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Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey Conducted in 2014, Rev. 0, Appendix G, Part 7 of 11
	ML16294A198
Person / Time
Site:	West Valley Demonstration Project, P00M-032
Issue date:	08/22/2016
From:	; MJW Technical Services
To:	; Office of Nuclear Material Safety and Safeguards, State of NY, Energy Research & Development Authority, Office of Nuclear Reactor Regulation
Shared Package
ML16293A155	List: ML16293A130; ML16293A131; ML16293A132; ML16293A133; ML16293A134; ML16293A135; ML16293A136; ML16293A137; ML16293A139; ML16293A140; ML16293A141; ML16293A142; ML16293A143; ML16293A178; ML16293A179; ML16293A180; ML16293A181; ML16293A182; ML16293A183; ML16293A184; ML16293A185; ML16293A186; ML16293A187; ML16293A278; ML16293A279; ML16293A281; ML16293A282; ML16293A364; ML16293A365; ML16293A366; ML16293A367; ML16293A368; ML16293A389; ML16293A391; ML16293A392; ML16293A393; ML16293A394; ML16293A674; ML16293A675; ML16293A676; ML16293A677; ML16293A678; ML16293A808; ML16293A809; ML16293A810; ML16293A811; ML16293A812; ML16293A843; ML16293A844; ML16293A846; ... further results
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{{#Wiki_filter:Appendix G-Sub-Area 3.2 - COA

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Repmt Date: December 4, 20 I 5 Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228

Contact:

Ms .. Laurie Losey

      . . *"- _.. ~!~J_ect.:               . . . . S°'il. Radioisotopes Client Sample ID: 3.2. l .R. I                                                                                                                     Project:                MJWCOOl 15 Sample ID:                       .385070020                                                                                                       Client ID:               i\*1JWCOO!

Ma1rix: Soil Collect Date: 16-0C'T-15 15:05 Receive Date: 05-NOV-15 Collector: Client Moisture: 26.1% Parameter Qualifier Result Uncertainty MDC RL Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 26 l pcrcem CXCI 1 lilO/l5 1319 !521842 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Actimum-227 l! -0 125 +f-0 289 ll 536 pC1/g RXF2 12103115 1307 1522383 Antimony-125 u () 0292 +/-0.120 0229 pCi!g C'<:$ium-137 0.468 +/-0 126 0.0895 0 IQO pC1/g Cobalt-60 U. 0 00212 +/-0 0502 0.099 pC1lg Europium-154 u -0 00831 +i-0.157 \l.3Cll} pCllg Protactmium-231 u 0.568 ;./.() 585 I 19 pCi/g Radium-226 0 64 I +/-0.190 0.166 pCi/g Ra<lium-228 0.856 +1-0.261 0 377 pC1/g Tin-126 U 0 106 +/-0.177 0189 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AiB, solid "Dry Weight Corrected" /llpha 14 7 +/.J 11 3.45 400 pC1/g KXB2 12i02/l5 1125 1525757 3 Beta 22 9 +!-3.59 3.7J IO!l pCt/g

f.hc: f.(J!l_oyv,i~£;..~ri_:p !\1~~~~_4.s .~.cr~.P~ri~!1tti:d.:_ . . . ... ...... . . ... .... . . .. .. . .. . .............. _. . .... ... . . ... ,....................... _................ **-

Method Description Analyst Date Time Prep Batch biY s;,*,i *ri-e"P. **- *** ****** ** *D"..y-~foi.i"P'rcpciC-RAn-A::o2T*-**** ****--* *** ** * ** **** ****cxcf* - i"ii1(J/!5 * *****-**

ffi"~i* ******
t"s2Ts42 ** ******

The. foll.a.~ i.~¥.-~~'.':lyt~c~l.. ~~e~~?~s :'.'e:e._perf?J'ltl~d :.. _. ... .. . . . . ... . .... . .... . ..... .. .. . .... .. . .. . ..

.~Jetl!.o.<L            ******-*- ......_Qf!.s~.riptiq.1.1 ******-****- ....... *--*** .................. ***--* .... .                                       ......... Ana!_y!!t.C()!n.t:rl.<!!11,lL .......... -*** ...................... _....

ASTM D2216{Mod1fied) 2 DOE HASL 300, 4 5 2 3iGa-O I*R 3 EPA 900.0ISW846 93\0iSM 71 \0B Modified Notes: Counting Uncertainty is calculated at the 95% confidence level (I .96-sigma).

GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Anal;ysis Company: MJW Corpornlion Address: 15 Hazelwood Drive Suite 1l2 Buffalo. New York 14228 Report Date: December 17, 2015

Contact:

