/2020 Page 73
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 2:32:39PM Page3 of7 Analysis Report for L2-SU B-102-AJGS-019-SB 04/05/18 - 1229 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 12 609 . 22 2 . 12E+02 32 . 99 4 . 12E+01 2 . 42E+01 1 . 71E+02 4 . 09E+Ol F 13 910 . 95 8 . 82E+01 22 . 13 8 . 82E+Ol 2 . 21E+Ol F 14 968 . 82 5 . 70E+Ol 20 . 73 5 . 70E+Ol 2 . 07E+Ol F 15 1120 . 14 4 . SOE+Ol 17 . 03 4 . SOE+Ol l . 70E+Ol F 16 1332 . 54 2 . 57E+Ol 12 . 72 2 . 57E+Ol 1 . 27E+Ol F 17 1460 . 56 5 . 19E+02 46 . 96 5 . 63E+Ol 1 . 71E+01 4 . 62E+02 5 . 00E+Ol F 18 1764 . 38 2 . 81E+Ol 11. 75 l . 52E+Ol 9 . 80E+OO 1.29E+Ol l . 53E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncerta inty K- 40 0 . 99 1460 . 75
- 10 . 67 7 . 23E+OO 8 . 79E - 01 PB - 212 0 . 99 77 . 11
- 17 . so 5 . 49E- 01 1. 07E-01 238 . 63
- 44 . 60 3 . 12E- 01 4 . 23E-02 BI - 214 0 . 78 609 . 31
- 46 . 30 2 . 83E - 01 6 . 95E- 02 1120 . 29
- 15 . 10 3 . 94E - 01 l . SOE - 01 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49
- 15 . 80 l . 60E- 01 1.90E - 01 PB-214 0 . 99 77 . 11
- 10 . 70 8 . 97E- 01 l . 75E - 01 295 . 21
- 19 . 20 2 . 70E - 01 6 . 65E - 02 351 . 92 37 . 20 2 . 19E- 01 6 . 63E- 02 RA- 226 1.00 186 . 21
- 3 . 28 l . 09E+OO 3 . 79E - Ol AC - 228 0 . 60 209 . 28 4 . 40 338 . 32
- 11. 40 4 . 77E- 01 l . lSE - 01 794 . 70 4 . 60 911 . 60
- 27 . 70 3 . SlE- 01 8 . 94E - 02 96 4. 60 5 . 20 969 . 11
- 16 . 60 4 . 00E-01 l . 46E-01 10/7/2020 Page 74
LAC LTP - Final Status Survey Package - 3/21/2018 4/612018 2:32:39PM Page4 of7 Analysis Report for L2-SUB-102-AJGS-019-SB 04/05/ 18 - 1229
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)
K-40 0 . 994 7 . 23E+OO 8 . 79E - 01 PB-212 0 . 997 3 . 23E - Ol 3 . 95E-02 BI-214 0 . 786 2 . 88E-Ol 5 . 98E - 02 PB-214 0 . 998 2 . 53£-01 4 . SSE - 02 RA-226 1 . 000 1 . 09E+OO 3 . 79E - 01 AC - 228 0 . 604 3 . 99E - 01 6 . 35E - 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 75
LAC LTP - Final Status Survey Package - 3/21/2018 4/612018 2:32:39PM Page 5 of7 Analysis Report for L2-SUB-102-AJGS-019-SB 04/05/18 - 1229 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/6/2018 2:32:30PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 1 74 . 60 5 . 05166E- 02 12 . 21 fi- t,t iji:1f K01j1 M 3 87 . 12 4 . 83439E-02 17 . 15 Tol. EU - 155 m 4 91 . 91 6 . 15711E- 02 1 4 . 16 --(A ... z~I/ m 8 300 . 08 1 . 06542E - 02 29 . 4 8 :a, . , -z,J-Z., F 11 583 . 00 3 . 15025E- 02 11. 42 ,r-1,z,tJfJ F 16 1332 . 54 7 . 13670E- 03 24 . 75 e~-u.v M = First peak in a multiplet region m = other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{%) Activity Nuclide MDA LlneMDA Name (pCl/grams) (pCl/grams) (pC//grams) (keV)
+ K- 40 1460 . 75
- 10 . 67 7 . 23E+00 7 . 44 E-01 7 . 44E - 01
+ AR - 41 1293 . 64 99 . 16 5 . 58E+02 l . 18E+03 l . 18E+03 CO-60 1173 . 22 100 . 00 2 . 02E- 02 7 . 07E-02 8 . 21E - 02 1332 . 4 9 100 . 00 4 . 94 E- 02 7 . 07E-02
+ KR- 85 513 . 99 0 . 43 l . 54E+0l l . 25E+Ol l . 25E+Ol 10/7/2020 Page 76
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2018 2:32:39PM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-019-SB 04/05/1 8 - 1229 Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (pCilgrams) (pCi/grams) (pCilgrams) (keV)
+ Y-88 898.04 93 . 70 7 . 16E-03 4 . 71E- 02 5 . 94E-02 1836 . 06 99 . 20 -4 . 62E-02 4 . 71E-02 NB-94 702 . 63 100 . 00 l . 59E-03 5 . 41E-02 5 . 41E-02 871 . 10 100 . 00 -8 . 42E- 03 6.03E-02
+ I-131 284 . 30 6 . 06 -7 . 70E-01 5 . 54E-02 7 . 30E-01 364. 48 81. 20 2 . 55E-02 5 . 54E-02 636 . 97 7 . 27 2 . 14E-01 7 . 85E-01
+ CS - 134 604 . 70 97 . 60 -2 . 39E-02 6 . 33E-02 7 . 20E-02 795 . 84 85 . 40 -4.43E-02 6 . 33E-02
+ CS - 137 661 . 65 85 . 12 1. 06£-01 7 . 45E-02 / 7 . 45E - 02
+ CE-144 80 . 12 1. 36 -3 . 63E-01 3 . 40E-01 4.67E+00 133 . 51 11. 09 l.12E - 03 3 . 40E-01
+ EU-152 121 . 78 28 . 40 -5.84£-02 1. 34E-01 ./ 1 . 34£-01 244 . 69 7 . 49 - 2 . 09£+00 6 . 97£-01 964 . 00 14 . 44 - 2 . l0E - 01 5 . 34£-01 1408 . 00 20 . 74 1. 4 6E - 0l 2 . 95E - 0 1
+ EU-154 123 . 07 40 . 40 -3 . 48E-02 9 . 43E - 02 ./ 9 . 43E - 02 247 . 94 6 . 60 -3 . 73E 00 6.73E-0l 723 . 30 19 . 70 2 . 87E - 01 2.92E-01 873 . 20 11. 50 3 . 67E-0l 5 . 26E-01 1004.76 17.90 -2 . 35E-01 3 . 21E - 01 1274 . 51 35 . 50 5 . 85E-02 1.93E-01
+ EU - 155 86 . 54 32 . 80 -1. 36E-02 l . 61E-01 1 . 61E-01 105.31 21. 80 -l. l0E - 02 l . 84E-01
+ BI - 214 609.31
- 46 . 30 2 . 83E-01 1 . 08E- 01 l . 08E-01 1120 . 29
- 15 . 10 3 . 94£-01 3 . 12E-01 1238 . 11 5 . 94 - 7 . 92E-01 l . 46E+00 1377 . 67 4 . 11 7 . llE-01 1.41E+00 1407 . 98 2.48 1.22E+00 2 . 47E+00 1509 . 19 2 . 19 -5.88E-02 2 . 21E+00 1764 . 49
- 15 . 80 1. 60E-01 3 . 45E-01
+ PB-214 77 . 11
- 10 . 70 8 . 97E - 01 1 . 09£ - 01 3 . 39£ - 01 295 . 21
- 19.20 2 . 70E-01 l . 18E- 01 351 . 92
- 37 . 20 2 . 19E- 01 1.09£- 01
+ PA - 228 89 . 95 22 . 00 l.26E+00 2 . 99£- 01 5 . 24E-01 93 . 35 35 . 00 - 5 . 28£ - 02 2 . 99£- 01 105 . 00 16 . 30 4 . 65E - 02 5 . 54E-01 129 . 22 2 . 97 - 1 . 07E+00 2 . 81E+00 338 . 32 5 . 30 7 . 73E - 01 1 . 92E+00 463 . 00 13 . 80 -2 . 24E-01 7.84E-01 911.23 16 . 70 l. l 7E+00 1. 02E+00
+ AM- 241 59 . 54 36 . 30 8 . 95£-02 2 . 85£ - 01 2.85E - 0l
+ CM-243 103 . 76 23 . 00 6 . 22£-02 1 .7 6£-01 1 . 76E-0l 228 . 18 10 . 60 - l . 02E-0l 3 . 60£-01 277 . 60 14 . 00 -2. 4 6E-01 2 . 89£- 01 10/7/2020 Page 77
LAC LTP - Final Status Survey Package - 3/21/2018 4/6/2010 2:32:39PM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-019-SB 04/05/18 - 1229
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 78
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 12:17:31PM Page I of7
~pex-Gamma Analysis Report for L2-SUB-102-AJGS-020-SB 04/05/18 -1351 L2- ~()\ \ -102 f!_.A
(_,v..lD So; I GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-020-SB / Sample Description : 04/05/18 - 1351 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 8.359E+02 grams Facility : Dairyland_NPP Sample Taken On : 4/512018 1:51 :00PM Acquisition Started : 4/9/2018 11 :17:08AM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3610.8 seconds Dead Time : 0.30 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100- 4096 Peak Area Range (in channels) : 100- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4240 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/9/2018 12:17:22PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 79
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 12:17:31PM Page 2 of7 Ana lysis Report for L2-SUB-102-AJGS-020-SB 04/05/18 - 1351 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 75 . 95 147 - 161 152 . 45 2 . 26E+02 62 . 54 1. 37E+03 4 . 41 F 2 185 . 63 364 - 377 371 . 76 8 . 85E+Ol 38 . 57 8 . 13E+02 1. 83 F 3 238 . 49 4 70 - 485 477 . 46 2 . 65E+02 41. 30 6 . 60E+02 1. 26 F 4 295 . 11 582 - 596 590 . 68 7 . 04E+ Ol 27 . 82 4 . 96E+02 1. 32 F 5 338 . 21 673 - 683 67 6 . 85 6 . 28E+Ol 23 . 54 2 . 22E+02 1. 43 F 6 351 . 68 698 - 709 703 . 79 l . 53E+02 31.55 2 . 70E+02 1. 51 F 7 582 . 93 1161 - 1173 1166 . 21 9 . 84E+Ol 25 . 08 l . 39E+02 1. 94 F 8 609 . 21 1212 - 1224 1218 . 76 l . 42E+02 27 . 41 l . 01E+02 1. 99 F 9 721 . 5 4 1440 - 1449 1443 . 37 l . 54E+Ol 11 . 67 6 . 80E+Ol 0 . 97 F 10 91 0 . 81 1816 - 1827 1821. 86 5 . 99E+Ol 19 . 72 l . 02E+02 1. 57 F 11 1119 . 29 2234 - 2244 2238 . 77 2 . 83E+Ol 13 . 95 4 . 73E+Ol 1 . 75 F 12 1460 . 31 2912 - 2929 2920 . 73 5 . 14E+02 45 . 89 2 . 23E+Ol 2 . 39 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/9/2018 12:17:22PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 75 . 95 2 . 26E+02 62 . 54 2 . 26E+02 6 . 25E+Ol F 2 185 . 63 8 . 85E+Ol 38 . 57 8 . 85E+Ol 3 . 86E+Ol F 3 238 . 49 2 . 65E+02 41. 30 2 . 65E+02 4 . 13E+Ol F 4 295 . 11 7 . 04E+Ol 27 . 82 7 . 04E+Ol 2 . 78E 01 F 5 338 . 21 6 . 28E+Ol 23 . 54 6 . 28E+Ol 2 . 35E+Ol F 6 351 . 68 l . 53E+02 31. 55 8 . 36E+Ol 3 . 72E+Ol 6 . 95E+Ol 4 . 88E+Ol F 7 582 . 93 9 . 84E+Ol 25 . 08 9 . 84E+Ol 2 . SlE+Ol F 8 609 . 21 l .4 2E+02 27 . 41 4.12E+Ol 2 . 42E +Ol 1 . 01E+02 3 . 66E+Ol F 9 721 . 54 1 . 54E+Ol 11 . 67 1 . 54E+Ol l . 17E+Ol F 10 910 . 81 5 . 99E+Ol 19 . 72 5 . 99E+01 l . 97E+Ol F 11 1119 . 29 2 . 83E+Ol 13 . 95 2 . 83E+Ol l . 39E+Ol F 12 1460 . 31 5 . 14E+02 45 . 89 5 . 63E+Ol l . 71E+Ol 4 . 57E+02 4 . 90E+Ol 10/7/2020 Page 80
LAC LTP - Final Status Survey Package - 3/21/2018 4/912018 12:17:31PM Page 3 of 7 Analysis Report for L2-SUB-102-AJGS-020-SB 04/05/18 -1351 M = First peak in a multiplet reg ion m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_ NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 96 1460 . 75
- 10 . 67 5 . 96E+OO 7 . 19E- 01 PB- 212 0 . 55 77 . 11 17 . 50 238 . 63
- 44 . 60 l . 63E-01 2 . 68E- 02 BI - 214 0 . 55 609 . 31
- 46 . 30 l . 39E - 01 5 . lOE-02 1120.29
- 15 . 10 2 . 07E - 01 l . 02E - 01 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB- 214 0 . 71 77 . 11 10 . 70 295 . 21
- 19 . 20 l . 20E- 01 4 . 80E-02 351 . 92
- 37 . 20 7 . 18E- 02 S . 05E - 02 RA- 226 0 . 94 186 . 21
- 3 . 28 6 . 2 4£ - 01 2 . 74E - 01
* = Energy line found in the spectrum .
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT 10/7/2020 Page 81
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 12:17:31PM Page4 of7 Analysis Report for L2-SUB-102-AJGS-020-SB 04/05/18- 1351 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams) K- 40 0 . 969 5 . 96E+00 7 . 19E- 01 PB-212 0 . 558 1. 63E - 0 1 2 . 68E - 02 BI - 214 0 . 559 l . 52E - 01 4 . 56E - 02 PB- 214 0 . 716 9 . 74E- 02 3 . 48E - 02 RA- 226 0 . 947 6 . 24E- 01 2 . 74E-01
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 82
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 12:17:31PM Page: 5 of7 Analysis Report for L2-SUB-102-AJGS-020-SB 04/05/18 - 1351 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/9/2018 12:1 7:22PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F F 1 5 75.95 338 . 21 6 . 26951E-02 l . 74381E - 02 13 . 85 18 . 75 Tol.
-r-r r,&tJ AC-228 PA- 228 F 7 582 . 93 2 . 73365E - 02 12 . 74 '1/ , ic,tJ F 9 721 . 54 4 . 27114E - 03 37 . 96 ?o,1 f-v ~ /5'1/-
F 10 910 . 81 l . 66347E-02 16. 46 Tol. AC-228 PA- 228 M = First peak in a multiplet region m = Other peak in a multiplet region F " Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland _NPP\librarylHOTLAB. NLB Nuclide Energy Yield(3/4) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCl/grams) (pCilgrams) {ke V)
+ K-40 1460 . 75
- 10.67 S . 96E+00 5 . 87E-01 5 . 87E-01
+ AR- 41 1293 . 64 99 . 16 - 4 . 34E+l3 1 . 56E+14 ../ 1 . 56£+14 CO-60 1173 . 22 100 . 00 5 . 72E-02 5 . 60E-02 6 . 58£ - 02 1332 . 49 100 . 00 6 . 27£- 02 5 . 60£-02
+ KR- 85 513 . 99 0 . 43 1.47£+01 1 . 0lE+Ol l . 0lE+0l
+ Y-88 898 . 04 93 . 70 2 . 56£-03 4 . 09£ - 02 5 . 0SE - 02 1836 . 06 99 . 20 8 . 42E-03 4 . 09£-02
+ NB-94 702 . 63 100 . 00 9 . 70£-03 4 . llE -02 4 . llE-02 871.10 100 . 00 -2.62E-03 4 . SSE-02 10/7/2020 Page 83
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 12:17:31PM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-020-SB 04/05/18 - 1351 Nuclide Energy Yield{%) Activity Nuclide MDA LineMDA Name {pCilgrams) (pCilgrams) (pCilgrams) {keV)
+ I-131 284 . 30 6 . 06 - 5 . 41E-02 5 . 43E-02 7 . 18E-Ol 364 . 48 81.20 -l . OlE - 02 5 . 43E - 02 636 . 97 7 . 27 4 . 27E - 01 6 . 98E-01
+ CS - 134 604 . 70 97 . 60 2 . 07E - 03 5 . 13E- 02 5 . 22E-02 795 . 84 85 . 40 8 . 58E - 03 5 . 13£ - 02
+ CS - 137 661 . 65 85 . 12 6 . 65E - 02 5 . 51£ - 02 ,/ 5 . 51E-02
+ CE- 144 80 . 12 1. 36 -1 . 40E+OO 2 . 73E - 01 3 . 41E+OO 133 . 51 11.09 - 2 . 88E-02 2 . 73E - 01
+ EU - 152 121 . 78 28 . 40 -9 . 18E- 02 1 . 02E-Ol 1 . 02E - 01 244 . 69 7 . 49 - 2 . 74E- 01 4 . 85E - 01 964 . 00 14 . 44 1 . 30E - 01 3 . 73E - 01 1408 . 00 20 . 74 4 . 36E - 02 2 . 02E - 01
+ EU - 154 123 . 07 40 . 40 - 3 . 61E - 02 7 . 20E- 02 7. 20E - 02 247 . 94 6 . 60 -9 . 19E- 01 4 . 82E - 01 723 . 30 19 . 70 7 . 31E - 02 2 . 12E- 01 873 . 20 11. 50 7 . 64E - 02 3 . 88E-01 1004 . 76 17 . 90 - 2 . llE - 02 2 . 60E-01 1274 . 51 35 . 50 - 5 . 42E - 02 l . 72E-01 EU - 155 86 . 54 32 . 80 - 8 . 65E- 02 l . 16E- 01 l . 16E-01 105 . 31 21.80 - 2 . 90E- 02 1. 42E-01
+ BI-214 609 . 31
- 4 6 . 30 1. 39E- 01 8 . 48E-02 8 . 48E - 02 1120 . 29
- 15 . 10 2 . 07E - 01 2 . 04E - 01 1238 . 11 5 . 94 2 . SOE-01 l.12E+OO 1377 . 67 4 . 11 8 . 23E - 01 l . 03E+OO 1407 . 98 2 . 48 3 . 64E - 01 l . 68E+OO 1509 . 19 2 . 19 4 . 90E-01 l . 78E+OO 1764 . 49 15 . 80 3 . 69E-01 3 . 35E-01
+ PB - 214 77 . 11 10 . 70 8 . 13E- 01 9 . 72E-02 4 . 68E-01 295 . 21
- 19 . 20 1. 20E - 01 l . 56E - 01 351 . 92
- 37 . 20 7 . 18E- 02 9 . 72E - 02
+ PA- 228 89 . 95 22 . 00 2 . 67E+OO 1 . 92E+OO 3 . 23E+00 93 . 35 35 . 00 -l . 09E-01 1 . 92E+OO 105 . 00 16 . 30 - 2 . 19E+OO 3 . 65E +OO 129 . 22 2 . 97 8 . 37E+00 l . 95E+Ol 338 . 32 5 . 30 5 . 81E+OO l . 23E+Ol 463 . 00 13 . 80 4 . 09E+OO 5 . 06E+OO 911 . 23 16 . 70 8 . 87E+OO 6 . 95E 00
+ AM- 241 59 . 54 36 . 30 8 . 41E-02 2.19E-01 2 . 19E-01
+ CM- 243 103 . 76 23 . 00 - 7 . 09E - 02 1 . 35E - Ol 1. 35E - 01 228 . 18 10 . 60 2 . 13E-02 2 . 78E - 01 277 . 60 14 . 00 1 . 12E- 01 2 . 30E - 01
+ := Nuclide Identified during the nuclide identification
= Energy line found in the spectrum
> :::: MDA value not calculated
@ :::: Half-life too short to be able to perform the decay correction 7 = CAUTION: MDA value Is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 84
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 12:17:31PM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-020-SB 04/05/18 - 1351 10/7/2020 Page 85
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 1:19:47PM Page I of7 pex-Gamma Analysis Report for L2-SUB-102-AJGS-021-SB 04/05/18 - 1357 L 7- - ~\l - l<YL te.A (_v..J {) ~o;/ GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-021-SB / Sample Description : 04/05/18 - 1357 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 8.526E+02 grams Facility : Dairyland_NPP Sample Taken On : 415/2018 1:57:00PM ACQuisllion Started : 4/9/2018 12:1 9:25PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3611.0 seconds Dead Time : 0.30 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4241 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/912018 1:19:38PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 86
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/20 18 1:19:47PM Page 2 of7 Analysis Report for L2-SUB-102-AJGS-021-SB 04/05/18 - 1357 Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) M 1 74 . 51 144 - 160 149 . 57 1 . 21E+02 40 . 50 9 . 59E+02 1. 44 m 2 76 . 88 144 - 160 154 . 30 2 . 02E+02 47 . 53 l . 09E+03 1. 44 F 3 92 . 96 183 - 190 186 . 45 7 . 64E+0l 40 . 38 8 . 14E+02 1.25 F 4 209 . 34 416 - 423 4 19 . 17 5 . 76E+0l 32 . 03 4. 34E+02 1. 48 M 5 238 . 52 469 - 490 477 . 52 4 . 25E+02 50 . 46 5 . 14E+02 1. 62 m 6 241 . 52 469 - 490 483 . 52 l . 42E+02 34 . 21 5 . 26E+02 1. 62 F 7 295 . 14 585 - 604 590 . 73 2 . 23E+02 38 . 19 5 . 90E+02 1. 73 F 8 338 . 35 671 - 685 677 . 1 4 9 . 36E+0l 28 . 46 3 . 20E+02 1. 87 F 9 351 . 78 700 - 709 703 . 98 3 . 46E+02 42 . 35 2 . 21E+02 1. 57 F 10 582 . 84 1156 - 1172 1166 . 03 l . 49E+02 29 . 06 2 . 03E+02 1. 75 F 11 609 . 09 1211 - 1224 1218 . 52 2 . 57E+02 34 . 95 1 . 30E+02 1. 79 F 12 767 . 76 1531 - 1541 1535 . 80 2 . 78E+0l 13 . 60 8 . 13E+0l 0 . 93 F 13 911 . 13 1817 - 1830 1822 . 50 9 . 28E+0l 23 . 14 9 . 15E+0l 2 . 14 F 14 968 . 66 1933 - 1944 1937 . 55 4 . 80E+0l 18 . 61 8 . 71E+0l 1. 89 F 15 1120 . 00 2236 - 2248 2240 . 19 5 . 05E+0l 18 . 24 8 . 43E+0l 1. 78 F 16 1332 . 11 2659 - 2669 2664 . 36 l . 80E+0l 11.07 3 . 02E+0l 1. 61 F 17 1460 . 38 2912 - 2929 2920 . 87 5 . 18E+02 46 . 55 2 . 71E+0l 2 . 40 F 18 1763 . 78 3521 - 3534 3527 . 63 4 . 60E+0l 14 . 84 1. 43E 01 2 . 84 M : First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/9/2018 1:19:38PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364 .CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. M 1 74 . 51 1 . 21E+02 40 . 50 l . 21E+02 4 . 05E+0l m 2 76 . 88 2 . 02£+02 47 . 53 2 . 02E+02 4 . 75E+0l F 3 92 . 96 7 . 64E+0l 40 . 38 7 . 64E+0l 4 . 04E+0l F 4 209 . 34 5 . 76E+0l 32 . 03 5 . 76E+0l 3 . 20E+0l M 5 238 . 52 4 . 25£+02 50 . 46 4 . 25E+02 5 . 05E+0l m 6 241. 52 l . 42E+02 34 . 21 l . 42E+02 3 . 42E+0l F 7 295 . 14 2 . 23E+02 38 . 19 2 . 23E+02 3 . 82E+0l F 8 338 . 35 9.36E+0l 28 . 46 9 . 36E+0l 2 . 85E+0l F 9 351 . 78 3 . 46£+02 42 . 35 8 . 36E+0l 3 . 72E+0l 2 . 63E+02 5 . 64E+0l F 10 582 . 84 1 . 49E+02 29 . 06 1 . 49E+02 2 . 91E+0l F 11 609 . 09 2 . 57E+02 34 . 95 4. 12E+0l 2 . 42E+0l 2 . 16E+02 4 . 25E+01 10/7/2020 Page 87
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 1:19:47PM Page 3 of7 Analysis Report for L2-SUB-102-AJGS-021 -SB 04/05/18 - 1357 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. {keV) Area Uncertainty Background Uncert. Area Uncert. F 12 767 . 76 2 . 78E+Ol 13 . 60 2 . 78E+Ol 1. 36E+Ol F 13 911 . 13 9 . 28E+Ol 23 . 14 9 . 28E 01 2 . 31E+Ol F 14 968 . 66 4 . 80E+Ol 18 . 61 4 . 80E+Ol 1 . 86E+Ol F 15 1120 . 00 5 . 05E+Ol 18 . 24 5 . 0SE+Ol l . 82E+Ol F 16 1332 . 11 l . 80E+Ol 11. 07 1 . 80E+Ol l . llE+Ol F 17 1460 . 38 5 . 18E+02 46 . 55 5 . 63E+01 1 . 71E+Ol 4 . 62E+02 4 . 96E+Ol F 18 1763 . 78 4 . 60E+Ol 14 . 8 4 l . 52E+Ol 9 . 80E+OO 3 . 08E+01 l . 78E+Ol M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(3/4) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0 . 97 1460 . 75
- 10 . 67 5 . 90E+OO 7 . 13E- 01 PB-212 0 . 99 77 . 11
- 17 . 50 3 . 35E-01 8 . 18E-02 238 . 63
- 44 . 60 2 . 57E-01 3 . 33E-02 BI - 214 0 . 76 609 . 31
- 46 . 30 2 . 91E - 01 5 . 97E- 02 1120 . 29
- 15 . 10 3 . 62E-01 1. 32E-01 1238 .11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49
- 15 . 80 3 . llE-01 l . 81E-01 PB - 214 0 . 99 77 . 11
- 10 . 70 5 . 47E-01 1. 34E - 01 295 . 21
- 19 . 20 3 . 73E-01 6 . 66E- 02 351 . 92
- 37 . 20 2 . 66E-01 5 . 86E - 02 AC-228 0 . 78 209 . 28
- 4 . 40 3.20E-01 1 . 79E- 01 338 . 32
- 11. 40 2 . 99E-01 9 . 20E - 02 794 . 70 4 . 60 911 . 60
- 27 . 70 3 . 02E - 01 7 . 64E - 02 964 . 60 5 . 20 969 . 11
- 16 . 60 2 . 75E- 01 l . 07E- 01 10/7/2020 Page 88
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 1:19:47PM Page4 of7 Analysis Report for L2-SUB-102-AJGS-021-SB 04/05/18 - 1357
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
K- 40 0 . 978 5 . 90E+OO 7 . 13E-Ol PB- 212 0 . 996 2 . 42E-01 3 . lOE-02 BI-214 0.768 3 . 04E - 01 5 . 21E-02 PB-214 0 . 997 2 . 97E-0 1 4 . 21£-02 AC - 228 0 . 780 2.97E-01 4.95E-02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 89
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 1:19:47PM Page 5 of 7 Analysis Report for L2-SUB-102-AJGS-021-SB 04/05/18 - 1357 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/9/2018 1:19:38PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 1 74 . 51 3 . 35439E - 02 16 . 77 (b ,~,.,,fa,11/-- KOf~ F 3 92 . 96 2 . 12208E-02 26 . 43 Tol. PA-228 m 6 241. 52 3.93232E- 02 12 . 08 7b ,z,,tJ F 10 582 . 84 4.14703E-02 9 . 73 -,? ., t,c,f; F 12 767 . 76 7 . 73564E- 03 24 . 43 p, - Z.,J" F 16 1332 . 11 5 . 00691E-03 30 . 70 eo-Jo M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigrna NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield{3/4) Activity NuclideMDA UneMDA Name {keV) (pCilgrams) (pCilgrams) (pCilgrams)
+ K- 40 1460 . 75
- 10 . 67 5 . 90E+00 5 . 89£-01 5 . 89£-01
+ AR - 41 1293 . 64 99 . 16 -2 . 61E+13 2 . 27E+14 2 . 27E+14
+ CO-60 1173 . 22 100 . 00 6 . 31E-02 5 . 66E - 02 6 . 82E- 02 1332 . 49 100 . 00 4 . 13£- 02 5 . 66E- 02
+ KR-85 513 . 99 0 . 43 l.43E+0l l . 02E+0l 1. 02E+0l
+ Y- 88 898 . 04 93 . 70 -8 . 47E-03 3 .4 3E-02 5 . 18E-02 1836 . 06 99 . 20 -1. 52E- 03 3 . 43E - 02
+ NB - 94 702 . 63 1 00 . 00 -8.69E- 03 4 . 17E- 02 4 . 17E-02 871.10 100 . 00 -4 . 48E-03 4.40E-02 10/7/2020 Page 90
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 1:19:47PM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-021-SB 04/05/1 8 - 1357 Nuclide Energy Yield{%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCi/grams) (pCilgrams) (keV)
+ I-131 284 . 30 6 . 06 l . 18E-01 6 . 0lE-02 7 . 67E-Ol 364 . 48 81. 20 4 . 68E-02 6 . 0lE - 02 636 . 97 7 . 27 -8 . SlE- 02 7 . 62E-01
+ CS - 134 604 . 70 97 . 60 - 5 . 53E - 03 5 . 0lE- 02 6 . 12E-02 795 . 84 85 . 40 - 3 . 98£ - 02 5 . 0lE-02
+ CS-137 661. 65 85 . 12 9 . 46E - 03 5 . 56E-02 ii 5 . 56E - 02
+ CE- 144 80 . 12 1. 36 - l . 33E+OO 2 . 91E- 01 3 . 71E+OO 133 . 51 11.09 -6 . 72E - 03 2 . 918-01
+ 8U- 152 121 . 78 28 . 40 -7 . 35E - 02 l . 13E - 01 l . 13E - 01 244 . 69 7 . 49 4 . 84E - 02 5 . 598 - 01 964 . 00 14 . 44 6 . 02E - 01 4 . 158-01 1408 . 00 20 . 74 - 3 . 22E-02 / 1 . 888 - 01
+ EU - 154 123 . 07 40 . 40 -2 . 24E - 02 7 . 948 - 02 7 . 94E - 02 247 . 94 6 . 60 7 . 52E- 02 5 . 558 - 01 723 . 30 19 . 70 2 . 24£-01 2 . 338 - 01 873 . 20 11 . 50 -1. 43E - 01 3 . 808- 01 1004 . 76 17 . 90 1. 85E - 01 2 . 81E - 01 1274 . 51 35 . 50 - 1 . 03E-01 1 . 578-01
+ EU-155 86 . 54 32 . 80 -6 . 09E - 02 l . 27E - 01 l . 27E-01 105 . 31 21 . 80 -l . 31E-Ol 1. 52E - 01
+ BI-214 609 . 31
- 46 . 30 2 . 91E-01 8 . 87£ - 02 8 . 87E-02 1120 . 29
