ML16294A234

Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey Conducted in 2014, Rev. 0, Appendix G, Part 11 of 11

ML16294A234
Person / Time
Site:	West Valley Demonstration Project, P00M-032
Issue date:	08/22/2016
From:	MJW Technical Services
To:	Office of Nuclear Material Safety and Safeguards, State of NY, Energy Research & Development Authority, Office of Nuclear Reactor Regulation
Shared Package
ML16293A155	List: ML16293A130 ML16293A131 ML16293A132 ML16293A133 ML16293A134 ML16293A135 ML16293A136 ML16293A137 ML16293A139 ML16293A140 ML16293A141 ML16293A142 ML16293A143 ML16293A178 ML16293A179 ML16293A180 ML16293A181 ML16293A182 ML16293A183 ML16293A184 ML16293A185 ML16293A186 ML16293A187 ML16293A278 ML16293A279 ML16293A281 ML16293A282 ML16293A364 ML16293A365 ML16293A366 ML16293A367 ML16293A368 ML16293A389 ML16293A391 ML16293A392 ML16293A393 ML16293A394 ML16293A674 ML16293A675 ML16293A676 ML16293A677 ML16293A678 ML16293A808 ML16293A809 ML16293A810 ML16293A811 ML16293A812 ML16293A843 ML16293A844 ML16293A846 ... further results
References
Download: ML16294A234 (32)

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{{#Wiki_filter:Appendix G WNYNSC Confirmatory Certificate of Analysis I I WNYNSC Confirmatory (C) -COA GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company : MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: ......... _ .... Client Sample ID: C.l.Cl Sample JD; 385101001 Matrix: Soil Collect Date: 15 l 4:50 Receive Date: Collector: Moisture: 05-NOV-15 Clienl 34.5% ............. -* .... ... __ :Resu!_t_. _Uncertaint1 .... Gravimetric Solids ASTM D 2216 % Moisture "As Received" 345 Rad Gamma Spec Analysis Gmnrnaspcc, Gamma, Solid Aclmium-227 "Dry Weight C01Tected" l.I I) \[)9 +/-0 348 Antimony-12j u Cesiurn-137 Cobalt-60 ti Europium-154 u Protactmmm-231 lJ Radtum-226 0.0694 I 24 -0.00666 0 162 0.891 0.886 +/-0 137 +J,(J.141 +/-0.0499 +/-0 229 +/-0.714 +!-() 1% Radiurn-228 I 06 +/-0 358 Tm-126 U 0 133 +l-0 143 Rad Gas Flow Proportional Counting GFPC. Gross AIB. solid "Dry Weight Corrected" Alpha 9 44 +/-3 16 Betu 290 +/-2 82 P_re_p ... Metllod Description

• br}-.. s<<i1f Prep . *-** .. . .........
  • -*D";y**so*il

__ ........... . .. .................... . ASTM D2216(Modificd) DOE llASL 300, 4 S.2.3/Ga-01-R 0.652 0257 0.0961 (J 0949 0.370 i.:w ll 192 0 321l () 164 3.84 222 ****-* ---** ... I 2 3 EPA 900 OiSW846 9310/SM 71 IOB Modified Notes: RL I) !00 .j 00 JOO Project: Client JD: MJWCOOl 15 MJWCOOl . _ ..... __ -* . _ *-. Time Batch Method percent LYTI l lfl0115 0955 1521927 pCtlg RXF2 12103/15 0721 15223$6 2 . pC1/g pCilg pC1/g pC1lg pC1ig pC1/g pCilg pCilg pC1lg JXB7 12i02/15 !405 1525768 3

• pCilg . ... ... .. ... -**-*--* ***-**-**
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• -***** .... . ... **-* Date Time Prep Batch Analyst 1:v*t"f .. *-*-*nifoiw** -. -*0955*--. *-B:21";i.2f . .

....... *-** . -* .. -.. . Counting Unce1tuinly is calculated at the 95%, confidence level ( 1.96-sigma). GEL LABORATORIES Ll.C 2040 Savage Ro.ad Charleston SC 29407 -(843) 556-8171 -v-rww.gel.com Certificate of Analysis Company: Address: Contact: Project: MJW Corporation l5 Ha-1.clwood DriYe Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Soil Radioisotopes Client Sample !D: CJ.Cl 385101001 Soil 27-0CT-15 05-NOY-!5 Client 34.5% Saiuple ID: Matrix: Collect Date: Receive Date: Collector: Moisture: Par:rmctcr Result .. : .. .. _'.\I.DC: Gra,*irnctric Solids AST..\1D2216 ?a Mois111re "As Rect'il't>d" Moisture Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry Weight Corrected" Actlnmm-227 u 0.109 +1-0 348 Antimony-125 LI 0.0694 +f-(l 137 Bismuth-2!2 UI lJ.Otl +{.[) 845 Bismuth-214 0.&86 '*/-0 196 Ccsmm-137 l.24 +1-0.141 Coba\t-6fl \j -u.00666 .. /.lJ.(J41l9 Europiurn-154 l.' 0.162 +1-U.229 1 23 +f-(} 144 Lead-214 1 26 +/-0.212 Potassmm-40 22.(l +/-2.03 Promctmmm-231 lH 000 t*/-0.714 Radium-226 0 886 +/-0 1% Radiwn-228 1 06 +1-0 358 Thallium-208 {) 334 +/-0.0978 Tm-126 lJI 000 +i-0 143 Rad Gas Flow Proportional Cnunting GFPC. Gross Aill. solid "Dry Weigh! Co1*rectt'd" Alpha 9 44 +/-3.16 Beta 29.0 +/-2.82 *1:h_e __ .er.i!Jl ':cr_c pe_r.fo.rm_cd.

• • -*** ..... . l\fothod Descri11tion l)ry Soil Prep we.i:e

.... Method Description 2 3 ASTM D 2216 (Modrfied) DOE HASL 300. 4.5 2.3iGa-Ol-R EPA 9UU.0/SW846 9310.ISM 7110l3 Mod1tied Surrogatc!l'rncer Recovery Test U.t\52 0.257 1.69 ll.192 0,0%1 0.0949 0 370 0 140 0 402 tl.730 l.2ll (}.1<)2 0 320 () 0761 0.164 3.84 2.22 Le !) 307 .j./-().352 () l20 +l-!l. l40 (J 783 +/-1.10 0 0884 +/-{)2!0 0 0..\.37 +f-0 174 () 04(16 +/-0 050 j) 16(> +/-0 241 () 0658 +/-0. l.76 0 194 +/-0.237 0296 +i-2 82 0.563 +/--0742 0.0834 .. /.(l 210 () 141 +/-0 391 0 U341 +/-0 102 r.1.0777 +/-0 1*14 I 67 +/-3 65 I 03 +l-5 06 Analyst Date Project: Client ID: Report Date: December !7. 20!5 MJWCOOl 15 MJWCOOl LYT1 1 lfW/15 0955 1521927 pCtlg RXF2 12103115 0721 1522386 2 pCi.lg pC1/g pCifg () 100 pC1fg pCi!g pC1.lg pC1/g pC1/g pCi/g pCi/g pC1/g pCi/g pC1/g pl'i/g 4.00 pCi!g JXB7 \2102/\5 1405 1525768 3 It) tl rCii!,! Prep B11.tch LYT1 11/\()115 Time ()955 1521927 Balch ID Rccove1*y% AcccptableUmits GEL LABORATOR1ES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Corporation 15 Hazch,ood Drive Suitc112 Buffalo. New York 14228 , Contact: Ms. Laurie Lo5ey Prnject: Soi1 Client Sample ID: C'.1.C l Sample ID: 385101001 Parnmctcr ... *-*** .... -*-. 1Ju11li_fi1_?_r. Result Surrogatcfl'raccr Recovery Notes: Certificate of Analysis Report Dntc: December 17. 2015 Project: MJWCOOJ t5 Client ID: MJWCOOJ ...... *'"1.DC ....... L_c __ . .. . .. 'f.P.V.. . . __ g_L **-* .l.ini_ts .. _ Ii.m_c .. !J::itc_h J\:1t_cl Batch ID Recovery% Acceptable Limits TPU and Counting Uncertainty are calculated at the 95% confidence level (l.96-sigma). l I GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -vJWW.gel.com Company: Address: Contact: MJW Corporation 15 I !azelwo(1d Dri\'e Suite 112 Buffalo. New York. 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: C. l.C5 Sample ID: 387899006 Matrix: Water Collect Date: 27-0CT-I 5 Receive Date: 2 1-DEC-15 Certificate of Analysis Prnject: Client !D: Report Date: MJWCOOl 15 MJWCOOl January 19, 2016 ........ ..........

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  • -............ . P:1_rl!.fllc1eJ:' . .. . . .. . . ......