Ms. Laurie Losey Project Soil Radioisotopes Client Sample ID: 3.2. l .R. l Project: MJWCOOI 15 Sam~le ID: 3&5070020 Client ID: MJ\VCOOI Matm;: Soil Collect Date: 16-0CT-15 Receive Date: 05-NOV-J 5 C'ollector: Client Moisture: 26.1 %

 ~~~~.B.1~ter_      ..... -*** .... _9ual!~~r.: ..... Result _____ rJ*~~rt_a.i_ll~-". ....... ~f[)f:'..... Le           .... Tf'.r. ........ !l.1:.. _..~*.u.~ts.... Ilf'. _:\n_al,r.st    Dale Time Batch Mtd.

Gravimetric Solids ASTM D 2216 % Mois!llre "As Received" Mo18ture 26 l percent C'XCI - l \110115 1319 1521842 Rad Gamma Snee Arrnlysis Gamma.wee, Gamma. Solid "Dt}' WC!ight C01*1*ecfed" Actinium-227 u -0. 125 +/-0 289 0 536 0 248 +/-0 295 pC1/g RXF2 12i'03115 1307 1522383 2 Anllmony-125 u 00292 +1-0 120 0229 () 105 +!-0 121 pC1/g Bismutl1*2 I2 u 0 723 +i-t 05 l 65 (J 759 +/-1 10 pC:i/g Bismuth-214 0.641 +/-0.190 0 16& 0.0747 +/-0 19~ p('ilg Ccsium-137 0.468 +/-0 126 0 08')5 0.0401 +/-0 IJ2 0 100 pC'i!g Cobalt-60 l! 0 002.12 +i-0 0502 0.099 110421 +/-0 0502 pCi/g Europmm-154 c -000831 +/-0.157 0 30(1 0 130 +1-0.157 pCi!g Lead-212 I 21 +1-0.144 0 121> 00589 +/-0 175 pC1/g . Lead-214 0.983 +/.().215 0173 {J.07')6 +/-0 231 pC1/g l'olilss1um-40 143 +/-1.80 0.609 0.231 +/-2 18 p('t/g Prot;11;tinium-23 I Ul 0.00 +/-0.585 l.19 0 55& +/-0.651 pCilg Radium-226 064! +/-0. \90 0 166 0.0747 +!-0 198 pC1/g Radiutn-228 () 856 +/-0 261 0.377 0.168 +l-(1 286 pC1fg Thalhum-zog 0.343 +l-0 l09 () 074 I) 0328 +1-0l13 pCilg Tin-126 UI 0.00 +/-0.177 0.189 1).1)899 +/-O. l7S pC1fg Ratl GllS Flow l'roportional Counting GFPC. Gmss ;J B, solid "Dry Weight C'orrec1ed" Alpha 14 7 +l-4 l l 3.45 1 34 +!-5 00 400 pC1/g KXB2 12/02/15 1125 1525757 3 Bew 22 9 +/-3.59 3.73 1.72 +/-4 84 JO 0 pC1/g

 !ht! _f()~l11wii:ig J>r~p :V!~t.~_()?.S.~\'.t!_~CJler~~rlll~~ ........ **--*- ........................ .

Method Dc.~cription . Analyst Date Time Prep Batch Dry Soil Prep D1y Soil Prep UL-RAD-A-021 CXCI 11110115 1319 1521842 "f 11(!_ fo_l_~o~_i1_1_~-~!l;tl;rt.Ica.I ~I.cthod~. ~--~re r.~r.ro.i:n_1e~ *- _ ... Method Description I ASTM D 2216 \Modificd) 2 DOE l lt\SL 300, 4 5.2.3iGa-Ol-R 3 EPA 900 O!SW846 93 IO/SM 71 IOB Modillcd Su rrogate!fracer Recover}' Test Batch LO Rec1wcry% Acceptable Limits

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis C.ompany: MJ W Corporation Address: I :i Hazelwood Orivc Suite 112 Buffalo. New York 14228 Report Dnte: December 17. 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.1.R. I Project: MJWCOOI 15 Sample ID: 385070020 Client lD: MJWC'OOl Surrngateffcaccr Recovery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( l.96-sigma).

GELLABORATO~ESLLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Sui1e 112 Buffalo. New York 14228 Report Dme: December 17. 20!5

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample lD: 3.2.i.R.I Project: MJWCOOl 15 SamelelD: 385070020 Client ID: MJWCOOJ Matrix: Soil Collect Date: !6-0CT-15 Receive Date: 05-NOV-15 Collector:. Client Moisture: 26.1% Parameter Gra\*ime!ric Solidi1

  /JSTM D 2216 % Mois111re "As Received" Moisture                                                  26.1                                                                                           percent        CXCl   I l/Hl/15 1319  1521842 Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "D1:1* lf..eig/11 Corrected" Actmium-227                               u           -0 125          +/-0.289                 0 536      0 248               +/-0 295                     pCi/g        RXF2   12/UJ/15 1307 1522383     2 Ant1mo11y-125                             11          0.0292          +1.0.120                 () 22*;    ll l(J5             +/-0 121                     pC1/g Bismuth-212                               lJ            CJ.723         +l-1 05                    \.(15   0759                  +/-LIO                     pCilg*

Bismuth-214 0641 +/.() 190 () 166 0 0747 +/-0.l'IS pC'ilg C'esium-l 37 0468 +f-0 126 0 0895 00401 +l-11132 0 100 pCilg Coball-60 u 0002!2 +/-0.0502 0.099 0.0421 +/-0 0502 pC1lg Europium-154 LI -0.00831 +/-{} 157 0 3(10 0 130 +/.!) 157 pC1/g Lcad-212 1.21 +f-U !44 0 126 0 0589 +/-0 175 pC1/g Lcad-214 0 983 +/-ll.215 0 173 0 0796 +/-0.231 pC'ilg Potassium-4 0 143 +/-1.80 0609 0 231 +/-2 JS pCitg Protattinium-231 Ul ()00 +/-0 585 l 19 0 556 +/-0 651 pCi/g Radium-226 ll.641 +/-0. \90 0 166 ()0747 +1-0.198 pCilg Radium-228 0.&56 i-/-0.261 0.377 0 !68 +(-0286 pCi/g Thallium-208 0 343 +1-0.109 0074 0 0328 +/-0 113 pCi!g Tin-126 Ul 0 00 +/-0.177 {) 189 0.0899 +/-0 17~ pC1!g Rad Gas Flow Proportional Counting GFPC, Gross A:B, solid "Dt:v Weig/If Corrected" Alpha 14 7 +/-411 3 45 1.34 +l-5.00 400 pCi/g KXB2 11102115 l I25 1525757 3 Beta 22 9 +1-3 59 173 I 72 +/-4.84 LOO pCilg T~~. roH<mJ~R!':r.ep i\Ij!thl)ds..~r.~_perf.o.r:~c~ ....... **- ***- ............... " ................ *- ...... *-* ........ *- ..... *-. Method Description Analyst Date Time Prep Batch Dry Soll Prep Dry Sml Pr~'P OL-RAD-A-021 CXCI 11/10/15 1319 1521842 Th~ _fon.o,~!.ng.:'.\~'.1_1yt_i~al.~~th.()~ls.:w.~.r:c.P~r.f()~m.c~. _ .................. _...... ---* _ .. .... *-*- .. . . ... . l\rlethod Description ASTM D 2216 (Mod1!icd) 2 DOIO liASL 300.4.5 2*.JrGa-Ol-R 3 EPA 900.0/SW846 93 lOiSM 71 toB Modified Surrogateffr:iccr Recovery Test Batch ID Recovery% Acceptable Limits

- - - - - -f - - - - - - - - - - - - - - - - GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJ W Corporation Address: 15 l-lazeh~ood Drive Snite 112 Buffalo, New York 14228 Report Date: December 17. 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.l.R. J Project: MJWCOOJ 15 Sample JD: 385070020 Client ID: MJWCOOl Pan~fll~le~- .. . . .. .. . ... _9~~1~_fic.r.. ___ ......Il~su_ft_ .. __l'nc~rtaintv ..... ;vi_[)C ..... ~c ....... __ . "P'V ......... )l~ .. ~:_ll_il~ .1?*~- -~trn_lys._t__ .. l?!l_le _T.iine__ !3.ll_t_i;~----~l_td_._ Surrogate(fraccr Rcco\*cry Test Batch JD Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 2015 Compru1y: MJW Corporation Address: 15 Hazelwood Drive Suite l 12 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.l.R.5 Project: MJWCOOJ 15 Sample ID: 385070021 Client lD: MJWCOOJ Matrix: Soil Collect Date; !6-0CT-15 14:05 Receive Date: 05~NOV-15 Collector: Client Moisture: 26.1% Parameter Qualifier

Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 26 I percent cxc l 11/I0/!5 13!9 1521842 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight CoJTected" Plutomum-23B IJ 0 ll398 +1-0.0682 0 05'J7 \.00 pCifg HAKB 11123/15 1501 1522577 2 Plutonmm-239/240 U -0.0223 +/-0.076 0.188 t 00 pC1lg ASP Uranium Isotopic, Solid "Dry Weight Corrected" Urann*m-232 U -0.0077 +l-0 0532 0 12') 1 00 pcilg l!AKl3 11124115 0851 1522580 3 Uranium-2331234 0 738 +/-0 260 () 126 1.00 p~1/g Uramum-2351236 0.159 +1-0.127 0 0683 I OU pcilg Uranmm-238 L09 +/-0.312 !l.0681 LOO pci/g Alphaspec Np237, Solid "Dry Weight Corrected" Neplumum-237 ll *O 083 +/-0.157 0.485 I 00 pCilg HAKB 11123115 1707 1522576 4 Alphaspec Th2.29 + 228,230,232 Sol.id "Dry Weight Corrected" Tiiorium-22& 0.992 +/.Q 587 0.6(>3 LOO pCi!g 11AKB 11124/15 1.G\4 1522579 s Thorium-229 U -0.0684 +l*O 279 0.659 IOCl pC1/g Thonum-230 l.l 6 +/-0.006 0629 LUO pCilg Thormm-232 0.6<>3 +/-0 431 OJ49 I 00 p(1/g Arn24 I, Cm Solid "Dry Weight Corrected" Ameri~ium-241 U -0.Ql63 +/.(J.0308 0 ()951 \ 00 pC1/g HAKB 11124!15 !042 1522571 6 Cunum-N2 U -00!52 +/-0035\ 0 104 l 00 pCilg Curium-243/244 U 0 00697 +/-0 03g7 0 0743 LOO pCtlg Cur1um-245i246 X 0 0775 +/-0.0748 0 0465 1.0ll pC1!g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U -0.504 +l-6.04 \0.5 15() pCi/g HAK.B 11125'15 1132 1522578 7 Rad Gamma Spec Analysis Gamma 1!29, Solid Dry Weight Corrected"

 !odinc-129                                             U              -0 l!J9            +1-0 287    . 0447        1.00   pCilg         MJHI   12i02/15  1441 1522374   8 Gammaspec, Gamma, Solid "Dry Weight Corrected" Aclmium-227                                            U               -0.16             +l-0:283       0.48&             pCi/g         R.XF2 !2i03/15   !307 1522383   9 Antimimy-125                                           ll         -0.00147               +/-0.lOS       1119!!            pCi!g Ccsium-137                                                              O 543           +1-0 0972     00808      0.100    pCJ/g Cobalt-60                                              U              00104             +!-OJJ271     00653               pCi/g Europium-154                                          U            -0.0576              +l-0 136       0242              pCi/g Protactimum-231                                       U                0.844             +/-0 607        1.1 ll           pC1/g

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 20 l5 Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228

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Ms. Laurie-Losey Project; S~il _Rad~ois_ot°.pe_~_ .. ......... **-* .. Client Sample ID: 3.2.1.R.5 Project: MJWCOOJ 15 Sample lD: 385070021 Client ID: MJWCOOI Rad Gamma Spec Analysis Gammaspcc, Gamma, Solid "Dry Weight Corrected" R.adiwn-226 0 886 +/-[) 155 0.149 pC1lg Radium-228 0.664 +/-0 346 0272 pCJ/g Tin-126 ll 0.064 +/-0.128 0 162 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha 13 7 +!-4 03 H8 4.00

pCilg JXl37 12i02115 1221 1525762 10 Beta 229 +1-2 95 2.20 JOO pCi/g GFPC, Sr90, solid "Dry Weight Corrected"-

Strontium-90 l.J -0.702 +/-0 599 I 38 2 0() pCi/g. KSDl I2i02/15 1655 1525755 II Rad Liquid Scintillation Analysis LSC. Tritium Dist, Solid "Dry Weight Con-ected" Tntium u 1.88 +l-2 06 343 6.00 pC1lg TXJI 12102115 1459 1522724 12 Liquid Scint CJ 4, Solid "Dry Weight Corrected" Carbon-14 u -0.282 +/-0 648 I II 2 00 pC1lg TXJl 12104115 0155- 1522716 13 Liquid Scint Tc99, Solid "Dry Weight Corrected" l'echnetium-99 u 1.88 +/-1.70 2 83 5.0lJ pCi/g MYMI 11129/15 1110 1522715 [4 T~~..foHc_i_w!ng_Prep ~1eth~~.\.V~re__p~_rfo.r.!l1e.~=-*****-* ...... __ .. . Method . Description Analyst Date Time Prep Batch or;**scili P-fcii ** * ***-- ***- *** **** *****oi}* soiriirep.ol.~RA.o~;\~oi*1 **** *** *************** cxC.'i .. *** *** *

1"1hoii:i" ********- 1Ti9. *-*** *i.s21s42

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company; MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: 0 00* 0 0 **** 0 o**o 0 0000 Soil Radioisotopes 0 *--M****** -****** Client Sample ID: 3.2. 1.R.5 Project: MJWC00!15 Sample JD: 385070021 Client ID: MJWCOOI _Th_~ __fol_l_~Y'.'.~~-g :\'~~l~tic:_a~- ~-e,t~c_>~~- ~-:re_ perf.ori~~~-=. ___ _ M~_t!lQ~ . . . . ... . .. . ... .-* . .Qe~.ci:i_p!i.0.11 _-** ***-** ... . . _. ASTM D 2116 (Modified) 2 DOE EML HASL-300. Pu-1 I-RC Modified 3 DOE EML 111\SL-300. U-02-RC Modified 4 ASTM C 1476-00 Modified 5 DOE EML HASL-300, Th-01-RC Modified Ii DOE EML HASL-300, Am-05-RC Modified 7 DOE EML HASL-300, Pu-11-RC Modtlfod g DOE EML l*IASL-300,1-01 Modified !I DOE HASL 300, 4.5.2 3/Gu-01-R IO EPA 900.0iSW846 9310/SM 71 IOB Modified 11 EPA 905.0 Modified!DOE RP501 Rev I Modified 12 EPA 906 0 Modified 13 EPA £ERF C-01 Modified 14 DOE EML HASL-300, Tc-02-RC Modified ~-urro~ate/_Trac.~~ {l~c_O\'.e_ry___ . _Te.~.~- __ ........................ *-*-**-* ****- _...... _...................... _~~~ult Nominal .. R.:eC<:J':/~f)'.o/.~ .f:.~cer.t.~ble__q_mits Plutonmm-242 Tracer ASP Plutm1ium !sotop1c. Sohd "Dry Weight 807 (15%-125%} Corrected Uramum-232 Tracer ASP Uranium Isotopic, Solid "Dry Weight 65B 115%-125%) Corrected Urunium-2351236 Trncer ASP Uramum Isotopic. Solid "Dry Weight 66 8 (15%-125%) Corrected" Amencium-243 Tracer Alpha~pec Np237. Sol 1d "Dry We1gh1 Corrected" 90 3 (!5%-125%) Aclm*um-227 Tracer Alphaspec Th229 + 228,230,232 Solid "DI)* &.J..8 {!5%-125%) Weight Corrected Americium-243 Tracer Am241, Cm Solid "Dry Weight Corrected" 90 8 (15%-125%) PI utonmm-24 2 Tracer Liquid Scint Pu24 I, Soltd "Dry Weight Correctl!d" 80.7 (15%-125%) Strontium Camer GFl'C. Sr90, ~olid "Dry Weight Corrected" &9 9 {25%-125%) Technetium-99m Trnccr L1qmd Scmt Tc99, Solid "Dry Weight Corrected" 98.1 (15%-125%) Notes: Counting Uncertainty is calculated at the 95% co1Jfidcnce level ( 1.96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis

         . Company:                MJW Corporation Address:                15 Hazelwood Drive Suite 112 Buffalo. New York 14228                                                                               Rcp6rl Date:  D~ccmber ! 7, 2015

Contact:

Ms; Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.1.R.5 Project: MJWCOOllS Sample ID: 38507002 l Client lD: MJWCOOl Matrix: Soil Collect Date: \6-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 26.!% PatalJl.~!.~.~ .................. quaHfie_r_ . Result .. -~:r.iee.rt.:i_inty. MDC Le TPl' Gravimetric Solids AST?.1 D 2216 % .\4oislure As Received" Moisture :26 L per~cnc CXCJ ll/10/15 1319 1521842 Rad Alpha Spec Arsalysis ASP Phitoni11m Isotopic, Solid "Dry Weight Corrected" Pluiomum-238 0.0398 +f.O 0682 0.0597 () 00 +-1-0 0635 1 00 pCi/['. HAKB 11123115 1.501 1522577 2 Plutonium-2391240 u -0 0223 +/-0.076 0 188 0.0643 <-f-0 0761 I 00 pCi/g ASP Uranium Isotopic. Solid "fJry Weig/it Corrected" Urarnum-232 u -0 0077 +f-0.0532 0.129 () 0385 +/-0 0533 I 00 pc1/g 1-IAKB 11/24115 085 l 1522580 llnuuum-2331234 0 738 +f-0 260 0.126 0()288 +f-0 301 I 00 pci/g Uram1J111-235/236 0.159 +f-0 127 00683 000 +/-0.131 1.00 pct!g l/ranium-238 \.09 +/-0.312 (J.068! 0.00 +/-0384 1 00 pci/g A/phaspec Np237, Solid "D1:~* U-'eight Corrected" Ncptumum-237 u -OlllH +f-0. \51 0 485 ll 139 +/-0 157 \ 00 pC'i/g HAKB I l/23fl5 1707 1522576 4 Alplraspec Th229 ~ 228,230,232 Solid DI')' Weight Corrected" Thorium-2W 0 992 +/-0.587 () 663 0 233 +f-0 609 I 00 pC1lg HAKB 11124/IS 1014 1522579 5

    *niorium-229                             .U     -0 0684        +/-0 279          0.659      () 234    +l-027'1        1.00   pCilg Thormm-230                                             I 16    +/-0.606          0.629      0220       <-1-0 634      LOO    pCtlg Tnonu111-232                                        il.663      +l-0 431         {) 349   U.0799       *t-/-0.444     I 00   pC1/g Am2./J, Cm Solid "D1~* Jl!eiglzt Corrected" Americium-241                             u     -0.0163       +/-0 0308        0 0951     0 0272     +/-0.03(!9       l 00   pC1/g         HAKB 11/24115 1042 1522571     6 Cimum-242                                 l)    -0.0152       +/.1)0351          0. \04   {) 0284    +/-0 0352        I 00   p(Vg Curium-2431244                            u      0 00697      +1-0.0387        00743        0017     +/-Cl.03&8       1.llO  pCilg Curium-245/246                            x       0.0775      +l-0 0748        () 0465         0 Oil +l-0 0754"       \ l!O  p('1!g Uquid Scint.fu241. Solid "Dry Weigh! Con*ected

Plutomum-241 lf -0 504 +l-604 105 5.08 +1-6 04 15.0 pCi!g HAKB I !125/15 1132 I 522578 . 7 Rad Gamina Spec Analysis Gamma I 129. Solid "D1:1* Weight Cor/'ecced" lodine-129 lJ -0109 +/-0.287 04.J.7 () 204 +/-0.291 1.0() pCt!g MJH l 1210211 S 1441 1522374 8 Gamina.spec. Gamma, Solid "D1:r IYeighl Corrected" Aclimum-227 u -0 16 +J-0.28J 0.483 0.228 +/-0.293 p('1lg RXF2 12i03fl 5 1307 1522383 'l Antunony-125 u -0,0()147 +1-0 105 0 193 00914 +/-0 105 pCilg

    !31smuth-2 \2                             UJ           0.00     +/-0.889            I .JB   ()694        +1-1 30             pCilg_

13tsmulh-214 0.886 +/.Q 155 lJ.149 0.0683 +/-0.171 pCi!g Ccsmm-137 ll.543 +f-0.[)972 0.0808 0 ll369 +/-IU06 0.100 pCi/g Cobalt-60 u 0.0104 +1-o.o:n1 IJ0(*53 0 0273 +l~O 0271 pCi!g Eur11pmm-154 LI -00576 +/-0.136 !l.242 0.107 +f-0 138 pC1lg Lead~212 () 986 +/-0.129- a 114 0.0539 +l-0. \56 pC1!~ Lead-214 0.997 +!-0 167 0.154 0.0715 -r/-0. 186 pCi/g

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 55&-8171

www.gel.com Certificate of Analysis Compan}': MJW Corporation Address: 15 Ha;r,elwood Drive Suite 112 Buffalo. New York 14228 Report .Date: December 17, 2015

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Ms. Laurie Losey Project Soil Radioisotopes Client Sample ID: 3.2.1.R.5 Project: MJWCOOJ !5 Sample lD: 385070021 Client ID: MJWCOOI Parameter Date Time Batch Mtd. Rad Gamma Spec .Annlysis Gammaspec, Gamma, Solid "Dry Weight Correr:t1?d" Potus~ium-40 13 8 +l-1 49 () 6113 ll.248 +I-I 92 pC1/g Protacumum-23 l

U! 0.00 +1-0 607 I 10. 0 517 +1-0 742 pC[/g Rn<lmm-226 0.886 +/-0 155 u 14') 00683 +/-0 171 pCtlft Radiuni-228 0664 +/-0 346 0272 0.121 +/-0.358 pC1/g Thallium-208 {) 303 +/-0.0876 0.0665 0.0301 +/-ll.091 pCilg Tm-126 .u 0064 +/-0.128 0 I (12 () 0778* +/-() 129 pC1lg Rad Gas Flow Proportional Counlinp:

GFPC, G/'oss A'B. solid "Dry Weigh! Corrected" Alpl1a . 13 7 +/-4.03 388 I 58 +/-4.85 4.00 pCr/g JXB7 12i02/15 1221 1525762 10 Beta 22 9 +/-2 95 2 20 {) 984 +/-4 50 100 pCi/g GFPC. Sr90. solid "Dry Weight Corrected" Stronuum-90 lJ -0 7()2 +f.(l 599 1.38 ll.602 +/-0 599 200 pCi/g KSDI 12102115 1655 1525755 11 R:id Liquid Scintillation Analysis LSC. Tri1ium Dist. Solid "Dry Weight Co/'/"ecled" TriLtum 1.&8 +1-2 06 3'13 1.50 +i-2 06 6.00 pCilg TXJI 12102/15 1459 . 1522724 12 Liquid Sein/ C 14. Solid "Dry Weigh! Corrected" Carbon-14 U -0 282 +/-0.648 I II 0.548 +l-0 648 2.00 pCilg TXJI 12!04/15 0155 15227[0 u Liquid Scilll Tc99, Solid "Dry Weigh! Corrected" Technetium-99 1.88 +I-I 7() 2.83 I 36 +/-I 72 5 00 pCi/g MYM 11/29/15ll10 1522715 14 I

r.11e... ~O.!~o.wing_P_r.ep _l\'~~t_h.O.~ls-~e.r.e.Jler.~orin~d ........................ _.... . , .. **~

Method . Description Analyst Date Time Prep Balch Dry Soil Prep Dry Soil Prep GL-RAD*A-021 C'XC'l I l/10115 1319 1521842. .'!'~~--~o_l~IJ.'V..i1?-g_}\nalytiea_l__ ~lc!l1.<!~.l!'_:"l'.~~c r..e~ro.r.111~!1 .. -* ..... *--*. -*** ... _..... . ~tethod Description ASTM D 2216 (Modifietl) 2 DOE EML HASL-300. Pu-! !-RC Modified DOE EML MASL-300. U-02-RC Modified 4 ASTM C 1476-00 Modified 5 DOE EML HASL-300, Th-Ol-RC Modified 6 DOE EML !-1ASL-30tl, Ani-05-RC Modiffcd 7 DOE EML HASL-300, Pu-11-RC Mollified 8 DOE EMI. HASL-300J-Ol Moo[fi~d 9 DOE HASL 300.4 5 23/Ga-01-R JO EPA 900.0ISW846 9310/SM 711013 Modified 11 EPA 905 0 Modified/DOC: RP501 R~v. I Modified 12 EPA 906.0 Modified 13 EPA EERF C-01 Modified

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: l\i!JW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Report Date: December 17, 2015

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!vis. Laur.ie Lose}' Project: Soil Radioisotopes Client Sample ID: 3.2.1.R.5 Project: MJWCOO 115 Sample ID: 385070021. Client ID: MJWCOOJ Parameter Result Cncertainh' MDC Le TPL... _ ...... ...l~.i:. ....... ~'.fl.!!.S. _ P~ . .r\!J.:ct!Y.~.~ Date Time Batch !\.-ttd. 14 DOE EML HASL-300. T~-02-RC' Modified Surrogatcffracer Recovery Test B:iteh ID Recovery% Am~ptJJble Limits Plutonium-242 Trace*r ASP Plutonium Isotopic, Solid Dry \Veight Corrected" 1522577 80.7 (l5%*125%) Uranium-232 Tracer ASP Uranium lsotopic. Solid "Dry Weight Corrected" 1522580 65.8 (15%-125%) Uranium-235/236 Tracer ASP Uranium Isotopic, Solid "Dry Weight Corrected" 1522580 66.8 (15%-125%) Americiurn-243 Tracer Alphaspcc Np237, Solid "Dry Weight Corrected" 1522576 9(}.3 (15%-125%) Actinium-227 Tracer Alpha.;;pec '1'11229 + 228,230.232 Solid "Dry Weight Corrected" 1522579 84.8 (15%-125%) Americium-243 Tm;cr Am24 l. Cm Solid "Dry Weight Corrected" 1522571 90.8 {15%*125%) Plutonium-242 Tracer Liquid Seim Pu24 I. Solid "Dry \Vcight Corrected" 1522578 80.7 (15%-125%) Strontium Currier Gl'PC', Sr90, solid "Dry Wcighl Corrected" 1525755 89.9 {25%-125%) Tccl1nctiurn-99m Tracer Liquid Scint Tc99, Solid "Dry Weight Corrected 15227!5 98.l (15%-125%) Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: lv1JW Curporation Address: 15 Hazelwood Drive Suite l l2 Bufralo. New York 14228 Report Dntc; December 17. 2015

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Ms. Laurie Losey Project: Soil Radioisotopes Client Sample lD: 3.2.1.R.5 Project: MJWCD0115 Sample ID: 385070021 Client ID: MJWCDOl Matrix: Soil Co!lectDate: 16-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 26.1% l'ara~ete~.. *****-** .. __ .... _.9~~-~i.l_!.~r, _ Result l.'.ncertninh*

                                                          .......................... MDC           Le .......... TP..L ...   . ..R.."" ... l_:_o_its .. DF .:~n.i:i!~:st....})at~. T.~_n1_c___Batc.11 . ~Hd.*.

Grm.-imcti*ic Solicls ASJ;111f D 2216 %Moisture "11s Receil*ed" Moisture 26.1 percent CXCI- I lll0/15 1319 1521842 Rat.I Alpna Spec Analysis ASP Plutonium Isotopic. Solid "Dry Weigli1 Cm-reeled" Plutomum-238 0 0398 +l-0.0682 () 0597 000 +1-0 0685 1.00 pC1/g HAKB I LQ.3/15 1501 1522577 2 Pluronium-239/240 u -0.0223 +/-0.076 0 188 O.U643 +l-0 0761 I 00 pCi/g ASP [,'ranium isotopic. Solid "Dry Weighl Corrected" IJr.amum-232 u -0.0()77 +{.!) 0534 0.129 0 0385 +1-0.0533 I 00 p~!lg HAKB 11/24115 0851 1522580 3 L'ranium-233.1234 0.738 +/-0 260 0 126 0.0288 +/-0 301 1.00 pci!g t.:rarnum-235i236 n 159. +/-0.127 [) 0683 0 00 +/-0 131 I.OU pci/g Urnmum-238 I 09 +l-0 312 () 0681 0.00 +/-0.38.4 1.00 p<:ilg Afpliaspec Sp237, Solid "Dry Weight Corrected" Neptunium-23 7 u -0.083 +/-0 157 () 485 0.139 +/-0.!57 1 00 pCilg llAKLl \ 1123115 \707 1522576 4 A!pha~pec T!1229 + 228.230.232 Solid."Dry Weight Corrected" Thonum-228 0.992 +/-0.587 0.66J 0.233 -t-/-0 609 1 on pC1/g HAK.B 11124/t 5 1014 1522579 5 Thonum-229 u -0 0684 . +/-0.27'l 0 659 0234 +/-0279 1.00 pCi/g Thorium-230 l 16 +/-0 606 I} 629 0220 +/-0.634 100 pCi/g Th.om.mi-232 0.663 +/-0 431 0.349 0.0799 +/-0.444 1 00 pCl/g Am241. On Solid "Dry Weight Corrected" Amcricium-241 u -00163 +/-0 0308 00951 00271 +/-0.0309 - l 00 pC1/g HAKB 11124115 !042 1522571 6 Curium-242 u -00152 +1-0.0351 0 104 0.0284 +/-0.0352 1.00 pC'1/g Cur1um-24 31244 u O.OD697 +/-0.0387 0.0743 0017 +/*O 0388 ].{)0 pC1lg Cmium-2451246 x 0 0775 +1-0 0748 00465 O.Ull ..1.0.0754 1 ()() pCilg liquid Scinr Pu24 l. Solid "Dry Weight Corrected Plutomurn-241 lJ *0.504 +/-6.04 I0.5 5.08 +/-6.04 15.ll pCilg llAKB 11125115 1132 \522578 7 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Cor*rected" lodine-129 u .o 109 +/-0.287 0.447 0.204 +1-0 291 1.00 pC1/g MJHl 12102115. 1441 1522374 8 Gammaspec, Gamma. Solid "Dry Weight Corrected" Acliniurn-227 ti -0.16 +l-0 283 0.488 () 228 +1-0 293 pCilg RXF2 12i03/l5 1307 15223113 9 Anlimony-125 u -0.00147 +/-U.105 0.198 00914 +/-0.105 pC1lg Bismuth-212 UI 0 00 +/-ll.889 I 48 ll.694 +/-l .30 pCilg Bismuth-214 0.886 +/-0.155 0 149 0 0683 +/-0 l 71 pCi!g Ccsium-137 0.543 +/-0.0972 U 08llR . IJ.0369 -;-/.() 106 0. \00 pC1/g Cobah-60 u 0.0104 +/-0.0271 0.0653 0 0273 +/-0 0271 pCilg Europium-154 l! -0 0576 +/-0 l31i 0242 0.107 **l*ll t 38 pCi/g. Lcad-212 0.986 +/-0 129 0 114 (J 0539 +!-0. \56 pCilg Lead-214 0 997 +/-0 l67 () 154 0 0715 +/-0.186 pCt/g

                                                                                                                                                                                                                                     -  --~--.*---- _ _ _                         '

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 5.56-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazel\\ood Drive Suite 112 BufTalo.NcwYork 14228 Report Date: December 17. 2015

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Ms. Laurie I .owy Project: Soil Radioisotopes Client Sample ID: 3.2.1.R.5 Project: MJWCOOl 15 Sample ID; 385070021 C!i~nt ID: MJWCOOl

                                                                                                '.\:lDC              Le Rad Gamma Spec Analysis Gammasp<!c:, Gamma. Solid "Dry Weight ('01*rected" Potassimn-40                                                     . 13.8              +/-1.49        {) 603          0.248            +/-1.'12                               pCi!g Protactmium-231                                       UI             0.00          **1-0.607           I Ill        0 517          +l-0 742                                 pC1!g Radmm-22/i                                                         0 88(,          +/-0.155         () 149        0.0683           +l-0 171.                                pCilg Radium-228                                                        0.664           +/-0.346         0 271           0.121          +/-0.358                                 pCitg Thallium-208                                                       0 303          +1-0.0876       0 0665          () 0301          +/-0.091                                 pCl/g Tin-126                                                u           0064            +/-0 128         0 162         0 0778           +i-0 129                                 pCi/g Rall Gas Flow Proportional Counting GFPC. Gross A.'B, solid "D1:r Weight Correctr:d" Alpha                                                               1!7             +/-4.03          3.88             1.58         +/-4.S5                    4 00         pCi/g                        JXB7           12/02115 1221                   1525762             10 Beta                                                                229             +/-2 95          2.20          (J 984          +/-450                      10.0        pCi/g GFPC. Sr9D. solid "DrJ' Weight Corrected" Strontium-<JU                                          U          -0.702           +/-l).599           1.38         (l 602         +!-0 599                    2 DO         pCi/g                        K:SDI           12!02/15 1655 1525755                              II Rad Liquid Scintillation Analysis LSC.* friliwn Dist. Solid "DtJ' Weight ('01rected 11 Tntium                                                              l 88            +/-2:()6         3 43             l 50         +/-2.06                    6.00 . pC1/g                             *TXJ\            12/02115 1459 1522724                              12 Liquid Sci'nt Cl4. Solid "Dry Weight Corl'ected

Carbon-14 U -0.282 +/-0 648 1 11 l) 548 +/-0 648 2.llO pCi/g TXJ! l2i04/l 5 OJ 55 1522716 13 Liquid Sein/ Tc99. Solid "Dry Weight Corrected" Teclmctium-99 1 88 +/-1.70 2 S3 136 +/-1 72 5 00 pCilg MYM 11129115 1110 1522715 14 I T.~.c .fO.!l_1n~:i.11g _Pre.I? ..~:lc_t.f!.O.~.S...~:~r~ p~_r.ro.rl!.'e~ ....... . ..... ...... .. *-*****-* ..... ****** ............ . ..... ..... ............ . ......... .. ....... Method Description Annlysl Date Time !'rep Batch D1y Soi.I Prep DrySClil Prep GL-RAD-A-02 l CXCJ 11/10/15 1319 1521&42 Thc..ft>.!.1.0.~~}f.!g .*~-'~~Y.1.~~l_l\-!_l:t~a.d.s._wcr.c pc,i;for~~d Methotl Description

ASTM D2216(Modified) 2 DOE EML HASL-300. Pu-11-RC' Modified 3 DOE EML HASL-300. li-02-RC Modified 4 ASTM C J476-00 i\fodificd 5 DOE EMI. HASl.-300. Th-OJ-RC Modified 6 DOE EML HASL-300: Am-05-RC" Modified DOE EML HA SL-JOO, Pu-I I-RC l\iloditicd DOE EML H.l\SL-J00.[-01 Mod1lied 9 DOE llASL 30(!,4.5 2.3fl3a.-Ol-R JO EPA 900.0/SW846 93 IO.ISM 7 l \OB Modified ll EPA 905.0 Modified/DOE RP50 I Rev I Mod1fkd 12 EPA 906.0 Modtticd 13 EPA EERF C-01 Mod11icd

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Rcporl Date: December I 7, 2015

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Ms. Laurie Losey Project: Soil Radioisotopes C'!ient Sample ID: 3.2.1.R.5 Project: MJWCOOl 15 Sample ID: 385070021 Client JD: MJWCOOl Parameter ..9.?.'.l!i~_~_r. .......}~_e.s_~l!_ .... JLn£~r.!!!Jr1_~y__ ..... _l\:l!?.f__ .... ___I~~ ...............Tl'..L _. . RL .l 'nits °-~- ,\n:iirs~ _~a!~ __!_in1c_ Batch ~Hd. 14 DOE BML l-IASL-300, Tc-02-RC Modified Sutrogatcrfraccr Recovery Tesl Batch ID. Recovery% Acceptable L_imits Plu\oaium-242 Tracer ASP Plutonium Isotopic. Solid "Dry Weight Corrected" 1522577 80.7 (15%-115%) Uranium-232 Tracer ASP Uranium Isotopic. Solid "Dry Weight Corrected" 1522580 65.8 (15%-125%) Urnnium-2351236 Tracer ASP Uranium Isotopic, Solid "Dry Weight C"orrcctcd" 1522580 66.8 tl5%-125%) Americium-243 Tracer Alphaspcc Np237, Solid "Dry Weight Corrected" . 1522576 90.3 <150..;,: 125%J Actiniurn-227 Tracer Alphaspec 'rh22C} + 228,230.232 Solid "Dry Weight Corrected" 1522579 84.8 (15%-125%) Arncricium-243 Tracer Am24 l. Cm Solid "Dry Weight Corrected" 1522571 90.8 (15%-125%) P lutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 1522578 80.7 (15%-125%} Strontiu111 Carrier GFPC, Sr90. ~olid "Dry Weigh! Corrected" 1525755 89.9 (25'%-125%) Tcdinctium-99m Tracer Liquid Scint Tc99. Solid "Dry Weight Corrected" 1522715 98.1 (15%-125%) Notes: TPU and Counting Uncertainty are calcula1cd at the 95% confidence level (1.96-sigma).

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - WWW.gel.cam Certificate of Analysis Report Date: December 4, 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite l 12 Buffalo, New York 14228

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Ms. Laurie Losey Project: ... Soil Radioisotopes Client Sample ID: 3.2.1.R.6 Project: MJWCOOl 15 Sample ID: 385070022 Client ID: MJWC'OOJ Matrix: Water Collect Date: 16-0CT-15 !5:52 Receive Date: 05-NOV-l 5 Collector: Client P.ar_a~et~1_*................ 9ual_ifi:~... __ 13-e_su~t .lJ..1~~~r.'.'.l!J11Y.. ....... ~I:)~ RL Rad Gamma Spec Analysis Gammaspec, Gamma, Liquid {Standard List) "As Received" Actmmm-227 U 6 77 +/-23 6 43 /) pCl'L MJHI 11/17115 0712 1521915 Anlimony- !25 U -4 08 +/-8 38 143 pCiil. Ccsium-137 U 2 65 +1-3. 71 7.33 100 pCtll.. Cobalt-60 U -2.49 +1-3 56 6.15 pCllL Europmm-15<1 U -7.84 +/-J 1 2 11>.2 pC1r1. Protactinium-231 lJ 30 0 +1-57.5 BO 4 pC1/L Radium-22!\ U 13.2 +/-23.9 31.1 pC1iL Tm-12<i U -6.92 +l-S.98 12.S pC1/L Rad Gas Plow Proportional Counting GFPC. Gross AIB, liquid "As Received Alpha lJ -0.452 +/. J 39 3 15 500 pCi!L JXB7 12/02115 1307 1525771 2 Bera U 2.79 *+f-2 9l 4 83 5 (JO pCIIL T_he ra.1_1owin~-~~1~ly_ti~~1. fVl~t~.o~.s _\Ver~. p~rf?f11.le.~_:_ ..... . t_vl~t.h.94 ............................ D~s.criptio!l.. . . ...:......... .f\najyst<;;.Qt)"_ll_l!l,';P..~ ............... ***********-*-*** ............ EPA 901.1 2 EPA 900 O/SWS469~10 Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.geLcom Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Report Date: December l 7. 2015

Contact:

Ms. Laurie Lo8ey Project: Soii Radioisotopes C'!ient Sample ID: 3 .2. !.R.6 Project: MJWCOOl 15 Sample ID: 385070022 Client JD: MJWCOOl Matrix: Water Co!lect Date; 16-0CT-15 Receive Date: OS-NOV-15

 ... --~~)l~ct~_r:_.,                    . *--~!~~t.......... .

Parameter MDC ......~..: ... . .T.PL__ ..... RL Rad G:imrna Spec Analy5is Gammaspec, Gammcr. liquid (Standard Lisi) "As Recehed" Actimum-227 u 6 77 +/-23 6 43.h 20 6 +/-23 9 pCiiL MJfl 1 11117115 0712 1521915 Anlimony-125 u -4 08 +f-8 38 l4.3 6.59 +f-8 58 pCi/L Bismuth-212 u 3.13 +/-46.7 88.3 40 3 H-46 8 pC1iL B1s1mith-2 I 4 LI[ Cl 00 +/-12.9 12 1 5 54 +/-13.Cl pCilL C'csium-137 l! 2 65 +!-3.72 7.33 339 +/-3 92 10 0 pCt!l. Cobah-60 u -2 *19 +/-3.56 l>.15 265 +l-3 74 pCi11. l.::uropium- l 54 u -7 84 +l-11.2 16.2 {i9:t . +/-1 ! ll pCllL Lead-2l2 Li 4 34 +l-9.59 11 S 566 +/-9.79 pCilL l.elld-214 U! 0.00 +/-12 2 15.3 726 +f-13.1 pCliL Pota~sium-40 u -25 ~l-44.4 79 5 35.S +/-45.9. pCiiL Pro1ac1inium-23 I t.: 300 +/-57.5 &U.4 .n.8 "':-/-57.9 pCi.il. Radiwn-228* u IN +/-23 9 31 l 14.4 +/-'}.4 7 pCi1L Tlmllmm-208 U! 0 00 +/-4.65 . 5.82 2r15 +/-4.66 pCi/L Tm-126 u -6.92 "'"/-8.9S 12.5 5 93 +1-9 53 pC11l. Rad Gas Flow Proportional Counting GFPC. Gross A* B. liquid "As Received" Alpha u *0.452 '4-/-1 39 3 IS ! 27 +/-1.39 . 5 (Ill pCi1l, JXB7 12/02115 1307 1525771 2 Beta 2 79 +J-2 91 4.&3 :i.:n +/-2 95 5.()(J p{'i/L Tl_1~...f.o.l.!~.~i_l!g_ '..\n:1.l~~i1:11.! ..:\'l_clh!)_q_s.. ~e.re. pcr..~l!.~fi.le.~........ _. ...... ........ ....... .. ...................... Method Description EPA901 I 2 EPA 900.0/SWS46 9310 Snrrognte!fracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( l .96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.. gel.com Certificate of Analysis Company: M.TW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Report Date: December 17, 20 15

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Smnple 10: 3.2. l.R.6 Project: MJWCOO!JS Sample ID: 385070022 Clie11t ID: MJWCOOI Ma1rix: Water Collect Date: 16-0CT-15 Receive Date: 05-NOV-15 Collector: ..

Client

                                                                                                . \"IP.~ ..... _Le            TPl'               RL       t:nits ******-**********

DF Ana\-yst Date Time Batch Mtd . Rad Gamma Spec Analysis Gammaspec, Gamma, liquid (S1a11dard list) .'ls Received" Actmmm-227 lJ 6 77 +/-23.6 43 6 2t) 6 +/-23.9 pCifL MJHI 11117/15 07\2 1521915 Antimon}-125 u -4.0& +/-& 3& 14 3 6.59 +l-&.58. p('i/L Bismuth-212 lJ g 13 +/..46 7 88 J 41).3 +/-46.8

pC1/L Bismuth-214 U! 0.00 +/-12 9 12.1 5_54 +1-13.0 pC1/L Cesium-137 u 2.65 +l-3 72 7-33 3 39 +/-3.92 llJ.O pCilL Cobalt-60 LI -2.49 +/-3.56 6 15 2 65 +i-3 74 pCi/L Guropium-154 u -7.84 +/-112 16.2 6.94 +1-11 g pC1/L Lcad-212 u 4.34 +/-9 59 11.8 5.66 +/-9.79 pCilL l..,ead-214 UI 0.00 i*/-12.2. 15 3 7.26 +/-13.2 pCi/L Polass1um-40 u -25 +/-44.4 79 5 35 5 +/-45 9 pC1/L Protactmmm-231 u 30.0 +/-57.5 80 4 37.8 +/-579 p('i/L llndium-228 u 132 +f-23_9 31 I 14.4 +f-24 7 pC'i/L Tballium-208 Ul O.OD +/-4 65 5 !!2 2 65 -f-/-4.66 jlC:ill.