- 15 . 10 3 . 62£-01 2 . 70E - Ol 1238 . 11 5 . 94 8 . 69£ - 01 1 . 17E 00 1377 . 67 4 . 11 2 . 29E-01 1 . 03E+00 1407 . 98 2 . 48 - 2 . 69E-01 l . 57E+OO 1509 . 19 2 . 19 8 . 70£-02 l . 86E+OO 1764 . 49
- 15 . 80 3 . llE - 01 2 . 84E- 01
+ PB- 214 77 . 11
- 10 . 70 5 . 47E - 01 8 . 97E- 02 3 . 02E - 01 295 . 21
- 19 . 20 3 . 73E - 01 1 . 84E-01 351 . 92
- 37 . 20 2 . 66£-01 8 . 97E-02
+ PA-228 89 . 95 22.00 4 . 79£+00 2 . 19E+OO 3 . 688+00 93 . 35 35 . 00 8 . 60£-01 2 . 19E+OO 105 . 00 16 . 30 - l . 94E+00 4 . 0SE+OO 129 . 22 2 . 97 l . 12E+Ol 2 . 14E+Ol 338 . 32 5 . 30 5 . 0lE+OO l . 34E+Ol 463 . 00 13 . 80 1. 24E+OO 5 . 59E+OO 911 . 23 16 . 70 1 . 19E+Ol 7 . 48E+OO
+ AM-241 59 . 54 36 . 30 1. 83£-01 2 . 32£-01 2 . 32E-01
+ CM - 243 103 . 76 23 . 00 - 1 . 78£- 02 1 . 46E - 01 l . 46E - 01 228 . 18 10 . 60 - 6 . 16£- 02 2 . 99E-01 277 . 60 14 . 00 1 . 89£-01 2 . 48£ - 01
+ = Nuclide identified during the nuclide identification
= Energy line round in the spectrum
;,, = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 91
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 1:19:47PM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-021-SB 04/05/18 - 1357 10/7/2020 Page 92
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 2:22:30PM Page I of7 pex-Gamma Analysis Report for L2-SUB-102-AJGS-022-SB 04/05/18 - 1428 0( { l--Z,,,-~-/D2- R_{J,_
~ c_....;O -S.o;- (
GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-022-SB / Sample Description : 04/05/18 - 1428 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 9.146E+02 grams Facility : Dairyland_NPP Sample Taken On : 4/5/2018 2:28:00PM Acquisition Started : 4/9/2018 1:22:08PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live Time : 3600.0 seconds Real Time : 3610.7 seconds Dead Time : 0.30 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4242 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/9/2018 2:22:21 PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 93
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 2:22:30PM Page 2 of7 Analysis Report for L2-SUB-102-AJGS-022-SB 04/05/1 8 - 1428 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 76 . 09 147 - 161 152 . 72 3 . 02E+02 61 . 98 1. 34E+03 3 . 22 F 2 238 . 54 469 - 485 477 . 55 3 . 73E+02 48 . 38 8 . l0E 02 1. 44 M 3 295 . 26 586 - 603 590 . 97 1 . 03E+02 28 . 06 2 . 56E 02 1. 33 m 4 299 . 87 586 - 603 600 . 18 4 . 20E+0l 20 . 98 2 . 07E+02 1.33 F 5 338 . 08 672 - 683 676 . 60 5 . 33E+0l 24 . 27 3 . 01E+02 1.45 F 6 351.86 700 - 711 704 . 14 1 . 80E+02 33 . 18 2 . 45E+02 1. 69 F 7 582 . 94 1161 - 1172 1166 . 21 1 . 09E+02 24 . 27 l.03E+02 1. 52 F 8 609 . 00 1211 - 1226 1218 . 33 l . 17E+02 26 . 48 2 . 04E+02 1. 64 F 9 911 . 25 1818 - 1829 1822 . 73 6 . 14E+0l 19 . 48 7 . 13E+0l 1. 99 F 10 1460 . 38 2911- 2928 2920 . 87 4 . 95E+02 45 . 55 3 . 03E+0l 2 . 39 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/9/2018 2:22:21 PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76 . 09 3 . 02E+02 61. 98 3 . 02E+02 6 . 20E+0l F 2 238 . 54 3 . 73E+02 48 . 38 3 . 73E+02 4 . 84E+0l M 3 295 . 26 1 . 03E+02 28 . 06 l . 03E+02 2 . 81E+0l m 4 299 . 87 4 . 20E+0l 20 . 98 4 . 20E+0l 2 . l0E+0l F 5 338 . 08 5 . 33E+0l 24 . 27 5 . 33£+01 2 . 43E+0l F 6 351 . 86 1 . 80E+02 33 . 18 8 . 36E+0l 3 . 72E+0l 9 . 61E+0l 4 . 99E+0l F 7 582 . 94 1 . 09E+02 24 . 27 1 . 09E+02 2 . 43E+0l F 8 609 . 00 1 . 17E+02 26 . 48 4 . 12E+0l 2 .4 2E+0l 7 . 59E+0l 3 . 59E+0l F 9 911 . 25 6 . 14E+0l 19 . 48 6 . 14E+0l l . 95E+0l F 10 1 4 60 . 38 4 . 95E+02 45 . 55 5 . 63E+0l 1 . 71E+0l 4 . 39E+02 4 . 87E+0l M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma 10/7/2020 Page 94
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/201 ts 2:22:30PM Page 3 of7 Analysis Report for L2-SUB-102-AJGS-022-SB 04/05/18 - 1428 NUCLIDE IDENTIFICATION REPORT Nuclide Ubrary Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0 . 97 1460 . 75
- 10 . 67 5 . 23E+OO 6 . 48E-01 PB-212 0 . 55 77 . 11 17 . 50 238 . 63
- 44 . 60 2 . llE-01 2 . 94E-02 BI-214 0 . 34 609 . 31
- 4 6 . 30 9 . 56E-02 4 . SSE-02 1120 . 29 15 . 10 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49 15 . 80 PB- 21 4 0 . 72 77 . 11 10 . 70 295 . 21
- 19 . 20 l . 62E - 01 4 . 4 6E- 02 351. 92
- 37 . 20 9 . 08E - 02 4 . 73E - 02 AC - 228 0 . 30 209 . 28 4 . 40 338 . 32
- 11. 40 1. 59E-01 7 . 26E-02 794 . 70 4 . 60 911 . 60
- 27 . 70 l.86E-Ol 5 . 96E - 02 964 . 60 5 . 20 969 . 11 16 . 60
* =Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
=
@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV
=
Nuclide confidence index threshold 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT I 10/7/2020 Page 95
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 L.l2:30PM Page 4 of 7 Analysis Report for L2-SUB-102-AJGS-022-SB 04/05/18 - 1428 Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams) K- 40 0 . 978 S . 23E+OO 6 . 48E - 01 PB - 212 0 . 559 2 . llE - 01 2 . 94E - 02 BI - 214 0 . 342 9 . 56E - 02 4 . SSE - 02 PB- 214 0 . 721 l . 28E - 01 3 . 24E - 02 AC - 228 0 . 301 l . 75E- 01 4 . 61E - 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 96
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 2:22 :30PM Page 5 of? Analysis Report for L2-SUB-102-AJGS-022-SB 04/05/18 - 1428 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/9/2018 2:22:21 PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 1 76 . 09 8. 37514E- 02 10.28 ~--u,~ m 4 299 . 87 l . 16796E-02 24 . 95 71--v-v F 7 582 . 94 3 . 04022E-02 11.09 '7(,, ~t:J M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(3/4) Activity NuclideMDA LlneMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV)
+ K-40 1460 . 75
- 10 . 67 5 . 23E+00 5 . SSE - 01 5 . SSE-01
+ AR-41 1293 . 64 99 . 16 -4 . 85E+l3 2 . 59E+l4 / 2 . 59E+14
+ CO- 60 1173 . 22 100 . 00 3 . 42E-02 S . 12E-02 6 . 12E- 02 1332 . 49 100 . 00 2 . 89E - 02 5 . 12E- 02
+ KR-85 513.99 0 . 43 3 . 89E+00 8 . 59E+00 8.59E+00
+ Y-88 898 . 04 93 . 70 -1 . 14E- 02 3 . 82E - 02 4 . 68E-02 1836 . 06 99 . 20 -9 . llE-03 3 . 82E - 02
+ NB-94 702 . 63 100 . 00 l . 89E-02 3 . 68E-02 3 . 68E-02 871 . 10 100 . 00 -5.12E-02 3 . 86E- 02
+ I-131 284 . 30 6.06 5 . 60E-02 5 . 24E-02 6 . 72E-01 364 . 48 81. 20 2 . 37E - 02 5 . 24E-02 636 . 97 7 . 27 3 . 40E-01 6 . 93E - 01
+ CS - 134 604 . 70 97 . 60 l . 03E-02 4 . 95E-02 4 . 95E - 02 10/7/2020 Page 97
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 2:22:30PM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-022-SB 04/05/1 8 - 1428 Nuclide Energy Yield(3/4) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCilgrams) (pCilgrams) (keV) CS - 134 795.84 85 . 40 2 . 21E-02 4 . 95E-02 5 . 03E- 02
+ CS - 137 661. 65 85 . 12 7 . 13E- 02 5 . 02E - 02 5 . 02E- 02
+ CE - 144 80 . 12 1. 36 -5 . 71E-01 2 . 58E-01 3 . 27E+OO 133 . 51 11.09 -l . 53E-01 2 . 58E-01
+ EU - 152 121 . 78 28 . 40 - 2 . 78E -02 9 . 89E-02 ./ 9 . 89E-02 244 . 69 7 . 49 - 3 . 68E - 01 4 . 85E-Ol 964 . 00 14 . 44 3 . 27E-02 3 . 50E - 01 1408 . 00 20 . 74 1 . 70E-Ol 2 . 02E - 01
+ EU -154 123 . 07 40 . 40 - 2 . 46E- 02 6 . 96E - 02 I 6 . 96E- 02 247 . 94 6 . 60 -1 . 0JE+OO 4 . 71E - 01 723 . 30 19 . 70 9 . 40E - 02 2 . 0lE - 01 873 . 20 11. 50 2 . 26E - 01 3 . 58E-01 1004 . 76 17 . 90 9 . 85E - 04 2 . 41E-01 1274 . 51 35 . 50 -3 . 97E-02 l.48E-01
+ E0 - 155 86 . 54 32 . 80 -6 . 96E-02 l . llE-0 1 1 . llE-01 105 . 31 21. 80 4 . 79E-02 l . 35E-01
+ BI-214 609 . 31
- 4 6 . 30 9 . 56E-02 9 . 54E-02 9 . 54E-02 1120 . 29 15 . 10 5 . 12E- Ol 4 . 06E-01 1238 . 11 5 . 94 -3 . 38E-01 l . 02E+OO 1377 . 67 4 . 11 -8 . 69E-01 l. llE+OO 1407 . 98 2 . 48 1 . 42E+OO l . 68E+OO 1509 . 19 2 . 19 8 . 65E - 01 1. 80E+OO 1764 . 49 15 . 80 2 . 52E- 01 2.92E - 01
+ PB-214 77 . 11 10 . 70 5 . llE- 01 8 . 66E - 02 4 . 32E-01 295 . 21
- 19 . 20 1 . 62E-Ol 8 . 66E-02 351 . 92
- 37 . 20 9 . 08E-0 2 8 . 73E - 02
+ PA-228 89 . 95 22 . 00 6 . 77E- 01 1 . 91E+OO 3 . 24E+OO 93 . 35 35 . 00 - 8 . 32E - 01 1 . 91E+OO 105 . 00 16 . 30 - 4 . 14E- 01 3 . 64E+OO 129 . 22 2 . 97 1. 51E+Ol 1. 97E+Ol 338 . 32 5 . 30 1 . 42E+Ol 1. 23E+Ol 463 . 00 13 . 80 6 . 91E-01 4 . 94E+OO 911 . 23 16 . 70 9 . 92E+OO 6 . 46E+OO
+ AM-241 59 . 54 36 . 30 -9 . 03E- 02 2.0lE - 01 2 . 0lE- 01
+ CM-243 10 3 . 76 23 . 00 -8 . 63E - 02 1 .28E- 01 l . 28E- Ol 228 . 18 10 . 60 6 . ll E-02 2 . 63E-Ol 277 . 60 14 . 00 -l . 45E-Ol 2 . 04E-Ol
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able lo perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 98
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 2:22:30PM Page 7 of 7 Analysis Report for L2-SUB-102-AJGS-022-SB 04/05/18 - 1428 10/7/2020 Page 99
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 4:40:38PM Page I of6 pex-Gamma Analysis Report for L2-SUB-102-AJGS-023-SB 04/05/18 - 1453 L-Z.-ot( ..... ) o-Z... 62,_~ C..v C> ~o; ( GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-023-SB / Sample Description : 04/05/18 - 1453 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 8.413E+02 grams Facility : Dairyland_NPP Sample Taken On : 4/5/2018 2:53:00PM Acquisition Started : 4/9/2018 3:40:16PM Procedure : 500ml Marinelli Operator : Administrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live lime : 3600.0 seconds Real Time : 3611.0 seconds Dead Time : 0.30 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 7/8/2014 Efficiency Calibration Description Sample Number : 4244 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/9/2018 4:40:29PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 100
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 4:40:38PM Page 2 of6 Analysis Report for L2-SUB-102-AJGS-023-SB 04/05/1 8 - 1453 Peak Energy ROI ROI Peak NetPeak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) F 1 76 . 28 148 - 160 153 . 10 2 . 81E+02 62 . 42 l . 18E+03 4 . 40 F 2 238 . 42 469 - 481 477 . 32 2 . 80E+02 4 6 . 27 7 . 34E+02 1. 40 M 3 288 . 58 574 - 595 577 . 61 2 . 75E+Ol 18 . 47 2.03E+02 1. 21 m 4 295 . 14 574 - 595 590 . 73 9 . 81E+Ol 28 . 15 2 . 45E+02 1. 22 F 5 337 . 99 668 - 683 676 . 40 5 . 09E+Ol 21. 89 3 . 51E+02 1.15 F 6 351 . 73 697 - 712 703 . 88 2 . 16E+02 35 . 30 3 . 37E+02 l. 60 F 7 582 . 95 1161 - 1174 1166 . 24 7 . 62E+Ol 20 . 37 l . 57E+02 0 . 87 F 8 608 . 98 1211- 1223 1218 . 29 1 . 58E+02 29 . 23 l. 39E+02 1. 78 F 9 910 . 92 1816 - 1828 1822 . 08 9 . SSE+Ol 22 . 75 6 . 19E+Ol 2 . 28 F 10 968 . 72 1931 - 1942 1937 . 66 4 . 08E+Ol 17 . 15 7 . 23E+Ol 1. 99 F 11 1120 . 34 2236 - 2247 2240 . 86 4 . 75E+Ol 17 . 78 7 . 14E 01 1. 83 F 12 1460.36 2913 - 2929 2920 . 82 5 . 01E+02 45 . 35 2 . 48E+Ol 2 . 50 F 13 1764 . 53 3524 - 3535 3529 . 12 3 . 20E+Ol 12 . 32 8 . 65E+OO 2 . 99 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/9/2018 4:40:29PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 1 76 . 28 2 . 81E+02 62 . 42 2 . 81E+02 6 . 24E+Ol F 2 238 . 42 2 . 80E+02 46 . 27 2 . 80E+02 4 . 63E+Ol M 3 288 . 58 2 . 75£+01 18 . 47 2 . 75£+01 l . 85E+Ol m 4 295 . 14 9 . 81£+01 28 . 15 9 . 81E+Ol 2 . 82E+Ol F 5 337 . 99 5 . 09E+Ol 21. 89 5 . 09E+Ol 2 . 19E 01 F 6 351 . 73 2 . 16E+02 35 . 30 8 . 36E+Ol 3 . 72E+Ol 1 . 32E+02 5 . 13E+Ol F 7 582 . 95 7 . 62E+Ol 20 . 37 7 . 62E+Ol 2 . 04E+Ol F 8 608 . 98 l . 58E+02 29 . 23 4. 12E+Ol 2 . 42E+Ol l . 17E+02 3 . BOE+Ol F 9 910 . 92 9 . 55E+Ol 22 . 75 9 . 55E+Ol 2 . 28E+Ol F 10 968 . 72 4 . 08E+Ol 1 7 . 15 4 . 08E+Ol 1 . 72E +Ol F 11 1120 . 34 4 . 75E+Ol 17 . 78 4 . 75E+Ol 1 . 78E +Ol F 12 1460 . 36 5 . 01E+02 45 . 35 5 . 63E+Ol l . 71E+Ol 4 . 45E+02 4 . 85E+Ol F 13 1764 . 53 3 . 20£+01 12 . 32 l . 52E+Ol 9 . 80E+OO l . 6 9E+Ol 1 . 57E+Ol 10/7/2020 Page 1
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 4:40:38PM Page 3 of 6 Analysis Report for l2-SUB-102-AJGS-023-SB 04/05/18 - 1453 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairytand_NPP\Library\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K- 40 0 . 97 1460 . 75
- 10 . 67 5 . 76E+OO 7 . 04E - Ol PB - 212 0 . 96 77 . 11
- 17 . 50 4 . 78E - Ol 1 . llE - 01 238 . 63
- 44 . 60 1 . 71E - 01 2 . 97E - 02 BI - 214 0 . 77 609 . 31
- 46 . 30 l . 60E - 01 5 . 27E- 02 1120 . 29
- 15 . 10 3 . 45£ - 01 l . 30E- 01 1238 . 11 5 . 94 1377 . 67 4 . 11 1407 . 98 2 . 48 1509 . 19 2 . 19 1764 . 49
- 15 . 80 l . 73E- Ol 1 . 62E - 01 PB - 214 0 . 97 77 . 11
- 10 . 70 7 . 82E- 01 l . BlE-01 295 . 21
- 19 . 20 1 . 67£- 01 4 . 86E - 02 351. 92
- 37 . 20 1. 36E - 01 5 . 31E- 02 AC - 228 0 . 59 209 . 28 4 . 40 338 . 32
- 11. 40 l . 64E - 01 7 . 12E- 02 794 . 70 4 . 60 911 . 60
- 27 . 70 3 . 15E- 01 7 . 62E- 02 964 . 60 5 . 20 969 . 11
- 16 . 60 2 . 37E - 01 l . OOE- 01
* = Energy line fou nd in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma 10/7/2020 Page 2
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/20 18 4:40:38PM Page 4 of6 Analysis Report for L2-SUB-102-AJGS-023-SB 04/05/ 18 -- 1453 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams) K-40 0 . 975 5 . 76E+OO 7 . 04E - 01 PB- 212 0 . 965 l . 85E - 01 2 . 87 E- 02 BI - 214 0 . 779 l . 85E - 01 4 . 68 E-02 PB- 214 0 . 979 1 . 65E - 01 3 . 52E - 02 AC - 228 0 . 596 2 . 35E - 01 4 . 62 E- 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 3
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 4:40:38PM Page 5 of6 Analysis Report for L2-SUB-102-AJGS-023-SB 04/05118 - 1453 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/9/2018 4:40:29PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide M 3 288 . 58 7 . 63489E - 03 33.60 ?o,~ ---ii,,. Z,-Z,-, F 7 582 . 95 2 . 11646E-02 13 . 37 -rJ..-u;I!, M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Llbrary\HOTLAB.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCl/grams) {pCilgrams) (keV)
+ K-40 1460 . 75 10 . 67 5 . 76E+00 5 . 87E-01 5 . 87E-01
+ AR-41 1293 . 64 99 . 16 -l . 05E+l3 5 . 64E+l4 5 . 64E+l4
+ CO- 60 1173 . 22 100 . 00 2 . 93E-02 5 . 73E-02 6 . 12E-02 1332 . 49 100 . 00 l.76E-02 5 . 73E-02
+ KR-85 513 . 99 0 . 43 l . 14E+0l 9 . 32£+00 9 . 32E+00
+ Y-88 898 . 04 93 . 70 5 . 21E- 02 3 . 79E - 02 5 . 06E- 02 1836 . 06 99 . 20 -1. 39E-02 3 . 79£-02
+ NB - 94 702 . 63 10 0 . 00 l . 47E-02 4.08£-02 4.08£-02 871 . 10 100 . 00 2 . 02E - 02 4 . 30E-02
+ I-131 284.30 6.06 -4.90E-02 5 . 68£-02 7.13£-01 364 . 48 81 . 20 5 . 52E-03 5 . 68£ - 02 636 . 97 7 . 27 1. 58£-01 7 . 34£-01
+ CS-134 604 . 70 97 . 60 8 . 59E - 02 5.06£ - 02 5 . 44E-02 795 . 84 85 . 40 - 3 . 03E - 02 / 5 . 06E-02
+ CS-137 661. 65 85 . 12 4 . 82E-02 S . 23E-02 S . 23E-02
+ CE-144 80 . 12 1.36 -2 . lBE+00 2 . 81£-01 3 . 47E+00 10/7/2020 Page 4
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 4:40:38PM Page 6 of6 Analysis Report for L2-SUB-102-AJGS-023-SB 04/05/ 18 - 1453 Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCl/grams) (pCilgrams) (keV) CE - 144 133 . 51 ll . 09 3 . 96E - 01 2 . 81E - 01 ,/ 2 . 81E - 01
+ EU - 152 121. 7 8 28 . 40 - 9 . 0JE - 02 l . 03E - 01 1 . 03E - 01 244 . 69 7 . 49 - 8 . 33E - 01 5 . 04E - 01 964 . 00 14 . 44 l . 24E - 01 3 . 75E- 01 1408 . 00 20 . 74 8 . 63 E- 02 2 . 26£ - 01
+ EU - 154 123 . 07 40 . 40 - 5 . 14£- 02 7 . 22E - 02 .,/ 7 . 22E - 02 247 . 94 6 . 60 - 2 . 14E+OO 4 . 98E- 01 723.30 19 . 70 1 . 73£ - 01 2 . 39E-01 873 . 20 11 . 50 - 2 . 49E - 01 3 . 58£ - 01 1004 . 76 17 . 90 6 . 68£ - 02 2 . 79E - 01 1274 . 51 35 . 50 - 1 . 49E - 02 1 . 56E - 01
+ EU- 155 86 . 54 32 . 80 - 8 . 99E - 02 1 . 16E - 01 l . 16E- 01 105 . 31 21. 80 - 4 . llE-02 l.43E - 01
+ BI - 214 609 . 31
- 46 . 30 1 . 60£ - 01 9 . 03E - 02 9 . 03£-02 1120 . 29 15 . 10 3 . 45E - 01 2 . 49E - 01 1238 . 11 5 . 94 - 2 . 77E - 01 l.05E 00 1377 . 67 4 . 11 8 . 06E - 01 l . 17E+OO 1407 . 98 2 . 48 7 . 21E - 01 l.89E+OO 1509 . 19 2 . 19 1. 30E+OO 1. 83E+OO 1764 . 49
- 15 . 80 1 . 73£ - 01 2 . 66£ - 01
+ PB-214 77 . 11
- 10 . 70 7 . 82£ - 01 9 . 22£ - 02 3 . 69E - 01 295 . 21
- 19 . 20 l . 67E - 01 9 . 22E - 02 351. 92
- 37 . 20 1 . 36E - 01 1 . 06E- 01
+ PA- 228 89 . 95 22 . 00 2 . 90E+OO 2 . llE+OO 3 . 60E+OO 93 . 35 35 . 00 2 . 42E - Ol 2 . llE+OO 105 . 00 16 . 30 8 . 25E - 01 4 . 13E+OO 129 . 22 2 . 97 l . 21E+Ol 2 . 18E+Ol 338 . 32 5 . 30 8 . 78E+OO l . 38E+Ol 463 . 00 13 . 80 3 . 3 4 E+OO 5 . 55E+OO 911 . 23 16 . 70 9 . 0lE + OO 7 . 498+00
+ AM- 241 59 . 54 36 . 30 9 . 0lE - 02 2 . 19£- 0 1 2 . 19E- 0 1
+ CM- 243 103 . 76 23 . 00 - l.13E - 02 l . 36E- 01 l . 36E - 01 228 . 18 10 . 60 6 . 79 E- 02 2 . 89 E- 01 277 . 60 14 . 00 - 3 . 04£ - 02 2 . 22£ - 01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short lo be able to perform the decay correction
? = CAUTION: MDA value is Inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 5
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 6:07:29PM Page I of7
~~~pex-Gam ma Analysis Report for L2-SUB-102-AJGS-024-SB 04/05118 -1458 1-..2 - 01(-lt)l/ f2_A C.J-~ D ~o; (
GAMMA SPECTRUM ANALYSIS Sample Identification : L2-SUB-102-AJGS-024-SB / Sample Description : 04/05/18 - 1458 Sample Type : 500 ml Marinelli Unit Sample Point Sample Size 8.383E+02 grams Facility : Dairyland_NPP Sample Taken On : 4/512018 2:58:00PM Acquisition Started : 4/912018 5:07:0?PM Procedure : 500ml Marinelli Operator : Admin istrator Detector Name : HOTLAB Geometry : 500ml Marinelli Live lime : 3600.0 seconds Real Time : 3611 .1 seconds Dead Time : 0.31 % Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 7/8/2014 Efficiency Calibration Used Done On : 718/2014 Efficiency Calibration Description Sample Number : 4245 PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/912018 6:07:20PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 10/7/2020 Page 6
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 6:07:29PM Page 2 of7 Analysis Report for L2-SUB-102-AJGS-024-SB 04/05/18 - 1458 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) M 1 74 . 72 146 - 159 149 . 98 1 . 37E+02 42.12 9 . 48E+02 1. 28 m 2 77 . 01 146 - 159 154 . 57 2 . 08E+02 47 . 28 1. 04E+03 1. 28 F 3 129 . 14 255 - 262 258 . 80 6 . 24E+Ol 33 . 06 7.20E+02 0 . 93 F 4 185.85 369 - 379 372 .19 1. 31E+02 37 . 72 7.54E+02 1. 34 M 5 238 . 60 472 - 492 477 . 68 4 . 51E+02 52 . 91 5.92E 02 1. 66 m 6 241.87 472 - 4 92 484 . 22 l.45E+02 34 . 92 5 . 54E+02 1. 67 M 7 295 . 15 584 - 606 590 . 75 2 . 47E+02 38 . 64 3 . 07E+02 1. 56 m 8 299.94 584 - 606 600 . 32 5 . 02E+Ol 22 . 94 3 . 04E+02 1. 57 F 9 338 . 32 672 - 682 677 . 06 6 . 1 6E+Ol 24 . 66 3 . 12E 02 1.21 F 10 351.79 700 - 712 704 . 00 3 . 92E+02 45 . 18 2 . 83E +02 1. 59 F 11 583 . 02 1159 - 1174 1166 . 39 1 . 46E+02 28 . 09 1 . 53E+02 1. 92 F 12 609 . 02 1211 - 1225 1218.37 3 . 11E+02 38.66 1 . 65E+ 02 1. 86 F 13 661. 39 1319 - 1331 1323.10 l.15E+02 24 . 80 9.56E+Ol 2 . 04 F 14 910.95 1815 - 1830 1822 . 14 8 . 60E+Ol 22 . 30 9 . 37E+Ol 2 . 26 F 15 968 . 68 1933 - 1943 1937 . 59 4 . 08E+Ol 17.52 8 . 93E+Ol 1. 55 F 16 1119 . 97 2236 - 2245 2240 . 13 3 . 58E+Ol 16 . 92 7 . 05E+Ol 1. 74 F 17 1237 . 91 2471 - 2481 2475 . 97 2 . 08E+Ol 12 . 33 5 . 53E+Ol 1. 2 7 F 18 1460 . 41 2913 - 2931 2920 . 93 4 . 77E+02 45 . 00 4.27E+Ol 2 . 40 F 19 1763 . 98 3521 - 3534 3528 . 03 3 . 89E+Ol 13 . 77 1. 05E+Ol 2 . 95 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma BACKGROUND SUBTRACT REPORT Peak Analysis Performed on : 4/9/2018 6:07:20PM Env. Background File : C:\Canberra\Apex\Root\Dairyland_ NPP\Data\0000001364.CNF Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. M 1 74 . 72 1. 37E+02 42 . 12 1 . 37E+02 4.21£+01 m 2 77 . 01 2 . 08E+02 47 . 28 2 . 08E+02 4 . 73E+Ol F 3 129 . 14 6 . 24E+Ol 33 . 06 6 . 24E+Ol 3 . 31E+Ol F 4 185 . 85 l . 31E+02 37 . 72 l . 31E+02 3 . 77E+Ol M 5 238 . 60 4 . 51E+02 52 . 91 4 . 51E+02 5 . 29E+Ol m 6 241.87 l . 45E+02 34 . 92 1 . 45E+02 3 . 49E+Ol M 7 295 . 15 2 . 47E+02 38 . 64 2 . 47E+02 3 . 86E+Ol m 8 299 . 94 5 . 02E+Ol 22 . 94 5 . 02E+Ol 2 . 29E+Ol F 9 338 . 32 6 . 16E+Ol 24 . 66 6 . 16E+Ol 2.47E+Ol F 10 351.79 3 . 92E+02 45.18 8 . 36E+Ol 3 . 72E+Ol 3 . 09E+02 5 . 85E+Ol 10/7/2020 Page 7
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 6:07:29PM Page 3 of7 Analysis Report for L2-SU B-102-AJGS-024-S8 04/05/18 - 1458 Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted No. (keV) Area Uncertainty Background Uncert. Area Uncert. F 11 583 . 02 1 . 46E+02 28 . 09 1 . 46E+02 2 . 81E+Ol F 12 609 . 02 3 . 11E+02 38 . 66 4.12E+Ol 2.42E 01 2 . 70E+02 4 . 56E+Ol F 13 661.39 l . 15E+02 24 . 80 6 . 61E+Ol 2 . 54E+Ol 4 . 89E+Ol 3 . 55E+Ol F 14 910 . 95 8 . 60E+Ol 22 . 30 8 . 60E+Ol 2 . 23E+Ol F 15 968 . 68 4 . 0BE+Ol 17 . 52 4 . 08E+Ol l . 75E+Ol F 16 1119 . 97 3 . 58E+Ol 16 . 92 3 . 58E+Ol 1 . 69E+Ol F 17 1237 . 91 2 . 08E+Ol 12 . 33 2 . 08E+Ol l . 23E+Ol F 18 1460 . 4 1 4 . 77E+02 45 . 00 5 . 63E+Ol 1 . 71E+Ol 4 . 21E+02 4 . 82E+Ol F 19 1763 . 98 3 . 89E+Ol 13 . 77 1 . 52E+Ol 9 . 80E+OO 2 . 37E+Ol 1 . 69E:+01 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Dairyland_NPP\Llbrary\HOTLAB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{3/4) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0 . 98 1460 . 75
- 10 . 67 5 . 47E 00 6 . 95£ - 01 CS-137 0 . 98 661 . 65
- 85 . 12 3 . 94£-02 2 . 87E-02 PB-212 0 . 99 77 . 11
- 17 . 50 3 . 50E-01 8 . 28E - 02 238 . 63
- 44 . 60 2 . 77E-01 3 . 56E-02 BI-214 0 . 85 609 . 31
- 46 . 30 3 . 70£-01 6.60£-02 1120 . 29 15 . 10 2 . 61E-01 l.24E-01 1238. 11
- 5 . 94 4 . 21£-01 2 . SOE-01 1377 . 67 4 . 11 1407 . 98 2.48 1509 . 19 2 . 19 1764 .4 9