...... ..... ..... .... [_,C. ... _ Rad Gamma Spec Analysis Gammaspec. Gamma. Liquid (Standard Lis() "As R!!ceived" Actinium-227 u -9.34 "t"/-24 0 4l! 5 19 () +/-24 5 pCi/L MJll\ Ol/11116 0658 1532831 Antimony-125 l' 3 87 .,./-8 6\ 16 4 76(J +l-8.79 pCi/I. Bisnunh-212 u 8 19 +/-47.7 91.4 41 7 +l-+7.9 pCiiL Bismllth-2 l-l ur 000 +/-12.6 l l 8 5 43 +1-!2 6 pCi/L u -0 221 +-1-3 n 5 77 2 62 +-1-3.23 10.0 p(i!L Cobalt-60 u -1 16 +1-3 52 . 6 53 2.84 +l-3 56 pCiit. Europillm-154 L: -0913 18 4 8 07 +.'-9.58 pC1iL Lcad-212 U! 0 DO +/-9.96 !24 5 92 +I-! I 6 pCllL. Lcad-214 I..' 0.0996 +/-8 56 J3(, 6.41 +/-l!.56 pCllL Pot11ss1um-40 Ul (l 00 +l-57 fi 67 2 29.4 t/-.'i8 (l pC1/L Prolactimurn-231 Ul 00() +/-42 6 81 I 38 I +/-49 7 pCi/L Radmm-228 ll I O.{)() +/-I [J.2 25 3 11 5 +f-11 5 pC1!L Thallmm-208 t.: -I 15 +1-4.93 702 3.25 +r-4% pCtiL Trn-\26 0 2!!5 +1-762 13 4 6 38 +r-7.62 pCiiL Rad Gas Flow Proportional Counting GfPC. Gross A*B. /iqr1id ".-ls Receiwd" Alpha u () 838 +1-l 6(> 315 I ll +1-I .6£i s 00 pC1/L JXIl7 Oll05!16 1148 1533798 2 Beta l' " 00479 +{.) IJ\ 361 I 56 fl-I 91 s.no pC11l. n:cre -......... -.. *-** .......... _ .......................... .. l\'lethod Description EPA 901 l EPA 900.fJiSW846 9310 Surrog:itcrrr:1ecr Recovery Test Batch ID Recovery% Acccptab!e Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( l. 96-sigma). GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171

• www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: Address: Contact: Project: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Soil Radioisotopes . . . .... .. ... . .. . . .. ... .... '""'*".

.... . ........... , ................ . Client Sample JD: Sample ID: Matrix: Collect Date: Receive Date: Collector: Moisture: C.2.CI 385101002 Soil 27-0CT-15 10:34 05-NOV-15. Client I l.1% Parameter Qualifier ... Uncertainty Gravimetric Solids ASTM D 2216 % Moisture "As Received" 11.1 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry *weight Corrected" u -0 0628 +/-0 300 A1111mony-125 ll 0.0662 +}.() 122 Cesmm-137 8 68 +!-() 236 Cohalt-60 u 0 IJl43 +/-0 0287 I:uropium-15*1 u -0.0807. +/-0.0904 Protactimum-231 u 0 631 +1-0.733 Radium-226 0.641 +/-0 134 Rudium-228 UI 0.00 +/-0 240 Tm-126 ll 0.156 +/-0.125 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corret..-ted Alpha 8 06 +/-3119 Beta 20.f +l-3 40 . . . .. . . . . . .. .. Method Description tii; .. siiii""Prep _ ... -* ........ . ..... "'b'r): Soil'Prep i.. . ........... .. Project: MJWC'OO l l 5 Client lD: l'vlJWCOO I MDC RL 0554 0 232 0.0642 0 0581 0.154 0.975 0139 0372 DHii 3 37 3 92 ll JOO 4 OU JO 0 perc-cnl pC1/g pCilg pC1lg pCi/g pC1!g pC1!g pCl/g pCl!g pCifg pC1/g pCilg LYTI 11110.115 0955 1521927 lDff2 12/03/IS 0721 1522386 JXB7 12102/15 1406 1525768 Analyst Date Time Prep Batch *t.vt*i"** ....... **1 f11i.HiS ........... QiJs5 ....... i'521927 .......................... .. 2 3 :rh.e fl:'letho<l.s w.ere. ... .. .... . ....... ........ .. .._.. .... .. .. ... . . . .. . . . . .. .. ...... . ... .. ... .. . ............................

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..................... __ .. --* ............... . . ..... -.-........ _ .... _._ .... _ ..... .A!1.!!-!Y.st..C:()mrr1ents ............... . I ASTMD22\6(:vlo,litied) 2 DOEHASL30U,4.5.'.! JIGa-01-R 3 EPA 900 OiSW846 931lJ!SM 71 IOB Modilied Notes: Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma). GEL LA BORA TORlES LLC 2040 Savage Road Charleston SG 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Corporation 15 Hazelwood Dri\'e Suite 112 Buffnlo. New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: C.2.Cl Sample ID: 385101002 Matrix: Soil Collect Date: 27-0CT-l 5 Receive. Date: 05-NOV-15 Collector: Client Moisture: 11.1%

.. Gra,*imctric Solids AS?;\1D2216

% Moisture "As Recefred" Moisture Rael Gamma Spec I! I Gammaspec, Gamma, Solid "f)ry Weight Com!cled" Acuruum-227 lJ -0 (J62R +/-0.300 A.ntimony-125 lJ 0 0662 +1-0 122 lJ 0.360 +/-() 441 Cesium-137 Cobalt-60 Europrnm-154 Lead-112 Lend-214 Potnss1um-4(i Pmmctmmm-23 l Radmm-226 Radmm-228 Thallium-208 Tm-126 u u lll UI t:I Rad Gas Fhm Proportional Counting 0.641 8 68 I) 0143 :o ()307 ll.985 0 903 14 000 OMI 0.00 0243 U.00 Gl-1'C. Gross ArB. solid "Dry Weight C'oriw:wd" Alpha S.06 bm W4 +-/-0 134 +/-0.236 +/-() 0287. +/-00904 +/-0 !29 ... /.(l.172 +/-1.23 +/-0 733 +/-0 134 +/-0.240 +f-0.()66 tl-0.125 +/-3.09 t/-3.40 Tl.1.c fC)llo_wing._Prep ..... ___ .. . . .. _ Method Description Dry S01l Prep Dry Sm! Prep GL-RAD-A-021 wcre.p.e_r..for.Jl1<<!.d ...... . Meth1>d Description ASTM D 2216 (Modified) '.! DOE llASL 300, 4.5.2 3/Ga-01-R EPA 900 OiSW846 93 lO.'SM 71 lOB Modified SurrogatefTraccr Recovery Test MDC Le .. .. . ***-*** .. *-* . . . . ... 0.554 t) 23::! () 875 0.139 1).0642 (J.0SS1 n.154 0 115 0.165 0412 IJ.975 [J 139 0 372 00676 (I lf>I 3.37 3 92 0267 0 112 0411 0065Y () 0302 0 0262 0.(1693 0 0553 0 0795 () 17& () 468 00659 0.178 (l 032 00778 1 35 l 84 A!lalyst LYTI Report Date: December 17, 2015 Project: Client ID: MJWCOOl 15 MJWCOOI ....... TP.l' . percent LYTI l 1/Hlil5 il955 1521927 +/-0.301 pCi/g R..'ff2 12i()3115 0721 1522386 2 +/-0 126 pC1/g +/-ll 471 pC1lg +1-0 144 pCilg +/-0 740 0100 pCiig +1-0 0294 pCi/g +l-0 0977 pC1/g rf-(} 152 pCi/g r/-0.187 pCtig +1-1 76 pC'ilg .+f*D 747 pC1!g +l-0 144. *pCtig +/.() 430 pC1/g +/.(l.(J69! pC'1ig +!-0 126 pC1/g +/-3.46 400 p('iig JXB7 11102/1 S 1406 1525768 3 +1-44.J \(J_(I Date Time Prep Batch 11/10/15 0955 1521927 Batch II> Recovery% Acceptable Limits GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Corporation l 5 Hazelwood Drive Suite 112 Buffalo, New York 1<1228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: C.2.Cl Sample ID: 385101002 Certificate of Analysis Report Dnte: December 17. 2015 Project: MJWCOO 115 Client ID: Jv1JWCOOI Pararneter .... c:nc!!.!:tah1_tJ

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.. Le . ... TJ>l'. ... *--.. ... .. . ... _!)_ate_ rime. Mtd. !latch ID Recovery% Acceptable Limits Surrogatcffracer Rcc<rrcry Test Notes: TPlJ and Counting Uncertainty me calculated al the 95'!*o confidence level ( l .96-sigma). GEL LAB ORA TORIES LLC 2040 Savage Road Charleston SC 29407-(843} 556-8171-ww'.v.gel.cam Company; Address: Contact: Project: Client Sample ID: MJW Corporation 15 Hazelwood Drive Suite 112 Certificate of Analysis Buffalo, New York 14228 Ms. Laurie Losey Soil Radioisotopes ........... _ ....... . C.2.C4 Repo11 Date: December 4, 2015 Project: Sample [D: 385101003 Soi! Client ID: MJWC001 l5 MJWCOO! Matrix: Collect Date: Receive Date: Collector: Moisture: Parameter Gravimetric Solids 27-0CTvlS 10:55 05-NOV-IS Clieni 14.3% ASTM D 2216 Moisture" As Received" Mo1smrc 14.3 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 l! -0333 +/-0.615 Antimony-125 l! -0 0534 +/-0 29ll Ccsium-137 302 +/-0 572 Cobalt-60 l.! .()(1()261 +/ .. tJ.038 Europmm-J 54 lJ 0.0645 +i-0.JJ3 Protactmmm-2J 1 ll t.05 -ti-\ 19 R.admm-226 0 720 +/-0.224 Radtum-228 0.797 +/-0.356 Tin-126 UI 0.00 +/-0.179 Rad Gas Flow Proportional Counting GFPC, G!'oss A/B, solid "Dry Weight Corrected" Alpha 13 I "'/-3,94 lleta 46.8 +/-4.09 MDC RL Units DF Analyst Date Time Batch Method ....... ***-......................