Tm-116 ll -6.92 +/-8.98 12 s 5 93 +f-9 53 pC1/L Rml Gas 1'"1ow Proportional Counting GFPC, Grass A 18. liquid "A~* Received" Alpha u -0.452 +1-1 39 3 15 127 +/-1.39 5 00 pCifL JXB7 12/02115 1307 1525771 2 Beta 2.79 +/-2.91 4.83 2.22 +f-2 95 5.00 pC1/L Th..C. fo.1.1.~_W\f!g_~n~~.Y.t~~~~ l\~ct.~l)dS ,~_er~ pcrfri.rn~~d. *-*-**********-*** -* ............... ............ _ Method Description EPA 901.1 2 t;J>A 900 O/SW846 9310 Surrogateffracer Recovery Test Batch ID Rccovc1-y% Acceptable Limits Notes: TPU and Counting Uncertainty arc calculated at the 95% confidence level ( I.96-sigma).

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysi~ Report Date: December 4, 2015 Company :

MJW Corporation Address : 15 Hazel wood Drive Suite l 12 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes ....... ,. Client Sample ID: 3.2.2.R. I Project: MJWCOOl 15 Sample ID: 385070023 Client JD: MJWCOOI Matrix: Soil Collect Date: 16-0CT-15 11:30 Receive Date: 05-NOV-15 Collector: Client Moisture: 24.3% P.~.r.~i.r:_et~r ........ _......... .9.11.al!fi~r ___ --~~s-~~-t. __LJ_ncerta,in.t~ MDC RL Units OF Analyst Date Time Batch Method Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 24.3 percent CXC'l 11110!15 1319 1521842 Rad Gamma Spec Analysis Garnmaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 U 0 128 +/-0 28 ! 0.532 pCi/g

RXF2 !2103.115 1308 1522383 2 Antmiony-125 u 0.0566 +/.Q l 12 02)9 pCi!g Cesium-137 0 597 +!-0 0934 00888 0.100 pC!lg Cobalt-60 lJ -0.0062 +/-0 0496 () 0942 pCi/g EL1rop1um-154 u 0.0739 +l-0 163 0327 pC1/g Proiactimum-23 l u 0.560 +/-0 728 () 939 pCt!g Radiurn-226 0 964 +l-0 \ 75 0.136 pC1lg Radium-228 I 0(1 +/-0.332 0.293 pCi/g Tm-126 Ul 0.00 +/-0 171 0.122 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross A!B. solid "D1y Weight Corrected" Alpha 126 +/-379 383 4.00 pCi/g JXJ37 12/02115 \2\5 1525762 J Bela 18.5 +/-2.B8 2.64 JO 0 pC1/g

.T!1e_foll_()~~i_n$.. Pr~p_ !v1e_tl1_c;i_d_~__\'l~re_perf()r_111e.~: .. ___ --*****-*. _ .. .. . .. . .. .... . ___ . ... ... . _ __ ..... ... . . . . ..__ . ___ .. **-. _ -*---*--*-- .... Method Description Analyst Date Time Prep Batch of}-sCiiihcii***** *** ** * **** ** * -**o;y*s1i11 i>"rcr dCR..AO::i.-:02c * * * ****** ** *- **** * * ** ** *cxcf- ...

i"1ii1in"s- ***** **-* -13(9* * *--"i5.ifs42 -* * **** * *** * * *****

!.~_e__fo!!_o;~i_n.?.. ~na!Y.t~~~l. !Vf~t~<:>_ds_ :w.~r.~. r.~r~o_rn1~d:              .............. __ . .            .......... -* .....,................. -* .... .... . .. .. .... ... ... . .... .

Method

 ***-***- ..... **-* -** *- .....      P.~~~r.iptiog_ .................. m    - -  - ************                     .......................... _A.i::ud_yst C_orm.nen_t~ ....

ASTM D 2216 (Modified) 1 DOE !-!ASL 300. 4.5.2 3/Ga-01-R 3 EPA 900 O/SW846 93 IOiSM 71 IOB Modified Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite I 12 Buffalo, New York 14228 Report Date; December 17. 2015

Contact:

Ms. Laurie Lost:y Project: Soil Radioisotopes Client Sample ID: 3.2.2.R.1 Project: MJWCOOl 15 Sample ID: 385070023 Client JD: MJWCOOJ Matrix: Soil Collect Date: \6-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 24.3% raramcicr __ Q.~a.l_ilier....... Rl!sull ____ll11ccr.~ai!'!t\-' ..... '.\1.IJ.~* Le .. .....TPl" rnits ,,DF RL................ __..... An:ih*st

                                                                                                                                                                      . * .. ?"* ... Oate' ................................
                                                                                                                                                                                      , ...... Timl' Balch . Mtd. .

Gravimetric Sc1lids ASTA! D 2216 % Moiswre "As Received" Moisture 24.3 percent CXCl ! 1!!0115 1319 1521842 Rad Gummn Spec Analyst:; Gammaspec. Gamma. Solid "Dry H'r:ig/rl Corrected. ActintLJm-227 u 0.128 +l-0.281 0 532 0251 */-0 288 pCilg: RXF2 12i03/J5 1308 1522383 2 Antunony-125 u 0.0566 +/-0 112 0 219 0 102 +/-0,115 pCiig Bismuth-212 UI 000 ;-/.1.30 1 38 0.636 -i-/.IJ6 pCilg. Bismuth-2 I4 0.964 +i-0 175 0 136 0.0612 +/-11.194 pC1lg Ceshim-137 0597 +/-0.0934 0.0888 0.0406 +/-0 106 0 100 pC1lg C{)hal\-60 l.1 -0.0062 +/-0.0496 009.+2 0041 +/-(J 0497 pC1/g EurO]JiUm-154 lJ 0.0739 +/.Q.163 0.327 0 147 +/-0.166 pC1/g Lead-212 * . 0.992 +l-0 161 0.158 D0759 t-1-0 201 pCi/g: Lead-214 1.13 .;./-"() 191 0.165 0 !!773 +/-0 214 pCilg Potassium-40 14.5 t-/-1.67 0 518 () 1.98 +/-2 l'l pC1/g Protact1mum*23 I UI 0.00 1-/-0 718 () 939 (J 4J9 +/-0 739 pC1/l,!. Radmm-226 0964 1-/-0 175 0 136 Oll6l2 +/-0 (94 pC!lg Radmm-228 I 00 +/-0.332 0293 () 130 +1-0.357 pCi/g. Thalhum-208 0 301 +/-!) l05 0.0761 0 0346 +1-0.108 pC1/g Tm-126 Lil 0.00 +/-{l 171 0122 II 0588 +/-0.173 pCi/g Rad Gas Flow Proporthmal Counting GFPC'. Gross A:B, solid "Dry Weighr Corre<:led" Alpha 126 1-/-3 79 3 83 1.59 +l-4.55 4 ()() pCi/g JX\37 12:0:2115 1215 1525762 3 Bera 18 5 +/-2.88 2.64 I 19 +/-3 89 IO.O pCi/g i:~e- ~~~l~~vii:ig ~*r~.P.. ~1. e_tl1~1!1~ ..'~~_r,c P~!".f.o.i:.ltl~.d. ..... Method

Description Analyst Date Time Prep Batch Dry Soil Prep Di)' Soil PrepGL-RAD-A-021 CXC! 1111 Oil S 13!9 1521842 The folluwing Analytical Methods were performed

~1-~ti;*od*** ....... ***- *D~~~;iptl~~..... . *-*. *--* .... *. ***, . ASTM D 2216 (Modified) 2 DOE llASL 300.4 5.2.3/Ga-Ul-R J EPA 900.0/SW846 931 OiSM 71 lOU Modified Surrogateffr:1cer Recovery Test Batch ID Rcco\*ery% Acceptable Limits

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 -www.gel.com Certificate of Analysis CQmpany: MJW Corporation 5 Address: [j Hazelwood Drive Suite 112 Buffalo, Ncv York 14228 Report !]ate: December 17, 2015 Contact Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.2.R. l Project: MJWC00115 Sample 10: 385070023 Client ID: MJWCOOI _P,_11.r~ll~.ct~.r.. .. . .. .... .... .. 9.11.a~i.~ci: ....... R..es.u. It ... ~!Jl(!C!'.1-l!i.11~"* ...... ~11).t;:'.. . Le Surrogat~~~*n..~~~...R.~c_o~e?'.. ... . !~s~ . .............. :. . . . . . . . .... ... ... . . .... .. . . . . . . . . . . .... . ... . . . .. .. Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma}. I I

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analxsis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Report Date: December 17, 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.2.R.1 Project: MJWCOOI15 Samele ID: 385070023 Client lD: MJWCOO! Matrix: Soil Collect Date: 16-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 24.3% P~!.lll_lle_t.~r .................. _9ua_lifi_er .... Rc_s.l:'l_t_ rncer,t.~h,11:\: .... }'ID~ .. Le TPU

                                                                                                                        ........................... RL Gravimetric Solids ASTJf D 2216 % Maist11re "As Received" M01s1urc                                                              24 3                                                                                   percent       CXCI    lll!Ofl5 1319  !521842 Rud Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry Weight Corrected"*

Actinmm-227 u 0.128 +/-0 281 0.532 0.251 +f-0 2!{8 pCi/g RXF2 12103_115 1308 1522383 2 Ant1mony-!25 u 0.0566 +1-0 112 ll.219 0.1()2 +/-0.115 pC1!g Aismuth-212 [)] 0.00 +/- J.30 1.38 ll.636 +/-1.36 pCi/g Bismuth-214 0964 +1-0.175 0.136 0.0612 +/-(}.194 pCi/g Cesmm-137 l) 597 +/-0.0934 0.0888 0 04U6 +/-0.106 0 100 pCi/g Cobalt-60 lJ -0 0062 +/-0.0496 0.0942 0.041 +/-0 0497 pC'i/g Europmm-154 u 0.0739 +l-0 163 0.327 0 147 +f-0.166 pCi/g Lcad-212 0992 +l-0 161 0 15R 0 0759 +f-0.201 pCilg Lcad-214 I 13 +/-0.191 0 1{15 IJ.()773 +l-0 2J.1. pC1/g ?omssmm-40 14.5 +/-1.67 0.518 0 ..198 +!-2 i 9 pC1/g Protactmium-23 l lH o_oo +/-0 728 0 939 0.439 +/-0.739 pC1/g Radium-226 0.964 +/-ll.175 0.136 u0612 +/-0.194 pCilg. Radium-228 I 00 +l-0 332 0 293 0.130 +/-0.357 pCi!g Thallium-208 !UOI +/-0.105 (I 0761 0 0346 +/-0.108 pCilg Tm-12t. U! 0.00 +/-0 171 0 122 [).()588 +/-[l, 173 pCi/g Rad Gas Flow Proportional Counting Gf.'"PC. Gross A.-B, solid "Dry Weight Corrected" Alpha 12.6 +/-3.79 3.83 1.59 +!-4.55 4 00 pC1/g JXB7 12i02!15 1215 1525762 3 Beta 18.5 +/-2 88 264 1.19 +/-3 89 100 pC'i/g

!..h.~, fo_l!o~i'!g_Pr~!?}~:!~t~od.~ .."'.~'::~ ll~~fo.~~c<~ -*

Method Description Am1lyst Date Time Prep .Batch Dry Soil Prep Dry S01l Prep GL-RAD-1\-02 I CXCI l !Jl0!15 1319 1521842 I~~-!<Jl'.g\1:i_rig :'\~_alr~.ica_l_1\le_t!J~.~s. 1.~:.c.rc..P.~'.".f!lr'1.'.c.d ___ _ Method Description ASTM 0 2216 (Modified) 2 DOF. HASL 300, 4.5.2 3/Ga-01-R 3 EPA 900.0/SW846 93 IOJSM 71 IOB Modified Surrogatcffniccr Recover~' Test Batch ID Recovery% Acceptable Limits

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: ! 5 1-lazelwood Drive Suite 112 13u!Ta!o. New York 14228 Report Date: Dccembcr 17. 2015

Contact:

Ms. Laurie Losey Pl'Oject: Soil Radioisotopes Client Sample JD: 3.2.2.R. l Prnject: MJWCOO Ii 5 Sample ID: 385070023 Client ID: MJWC001 Parameter . .. qu11lifi~r_- _ . -~es_u_l_t ..... __l.!_11ci:rtain_I): . MDC* Le

                                                                                              .................. . TP.L ..... -~L .J'.nit~ . J:?.l'.. A~aly~t __ l)a~~ ..Thn.c .B.al~h. ;\II!~~

Sutrogak!Tr~ccr Rcc1r.-ery Test Batch ID Recovery% Acceptable Limits Notes: TPlJ and Counting Uncertainty arc calculated at the 95% confidence level (1.96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite ll2 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.3.R.1 Project: MJWC'OOl 15 Sample lD: 385070024 Client I.D: MJWCOOJ Matrix: Soil Collect Date: 16-0CT-15 1.2:00 Receive Date: 05-NOV- l 5 Collector: Client Moisture: 27.1 % Parameter

- - - - **-* ................... __ q~~~i~-~-r.. . ____ R~.s~Jt _ Un~_e_rt.~i~ty __ MDC ....~ . _ --****.~nits_ ........... _D~- .A_n~lr.st ___ ~_'.lt: ___!.i'.11_~ B_atch __ Method Gravimetric Solids ASTl\!( D 2216 % Moisture "As Received" Moisture 27 l percent CXCl 11110/15 1328 1521844_

Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinmm-227 U 0 0642 +/-0.286 0 546 pCi/g RXF2 12/03/15 0720 1522386 2 Anumony-125 lJ -0.0231 +/-0.109 0196 pCi/g Ce~ium-137 0.527 +/-0.0938 0.07H8 0 JOO pCi/g Cobalt-60 U 0.00422 +l-0.0399 0.0806 pCi!g Europium-154 U -00114 +1-0.112 0.219 pC1!g Protactmium-23 l lJ 0.6?.9 +1-0.815 0.933 pCi!g Rudmm-226 0.780 +/-0 148 (J.152 pC1!g Radium-228 0.886 +/-0 277 U.315 pCi/g Tin-126 U 0.()72? +l-0 102 (} 127 pC1/g Rad Gas Flow Prop011ional Counting GFPC, Gross A/B, solid "D1y Weight C01Tected". Alpha 15.1 +/-HS 3.90 4.00 pCi/g JXl37 121-02flj 1223 1525762 3 Beta 15.0 +/-3 82 4.91 JO 0 pCi/g Th~[.oll<?!~i~~--l_;l~eP.J~1~t.l)~.~s ~er.~JJ:r_fo!n_11!!d: ___ . **-**** .... __ .. _____ . _ ___ ___ __ ___ _____________________ .... __ -*-*** .. Method Description Analyst Date Time Prep Batch tliY*so-;ci>ieµ*-----*--- *- **-* * **-**-r:it)*-~>'01f-P.icii..dCR.A"D"-~\:*021 *** * *******- ***** *- ** cxc1* * *---- * --Tilfoiff ..ijig ...... - 15f1844" .... --*.

 !h~-~°-ll_?,\Vi1_1~--~~ly_Hc_al _ ~1.~t~o_d_5. ~ve'.e__ Pe,~f.()_n:1~d:

Mi:tho~. _..... _........... __ .D.e.s.~_ripti_91_1_ ____ ....... __ ....... m. __ ** .. . . . . .Ar.i?.l.xstC91pm_e!1ts .... . . . ___ .... _ ........... ___ ... _.... _... _... . ASTM D 2216 (Modified) 2 DOE !-IASL 300. 4 5.2 3/Ga-01-R 3 EPA 900.0ISWR46 93 IO!SM 711 OB Modified Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corpora.Lion Address: 15 Haz.e]wood Drive Suite l !2 Buffalo, New York 14228 Report Date: December 17. 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.3.R. l Project: MJWCOO!l5 Sample TD: 385070024 Client ID: MJWCOO! Matrix: Soil Co Hect Date: J6-0CT-15 Receive Date: 05-NOV- l 5 Collector: Client Moisture: 27.1% Resuh ...vr.i~.~r.t_a_i_n._tY ...... ~g>_c:.... Le .... TP.l'. ........ ~L-Gravimetric Solids AS7M D 2216 % Moisture "As Received" Moisture 27.1 p~rccnt CXC'l 11110115 132.8 1521844 1. Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry Weight Carrec1ed" Aclinium-227 LT 0 0642 +/-0 286 0 546 0 256 +1-0.288 pCi/g R.XF2 12/03115 0720 1522386 2 Anumony-125' u -0 0231 +/-0.\09 0.196 ().l)90 +/-0.109 pC1/g Bismulh-212 Ul 0.00 +1-l ()9 I 52 0706 +/-126 pCifg Bismuth-.21 *I 0.780 .../-0.148 0 152 0 0693 +f-0161 pCi!g Ccsium-137 0.527 +/-0 0938 0.0781! 0.0356 +/-0 103 0.100 pC1fg Cobnlt-60 u 0.00422 +/-0 0399 () 08()(, 0.03.l.5 +/-0.0399 pCilg F.uropmm-154 u -00114 +/-0.112 0 219 0.0934 +/-0 112 pC1/g Lead-212 1.07 +/-0 125 . 0 109 0.l15!2 +/-0 154 pC1/g Lcad-214 0 398 +/-0165 0.141 0.0647 +/-0.181 pC1/g Porassmm-40 14.l +l-1 5() 0 488 0 186 +/-1 93 pCi/g Protactimum-231 \JI 000 +!-0 815 0.~33 0 433 +1-0.828 pCi!g Radium-226 0 78!.l +l-0 148 0.152 0.0693 +/-0.161 pC1/g Radiuin-228 0 886 +/-0.277 0 315 0 141 +1-0 305 pC1lg Thallium-208 0276 +/-0 0868 0.0744 0 Cl338 +/-0.0896. pC1lg Ttn-126 UJ 0 00 +/-tl.!02 () 127 0 0602 +/-0.103 pC1/g Rad Gas Flow Proportional Countiug GFPC. Grass A.B. sofid "DI'.\' Weigh! Correc1ed" Alpha 15 I +1-4 45 3.90 I 53 +J-5 32 400 pC1/g JXB7 12!02/15 1223 1525762 3 Beta 15.0 +1-3 82 4 91 2.2& +/-4 43 tll.O pC1/g T~.e ~11_10."'.ill.g f..rc_p_ ~!~.!.~.f:!~S. ~~-r~..P.~r.f~r.in~d. .... . .. ... .................................................... *****-*** ..... *-* ............... .

\'let hod Description Analyst Date Time Prep B:ttcb Dry Soil Prep Dry Soil Prep GL-Ri\D-A-021 CXCI 1\/10'15 132& 1521844

r.~c 1:a.11~.1~_ii:ig_A_n:l!!rtic.~l-~l_c~bo~~ .\~.C.~~-P.~1:"ra1*ru.!~

Method Description I ASTM D 2216 (Modified) 2 DOE l-lr\SL 300, 4 5.2.3/Ga-01-R 3 EPA 900 ll1SW846 93ltJISM 7110!3 Modified Surrogatcfl'raccr Reconry Tc~t Batch ID Recovery% Acceptable Limits

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556"8171 ~ www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo. New York 1422& Report Date: December 17, 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes

   - Client Sample ID:     3.2.3.R. l                                                                  Project:            MJWCOOl 15 Sample ID:            385070024                                                                   Client ID:          MJWCOOI

~~r.?~~t_i:r _ ___ qual~fie_r ____ ~~s_~!t_ ______ i,:i:icer.~1_1!~!Y _______ ;'vii?.~-- _ Le Trr .. . RL l'.nits. .. . DF Analyst

                                                                                                                                       . .. . .. t.. . .

Date. . .Time

                                                                                                                                                         . .. *' ~

Balch i\'ltd. Surrogateffraccr Recovery Test Baldi W l~ceoYer)'% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( \ _96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Report Dale: December 17, 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.3.R.1 Project: MJWC00\15 Sample ID: 385070024 Client ID: MJWCOO\ Matrix: Soil Collect Date: ! 6-0CT- l S Receive Date: 05-NOV-!5 Collector: Client Moisture: 27.1 % _Para.1nc.~c_r_ .. ... . .. . . ... ..Q~al_i_ficr_ ..... ~cs~_l_t . Gravimelric Solids AST.'vf D 2216 % Moisture "As R!!ceived" Moisture 271 percent CXC'l 11/10!15 1328 1S21844 Rat.I Gamma Spec .Analysis Gammaspec. Gamma. Solid "Dry Weight Corrected Actimum-227 u U.0642 +1-0.286 0.546 0 251\ +/-0.288 pCilg RXF2 12/03/15 0720 1522386 2 Antimony-125 u -0.0231 +!-0 I 09 0 196 0 090 +/-0 109 pCilg Bismuth-112 Ul O.DO +/-1.09 1.52 0.706 +/-1.26 pC1/g Bismuth-214 0 780 +/-0 148 0 152 0.0693 +/-0.161 pCilg Cesmm-137 (}527 +/-0 0938 n 01ss 0 0356 +/-0 103 () 100 pC1tg Cobalt-60 u 0.00422: +/-0.0399 0080(> () 0345 +J-0 0399 pCi/g Europrum-154 lJ -0.0114 +1-0 !12 0.219 0.0934 +1-0 112 pCi/g Lead-212 \.07 +1-0 125 . (}.109 0.0512 +1-0.154 pCilg L!!ad-214 0 898 +1-0 165 0.141 00&47 +1-0.181 pCrJg Potassium-40 14.1 +/-1.50 0488 0 186 +/-1.93 pC1/g Protactimum-131 Ul 0.00 +1-0815 0 933 0433 +/-0 828 pCilg Radium-226 0.780 +f*O 148 (l \52 0.0693 +/-0 161 pC1/g Radium-228 [) 886 +/-0 277 () 315 0 141 +/.{).305 pClfg Thallium-208 (i 276 +/-0 0868 (}07-14 0.0338 +/-0 (}896 pC1/g Tm-126 lll 0.00 +/-0 102 0.127 0 0602 +l-0 IOJ pCilg Ratl Gas Flow Proportional('ounting GFPC. GrossA . B. solid "Dry WeightCorrecled" Alpha 15.1 +/-4 45 390 1.53 +/-5.32 4.00 pC1/g JXB7 12/02/15 1223 1525762 3 Octa 150 +/-3 82 491 2 28 l*/-4 43 !O.O pC'ifg Thll. f.~!l~~v.i11~.P.t:e.P. .1\:~~~.h.~s wl?~t:.Pi:~r~Tn:t!l~ ... Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 CXC\ ll/10115 1328 1521844

i:~e fl)ll()'\'i!lg ~ n.a.:~~:ti~J:l.1.~1-~t~o~s. 'fcr~_r.crfor,me.~ ...