- 15 . 80 2 . 43E-01 l . 74E-Ol PB-214 0 . 99 77 . 11 10 . 70 5 . 73E-01 l . 35E - Ol 295 . 21
- 19 . 20 4 . 21E-01 6 . 91E - 02 351 . 92
- 37 . 20 3 . 18E- 01 6 . 23£- 02 RA-226 0 . 97 186 . 21
- 3 . 28 9 . 21E- 01 2 . 70E- 01 AC - 228 0 . 60 209 . 28 4 . 40 338 . 32
- 11 . 40 2 . 00E-01 8 . 06E-02 794 . 70 4 . 60 911 . 60
- 27 . 70 2 . 85E-01 7 . 48E-02 964 . 60 5 . 20 10/7/2020 Page 8
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 6:07:29PM Page 4 of7 Analysis Report for L2-SUB-102-AJGS-024-S8 04105118 - 1458 Nuclide Id Energy Yield(%) Activity Activity Name Confidence {keV) (pCilgrams) Uncertainty AC - 228 0 . 60 969 . 11
- 16 . 60 2 . 38E-01 l . 03E-01
* = Energy line found In the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCil grams)
K-4 0 0.981 S . 47E+00 / 6.95E-0l CS-137 0.989 3 . 94E-02 2 . 87E-02 PB -2 12 0 . 999 2 . 56E-01 3 . 29E - 02 BI-214 0 . 859 3 . 40E-01 5 . 39E - 02 PB -2 14 0.998 3 . 42E - 0l 4 . 41E-02 RA-226 0 . 979 9 . 21E-01 2 . 70E- 01 AC -2 28 0 . 600 2.44E - 01 4 . 84E - 02
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/7/2020 Page 9
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 6:07:29PM Page 5 of 7 Analysis Report for L2-SUB-102-AJGS-024-SB 04/05/18 - 1458 UNIDENTIFIED PEAKS Peak Locate Performed on : 4/9/2018 6:07:20PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peale Size (CPS) Uncertainty Type Nuclide M 1 74 . 72 3 . 80410E- 02 15 . 38 t1it)ir;/" f"l'JM(!, F 3 129 . 14 l . 73297E - 02 26 . 50 Tol. PA- 228 m 6 24 1. 87 4 . 02639E-02 12 . 04 r1, -t,I t/, m 8 299 . 94 l . 39401E- 02 22 . 85 f1 . . z,,-z.- F 11 583 . 02 4 . 046 43E - 02 9 . 64 -11 ..-tcJ~ M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dairyland_NPP\Library\HOTLAB.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl/grams) (pCi/grams) (pCl/grams) (keV)
+ K- 40 14 60 . 7 5
- 10 . 67 5 . 47E+OO 6 . 37E - 01 6 . 37E-01
+
+
AR- 41 C0-60 1293 . 64 1173 . 22 99 . 16 100 . 00
-7 . 82E+l3 2 . 30E- 02 1 . OOE+l5 5 . 69E-02 1 6 . 43£- 02 1 . OOE+15 1332 . 49 100 . 00 2 . 76E- 02 5 . 69£-02
+ KR- 85 513 . 99 0 . 43 1 . 68E+Ol l . 07E+Ol l . 07E+Ol
+ Y- 88 898 . 04 93 . 70 - 2 . 21E - 02 3 . 80E - 02 5 . 08E-02 1836 . 06 99 . 20 - 8 . 66E - 03 3 . 80E- 02 10/7/2020 Page 10
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 6:07:29PM Page 6 of7 Analysis Report for L2-SUB-102-AJGS-024-SB 04/05/18 - 1458 Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams) (keV)
+ NB - 94 702 . 63 100 . 00 6 . 59E - 03 4 . 27E - 02 4 . 27E-02 871 . 10 100 . 00 -6 . 36E - 02 4 . 33E-02
+ I-131 284 . 30 6 . 06 -2 . 00E-01 6 . 12E-02 8 . 09E - 01 364 . 48 81. 20 2 . 51E- 02 6 . 12E- 02 636 . 97 7 . 27 2 . 06E - 01 7 . 68E - 01
+ CS - 134 604 . 70 97 . 60 - 5 . 82E - 03 5 . 74E - 02 6 . 73E - 02 795 . 84 85 . 40 -3 . 23E- 02
- 5 . 74E - 02
+ CS-137 661. 65
- 85 . 12 3 . 94E- 02 5 . 23£ - 02 . / 5 . 23E - 02
+ CE- 144 80 . 12 1. 36 -l . 36E+OO 3 . 00E-01 3 . 94E+OO 133 . 51 11.09 - 2 . 26E- 01 3 . 00E-01
+ EU - 152 1 21 . 78 28 . 40 - 7 . 21E- 02 1 . 13E- 01 / 1 . 13E- 01 244 . 69 7 . 49 4 . 75E- 02 5 . 93E- 01 964 . 00 14 . 44 4 . 26E - 01 4 . 17E-Ol 1408 . 00 20 . 74 l.50E-01 2 . 57E - 01 EU-154 123 . 07 40 . 40 -5 . 07E- 02 8 . 04E - 02 / 8 . 04E - 02 247 . 94 6 . 60 l . 75E-01 5 . 83E-01 723 . 30 19 . 70 1 . 52E-02 2 . 26E-01 873 . 20 11 . 50 - 2 . 58E-01 3 . 81E - 01 1004 . 76 17 . 90 -3 . 77E - 02 2 . 84E-01 1274 . 51 35 . 50 8 . 80E-02 1 . 65E - 01
+ EU-155 86 . 54 32 . 80 -2 . 67E-04 l . 36E-01 1. 36E-Ol 105 . 31 21 . 80 - 7 . 33E - 03 1 . 58E- Ol
+ BI-214 609 . 31
- 4 6 . 30 3 . 70E - 01 9 . 73E - 02 9 . 73E-02 1120 . 29
- 15 . 10 2 . 61E - 01 2 . 34E-01 1238 . 11
- 5 . 94 4 . 21E - 0 1 5 . 99E - 01 1377 . 67 4 . 11 - l . 60E - 02 l . 22E+OO 1407 . 98 2 . 48 1 . 25E+OO 2 . 15E+OO 1509 . 19 2 . 19 2 . 85E - 01 l . 84E+OO 1764 . 49
- 15 . 80 2 . 43E- 01 2 . 76E - 01
+ PB-214 77 . 11
- 10 . 70 5 . 73E-01 9 . 96E - 02 2 . 99E-Ol 295 . 21
- 1 9 . 20 4 . 21E - 01 l . 03E-01 35 1. 92
- 37 . 20 3 . 18E- 01 9 . 96E-02
+ PA-228 89 . 95 22 . 00 4 . 67E+O O 2 . 59E+OO 4 . 36E+OO 93 . 35 35 . 00 3 . 04E+00 2 . 59E+OO 105 . 00 16 . 30 - 1 . 99E+OO 4 . 72E+OO 129 . 22 2 . 97 9 . 79E+OO 2 . 48E+Ol 338 . 32 5 . 30 6 . 08E+OO l . 60E+Ol 463 . 00 13 . 80 3 . 63E+OO 6 . 47E+OO 911. 23 16 . 70 9 . 63E+OO 8 . 33E+OO
+ AM-241 59 . 54 36 . 30 - 6 . 60E-02 2 . 35E - 01 2 . 35E - 01
+ CM- 243 103 . 76 23 . 00 3 . 02E-02 1. 51E - 01 1 . 51E-01 228 . 18 10 . 60 1 . llE - 02 3 . 16E-01 277 . 60 14 . 00 - l . 18E- 01 2 . 55E-01
+ = Nuclide identified during the nuclide identlficatlon
= Energy line found in the spectrum
> MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION : MDA value is inconsistent with Currie MDA at 95% confidence level 10/7/2020 Page 11
LAC LTP - Final Status Survey Package - 3/21/2018 4/9/2018 6:07:29PM Page 7 of7 Analysis Report for L2-SUB-102-AJGS-024-SB 04/05/18 - 1458 10/7/2020 Page 12
FSS RELEASE RECORD REVISION 1 SURVEY UNIT L2-011-104 ~ G3 CRIB HOUSE, CIRC. WATER DISCHARGE LAND LACROSSESOLUTIONS ATTACHMENT 8 GEL LABORATORIES ANALYTICAL REPORTS 338
[i]ij* I Laboratories LLc PO Bex 30712 Charleston SC 29417 a member of The GEL Group INC 2040 Sa*1a,;ie Road Charleston. SC 29407 P 843 556.8171 F 84:;_766.117B gel.c om October 15, 2019 Mr. Jason Q. Spaide LaCrosseSolutions S4601 State Hwy 35 Genoa, Wisconsin 54632 Re: LACBWR Site Restoration Project Work Order: 490846
Dear Mr. Spaide:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on September 20, 2019. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4453. Sincerely, Edith Kent Project Manager Purchase Order: 672583 Enclosures
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report for ENRG070 LaCrosseSolutions, LLC (672583) Client SDG: 490846 GEL Work Order: 490846 The Qualifiers in this report are defined as follows:
- A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis. The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the 'U' qualifier above. This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Edith Kent. Reviewed by Page 2 of 37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-A24-SB Project: ENRG07001 Sample ID: 490846001 Client ID: ENRG070 Matrix: Soil Collect Date: 03-JUL-19 12:56 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0174 +/-0.0686 0.134 0.400 pCi/g JXC9 10/07/19 1511 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 3 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-A25-SB Project: ENRG07001 Sample ID: 490846002 Client ID: ENRG070 Matrix: Soil Collect Date: 03-JUL-19 13:01 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0855 +/-0.0784 0.128 0.400 pCi/g JXC9 10/07/19 1511 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 4 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-FJGS-A12A-SB Project: ENRG07001 Sample ID: 490846003 Client ID: ENRG070 Matrix: Soil Collect Date: 12-JUL-19 13:02 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0271 +/-0.0476 0.104 0.400 pCi/g JXC9 10/07/19 1511 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 84 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 5 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-107-FJGS-005-SS Project: ENRG07001 Sample ID: 490846004 Client ID: ENRG070 Matrix: Soil Collect Date: 08-AUG-19 15:29 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.033 +/-0.0803 0.145 0.400 pCi/g JXC9 10/07/19 1511 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 70.7 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 6 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-107-FJGS-016-SS Project: ENRG07001 Sample ID: 490846005 Client ID: ENRG070 Matrix: Soil Collect Date: 09-AUG-19 14:00 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0505 +/-0.0835 0.167 0.400 pCi/g JXC9 10/07/19 1511 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 81.8 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 7 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-101-FJGS-003-SS Project: ENRG07001 Sample ID: 490846006 Client ID: ENRG070 Matrix: Soil Collect Date: 08-AUG-19 14:21 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.00619 +/-0.0654 0.121 0.400 pCi/g JXC9 10/08/19 0817 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 81.8 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 8 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-102-FJGS-010-SS Project: ENRG07001 Sample ID: 490846007 Client ID: ENRG070 Matrix: Soil Collect Date: 15-AUG-19 08:48 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0125 +/-0.0576 0.106 0.400 pCi/g JXC9 10/08/19 1106 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 79.6 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 9 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-103-FJGS-008-SS Project: ENRG07001 Sample ID: 490846008 Client ID: ENRG070 Matrix: Soil Collect Date: 14-AUG-19 10:25 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0247 +/-0.0832 0.149 0.400 pCi/g JXC9 10/07/19 1510 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 90.6 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 10 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: LI -010-104-F JGS-006-SS Project: ENRG07001 Sample ID: 490846009 Client ID: ENRG070 Matrix: Soil Collect Date: 23-AUG-19 08:44 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0047 +/-0.0675 0.130 0.400 pCi/g JXC9 10/07/19 1510 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 81.8 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 11 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-105-FJGS-008-SS Project: ENRG07001 Sample ID: 490846010 Client ID: ENRG070 Matrix: Soil Collect Date: 23-AUG-19 13:39 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0453 +/-0.0588 0.125 0.400 pCi/g JXC9 10/08/19 0817 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 77.3 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 12 of 37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: LI -010-106-F JGS-004-SS Project: ENRG07001 Sample ID: 490846011 Client ID: ENRG070 Matrix: Soil Collect Date: 28-AUG-19 10:39 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.024 +/-0.0648 0.117 0.400 pCi/g JXC9 10/07/19 1510 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 92.8 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 13 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-106-FJGS-017-SS Project: ENRG07001 Sample ID: 490846012 Client ID: ENRG070 Matrix: Soil Collect Date: 28-AUG-19 14:31 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.023 +/-0.0397 0.0872 0.400 pCi/g JXC9 10/08/19 0817 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 84 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 14 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-106-FJGS-018-SS Project: ENRG07001 Sample ID: 490846013 Client ID: ENRG070 Matrix: Soil Collect Date: 28-AUG-19 14:51 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0371 +/-0.0984 0.174 0.400 pCi/g JXC9 10/07/19 1510 1921875 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 86.2 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 15 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-CJGS-A0 I-SB Project: ENRG07001 Sample ID: 490846014 Client ID: ENRG070 Matrix: Soil Collect Date: 27-JUN-19 10:51 Receive Date: 20-SEP-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 u 0.0233 +/-0.0336 0.0405 0.400 pCi/g MXS2 10/14/19 0853 1919949 Americium-243 u -0.0154 +/-0.0278 0.0708 0.400 pCi/g Curium-243/244 u -0.00404 +/-0.0179 0.0466 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 u -0.00044 +/-0.00286 0.0059 0.010 pCi/g MXS2 10/13/19 1023 1919950 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 u 0.0035 +/-0.0399 0.0848 0.400 pCi/g MXS2 10/14/19 0738 1919951 3 Plutonium-239/240 u -0.00481 +/-0.0332 0.0808 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 u 3.99 +/-3.10 5.16 5.00 pCi/g MXS2 10/14/19 2041 1919952 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 u -0.464 +/-1.15 1.82 5.00 pCi/g TXJl 10/11/19 0816 1921366 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 0.312 +/-0.0643 0.0341 1.00 pCi/g MXR.1 10/05/19 1250 1919313 6 Cobalt-60 u 0.00967 +/-0.0204 0.0438 pCi/g Europium-152 u 0.031 +/-0.0481 0.0992 pCi/g Europium-154 u 0.0292 +/-0.0612 0.129 pCi/g Europium-155 u 0.00749 +/-0.0528 0.102 pCi/g Niobium-94 u 0.00999 +/-0.0155 0.0334 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 u 0.0873 +/-0.113 0.192 0.400 pCi/g JXC9 10/07/19 1510 1921875 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium u 4.06 +/-4.58 7.69 10.0 pCi/g EW3 10/04/19 0308 1921574 8 Liquid Scint C14, Solid "As Received" Carbon-14 u -2.58 +/-2.02 3.60 5.00 pCi/g TXP3 10/09/19 1559 1921585 9 Liquid Scint Tc99, Solid "As Received" Tecbnetium-99 u -0.45 +/-0.886 1.55 2.00 pCi/g JJ3 10/06/19 0743 1921541 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 u -1.7 +/-5.55 7.59 10.0 pCi/g TXJl 10/11/19 1543 1921313 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 16 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-CJGS-A0 I-SB Project: ENRG07001 Sample ID: 490846014 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U 1.70 +/-2.13 3.60 5.00 pCi/g TXJl 10/11/19 1554 1921355 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 RYHl 09/25/19 1209 1919153 The following Analytical Methods were performed: Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-0l-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 71.8 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 84.8 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 97.2 (15%-125%) Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 55.2 (15%-125%) Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 55.2 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 108 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 86.2 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 104 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 64.4 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 81.5 (25%-125%) Notes: Page 17 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: October 15, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-SUB-TDS-CJGS-A0 I-SB Project: ENRG07001 Sample ID: 490846014 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 18 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC SummaIT Report Date: October 15, 2019 LaCrosseSolutions Page 1 of 7 S4601 State Hwy 35 Genoa, Wisconsin
Contact:
Mr. Jason Q. Spaide Workorder: 490846 Parmname NOM Sam~le Qual QC Units RPO% REC% Range Anlst Date Time Rad Alpha Spec Batch 1919949 QC1204388648 490846014 DUP Americium-241 u 0.0233 u 0.0153 pCi/g NIA NIAMXS2 10/14/19 08:53 Uncertainty +l-0.0336 +l-0.0404 Americium-243 u -0.0154 u -0.00504 pCi/g NIA NIA Uncertainty +l-0.0278 +l-0.0171 Curium-2431244 u -0.00404 u -0.0184 pCi/g NIA NIA Uncertainty +l-0.0179 +l-0.0318 QC1204388649 LCS Americium-241 1.92 1.77 pCi/g 92.4 (75%-125%) 10/14/19 08:53 Uncertainty +l-0.186 Americium-243 u -0.0226 pCi/g (75%-125%) Uncertainty +l-0.0444 Curium-2431244 2.26 1.89 pCi/g 83.8 (75%-125%) Uncertainty +l-0.191 QC1204388647 MB Americium-241 u -0.00254 pCi/g 10/14/19 08:53 Uncertainty +l-0.0237 Americium-243 u 0.000499 pCi/g Uncertainty +l-0.0229 Curium-2431244 u -0.00426 pCi/g Uncertainty +l-0.0193 Batch 1919950 QC1204388651 490846014 DUP Neptunium-237 u -0.00044 u -0.00249 pCi/g NIA NIAMXS2 10/13/19 10:23 Uncertainty +l-0.00286 +l-0.00293 QC1204388652 LCS Neptunium-237 1.44 1.55 pCi/g 108 (75%-125%) 10/13/19 10:23 Uncertainty +l-0.056 QC1204388650 MB Neptunium-237 u -0.00178 pCi/g 10/13/19 10:23 Uncertainty +l-0.00276 Page 19 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC SummaIT Workorder: 490846 Page 2 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1919951 QC1204388654 490846014 DUP Plutonium-23 8 u 0.0035 u 0.0176 pCi/g NIA NIAMXS2 10/14/19 07:38 Uncertainty +l-0.0399 +/-0.0379 Plutonium-2391240 u -0.00481 u -0.0268 pCi/g NIA NIA Uncertainty +l-0.0332 +/-0.0203 QC1204388655 LCS Plutonium-238 u 0.00911 pCi/g 10/14/19 07:38 Uncertainty +/-0.0382 Plutonium-2391240 1.96 1.86 pCi/g 95.3 (75%-125%) Uncertainty +l-0.244 QC1204388653 MB Plutonium-238 u -0.00287 pCi/g 10/14/19 07:38 Uncertainty +/-0.0268 Plutonium-2391240 u 0.00918 pCi/g Uncertainty +/-0.0253 Batch 1919952 QC1204388657 490846014 DUP Plutonium-241 u 3.99 u 3.44 pCi/g NIA NIAMXS2 10/15/19 02:00 Uncertainty +l-3.10 +l-2.41 QC1204388658 LCS Plutonium-241 162 184 pCi/g 113 (75%-125%) 10/15/19 04:04 Uncertainty +l-4.54 QC1204388656 MB Plutonium-241 u 1.84 pCi/g 10/14/19 22:45 Uncertainty +l-2.15 Rad Gamma Spec Batch 1919313 QC1204386990 490846014 DUP Cesium-137 0.312 0.350 pCi/g 11.5 (0%-20%) MXRl 10105/19 15:03 Uncertainty +l-0.0643 +/-0.0553 Cobalt-60 u 0.00967 u 0.0062 pCi/g NIA NIA Uncertainty +l-0.0204 +/-0.0199 Europium-152 u 0.031 u -0.00481 pCi/g NIA NIA Uncertainty +l-0.0481 +l-0.0438 Page 20 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC SummaIT Workorder: 490846 Page 3 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1919313 Europium-154 u 0.0292 u 0.00422 pCi/g NIA NIAMXRl 10105/19 15:03 Uncertainty +l-0.0612 +/-0.0613 Europium-155 u 0.00749 u -0.0257 pCi/g NIA NIA Uncertainty +l-0.0528 +/-0.0382 Niobium-94 u 0.00999 u 0.0181 pCi/g NIA NIA Uncertainty +l-0.0155 +l-0.0137 QC1204386991 LCS Americium-241 487 510 pCi/g 105 (75%-125%) 10105/19 12:52 Uncertainty +l-5.36 Cesium-137 167 164 pCi/g 98.3 (75%-125%) Uncertainty +l-3.96 Cobalt-60 108 107 pCi/g 98.5 (75%-125%) Uncertainty +l-3.72 Europium-152 u -0.591 pCi/g Uncertainty +l-1.40 Europium-154 u -0.258 pCi/g Uncertainty +l-0.900 Europium-155 u 0.655 pCi/g Uncertainty +l-1.02 Niobium-94 u 0.231 pCi/g Uncertainty +l-0.450 QC1204386989 MB Cesium-137 u -0.00479 pCi/g 10105/19 12:51 Uncertainty +l-0.0152 Cobalt-60 u -0.00517 pCi/g Uncertainty +l-0.0145 Europium-152 u -0.000709 pCi/g Uncertainty +l-0.0424 Europium-154 u -0.0286 pCi/g Uncertainty +l-0.038 Europium-155 u 0.0641 pCi/g Uncertainty +l-0.0928 Page 21 of 37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC SummaIT Workorder: 490846 Page 4 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1919313 Niobium-94 u 0.00784 pCi/g MXRl 10105/19 12:51 Uncertainty +/-0.0142 Batch 1921366 QC1204391968 490846014 DUP Nickel-59 u -0.464 u -0.171 pCi/g NIA NIA TXJl 10/11/19 08:17 Uncertainty +l-1.15 +l-0.691 QC1204391969 LCS Nickel-59 92.8 100 pCi/g 108 (75%-125%) 10/11/19 09:30 Uncertainty +l-6.10 QC1204391967 MB Nickel-59 u 1.07 pCi/g 10/11/19 08:17 Uncertainty +l-1.85 Rad Gas Flow Batch 1921875 QC1204393106 490846005 DUP Strontium-90 u -0.0505 u 0.0293 pCi/g NIA NIA JXC9 10107/19 15:10 Uncertainty +l-0.0835 +l-0.0985 QC1204393107 LCS Strontium-90 5.36 5.83 pCi/g 109 (75%-125%) 10107/19 15:10 Uncertainty +l-0.340 QC1204393105 MB Strontium-90 u 0.Q15 pCi/g 10107/19 15:10 Uncertainty +l-0.0671 Rad Liquid Scintillation Batch 1921313 QC1204391802 490846014 DUP lron-55 u -1.7 u -0.904 pCi/g NIA NIA TXJl 10/11/19 18:19 Uncertainty +l-5.55 +l-5.29 QC1204391803 LCS Iron-55 76.4 71.5 pCi/g 93.5 (75%-125%) 10/11/19 19:37 Uncertainty +l-5.37 QC1204391801 MB Iron-55 u 1.03 pCi/g 10/11/19 17:01 Uncertainty +l-4.39 Page 22 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC SummaIT Workorder: 490846 Page 5 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1921355 QC1204391926 490846014 DUP Nickel-63 u 1.70 u -0.61 pCi/g NIA NIA TXJl 10/11/19 16:28 Uncertainty +l-2.13 +l-2.12 QC1204391927 LCS Nickel-63 96.5 101 pCi/g 104 (75%-125%) 10/11/19 16:44 Uncertainty +l-5.11 QC1204391925 MB Nickel-63 u -0.418 pCi/g 10/11/19 16:11 Uncertainty +l-2.23 Batch 1921541 QC1204392284 490846014 DUP Technetium-99 u -0.45 u -0.161 pCi/g NIA NIA JJ3 10106/19 08:48 Uncertainty +l-0.886 +l-0.901 QC1204392285 LCS Technetium-99 41.1 36.7 pCi/g 89.3 (75%-125%) 10106/19 09:20 Uncertainty +l-1.70 QC1204392283 MB Technetium-99 u -0.684 pCi/g 10106/19 08:15 Uncertainty +l-0.898 Batch 1921574 QC1204392383 490846014 DUP Tritium u 4.06 u 4.45 pCi/g NIA NIA EW3 10104/19 05:53 Uncertainty +l-4.58 +l-4.62 QC1204392385 LCS Tritium 146 129 pCi/g 88.1 (75%-125%) 10104/19 07:27 Uncertainty +l-8.79 QC1204392382 MB Tritium u 3.98 pCi/g 10104/19 03:55 Uncertainty +l-4.49 QC1204392384 490846014 MS Tritium 149 u 4.06 124 pCi/g 83.3 (75%-125%) 10104/19 06:40 Uncertainty +l-4.58 +l-8.95 Page 23 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 490846 Page 6 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1921585 QC1204392425 490846014 DUP Carbon-14 u -2.58 U -1.82 pCi/g NIA NIA TXP3 10/09/19 17:34 Uncertainty +/-2.02 +/-2.01 QC1204392427 LCS Carbon-14 142 133 pCi/g 93.5 (75%-125%) 10/09/19 19:10 Uncertainty +/-4.36 QC1204392424 MB Carbon-14 u 0.0484 pCi/g 10/09/19 16:46 Uncertainty +/-2.08 QC1204392426 490846014 MS Carbon-14 146 u -2.58 132 pCi/g 90.2 (75%-125%) 10/09/19 18:23 Uncertainty +/-2.02 +/-4.40 Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). The Qualifiers in this report are defined as follows:
** Analyte is a Tracer compound < Result is less than value reported > Result is greater than value reported BD Results are either below the MDC or tracer recovery is low FA Failed analysis.