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• -*-..... . percent LY'fl ll/I0/15 0955 1521927 0 935 pCilg RX F2 \ 2i03115 0722 1522386 2 0.533 pC1/g () ()\)99 !1100 pCilg 00751 pCifg 0.275 pC11g 2.02 pC1ig 0 23.2 pCilg 0.2\:19 pCilg () 154 pC'1ig 3 96 400 pC1!g JXB7 12/02tl5 1409 1525768 3 2.63 10.0 pCi/g

.... _ .......... "..... . .... __ -* ....... ... . . .... _ -* ............................ . Method Description Analyst Date Time oi): 'so1i'Prcj:i"" ., ............ 'oiY Soffi"rep'C:i't:R.xo:;,_(iiJ -...... -* ........... -. "1..ST'i" ......... 111i&ri5""" . --"<i'>55' Prep Batch 1521927 .. . Method .. . -******* *--*---.. ***-**. .IJ.e.sc.r.ip*m ... _ . _ _ .............. . .. Ana!Y.1>.t ........ l 2 3 Notes: . ASTM D 2216 (Moditkd) DOE HA.SL JOO. 4.5 2.3fGa*Ol-R 'EPA 900.0iSW846 9310iSM 71 IOB Mod1ticd Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

• f GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843} 556-8171 -WW\v.geLcom Certificate of Analysis Company: Address; MJW Corporation 15 1-lw.clwood Drh*e Suite 112 Buffalo, New York 14228 Contact: M.s.

Losey Project: Soil Radioisotopes Client Sample ID: C.2.C4 Sample ID: 38510l003 Matrix; Soil Collect Date: 27-dCT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 14.3% Parameter Gravimetric Solids ASTM D 22 !6 % Moisture .,Is Received" Moisture Rael Gamma Spec Analy.s[s 14 3 Gammaspec. Gamma. Solid "lJry IVeight Correcred" Actimum-227 ll -0 333 +/-0.615 Amencium-241 0 141 +/-0 !09 Antnnony-125 l! -(l.0534 +/-0.298 Bismutb-212 U! HOO ***!-\ 06 Btsmuth-214 0 720 +/-(1224 Ccsium-137 30 2 +J-0.572 u -0.00261 +i-0 038 Europium-154 u 0.0645 +/-(} 133

l. lO +/-() 163 Load-214 0.924 +t.o 346 f>otassn_\m-40 16 6 H-1 63 Protacmmtm-231 lJl 0.00 +f-1 19 Rudium-226 0 720 +/-0224 Radium-22&

0 797 +/-0 356 Thallmm-208 0.319 H-0 Tm-12(* Ul () 00 +/-0 179 Rad Gas Flow Proportional Counting GFPC. Grvss A-B. solid "D1:i* Weight Correcred" Alpha 13.l +f-3 94 Beta 46 8 -t-/-409 Pt:r.fo_r_I11_ctl _ ____ ___ ................ . Method Oescriplion _DrySotl Prep Dry Soil Prep GL-RAD-A-021 _w_e.r.e [lC!:f?r.*11.t:d_ .. Method Description I 2 3 ASTM D 2216 (.\fodificd) DOE HASL 300, 4 5 2.3/Ga-01-R EPA 900.0!S\\'&46 9310/SM 71 IOB Modified Surrogatelfraccr Reco,*cry Test lJ 935 (I 139 0.533 1 55 0232 () 0999 00751 () 275 0 213 0 353 0.871 2 02 0232 0299 0125 0 154 396 2 63 Le 0.453 0 0 259 0726 () 110 0 0463 0 ll318 0 122 0.!04 0 172 0 377 0 983 0.1 l(I () 134 0 0595 () 0747 I 04 1.19 Analyst LYTI ... Tl.'.L. +/-0.110 -t-i-0.299 +/-l.37 +/-0 232 -<-/-2.60 +/-0.038 +/-0 136 +1-0212 +/-() 355 +/-2 29 H-131 +/-0 232 +i-0 371 f/-0.118 +/-0.182 +f-4 70 +f-7 87 Dale ---Project: Client ID: Report Date: December l 7. 2015 MJWC'OOl 15 MJWCOOI. RL l'nil.<i _ DF ... . _ !i_ll]': Batch Mtd

• pcn;ent LYTI 11/10.'15 0955 1521927 pC1!g RXF2 12/03!15 0722 1522386 2 pC'ilg pCi!g pCilg pC1lg 0 100 pCilg pC11g pCilg pC1/g pCilg pCi.lg pCi/g pCi/g. pCilg pC'1/g pCilg 4 00 pC1!g JXl37 12102/15 1409 1525768 3 I0.0 pCi/g **-*******

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*-* ..... . ***-.. .. -******** . .. _ .. Tinie Prep Batch ******-* .........

11/to!\5 0955 1521927 . .... .........

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.. ..... ****** . ............ ... ****-*-*-** .. *-* .. ****** *-*** . Batch ID Recovery% Acceptable GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 1422& Ms. Laurie Losey Project: Soil Radioisotopes Client Sample TD: C.2.C4 Sample ID: 385101003 Certificate of Analysis . --.. ******* ....................

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............. -*-**--.... ' .... ****** . . . . ***** .... . .. Report Date: Dcex!mbcr

17. 2015 Project: MJWCOOI 15 Client ID: MJWCOOJ .

___ ...... -* .... ___ -*. ... .:\1[).C:: Le ........ ........ RL l_;11Hs .. DI'. :\n.a!ys.t .... .IJ:ttch [\-1_td: Surr:ogateffracer Recovery Test Hatch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJ\V Corporation 15 Hazelwood Drive Suite 1 !2 Certificate of Analysis Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes .. -*' ...... .... ..... . ................

• -*** ......... . Client Sample ID: C.2.C5 Sample ID: 385101004 Matrix: Soil Collect Date: 27-0CT-15

! l :00 Receive Date: 05-NOV-15 Collector: Client Moisture: 15.6% *A******** Project: Client ID: Report Date: December 4. 2015 MJWCOOl 15 MJWCOOl .. _ __ .... ... _ __ . *--.. __ . *--[)F _ _Date .. _T_ipte Batch Method Gravimetric Solids ASTM D 2216 % Moisture "As Received" 15.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonmrn-238

• U D.00 +/-(} 048<J Plu!omum-.:?.39i240 U 0 0679 +f-0. l Jn ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 U U 0424 +/-0 ll2 llramum-233/234 l 07 +/-0 3 \2
• Uranium-235123(>

U 0 0461 +f-0 0789 llramum-238 () 959 +f-0.295 Alphaspec Np237. Solid "Dry Weight Corrected" Ncplunium-237 ll 0.05"63 +/-0 252 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 I 10 +/-0 546 Thorrnm-229 U -0.0266 +/-0 184 Thonum-230 0.891 +/.() 475 111onum-232 1.02 +/.(I. 50 I Am241, Cm Solid "Dry Weight Corrected" Amcr1c1um-24 l 0 107 +/-0 0881 Clll'ium-242 U 0 OIJ +i*0.0354 Cur1um-243i244 U -0 00374 H-0 0323 Cur1um-245/24fa ll () 0361 +/.() 0619 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 l: -2.42 +/-7 71 Rad Gamma Spec Analysis Gamma 1129. Solid "Dry Weight Corrected" lodine-129 U -0.112 +/-0.284 Gamrnnspec, Gamma, Solid "Dry Weight Corrected Acunium-221 ti 00119 +/-0.463 Anllmony-125 U 0.166 +/-0.218 Ccsrnm-137 Cobalt-60 Europrum-154 Protactmium-231 u u u 23.8 +/-O..J07 0 0023 +l-0 0362 -0 183 +/-0.117 -0 677 +/-1 1Cl I} 0728 0 170 () 207 0 127 0 06')] 0 I JO 0.494 0.432 ll.447 !l."289 o !SI 0.0757 00527 (J074ll (l 0542 13 4 0 479 0 841 0 402 0 090 0 0601 0.175 1.65 l 00 J_(J{) l 00 1 00 t no l.00 I (lll I 00 I 00 1 no l.tJO 1 00 I 00 I 00 I 00 IS 0 I 00 ()_!O[J percent pC1/g pCi!g ixitg

• pcifg pc1/g pci/g pCi!g pCi/g pCl/g pC1/g
• pCiig pCi!g pCi/g pCt!g pl'1.lg pCilg pCllg pCr!g pCrlg pCl/g pCi/g pCi/g pCrlg LYTI I i/I0/15 0955 1521927 HAKB 11/23/15 1501 1522577 2* llAKB I 1i24/15 0851 1521580 3 HAKB \ l/23115 1711 1522576 4 liAKll 1 l/24115 1014 1522579 5 I !AKB JJ/24fl5 1039 I 522571 6 HAKB 11/25/I S 1638 1522.578 7 MJHI 12i02!15 1711.l* \522374 8 RXF2 \2{()3/\5 0733 1522386 9 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -{843) -WNw.gel.com Certificate of Analysis .Report Date: December 4. 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes

..... . ...................... . Client Sample ID: C.2.C'5 Sample ID: 385101004 Rad Gamma Spec Analysis Gainmaspec. Gamma, Solid "Dry Weight Corrected" Radium-226

• 0 822 +1-'1.213 Rudium-228 0 943 +1-0 380 Tin-126 U 0 175 +/.0.216 Rad Gas Flow Proportional Counting GFPC, Gross AiB, solid "DI)* Weight CoJTected" 13.1 +/-3 90 39.9 +/-4 01 GFPC, Sr90, solid "Dcy Weight Corrected" Stron!ium-9ll U 1.25 +/-l. 10 Rad Liquid Scintillation Analysis LSC. Tritium Dist, Solid .Dry Weight Corrected" Tritium U 0 52Cl +l-1.65 Liquid Scint Cl4, *solid "Dry Weight Corrected" Carbon-14 . U -C}.615 +/-U 809 Liquid Scint Tc99. Solid "Dry Weight Corrected" Tcchnctium-99 U I 15 +/-1 37 f? l!oy.:in.g.