Method Description ASTM D 2216 (Modified) DOE HASI.. 300. 4.5.23i'Ga-01-R 3 EPA 900.0ISW846 93!0/SM 7110D Modified SurrogateJTraccr Recovery Test R:itch ID Recovery% Acceptable Limits

GEL LABORATORIES LLC 2040 Savage Road Charfeston SC 29407 - (843) 556.8171 ~ www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 I [azelwuod Drive Suite [ 12 Buffalo, New York 14228 Report Dale: December 17. 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.3.R.1 Project: MJWCOD 115 Sample JD: 385070024 Client !D: MJWC-001 Pammctcr ........O.ua_li_~er .. ~~S1Jlt..... Fnccrt_:1ir1ty .......:\:IDC Le Tl'U

                                                                                     . *-******. --*.. fl.~....... _l)_1_1j_t_s_ ... I>.f .. ~!:'a.lr,st__ . _D_at.c_ ~rin1~ . :B.at~~. :\-I~~:-

Surrugntc/Trnccr Rec11vcry Tes I R11tch JD Recovery% Acccptnble Limits Notes: TPU and Counting Uncertainty are calculated at the 95<!*ii confidence level ( 1.96-sigma).

GEL LA BORA TORIES LLC 2040 Savage Ro.ad Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 7, 2015 Company:

MJW Corporation Address; l 5 Hazelwood Drive Suite 112 Buffalo, New York 14228

Contact:

Ms. Laurie Losey

                   ..rr~~ect;                .. _. . .~~il R~~.ioi~otop~~.

Client Sample ID: 3.2.4.R. l ."" "r'i-~j e~t~ MJWCOOJ 15 Sample ID: 38506800 I Client ID: MJWCOOl Matrix: Soil Collect Date: 19-0CT-15 10:00 Receive Date: 05-NOV-!5 Collector: Client Moisture: 25.8% ~arlll!1.~t:r _..... __ ***-* __9_U.a1.i~.~r...... ~e_s.~1~. _L1n~7rta.inty ........ MDC RL ............ lJ~.i~.~.... . __ J?~. f\..n.a.lyst Date Time Batch .. ~1etl1?d. Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 25. 8 percent CXCl \1/\0115 1326 1521841 Rad Gamma Spec Analysis Gammaspcc, Gamma, Solid "Dry Weight Corrected" Actmium-227- U 0.159 +/-0 229 0.438 pCilg R..XF2 r2i03/I 5 0704 1522393 2 Anlrmony-125 U 0.0132 +/-0 101 0 19\ pCilg C'csiuni-137 0.556 +1-0 0885 ll.ll('92 0 100 pC1lg Cobalt-60 U 0 0158 +-/-tl.035 0.0737 pCi/g Europrum-154 L' 0 0443 +/"() (J66S () 187 pCi/g Protnctmmm-231 U 0.400 +/-0.647 0.953 pC1lg Radium-226 0 743 +/-0.148 0I12 pCi/g Radium-228 D 757 +/-0.237 0.288 pCr/g Tm-126 UI 0.00 +/-0.104 0 129 pC11g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha 10.3 +/-3.60 3 90 4.00 pC1/g JXl37 12/02115 1215 !525762 Beta 19.1 +f-3 10 2.93 10.0 pCi/g !l~~_f()~IC?~~i11¥. ~.re.i;i .N.f~t~~d~ .':".~~ p~rfc:ir11,1cd: Method Description Analyst Date Time Prep Batch o;y *s*oii ..r,:*;;iJ *........ *-....... *** of).o *5*c;;i *r~eii aDRXo~A':O:Zi' ....... i:'xc1 * .. 11/10/IS !326 1521H41 .T.h~.foU?.\V.i.n..~.~~~-l.Y.t.i.c.a.1..rv!~tl1~~s ..w~.r.~. P.~~Cl~rned*:*.

~1~\l).od. ................... .Descr.,(pt!c;i.n . . .. .................. ..                                  . ._ .._.......................... Ar.ia,lyst Coni111e11ts_ .

ASTM D 2216 (Mod1fierlJ 2 DOE HASL 300. 4 :5.2 3/Ga-01-R ,l EPA 900.0/SW846 93101SM 71 IOB Modilied Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96*sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - Www.gel.com Certificate of Analysis Company; !Vi.IW Corporation Address: 15 Hazelwood Drive Suite I !2 Buffalo, New York 14228 Report Date: December 17. 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample JD: 3.2.4.R.1 Project: MJWCOOl 15 Sam~le ID: 385068001 Client ID: MJWCOOl Matrix: Soil Collect Date: \9-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 25.8% Priramctc.r ..... , . _ ........ 9..II:i~i_fl:".1.' ........ R~~l!H . ......... l'nccrtaint\* Le __ ..... __ J_Pl_: ___ , _........ ~!'~--- _J!l_it_s __[)F. ;\n_al~:~t___ Qa_le _T_i_ru_e_ ~~~t_c~ .i\*ftd_* Gravimelrk Solids AST;\/ D 2216 % Moisture "As Recei\*ed" Moisture 25.8 percent CXCI 11/10/15 1326 1521841 Rad Gamma Spec Analysis Gmnmaspec, Gamma, Solid "D1:r Weight Corrected" Actmium*227 u 0.159 +/-0.229 0438 () 204 +/.().241 pCt/g RXF2 12103115 0704 1522393 2 i\numony-125 u 0.0132 +/-0.101 [) 191 0.0882 +l-0 101 pC1/g llism-.th-212 Ul () 00 +/-0 616 ) 16 0 535 +/-0 839 pCi/g Bismulh-214 ()743 +l-0 148 0.112 0.0498 +!-0 160 pC1/g Cesmm-137 0.556 f*/-0.0885 0.0692 \HBl2 +/-0 0988 0 100 pC1lg Cobalt--60 lJ 00158 +l--0 035 () (\737 () 0317 +/-0 0358 pC1/g Europium-154 u. 0 0443 +1-0.0665 (J 187 tl 0793 +/-0 0696 pCi/g Lead-212 0962 +/-0.118 00972 0 0455 +/-0.142 pC1fg Lcad-214 () 896 +/-0 184 0.304 0.147 +f-0 197 pCi/g. !'otassium;40 12.4 +1-1.44 0 639 0 269 +/-l.83 pC1/g Protactmiurn-231 u 0.400 +1-0647 0 953 D.447 +/-0 653 p(1/g Radiiun-226 0.743 +/-0 148 !) 112 0 0498 +/-0.160 pC1lg Radium-228 0.757 +/-0 237 0 288 () _130 +/-0 259 pC1/g Thallium-208 0.233 +/-0.0763 0.0664 0 0302 +l-0 0787 pC'ifg Tm-126 UI n.oo +f-0 W4 0 129 00612 +/-ll.106 pC'1/g Rat! Gas Flow Proportional Counting GFPC. Gross A.B. solid "D1y Weight Correc1ed" 10.3 +1-Ht(l 3 90 160 +/-4.12 4.00 pC'1f~ JXB7 12/02115 1215 1525762 3 Alpha 19 I +-1-3 10 2.93 132 +/-4.18 10.0 pCi/g B~ta Tl~~ fo_l!_o__l".i1:'g Pre_jl _l\:Ii:!~O~~- ~y.e:r,i:_ P!::rfo.rrned _.. __ ... _.. *- ................. *-* ........ Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD*A*021 CXC' I 11/10/15 1326 1521841 Ih..e. _l~llo_,v!11_g_~f]'.:\_~y~ic:it M~t!10,~~ l~'l!_r~ pcrf.orl!lcd __ Method Description ASTM D 2216 (Modified) 2 DOE 1-lAS L 300, 4.5.2J/Ga-01 *R J F.PA 9000iSW846 93JOiSM 711013 Modified Surrogalcrfraecr Rcco,*cry Test- Batch ID Recovery% Acceptable Limits

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo. New York !4228 Report Date: December 17. 2015

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Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.4.R.1 Project: MJWCOOl 15 Sample lD: 385068001 Client ID: MJWCOO I P.~.ra.m~t~r.. _______ .. **-* ... q~a.l_it_ie~--- . _R.~_s_ul_t...... Vn.c~r.t.!l_~ll.1'-'... _... ~IPL ..... Le..... _ .. TPl.' ..... R.~ .. _l!_n~t.s...l?.f'~:°~ ~y~t......D..a.t!! ..1:ilJ1~ __Ba_tc_l1 --~~t.d~ Surrogateffracer Recover)* Test Batch rn Recovery% Acceplable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).

GELLABORATOruESLLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 7, 2015 Company: MJW Corporation Address : I 5 Hazelwood Drive Suile ll2 Buffalo, New York 14228

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Ms. Laurie Losey Project: Soil RadiOisotopes Client Sample ID: 3 .2.4.R.3 Projeci: MJWCOO I 15 Sample ID: 385068002 Client ID: MJWCOO t Matrix: Soil CollectDate: 19-0CT-15 10:35 Receive Date: 05-NOV-15 Collector: Client MoistLire: 1&% Parameter Qualifier Result . lJ..nceitai_n~r MDC RL Units Gravimetric Solids ASTM D 2216 % Moisture "As Received Moisture l 8.0 percent CXC\ ll/10115 1326 1521841 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Aclinrnm-227 U 0.162 +/-0.331 0 667 pCi/g RXF2 12/031\5 0707 1522393 l Antimony-125 u 0 0327 t/-tJ 123 0241 p('i/g Cesium-B7 () 129 +f*O 0839 0 105 IJ.100 pCi/g Cobalt-60 LI -0 0185 +/-0.0575 0 108 pCi/g Europmm-154 u -0 000223 +/-(J.173 0.342 pCilg Protacumum-231 Ul 0.00 ~/-091!1 I 16 pCi/g Radium-226 l 05 +/-0.214 0.12CJ pCtlg Radium-228 l 02 +/-0.350 0.33.J pC1/g Tin-126 {J 0.0598 +/-fl 141 0 175 pC1/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Co1Tected" Alpha 1 t.5 ...;.3 65 3.82 *I 00 _pC'*lg JXB7 12i02115 1218 1525762 Beta 19 4 +/-3.13 3 13 lU 0 pCi/g .!~~ [o!!.o~}J1¥;_f'..~e.e ~et!1~q_s_~r:i:.~ ~e_rf.o,rn.:i~d:, *- .. ..... .. . .. .. .......... , .. Method Description Analyst Date Time Prep Batch or:;;-soti.rrtir* * * **** * * * ****** bi-y soii Pie.P'Cil.-R:P-.ti~.A::o2i'* .....................

c*xc*i******** 11110/15 '1326 1521841

_!_h_~--f~!-~?.~i~E- ~-n.~I~t~c.~J. ~e~h()dS .i:vere per,f~~~°.d: .f\.1e.thQg.... **-*- ... -...... _..__ . P.t;~~.ription..._.................... . ASTM D 2216 (Modified) 2 DOE llASL 300, 4 5 2 3/Gu-01-R 3 EPA 900 OISW846 9310-'SM 71 IOB Modt!lcd Notes: Counting Unce11ainty is calculated at the 95% confidence level ( 1.96-sigma).

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Iluffalo, New York 14228 Report Date: December 17. 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisot_opes Client Sample ID: 3.2.4.R.3 Project: MJWCOO I 15 Sample ID: 385068002 Client ID: MJWCOOI Matrix: So.il Collect Date: 19-0CT- l 5 Receive Date: 05-NOV-15 Collector: Client Moisture: !8% Parameter 9_u_a\ifi_er. . l:les1.1lt_ .. l'!!ci:.~~:iin~x ....... :-,,rnc Le Gravimetric Solids ASTM D2216 % ;\>foistzwe "As R1n*eived" Moistur~ ISO p~rcent CXC! i 1/\0/15 I 326 1521841 R.atl Gomma Spec Anulysis Gammaspec, Gamma, Solid "Dry Weight Correc1ed" Acllnium-227 u 0 162 +/,().331 0.667 0.309 +/,Q.340 pCllg RXF2 12/(13115 0707 1522393 2 Anumony* 125 u 0.0327 +/-0123 0241 U.109 +/-0.124 pC1/g Blsmulh-2 l 2 Ui 0.00 +/-0925 1.9& 0 912 +/-1.18 pCiig Bismuth-214 l.05 +/-0214 0 129 00543 -H..(I 231 pC1/g c~sium-137 0. \29 +!-0 0831,J 0.!05 (!0468 +1-0 0845 0 WO pCi/g Cobalt-60 u -0 0185 +/-0 0575 (1.108 00448 +/,0.0581 pCilg Europ111m- 154 lJ -0.000223 +i-0.173 0342 0147 +/,(! 173 pCi/g Lcad-212 I 19 **/,0-174 0.129 00595 +i,Q.209 pCi/g Lead,214 0 882 +1-0 221 0 215 OO'f9 +/-0.232 pCi/g Polas>mmAO 15.\l +/-1.99 0.950 0 386 +/-l 40 pCi/g Protacllnium,231 l!I 0.00 +/-0 90! l.16 0-531 +1-0 948 pC1/g Radmm,226 I.OS +1-0214 0.129 00543. +/-0 231 pC1fg Radmm-228 1.02 +/,() 350 0.334 (J.142 +/,0.367 pCi/g Tlmlliun1,208 0 321 +/-0.115 00949 00422 +/-0 118 pCi!g Tin,126 u 0 0598 +/-0.141 0 175 00842 +f,() 142 pC1fg Rad Gas Flow Proportional Counting GFPC. Gro.~s A *B. solid "Dry Weighr Corrected" Alpha 11.5 +/-3 65 H2 l 58 +/-4 26 4.00 pC1/g JXB7 I2!02115 1218 1525762 3 Bem 19.4 +f.3 13 3 13 l 43 +/-4 16 HJ 0 pCi/g

r_h.~. rii.n~~V..i.".~..l'~er .~Ic.t~ods :er~ .r~r,f~r,~c~ ...... .

Method Description Analyst* Date Time Prep B:itch Dry Sod Prep Dry Sml Preµ GL-RAD,A-021 CXCl 11/10!15 1326 1521841 !_h_l_l__f()ll(J'~*ing_ ':\lla.lytic~l. ~Iet_h()<ls _,ve_rc .Jll'.ffo_!'~.e.d. Mctboil Description ASTM D 2216 (Modified) 2 DOE HASL 300, 4 5 2 31Ga*Ol-R 3 EPA 900.0ISW846 93lOiSM 71 IOD Modified Sm*rogatcffraccr Recovery Test Batch ID Reco,*ery% Acce1>tablc Limits

GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www-_gel.com Certificate of Analysis Company: MJW Corporation Arldress: 15 Hazelwood Drive Suite 112 Buffulo. New York 14228 Report Date: December 17. 2015

Contact:

1\fa. Laurie Cosey Project: Soil Radioisotopes Client Sample ID: 3.2.4.R.3 Project: MJWCOO 115 Sample ID: 385068002 Client ID: l\UWCOO ! _P_ara111_et.~r. ......... _...............9.~~-li~~1~ Rcsu_l_t: -* ~*ri.cer:t.a.i.11.1~: .......... MDC Le .... "R:~~- .. _l'n_~ts .. n.r_ ~\.i:i_a.ly.~t. . Q~l!: '.fi_n.ie.. B;1_tc_h . ;v1t~~ Surrogate!Tracer Recovery Test Batch ID Recovery% Acceptable Limits No~es: TPU and Counting Uncertainty are calculated at the 95% confidence level (l.96-sigma).

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 7, 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite l 12 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.4.R.4 Project: MJWCOOl 15 Sample ID: 385068003 Client ID: MJWC'OOI Matrix: Soil Collect Date: 19-0CT-15 14:10 Receive Date: 05-NOV-!5 Collector: Client Moisture: 8.9% Parameter Qualifier ........... --***** ....... -** .............. _. ... . ... . Result Uncertainty MDC RL . Units Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moistur~ . 8 90 percent CXCl 11110!15 1326 1521841 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected Actmnim-227 lJ 0.058:5 +1-0.289 0 545 pCi/g RXF2 12i03!15 0707 1522393 2 Antimony-125 U 0 00225 +/-0 l l 2 ll.205 pC1/g Ccsium-137 U 0 0&06 +/-0 0521 0 0878 0.100 pCtlg Cobalt-60 U -0 0334 +1-0.0537 00943 pC1lg Europium- I 54 U O O196 +/-0. 152 {J 298 pC1/g Protactimum-231 tll 0 00 +/-0 7<>0 () 952 pCi/g R.adium-226 O774 +/-0.174 0 149 pCtlg Rac!ium-228 0.644 +/-O.n6 0 315 pC'1/g Tm-126 U 0 144 t-/-0 170 0211 pCi/g Rad Gas Flow Proportional Counting GFPC. Gross AiB, solid "Dry Weight Corrected" Alpha 7 79 +/-3 14 3.84 +on JXB7 12/02115 1548 1525762 3 Bota 22 I +/-3 13 J.()6 10 () Th.~ .f.ol_!~~i~~ ..~rep ~et~o-~.s _\V(:!:<:..P~_r.f'?'.l]l(:d_: . , .. **- ... _ *- ......... **-** *- .. _... ...... .. ......... ....... . .... -. _......... ,............ __ ............... *-- Method Description Analyst Date Time Prep Batch oir*soii *Prep .. -.......... - -**- *-15;y*siiiiWt!i> dCi~f\"o~,\-iiii ....._. __ --.. *** ...... *

cxcf *-* . . ***** * *i f1101Tr-* ** **** in6*-***-** f5iis41 ** ..... --* **

.!~.~ '.,~l_kl_\.~'.~!lg.:'-~~l_Y~:_a~~!e_t~o~s. \~~.re._per.f~n~.e~.:._ ...... -*- ............................... *-*** ..... __ **- ............ ***- ...................................... *-*** _ . _... .

M~!l.1.9.L ....._. _.... _..... P.~sc.r!.Pt!<:~~ ............ _.......................... --***-.. *. -*- ...... __ ...... A.11alys.t Cp~1~~11Js. .. _ .... -**-* ...-**-*-** _.. l ASTM D 2216 (Modified) 2 DOE HASL 300. 4 5 2 3/Go.-01-R 3 EPA 900.0iSW846 9310iSM 71108 Modified Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

GEL LA BORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analrsis Company: MJW Corporation Address: 15 Hazelwood Drive Suite l 12 Bu!Talo. New York 14228 Report Date: December 17. 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.4.R.4 Project: MJWCOOl 15 Sample ID: 385068003 ClientlD: MJWCOOI Matrix: Soil Collect Date: 19-0CT- I 5 Receive Date: 05-NOV-15 Collector: Client Moisture: S.9% P~1*_a?.1e_ter ____ ... _ ......... __ Q.u.~_lilie_r_ .. Result Le TPr ......... ~L... r11\ts. . . l?.:F..;\n:it:r.st. Date Time Bat<:~. .~ltd~. Gravimetric Solids AST!vf D 2216 % Jfoisture "As Received" Mmsturc 8.90 percent CXCI t t/1\1115 1326 1521841 Rml Gamma Spec A.ualysi$ Gam(1wspec, Gamma. Solid "DIJ' Weight Corrected" Actimum-227 U 0 05S5 +/-0 289 () 545 0.254 -;-/.0290 pC1/g RXF2 l2i03/15 0707 1522393 2 Antimony-125 u 0.00225 +/-0.112 0205 () 0937 +/-0_! 12 pC!/1! fhsmuth-212 U! 0.00 +/-0.754 1.46 0674 +/-0 961 pCi/g Bismuth-214 0 774 +/-0.174 0 149 0.0674 +/-0. l&S pCilg. Ccsium-137 0 0806 +1-0 0521 0.0878 0.040 ~1-0.0526 0 JOO pCi/g Coball-60 u -0 0334 +1-0.0537 0 0943 0.0409 .;./.()0559 p(\/g Europ1um-l 54 u O.oJIJ6 +/-0.152 0.298 Cl.132 +/-0 152 pCi/g Lcad*212 I.JO +/-0.143 0 128 0.0602 +/-0 176 pCi/g Lead-214 0989 +/-0.206 0 17\ 0.0793 +/-0224 pC1lg Potassium-40 15 5 +/-\.67 ll.775 (\ 324 +/-2 13 pC1/g Pro!actmimn-231 Ul 0 00 +/-0 760 d 952 (J.439 +/-0.832 pCilg Radium-226 0.774 +/-0 174 ll.149 () 0674 +/-0 188 pCi/g Radium-228 0644 +1-0 326 0.3\5 0 140 +l-0 341 p{'i/g

'.llmllium-208                                                 0349             +/-0.0761         00597    00312       +/.() 0823                 pCi/g Tm-126                                          UI               o.no             +/-0.170         n..!ll    ().101      H-0171                   pCi!g Rad Gas Flow Proportional Counting GFPC. Gross A-B. solid "D1y Weight Correc1ed" Alpha                                                            7.79              +/-3.14            3 84      1 (j l     +1*3.48         4.00   pCilg              JXll7      12/02115 1548 1525762       3 Bein                                                            22.l              +/-3 1J            3 06      1.41       +l-4 42         HJ()   pCi.lg
 !.~.it;, ~~-1.ltn~i-~g:l~rcp -~f~_tl~o~~ ~:c~e .P.l!rf.oi:lllc~..

Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Sml Prep GL-RAD-A-021 CXCI J 1/10115 1326 1521&41 '_r!1e_ f()ll~_lXi~g_':\'.1.~.1xti_~~1. i\~_ethods wc:re.Jll!l.'f.'.1.1:!.':1~_d ........... _. _.

\lcthod Dcsc1*iption ASTM D 2216 (Modified) 2 DOE t!ASL 300, 4.5.2.31Ga-Ol*R 3 EPA 900 OiSW846 9310iSM 11106 Mod1fi~d Surrogat*effraccr Reco\*cry Test Balch ID Recovery% Acceptable Limits

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite! 12 Buffalo. New York 14228 Report Date: December l 7, 2015.

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.4.R.4 Project: MJWCOOl 15 Sample ID: 385068003 Client ID: MJWCOO l Le Tl'l" .... -~-~-.... l~_n_it.~ ....!)r-:. _;\n:tly~t .. J?.~te. !~me__ !J.~t.~~-- _:\'lt<l.: Surrogateffracer Recovery Test Batch ID Recovery% Acceptable Limit.~ Notes: TPU and Counting Uncertainty are calculated at the 95'l-~ confidence level ( 1.96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (a43) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 7.1015 Company: MJW Corporation Address; 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact Ms. Laurie Losey Project: Soil Radioisotopes 000'** ***' HOOHO ,., .... .. .. .. . ... . . ..... Client Sample ID: 3.2.4.R.5 Project: MJWCOOl15 Sample ID: 385068004 Client ID: MJWCOOl Matrix: Soil Collect Date: 19-0CT-!5 14:[0 Receive Date: 05-NOV-IS Collector: Client Moisture: 9.&7%)