H Analytical holding time was exceeded J See case narrative for an explanation J Value is estimated K Analyte present. Reported value may be biased high. Actual value is expected to be lower. L Analyte present. Reported value may be biased low. Actual value is expected to be higher. M M if above MDC and less than LLD M REMP Result> MDC/CL and< RDL NIA RPD or %Recovery limits do not apply. Nl See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER. R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD. UI Gamma Spectroscopy--Uncertain identification Page 24 of37 SDG: 490846
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 490846 Page 7 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time UJ Gamma Spectroscopy--Uncertain identification UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier y Other specific qualifiers were required to properly define the results. Consult case narrative. A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. h Preparation or preservation holding time was exceeded NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/- the RL is used to evaluate the DUP result.
- Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 25 of37 SDG: 490846
Radiochemistry Technical Case Narrative LaCrosseSolutions, LLC SDG #: 490846 Product: Alphaspec Isotopic Am241 Am243, Cm243/244, Solid Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 27 Analytical Batch: 1919949 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 490846014 Ll-SUB-TDS-CJGS-A0 1-SB 1204388647 Method Blank (MB) 1204388648 490846014(Ll-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204388649 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Recounts The Cm-244 portion of sample 1204388647 (MB) was recounted due to results more negative than the three sigma TPU. The recount is reported. Product: Alphaspec Np, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-032 REV# 22 Analytical Batch: 1919950 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 pfJc ~e,rp!Pfi~ : 49~.:M< 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 490846014 L 1-SUB-TDS-CJGS-A0 1-SB 1204388650 Method Blank (MB) 1204388651 490846014(Ll-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204388652 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: Alphaspec Pu238, 239/240, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 27 Analytical Batch: 1919951 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 490846014 Ll-SUB-TDS-CJGS-A0 1-SB 1204388653 Method Blank (MB) 1204388654 490846014(Ll-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204388655 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: Dry Weight Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 pfJc ~e,rp!Pfi~ : 49~.:M< 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
The following samples were analyzed using the above methods and analytical procedure(s). GEL Samnle ID# Client Samnle Identification 490846001 L 1-SUB-TDS-FJGS-A24-SB 490846002 L 1-SUB-TDS-FJGS-A25-SB 490846003 Ll-SUB-TDS-FJGS-A12A-SB 490846004 Ll-010-107-FJGS-005-SS 490846005 Ll-010-107-FJGS-016-SS 490846006 Ll-010-101-FJGS-003-SS 490846007 Ll-010-102-FJGS-010-SS 490846008 Ll-010-103-FJGS-008-SS 490846009 L1-010-104-F JGS-006-S S 490846010 Ll-010-105-FJGS-008-SS 490846011 Ll-010-106-FJGS-004-SS 490846012 Ll-010-106-FJGS-017-SS 490846013 Ll-010-106-FJGS-018-SS 490846014 Ll-SUB-TDS-CJGS-A0 1-SB The samples in this SDG were analyzed on an "as received" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 Analytical Method: DOE HASL 300, 4.5.2.3/Ga-01-R Analytical Procedure: GL-RAD-A-013 REV# 27 Analytical Batch: 1919313 Prenaration Method: Dry Soil Prep Prenaration Procedure: GL-RAD-A-021 REV# 23 Prenaration Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s). GEL Samnle ID# Client Samnle Identification 490846014 Ll-SUB-TDS-CJGS-A0 1-SB 1204386989 Method Blank (MB) 1204386990 490846014(Ll-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204386991 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. pfJc ~e,rp!Pfi~ : 49~.:M< 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Product: Gamma Ni59, Solid Analytical Method: DOE RESL Ni-1 Analytical Procedure: GL-RAD-A-022 REV# 19 Analytical Batch: 1921366 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 490846014 L 1-SUB-TDS-CJGS-A0 1-SB 1204391967 Method Blank (MB) 1204391968 490846014(Ll-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204391969 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: GFPC, Sr90, Solid Analytical Method: EPA 905 .0 Modified/DOE RP501 Rev. 1 Modified Analytical Procedure: GL-RAD-A-004 REV# 21 Analytical Batch : 1921875 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 490846001 Ll-SUB-TDS-FJGS-A24-SB 490846002 Ll-SUB-TDS-FJGS-A25-SB 490846003 Ll-SUB-TDS-FJGS-A 12A-SB 490846004 Ll-010-107-FJGS-005-SS 490846005 Ll-010-107-FJGS-016-SS 490846006 Ll-010-101-FJGS-003-SS 490846007 Ll-010-102-FJGS-010-SS 490846008 Ll-010-103-FJGS-008-SS 490846009 Ll-0 10-104-FJGS-006-SS pfJc ~e,rp!Pfi~ : 49~.:M< 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
490846010 Ll-010-105-FJGS-008-SS 490846011 Ll -010-106-F JGS-004-S S 490846012 Ll-010-106-FJGS-0l 7-SS 490846013 Ll-010-106-FJGS-0l 8-SS 490846014 L 1-SUB-TDS-CJGS-A0 1-SB 1204393105 Method Blank (MB) 1204393106 490846005(Ll-010-107-FJGS-016-SS) Sample Duplicate (DUP) 1204393107 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Recounts Samples 490846006 (Ll-010-101-FJGS-003-SS), 490846007 (Ll-010-102-FJGS-010-SS), 490846010 (Ll-010-105-FJGS-008-SS) and 490846012 (Ll-010-106-FJGS-0l 7-SS) were recounted due to results more negative than the three sigma TPU. The second counts are reported. Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 21 Analytical Batch: 1919952 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 490846014 Ll-SUB-TDS-CJGS-A0 1-SB 1204388656 Method Blank (MB) 1204388657 490846014(Ll-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204388658 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. pfJc l:ffl>e,rp!Pfi~ : 49~.:M< 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Product: Liquid Scint Fe55, Solid Analytical Method: DOE RESL Fe-1, Modified Analytical Procedure: GL-RAD-A-040 REV# 13 Analytical Batch: 1921313 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 490846014 L 1-SUB-TDS-CJGS-A0 1-SB 1204391801 Method Blank (MB) 1204391802 490846014(Ll-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204391803 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Recounts Samples were recounted due to high MDCs. The recounts are reported. Product: Liquid Scint Ni63, Solid Analytical Method: DOE RESL Ni-1, Modified Analytical Procedure: GL-RAD-A-022 REV# 19 Analytical Batch: 1921355 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1919153 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 490846014 Ll-SUB-TDS-CJGS-A0 1-SB 1204391925 Method Blank (MB) 1204391926 490846014(Ll-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204391927 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. pfJc l:l1#Je,rp!Pfi~ : 49~.:M< 30712 Char1eston, SC 29417 2040 Savage Road Charleston , SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 5 Analytical Batch: 1921541 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 490846014 L 1-SUB-TDS-CJGS-A0 1-SB 1204392283 Method Blank (MB) 1204392284 490846014(Ll-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204392285 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: LSC, Tritium Distillation, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 23 Analytical Batch : 1921574 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 490846014 Ll-SUB-TDS-CJGS-A0 1-SB 1204392382 Method Blank (MB) 1204392383 490846014(Ll-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204392384 490846014(Ll-SUB-TDS-CJGS-A01-SB) Matrix Spike (MS) 1204392385 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. pfJc ~e,rp!Pfi~ : 49~.:M< 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 16 Analytical Batch: 1921585 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 490846014 L 1-SUB-TDS-CJGS-A0 1-SB 1204392424 Method Blank (MB) 1204392425 490846014(Ll-SUB-TDS-CJGS-A01-SB) Sample Duplicate (DUP) 1204392426 490846014(Ll-SUB-TDS-CJGS-A01-SB) Matrix Spike (MS) 1204392427 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. pfJc ~e,rp!Pfi~ : 49~.:M< 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
'"d rf6 (I) u.) .j:::.. Y 9 o fl-/ to 0 Page: _ _ _ ! _ _ _ of _ _ _ 2 ~ ~* I , GEL Laboratories. LLC >-+-,
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-..J Project # LACBWR GEL Quote#: - -- - - - - -- -----,
Site l!tl-1 "'" """' Laboratories LLC Cllemistry I Radiochemistry I Ractiobloa:ssny I Specialty Analytics 2040 Savage Road Charleston, SC 29407 r./) COC Number 0 >: Phone: (843) 556-8171 u PO Number: 672583 -===-- - Fax: {843) 766-1178 0 Client Name: La Crosse Solutions Phone # 608-689-4259 I Sample Analys~_Requested <5> (Fill in the number of containers for <!ach test)
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I.O Project/Site Name: LACBWR-Genoa WI Fax# 0 00 Address: 54601 State Road 35
.j:::.. Comments O'I 0 Note: extra sample is
'c required for sample specific QC LJ,SUB-TDS_-FJGS-A25-SB LI-SUB-TDS-FJGS-A I 2A-SB L l-010-107-FSGS-005-SS Ll-0 10-107-FJGS-016-SS LI-0rn-1 o1,.rsGs-003,ss Ll-010cl03:FSGS-008-SS L 1-0 I 0-104-FSGS-006-SS Ll-0I o,.foj,F.SG.ScOOS~.SS
- 1. Kevin L Murrav ocroo Level 3 Level 4 2 2 For Lah Receiving Use Only: _Custo,(y Seal Intact? 1 l Yes LJ No _ C{)(J_ler Temp_:_~ °C
>-For sample shipping am/ delivt!_ry detail:;, see Sam}le Receipt & Re,1L'W form (SRR.) - Siimpte*collectio11 Tin,e Zomt ;_[ ] Eastern [ ] Paci fic - [X] Central ( J!\-fountain [ J Other:
I.) Chain of Custo:lr Number = Client Determined 2.) QC Codes: N Nomml S.implc, TB """ Trip Blank FD = Field Duplicate. EB"" Equipment Blank, MS = !\.fotrix Spike Sample, MSD c:. Mntrix Spike Dupliemc Sample, G "' Grab, C "" Composite
,:c 3.) Field Filtered; For liquid matrices, indicate with a - Y - for yes the sample \\'3S fi eld fi ltered or - N - for s.1mplc was not field filtered.
4.) Matrix Codes: DW=Drinki ng Water, GWc:--Groundwatcr, SW-=Surfacc Water, WW,,.Wastc Water, W=Watcr, ML==Misc Liquid, SO,.,,Soil. SIFScdimcnt, SL::cSludgc, SS=Solid Waste, O"'Oil. f',,,fiJtcr. P""'Wipc. u,,,Urinc, F=Fccnl, N=Nasal 5.) Sample Analysis Requested: Ana1)1 ical method rcqucslcd (i .e. 82608 , 60 l 0Bn470A) and number of cont.iincrs pro"'ided for each (i.e. 8260H -3_.60/0B/7470A -1). 6.) Prcscrvi'.ltivc Type: HA = Hydrochloric Ac.id, NI "" Nitric Acid, SH""' Sodium Hydroxide, SA = Sulfuric Acid, AA "" Ascorbic Acid, HX =Hexane.ST "' Sodium Th iosulfate, Ifno prcscrvati\"Cis added ~ leave field blank
"'d ~ (1) w VI i-t 9 O ~l-/ io 0 Page: _ _ _2_ _ _ of _ _ _2 I , GEL Laboratories, LLC >-+, w '-1 Project # LACBWR Site GEL Quote #: - - - - - - - - - --------< [!tJ:J!I Laboratones LLC s,,toom Chemistry I Radiochemistry I Radiobioossay I Specially Analytics 2040SavageRoad Charleston, SC 29407 r/J coc Numbcr(lt Chain of Custod and Anal tical Re uest Phone: (843) 556-8171 0 Cl PO Number: 672583 "---'"-~~---'-"~----=-~'-'---=-----------'= Fax: {843) 766-1178 Client Name: La Crosse Solutions Phone# 608-689-4259 I Sample Analysis Requested <~l (Fill in the number of containers for each test) ~ ID 0 Projecl/Site Name: LACBWR-Genoa WI Fax# I I I I I I I I I 00 .,. ;;; ~ Address: 54601 State Road 35 0- ,; .,., M .,..,,. O'I
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N N Collected By: Kevin L Murray Send Results To:Scott Zoller sgzollcr@energysolutions.com 0- N E o'i:: "'
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0: < E E z ,j u MDC <0.0 l pCi NE_-237 Chain of Custody Signatures Relinquished By (Signed) Date Time Received by (signed) Date Time I. Kevin L Murray °l/1 8/1'1 D"'foo er~ Xl Level 2 LJ Level 3 1Level 4 2 2 Addilional Remarks: None 3 For Lab Receiving_ Use On{y: Custody Seal_lnla<1? [ ] Yes JNo Cooler Temp: = °C
>For san1pfe shipping and tfelivery 1left11ts: see Sample Receipt & Reviewform (SRR.) Sa11,plt! Colkction Ti111t! Zont! : ( ) Eastern [ ) Pacific [X) Central [ ) Mountain [ ] Other:
I.) Chain of Custody Numlx--r:: Client Dctcnnincd 2.) QC Codes: N"" Normal Sample, TB = Trip Blank. FD = Field Duplicate, EB=,, Equipment Blank. MS"" ~,fatrix Spike Samplc, l\lSD"" Malrix Spike Duplicnle Sample. G ~ Grab, C""" Composite 3.) Field Fihcrcd: For liquid matrices, indicate with a - Y ~ for yes the sample was field filtcf\."d or - N - for sample was not field filtcrect 4.) Matrix Codes: DW"°Drinking Waler, GW~roundwatcr, SW,,,,Surfacc Water, w,v""Wastc Water, W""-Watcr. ML""Misc Liquid, SQ,:ocSoil, SD ~Sedimcnt, SL"'Sludgc, SS"'Solid Waste, O=:Oil, F""Fillcr, P""\Vipe, U""Urinc. F""-Fecal, N=Nasal 0 5.) Sample Analysis Requested: Anal)tic.al method rcqucslcd (i.c, 8260B, 6010B/7470A) and number of containers provided for each (i.e. 8260/J - 3, 60/0W7470A ~ l), 6.) Prcscn*.,1frc Typ.:: HA "" Hydrochlorfo Acid, NI = Nitric Add, SH""' Sodium Hydroxide, SA""" Sulfuric Acid, AA"" Ascorbic Acid, HX""' Hexane, ST= Sodium Thios:ulfatc. If no preservative is added ~-c- Jem*c field blank
==-----=-======~
irritants, other
SAMPLE RECEIPT & REVIEW FORM Client: i::.NQ<Z SDGIAHJCOC/Wurk Onlcr: LI Ci 021-llo Rccci\'cd Dv: f.iTA f \/ A(\f'd'1 E DatcRccciYcll: 20 - .~l=PT - lq Citric AppliolJfc; Fc~~rcss FedEx Ground UPS Field Services Courier Other Cnriier :md Trncltlng Number 1 1t:..? -,,:;. ? R A 4Ul
~ z C
Suspected Hnznr<l lnronnution "u*N~1 Coums :* l00cpm on s..1111plc.s not mmkcd 11 radioactivc. 11, coUlnci the l~1din1ion Sn.fciy G10\1p for fmthcr invc:s1i~1 ion. linzard Class Shipped: UNf!: A}Shioocd as a DOT H.12.llrdous?
.,,. ~UN29JO, Is 1hc Rndioacli vc Shipment SUrn:.y Complimu*1 Yes _ _ No _
B) Did the client dcsig,m1c 1hesrunplcs nre to be , / reoc nolntion or radicactiYe stickcIS 011 ecntniuors cq,ml clicnl designation. recei\'cd-ns rndioncti\'c? Ncl CounlS Obscr"cd' (Obscrwd Counts - An:a Background Comlls): _$lf__ CPM I mRJHr C) Did the RSO classify the snmplcs ns ..,,, {1n.ximum Clnssificu as: Rad l Had 2 lbd 3 radiollelivc?
/ COC no1mioi1 or hazard labels on containers equal chem dcs ign.-11iotL D) Did 1hc r.licnl dcsi,,m1c snmolcs arc luu.mdous'I lfD or E is yes. select Hazards below.
/i?CB's f!nnurnlblc Fon:ign Soil RCRA Asbesios Beryllium Olhcr:
E) Did the RSO ide1Uifr Possible lw,arrls? Snni11!c Rccci11t Criteria ~ z z C Commcuts/Qtfnlifie~ {Rcc1uircd ror Nnn-Confonning. Hems) Shipping containers received imnct nud 1 scaled? t~
*r;:*
Circl:: Applicabl:: : S:::ats broken Damaged c:onlain~r Lc:ikin~ conl:i,incr Other (desc ribe) I / '~i
- tt CO C created upon receipt Chain of custody docmrr.nls ilicludcd A,,r Cird: .-\ppli:::ibl:: CUenl .:onHlc!cd oindyro\'idcd C~C.
2 with shipment"? @; 3 Sm11plcs requiring cold preservation within (0 < 6 de* Cr?*
,./,.
Prcsc1vn1ion Jvlcthod: Wei Jee !er. Pocks
*a1l 1cmp::rn1urcs nrc recorded in Celsius D1J ice None Oihcr.
TEMP: ZI c Dnily ch~ck petfornl!d nlld passed 4 1empcrnturc gun*) oil 1R
/
Temperature DcYice Serini#: * ~ 1- ,~ Sccondmy Tcmpom111re Dc"icc Serini I! (If Applicnlilc): Cin:b Applicabl:,: Seals brol:cn D ~n\."lp.cd c onlain:r Lc.ikin~ conlnincr Oth::r (dcs::ribc} 5 Sample containers intnct and scnlcd? Sampl:: !D's and Contninm .-\trcctcd: Samples requiring chemical preservation 6 / at proper pH? lfl 1 n:s.cn-ation added. Lot.#: 1f Yes, an: Encores or Soil Kits proscnl for solids'/ Ycs No NA (lf )'CS, IMC to VOA Freezer) 7 Do any samples require Volatile Analysis? !~-
~..~
~~
~
Do liquid VOA vinls conlain acid prcso1vation? Ycs Arc liquid VO/I l'inlsfn:cofhc:idspa::c'I Yes_ No Samp; ID's and contain:rs affccied: No NA NA (lfunknow,~ sclcc1 No)
~l
!D's nnd lcs1s affected:
8 Samples received within holding time? .,dt
;~-
~- !D's and contninc,s affcclcd:
Sample JD's on COC mncb JD's Oil 9 bottles? ,/ t?t
- Cin:lc Appl ic::\blc: No dntcs on con1ni nc1s No limes on consai ncrs coc*1nissing info 01her idcscribc>
D:uc & titre on COC match date & time 10 on bolllcs? I/ 11 Cin:lc Applicable: No co,uainer count on COC 01hcr (describe) Number of containers received ml!ch / 11 number indic.ited on COC? 't
- t .