...... ., . . . . . . .. Method Description

• oiY sCiii Prer ***** ** brysCii1 i;rcii dL-RA.t>-"A::o2*1-****-*

0. l!l7 (J 254 0212 .l.54 4.00 2.71 IO.O 1.78 20() 3 02 (>I}() l 41 200 2.J[ 5.00 Analyst *i':vt!* *****-****

Project'. Client fD: pCi!g pC1lg pCi/g pC1lg pC1/g p('i/g p('ilg pCi!g pCilg MJWCOOl 15 MJWCOOl JX\37 12102115 KSDI l2i02fl5 TXJI 12102115 nm 12104115 MYMl 11129115 Diite Time Prep Batch *****i**u10hs*****-**-****a9ss .. *** .. is219i7 ***

• J<l 11 1525768 10 1710 1525755 It 1856 1522724 12 0407 1522716 13 1323 1522715 14 *--*********
  • • • -****

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843} 556-8171 -wvvw.gel.com Certificate of Analysis Report Date: December 4, 20 l 5 Company: Address: MJW Corp*oration 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Contact: Ms: Laurie Losey Project: Soil Radioisotopes ............ ,.. . .. . .... -* -**** ...... -........ . Client Sample ID: C.2.C5 Sample ID: 385 l 0 I 004 The .......... . . .. . . . . . . . ..... . . ........ . ASTM D 2216 2 DOE EML HASL-300, Pu-11-RC Modified 3 DOE EML !*IASL-300, ll-02-RC Modified 4 ASTM C 1476-00 Modified 5 6 7 II 9 JI) II 12 13 l*i" DOE EML HASL-30U, Th-01-RC Modified DOE EMJ. HASL-300. Am-05-RC Modifict! DOE EML HASL-300. Pu-! 1-RC Mothficd DOE EML HASL-300J-01 Modified DOE HAST. 300.4.5 23/Ga-01-R EPA 900.0/SW846 93 !0!SM 7l ll!R Modified EPA 905.0 Modified/DOE RP501 Rev ! Modified EP,\ 906.0 Modified EPA EERF C-01 Modi fled DOE EML HASL-300, Tc-02-RC Modified ...... . .. . ...................... . l'lutonium-242 Tracer Vranium-232 'Tract!r Uranium-235/236 Tracer Amcricium-243 Tracer Actinium-227 Tracer Amcricium-243 Tracer Plutomum-242 Tracer Strontium CM1"1cr Techneuum-99m Tracer Notes: ASP l'lutonium lsotop1c, Sohd "Dry Weight Corrected" ASP Uranium Isolop1c, Solid "Dry Weight Corrected" AS!' Uranium Isotopic. Solid "Dry Weight Corrected" Alphaspcc Np237. Sohd "Dry Weight Corrected" Alphaspec Th229 + 228.230,232 Sohd "Dry Weight Corrected" Am24 l. Cm Solid "Dry Wcrght Corrected" L1qu1tl Scmt Pu24 l, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" L1qutd Scint Tc99, Solid Dry Weight Corrected Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma). Project: MJWCOOl 15 Client ID: MJWCOOI . .. -********* .. -********* .... . .......... . . .......... A11.a.lyst (gmnlCfl.ti; ... . . .. .... . .. . ... .. ... . ......... _ Result Nominal . !_tcc()veryo/o_ .... .. 63 2 [15%-125%) 63.4 (!5%-125%) 68 I (15%-125%) 93.3 (15%-125%) S7 7 (15%-125%) 94.4 (15%-125%) 63 2 (15%-125%) 84 6 (2.5%-125%) 95.9 {15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: rv!J\\' Corporntiou 15 Hazelwood Drive Suite 112 Buffalo, Ne\'I' York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: C.2.C5 Sample ID: 38510!004 l\*1atrix: Soil Collect Date: 27-0Cr-ts Receive Date: 05-NOV-15 Collector: Client Moisture: 15.6%, . .. . . ......... . ____ ... l.)cer:t:iiriJy _ . Gravimetric Solids ASTM D 2216% Moisrure "As Received" Moisture 15.6 Rad Alpha Spec Analysis .*ISP Piutoni11m Isotopic. Solid "Dry Weight Corrected" i'luton1um-238 0.00 *>/-U.0489 Plu1\lnium-239i240 0.0671) +!-0 110 A.SP Ur(lnium Isotopic. Solid "Dry Weig/1/ Corrected" llrnnmm-232 u 0.0424 +f-0.112 Uranium-2331234 1 07 +1-0312 Uramum-2351236 0.0461 +/-0.0789 Ummum-238 0.959 +f-0 295 .:ilplraspec

\/J237. Solid "D1

1* l'Verght Con*ectcd" Neptumum-237 ll 0 0563 +1-0.252 Alphas-pee Th229 +* 228.230,232 Solid "D1:1* Weight Corrected" Thormm-228 I 10 +/-0 546 Thori11m-229 u -0.0266 +/-0 184 Thorium-230 0.891 +/-0.475 Tlionum-232 J.{J2 ..-/.(J.501 AmU !, Cm Solid "Dry Weighl CorreCled" Amcricium-241 0 10'7 *l*/-0 0&8\ Curium-242 0.0ll +/-U.0354 Cunum-2431244 lJ -000374 +/-0 0323 C'uriurn-245/246 0 0361 +/*IJ.0619 Liquid Sr:im Pu24/, Solid "DI)' Weight Correcied" Ph1to11ium-241 LI -2 42 +/-771 R11d Gamma Spec Analysis Gamma l/29, Solid "D1:r lfeigh1 Corrf'cted" lodine-\29 LT -0 112 +1-0 284 Gammaspec.

Gamma, Solid "Dry Weight Corrected" Actimum-227 ll () 0119 +/-().463 A11t1mony-125 u 0.166 .;-/.0.218 Bismulh-212 ur 0 00 +/-0)71 Bismuth-214 0 822 +/-0.213 23 8 +/-ll.407 Coba.ll-60 u 0 0023 4/.IJ.0362 Eurnpmm-154 u -0 183 +/-0 117 Lcad-212 1.04 +/-0 161. J.ead-214 0 940 +!-018!i :\1DC Le .. _TPr_ 0 .. 0728 o.on +!-0.0491 0 170 ll.0486 i*/-0 I 10 ll207 0 0784 +/-0. I JJ 0.1:!7 ll 0291 +/-0.382 0.0691 0.00 +/-0 0795 0 \ \0 0(1206 +/-0.355 0 494 U.141 +/.(I 253 0 432 0 123 +1-0 572 0447 0.133 +1-0 184 () ).89 0.0542 +1-0494 0.181 0110 +/-(1.524 0.0757 0.Ul42 +1-0 OR92 (I 0517 !l.00 +1-00355 0.0748 0014 +!-0.0323 0 0542 . 000 +/-0.0621 134 (>53 'i"/-771 0479 0.212 +l-0289 0.841 0.409 +J-0 463 0.402 0 196 +/-0.231 I .1)7 0 506 +/-0.853 0.187 (J.0897 +i-0.224 0 090 0.0428 H-2 JO 0 0601 0.0267 +/-() 0362 0.175 0.0782 +/-0.144 () 187 I) 0912 **l-0 180 0341 0.167 -+l-0295 Project: Client JD: RL Report Date: December 17, 2015 MJWCOOl 15 MJWCODI percent LYTI 11/I0/15 0955 1521927 I 00 pCilg l*lAKB \ t/23/15 I SOI 1522577 2 1.00 pCtltc l 00 pci!g MAKB 11i24/l5 0851 1522580 3 I 00 pc1lg I 00 pci/g l 00 pc1.1 g I 00 pCi/g HAKB 11/23(15 1711 1522576 4 I 00 pC1/g HAKB 11124115 l014 1522579 5 I 00 pCi/g l 00 pC1/g 1.00 pClfg LOO pC1/g HAK°Ei 11/24115 1039 152257! 6 1.00 pCilg 1.00 pC'1/g I UO pC1.lg 15 0 pC1lg HAKB 11125115 1638 1522578 7 I (Jl) pC1/g MJH I 12102/15 1710 1522374 8 pCt/g RXF2 12103/15 0733 1522386 9 p('i/g pC1/g pCi!g 0.100 pC1/g pCtlg pCi/g pCilg pCi!g Company: Address: GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com MJW Corporation 15 Huzelwoocl Drive Suite 112 Certificate of Analxsis Buffalo, New York 14228 Report Date; December 17. 2015 Contact: Ms. Laurie Lose) Project: Soil Radioisotopes Client Sample ID: C.2.C5 Sample ID: 38510 I 004 Parameter Rad Gamma Spec Analysis Gwnmasper:, Gamma. Solid "Dry Weight Co1*rectcd" Potassium-40 14 7 Protactini um-2 31 l.' .() 677 Radi11m-226 0.822 Radium-228 0 '}43 Thallium-208 0 396 Tm-126 UI 0 00 Rad G:is Flow Proportional Counting GFPC'. Dross kB. solid "DIJ' Weighr Corrected" Alpha 13 7 Beta 39 9 GFPC. Sr90, solid "Dry Wt'ighl C'orrer:ted" Strontium-90 1 25 Rad Liquid Scintillation Analysis LSC. Tritium Dist. Solid "Dry Weight Con*ecle!d" Tnt1urn U 0.520 Liqztid Sr:i11t CI./, Solid "Dry Weight Corrected" Carbon-14 U .. () 6 \5 Liquid Scint Tc_99. Solid "D1:1* Weight Correcred" 1.15 +/-1 23 +/-1 10 +/-0 213 +1-0.380 +/ .. {) 109 +/ .. () 216 +1-3.90 +/-4 o:. +f-1.10 +f*I (>5 +/-0 809 +/-1 37 ............................... . Method Description Ory Sm! Prep Diy Sml Prep GL-RAD-A-02 l Th_e