~~~:~m.:~e:._ ......................... g_lia~~.:~.        Result ..l!.~~.:rt_ain.tr ........ ~ll)C: ....... R:L .............. l!.~_i_ts .......... J::>~ . t\~~IY.s! ..!)~t~. *-*!~~!le ~.~~ch. ~~e_t~o,~.

Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 9 87 percent CXCI 11/10115 1326 1521841 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutomum-238 l! -0.00459 +/-0.03% 0 0917 I 00 pCi!g HAKB l l/23115 1501 1522577 2 Plutonium-2391240 U U.00153 +f-0 ll7U2 0 154 I.DO pCti!,l. ASP Uranium Isotopic, Solid "Dry Weight Corrected Uramum-232 lJ !} 0125 +f-0.0672 0.126 I 00 pci!g HAKB 11/24115 0851 l.522580 3 llramum-233/234 0. 940 *~/-ti 258 0 0991 I 00 pclfg. Uranium-2351236 0 ogg7 +f-0.0866 0.0538 I 00 pci/g Uranium-238 0. 769 +/-0 233 0 0537 I 00 pc1/g Alphaspec Np237, Solid "Dry Weight Corrected Ncpmnium-237 U -0.033 l +/-0.146 0.382 I 00 pC1/g HAKB 11/23115 1706 1522576 Alphaspec Th229 + 228,230,232 Solid "01)1 Weight Corrected" Thorium-228 l! 0.416 +1-0.459 0.725 1.00 pC1/g HAKB l 1/24/15 1014 1522579 5 Thorium-229 ll 0 161 * +/..() 261 0421 1.00 pCi/g Thonum-230 0 796 +/-0.424 0 318 l.llO pCi!g Thonum-232 1 14 +/-0 501 () 342 ! 00 pCr/g Am24 l, Cm Solid "Dry \\ieight Corrected" Ammcium-241 . U 0.0114 +/-0.080 0.164 1 00 p('t!g HAKB \ i/24115 1042 1522571 Curium-242 U 0.00 +/-0 044 0.0654 l.00 pCt/g Curium-243/244 U 0 021 +/-0. 133 0261 1 0() pCi!g Curium-2451246 IJ 0.(1494 +/-0.0874 0 132 l ()fl pCi/g Liquid Scint Pu24!, So.lid "Dry Weight Corrected" Plutonium-24 I U -I 12 .,./-6 25 10 8 15 0 pCilg HAKl3 11125115 0728 1522578 7 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" lodme-129 U -0'.040S +/-0 283 0496 1.00 pCi/g MJH l 12/02f15 l 3.J I 15223 74 8 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actimum-227 U -0.042 +/-0.264 (} 50[) pCifg RXF2 12/03/15 0707 15223'>3 9 Anlimony-125 U 00101 +/-0.106 01()() pC1/g Cesrum-137 O.U82 I +/*0.0612 0 0811 ll.1.00 pCifg Cobalt-60 U O.ol 19 +/-0 0448 0.0924 pCilg Europium-15.J U 0.0149 +1-0*130 0261 pCilg Protactrnium-231 lJ (i.675 +l-0.529 l 08 pC1/g