.v.i Ase sample containers identifiable ns -;a /
12 GEL orovided'l COC fonn is properly signed in 13 relinquished/rcceh*ed sections?
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Circle Applicable: Nol rclinquisl,ed Oilier (describe) Comments (Use Cominunlion Fom1 if needed): PM (or PMAI n:vicw: htitials f. . A Y-< Di1\C t:\ fZ~ 11'1 Pa~_J_or.....L I I GL-CHL-SR-001 Rev 6 Page 36 of 37 SDG: 490846
List of current GEL Certifications as of 15 October 2019 State Certification Alaska 17-018 Arkansas 88-0651 CLlA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 DoD ELAP/ ISOl 7025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (AI33904) Maine 2019020 Maryland 270 Massachusetts M-SC012 Massachusetts PFAS Approv Letter Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada SC000122020-1 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 2019-165 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee 1N 02934 TexasNELAP T104704235-19-15 UtahNELAP SC000122019-28 Vermont VT87156 Virginia NELAP 460202 Washington C780 Page 37 of 37 SDG: 490846
[i]ij* I Laboratories LLc PO Bex 30712 Charleston SC 29417 a member of The GEL Group INC 2040 Sa*1a,;ie Road Charleston. SC 29407 P 843 556.8171 F 84:;_766.117B gel.c om November 14, 2019 Mr. Jason Q. Spaide LaCrosseSolutions S4601 State Hwy 35 Genoa, Wisconsin 54632 Re: LACBWR Site Restoration Project Work Order: 493624
Dear Mr. Spaide:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on October 21, 2019. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4453. Sincerely, Edith Kent Project Manager Purchase Order: 672583 Enclosures
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report for ENRG070 LaCrosseSolutions, LLC (672583) Client SDG: 493624 GEL Work Order: 493624 The Qualifiers in this report are defined as follows:
- A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound H Analytical holding time was exceeded U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
h Preparation or preservation holding time was exceeded Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis. The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the 'U' qualifier above. This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Edith Kent. Reviewed by Page 2 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-002-SS Project: ENRG07001 Sample ID: 493624001 Client ID: ENRG070 Matrix: Soil Collect Date: 08-SEP-16 11:05 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 HUh 0.0084 +/-0.0467 0.0895 0.400 pCi/g HAKB 11/06/19 0953 1929693 Americium-243 HUh 0.0346 +/-0.0974 0.104 0.400 pCi/g Curium-243/244 HUh -0.00429 +/-0.037 0.0857 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.00125 +/-0.00299 0.00529 0.010 pCi/g HAKB 11/11/19 1231 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.00487 +/-0.0271 0.0519 0.400 pCi/g HAKB 11/06/19 0922 1929695 3 Plutonium-239/240 HUh -0.00402 +/-0.0278 0.0676 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.25 +/-2.38 4.12 5.00 pCi/g HAKB 11/09/19 0252 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 HUh -0.18 +/-1.68 3.01 5.00 pCi/g TXJl 10/30/19 0619 1931847 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 Hh 0.113 +/-0.0594 0.0518 1.00 pCi/g MXR.1 10/30/19 0857 1929624 6 Cobalt-60 HUh 0.036 +/-0.0349 0.0881 pCi/g Europium-152 HUh -0.00616 +/-0.0669 0.115 pCi/g Europium-154 HUh -0.0128 +/-0.0717 0.149 pCi/g Europium-155 HUh 0.0587 +/-0.0622 0.134 pCi/g Niobium-94 HUh 0.0376 +/-0.0275 0.0407 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 HUh 0.0238 +/-0.0658 0.120 0.400 pCi/g JXC9 11/06/19 1419 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU 1.65 +/-5.62 9.75 10.0 pCi/g EW3 10/28/19 2327 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 1.92 +/-1.76 2.94 5.00 pCi/g TXP3 11/08/19 1739 1934551 9 Liquid Scint Tc99, Solid "As Received" Tecbnetium-99 HU -0.00734 +/-0.483 0.861 2.00 pCi/g JJ3 11/05/19 2229 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 HUh -1.57 +/-12.1 18.7 10.0 pCi/g RPI 11/01/19 0908 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 3 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-002-SS Project: ENRG07001 Sample ID: 493624001 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 lillh -0.424 +/-1.17 2.08 5.00 pCi/g RPI 10/30/19 1251 1931689 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 35 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 18.2 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 91.7 (15%-125%) Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 79.9 (15%-125%) Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 79.9 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 98.8 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 92.8 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 92.1 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 20.5 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 97.4 (25%-125%) Notes: Page 4 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-002-SS Project: ENRG07001 Sample ID: 493624001 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 5 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-004-SS Project: ENRG07001 Sample ID: 493624002 Client ID: ENRG070 Matrix: Soil Collect Date: 13-SEP-16 11:00 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 HUh -0.00947 +/-0.0286 0.0803 0.400 pCi/g HAKB 11/06/19 0953 1929693 Americium-243 HUh 0.049 +/-0.0706 0.0851 0.400 pCi/g Curium-243/244 HUh -0.0105 +/-0.0316 0.0888 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.00322 +/-0.00457 0.00708 0.010 pCi/g HAKB 11/11/19 1407 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0216 +/-0.043 0.0698 0.400 pCi/g HAKB 11/06/19 0922 1929695 3 Plutonium-239/240 HUh 0.00537 +/-0.0299 0.0572 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -0.71 +/-2.66 4.58 5.00 pCi/g HAKB 11/09/19 0453 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 HUh 0.790 +/-1.61 1.85 5.00 pCi/g TXJl 10/30/19 0732 1931847 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 HUh -0.00991 +/-0.0244 0.0436 1.00 pCi/g MXR.1 10/30/19 2007 1929624 6 Cobalt-60 HUh -0.0119 +/-0.0357 0.0682 pCi/g Europium-152 HUh 0.0185 +/-0.085 0.158 pCi/g Europium-154 HUh -0.0397 +/-0.0855 0.151 pCi/g Europium-155 HUh 0.0322 +/-0.121 0.245 pCi/g Niobium-94 HUh 0.00172 +/-0.0225 0.0424 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 HUh -0.0186 +/-0.0688 0.136 0.400 pCi/g JXC9 11/07/19 0654 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU 6.63 +/-5.88 9.76 10.0 pCi/g EW3 10/29/19 0019 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 0.791 +/-1.54 2.62 5.00 pCi/g TXP3 11/10/19 1745 1934551 9 Liquid Scint Tc99, Solid "As Received" Tecbnetium-99 HU 0.117 +/-0.461 0.809 2.00 pCi/g JJ3 11/05/19 2312 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 HUh -8.13 +/-10.8 16.8 10.0 pCi/g RPI 11/01/19 1112 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 6 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-004-SS Project: ENRG07001 Sample ID: 493624002 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 lillh -0.325 +/-1.16 2.04 5.00 pCi/g RPI 10/30/19 1308 1931689 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 45.5 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 29.7 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 77.2 (15%-125%) Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 72.9 (15%-125%) Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 72.9 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 106 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 75.1 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 95.4 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 23.8 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 101 (25%-125%) Notes: Page 7 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RAGS-004-SS Project: ENRG07001 Sample ID: 493624002 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 8 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-004-SS Project: ENRG07001 Sample ID: 493624003 Client ID: ENRG070 Matrix: Soil Collect Date: 14-OCT-16 09:02 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 lillh 0.00515 +/-0.0286 0.0549 0.400 pCi/g HAKB 11/11/19 2243 1929693 Americium-243 lillh 0.0273 +/-0.0467 0.0409 0.400 pCi/g Curium-243/244 lillh 0.0083 +/-0.0311 0.0524 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 lillh 0.00372 +/-0.00542 0.00881 0.010 pCi/g HAKB 11/11/19 1407 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 lillh 0.00351 +/-0.0367 0.0765 0.400 pCi/g HAKB 11/06/19 0922 1929695 3 Plutonium-239/240 lillh 0.0186 +/-0.0427 0.0677 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 lillh -2.96 +/-3.25 5.69 5.00 pCi/g HAKB 11/09/19 0654 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 lillh -1.19 +/-1.81 3.10 5.00 pCi/g TXJl 10/30/19 0732 1931847 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 Hh 0.165 +/-0.0676 0.0583 1.00 pCi/g MXR.1 10/30/19 2007 1929624 6 Cobalt-60 lillh 0.00774 +/-0.0495 0.104 pCi/g Europium-152 lillh 0.00852 +/-0.0674 0.143 pCi/g Europium-154 lillh -0.0312 +/-0.128 0.242 pCi/g Europium-155 lillh 0.0809 +/-0.0975 0.216 pCi/g Niobium-94 lillh 0.0112 +/-0.0238 0.0472 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 lillh -0.0302 +/-0.0603 0.125 0.400 pCi/g JXC9 11/06/19 1419 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU 2.06 +/-5.54 9.58 10.0 pCi/g EW3 10/29/19 0111 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 1.88 +/-1.91 3.20 5.00 pCi/g TXP3 11/08/19 1914 1934551 9 Liquid Scint Tc99, Solid "As Received" Tecbnetium-99 HU 0.210 +/-0.757 1.32 2.00 pCi/g JJ3 11/05/19 2354 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 lillh -3.06 +/-10.9 16.7 10.0 pCi/g RPI 11/01/19 1316 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 9 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-004-SS Project: ENRG07001 Sample ID: 493624003 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 lillh -0.265 +/-1.50 2.64 5.00 pCi/g RPI 10/30/19 1324 1931689 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 63.2 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 38.5 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 67 (15%-125%) Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 58.2 (15%-125%) Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 58.2 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 84.1 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 90.6 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 83.5 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 24.3 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 77.5 (25%-125%) Notes: Page 10 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-004-SS Project: ENRG07001 Sample ID: 493624003 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 11 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-007-SS Project: ENRG07001 Sample ID: 493624004 Client ID: ENRG070 Matrix: Soil Collect Date: 24-OCT-16 09:05 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 lillh 0.0113 +/-0.0385 0.0714 0.400 pCi/g HAKB 11/06/19 0953 1929693 Americium-243 lillh 0.0127 +/-0.0397 0.0744 0.400 pCi/g Curium-243/244 lillh -0.00764 +/-0.0449 0.107 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 lillh 0.00296 +/-0.00441 0.00677 0.010 pCi/g HAKB 11/11/19 1407 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 lillh 0.0131 +/-0.0504 0.0977 0.400 pCi/g HAKB 11/07/19 0836 1929695 3 Plutonium-239/240 lillh -0.0113 +/-0.0263 0.0779 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 lillh -3.33 +/-2.87 5.04 5.00 pCi/g HAKB 11/09/19 0856 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 lillh 0.384 +/-1.43 2.69 5.00 pCi/g TXJl 10/30/19 0901 1931847 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 Hh 0.174 +/-0.128 0.107 1.00 pCi/g MXR.1 10/30/19 2008 1929624 6 Cobalt-60 lillh 0.010 +/-0.0701 0.154 pCi/g Europium-152 lillh -0.0434 +/-0.125 0.241 pCi/g Europium-154 lillh 0.0975 +/-0.198 0.446 pCi/g Europium-155 lillh 0.184 +/-0.157 0.316 pCi/g Niobium-94 lillh -0.0248 +/-0.0531 0.0943 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 lillh -0.0921 +/-0.0818 0.172 0.400 pCi/g JXC9 11/06/19 1419 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU -0.242 +/-5.47 9.57 10.0 pCi/g EW3 10/30/19 0546 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 1.60 +/-1.86 3.13 5.00 pCi/g TXP3 11/08/19 2000 1934551 9 Liquid Scint Tc99, Solid "As Received" Tecbnetium-99 HU 0.0756 +/-0.755 1.33 2.00 pCi/g JJ3 11/06/19 0037 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 lillh -2.34 +/-9.51 14.1 10.0 pCi/g RPI 11/01/19 1519 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 12 of72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-007-SS Project: ENRG07001 Sample ID: 493624004 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 lillh -0.239 +/-1.48 2.61 5.00 pCi/g RPI 10/30/19 1340 1931689 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 57.8 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 55.4 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 61.1 (15%-125%) Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 67.4 (15%-125%) Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 67.4 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 77.8 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 79.7 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 33.8 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 75.7 (25%-125%) Notes: Page 13 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-RBGS-007-SS Project: ENRG07001 Sample ID: 493624004 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 14 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A0 1-SS NE Project: ENRG07001 Sample ID: 493624005 Client ID: ENRG070 Matrix: Soil Collect Date: 04-MAY-17 08:25 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 lillh 0.00418 +/-0.0437 0.0913 0.400 pCi/g HAKB 11/06/19 0953 1929693 Americium-243 lillh 0.0805 +/-0.113 0.180 0.400 pCi/g Curium-243/244 lillh 0.0123 +/-0.046 0.0774 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 lillh 0.0027 +/-0.0048 0.00826 0.010 pCi/g HAKB 11/11/19 1407 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 lillh 0.00535 +/-0.0297 0.057 0.400 pCi/g HAKB 11/07/19 0919 1929695 3 Plutonium-239/240 lillh 0.00565 +/-0.0365 0.0746 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 lillh -1.69 +/-2.64 4.58 5.00 pCi/g HAKB 11/09/19 1057 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 lillh -0.319 +/-1.80 3.04 5.00 pCi/g TXJl 10/30/19 0902 1931847 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 lillh -0.0202 +/-0.0335 0.062 1.00 pCi/g MXR.1 10/31/19 1914 1929624 6 Cobalt-60 lillh -0.000764 +/-0.0486 0.105 pCi/g Europium-152 lillh -0.0349 +/-0.0944 0.189 pCi/g Europium-154 lillh 0.0419 +/-0.107 0.261 pCi/g Europium-155 lillh 0.0633 +/-0.0849 0.189 pCi/g Niobium-94 lillh -0.0074 +/-0.0313 0.0606 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 lillh -0.0141 +/-0.058 0.117 0.400 pCi/g JXC9 11/06/19 1419 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU 3.03 +/-5.68 9.73 10.0 pCi/g EW3 10/29/19 0406 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 2.67 +/-1.65 2.70 5.00 pCi/g TXP3 11/08/19 2047 1934551 9 Liquid Scint Tc99, Solid "As Received" Tecbnetium-99 HU 0.468 +/-0.587 0.992 2.00 pCi/g JJ3 11/06/19 0235 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 lillh -2.65 +/-8.40 12.7 10.0 pCi/g RPI 11/01/19 1723 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 15 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A0 1-SS NE Project: ENRG07001 Sample ID: 493624005 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 lillh 0.190 +/-1.16 2.01 5.00 pCi/g RPI 10/30/19 1357 1931689 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-0l-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 40 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 32.4 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 89.7 (15%-125%) Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 71.9 (15%-125%) Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 71.9 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 98 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 95.2 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 28.8 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 101 (25%-125%) Notes: Page 16 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A0 1-SS NE Project: ENRG07001 Sample ID: 493624005 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 17 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A03-SS SW Project: ENRG07001 Sample ID: 493624006 Client ID: ENRG070 Matrix: Soil Collect Date: 04-MAY-17 09:30 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 lillh -0.00883 +/-0.0399 0.101 0.400 pCi/g HAKB 11/06/19 0953 1929693 Americium-243 lillh 0.00791 +/-0.0933 0.197 0.400 pCi/g Curium-243/244 lillh -0.00337 +/-0.0291 0.0673 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 lillh 0.00226 +/-0.004 0.00662 0.010 pCi/g HAKB 11/11/19 1407 1929694 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 lillh -0.0135 +/-0.0384 0.0935 0.400 pCi/g HAKB 11/06/19 0953 1929695 3 Plutonium-239/240 lillh 0.00711 +/-0.0355 0.071 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 lillh -1.48 +/-2.38 4.14 5.00 pCi/g HAKB 11/09/19 1258 1929696 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 lillh 0.850 +/-0.613 1.77 5.00 pCi/g TXJl 10/30/19 0902 1931847 5 Gamma, Cs 137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 lillh -0.0164 +/-0.0249 0.0423 1.00 pCi/g MXR.1 11/01/19 0622 1929624 6 Cobalt-60 lillh 0.00904 +/-0.0233 0.0583 pCi/g Europium-152 lillh 0.123 +/-0.0925 0.150 pCi/g Europium-154 lillh -0.097 +/-0.081 0.110 pCi/g Europium-155 lillh 0.0555 +/-0.0883 0.181 pCi/g Niobium-94 lillh 0.0103 +/-0.0227 0.049 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 lillh -0.0582 +/-0.055 0.122 0.400 pCi/g JXC9 11/06/19 1419 1933651 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium HU 3.85 +/-5.29 8.96 10.0 pCi/g EW3 10/29/19 0458 1929721 8 Liquid Scint C14, Solid "As Received" Carbon-14 HU 1.65 +/-1.66 2.79 5.00 pCi/g TXP3 11/10/19 1832 1934551 9 Liquid Scint Tc99, Solid "As Received" Tecbnetium-99 HU -0.11 +/-1.09 1.95 2.00 pCi/g JJ3 11/06/19 0317 1929739 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 lillh -1.18 +/-6.18 8.97 10.0 pCi/g RPI 11/01/19 1927 1931683 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 18 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A03-SS SW Project: ENRG07001 Sample ID: 493624006 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 lillh -0.546 +/-1.17 2.08 5.00 pCi/g RPI 10/30/19 1413 1931689 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 42.8 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 27.2 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 69.5 (15%-125%) Plutonium-242 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 80 (15%-125%) Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 80 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 98.4 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 95 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 63.8 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 43.4 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 96.5 (25%-125%) Notes: Page 19 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-IJGS-A03-SS SW Project: ENRG07001 Sample ID: 493624006 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 20 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: S3-012-109B-FJGS-062-SM Project: ENRG07001 Sample ID: 493624007 Client ID: ENRG070 Matrix: Soil Collect Date: 22-AUG-19 10:05 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0139 +/-0.0617 0.113 0.400 pCi/g JXC9 11/06/19 1419 1933651 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 110 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 21 of72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: S3-012-109B-FJGS-063-SM Project: ENRG07001 Sample ID: 493624008 Client ID: ENRG070 Matrix: Soil Collect Date: 22-AUG-19 10:14 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.00923 +/-0.0636 0.121 0.400 pCi/g JXC9 11/06/19 1419 1933651 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 104 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 22 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: S3-012-109B-FJGS-064-SM Project: ENRG07001 Sample ID: 493624009 Client ID: ENRG070 Matrix: Soil Collect Date: 22-AUG-19 13:12 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0355 +/-0.0445 0.0974 0.400 pCi/g JXC9 11/06/19 1419 1933651 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 104 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 23 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-011-101-FSGS-013-SS Project: ENRG07001 Sample ID: 493624010 Client ID: ENRG070 Matrix: Soil Collect Date: 20-SEP-19 10:43 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0706 +/-0.085 0.144 0.400 pCi/g JXC9 11/06/19 1419 1933651 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 97.2 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 24 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-011-104-FSGS-001-SS Project: ENRG07001 Sample ID: 493624011 Client ID: ENRG070 Matrix: Soil Collect Date: 09-SEP-19 14:08 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0354 +/-0.0446 0.096 0.400 pCi/g JXC9 11/06/19 1419 1933651 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 113 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 25 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-011-104-FSGS-010-SS Project: ENRG07001 Sample ID: 493624012 Client ID: ENRG070 Matrix: Soil Collect Date: 09-SEP-19 14:46 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0194 +/-0.0367 0.0792 0.400 pCi/g JXC9 11/07/19 0654 1933651 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 97.2 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 26 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-FSGS-004-SS Project: ENRG07001 Sample ID: 493624013 Client ID: ENRG070 Matrix: Soil Collect Date: 05-SEP-19 08:58 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.112 +/-0.084 0.133 0.400 pCi/g JXC9 11/06/19 1419 1933651 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 92.8 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 27 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-109-FSGS-005-SS Project: ENRG07001 Sample ID: 493624014 Client ID: ENRG070 Matrix: Soil Collect Date: 24-SEP-19 08:05 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0801 +/-0.0672 0.107 0.400 pCi/g JXC9 11/06/19 1419 1933651 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 28 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-109-FSGS-006-SS Project: ENRG07001 Sample ID: 493624015 Client ID: ENRG070 Matrix: Soil Collect Date: 24-SEP-19 10:36 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0454 +/-0.038 0.0913 0.400 pCi/g JXC9 11/06/19 1419 1933651 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 104 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 29 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-109-FSGS-011-SS Project: ENRG07001 Sample ID: 493624016 Client ID: ENRG070 Matrix: Soil Collect Date: 23-SEP-19 14:09 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0482 +/-0.0493 0.111 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 92.8 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 30 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-107-FSGS-008-SS Project: ENRG07001 Sample ID: 493624017 Client ID: ENRG070 Matrix: Soil Collect Date: 08-AUG-19 15:00 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0295 +/-0.0766 0.151 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 84 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 31 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-101-FSGS-015-SS Project: ENRG07001 Sample ID: 493624018 Client ID: ENRG070 Matrix: Soil Collect Date: 08-AUG-19 15:12 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0436 +/-0.0544 0.118 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 32 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-102-FSGS-007-SS Project: ENRG07001 Sample ID: 493624019 Client ID: ENRG070 Matrix: Soil Collect Date: 14-AUG-19 15:18 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0969 +/-0.0724 0.155 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 33 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-103-FSGS-005-SS Project: ENRG07001 Sample ID: 493624020 Client ID: ENRG070 Matrix: Soil Collect Date: 14-AUG-19 10:13 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0229 +/-0.0522 0.109 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1024 1929602 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 90.6 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 34 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-104-FSGS-016-SS Project: ENRG07001 Sample ID: 493624021 Client ID: ENRG070 Matrix: Soil Collect Date: 23-AUG-19 09:57 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0967 +/-0.087 0.141 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 79.6 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 35 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-010-105-FSGS-007-SS Project: ENRG07001 Sample ID: 493624022 Client ID: ENRG070 Matrix: Soil Collect Date: 23-AUG-19 13:29 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0341 +/-0.0859 0.154 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 79.6 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 36 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-011-101-FSGS-005-SS Project: ENRG07001 Sample ID: 493624023 Client ID: ENRG070 Matrix: Soil Collect Date: 20-SEP-19 14:01 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0135 +/-0.0736 0.141 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 37 of72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-011-104-FSGS-011-SS Project: ENRG07001 Sample ID: 493624024 Client ID: ENRG070 Matrix: Soil Collect Date: 09-SEP-19 14:52 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.058 +/-0.0508 0.117 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.4 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 38 of72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-101-FSGS-005-SS Project: ENRG07001 Sample ID: 493624025 Client ID: ENRG070 Matrix: Soil Collect Date: 05-SEP-19 13:00 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0836 +/-0.0864 0.144 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 102 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 39 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-109-FSGS-014-SS Project: ENRG07001 Sample ID: 493624026 Client ID: ENRG070 Matrix: Soil Collect Date: 23-SEP-19 14:21 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0202 +/-0.0604 0.110 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 97.2 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 40 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-109-FSGS-017-SS Project: ENRG07001 Sample ID: 493624027 Client ID: ENRG070 Matrix: Soil Collect Date: 24-SEP-19 13:52 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0116 +/-0.0446 0.0829 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 115 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 41 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-PAD-GR5-AJGS-006-SS Project: ENRG07001 Sample ID: 493624028 Client ID: ENRG070 Matrix: Soil Collect Date: 12-JUL-19 12:22 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0456 +/-0.0691 0.119 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 104 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 42 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: November 14, 2019 Company: LaCrosseSolutions Address: S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: Ll-PAD-GRl0-AJGS-007-SS Project: ENRG07001 Sample ID: 493624029 Client ID: ENRG070 Matrix: Soil Collect Date: 13-JUL-19 13:48 Receive Date: 21-OCT-19 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0349 +/-0.0546 0.0954 0.400 pCi/g JXC9 11/06/19 1526 1933654 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXB7 10/22/19 1034 1929603 The following Analytical Methods were performed: Method Description Analyst Comments EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 97.2 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Le/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 43 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC SummaIT Report Date: November 14, 2019 LaCrosseSolutions Page 1 of 7 S4601 State Hwy 35 Genoa, Wisconsin
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Mr. Jason Q. Spaide Workorder: 493624 Parmname NOM Sam~le Qual QC Units RPO% REC% Range Anlst Date Time Rad Alpha Spec Batch 1929693 QC1204411092 493624001 DUP Americium-241 lillh 0.0084 HU 0.0166 pCi/g NIA NIAHAKB 11/06/19 09:53 Uncertainty +l-0.0467 +l-0.0457 Americium-243 lillh 0.0346 HU -0.012 pCi/g NIA NIA Uncertainty +l-0.0974 +l-0.0532 Curium-2431244 lillh -0.00429 HU -0.0069 pCi/g NIA NIA Uncertainty +l-0.037 +l-0.0305 QC1204411093 LCS Americium-241 1.92 1.99 pCi/g 104 (75%-125%) 11/07/19 09:18 Uncertainty +l-0.348 Americium-243 u 0.00469 pCi/g (75%-125%) Uncertainty +l-0.0491 Curium-2431244 2.26 2.33 pCi/g 103 (75%-125%) Uncertainty +l-0.373 QC1204411091 MB Americium-241 u 0.014 pCi/g 11/06/19 09:53 Uncertainty +l-0.0279 Americium-243 u 0.0163 pCi/g Uncertainty +l-0.0371 Curium-2431244 u 0.00352 pCi/g Uncertainty +l-0.0196 Batch 1929694 QC1204411095 493624003 DUP Neptunium-237 lillh 0.00372 HU 0.00341 pCi/g NIA NIAHAKB 11/11/19 14:07 Uncertainty +l-0.00542 +l-0.00442 QC1204411096 LCS Neptunium-237 0.869 1.01 pCi/g 116 (75%-125%) 11/11/19 14:07 Uncertainty +l-0.0485 QC1204411094 MB Neptunium-237 u -0.000288 pCi/g 11/11/19 14:07 Uncertainty +l-0.00229 Page 44 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC SummaIT Workorder: 493624 Page 2 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1929695 QC120441 I098 493624001 DUP Plutonium-23 8 HUh 0.00487 HU 0.0052 pCi/g NIA NIAHAKB 11/06/19 09:53 Uncertainty +l-0.0271 +/-0.0366 Plutonium-2391240 HUh -0.00402 HU -0.00169 pCi/g NIA NIA Uncertainty +l-0.0278 +/-0.0254 QC1204411099 LCS Plutonium-238 u -0.00294 pCi/g 11/06/19 09:53 Uncertainty +/-0.0203 Plutonium-2391240 1.96 2.06 pCi/g 105 (75%-125%) Uncertainty +l-0.231 QC1204411097 MB Plutonium-238 u 0.00862 pCi/g 11/06/19 09:53 Uncertainty +/-0.0295 Plutonium-2391240 u 0.00663 pCi/g Uncertainty +/-0.0297 Batch 1929696 QC1204411101 493624001 DUP Plutonium-241 HUh -1.25 HU -2.36 pCi/g NIA NIAHAKB 11/09/19 17 :00 Uncertainty +l-2.38 +l-2.42 QC1204411102 LCS Plutonium-241 162 155 pCi/g 95.5 (75%-125%) 11/09/19 19:02 Uncertainty +l-4.78 QC1204411100 MB Plutonium-241 u -0.546 pCi/g 11/09/19 14:59 Uncertainty +l-1.98 Rad Gamma Spec Batch 1929624 QC1204410975 493624001 DUP Cesium-137 Hh 0.113 H 0.0865 pCi/g 26.4 (0% - 100%) MXRl 11/01/19 06:24 Uncertainty +l-0.0594 +/-0.0561 Cobalt-60 HUh 0.036 HU 0.0428 pCi/g NIA NIA Uncertainty +l-0.0349 +/-0.0446 Europium-152 HUh -0.00616 HU 0.070 pCi/g NIA NIA Uncertainty +l-0.0669 +l-0.0644 Page 45 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC SummaIT Workorder: 493624 Page 3 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1929624 Europium-154 HUh -0.0128 HU -0.0196 pCi/g NIA NIAMXRl 11/01/19 06:24 Uncertainty +l-0.0717 +l-0.109 Europium-155 HUh 0.0587 HU 0.0597 pCi/g NIA NIA Uncertainty +l-0.0622 +l-0.088 Niobium-94 HUh 0.0376 HU -0.0216 pCi/g NIA NIA Uncertainty +l-0.0275 +l-0.0246 QC1204410976 LCS Americium-241 487 512 pCi/g 105 (75%-125%) 11/01/19 06:24 Uncertainty +l-6.27 Cesium-137 167 166 pCi/g 99.4 (75%-125%) Uncertainty +l-3.92 Cobalt-60 107 106 pCi/g 98.5 (75%-125%) Uncertainty +l-3.73 Europium-152 u -1.13 pCi/g Uncertainty +l-1.44 Europium-154 u -0.069 pCi/g Uncertainty +l-1.07 Europium-155 u -1.32 pCi/g Uncertainty +l-1.03 Niobium-94 u -0.276 pCi/g Uncertainty +l-0.508 QC1204410974 MB Cesium-137 u 0.00323 pCi/g 11/01/19 06:23 Uncertainty +/-0.0103 Cobalt-60 u 0.0164 pCi/g Uncertainty +l-0.0236 Europium-152 u 0.0135 pCi/g Uncertainty +l-0.0399 Europium-154 u 0.0106 pCi/g Uncertainty +l-0.0612 Europium-155 u -0.00293 pCi/g Uncertainty +l-0.0231 Page 46 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC SummaIT Workorder: 493624 Page 4 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1929624 Niobium-94 u 0.00978 pCi/g MXRl 11/01/19 06:23 Uncertainty +l-0.020 Batch 1931847 QC1204415727 493624001 DUP Nickel-59 lillh -0.18 HU -0.803 pCi/g NIA NIA TXJl 10130/19 10:43 Uncertainty +l-1.68 +l-1.60 QC1204415728 LCS Nickel-59 90.3 73.2 pCi/g 81.1 (75%-125%) 10130/19 10:44 Uncertainty +l-6.52 QC1204415726 MB Nickel-59 u -0.45 pCi/g 10130/19 10:43 Uncertainty +l-1.04 Rad Gas Flow Batch 1933651 QC1204420255 493624005 DUP Strontium-90 lillh -0.0141 HU -0.134 pCi/g NIA NIA JXC9 11/06/19 14:18 Uncertainty +l-0.058 +l-0.105 QC1204420256 LCS Strontium-90 5.40 4.94 pCi/g 91.4 (75%-125%) 11/06/19 14:20 Uncertainty +l-0.313 QC1204420254 MB Strontium-90 u -0.00246 pCi/g 11/06/19 14:18 Uncertainty +/-0.0478 Batch 1933654 QC1204420263 493624025 DUP Strontium-90 u 0.0836 u 0.0226 pCi/g NIA NIA JXC9 11/06/19 15:26 Uncertainty +l-0.0864 +l-0.0608 QC1204420264 LCS Strontium-90 5.51 6.75 pCi/g 122 (75%-125%) 11/07/19 06:45 Uncertainty +l-0.356 QC1204420262 MB Strontium-90 u -0.02 pCi/g 11/06/19 15:26 Uncertainty +l-0.0423 Page 4 7 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC SummaIT Workorder: 493624 Page 5 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1929721 QC1204411179 493624001 DUP Tritium HU 1.65 HU -3.61 pCi/g NIA NIA EW3 10130/19 06:58 Uncertainty +l-5.62 +l-5.09 QC1204411181 LCS Tritium 142 152 pCi/g 107 (75%-125%) 10129/19 07:49 Uncertainty +l-17.1 QC 1204411178 MB Tritium u 0.00583 pCi/g 10/29/19 05:50 Uncertainty +l-4.35 QC1204411180 493624001 MS Tritium 171 HU 1.65 H 138 pCi/g 80.3 (75%-125%) 10/29/19 07:33 Uncertainty +l-5.62 +l-17.9 Batch 1929739 QC1204411223 493624001 DUP Technetium-99 HU -0.00734 HU 0.523 pCi/g NIA NIA JJ3 11/06/19 04:42 Uncertainty +l-0.483 +l-0.575 QC 1204411224 LCS Technetium-99 38.8 37.5 pCi/g 96.7 (75%-125%) 11/06/19 05 :25 Uncertainty +l-2.62 QC1204411222 MB Technetium-99 u 0.488 pCi/g 11/06/19 04:00 Uncertainty +l-0.492 Batch 1931683 QC1204415380 493624001 DUP lron-55 HUh -1.57 HU -9.54 pCi/g NIA NIA RPl 11/01/19 21:31 Uncertainty +l-12.1 +l-8.16 QC1204415381 LCS Iron-55 75.4 73.8 pCi/g 97.8 (75%-125%) 10131/19 18:25 Uncertainty +l-4.98 QC1204415379 MB Iron-55 u 2.24 pCi/g 10131/19 16:19 Uncertainty +l-3.57 Page 48 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC SummaIT Workorder: 493624 Page 6 of 7 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1931689 QC1204415395 493624001 DUP Nickel-63 HUh -0.424 HU -0.114 pCi/g NIA NIA RPI 10130/19 14:46 Uncertainty +l-1.17 +l-1.26 QC1204415396 LCS Nickel-63 70.5 60.2 pCi/g 85.4 (75%-125%) 10130/19 15:03 Uncertainty +l-3.12 QC1204415394 MB Nickel-63 u -0.312 pCi/g 10130/19 14:30 Uncertainty +l-1.36 Batch 1934551 QC1204422492 493624001 DUP Carbon-14 HU 1.92 HU 1.76 pCi/g NIA NIA TXP3 11/08/19 22:21 Uncertainty +l-1.76 +l-1.72 QC1204422494 LCS Carbon-14 128 125 pCi/g 97.6 (75%-125%) 11/08/19 23:55 Uncertainty +l-3.84 QC1204422491 MB Carbon-14 u 1.00 pCi/g 11/09/19 12:08 Uncertainty +l-1.18 QC1204422493 493624001 MS Carbon-14 150 HU 1.92 H 146 pCi/g 97.3 (75%-125%) 11/08/19 23 :08 Uncertainty +l-1.76 +l-4.51 Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). The Qualifiers in this report are defined as follows:
** Analyte is a Tracer compound < Result is less than value reported > Result is greater than value reported BD Results are either below the MDC or tracer recovery is low FA Failed analysis.
H Analytical holding time was exceeded J See case narrative for an explanation J Value is estimated K Analyte present. Reported value may be biased high. Actual value is expected to be lower. L Analyte present. Reported value may be biased low. Actual value is expected to be higher. Page 49 of 72 SDG: 493624
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 493624 Page 7 of 7 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time M M if above MDC and less than LLD M REMP Result> MDC/CL and< RDL NIA RPD or %Recovery limits do not apply. Nl See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER. R Sample results are rejected u Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD. UI Gamma Spectroscopy--Uncertain identification UJ Gamma Spectroscopy--Uncertain identification UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier y Other specific qualifiers were required to properly define the results. Consult case narrative. I\ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. h Preparation or preservation holding time was exceeded NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable.
/\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/- the RL is used to evaluate the DUP result.
- Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 50 of 72 SDG: 493624
Radiochemistry Technical Case Narrative LaCrosseSolutions, LLC SDG #: 493624 Product: Alphaspec Isotopic Am241 Am243, Cm243/244, Solid Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 27 Analytical Batch: 1929693 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411091 Method Blank (MB) 1204411092 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204411093 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204411092 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-l 7 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 pfJc ~eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Recounts The Am-243 traced portion of sample 493624003 (L3-012-101-RBGS-004-SS) was recounted due to a suspected false positive. The recount is reported. Product: Alphaspec Np, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-032 REV# 22 Analytical Batch: 1929694 Preparation Method : Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411094 Method Blank (MB) 1204411095 493624003(L3-012-101-RBGS-004-SS) Sample Duplicate (DUP) 1204411096 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204411095 (L3-012-10 l-RBGS-004-SSDUP) Received 21-OCT-19, out of holding 12-APR-l 7 493624001 (L3-012-10 l-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-10 l-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 2 l-OCT-19, out of holding 31-OCT-17 pfJc ~eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
1493624006 (L4-OFF-SOL-IJGS-A03-SS SW) IReceived21-0CT-19, out ofholding 31-0CT-171 Product: Alphaspec Pu238, 239/240, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 27 Analytical Batch: 1929695 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411097 Method Blank (MB) 1204411098 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204411099 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204411098 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out ofholding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out ofholding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-l 7 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 pfJc ~eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Recounts Samples 493624004 (L3-012-101-RBGS-007-SS) and 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) were recounted due to a peak shift. The recounts are reported. Miscellaneous Information Additional Comments The tracer peak centroid for sample 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) is greater than 50 keV from the expected library energy value for the tracer; however, the tracer yield requirement was met and the tracer peak is within the tracer region of interest. Product: Dry Weight Preparation Method : Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 493624007 S3-012-109B-FJGS-062-SM 493624008 S3-012-109B-FJGS-063-SM 493624009 S3-012-109B-FJGS-064-SM 493624010 L2-0l l-101-FSGS-013-SS 493624011 L2-0l l-104-FSGS-001-SS 493624012 L2-0l l-104-FSGS-010-SS 493624013 L3-012-101-FSGS-004-SS 493624014 L3-012-109-FSGS-005-SS 493624015 L3-012-109-FSGS-006-SS 493624016 L3-012-109-FSGS-0l l-SS 493624017 Ll-010-107-FSGS-008-SS 493624018 Ll-010-101-FSGS-015-SS 493624019 Ll-010-102-FSGS-007-SS 493624020 Ll-010-103-FSGS-005-SS The samples in this SDG were analyzed on an "as received" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. pfJc ~eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Product: Dry Weight Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929603 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624021 Ll-010-104-FSGS-016-SS 493624022 Ll-010-105-FSGS-007-SS 493624023 L2-011-101-FSGS-005-SS 493624024 L2-011-104-FSGS-011-SS 493624025 L3-012-101-FSGS-005-SS 493624026 L3-012-109-FSGS-014-SS 493624027 L3-012-109-FSGS-017-SS 493624028 L 1-PAD-GR5-AJGS-006-SS 493624029 Ll-PAD-GRl0-AJGS-007-SS The samples in this SDG were analyzed on an "as received" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 Analytical Method: DOE HASL 300, 4.5.2.3/Ga-01-R Analytical Procedure: GL-RAD-A-013 REV# 27 Analytical Batch: 1929624 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204410974 Method Blank (MB) 1204410975 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204410976 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. pfJc ~eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204410975 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out ofholding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out ofholding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-l 7 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-l 7 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Product: Gamma Ni59, Solid Analytical Method: DOE RESL Ni-1 Analytical Procedure: GL-RAD-A-022 REV# 19 Analytical Batch : 1931847 Preparation Method : Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204415726 Method Blank (MB) 1204415727 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204415728 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. pfJc ~eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204415727 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out ofholding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out ofholding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-l 7 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-l 7 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Product: GFPC, Sr90, Solid Analytical Method: EPA 905 .0 Modified/DOE RP501 Rev. 1 Modified Analytical Procedure: GL-RAD-A-004 REV# 21 Analytical Batch : 1933651 Preparation Method : Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 493624007 S3-012-109B-FJGS-062-SM 493624008 S3-012-109B-FJGS-063-SM 493624009 S3-012-l 09B-FJGS-064-SM 493624010 L2-011-101-FSGS-013-SS 493624011 L2-0l 1-104-FSGS-001-SS 493624012 L2-011-104-FSGS-010-SS 493624013 L3-012-101-FSGS-004-SS pfJc ~eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
493624014 L3-012-109-FSGS-005-SS 493624015 L3-012-109-FSGS-006-SS 1204420254 Method Blank (MB) 1204420255 493624005(L4-OFF-SOL-IJGS-A01-SS NE) Sample Duplicate (DUP) 1204420256 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204420255 (L4-OFF-SOL-IJGS-A01-SS NEDUP) Received 2 l-OCT-19, out of holding 3 l-OCT-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-l 7 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-l 7 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-l 7 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT- l 9, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT- l 9, out of holding 3 l-OCT-17 Recounts Samples 493624002 (L3-012-101-RAGS-004-SS) and 493624012 (L2-011-104-FSGS-010-SS) were recounted due to results more negative than the three sigma TPU. The second counts are reported. Product: GFPC, Sr90, Solid Analytical Method: EPA 905 .0 Modified/DOE RP501 Rev. 1 Modified Analytical Procedure: GL-RAD-A-004 REV# 21 Analytical Batch: 1933654 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batches: 1929602 and 1929603 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624016 L3-012-109-FSGS-0l l-SS 493624017 Ll-010-107-FSGS-008-SS pfJc ~eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
493624018 Ll-010-101-FSGS-015-SS 493624019 Ll-010-102-FSGS-007-SS 493624020 Ll-010-103-FSGS-005-SS 493624021 Ll-010-104-FSGS-016-SS 493624022 Ll-010-105-FSGS-007-SS 493624023 L2-0ll-101-FSGS-005-SS 493624024 L2-0l l-104-FSGS-0l l-SS 493624025 L3-012-10 l-FSGS-005-SS 493624026 L3-012-109-FSGS-014-SS 493624027 L3-012-109-FSGS-0l 7-SS 493624028 L 1-PAD-GR5-AJGS-006-SS 493624029 Ll-PAD-GRl0-AJGS-007-SS 1204420262 Method Blank (MB) 1204420263 493624025(L3-012-101-FSGS-005-SS) Sample Duplicate (DUP) 1204420264 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Recounts Sample 1204420264 (LCS) was recounted due to high recovery. The recount is reported. Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 21 Analytical Batch : 1929696 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411100 Method Blank (MB) 1204411101 49362400l(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204411102 Laboratory Control Sample (LCS) pfJc ~eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information RDLMet Sample (see below) did not meet the detection limit due to a lower sample yield. The client yield requirement was met. The sample was counted the maximum count time in order to achieve the lowest possible MDAs. Sample Analyte Value 493624003 (L3-012-101-RBGS-004-SS) Plutonium-241 Result -2.96 < MDA 5.69 > RDL 5 pCi/g Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204411101 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Miscellaneous Information Additional Comments The tracer peak centroid for sample 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) is greater than 50 keV from the expected library energy value for the tracer; however, the tracer yield requirement was met and the tracer peak is within the tracer region of interest. Product: LSC, Tritium Distillation, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 23 Analytical Batch: 1929721 pfJc '6WeflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411178 Method Blank (MB) 1204411179 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204411180 493624001(L3-012-101-RAGS-002-SS) Matrix Spike (MS) 1204411181 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204411179 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 1204411180 (L3-012-101-RAGS-002-SSMS) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Recounts Samples 1204411179 (L3-012-101-RAGS-002-SSDUP) and 493624004 (L3-012-101-RBGS-007-SS) were recounted due to high MDCs. The recounts are reported. Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 5 Analytical Batch: 1929739 pfJc l@l:JeflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204411222 Method Blank (MB) 1204411223 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204411224 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204411223 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-l 7 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 3 l-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 3 l-OCT-17 Product: Liquid Scint Fe55, Solid Analytical Method: DOE RESL Fe-1, Modified Analytical Procedure: GL-RAD-A-040 REV# 13 Analytical Batch: 1931683 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 pfJc l@J>eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204415379 Method Blank (MB) 1204415380 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204415381 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (OC) Information RDLMet Samples (see below) did not meet the detection limits. Samples were counted the maximum count time in order to achieve the lowest MDAs possible. Sample Analyte Value 1204415380 (L3-012-101-RAGS-002-SSDUP) lron-55 Result -9.54 < MDA 12.4 > RDL 10 pCi/g 493624001 (L3-012-101-RAGS-002-SS) lron-55 Result-1.57 < MDA 18.7 > RDL 10 pCi/g 493624002 (L3-012-101-RAGS-004-SS) lron-55 Result-8.13 < MDA 16.8 > RDL 10 pCi/g 493624003 (L3-012-101-RBGS-004-SS) lron-55 Result -3 .06 < MDA 16.7 > RDL 10 pCi/g 493624004 (L3-012-101-RBGS-007-SS) lron-55 Result -2.34 < MDA 14.1 > RDL 10 pCi/g 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Iron-55 Result -2.65 < MDA 12.7 > RDL 10 pCi/g Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204415380 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out ofholding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out ofholding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-l 7 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 pfJc ~eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Recounts Samples 1204415380 (L3-012-101-RAGS-002-SSDUP), 493624001 (L3-012-101-RAGS-002-SS), 493624002 (L3-012-101-RAGS-004-SS), 493624003 (L3-012-101-RBGS-004-SS), 493624004 (L3-012-101-RBGS-007-SS), 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) and 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) were recounted due to high MDCs. The recounts are reported. Product: Liquid Scint Ni63, Solid Analytical Method: DOE RESL Ni-1, Modified Analytical Procedure: GL-RAD-A-022 REV# 19 Analytical Batch: 1931689 Preparation Method : Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 23 Preparation Batch: 1929602 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204415394 Method Blank (MB) 1204415395 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204415396 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204415395 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out of holding 07-MAR-17 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-17 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-17 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-17 pfJc '61J:leflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 21-OCT-19, out of holding 31-OCT-17 Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 16 Analytical Batch: 1934551 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 493624001 L3-012-101-RAGS-002-SS 493624002 L3-012-101-RAGS-004-SS 493624003 L3-012-101-RBGS-004-SS 493624004 L3-012-101-RBGS-007-SS 493624005 L4-OFF-SOL-IJGS-A01-SS NE 493624006 L4-OFF-SOL-IJGS-A03-SS SW 1204422491 Method Blank (MB) 1204422492 493624001(L3-012-101-RAGS-002-SS) Sample Duplicate (DUP) 1204422493 493624001(L3-012-101-RAGS-002-SS) Matrix Spike (MS) 1204422494 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Samples (See Below) were received and analyzed outside the hold time. Sample Value 1204422492 (L3-012-101-RAGS-002-SSDUP) Received 21-OCT-19, out ofholding 07-MAR-17 1204422493 (L3-012-101-RAGS-002-SSMS) Received 21-OCT-19, out of holding 07-MAR-l 7 493624001 (L3-012-101-RAGS-002-SS) Received 21-OCT-19, out of holding 07-MAR-l 7 493624002 (L3-012-101-RAGS-004-SS) Received 21-OCT-19, out of holding 12-MAR-17 493624003 (L3-012-101-RBGS-004-SS) Received 21-OCT-19, out of holding 12-APR-l 7 493624004 (L3-012-101-RBGS-007-SS) Received 21-OCT-19, out of holding 22-APR-l 7 493624005 (L4-OFF-SOL-IJGS-A01-SS NE) Received 21-OCT-19, out of holding 31-OCT-17 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) Received 2 l-OCT-19, out of holding 3 l-OCT-17 pfJc l@eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Recounts Samples 493624002 (L3-012-101-RAGS-004-SS) and 493624006 (L4-OFF-SOL-IJGS-A03-SS SW) were recounted to verify sample results. Recounts are reported. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. pfJc ~eflJWi~ : 49~ 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
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L3-0 .1 2-l0I-RAGS-004-SS L3-012-10 I-RBGS-004-SS L3-0l 2-101-RBGS-007-SS Date Time I. Kevin L Murray _0/16/2019 L3tS-2 2 3 3 For Lab ReceM11g Use 011ly: Custody Seal Intact?_ [ ] Y":5 _[ ] No I.) Ch:iin of Custody Number= Client Determined 2.) QC Codes: N = Nom1al Sample. TB = Trip Blank. FD = Field Duplicate, EB = Equipment Blank, MS= Matrix Spike Sample, MSD = Matrix Spike Duplicate Sample, G = Grab, C = Composite 3.) Field Filtered: For liquid matrices. indicate with a~ Y for yes the sample was field filtered or N ~ for sample \vas not field filtered 4 4 4.) Matrix Codes: DW=Drinlcing Waler, GW=Groundwater, S\V=Surface Water, \VW=Wastc Water, \V=*Water. ML=Misc Liquid, SO=Soil, SO=,Sediment, SL=Sludge, SS=Solid Waste, O=-Oil, F=Filter, P=Wipe, U=Urine, F=Fecal, N=Nasal 5.) Sample Analysis Requested: Analytical method requested (i.e. 82608, 6010Bn 470A) and number of containers provided for each (i .e. 81608
- 3, 60/0IJl74i 0A - l).
6.) Preservativ¢ Type: HA = Hydrochloric Acid, NI= Nitric Acid, SH = Sodium Hydroxide, SA= Sulfuric Acid, AA= Ascorbic Acid, HX =Hexane, ST= Sodium Thiosulfate, Ifno preservative is added= leave field blank
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~::sc1LLC Charleston, SC 29407 r.n COC Number 0 i: Uest Phone:(843)556-8171 l;j PO Number: 672583 Sf!_~f!!_-!JB~iJ!!:~'l!!l.8.._______________________ 2_______2_______Jr~: (8j3) 766-1178 a Client Name: La Crosse Solutions Phone# 608-689-4259
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'-0 Project/Site Name: LACBWR-Gcnoa WI Fax II I I I I I I I I I
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O'I Address: 54601 State Road 35 N
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S3-0 J 2-1 ()913-FJGS:OiiJ-SM S3-0 .12-1 098-FJGS-064-SM L2-0 l re IO FFSGS-013-SS L2-0l l-l 04-FSGS-001-SS L2-0 l l-1 04-FSGS-0l 0-SS L3-0l 2-101-FSGS-004-SS L3-0 12-109-FSGS-005-SS L3-012-109-FSGS-006-SS L3-012-l09-FSGS-0 l l-SS Relinquished By (Signed) Date Time I. Kevin L Murra 0/16/2019 /31.J.,-- 2 2 3 For Lab Receivinc Use Oll_l.v: Custody Seo/ lt,tac/? [ ] Yes [ ] No Cooler'J'_e_mp:~ °C I.) Chain of Custody Number "*' Clit.'l lt Determined 2,) QC Codes: N = Nonna! Sample, TB = Trip Blank, FD,:,:: Field Duplicate, EB = .EquipnlCTlt Bbnk. MS = Matrix Spike Sample, MSD = Matri:-: Spike Duplicate. Sample. G = Grab, C = Composite 3.) Field Filtcnxl: For liquid matrices, indicate with a - Y - fo r yes the sample ,vas field filtered or - N - for sample was not field filtered. 4.) Ma1rix Codes: DW=Drinking Water. GW=Groundwntcr, SW:cc:Surfucc Water, WW=Wastc Water. W=\Vatcr, ML=Misc Liquid. SO"'Soil, SD=Scdirm,'flt, SL=Sludgc, SS=Solid Waste, 0:c-:Oil. F=Filtcr, P:::::Wipc, lJ =Urinc, F=Fcc..1.l, N=Nasal 5.) Sample Analysis Rcqu~ tcd: An.1.1)1ical method requested (i.e. 82608, 60JOB/7470A) .i.nd number of containers provided for each (i.e. 8260B -3. 60/0fli74 70A -1). 6.) Pn.-scrvativc Type: HA ::::: Hydrochloric Acid, NI=-" Nitric Acid, SH .::: Sodium Hydroxide, SA = Sulfuric Acid, AA = Ascorbic Acid. HX = Hex.inc, ST = Sodium Thiosulfatc, lfno preservative is added= leave field blank
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-....J N GEL Quote#: - - - - - - - - - - - - - - < gol.oom Chemistry I Radiochemistry l Radlobioassay I Specialty Annlytlcs Charleston, SC 29407 rfJ coc Number(lt Chain of Custod and Anal ical Re uest Phone: (843) 556-8171 u PO Number: 672583 GEL.Work Orde,:_Number: GEL ProjectMa11ager: ** Fax: (843) 766-1178 0 Client Name: La Crosse Solutions Phone # 608-689-4259
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Project/Site Name: LACBWR-Genoa WI Fax#
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0\ Address: 5460.1 State Road 35
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Ll-0 l 0-1 O1-FJGS~Ol 5"-SS L1-010-102-FSGS-007-SS L1-0 I0-103-FSGS-005-SS L2-0ll-104-FSGS-0lf-SS L3-012-10 t-FSGS-005-SS L3-012-l09-FSGS-0t .4-SS Relinquished By (Signed) Date Time
- l. Kevin L Murray /16/2019 l>tJ Level 4 2
3 3 For Lab Receiving Use 011(v:_ Cus{od}' Seal Intact?_l_l_Yes [ _) No _Cooler Temp: = ° C 1,) Chain of Custody Number "" Client Detem1ined 2.) QC Codes: N = Normal Sample, TB = Trip Blank, FD = Field Duplica.te. EB = Equipment Blank. MS= 1\.fatrix Spike Sample. MSD = Matrix Spike Duplicate Sample, G = Grab. C ~"' Composite 3.) field Filtered: For liquid matrices, indicate ,\1th a- Y - for yes the sample was field filtered or- N - for sample was mlt field filtered. 4.) Matrix Codes: DW"""'Drinking Water, GW=-Grouodwater, S\V=Surface Water. \\1\V0=Waste \Vater, \V==Water. l\-tL=Misc Liquid, SO:c:Soil, SD""Sediment. SL=Sludge. SS=Solid Waste, O=Oil, F=Filter, P=Wipe, U::,;Urine. F=Fecal, N=Na.sal 5.) Sample Analysis .Requested: Analytical method requested (i.e. 8260B, 60JOB/7470A) and number of containers provided for each (i.e. 8260B - 3. 60JOB/J.170A - I}. 6.) Preservative Type: HA = Hydrochloric Acid, NI=- Nitric Acid. SH=, Sodium Hydroxide, SA *="' Sulfuric Acid. AA= Ascorbic Acid, HX =Hexane, ST= Sodium Thiosulfa1e. Ifno preservative is added = leave fidd blank
'"d ~ aI (1) -.....:i L--{9302' 0 Page: _ _ _4_ _ _ of _ _ _4 _ _ , GEL Laboratories, LLC (CJ !I Laboraton es 0 >-+-, -.....:i Project # LACBWR Site LLC 2040 Savage Road N GEL Quote#: - - - - - - - - - - - - - - - < go1.oom Chemistry I Radiochemistry I Radiobloossay I Specialty Analytics Charleston, SC 29407 rfJ u COC Number(ltiii=========l§]~B:3~~~:E~~2i8J8J238J8J2J~~~~~ffi]~'.28Jl82i238J8J8J8J8J8J8J8J8JI:iphone: PO Number: 672583 vm.rw,,r: , (843) Fax: (843) 556-8 171 766-1178 0 Client Name: La Crosse Solutions Phone# 608-689-4259
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Project/Site Name: LACBWR-Genoa WI Fax#
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0\ Address: 5460 I State Road 35 N
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Relinquished By (Signed) I, 10/16/2019 )'3/J 2 2 Additional /?emarks: None 3 3 ForLabRecei11i11!{_Use()_nl,r:__C11s1_ody Sea/!111ac1? [] Yes [ ]No CoolerTemJJ: = ° C
"'lfo1<saftipleH1ippi11gia11ddeliverJdetalls, I,) Chain of Custody Number= Client Determined 2.) QC Codes: N = Normal Sample, TB :::: Trip Blank, FD = Field Duplicate, EB ::c: Equipment Bhmk, MS= .'Matrix Spike Sample., MSD = !vfatrix Spike Duplicate Sample, G ""Grab. C =Composite 3.) Field Fihercd: For liquid matrices. indicate with a- Y ~ for yes 1he sam,ple was field filtered or- N - for sample was not field filtered.
4.) Matrix Codes: DW=Drinking \Yater. G\V=Gr0tmdwatcr, SW=Surfacc Water, WW=Waste Water. \V=Watcr, ML=Misc Liquid. SO=Soil, SD=Sediment. SL=S ludge, SS=Solid Waste. O=Oil, F= Filter, P=Wipe, U=Urine, F= Fecal, N=Nasal 5.) Sample Analysis Requested: Anal}1icul method requested (i,e. 8260B, 60l0Bn470A) and mlmberof containers provided fo r each (i .e, 8260/J -3, 6010B/7470A - .t), 6.) Preservntive Type: HA = .Hydrochloric Acid. NI= Nitric Acid, SH= Sodium Hydroxide, SA = Sulfuric Acid. AA= Ascorbic Acid, HX c:: Hexane, ST ,0:. Sodium 111iosulfate, Ifno preservative is added = leave fie ld blank
. - EK- SAMPLE RECEIPT & REVIEW FORM i Client: f-_...A /f r, SDG/AR/COC/Work Ord~r;. L
'C.: 135 !,i 'L4
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Rccei\'Cd By: -;l{yJ~ Da tc Received: ~{1 *
._ , Circk Applicable*
J CFedEx Expre~ FedEx Ground LI PS Field Services Courier Other Carrier and Tracking Number 11C7 3575 tf'f7/f Suspected H,m,rd Information "-' 0 *If Net Counts > I00cpm on samples 1101 marked "radioactive". contact the Radiation Safety Group for further investigation.
>- z Hazard Class Shipped: UN#: ;\)Shipped as a DOT Hazardous I lfl/N2910, Is the Radioactive Shipment Surl'cy Compliant Yes___ No __
B) Did the client designate the samples arc to be received as radioactive? I/ COC notation or rnclioactive stickers on containers equal client dcsigifotion. __/{!__cPM / mR/Hr C) Did the RSO classify the samples as radioactive'? I/ Maximum Net Counts Observed* (Observed Counts* Arca Background Counts): Classified as: Rad t Rad 2 Rad J D) Did the client designate samples are hazardous? I COC notation or hazard labels 011 containers equal client desii,mntion. r\f Dor E is yes. select Hazards below. E) Did the RSO identify possible hazards? I/ PCB's Flammable Foreign Soil RCRA Asbestos Beryllium Other:
~
z< z e Sample Rccei11t Criteria ;i. Comments/Qualifiers (Required for Non-Conforming Items) Circle Applicable: Seals broken Damaged container Leaking contai ner Other (describe) Shipping conrainers received intact and I sealed? ' Chain of custody documents included Circle Applicable: Client contacted and provided COC COC created upon receipt 2 with shipment? 3 Samples requiring cold preservation Preservation Method: Wet Ice Ice Packs
'all tempcrntures are recorded in Celsius Dry ice es) Other:
TEMP:
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within (0 < 6 deg. C)"* Temperature Device Serial#: /. 'f,U/ -T.t.* 4 Daily check performed and passed on IR temperature gun° I Secondary Temperature Device Serial ii (If Applicable): Circle Applicable : Seals broken Damaged container Leaking container Other (describe) 5 Sample containers intact and scaled S.implc ID's :md Containers Affected: Samples requiring chemical preservation 6 ar proper pH'1 If Prcscrrnlinn add *d Lot #* If Yes. arc Encores or Soil Kits present for solids Yes No NA (If yes, take to VOA Freezer) Do any samples require Volatile Do liquid VOA vials contain acid preservation? Yes No NA (If unknown, select No) 7 i\rc liquid VOA vials fm, ofhcadspacc 0 Yes_ No__ NA--- ** Analysis? S;irnple tD's :md containers affcctcd: ID's and tests affected: 8 Samples received within holding time? Sample !D's on COC match !D's on !D's and containers affcc\cd: 9 bottles'> Date & time cm COC match date & time Circle t\pplicablc: No dates on containers No times on containers COC missing info Other (describe) to on bottles? Number or containers received match Circle Applicable: No container count on COC Other (describe) II number indicated on COC Ar.: sample containers identifiable as l 12 GEL nrovided COC form is properly signed in Circle Applicable: Not relinquished Other (describe) (3 relinquished/received sections Comments (Use Continuation Form if needed):
.. M 8_ ____ Dale .,, LOI*7 2.I l'l PM (or l'iVIA) review: Initials *-- ffi~ ** ~*-"
Page of
' GL-CHL-SR-001 Rev 6 Page 71 of 72 SDG: 493624
List of current GEL Certifications as of 14 November 2019 State Certification Alaska 17-018 Alaska Drinking Water SC00012 Arkansas 88-0651 CLlA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 DoD ELAP/ ISOl 7025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (A133904) Maine 2019020 Maryland 270 Massachusetts M-SC012 Massachusetts PFAS Approv Letter Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada SC000122020-1 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 2019-165 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee 1N 02934 TexasNELAP T104704235-19-15 UtahNELAP SC000122019-29 Vermont VT87156 Virginia NELAP 460202 Washington C780 Page 72 of 72 SDG: 493624
[i]ij* I Laboratories LLc PO Bex 30712 Charleston SC 29417 a member of The GEL Group INC 2040 Sa*1a,;ie Road Charleston. SC 29407 P 843 556.8171 F 84:;_766.117B gel. com June 07, 2018 Mr. Jason Q. Spaide LaCrosseSolutions S4601 State Hwy 35 Genoa, Wisconsin 54632 Re: LACBWR Site Restoration Project Work Order: 449877
Dear Mr. Spaide:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on May 10, 2018. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4453. Sincerely, Kaitlyn Stone for Edith Kent Project Manager Purchase Order: 672583 Enclosures Page 1 of 60 I I 1111 1 11 1 I 11111 111 111
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for ENRG070 LaCrosseSolutions, LLC (672583) Client SDG: 449877 GEL Work Order: 449877 The Qualifiers in this report are defined as follows:
- A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