.\.n.a_l>'.l!ca.1

.. .. _. :\'let hod Dese1*iption 2 3 4 5 6 1 8 9 10 II .12 13 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-JOO, U-02-RC Modified ASTM C 1476--00 Modified DOE EML HASL-300. Th*ll 1-RC Modified DOE EML HASL-300. Am-05-RC Mod1lied DOE EML Pu-11-RC' Modified DOE EML l!ASL-300,1-01 Modified DOE HASL 300, 4 5.231Ga-O1-R EPA 900 ll.1 SW846 9310/SM 7\ !OB Modified EPA 905 0 Modified/DOE RP501 Rev I Modified EPA 906 0 Mod1!icd EPA EERF C-01 Modified 0 515 1.65 0 187 0254 0 0971 0 212 3 54 1 71 I 7S 3 02 I 41 2.3 f Project: Client ID: MJWCOOl 15 MJWCOOI 0 225 +f-1 76 pCt!g 0 804 +/-I 15 . 0.0897 +1-0.224 pCilg () 117 +/-0.392 pCilg 0 0466 +/-0.114 pCi/g 0 103 +1-0.216 p(\lg l .\2 +/-469 4.0ll pC1.lg JXB7 1 22 +/-6.Sl I (HI pCi/g 0.784 +/-1.13 2.00 pCi/g KSDI I JI +f-l.65 600 pC1ig TXJI 0.690 +/-0.809 2.00 pCi!g TXJI 111 -t/-1 5.00 pCilg MYM I **-***** *-** .... . ... --*** **-..... Analyst Date Time Prep Batch ... *-****** *-* . ........... ......... -* .................... LYTl ! 1/10!15 0955 1521927 ... **-**** ............ . --****** .... . .. ....... -********--***** ......... 121()2/15 1411 1525768 I 2i02/15 1710 !525755 12102/15 1856 1522724 12/04/15 0407 I 112'1/15 1323 1522715 ... _ ........ . .... . ............................ .. ........ .. .. . .. .. -*--**. ***-***. ..... HI 11 12 13 14 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -w.w.gel.com

• Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Contact: Ms. Laurie Losey Project: SoH Radioisotopes Client Sample ID: C.2.CS Sample ID: 385!0!004 Certificate of Analysis
  • • -* ... *-*** __

...... ...... ..... MDC TPl' ***-**** ......... . Le 14 DOE EML l!ASL-300. Tc-02-RC l\..todificd Surrogaleffraccr Rccm'cry Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Amcricium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier rechnetium-99m Tracer Notes: Test .:S .... ASP Plutonium Isotopic. Solid "Dry Weight Corrected" ASP Uranium Isotopic. Solid Dry Weight Corrected" ASP Uranium Isotopic. Solid "Dry Weight Corrected Alphaspcc Np237. Solid "Dry \\'eight Corrected" Alphaspec Th229 + 228.230,232 Solid "Dry Weight Corrected" Am24 !, C'rn Solid "Dry Weight Corrected" Liquid Sclnt Pu24 l. Solid Dry Weight Corrected" GFPC, Sr90. wlid "Dry Weight Corrected" Liquid Sein! Tc99. Solid "Dry Weight Corrected" TPU and Counting Uncertainty are calculated at the 95% confidence level ( l .96-sigma). Project: Client JD: Report Date: December 17. 2015 MJWCOOl 15 MJWCOOl Batch ID Recovery% 1522577 63.2 1522580 63.4 1522580 68. l 1522576 93.3 l 522579 87.7 1522571 94.4 1522578 63.2 1525755 84.6 !512715 95.9 Acceptable Limits ****-** .. ******** ........ *-****** (l.5%-125%) (15%-125%) (15%-125%) (15%-125%) {15%-125%) (15'%-125%) (25%1* I 25'3i1) (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 7, 2015 Company: MJW Corporation Address : 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact Ms. Laurie Losey Project: Soil Radioisotopes .... .. . .... .... ... . .. ... . ......... . . . . ..... -.. *-. ***-* ... , ... . Client Sample ID: C.3.CI Sample ID: 385068005 Matrix: Collect Date: Receive Date: Collector: Moisture: Parameter ..... *************

• • • • • • • • • • -*****-**

Gravimetric Solids Soil 02-NOV-15 09:30 05-NOV-15 CHent 42% ASTM D 2216 % Moisture "As Received" 11 .. \01s\ure 42.0 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Acti11ium-227 "Dry Weight Corrected" lJ -0 21l3 +/-0 448 i\numony-125 ll 0.0343 +/-0.153 Cesium-137 0.935 +f-0 214 Cobalt-60 u -0 02 \6 +l-0 0696 Europium-154 Proiactinium-231 Radium-226 Radium-228 l! lJ Tm-126 lJ Rad Gas Flow Proportional Counting 0 141 0 162 0744 0602 0.0618 GFPC, Gross AIB. solid "Dry Weight Corrected" Alpha IQ I f o, +/-0 200 +/-0.244 +/-0.3SO t/-0 157 +1-3.43 +l-2 27 Method . Description Dry so11 Prep * ** ** *-***-* * ***bi): 1>;.;;*r

• • • * ** **
• __

__ _ lvl_ethog. ....... ____ .. * ... __ .. I ASTM D 2216 (Modified) 2 DOE HASL 300. 4 5 2 3/Ga-01-R 3 EPA 900 OiSW846 93 WiSM 71108 Modified 0.755 0297 0 133 0.134 0.443 I 59 0.202 0.510 ()204 3 84 2.71 0 100 4 ()0 10.0 Analyst C':Xt;'( .... . .. . ............................... . Project: MJWCOOl 15 Client ID: MJWCOOl Units CXCl 11/10115 !326 1521841 pC'1!g RXF2 I 2i03!15 0708 1522393 pCilg pC1/g pC!/g pCi!g pC!lg pCllg pCilg pC1lg pCi!g JXll7 12102115 1221 1525762 pC1/g Date Time Prep Batch

• iTiloh.S *1326 ***** * ***-is2i"84i.
  • • • • • • * * * . ...................

__ ................... _ .... , ..... . Notes: Counling Uncertainty is calculated at the 95% confidence !eve! { l .96-sigma). 2 J GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-.8171 -www.gel.com Certificate of Analysis Company: Address: MJW C"orpon1tion 15 !-la?.elwood Drive Suite l 12 Buffalo. New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample lD: C.3.C I Sample ID: 385068005 Matrix: Soil Collect Date: 02-NOV-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 42% Project: Client ID: Report Date: December 17, 2015 MJWCOOll5 MJWCOOI .. ..... _ .. __ ...... ........ . ...... MDC Le ........ JT.l!.. ..... RL Vnits . D..l'. .. .. t .. .. !}.1nc Balch Mtd. G ravin1ctric Solids ASTM D 2216 % Moisture Received" Moisture 420 Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry JJ*"eight Corrected" Actmium-227 u -0 203 Amimony* 125 u () 0343 l31smmh-212 Ul 0 00 B1smuth*2t4 0744 Cesium-137 0 935 Ccibalt-60 u -0.0216 F.uropmm-154 u 0 141 Lead-212 0.975 Lcad-214 1.21 Potassium-40 9.35 Protactinium-231 u 0 162 Radium-226 0 744 Ratlium-228 0602 Thallnnn-208 0.25 \ Tin-126 u 0.0618 ltnd Gas Fl01,,* Pn;1porlional Counting GFPC. Gross A/B, solid "Dry Weight Correc/f!d Alpha 10 I Bela 8.69 folllJ.'". iJ.ig_.P.r.ep c.d. ....... __ . '.\lctbod Description Dry SOJI Prep Dry Sm 1 Prep GL-RAD-A-ll2 l +/-0 448 +/-0.153 +/-1.45 +/-0 244 +f-Q 214 +f.(J06% +/-0.20()

• +l-0. i5S +/-0.260 +/-201 +l-0 833 +!-0 244 +l-0 350 +/-0.104 +/-0.157 +/-3.43 +/-2.27

.. ... Method Description ASTM D 2ZJ6 (Modified) 2 DOE l:-IASL 300. 4.5 2 3/Ga-0\-R 3 EPA 900.0iS\\'84(, 9310/SM 711013 Modrlfod Surrogate!l'raccr Test percent CXCI 11110/15 1326 152184 l 0755 0.348 +l-0458 pCilg RXF2 l 2i03/l 5 0708 1522393 2 0.297 () 133 +/-0 154 pCi!g 2.32 1.05 +/. \.54 pC1/g 0 211.'.\ 0 0875 +/-0.251 pCilg 0.133 (} 0585 +!-0 226 \).10() pCl!g ll 134 00543 +/-0.0703 pCilg lJ 443 tJ.187 +-f-0 210 pC'i/g 0.156 0()721 +f-0 178 pC1/g 0 507 IJ.243 +l-0 278 1.14 0 440 +l-2.16 pCt!g 1 59 0.735 +/-0.837 pCt/g ll.202 0 0875 +/-02SI pC1!g 0.510 () 221 +/-0.357 pC1/g .ON3 +J-0 106 pCilg ll.2!l.t 0.0966 +/-0 157 pCi.!g 3 84 161 +i-3.91) 400 pCiig. JXB7 12/02/15 1221 1525762 3 2 71 1.23 +/-2 54 10 () pCi/g Analyst Date Time Prep Batch .... .. ................ .. . ............................ CXCl 11/10115 1326 1521841 .. ... . Batch IO ]:tecovcry% Acceptable Limits GEL LAB ORA TORIES LLC 2040 Savage Road Charleston SC 29407 -{843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Corpormion ! 5 Hazelwood Dri\'e Suite 112 Ilullhlo. New York 14228 Ms. Laurie Losey Project: Soil Ra<lioisotopcs Client Sample lD: C.3.C I Sample ID: 385068005 . . ... . .. .... .. .. .9.lla.lificr SurrogatcJTr:m:r Reco,*ery Tes! Result ..... ...... _ili1RC ................ ...... *-******************.