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 7. 2015 Company: MJW Corporation Address:. 15 Hazelwood .Drive Suite 112 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil ~adioisotopes

             '* M. 0 ~           0 **' '*' 0 0 '                  '. "'" -*  M ** 00 0 *-**

Client Sample ID: 3.2.4.R.5 Project: MJWCOOl 15 Sample ID:. 385068004 Client lD: MJWCOO! Rad Gamma Spec Analysis Oammaspec, Gamma, Solid "Dry Weight Corrected" Radium-226 0 650 +/-0 197 0 142 pCi/g Radium-228 0.740 +/-0.344 0.254 p('l/g Tm-126 U 0 0509 +f-0.118 0.136 pCi!g Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid Dry Weight Corrected" Alpha 14.3 +1-4 0(1 3 97 4 (]() pCi/g JXIl7 12102!1 S 1218 1525762 10 B~ n1 +/-3 26 3 20 ll)O pC1/g OFPC, Sr90, solid "Dry Weight Corrected" Strmllhun-90 U -0.149 +1-0.410 0857 2.00 pC1!g KSDl 12/03115 1125 J 525755 11 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium

U 1 83 +/-1 74 2B3 6.0!l pC1/g TXJ I 12102115 1149 1522724 12 Liquid Scint C 14, Solid "Dry Weight Corrected" Cnrbon-14 U -0 897 +l-0756. *I 33 2.00 pC1fg TXJ I 12/03115 1828 l 522716 13 Liquid Scint Tc99, SoHd "Dry Weight Corrected" Tcchnctium-99
V. I 61 +/-1.50 250 5.00 pCilg MYMl 11129115 092.J 1522715 14 T~.e .fo)lo~i~~- ~~t:P JY!e.thci.~~."'.e.:.e p~f.fgi:r.ne.d:.......-.. -* .......... **-* .......

Method Description Analyst Date Time Prep Batch n;:;;.-~iOii *iircii. * * ***** *- ** **** ** ** oiY.sol°i°.Prcii.df::.R,\i::i:A::oii *** ***** **** *cxcr- -* * **-******1iii0/i5**** 1326 ***---*-fs*ff84r*** *--*-* ******* .... ***-**-**-** *--*-***-***

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 7, 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite I 12 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.4.R.5 Project: MJWCOOl 15 Sample ID: 385068004 Client lD: MJWCOOI

!~c _f()_l.~o~vin~ -~~~lY._t_i~al_jyf~~h..".d.5. :".e.r~ perf??Jle~:.

.MeJh9d___ .. ... ... . ........ Pe!ic_rip~!IJ..11_ -**** ... . ... ... .. ....... _.. _ ........ _ -* *--**-** .............. *-* ...-**. ....... A.rii;h'.§1.C:.orn.I11.e1!!S ..... - .......... ***-* *-* .... _.. .. ... . I ASTM D 2216 (Modified) 2 DOE EML HASL-300. Pu-11-RC Modified 3 DOE EML HASL-300. U-02-RC Modified 4 ASTM C 1476-00 Modified DOE EML HASL-300. *111-01-RC Modified 6 DOE EML HASL-300, Am-05-RC Modi!ied 7 DOE EML HASL-300, Pu-11-IK Modified 8 DOE EML HASL-3QOJ-OJ Modified 9 DOE HASL 300, 4.5.2 J/Ga-Ol-R

!(I                                    EPA 900.0/SW846 9310/SM 71108 Modified 11                                     EPA 905.0 .Modified/DOE RP50 I Rev I Modified 12                                     EPA 906.0 Modified 13                                     EPA EERF C-01 Modified J4                                     DOE EMI.. l!ASl.-300. Tc-02-RC Modified S!-!l!~~~~~T.:.zice'. .I3:~~.oyery           Test Plulonium-242 Tracer                        ASP Plutonium lwtopic, Solid "Ory Weight                                                                                          75 3               (15%-125%)

Corrected"

Uranium-232 Tracer ASP lJramum lso1op1c, Solid "Dry Weight 79.1 (15%-125%)

Comictcd" Uramum-2J5/236 Tracer ASP Uranium Jsotop1c, Soiid "DI)' Wt:tght 78 3 (15%-125%) Corrected" Amcricmm-243 Tracer Alplmspcc Np237, Solid "Dry Weight Corrected 96.2 (15%-125%) Actimum-227 Tracer Alphaspcc Th229 + 228.230.232 Solid Dry 102 (15%-125%) Weight Corrected"

Americium-243 Tracer Arn241, Cm Solid "Dry Weigh! Corrected" 65.6 '15~*~-125~~)

Plutomum-242 Tracer Liquid Scmt Pu24 I. Solid "Dry Weight Corrected" 75.3 (15%-125%) Strontium Carri~r GFPC. Sr90, soh<l "Dry Weight Corrected" 91 {25%-125%} Technet1um-99m Tracer Liquid Scint Tc99, Solid "Dry Weight Corrected" 96 3 (15%-125%) Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address:* 15 Hazelwood Drive Suite 112 Buffalo_ New York 14228 Report Date: December 17, 2015

Contact:

Ms. Lnurie Losey Project Soil Radioisolopes Client Sample ID: 3.2.4.R.5 Project: MJWCOO 115 Sample ID: 385068004 Client ID: MJWCOOI Matrix: Soil Collect Date: i 9-0CT-15 Receive Date: 05-NOV-J 5 Collector: Client Moisture: 9.87%

Parameter Le Gra,*imetric Solitls AST..\1 D 2216 % Moisture "As Received" Moisture 9.87 percent CXCI ll/HJflS 1326 1521&41 Rad Alpha Spec Analysis ASP P/11/011ium Isotopic. Solid "Dry Weight Corrected" Plutonium-238 u -0.00459 +f-0.0396 0.0917 o.om H-0 0397 1.00 pC1/g HAKB 11/23!15 1501 1522577 2 Pltitonium-239/240 tJ 0.00153 .fo/.Q ll702 () 154 l) 1)485 +l-0 0703 LOO pCilg ASP Uranium Isotopic. Solid "Dry rVeighr Corl'ec/ed" Urnmwn-232 u 0.0125 +f-0.0672 () 126 (J 0529 +f-00673 1.00 p<.:1/g HAKB 11124115 0851 15225&0 3 Uromum*233i234 0940 +l-0.258 ()0991 0.0227 +/-OJI I 1.00 pclfg Uramum-235/236 ll.08_97 +/-0.0866 () 0538 000 +/-() 0881 1.00 ~1/g Uramum-238 0.769 +l-0 233 0.0537 00() +/-0.273 1.00 pci.lg Atphaspec ,\'p137, Solid "Dry lfeight Corrected" Neptumum-237 u -0.0331 +/-0.146 0.382 0 0874 +l-0. ).i(, 1.00 pC1/g HAKH 11123/15 l7n6 1522576 4 Alphasper: T'1229 + 228.230.232 Solid "Dry Weight Corrected" Thonum-228 0.4 Hi +/-0 459 0 725 0.282 +/-0 464 100 pC1lg f-IAK8 l 1124115 l0l4 1522579 5 Thorium-229 0.161 +/-0 261 0421 0 132 +/-0.262 l.1)0 pC1lg 11torium-230 0 796 +/-0.424 0 318 Cl 08U9 +/-0.439 I, 00 pCl/g Thorium-232 l 14 +/-0.501 () 342 0.0932 +l-0 528 I 00 pCi/g

    .4111241. Cm Solid "D1y Weight Con*er:ted" Amcncium-.24 l                         u        0.0114       +/-0.08(}       0164    (l  0538     +/-Cl.080       LOO     pC1ig         HAKE ll/24115 !042 1522571    6 Curium-242                                         0.00      +/-0044       ()()654        ()(}() +/-0.0441        I 00    pC1!g Cunum-243/244                         u          0021        +/-0.133         0.261     0.102     +/-0.133        1.00    pC1lg Curium-2451246                                  0.0494    +l-0 087*1          0.132  0.0337      +1-0.mm           I 00   pC1lg Liquid Seim Pi124 l. Solid D1:i* IVeight Correcred" Plutonium-241                          lJ        *Lil          +/.(, 25         10 s      s 27       +f-6.25      15 0    pCilg         HAKB 11125!15 0728 1522578    7 Rad Gamma Spec Analysis Gamma 1!19. Solid Dry Weighr Col'/'ected" lodine-129                             u      *O 0408        +/-0 283         0 496     0228       +/.(l 283       1.00   pCilg          MJHI .!2/021151341   1522374 8 Gammaspec.. Gamma. Solid "Dry Weig/it Corrected" Actinium-227                          u        -0.042       +/.(J 264        0 500     0.233      +/-0.264               pC\lg          RXP2   12103/15 0707 1522393 Y Antnnony- 125                         u        0.0101       +1-0 wt,         0.200   0.0919       -+-/-U I06             pC1/g Bi;muth-212                                         l 93       +1-1 (16       0.957     0.425        +f-1 08              pCi.fg Bismuth-214                                      0.650      +/-0.197         (] 142  00643        <-/-0.205              pCilg Ccsium-137                                      0.0821     +l-0 0612        0 0811    0.0367     +/-l)06Hi       O. IO(J  pC1/g Coball-60                              lJ       0 0119     +1-D 044&        0.0924    0.0402     +/-0 0451                pC11g Emopium-1 54                          u        0.0149       +/-0.130         0.261     0 114      +/-0.130               pC1/g Lcad-212                                            1.13    +/-0 137         0 !07   0 0496       +/.!) 168              pCc/g Lcad-214                                         0 999      +/.() 167        0 154   (J 0713      +/.(J 187              pC1!g

GEL LA BORATORIES LLC 2040 Savage Road Charleston SC 29407 - {843) ~56-8171 - www.geLcorn Certificate. of Analysis Company: MJW Corporation* Address: 15 Hazelwood Drive Suite 112 Bu!Talo. New York 14228 Report Date: December 17. 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.4.R.5 Project: MJWCOOJ 15 Sample ID: 385068004 Client ID: MJWCOO\ Parameter Result......... t:nccrtaintv

                                                                              -* ....                    :VIDC Rad Gamma Spec Am1l;rsis -'