UI Gamma Spectroscopy-Uncertain identification Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis. The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the 'U' qualifier above. This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Edith Kent. Reviewed by Page 2 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-102-FSGS-004-SG Project: ENRG07001 Sample ID: 449877001 Client ID: ENRG070 Matrix: Soil Collect Date: 12-MAR-18 14:47 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0896 +/-0.207 0.364 0.400 pCi/g LXB3 05/22/18 1648 1765102 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 97.9 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 3 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-102-FSGS-009-SS Project: ENRG07001 Sample ID: 449877002 Client ID: ENRG070 Matrix: Soil Collect Date: 12-MAR-18 14:48 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0556 +/-0.174 0.368 0.400 pCi/g LXB3 05/22/18 1648 1765102 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 78.8 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 4 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L3-012-102-FSGS-008-SS Project: ENRG07001 Sample ID: 449877003 Client ID: ENRG070 Matrix: Soil Collect Date: 12-MAR-18 13:22 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0144 +/-0.198 0.377 0.400 pCi/g LXB3 05/22/18 1648 1765102 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.3 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 5 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-PAD-Q01-AJGS-103-SS Project: ENRG07001 Sample ID: 449877004 Client ID: ENRG070 Matrix: Soil Collect Date: 04-MAR-18 14:45 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.126 +/-0.218 0.376 0.400 pCi/g LXB3 05/22/18 1648 1765102 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 100 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 6 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-PAD-Q03-AJGS-201-SS Project: ENRG07001 Sample ID: 449877005 Client ID: ENRG070 Matrix: Soil Collect Date: 20-MAR-18 10:23 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.137 +/-0.175 0.385 0.400 pCi/g LXB3 05/22/18 1648 1765102 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 88.3 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 7 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-PAD-Q03-AJGS-303-SS Project: ENRG07001 Sample ID: 449877006 Client ID: ENRG070 Matrix: Soil Collect Date: 27-MAR-18 15:44 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0191 +/-0.189 0.361 0.400 pCi/g LXB3 05/22/18 1648 1765102 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 95.5 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 8 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-PAD-Q02-AJGS-401-SS Project: ENRG07001 Sample ID: 449877007 Client ID: ENRG070 Matrix: Soil Collect Date: 02-APR-18 14:46 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0628 +/-0.206 0.376 0.400 pCi/g LXB3 05/22/18 1649 1765102 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 93.1 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 9 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L1-PAD-Q01-AJGS-501-SS Project: ENRG07001 Sample ID: 449877008 Client ID: ENRG070 Matrix: Soil Collect Date: 02-MAY-18 14:45 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0497 +/-0.200 0.369 0.400 pCi/g LXB3 05/22/18 1649 1765102 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 83.5 (25%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 10 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-024-SB Project: ENRG07001 Sample ID: 449877009 Client ID: ENRG070 Matrix: Soil Collect Date: 05-APR-18 14:58 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 U 0.0136 +/-0.0192 0.0298 0.400 pCi/g BXA4 06/03/18 2146 1764672 1 Americium-243 U 0.0157 +/-0.0274 0.0473 0.400 pCi/g Curium-243/244 U -3.38E-05 +/-0.011 0.0239 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U 0.00131 +/-0.00388 0.00687 0.010 pCi/g BXA4 06/02/18 1857 1764673 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 U -0.00711 +/-0.024 0.0624 0.400 pCi/g BXA4 06/02/18 1801 1764674 3 Plutonium-239/240 U 0.0312 +/-0.0379 0.0509 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U 0.935 +/-2.60 4.41 5.00 pCi/g BXA4 06/05/18 0640 1764675 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 U 0.577 +/-1.37 2.86 5.00 pCi/g TXJ1 05/24/18 0839 1763607 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 U 0.00146 +/-0.0333 0.0636 1.00 pCi/g RXF2 05/14/18 1401 1763697 6 Cobalt-60 U 0.0379 +/-0.0424 0.0869 pCi/g Europium-152 U 0.00914 +/-0.0655 0.128 pCi/g Europium-154 U 0.0149 +/-0.0833 0.179 pCi/g Europium-155 UI 0.00 +/-0.129 0.150 pCi/g Niobium-94 U 0.0183 +/-0.0191 0.0456 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.223 +/-0.162 0.373 0.400 pCi/g LXB3 05/22/18 1648 1765102 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium U 2.40 +/-4.17 7.13 10.0 pCi/g MXH8 05/17/18 1647 1763551 8 Liquid Scint C14, Solid "As Received" Carbon-14 U 0.617 +/-2.27 3.88 5.00 pCi/g BXM4 05/21/18 1217 1765373 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 U 0.126 +/-0.692 1.20 2.00 pCi/g CXS7 05/20/18 1944 1763527 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U 2.06 +/-3.52 5.66 10.0 pCi/g TXJ1 05/25/18 2118 1763512 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 11 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-024-SB Project: ENRG07001 Sample ID: 449877009 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U 0.432 +/-1.76 3.01 5.00 pCi/g TXJ1 05/25/18 1759 1763518 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 102 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 88.6 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 94.5 (15%-125%) Plutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 78 (15%-125%) Corrected" Plutonium-236 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 78 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 96.2 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 93.1 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 87.2 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 69.9 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 64.5 (25%-125%) Notes: Page 12 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-024-SB Project: ENRG07001 Sample ID: 449877009 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 13 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-001-SS Project: ENRG07001 Sample ID: 449877010 Client ID: ENRG070 Matrix: Soil Collect Date: 30-MAR-18 12:05 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 U 0.00462 +/-0.0137 0.0248 0.400 pCi/g BXA4 06/03/18 2146 1764672 1 Americium-243 U -0.00366 +/-0.0221 0.047 0.400 pCi/g Curium-243/244 U -0.0156 +/-0.0158 0.0424 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U 0.0017 +/-0.00329 0.00498 0.010 pCi/g BXA4 06/02/18 1854 1764673 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 U 0.00662 +/-0.0312 0.0577 0.400 pCi/g BXA4 06/04/18 1044 1764674 3 Plutonium-239/240 U -0.0108 +/-0.0238 0.072 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U 1.06 +/-3.25 5.53 5.00 pCi/g BXA4 06/05/18 0841 1764675 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 U -0.102 +/-0.199 0.342 5.00 pCi/g TXJ1 05/24/18 0939 1763607 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 UI 0.00 +/-0.0402 0.0482 1.00 pCi/g RXF2 05/14/18 1402 1763697 6 Cobalt-60 U -0.000419 +/-0.0304 0.0626 pCi/g Europium-152 U 0.0163 +/-0.0748 0.134 pCi/g Europium-154 U -0.0315 +/-0.0968 0.183 pCi/g Europium-155 U 0.0278 +/-0.0799 0.147 pCi/g Niobium-94 U -0.0102 +/-0.0248 0.0437 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.19 +/-0.179 0.389 0.400 pCi/g LXB3 05/22/18 1648 1765102 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium U 2.31 +/-3.97 6.79 10.0 pCi/g MXH8 05/17/18 1739 1763551 8 Liquid Scint C14, Solid "As Received" Carbon-14 U 0.0526 +/-2.06 3.52 5.00 pCi/g BXM4 05/18/18 0526 1763558 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 U 0.669 +/-0.715 1.20 2.00 pCi/g CXS7 05/20/18 2017 1763527 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U 1.36 +/-3.76 6.14 10.0 pCi/g TXJ1 05/25/18 2150 1763512 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 14 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-001-SS Project: ENRG07001 Sample ID: 449877010 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U -0.371 +/-1.31 2.28 5.00 pCi/g TXJ1 05/25/18 1831 1763518 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 92.2 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 92.1 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 105 (15%-125%) Plutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 63.8 (15%-125%) Corrected" Plutonium-236 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 63.8 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 91.5 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 93.1 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 91.5 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 67.6 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 85.5 (25%-125%) Notes: Page 15 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-001-SS Project: ENRG07001 Sample ID: 449877010 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 16 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-019-SB Project: ENRG07001 Sample ID: 449877011 Client ID: ENRG070 Matrix: Soil Collect Date: 05-APR-18 12:29 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 U 0.00558 +/-0.0212 0.0403 0.400 pCi/g BXA4 06/03/18 2146 1764672 1 Americium-243 U 0.00333 +/-0.0128 0.0238 0.400 pCi/g Curium-243/244 U 0.0111 +/-0.0285 0.0519 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U -0.00146 +/-0.00325 0.008 0.010 pCi/g BXA4 06/02/18 1854 1764673 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 U 0.0383 +/-0.0479 0.0722 0.400 pCi/g BXA4 06/02/18 1801 1764674 3 Plutonium-239/240 U 0.00665 +/-0.0298 0.0583 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U -0.596 +/-3.22 5.54 5.00 pCi/g BXA4 06/05/18 1042 1764675 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 U -0.0772 +/-1.38 2.73 5.00 pCi/g TXJ1 05/24/18 0942 1763607 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 U 0.0445 +/-0.037 0.0542 1.00 pCi/g RXF2 05/14/18 1402 1763697 6 Cobalt-60 U -0.018 +/-0.0282 0.0477 pCi/g Europium-152 U 0.0106 +/-0.0689 0.136 pCi/g Europium-154 U -0.0209 +/-0.0943 0.178 pCi/g Europium-155 U 0.036 +/-0.0741 0.142 pCi/g Niobium-94 U -0.0111 +/-0.0318 0.0484 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0228 +/-0.213 0.394 0.400 pCi/g LXB3 05/22/18 1649 1765102 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium U 2.76 +/-4.15 7.05 10.0 pCi/g MXH8 05/17/18 1832 1763551 8 Liquid Scint C14, Solid "As Received" Carbon-14 U -0.879 +/-2.10 3.64 5.00 pCi/g BXM4 05/18/18 0613 1763558 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 U 0.196 +/-0.609 1.05 2.00 pCi/g CXS7 05/20/18 2049 1763527 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U -1.89 +/-3.40 5.83 10.0 pCi/g TXJ1 05/25/18 2221 1763512 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 17 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-019-SB Project: ENRG07001 Sample ID: 449877011 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U -0.0474 +/-1.67 2.88 5.00 pCi/g TXJ1 05/25/18 1903 1763518 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 81.1 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 94 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 102 (15%-125%) Plutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 63.8 (15%-125%) Corrected" Plutonium-236 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 63.8 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 95.8 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 100 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 98.8 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 69.8 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 68 (25%-125%) Notes: Page 18 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-019-SB Project: ENRG07001 Sample ID: 449877011 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 19 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-001-AV Project: ENRG07001 Sample ID: 449877012 Client ID: ENRG070 Matrix: Soil Collect Date: 30-MAR-18 10:40 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 U -0.0098 +/-0.0131 0.0358 0.400 pCi/g BXA4 06/03/18 2208 1764672 1 Americium-243 U 0.00895 +/-0.0222 0.0395 0.400 pCi/g Curium-243/244 U -0.0114 +/-0.0154 0.040 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U 0.000668 +/-0.00384 0.00743 0.010 pCi/g BXA4 06/02/18 1854 1764673 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 U 0.00761 +/-0.026 0.0482 0.400 pCi/g BXA4 06/02/18 1801 1764674 3 Plutonium-239/240 U 0.00205 +/-0.0214 0.0446 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U -0.314 +/-2.38 4.10 5.00 pCi/g BXA4 06/05/18 1243 1764675 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 U -0.154 +/-0.809 1.54 5.00 pCi/g TXJ1 05/24/18 1455 1763607 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 U 0.00275 +/-0.031 0.0614 1.00 pCi/g RXF2 05/14/18 1402 1763697 6 Cobalt-60 U 0.00804 +/-0.0244 0.0574 pCi/g Europium-152 U 0.0111 +/-0.0662 0.135 pCi/g Europium-154 U -0.003 +/-0.0689 0.144 pCi/g Europium-155 U -0.004 +/-0.0691 0.127 pCi/g Niobium-94 U 0.0519 +/-0.0574 0.065 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.00285 +/-0.199 0.374 0.400 pCi/g LXB3 05/22/18 1648 1765102 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium U 3.40 +/-4.14 6.99 10.0 pCi/g MXH8 05/17/18 1924 1763551 8 Liquid Scint C14, Solid "As Received" Carbon-14 U -1.1 +/-1.95 3.38 5.00 pCi/g BXM4 05/18/18 0700 1763558 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 U -0.289 +/-0.667 1.18 2.00 pCi/g CXS7 05/20/18 2121 1763527 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 7.46 +/-3.65 5.43 10.0 pCi/g TXJ1 05/25/18 2253 1763512 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 20 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-001-AV Project: ENRG07001 Sample ID: 449877012 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U -0.177 +/-1.31 2.28 5.00 pCi/g TXJ1 05/25/18 1934 1763518 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 90.5 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 59 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 101 (15%-125%) Plutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 86.7 (15%-125%) Corrected" Plutonium-236 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 86.7 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 111 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 95.5 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 89.6 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 66.7 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 84 (25%-125%) Notes: Page 21 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-102-AJGS-001-AV Project: ENRG07001 Sample ID: 449877012 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 22 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-VAR-AJGS-004-SB Project: ENRG07001 Sample ID: 449877013 Client ID: ENRG070 Matrix: Soil Collect Date: 06-APR-18 13:24 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 U 0.0119 +/-0.0178 0.0273 0.400 pCi/g BXA4 06/03/18 2208 1764672 1 Americium-243 U 0.011 +/-0.0164 0.0252 0.400 pCi/g Curium-243/244 U -0.00695 +/-0.0173 0.0409 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U 0.00207 +/-0.004 0.00606 0.010 pCi/g BXA4 06/02/18 1855 1764673 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 U 0.0456 +/-0.0505 0.0666 0.400 pCi/g BXA4 06/02/18 1801 1764674 3 Plutonium-239/240 U 0.0406 +/-0.0464 0.058 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U -3.77 +/-3.53 6.18 5.00 pCi/g BXA4 06/05/18 1444 1764675 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 U 0.0765 +/-0.421 0.935 5.00 pCi/g TXJ1 05/24/18 1456 1763607 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 0.369 +/-0.0794 0.0396 1.00 pCi/g RXF2 05/14/18 1403 1763697 6 Cobalt-60 U 0.000997 +/-0.0251 0.0484 pCi/g Europium-152 U 0.0361 +/-0.0543 0.116 pCi/g Europium-154 U -0.0448 +/-0.072 0.109 pCi/g Europium-155 U 0.00864 +/-0.0585 0.116 pCi/g Niobium-94 U 0.00999 +/-0.0202 0.0433 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.191 +/-0.177 0.385 0.400 pCi/g LXB3 05/22/18 1649 1765102 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium U 2.18 +/-1.70 2.80 10.0 pCi/g MXH8 05/17/18 2016 1763551 8 Liquid Scint C14, Solid "As Received" Carbon-14 U 1.38 +/-2.13 3.61 5.00 pCi/g BXM4 05/18/18 0747 1763558 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 U 0.779 +/-0.686 1.14 2.00 pCi/g CXS7 05/20/18 2153 1763527 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U 0.444 +/-3.29 5.43 10.0 pCi/g TXJ1 05/25/18 2325 1763512 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 23 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-VAR-AJGS-004-SB Project: ENRG07001 Sample ID: 449877013 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U -0.269 +/-1.59 2.77 5.00 pCi/g TXJ1 05/25/18 2006 1763518 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 81.4 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 87.4 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 103 (15%-125%) Plutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 56.5 (15%-125%) Corrected" Plutonium-236 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 56.5 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 94.4 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 93.1 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 94.5 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 72.2 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 71.1 (25%-125%) Notes: Page 24 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-VAR-AJGS-004-SB Project: ENRG07001 Sample ID: 449877013 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 25 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-AJGS-B01-SB Project: ENRG07001 Sample ID: 449877014 Client ID: ENRG070 Matrix: Soil Collect Date: 23-MAR-18 13:25 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 U -0.0147 +/-0.0148 0.0397 0.400 pCi/g BXA4 06/03/18 2208 1764672 1 Americium-243 U 0.00944 +/-0.0183 0.0303 0.400 pCi/g Curium-243/244 U -0.0117 +/-0.0141 0.0371 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U -0.000155 +/-0.00427 0.00904 0.010 pCi/g BXA4 06/02/18 1855 1764673 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 U 0.033 +/-0.0584 0.0974 0.400 pCi/g BXA4 06/02/18 1801 1764674 3 Plutonium-239/240 U 0.0325 +/-0.0526 0.0814 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U 0.611 +/-3.55 6.06 5.00 pCi/g BXA4 06/05/18 1646 1764675 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 U 0.708 +/-1.67 3.50 5.00 pCi/g TXJ1 05/24/18 1725 1763607 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 U -0.0113 +/-0.0356 0.0651 1.00 pCi/g RXF2 05/14/18 1403 1763697 6 Cobalt-60 U 0.020 +/-0.0326 0.078 pCi/g Europium-152 U -0.0485 +/-0.0727 0.132 pCi/g Europium-154 U -0.0347 +/-0.130 0.249 pCi/g Europium-155 U 0.0747 +/-0.0829 0.169 pCi/g Niobium-94 U 0.00467 +/-0.023 0.0479 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.113 +/-0.210 0.367 0.400 pCi/g LXB3 05/22/18 1648 1765102 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium U 1.47 +/-1.68 2.83 10.0 pCi/g MXH8 05/17/18 2108 1763551 8 Liquid Scint C14, Solid "As Received" Carbon-14 U 0.796 +/-2.07 3.52 5.00 pCi/g BXM4 05/18/18 0834 1763558 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 U -0.27 +/-0.708 1.25 2.00 pCi/g CXS7 05/20/18 2225 1763527 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U 1.31 +/-3.78 6.18 10.0 pCi/g TXJ1 05/25/18 2356 1763512 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 26 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-AJGS-B01-SB Project: ENRG07001 Sample ID: 449877014 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U -0.785 +/-1.41 2.47 5.00 pCi/g TXJ1 05/25/18 2038 1763518 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 88.6 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 66.8 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 96.1 (15%-125%) Plutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 58.5 (15%-125%) Corrected" Plutonium-236 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 58.5 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 78.4 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 95.5 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 85.2 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 67.4 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 79.3 (25%-125%) Notes: Page 27 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L4-OFF-SOL-AJGS-B01-SB Project: ENRG07001 Sample ID: 449877014 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 28 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: S1-102-CWD-FIFS-A02-SM Project: ENRG07001 Sample ID: 449877015 Client ID: ENRG070 Matrix: Soil Collect Date: 24-APR-18 08:30 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 U 0.067 +/-0.136 0.196 0.400 pCi/g BXA4 06/07/18 0928 1770886 1 Americium-243 U 0.0132 +/-0.085 0.174 0.400 pCi/g Curium-243/244 U -0.0325 +/-0.0806 0.241 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U -0.00174 +/-0.00276 0.00751 0.010 pCi/g BXA4 06/02/18 1855 1764673 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 U 0.0288 +/-0.0433 0.0673 0.400 pCi/g BXA4 06/02/18 1801 1764674 3 Plutonium-239/240 U 0.0306 +/-0.0387 0.0481 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U -0.992 +/-2.98 5.15 5.00 pCi/g BXA4 06/05/18 1847 1764675 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 U 0.162 +/-0.403 1.17 5.00 pCi/g TXJ1 05/24/18 1726 1763607 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 8.23 +/-0.306 0.059 1.00 pCi/g RXF2 05/14/18 1707 1763697 6 Cobalt-60 0.299 +/-0.0796 0.0469 pCi/g Europium-152 UI 0.00 +/-0.442 0.228 pCi/g Europium-154 U 0.0207 +/-0.0797 0.176 pCi/g Europium-155 U 0.095 +/-0.0929 0.187 pCi/g Niobium-94 U 0.0383 +/-0.0424 0.0587 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U -0.0228 +/-0.216 0.393 0.400 pCi/g LXB3 05/22/18 1648 1765102 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium U 1.57 +/-3.62 6.23 10.0 pCi/g MXH8 05/17/18 2200 1763551 8 Liquid Scint C14, Solid "As Received" Carbon-14 U -1.57 +/-2.08 3.63 5.00 pCi/g BXM4 05/18/18 0921 1763558 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 U -0.0495 +/-0.904 1.54 2.00 pCi/g CXS7 05/20/18 1710 1763527 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U 1.33 +/-4.39 7.22 10.0 pCi/g TXJ1 05/26/18 0028 1763512 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 29 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: S1-102-CWD-FIFS-A02-SM Project: ENRG07001 Sample ID: 449877015 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 3.34 +/-1.64 2.66 5.00 pCi/g TXJ1 05/25/18 2109 1763518 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 61.6 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 48.5 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 97.8 (15%-125%) Plutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 67.4 (15%-125%) Corrected" Plutonium-236 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 67.4 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 92 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 105 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 42.6 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 60.8 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 75 (25%-125%) Notes: Page 30 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: S1-102-CWD-FIFS-A02-SM Project: ENRG07001 Sample ID: 449877015 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 31 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-103-AJGS-002-SB Project: ENRG07001 Sample ID: 449877016 Client ID: ENRG070 Matrix: Soil Collect Date: 23-FEB-18 14:03 Receive Date: 10-MAY-18 Collector: Client Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Alpha Spec Analysis Alphaspec Isotopic Am241 Am243, Cm243/244, Solid "Dry Weight Corrected" Americium-241 U -0.0124 +/-0.0192 0.049 0.400 pCi/g BXA4 06/03/18 2208 1764672 1 Americium-243 U -0.00173 +/-0.0184 0.0391 0.400 pCi/g Curium-243/244 U -0.0266 +/-0.0218 0.0599 0.400 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U 0.000265 +/-0.00323 0.0063 0.010 pCi/g BXA4 06/02/18 1855 1764673 2 Alphaspec Pu238, 239/240, Solid "Dry Weight Corrected" Plutonium-238 U -0.0199 +/-0.0284 0.0747 0.400 pCi/g BXA4 06/02/18 1801 1764674 3 Plutonium-239/240 U 0.00196 +/-0.0224 0.0476 0.400 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U -0.292 +/-2.14 3.68 5.00 pCi/g BXA4 06/05/18 2048 1764675 4 Rad Gamma Spec Analysis Gamma Ni59, Solid "Dry Weight Corrected" Nickel-59 U -0.612 +/-1.35 2.53 5.00 pCi/g TXJ1 05/24/18 2137 1763607 5 Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 "Dry Weight Corrected" Cesium-137 UI 0.00 +/-0.0406 0.0489 1.00 pCi/g RXF2 05/14/18 1707 1763697 6 Cobalt-60 U 0.014 +/-0.028 0.066 pCi/g Europium-152 U -0.0424 +/-0.0667 0.119 pCi/g Europium-154 U 0.0129 +/-0.105 0.196 pCi/g Europium-155 U 0.00458 +/-0.0649 0.132 pCi/g Niobium-94 U 0.00695 +/-0.0253 0.0518 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.209 +/-0.172 0.268 0.400 pCi/g LXB3 05/23/18 1036 1765102 7 Rad Liquid Scintillation Analysis LSC, Tritium Distillation, Solid "As Received" Tritium U -0.41 +/-3.66 6.50 10.0 pCi/g MXH8 05/17/18 2252 1763551 8 Liquid Scint C14, Solid "As Received" Carbon-14 U -1.82 +/-2.12 3.71 5.00 pCi/g BXM4 05/18/18 1009 1763558 9 Liquid Scint Tc99, Solid "As Received" Technetium-99 U -0.412 +/-0.585 1.05 2.00 pCi/g CXS7 05/20/18 2257 1763527 10 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U 0.466 +/-3.22 5.30 10.0 pCi/g TXJ1 05/26/18 0100 1763512 11 Liquid Scint Ni63, Solid "Dry Weight Corrected" Page 32 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-103-AJGS-002-SB Project: ENRG07001 Sample ID: 449877016 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U -0.353 +/-1.49 2.60 5.00 pCi/g TXJ1 05/25/18 2141 1763518 12 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 MPK1 05/11/18 0856 1763443 The following Analytical Methods were performed: Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 DOE RESL Ni-1 6 DOE HASL 300, 4.5.2.3/Ga-01-R 7 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE EML HASL-300, Tc-02-RC Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Americium-243 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 80.1 (15%-125%) Solid "Dry Weight Corrected" Curium-243/244 Tracer Alphaspec Isotopic Am241 Am243, Cm243/244, 80 (15%-125%) Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 101 (15%-125%) Plutonium-236 Tracer Alphaspec Pu238, 239/240, Solid "Dry Weight 95.3 (15%-125%) Corrected" Plutonium-236 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 95.3 (15%-125%) Nickel Carrier Gamma Ni59, Solid "Dry Weight Corrected" 101 (25%-125%) Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 95.5 (25%-125%) Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 97.3 (15%-125%) Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 73.1 (15%-125%) Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 75.4 (25%-125%) Notes: Page 33 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: June 7, 2018 Company : LaCrosseSolutions Address : S4601 State Hwy 35 Genoa, Wisconsin 54632
Contact:
Mr. Jason Q. Spaide Project: LACBWR Site Restoration Project Client Sample ID: L2-SUB-103-AJGS-002-SB Project: ENRG07001 Sample ID: 449877016 Client ID: ENRG070 Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 34 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: June 7, 2018 LaCrosseSolutions Page 1 of 8 S4601 State Hwy 35 Genoa, Wisconsin
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Mr. Jason Q. Spaide Workorder: 449877 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1764672 QC1204029320 449877009 DUP Americium-241 U 0.0136 U 0.00375 pCi/g N/A N/A BXA4 06/03/18 21:46 Uncertainty +/-0.0192 +/-0.0127 Americium-243 U 0.0157 U 0.0277 pCi/g N/A N/A Uncertainty +/-0.0274 +/-0.0249 Curium-243/244 U -3.38E-05 U -0.0026 pCi/g N/A N/A Uncertainty +/-0.011 +/-0.0108 QC1204029321 LCS Americium-241 1.94 1.82 pCi/g 93.8 (75%-125%) 06/03/18 21:46 Uncertainty +/-0.150 Americium-243 U 0.024 pCi/g (75%-125%) Uncertainty +/-0.0216 Curium-243/244 2.40 2.30 pCi/g 95.7 (75%-125%) Uncertainty +/-0.166 QC1204029319 MB Americium-241 U 0.00211 pCi/g 06/05/18 09:43 Uncertainty +/-0.0221 Americium-243 U 0.00436 pCi/g Uncertainty +/-0.0182 Curium-243/244 U -0.00297 pCi/g Uncertainty +/-0.0278 Batch 1764673 QC1204029323 449877009 DUP Neptunium-237 U 0.00131 U 0.000957 pCi/g N/A N/A BXA4 06/02/18 18:57 Uncertainty +/-0.00388 +/-0.00461 QC1204029324 LCS Neptunium-237 1.48 1.57 pCi/g 106 (75%-125%) 06/02/18 18:57 Uncertainty +/-0.0679 QC1204029322 MB Neptunium-237 U -0.00112 pCi/g 06/02/18 18:57 Uncertainty +/-0.00244 Page 35 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 2 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1764674 QC1204029326 449877009 DUP Plutonium-238 U -0.00711 U 0.00608 pCi/g N/A N/A BXA4 06/02/18 18:01 Uncertainty +/-0.024 +/-0.0228 Plutonium-239/240 U 0.0312 U 0.0144 pCi/g N/A N/A Uncertainty +/-0.0379 +/-0.0326 QC1204029327 LCS Plutonium-238 U 0.033 pCi/g 06/02/18 17:56 Uncertainty +/-0.0418 Plutonium-239/240 1.95 1.72 pCi/g 88.3 (75%-125%) Uncertainty +/-0.250 QC1204029325 MB Plutonium-238 U -0.0151 pCi/g 06/02/18 18:01 Uncertainty +/-0.0378 Plutonium-239/240 U 0.0233 pCi/g Uncertainty +/-0.0379 Batch 1764675 QC1204029329 449877009 DUP Plutonium-241 U 0.935 U -0.684 pCi/g N/A N/A BXA4 06/06/18 00:50 Uncertainty +/-2.60 +/-2.82 QC1204029330 LCS Plutonium-241 69.2 90.6 pCi/g 131 * (75%-125%) 06/06/18 04:04 Uncertainty +/-10.6 QC1204029328 MB Plutonium-241 U -0.414 pCi/g 06/05/18 22:49 Uncertainty +/-2.80 Batch 1770886 QC1204043372 449877015 DUP Americium-241 U 0.067 U 0.0877 pCi/g N/A N/A BXA4 06/06/18 09:06 Uncertainty +/-0.136 +/-0.0893 Americium-243 U 0.0132 U 0.0314 pCi/g N/A N/A Uncertainty +/-0.085 +/-0.0864 Curium-243/244 U -0.0325 U -0.00875 pCi/g N/A N/A Uncertainty +/-0.0806 +/-0.0387 Page 36 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 3 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1770886 QC1204043373 LCS Americium-241 3.83 3.50 pCi/g 91.5 (75%-125%) BXA4 06/06/18 09:06 Uncertainty +/-0.417 Americium-243 U -0.0133 pCi/g (75%-125%) Uncertainty +/-0.0449 Curium-243/244 4.74 4.39 pCi/g 92.5 (75%-125%) Uncertainty +/-0.463 QC1204043371 MB Americium-241 U 0.0315 pCi/g 06/06/18 09:06 Uncertainty +/-0.0999 Americium-243 U 0.0111 pCi/g Uncertainty +/-0.0619 Curium-243/244 U -0.00372 pCi/g Uncertainty +/-0.0321 Rad Gamma Spec Batch 1763607 QC1204026770 449877009 DUP Nickel-59 U 0.577 U 1.15 pCi/g N/A N/A TXJ1 05/25/18 06:15 Uncertainty +/-1.37 +/-1.33 QC1204026771 LCS Nickel-59 92.0 80.1 pCi/g 87.2 (75%-125%) 05/25/18 06:15 Uncertainty +/-5.92 QC1204026769 MB Nickel-59 U 0.775 pCi/g 05/24/18 21:38 Uncertainty +/-1.39 Batch 1763697 QC1204026986 449877009 DUP Cesium-137 U 0.00146 U 0.0132 pCi/g N/A N/A RXF2 05/14/18 17:08 Uncertainty +/-0.0333 +/-0.0439 Cobalt-60 U 0.0379 U 0.0132 pCi/g N/A N/A Uncertainty +/-0.0424 +/-0.0416 Europium-152 U 0.00914 U 0.0143 pCi/g N/A N/A Uncertainty +/-0.0655 +/-0.0972 Page 37 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 4 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1763697 Europium-154 U 0.0149 U 0.0302 pCi/g N/A N/A RXF2 05/14/18 17:08 Uncertainty +/-0.0833 +/-0.141 Europium-155 UI 0.00 U 0.0842 pCi/g N/A N/A Uncertainty +/-0.129 +/-0.0712 Niobium-94 U 0.0183 U 0.0142 pCi/g N/A N/A Uncertainty +/-0.0191 +/-0.0351 QC1204026987 LCS Americium-241 488 567 pCi/g 116 (75%-125%) 05/14/18 17:08 Uncertainty +/-14.7 Cesium-137 173 168 pCi/g 97.6 (75%-125%) Uncertainty +/-3.16 Cobalt-60 130 127 pCi/g 97.8 (75%-125%) Uncertainty +/-3.30 Europium-152 U -0.424 pCi/g Uncertainty +/-1.48 Europium-154 U -0.169 pCi/g Uncertainty +/-0.846 Europium-155 U -0.628 pCi/g Uncertainty +/-1.24 Niobium-94 U 0.529 pCi/g Uncertainty +/-0.442 QC1204026985 MB Cesium-137 U 0.00433 pCi/g 05/14/18 17:08 Uncertainty +/-0.0166 Cobalt-60 U 0.00328 pCi/g Uncertainty +/-0.0221 Europium-152 U 0.00387 pCi/g Uncertainty +/-0.0407 Europium-154 U -0.0139 pCi/g Uncertainty +/-0.0688 Europium-155 U -0.0207 pCi/g Uncertainty +/-0.0384 Page 38 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 5 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1763697 Niobium-94 U 0.0152 pCi/g RXF2 05/14/18 17:08 Uncertainty +/-0.0121 Rad Gas Flow Batch 1765102 QC1204030329 449877005 DUP Strontium-90 U -0.137 U -0.0855 pCi/g N/A N/A LXB3 05/22/18 16:48 Uncertainty +/-0.175 +/-0.192 QC1204030330 LCS Strontium-90 21.5 22.2 pCi/g 103 (75%-125%) 05/22/18 16:48 Uncertainty +/-1.25 QC1204030328 MB Strontium-90 U -0.0123 pCi/g 05/22/18 16:48 Uncertainty +/-0.179 Rad Liquid Scintillation Batch 1763512 QC1204026506 449493001 DUP Iron-55 U 0.839 U -1.31 pCi/g N/A N/A TXJ1 05/26/18 02:03 Uncertainty +/-4.13 +/-3.87 QC1204026507 LCS Iron-55 106 94.7 pCi/g 89 (75%-125%) 05/26/18 02:35 Uncertainty +/-5.96 QC1204026505 MB Iron-55 U -0.679 pCi/g 05/26/18 01:31 Uncertainty +/-2.67 Batch 1763518 QC1204026519 449493001 DUP Nickel-63 U 2.48 U 1.03 pCi/g N/A N/A TXJ1 05/25/18 22:44 Uncertainty +/-1.91 +/-1.58 QC1204026520 LCS Nickel-63 85.6 86.2 pCi/g 101 (75%-125%) 05/25/18 23:16 Uncertainty +/-3.08 QC1204026518 MB Nickel-63 U -0.212 pCi/g 05/25/18 22:13 Uncertainty +/-1.44 Page 39 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 6 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1763527 QC1204026545 449493001 DUP Technetium-99 U 0.580 U 0.0653 pCi/g N/A N/A CXS7 05/21/18 00:02 Uncertainty +/-0.754 +/-0.642 QC1204026546 LCS Technetium-99 40.9 36.0 pCi/g 87.9 (75%-125%) 05/21/18 00:34 Uncertainty +/-1.38 QC1204026544 MB Technetium-99 U -0.0178 pCi/g 05/20/18 23:29 Uncertainty +/-0.560 Batch 1763551 QC1204026612 449877009 DUP Tritium U 2.40 U 4.95 pCi/g N/A N/A MXH8 05/18/18 00:36 Uncertainty +/-4.17 +/-4.27 QC1204026614 LCS Tritium 24.9 25.2 pCi/g 101 (75%-125%) 05/18/18 02:21 Uncertainty +/-2.69 QC1204026611 MB Tritium U 0.995 pCi/g 05/17/18 23:44 Uncertainty +/-1.70 QC1204026613 449877009 MS Tritium 126 U 2.40 112 pCi/g 89 (75%-125%) 05/18/18 01:28 Uncertainty +/-4.17 +/-12.5 Batch 1763558 QC1204026633 449877010 DUP Carbon-14 U 0.0526 U -0.719 pCi/g N/A N/A BXM4 05/18/18 11:43 Uncertainty +/-2.06 +/-1.97 QC1204026635 LCS Carbon-14 136 104 pCi/g 76.5 (75%-125%) 05/21/18 08:39 Uncertainty +/-6.50 QC1204026632 MB Carbon-14 U -0.0751 pCi/g 05/18/18 10:56 Uncertainty +/-1.97 QC1204026634 449877010 MS Carbon-14 334 U 0.0526 265 pCi/g 79.5 (75%-125%) 05/18/18 12:30 Uncertainty +/-2.06 +/-9.21 Page 40 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 7 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1765373 QC1204030910 449877009 DUP Carbon-14 U 0.617 U -1.16 pCi/g N/A N/A BXM4 05/21/18 13:39 Uncertainty +/-2.27 +/-2.14 QC1204030912 LCS Carbon-14 136 131 pCi/g 95.7 (75%-125%) 05/21/18 15:02 Uncertainty +/-4.42 QC1204030909 MB Carbon-14 U -0.0248 pCi/g 05/21/18 12:58 Uncertainty +/-2.16 QC1204030911 449877009 MS Carbon-14 351 U 0.617 346 pCi/g 98.7 (75%-125%) 05/21/18 14:21 Uncertainty +/-2.27 +/-11.5 Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). The Qualifiers in this report are defined as follows:
** Analyte is a Tracer compound
< Result is less than value reported
> Result is greater than value reported BD Results are either below the MDC or tracer recovery is low FA Failed analysis.