• • -** -******-******--*

.. ******* ***-* ................... . Notes: Le .......... JrV TPU and Counting Uncertainty arc calculated at the 95% confidence level ( 1.96-sigma). Report Date: December 17, 2015 Project: MJWCOOl 15 Client ID; MJWCOO I ............

• --*-* .... . ....... '* ........ -............ . RL ...

.... !:>.!' .. Date Time Bat<:l.1 .. :\.-1!4*. Batch ID RccoHry% Acccplable Limits GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 7, 20 I 5 Company : MJW Corporation Address : 15 Hazelwood Drive Suitell2 Buffalo, New York 14228 Contact: Ms. Laude Losey Project: Soil Radioisotopes .......... --**-*** ************************** ........ . .. *-********** Parameter Client Sample ID: C.4.CI Sample ID: 385068006 Matrix: Soil Collect Date: 02-NOV-15 11 :40 Receive Date: Collector: Moisture: 05-NOV-15 Client 37.6% Gravimetric Solids ASTM D 2216 % Moisture "As Received" Mmsture 37.6 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Co!1'ected" Actirnurn-227 ll -0 386 +/-0 371 i\nlnnony-125 u 0.0167 +/-0 152 Ccsiwn-137 1.41 +/-0.172 Cobnlt-60 u 0 0584 +f-0 Europium-154 L: 0 031 +/-0 20ll Protactmium-231 Ul ouo +l..0.995 Radmm-226 1.03 +/-0.213 Radium-228

1. \S +l-0 351 Tin-126 LJI 0.00 +l-0 156 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha 113 +f-5.11 Beta 402 +/-4.42 :-.me RL 0.627 0278 0 l30 O.JOO O.UJ 0.393 I 29 0 165 0 351 0 189 3 98 4 00 3 \5 10.0 Project: Client ID: MJWCOOl 15 MJWCOOl Units OF Analyst Date Time Batch Method percent CXCI 11110115 1326 152\84\ pC1/g RXF2 12/03/1 S 0708 1522393 2 pC1/g pCilg pCi!g pCt/g pC1/g pCl/g pCilg p('ifg pC1lg JXB7 12102115 ll23 1525762 3 pC1/g .

.... **-*. . ................ ___ ... ****-* _ .... .. . . . . ... . . . ... . . ........ . Method Description Analyst Date Time Prep Batch .Df:i.soil"fieii***

• • • *** *******-*****

or}**s-oif

• • -* *-* * -********--
    • • • -*cxd*
    • * * -** *nifoiis*****

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.... _ .........

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...... -*****-*****-. .. -*** .. ....... . ..................

• • -* ..... _ **-..............

A.rwh'stG_c:imn::ienis

..... . ............. . l ASTM D 2216 (t\fodtficd) 2 DOE HAS\. 300.4 5 2 31Ga-Ol-R 3 EPA 900 OiSW846 93lO!SM 71108 Modified Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sjgma). GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com . Certificate of Analysis Company: Address: !\.1JW Corporation 15 Hazelwood Drive Suite 112 Buffalo. Ne\v York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: C.4.Cl Sample ID: 385068006 Matrix: Soil Co!lect Date:. 02-NOV-!5 Receive Date: 05-NOV-15 Collector: Client Moisture: 37.6% Gravimetric Solills AST;\,{ D 2216 % Motsture "As Received" Moisture 37.6 Rad Gamma Spec Analysis (}ammaspec. Gamma. Solid "Dry Weight Corr.::cted" Actmium-227 u -0.386 Amirnony-125 u 00167 Bismuth-212 UI 000 Btsmuth-214 I.03 Cesium-137 1 41 Cobalt-60 lll 0.00 Europtum-154 u II 031 Lead-212 l.14 !.ea<l-214 1 2() 17.8 Protactmium-231 UJ 0.00 Radium-226 I.OJ fludium-228 \.18 Thalhum-2ll8 0.26"6 Tm-126 \JI 0.00 Rad Gas l'low Proportional Counting GFPC. Gross A/B, solid "Dry Weight Corrected" Alpha 22.3 Beta 40.2 +l-0 371 ;./-0.152 +1-1 34 +l-0 213 +/-0.172 +/-U.0587 +/-0 200 +/-0 155 +/-0.209 +/-2.13 +/-0.995 +/-0.213 +/-() 351 +1-D.0923 +/-0 156 +l-5 12 +/-4.42 __ Pr.cp ................... . :\lctbod Description --*-********-** -*** ...............

• • -**********-**
• -. Dry Soll Prep Dry So.ii Prcp*Gl,-RAD-A-02\

Method Description 2 3 ASTM D 2216 (Madi!icd) DOE UASL 300. 4.5). 3/Ga-0\-R EPA 900 OISW846 9310/SM 71 IOB Modified Surrogntcffraccr Rceovcry Test 0.627 0.278 l.!12 {) 165 ll.130 () 133 0.393 () 144 044U 1 06 1.29 0.165 0.351 fUOl 0.189 3 98 . 3.15 Report Date: December ! 7. 2015 Project: Client ID: MJWCOOl 15 MJWCOOJ Le TPl' RL . ****-*-***-*-**-........... . l"nits DF r\_nn_lys! __ .!?.'.1.t! Bakh '.\1td. percent CXCl 11fl0/l5 1326 1521841 0291 413 pC1lg R..\'.F2 12103115 0708. 1522393 2 0 128 +1-0.152 pC11g 0.839 +/-1 57 pCi/g 0.0737 +/-0.232 pCi.tg 0.0596 +/-()2l l 0 100 pCt/g 0 0583 +/-0.0MS pC1/g 0.174 ... 1-0 201 pCi/g 0.0674 +/-0. l&l pCi!g 0.213 +/-0.232 pC1/g () 447 ..-/-2 61 pC1/g 0.599 pCilg 0 0737 +l-0 232 pCi/g 0 15-l +/-0 391 pCi/g 011457 +/-0 0952 re ifs 0 0895 +f-0.158 pCilg 1.59 .\-/-6.67 4.00 pC1lg JXB7 12102115 1223 1525762 3 142 +/-7 26 JO 0 pCi.ig Analyst Date Time Prep Balch ........ ...........

• • • • • • ---***--*-

-*** ....... **********-

• -*****-***-**

............. . CXCI 11110.115 1326 1521841 Batch ID Recovery% Acceptable Limits ,, ... ***-*********--***=*** ..... -*-*****************-.

• • • • • -** .................
        • *-**-*********

..... . GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: C.4.CI Sample ID: 385068006 Certificate of Analysis ................... ....... _Result .....

';11).C:

..... !*.c . _ ........... TPl.'. Surrogatcffraccr Recovery Test Notes: TPU and Counting Uncertainty are calculated at the 95% confidence !eve! ( 1.96-sigma). Report Date: December 17. 201 S Project: l\.UWCOOJ 15 Client ID: MJWCOO I . .. RI, ..... .... l?.F. .... P..a.te .. Y.ilJle. .13.at;:h_ .. Batch ID Recovery% Acceptable Limits GEL tABORA TORIES LLC

• 2040 s.avage Road SC 29407 -(843) 556'-8171 , V..WW;getcom .Certificate
• of'Analysis

.: Addres.s: r\1JW><;p.rp9rait01J 1'5 .Hazelwood Drive

• *
• Bu(falq,New

!(ork t 4228 ,Contact: Ms. taui'ieLo$ey §?l! (:lient $'amplelDi . . Matrix:: Co1lect Date: 'Receive JY.!oisfurt:: CA.C.5 os::NOV-:15 tilent J6:q% Gravimetric Stilids llSTM b 22.1.6.% Moisture "As Recelved 11 ,Moisture .36:3 .. Anaiysis * .JSP*PMoniiim*Jsoi6pii:,*so1id u U Q.022 ASP UrafHiim Jso1iip1c. Solid "OiJi Urariiun\..:232

• .ti ci.000963

1-/"0

0714

• * *o:859'.

0.136 +1-0;129 Uianiuin-238' 1 .. 02 .+/;-0.31.6 . AlphasPf!cNp23.7. SqJid ;'.D1y Corrected"

• * {1 *
• M208. .+/.o.m th229+

SolirJ Dry WefghiCorredecf'

• 0:89J * +/-O.Sl2 i'horium-229 .U

+/"O. W Thoiiuiri-230 0:97.1 +/-0517 11ioritii'li*232

o:sn . An1241,.cm*solid "i)rji Weight

.. . o.09§2 u Curium-2431244 (J l $7

• Curiuni'24S/246 \).0756 +/-0.48.3

+l-C(Q7Bj +i,6.o3il . liquid Sci11t*P1124 LSolid Dry WelghtCorrecled!' Piu!oii1,,ffii,24i. u -3J6. Rad Gamma Spec Analysis

• Gainliia JJ29 .. siJlld Dry Weight U .Q. 136 +/-0.373 Gammaspec.

Gamma.Solid "Dry Weig/ii firriedea" Aciinium-227 u

• 0.0917 -r/-0:392 A1.itimori1-.12s u ;o.9iO:t 145 Btsn1U!h,2);2 Ul Mo BiSJ111!th:2i4.

+(-1:j;209 Cesium-137 J-.49 +/"0.1.61 p;ibalt*60 u lw9257 u .0.122 +1:.0.111 Lead'2i2' U.8 Lead-214 1.26 +1-0.216 Qt. ,0,134_ '0.1 .. ,. '. .. *, . . 0.16,5 Q,(

o:O* 0.\62 *o.o 0.136 O.(lJ 0:136 .Q.Q3l Ji.454 ().116, tf-Q,2;1,8' 0.447 0.126 t1-o.m.