Gammaspec, Gamma, Solid "Dr_r Weight Corrected" Potassium-40 14.5 +f-1 64 0577 0-228 +/-2 07 pCi/g ProlaCllnium-231 lll o_oo +1-0.529 LO& 0 505 +/-ll 62<J pC1/g Radium-226 0.650 +f-0.197 0 \42 () 0643 +!-0.205 pCi/g Radium-228 0.74(} +1-0 344 0 254 0.111 +l-0.361 pCilg Thallmrn-208 0-348 +l-0 080 0.()64 oo:m +/-0.0854 pCi/g Tin-126 lJ 0. 0509 +/-0 118 0 136 0_1164 +/-() 119 rCifg Rad Gas Flow Proportion11I Counting GFPC. GYOSS A.:B. solid "D1y Weig/it Corrected Alpha 14 3 +/-4.06 3.97 1 65 +/-4 97 4 ()() pCilg JXB7 12102115 1218 1525762 10 Bm n3 +/.3.26 3.20 147 +/-4 65 ]()_0 pC1!g GFPC'. Sr90. solid "DIJ' Weight Correcred" Stronlmm-90 U -0 149 +/-0 410 () 857 0 367 +/-CJ-410 200 pCi/g KSDI 1,2/()3115 1125 1525755 II Rad Liquid Scintillation Analysjs LSC, Tritium Dist, Solid "D13* Weight Corrected" Tritium I 83 i/.J.74 2.83 123 +1-1-74 6 00 pCr/g TXJl 12102115 1149 1522724 12 Liquid Scint CJ./. Solid "D1J' /Veight Corrected" Carbon-14 U -0.897 +1-0.756 i 33 0.650 +/-0.756 200 pC'i/g TXJ\ I2i03/I s 1828 1522716 13 Liquid Seim Tc99, Solid "Dry Weig/it Correcled" Tcchnet1um*99 1.61 +1-1-50 2 50 1.20 l-1-1 51 s 0() JiCifg MYM 11129115 0924 1522715 14 I J~~ __fo_l_lo~'\'!n_g Pr~_Met~~~-~ _wc.re_11,l!rro_r.111_~d. __ .......................................................................... *-**** ....... .... .. ... ******* .. ***** .............. . !'l*lethod Ocscription - Analyst Date Time Prep B11tcfi Dry Soil Prep - Dry Soil Prep GL-RAD-A*021 CXCl - 11110115 1326 1521841 T_he foll':l'Y.!~g_A_n~IIt!c_nl__l\.~~th_o~~-l\'e.r.1: r.~rl~_r_01_c~-- Methnd Descriptian ASTM D 22 \C> (Modified) 2 DOE EML l!ASL-300. Pu- I I-RC Modilied J DOE EMI. l-IASL-300, U-02-RC Modified 4 ASTM C 1476-00 Modified s DOE EML HASL-300. Th-01-RC Modified 6 DOE EML HASL-300, Am-05-RC Mod1ficil 7 DOE EML HASL-300, t>u-11-RC Modified s DOE EMLHASL-3t)().HJI Modified 9 DOE HAS!- 300, 4 5.2 3/Ga-01-R 10 EPA 900_0.ISW846 93 IO/SM 71 IOB Modified 11 EPA 905.0 Mod1l1cd!DOE RP501 Rev I Modified 12 EPA 9D6.0 Modified 13 EPA EF..RI' C-01 Modified

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: IS 1-lw.c:lwood Drive Suite 112 Buffalo, New York 14228 Report Date: December 17. 20 J 5

Contact:

Ms. Laurie Losey Project: Soil Rudioisotopcs Client Sample JD: 3.2.4.R.5 Project: MJWCOOI 15 Sample ID: 385068004 Client ID: MJWCOOI Parameter ___ .._____ . _Q~~l}fl~r. __ .. . .. - ... -**FncertaintY Result . --****-*--**--* - .... MDC Le .... Il'.l' ___ ..... l~L. _..l~ni~_ .. _l>f . .~"'!~l~t _.. pate__Tin_1i: __ 1lll~c.h,. Mtd. 14 DOE EML HASL-300. Tc-02-RC Modified Surrogatcffr.accr RecDl'ery Test Batch JD Recovery% Acceptable Limits Plutonium-242 Tmcer ASP Plutonium Isotopic. Solid "Dry Weight Corrected" 1522577 75.3 (15%-125%) Uranium-232 Tracer ASP l!ranium Isotopic. Solid "Dry Weight Corrected" 1522580 79.1 (15%-125%) Uranium-235/236 Tracer ASP Uranium Isotopic, Solid "Dry Weight Correc1ed" 1522580 78.3 (!5%*125%) Americium-243 Tracer A!phnspcc Np237, Solid "Dry Weight Corrected" 1522576 96.2 ( 15%- ! 25%i) Actinium-227 Tracer Alphaspec Th229 + 228,230.232 Solid "Dry Weight Corrected" 1522579 102 (15%*125%) Amcricium-243 Tracer Am24 I, Cm Solid "Dry Weight Corrected" 1522571 . 65.6 (15%-125'%) Plutonimn-242 Tracer Liquid Scint Pu24 I, Solid "Dr) Weight Corrected" 1522578 75.3 (15%-125%) Strontium Carrier GFPC. Sr90, solid "Dry Weight Corrected" 1525755 91 (25%-125%) Technetium-99111 Tracer Liquid Scint Tc99, Solid "Dry Weight Corrected" 15227,15 96.3 (15%-125%) Notes: TPU and Counting Uncertainty arc calculated at the 95% i;:onfidence level ( 1.96-sigma).}}

@@ Line 16: / Line 16: @@
 =Text=
-{{#Wiki_filter:Appendix Sub-Area 3.2 -COA GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms .. Laurie Losey . . *"-_ .. . . . . S&deg;'il. Radioisotopes Client Sample ID: 3.2. l .R. I Sample ID: .385070020 Ma1rix: Collect Date: Receive Date: Collector:
+{{#Wiki_filter:Appendix G-Sub-Area 3.2 - COA
-Moisture:
-Soil 16-0C'T-15 15:05 05-NOV-15 Client 26.1% Parameter Qualifier Result Uncertainty MDC .........
-***.*** ...... --***-***********
-.. . Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 26 l Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Actimum-227 "Dry Weight Corrected" l! -0 125 +f-0 289 Antimony-125 u () 0292 +/-0.120 C'<:$ium-137 0.468 +/-0 126 Cobalt-60 Europium-154 Protactmium-231 Radium-226 Ra<lium-228 U. u u Tin-126 U Rad Gas Flow Proportional Counting 0 00212 -0 00831 0.568 0 64 I 0.856 0 106 GFPC, Gross AiB, solid "Dry Weight Corrected" /llpha 14 7 Beta 22 9 +/-0 0502 +i-0.157 ;./.() 585 +/-0.190 +1-0.261 +/-0.177 +/.J 11 +!-3.59 ll 536 0229 0.0895 0.099 \l.3Cll} I 19 0.166 0 377 0189 3.45 3.7J Project: Client ID: RL pcrcem pC1/g pCi!g 0 IQO pC1/g pC1lg pCllg pCi/g pCi/g pC1/g pCi/g 400 pC1/g IO!l pCt/g Repmt Date: December 4, 20 I 5 MJWCOOl 15 i\*1JWCOO!
-CXCI 1 lilO/l5 1319 !521842 RXF2 12103115 1307 1522383 KXB2 12i02/l5 1125 1525757 3 :f.hc:
-.. . . . ... ...... . . ... .... . . . . .. . .. . ..............
-_. . .... ... . . ... , .......................
-_ ................
-**-Method Description Analyst Date Time Prep Batch biY s;,*,i *ri-e"P. * *-*** * * **** **
-****--* * ** ** * ** **** * ***cxcf* -i"ii1(J/!5
-* *****-** *
-******
-* t"s2Ts42 ** ****** The.
-..
-: .. _. ... .. .. . . . ... . .... .. .... .. . . ... .. .. . .... .. . .. . . . .
-******-*-......
-******-****-
-....... *--*** ..................
-***--* .... . . ........ Ana!_y!!t.C()!n.t:rl.<!!11,lL
-..........
--*** ......................
-_ ... . ASTM D2216{Mod1fied) 2 DOE HASL 300, 4 5 2 3iGa-O I *R 3 EPA 900.0ISW846 93\0iSM 71 \0B Modified Notes: Counting Uncertainty is calculated at the 95% confidence level (I .96-sigma).
-GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Anal;ysis Company: Address: Contact: MJW Corpornlion 15 Hazelwood Drive Suite 1 l2 Buffalo. New York 14228 Ms. Laurie Losey Project Soil Radioisotopes Client Sample ID: 3.2. l .R. l ID: 3&5070020 Matm;: Soil Collect Date: 16-0CT-15 Receive Date: 05-NOV-J 5 C'ollector:
-Client Moisture:
-.1 %
-..... -*** ....
-..... Result _____
-.......
-Le Gravimetric Solids ASTM D 2216 % Mois!llre "As Received" Mo18ture 26 l Rad Gamma Snee Arrnlysis Gamma.wee, Gamma. Solid "Dt}' WC!ight C01*1*ecfed" Actinium-227 u -0. 125 +/-0 289 0 536 Anllmony-125 u 00292 +1-0 120 0229 Bismutl1*2 I 2 u 0 723 +i-t 05 l 65 Bismuth-214 0.641 +/-0.190 0 16& Ccsium-137 0.468 +/-0 126 0 08')5 Cobalt-60 l! 0 002.12 +i-0 0502 0.099 Europmm-154 c -000831 +/-0.157 0 30(1 Lead-212 I 21 +1-0.144 0 121> . Lead-214 0.983 +/.().215 0173 l'olilss1um-40 143 +/-1.80 0.609 Prot;11;tinium-23 I Ul 0.00 +/-0.585 l.19 Radium-226 064! +/-0. \90 0 166 Radiutn-228
-() 856 +/-0 261 0.377 Thalhum-zog 0.343 +l-0 l09 () 074 Tin-126 UI 0.00 +/-0.177 0.189 Ratl GllS Flow l'roportional Counting GFPC. Gmss ;J B, solid "Dry Weight C'orrec1ed" Alpha 14 7 +l-4 l l 3.45 Bew 22 9 +/-3.59 3.73 !ht!
-........ **--*-........................ . Method Dry Soil Prep D1y Soil Prep UL-RAD-A-021 "f 11(!_
-*-_ ... Method Description I 2 3 ASTM D 2216 \Modificd)
-DOE l lt\SL 300, 4 5.2.3iGa-Ol-R EPA 900 O!SW846 93 IO/SM 71 IOB Modillcd Su rrogate!fracer Recover}'
-Test 0 248 () 105 (J 759 0.0747 0.0401 110421 0 130 00589 {J.07')6 0.231 0 55& 0.0747 0.168 I) 0328 1).1)899 1 34 1.72 . Analyst CXCI Report Date: December 17, 2015 Project: Client ID: MJWCOOI 15 MJ\VCOOI .... Tf'.r. . ....... !l.1: .. _ ..
-.... Ilf'. _:\n_al,r.st Dale Time Batch Mtd. percent C'XCI -l \110115 1319 1521842 +/-0 295 pC1/g RXF2 12i'03115 1307 1522383 2 +!-0 121 pC1/g +/-1 10 pC:i/g +/-0 p('ilg +/-0 IJ2 0 100 pC'i!g +/-0 0502 pCi/g +1-0.157 pCi!g +/-0 175 pC1/g +/-0 231 pC1/g +/-2 18 p('t/g +/-0.651 pCilg +!-0 198 pC1/g +l-(1 286 pC1fg +1-0l13 pCilg +/-O. l7S pC1fg +!-5 00 400 pC1/g KXB2 12/02/15 1125 1525757 3 +/-4 84 JO 0 pC1/g Date Time Prep Batch 11110115 1319 1521842 Batch LO Rec1wcry%
-Acceptable Limits GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com C.ompany:
-Address: MJ W Corporation I :i Hazelwood Orivc Suite 112 Buffalo. New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.1.R. I Sample ID: 385070020 Surrngateffcaccr Recovery Test Notes: Certificate of Analysis TPU and Counting Uncertainty are calculated at the 95% confidence level ( l.96-sigma).
-Report Dnte: December 17. 2015 Project: MJWCOOI 15 Client lD: MJWC'OOl Batch ID Recovery%
-Acceptable Limits
-Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: Project: MJW Corporation 15 Hazelwood Drive Sui1e 112 Buffalo. New York 14228 Ms. Laurie Losey Soil Radioisotopes Client Sample lD: Certificate of Analysis Report Dme: December 17. 20
+GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Repmt Date: December 4, 20 I 5 Company:                         MJW Corporation Address:                         15 Hazelwood Drive Suite 112 Buffalo, New York 14228
+==Contact:==
+Ms .. Laurie Losey
+       . . *"- _.. ~!~J_ect.:               . . . . S&deg;'il. Radioisotopes Client Sample ID: 3.2. l .R. I                                                                                                                     Project:                MJWCOOl 15 Sample ID:                       .385070020                                                                                                       Client ID:               i\*1JWCOO!
+Ma1rix:                          Soil Collect Date:                     16-0C'T-15 15:05 Receive Date:                     05-NOV-15 Collector:                       Client Moisture:                        26.1%
+Parameter                                Qualifier          Result Uncertainty                           MDC                    RL Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture                                                            26 l                                                                                     pcrcem                            CXCI 1 lilO/l5                  1319 !521842 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Actimum-227                                           l!        -0 125          +f-0 289                     ll 536                                              pC1/g                         RXF2 12103115                   1307 1522383 Antimony-125                                          u         () 0292         +/-0.120                     0229                                                pCi!g C'<:$ium-137                                                      0.468         +/-0 126                   0.0895                   0 IQO                        pC1/g Cobalt-60                                             U.       0 00212        +/-0 0502                      0.099                                               pC1lg Europium-154                                          u      -0 00831           +i-0.157                     \l.3Cll}                                            pCllg Protactmium-231                                       u           0.568         ;./.() 585                       I 19                                            pCi/g Radium-226                                                        0 64 I        +/-0.190                     0.166                                              pCi/g Ra<lium-228                                                       0.856         +1-0.261                     0 377                                               pC1/g Tin-126                                               U           0 106         +/-0.177                     0189                                                pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AiB
 ASP Uranium Isotopic, Solid "Dry Weight Corrected''
-ASP Uramum Isotopic.
+Uramum-232                                        lJ          !} 0125       +f-0.0672           0.126             I 00            pci!g                        HAKB 11/24115      0851    l.522580       3 llramum-233/234                                                  0. 940        *~/-ti   258    0 0991             I 00            pclfg.
-Solid "Dry Weight Corrected" Np237. Sol 1d "Dry We1gh1 Corrected" Alphaspec Th229 + 228,230,232 Solid "DI)* Weight Corrected''
+Uranium-2351236
-Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu24 I, Soltd "Dry Weight Correctl!d" GFl'C. Sr90, "Dry Weight Corrected" L1qmd Scmt Tc99, Solid "Dry Weight Corrected" Counting Uncertainty is calculated at the 95% co1Jfidcnce level ( 1.96-sigma).
-Project: Client ID: Nominal Report Date: December 4, 2015 MJWC00!15 MJWCOOI ..
-65B 66 8 90 3 &.J..8 90 8 80.7 &9 9 98.1
-__ q_mits (15%-125%}
-%-125%)
-(15%-125%)
-(!5%-125%)
-{!5%-125%)
-(15%-125%)
-(15%-125%)
-{25%-125%)
-(15%-125%)
-' --------------------------------GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis . Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Contact: Ms; Laurie Losey Project: Soil Radioisotopes Client Sample ID: 3.2.1.R.5 Sample ID: 38507002 l Matrix: Soil Collect Date: \6-0CT-15 Receive Date: 05-NOV-15 Collector:
-Client Moisture:
-.!%
-..................
-quaHfie_r_
-.. Result ..
-MDC Gravimetric Solids AST?.1 D 2216 % .\4oislure
-''As Received" Moisture :26 L Rad Alpha Spec Arsalysis ASP Phitoni11m Isotopic, Solid "Dry Weight Corrected" Pluiomum-238 0.0398 +f.O 0682 0.0597 Plutonium-2391240 u -0 0223 +/-0.076 0 188 ASP Uranium Isotopic.
-Solid "fJry Weig/it Corrected" Urarnum-232 u -0 0077 +f-0.0532 0.129 llnuuum-2331234 0 738 +f-0 260 0.126 Uram1J111-235/236 0.159 +f-0 127 00683 l/ranium-238
-\.09 +/-0.312 (J.068! A/phaspec Np237, Solid U-'eight Corrected" Ncptumum-237 u -OlllH +f-0. \51 0 485 Alplraspec Th229 228,230,232 Solid ''DI')' Weight Corrected" Thorium-2W 0 992 +/-0.587 () 663 *niorium-229 .U -0 0684 +/-0 279 0.659 Thormm-230 I 16 +/-0.606 0.629 Tnonu111-232 il.663 +l-

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