H Analytical holding time was exceeded J Value is estimated K Analyte present. Reported value may be biased high. Actual value is expected to be lower. L Analyte present. Reported value may be biased low. Actual value is expected to be higher. M M if above MDC and less than LLD M REMP Result > MDC/CL and < RDL N/A RPD or %Recovery limits do not apply. N1 See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER. R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD. UI Gamma Spectroscopy--Uncertain identification UJ Gamma Spectroscopy--Uncertain identification Page 41 of 60
GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 449877 Page 8 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y Other specific qualifiers were required to properly define the results. Consult case narrative.
^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.
- Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 42 of 60
Radiochemistry Technical Case Narrative LaCrosseSolutions, LLC (ENRG) SDG #: 449877 Product: Alphaspec Isotopic Am241 Am243, Cm243/244, Solid Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1764672 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877009 L2-SUB-102-AJGS-024-SB 449877010 L2-SUB-102-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-019-SB 449877012 L2-SUB-102-AJGS-001-A V 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B01-SB 449877016 L2-SUB-103-AJGS-002-SB 1204029319 Method Blank (MB) 1204029320 449877009(L2-SUB-102-AJGS-024-SB) Sample Duplicate (DUP) 1204029321 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Recounts The U-232 traced portion of sample 1204029319 (MB) was recounted due to results more negative than the three sigma TPU. The second count is reported. Product: Alphaspec Np, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-032 REV# 21 Analytical Batch: 1764673 GEL Page 43Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877009 L2-SUB-102-AJGS-024-SB 449877010 L2-SUB-102-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-019-SB 449877012 L2-SUB-102-AJGS-001-A V 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B01-SB 449877015 Sl-102-CWD-FIFS-A02-SM 449877016 L2-SUB-l 03-AJGS-002-SB 1204029322 Method Blank (MB) 1204029323 449877009(L2-SUB-102-AJGS-024-SB) Sample Duplicate (DUP) 1204029324 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: Alphaspec Pu238, 239/240, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1764674 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877009 L2-SUB-102-AJGS-024-SB 449877010 L2-SUB-102-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-0 19-SB 449877012 L2-SUB-102-AJGS-001-AV 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B0 1-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-103-AJGS-002-SB 1204029325 Method Blank (MB) 1204029326 449877009(L2-SUB-102-AJGS-024-SB) Sample Duplicate (DUP) 1204029327 Laboratory Control Sample (LCS) GEL Page 44Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P843.556.8171 F 843.766.1178 www.gel.com
The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Recounts Sample 449877010 (L2-SUB-102-AJGS-001-SS) was recounted due to a suspected false positive. The recount is reported. Miscellaneous Information Additional Comments Samples 449877009 (L2-SUB-102-AJGS-024-SB), 449877011 (L2-SUB-102-AJGS-019-SB), 449877012 (L2-SUB-102-AJGS-001-AV) and 449877013 (L2-SUB-VAR-AJGS-004-SB) did not meet the resolution requirement of having a full width half maximum of 100 keV or less for the tracer; however, the tracer yield requirement was met and the tracer peaks are within the tracer region of interest. Product: Alphaspec Isotopic Am241 Am243, Cm243/244, Solid Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1770886 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877015 S 1-102-CWD-FIFS-A02-SM 1204043371 Method Blank (MB) 1204043372 449877015(Sl-102-CWD-FIFS-A02-SM) Sample Duplicate (DUP) 1204043373 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Sample Re-prep/Re-analysis Sample 449877015 (Sl-102-CWD-FIFS-A02-SM) was reprepped due to suspected interference. The reanalysis GEL Page 45Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
is being reported. Recounts The Am-243 traced portion of sample 449877015 (S 1-102-CWD-FIFS-A02-SM) was recounted due to a suspected false positive. The recount is being reported. Product: Dry Weight Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877001 L3-012-102-FSGS-004-SG 449877002 L3-012-102-FSGS-009-SS 449877003 L3-012-102-FSGS-008-SS 449877004 Ll-PAD-Q0l-AJGS-103-SS 449877005 Ll-PAD-Q03-AJGS-201-SS 449877006 Ll-P AD-Q03-AJGS-303-SS 449877007 Ll-PAD-Q02-AJGS-401-SS 449877008 Ll-PAD-Q0l-AJGS-501-SS 449877009 L2-SUB-l 02-AJGS-024-SB 449877010 L2-SUB-l 02-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-019-SB 449877012 L2-SUB-102-AJGS-001-A V 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B01-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-l 03-AJGS-002-SB The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Miscellaneous Information Additional Comments Sample 449877012 was asphalt. It count not be sieved. 449877012 (L2-SUB-102-AJGS-001-AV). Product: Gamma Ni59, Solid Analytical Method: DOE RESL Ni-1 Analytical Procedure: GL-RAD-A-022 REV# 18 GEL Page 46Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Analytical Batch: 1763607 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877009 L2-SUB-l 02-AJGS-024-SB 449877010 L2-SUB-l 02-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-019-SB 449877012 L2-SUB-102-AJGS-001-A V 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B01-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-l 03-AJGS-002-SB 1204026769 Method Blank (MB) 1204026770 449877009(L2-SUB-102-AJGS-024-SB) Sample Duplicate (DUP) 1204026771 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: Gamma, Cs137, Co60, Nb94, Eu152, Eu154, Eu155 Analytical Method: DOE HASL 300, 4.5.2.3/Ga-01-R Analytical Procedure: GL-RAD-A-013 REV# 27 Analytical Batch: 1763697 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877009 L2-SUB-102-AJGS-024-SB 449877010 L2-SUB-102-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-0 19-SB 449877012 L2-SUB-102-AJGS-001-AV 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B0 1-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-103-AJGS-002-SB 1204026985 Method Blank (MB) 1204026986 449877009(L2-SUB-102-AJGS-024-SB) Sample Duplicate (DUP) GEL Page 47Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
1204026987 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Qualifier Information Qualifier Reason Analyte Sample Client Sample Results are considered a UI false positive due to high Cesium-137 449877016 L2-SUB-103-AJGS-002-SB counting uncertainty. Results are considered a UI false positive due to high 449877010 L2-SUB-l 02-AJGS-00 1-SS peak-width. Results are considered a UI false positive due to low Europium-152 449877015 S 1-102-CWD-FIFS-A02-SM abundance. Europium-155 449877009 L2-SUB-l 02-AJGS-024-SB Product: GFPC, Sr90, Solid Analytical Method: EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Analytical Procedure: GL-RAD-A-004 REV# 19 Analytical Batch: 1765102 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877001 L3-012-102-FSGS-004-SG 449877002 L3-012-102-FSGS-009-SS 449877003 L3-012-102-FSGS-008-SS 449877004 Ll-PAD-Q0l-AJGS-103-SS 449877005 Ll-PAD-Q03-AJGS-201-SS 449877006 L 1-PAD-Q03-AJGS-303-SS 449877007 Ll-PAD-Q02-AJGS-401-SS 449877008 Ll-PAD-Q0l-AJGS-501-SS 449877009 L2-SUB-102-AJGS-024-SB 449877010 L2-SUB-102-AJGS-00 1-SS GEL Page 48Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
449877011 L2-SUB-102-AJGS-019-SB 449877012 L2-SUB-102-AJGS-001-A V 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B01-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-l 03-AJGS-002-SB 1204030328 Method Blank (MB) 1204030329 449877005(Ll-PAD-Q03-AJGS-201-SS) Sample Duplicate (DUP) 1204030330 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Recounts Sample 449877016 (L2-SUB-103-AJGS-002-SB) was recounted due to results more negative than the three sigma TPU. The second count is reported. Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 19 Analytical Batch: 1764675 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877009 L2-SUB-102-AJGS-024-SB 449877010 L2-SUB-102-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-019-SB 449877012 L2-SUB-102-AJGS-001-A V 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B0 1-SB 449877015 Sl-102-CWD-FIFS-A02-SM 449877016 L2-SUB-103-AJGS-002-SB 1204029328 Method Blank (MB) 1204029329 449877009(L2-SUB-102-AJGS-024-SB) Sample Duplicate (DUP) 1204029330 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. GEL Page 49Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P843.556.8171 F 843.766.1178 www.gel.com
Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information Laboratory Control Sample (LCS) Recovery The Laboratory Control Sample (See Below) does not meet the recovery requirement, however, all sample results are less than the MDC. Since the sample results are non-detects, the implied high bias does not carry over to the associated samples. Sample Analyte Value 1204029330 (LCS) Plutonium-241 131 * (75%-125%) RDLMet Samples (See Below) did not meet the detection limits, however the 10CFR61 limitations were met. Sample Analyte Value 449877010 (L2-SUB-l 02-AJGS-00 1-SS) Plutonium-241 Result 1.06 < MDA 5.53 > RDL 5 pCi/g 449877011 (L2-SUB-l 02-AJGS-0 19-SB) Plutonium-241 Result -0.596 < MDA 5.54 > RDL 5 pCi/g 449877013 (L2-SUB-VAR-AJGS-004-SB) Plutonium-241 Result -3.77 < MDA 6.18 > RDL 5 pCi/g 449877014 (L4-OFF-SOL-AJGS-B0 1-SB) Plutonium-241 Result 0.611 < MDA 6.06 > RDL 5 pCi/g Miscellaneous Information Additional Comments Samples 449877009 (L2-SUB-102-AJGS-024-SB), 449877011 (L2-SUB-102-AJGS-019-SB), 449877012 (L2-SUB-102-AJGS-001-AV) and 449877013 (L2-SUB-VAR-AJGS-004-SB) did not meet the resolution requirement of having a full width half maximum of 100 keV or less for the tracer; however, the tracer yield requirement was met and the tracer peaks are within the tracer region of interest. Product: Liquid Scint Fe55, Solid Analytical Method: DOE RESL Fe-1, Modified Analytical Procedure: GL-RAD-A-040 REV# 13 Analytical Batch: 1763512 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877009 L2-SUB-l 02-AJGS-024-SB GEL Page 50Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P843.556.8171 F 843.766.1178 www.gel.com
449877010 L2-SUB-l 02-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-019-SB 449877012 L2-SUB-102-AJGS-001-A V 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B01-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-l 03-AJGS-002-SB 1204026505 Method Blank (MB) 1204026506 449493001(Sl-102-CWD-FIFS-A01-SM) Sample Duplicate (DUP) 1204026507 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Recounts Sample 449877012 (L2-SUB-102-AJGS-001-AV) was recounted to verify sample results. The recount results are similar to the original results. Original results are reported. Product: Liquid Scint Ni63, Solid Analytical Method: DOE RESL Ni-1, Modified Analytical Procedure: GL-RAD-A-022 REV# 18 Analytical Batch: 1763518 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 22 Preparation Batch: 1763443 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877009 L2-SUB-102-AJGS-024-SB 449877010 L2-SUB-102-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-019-SB 449877012 L2-SUB-102-AJGS-001-AV 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B0 1-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-103-AJGS-002-SB 1204026518 Method Blank (MB) 1204026519 449493001(Sl-102-CWD-FIFS-A01-SM) Sample Duplicate (DUP) 1204026520 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. GEL Page 51Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P843.556.8171 F 843.766.1178 www.gel.com
Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Recounts Sample 449877015 (Sl-102-CWD-FIFS-A02-SM) was recounted to verify sample results. The recount results are similar to the original results. Original results are reported. Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 5 Analytical Batch: 1763527 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877009 L2-SUB-l 02-AJGS-024-SB 449877010 L2-SUB-l 02-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-019-SB 449877012 L2-SUB-102-AJGS-001-A V 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B01-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-l 03-AJGS-002-SB 1204026544 Method Blank (MB) 1204026545 449493001(Sl-102-CWD-FIFS-A01-SM) Sample Duplicate (DUP) 1204026546 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: LSC, Tritium Distillation, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 22 Analytical Batch: 1763551 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification GEL Page 52Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P843.556.8171 F 843.766.1178 www.gel.com
449877009 L2-SUB-l 02-AJGS-024-SB 449877010 L2-SUB-l 02-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-019-SB 449877012 L2-SUB-102-AJGS-001-A V 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B01-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-l 03-AJGS-002-SB 1204026611 Method Blank (MB) 1204026612 449877009(L2-SUB-102-AJGS-024-SB) Sample Duplicate (DUP) 1204026613 449877009(L2-SUB-102-AJGS-024-SB) Matrix Spike (MS) 1204026614 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Miscellaneous Information Additional Comments The matrix spike, 1204026613 (L2-SUB-102-AJGS-024-SBMS), aliquot was reduced to conserve sample volume. Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 16 Analytical Batch: 1763558 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877010 L2-SUB-102-AJGS-00 1-SS 449877011 L2-SUB-102-AJGS-019-SB 449877012 L2-SUB-102-AJGS-001-AV 449877013 L2-SUB-V AR-AJGS-004-SB 449877014 L4-OFF-SOL-AJGS-B01-SB 449877015 S 1-102-CWD-FIFS-A02-SM 449877016 L2-SUB-103-AJGS-002-SB 1204026632 Method Blank (MB) 1204026633 449877010(L2-SUB-102-AJGS-001-SS) Sample Duplicate (DUP) 1204026634 449877010(L2-SUB-102-AJGS-001-SS) Matrix Spike (MS) 1204026635 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and GEL Page 53Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P843.556.8171 F 843.766.1178 www.gel.com
procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Recounts Sample 1204026635 (LCS) was recounted due to low recovery. The recount is reported. Miscellaneous Information Additional Comments The matrix spike, 1204026634 (L2-SUB-102-AJGS-001-SSMS), aliquot was reduced to conserve sample volume. Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 16 Analytical Batch: 1765373 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 449877009 L2-SUB-l 02-AJGS-024-SB 1204030909 Method Blank (MB) 1204030910 449877009(L2-SUB-102-AJGS-024-SB) Sample Duplicate (DUP) 1204030911 449877009(L2-SUB-102-AJGS-024-SB) Matrix Spike (MS) 1204030912 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Miscellaneous Information Additional Comments The matrix spike, 1204030911 (L2-SUB-102-AJGS-024-SBMS), aliquot was reduced to conserve sample volume. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. GEL Page 54Laboratories of 60 LLC PO Box 30712 Char1eston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com
Page 55 of 60 Page: _ _ _ I _ _ _ of 2_ GEL Laboratories, LLC Proje_c_t # LACBWR GEL Quote#: COC Number(I': Site tfl 9.11 k~£ ~~~!eS~l~~io~~sy I Speclalcy Anal~ics Chain of Custody and Analvtical Request 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 PO Number: 672583 GEL Work Order Number: "1,,'t,1{ £) / / GEL Project Manager: Fax: (843) 766-1178 Client Name: La Crosse Solutions Phone# 608-689-4259 5 Sample Analysis Requested < > (Fill in the number of containers for each test) Project/Site Name: LACBWR-Genoa WI Fax # Should this <-- Preservative Type ( 6) sample be ~ ;;'; Address: 54601 State Road 35 considered: -~ °'z"" ., M e .0 0 UJ ;;: "'
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> For sample s//ippi11g a11d delivery details, see Sample Receipt & Review form (SRR.) Sample Collectio11 Time Zo11e: [ ] Eastern [ ] Pacific [X] Central [] Mountain [ JOther:
I.) Chain of Custody Number= Client Determined 2.) QC Codes: N = Normal Sample, TB= Trip Blank, FD = Field Duplicate, EB = Equipment Blank, MS = Matrix Spike Samplc. l\*1S D = Matrix Spike Duplic.itc S:m1plc, G = Grnb, C "" Composite 3.) Field Filtered: For liquid matrices, indicate ,,ith a - Y - for yes the sample was field filtered or- N - for sample was not field filtered. 4.) Matrix Codes: DW=Drinking \V:itcr, GW=Groundwatcr, SW=Surfocc Water, WW=Wastc Water, W=\Vatcr, l\fL=Misc Liquid, SO=Soil, SO=Scdimcnt, SL=Sludgc, SS=Solid Waste, O=Oil, F=Filtcr, P=Wipc, U=Urinc, F=Fccal. N=Nasal 5.) Sample Analysis Requested: Anal)1ical method requested (i.e. 82608, 6010B/7470A) and number of containers pro\'ided for each (i .e. 8260B - 3, 60/0Bl7./70A - I). 6.) PrcscrYati\'c Type: HA= Hydrochloric Acid, NI= Nitric Acid, SH= Sodium Hydroxide, SA= Sulfuric Acid, AA= Ascorbic Acid, HX = Hexane, ST= Sodium Thiosulfotc, lfno prcscrvati,*c is added= lca,*c field blank 7.) KNOWN OR POSSIBLE HAZARDS )Characteristic Hazards IListed Waste Other Please provitfe a11y additimral tfetai!s FL= Flammable/Ignitable LW= Listed Waste OT= Other/ Unknown below regartfi11g lra111flillg amllor disposal RCRA Metals I CO = Corrosive (F,K,P and U-listed wastes) (i.e.: High/low pH, asbestos. beryl/i11111, irritants, ot/rer co11cems. (i.e.: Origin ofsample(s), type As =Arsenic Hg= Mercury RE = Reactive Waste code(s): misc. /rea/t/r /razard,, etc) ofsite collectedfrom , odd matrices, etc.) Ba =Barium Se= Selenium Descriptio11: Cd=Cadmium Cr= Chromium Ag= Silver MR= Misc. RCRA metals ITSCA Re~lated PCB = Polychlorinated I Pb= Lead biphenyls
Page 56 of 60 Page: _ _ _2_ _ _ of 7
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> For sample shippi11g a111I tlelivery details, see Sample Receipt & Review form (SRR.) Sample Collectio11 Time Zo11e: [ ] Eastern [ ] Pacific [X] Central [ ] Mountain [ ] Other:
I.) Chain or Custody Number= Client Determined 2.) QC Codes: N = Nom1::il S.i.mplc, TB = Trip Blank, FD = Field Duplicate, EB "" Equipment Blilnk, MS= M;llrix Spike Sample, MSD = Matrix Spike Duplicate Sample, G = Gr.ib. C = Composite 3.) Field Filtered: For liquid matrices, indicate with a - Y - for yes the sample was field filtered or- N - for sample was not field filtered.. 4.) Matrix Codes: DW=Drinking \V::itcr. GW=Groundwatcr. SW=Surfocc W.itcr, W\V:=Wastc Water. W=W:ucr, ML=Misc Liquid. SO=Soil. SIFScdimcnL SL=Sludgc. SS=:Solid W.istc, Q::Qil, F=Filtcr, P=\Vipc, U=Urinc, F=Fccal, N=Nasal 5.) Sample An.1Iysis Requested: Anal}1ical mclhod requested (i .e. 8260B, 6010B/7470A) and number of containers provided for each (i.e. 82608 -3. 60/08O .J?0A -1). 6.) Preservative Type: HA ""' Hydrochloric Acid, NI= Nitric Acid, SH"" Sodium Hydroxide, SA = Sulfuric Acid. AA = Ascorbic Acid, HX = Hexane, ST = Sodium Thiosulfate, lfno preservative is added = leave field blank 7.) KNOWN OR POSSIBLE HAZARDS Characteristic Hazards I IListed Waste Other Please provitfe a11y atltfilio11a/ details FL = Flammable/Ignitable LW= Listed Waste OT= Other/ Unknown below regardi11g l1a11d/i11g a11dlor disposal RCRA Metals I CO= Corrosive {F,K,P and U-listed wastes.) {i.e.: High/ low pH, asbestos, beryllium, irritants, other c011cems. (i.e. : Origin ofsample(.v), type As= Arsenic Hg= Mercury RE= Reactive Waste codeM: misc. health hazard,*, etc.) ofsite cal/ectedfrom, odd matrices, etc.) Ba =Barium Se= Selenium Descriptio11: Cd=Cadmium Cr= Chromium Ag= Silver MR= Misc. RCRA metals ITSCA Re~lated PCB = Polychlorinated I Pb= Lead biphenyls
ma! I LaboratoriesL c SAMPLE RECEIPT & REVIEW FORM Client: Q,G Received By: Date Received: S I0
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FedEx Express F~ UPS Field Services Courier Other Carrier and Tracking Number Suspected Haianl Infonnation ,!! 0 *If Net Counts> l00cpm on samples not marked "radioactive", contact the Radiation Safety Group for further
,.... Z investigation.
Shipped as a DOT Hazardous? UN#: COC/Samples marked or classified as aximum Net Counts Observed* (Observed Counts - Area Background Counts): e:> (§bi1mR1Hr radioactive? Classified as: Rad 1 Rad 2 Rad 3 If yes, select Hazards below, and contact the GEL Safety Group. Is package, COC, and/or Samples marked HAZ? PCB's Flammable Foreign Soil RCRA Asbestos Beryllium Other. Sample Receipt Criteria Comments/Qualif iers (Required for Non-Conforming Items) Shipping containers received intact and Circle Applicable: Seals broken Damaged container Leaking container Other (describe) 1 sealed? Chain of custody documents included 2 with shipment? Preservation Method: Wet Ice 3 Samples requiring cold preservation within (0 !S 6 deg. C)?* lee Packs
*all temperatures are recorded in Celsius Dry ice Other.
TEMP: 21 c Daily check performed and passed on JR Temperature Device Serial #: _ _"'"'"IR....;.3;;....-....:.1..;..6_ __ 4 temperature gun? Secondary Temperature Device Serial# (If Applicable): Circle Applicable: Seals broken Damaged container Leaking container Other (describe) 5 Sample containers intact and sealed? Samples requiring chemical preservation Sample !D's and Containers Affected: 6 at proper pH? If Yes, Are Encores or Soil Kits present? Yes__ No_ (If yes, take to VOA Freezer) Do VOA vials contain acid preservation? Yes_ No_ NIA_ (If unknown, select No) Do any samples require Volatile VOA vials free of headspace? Yes_ No_ NIA._ 7 Analysis? ample ID's and containers affected: 8 Samples received within holding time? Sample ID's on COC match ID's on 9 bottles? Date & time on COC match date & time
-oot-s 10 on bottles?
Number of containers received match 11 number indicated on COC? Are sample containers identifiable as 12 GEL rovided? COC form is properly signed in 13 relinquished/received sections? Comments (Use Continuation Form if needed): C,\ , e,,N* e \..,/\ 0v~\ ect DO\-* s c;. , s -L-~ C:orr ect- ~CLrn-p lJL . PM (or PMA) review: Initials _ _ Q_JJ' _____ Date _ _...._+.-JW...,.-"'l'F-- Page _ L of-L GL-CHL-SR-001 Rev 5 Page 57 of 60
RE: Soils Received Today from Lacrosse, 05/10/18 - Sample Receipt ...
Subject:
RE: Soils Received Today from Lacrosse, 05/10/18 - Sample Receipt Discrepancy - Please Advise From: "Scott G. Zoller" <sgzoller@energysolutions.com> Date: 5/10/2018 2:02 PM To: "Edie Kent (emk@gel.com)" <emk@gel.com> CC: "Jason Q. Spaide" <jqspaide@energysolutions.com>, "Joseph D. Jacobsen"
<jdjacobsen@energysolutions.com>, "Bill M. Bishop" <bmbishop@energysolutions.com>
Edie, The L2-SUB-102-AJGS-001-SS is the correct sample to analyze. The sample time of 1205 is correct. The identification of the -SB sample ending is incorrect on the Coe and should be -SS. If you any further questions, let me know. Thank you . Scott Zoller From: Joseph D. Jacobsen Sent: Thursday, May 10, 2018 11:08 AM To: Scott G. Zoller Cc: Jason Q. Spaide; Joseph D. Jacobsen
Subject:
FW: Soils Received Today from Lacrosse, 05/10/18 - Sample Receipt Discrepancy - Please Advise Here is one for you ... Joe J From: Edie Kent [1] Sent: Thursday, May 10, 2018 11:06 AM To: Joseph D. Jacobsen; Jason Q. Spaide Cc: team.kent
Subject:
Soils Received Today from Lacrosse, 05/10/18 - Sample Receipt Discrepancy - Please Advise We did not receive sample L2-SUB-102-AJGS-001-SB. We did receive a container labeled L2-SUB-102-AJGS-001-SS. The data of collection matches L2-SUB-102-AJGS-001-SB but the time of collection does not match the chain. It is 12:05 . Please advise on whether the sample we received is the correct sample and if so, what the ID and time of collection are. Edie Edith M. Kent Project Manager Page 58 of 60 1 of2 5/10/2018 2:51 PM
RE: Soils Received Today from Lacrosse, 05/10/18 - Sample Receipt ... Laboratories LLC 2040 Savage Road, Charleston, SC 29407 I PO Box 30712, Charleston, SC 29417 Office Direct: 843.769.73851 Office Main: 843.556.81711 Fax: 843.766.1178 E-Mail: emk@gel.com IWebsite: www.gel.com Analytical Testing IEnvironmental IEngineering I Surveying Ci) 0 CONFIDENTIALITY NOTICE: This e-mail and any files transmitted with it are the property of The GEL Group, Inc. and its affiliates. All rights, including without limitation copyright, are reserved. The proprietary information contained in this e-mail message, and any files transmitted with it, is intended for the use of the recipient(s) named above. If the reader of this e-mail is not the intended recipient, you are hereby notified that you have received this e-mail in error and that any review, distribution or copying of this e-mail or any files transmitted with it is strictly prohibited. If you have received this e-mail in error, please notify the sender immediately and delete the original message and any files transmitted. The unauthorized use of this e-mail or any files transmitted with it is prohibited and disclaimed by The GEL Group, Inc. and its affiliates. http://www.gellaboratories.com Page 59 of 60 2 of2 5/10/2018 2:51 PM
List of current GEL Certifications as of 07 June 2018 State Certification Alaska 17-018 Arkansas 88-0651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 Delaware SC00012 DoD ELAP/ ISOl 7025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho Chemistry SC00012 Idaho Radiochemistry SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana NELAP 03046 (AI33904) Louisiana SDWA LA180011 Maryland 270 Massachusetts M-SC012 Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada SC000122018-1 New Hampshire NELAP 205415 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 South Carolina Chemistry 10120001 Tennessee TN 02934 TexasNELAP T104704235-18-13 UtahNELAP scooo 122018-26 Vermont VT87156 Virginia NELAP 460202 Washington C780 West Virginia 997404 Page 60 of 60}}