0:0572 tMP82 0.0988 +J.:o.539 oj04' o.os69 --+1:0,so2 .o:o&o7 0,02Q5 +1,0i/196 o:os7s 0:0223 +t-0.03.12 0.0915 "'!-0:0297 jid4$4 _Q,QO !L8 5'75 +F6.7_6 .<f717 9:324 .0;107 pj37 '-0':261. o.iio +1-0;145 1.90 0:88$ +!--O.M8 0.225 0.104 't/-0.226 o.6461 ._ .. -**. 0. 10,3

• • • -o.i 18 0:051 :tM,0597 0.377 0.167 0'139 .0.0649 +/-0.185 0.4jl o.209 +1-iti3s Reppj't. Pa.te:

17; 21)1 5 CJieri.t ID: 'MJWC0'01f5 MJWCOOI . RL OF .Analyst 'Qate Tilrie IJatch Mtd. }111()/IS m§ isi.1841 ;j HAKB ili24ils 08si i.52258'0 j *. vV J:,00 p(?i/g 1-IM$E! 11i231\? rib6 .1522576 4 LOO pt;U,g Loo pCi/g }\AKB tl/24/15 . .JOJ4 _1$22579 5 LOO pciig Loo P.tilg. Loo pCifg llAKB U/24115 1042* 1522571

• _6 LQl) 'Ji(.'iig toO i:tio pCi/& *15:() i)¢Vg 'HAJ(B l If25fi 5
• 0829. i522578 '7 1:00 MJHi 121021is 1342 15223.74 ,8 pCiig 1210'.ln:s ,oios: 1s2zJ93 9 pCi/g p{;i(g 0:100 pCi/g pCi/g pCi/g .p(:iig *pdit.g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December 7. 20 l 5 Company: Address: Contact: MJW Corporation 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey

........ *-** ...... _.. ... . . ..... *-... . Project: ....... **********

• • • -***********

.... Client Sample ID: C.4.C.5 Samp!e lD: 385068007 Rad Gamma Spec Analysis Gammaspec. Gamma, Solid "Dry Weight Corrected" Radrnm-226

0. 946 +f-!J 209 0 225 Radium-228 0.954 +1-0.381 0 469* Tm-126 lJ 0.0919 +/-0.145 0203 Rad Gas Flow Proportional Counting . GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha l & 4 +l-5 26 3.81 4.on Beta 27 I ol-/-4A5 3 84 10 () GFPC, Sr90, solid "Dry Weight Corrected" Strontrnm-90 U -0 371 +/-IJ 653 1 39 2.00 Rad Liquid Scintillation Analysis LSC Tritium Dist, Solid "Dry Weight Corrected" Tritium L' 1.20 +1-:us '3.98 600 Liquid Sc int Cl4. Solid "Dry Weight Corrected" Carbon-14 lJ 0 243 +/.() 739 125 2.Ull Liquid Scint Tc99, Solid '1 D1y Weight Corrected" lJ 1.15 .. /-2 20 3 75 5 00

.. ............ .' .... __ ... Project: Client ID: pC1/g. pC1/g pCi/g pCi/g pCi!g pC1fg pC1/g pCilg pC1/g MJWCOOl 15 MJWCOOl JXB7 \2i021\5 KSPI l2i02/15 TXJl 121021\5 TXJl I 2i03/l 5 MYMl 11129/15 1121 1641 1236 2242 0951 Method Descdptiqn Analyst Date Time Prep Batch bi}-Senf Prep"-"""' .... " .. ......................... ""'C:ii:C.;1"""*""* .. '"T1ii<iii5"' ...... 1326 ... 'i5:i184T -* --*. 1525762 . lO )525755 II 1522724 12 1522716 13 1522715 14 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843} 556-8171 -Www.gel.com Certificate of Analysis Company: MJW Corporation Address; 15 Hazehwod Drive Suite 112 Buffalo, New York 1422& Contact: Ms. Laurie Losey _ ............

• • --******

... _ .. Client Sample ID: C.4.C.5 Sample lD: 385068007 Matrix: Soil Collect Date: 02-NOV-1511:45 Receive Date: 05-NOV-I 5 Collector: Client Moisture: 36.3% Parameter

• • • • • • • • • • • -*-.

Gravimetric Solids ASTh1 D 2216 % Moisture "As Received" Moisture 36 3 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected;; Plutoniu!l1-23S lJ 0 000816 +1-0 0605 Plu1on1um-2391240 u 0.022 +/-0.0849 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uramum-232 U 0 000963 +1-0 0714 Uramuin-233/234 0 859 +/-0.293 llrunium-235/236 U 0 136 +/-0 !29 Urnmum-238 l 02 -+/-0J16 Alphaspec Np23 7, Solid "Dry Weight Co1Tected" J\/<;plumum-237 U D.0208 +/-0218 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Conected" Timrium-228 . (l 893 -+!-0.512 Thorium-229 ll 0.0484 +l-0 I S2 Thorium-230 0 971 Thormm-232 0 872 Am241, Cm Solid "Dry Weight Corrected" +l-<i.517 +/-0483 Americium-241 0.0962 +1-0.0787 Curmm-242 U -0 0 l 03 +/-0 031 l Cunum-243/244 U -0.0\57 +1-0.0297 Curium-245/246 X 0 0756 +/-0 0729 Liquid Scint Pu24l, Solid "Dry Weight Corrected Plutonium-241 U -3 16 +/-6. 76 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" !odine-129 U () 136 +/-0 J73 Gammaspec, Gamma. Solid "Dry \\'eight Corrected" Actimum-227 u 0.0917 +1-0 3n Antimony-125 ll 0 lll07 +1-0 145 Ccsium-137 I 49 +/*O 16-1 Cobah-60 t: 0 00257 +/-0 05% Eurnpmm-154 lJ () 122 +/-0 177 Protacumum-231 Ul 0.00 +/-1 06 U.134 0 165 () 159 {) 162 0 136 0.136 (J.454 {).4*17 0.305 0 383 ()J()4 0.0807 0 087.'i 0.0915 0.0454 1 l 8 0717 ()707 I) 26! 0.103 0 llR 0 377 1.25 RL 1.00 l 00 I 00 ! 00 1 ()() 1.00 I 00 1 Oll 1.00 1 Oil "l 1)0 LOO I UO LOO I UO 15.0 I 00 0 IOtl Project: Client ID: percent pC1/g pC1/g pcilg pc1/g pci/g pci!g pCiig pC1/g pC1/g pC'i/g pCi!g pC1!g pC1!g pC\/g pCilg pC1/g pC'i/g pCiig pCi/g pC1/g pCLlg pCl/g pC1.lg Report Dale: December 7, 2015 MJWCOOl 15 MJWCOOI CXCI 11/10/15 1326 1521841 HAKB 11/23115 1501 1522577 HAKB 11124115 0851 1522580 l-IAKB I 1/23/!5 1706 1522576 liAKB 11/24115 1014 1522579 HAKB 11124115 1042 152257! HAKB 11125115 0829 1522578 MJHI 12/02/15 !342 1522374 RXF2 1:!/03/I S 0708 1522393 2 3 4 .s 6 7 8 9 Company: Address: GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.oom MJW Corporation 15 Hrrz:elwood Drive Suite 112 Certificate of Analysis Buffalo, New York 14228 Report Oatc: Dcecmhcr 17. 2015 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: C.4.C.5 . Sample ID:

• 385068007 Parameter

...........

• -***

X.l!ccr.tainty __ Rad Gamma Spec Analysis Ga111111aspec. Gamma, Solid "D1:)' Weight.Corrected Potassmm-40 l 9. 7 Ul 0 00 Radium-226 0 946 Rudium-228 0.954 "11iulhum*208 0.405 tm-126 U 00919 Rad Gas Flow Proportional Counting GFPC. Gross A 'B. solid "Dry !Feight Corrected" Alplta 16.4 27 I GFPC. Sr90, solid "Dry Weight Corrected" Strontmm-90 U -!U71 Rad Liquid Scintillation Annlysis LSC. Tritium Dist, Solid "Dry Weigh! Ca!"l"ected" Tmnrm CJ \ .20 Liquid Sein/ C 14. Solid "Dry Weight CorNcted" Carbon-14 tJ O 243 Uquid Sci11t 1"c99, Solid "Dry Wefghl Corrected" Technetium-99 U I 15 +/-209 +l-1.06 +/-0 209 +1-0.38! +/-00953 +1-0 !45 +i-5.26 +1-4 45 +/-0.653 +1-2.25 ... ;.o 739 +1-2 20 0 888 125 0.225 ti.469 0.0778 0.203 3.81 3 84 1 39 3.98 I 25 J.75 __ r_e_p_ .. ........... . ._ ................. !\.Iethod Descriplion .................... Dry Sorl Prep Dry Sml-r'rcp Gl.-RAD-A-021 ... -** *-******-*- _ Method 2 3 4 5 6 7 8 9 10 11 12 13 ASTM 02216 (Modified) DOE EML HASL-300_ Pu-11-RC Modified DOE EML !IASL-300. l!-02-RC Modrtkd ASTM C 1476-00 Modified DOE EML l!ASL-300. Th-01-RC Modified DOE EML HASL-300, Am-OS-RC Modified DOE EML llASL-300. Pu-l 1-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, *I 5.2.3/Ga-Ol-R EPA 900.0/SW846 93 IOi.SM 71 IOB Modilied EPA 905 0 Modified/DOE RP50! Rev 1 Modifictl EPA 906.0 Modified !!PA EERF C-01 Modified Le 0.363 0 581 () 104 ().2 !3 0.0345 00%1 Ul l.70 () 603 !"73 0.6!7 1.80 ****--**--* Analyst Project: Client ID: lvlJWCOOl l5 MJWCOOJ TPF RL +/-2.6 1) pC1lg +/-\ J l pCi/g +/-0.226 pCJ/g +1-0410 pCilg +l-0 102 pCi!g +!-0 146 pCi/g +1-6 08 4.00 pCi!g JXll7 12/02/!5 1221 +/-5.65 JO 0 pC1ig +/-0 654 2 0(1 pC1/g KSDl !2102/l.5 1641 +/-2.25 6.1)0 pC1ig TXJl 12102115 1236 +/-0 739 2.00 pCilg TXJl 12/03115 2242 +J-2 20 5.00 pCi/g MYM 11129/I 5 0951 I ****-* ...... ........... . ... . ..... ****** ..... . ........... -*--....... Dale Time Prep Batch '* ....... *-*** . ........................................ . ... CXCI l\/10/15 1326 152 IB41 1525762 1525755 1522724 1522716 1522715 10 JI !2 13 14 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843} 556-8i71 -www.gel.com Certificate of Analysis Report Date: December?, 2015 Company : MJW Corporation Address : 15 Hazelwood Drive Suite l 12 Buffalo, New York 14228 Contact: Ms. Laurie Losey . __ .. . . . Client Sample ID: C.4.C.5 Sample ID: 385068007 __ T_h"'. ...... _ . . . *-*-* ...........

• • • • • • • -............... . ASTM D 2216 (Modified) 2 DOE EML HASL-300, Pu-11-RC Modified 3 DOE EML HASL-300, ll-02-RC Modified 4 5. 6 7 ') 10 ll 12 \3 14 ASTM C 1476-00 Modified DOE EML HASL-300, Th-Pl-RC Modified DOE EML HASL-300, Am-05-RC Mod11icd DOE EML llASL-300.

Pu-\ I-RC Modified DOE EML HASL-300,1-0l Mod1Jicd DOE HASL 300,4.5 2 3iGa-Ol-R EPA 900.0/SW846 93 lO!SM 71 Wl3 Modified EPA 905.0 Moddied1DOE RP501 Rev I Modified EPA 906.0 Modified EPA EERF C-01 MoiJ1lfo<l DOE EML HASL-300, Tc-02-RC Modified Pluloniurn-242 Tracer Test .. ***-*----*** ....... *-***. ....... . .... *-** -** ASP Plutonium Solid "Dry Wc1gilt Corrected" \Jranmm-232 Tracer Uranillm-2351236 Tracer Americ1um*243 Tracer Actimum-227 Trncer Amcrictum-243 Tracer Plmonium-242 Tracer Strontium Carner Techrtelrnm-99m Tracer ASP Umnium Isotopic, Sohd "Dry Weight Corrected" ASP Uramum Isotopic: Solid "Dry Weigh! Corrected A.!phaspec Np'.!37. Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230.232 Slllid "Dry Weight Corrected" Am24 I, Cm Solid "DI)' WeighL Corrected'" Liquid Scmt Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "01}' Weight Corrected" Liq111d Scint Tc99. Solid "Dry Corrected Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma). .... -** Project: MJ'NCOO! !5 Client ID: MJWCOO! *"*" *" ********** W*** ** * ***** .. -*****-* .A.l)i!\yS_t ..................... . .... .. _ .... .. LimHs_ 70.3 (15%-125%) 56.ll (15%* \25%) 6.0 (15%-\15%) 93.9 (15%-125%) 95.5 (15%*125%) 82.3 (15%-125%) 70 3 (l5%-l25%) 89.9 (25%-125%) 94.9 ( 15%-125%] GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -{843) 556-8171 -www.gel.com Company:* Address: J\11\V Corporation 15 Hazelwood Drive Suite I 12 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project; Soil Radioisotopes Client Sample rD: C.4.C.5 Sample ID: 385068007 Certificate of Analysis _________ -..... _ ....... .. __ ..... ...... .. ,,_ ....... !PL_ 14 DOE EML HASL-300, Modt!kd Surrogatcffracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Urnnium-2351236 Tracer Amcricium*243 Tracer Actiniurn-227 Tracer Americiurn-243 Tracer Plutonium-242 Tracer Strontium Carrier Tccbnctium-99m Tracer Notes: Test ASP Plutonium Isotopic. Solid "DI) Weight Corrected" ASP Uranium Isotopic. Solid "Dry Weight Corrected ASP Uranium Isotopic. Solid "Dr)' Weight Com:cte<l" Alpha.spec Np237. Solid "Dry Weight Corrected" Alphaspcc Th229 + 228,230.232 Solid "Dry Weight Corrected" Am24l, Cm Solid "Dry Weight Corrected" Liquid Sc.int Pu24 I. Solid "Dry Weig.ht Corrected" GFPC. Sr90, solid "Dry Weight Corrccled" Liquid Scint Tc99. Solid "Dry Weight Corrected" TPU and Counting Uncertainty are calculated at the 95Ai confidence level (_1.96-sigma). Project: Client ID: RL Report Date: December 17, 2015 MJWCOOl 15 MJWCOOI Batch ID Recovery% Acceptable Limits 1522577 1522580 1522580 1522576 1522579 1522571 1522578 !525755 1522715 ......... 70.3 56.8 60 93.9 95.5 82.3 70.3 89.9 94.9 .................. (15%-125%} (15%-125%} (15%-125%) (15%-12.5%) {15%1-125%) (15'%-125%) (15%-125%) (25%-125%) (!5%-125%)

• • GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date; December 7. '.WIS Company: Address: MJW Corporation 15 Hazelwood Drive Suite I 12 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project Soil Radioisotopes
• -**-****

.. **--* .............. . Client Sample ID: C.4.C.6 Sample ID: 385068008 Matrix: Water Collect Date: 02-NOV-15 13:00 Receive Date: 05-NOV-l 5 Collector: Client ...............

• • -......

..... .. ........ !':IDS" ... _ .... RL Rad Gamma Spec Analysis Gammaspec, Gamma, Liquid (Standard List) "As Received Attimurn-227 U -21 'l +/-33.6 Anumony-125 lJ 3.50 +/-11 S Cesium-137 U -5 ol +l-5 85 Cobalt-60 LI -3.J +/-3.89 Europium-154. U 9 18 +-/-l0.2 l'rotactmmm-231 U 24.2 +/-61 5 Rlidium-228* l! 12 5 +/-20 0 Tin-126 lJ 0.485 '"/-$ 88 Rad Gas Flow Proportional Counting* GFPC, Gross A/B, liquid "As Received" Alpha U -0619 +/-l 89 Reta ll -191 +/-234 ........ -* _t_y1etJ.1()d. . ....... . .. .. .. . . .. . .. . ... .. .. . . . . . ........ __ EPA 'l!ll I 2 EPA 900 O/SWR46 93 IO Notes: 55.5 21 5 7.69 10.0 6 33 21.4 t()7 31.0 15 8 4 24 5.llll ai son Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma). Project MJWCOOl 15 Client ID: MJWCOO I pCiiL pC1.'L pCilL pCtlL pCi.iL pC1il. pC1/L pCifL pCiiL pC1/L .MJJll 1 lil6'15 0714 1521915 JXB7. 12!02!!5 1255 1525771 .......... An.!!!Y.sr .. .............. .. 2 ,. ,, GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407-(843) 550-8171 -www.gel.com Company: Address: MJW Corporation 15 1-lazelwood Dri\'C Suite l I2 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Rudioisolopes Client Sample ID: C.4.C.6 Sample ID: 385068008 Matrix: Water Collect Date: 02-NOV-15 Receive Date: 05-NOV-15 Collector: Client .. ***********-**-. --*********

• -...........

-. *-...... -**. ***-* Certificate of Analysis Project: Client ID: Report Date: *December

17. 2015 MJWCOOl 15 MJWCOO! .

-* ... _ .......... __ . .. ....... .. __ .. . L<:. . ........ ... . ... _ llt.. .... .. l!l'. ... _l)atc Time ... Ratl Gamma Spec Analysis Gammaspec, Gamma, liquid (Standard LisrJ .,Is Received" U -21 9 +/-33.6

• Anumony-125 U J.50 +l-11 8 ll -154 +l-69 6 B1smutl1-214 Ccsmm-137 Cobalt-60 Europium-154 Lcad-212 Lcud-214 Potnssium--10 Protac!inium-231 Radium-228 Thalhum-208 UI u u lJ Ul u u lJ u lJ 0.00 +f-17 7 . -561 +/-5 SS -3 3 +f-3.89 9.l8 +f-\0.2 0.00 +/-10.5 6 56 +/-14.7 -6.75 +/-52.9 24 2 +/-615 125 -223 Tm-126 U 0.485 +/-20.0 +!-560 +/-8.88 Rad Gas Flow Proportional Counting GFPC'. Gross AB, liquid "As Received" Atplm L' -0 619 lkla l.' -\ 91

... Method Description EPA9lll l I 2 EPA 900 WSW846 9310 Surl'Ogateffruccr Recovery Test Notes: +1-1 89 +/-2.34 55 5 21.5 90 5 18.8 7.(>9 6 33 21 4 14.3 181 102 to7 310 8.56 IS li 424 4 82 26 6 10.2 416 s 93 3 58 2.71 9 6! 6 89. 8.65 469 51 3 lH 404 761 1.72 2 16 +/-35 l +/-1 ! 9 +1*99 6 +/-18 3 +(.(, 39 +f-4.17 ;-/-[!.() r/-! l l +/-150 +/-53 (} +/:62.7 +1-20.9 +l-5.69 +/-8 88 +f-l 89 +/-2 34 TPU and Counting Uncertainty are calculated at the 95% confidence level (l.96-sigma). pC1/L pCi!L pCilL pCi/L 10.0 pCilL pCi1L pCt.IL pC1/L pCiiL pCi/L pC1!L pC11L pCVL pC'i/L 500 pC1/L 5 00 pC'i!L MJl!l 11/16115 0714 15219!5 JXB7 12i02.115 1255 1525771 2 Batch II) Recovery% Limits}}